WS-5067_5067_CA_MRP_20240730

July 30, 2024

Mr. Gene Mao, LG
Guilford County Department of Public Health Environmental Health Division 400 West Market Street
Greensboro, North Carolina 27401
RE: Annual Monitoring Report Former Greensboro Terminal #1760
7115 West Market Street, Greensboro, North Carolina NCDEQ site ID #5067
Dear Mr. Mao:
On behalf of RETIA USA, LLC (RETIA), Groundwater & Environmental Services, Inc. (GES) is pleased to submit the enclosed Annual Monitoring Report for the above referenced site. This
report documents activities completed from May 2023 through April 2024.
If you have any questions or comments, please do not hesitate to contact the undersigned at 866-222-7786 extension 4094 or at [e-mail].
GROUNDWATER & ENVIRONMENTAL SERVICES, INC.

Enclosure

cc: Mr. Vincent Swadis, Portfolio Manager, RETIA USA (electronic)
File, GES PSID #1013142

TotalEnergies Petrochemicals and Refining USA, Inc.
Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

May 30, 2024

Annual Monitoring Report
Former Greensboro Terminal #1760 TotalEnergies Petrochemicals & Refining USA, Inc. 7115 West Market Street Greensboro, North Carolina 27409
RETIA USA, LLC 1201 Louisiana Street, Suite 1800 Houston, Texas 77002
Groundwater & Environmental Services, Inc. 571 Southlake Boulevard North Chesterfield, Virginia 23236 TEL: [phone] www.gesonline.com

May 30, 2024

Senior Project Manager
Christopher J. Mulry, P.G. Principal Hydrogeologist
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Table of Contents
Executive Summary and Introduction ......................................................................................... 7
1 Site History and Characterization .......................................................................................11
1.1 Introduction ...................................................................................................................11
1.2 Site Geology, Topography, and Hydrology ....................................................................12
1.3 Sensitive Receptors .......................................................................................................13
1.4 Surrounding Properties and Releases ...........................................................................14
1.4.1 Magellan Terminal Property – EDR Report Review ................................................14
1.4.2 Former Phillips Terminal .........................................................................................14
1.4.3 Other Documented Releases .................................................................................15
1.5 Previous Investigations ..................................................................................................16
1.6 Summary of Remedial Activities ....................................................................................19
1.7 Site Strategy ..................................................................................................................21
1.7.1 Monitoring Well Optimization ..................................................................................21
1.7.2 New Technology Cleanup Plan ...............................................................................22
1.7.3 Enhanced In-Situ Bioremediation (EISB) Evaluation ...............................................22
1.8 Report Objectives ..........................................................................................................23
2 Methodology ......................................................................................................................24
2.1 Groundwater Monitoring and Sampling..........................................................................24
2.2 Surface Water Monitoring ..............................................................................................26
2.3 Recovery Well Abandonment ........................................................................................26
3 Site Investigation Results ...................................................................................................27
3.1 Barrier Wall Gauging .....................................................................................................27
3.1.1 Routine Gauging Events .........................................................................................27
3.1.2 Historical Time Trend Graphs .................................................................................28
3.1.3 FPZ-10 Historical LNAPL Time Trend Graph ..........................................................28
3.1.4 LNAPL Recovery Efforts .........................................................................................29
3.1.5 Hydraulic Head Distribution ....................................................................................29
3.1.6 On-Site Concentrations Over Time .........................................................................30
3.1.7 July 2023 Isoconcentration Contours ......................................................................30
3.1.8 December 2023/February 2024 Groundwater Analytical Results ............................30
3.1.9 Cross Sections .......................................................................................................30
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

3.1.10 Groundwater Sampling Results – On-Site Wells ................................................32
3.1.11 Groundwater Sampling Results – Off-Site Wells ................................................33
3.1.12 Geochemical Trends ..........................................................................................34
4 Mass Flux Analysis ............................................................................................................37
4.1 Mass Flux Background and Concepts ...........................................................................37
4.2 Mass Flux Application ....................................................................................................38
4.2.1 Geology and Contaminant Behavior .......................................................................38
4.2.2 Cluster Well Installation ..........................................................................................38
4.3 Mass Flux Calculations and Groundwater Gradients .....................................................39
4.4 Findings .........................................................................................................................39
4.4.1 TBA ........................................................................................................................40
4.4.2 MTBE .....................................................................................................................41
4.4.3 1,2-DCA .................................................................................................................41
4.5 Groundwater Head Evaluation .......................................................................................42
4.6 Discussion .....................................................................................................................43
5 Discussion .........................................................................................................................44
5.1 Summary .......................................................................................................................44
5.2 Updated Conceptual Site Model ....................................................................................45
5.2.1 Groundwater Concentration Trends and Mass Flux Evaluation ..............................46
5.2.2 Groundwater Flow Patterns ....................................................................................47
5.2.3 LNAPL Monitoring and Recoverability ....................................................................47
6 Conclusions & Recommendations ......................................................................................48

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Figures
Figure 1 – Site Location Map Figure 2 – Detailed Topography Map
Figure 3 – Site Map (Aerial) Figure 4 – Site Map Figure 5 – Local Area Map Figure 6 – Barrier Wall Monitoring Wells Groundwater Elevation – July 17, 2023
Figure 7 – Barrier Wall Monitoring Wells Groundwater Elevation – September 18, 2023
Figure 8 – Barrier Wall Monitoring Wells Groundwater Elevation – December 6, 2023
Figure 9 – Barrier Wall Monitoring Wells Groundwater Elevation – March 1, 2024
Figure 10 – Groundwater Elevation Map Shallow Wells – July 17, 2023
Figure 11 – Groundwater Elevation Map Intermediate Wells – July 17, 2023
Figure 12 – Groundwater Elevation Map Deep Wells – July 17, 2023
Figure 13 – Groundwater Elevation Map Bedrock Wells – July 17, 2023
Figure 14 – Groundwater Elevation Map Shallow Wells – December 6, 2023
Figure 15 – Observed Total BTEX Groundwater Concentrations Over Time
Figure 16 – Groundwater Benzene Concentration Map Shallow Wells – July 2023
Figure 17 – Groundwater Benzene Concentration Map Intermediate Wells – July 2023
Figure 18 – Groundwater Benzene Concentration Map Deep Wells – July 2023
Figure 19 – Groundwater Benzene Concentration Map Bedrock Wells – July 2023
Figure 20 – Groundwater TBA Concentration Map Shallow Wells – July 2023
Figure 21 – Groundwater TBA Concentration Map Intermediate Wells – July 2023
Figure 22 – Groundwater TBA Concentration Map Deep Wells – July 2023
Figure 23 – Groundwater TBA Concentration Map Bedrock Wells – July 2023
Figure 24 – Groundwater Analytical Results – December 2023
Figure 25 – Cross Section Location Map
Figure 26 – Cross-Section A-A’ Dissolved Benzene Contours
Figure 27 – Cross-Section B-B’ Dissolved Benzene Contours
Figure 28 – Cross-Section C-C’ Dissolved Benzene Contours
Figure 29 – Cross-Section D-D’ Dissolved Benzene Contours
Figure 30 – Cross-Section E-E’ Dissolved Benzene Contours
Figure 31 – Cross-Section F-F’ Dissolved Benzene Contours
Figure 32 – Cross-Section G-G’ Dissolved Benzene Contours
Figure 33 – Cross-Section A-A’ Dissolved TBA Contours
Figure 34 – Cross-Section B-B’ Dissolved TBA Contours
Figure 35 – Cross-Section C-C’ Dissolved TBA Contours
Figure 36 – Cross-Section D-D’ Dissolved TBA Contours
Figure 37 – Cross-Section E-E’ Dissolved TBA Contours
Figure 38 – Cross-Section F-F’ Dissolved TBA Contours
Figure 39 – Cross-Section G-G’ Dissolved TBA Contours
Figure 40 – Geochemical Indicators Parameter Map – Shallow Wells – July 2023
Figure 41 – Geochemical Indicators Parameter Map – Intermediate Wells – July 2023
Figure 42 – Geochemical Indicators Parameter Map – Deep Wells – July 2023
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Figure 43 – Geochemical Indicators Parameter Map – Bedrock Wells – July 2023
Figure 44 – Groundwater Dissolved Oxygen Concentration Map – Shallow Wells – July 2023
Figure 45 – Groundwater Dissolved Oxygen Concentration Map –Intermediate Wells – July 2023
Figure 46 – Groundwater Dissolved Oxygen Concentration Map – Deep Wells – July 2023
Figure 47 – Groundwater Dissolved Oxygen Concentration Map – Bedrock Wells – July 2023
Figure 48 – Groundwater Oxidation Reduction Potential Concentration Map – Shallow – July 2023
Figure 49 – Groundwater Oxidation Reduction Potential Concentration Map – Intermediate – July 2023
Figure 50 – Groundwater Oxidation Reduction Potential Concentration Map – Deep Wells – July 2023
Figure 51 – Groundwater Oxidation Reduction Potential Concentration Map – Bedrock Wells – July 2023
Figure 52 – Groundwater Temperature Concentration Map – Shallow Wells – July 2023
Figure 53 – Groundwater Temperature Concentration Map – Intermediate Wells – July 2023
Figure 54 – Groundwater Temperature Concentration Map – Deep Wells – July 2023
Figure 55 – Groundwater Temperature Concentration Map – Bedrock Wells – July 2023
Tables
Table 1 – Well Construction Details Table 2 – Historical Groundwater Elevation Data – On-site Wells Table 3 – Historical Groundwater Elevation Data – Off-site Wells Table 4 – Groundwater Geochemical Field Parameters Table 5 – Groundwater Laboratory Analytical Data – On-site Wells Table 6 – Groundwater Laboratory Analytical Data – Off-site Wells
Table 7 – Cluster Well Head Evaluation
Appendices
Appendix A - Mass Flux Figures and Tables
Appendix B – Historical Plume Delineation Map
Appendix C – Groundwater Sampling Forms (July 2023)
Appendix D – Groundwater Sampling Forms (December 2023/February 2024)
Appendix E – Laboratory Analytical Reports – Groundwater (July 2023)
Appendix F – Laboratory Analytical Reports – Groundwater (December 2023/February 2024)
Appendix G – Waste Documentation
Appendix H – Updated Well Permit List and May 7, 2024 Guilford County Email Correspondence
Appendix I – Barrier Wall Well Gauging Data Graphs

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Executive Summary and Introduction
Groundwater and Environmental Services, Inc. (GES) is pleased to submit this Annual Monitoring
Report to the North Carolina Department of Environmental Quality (NCDEQ) and Guilford County
on behalf of RETIA USA, LLC (RETIA), for the site located at 7115 West Market Street,
Greensboro, North Carolina (NCDEQ site ID #5067). RETIA is a subsidiary of TotalEnergies
Petrochemicals & Refining USA, Inc. (TEPRI), formerly Total Petrochemicals & Refining USA,
Inc. (TPRI), with specific responsibility for remediation and risk management activities at former
and current TEPRI sites. The location of the property (herein referred to as the “site”) and
surrounding topography is provided in Figure 1. The purpose of this site assessment is to:
• Discuss the extent of post-remediation contaminants of concern (COCs), and evaluate
potential groundwater transport mechanics in order to refine the Conceptual Site Model
(CSM);

• Present results of semi-annual and annual groundwater monitoring and sampling activities
conducted for site wells in order to assess current groundwater quality conditions and to
establish trends for a future monitoring plan;

• Evaluate the measured liquid levels and light non-aqueous phase liquids (LNAPL)
characteristics at off-site wells near the barrier wall; and

• Evaluate and quantify contaminant mass flux across the site using a transect-based
method, to support formulation of a long-term risk management strategy for the site.

This report summarizes a brief history of the site, the methods utilized for additional site
characterization, presents the data and findings of the additional investigations, and presents
appropriate steps to define the near-term path forward for the site.
Initial environmental investigations were conducted between 1990 and 1995 at the site, when it
was determined that soils and groundwater were impacted by petroleum hydrocarbons from
historical activities. In response to a Notice of Violation (NOV) issued on April 15, 1993, by the
North Carolina Department of Environment and Natural Resources (NCDENR, now NCDEQ),
Division of Environmental Management, a Comprehensive Site Assessment (CSA) was
conducted and submitted in 1993. Incident No. 5067 was issued for the site.
In late 1996, TEPRI installed an in situ vacuum-enhanced recovery system (i.e., bioslurping) that
extended from its property across West Market Street onto the Piedmont Triad International
Airport (PTIA) property to the north. The eastern-most part of the PTIA property is both
topographically downslope and hydraulically downgradient of the site. In addition to the
bioslurping system, a barrier wall was installed in 1997 under a Corrective Action Plan Addendum
(CAPA) to prevent the migration of LNAPL to a pond on the PTIA property. Following the
completion of an updated CSA and evaluation of pilot test data by Arcadis in 2004, a thermal
remediation technology, using Electro Thermal Dynamic Stripping Process™ (ET-DSP™), was
selected to remediate the on-site source area. GES summarized the remedial design for ET-
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

DSP™ in the Source Area Removal Workplan – 2005. The workplan was approved in 2005 by
the NCDENR (now NCDEQ), Winston-Salem Regional Office Aquifer Protection Section, and
Guilford County. The system’s infrastructure construction was completed in January 2007 and
the ET-DSP™ system became fully operational for Zone 1 in March 2007. The area was divided
into four separate zones for sequential treatment. Zone 1 operations were completed in
December 2007; Zone 2 operations were completed in April 2009; Zone 3 operations were
completed in June 2010; and Zone 4 operations were completed in October 2012.
The in situ thermal remediation (ISTR) system removed an estimated 880,000 pounds (lbs) of
petroleum hydrocarbon from the subsurface. The ISTR strategy achieved its objectives in the
treatment zones by removing approximately 75% of the original baseline petroleum mass and
approximately 96% of the original dissolved-phase benzene mass. The NCDENR Air Quality
Permit (No. 09563R01) and the Groundwater Remediation Permit (No. WQ002919) were
rescinded in 2013. Additionally, the City of Greensboro closed the grading permit (No. 2299) in
June 2015.
Subsurface soils at the site are characterized as sandy silt to clayey silt saprolite that has been
chemically weathered in situ from underlying, metamorphosed granitic to dioritic parent bedrock.
On the former terminal property, the saprolitic materials are present from near ground surface to
depths of approximately 70-80 feet below ground surface (bgs) and bedrock is found below these
depths. North of West Market Street, the bedrock/saprolite interface is present at depths of
approximately 60-100 feet bgs.
The local groundwater flow system is dynamic due to its positioning on both a regional and local
drainage divide. Interpretive groundwater contour maps prepared for the site indicate that a
groundwater high exists near the southeastern boundary of the TEPRI property; this groundwater
high extends onto the adjacent (to the southeast) Magellan terminal property. Groundwater flows
away from this topographic high, which runs nearly parallel to the southern property boundary
line. From a regional perspective, groundwater flow would be expected to mirror surface
topography as is demonstrated via local topography and watershed basins (see Figure 2). At the
northern end of the site, groundwater generally moves in a north/northwest direction towards a
small swale on the PTIA property. Historical liquid level data suggests that this small drainage on
the PTIA property influences groundwater flow in the shallow aquifer and is consistent with the
typical recharge-discharge model in the Piedmont physiographic province.
No potable wells have been identified within the footprint of the known extent of site-related
impacts or within the local groundwater drainage basin. There are several natural and man-made
surface water bodies including ponds, an unnamed tributary to the northwest and Horsepen Creek
to the northeast of the site. The ponds may be discharge points for shallow groundwater aquifers
while drainages further downgradient are likely groundwater discharge points for the deeper
saprolite and upper bedrock aquifers. The area just beyond the northern property fence line,
under the railroad tracks and West Market Street includes multiple underground utilities. Workers
performing maintenance on these utilities have little risk of exposure to site-related contaminants
due to the average depth to water at approximately 20 feet bgs.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

This report documents the following activities completed by GES from May 2023 through April
2024:
• Four quarterly gauging events of off-site monitoring wells in the vicinity of the barrier wall
to measure elevations of groundwater and LNAPL, if present;
• Two groundwater monitoring and sampling events of on-site and off-site wells;
• Abandonment of two former recovery wells; and
• Evaluation of mass flux through data gathering and calculations.

The groundwater sampling of monitoring wells located on-site as well as off-site on the PTIA
property was conducted in July and December 2023. Due to insufficient water levels for sampling
in December 2023, one on-site well (Z2-PZ-09) was sampled in February 2024. The samples
were obtained using low-flow sampling techniques, utilizing a submersible or peristaltic pump,
and analyzed for a list of 14 volatile organic compounds (VOCs) via United States Environmental
Protection Agency (USEPA) Method 8260 including 1,2,4-trimethylbenzene, 1,2-dibromoethane
or ethylene dibromide (EDB), 1,2-dichloroethane (1,2-DCA), 2-methyl naphthalene, isopropyl
toluene, benzene, chloroform, ethylbenzene, methyl tert-butyl ether (MTBE), methylene chloride,
naphthalene, toluene, total xylenes, and tertiary-butyl alcohol (TBA). Select monitoring wells were
also analyzed for additional monitored natural attenuation parameters including nitrate/nitrite,
sulfate, ferrous iron, manganese, total iron, alkalinity, and methane.
Analytical data from semi-annual groundwater monitoring and sampling events suggest that
concentrations of primary COCs dissolved in groundwater are decreasing. Despite this decrease,
many wells exceed allowable COC concentrations as promulgated in North Carolina
Administrative Code (NCAC) Title 15A Subchapters 2L (2L Standards) or Interim Maximum
Allowable Concentrations (IMAC) standards. The plume dimensions for some COCs i.e.,
benzene, toluene, ethylbenzene, and xylenes (BTEX), MTBE, etc. appear to be shrinking.
However, in the case of TBA, the plume appears to be expanding, but has also shown an overall
decrease in concentrations compared with the 2016 data.
In addition to the semi-annual groundwater monitoring and sampling events, quarterly barrier wall
well gauging events were conducted in July 2023, September 2023, December 2023, and March
2024. During the gauging event on December 3, 2023, LNAPL was detected at a thickness of
0.07 feet in FPZ-10. This is the first LNAPL detection at that location since May, 2018 and the
lowest measured water elevation at that location since late 2017.
The groundwater quality data is presented in the context of a mass flux model with a series of five
transects representing discrete vertical intervals of the site groundwater flow regime arranged
roughly perpendicular to overall groundwater flow. This technique has been documented by the
USEPA, United States Geological Survey (USGS), Interstate Technology and Regulatory Council
(ITRC) and others as a practical way to evaluate and prioritize site actions by identifying areas
within a contaminant plume where contaminant transport may be taking place. Use of mass flux
concepts and tools provide a valuable focus to the large volume of data collected for this
historically and physically complex site. The Mass Flux Transect Cross Sections and Mass Flux
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Transect Profiles including the supporting calculation spreadsheets, are included in Appendix A.
Further detail is discussed in Section 4 of this report.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

1 Site History and Characterization
1.1 Introduction
The site is located at 7115 West Market Street, Greensboro, North Carolina, and is approximately
10 acres in size. The former Greensboro bulk fuel terminal was originally built in 1952 and was
independently operated by Sinclair Oil Company and British Petroleum (BP) through May 1973.
Fina Petrochemicals, Inc. a predecessor company of TEPRI, acquired the terminal from BP and
operated the facility until November 1990, at which time, the terminal was permanently closed.
The fuels commonly stored at the terminal included several grades of gasoline (leaded and
unleaded), kerosene, and fuel oil #2. During operation of the terminal, six aboveground storage
tanks (ASTs) ranging in capacity from 840,000 gallons to 2,268,000 gallons were used to store
refined petroleum products. The petroleum products were delivered to the terminal via
underground pipelines owned and operated by Colonial Pipeline Company and Plantation
Pipeline Company. A wastewater storage tank, additive tanks, oil/water separators, and five
underground storage tanks (USTs) were also used at various times at the site. The USTs ranged
from 500-gallon to 2,000-gallon capacity, and were used to store fuel oil, motor fuels, and phase-
separated fuels derived from the oil/water separators and loading rack spill containment/vapor
recovery systems. The terminal was razed between May 1993 and May 1994.

The site is overseen by the Guilford County Health Department – Health and Risk Assessment
(HERA) Team. HERA assigned the former Greensboro Terminal site Incident Number (#) 5067,
under the Non-UST Section. Guilford County enforces 2L Standards and North Carolina Oil
Pollution and Hazardous Substances Control Act. Regulatory guidance, Guidelines for Initial
Response and Abatement, Assessment, and Corrective Action for Non-UST Releases of
Petroleum (Guidelines), was issued by NCDNER (now NCDEQ) in July 2012 (effective date July
1, 2012). In accordance with the 2L Standards and Guidelines, the groundwater remediation
goals specific to the site are established at concentrations equal to or less than the standards
outlined in 15A NCAC 2L.0202. The Guidelines also discuss the need for a Corrective Action
Plan (CAP) and the alternative CAPs allowed under NCAC 2L.0106 (k) or .0106 (l). The alternate
CAPs (k-CAP or l-CAP) allow for NCDEQ to approve a CAP without requiring groundwater
remediation to the 2L Standards or a plan based upon natural processes of degradation and
attenuation of contaminants.

Currently, the TEPRI property is vacant and undeveloped. The adjacent, downgradient portion
of the PTIA property is also undeveloped. A total of 136 wells exist on-site and off-site for the
purpose of monitoring groundwater conditions. The well network includes 21 remediation wells,
27 monitoring wells, and seven piezometers on-site and 81 monitoring wells off-site. A
generalized Site Map showing the locations of the existing monitoring well network is included as
Figure 3. The former site features are shown on Figure 4.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

1.2 Site Geology, Topography, and Hydrology
The former Greensboro Terminal is a rectangular piece of property with the approximate
dimensions of 520 feet by 840 feet (10 acres). The site is generally flat with a slight downward
slope to the north towards Market Street and the PTIA property. The ground surface elevation is
approximately 900 feet above mean sea level (amsl). Railroad tracks and a utility corridor run
along the northern boundary of the site. The site lies astride or just north of a drainage divide (as
mapped by Guilford County) that is oriented northwest to southeast as shown on Figure 2.
The local topography slopes from an elevation of 900 feet amsl on-site to an elevation of 834 feet
amsl off-site near the confluence of two unnamed branches of Horsepen Creek north of Old
Friendly Road, approximately 2,900 feet north/northeast. To the south and southwest of the site,
topography slopes to an elevation of approximately 840 feet amsl near the confluence of two
unnamed tributaries of the East Fork Deep River. Surface water drains on-site to the north.
Topography to the northwest, towards the PTIA is generally the same elevation as the site along
the drainage divide and surface water flows to the north. Areas to the east of the site are generally
at a higher elevation along the drainage divide. A detailed topographic map demonstrating these
relationships is included as Figure 2.
Guilford County is located within the Carolina Slate Belt (Guilford County Groundwater Monitoring
Network Status Report, June 2007). The site is located above a metamorphosed igneous intrusion
described as metacrystic, well foliated, metamorphosed granitic rock. A geologic contact with
non-metamorphosed granite is mapped to the northwest of the site near the PTIA. The contact
is generally oriented from the southwest to the northeast.
Subsurface soils at the site are characterized as sandy silt to clayey silt saprolite that has
chemically weathered in situ from the underlying, metamorphosed parent bedrock. On the
terminal property, the saprolitic materials are present from just below the ground surface to depths
of approximately 70-80 feet bgs. The installation of 12 soil borings and subsequent monitoring
wells in December 2017 and January 2018, demonstrated the saprolite layer to the north of West
Market Street on the PTIA property is more variable in thickness and depths to bedrock vary
widely, ranging from 57-100 feet bgs. The overburden saprolite is micaceous and contains relict
structures of the parent rock including mineral veins, fractures, and metamorphic foliation planes.
These structures may form secondary porosity and permeable micro-conduits that can affect
contaminant migration and distribution.
Grain size analyses performed on two direct-push technology (DPT) samples collected in April
2003 indicated that the saprolite soils in the area are predominately fines. One sample was
located on-site and the other was from the off-site PTIA property. Both samples were collected
from depths within the historical smear zone located between the historical high and low water
table elevations. Results from the analyses indicated that the saprolitic soils can be greater than
90 percent silt and clay. The saprolite is defined as a dual-porosity, fractured, porous medium,
which may locally contain small macropores. No subsurface investigative work conducted at the
site to date (to include the PTIA property) has yielded evidence of fractures or other structural
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

features in the saprolite or underlying bedrock that would represent preferential groundwater flow
pathways,
1.3 Sensitive Receptors
In 2013, RETIA commissioned GES to conduct a preliminary risk assessment study to identify all
sensitive receptors in the area. Potential off-site receptors were identified utilizing a combination
of office and field reconnaissance tasks. The local Guilford County Well Records were reviewed,
and GES personnel conducted a windshield receptor survey over an area that encompassed the
local drainage basin. The windshield survey was used to identify potential undocumented wells
as well as to confirm the location of potential wells identified in an Environmental Essentials
Package obtained by GES from Environmental Data Resources, Inc. (EDR) and Guilford County
files. The EDR package was submitted in the subsequent reports submitted to the NCDEQ and
Guilford County.
No potable wells have been identified within a half mile of the footprint of the known extent of site-
related impacts or within the groundwater drainage basin. There are several surface water bodies
including man-made ponds, unnamed tributaries to Horsepen Creek and Horsepen Creek to the
north of the site. The ponds may be groundwater discharge points for shallow groundwater
aquifers while drainages further downgradient are potentially groundwater discharge points for
the deeper saprolite and upper bedrock aquifers. During the windshield survey, flowing water
was identified in the unnamed tributaries of Horsepen Creek at a time of limited rainfall which
suggests that the stream is fed by local groundwater discharge. An evaluation of groundwater
and surface water elevations further supports this relationship.
The area just north of the TEPRI property fence line, under the railroad tracks and West Market
Street includes multiple underground utilities. Workers performing maintenance on these utilities
have little risk of exposure to site-related contaminants due to the average depth to water at
approximately 20 feet bgs.
According to the National Wetlands Inventory map in the EDR Report previously referenced, a
small wetland exists immediately south and adjacent to the man-made pond on the PTIA property,
north of the site. The pond itself is not listed. The pond and adjacent wetlands may be considered
potential receptors. Historical sampling data from 2006 indicates the pond was not impacted by
petroleum hydrocarbon compounds at that time. Additional data collected from surface water
sampling at the off-site stream/pond interface (SG-1) in 2018 and 2020, indicate the surface water
is also integrated with the local, shallow groundwater system and is not impacted by any of the
site-specific VOCs. Current data from the furthest downgradient monitoring well before the pond,
FPZ-5, indicates shallow groundwater is not affected by petroleum hydrocarbons, suggesting
discharge to the pond is also free of such impacts. Additionally, the 12 monitoring wells north of
the pond (configured in three clusters of four wells each at shallow, intermediate, deep saprolite
and bedrock intervals) indicate no impacts of petroleum hydrocarbons above applicable
regulatory standards. No other potential receptors were identified within the drainage basin
comprising the TEPRI site.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

1.4 Surrounding Properties and Releases
Adjacent to the TEPRI property are two other former bulk fuel storage terminal properties: the
former Amoco Oil Company (Amoco) to the east and the former Phillips Pipeline Company
(Phillips) to the west. The former Amoco terminal has been reactivated and is currently owned
and operated by Magellan Terminals Holdings, L.P. (Magellan). The former Phillips property is
now owned by AAA Cooper and is vacant. These adjacent areas are shown on the Local Area
Map included as Figure 5.

The PTIA property, located north of the TEPRI property, is impacted by petroleum constituents
that likely originated from multiple sources. The PTIA property is separated from the TEPRI
property by the Southern Railway rail line and West Market Street. A surface water impoundment
and intermittent stream (drainage ditch) exist on the PTIA property (Figures 3, 4, and 5). GES
obtained an EDR report that included an EDR Aerial Photo Decade Package. The 1955 photo in
the EDR report previously provided, shows the pond was created by a man-made dam/berm.
1.4.1 Magellan Terminal Property – EDR Report Review
The Magellan terminal property has documented hydrocarbon impacts at the facility; BP/Amoco
retains the environmental liability for past hydrocarbon releases at that location. The EDR
package also included an EDR Radius Map™ Report with Geocheck®. The EDR report was
included in monitoring reports previously submitted to the NCDEQ and Guilford County. The
following incidents associated with the Magellan terminal property were noted:

• The Leaking Aboveground Storage Tank (LAST) database lists Greensboro Terminal II
being associated with contamination in groundwater from an aboveground source. The
leak was reported by BP Products of North America on October 16, 1989, and incident
Number 5068 was issued. The incident was reported to be closed. No additional
information was provided in the EDR report.

• The Leaking Underground Storage Tank (LUST) database lists Greensboro Terminal II
being associated with petroleum contamination in soil from an underground source. The
leak was reported by Atlantic Richfield Co, on December 20, 1991, and incident Number
7871 was issued. The incident was reported to be closed out on December 15, 1993. No
additional information was provided in the EDR report.

• The Incident Management Database (IMD) database lists Amoco Tank Farm being
associated with off-site contamination in groundwater from gasoline, diesel, and/or fuel oil.
A NOV was issued on April 28, 1993. No additional information was provided in the EDR
report.
1.4.2 Former Phillips Terminal
The former Phillips terminal to the west has been closed and razed. The northern portion of the
former Phillips terminal is now a vacant grassy field owned by AAA Cooper Transportation. This
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

area is enclosed by a fence and also serves as the entrance to the TEPRI property. The southern
portion of the former Phillips terminal is now owned and operated by AAA Cooper Transportation
as a commercial trucking depot and repair facility. The former Phillips site is bordered to the south
by the Welsh Paper Company. An underground pipeline easement abuts the site and a
documented product release occurred from this pipeline along the TEPRI property boundary (see
below).

There are two documented releases from the Phillips property (Monitoring Report January –
August 2016, ATC Associates of North Carolina, 2016). A gasoline release from the loading rack
reported in 1987 that received a no further action letter in 2005, and a heating oil/kerosene release
from the pipeline connection located along the eastern portion of the former Phillips property
reported in 1987. The pipeline release was assigned Groundwater Incident No. 14636 by the
NCDEQ. On March 1, 2016, the NCDEQ initiated a regulatory change that allows for risk-based
closures at non-UST releases with no free product. The Former Phillips Terminal is pursuing
risked based closure for the pipeline release (IN# 14636). The receptor survey was updated with
water supply wells, well houses, water meters, and surface water bodies. Research has indicated
the site is low risk and there are no water supply wells within 1,000 feet of the site and no “notable”
surface water bodies within 500-feet of the site. In May and June 2018, the consultant conducted
additional soil and groundwater sampling activities and subsequently submitted the September
24, 2018 Site Closure Request Report to Guilford County, under a risk-based scenario with a
notice of residual petroleum. It is TEPRI's understanding that a CAP, in accordance with Title
15A NCAC 2L .0106 to address soil and groundwater impacts associated with the petroleum
pipeline release, has never been developed for this release. The plume is monitored on a semi-
annual basis.
1.4.3 Other Documented Releases
Additional releases have been documented in the Assessment of Active On-Site and Off-Site
Remediation Systems and Contributions from Multiple Off-Site Source Areas Report (Arcadis,
1998). The report identifies over 17 separate releases that occurred on adjacent properties or
on-site prior to TEPRI’s ownership. Excerpts from the report, including Figure 1-2: Terminal-
Complex Map with Areas Impacted by Known Off-Site Releases and Table 3-1: Known Off-Site
Releases and On-Site Releases Prior to Fina’s Ownership, Fina Oil and Chemical Company
(#1760), Greensboro, North Carolina, were included in monitoring reports previously submitted to
the NCDEQ and Guilford County. The largest documented releases from the Arcadis report are
summarized below:

• May 1966 – Approximately 7,000 gallons of diesel fuel was released to the ground surface
when a train collided with a tanker truck. Most of the fuel was not recovered, and the fuel
reportedly ponded in ditches and absorbed into surface soils.

• 1969 – Approximately 2,500 to 3,000 gallons of diesel fuel were released to the ground
surface due to an accident involving a tanker truck on the Amoco property. The Fire
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Department washed the fuel into surface ditches along Market Street. Substantial
quantities of product accumulated in the front ditch and absorbed into the ground.

• July 1977 – Approximately 5,000 gallons of gasoline were released to the surface ditches
along West Market Street when a train collided with a tanker truck. The Fire Department
washed the fuel into surface ditches along West Market Street and then attempted to
recover fuel and contaminated wash-down water the following day. According to this
information, contaminated soil was left in place.

• 1981 – Approximately 7,500 gallons of gasoline were released along the front boundary
of the former TEPRI terminal, when a train collided with a tanker truck at the Gallimore
Dairy Road crossing. Attempts to salvage the product were made.

• July 1997 – Approximately 5,000 gallons of gasoline were released to the surface ditches
along Market Street when a train collided with a tanker truck. The Fire Department washed
the fuel into surface ditches along Market Street and then attempted to recover fuel and
contaminated wash water the following day. According to the information provided, the
contaminated soil was left in-place.
1.5 Previous Investigations
Initial environmental investigations at the site were conducted between 1990 and 1995 and
determined that soils and groundwater were impacted from historical activities at the former
TEPRI terminal. In response to a NOV issued on April 15, 1993 by the NCDENR (now NCDEQ),
a CSA was conducted and submitted in 1993. Incident No. 5067 was assigned for this site by
Guilford County HERA.
TEPRI completed additional soil and groundwater assessment activities in 2004. These
additional activities were recommended in the 2003 CSA Report - Phase II prepared by Arcadis
G&M of North Carolina, Inc. (Arcadis), to further assess the horizontal and vertical extent of
petroleum constituents within soil and groundwater below the site and adjacent properties. A
Membrane Interface Probe (MIP) survey was conducted at 57 sample locations on the TEPRI,
AAA Cooper, and PTIA properties, to assist with delineation of hydrocarbons in the subsurface.
The MIP data points collected between April and May 2003 provided a snapshot of the lateral and
vertical extent of relative hydrocarbon concentrations and provided a preliminary spatial outline
of the source area.

The former source zone is described in the August 2005 Source Area Removal Workplan (GES),
approved by NCDENR (now NCDEQ) in an October 12, 2005 correspondence. The volumetric
extent of the “source area” was refined as data were collected during the execution of ET-DSP™
efforts. An extensive “smear zone” was identified across the site based on soil data, MIP survey
data, and historic water table fluctuations. The initial (pre-remediation) source mass was
estimated to be over 1.1 million pounds (192,000-gallon equivalent). The smear zone was
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

approximately 260,000 square feet (6 acres) and roughly 12-feet thick in the terminal area and
included the free oil zone bounded above and below by residual oil zones.
Preliminary delineation of the horizontal and vertical extent of impacts on-site and off-site (AAA
Cooper and PTIA sites) was conducted using the flame ionization detector (FID) response data
collected during the 2003 MIP investigation. The highest levels of FID responses were observed
on the terminal site and the northeastern corner of the AAA Cooper property. The results of the
MIP investigation further defined the extent of the “smear zone” located along the site and
adjacent properties, and indicated decreasing impacts at depths below approximately 25 to 30
feet bgs (bottom of smear zone) as shown in Appendix B. The smear zone extended from near
the southern property boundary to the hydrocarbon interceptor trench located to the north on the
PTIA site.
As discussed in Section 1.6, extensive source remediation efforts were implemented for the on-
site source area. Residual source mass likely exists in areas that were not affected by thermal
remediation. These areas include the on-site area just to the north of Zone 4, the area underlying
the railroad tracks and below West Market Street.
The 2004 CSA Report – Phase III (Submitted by Arcadis, June 2005), provides a description of
subsequent investigative activities conducted from March through October 2004, including aquifer
testing, installation and sampling of six groundwater monitoring wells, an annual groundwater
sampling event, a subsurface soil investigation on the adjacent AAA Cooper and PTIA properties,
and a comprehensive investigation of the drainage features on the PTIA property. Additionally,
in an ongoing effort to evaluate technologies that may be used for source area remediation of the
site, Arcadis also documented the findings of three remedial pilot studies conducted in 2004.

The pilot studies were conducted to address remediation of the primary source area. The pilot
tests included a combined dewatering/high-vacuum extraction test (conducted by Arcadis), a
combined air sparge/high-vacuum extraction test (conducted by Arcadis), and an aggressive in-
situ thermal remediation study using ET-DSP™ (conducted by GES). Each of the pilot studies
were effective in recovering hydrocarbons from the subsurface, and a brief description of the
results of the combined dewatering/high-vacuum extraction test and the combined air
sparge/high-vacuum extraction test is included in the 2004 CSA Report – Phase III (Submitted by
Arcadis, June 2005).

An additional soil investigation was conducted by GES in February and March 2005, to further
delineate both vadose zone and saturated zone soil impacts (vertically to the lowest historical
water table elevation) across the assumed “source area” located on the TEPRI and AAA Cooper
properties.

The 2015 Comprehensive Site Assessment Report (Submitted by GES, March 2016), submitted
to Guilford County and the NCDEQ, provides a description of subsequent investigative activities
conducted from January through December 2015, including a surficial geophysical survey,
installation and sampling of 27 groundwater monitoring wells, a site-wide comprehensive
groundwater sampling event, LNAPL baildown testing, and LNAPL fingerprinting. Additionally in
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

the 2015 Comprehensive Site Assessment Report, a Sampling and Analysis Plan (SAP) and
Mass Flux Work Plan were included. In an April 11, 2016 correspondence, the NCDEQ
acknowledged receipt of the 2015 Report and approved the Mass Flux Work Plan as the basis
for developing a new remedial action plan for the site. In the correspondence, the NCDEQ also
requested additional information with regards to the LNAPL detected in monitoring well FPZ-10,
for developing a free product recovery strategy. TEPRI addressed the NCDEQ’s April 11, 2016
correspondence with the July 6, 2016 submittal of the Response to NCDEQ Acknowledgement
of Report Receipt. In a correspondence dated July 26, 2016, the NCDEQ approved the
recommendations made in the in the 2015 Comprehensive Site Assessment Report for additional
assessments and remediation activities at the site. Copies of the NCDEQ correspondences were
included in the 2015 Comprehensive Site Assessment Report.

The 2017 Annual Monitoring Report / Comprehensive Site Assessment Report (GES, August
2017), submitted to Guilford County and the NCDEQ, provides a description of subsequent
investigative activities conducted from January 2016 through April 2017, including the installation
and sampling of 18 groundwater monitoring wells, semi-annual site-wide comprehensive
groundwater sampling events, and quarterly liquid level gauging of off-site monitoring wells at the
barrier wall to measure elevations of groundwater and LNAPL. Additionally in the 2017 Annual
Monitoring Report / Comprehensive Site Assessment Report, an updated SAP was included. In
a September 25, 2017 correspondence, the NCDEQ acknowledged receipt of the 2017 Report
and approved the proposal to install three additional monitoring well clusters to delineate the
extent of contaminant plumes downgradient on the PTIA property for completing mass flux
estimates.

The 2018 Annual Monitoring Report / Comprehensive Site Assessment Report (GES, May 2019),
submitted to Guilford County and the NCDEQ, provides a description of subsequent investigative
activities conducted from May 2017 through April 2018, including the installation and sampling of
12 groundwater monitoring wells, semi-annual site-wide comprehensive groundwater sampling
events, and quarterly liquid level gauging of off-site monitoring wells at the barrier wall to measure
elevations of groundwater and LNAPL. Additionally in the 2018 Annual Monitoring Report /
Comprehensive Site Assessment Report, an evaluation of mass flux through data gathering and
calculations was included.

On December 17, 2018, three wells were abandoned including on-site extraction well Z1-X09 and
off-site monitoring wells FMW-19 and OW-5. Additionally, attempts to locate on-site piezometer
Z4-PZ-10 were conducted; however, it could not be found. On January 8, 2019, the Well
Abandonment Records were submitted to Guilford County, and the Monitor Well Construction
Permit was subsequently amended from 141 to 138 permitted wells per a January 11, 2019
correspondence from Guilford County to TEPRI. Since on-site extraction well Z1-X09 was not on
the current permit and on-site piezometer Z4-PZ-10 has been missing and presumably destroyed
since April 2013, the current permit for 138 wells is still valid.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

On June 12, 2020, GES and RETIA requested approval from Guilford County to suspend
monitoring and sampling of 21 select monitoring wells included in the approved Monitor Well
Construction Permit #143-96-MW115-RW23. The 21 monitoring wells demonstrated at least six
semi-annual rounds of either non-detect results or had minor detections below the NCAC 2L and
IMAC standards of all site-specific dissolved petroleum compounds. Additionally, the 21
monitoring wells are not part of the ongoing mass flux evaluation for the site. In an email
correspondence on June 12, 2020, Guilford County approved the request.
GES conducted an evaluation of the magnitude and extent of residual hydrocarbon impacts on
the PTIA and TEPRI properties following completion of ISTR in 2012. Based on the most recent
groundwater sampling events conducted from 2013 through 2023, data indicates that the
dissolved-phase impacts to the shallow groundwater interval have been greatly reduced on the
TEPRI property. With the recent installation of the new monitoring well clusters on the PTIA
property, the data gaps that were previously reported have been largely resolved. Such data
gaps included determining the extent of off-site residual impacts underlying the space around
West Market Street and the railroad tracks to the north of the site (i.e., between on-site and off-
site monitoring wells), potential discharge and recharge locations of groundwater to surface water
bodies off-site, and the vertical and horizontal distribution of the dissolved-phase TBA plume and
TBA migration potential – particularly within the deep saprolite and bedrock hydraulic regimes. It
should also be noted that the investigative work completed on-site and off-site in 2015 through
2017 did not yield evidence of soil quality in excess of industrial risk standards for the entire suite
of compounds analyzed.
1.6 Summary of Remedial Activities
In late 1996, TEPRI installed a vacuum-enhanced recovery system (bioslurping) that extended
from its property onto the neighboring Phillips property. The bioslurping system was operational
from January 1997 until 2005. The system consisted of more than 27 single and dual-screen
recovery wells covering an area of approximately 2.75 acres. The bioslurping system generated
liquid and gas waste streams, which were treated in separate treatment units. The soil gas was
removed in a knockout tank upstream of the water treatment equipment. The recovered
petroleum product was phase-separated from the groundwater in an initial settling tank and later
in an oil/water separator. The dissolved-phase contaminants were removed from the groundwater
by an air stripping system. The bioslurping system was decommissioned and dismantled in 2005.

In addition to the bioslurping system, a hydrocarbon interceptor wall was installed under a CAP
Addendum in 1997 on the PTIA property, to prevent the migration of LNAPL into the downgradient
pond. The location of the hydrocarbon interceptor wall is depicted on Figures 2, 3, and 4.
Pneumatic oil skimming pumps were also used in two recovery wells (RW-1 and RW-2) on the
PTIA property to remove any accumulated product within the permeable backfill upgradient of the
hydraulic barrier wall. The hydrocarbon interceptor wall remains in place, but LNAPL recovery
operations from recovery wells RW-1 and RW-2 was discontinued in approximately 2014.
Existing monitoring wells and piezometers in the vicinity of the barrier wall on the PTIA property
are gauged on a quarterly basis to verify that LNAPL has not migrated past this wall. LNAPL was
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

last detected in RW-2 in January 2004 at an in-well thickness of 0.02 feet. No record of LNAPL
accumulation exists for RW-1. LNAPL has not been observed in the area of the interceptor trench
since 2018 and has not been observed in any on-site wells since 2013.

Following the completion of the CSA in 2004 and evaluation of the pilot test data mentioned in
Section 1.5, ISTR using ET-DSP™ technology was selected to remediate the source area. The
remedial design for ET-DSP™ was summarized in the Source Area Removal Workplan (GES
2005). The workplan was approved by NCDNER (now NCDEQ) Winston-Salem Regional Office
Aquifer Protection Section and Guilford County in 2005.

The ET-DSP™ technology is a licensed/patented technology implemented by McMillan-McGee
Corporation (Mc2) of Calgary, Alberta Canada. ET-DSP™ is a remediation technique, similar to
electrical resistance heating (ERH), in which electricity is supplied to buried electrodes to create
a heated zone in the subsurface. When using the ET-DSP™ technology, heat is generated within
an electrode field due to soil properties that resist the transfer of electricity. The resultant heat
vaporizes water and petroleum hydrocarbons and generates in situ steam that serves to transport
subsurface volatile and semi-volatile compounds to the surface. Soil Vapor Extraction (SVE) or
Multi-Phase Extraction (MPE) techniques are then used to capture the gasses and liquids driven
off by heat for aboveground treatment.

The construction of the thermal remediation system was completed in January 2007. The
treatment area was divided into four separate zones for sequential treatment. Zone 1 operations
were completed in December 2007; Zone 2 operations were completed in April 2009; Zone 3
operations were completed in June 2010; and Zone 4 operations were completed in October
2012. The ISTR strategy removed an estimated 880,000 pounds of petroleum hydrocarbon mass,
including 657,000 pounds (75%) recovered in the vapor phase; 202,000 pounds (23%) recovered
as non-aqueous phase liquid; and 21,000 pounds (2%) recovered as dissolved-phase in extracted
groundwater. The ISTR overachieved its stated objectives in the treatment zones by removing
approximately 75% (remedial target = 70%) of the original baseline petroleum mass and
approximately 96% (remedial target = 93%) of the original dissolved-phase benzene mass.
Removing over 70% of the cumulative mass recovered has eliminated the majority of the on-site
source area hydrocarbon mass, reduced contaminant flux to groundwater and promoted post-
heating petroleum hydrocarbon degradation via aerobic bioremediation. The removal of over
93% benzene will facilitate restoration of groundwater by allowing the upper aquifer to return to
aerobic conditions, which will promote further groundwater restoration via monitored natural
attenuation.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

1.7 Site Strategy
1.7.1 Monitoring Well Optimization
Due to the extensive monitoring well network at the site (i.e., over 130 wells), GES and RETIA
conducted an optimization analysis of the existing groundwater sampling program, using the
Monitoring and Remediation Optimization system (MAROS) software package developed by GSI
Environmental, Inc. for the Air Force Center for Engineering and the Environment. The MAROS
software provides a highly prescriptive process for analyzing and iteratively comparing alternate
networks of well sampling for a specific site.
MAROS analyzes both temporal and spatial data to provide recommendations for eliminating
wells from the sampling program and/or reducing the frequency of sampling. The objective of the
MAROS optimization is to minimize the sampling program by eliminating data that provide no
significant value to the analysis while ensuring adequate future characterization for the
contaminant plume.
GES performed an additional spatiotemporal analysis to verify the MAROS determination of
trends for both individual wells and overall plume mass estimates. The Groundwater
Spatiotemporal Data Analysis Tool (GWSDAT) software package was developed by Shell to
provide interpolated groundwater concentrations of specified COCs over time. GWSDAT also
allows plume extent thresholds to be specified by the user. If the interpolation provides for
complete delineation to the specified threshold, then GWSDAT will calculate the center of mass
location as well as estimates of plume mass and average concentration. This output can then be
used to evaluate the stability of the plume overall and can help in identifying systemic changes
that may indicate new releases and/or off-site plume encroachment. GWSDAT also provides
trend charts that plot observed analytical concentrations and confidence intervals for the trend.
Using the output provided by MAROS and GWSDAT in conjunction with project-specific
knowledge (i.e., key operational remedial system wells, site characterization/delineation wells,
and off-site monitoring wells), results indicated the sampling frequency for some wells could be
reduced based on sufficient recent and historical data showing low rates of change. There were
eight wells that did not show a strong enough decreasing trend to recommend a reduction in
sampling frequency at those locations. Additionally, the results indicated that it was feasible to
remove 26 wells from the monitoring program as the plume is stable across these wells and most
analytes. Currently, 107 wells are sampled on an annual basis and eight wells are sampled semi-
annually.
The results of the optimization analysis were included in the December 3, 2021 (Rev. January
2022) Groundwater Monitoring Plan Optimization Analysis report submitted to Guilford County.
The report was approved in a February 11, 2022 correspondence.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

1.7.2 New Technology Cleanup Plan
A New Technology Cleanup Plan (NTCP) was submitted by GES on behalf of RETIA, to the
NCDEQ and Guilford County on November 15, 2022. The purpose of the NTCP was to:

• Discuss the extensive history, assessment, and remediation of the site to further evaluate
and propose additional remedial options for a long-term site strategy;
• Discuss the extent of post-remediation contaminants of concern (COCs), and evaluate
potential groundwater transport mechanics in order to refine the Conceptual Site Model
(CSM);
• Present historical results of soil, groundwater, and surface water monitoring and sampling
activities conducted to assess current conditions and to establish trends for a future
monitoring plan;
• Present risk classification and applicable cleanup goals for soil, groundwater, and surface
water;
• Discuss results of an ongoing contaminant mass flux analysis across the site to support
formulation of a long-term risk management strategy for the site;
• Discuss in-place remedial technologies such as the LNAPL barrier wall and natural
attenuation and their effectiveness to be viable remedial options, and propose a plan to
enhance natural attenuation with an in-situ biostimulation approach; and
• Present potential risk based corrective action approaches such as filing a Notice of
Contaminated Site for both the on-site and off-site properties.
The NTCP was approved in a November 22, 2022 correspondence (incorrectly dated November
22, 2021).
1.7.3 Enhanced In-Situ Bioremediation (EISB) Evaluation
A combination of natural attenuation plus the ongoing use of the LNAPL barrier wall is a viable
remedial option; however, based on a half-life analysis of data collected from 2012-2021, it would
take an extended period of time to achieve the 2L standards and even GCLs if those were
approved via a risk reduction mechanism. Therefore, and rather than natural attenuation as the
sole remedial process for groundwater contamination, RETIA proposed to undertake an
evaluation of the effectiveness of an enhanced in-situ bioremediation (EISB) remedy at locations
where mass flux calculations suggest there is significant VOC transport.
An EISB Evaluation Work Plan was submitted by GES on behalf of RETIA, to the NCDEQ and
Guilford County on January 13, 2023 (later revised on January 25, 2023) to outline work to be
completed to evaluate the effectiveness of an EISB remedy.

Further understanding the chemical, geochemical, and biological conditions at the site is
necessary to assess the potential for EISB. It is important to understand the particular petroleum
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

degrading microorganisms that are present as well as which electron acceptor (oxygen, sulfate,
or nitrate) is most favorable towards the existing biological community and geochemical state to
ensure the success of an EISB approach.
To facilitate this understanding, GES completed additional groundwater sampling and microcosm
studies in 2023 to assess the petroleum hydrocarbon and fuel oxygenate degrading capabilities
and activities of the naturally-occurring organisms via molecular biological tools (MBTs). MBT
studies use laboratory testing to assess whether the indigenous microorganisms are actively
degrading contaminants. Data generated from the studies are used to directly support the
presence of natural attenuation processes at the site and the ability to enhance the degradation
with amendments intended to increase the in-situ microbial population. The data collected for the
study are still under evaluation to definitively determine the presence and activity of the naturally-
occurring organism under enhanced conditions.
Once the study is finalized, an EISB Evaluation Report will be submitted to the NCDEQ and
Guilford County under separate cover.
1.8 Report Objectives
The objectives of this Annual Monitoring Report include presentation of:
• A discussion of the extent of post-remediation COC impacts, and proposed additional
measures to evaluate groundwater transport mechanics in order to refine the CSM;
• A summary of groundwater monitoring and sampling activities for site wells to assess
current groundwater quality conditions and to establish trends for a future monitoring plan;
• An evaluation of the measured liquid levels and LNAPL, if present, at off-site wells near
the barrier wall on the PTIA property;
• An evaluation of the current monitoring well network and sampling frequency, for
optimization purposes; and
• An assessment of the lateral and vertical integrated network for the purpose of calculating
contaminant mass flux.

The following subsections summarize the methods utilized for additional site characterization,
present the data and findings of the additional investigations, and present the appropriate steps
to define the near-term path forward for the site.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

2 Methodology
2.1 Groundwater Monitoring and Sampling
GES conducted quarterly gauging of shallow monitoring wells designated as the barrier wall wells,
during events in July 2023, September 2023, December 2023, and March 2024. A total of 30
barrier wall wells were gauged during all events except in March 2024, where only 28 barrier wall
wells were gauged. Two former recovery wells, which also served as barrier wall wells, were
properly abandoned in February 2024 (see Section 2.3). The quarterly barrier wall well gauging
events for July and December 2023, were conducted in conjunction with semi-annual and annual
groundwater sampling events. Gauging of the barrier wall well network has been conducted on
a weekly, monthly, bi-monthly, and/or intermittent basis since approximately 1997. Results of the
barrier wall gauging events are discussed in Section 3.1.
Additionally, GES conducted two groundwater monitoring and sampling events at the site in July
and December 2023. Due to insufficient water levels for sampling in December 2023, on-site well
Z2-PZ-09 was sampled in February 2024. The groundwater monitoring and sampling events were
conducted in accordance with the approved SAP (submitted in the 2015 Comprehensive Site
Assessment Report), and the approved December 3, 2021 (Rev. January 2022) Groundwater
Monitoring Plan Optimization Analysis report, which reduced and/or eliminated the sampling
frequency of select site monitoring wells and piezometers.
Prior to sampling, liquid-level measurements were collected from each well utilizing an oil/water
interface probe. Both the measurements of water and oil, if applicable, were recorded in a field
notebook to the nearest 0.01-foot below the TOC. The well construction details along with survey
information for each well are included on Table 1. Tables 2 and 3 contain the recorded gauging
data and groundwater elevations for on-site and off-site wells, respectively.
Between July 17 through 20, 2023, GES personnel monitored and sampled a total of 115 out of
138 permitted wells including, 27 on-site monitoring wells, 19 on-site extraction wells, seven on-
site piezometers, and 62 off-site monitoring wells. The remaining 23 extraction wells and/or
monitoring wells of the 138 total permitted wells were only gauged and not sampled, per the
approved reduction discussed in Section 1.7.1.
On December 6, 2023, GES personnel monitored a total of eight out of 138 permitted wells
including, one on-site monitoring well, one on-site piezometer, and six off-site monitoring wells.
During the event, one well (piezometer Z2-PZ-09) was observed to be dry and therefore, not
sampled. The remaining 130 extraction wells and/or monitoring wells of the 138 total permitted
wells were not gauged during this event; except for the designated barrier wall wells that are
gauged on a quarterly basis. In conjunction with other activities on February 2, 2024, monitoring
well Z2-PZ-09 was gauged and subsequently sampled.
Groundwater samples were collected from the monitoring wells using the low-stress (low-flow)
purging and sampling methods outlined in the SAP. Field geochemical parameters, including pH,
electrical conductivity, temperature, dissolved oxygen (DO), oxidation-reduction potential (ORP),
and turbidity, were recorded by GES staff in the field. Each well was purged at low-flow rates,
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

approximately 200-300 milliliters per minute (mL/min) until field geochemical parameters had
stabilized. The geochemical parameters were measured using a YSI DDS Pro multi-parameter
meter using a flow through cell, and the results were recorded at regular intervals in a field
notebook. In addition, draw-down was measured utilizing an oil/water interface probe. The
stabilized groundwater parameters for each monitoring well are provided in Table 4. Groundwater
sampling forms completed during the July 2023 and December 2023/February 2024 sampling
events, are included in Appendices C and D, respectively.
Groundwater samples, including field duplicates, equipment blanks, and field blanks were
collected in either unpreserved or pre-preserved, laboratory-prepared bottleware and placed in a
cooler on ice immediately following collection. Equipment blanks were taken daily by running
deionized water through the sampling equipment to ensure proper decontamination between
wells. Appropriate chain-of-custody documentation accompanied the samples to ALS
Environmental located in Houston, Texas. Groundwater sample analysis utilized the following
USEPA methods:

• Method 8260B: Site-specific VOCs including trimethylbenzene, EDB, 1,2-DCA, 2-
methyl naphthalene, isopropyl toluene, benzene, chloroform,
ethylbenzene, MTBE, methylene chloride, naphthalene, toluene,
total xylenes, and TBA;
• Method 8011: EDB;
• Method RSK-175: Methane and/or isobutylene;
• Method 353.2: Nitrate/nitrite;
• Method 9038: Sulfate;
• Method 2320B: Alkalinity;
• Method 3500F+2B: Ferrous iron; and
• Method 6010C: Manganese and iron.

The groundwater analytical laboratory reports from ALS Environmental for the July 2023 and
December 2023/February 2024 sampling events, are included in Appendices E and F,
respectively.
Groundwater analytical results are summarized in Tables 5 and 6 for on-site and off-site wells,
respectively. The analytical results were then compared to the NCDEQ NCAC2L and/or IMAC
standards for petroleum releases for all analyzed VOCs.

All purge water and decontamination fluid associated with the sampling event was placed into
temporary storage tanks. Following completion of the site activities the sediment suspended in
the purge water was allowed to settle out prior to transport. Documentation from A&D
Environmental, Inc., for removal and disposal of purge water and decontamination liquids from
the July 2023 groundwater monitoring and sampling event is provided in Appendix G.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

2.2 Surface Water Monitoring
During semi-annual and quarterly groundwater monitoring events, GES gathered the surface
water elevation from a calibrated stream gauge (SG-1) that was previously installed at the off-site
stream/pond interface. Table 3 contains the recorded gauging data and groundwater elevations
for stream gauge SG-1. This surface water elevation value is incorporated into the shallow
groundwater flow maps provided as Figures 6 through 10.
2.3 Recovery Well Abandonment
On February 2, 2024, two off-site wells were abandoned including former recovery wells RW-1
and RW-2. The Well Abandonment Records were submitted to Guilford County via email on
February 28, 2024. Per the email correspondence dated May 7, 2024, the Monitoring Well
Construction Permit will be amended from 138 to 136 permitted wells. An updated list of permitted
wells along with the May 7, 2024 Guilford County correspondence, is provided in Appendix H.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

3 Site Investigation Results
3.1 Barrier Wall Gauging
In May 2023 through March 2024, GES personnel completed quarterly gauging of the shallow
monitoring wells designated as the barrier wall wells. Additionally in conjunction with these
events, GES gathered the surface water elevation from stream gauge SG-1 at the off-site
stream/pond interface. A compilation of these gauging data combined with historical gauging
data can be found in Tables 2 and 3. Groundwater elevation maps for the July 2023, September
2023, December 2023, and March 2024 barrier wall well gauging events are included as Figures
6, 7, 8, and 9, respectively. Groundwater flow was shown to be consistent with historical
observations, flowing in a northerly direction with localized deflection around the barrier wall. The
2023 and 2024 gauging events completed during this reporting period are summarized below.
3.1.1 Routine Gauging Events
Gauging Event
Gauging Date: July 17, 2023
Wells Gauged: AMW-11S, AMW-13S, AMW-14S, AMW-15S, AMW-16S,
AMW-17S, AMW-18S, DEM-MW6R, FMW-20, FMW-21,
FMW-23R, FPZ-5, FPZ-6, FPZ-7, FPZ-8, FPZ-10, FPZ-11,
FPZ-12, FPZ-13, FPZ-14, FPZ-15, OW-1, OW-2, OW-3,
OW-4, OW-6, OW-7, OW-8, RW-1, RW-2, and stream gauge
SG-1
LNAPL: Not present
Depth to Water Range: 4.24 (FPZ-5) to 16.14 (DEM-MW6R) feet below top of
casing
Groundwater Flow Direction: Northeasterly (at close proximity to the barrier wall) and
Easterly (at western portion of barrier wall)
Groundwater Elevation: 870.55 (FPZ-5) to 877.48 (AMW-14S)
Present Hydraulic Gradient: 0.014 feet/foot between AMW-14S and FPZ-5

Gauging Event
Gauging Date: September 18, 2023
Wells Gauged: AMW-11S, AMW-13S, AMW-14S, AMW-15S, AMW-16S,
AMW-17S, AMW-18S, DEM-MW6R, FMW-20, FMW-21,
FMW-23R, FPZ-5, FPZ-6, FPZ-7, FPZ-8, FPZ-10, FPZ-11,
FPZ-12, FPZ-13, FPZ-14, FPZ-15, OW-1, OW-2, OW-3,
OW-4, OW-6, OW-7, OW-8, RW-1, RW-2, and stream gauge
SG-1
LNAPL: Not present
Depth to Water Range: 5.31 (FPZ-5) to 18.53 (FMW-20) feet below top of casing
Groundwater Flow Direction: Northeasterly (at close proximity to the barrier wall) and
Easterly (at western portion of barrier wall)
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Groundwater Elevation: 869.48 (FPZ-5) to 875.17 (AMW-14S)
Present Hydraulic Gradient: 0.011 feet/foot between AMW-14S and FPZ-5

Gauging Event
Gauging Date: December 6, 2023
Wells Gauged: AMW-11S, AMW-13S, AMW-14S, AMW-15S, AMW-16S,
AMW-17S, AMW-18S, DEM-MW6R, FMW-20, FMW-21,
FMW-23R, FPZ-5, FPZ-6, FPZ-7, FPZ-8, FPZ-10, FPZ-11,
FPZ-12, FPZ-13, FPZ-14, FPZ-15, OW-1, OW-2, OW-3,
OW-4, OW-6, OW-7, OW-8, RW-1, RW-2, and stream gauge
SG-1
LNAPL: 0.07 feet in FPZ-10
Depth to Water Range: 6.55 (FPZ-5) to 20.22 (FMW-20) feet below top of casing
Groundwater Flow Direction: Northeasterly (at close proximity to the barrier wall) and
Easterly (at western portion of barrier wall)
Groundwater Elevation: 868.24 (FPZ-5) to 873.43 (AMW-14S)
Present Hydraulic Gradient: 0.010 feet/foot between AMW-14S and FPZ-5

Gauging Event
Gauging Date: March 1, 2024
Wells Gauged: AMW-11S, AMW-13S, AMW-14S, AMW-15S, AMW-16S,
AMW-17S, AMW-18S, DEM-MW6R, FMW-20, FMW-21,
FMW-23R, FPZ-5, FPZ-6, FPZ-7, FPZ-8, FPZ-10, FPZ-11,
FPZ-12, FPZ-13, FPZ-14, FPZ-15, OW-1, OW-2, OW-3,
OW-4, OW-6, OW-7, OW-8, and stream gauge SG-1
LNAPL: Not present
Depth to Water Range: 3.30 (FPZ-5) to 17.60 (OW-8) feet below top of casing
Groundwater Flow Direction: Northeasterly (at close proximity to the barrier wall) and
Easterly (at western portion of barrier wall)
Groundwater Elevation: 870.75 (SG-1) to 877.36 (AMW-14S)
Present Hydraulic Gradient: 0.012 feet/foot between AMW-14S and SG-1
3.1.2 Historical Time Trend Graphs
The groundwater elevation for each gauging event from January 2014 to present was compared
to the total amount of precipitation received each month, as depicted in Appendix I. The total
monthly precipitation for July 2023 was 3.08 inches. The highest total monthly precipitation over
this evaluation period was 7.10 inches in December 2023. In general, a corresponding increase
in groundwater elevation is observed after higher total monthly precipitation amounts. Historical
monthly precipitation data from 1987 through March 2024 are shown in Appendix I.
3.1.3 FPZ-10 Historical LNAPL Time Trend Graph
The LNAPL and groundwater elevation time trend graph for monitoring well FPZ-10 is presented
in Appendix I. Monitoring well FPZ-10 is located approximately 40 feet upgradient of the barrier
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

wall. From July 1997 to January 2008, LNAPL amounts ranging from 0.01 feet to 2.27 feet had
been detected in FPZ-10. During the gauging event on July 30, 2015, LNAPL was detected at a
thickness of 0.17 feet. Prior to July 2015, LNAPL had not been detected since January 2008.
During this reporting period, 0.07 feet of LNAPL was detected in monitoring well FPZ-10 during
the December 6, 2023 event. During a follow-up field event on February 2, 2024, monitoring well
FPZ-10 was gauged and no LNAPL was detected. The December 2023 gauging event
represented the lowest groundwater elevation at FPZ-10 since December, 2017.
3.1.4 LNAPL Recovery Efforts
Per the approved free product recovery strategy, passive recovery via absorbent socks was
initiated in May 2016. Absorbent socks have been replaced as necessary during subsequent
gauging events. Currently, absorbent socks are installed in monitoring wells FPZ-10 and FPZ-
15, and will be routinely inspected and replaced as necessary.
3.1.5 Hydraulic Head Distribution
Liquid-level measurements were collected using an oil/water interface probe and measured to the
nearest 0.01-foot during the quarterly barrier wall gauging and semi-annual groundwater
monitoring and sampling events. LNAPL was detected in monitoring well FPZ-10 in December
2023. No other detections of free product were observed during this reporting period.
Tables 2 and 3 contain the recorded gauging data and groundwater elevations for on-site and
off-site wells, respectively. These liquid-level measurements were used to calculate the
groundwater elevation at each monitoring well location.
Groundwater elevations for the July 2023 groundwater monitoring and sampling event were
utilized to develop shallow, intermediate, deep, and bedrock groundwater elevation contour maps,
Figures 10 through 13. Additionally, Figure 14 includes the groundwater elevation contours for
the shallow zone from the December 2023 monitoring and sampling event. The maps depict the
interpreted groundwater flow at the site at the time of gauging during each event.
From the groundwater monitoring and sampling events conducted in July and December 2023,
groundwater flow in the shallow, intermediate, deep, and bedrock zones trended from northwest
on-site to northeast off-site.
In addition, calculations were performed to evaluate the head differences or vertical gradients
between adjacent vertical zones in each of the 22 well clusters across the site. These calculations
followed a center-of-screen to center-of-screen technique as described by the USEPA
(http://www3.epa.gov/ceampubl/learn2model/part-two/on-site/vgradient02.html). A summary of
these vertical gradients is provided in Table 7. The gradient value for each identified well is the
result of the head comparison/calculation to the well immediately above it in the same cluster.
This is discussed in greater detail in Section 4.5.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

3.1.6 On-Site Concentrations Over Time
An evaluation of the extent of on-site residual hydrocarbon impacts over time has been
undertaken to visually illustrate contaminant trends over time. Several groundwater monitoring
and sampling events from 2006 through 2023, and select contaminants of concern, were used to
evaluate the on-site extent and strength of the dissolved-phase hydrocarbon plume prior to,
during, and post-ISTR. Based on the most recent groundwater sampling event conducted in July
2023, data indicates that the dissolved-phase impacts to the shallow groundwater interval have
been greatly reduced on the TEPRI property. Despite this substantial reduction, exceedances of
the relevant state standards still exist in a number of on-site and off-site wells. The following map
is provided to illustrate the reduction of on-site shallow dissolved-phase impacts of BTEX over
time:

• Figure 15: Observed Total BTEX Groundwater Concentrations Over Time
3.1.7 July 2023 Isoconcentration Contours
Laboratory analytical results for the July 2023 sampling event are included in Appendix E.
Results were tabulated and screened against the NCDEQ NCAC 2L or IMAC standards where
applicable and are summarized on Tables 5 and 6. The following isoconcentration maps are
provided to illustrate the most recent comprehensive sampling results for the following site-
specific analytes:
• Figure 16: Groundwater Benzene Concentration Map – Shallow Wells – July 2023
• Figure 17: Groundwater Benzene Concentration Map – Int. Wells – July 2023
• Figure 18: Groundwater Benzene Concentration Map – Deep Wells – July 2023
• Figure 19: Groundwater Benzene Concentration Map – Bedrock Wells – July 2023
• Figure 20: Groundwater TBA Concentration Map – Shallow Wells – July 2023
• Figure 21: Groundwater TBA Concentration Map – Int. Wells – July 2023
• Figure 22: Groundwater TBA Concentration Map – Deep Wells – July 2023
• Figure 23: Groundwater TBA Concentration Map – Bedrock Wells – July 2023
3.1.8 December 2023/February 2024 Groundwater Analytical Results
Laboratory analytical results for the December 2023/February 2024 sampling event are included
in Appendix F. Results were tabulated and screened against the NCDEQ NCAC 2L or IMAC
standards where applicable and are summarized on Tables 5 and 6. Figure 24 provides the
results of site-specific analytes for the December 2023 groundwater sampling event.
3.1.9 Cross Sections
To better evaluate the volumetric distribution of dissolved impacts, a series of cross sections have
been prepared depicting the vertical extent of the monitoring well network (former and current).
Where applicable, temporal data have been shown to illustrate the changes in water quality over
time.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Cross sections were constructed along the seven transects (A-A’, B-B’, C-C’, D-D’, E-E’, F-F’, and
G-G’) as shown on Figure 25. Interpreted dissolved benzene contours are shown along each
transect on Figures 26 through 32, respectively, and dissolved TBA contours along each transect
are shown on Figures 33 through 39, respectively. Note that the cross sections were prepared
using data from the July 2023 comprehensive groundwater sampling event.
Note that in July 2018, the naming convention for the original transects included in prior reports
was revised to keep consistency with the names of the mass flux transects. Transects F-F’ and
G-G’ were not used in the mass flux evaluation as they are aligned parallel to groundwater flow.
Additionally, and per the August 15, 2019 Guilford County email correspondence, Transects F-F’
and G-G’ were revised to include additional wells to better evaluate plume behavior and/or remove
former/abandoned wells.
Furthermore, and to satisfy the requirements of the November 2022 NTCP, the naming
convention of the transects included in the NTCP differ from those used in Annual Monitoring
Reports and the mass flux analysis.
On-site, parallel with West Market Street is transect A-A’, which includes several of the monitoring
well clusters that were installed in late 2015 (Figures 26 and 33). TBA was detected above the
IMAC of 10 micrograms per liter (ug/L) in all zones extending into the upper portion of the fractured
bedrock zone (ranging from 89 ug/L in Z3-X80 to 100,000 ug/L in MW-B-B). Benzene was not
detected above the NCAC 2L of 1 ug/L in any monitoring well along this transect.
On-site, parallel with West Market Street, is transect B-B’, which includes several of the monitoring
well clusters that were installed in late 2015 (Figures 27 and 34). Benzene was detected above
the NCAC 2L of 1 ug/L in the shallow zone at the MW-E cluster (Z4-X47). Benzene was not
detected above the NCAC 2L of 1 ug/L in any of the intermediate or bedrock zones along this
transect. TBA was detected above the IMAC of 10 ug/L in the intermediate zone in the MW-H
cluster and in the deep zone in the MW-F and MW-G clusters, ranging from 29 ug/L in MW-H-I to
23,000 ug/L in MW-G-B. TBA was not detected in the shallow or bedrock zones.
Transect C-C’ is aligned just north of and parallel with West Market Street on the PTIA property.
This includes several of the monitoring well clusters that were installed in late 2016 (Figures 28
and 35). Benzene was detected above the NCAC 2L of 1 ug/L in the shallow, intermediate, and
deep zones along this transect (ranging from 2.4 ug/L in MW-K-I to 38 ug/L in SBMW-1R). TBA
was detected above the IMAC of 10 ug/L in the intermediate, deep, and bedrock zones,
centralized around the SBMW-2 cluster (ranging from 120 ug/L in PMW-L-I to 15,000 ug/L in
SBMW-2D and SBMW-2B). The SBMW-2 cluster is situated just north of West Market Street.
Transect D-D’ on the PTIA property includes several of the monitoring well clusters that were
installed in late 2016 (Figures 29 and 36). Benzene was detected above the NCAC 2L of 1 ug/L
in the shallow and intermediate zones along this transect (ranging from 4.9 ug/L in FMW-23R to
7,100 ug/L in FMW-24. Benzene was not detected in the PMW-N cluster. TBA was detected
above the IMAC of 10 ug/L in the shallow, intermediate, and deep zones (ranging from 280 ug/L
in PMW-N-D to 27,000 ug/L in DEM-MW6I). TBA was not detected in the bedrock zone.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Transect E-E’ on the PTIA property includes the three monitoring well clusters that were installed
in December 2017 and January 2018 (Figures 30 and 37). All monitoring wells along this transect
have either been non-detect for all dissolved petroleum compounds or have had minor detections
of 1,2,4-trimethylbenzene, EDB, chloroform, naphthalene, and/or toluene, below the NCAC 2L
standards.
As shown on transect F-F’ (Figures 31 and 38), neither benzene nor TBA were detected in the
furthest upgradient source zone well (Z1-X01). Benzene was detected above the NCAC 2L of 1
ug/L in the shallow zone along the northern edge of the former Terminal property at a
concentration of 3.2 ug/L in Z4-PZ04, and across West Market Street at a concentration of 14
ug/L in DEM-MW6R. TBA concentrations above the IMAC of 10 ug/L were observed across all
zones along this transect (ranging from 89 ug/L in Z3-X80 to 100,000 to ug/L in MW-B-B). At the
northeastern portion of the barrier wall along this transect, TBA was detected above the IMAC of
10 ug/L in the shallow zone at a concentration of 7,200 ug/L in FMW-21. TBA was not detected
in the MW-A cluster. Across the barrier wall along this transect is FPZ-5, in which sampling at
this location was suspended after the December 2019 event. TBA has been non-detect at FPZ-
5 since sampling began.
On-site to the west and running parallel with transect F-F’ is transect G-G’ (Figures 32 and 39).
This transect runs from the western portion of the site starting in Zone 4, across West Market
Street, to the monitoring well FPZ-12 cluster downgradient of the barrier wall. On-site, benzene
was detected above the NCAC 2L of 1 ug/L in the shallow zone in Z4-X63 and Z4-X47, at
concentrations of 1.1 ug/L and 8.2 ug/L, respectively. Across West Market Street, benzene was
detected above the NCAC 2L in the shallow zone in FMW-24, AMW-11S, and AMW-13S, at
concentrations of 7,100 ug/L, 2.6 ug/L, and 260 ug/L, respectively. Benzene was detected above
the NCAC 2L in the intermediate zone in FMW-24I at a concentration of 5.6 ug/L. Benzene was
not detected in the deep and bedrock zones along this transect. TBA concentrations above the
IMAC of 10 ug/L were observed across the intermediate, deep, and bedrock zones along this
transect, with concentrations ranging from 220 ug/L in PMW-O-I to 1,900 ug/L in AMW-13B.
3.1.10 Groundwater Sampling Results – On-Site Wells
The following section presents the water quality results from the July 2023 and December
2023/February 2024 groundwater sampling events of the on-site shallow extraction wells,
piezometers, and monitoring wells. The on-site shallow well network consists of 23 extraction
wells, seven piezometers, and 27 monitoring wells.
As previously discussed in Section 1.7.1, a groundwater optimization analysis was approved by
Guilford County in February 2022, and most on-site wells are only sampled on an annual basis.
There are a select number of on-site wells sampled semi-annually. During this reporting period,
the annual sampling event was completed in July 2023 and the semi-annual event in December
2023. One on-site well had insufficient water for sampling in December 2023; therefore, it was
subsequently sampled in February 2024.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Historical groundwater analytical results for all existing on-site wells are provided in Table 5.
Analytical results of site-specific VOCs in the existing on-site wells during the July 2023 and
December 2023/February 2024 groundwater sampling events were observed as follows:
• No VOC exceedances were observed in 10 extraction wells and 14 monitoring wells;
• One or more of the site-specific VOCs exceeded the NCAC 2L and/or IMAC standards
including 1,2-DCA (0.4 ug/L), 2-methylnaphthalene (30 ug/L), benzene (1 ug/L), MTBE
(20 ug/L); naphthalene (6 ug/L), and TBA (10 ug/L);
• Two NCAC 2L exceedances of EDB (0.02 ug/L) were observed; and
• No exceedances of NCAC 2L standards were observed for 1,2,4-trimethylbenzene (400
ug/L), 4-isopropyltoluene (25 ug/L), chloroform (70 ug/L), ethylbenzene (600 ug/L),
methylene chloride (5 ug/L), toluene (600 ug/L), or total xylenes (500ug/L).

Analytical data from the most recent groundwater sampling events conducted from 2015 through
February 2024, suggests that the core of on-site groundwater impacts have remained stable or
exhibited an overall decreasing trend. Based on the most recent comprehensive groundwater
sampling event conducted in July 2023, data indicates that the dissolved-phase impacts to the
shallow groundwater interval have been greatly reduced on the TEPRI property. Further, as is
apparent in subsequent discussions of both mass flux and well cluster head evaluations, in most
cases, the highest concentration of a given COC is not detected in the low head interval for the
specific well cluster the sample was collected. This finding is nearly universal for on-site wells
with the exception of monitoring wells MW-B-B and MW-H-B where the bedrock VOC impacts
coincide with the low head interval for these two well clusters only.
3.1.11 Groundwater Sampling Results – Off-Site Wells
The following section presents the water quality results from the July and December 2023
groundwater sampling events of the off-site monitoring network which consisted of 81 monitoring
wells.
As previously discussed in Section 1.7.1, a groundwater optimization analysis was approved by
Guilford County in February 2022, and most on-site wells are only sampled on an annual basis.
There are a select number of on-site wells sampled semi-annually. During this reporting period,
the annual sampling event was completed in July 2023 and the semi-annual event in December
2023.
Historical groundwater analytical results for all existing off-site wells are provided in Table 6.
Analytical results of site-specific VOCs in the existing off-site wells during the July and December
2023 sampling events were observed as follows:
• No VOC exceedances were observed in 30 off-site wells;
• One or more of the site-specific VOCs exceeded the NCAC 2L and/or IMAC standards for
1,2,4-trimethlybenzene (400 ug/L), 1,2-DCA (0.4 ug/L), 2-methylnaphthalene (30 ug/L),
benzene (1 ug/L), ethylbenzene (600 ug/L), MTBE (20 ug/L), naphthalene (6 ug/L), TBA
(10 ug/L), and total xylenes (500 ug/L);
• No NCAC 2L exceedances of EDB (0.02 ug/L) were observed; and
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

• No exceedances of NCAC 2L standards were observed for 4-isopropyltoluene (25 ug/L),
chloroform (70 ug/L), methylene chloride (5 ug/L), or toluene (600 ug/L).

Analytical data from groundwater sampling events conducted from 2015 through 2023, suggests
that the core of off-site groundwater impacts have overall remained stable or exhibited an overall
decreasing trend. Further, as is apparent in subsequent discussions of both mass flux and well
cluster head evaluations, in most cases, the highest concentration of a given COC is not detected
in the low head interval for the specific well cluster the sample was collected. This finding is nearly
universal for off-site wells with the exception of monitoring wells FMW-24, PMW-K-D, and PMW-
L-D, PMW-N-I, where shallow, deep, and/or intermediate VOC impacts coincide with the low head
interval for these well clusters.
Overall, dissolved phase COCs are shrinking in their extent on-site and stable off-site.
3.1.12 Geochemical Trends
A summary of the geochemical data collected at the site during the July 2023, December 2023
and February 2024 monitoring and sampling events is presented on Table 4. Field data collected
and analyzed include DO, pH, temperature, specific conductivity, and ORP. The geochemical
parameters change as groundwater moves into areas of the site where residual petroleum
impacts exist.

These parameters, when combined with analytical data for nitrate, manganese, ferrous iron,
sulfate, and methane can be used to evaluate the predominant terminal electron acceptor species
in supporting microbial activity to break down the contaminant plume. As microbes use available
DO in the aquifer to metabolize the hydrocarbon plume, they will sequentially begin to use less
thermodynamically favorable electron acceptors for respiration such as nitrate, manganese, ferric
iron, sulfate, and finally methane.

Figures 40 through 43 show the distribution of inorganic parameters that help define predominant
terminal electron acceptor (TEA) species and when evaluated over time, can determine the
effective monitored natural attenuation (MNA) process for each well for the July 2023 groundwater
monitoring and sampling event, and gives an indication of aquifer conditions which are
summarized below:

• Aerobic – On-site monitoring well Z1-X27; Off-site monitoring well AMW-16S
• Anaerobic Manganese/Iron Reducing – On-site monitoring wells Z1-X28 and Z4-X70;
Off-site monitoring wells FMW-23R, FMW-24, AMW-18S, DEM-MW6R, and SBMW-1R
• Anaerobic Iron Reducing – On-site monitoring well Z4-X89; Off-site monitoring well
AMW-13S
• Minimal COCs Reductive – Off-site monitoring well MW-B-B
• Minimal COCs Oxidative – On-site monitoring well Z2-X20; Off-site monitoring well
SBMW-2I

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

*Underlined monitoring wells exhibit detections and/or exceedances of site-specific VOC’s.
DO maps for shallow, intermediate, deep, and bedrock groundwater zones, to illustrate the most
recent data collected during the July 2023 sampling event, are included as Figures 44 through
47, respectively. Generally, DO levels decline in the former source zones to < 1 mg/L and spatially
correlate with the highest dissolved benzene concentrations. Aerobic bacteria will preferentially
utilize oxygen as the electron acceptor when metabolizing benzene or other hydrocarbon
compounds. When the available oxygen is depleted (DO drops below 1 mg/L), microbial colonies
that utilize other terminal electron acceptors will drive the natural biodegradation process. In
these cases, elements such as nitrate, sulfate, and ferric iron become electron acceptors. When
the available supply of these is exhausted, fermentation begins to generate methane. The
presence of detectable DO in all samples may also be attributed to the lengths of well screens
being longer than the vertical dimensions of the micro-environments.
ORP maps for shallow, intermediate, deep, and bedrock groundwater zones are provided as
Figures 48 through 51, respectively, to illustrate data collected during the July 2023 sampling
event. Background shallow groundwater exhibits strong positive values > 100 mv. In the source
zones, the ORP levels become negative, correlating spatially with the lowered values of DO and
higher benzene concentrations. Spatial variations in both DO and ORP levels are likely
attributable to the lengths of well screens straddling small-scale microbial environments with
different geochemical conditions. Taken together, the generalized patterns of DO and ORP still
correlate with dissolved benzene concentrations in and near known source areas which are
anoxic.
Groundwater temperature maps for shallow, intermediate, deep, and bedrock groundwater zones,
compiled from the July 2023 sampling event, are included as Figures 52 through 55, respectively.
On-site, the highest groundwater temperatures are observed throughout Zones 3 and 4 and
correlate with the most recent thermal remediation operations that ceased in October 2012.
These data demonstrate the slow restoration of thermal equilibrium.
Historically, all of the monitoring wells on the Greensboro site have supported ongoing anaerobic
reductive degradation. As the overall concentration of COCs on-site has decreased, and currently
many monitoring wells report no detected COC concentrations, the site conditions are slowly
equilibrating back to a natural, pre-release state. This pre-release state of aerobic geochemical
conditions is exemplified on-site by an increase in DO, ORP, nitrate, and sulfate concentrations,
with a corresponding decrease in dissolved iron and manganese as these metals are oxygenated
and precipitate out of solution.
In monitoring wells where there are detections of organic COCs, the geochemistry continues to
indicate anaerobic reductive degradation, exemplified by low or negative ORP, loss of nitrate,
increasing manganese and/or ferrous iron, and in highly reductive areas, a loss of sulfur with or
without methane production. Where there is no longer detectable COCs in an area, the previously
anaerobic areas are switching back to aerobic conditions. This is noted by indicating the change
in conditions in the monitoring well from anaerobic to aerobic (anaerobic/aerobic on the figures).
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409
Evaluation of these geochemical conditions over time indicates that many wells display conditions
that could be interpreted as marginally aerobic or marginally anaerobic at sequential monitoring
intervals or even at the same time. This suggests the groundwater system is both complex and
tipping towards equilibrium conditions where petroleum hydrocarbon compounds are absent from
the host of potential metabolic sources for indigenous microbial consortia. Where there is an
absence of detectable COCs, this distinction may not be critical to understanding the MNA
process for the site. However, it is evident from a number of lines of evidence, including long-
term changes in geochemistry and comparison of COC mass flux from cross-gradient transects,
that groundwater quality continues to demonstrate improvement relative to persistence and extent
of dissolved phase COCs.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409
4 Mass Flux Analysis
4.1 Mass Flux Background and Concepts
It has long been recognized that contaminant transport through complex aquifer systems can be
a challenge to understand and quantify. Numerous case studies have reported that as much as
90% of contaminant migration occurs through as little as 10% of the overall affected aquifer
volume. This migration pattern is driven by the large range in hydraulic conductivity found
throughout most aquifer systems. Contaminants can be “stored” in low conductivity or poorly
interconnected aquifer media (moving primarily via diffusive chemical flow) and can migrate
rapidly through high conductivity channels or zones (via adjective groundwater flow). This natural
range of physical properties and resultant contaminant transport behavior has driven complex
environmental contamination projects towards high-resolution site characterization (HRSC)
techniques, which the USEPA, the ITRC, and others have espoused as best practices for complex
site investigation and development of effective CSMs.
ITRC published guidance on “Use and Measurement of Mass Flux and Mass Discharge” (ITRC,
2010) that offers several means to measure mass flux and incorporate the concepts and data into
effective CSMs. Some of the benefits of employing mass flux concepts for site management as
articulated in the ITRC guidance include:
•“Mass flux is now being used more frequently to characterize and monitor groundwater
contamination (USEPA 2003) due to a growing recognition that mass flux data can provide
a more complete measure of the exposure posed by the contaminants than static point
concentration estimates alone (Einarson and Mackay 2001; Buscheck, Nijhawan, and
O’Reilly 2003).”
•“Mass flux estimates can better characterize a contaminated site than typical monitoring
networks (Feenstra, Cherry, and Parker 1996).”
•“A mass flux calculation requires measurement of the variability in concentrations and
velocities within a plane of the plume and therefore is based on a more thorough site
characterization. Additionally, mass flux values at different times and places along a plume
show the combined impact of all of the physical, chemical, and biological processes acting
on the contaminants.”
The site has undergone extensive remediation over the past 15-plus years: specifically, the 2007
to 2012 electrical resistive heating program. Thus, as a function of this source removal, it may
not fit neatly into the “source-pathway-receptor” framework used by EPA and ITRC to embody
the benefits of employing mass flux techniques. Nonetheless, given significant concentrations of
residual MTBE and TBA compounds, application of mass flux concepts can offer improved
understanding of subsurface contaminant behavior. This improved understanding in turn, should
allow for more focused decision making and development of a remedial program aligned with site
risk and contaminant transport attributes.
Given the large number of existing groundwater monitoring wells at the site and good spatial
delineation of dissolved-phase petroleum hydrocarbon compounds that exceed applicable
concentration standards, a transect-based method was selected to evaluate and quantify
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

contaminant mass flux across the site. This method provides the greatest data density and
degree of confidence in the outcome.
4.2 Mass Flux Application
4.2.1 Geology and Contaminant Behavior
Historical site investigation work (Arcadis, 2004) has shown the former Fina terminal and
downgradient off-site PTIA property to be underlain by deeply weathered saprolite derived from
the underlying Cambrian-aged, metamorphosed diorite of the Carolina Slate Belt (Piedmont
Physiographic Province). Depths to competent, crystalline bedrock range from approximately 55
to 100 feet bgs across the site. Groundwater generally flows from south to north towards the
PTIA property and thence to an unnamed tributary of Horsepen Creek. Depths to groundwater
typically range from five to 25 feet bgs thereby indicating a thick saturated water table residing
within the saprolite over the top of rock for the entire area.
Historical in-situ thermal remediation was effective in the elimination of LNAPL (source) and
related dissolved petroleum compound constituents in the groundwater system, however, follow-
up groundwater quality investigations conducted both on-site and at the PTIA property indicated
that several petroleum compounds can still be detected at concentrations above applicable IMAC
and/or NCAC 2L standards. This finding, and a small number of high-concentration TBA
detections in the bedrock aquifer prompted a 2015 re-evaluation of groundwater quality using a
mass flux approach to better understand contaminant migration potential across the site.
4.2.2 Cluster Well Installation
To accomplish this objective, a series of 18 additional well clusters comprised of shallow (water
table), intermediate, deep, and bedrock wells were installed between 2015 and 2018. Half of
these clusters were installed on the TEPRI property and half off-site on the PTIA property. In
general, cluster well installation was completed as follows:
1. A deep boring was advanced via sonic drilling techniques to confidently identify the top of
bedrock and provide quality soil cores for identification and description.
2. Borings were advanced into the bedrock aquifer a minimum depth of 15 feet or until
evidence of some water production was noted.
3. A water table well, (denoted as “Shallow” in report figures and data tables), was installed
if a shallow well did not already exist in close proximity to a corresponding deep well
cluster. This was done for the furthest downgradient well clusters PMW-P, PMW-Q, and
PMW-R only. The existing water table wells are generally screened from depths of five to
20 feet bgs.
4. An “Intermediate” saprolite zone well was installed - typically screened with 10-foot lengths
in the 30 to 50 feet bgs depth range.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

5. A “Deep” saprolite zone well was installed such that the bottom of the well screen sits atop
bedrock. These deep wells are typically completed with 10-foot screen intervals in the 50
to 90 feet bgs depth range.
6. A “Bedrock” zone well was installed – constructed with open-well completion from about
15 feet below the top of rock surface to a zone making water. Open intervals for the 18
bedrock wells range from 10 to 47 feet in length, average 15 feet in length and are found
between 74 and 157 feet bgs.
These 18 well clusters, in addition to three existing well clusters, were arranged into five linear
transects aligned approximately perpendicular to established groundwater flow, as per ITRC
guidance. These transects are identified as A-A’, B-B’, C-C’, D-D’, and E-E’ moving from south
to north across the site. The wells comprising each transect are shown in the Mass Flux Transect
Locations Map and are also identified explicitly in the Mass Flux Raw Data Table (Appendix A).
Transect E-E’, located farthest downgradient and north of the PTIA retention pond, have either
been non-detect for all dissolved petroleum compounds or have had minor and/or anomalous
detections of 1,2,4-trimethylbenzene, EDB, chloroform, naphthalene, and/or toluene, below the
NCAC 2L; therefore, no mass flux calculations were performed for those wells or along that
transect.
4.3 Mass Flux Calculations and Groundwater Gradients
The 2018 Annual Monitoring Report / Comprehensive Site Assessment Report (GES, May 2019),
submitted to Guilford County and the NCDEQ, provides a detailed description of the cell set-up
and calculations used to determine the mass flux for a given contaminant per transect cell.
Groundwater gradients were determined for each of the four zones based upon well gauging data
from July 2023. The horizontal groundwater elevation gradients in all four hydraulic zones show
little difference, returning values of 0.015, 0.012, 0.013 and 0.013 feet/foot for the shallow,
intermediate, deep and bedrock zones, respectively. The July 2023 groundwater analysis results
were used to provide contaminant mass input for the flux calculations. Where a non-detect result
was returned, half of the method detection limit was substituted to achieve a flux value. Cells
highlighted in green on the Flux Calcs spreadsheets of Appendix A, indicate where this half-
detection value technique was employed. The July 2023 groundwater analytical results are
summarized in the mass flux tables in Appendix A and also on Tables 5 and 6.
4.4 Findings
The Flux Calcs spreadsheets in Appendix A provide summaries of the input data and mass flux
output for each of the 62 cells for the compounds TBA, MTBE, and 1,2-DCA, respectively. The
estimated mass of each compound that moves through each of the four transects aligned
perpendicular to groundwater flow is provided in the Appendix A worksheets and is summarized
below for the July 2023 sampling event. The calculation outputs are expressed in grams per day
(g/day) through each cell and further summed by transect. An interpretive summary of the findings
is provided below by analyte.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Transect-to-transect mass changes: TBA (g/day) Moving through A: 292.212 Change A to B: 58.333 20% increase Moving through B: 350.545 Change B to C: 621.133 177% increase
Moving through C: 971.68 Change C to D: -839.335 -86% decrease Moving through D: 132.344 leaving system
Transect-to-transect mass changes: MTBE (g/day)
Moving through A: 0.021 Change A to B: 0.0705 337% increase
Moving through B: 0.0915 Change B to C: 0.147 161% increase
Moving through C: 0.238 Change C to D: -0.194 -82% decrease
Moving through D: 0.0441 leaving system

Transect-to-transect mass changes: 1,2 DCA (g/day)
Moving through A: 0.0002 Change A to B: 0.0023 1209% increase
Moving through B: 0.0025 Change B to C: 0.001428 566% increase
Moving through C: 0.0168 Change C to D: -0.0019 -11% decrease
Moving through D: 0.0149 leaving system

4.4.1 TBA
• Some discernable level of TBA flux can be calculated for 55 of the 62 total cells in all four
transects or 89% of the total cells analyzed. However, most of these determinations were
derived from non-detect lab results (31 of the 55). Further, less than half (26 of the 62
cells or 42%) yielded a TBA flux in excess of 0.1 g/day. The majority of TBA flux across
the site (86% of the sum of all four transects) occurred through only 3 of the 62 cells which
represent only 4.8% of the aggregate transect area. Of these three high flux zones, only
one coincided with the low head feature for that well cluster – the on-site bedrock well B.
• Flux from on-site sources (transects A-A’ & B-B’) are calculated at 292.2 and 350.6 g/day,
respectively, indicating a remaining on-site source for TBA. These values are similar in
magnitude to those calculated since this mass flux initiative was undertaken in December
2017 and suggest that the system is geochemically stable.
• Transect E-E’ with 12 wells located north of the pond on PTIA property, returned all non-
detect results for all constituents analyzed in groundwater samples, suggesting that
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

complete compound degradation is realized within this area of the site. No flux
calculations were undertaken for any of these 12 “clean” wells.
• No significant change in TBA flux across the D-D’ transect is noted since Dec 2017; this
value has ranged from 20.1 to 146.5 g/day, indicting MNA is capable of effectively
mitigating the contaminant flux from residual source areas upgradient of the D-D’ transect
area.
• TBA flux across transect C-C’ is 971.7 g/day, of which 966.8 g/day (99%) occurs in the
bedrock portion of the SBMW-2 cluster. Thus, one of 16 cells across transect C-C’ is
responsible for nearly all of the net TBA transport across this integrated aquifer cross
section. This SBMW-2 bedrock cell is not the low-head interval of that well cluster, further
diminishing the potential for TBA transport out of the system from this location.
• A TBA flux reduction of 86% is calculated from transect C-C’ to transect D-D’ on the PTIA
property, consistent with previous calculations and indicative of intrinsic remediation
effectiveness.
• Overall TBA flux values and transect to transect relationships have remained relatively
consistent across the site since December 2017 and do not demonstrate evidence of
migration outside of the groundwater system defined by the local watershed.
4.4.2 MTBE
• Some MTBE flux was measured in 22 of 62 cells total (35%). Only 1 of 62 cells
demonstrated MTBE flux in excess of 0.1 g/day at 0.2007 g/day.
• The observation of small MTBE flux values is partially associated with the amount of non-
detect results obtained for MTBE (41 of 62 wells returned non-detect results).
• The magnitude of MTBE flux is quite low across all transects with a system-wide total of
only 0.40 g/day. Also, as noted, this “system-wide” total is not a true sum value as
changes in MTBE concentration from transect to transect are clearly evident.
• As was seen in prior years (but not in June 2022) with TBA, transect C-C’ yielded the
highest flux across the aquifer flow field and a reduction of 82% was calculated from
transect C-C’ to transect D-D’, again indicating some residual source beneath West
Market Street as well as robust monitored natural attenuation activity downgradient of
West Market Street.
• Overall, MTBE flux does not appear to be a concern at this site and there is no evidence
of MTBE migration outside of the groundwater system defined by the local watershed.
4.4.3 1,2-DCA
• 19 of the 62 cells analyzed across all four transects (31%) yielded evidence of some
detectable 1,2-DCA flux. No cells yielded a flux value in excess of 0.1 g/day.
• The magnitude of 1,2-DCA flux is quite low across all transects with a total of only 0.034
g/day system-wide.
• 11 of the total flux detections (58%) are deep or bedrock zones, and nearly half (5 of 11)
align with low head flow zones. Similarly, 15 of the 19 total cells (79%) where some 1,2-
DCA flux was calculated are located in the off-site transects C-C’ and D-D’.
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409
•Relative groundwater head relationships combined with 1,2-DCA mass flux results
suggest that this compound may be from a regional source as detectable mass flux is
calculated in the low-head interval in 5 of 16 well clusters, with all 5 in the off-site well
clusters.
•Measurable 1,2-DCA mass flux occurred in 13% of on-site cells and 50% of off-site cells.
•1,2 DCA flux from the former TEPRI site equals 0.003 g/day across both the A-A’ and B-
B’ transects combined. This value increased one order of magnitude for the C-C’ and D-
D’ transects to 0.03 g/day, but still remains quite low and as noted above, detectable 1,2
DCA flux is found in 5 of 9 off-site low head zones – supporting the concept of a separate
source and/or more regional presence.
Overall, as noted previously, the source removal remediation performed from 2007-2012 on the
TEPRI property has resulted in atypical source-pathway-receptor relationships for the site. From
a mass flux standpoint, this has yielded low VOC flux values from on-site transects A-A’ and B-B’
and the greatest mass flux across transect C-C’ with a recognized decline in flux for TBA and
MTBE from transects C-C’ to D-D’ indicative of robust natural degradation (monitored natural
attenuation) processes. This is further supported by the fact that the entirety of transect E-E’ (12
discrete sampling locations in all four aquifer zones) have either been non-detect for all dissolved
petroleum compounds or have had minor and/or anomalous detections of EDB, isobutylene,
and/or toluene. Thus, all detectable contaminants passing through the D-D’ transect have been
fully degraded or have by-passed the E-E’ transect wells. Further, there are no detections of any
monitored compounds in surface water samples collected to date.
4.5 Groundwater Head Evaluation
Evaluation of synoptic groundwater head data collected from all cluster wells in July 2023,
suggests that the aggregate groundwater flow system at the Greensboro site behaves as an
integrated continuum through the saprolite material and shows evidence of both downward flow
and upward flow (regional groundwater discharge) through the bedrock aquifer. Also as
described in Section 3.2.1, vertical gradients were evaluated for vertically adjacent well couplets
according to the center-point to center-point method presented in EPA Region 4 modeling
guidance. A total of 64 vertical gradient values were obtained from 22 well clusters (of which 20
contain a bedrock component) across the site. These data are summarized in Table 7. The
calculated vertical gradients from cell to cell are primarily low, ranging from under 0.1% with only
8 of 64 values above 10%. Low head zones per well cluster were also identified using these July
2023 gauging data and are shown both in the mass flux calculations and mass flux cross sections
in Appendix A.
The mass flux data summary and calculations are presented in Appendix A. In addition to
determining a mass value for selected compound migration through the defined cells and
transects, this evaluation also considers groundwater head and resultant flow behavior from
transect to transect. Vertical groundwater gradients are typically downward into the deep saprolite
and bedrock zones on-site. The bedrock zone represents the low head component of six of nine
on-site well clusters analyzed, but only three of 13 off-site clusters analyzed. Two of the 13 off-
site well clusters do not have a bedrock well component. Upward flow from the bedrock aquifer
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409
is prevalent on the PTIA property where the deep saprolite zone represents the low head interval
in seven of 13 well clusters analyzed. This finding fits with a regional groundwater flow model
where discharge to surface water is likely to occur to the north at Horsepen Creek and is
supported by a simple analysis of groundwater heads versus surface water elevations across the
local site area. GES will continue to track relative head values for each hydraulic zone and the
system as a whole. This will include collecting surface water elevations during monitoring events.
The identification of mass flux combined with low head will better inform the site CSM and
understanding of potential contaminant migration pathways.
4.6 Discussion
This on-going evaluation of mass flux and discharge at the site continues to offer valuable insight
into groundwater dynamics and contaminant fate and transport. By evaluating mass discharge
at the site, and thereby accounting for the combined effects of concentration and groundwater
velocity on contaminant movement, we have a more complete understanding of the site, which
will inform decision making. This evaluation will continue for TBA as the primary COC; however,
the mass flux values for MTBE and 1,2-DCA are very low and additional evaluation of mass flux
for these contaminants provide little value in the overall CSM understanding. For example,
contaminant concentrations alone cannot provide a complete picture of the processes governing
plume behavior because groundwater velocity (which varies across a site) is an integral
component of plume behavior. However, incorporating mass discharge and hydraulic head
information into the CSM improves our understanding of plume behavior, identifies high-priority
layers in dynamic aquifer systems, and provides a better analysis of natural attenuation rates
(because transect data are less susceptible to temporal variations in flow direction and strength).
Additionally, the results produced thus far point to both stability and natural attenuation of the
selected dissolved organic compounds across the site as a whole and is further corroborated by
both organic and inorganic chemical data over time. Mass flux and discharge estimates are
valuable tools for contaminated site management.
_____________________________________________________________
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

5 Discussion
5.1 Summary
As outlined in Section 1.6 of this report, extensive remedial efforts were undertaken by TEPRI
from January 1997 through October 2012. The goal of these source removal actions was to
remove over 70% of the subsurface petroleum hydrocarbon mass such that the remaining
residual mass would subsequently bioattenuate; this goal was achieved. These remedial efforts
significantly reduced concentrations of COCs in groundwater both across the site, as well as at
downgradient locations off-site. Additionally, LNAPL has not been detected in any on-site well
since April 2013.
There have been considerable reductions in dissolved benzene concentrations since ISTR was
initiated in 2007 – in most cases contaminant concentrations decreased by at least three orders
of magnitude in on-site wells and at least two orders of magnitude in off-site wells. Trends are
less dramatic for TBA, as described below. TBA is typically derived from gasoline sources either
as an oxygenate additive from 1979 to 2005, as an impurity in the additive MTBE, or as a
breakdown product of the biodegradation of MTBE. MTBE has been historically detected at low
to moderate levels in groundwater at the site – primarily prior to the in situ thermal remediation
program undertaken by TEPRI.
The presence of MTBE in groundwater is often associated with the presence of TBA. The source
of TBA at MTBE-contaminated sites is difficult to identify. TBA has been shown in laboratory
studies to be a product of MTBE biodegradation under both aerobic and anaerobic conditions.
Studies have shown that MTBE can be transformed abiotically to TBA under methanogenic
conditions. Research suggests that TBA can be generated by in-situ microbial breakdown of
isobutene – another gasoline compound (API, 2012b). While MTBE is highly soluble in water,
TBA is completely miscible and has a low affinity for gasoline. Therefore, minute amounts of TBA
in the MTBE blended gasoline as an impurity can result in high aqueous TBA concentrations when
MTBE oxygenated gasoline comes in contact with water. Thus, there are a number of potential
sources and hydrocarbon breakdown mechanisms that can explain the presence of TBA – either
as a primary or secondary (intermediate) product of a hydrocarbon release.
Other potential sources of TBA from MTBE-containing gasoline (API, 2012b), include:
• TBA as an oxygenate: Beginning in 1979 and into the early 1980’s, and in a small
proportion of the gasoline supply, TBA itself was sometimes added to gasoline as an
octane‐enhancer, with methanol as a cosolvent.
• TBA in fuel grade ether oxygenates: As a byproduct of the manufacturing process, low
concentrations of TBA (~2 wt%) were common in the “fuel grade” ether oxygenates such
as MTBE.
• TBA as a product of ether oxygenate biodegradation: TBA is well‐established as a product
of MTBE biodegradation processes catalyzed by microorganisms in the environment.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

There are significant differences in the physical/chemical properties of MTBE and TBA. The loss
of the more volatile VOC mass, including MTBE, results in the redistribution of the remaining mass
between phases in the unsaturated zone, including an increased TBA mole fraction in any
nonaqueous phase gasoline, an apparent enrichment of TBA mass due to increased aqueous
TBA concentrations, and aqueous TBA/MTBE concentration ratios that increase with time. Thus,
volatilization may play a role in, or dominate, TBA and MTBE concentration trends observed at
spill sites with MTBE. Given its high volatility, MTBE is relatively quickly depleted from the system,
reducing its concentration in the NAPL and pore water. In contrast, TBA is depleted very slowly,
and therefore persists in the pore water (Eweis, 2007). The persistence of TBA relative to MTBE
may explain the TBA concentrations being observed at the site. However, post-ISTR monitoring
data for the site as a whole does point out reductions in dissolved MTBE ahead of TBA,
suggesting that the MNA process is effectively reducing concentrations of both compounds and
likely MTBE preferentially over TBA. Data collected thus far from the deep saprolite and bedrock
aquifer zones suggest that the groundwater system at the site is vertically integrated through the
saprolite zone (illustrated by minimal vertical gradients) but demonstrates higher head and
upward vertical gradients in the bedrock zone, primarily in the off-site well clusters – possibly
existing under confined or semi-confined conditions. Data and field observations collected thus
far also demonstrate limited hydraulic capacity or conductivity in either the saprolite or bedrock
aquifers. No evidence of high-yield or active flow zones in either setting was noted during
geophysical investigations, well installation field observations or well development, purging, slug
testing or sampling activities. The detection of elevated dissolved concentrations of certain
COCs, particularly TBA, may be a function of limited groundwater flux and a reduced rate of
natural biodegradation – the latter being a reasonable expectation following extensive heating of
the subsurface where indigenous microbial populations would be largely sterilized. It is expected
that re-establishment of microbial colonies would ensue after post-ISTR temperature equilibration
and reintroduction of indigenous microbial communities through groundwater flux.
Analytical data from semi-annual comprehensive groundwater monitoring and sampling events
suggest the concentration of primary constituents of concern dissolved in groundwater is either
decreasing or generally stable. The plume dimensions for some COCs (i.e., BTEX, MTBE, etc.)
appears to be shrinking; and in the case of TBA, the larger plume shows an overall decrease in
concentration compared with the 2015 and 2016 data.
Additional data collected from surface water sampling at the off-site stream/pond interface,
indicate the surface water is also integrated with the local, shallow groundwater system and is not
impacted by any of the site-specific VOCs.
5.2 Conceptual Site Model
During 2007 through 2012, aggressive thermal remediation in the former AST area removed
significant quantities of LNAPL mass, reducing the primary source area for groundwater
contaminants. The most recent LNAPL detection on-site was in April 2013. The remedial actions
also significantly reduced the mass flux of COCs leaving the primary source area and moving off-
site. Concentrations of the primary risk driver benzene in the source area, which previously
exceeded 10,000 ug/L, reduced three to four orders of magnitude. The primary risk driver
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

changed to TBA, having concentrations that were generally reduced in groundwater samples from
the source area. The off-site area became the focus of investigations after 2012 when the
updated CSM yielded data gaps related to groundwater flow patterns and potential COC migration
to surface waters, along with the occasional LNAPL observations in the vicinity of the hydrocarbon
interceptor wall. Further investigations to improve the CSM relative to off-site groundwater and
LNAPL conditions were needed. Our current understanding is discussed below.
5.2.1 Groundwater Concentration Trends and Mass Flux Evaluation
During this reporting period, two groundwater monitoring and sampling events were conducted at
the site. Laboratory analytical results show concentrations of site-specific VOCs, including 1,2,4-
trimethylbenzene, 1,2-dichloroethane, 2-methylnaphthalene, 4-isopropyltoluene, benzene,
ethylbenzene, xylenes, MTBE, TBA, and naphthalene, which exceed the regulatory standard.
Groundwater samples collected from the three most downgradient well clusters that were installed
in December 2017 and comprise the E-E’ transect presented in Figures 30 and 37, have either
been non-detect or have had minor and/or anomalous detections of 1,2,4-trimethylbenzene, EDB,
chloroform, isobutylene, naphthalene, and/or toluene.
On-site, TBA was detected above the IMAC standard in 16 out of 53 wells sampled, including
detections in all four hydraulic zones. Dissolved TBA is adequately defined across the site
especially given the identification of upward groundwater flow from the bedrock zone on the PTIA
property. As noted in earlier analysis, there is strong evidence of robust and effective MNA activity
that, coupled with upward hydraulic gradients, would likely preclude dissolved TBA migration
beyond the local watershed.
Benzene was detected mostly in the shallow wells and appears to be attenuating either by
adsorption to soil particles or undergoing microbial degradation prior to downward groundwater
migration (or both). Overall, benzene continued to show an overall stable or decreasing trend in
comparison with historical data.
In off-site wells, an overall stable trend of benzene and TBA was observed. Off-site, TBA was
detected above the IMAC standard in all zones within the historical plume footprint. The mass of
the TBA plume is centered on the on-site monitoring well MW-B cluster to near the monitoring
well DEM-MW6 cluster off-site to the northeast. Downgradient, the TBA plume extends off-site
to just beyond the barrier wall in the intermediate and deep wells in the MW-O cluster. The
horizontal widening of the TBA plume as it moves off-site reflects the compound’s total miscibility
in water and the complicated groundwater flow of the area.
The high concentrations of benzene detected in wells FMW-23R, FMW-24, AMW-11S, AMW-
13S, and AMW-18S, suggest another source or a large section of the plume went untreated during
the thermal remedial event. The area to the west of off-site well FMW-24, is delineated with the
historical data from former well FMW-19 prior to its abandonment in December 2018.
TBA is reasonably well delineated in the shallow zone with the possible exception of one area off-
site near FMW-21 to the east. On-site in the intermediate, deep, and bedrock zones, TBA is
delineated to the east and south, but not to the west. Off-site in the intermediate, deep, and
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

bedrock zones, TBA is not delineated to the west and/or east; however, TBA is delineated to the
north with the three new well clusters downgradient of the pond on the PTIA property.
5.2.2 Groundwater Flow Patterns
The groundwater flow direction at the site throughout all hydraulic zones is generally in a northerly
direction; however, slight fluctuations between the northwest and northeast have been observed
since the December 2015 monitoring and sampling event. A localized groundwater mound and
flow deflection exists around the barrier wall on the PTIA property. The interpreted flow directions
and gradients from the gauging events are consistent with historical interpretations.
Monitoring of water levels in wells completed to different depths in the saprolite and bedrock
zones has provided data for inferring hydraulic gradients in three dimensions. While vertical
gradients are more consistently downward in the saprolite zone of the former terminal area, they
are consistently upward from the bedrock to saprolite zones off-site on the PTIA property.
Incorporation of surface water head data support this regional flow model where some component
of shallow groundwater will discharge to the pond and adjacent surface streams on the PTIA
property and deeper groundwater may feed streams such as Horsepen Creek farther north. These
same hydraulic relationships were referenced in previous CSM versions and flow models
prepared for this site.
5.2.3 LNAPL Monitoring and Recoverability
From May 2017 through April 2024, LNAPL in the vicinity of the barrier wall was monitored via
quarterly gauging events of select monitoring wells and comprehensive groundwater monitoring
and sampling events. These results are summarized in Section 3.1.1 of this report. During the
gauging event on July 30, 2015, LNAPL was detected in FPZ-10 at a thickness of 0.17 feet. Prior
to July 2015, LNAPL had not been detected since January 2008. During the December 6, 2023
gauging event, 0.07 feet of LNAPL was detected in monitoring well FPZ-10. During a follow-up
field event on February 2, 2024, monitoring well FPZ-10 was gauged and no LNAPL was detected.
Prior to the December 2023 event, LNAPL was not observed at the site since 2018.
As previously stated, given the low transmissivity values, the LNAPL in the barrier wall wells is
not considered recoverable and active LNAPL recovery is not believed to be a beneficial
undertaking. Per the approved free product recovery strategy, passive recovery via absorbent
socks installed in wells FPZ-10 and FPZ-15 was initiated in May 2016. Absorbent socks were
replaced, as needed, during the routine events.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

6 Conclusions & Recommendations
Given the large dissolved-phase plume and inherent geologic complexities at the site, the
evaluation of mass flux and mass discharge has been adopted to assess contaminant fate and
transport and manage risk. Mass flux is being measured using transects perpendicular to
groundwater flow to assess contaminant discharge and plume attenuation rates and devise an
appropriate long-term management strategy. Dissolved TBA occurs in groundwater at the site
above applicable standards and monitored natural attenuation is likely to have a key role in the
overall strategy for risk management. This approach to focus on groundwater quality and
attendant mass flux conditions is appropriate given recent investigative findings whereby soil
quality meets both NCDEQ Industrial/Commercial and Residential cleanup standards for all
compounds analyzed site-wide.
With the large number of existing groundwater monitoring wells at the site and good spatial
delineation of dissolved-phase petroleum hydrocarbon compounds that exceed applicable
concentration standards, a transect-based method was used to evaluate and quantify
contaminant mass flux across the site. On-site transects (A-A’ and B-B’) yielded low flux values
for MTBE and 1,2 DCA, but the highest TBA flux. The greatest mass flux for both TBA and MTBE
is observed in the off-site transect just across West Market Street on the PTIA property (transect
C-C’). A one order of magnitude increase in mass flux was calculated from the B-B’ to the C-C’
transects for MTBE and an increase of 177% was determined for TBA across this same area. A
decline of flux of 86% and 82% is observed from transects C-C’ to D-D’ for the volatile compounds
TBA and MTBE, respectively, indicating very effective monitored natural attenuation processes.
This is also evident by the fact that the entirety of transect E-E’ (12 monitoring wells in all four
aquifer zones installed in December 2017 and January 2018) has yielded non-detect results for
all dissolved petroleum compounds or have had minor and/or anomalous detections of 1,2,4-
trimethylbenzene, EDB, chloroform, isobutylene, naphthalene, and/or toluene. Thus, all
detectable contaminants passing through the D-D’ transect have been fully degraded or have by-
passed the E-E’ transect wells. The relative concentrations of 1,2 DCA appear to be driven by
regional hydraulics as flux values are consistently low, but detectable in nearly all low head zones
of all four transects analyzed.
The mass flux evaluation offers exceptional insight into groundwater dynamics and contaminant
fate and transport for the site. Evaluating mass discharge and thereby accounting for the
combined effects of concentration and groundwater velocity on contaminant movement promotes
a more complete understanding of the site. This approach, combined with a corresponding
evaluation of relative hydraulic heads, will be continued to evaluate plume dynamics, potential
contaminant transport avenues and natural attenuation. This evaluation will continue for TBA as
the primary COC; however, the mass flux values for MTBE and 1,2-DCA are very low and
additional evaluation of mass flux for these contaminants provide little value in the overall CSM
understanding. Additionally, the results produced thus far point to stability of the selected
dissolved organic compounds across the site as a whole.
In keeping with this approach, RETIA proposes the following steps to define the near-term path
forward for the site over the next year:
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

• Continue to monitor liquid levels, on a quarterly basis, at the wells near the barrier wall
located on the PTIA property to confirm that LNAPL has been fully remediated;
• Continue to gather surface water elevations during groundwater monitoring events, to
confirm no changes to groundwater-surface water interactions;
• The current well network comprises 136 wells, of which 115 wells will continue to be
sampled on an annual basis in June (per the approved Groundwater Monitoring Plan
Optimization Analysis report. Additionally, 8 of these 115 wells will be sampled on a
semi-annual basis in December. GES and RETIA will continue to evaluate the
groundwater monitoring program and make recommendations to further reduce the
network, eliminating wells that provide little value to the overall understanding of the
CSM;
• Eliminate MTBE and 1,2-DCA from future mass flux evaluations;
• GES and RETIA are currently conducting an evaluation of the effectiveness of an EISB
remedy at locations where mass flux calculations suggest there may be VOC
transport. An EISB Evaluation Work Plan was submitted by GES on behalf of RETIA,
to the NCDEQ and Guilford County on January 13, 2023 (later revised on January 25,
2023) to outline work to be completed. Data generated from the studies are used to
directly support the presence of natural attenuation processes at the site and the ability
to enhance the degradation with amendments. The data were collected in 2023 and
are currently being evaluated to definitively determine if enhancement of the naturally
occurring biodegradation process will significantly increase degradation of site
contaminants. An EISB Evaluation Report will be submitted to the NCDEQ and
Guilford County under a standalone cover; and
• Continue to provide annual update reports to stakeholders including NCDEQ and
Guilford County.
The collection and evaluation of these additional data will continue to support formulation of a
long-term risk management strategy for the site. The data indicate that MNA is an effective
remedy for this site given the scope of historical remediation, current site attributes, in particular
the lack of LNAPL, and potential receptors.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

References
API, 2012b. Tertiary Butyl Alcohol (TBA) Biodegradation: Some Frequently Asked Questions,
Technical Bulletin No. 26, 6 pp.
Arcadis, 1998. Assessment of Active On-Site and Off-Site Remediation Systems and
Contributions from Multiple Off-Site Source Areas Report, 70 pp, with appendices.
Arcadis, 2005. 2004 Comprehensive Site Assessment Report – Phase III. 614 pp, with
appendices.
Buscheck T. E., N. Nijhawan, and K. T. O’Reilly. 2003. “Mass Flux Estimates to Assist
Remediation Decision-Making,” in Proceedings, 7th International Symposium on In Situ and On-
Site Bioremediation, Orlando, Fla., June 2–5. Columbus, Ohio: Battelle.
Einarson, M. D., and D. M. Mackay. 2001. “Predicting the Impacts of Groundwater
Contamination,” Environmental Science and Technology 35(3): 66A–73A.
Eweis, Juana, & E.M Labolle (2007). Role of Volatilization in Changing TBA and MTBE
Concentrations at MTBE-Contaminated Sites. Environmental Science & Technology, 41 (19),
6822-6827
Feenstra, S., J. A Cherry, and B. L. Parker. 1996. “Conceptual Models for the Behavior of DNAPLs
in the Subsurface,” Chap. 2 in Dense Chlorinated Solvents and Other DNAPLs in Groundwater,
J. F. Pankow and J. A. Cherry, eds. Portland, Ore.: Waterloo Press.
GES, 2005. Source Area Removal Workplan. 905 pp, with appendices.
GES, 2017. 2017 Annual Monitoring Report / Comprehensive Site Assessment Report. 2,345 pp,
with appendices.
GES, 2019. Annual Monitoring Report / Comprehensive Site Assessment Report. 2,120 pp, with
appendices.
ITRC, 2010. Use and Measurement of Mass Flux and Mass Discharge, prepared by the Interstate
Technology and Regulatory Council LNAPL team, 444 No. Capital St., Suite 445, Washington, D.
C. 20001, 103 pp, with appendices.
USEPA. 2003. The DNAPL Remediation Challenge: Is There a Case for Source Depletion?
EPA/600/R-03/143.

Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Figures

!\]
SITE
Copyright:© 2013 National Geographic Society, i-cubed
L:\Projects\TPU\GreensboroNC\GIS\2019_Greensboro_SLM.mxd - Scale 1:27,222 - 7/23/2019 11:46:55 AM - GStewart - NAD 1927 StatePlane Pennsylvania South FIPS 3702
Sources:USGS 7.5 Minute SeriesTopographic QuadrangleHartstown and Greenville West
© 2011 National Geographic Society, i-cubed
Drawn
0 2,000
Scale In Feet (Approximate)
7/23/19
Site Location Map
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure1
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
930
910
920
900
880
870
890
850
840
830
850
820
900880
860
850
840
830
910
900
930
920
860
850
840 940
920
910 900
890
880
870
860
860
850
850
830
850
840
840
820
910
900
890 880
890
880
890
880
870
860
860
850
850
830
830
820
910
900
910
900
900
890
880
870
870
860
870
860
860
850
880
890
870
870
850
840
840
860
830
890
880
870
860
840
840
830
930
940
930930
930
920
920
920
910
910
900
890
890
900
900
890
890
880
880
880
880
880
880
880
870
870
870
870
870
870
860
860
860
860
860
860 860
860
850
850
850
840
840
840
830
830
830
830
830
830
820
820
820
820
830
820
810
900
890
860
820
CZgPPg
CZgPzZg
PPg
PzZg
MILLWOOD
SCHOOL RD
N
CHIMNEY
ROCK
RD
T H O R N D I K ERD
ALBERT
PICK
RD
HICKORY RIDGE
D
R
I-40
E
W FRIENDLY AV
N

R
E
G
I
O
N
A
L

R
D
SUNSHINE
WAY
F
O
R
S
Y
T
H
I
A
DR
W
MARKET
ST
H O L L Y D A L EDR
G R A S S Y M E A D O WRD
S
REGIONAL
RD
S W I N GCT
PRAIR IE TR
S
T
A
G
E
C
O
A
C
H
T
R
GALLIMORE
DAIRY
RD
ONRAMP
I-40 W
ON RAMP I-40 W
O L D S T A G ECOACH T R
BASE
LEG
RD
ON RAMP I-40 W
BUCKBO ARD
LN
IRON
CARRIAGECT
V A L E C I A N W A Y
P A R D U E C T
B
R
U
S
H
W
O
O
D
C T
N
C
6
8
S
ADA
I
R
R
D
O F FRAM PI-4 0 E
AMERICHASE
DR
ONRAMPI-40E
FUTURE I-40 E
WAGON
WHEEL
DR
N
S
W
I
NG
RD
G R E E N T R E EDR
OF F RAMPI-4 0 W
G
R
A
S
S
Y
M
E
A
D
O
W
CT
C A C T U SCT
OFF
RAMP
I-40
W
PA I PK
OFF
RAMP
I-40 E
CA NOERD
S

S
W
I
N
G

R
D
BURNT
POPLARCT
O F F R AMPI-40W
H I C K O R YBRANCHDR
OLD FRIENDLY RD
I
-
8
4
0

W
CITATION
CT
AERO
CT
I
-
8
4
0

E
LOCKHEED
CT
GRUMMAN R D
B R U S H WOO
D
R
D
N
C
6
8
S
CESSNA
DR
EXI T 212A
I -73S E
X
I
T
1
I
-
840E
S H ERWIN
RD
SHARPSAIRPARKCT
BRUS
H

RD
I-40
W
BO EI N G D ROFF
RAMP
I-40
W
AR
ROW
R
D
BURNT
POPLAR
RD
F
R
I
E
NDSHIP
DR
EXIT
103B
I-40W
DOWNWIND
RD
S
CHIMNEY
ROCK
RD
INTERNATIONAL
DRNATI
O
NAL
SERVIC
E
RD
PPG
RD
DISTRI
BUT
ION
DR
O
R
V
I
L
L
E
W
RIGHT
D
R
SERVICE
CENTER
DR
W
OODST
R
EAM
LN
EXIT
1
AIRLINE
RD
I
-
8
4
0
O
N
R
A
M
P
W
F
R
I
E
N
D
LY
A
V
E
E
X
I
T
2
W
F
R
I
E
N
D
L
Y
A
V
E
E
X
I
T
2
BOULDER
RD
A
M
E
R
I
C
A
N

A
V
RADA
R
RD
EXIT
212A
I-73S
I
-
8
4
0

O
N

R
A
M
P
S
T
A
GE
C
O
A
C
H
CT
I-40
W
I-840
I-40E
I-40W
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community
Legend
Project Site Boundary
Site Radius
0.25 mile
0.5 mile
1 mile
Drainage Feature
Watershed
Geologic Contact
Guilford Streets
Parcels
Contours
2 foot
10 foot
Streams
Floodzone AE
Floodzone A
Floodzone 500
Parcel Status
Abandoned Well
Potentially Used Well
Actively Used Well
Sensitive Receptor
L:\Projects\TPU\GreensboroNC\GIS\Greensboro_Detailed_Topography_Map.mxd - Scale 1:5,160 - 8/10/2021 12:01:05 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
DRAFT
Magellan Terminal
AAACooper
Piedmont-TriadInternational Airport
TPRI
Drawn
0 430
Scale In Feet (Approximate)
8/10/21
Detailed Topography Map
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Date
Figure2
GKS
DMC
DB
Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<
&<
&<&<&<&<
#
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
#
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
AMW-10S
AMW-11S
AMW-12S
AMW-13B AMW-13DAMW-13IAMW-13S
AMW-14S
AMW-15S
AMW-16S
AMW-17S
AMW-18S
AMW-8S
AMW-9S
DEM-MW6D
DEM-MW6IDEM-MW6R
FMW-15
FMW-20
FMW-21
FMW-22
FMW-23RFMW-24FMW-24D
FMW-24I FPZ-10FPZ-10I
FPZ-11
FPZ-12
FPZ-12I
FPZ-13
FPZ-14
FPZ-15
FPZ-5
FPZ-6
FPZ-7 FPZ-8
MW-A-B
MW-A-D
MW-A-I
MW-B-BMW-B-D
MW-B-I
MW-C-BMW-C-D MW-C-I
MW-D-B MW-D-D
MW-D-I
MW-E-B
MW-E-D
MW-E-I
MW-F-B
MW-F-DMW-F-I
MW-G-B
MW-G-DMW-G-I
MW-H-B
MW-H-DMW-H-I
MW-I-BMW-I-D
MW-I-I
PMW-J-B
PMW-J-DPMW-J-I
PMW-K-B
PMW-K-D
PMW-K-I
PMW-L-B
PMW-L-DPMW-L-I
PMW-M-BPMW-M-D
PMW-M-I
PMW-N-B PMW-N-D
PMW-N-I
PMW-O-BPMW-O-DPMW-O-I
OW-1
OW-2
OW-3
OW-4
OW-6
OW-7
OW-8
RW-1
RW-2
SBMW-1R
SBMW-2B
SBMW-2D
SBMW-2I
SBMW-2R
Z1-X01
Z1-X25 Z1-X27Z1-X28
Z2-PZ-06
Z2-PZ-08
Z2-PZ-09
Z2-PZ-10
Z2-X03
Z2-X16
Z2-X18
Z2-X20
Z2-X29Z2-X31
Z2-X35Z3-X80
Z3-X82
Z4-PZ04
Z4-PZ07Z4-PZ09
Z4-X21 Z4-X30Z4-X35
Z4-X47Z4-X55
Z4-X63
Z4-X68
Z4-X70 Z4-X72Z4-X89
SG-1
PMW-P-B
PMW-P-D
PMW-P-IPMW-P-S PMW-Q-B
PMW-Q-DPMW-Q-IPMW-Q-S
PMW-R-B
PMW-R-D
PMW-R-I
PMW-R-S
Source: Esri, Maxar, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community
L:\Projects\TPU\GreensboroNC\GIS\Greensboro_Site_Map_20180328.mxd - Scale 1:2,926 - 8/31/2021 11:43:18 AM - jbarnard - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Legend
Type of Sampling Location
&<Monitoring Well
#StreamInterceptor WallProperty BoundaryPipelineFenceFormer FeatureSurface WaterRemediation Zones
[[Fence LineParcels
Groundwater & Environmental Services, Inc.
Drawn
0 250
Scale In Feet (Approximate)
8/31/21
Site Map
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure3
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
PO TENT IALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
TOP OF BAN
K
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<
&<
&<&<&<&<
#
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
#
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
AMW-10S
AMW-11S
AMW-12S
AMW-13B AMW-13DAMW-13IAMW-13S
AMW-14S
AMW-15S
AMW-16S
AMW-17S
AMW-18S
AMW-8S
AMW-9S
DEM-MW6D
DEM-MW6IDEM-MW6R
FMW-15
FMW-20
FMW-21
FMW-22
FMW-23RFMW-24FMW-24D
FMW-24I FPZ-10FPZ-10I
FPZ-11
FPZ-12
FPZ-12I
FPZ-13
FPZ-14
FPZ-15
FPZ-5
FPZ-6
FPZ-7 FPZ-8
MW-A-B
MW-A-D
MW-A-I
MW-B-BMW-B-D
MW-B-I
MW-C-BMW-C-D MW-C-I
MW-D-B MW-D-D
MW-D-I
MW-E-B
MW-E-D
MW-E-I
MW-F-B
MW-F-DMW-F-I
MW-G-B
MW-G-DMW-G-I
MW-H-B
MW-H-DMW-H-I
MW-I-BMW-I-D
MW-I-I
PMW-J-B
PMW-J-DPMW-J-I
PMW-K-B
PMW-K-D
PMW-K-I
PMW-L-B
PMW-L-DPMW-L-I
PMW-M-BPMW-M-D
PMW-M-I
PMW-N-B PMW-N-D
PMW-N-I
PMW-O-BPMW-O-DPMW-O-I
OW-1
OW-2
OW-3
OW-4
OW-6
OW-7
OW-8
RW-1
RW-2
SBMW-1R
SBMW-2B
SBMW-2D
SBMW-2I
SBMW-2R
Z1-X01
Z1-X25 Z1-X27Z1-X28
Z2-PZ-06
Z2-PZ-08
Z2-PZ-09
Z2-PZ-10
Z2-X03
Z2-X16
Z2-X18
Z2-X20
Z2-X29Z2-X31
Z2-X35Z3-X80
Z3-X82
Z4-PZ04
Z4-PZ07Z4-PZ09
Z4-X21 Z4-X30Z4-X35
Z4-X47Z4-X55
Z4-X63
Z4-X68
Z4-X70 Z4-X72Z4-X89
SG-1
PMW-P-B
PMW-P-D
PMW-P-IPMW-P-S PMW-Q-B
PMW-Q-DPMW-Q-IPMW-Q-S
PMW-R-B
PMW-R-D
PMW-R-I
PMW-R-S
L:
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
S
i
t
e
_
M
a
p
_
2
0
1
8
0
3
2
8
.
m
x
d

-

S
c
a
l
e

1
:
2
,
9
2
6

-

8
/
3
1
/
2
0
2
1

1
1
:
4
2
:
4
0

A
M

-

j
b
a
r
n
a
r
d

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Legend
Type of Sampling Location
&<
#
[[
8/31/21
Site Map
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Figure4
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
I
II
I
I
\
\
\
\
\
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
UPS SupplyChain Solutions
PiedmontTriad-International Airport
PiedmontTriad-International Airport
PiedmontTriad-International Airport
Restaurant
Sheetz RetailGas Station
Ryerson MetalSupplier
AAA Cooper
RETIA
Magellan TerminalsHoldings
AAA CooperTrucking Terminal
Welsh PaperConverter
FiltronaGreensboro
W
MARKET
ST
GALLIMORE
DAIRY
RD
B A S E L E G R D
INTERNATIONAL
DR
W
FRIENDLY
AV
L:\Projects\TPU\GreensboroNC\GIS\Greensboro_Local_Area_Map.mxd - Scale 1:2,926 - 8/10/2021 12:05:16 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Legend
Interceptor Wall
[[Fence LineParcelsBuilding FootprintsStreams
I
II
I
I
\
\
\
\
\
Wetlands
Drawn
0 250
Scale In Feet (Approximate)
8/10/21
Local Area Map
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure5
GKS
DMC
Date
Groundwater & Environmental Services, Inc.
DB
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
#
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<
##
AMW-11S873.72
AMW-13S873.35
AMW-14S877.48
AMW-15S871.59
AMW-16S871.16
AMW-17S872.69
AMW-18S871.32
DEM-MW6R876.63
FMW-20872.79
FMW-21871.94
FMW-22876.22
FMW-23R873.17
FMW-24873.85
FPZ-10871.85
FPZ-11872.61
FPZ-12871.41
FPZ-13871.20FPZ-14871.41
FPZ-15871.33
FPZ-5870.55
FPZ-6872.22
FPZ-7871.93 FPZ-8871.16OW-1873.36
OW-2872.47
OW-3872.95
OW-4871.68
OW-6872.53
OW-7872.86
OW-8873.60
RW-1873.33
RW-2872.57
SG-1871.42
871
877
876
875
874
873
872
872
872
W
MARKET
ST
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_Barrier_Wall_Monitoring_Wells_GWE.mxd - Scale 1:960 - 4/18/2024 2:31:46 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Legend
&<Monitoring Well, Gauged
##Stream Location, GaugedGroundwater Elevation Contour (ft)Groundwater Flow
&<Monitoring Well
#Stream LocationBarrier Wall
[
[
[Fence LineParcels
Drawn
0 80
Scale In Feet (Approximate)
4/18/24
Barrier Wall Monitoring WellsGroundwater Elevation - July 17, 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure6
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
#
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<
##
AMW-11S871.16 AMW-13S870.91
AMW-14S875.17
AMW-15S869.77
AMW-16S870.04
AMW-17S870.12
AMW-18S870.32
DEM-MW6R874.30
FMW-20870.93
FMW-21870.22FMW-23R871.28
FPZ-10870.09
FPZ-11870.96
FPZ-12870.19
FPZ-13870.36FPZ-14869.53
FPZ-15869.92
FPZ-5869.48
FPZ-6870.61
FPZ-7870.46 FPZ-8869.82
OW-1872.52
OW-3872.34
OW-4872.43
OW-6872.37
OW-7870.99
OW-8871.55
RW-1872.51
RW-2872.31
SG-1871.33
875
874
870
873
872
871
872
871870
872 872
872
871
W
M

A

R

K

E

T

S

T
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
B
a
r
r
i
e
r
_
W
a
l
l
_
M
o
n
i
t
o
r
i
n
g
_
W
e
l
l
s
_
G
W
E
.
m
x
d

-

S
c
a
l
e

1
:
9
6
0

-

4
/
2
6
/
2
0
2
4

1
2
:
3
5
:
1
9

P
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Legend
&<Monitoring Well, Gauged
##Stream Location, Gauged
Groundwater Elevation Contour (ft)
Groundwater Flow
&<Monitoring Well
#Stream Location
Barrier Wall
[
[[Fence Line
Parcels
Drawn
0 80
Scale In Feet (Approximate)
4/26/24
Barrier Wall Monitoring Wells Groundwater Elevation - September 18 , 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure7
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
#
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<
##
AMW-11S868.56 AMW-13S869.27
AMW-14S873.43
AMW-15S868.40AMW-16S868.58
AMW-17S868.67
AMW-18S868.69
DEM-MW6R872.73
FMW-20869.24
FMW-21868.96
FMW-23R869.63
FMW-24870.16
FPZ-10868.59
FPZ-11869.28
FPZ-12868.64
FPZ-13868.42
FPZ-14868.53
FPZ-15868.47
FPZ-5868.24
FPZ-6869.03
FPZ-7868.86
FPZ-8868.41
OW-1872.88
OW-2869.00
OW-3869.03
OW-4869.09
OW-6869.06OW-7869.30
OW-8870.31
RW-1870.78
RW-2870.56
SG-1871.09
873
872
871
869
870
872
871
870 869
869
870
871
869 870
W
MARKET
ST
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_Barrier_Wall_Monitoring_Wells_GWE.mxd - Scale 1:960 - 4/26/2024 1:11:06 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Legend
&<Monitoring Well, Gauged
##Stream Location, Gauged
Groundwater Elevation Contour (ft)
Groundwater Flow
&<Monitoring Well
#Stream Location
Barrier Wall
[
[
[Fence Line
Parcels
Drawn
0 80
Scale In Feet (Approximate)
4/26/24
Barrier Wall Monitoring WellsGroundwater Elevation - December 6, 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure8
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
#
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
##
AMW-11S873.07 AMW-13S872.97
AMW-14S877.36
AMW-15S871.86
AMW-16S872.05
AMW-17S872.11
AMW-18S872.14
DEM-MW6R876.28
FMW-20872.85
FMW-21872.47
FMW-23R873.19
FPZ-10872.03
FPZ-11873.87
FPZ-12871.96
FPZ-13871.84
FPZ-14871.99
FPZ-15871.93
FPZ-5871.49
FPZ-6872.53
FPZ-7872.61
FPZ-8871.86OW-1874.01
OW-2873.16
OW-3873.20
OW-4873.25
OW-6873.21
OW-7872.97
OW-8870.37
SG-1870.75
877
876
875
874
873
872
874
872
871
873
871
W
MARKET
ST
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_Barrier_Wall_Monitoring_Wells_GWE.mxd - Scale 1:960 - 4/26/2024 12:40:25 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Legend
&<Monitoring Well, Gauged
##Stream Location, Gauged
Groundwater Elevation Contour (ft)
Groundwater Flow
&<Monitoring Well
#Stream Location
Barrier Wall
[
[
[Fence Line
Parcels
Drawn
0 80
Scale In Feet (Approximate)
4/26/24
Barrier Wall Monitoring WellsGroundwater Elevation - March 1, 2024
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure9
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<&<&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<&<&<&<
&<
&<&<
&<
&<
&<&<&<
&<&<
&<
&<
##
&<
&<&<&<
&<
&<
&<
&<&<&<
&<&<&<&<
&<
&<
&<
&<&<
&<
&<
&<&<&<&<
&<
AMW-10S881.37
AMW-11S873.72
AMW-12S882.69
AMW-13S873.35
AMW-14S877.48
AMW-15S871.59
AMW-16S871.16
AMW-17S872.69
AMW-18S871.32
AMW-8S874.48
AMW-9S876.98
DEM-MW6R876.63
FMW-15881.73
FMW-20872.79
FMW-21871.94FMW-22876.22
FMW-23R873.17FMW-24873.85
FPZ-10871.85
FPZ-11872.61
FPZ-12871.41
FPZ-13871.20
FPZ-14871.41
FPZ-15871.33
FPZ-5870.55
FPZ-6872.22
FPZ-7871.93
FPZ-8871.16
OW-1873.36
OW-2872.47
OW-3872.95
OW-4871.68
OW-6872.53
OW-7872.86
OW-8873.60
PMW-P-S864.91
PMW-Q-S861.88 PMW-R-S858.14
RW-1873.33 RW-2872.57
SBMW-1R878.79
SBMW-2R876.71
SG-1871.42
Z1-X01885.48
Z1-X25883.76
Z1-X27884.74Z1-X28882.75
Z2-PZ-08878.20
Z2-PZ-09878.60
Z2-X03884.53
Z2-X16883.36
Z2-X18883.79
Z2-X20883.32
Z2-X29881.81
Z2-X31881.56
Z2-X35882.53
Z3-X80880.75
Z3-X82881.24
Z4-PZ09877.97
Z4-X21877.75
Z4-X30878.01Z4-X35877.62
Z4-X47877.43
Z4-X55876.43
Z4-X63876.36
Z4-X68877.24
Z4-X70876.17
Z4-X72876.96
Z4-X89880.03
882880878
874
872
870
868
866
864
862
860
884
876
872
858
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_GWE.mxd - Scale 1:3,000 - 4/26/2024 12:24:29 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Drawn
0 250
Scale In Feet (Approximate)
4/26/24
Groundwater Elevation MapShallow Wells - July 17, 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure10
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
Legend
&<Monitoring Well, Gauged
##Stream Location, Gauged
Groundwater Flow
Groundwater Elevation Contour (ft)
&<Monitoring Well
Interceptor Wall
[
[
[Fence Line
Parcels
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<
AMW-13I872.84
DEM-MW6I876.61
FMW-24I873.68
FPZ-10I871.96
FPZ-12I870.65
MW-A-I882.81
MW-B-I880.11
MW-C-I879.31
MW-D-I880.84
MW-E-I877.66
MW-F-I878.75
MW-G-I879.80 MW-H-I880.43
MW-I-I881.64
PMW-J-I873.13
PMW-K-I877.75
PMW-L-I880.44
PMW-M-I872.39
PMW-N-I875.10
PMW-O-I872.63
PMW-P-I865.23
PMW-Q-I860.73 PMW-R-I858.69
SBMW-2I877.79
878
876
874
872
870
868
866
864
862
860
882
880
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_GWE.mxd - Scale 1:3,000 - 4/26/2024 12:26:31 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Drawn
0 250
Scale In Feet (Approximate)
4/26/24
Groundwater Elevation MapIntermediate Wells - July 17, 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure11
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
Legend
&<Monitoring Well, Gauged
Groundwater Flow
Groundwater Elevation Contour (ft)
&<Monitoring Well
Interceptor Wall
[
[
[Fence Line
Parcels
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<
AMW-13D872.74
DEM-MW6D876.44
FMW-24D873.56
MW-A-D882.58
MW-B-D879.89
MW-C-D878.86
MW-D-D880.44
MW-E-D877.45
MW-F-D878.16MW-G-D879.64
MW-H-D883.71
MW-I-D881.55
PMW-J-D872.97
PMW-K-D877.72
PMW-L-D880.35
PMW-M-D872.36
PMW-N-D875.42
PMW-O-D871.37
PMW-P-D864.16
PMW-Q-D859.98
PMW-R-D858.19
SBMW-2D877.62
878
876
874
872
870
868
866
862
882
880
864
860
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_GWE.mxd - Scale 1:3,000 - 4/18/2024 3:00:24 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Drawn
0 250
Scale In Feet (Approximate)
4/18/24
Groundwater Elevation MapDeep Wells - July 17, 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure12
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
Legend
&<Monitoring Well, GaugedGroundwater FlowGroundwater Elevation Contour (ft)
&<Monitoring WellInterceptor Wall
[
[
[Fence LineParcels
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
AMW-13B870.64
MW-A-B882.44
MW-B-B879.57
MW-C-B877.98
MW-D-B880.42
MW-E-B877.20 MW-F-B878.12 MW-G-B879.58
MW-H-B878.69 MW-I-B881.63
PMW-J-B873.10
PMW-K-B877.72 PMW-L-B880.36
PMW-M-B883.04
PMW-N-B880.62
PMW-O-B869.18
PMW-P-B866.34
PMW-Q-B860.82
PMW-R-B857.12
SBMW-2B877.67
878
876874
872
870
868
866
864
862
860
882
880
858
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_GWE.mxd - Scale 1:3,000 - 4/18/2024 2:51:45 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Drawn
0 250
Scale In Feet (Approximate)
4/18/24
Groundwater Elevation MapBedrock Wells - July 17, 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure13
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
Legend
&<Monitoring Well, GaugedGroundwater FlowGroundwater Elevation Contour (ft)
&<Monitoring WellInterceptor Wall
[
[
[Fence LineParcels
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
AMW-11S868.56
AMW-14S873.43
FMW-21868.96
FMW-24870.16 872
870
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_GWE.mxd - Scale 1:3,000 - 4/18/2024 1:51:08 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Drawn
0 250
Scale In Feet (Approximate)
4/18/24
Groundwater Elevation MapShallow Wells - December 6, 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure14
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
Legend
&<Monitoring Well, GaugedGroundwater Elevation Contour (ft)Groundwater Flow
&<Monitoring WellInterceptor Wall
[
[
[Fence LineParcels
L:
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
2
4
x
3
6
_
P
a
n
e
l
_
T
o
t
a
l
_
B
T
E
X
.
m
x
d

-

S
c
a
l
e

1
:
1
,
2
0
0

-

2
/
2
4
/
2
0
1
6

1
0
:
5
3
:
1
6

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
POTENT
I
A
L
BURIED
METAL
O
B
J
E
C
T
AAACOOPE
R
TPRI
MAGEL
L
A
N
TERMI
N
A
L
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
GRAV
E
L

D
R
I
V
E
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
Conoc
o
P
h
i
l
l
i
p
s
ZONE

1
ZONE
2
ZONE
3
ZONE
4
!(!(!(!(
!(!(
!(
!(
!(
!(
!(
!(!(!(!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(!(
!(!(
!(!(!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
Z1-X01
Z1-X02
Z1-X03
Z1-X05
Z1-X06
Z1-X04
Z1-X07
Z1-X08
Z1-X10
Z1-X11
Z1-X14Z1-X21
Z1-X22Z1-X26
Z1-X30
Z1-X31
Z1-X32
Z1-X37
Z1-X38
Z1-X18 Z1-X19
Z1-X20
Z1-X28
Z1-X29
Z1-X33
Z1-X34
Z1-X35
Z1-X15
Z1-X16
Z1-X23
Z1-X24
Z1-X12
Z1-X25
Z1-X36
Z1-X09
Z1-X13
Z1-X17
Z1-X27
Z2-X06
Z2-X07
Z2-X11
Z2-X15
Z2-X14
Z2-X18Z2-X21
Z2-X22
Z2-X25
Z2-X26
Z2-X35
Z2-X37
Z2-X38
Z2-X17
Z2-X19
Z2-X23
Z2-X27
Z2-X28
Z2-X29
Z2-X30
Z2-X31
Z2-X32
Z2-X33
Z2-X34
Z2-X36
Z2-X01
Z2-X02Z2-X08
Z2-X09
Z2-X10
Z2-X12
Z2-X13Z2-X16
Z2-X20
Z2-X24
Z2-X03
Z2-X04
Z2-X05
POTENT
I
A
L
BURIED
METAL
O
B
J
E
C
T
AAACOOPE
R
TPRI
MAGEL
L
A
N
TERMI
N
A
L
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
GRAV
E
L

D
R
I
V
E
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
Conoc
o
P
h
i
l
l
i
p
s
ZONE

1
ZONE
2
ZONE
3
ZONE
4
!(
!(
!(
!(
!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
!(!(
PZ-04
PZ-05
PZ-06
PZ-07
PZ-08
Z2-X01
Z2-X02
Z2-X03
Z2-X04
Z2-X05
Z2-X06
Z2-X07
Z2-X08
Z2-X09 Z2-X10
Z2-X11
Z2-X12 Z2-X13
Z2-X14
Z2-X15
Z2-X16
Z2-X17
Z2-X18
Z2-X19
Z2-X20
Z2-X21
Z2-X22
Z2-X23
Z2-X24
Z2-X25
Z2-X26
Z2-X27
Z2-X28
Z2-X29
Z2-X30
Z2-X31
Z2-X32
Z2-X33
Z2-X34
Z2-X35 Z2-X36
Z2-X37
Z2-X38
POTENT
I
A
L
BURIED
METAL
O
B
J
E
C
T
AAACOOPE
R
TPRI
MAGEL
L
A
N
TERMI
N
A
L
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
GRAV
E
L

D
R
I
V
E
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
Conoc
o
P
h
i
l
l
i
p
s
ZONE

1
ZONE
2
ZONE
3
ZONE
4
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
!(
!(!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(!(
!(!(
Z3-X07
Z3-X16
Z3-X18
Z3-X28
Z3-X39
Z3-X45
Z3-X51
Z3-X82
Z3-X83
Z3-X84
Z3-X85
Z3-X87
Z3-X100
Z3-X101Z3-X102
Z3-X103
Z3-X104
Z3-X105
Z3-X106
Z3-X24
Z3-X26Z3-X35
Z3-X37
Z3-X41
Z3-X47
Z3-X49
Z3-X52
Z3-X54 Z3-X64
Z3-X66
Z3-X68 Z3-X70
Z3-X75
Z3-X77
Z3-X86
Z3-X92
Z3-X93
Z3-X94
Z3-X95
Z3-X96
Z3-X97
Z3-X98
Z3-X99
POTENT
I
A
L
BURIED
METAL
O
B
J
E
C
T
AAACOOPE
R
TPRI
MAGEL
L
A
N
TERMI
N
A
L
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
GRAV
E
L

D
R
I
V
E
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
Conoc
o
P
h
i
l
l
i
p
s
ZONE

1
ZONE
2
ZONE
3
ZONE
4
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
!(
!(!(
!(
!(
!(
!(
!(!(
!(!(!(
!(
!(
!(!(
!(!(!(
!(
!(
!(!(
!(
!(!(!(
!(
!(
!(!(!(!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(!(!(
!(!(
!(!(
!(
!(
!(
!(!(!(!(!(!(
!(
!(!(!(!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(!(!(
!(!(!(
!(!(
!(
!(
!(
!(
!(!(
!(
!(!(
!(
!(!(
!(
!(
!(
!(!(!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
Z2-X29
Z2-X03
Z2-X18
Z1-X27
Z1-X25
Z4-X61Z4-X60
Z1-X01
Z4-X57
SBMW-1R
Z4-X01
Z3-X80
Z4-X04
Z4-X38
Z4-X55
Z4-X50
Z1-X28
Z4-X08
Z4-X56
Z4-X30
Z4-X37
Z2-X31
Z4-X17
Z2-X20
Z4-X48
Z4-X52
Z4-X27
Z4-X41
Z4-X18
Z4-X28
Z4-X13
Z4-X59
Z4-X21Z4-X32
Z4-X12RZ4-X47
Z4-X20
Z4-X45
Z4-X33
Z4-X14
Z4-X26
Z4-X46Z4-X51
Z4-X29R
Z4-X24
Z4-X42
Z4-X25
Z4-X05
Z4-X58
Z4-X43
Z4-X06
Z4-X11
Z4-X53
Z4-X49
Z4-X39
Z4-X40
Z4-X19
Z4-X44
Z4-X02
Z4-X23Z4-X31
Z4-X36
Z4-X35
Z4-X09
Z4-X10
Z4-X22
Z4-X16
Z4-X34
Z4-X15
Z4-X07
POTENT
I
A
L
BURIED
METAL
O
B
J
E
C
T
AAACOOPE
R
TPRI
ELLAN
RMINA
L
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
FORME
R
TANK
GRAV
E
L

D
R
I
V
E
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
Conoc
o
P
h
i
l
l
i
p
s
ZONE

1
ZONE
2
ZONE
3
ZONE
4
!(
!(
!(
!(!(
!(
!(
!(!(
!(
!(
!(!(!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
!(!(
!(!(
!(
!(
!(
!(!(!(
!(
!(
!(
!(
!(
!(
!(!(!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
Z1-X25
Z2-X03
Z2-X18
Z2-X29
Z2-X35
Z4-X48
Z1-X27
Z4-X74
Z4-X87
Z4-X62
Z4-PZ01
Z4-X60 Z4-X67
Z4-X54
Z4-X61 Z4-X26
Z2-X16
Z4-X25
Z4-X23
Z4-X59
Z4-X56
Z3-X83
Z4-X24
Z4-X55
Z4-PZ10
Z4-X12RZ4-X19
Z4-X57
Z2-X20
Z4-X52
Z3-X80
Z3-X16
Z4-X27
Z4-X17
Z4-X14
Z1-X09
Z1-X01
Z4-X05
Z4-X50
Z4-X73
Z4-X58
Z4-X18
Z4-X71
Z4-X41
Z4-X30
Z4-X20
Z4-X15
Z4-X78
Z4-X03
Z4-X42
Z4-X88
Z4-X49
Z4-X38
Z4-X33
Z4-X43
Z4-X16R
Z4-X51
Z4-X53
Z4-X36
Z4-X75
Z4-X44
Z4-X70
Z4-X11
Z4-PZ04
Z4-X06
Z4-X39
Z4-X72
Z4-X29R
Z4-X45
Z3-X52
Z4-X68
Z4-X76
Z4-X46
Z4-X13
Z4-X69
Z4-X31
Z4-X09
Z4-X28
Z4-X32
Z4-X66
Z4-X01
Z4-X37
Z4-X35 Z4-X10
Z4-X64
Z4-X21
Z3-X24
Z4-X40
Z3-X45
Z1-X28
Z4-X47
Z3-X22
Z2-X31
Z4-X65
Z4-X07Z4-X02
Z4-X77
Z4-X85
Z4-PZ09
Z4-X86
Z4-X79
Z4-X08
Z3-X43
Z4-X04
Z4-PZ07
Z4-X89
ELLAN
RMINA
L
!(
!(
!(
!(
!(
!(
!(
2006 2008 2010
2011 2013
Legend
Sampling Locations
Total BTEX Concentration (ug/l)
!(> 100,000
!(> 50,000 - 100,000
!(> 10,000 - 50,000
!(> 1,000 - 10,000
!(> 500 - 1,000
!(> 100 - 500
!(> 10 - 100
!(< 10
Interpolated Concentrations
Total BTEX Concentration (ug/l)
> 100,000
> 50,000 - 100,000
> 10,000 - 50,000
> 1,000 - 5,000
> 500 - 1,000
> 100 - 500
> 10 - 100
< 10
Note:Control was utilized to the east of the site due to the largevariation of sample points among time frames.2.Plume extents were generated based on the interpolationof data included from bounding years and control pointsgenerated based on professional judgement. Therefore,plume extents represent conservative, simulatedconcentrations in areas not sampled in the specified timeperiod.3.Anomalous values at Z2-X34 in 2006 and 2008, Z2-X37 in2008, and at Z4-X01 in 2011 were not included in establishing the interpolated concentrations, but are presented for reference.4.Z4-X30, Z4-X68, and Z4-X72 overlap shallow andintermediate zones and were therefore excluded from interpolation analysis.5.Concentration grids represent interpolated data in ug/lfrom the following dates: 2006: May & June2008: February & March 2010: April & June2011: May, July, & September 2013: April2022: June
8814145515
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
%
&<
&<&<&<
&<
&<
&<&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<&<&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<AMW-10S< 0.2
AMW-11S2.6
AMW-12S1
AMW-13S260
AMW-15S< 0.2
AMW-16S250
AMW-18S870
AMW-8S< 0.2
AMW-9S12
DEM-MW6R14
Z4-X631.2
FMW-15< 0.2
FMW-21< 0.2
FMW-22< 0.2
FMW-23R4.9
FMW-247100
FPZ-104.1
OW-4< 0.2
OW-8< 0.2
PMW-P-S< 0.2
PMW-Q-S< 0.2
PMW-R-S< 0.2
SBMW-1R38
SBMW-2R< 0.2
Z1-X270.82 J
Z2-PZ-100.58 J
Z2-PZ-0611
Z2-PZ-08< 0.2
Z2-PZ-09< 0.2
Z2-X200.57 J
Z2-X29< 0.2
Z2-X310.41 J Z2-X35< 0.2
Z4-X30< 0.2
Z4-X478.2
Z4-X68< 0.2
Z4-X700.45 J
Z4-X890.59 J
AMW-14S< 0.2
Z3-X80< 0.2
Z4-X72< 0.2
Z1-X28< 0.2
Z2-X16< 0.2
Z3-X820.61 J
Z4-X21< 0.2
Z4-X35< 0.2
100
100
1
1
1
1000100
10 1
Legend
&<Monitoring Well, Sampled
&<Monitoring Well
%Stream
Benzene Contour (ug/L)
Interceptor Wall
Property Boundary
Pipeline
Fence
Former Feature
Surface Water
Remediation Zones
[[
[Fence Line
Parcels
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_WG_AR_Benzene_Shallow_3Q2023.mxd - Scale 1:3,000 - 4/23/2024 1:55:25 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Drawn
0 250
Scale In Feet (Approximate)
4/23/24
Groundwater Benzene Concentration MapShallow Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure16
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Note:North Carolina Administrative
Code 2L (NCAC 2L) standardfor Benzene is 1 ug/L.
J - indicates the analylte wasdetected below quantitationlimits.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
%
&<
&<&<&<
&<
&<
&<&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
AMW-13I< 0.2
DEM-MW6I< 0.2
FMW-24I5.6
FPZ-10I< 0.2
MW-B-I< 0.2
MW-C-I< 0.2
MW-D-I< 0.2
MW-E-I< 0.2
MW-G-I< 0.2
MW-H-I< 0.2
MW-I-I< 0.2
PMW-J-I< 0.2
PMW-K-I2.4
PMW-L-I< 0.2
PMW-M-I< 0.2
PMW-O-I< 0.2
PMW-P-I< 0.2
PMW-Q-I< 0.2
PMW-R-I< 0.2
SBMW-2I0.49 J
MW-F-I0.42 J
PMW-N-I< 0.2
MW-A-I< 0.2
1
1
Legend
&<Monitoring Well, Sampled
&<Monitoring Well
%Stream
Benzene Contour (ug/L)
Interceptor Wall
Property Boundary
Pipeline
Fence
Former Feature
Surface Water
Remediation Zones
[[
[Fence Line
Parcels
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_WG_AR_Benzene_Intermediate_3Q2023.mxd - Scale 1:3,000 - 4/23/2024 1:53:23 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Drawn
0 250
Scale In Feet (Approximate)
4/23/24
Groundwater Benzene Concentration MapIntermediate Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure17
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Note:North Carolina AdministrativeCode 2L (NCAC 2L) standardfor Benzene is 1 ug/L.
J - indicates the analylte wasdetected below quantitationlimits.
There were no results above theNCAC 2L, and therefore nocontours were created.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
%
&<
&<&<&<
&<
&<
&<&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
AMW-13D< 0.2
DEM-MW6D< 0.2
FMW-24D< 0.2
MW-B-D< 0.2MW-C-D< 0.2
MW-D-D< 0.2
MW-E-D< 0.2
MW-G-D< 0.2
MW-H-D< 0.2
MW-I-D< 0.2
PMW-J-D< 0.2
PMW-K-D< 0.2 PMW-L-D< 0.2
PMW-M-D< 0.2
PMW-O-D< 0.2
PMW-P-D< 0.2 PMW-Q-D< 0.2 PMW-R-D< 0.2
SBMW-2D8.5
MW-F-D< 0.2
PMW-N-D< 0.2
MW-A-D< 0.2
1
Legend
&<Monitoring Well, Sampled
&<Monitoring Well
%Stream
Benzene Contour (ug/L)
Interceptor Wall
Property Boundary
Pipeline
Fence
Former Feature
Surface Water
Remediation Zones
[[
[Fence Line
Parcels
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_WG_AR_Benzene_Deep_3Q2023.mxd - Scale 1:3,000 - 4/23/2024 1:51:30 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Drawn
0 250
Scale In Feet (Approximate)
4/23/24
Groundwater Benzene Concentration MapDeep Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure18
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Note:North Carolina AdministrativeCode 2L (NCAC 2L) standardfor Benzene is 1 ug/L.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<&<&<&<&<&<&<
&<&<&<&<
&<&<
&<
&<&<&<&<
%
&<
&<&<&<
&<
&<
&<&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<
&<
AMW-13B< 0.2
MW-A-B< 0.2
MW-B-B< 0.2
MW-C-B< 0.2
MW-D-B< 0.2
MW-E-B< 0.2
MW-G-B< 0.2MW-H-B< 0.2
MW-I-B< 0.2
PMW-J-B< 0.2
PMW-K-B< 0.2
PMW-L-B< 0.2
PMW-M-B< 0.2
PMW-O-B< 0.2
PMW-P-B< 0.2
PMW-Q-B< 0.2
PMW-R-B< 0.2
SBMW-2B< 0.2
MW-F-B< 0.2
PMW-N-B< 0.2
Legend
&<Monitoring Well, Sampled
&<Monitoring Well
%Stream
Interceptor Wall
Property Boundary
Pipeline
Fence
Former Feature
Surface Water
Remediation Zones
[[
[Fence Line
Parcels
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_WG_AR_Benzene_Bedrock_3Q2023.mxd - Scale 1:3,000 - 4/23/2024 1:52:10 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Drawn
0 250
Scale In Feet (Approximate)
4/23/24
Groundwater Benzene Concentration MapBedrock Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure19
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Note:North Carolina AdministrativeCode 2L (NCAC 2L) standardfor Benzene is 1 ug/L.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<&<
&<
&<
&<&<
&<
&<&<&<&<
%
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<&<&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<AMW-10S< 10
AMW-11S< 10
AMW-12S< 10
AMW-13S< 10 AMW-15S< 10
AMW-16S< 10
AMW-18S< 10
AMW-8S< 10
AMW-9S< 10
DEM-MW6R5,800
FMW-15< 10
FMW-217,200
FMW-22< 10
FMW-23R< 10
FMW-24< 10
FPZ-10< 10
OW-4< 10
OW-8930
PMW-P-S< 10 PMW-Q-S< 10 PMW-R-S< 10
SBMW-1R< 10
SBMW-2R< 10
Z1-X27< 10
Z2-PZ-10< 10
Z2-PZ-06< 10
Z2-PZ-08< 10
Z2-PZ-09< 10
Z2-X20630
Z2-X29< 10Z2-X31110
Z2-X35< 10
Z4-X30< 10Z4-X47< 10
Z4-X63< 10
Z4-X68< 10
Z4-X7051
Z4-X89< 10
AMW-14S110
Z3-X8089
Z4-X72140
Z1-X28< 10
Z2-X16< 10
Z3-X8274
Z4-X21< 10
Z4-X35< 10
100
1,000 100
10
10
Legend
&<Monitoring Well
%Stream
&<Monitoring Well, Sampled
TBA Contour (ug/L)
Interceptor Wall
Property Boundary
Pipeline
Fence
Former Feature
Surface Water
Remediation Zones
[[
[Fence Line
Parcels
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_WG_AR_TBA_Shallow_3Q2023.mxd - Scale 1:3,000 - 4/23/2024 2:14:19 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Note:The Interim Allowable Concentration(IMAC) standard for TBA is 10 ug/L.
Drawn
0 250
Scale In Feet (Approximate)
4/23/24
Groundwater TBA Concentration MapShallow Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure20
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<&<
&<
&<
&<&<
&<
&<&<&<&<
%
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
AMW-13I< 10
DEM-MW6I27,000
FMW-24I< 10
FPZ-10I190
MW-B-I400
MW-C-I1,300
MW-D-I380
MW-E-I< 10 MW-G-I< 10
MW-H-I29 MW-I-I< 10
PMW-J-I< 10
PMW-K-I< 10
PMW-L-I120
PMW-M-I4,500
PMW-O-I220
PMW-P-I< 10 PMW-Q-I< 10 PMW-R-I< 10
SBMW-2I420
MW-F-I< 10
PMW-N-I2,200
MW-A-I< 10
10010
100
1,000
1,000
100
10,000
10
Legend
&<Monitoring Well
%Stream
&<Monitoring Well, Sampled
TBA Contour (ug/L)
Interceptor Wall
Property Boundary
Pipeline
Fence
Former Feature
Surface Water
Remediation Zones
[[
[Fence Line
Parcels
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_WG_AR_TBA_Intermediate_3Q2023.mxd - Scale 1:3,000 - 4/23/2024 1:49:54 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Note:The Interim Allowable Concentration(IMAC) standard for TBA is 10 ug/L.
Drawn
0 250
Scale In Feet (Approximate)
4/23/24
Groundwater TBA Concentration MapIntermediate Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure21
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<&<
&<
&<
&<&<
&<
&<&<&<&<
%
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<
&<
&<
&<
AMW-13D< 10
DEM-MW6D15,000
FMW-24D< 10
MW-B-D30,000
MW-C-D7,600
MW-D-D< 10
MW-E-D< 10
MW-G-D23,000
MW-H-D< 10
MW-I-D< 10
PMW-J-D< 10
PMW-K-D< 10
PMW-L-D240
PMW-M-D3,900
PMW-O-D560
PMW-P-D< 10 PMW-Q-D< 10 PMW-R-D< 10
SBMW-2D< 10
MW-F-D2,900
PMW-N-D280
MW-A-D< 10
100
1
100
1,000
10
1,000
10,000
10,000
Legend
&<Monitoring Well
%Stream
&<Monitoring Well, Sampled
TBA Contour (ug/L)
Interceptor Wall
Property Boundary
Pipeline
Fence
Former Feature
Surface Water
Remediation Zones
[[
[Fence Line
Parcels
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_WG_AR_TBA_Deep_3Q2023.mxd - Scale 1:3,000 - 4/23/2024 2:06:25 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Note:The Interim Allowable Concentration(IMAC) standard for TBA is 10 ug/L.
Drawn
0 250
Scale In Feet (Approximate)
4/23/24
Groundwater TBA Concentration MapDeep Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure22
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<&<
&<
&<
&<&<
&<
&<&<&<&<
%
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<
&<
&<
AMW-13B1,900
MW-A-B< 10
MW-B-B100,000
MW-C-B< 10
MW-D-B< 10
MW-E-B< 10
MW-G-B< 10
MW-H-B75
MW-I-B< 10
PMW-J-B< 10
PMW-K-B< 10
PMW-L-B< 10
PMW-M-B< 10
PMW-O-B< 10
PMW-P-B< 10
PMW-Q-B< 10 PMW-R-B< 10
SBMW-2B15,000
MW-F-B< 10
PMW-N-B< 10
1,000
10
100
10
100
1,000
10,000
10,000100,000
Legend
&<Monitoring Well
%Stream
&<Monitoring Well, Sampled
TBA Contour (ug/L)
Interceptor Wall
Property Boundary
Pipeline
Fence
Former Feature
Surface Water
Remediation Zones
[[
[Fence Line
Parcels
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_WG_AR_TBA_Bedrock_3Q2023.mxd - Scale 1:3,000 - 4/23/2024 2:21:12 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Note:The Interim Allowable Concentration(IMAC) standard for TBA is 10 ug/L.
Drawn
0 250
Scale In Feet (Approximate)
4/23/24
Groundwater TBA Concentration MapBedrock Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure23
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIVE
TOP OF BANKTOP OF BANK
TOP OF BANK
TOP OF BANK
TOP OF BANK
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<&<&<&<
&<
&<&<&<&<
&<
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<
&<&<
&<&<
&<
&<
&<
&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<
&<&<&<&<
&<&<&<
&<&<&<&<&<&<
&<
&<&<
&<
&<
&<&<
&<
&<&<&<&<
#
&<
&<&<&<
&<
&<
&<
&<
&<
&<&<&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<&<
&<&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<&<&<
&<
AMW-10S
AMW-11S
AMW-12S
AMW-13B AMW-13DAMW-13IAMW-13S
AMW-14S
AMW-15S
AMW-16S
AMW-17S
AMW-18S
AMW-8S
AMW-9S
DEM-MW6D
DEM-MW6IDEM-MW6R
FMW-15
FMW-20
FMW-21
FMW-22
FMW-23RFMW-24FMW-24D
FMW-24I FPZ-10FPZ-10I
FPZ-11
FPZ-12
FPZ-12I
FPZ-13
FPZ-14
FPZ-15
FPZ-5
FPZ-6
FPZ-7 FPZ-8
MW-A-B
MW-A-D
MW-A-I
MW-B-BMW-B-D
MW-B-I
MW-C-B
MW-C-D MW-C-I
MW-D-B MW-D-D
MW-D-I
MW-E-B
MW-E-D
MW-E-I
MW-F-B
MW-F-DMW-F-I
MW-G-B
MW-G-DMW-G-I
MW-H-B
MW-H-DMW-H-I
MW-I-BMW-I-D
MW-I-I
PMW-J-B
PMW-J-DPMW-J-I
PMW-K-B
PMW-K-D
PMW-K-I
PMW-L-B
PMW-L-DPMW-L-I
PMW-M-BPMW-M-D
PMW-M-I
PMW-N-B PMW-N-D
PMW-N-I
PMW-O-BPMW-O-DPMW-O-I
OW-1
OW-2
OW-3
OW-4
OW-6
OW-7
OW-8
RW-1
RW-2
SBMW-1R
SBMW-2BSBMW-2D
SBMW-2I
SBMW-2R
Z1-X01
Z1-X25 Z1-X27Z1-X28
Z2-PZ-06
Z2-PZ-08
Z2-PZ-09
Z2-PZ-10
Z2-X03
Z2-X16
Z2-X18
Z2-X20
Z2-X29Z2-X31
Z2-X35Z3-X80
Z3-X82
Z4-PZ04
Z4-PZ07Z4-PZ09
Z4-X21 Z4-X30Z4-X35
Z4-X47Z4-X55
Z4-X63
Z4-X68
Z4-X70 Z4-X72Z4-X89
SG-1
PMW-P-B
PMW-P-D
PMW-P-IPMW-P-S PMW-Q-B
PMW-Q-DPMW-Q-IPMW-Q-S
PMW-R-B
PMW-R-D
PMW-R-I
PMW-R-S
N:\Blacksburg\Projects\TPU\GreensboroNC\GIS\Greensboro_GW_AR_Dec2023.mxd - Scale 1:2,926 - 3/27/2024 1:43:22 PM - GStewart - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Legend
Type of Sampling Location
&<Monitoring Well
#Stream
Interceptor Wall
Property Boundary
Pipeline
Fence
Former Feature
Surface Water
Remediation Zones
[[Fence Line
Parcels
Groundwater & Environmental Services, Inc.
Drawn
0 250
Scale In Feet (Approximate)
3/27/24
Groundwater Analytical ResultsDecember 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure24
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
Chemical Name Abbreviation NCAC 2L/IMAC Standards (ug/L)1,2,4-Trimethylbenzene 124-TMB 4001,2-Dibromoethane 1,2-DBE 0.021,2-Dichloroethane 1,2-DCA 0.42-Methylnaphthalene 2-M 30BenzeneBen1ChloroformChl70EthylbenzeneEthyl600Methyl tert-butyl ether MTBE 20Methylene chloride MC 5NaphthaleneNaph6p-Isopropyltoluene p-IT 25tert-Butyl alcohol TBA 10TolueneTol600Xylenes, Total Xyl 500
< - Result is non-detect at the method detection limitJ - Result is an estimate
Notes:Results given in units of micrograms per liter (ug/L)Bold - DetectionsBold- Exceedance of the NCAC 2L StandardBold- Exceedance of the IMAC Standard
124-TMB < 0.30 1,2-DBE < 0.20 1,2-DCA < 0.20 2-M < 1.0 Ben < 0.20 Chl < 0.20 Ethyl < 0.30 MTBE < 0.20 MC < 1.0 Naph < 0.30 p-IT < 0.30 TBA < 10 Tol < 0.20 Xyl < 0.30
AMW-13B12/6/2023
124-TMB < 0.30 1,2-DBE < 0.20 1,2-DCA < 0.20 2-M < 1.0 Ben < 0.20 Chl < 0.20 Ethyl < 0.30 MTBE < 0.20 MC < 1.0 Naph < 0.30 p-IT < 0.30 TBA 36Tol< 0.20 Xyl < 0.30
AMW-11S12/6/2023
124-TMB < 0.30 1,2-DBE < 0.20 1,2-DCA 902-M < 1.0 Ben 3.5Chl< 0.20 Ethyl < 0.30 MTBE 47MC< 1.0 Naph < 0.30 p-IT < 0.30 TBA 6,900Tol0.45 JXyl< 0.30
PMW-M-D12/6/2023
124-TMB 2,2001,2-DBE < 0.20 1,2-DCA < 0.20 2-M 370Ben6,600Chl< 0.20 Ethyl 1,400MTBE< 0.20 MC < 1.0 Naph 680p-IT < 0.30 TBA < 10 Tol 230Xyl5,400
FMW-2412/6/2023
124-TMB < 0.30 1,2-DBE < 0.20 1,2-DCA < 0.20 2-M < 1.0 Ben < 0.20 Chl < 0.20 Ethyl < 0.30 MTBE < 0.20 MC < 1.0 Naph < 0.30 p-IT < 0.30 TBA 150,000Tol< 0.20 Xyl < 0.30
MW-B-B12/6/2023
124-TMB 2701,2-DBE < 0.20 1,2-DCA 9.82-M 110Ben14Chl< 0.20 Ethyl 100MTBE29MC< 1.0 Naph 73p-IT < 0.30 TBA 1,100Tol3.8Xyl370
FMW-2112/6/2023
124-TMB 71,2-DBE < 0.20 1,2-DCA 6.12-M 15Ben< 0.20 Chl < 0.20 Ethyl < 0.30 MTBE 7.9MC< 1.0 Naph 5.9p-IT < 0.30 TBA < 10 Tol < 0.20 Xyl 0.93 J
AMW-14S12/6/2023
E'
E
F'G'
D'
D
C
C'
B'A'
A
B
G
F
Date
08/20/21
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
Scale In Feet
0 250
25Figure
Groundwater & Environmental Services, Inc.
N
LEGEND
FENCE
SURFACE WATER
PIPELINE
MONITORING WELL
PROPERTY BOUNDARY
FORMER FEATURE
REMEDIATION ZONES
Designed
D.B.
J.W.
Drawn
Approved
C.M.
CROSS SECTION LOCATOR MAP
TRANSECT A-A' (Z2-X31, MW-D-B, MW-D-D, MW-D-I, Z3-X80,
MW-B-B, MW-B-D, MW-B-I, MW-C-B, MW-C-D, MW-C-I & Z4-X89)
TRANSECT B-B' ( Z2-X29, MW-I-B, MW-I-D, MW-I-I ,Z2-X35, MW-H-B,
MW-H-D, MW-H-I, MW-G-B, MW-G-D, MW-G-I, Z4-X68, MW-F-D,
MW-F-B, MW-F-I, Z4-X30, Z4-X47, MW-E-I, MW-E-B, & MW-E-D)
TRANSECT C-C' (AMW-12S, AMW-10S, PMW-L-B, PMW-L-D,
PMW-L-I, SBMW-1R, PMW-K-B, PMW-K-D, PMW-K-I, SBMW-2B,
SBMW-2I, SBMW-2D, SBMW-2R, PMW-J-B, PMW-J-I, PMW-L-D ,&
AMW-8S)
TRANSECT D-D' (FMW-22, AMW-14S, PMW-N-D, PMW-N-I,
PMW-N-B, DEM-MW-6I, DEM-MW-6D, DEM-MW-6R, PMW-M-I,
PMW-M-B, PMW-M-D,FMW-23R, FMW-24, FMW-24D & FMW-24I)
TRANSECT E-E' (PMW-P-S, PMW-P-I, PMW-P-D, PMW-P-B,
PMW-Q-S, PMW-Q-I, PMW-Q-D, PMW-Q-B, PMW-R-S, PMW-R-I,
PMW-R-D, & PMW-R-P)
TRANSECT F-F' (Z1-X01, Z1-X25, MW-A-B, MW-A-D, MW-A-I,
MW-B-B, MW-B-D, MW-B-I, Z3-X80, Z4-X68, MW-G-B, MW-G-I,
MW-G-D, Z4-PZ04, SBMW-2B, SBMW-2I, SBMW-2D, SBMW-2R,
DEM-MW-6I, DEM-MW-6D, DEM-MW-6R, FMW-21 & FPZ-5)
TRANSECT G-G' (Z4-X63, Z4-X35, PMW-J-I, PMW-J-D, PMW-J-B,
Z4-X47, MW-E-I, MW-E-D, MW-E-B, FMW-24I, FMW-24D, FMW-24,
AMW-11S, AMW-13B, AMW-13D, AMW-13I, AMW-13S, FPZ-7, FPZ-11,
PMW-O-I, PMW-O-D, PMW-O-B, FPZ-12I, & FPZ-12)
L:
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
1
\
2
0
2
1
-
0
8
\
2
0
2
0
1
0
0
9
_
G
r
e
e
n
s
b
o
r
o
_
X
s
e
c
t
i
o
n
_
L
o
c
a
t
o
r
_
m
a
p
.
d
w
g
,

M
a
p
,

J
W
i
g
g
e
r
t
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
A'A
MW
-
D
-
D
MW
-
D
-
B
MW
-
D
-
I
MW
-
B
-
I
MW
-
B
-
D
MW
-
B
-
B
MW
-
C
-
D
MW
-
C
-
B
MW
-
C
-
I
Z4
-
X
8
9
Z3
-
X
8
0
Z2
-
X
3
1
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
0.41 J< 0.20
0.59 J
Designed
Date
04/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION A-A'
DISSOLVED BENZENE CONTOURS
A.H.
J.B.
26Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
D.B.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
75'
NOTES:·
1. NORTH CAROLINA ADMINISTRATIVE CODE 2L
(NCAC 2L) STANDARD FOR BENZENE IS 1 µg/L
2. VERTICAL EXAGGERATION = 6X
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
4. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
5. ·J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
DISSOLVED BENZENE
(µg/L)
10
100
1,000
1
MEASURED BENZENE (µg/L)
BEDROCK
#
SAPROLITE
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
B
E
N
Z
.
d
w
g
,

A
-
A
'
,

4
/
1
0
/
2
0
2
4

8
:
3
3
:
5
6

A
M
,

j
b
a
r
n
a
r
d
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
B'B
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
0.42J
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20 < 0.20
< 0.20 8.2
< 0.20
Z4
-
X
3
0
MW
-
E
-
D
MW
-
E
-
B
MW
-
E
-
I
Z4
-
X
4
7
Z4
-
X
6
8
MW
-
F
-
I
MW
-
F
-
B
MW
-
F
-
D
MW
-
G
-
I
MW
-
G
-
B
MW
-
G
-
D
MW
-
H
-
I
MW
-
H
-
B
MW
-
H
-
D
Z2
-
X
3
5
MW
-
I
-
I
MW
-
I
-
B
MW
-
I
-
D
Z2
-
X
2
9
Designed
Date
05/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION B-B'
DISSOLVED BENZENE CONTOURS
A.H.
J.B.
27Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
D.B.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
50'
NOTES:
1. NORTH CAROLINA ADMINISTRATIVE CODE 2L
(NCAC 2L) STANDARD FOR BENZENE IS 1 µg/L
2. VERTICAL EXAGGERATION = 6X
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
4. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
5. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
DISSOLVED BENZENE
(µg/L)
10
100
1,000
1
MEASURED BENZENE (µg/L)
BEDROCK
#
SAPROLITE
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
B
E
N
Z
.
d
w
g
,

B
-
B
'
,

5
/
1
0
/
2
0
2
4

9
:
1
6
:
2
4

A
M
,

j
b
a
r
n
a
r
d
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
C'C
AM
W
-
1
2
S
PM
W
-
J
-
B
PM
W
-
J
-
I
PM
W
-
J
-
D
AM
W
-
8
S
SB
M
W
-
2
B
SB
M
W
-
2
I
SB
M
W
-
2
D
SB
M
W
-
2
R
SB
M
W
-
1
R
PM
W
-
K
-
B
PM
W
-
K
-
D
PM
W
-
K
-
I
AM
W
-
1
0
S
PM
W
-
L
-
B
PM
W
-
L
-
D
PM
W
-
L
-
I
< 0.20 1.0
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
2.4
< 0.20
< 0.20
< 0.20
38
< 0.20
8.5
0.49 J
< 0.20
Designed
Date
04/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION C-C'
DISSOLVED BENZENE CONTOURS
A.H.
J.B.
28Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
D.B.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
NOTES:
1. NORTH CAROLINA ADMINISTRATIVE CODE 2L
(NCAC 2L) STANDARD FOR BENZENE IS 1 µg/L
2. VERTICAL EXAGGERATION = 6X
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
4. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
5. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
DISSOLVED BENZENE
(µg/L)
10
100
1,000
1
MEASURED BENZENE (µg/L)
BEDROCK
#
SAPROLITE
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
B
E
N
Z
.
d
w
g
,

C
-
C
'
,

4
/
1
0
/
2
0
2
4

8
:
3
6
:
4
2

A
M
,

j
b
a
r
n
a
r
d
900
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
D'D
FM
W
-
2
3
R
AM
W
-
1
4
S
FM
W
-
2
2
FM
W
-
2
4
D
FM
W
-
2
4
FM
W
-
2
4
I
PM
W
-
M
-
I
PM
W
-
M
-
D
PM
W
-
M
-
B
PM
W
-
N
-
I
PM
W
-
N
-
B
PM
W
-
N
-
D
DE
M
-
M
W
6
R
DE
M
-
M
W
6
D
DE
M
-
M
W
6
I
< 0.20
< 0.20
14
< 0.20
4.9 7,100
< 0.20
5.6
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
Designed
Date
04/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION D-D'
DISSOLVED BENZENE CONTOURS
A.H.
J.B.
29Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
D.B.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
NOTES:
1. NORTH CAROLINA ADMINISTRATIVE CODE 2L
(NCAC 2L) STANDARD FOR BENZENE IS 1 µg/L
2. VERTICAL EXAGGERATION = 6X
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
4. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
5. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
DISSOLVED BENZENE
(µg/L)
10
100
1,000
1
MEASURED BENZENE (µg/L)
BEDROCK
#
SAPROLITE
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
B
E
N
Z
.
d
w
g
,

D
-
D
'
,

4
/
1
0
/
2
0
2
4

8
:
3
7
:
0
3

A
M
,

j
b
a
r
n
a
r
d
E E'
800
820
840
860
880
920
900
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
780
800
820
840
860
880
920
900
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
780
760
740
720
760
740
720
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
PM
W
-
P
-
I
PM
W
-
P
-
B
PM
W
-
P
-
D
PM
W
-
P
-
S
PM
W
-
Q
-
I
PM
W
-
Q
-
B
PM
W
-
Q
-
D
PM
W
-
Q
-
S
PM
W
-
R
-
I
PM
W
-
R
-
B
PM
W
-
R
-
D
PM
W
-
R
-
S
Date
07/30/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION E-E'
DISSOLVED BENZENE CONTOURS
30Figure
Groundwater & Environmental Services, Inc.
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
75'
25'
Designed
A.H.
J.B.
Drawn
Approved
D.B.
NOTES:
1. VERTICAL EXAGGERATION = 6X
2. GRAYED OUT WELLS AND BORINGS ARE
ABANDONED
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
SAPROLITE
BEDROCK
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
B
E
N
Z
.
d
w
g
,

E
-
E
'
,

7
/
3
0
/
2
0
2
4

1
1
:
1
0
:
2
0

A
M
,

j
b
a
r
n
a
r
d
F F'
800
820
840
860
880
920
780
760
740
720
IN
T
E
R
C
E
P
T
O
R

W
A
L
L
SO
U
T
H
E
R
N

R
A
I
L
W
A
Y
WE
S
T

M
A
R
K
E
T
ST
R
E
E
T
/
U
S

4
2
1
Former Greensboro
Terminal
RIGHT
OF WAY Piedmont-Triad
International Airport
Property
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
800
820
840
860
880
920
780
760
740
720
900 900
< 0.20
< 0.20
14 < 0.20
NS
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
8.5
0.49 J
< 0.20
<0.20
NS 3.2
< 0.20
< 0.20
< 0.20
< 0.20
SB
M
W
-
2
B
SB
M
W
-
2
I
SB
M
W
-
2
D
SB
M
W
-
2
R
DE
M
-
M
W
6
I
DE
M
-
M
W
6
D
DE
M
-
M
W
6
R
Z1
-
X
0
1
MW
-
A
-
B
MW
-
A
-
D
MW
-
A
-
I
Z3
-
X
8
0
Z4
-
P
Z
0
4
FM
W
-
2
1
FP
Z
-
5
MW
-
B
-
B
MW
-
B
-
D
MW
-
B
-
I
Z1
-
X
2
5
Z4
-
X
6
8
MW
-
G
-
I
MW
-
G
-
B
MW
-
G
-
D
Date
05/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION F-F'
DISSOLVED BENZENE CONTOURS
31Figure
Groundwater & Environmental Services, Inc.
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
Designed
A.H.
J.B.
Drawn
Approved
D.B.
NOTES:
1. NORTH CAROLINA ADMINISTRATIVE CODE 2L
(NCAC 2L) STANDARD FOR BENZENE IS 1 µg/L
2. VERTICAL EXAGGERATION = 6X
3. GRAYED OUT WELLS AND BORINGS ARE
ABANDONED
4. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
5. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
6. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
7. ANALYTICAL DATA IS FROM THE JUNE 2019
SAMPLING EVENT
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
DISSOLVED BENZENE
(µg/L)
10
100
1,000
1
MEASURED BENZENE (µg/L)
BEDROCK
#
SAPROLITE
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
B
E
N
Z
.
d
w
g
,

F
-
F
'
,

5
/
1
0
/
2
0
2
4

9
:
1
9
:
0
3

A
M
,

j
b
a
r
n
a
r
d
800
820
840
860
880
920
900
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
780
800
820
840
860
880
920
900
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
780
760
740
720
760
740
720
SO
U
T
H
E
R
N

R
A
I
L
W
A
Y
WE
S
T

M
A
R
K
E
T
ST
R
E
E
T
/
U
S

4
2
1
IN
T
E
R
C
E
P
T
O
R

W
A
L
L
Piedmont-Triad
International Airport
Property
AAA COOPER
Fo
r
m
e
r

G
r
e
e
n
s
b
o
r
o
Te
r
m
i
n
a
l
RIGHT
OF WAY
G'G
Z4
-
X
6
3
Z4
-
X
3
5
Z4
-
X
4
7
AM
W
-
1
1
S
AM
W
-
1
3
B
AM
W
-
1
3
D
AM
W
-
1
3
I
AM
W
-
1
3
S
FP
Z
-
1
1
PM
W
-
O
-
I
PM
W
-
O
-
D
PM
W
-
O
-
B
FP
Z
-
7
FM
W
-
2
4
D
FM
W
-
2
4
FM
W
-
2
4
I
FP
Z
-
1
2
I
FP
Z
-
1
2
PM
W
-
J
-
B
PM
W
-
J
-
I
PM
W
-
J
-
D
MW
-
E
-
D
MW
-
E
-
B
MW
-
E
-
I
2.6
< 0.20
< 0.20
< 0.20
260
7,100
< 0.20
5.6
NS
NS
NS
NS
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
< 0.20
8.2 1.1
< 0.30
Date
04/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION G-G'
DISSOLVED BENZENE CONTOURS
32Figure
Groundwater & Environmental Services, Inc.
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
Designed
A.H.
J.B.
Drawn
Approved
D.B.
NOTES:
1. NORTH CAROLINA ADMINISTRATIVE CODE 2L
(NCAC 2L) STANDARD FOR BENZENE IS 1 µg/L
2. VERTICAL EXAGGERATION = 6X
3. GRAYED OUT WELLS AND BORINGS ARE
ABANDONED
4. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
5. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
6. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
DISSOLVED BENZENE
(µg/L)
10
100
1,000
1
MEASURED BENZENE (µg/L)
BEDROCK
#
SAPROLITE
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
B
E
N
Z
.
d
w
g
,

G
-
G
'
,

4
/
1
0
/
2
0
2
4

8
:
3
8
:
5
1

A
M
,

j
b
a
r
n
a
r
d
MW
-
D
-
D
MW
-
D
-
B
MW
-
D
-
I
MW
-
B
-
I
MW
-
B
-
D
MW
-
B
-
B
MW
-
C
-
D
MW
-
C
-
B
MW
-
C
-
I
Z4
-
X
8
9
Z3
-
X
8
0
Z2
-
X
3
1
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
A'A
100,000
30,000
400
< 10
7,600
1,300
< 10
< 10
380
110 89
< 10
Designed
Date
04/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION A-A'
DISSOLVED TBA CONTOURS
A.H.
J.B.
33Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
D.B.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
75'
NOTES:
1. THE INTERIM ALLOWABLE CONCENTRATION
(IMAC) STANDARD FOR TBA IS 10 µg/L
2. VERTICAL EXAGGERATION = 6X
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
4. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
5. TBA = TERT BUTYL ALCOHOL
6. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
MEASURED TBA (µg/L)
BEDROCK
DISSOLVED TBA
(µg/L)
10
100
1,000
10,000
100,000
#
SAPROLITE
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
T
B
A
.
d
w
g
,

A
-
A
'
,

4
/
1
0
/
2
0
2
4

1
0
:
2
0
:
5
8

A
M
,

j
b
a
r
n
a
r
d
Z4
-
X
3
0
MW
-
E
-
D
MW
-
E
-
B
MW
-
E
-
I
Z4
-
X
4
7
Z4
-
X
6
8
MW
-
F
-
I
MW
-
F
-
B
MW
-
F
-
D
MW
-
G
-
I
MW
-
G
-
B
MW
-
G
-
D
MW
-
H
-
I
MW
-
H
-
B
MW
-
H
-
D
Z2
-
X
3
5
MW
-
I
-
I
MW
-
I
-
B
MW
-
I
-
D
Z2
-
X
2
9
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
B'B
< 10
< 10
< 10
< 10
2,900
< 10
< 10
23,000
< 10
75
< 10
29
< 10
< 10
< 10
< 10 < 10
< 10 < 10
< 10
Designed
Date
04/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION B-B'
DISSOLVED TBA CONTOURS
A.H.
J.B.
34Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
D.B.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
50'
NOTES:
1. THE INTERIM ALLOWABLE CONCENTRATION
(IMAC) STANDARD FOR TBA IS 10 µg/L
2. VERTICAL EXAGGERATION = 6X
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
4. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
5. TBA = TERT BUTYL ALCOHOL
6. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
MEASURED TBA (µg/L)
BEDROCK
DISSOLVED TBA
(µg/L)
10
100
1,000
10,000
100,000
#
SAPROLITE
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
T
B
A
.
d
w
g
,

B
-
B
'
,

4
/
1
0
/
2
0
2
4

1
0
:
2
1
:
2
7

A
M
,

j
b
a
r
n
a
r
d
AM
W
-
1
2
S
PM
W
-
J
-
B
PM
W
-
J
-
I
PM
W
-
J
-
D
AM
W
-
8
S
SB
M
W
-
2
B
SB
M
W
-
2
I
SB
M
W
-
2
D
SB
M
W
-
2
R
SB
M
W
-
1
R
PM
W
-
K
-
B
PM
W
-
K
-
D
PM
W
-
K
-
I
AM
W
-
1
0
S
PM
W
-
L
-
B
PM
W
-
L
-
D
PM
W
-
L
-
I
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
C'C
< 10 < 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
240
120
< 10
<50
15,000
420
< 10
Designed
Date
05/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION C-C'
DISSOLVED TBA CONTOURS
J.B.
35Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
NOTES:
1. THE INTERIM ALLOWABLE CONCENTRATION
(IMAC) STANDARD FOR TBA IS 10 µg/L
2. VERTICAL EXAGGERATION = 6X
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
4. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
5. TBA = TERT BUTYL ALCOHOL
6. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
MEASURED TBA (µg/L)
BEDROCK
DISSOLVED TBA
(µg/L)
10
100
1,000
10,000
100,000
#
SAPROLITE
A.H.
D.B.
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
T
B
A
.
d
w
g
,

C
-
C
'
,

5
/
1
0
/
2
0
2
4

9
:
3
4
:
1
0

A
M
,

j
b
a
r
n
a
r
d
900
FM
W
-
2
3
R
AM
W
-
1
4
S
FM
W
-
2
2
FM
W
-
2
4
D
FM
W
-
2
4
FM
W
-
2
4
I
PM
W
-
M
-
I
PM
W
-
M
-
D
PM
W
-
M
-
B
PM
W
-
N
-
I
PM
W
-
N
-
B
PM
W
-
N
-
D
DE
M
-
M
W
6
R
DE
M
-
M
W
6
D
DE
M
-
M
W
6
I
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
D'D
NS
15,000
27,000
5,800
< 10
< 10 < 10
< 10
< 10
< 10
3,900
4,500
< 10
280
2,200
Designed
Date
04/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION D-D'
DISSOLVED TBA CONTOURS
J.B.
36Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
NOTES:
1. THE INTERIM ALLOWABLE CONCENTRATION
(IMAC) STANDARD FOR TBA IS 10 µg/L
2. VERTICAL EXAGGERATION = 6X
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
4. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
5. TBA = TERT BUTYL ALCOHOL
6. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
BEDROCK
DISSOLVED TBA
(µg/L)
10
100
1,000
10,000
100,000
SAPROLITE
MEASURED TBA (µg/L) #
A.H.
D.B.
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
T
B
A
.
d
w
g
,

D
-
D
'
,

4
/
1
0
/
2
0
2
4

1
0
:
2
2
:
4
3

A
M
,

j
b
a
r
n
a
r
d
E E'
800
820
840
860
880
920
900
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
780
800
820
840
860
880
920
900
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
780
760
740
720
760
740
720
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
PM
W
-
P
-
I
PM
W
-
P
-
B
PM
W
-
P
-
D
PM
W
-
P
-
S
PM
W
-
Q
-
I
PM
W
-
Q
-
B
PM
W
-
Q
-
D
PM
W
-
Q
-
S
PM
W
-
R
-
I
PM
W
-
R
-
B
PM
W
-
R
-
D
PM
W
-
R
-
S
Date
07/30/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION E-E'
DISSOLVED TBA CONTOURS
37Figure
Groundwater & Environmental Services, Inc.
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
75'
25'
Designed
A.H.
J.B.
Drawn
Approved
D.B.
NOTES:
1. VERTICAL EXAGGERATION = 6X
2. GRAYED OUT WELLS AND BORINGS ARE
ABANDONED
3. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
SAPROLITE
BEDROCK
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
T
B
A
.
d
w
g
,

E
-
E
'
,

7
/
3
0
/
2
0
2
4

1
1
:
0
9
:
4
9

A
M
,

j
b
a
r
n
a
r
d
F F'
800
820
840
860
880
920
780
760
740
720
IN
T
E
R
C
E
P
T
O
R

W
A
L
L
SO
U
T
H
E
R
N

R
A
I
L
W
A
Y
WE
S
T

M
A
R
K
E
T
ST
R
E
E
T
/
U
S

4
2
1
Former Greensboro
Terminal
RIGHT
OF WAY Piedmont-Triad
International Airport
Property
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
800
820
840
860
880
920
780
760
740
720
900 900
15,000
27,000
5,800 7,200
NS
< 10
< 10
< 10
100,000
30,000
400
< 10
23,000
< 10
15,000
< 10
420
< 10
< 10
NS
89 < 10
< 10
SB
M
W
-
2
B
SB
M
W
-
2
I
SB
M
W
-
2
D
SB
M
W
-
2
R
DE
M
-
M
W
6
I
DE
M
-
M
W
6
D
DE
M
-
M
W
6
R
Z1
-
X
0
1
MW
-
A
-
B
MW
-
A
-
D
MW
-
A
-
I
Z3
-
X
8
0
Z4
-
P
Z
0
4
FM
W
-
2
1
FP
Z
-
5
MW
-
B
-
B
MW
-
B
-
D
MW
-
B
-
I
Z1
-
X
2
5
Z4
-
X
6
8
MW
-
G
-
I
MW
-
G
-
B
MW
-
G
-
D
Date
07/30/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION F-F'
DISSOLVED TBA CONTOURS
38Figure
Groundwater & Environmental Services, Inc.
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
Designed
J.B.
Drawn
Approved
NOTES:
1. THE INTERIM ALLOWABLE CONCENTRATION
(IMAC) STANDARD FOR TBA IS 10 µg/L
2. VERTICAL EXAGGERATION = 6X
3. GRAYED OUT WELLS AND BORINGS ARE
ABANDONED
4. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
5. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
6. TBA = TERT BUTYL ALCOHOL
7. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
8. ANALYTICAL DATA IS FROM THE JUNE 2019
SAMPLING EVENT
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
MEASURED TBA (µg/L)
BEDROCK
DISSOLVED TBA
(µg/L)
10
100
1,000
10,000
100,000
#
SAPROLITE
A.H.
D.B.
800
820
840
860
880
920
900
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
780
800
820
840
860
880
920
900
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
780
760
740
720
760
740
720
Z4
-
X
6
3
Z4
-
X
3
5
Z4
-
X
4
7
AM
W
-
1
1
S
AM
W
-
1
3
B
AM
W
-
1
3
D
AM
W
-
1
3
I
AM
W
-
1
3
S
FP
Z
-
1
1
PM
W
-
O
-
I
PM
W
-
O
-
D
PM
W
-
O
-
B
FP
Z
-
7
FM
W
-
2
4
D
FM
W
-
2
4
FM
W
-
2
4
I
SO
U
T
H
E
R
N

R
A
I
L
W
A
Y
WE
S
T

M
A
R
K
E
T
ST
R
E
E
T
/
U
S

4
2
1
IN
T
E
R
C
E
P
T
O
R

W
A
L
L
FP
Z
-
1
2
I
FP
Z
-
1
2
Piedmont-Triad
International Airport
Property
AAA COOPER
Fo
r
m
e
r

G
r
e
e
n
s
b
o
r
o
Te
r
m
i
n
a
l
RIGHT
OF WAY
G'G
PM
W
-
J
-
B
PM
W
-
J
-
I
PM
W
-
J
-
D
MW
-
E
-
D
MW
-
E
-
B
MW
-
E
-
I
< 10
1,900
< 10
< 10
< 10 < 10
< 10
< 10
NS
NS
NS
NS
< 10
< 10
< 10
< 10
< 10
< 10
< 10
560
220
< 10 < 10 < 10
Date
04/10/24
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
CROSS SECTION G-G'
DISSOLVED TBA CONTOURS
39Figure
Groundwater & Environmental Services, Inc.
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
Designed
J.B.
Drawn
Approved
NOTES:
1. THE INTERIM ALLOWABLE CONCENTRATION
(IMAC) STANDARD FOR TBA IS 10 µg/L
2. VERTICAL EXAGGERATION = 6X
3. GRAYED OUT WELLS AND BORINGS ARE
ABANDONED
4. IN JULY 2018, THE NAMING CONVENTION FOR THE
ORIGINAL CROSS SECTIONS WAS REVISED
5. DISSOLVED CONCENTRATIONS ASSUMED WITHIN
THE SCREENED INTERVAL FOR CONTOURING
PURPOSES.
6. TBA = TERT BUTYL ALCOHOL
7. J = ANALYTE DETECTED BELOW QUANTITATION
LIMITS
LEGEND
WELL
SCREEN
INFERRED
WATERTABLE
MEASURED TBA (µg/L)
BEDROCK
DISSOLVED TBA
(µg/L)
10
100
1,000
10,000
100,000
#
SAPROLITE
A.H.
D.B.
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
4
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
s
e
c
t
i
o
n
s
_
T
B
A
.
d
w
g
,

G
-
G
'
,

4
/
1
0
/
2
0
2
4

1
0
:
2
3
:
5
2

A
M
,

j
b
a
r
n
a
r
d
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRI
V
E
TOP OF B
A
N
K
TOP OF B
A
N
K
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<&<
&<
&<
&<
&<
&<
&<&<
&<
&<
&<&<
&<
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
A
R
_
G
e
o
c
h
e
m
i
c
a
l
_
P
a
r
a
m
e
t
e
r
s
_
S
h
a
l
l
o
w
_
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
5
/
2
0
2
4

3
:
2
8
:
4
7

P
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Legend
&<Monitoring Well
%Stream
Interceptor Wall
[[Fence Line
Parcels
Note:Micrograms per liter (ug/l); Milligrams per liter(mg/l); Millivolts (mV)
J - indicates analyte was detected belowquantitation limits.
<# - indicates analyzed but not detected abovethe Method Detection Limit or Sample DetectionLimit.
+++ - indicates the result was too high for the fieldmeter to read.
Well ID UnitsBenzene ug/lToluene ug/lEthylbenzene ug/lXylenes, Total ug/lDissolved Oxygen mg/lORPmVNitrogen, Nitrate + Nitrite mg/lManganese mg/lFerrous Iron (lab) mg/lFerrous Iron (field) mg/lSulfate as SO4 mg/lMethane ug/l
Aquifer Condition
Drawn
0 250
Scale In Feet (Approximate)
4/25/24
Geochemical Indicators Parameter MapShallow WellsJuly 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure40
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
AMW-10S< 0.20 < 0.20 < 0.30 < 0.30 1.56104.50.948 J1.50.0510.91.562.2No COCs
AMW-13S2603.64.55.40.21-68.7< 0.0300 1.520.1060.6590.6291730AnaerobicIronReducing
AMW-16S2504.76.79.40.3818.6< 0.0300 0.7290.0942.561.79472Aerobic
AMW-18S8702.4< 0.30 570.04-40.1< 0.0300 2.060.30470.8922870AnaerobicManganese/IronReducing
DEM-MW6R14< 0.20 0.63 J1.4 J0.2-84.3< 0.0300 3.762.7610.4< 0.200 1610AnaerobicManganese/IronReducing
FMW-21< 0.20 < 0.20 < 0.30 < 0.30 0.46-18.6< 0.0300 2.780.863.70.77348No COCs
FMW-23R4.9< 0.20 9.82.1 J0.48-37.6< 0.0300 0.9390.1840.531.23381AnaerobicManganese/IronReducing
Z1-X270.82 J< 0.20 < 0.30 < 0.30 1.249.2< 0.0300 3.210.042.160.77893.4Aerobic
Z1-X28< 0.20 < 0.20 < 0.30 3.92.62-80.4< 0.0300 13.20.122167.451270AnaerobicManganese/IronReducing
Z2-X200.57 J< 0.20 < 0.30 < 0.30 4.19-48.1< 0.0300 4.841.2111.86.73450Minimal COCsOxidative
Z4-X700.45 J1.70.47 J1.1 J0.16-100.8< 0.0300 15.4NA191.122090AnaerobicManganese/IronReducing
Z4-X72< 0.20 < 0.20 < 0.30 < 0.30 0.08-96.1< 0.0300 7.9609.740.7032200No COCs
Z4-X890.59 J0.68 J1.1< 0.30 0.15-92< 0.0300 10.1NA15.10.7851890AnaerobicIronReducing
Z3-X80< 0.20 < 0.20 < 0.30 < 0.30 0.08-16.8< 0.0300 4.1201.841.2112.2No COCs
FMW-247100250120051000.34-16.90.899 J9.962.2420< 0.200 1610AnaerobicManganese/IronReducing
SBMW-1R380.38 J1.82.6 J0.11-98.6< 0.0300 9.952.297.45< 0.200 1200AnaerobicManganese/IronReducing
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRI
V
E
TOP OF B
A
N
K
TOP OF B
A
N
K
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<
&<
&<
&<
&<
&<
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
A
R
_
G
e
o
c
h
e
m
i
c
a
l
_
P
a
r
a
m
e
t
e
r
s
_
I
n
t
e
r
m
e
d
i
a
t
e
_
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
6
/
2
0
2
4

1
1
:
4
0
:
2
0

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Legend
&<Monitoring Well
%Stream
Interceptor Wall
[[Fence Line
Parcels
Well ID UnitsBenzene ug/lToluene ug/lEthylbenzene ug/lXylenes, Total ug/lDissolved Oxygen mg/lORPmVNitrogen, Nitrate + Nitrite mg/lManganese mg/lFerrous Iron (lab) mg/lFerrous Iron (field) mg/lSulfate as SO4 mg/lMethane ug/l
Aquifer Condition
Note:Micrograms per liter (ug/l); Milligrams per liter(mg/l); Millivolts (mV)
J - indicates analyte was detected belowquantitation limits.
<# - indicates analyzed but not detected abovethe Method Detection Limit or Sample Detection
Drawn
0 250
Scale In Feet (Approximate)
4/26/24
Geochemical Indicators Parameter MapIntermediate WellsJuly 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure41
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
DEM-MW6I< 0.20 < 0.20 < 0.30 < 0.30 0.51-61.8< 0.0300 0.0078300.0551.3142No COCs
FPZ-10I< 0.20 < 0.20 < 0.30 < 0.30 3.3551.4< 0.0300 0.00493 J00.0350 J1.440.829No COCs
MW-A-I< 0.20 < 0.20 < 0.30 < 0.30 0.643.2< 0.0300 0.4960.041.740.9194.02No COCs
MW-B-I< 0.20 < 0.20 < 0.30 < 0.30 1.44-30.1< 0.0300 1.900.5091.4633.4No COCs
MW-C-I< 0.20 < 0.20 < 0.30 < 0.30 0.18-84.60.326 J1.931.760.270.253 J26.8No COCs
MW-E-I< 0.20 < 0.20 < 0.30 < 0.30 0.19-5.2< 0.0300 0.6490.110.16731.165.1No COCs
MW-G-I< 0.20 < 0.20 < 0.30 < 0.30 0.140.6< 0.0300 2.760.210.2634.5616.7No COCs
MW-H-I< 0.20 < 0.20 < 0.30 < 0.30 2.94-58.30.338 J6.170.126.380.396 J182No COCs
SBMW-2I0.49 J< 0.20 < 0.30 < 0.30 0.91-30.6< 0.0300 0.1910.030.2645.7358.9Minimal COCsOxidative
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRI
V
E
TOP OF B
A
N
K
TOP OF B
A
N
K
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<
&<
&<
&<
&<
&<
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
A
R
_
G
e
o
c
h
e
m
i
c
a
l
_
P
a
r
a
m
e
t
e
r
s
_
D
e
e
p
_
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
6
/
2
0
2
4

1
1
:
3
6
:
2
7

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Legend
&<Monitoring Well
%Stream
Interceptor Wall
[[Fence Line
Parcels
Well ID UnitsBenzene ug/lToluene ug/lEthylbenzene ug/lXylenes, Total ug/lDissolved Oxygen mg/lORPmVNitrogen, Nitrate + Nitrite mg/lManganese mg/lFerrous Iron (lab) mg/lFerrous Iron (field) mg/lSulfate as SO4 mg/lMethane ug/l
Aquifer Condition
Drawn
0 250
Scale In Feet (Approximate)
4/26/24
Geochemical Indicators Parameter MapDeep WellsJuly 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure42
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Note:Micrograms per liter (ug/l); Milligrams per liter(mg/l); Millivolts (mV)
J - indicates analyte was detected belowquantitation limits.
<# - indicates analyzed but not detected abovethe Method Detection Limit or Sample Detection
DEM-MW6D< 0.20 < 0.20 < 0.30 < 0.30 0.5815.3< 0.0300 0.2220.360.2790.55515.6No COCs
MW-A-D< 0.20 < 0.20 < 0.30 < 0.30 1.19-23.9< 0.0300 2.9601.220.74614.3No COCs
MW-B-D< 0.20 < 0.20 < 0.30 < 0.30 3.630.8< 0.0300 5.3701.120.778101No COCs
MW-C-D< 0.20 < 0.20 < 0.30 < 0.30 0.3299.90.407 J4.712.086.480.771123No COCs
MW-D-D< 0.20 < 0.20 < 0.30 < 0.30 0.39-71.2< 0.0300 0.006840.18< 0.0200 3.7914.9No COCs
MW-E-D< 0.20 < 0.20 < 0.30 < 0.30 0.053.3< 0.0300 0.1840.10.1722.942.2No COCs
MW-F-D< 0.20 < 0.20 < 0.30 < 0.30 4.3-32.7< 0.0300 2.1300.2620.83436.3No COCs
MW-H-D< 0.20 < 0.20 < 0.30 < 0.30 6.16-60.70.793 J0.00462 J0.130.0380 J5.432.46No COCs
FMW-24D< 0.20 < 0.20 < 0.30 < 0.30 4.8434.7< 0.0300 0.08640.020.0340 J2.130.696No COCs
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRI
V
E
TOP OF B
A
N
K
TOP OF B
A
N
K
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
&<
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
A
R
_
G
e
o
c
h
e
m
i
c
a
l
_
P
a
r
a
m
e
t
e
r
s
_
B
e
d
r
o
c
k
_
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
5
/
2
0
2
4

3
:
2
1
:
2
6

P
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Legend
&<Monitoring Well
%Stream
Interceptor Wall
[[Fence Line
Parcels
Drawn
0 250
Scale In Feet (Approximate)
4/25/24
Geochemical Indicators Parameter MapBedrock WellsJuly 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure43
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID UnitsBenzene ug/lToluene ug/lEthylbenzene ug/lXylenes, Total ug/lDissolved Oxygen mg/lORPmVNitrogen, Nitrate + Nitrite mg/lManganese mg/lFerrous Iron (lab) mg/lFerrous Iron (field) mg/lSulfate as SO4 mg/lMethane ug/l
Aquifer Condition
Note:Micrograms per liter (ug/l); Milligrams per liter(mg/l); Millivolts (mV)
J - indicates analyte was detected belowquantitation limits.
<# - indicates analyzed but not detected abovethe Method Detection Limit or Sample Detection
AMW-13B< 0.20 < 0.20 < 0.30 < 0.30 0.057.1< 0.0300 0.07570< 0.0200 1.8925.2No COCs
MW-A-B< 0.20 < 0.20 < 0.30 < 0.30 1.19-12.6< 0.0300 0.023801.641.71.07No COCs
MW-B-B< 0.20 < 0.20 0.39 J1.7 J3.45-153< 0.0300 0.0074300.0513.532.25Minimal COCsReductive
MW-C-B< 0.20 < 0.20 < 0.30 < 0.30 5.27-5.31.63 J0.00423 J0.230.0490 J5.17< 0.107 No COCs
MW-E-B< 0.20 < 0.20 < 0.30 < 0.30 6.3862.80.568 J0.00152 J0.080.0370 J4.160.549No COCs
MW-F-B< 0.20 < 0.20 < 0.30 < 0.30 1.5950.2< 0.0300 0.00221 J00.0320 J1.380.514No COCs
MW-G-B< 0.20 < 0.20 < 0.30 < 0.30 5.6798.80.345 J0.006121.2< 0.0200 2.750.545No COCs
MW-H-B< 0.20 < 0.20 < 0.30 < 0.30 0.053.20.330 J1.120.150.3690.385 J61.3No COCs
MW-I-B< 0.20 < 0.20 < 0.30 < 0.30 7.6368.1< 0.0300 0.00304 J0.37< 0.0200 3.36< 0.107 No COCs
SBMW-2B< 0.20 < 0.20 < 0.30 < 0.30 0.09-117.1< 0.0300 1.030.360.1351.2132.8No COCs
MW-D-B< 0.20 < 0.20 < 0.30 < 0.30 7.45-70.8< 0.0300 < 0.000700 0.3< 0.0200 5.293.49No COCs
[
[
[
[
[
[
[
[
[
[
[

[
[
[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIV
E
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
TOP OF BANK
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(!(!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(!(
!(
!(!(!(
!(
!(
!(!(
!(
!(!(!(!(AMW-10S
AMW-13S
AMW-16S
AMW-18S
DEM-MW6R
FMW-21
FMW-23R
FMW-24
SBMW-1R
Z1-X27Z1-X28
Z2-X20
Z3-X80
Z4-X72
AMW-11S
AMW-12S
AMW-14S
AMW-15S
AMW-8S
AMW-9S
FMW-15
FMW-22
FPZ-10
OW-4
OW-8
PMW-P-S PMW-R-S
SBMW-2R
Z1-X01
Z2-PZ-06
Z2-PZ-08
Z2-PZ-09Z2-PZ-10
Z2-X16 Z2-X29
Z2-X31
Z2-X35
Z3-X82
Z4-X21
Z4-X30
Z4-X35 Z4-X47
Z4-X63 Z4-X68
Z4-X70
Z4-X89
Legend
Interceptor Wall
[[[Fence Line
Parcels
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
D
O
_
S
h
a
l
l
o
w
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
4
/
2
0
2
4

1
0
:
1
9
:
4
8

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
< 0.5
0.5 - 1
1 - 2
2 - 4
> 4
Drawn
0 250
Scale In Feet (Approximate)
Designed
Approved
Figure44
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID
Dissolved Oxygen Concentration (mg/L)
Well ID
Dissolved Oxygen Concentration (mg/L)AMW-10S 1.56 Z1-X01 0.44 AMW-11S 0.20 Z1-X27 1.24 AMW-12S 0.29 Z1-X28 2.62 AMW-13S 0.21 Z2-PZ-06 1.38 AMW-14S 0.26 Z2-PZ-08 0.21 AMW-15S 0.28 Z2-PZ-09 0.17 AMW-16S 0.38 Z2-PZ-10 1.12 AMW-18S 0.04 Z2-X16 0.15 AMW-8S 0.42 Z2-X20 4.19 AMW-9S 0.53 Z2-X29 0.14 DEM-MW6R 0.20 Z2-X31 0.35 FMW-15 0.41 Z2-X35 1.47 FMW-21 0.46 Z3-X80 0.08 FMW-22 8.48 Z3-X82 1.25 FMW-23R 0.48 Z4-X21 0.16 FMW-24 0.34 Z4-X30 3.20 FPZ-10 0.10 Z4-X35 1.21 OW-4 0.51 Z4-X47 0.09 OW-8 7.91 Z4-X63 0.40 PMW-P-S 2.97 Z4-X68 5.44 PMW-R-S 1.19 Z4-X70 0.16 SBMW-1R 0.11 Z4-X72 0.08 SBMW-2R 0.23 Z4-X89 0.15
[
[
[
[
[
[
[
[
[
[
[

[
[
[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIV
E
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
TOP OF BANK
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
DEM-MW6I
FPZ-10I
MW-A-I
MW-B-I
MW-C-I
MW-E-I
MW-G-I MW-H-I
SBMW-2I
AMW-13I
FMW-24I
MW-D-I
MW-F-I
MW-I-I
PMW-J-I
PMW-K-I
PMW-L-I
PMW-M-I
PMW-N-I
PMW-O-I
PMW-P-I
PMW-Q-I
PMW-R-I
Legend
Interceptor Wall
[[[Fence Line
Parcels
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
D
O
_
I
n
t
e
r
m
e
d
i
a
t
e
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
4
/
2
0
2
4

9
:
4
9
:
3
8

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Drawn
0 250
Scale In Feet (Approximate)
4/24/24
Groundwater Dissolved Oxygen Concentration MapIntermediate Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure45
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Dissolved OxygenConcentration (mg/L)
< 0.5
0.5 - 1
1 - 2
2 - 4
> 4
Well ID Dissolved Oxygen Concentration (mg/L)
AMW-13I 0.09 DEM-MW6I 0.51 FMW-24I 3.20 FPZ-10I 3.35 MW-A-I 0.60 MW-B-I 1.44 MW-C-I 0.18 MW-D-I 0.92 MW-E-I 0.19 MW-F-I 0.06 MW-G-I 0.10 MW-H-I 2.94 MW-I-I 0.13 PMW-J-I 1.79 PMW-K-I 0.83 PMW-L-I 1.94 PMW-M-I 0.36 PMW-N-I 0.22 PMW-O-I 0.41 PMW-P-I 7.66 PMW-Q-I 6.54 PMW-R-I 1.05 SBMW-2I 0.91
[
[
[
[
[
[
[
[
[
[
[

[
[
[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIV
E
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
TOP OF BANK
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
!(
DEM-MW6DFMW-24D
MW-A-D
MW-B-D
MW-C-D
MW-D-D
MW-E-D MW-F-D
MW-H-D
AMW-13D
MW-G-D
MW-I-D
PMW-J-D
PMW-K-D
PMW-L-D
PMW-M-D
PMW-N-D
PMW-O-D
PMW-P-D
PMW-Q-D PMW-R-D
SBMW-2D
Legend
Interceptor Wall
[[[Fence Line
Parcels
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
D
O
_
D
e
e
p
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
4
/
2
0
2
4

1
0
:
1
7
:
0
1

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Dissolved OxygenConcentration (mg/L)
< 0.5
0.5 - 1
1 - 2
2 - 4
> 4
Drawn
0 250
Scale In Feet (Approximate)
4/24/24
Groundwater Dissolved Oxygen Concentration MapDeep Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure46
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID Dissolved Oxygen Concentration (mg/L)
AMW-13D 0.98 DEM-MW6D 0.58 FMW-24D 4.84 MW-A-D 1.19 MW-B-D 3.63 MW-C-D 0.32 MW-D-D 0.39 MW-E-D 0.05 MW-F-D 4.30 MW-G-D 0.09 MW-H-D 6.16 MW-I-D 0.05 PMW-J-D 1.08 PMW-K-D 6.70 PMW-L-D 0.02 PMW-M-D 0.08 PMW-N-D 0.46 PMW-O-D 0.38 PMW-P-D 4.20 PMW-Q-D 5.95 PMW-R-D 0.05 SBMW-2D 7.33
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIV
E
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
TOP OF BANK
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
AMW-13B
MW-A-B
MW-B-B
MW-C-B
MW-D-B
MW-E-B MW-F-B MW-G-BMW-H-B
MW-I-B
SBMW-2B
PMW-J-B
PMW-K-B
PMW-L-B
PMW-M-B
PMW-N-B
PMW-O-B
PMW-P-B
PMW-Q-B
PMW-R-B
Legend
Interceptor Wall
[[[Fence Line
Parcels
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
D
O
_
B
e
d
r
o
c
k
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
4
/
2
0
2
4

1
0
:
1
4
:
5
2

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
> 0.5
0.5 - 1
1 - 2
2 - 4
> 4
Drawn
0 250
Scale In Feet (Approximate)
Designed
Approved
Figure47
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID Dissolved Oxygen Concentration (mg/L)AMW-13B 0.05 MW-A-B 1.19 MW-B-B 3.45 MW-C-B 5.27 MW-D-B 7.45 MW-E-B 6.38 MW-F-B 1.59 MW-G-B 5.67 MW-H-B 0.05 MW-I-B 7.63 PMW-J-B 6.33 PMW-K-B 2.67 PMW-L-B 6.23 PMW-M-B 0.19 PMW-N-B 0.09 PMW-O-B 0.03 PMW-P-B 7.75 PMW-Q-B 5.29 PMW-R-B 1.10 SBMW-2B 0.09
[
[
[
[
[
[
[
[
[
[
[

[
[
[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIV
E
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
TOP OF BANK
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(!(!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(!(
!(
!(!(!(
!(
!(
!(!(
!(
!(!(!(!(
AMW-10S
AMW-13S
AMW-16S
AMW-18S
DEM-MW6R
FMW-21
FMW-23R
FMW-24
SBMW-1R
Z1-X27Z1-X28 Z2-X20
Z3-X80
Z4-X72
AMW-11S
AMW-12S
AMW-14S
AMW-15S
AMW-8S
AMW-9S
FMW-15
FMW-22
FPZ-10
OW-4
OW-8
PMW-P-S PMW-R-S
SBMW-2R
Z1-X01
Z2-PZ-06
Z2-PZ-08
Z2-PZ-09Z2-PZ-10
Z2-X16
Z2-X29Z2-X31
Z2-X35
Z3-X82
Z4-X21
Z4-X30
Z4-X35 Z4-X47
Z4-X63 Z4-X68
Z4-X70
Z4-X89
Legend
Interceptor Wall
[[[Fence Line
Parcels
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
O
R
P
_
S
h
a
l
l
o
w
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
4
/
2
0
2
4

1
0
:
1
1
:
5
5

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
< -150
-150 - -50
-50 - 0
0 - 50
50 - 150
> 150
Drawn
0 250
Scale In Feet (Approximate)
Designed
Approved
Figure48
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID OxidationReductionPotential (mV)Well ID OxidationReductionPotential (mV)AMW-10S 104.5 Z1-X01 94.8 AMW-11S -50.2 Z1-X27 9.2 AMW-12S -28.9 Z1-X28 -80.4AMW-13S -68.7 Z2-PZ-06 -115.10AMW-14S -17.6 Z2-PZ-08 -93.4AMW-15S -64.7 Z2-PZ-09 168.40 AMW-16S 18.6 Z2-PZ-10 77.0 AMW-18S -40.1 Z2-X16 -74.7AMW-8S -56.9 Z2-X20 -48.1AMW-9S -114.9 Z2-X29 78.0 DEM-MW6R -84.3 Z2-X31 -90.3FMW-15 94.1 Z2-X35 28.70FMW-21 -18.6 Z3-X80 -16.8FMW-22 27.50 Z3-X82 -12.7FMW-23R -37.6 Z4-X21 -8.1FMW-24 -116.90 Z4-X30 -16.8FPZ-10 -87.6 Z4-X35 -82.9OW-4 -8.3 Z4-X47 -104.4OW-8 -33.7 Z4-X63 -94.6PMW-P-S 84.6 Z4-X68 -77.0PMW-R-S 101.50 Z4-X70 -100.8SBMW-1R -98.6 Z4-X72 -96.1SBMW-2R -3.3 Z4-X89 -92.0
[
[
[
[
[
[
[
[
[
[
[

[
[
[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIV
E
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
TOP OF BANK
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
DEM-MW6I
FPZ-10I
MW-A-I
MW-B-I
MW-C-I
MW-E-I
MW-G-I
MW-H-I
SBMW-2I
AMW-13IFMW-24I
MW-D-I
MW-F-I
MW-I-I
PMW-J-I
PMW-K-I
PMW-L-I
PMW-M-I
PMW-N-I
PMW-O-I
PMW-P-I
PMW-Q-I
PMW-R-I
Legend
Interceptor Wall
[[[Fence Line
Parcels
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
O
R
P
_
I
n
t
e
r
m
e
d
i
a
t
e
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
4
/
2
0
2
4

1
0
:
0
9
:
4
7

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Oxidation ReductionPotential (mV)
< -150
-150 - -50
-50 - 0
0 - 50
50 - 150
> 150
Drawn
0 250
Scale In Feet (Approximate)
4/24/24
Groundwater Oxidation Reduction PotentialConcentration MapIntermediate Wells - June 2022
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure49
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID OxidationReductionPotential (mV)AMW-13I 63.1 DEM-MW6I -61.8FMW-24I 121.2 FPZ-10I 51.4 MW-A-I 43.2 MW-B-I -30.1MW-C-I -84.6MW-D-I 18.7 MW-E-I -5.2MW-F-I 4.8 MW-G-I 40.6 MW-H-I -58.3MW-I-I -17.6PMW-J-I 30.5 PMW-K-I -42.6PMW-L-I 1.6 PMW-M-I -52.7PMW-N-I 2.9 PMW-O-I -10.2PMW-P-I 66.5 PMW-Q-I 88.2 PMW-R-I 25.4 SBMW-2I -30.6
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIV
E
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
TOP OF BANK
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
!(
DEM-MW6D
FMW-24D
MW-A-D
MW-B-D
MW-C-D
MW-D-D
MW-E-D MW-F-D
MW-H-D
AMW-13D
MW-G-D
MW-I-D
PMW-J-D
PMW-K-D
PMW-L-D
PMW-M-D PMW-N-D
PMW-O-D
PMW-P-D PMW-Q-D PMW-R-D
SBMW-2D
Legend
Interceptor Wall
[[[Fence Line
Parcels
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
O
R
P
_
D
e
e
p
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
4
/
2
0
2
4

1
0
:
0
7
:
3
3

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Oxidation ReductionPotential (mV)
< -150
-150 - -50
-50 - 0
0 - 50
50 - 150
> 150
Drawn
0 250
Scale In Feet (Approximate)
4/24/24
Groundwater Oxidation Reduction PotentialConcentration MapDeep Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure50
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID OxidationReductionPotential (mV)
AMW-13D 63.7 DEM-MW6D 15.3 FMW-24D 34.7 MW-A-D -23.9MW-B-D 0.8 MW-C-D 99.9 MW-D-D -71.2MW-E-D 3.3 MW-F-D -32.70MW-G-D 17.9 MW-H-D -60.7MW-I-D 44.2 PMW-J-D -14.9PMW-K-D 20.1 PMW-L-D -1.7PMW-M-D -115.1PMW-N-D 26.8 PMW-O-D 57.2 PMW-P-D 59.3 PMW-Q-D 80.3 PMW-R-D 65.3 SBMW-2D 15.4
[
[
[
[
[
[
[
[
[
[
[

[
[
[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DRIV
E
TOP OF BAN
K
TOP OF BAN
K
TOP OF BA
N
K
TOP OF BANK
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
AMW-13B
MW-A-B
MW-B-B
MW-C-B
MW-D-B
MW-E-B
MW-F-B
MW-G-B
MW-H-B
MW-I-B
SBMW-2B
PMW-J-B
PMW-K-B
PMW-L-B
PMW-M-B PMW-N-B
PMW-O-B
PMW-P-B PMW-Q-B PMW-R-B
Legend
Interceptor Wall
[[[Fence Line
Parcels
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
O
R
P
_
B
e
d
r
o
c
k
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
3
,
0
0
0

-

4
/
2
4
/
2
0
2
4

1
0
:
2
6
:
2
2

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Oxidation ReductionPotential (mV)
< -150
-150 - -50
-50 - 0
0 - 50
50 - 150
> 150
Drawn
0 250
Scale In Feet (Approximate)
4/24/24
Groundwater Oxidation Reduction PotentialConcentration MapBedrock Wells - July 2023
Former Fina Bulk Fuel OilTerminal #1760Greensboro, North Carolina
Designed
Approved
Figure51
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID OxidationReductionPotential (mV)AMW-13B 7.1 MW-A-B -12.6MW-B-B -153.0MW-C-B -5.3MW-D-B -70.8MW-E-B 62.8 MW-F-B 50.2 MW-G-B 98.8 MW-H-B 3.2 MW-I-B 68.1 PMW-J-B -74.1PMW-K-B -57.4PMW-L-B -33.7PMW-M-B -175.3PMW-N-B 23.6 PMW-O-B -14.2PMW-P-B -4.6PMW-Q-B -63.8PMW-R-B -126.6SBMW-2B -117.1
[
[
[
[
[
[
[
[
[
[

[
[
[

[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DR
I
V
E
TOP OF B
A
N
K
TOP OF B
A
N
K
TOP OF BA
N
K
TOP OF BA
N
K
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(!(!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(!(
!(
!(!(!(
!(
!(
!(!(
!(
!(!(!(
!(
AMW -10S
AMW -13S
AMW -16S
AMW -18S
DEM-MW 6R
FMW -21FMW -23R
FMW -24
SBMW -1R
Z1-X27Z1-X28
Z2-X20Z3-X80
Z4-X72
AMW -11S
AMW -12S
AMW -14S
AMW -15S
AMW -8S
AMW -9S
FMW -15
FMW -22
FPZ-10
OW -4
OW -8
PMW -P-S PMW -R -S
SBMW -2R
Z1-X01
Z2-PZ-06
Z2-PZ-08
Z2-PZ-09
Z2-PZ-10
Z2-X16 Z2-X29Z2-X31
Z2-X35
Z3-X82
Z4-X21
Z4-X30Z4-X35
Z4-X47
Z4-X63 Z4-X68
Z4-X70
Z4-X89
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
T
e
m
p
_
S
h
a
l
l
o
w
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
2
,
8
5
5

-

4
/
2
4
/
2
0
2
4

9
:
5
8
:
5
9

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Le ge nd
[[
Te m pe rature (ᵒC)
4/24/24
Ground w ate r Te m pe rature MapShallow W e llsJuly 2023
Form e r Fina Bulk Fue l OilTe rm inal #1760Gre e nsboro, North Carolina
52
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.Groundwater & Environmental Services, Inc.
Well ID Temperature (deg. C) Well ID Temperature (deg. C)AMW-10S 20.40 Z1-X01 17.50 AMW-11S 14.20 Z1-X27 19.00 AMW-12S 17.20 Z1-X28 27.80 AMW-13S 14.60 Z2-PZ-06 22.80 AMW-14S 14.40 Z2-PZ-08 20.80 AMW-15S 17.30 Z2-PZ-09 22.10 AMW-16S 14.90 Z2-PZ-10 21.00 AMW-18S 15.30 Z2-X16 21.00 AMW-8S 18.10 Z2-X20 21.10 AMW-9S 18.90 Z2-X29 19.00 DEM-MW6R 17.60 Z2-X31 23.10 FMW-15 15.90 Z2-X35 24.10 FMW-21 20.50 Z3-X80 20.70 FMW-22 20.70 Z3-X82 22.70 FMW-23R 15.30 Z4-X21 20.20 FMW-24 17.80 Z4-X30 22.30 FPZ-10 20.00 Z4-X35 24.10 OW-4 19.40 Z4-X47 23.10 OW-8 25.40 Z4-X63 22.80 PMW-P-S 19.90 Z4-X68 21.70 PMW-R-S 16.20 Z4-X70 24.50 SBMW-1R 17.10 Z4-X72 20.20 SBMW-2R 22.70 Z4-X89 24.20
[
[
[
[
[
[
[
[
[
[

[
[
[

[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[

[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DR
I
V
E
TOP OF B
A
N
K
TOP OF B
A
N
K
TOP OF BA
N
K
TOP OF BA
N
K
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
DEM-MW6I
FP Z-10I
MW-A-I
MW-B-I
MW-C-I
MW-E-I
MW-G-I
MW-H-I
SBMW-2I
AMW-13I
FMW-24I
MW-D-I
MW-F-I
MW-I-I
P MW-J-I
P MW-K-I
P MW-L-I
P MW-M-I
P MW-N-I
P MW-O-I
P MW-P -I P MW-Q-I P MW-R-I
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
T
e
m
p
_
I
n
t
e
r
m
e
d
i
a
t
e
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
2
,
8
5
5

-

4
/
2
4
/
2
0
2
4

9
:
5
5
:
2
1

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Legend
Interceptor Wall
[[Fence Line
ParcelsTem perature (ᵒC)
< 15
15 - 20
20 - 25
25 - 30
> 30
Drawn
0 250
Scale In Feet (Approximate)
4/24/24
Ground w ater Tem perature MapInterm ed iate WellsJuly 2023
Form er Fina Bulk Fuel OilTerm inal #1760Greensb oro, North Carolina
Designed
Approved
Figure53
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID Temperature (deg. C)AMW-13I 14.50 DEM-MW6I 16.80 FMW-24I 17.50 FPZ-10I 17.80 MW-A-I 26.10 MW-B-I 28.50 MW-C-I 25.50 MW-D-I 25.90 MW-E-I 24.50 MW-F-I 20.50 MW-G-I 20.70 MW-H-I 21.70 MW-I-I 20.20 PMW-J-I 18.30 PMW-K-I 20.10 PMW-L-I 17.20 PMW-M-I 16.80 PMW-N-I 14.00 PMW-O-I 13.50 PMW-P-I 19.90 PMW-Q-I 17.60 PMW-R-I 17.30 SBMW-2I 17.60
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DR
I
V
E
TOP OF B
A
N
K
TOP OF B
A
N
K
TOP OF BA
N
K
TOP OF BA
N
K
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(!(
!(
DEM-MW6D
FMW-24D
MW-A-D
MW-B-DMW-C-D
MW-D-D
MW-E-D
MW-F-D
MW-H-D
AMW-13D
MW-G-D
MW-I-D
P MW-J-D
P MW-K-D
P MW-L-D
P MW-M-D P MW-N-D
P MW-O-D
P MW-P -D P MW-Q-D P MW-R-D
SBMW-2D
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
T
e
m
p
_
D
e
e
p
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
2
,
8
5
5

-

4
/
2
4
/
2
0
2
4

1
0
:
0
3
:
2
2

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Le ge nd
Interceptor Wall
[[Fence Line
ParcelsTe m pe rature (ᵒC)
< 15
15 - 20
20 - 25
25 - 30
> 30
Drawn
0 250
Scale In Feet (Approximate)
4/24/24
Ground w ate r Te m pe rature MapDe e p We llsJuly 2023
Form e r Fina Bulk Fue l OilTe rm inal #1760Gre e nsboro, North Carolina
Designed
Approved
Figure54
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID Temperature (deg. C)AMW-13D 16.30 DEM-MW6D 17.80 FMW-24D 17.90 MW-A-D 23.10 MW-B-D 25.40 MW-C-D 26.30 MW-D-D 25.30 MW-E-D 22.90 MW-F-D 21.30 MW-G-D 21.00 MW-H-D 21.30 MW-I-D 19.80 PMW-J-D 17.50 PMW-K-D 17.90 PMW-L-D 16.80 PMW-M-D 17.30 PMW-N-D 13.80 PMW-O-D 13.50 PMW-P-D 17.40 PMW-Q-D 17.10 PMW-R-D 17.50 SBMW-2D 17.60
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
[
POTENTIALBURIEDMETAL OBJECT
HYDROCARBONINTERCEPTORWALL
AAACOOPER
TPRI
MAGELLANTERMINAL
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
FORMERTANK
PIEDMONT-TRIADINTERNATIONALAIRPORT
POND
GRAVEL DR
I
V
E
TOP OF B
A
N
K
TOP OF B
A
N
K
TOP OF BA
N
K
TOP OF BA
N
K
TOP OF BAN
K
ConocoPhillips
ZONE 1
ZONE 2
ZONE 3
ZONE 4
Z4-X68
Z4-X72
Z4-X63
Z4-X35
Z4-X47
Z4-X21
Z4-X70
Z4-X30
Z4-X89
Z4-X60
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
AMW -13B
MW -A-B
MW -B-B
MW -C-B
MW -D-B
MW -E-B
MW -F-B
MW -G-B
MW -H-B
MW -I-B
SBMW -2B
PMW -J-B
PMW -K-B
PMW -L-B
PMW -M-B PMW -N-B
PMW -O-B
PMW -P-B PMW -Q-B PMW -R -B
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
W
G
_
F
R
_
T
e
m
p
_
B
e
d
r
o
c
k
_
J
u
l
y
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
2
,
8
5
5

-

4
/
2
4
/
2
0
2
4

1
0
:
0
1
:
1
0

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

N
o
r
t
h

C
a
r
o
l
i
n
a

F
I
P
S

3
2
0
0

F
e
e
t
Le g e n d
Interceptor Wall
[[Fence Line
ParcelsTe mpe rature (ᵒC)
< 15
15 - 20
20 - 25
25 - 30
> 30
Drawn
0 250
Scale In Feet (Approximate)
4/24/24
Groun dw ate r Te mpe rature MapBe drock W e llsJuly 2023
Forme r Fin a Bulk Fue l OilTe rmin al #1760Gre e n sboro, North Carolin a
Designed
Approved
Figure55
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Well ID Temperature (deg. C)AMW-13B 13.60 MW-A-B 22.60 MW-B-B 26.20 MW-C-B 25.10 MW-D-B 27.10 MW-E-B 22.70 MW-F-B 20.70 MW-G-B 19.80 MW-H-B 22.30 MW-I-B 19.40 PMW-J-B 18.60 PMW-K-B 17.70 PMW-L-B 16.80 PMW-M-B 17.90 PMW-N-B 13.90 PMW-O-B 13.20 PMW-P-B 16.80 PMW-Q-B 16.80 PMW-R-B 16.20 SBMW-2B 17.00
Annual Monitoring Report Former Greensboro Terminal #1760 7115 West Market Street
Greensboro, North Carolina 27409

Tables

Table 1
Well Construction Details
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Well
Type
Installation
Date
Well Screen
Material Northing Easting Well
Diameter
Land
Surface
Elevation
Top of
Casing
Elevation
Screen
Top (from
GS)
Screen
Bottom
(from GS)
Screen
Top (from
TOC)
Screen
Bottom
(from TOC)
Screen
Top
Elevation
(from TOC)
Screen
Bottom
Elevation
(from TOC)
Well
Bottom
(Depth
from GS)
Well
Bottom
Elevation
(from GS)
Well
Bottom
Elevation
(from TOC)
ft ft in ft ft ft ft ft ft ft ft ft ft ft
Onsite Wells
Z1-X1 S 3/17/2006 Stainless Steel 849833.98 1723780.19 4 901.32 904.42 5.0 25.0 8.1 28.1 896.32 876.32 25.0 873.22 876.32
Z1-X25 S 3/29/2006 Stainless Steel 849764.20 1723746.12 4 900.95 903.92 5.0 35.0 8.0 38.0 895.95 865.95 35.0 862.98 865.95
Z1-X27 S 4/21/2006 Stainless Steel 849772.89 1723901.97 4 899.08 901.92 5.0 35.0 7.8 37.8 894.08 864.08 35.0 861.24 864.08
Z1-X28 S 3/31/206 Stainless Steel 849778.55 1723626.03 4 902.23 905.14 5.0 25.0 7.9 27.9 897.23 877.23 25.0 874.32 877.23
Z2-X3 S 5/4/2006 Stainless Steel 849843.34 1723937.36 4 899.12 902.84 5.0 35.0 8.7 38.7 894.12 864.12 35.0 860.40 864.12
Z2-X16 S 5/11/2006 Stainless Steel 849929.05 1723853.41 4 899.05 902.33 5.0 35.0 8.3 38.3 894.05 864.05 35.0 860.77 864.05
Z2-X18 S 6/1/2006 Stainless Steel 849938.83 1724010.88 4 898.70 901.86 5.0 25.0 8.2 28.2 893.70 873.70 25.0 870.54 873.70
Z2-X20 S 5/18/2006 Stainless Steel 849953.91 1723891.47 4 898.93 902.16 5.0 35.0 8.2 38.2 893.93 863.93 35.0 860.70 863.93
Z2-X29 S 6/1/2006 Stainless Steel 850008.58 1724045.99 4 898.08 900.96 5.0 35.0 7.9 37.9 893.08 863.08 35.0 860.20 863.08
Z2-X31 S 5/19/2006 Stainless Steel 850019.32 1723848.90 4 899.28 902.94 5.0 35.0 8.7 38.7 894.28 864.28 35.0 860.62 864.28
Z2-X35 S 5/25/2006 Stainless Steel 850049.38 1723965.12 4 897.74 900.96 5.0 35.0 8.2 38.2 892.74 862.74 35.0 859.52 862.74
Z2-PZ-6 S NA PVC NA NA 1 NA NA NA NA NA NA NA NA NA NA NA
Z2-PZ-8 S NA PVC 850075.22 1723987.30 1 897.11 899.29 NA NA NA NA NA NA NA NA NA
Z2-PZ-9 S NA PVC 850115.43 1723924.09 1 896.09 898.31 NA NA NA NA NA NA NA NA NA
Z2-PZ-10 S NA PVC NA NA 1 NA NA NA NA NA NA NA NA NA NA NA
Z3-X80 S 10/21/2009 Stainless Steel 850047.54 1723748.58 4 899.50 902.87 5.0 35.0 8.4 38.4 894.50 864.50 35.0 861.13 864.50
Z3-X82 S 10/22/2009 Stainless Steel 849978.31 1723712.46 4 899.92 903.51 5.0 35.0 8.6 38.6 894.92 864.92 35.0 861.33 864.92
Z4-X21 S 8/18/2010 Stainless Steel 850173.19 1723543.24 4 896.72 898.56 8.0 33.0 9.8 34.8 888.72 863.72 33.0 861.88 863.72
Z4-X30 S 8/23/2010 Stainless Steel 850206.42 1723764.69 4 895.97 897.55 8.0 43.0 9.6 44.6 887.97 852.97 43.0 851.39 852.97
Z4-X35 S 9/11/2010 Stainless Steel 850212.87 1723639.37 4 896.87 898.53 8.0 43.0 9.7 44.7 888.87 853.87 43.0 852.21 853.87
Z4-X47 S 8/28/2010 Stainless Steel 850269.50 1723670.07 4 895.24 896.98 8.0 43.0 9.7 44.7 887.24 852.24 43.0 850.50 852.24
Z4-X55 S 9/10/2010 Stainless Steel 850309.01 1723529.66 4 896.26 897.94 8.0 38.0 9.7 39.7 888.26 858.26 38.0 856.58 858.26
Z4-X63 S 11/21/2011 Stainless Steel 850107.67 1723632.83 4 898.38 898.68 18.0 38.0 18.3 38.3 880.38 860.38 38.0 860.08 860.38
Z4-X68 S 12/1/2011 Stainless Steel 850119.57 1723842.87 4 898.29 898.27 18.0 38.0 18.0 38.0 880.29 860.29 38.0 860.31 860.29
Z4-X70 S 12/7/2011 Stainless Steel 850146.99 1723677.62 4 898.06 898.06 18.0 48.0 18.0 48.0 880.06 850.06 48.0 850.06 850.06
Z4-X72 S 12/6/2011 Stainless Steel 850154.62 1723781.99 4 897.92 897.98 18.0 48.0 18.1 48.1 879.92 849.92 48.0 849.86 849.92
Z4-X89 S 5/4/2012 Stainless Steel 850113.53 1723700.31 4 898.58 901.77 8.0 38.0 11.2 41.2 890.58 860.58 38.0 857.39 860.58
Z4-PZ4 S 8/9/2010 PVC 850152.92 1723892.04 1 896.50 898.53 5.0 25.0 7.0 27.0 891.50 871.50 25.0 869.47 871.50
Z4-PZ7 S 8/9/2010 PVC 850236.83 1723772.60 1 895.40 898.90 5.0 25.0 8.5 28.5 890.40 870.40 25.0 866.90 870.40
Z4-PZ9 S 8/9/2010 PVC 850328.88 1723513.90 1 896.73 898.88 5.0 25.0 7.1 27.2 891.73 871.73 25.0 869.58 871.73
MW-A-I I 10/9/2015 PVC 849781.30 1723762.00 2 900.40 902.43 37.0 47.0 39.0 49.0 863.40 853.40 47.0 851.37 853.40
MW-A-D D 10/8/2015 PVC 849777.40 1723757.70 2 900.40 902.71 57.0 67.0 59.3 69.3 843.40 833.40 67.0 831.09 833.40
MW-A-B B 11/18/2015 Open 849786.10 1723751.10 6 900.40 899.96 82.0 92.0 81.6 91.6 818.40 808.40 92.0 808.84 808.40
MW-B-I I 9/22/2015 PVC 850032.90 1723760.20 2 898.50 901.28 35.0 45.0 37.8 47.8 863.50 853.50 45.0 850.72 853.50
MW-B-D D 9/22/2015 PVC 850026.80 1723761.30 2 898.60 901.18 67.0 77.0 69.6 79.6 831.60 821.60 77.0 819.02 821.60
MW-B-B B 11/18/2015 Open 850026.90 1723750.00 6 898.90 898.57 96.0 111.0 95.7 110.7 802.90 787.90 111.0 788.23 787.90
MW-C-I I 9/23/2015 PVC 850099.30 1723709.00 2 897.90 900.29 41.0 51.0 43.4 53.4 856.90 846.90 51.0 844.51 846.90
MW-C-D D 9/24/2015 PVC 850105.30 1723710.20 2 897.80 900.35 69.0 79.0 71.6 81.6 828.80 818.80 79.0 816.25 818.80
MW-C-B B 11/18/2015 Open 850099.00 1723720.30 6 898.00 897.68 96.0 130.0 95.7 129.7 802.00 768.00 130.0 768.32 768.00
Units
Page 1 of 4
Table 1
Well Construction Details
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Well
Type
Installation
Date
Well Screen
Material Northing Easting Well
Diameter
Land
Surface
Elevation
Top of
Casing
Elevation
Screen
Top (from
GS)
Screen
Bottom
(from GS)
Screen
Top (from
TOC)
Screen
Bottom
(from TOC)
Screen
Top
Elevation
(from TOC)
Screen
Bottom
Elevation
(from TOC)
Well
Bottom
(Depth
from GS)
Well
Bottom
Elevation
(from GS)
Well
Bottom
Elevation
(from TOC)
MW-D-I I 9/22/2015 PVC 850004.40 1723823.00 2 898.80 901.15 31.0 41.0 33.4 43.4 867.80 857.80 41.0 855.45 857.80
MW-D-D D 9/23/2015 PVC 850007.10 1723829.20 2 898.70 901.06 67.0 77.0 69.4 79.4 831.70 821.70 77.0 819.34 821.70
MW-D-B B 11/18/2015 Open 859995.10 1723828.60 6 899.10 898.81 96.0 106.0 95.7 105.7 803.10 793.10 106.0 793.39 793.10
MW-E-I I 9/29/2015 PVC 850282.80 1723633.00 2 894.30 896.94 42.0 52.0 44.6 54.6 852.30 842.30 52.0 839.66 842.30
MW-E-D D 9/28/2015 PVC 850284.84 1723629.02 2 894.30 897.11 72.0 82.0 74.8 84.8 822.30 812.30 82.0 809.49 812.30
MW-E-B B 11/18/2015 Open 850273.38 1723624.84 6 895.10 894.89 100.0 110.0 99.8 109.8 795.10 785.10 110.0 785.31 785.10
MW-F-I I 9/30/2015 PVC 850196.35 1723780.41 2 894.70 896.86 37.0 47.0 39.2 49.2 857.70 847.70 47.0 845.54 847.70
MW-F-D D 9/29/2015 PVC 850193.37 1723784.86 2 894.80 896.94 81.0 91.0 83.1 93.1 813.80 803.80 91.0 801.66 803.80
MW-F-B B 11/18/2015 Open 850185.65 1723773.72 6 895.60 895.34 106.0 116.0 105.7 115.7 789.60 779.60 116.0 779.86 779.60
MW-G-I I 10/7/2015 PVC 850133.67 1723861.51 2 896.00 898.12 32.0 42.0 34.1 44.1 864.00 854.00 42.0 851.88 854.00
MW-G-D D 10/1/2015 PVC 850130.29 1723868.70 2 896.00 898.40 47.0 57.0 49.4 59.4 849.00 839.00 57.0 836.60 839.00
MW-G-B B 11/18/2015 Open 850122.74 1723860.21 6 897.00 896.78 74.0 84.0 73.8 83.8 823.00 813.00 84.0 813.22 813.00
MW-H-I I 10/8/2015 PVC 850066.59 1723955.43 2 897.10 899.78 34.0 44.0 36.7 46.7 863.10 853.10 44.0 850.42 853.10
MW-H-D D 10/6/2015 PVC 850061.52 1723960.73 2 896.90 899.54 54.0 64.0 56.6 66.6 842.90 832.90 64.0 830.26 832.90
MW-H-B B 11/20/2015 Open 850055.33 1723949.56 6 897.40 897.00 81.0 91.0 80.6 90.6 816.40 806.40 91.0 806.80 806.40
MW-I-I I 10/9/2015 PVC 850016.84 1724015.81 2 897.70 900.21 42.0 52.0 44.5 54.5 855.70 845.70 52.0 843.19 845.70
MW-I-D D 10/7/2015 PVC 850011.28 1724022.53 2 897.80 900.11 67.0 77.0 69.3 79.3 830.80 820.80 77.0 818.49 820.80
MW-I-B B 11/20/2015 Open 850006.67 1724012.85 6 895.10 897.56 94.0 104.0 96.5 106.5 801.10 791.10 104.0 788.64 791.10
AMW-8S S 7/18/2003 PVC 850650.04 1723632.51 2 886.98 889.93 5.0 25.0 7.9 27.9 881.98 861.98 25.0 859.03 861.98
AMW-9S S 7/18/2003 PVC 850568.02 1723731.41 2 886.80 889.74 3.0 23.0 5.9 25.9 883.80 863.80 23.0 860.86 863.80
AMW-10S S 7/21/2003 PVC 850216.66 1724238.63 2 889.85 892.90 3.0 23.0 6.0 26.1 886.85 866.85 23.0 863.80 866.85
AMW-11S S 7/17/2003 PVC 850798.42 1723852.88 2 882.07 884.86 3.0 18.0 5.8 20.8 879.07 864.07 18.0 861.28 864.07
AMW-12S S 7/21/2003 PVC 850043.37 1724478.76 2 894.33 897.26 5.0 25.0 7.9 27.9 889.33 869.33 25.0 866.40 869.33
AMW-13B B 4/22/2004 PVC 850812.53 1723921.58 2 880.85 883.77 85.0 90.0 87.9 92.9 795.85 790.85 90.0 787.93 790.85
AMW-13S S 7/17/2003 PVC 850825.51 1723940.41 2 879.97 883.17 3.0 18.0 6.2 21.2 876.97 861.97 18.0 858.77 861.97
AMW-13I I 4/27/2004 PVC 850821.70 1723934.34 2 880.10 882.35 40.0 45.0 42.3 47.3 840.10 835.10 45.0 832.85 835.10
AMW-13D D 4/27/2004 PVC 850816.73 1723927.78 2 880.34 883.19 56.0 61.0 58.9 63.9 824.34 819.34 61.0 816.49 819.34
AMW-14S S 7/16/2003 PVC 850495.30 1724188.03 2 886.87 890.35 5.0 25.0 8.5 28.5 881.87 861.87 25.0 858.39 861.87
AMW-15S S 7/17/2003 PVC 850843.30 1724173.38 2 878.54 881.42 3.0 18.0 5.9 20.9 875.54 860.54 18.0 857.66 860.54
AMW-16S S 7/17/2003 PVC 850857.36 1724140.07 2 877.25 880.34 3.0 18.0 6.1 21.1 874.25 859.25 18.0 856.16 859.25
AMW-17S S 7/17/2003 PVC 850856.41 1724121.25 2 876.75 879.81 3.0 18.0 6.1 21.1 873.75 858.75 18.0 855.69 858.75
MW-18S S 7/17/2003 PVC 850855.59 1724100.21 2 877.07 879.96 3.0 18.0 5.9 20.9 874.07 859.07 18.0 856.18 859.07
DEM-MW6R S 7/16/2003 PVC 850602.56 1724030.59 2 889.30 892.77 5.0 30.0 8.5 33.5 884.30 859.30 18.0 855.83 859.30
DEM-MW-6I I 11/5/2003 PVC 850590.52 1724046.31 2 888.59 891.02 40.5 45.5 42.9 47.9 848.09 843.09 45.5 840.66 843.09
DEM-MW-6D D 10/30/2003 PVC 850598.51 1724036.28 2 889.06 891.12 64.5 69.5 66.6 71.6 824.56 819.56 69.5 817.50 819.56
FMW-15 S 6/20/1995 PVC 849304.21 1723329.15 2 900.43 902.76 10.0 24.5 12.3 26.8 890.43 875.93 24.5 873.60 875.93
FMW-20 S 6/21/1995 PVC 851012.85 1723876.25 2 887.52 889.46 12.0 27.0 13.9 28.9 875.52 860.52 27.0 858.58 860.52
FMW-21 S 6/21/1995 PVC 850766.90 1724218.54 2 882.21 884.52 6.0 18.0 8.3 20.3 876.21 864.21 18.0 861.90 864.21
Off-site Wells
Page 2 of 4
Table 1
Well Construction Details
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Well
Type
Installation
Date
Well Screen
Material Northing Easting Well
Diameter
Land
Surface
Elevation
Top of
Casing
Elevation
Screen
Top (from
GS)
Screen
Bottom
(from GS)
Screen
Top (from
TOC)
Screen
Bottom
(from TOC)
Screen
Top
Elevation
(from TOC)
Screen
Bottom
Elevation
(from TOC)
Well
Bottom
(Depth
from GS)
Well
Bottom
Elevation
(from GS)
Well
Bottom
Elevation
(from TOC)
FMW-22 S 6/21/1995 PVC 850453.09 1724555.44 2 886.07 888.28 6.0 15.5 8.2 17.7 880.07 870.57 17.2 868.36 870.57
FMW-23R S 7/17/2003 PVC 850725.32 1723857.92 2 884.41 887.45 3.0 18.0 6.0 21.0 881.41 866.41 18.0 863.37 866.41
FMW-24 S 6/22/1995 PVC 850666.98 1723738.71 2 885.66 888.02 5.5 20.0 7.9 22.4 880.16 865.66 22.6 863.30 865.66
FMW-24I I 11/5/2003 PVC 850674.56 1723721.70 2 885.74 888.25 40.5 45.5 43.0 48.0 845.24 840.24 45.5 837.73 840.24
FMW-24D D 11/4/2003 PVC 850671.50 1723729.36 2 885.75 888.11 60.0 70.0 62.4 72.4 825.75 815.75 70.0 813.39 815.75
FPZ-5 S 6/21/1995 PVC 850990.57 1724286.16 2 873.30 874.79 4.0 8.3 5.5 9.8 869.30 865.00 NA 863.51 865.00
FPZ-6 S 5/15/1997 PVC 850845.65 1723975.25 2 879.17 881.55 1.5 15.0 3.9 17.4 877.67 864.17 17.8 861.79 864.17
FPZ-7 S 5/15/1997 PVC 850893.86 1724074.45 2 876.61 878.84 1.5 15.0 3.7 17.2 875.11 861.61 17.1 859.38 861.61
FPZ-8 S 5/15/1997 PVC 850877.93 1724183.50 2 877.38 879.30 1.5 15.0 3.4 16.9 875.88 862.38 17.1 860.46 862.38
FPZ-10 S 5/16/1997 PVC 850836.22 1724126.60 2 877.75 880.01 1.5 15.0 3.8 17.3 876.25 862.75 17.1 860.49 862.75
FPZ-10I I 11/5/2003 PVC 850826.13 1724126.58 2 877.68 880.45 40.0 45.0 42.8 47.8 837.68 832.68 45.0 829.91 832.68
FPZ-11 S 5/16/1997 PVC 850877.15 1723954.60 2 878.91 880.95 1.5 15.0 3.5 17.0 877.41 863.91 17.5 861.87 863.91
FPZ-12 S 12/19/2002 PVC 850979.68 1724149.04 2 874.50 877.68 1.5 18.5 4.7 21.7 873.00 856.00 18.5 852.82 856.00
FPZ-12I I 11/5/2003 PVC 850978.69 1724140.54 2 874.48 877.63 40.5 45.5 43.7 48.7 833.98 828.98 45.5 825.83 828.98
FPZ-13 S 12/19/2002 PVC 850894.28 1724164.45 2 876.34 880.15 1.5 16.5 5.3 20.3 874.84 859.84 17.0 856.03 859.84
FPZ-14 S 12/19/2002 PVC 850891.45 1724141.76 2 876.17 879.87 1.5 16.5 5.2 20.2 874.67 859.67 17.0 855.97 859.67
FPZ-15 S 12/19/2002 PVC 850858.70 1724159.15 2 877.61 881.16 1.5 16.5 5.0 20.1 876.11 861.11 17.0 857.56 861.11
OW-1 S 7/11/1997 PVC 850887.03 1723905.30 4 880.59 883.49 1.5 12.0 4.4 14.9 879.09 868.59 14.8 865.69 868.59
OW-2 S 7/17/1997 PVC 850873.38 1724118.03 4 876.17 879.61 1.5 12.0 4.9 15.4 874.67 864.17 15.4 860.73 864.17
OW-3 S 7/18/1997 PVC 850839.57 1724195.32 4 878.98 882.42 1.5 12.0 4.9 15.4 877.48 866.98 15.4 863.54 866.98
OW-4 S 7/18/2003 PVC 850872.85 1724085.35 2 876.73 879.85 2.0 10.0 5.1 13.1 874.73 866.73 10.0 863.61 866.73
OW-6 S 7/18/2003 PVC 850873.60 1724138.19 2 876.60 879.45 2.0 10.0 4.9 12.9 874.60 866.60 10.0 863.75 866.60
OW-7 S 7/17/2003 PVC 850925.56 1723861.29 2 883.99 887.09 3.0 18.0 6.1 21.1 880.99 865.99 18.0 862.89 865.99
OW-8 S 7/16/2003 PVC 850701.37 1724251.12 2 885.12 887.97 3.0 18.0 5.9 20.9 882.12 867.12 18.0 864.27 867.12
RW-1 S 7/14/1997 PVC 850861.30 1723943.35 4 879.01 882.22 1.5 12.0 4.7 15.2 877.51 867.01 12.0 863.80 867.01
RW-2 S 7/17/1997 PVC 850874.31 1724170.97 4 877.33 880.44 1.5 12.0 4.6 15.1 875.83 865.33 12.0 862.22 865.33
SBMW-1R S 7/18/2003 PVC 850318.95 1724084.37 2 890.11 893.18 3.0 23.0 6.1 26.1 887.11 867.11 23.0 864.04 867.11
SBMW-2R S 7/18/2003 PVC 850473.05 1723863.59 2 888.47 891.54 3.0 23.0 6.1 26.1 885.47 865.47 23.0 862.40 865.47
SBMW-2I I 11/5/2003 PVC 850454.40 1723887.92 2 888.53 891.18 40.0 45.0 42.7 47.7 848.53 843.53 45.0 840.88 843.53
SBMW-2D D 10/31/2003 PVC 850464.41 1723875.24 2 888.47 890.80 65.0 70.0 67.3 72.3 823.47 818.47 70.0 816.14 818.47
SBMW-2B B 4/22/2004 PVC 850445.15 1723901.79 2 888.91 892.06 93.5 98.5 96.7 101.7 795.41 790.41 98.5 787.26 790.41
PMW-J-I I 1/19/2017 PVC 850636.11 1723649.08 2 885.90 888.45 52.0 62.0 54.6 64.6 833.90 823.90 62.0 821.35 823.90
PMW-J-D D 1/19/2017 PVC 850636.22 1723641.15 2 885.90 888.35 89.0 99.0 91.5 101.5 796.90 786.90 99.0 784.45 786.90
PMW-J-B B 2/1/2017 Open 850629.97 1723654.18 6 885.90 885.57 114.0 126.0 113.7 125.7 771.90 759.90 126.0 760.23 759.90
PMW-K-I I 1/19/2017 PVC 850332.88 1724067.61 2 889.30 891.75 33.0 43.0 35.5 45.5 856.30 846.30 43.0 843.85 846.30
PMW-K-D D 12/21/2016 PVC 850328.75 1724080.49 2 889.30 892.16 52.0 62.0 54.9 64.9 837.30 827.30 62.0 824.44 827.30
PMW-K-B B 1/19/2017 Open 850324.46 1724080.49 6 889.30 889.07 77.0 87.0 76.8 86.8 812.30 802.30 87.0 802.53 802.30
PMW-L-I I 1/4/2017 PVC 850232.47 1724221.18 2 888.80 891.23 25.0 35.0 27.4 37.4 863.80 853.80 35.0 851.37 853.80
PMW-L-D D 12/20/2016 PVC 850226.72 1724227.35 2 888.80 891.57 50.0 60.0 52.8 62.8 838.80 828.80 60.0 826.03 828.80
PMW-L-B B 1/19/2017 Open 850220.11 1724235.10 6 888.80 888.56 75.0 85.0 74.8 84.8 813.80 803.80 85.0 804.04 803.80
PMW-M-I I 1/19/2017 PVC 850654.80 1723860.05 2 885.50 888.48 40.0 50.0 43.0 53.0 845.50 835.50 50.0 832.52 835.50
Page 3 of 4
Table 1
Well Construction Details
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Well
Type
Installation
Date
Well Screen
Material Northing Easting Well
Diameter
Land
Surface
Elevation
Top of
Casing
Elevation
Screen
Top (from
GS)
Screen
Bottom
(from GS)
Screen
Top (from
TOC)
Screen
Bottom
(from TOC)
Screen
Top
Elevation
(from TOC)
Screen
Bottom
Elevation
(from TOC)
Well
Bottom
(Depth
from GS)
Well
Bottom
Elevation
(from GS)
Well
Bottom
Elevation
(from TOC)
PMW-M-D D 1/19/2017 PVC 850649.79 1723855.80 2 885.50 888.10 73.0 83.0 75.6 85.6 812.50 802.50 83.0 799.90 802.50
PMW-M-B B 1/19/2017 Open 850652.09 1723849.72 6 885.50 885.06 98.0 145.0 97.6 144.6 787.50 740.50 145.0 740.94 740.50
PMW-N-I I 1/19/2017 PVC 850581.48 1724202.07 2 885.40 888.48 40.0 50.0 43.1 53.1 845.40 835.40 50.0 832.32 835.40
PMW-N-D D 12/22/2016 PVC 850573.52 1724201.62 2 885.40 888.26 66.0 76.0 68.9 78.9 819.40 809.40 76.0 806.54 809.40
PMW-N-B B 1/19/2017 Open 850577.51 1724196.10 6 885.40 885.18 91.0 111.0 90.8 110.8 794.40 774.40 111.0 774.62 774.40
PMW-O-I I 1/19/2017 PVC 850883.79 1723953.87 2 877.75 880.66 50.0 60.0 52.9 62.9 827.75 817.75 60.0 814.84 817.75
PMW-O-D D 1/19/2017 PVC 850886.22 1723959.89 2 877.75 880.10 92.0 102.0 94.4 104.4 785.75 775.75 102.0 773.40 775.75
PMW-O-B B 2/1/2017 Open 850891.70 1723958.93 6 877.75 877.39 116.0 145.0 115.6 144.6 761.75 732.75 145.0 733.11 732.75
PMW-P-S S 1/4/2018 PVC 851615.95 1724138.01 2 880.26 883.26 3.0 18.0 6.0 21.0 877.26 862.26 145.0 859.26 862.26
PMW-P-I I 1/3/2018 PVC 851618.07 1724133.26 2 880.18 883.38 50.0 60.0 53.2 63.2 830.18 820.18 145.0 816.98 820.18
PMW-P-D D 12/11/2017 PVC 851610.95 1724135.58 2 880.00 883.36 80.0 90.0 83.4 93.4 800.00 790.00 145.0 786.64 790.00
PMW-P-B B 1/9/2018 Open 851618.73 1724133.21 6 880.32 879.84 95.0 105.0 94.5 104.5 785.32 775.32 145.0 775.80 775.32
PMW-Q-S S 1/3/2018 PVC 851610.01 1724290.98 2 875.25 878.60 3.0 18.0 6.4 21.4 872.25 857.25 145.0 853.90 857.25
PMW-Q-I I 12/13/2017 PVC 851604.72 1724292.70 2 875.04 878.29 25.0 35.0 28.3 38.3 850.04 840.04 145.0 836.79 840.04
PMW-Q-D D 12/13/2017 PVC 851599.87 1724290.07 2 875.06 878.28 49.0 59.0 52.2 62.2 826.06 816.06 145.0 812.84 816.06
PMW-Q-B B 1/9/2018 Open 851617.97 1724289.82 6 875.44 874.95 75.5 85.0 75.0 84.5 799.94 790.44 145.0 790.93 790.44
PMW-R-S S 12/13/2017 PVC 851596.52 1724458.48 2 873.84 877.23 3.0 18.0 6.4 21.4 870.84 855.84 145.0 852.45 855.84
PMW-R-I I 12/13/2017 PVC 851595.18 1724455.21 2 873.72 877.03 20.0 30.0 23.3 33.3 853.72 843.72 145.0 840.41 843.72
PMW-R-D D 12/13/2017 PVC 851593.38 1724458.18 2 873.71 877.20 40.0 50.0 43.5 53.5 833.71 823.71 145.0 820.22 823.71
PMW-R-B B 1/10/2018 Open 851582.17 1724455.85 6 873.98 873.47 147.0 157.0 146.5 156.5 726.98 716.98 145.0 717.49 716.98
SG-1 S 12/1/2016 NA 851053.24 1724212.61 NA 871.50 NA NA NA NA NA NA NA N N N
Notes:
in - inch
ft - feet
GS - ground surface
TOC - top of casing
S - shallow
I - intermediate
B - bedrock
D - deep
NA - not applicable
PVC - polyvinyl chloride
SG-1 - stream gauge
Page 4 of 4
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Units - ft ft ft ft ft
Z1-X01 5/9/2006 903.59 - - 20.18 883.41
Z1-X01 6/27/2006 903.59 19.22 0.01 19.23 884.37
Z1-X01 9/13/2006 903.59 - - 17.79 885.80
Z1-X01 10/24/2006 903.59 - - 17.71 885.88
Z1-X01 10/31/2006 903.59 - - 19.05 884.54
Z1-X01 7/17/2007 903.59 21.05 0.01 21.06 882.54
Z1-X01 10/10/2007 903.59 24.30 0.01 24.31 879.29
Z1-X01 3/21/2008 903.59 - - 23.28 880.31
Z1-X01 5/5/2008 903.59 - - 21.59 882.00
Z1-X01 7/21/2008 903.59 - - 21.78 881.81
Z1-X01 3/25/2009 903.59 - - 20.67 882.92
Z1-X01 5/22/2009 903.59 - - 18.15 885.44
Z1-X01 11/5/2010 904.42 - - 22.11 882.31
Z1-X01 5/24/2011 904.42 - - 20.49 883.93
Z1-X01 4/16/2013 904.42 - - 19.74 884.68
Z1-X01 10/26/2015 904.42 - -22.31 882.11
Z1-X01 5/9/2006 904.42 21.32 0.01 21.33 883.10
Z1-X01 6/27/2006 904.42 - - 20.83 883.59
Z1-X01 9/13/2006 904.42 - - 19.60 884.82
Z1-X01 10/24/2006 904.42 - - 19.35 885.07
Z1-X01 10/31/2006 904.42 - - 19.57 884.85
Z1-X01 7/17/2007 904.42 - - 21.36 883.06
Z1-X01 10/10/2007 904.42 25.30 0.01 25.31 879.12
Z1-X01 3/21/2008 904.42 24.64 0.04 24.68 879.77
Z1-X01 5/5/2008 904.42 23.16 0.06 23.22 881.25
Z1-X01 7/21/2008 904.42 22.60 0.09 22.69 881.80
Z1-X01 3/25/2009 904.42 - - 22.93 881.49
Z1-X01 4/16/2013 904.42 - - 19.74 884.68
Z1-X01 10/26/2015 904.42 - - 22.31 882.11
Z1-X01 7/11/2016 904.42 - - 17.76 886.66
Z1-X01 7/12/2016 904.42 - - 17.76 886.66
Z1-X01 7/15/2016 904.42 - - 17.89 886.53
Z1-X01 11/28/2016 904.42 - - 23.46 880.96
Z1-X01 12/15/2016 904.42 - - 24.97 879.45
Z1-X01 6/26/2017 904.42 - - 17.35 887.07
Z1-X01 12/11/2017 904.42 - - 27.90 876.52
Z1-X01 7/9/2018 904.42 - - 21.99 882.43
Page 1 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z1-X01 12/12/2018 904.42 - - 16.87 887.55
Z1-X01 6/10/2019 904.42 - - 16.21 888.21
Z1-X01 12/9/2019 904.42 - - 18.20 886.22
Z1-X01 6/11/2020 904.42 - - 13.07 891.35
Z1-X01 12/14/2020 904.42 - - 13.31 891.11
Z1-X01 6/14/2021 904.42 - - 16.23 888.19
Z1-X01 6/20/2022 904.42 - - 18.94 885.48
Z1-X01 7/17/2023 904.42 - - 18.94 885.48
Z1-X09 11/28/2016 NA - - 24.45 NA
Z1-X09 7/9/2018 NA - - 23.11 NA
Z1-X25 5/9/2006 903.09 21.1 0.01 21.11 881.99
Z1-X25 6/27/2006 903.09 - - 20.94 882.15
Z1-X25 9/13/2006 903.09 - - 19.90 883.19
Z1-X25 10/24/2006 903.09 - - 19.45 883.64
Z1-X25 10/31/2006 903.09 - - 20.61 882.48
Z1-X25 7/17/2007 903.09 21.06 0.01 21.07 882.03
Z1-X25 7/21/2008 903.09 - - 21.92 881.17
Z1-X25 5/22/2009 903.09 - - 18.85 884.24
Z1-X25 5/24/2011 903.92 - - 21.95 881.97
Z1-X25 4/16/2013 903.92 - - 21.43 882.49
Z1-X25 10/26/2015 903.92 - - 24.01 879.91
Z1-X25 7/11/2016 903.92 - - 19.39 884.53
Z1-X25 7/12/2016 903.92 - - 19.39 884.53
Z1-X25 7/15/2016 903.92 - - 19.48 884.44
Z1-X25 11/28/2016 903.92 - - 24.31 879.61
Z1-X25 12/15/2016 903.92 - - 24.85 879.07
Z1-X25 6/26/2017 903.92 - - 20.73 883.19
Z1-X25 12/11/2017 903.92 - - 26.68 877.24
Z1-X25 7/9/2018 903.92 - - 21.99 881.93
Z1-X25 12/12/2018 903.92 - - 18.57 885.35
Z1-X25 6/10/2019 903.92 - - 17.23 886.69
Z1-X25 12/9/2019 903.92 - - 20.17 883.75
Z1-X25 6/11/2020 903.92 - - 14.30 889.62
Z1-X25 12/14/2020 903.92 - - 15.69 888.23
Z1-X25 6/14/2021 903.92 - - 17.04 886.88
Z1-X25 6/20/2022 903.92 - - 21.30 882.62
Page 2 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z1-X25 7/17/2023 903.92 - - 20.16 883.76
Z1-X27 5/9/2006 901.15 18.35 0.01 18.36 882.80
Z1-X27 6/27/2006 901.15 - - 17.21 883.94
Z1-X27 9/13/2006 901.15 - - 16.05 885.10
Z1-X27 10/24/2006 901.15 - - 16.08 885.07
Z1-X27 10/31/2006 901.15 - - 17.40 883.75
Z1-X27 7/17/2007 901.15 - - 19.60 881.55
Z1-X27 7/21/2008 901.15 - - 19.16 881.99
Z1-X27 5/22/2009 901.15 - - 15.33 885.82
Z1-X27 5/24/2011 901.92 - - 19.87 882.05
Z1-X27 4/16/2013 901.92 - - 18.10 883.82
Z1-X27 10/26/2015 901.92 - - 20.61 881.31
Z1-X27 7/11/2016 901.92 - - 16.02 885.90
Z1-X27 7/12/2016 901.92 - - 16.02 885.90
Z1-X27 7/18/2016 901.92 - - 16.32 885.60
Z1-X27 11/28/2016 901.92 - - 21.49 880.43
Z1-X27 12/15/2016 901.92 - - 21.83 880.09
Z1-X27 6/26/2017 901.92 - - 16.28 885.64
Z1-X27 12/11/2017 901.92 - - 23.76 878.16
Z1-X27 7/9/2018 901.92 - - 23.22 878.70
Z1-X27 12/12/2018 901.92 - - 15.04 886.88
Z1-X27 6/10/2019 901.92 - - 14.23 887.69
Z1-X27 12/9/2019 901.92 - - 16.88 885.04
Z1-X27 6/11/2020 901.92 - - 11.36 890.56
Z1-X27 12/14/2020 901.92 - - 13.20 888.72
Z1-X27 6/14/2021 901.92 - - 14.62 887.30
Z1-X27 6/20/2022 901.92 18.69 883.23
Z1-X27 7/17/2023 901.92 17.18 884.74
Z1-X28 5/9/2006 904.31 - - 23.00 881.31
Z1-X28 6/27/2006 904.31 - - 22.94 881.37
Z1-X28 9/13/2006 904.31 - - 22.11 882.20
Z1-X28 10/24/2006 904.31 - - 22.57 881.74
Z1-X28 10/31/2006 904.31 - -22.61 881.70
Z1-X28 7/17/2007 904.31 - - 20.79 883.52
Z1-X28 10/10/2007 904.31 25.18 0.11 25.29 879.10
Z1-X28 3/21/2008 904.31 - - 25.94 878.37
Page 3 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z1-X28 5/5/2008 904.31 24.75 0.64 25.39 879.40
Z1-X28 7/21/2008 904.31 24.60 0.77 25.37 879.52
Z1-X28 3/25/2009 904.31 - - 24.55 879.76
Z1-X28 5/22/2009 904.31 - - 21.33 882.98
Z1-X28 11/5/2010 905.14 - - 25.00 880.14
Z1-X28 5/24/2011 905.14 - - 23.98 881.16
Z1-X28 4/16/2013 905.14 - - 23.73 881.41
Z1-X28 10/26/2015 905.14 - -26.31 878.83
Z1-X28 7/11/2016 905.14 - - 21.64 883.50
Z1-X28 7/12/2016 905.14 - - 21.64 883.50
Z1-X28 7/18/2016 905.14 - - 21.73 883.41
Z1-X28 11/28/2016 905.14 - - 26.39 878.75
Z1-X28 12/12/2016 905.14 - - 26.70 878.44
Z1-X28 6/26/2017 905.14 - - 23.33 881.81
Z1-X28 12/11/2017 905.14 - - Dry NA
Z1-X28 1/25/2018 905.14 - - Dry NA
Z1-X28 7/9/2018 905.14 - - 25.31 879.83
Z1-X28 12/12/2018 905.14 - - 21.33 883.81
Z1-X28 6/10/2019 905.14 - - 19.39 885.75
Z1-X28 12/9/2019 905.14 - - 22.48 882.66
Z1-X28 6/11/2020 905.14 - - 17.10 888.04
Z1-X28 12/14/2020 905.14 - - 18.98 886.16
Z1-X28 6/14/2021 905.14 - - 19.02 886.12
Z1-X28 6/20/2022 905.14 - - 24.43 880.71
Z1-X28 7/17/2023 905.14 - - 22.39 882.75
Z2-PZ-06 10/26/2015 NA - -19.91 NA
Z2-PZ-06 7/11/2016 NA - - 15.86 NA
Z2-PZ-06 7/12/2016 NA - - 15.86 NA
Z2-PZ-06 7/15/2016 NA - - 16.22 NA
Z2-PZ-06 7/19/2016 NA - - 14.00 NA
Z2-PZ-06 11/28/2016 NA - - 22.11 NA
Z2-PZ-06 6/26/2017 NA - - 19.93 NA
Z2-PZ-06 12/11/2017 NA - - 24.20 NA
Z2-PZ-06 7/9/2018 NA - - 21.01 NA
Z2-PZ-06 12/12/2018 NA - - 14.63 NA
Z2-PZ-06 6/10/2019 NA - - 14.74 NA
Z2-PZ-06 12/9/2019 NA - - 15.60 NA
Page 4 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z2-PZ-06 6/11/2020 NA - - 11.98 NA
Z2-PZ-06 12/14/2020 NA - - 10.99 NA
Z2-PZ-06 6/14/2021 NA - - 15.51 NA
Z2-PZ-06 6/20/2022 NA - - 19.61 NA
Z2-PZ-06 7/17/2023 NA - - 19.97 NA
Z2-PZ-08 10/26/2015 NA - -17.35 NA
Z2-PZ-08 7/11/2016 NA - - 14.64 NA
Z2-PZ-08 7/12/2016 NA - - 14.64 NA
Z2-PZ-08 7/19/2016 NA - - 15.68 NA
Z2-PZ-08 11/28/2016 NA - - 21.40 NA
Z2-PZ-08 6/26/2017 899.29 - - 12.32 886.97
Z2-PZ-08 12/11/2017 899.29 - - NA NA
Z2-PZ-08 7/9/2018 899.29 - - 20.41 878.88
Z2-PZ-08 12/12/2018 899.29 - - NA NA
Z2-PZ-08 6/10/2019 899.29 - - 13.39 885.90
Z2-PZ-08 12/9/2019 899.29 - - 9.50 889.79
Z2-PZ-08 12/14/2020 899.29 - - 9.73 889.56
Z2-PZ-08 6/14/2021 899.29 - - 14.51 884.78
Z2-PZ-08 6/20/2022 899.29 - - 18.55 880.74
Z2-PZ-08 7/17/2023 899.29 - - 21.09 878.20
Z2-PZ-09 7/11/2016 NA - - 16.34 NA
Z2-PZ-09 7/12/2016 NA - - 16.34 NA
Z2-PZ-09 7/18/2016 NA - - 17.87 NA
Z2-PZ-09 11/28/2016 NA - - 21.86 NA
Z2-PZ-09 6/26/2017 898.31 - - 16.19 882.12
Z2-PZ-09 12/11/2017 898.31 - - 24.10 874.21
Z2-PZ-09 7/9/2018 898.31 - - 19.76 878.55
Z2-PZ-09 12/12/2018 898.31 - - 15.63 882.68
Z2-PZ-09 6/10/2019 898.31 - - 15.01 883.30
Z2-PZ-09 12/9/2019 898.31 - - 17.09 881.22
Z2-PZ-09 6/11/2020 898.31 - - 12.47 885.84
Z2-PZ-09 12/14/2020 898.31 - - 11.98 886.33
Z2-PZ-09 6/14/2021 898.31 - - 15.05 883.26
Z2-PZ-09 6/20/2022 898.31 - - 7.49 890.82
Z2-PZ-09 12/5/2022 898.31 - - 18.00 880.31
Z2-PZ-09 7/17/2023 898.31 - - 19.71 878.60
Page 5 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z2-PZ-09 2/2/2024 898.31 - - 15.03 883.28
Z2-PZ-10 10/26/2015 NA - -21.35 NA
Z2-PZ-10 7/11/2016 NA - - 16.88 NA
Z2-PZ-10 7/12/2016 NA - - 16.88 NA
Z2-PZ-10 7/18/2016 NA - - 17.12 NA
Z2-PZ-10 11/28/2016 NA - - 21.75 NA
Z2-PZ-10 7/9/2018 NA - - 19.57 NA
Z2-PZ-10 12/12/2018 NA - - 16.26 NA
Z2-PZ-10 6/10/2019 NA - - 14.69 NA
Z2-PZ-10 12/9/2019 NA - - 17.45 NA
Z2-PZ-10 6/11/2020 NA - - 12.95 NA
Z2-PZ-10 12/14/2020 NA - - 13.89 NA
Z2-PZ-10 6/14/2021 NA - - 15.12 NA
Z2-PZ-10 6/20/2022 NA - - 19.07 NA
Z2-PZ-10 12/5/2022 NA - - 18.00 NA
Z2-PZ-10 12/12/2022 NA - - 17.47 NA
Z2-PZ-10 7/17/2023 NA - - 19.33 NA
Z2-X03 1/11/2008 900.95 - - 21.96 878.99
Z2-X03 2/12/2008 900.95 - - 21.72 879.23
Z2-X03 5/13/2008 900.95 - - 16.66 884.29
Z2-X03 7/20/2008 900.95 - - 21.75 879.20
Z2-X03 10/24/2008 900.95 20.86 0.63 21.49 879.93
Z2-X03 3/16/2009 900.95 - - 20.55 880.40
Z2-X03 11/5/2010 902.84 - - 21.28 881.56
Z2-X03 5/24/2011 902.84 - - 20.91 881.93
Z2-X03 4/16/2013 902.84 - - 18.90 883.94
Z2-X03 10/26/2015 902.84 - -21.59 881.25
Z2-X03 7/11/2016 902.84 - - 17.08 885.76
Z2-X03 7/12/2016 902.84 - - 17.08 885.76
Z2-X03 7/15/2016 902.84 - - 17.42 885.42
Z2-X03 11/28/2016 902.84 - - 22.61 880.23
Z2-X03 12/15/2016 902.84 - - 23.15 879.69
Z2-X03 6/26/2017 902.84 - - 16.74 886.10
Z2-X03 12/11/2017 902.84 - - 24.82 878.02
Z2-X03 7/9/2018 902.84 - - 21.26 881.58
Z2-X03 12/12/2018 902.84 - - 15.89 886.95
Page 6 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z2-X03 6/10/2019 902.84 - - 15.38 887.46
Z2-X03 12/9/2019 902.84 - - 17.53 885.31
Z2-X03 6/11/2020 902.84 - - 12.69 890.15
Z2-X03 12/14/2020 902.84 - - 13.42 889.42
Z2-X03 6/14/2021 902.84 - - 14.78 888.06
Z2-X03 6/20/2022 902.84 - - 16.77 886.07
Z2-X03 7/17/2023 902.84 - - 18.31 884.53
Z2-X16 1/11/2008 901.43 - - 23.71 877.72
Z2-X16 2/12/2008 901.43 - - 23.55 877.88
Z2-X16 5/13/2008 901.43 16.72 0.33 17.05 884.63
Z2-X16 7/20/2008 901.43 - - 22.50 878.93
Z2-X16 10/24/2008 901.43 22.49 3.17 25.66 878.15
Z2-X16 3/16/2009 901.43 - - 31.31 870.12
Z2-X16 11/5/2010 902.33 - - 21.67 880.66
Z2-X16 4/16/2013 902.33 - - 19.84 882.49
Z2-X16 10/26/2015 902.33 - -22.52 879.81
Z2-X16 7/11/2016 902.33 - - 17.93 884.40
Z2-X16 7/12/2016 902.33 - - 17.93 884.40
Z2-X16 7/13/2016 902.33 - - 18.03 884.30
Z2-X16 11/28/2016 902.33 - - 23.06 879.27
Z2-X16 12/15/2016 902.33 - - 23.60 878.73
Z2-X16 6/26/2017 902.33 - - 18.87 883.46
Z2-X16 12/11/2017 902.33 - - 25.25 877.08
Z2-X16 7/9/2018 902.33 - - 21.93 880.40
Z2-X16 12/12/2018 902.33 - - 17.16 885.17
Z2-X16 6/10/2019 902.33 - - 16.12 886.21
Z2-X16 12/9/2019 902.33 - - 18.56 883.77
Z2-X16 6/11/2020 902.33 - - 13.40 888.93
Z2-X16 12/14/2020 902.33 - - 14.06 888.27
Z2-X16 6/14/2021 902.33 - - 16.10 886.23
Z2-X16 6/20/2022 902.33 - - 18.41 883.92
Z2-X16 7/17/2023 902.33 - - 18.97 883.36
Z2-X18 1/11/2008 900.86 - - 21.81 879.05
Z2-X18 2/12/2008 900.86 - - 21.57 879.29
Z2-X18 5/13/2008 900.86 - - 11.06 889.80
Z2-X18 7/20/2008 900.86 - - 25.08 875.78
Page 7 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z2-X18 10/24/2008 900.86 - - 23.20 877.66
Z2-X18 3/16/2009 900.86 - - 17.86 883.00
Z2-X18 11/5/2010 901.86 - - 20.73 881.13
Z2-X18 5/24/2011 901.86 - - 19.29 882.57
Z2-X18 4/16/2013 901.86 - -17.90 883.96
Z2-X18 10/26/2015 901.86 - -20.89 880.97
Z2-X18 7/11/2016 901.86 - - 16.10 885.76
Z2-X18 7/12/2016 901.86 - - 16.10 885.76
Z2-X18 7/14/2016 901.86 - - 16.38 885.48
Z2-X18 11/28/2016 901.86 - - 22.40 879.46
Z2-X18 12/15/2016 901.86 - - 22.89 878.97
Z2-X18 6/26/2017 901.86 - - 14.40 887.46
Z2-X18 12/11/2017 901.86 - - 24.48 877.38
Z2-X18 7/9/2018 901.86 - - 20.73 881.13
Z2-X18 12/12/2018 901.86 - - 14.06 887.80
Z2-X18 6/10/2019 901.86 - - 13.28 888.58
Z2-X18 12/9/2019 901.86 - - 16.59 885.27
Z2-X18 6/11/2020 901.86 - - 12.34 889.52
Z2-X18 12/14/2020 901.86 - - 10.38 891.48
Z2-X18 6/14/2021 901.86 - - 11.46 890.40
Z2-X18 6/20/2022 901.86 - - 19.40 882.46
Z2-X18 7/17/2023 901.86 - - 18.07 883.79
Z2-X20 1/11/2008 901.27 - - 23.30 877.97
Z2-X20 2/12/2008 901.27 - - 23.14 878.13
Z2-X20 5/13/2008 901.27 17.13 5.38 22.51 882.80
Z2-X20 7/20/2008 901.27 - - 21.33 879.94
Z2-X20 10/24/2008 901.27 - - 22.15 879.12
Z2-X20 3/16/2009 901.27 - - 30.22 871.05
Z2-X20 11/5/2010 902.16 - - 21.59 880.57
Z2-X20 5/24/2011 902.16 - - 20.40 881.76
Z2-X20 4/16/2013 902.16 - - 19.40 882.76
Z2-X20 10/26/2015 902.16 - -22.24 879.92
Z2-X20 7/11/2016 902.16 - - 17.71 884.45
Z2-X20 7/12/2016 902.16 - - 17.71 884.45
Z2-X20 7/18/2016 902.16 - - 17.78 884.38
Z2-X20 11/28/2016 902.16 - - 22.93 879.23
Z2-X20 12/12/2016 902.16 - - 23.36 878.80
Page 8 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z2-X20 6/26/2017 902.16 - - 18.24 883.92
Z2-X20 12/11/2017 902.16 - - 25.05 877.11
Z2-X20 7/9/2018 902.16 - - 21.62 880.54
Z2-X20 12/12/2018 902.16 - - 16.72 885.44
Z2-X20 6/10/2019 902.16 - - 15.89 886.27
Z2-X20 12/9/2019 902.16 - - 18.40 883.76
Z2-X20 6/11/2020 902.16 - - 13.35 888.81
Z2-X20 12/14/2020 902.16 - - 13.10 889.06
Z2-X20 6/14/2021 902.16 - - 16.11 886.05
Z2-X20 6/20/2022 902.16 - - 20.00 882.16
Z2-X20 7/17/2023 902.16 - - 18.84 883.32
Z2-X29 1/11/2008 899.27 - - 21.57 877.70
Z2-X29 2/12/2008 899.27 - - 21.22 878.05
Z2-X29 5/13/2008 899.27 21.24 0.02 21.26 878.03
Z2-X29 7/20/2008 899.27 - - 22.85 876.42
Z2-X29 10/24/2008 899.27 - - 21.47 877.80
Z2-X29 3/16/2009 899.27 - - 18.08 881.19
Z2-X29 5/24/2011 900.96 - - 18.99 881.97
Z2-X29 4/16/2013 900.96 - - 17.74 883.22
Z2-X29 10/26/2015 900.96 - -20.81 880.15
Z2-X29 7/11/2016 900.96 - - 16.01 884.95
Z2-X29 7/12/2016 900.96 - - 16.01 884.95
Z2-X29 7/14/2016 900.96 - - 16.34 884.62
Z2-X29 11/28/2016 900.96 - - 22.11 878.85
Z2-X29 12/13/2016 900.96 - - 22.51 878.45
Z2-X29 6/26/2017 900.96 - - 14.80 886.16
Z2-X29 12/11/2017 900.96 - - 24.24 876.72
Z2-X29 7/9/2018 900.96 - - 20.59 880.37
Z2-X29 12/12/2018 900.96 - - 14.98 885.98
Z2-X29 6/10/2019 900.96 - - 13.04 887.92
Z2-X29 12/9/2019 900.96 - - 16.52 884.44
Z2-X29 6/11/2020 900.96 - - 12.36 888.60
Z2-X29 12/14/2020 900.96 - - 9.30 891.66
Z2-X29 6/14/2021 900.96 - - 15.06 885.90
Z2-X29 6/20/2022 900.96 - - 19.29 881.67
Z2-X29 7/17/2023 900.96 - - 17.85 883.11
Page 9 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z2-X31 1/11/2008 901.13 - - 24.61 876.52
Z2-X31 2/12/2008 901.13 - - 24.38 876.75
Z2-X31 5/13/2008 901.13 26.91 0.15 27.06 874.18
Z2-X31 7/20/2008 901.13 - - 19.54 881.59
Z2-X31 10/24/2008 901.13 - - 23.68 877.45
Z2-X31 3/16/2009 901.13 - - 25.90 875.23
Z2-X31 1/12/2010 901.13 18.79 0.03 18.82 882.33
Z2-X31 2/17/2010 901.13 16.96 0.05 17.01 884.16
Z2-X31 5/11/2010 901.13 - - 20.38 880.75
Z2-X31 5/24/2011 902.94 - - 22.84 880.10
Z2-X31 4/16/2013 902.94 - - 21.85 881.09
Z2-X31 10/26/2015 902.94 - - 24.75 878.19
Z2-X31 7/11/2016 902.94 - - 20.41 882.53
Z2-X31 7/12/2016 902.94 - - 20.41 882.53
Z2-X31 7/13/2016 902.94 - - 20.41 882.53
Z2-X31 11/28/2016 902.94 - - 25.18 877.76
Z2-X31 12/14/2016 902.94 - - 25.65 877.29
Z2-X31 6/26/2017 902.94 - - 21.56 881.38
Z2-X31 12/11/2017 902.94 - - 27.26 875.68
Z2-X31 7/9/2018 902.94 - - 24.05 878.89
Z2-X31 12/12/2018 902.94 - - 19.71 883.23
Z2-X31 6/10/2019 902.94 - - 18.22 884.72
Z2-X31 12/9/2019 902.94 - - 20.94 882.00
Z2-X31 6/11/2020 902.94 - - 16.18 886.76
Z2-X31 12/14/2020 902.94 - - 17.89 885.05
Z2-X31 6/14/2021 902.94 - - 18.41 884.53
Z2-X31 6/20/2022 902.94 - - 22.87 880.07
Z2-X31 7/17/2023 902.94 - - 21.38 881.56
Z2-X35 1/11/2008 899.92 - - 22.39 877.53
Z2-X35 2/12/2008 899.92 - - 22.11 877.81
Z2-X35 5/13/2008 899.92 18.81 0.01 18.82 881.10
Z2-X35 7/20/2008 899.92 - - 21.93 877.99
Z2-X35 10/24/2008 899.92 - - 21.57 878.35
Z2-X35 3/16/2009 899.92 23.55 0.42 23.97 876.26
Z2-X35 7/2/2009 900.96 - - 20.87 880.09
Z2-X35 7/2/2009 900.96 - - 18.64 882.32
Z2-X35 7/2/2009 900.96 - -21.56 879.40
Page 10 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z2-X35 7/2/2009 900.96 20.31 4.78 25.09 879.46
Z2-X35 11/20/2009 900.96 20.37 1.11 21.48 880.31
Z2-X35 11/20/2009 900.96 18.95 0.63 19.58 881.85
Z2-X35 11/20/2009 900.96 19.35 0.11 19.46 881.58
Z2-X35 12/17/2009 900.96 21.01 0.04 21.05 879.94
Z2-X35 12/17/2009 900.96 - - 20.31 880.65
Z2-X35 12/17/2009 900.96 - - 20.60 880.36
Z2-X35 1/12/2010 900.96 - - 22.27 878.69
Z2-X35 1/12/2010 900.96 - - 21.75 879.21
Z2-X35 1/12/2010 900.96 24.08 0.08 24.16 876.86
Z2-X35 1/20/2010 900.96 - - 23.85 877.11
Z2-X35 1/20/2010 900.96 - - 22.71 878.25
Z2-X35 1/20/2010 900.96 - - 22.58 878.38
Z2-X35 2/17/2010 900.96 23.48 0.76 24.24 877.29
Z2-X35 2/17/2010 900.96 - - 31.82 869.14
Z2-X35 2/17/2010 900.96 22.17 1.81 23.98 878.34
Z2-X35 5/3/2010 900.96 22.96 1.15 24.11 877.71
Z2-X35 5/3/2010 900.96 21.43 1.02 22.45 879.28
Z2-X35 5/3/2010 900.96 22.35 0.03 22.38 878.60
Z2-X35 5/3/2010 900.96 - - 22.48 878.48
Z2-X35 5/3/2010 900.96 - - 21.94 879.02
Z2-X35 5/9/2010 900.96 - - 22.93 878.03
Z2-X35 5/9/2010 900.96 22.86 0.02 22.88 878.10
Z2-X35 5/9/2010 900.96 22.86 0.01 22.87 878.10
Z2-X35 5/9/2010 900.96 24.35 0.15 24.50 876.57
Z2-X35 5/9/2010 900.96 25.53 0.03 25.56 875.42
Z2-X35 5/18/2010 900.96 - - 24.39 876.57
Z2-X35 5/18/2010 900.96 - - 21.72 879.24
Z2-X35 5/18/2010 900.96 22.30 1.03 23.33 878.40
Z2-X35 5/18/2010 900.96 27.10 0.13 27.23 873.83
Z2-X35 6/21/2010 900.96 21.20 1.39 22.59 879.41
Z2-X35 6/21/2010 900.96 21.75 1.38 23.13 878.87
Z2-X35 6/21/2010 900.96 20.24 1.25 21.49 880.41
Z2-X35 6/21/2010 900.96 21.58 0.38 21.96 879.29
Z2-X35 6/21/2010 900.96 21.45 0.16 21.61 879.47
Z2-X35 7/20/2010 900.96 20.95 0.05 21.00 880.00
Z2-X35 7/20/2010 900.96 22.74 0.63 23.37 878.06
Z2-X35 7/20/2010 900.96 22.15 0.36 22.51 878.72
Page 11 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z2-X35 7/20/2010 900.96 22.13 0.36 22.49 878.74
Z2-X35 8/11/2010 900.96 - - 22.20 878.76
Z2-X35 8/11/2010 900.96 23.50 0.61 24.11 877.31
Z2-X35 8/11/2010 900.96 24.55 0.1 24.65 876.39
Z2-X35 8/11/2010 900.96 - - 23.50 877.46
Z2-X35 8/11/2010 900.96 - - 21.46 879.50
Z2-X35 11/5/2010 900.96 - - 21.76 879.20
Z2-X35 11/5/2010 900.96 - -20.48 880.48
Z2-X35 11/5/2010 900.96 - - 21.23 879.73
Z2-X35 2/1/2011 900.96 - - 20.79 880.17
Z2-X35 2/1/2011 900.96 - - 20.76 880.20
Z2-X35 2/1/2011 900.96 23.39 0.07 23.46 877.55
Z2-X35 2/1/2011 900.96 - - 24.26 876.70
Z2-X35 2/1/2011 900.96 - - 23.31 877.65
Z2-X35 4/1/2011 900.96 - - 21.82 879.14
Z2-X35 4/1/2011 900.96 19.34 0.16 19.50 881.58
Z2-X35 4/1/2011 900.96 - - 20.60 880.36
Z2-X35 4/1/2011 900.96 - - 20.52 880.44
Z2-X35 4/16/2013 900.96 - - 20.44 880.52
Z2-X35 4/16/2013 900.96 - - 21.68 879.28
Z2-X35 4/16/2013 900.96 - - 22.00 878.96
Z2-X35 4/16/2013 900.96 - - 22.01 878.95
Z2-X35 4/16/2013 900.96 - - 22.30 878.66
Z2-X35 4/16/2013 900.96 23.75 0.06 23.81 877.20
Z2-X35 10/26/2015 900.96 - - 23.53 877.43
Z2-X35 7/11/2016 900.96 - - 17.00 883.96
Z2-X35 7/12/2016 900.96 - - 17.00 883.96
Z2-X35 7/14/2016 900.96 - - 17.15 883.81
Z2-X35 11/28/2016 900.96 - - Dry NA
Z2-X35 6/26/2017 900.96 - - 16.77 884.19
Z2-X35 12/11/2017 900.96 - - Dry NA
Z2-X35 1/25/2018 900.96 - - Dry NA
Z2-X35 7/9/2018 900.96 - - 21.09 879.87
Z2-X35 12/12/2018 900.96 - - 19.56 881.40
Z2-X35 6/10/2019 900.96 - - 15.21 885.75
Z2-X35 12/9/2019 900.96 - - 17.50 883.46
Z2-X35 6/11/2020 900.96 - - 12.97 887.99
Z2-X35 12/14/2020 900.96 - - 13.66 887.30
Page 12 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z2-X35 6/14/2021 900.96 - - 15.54 885.42
Z2-X35 6/20/2022 900.96 - - 19.63 881.33
Z2-X35 7/17/2023 900.96 - - 18.43 882.53
Z3-X80 11/20/2009 900.75 20.67 0.01 20.68 880.08
Z3-X80 1/12/2010 900.75 - - 19.54 881.21
Z3-X80 5/3/2010 900.75 - - 20.16 880.59
Z3-X80 5/9/2010 900.75 - - 20.15 880.60
Z3-X80 5/18/2010 900.75 - - 20.61 880.14
Z3-X80 6/21/2010 900.75 - - 21.50 879.25
Z3-X80 7/20/2010 900.75 - - 20.81 879.94
Z3-X80 8/11/2010 900.75 - - 20.78 879.97
Z3-X80 2/1/2011 902.87 - - 23.86 879.01
Z3-X80 4/1/2011 902.87 - - 23.67 879.20
Z3-X80 4/16/2013 902.87 - - 23.30 879.57
Z3-X80 10/26/2015 902.87 - -25.66 877.21
Z3-X80 7/11/2016 902.87 - - 21.19 881.68
Z3-X80 7/12/2016 902.87 - - 21.19 881.68
Z3-X80 7/19/2016 902.87 - - 22.02 880.85
Z3-X80 11/28/2016 902.87 - - 25.84 877.03
Z3-X80 6/26/2017 902.87 - - 22.76 880.11
Z3-X80 12/11/2017 902.87 - - 27.90 874.97
Z3-X80 7/9/2018 902.87 - - 24.79 878.08
Z3-X80 12/12/2018 902.87 - - 20.79 882.08
Z3-X80 6/10/2019 902.87 - - 18.85 884.02
Z3-X80 12/9/2019 902.87 - - 21.70 881.17
Z3-X80 6/11/2020 902.87 - - 17.16 885.71
Z3-X80 12/14/2020 902.87 - - 18.80 884.07
Z3-X80 6/14/2021 902.87 - - 19.23 883.64
Z3-X80 6/20/2022 902.87 - - 23.22 879.65
Z3-X80 7/17/2023 902.87 - - 22.12 880.75
Z3-X82 11/20/2009 901.71 - - 21.53 880.18
Z3-X82 1/12/2010 901.71 - - 20.53 881.18
Z3-X82 5/3/2010 901.71 - - 21.40 880.31
Z3-X82 5/9/2010 901.71 - - 21.18 880.53
Z3-X82 5/18/2010 901.71 - - 20.85 880.86
Z3-X82 6/21/2010 901.71 - - 23.84 877.87
Page 13 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z3-X82 7/20/2010 901.71 - - 21.62 880.09
Z3-X82 8/11/2010 901.71 - - 21.58 880.13
Z3-X82 2/1/2011 903.51 - - 24.05 879.46
Z3-X82 4/1/2011 903.51 - - 24.32 879.19
Z3-X82 4/16/2013 903.51 - - 23.10 880.41
Z3-X82 10/26/2015 903.51 - - 25.94 877.57
Z3-X82 7/11/2016 903.51 - - 21.48 882.03
Z3-X82 7/12/2016 903.51 - - 21.48 882.03
Z3-X82 7/13/2016 903.51 - - 21.73 881.78
Z3-X82 11/28/2016 903.51 - - 26.10 877.41
Z3-X82 6/26/2017 903.51 - - 23.27 880.24
Z3-X82 12/11/2017 903.51 - - 28.31 875.20
Z3-X82 7/9/2018 903.51 - - 25.04 878.47
Z3-X82 12/12/2018 903.51 - - 21.10 882.41
Z3-X82 6/10/2019 903.51 - - 19.24 884.27
Z3-X82 12/9/2019 903.51 - - 21.94 881.57
Z3-X82 6/11/2020 903.51 - - 17.25 886.26
Z3-X82 12/14/2020 903.51 - - 18.50 885.01
Z3-X82 6/14/2021 903.51 - - 19.81 883.70
Z3-X82 6/20/2022 903.51 - - 23.31 880.20
Z3-X82 7/17/2023 903.51 - - 22.27 881.24
Z4-PZ04 11/5/2010 898.53 - - 20.30 878.23
Z4-PZ04 4/16/2013 898.53 - - 18.41 880.12
Z4-PZ04 10/26/2015 898.53 - -21.51 877.02
Z4-PZ04 7/11/2016 898.53 - - 16.94 881.59
Z4-PZ04 7/12/2016 898.53 - - 16.94 881.59
Z4-PZ04 7/19/2016 898.53 - - 17.21 881.32
Z4-PZ04 11/28/2016 898.53 - - 21.84 876.69
Z4-PZ04 12/13/2016 898.53 - - 22.21 876.32
Z4-PZ04 6/26/2017 898.53 - - 17.04 881.49
Z4-PZ04 12/11/2017 898.53 - - 23.88 874.65
Z4-PZ04 7/9/2018 898.53 - - 20.62 877.91
Z4-PZ04 12/12/2018 898.53 - - 15.38 883.15
Z4-PZ04 6/10/2019 898.53 - - 14.71 883.82
Z4-PZ04 12/9/2019 898.53 - - 17.72 880.81
Z4-PZ04 6/11/2020 898.53 - - 13.04 885.49
Z4-PZ04 12/14/2020 898.53 - - 7.40 891.13
Page 14 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z4-PZ04 6/14/2021 898.53 - - 15.16 883.37
Z4-PZ04 6/20/2022 898.53 - - 19.15 879.38
Z4-PZ04 7/17/2023 898.53 - - 18.23 880.30
Z4-PZ07 11/5/2010 898.90 - - 21.59 877.31
Z4-PZ07 4/16/2013 898.90 - - 20.06 878.84
Z4-PZ07 10/26/2015 898.90 - -20.02 878.88
Z4-PZ07 7/11/2016 898.90 - - 15.14 883.76
Z4-PZ07 7/12/2016 898.90 - - 15.14 883.76
Z4-PZ07 7/14/2016 898.90 - - 15.20 883.70
Z4-PZ07 11/28/2016 898.90 - - 20.17 878.73
Z4-PZ07 6/26/2017 898.90 - - NA NA
Z4-PZ07 12/11/2017 898.90 - - 26.39 872.51
Z4-PZ07 7/9/2018 898.90 - - 21.36 877.54
Z4-PZ07 12/12/2018 898.90 - - 17.28 881.62
Z4-PZ07 6/10/2019 898.90 - - 16.46 882.44
Z4-PZ07 12/9/2019 898.90 - - 19.34 879.56
Z4-PZ07 6/11/2020 898.90 - - 13.74 885.16
Z4-PZ07 12/14/2020 898.90 - - 17.39 881.51
Z4-PZ07 6/14/2021 898.90 - - 15.96 882.94
Z4-PZ07 6/20/2022 898.90 - - 19.90 879.00
Z4-PZ07 7/17/2023 898.90 - - 18.94 879.96
Z4-PZ09 11/5/2010 899.62 - - 23.53 876.09
Z4-PZ09 11/5/2010 899.62 - - 18.95 880.67
Z4-PZ09 4/16/2013 899.62 - - 21.80 877.82
Z4-PZ09 4/16/2013 899.62 - - 20.12 879.50
Z4-PZ09 10/26/2015 899.62 - - 22.70 876.92
Z4-PZ09 7/11/2016 899.62 - - 20.14 879.48
Z4-PZ09 7/12/2016 899.62 - - 20.14 879.48
Z4-PZ09 7/18/2016 899.62 - - 20.99 878.63
Z4-PZ09 11/28/2016 899.62 - - 23.96 875.66
Z4-PZ09 6/26/2017 898.88 - - 20.99 877.89
Z4-PZ09 12/11/2017 898.88 - - Dry NA
Z4-PZ09 1/25/2018 898.88 - - Dry NA
Z4-PZ09 7/9/2018 898.88 - - 19.76 879.12
Z4-PZ09 12/12/2018 898.88 - - 11.28 887.60
Z4-PZ09 6/10/2019 898.88 - - 18.71 880.17
Page 15 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z4-PZ09 12/9/2019 898.88 - - 21.55 877.33
Z4-PZ09 6/11/2020 898.88 - - 17.35 881.53
Z4-PZ09 12/14/2020 898.88 - - 14.15 884.73
Z4-PZ09 6/14/2021 898.88 - - 18.97 879.91
Z4-PZ09 6/20/2022 898.88 - - 22.90 875.98
Z4-PZ09 7/17/2023 898.88 - - 21.95 876.93
Z4-X21 10/5/2010 898.56 - - 19.97 878.59
Z4-X21 4/1/2011 898.56 - - 21.10 877.46
Z4-X21 5/16/2011 898.56 - - 20.41 878.15
Z4-X21 6/23/2011 898.56 - - 21.45 877.11
Z4-X21 7/12/2011 898.56 - - 21.19 877.37
Z4-X21 8/23/2011 898.56 - - 22.44 876.12
Z4-X21 11/28/2011 898.56 - - 23.05 875.51
Z4-X21 12/12/2011 898.56 - - 21.93 876.63
Z4-X21 8/30/2012 898.56 - - 25.50 873.06
Z4-X21 12/20/2012 898.56 - - 23.11 875.45
Z4-X21 2/28/2013 898.56 - -20.25 878.31
Z4-X21 4/16/2013 898.56 - - 19.04 879.52
Z4-X21 10/26/2015 898.56 - -24.03 874.53
Z4-X21 7/11/2016 898.56 - - 19.59 878.97
Z4-X21 7/12/2016 898.56 - - 19.59 878.97
Z4-X21 7/13/2016 898.56 - - 19.55 879.01
Z4-X21 11/28/2016 898.56 - - 24.30 874.26
Z4-X21 12/14/2016 898.56 - - 24.64 873.92
Z4-X21 6/26/2017 898.56 - - 21.00 877.56
Z4-X21 12/11/2017 898.56 - - 26.19 872.37
Z4-X21 7/9/2018 898.56 - - 23.18 875.38
Z4-X21 12/12/2018 898.56 - - 19.42 879.14
Z4-X21 6/10/2019 898.56 - - 17.91 880.65
Z4-X21 12/9/2019 898.56 - - 20.40 878.16
Z4-X21 6/11/2020 898.56 - - 15.91 882.65
Z4-X21 12/14/2020 898.56 - - 17.11 881.45
Z4-X21 6/14/2021 898.56 - - 17.77 880.79
Z4-X21 6/20/2022 898.56 - - 21.86 876.70
Z4-X21 7/17/2023 898.56 - - 20.81 877.75
Z4-X30 9/30/2010 897.55 - - 18.92 878.63
Page 16 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z4-X30 4/1/2011 897.55 - - 25.48 872.07
Z4-X30 5/16/2011 897.55 - - 20.66 876.89
Z4-X30 6/23/2011 897.55 - - 20.43 877.12
Z4-X30 7/12/2011 897.55 - - 19.31 878.24
Z4-X30 8/23/2011 897.55 - - 22.50 875.05
Z4-X30 11/28/2011 897.55 - - 22.00 875.55
Z4-X30 12/12/2011 897.55 - - 21.38 876.17
Z4-X30 8/30/2012 897.55 - - 23.80 873.75
Z4-X30 12/20/2012 897.55 - - 21.52 876.03
Z4-X30 2/28/2013 897.55 - - 18.25 879.30
Z4-X30 4/16/2013 897.55 - - 17.45 880.10
Z4-X30 10/26/2015 897.55 - - 22.80 874.75
Z4-X30 7/11/2016 897.55 - - 18.13 879.42
Z4-X30 7/12/2016 897.55 - - 18.13 879.42
Z4-X30 7/14/2016 897.55 - - 18.20 879.35
Z4-X30 11/28/2016 897.55 - - 22.98 874.57
Z4-X30 12/14/2016 897.55 - - 23.39 874.16
Z4-X30 6/26/2017 897.55 - - 19.42 878.13
Z4-X30 12/11/2017 897.55 - - 24.96 872.59
Z4-X30 7/9/2018 897.55 - - 21.96 875.59
Z4-X30 12/12/2018 897.55 - - 17.38 880.17
Z4-X30 6/10/2019 897.55 - - 14.85 882.70
Z4-X30 12/9/2019 897.55 - - 18.82 878.73
Z4-X30 6/11/2020 897.55 - - 14.76 882.79
Z4-X30 12/14/2020 897.55 - - 14.35 883.20
Z4-X30 6/14/2021 897.55 - - 16.54 881.01
Z4-X30 6/20/2022 897.55 - - 20.93 876.62
Z4-X30 7/17/2023 897.55 - - 19.54 878.01
Z4-X35 10/6/2010 898.53 - - 20.20 878.33
Z4-X35 4/1/2011 898.53 - - 24.62 873.91
Z4-X35 5/16/2011 898.53 21.47 1.57 23.04 876.66
Z4-X35 6/23/2011 898.53 22.20 0.18 22.38 876.28
Z4-X35 7/12/2011 898.53 21.36 0.29 21.65 877.09
Z4-X35 8/23/2011 898.53 - - 24.38 874.15
Z4-X35 11/28/2011 898.53 22.85 2.23 25.08 875.12
Z4-X35 12/8/2011 898.53 21.91 1.86 23.77 876.15
Z4-X35 12/12/2011 898.53 21.65 1.65 23.30 876.46
Page 17 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z4-X35 12/20/2012 898.53 - - 22.78 875.75
Z4-X35 2/28/2013 898.53 - - 20.19 878.34
Z4-X35 4/16/2013 898.53 - - 19.06 879.47
Z4-X35 10/26/2015 898.53 - -24.19 874.34
Z4-X35 7/11/2016 898.53 - - 16.98 881.55
Z4-X35 7/12/2016 898.53 - - 16.98 881.55
Z4-X35 7/13/2016 898.53 - - 19.61 878.92
Z4-X35 11/28/2016 898.53 - - 24.18 874.35
Z4-X35 12/14/2016 898.53 - - 24.60 873.93
Z4-X35 6/26/2017 898.53 - - 21.47 877.06
Z4-X35 12/11/2017 898.53 - - 26.12 872.41
Z4-X35 7/9/2018 898.53 - - 23.17 875.36
Z4-X35 12/12/2018 898.53 - - 19.56 878.97
Z4-X35 6/10/2019 898.53 - - 17.82 880.71
Z4-X35 12/9/2019 898.53 - - 20.60 877.93
Z4-X35 12/14/2020 898.53 - - 17.17 881.36
Z4-X35 6/14/2021 898.53 - - 17.85 880.68
Z4-X35 6/20/2022 898.53 - - 22.95 875.58
Z4-X35 7/17/2023 898.53 - - 20.91 877.62
Z4-X47 9/29/2010 896.98 - - 19.12 877.86
Z4-X47 4/1/2011 896.98 26.20 0.91 27.11 870.55
Z4-X47 5/16/2011 896.98 21.55 6.25 27.80 873.87
Z4-X47 6/23/2011 896.98 22.69 0.41 23.10 874.19
Z4-X47 7/12/2011 896.98 20.68 0.12 20.80 876.27
Z4-X47 8/23/2011 896.98 23.52 0.13 23.65 873.43
Z4-X47 9/30/2011 896.98 - - 32.35 864.63
Z4-X47 11/28/2011 896.98 - - 22.60 874.38
Z4-X47 12/12/2011 896.98 - - 20.81 876.17
Z4-X47 12/20/2012 896.98 - - 21.79 875.19
Z4-X47 2/28/2013 896.98 - - 19.07 877.91
Z4-X47 4/16/2013 896.98 - - 17.89 879.09
Z4-X47 10/26/2015 896.98 - -22.85 874.13
Z4-X47 7/11/2016 896.98 - - 18.10 878.88
Z4-X47 7/12/2016 896.98 - - 18.10 878.88
Z4-X47 7/13/2016 896.98 - - 18.18 878.80
Z4-X47 11/28/2016 896.98 - - 22.78 874.20
Z4-X47 12/14/2016 896.98 - - 23.17 873.81
Page 18 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z4-X47 6/26/2017 896.98 - - 19.49 877.49
Z4-X47 12/11/2017 896.98 - - 24.70 872.28
Z4-X47 7/9/2018 896.98 - - 21.83 875.15
Z4-X47 12/12/2018 896.98 - - 18.13 878.85
Z4-X47 6/10/2019 896.98 - - 16.31 880.67
Z4-X47 12/9/2019 896.98 - - 19.30 877.68
Z4-X47 6/11/2020 896.98 - - 15.02 881.96
Z4-X47 12/14/2020 896.98 - - 15.84 881.14
Z4-X47 6/14/2021 896.98 - - 16.54 880.44
Z4-X47 6/20/2022 896.98 - - 20.67 876.31
Z4-X47 7/17/2023 896.98 - - 19.55 877.43
Z4-X55 10/1/2010 897.94 - - 20.45 877.49
Z4-X55 4/1/2011 897.94 - - 23.68 874.26
Z4-X55 5/16/2011 897.94 - - 22.00 875.94
Z4-X55 6/23/2011 897.94 - - 21.89 876.05
Z4-X55 7/12/2011 897.94 - - 21.80 876.14
Z4-X55 8/10/2011 897.94 - - 22.90 875.04
Z4-X55 8/23/2011 897.94 - - 23.69 874.25
Z4-X55 11/28/2011 897.94 - - 22.70 875.24
Z4-X55 12/12/2011 897.94 - - 21.53 876.41
Z4-X55 8/30/2012 897.94 - - 23.80 874.14
Z4-X55 12/20/2012 897.94 - - 23.27 874.67
Z4-X55 2/28/2013 897.94 - - 19.70 878.24
Z4-X55 4/16/2013 897.94 - - 18.90 879.04
Z4-X55 10/26/2015 897.94 - -24.31 873.63
Z4-X55 7/11/2016 897.94 - - 19.72 878.22
Z4-X55 7/12/2016 897.94 - - 19.72 878.22
Z4-X55 7/13/2016 897.94 - - 19.74 878.20
Z4-X55 11/28/2016 897.94 - - 24.60 873.34
Z4-X55 12/14/2016 897.94 - - 24.91 873.03
Z4-X55 6/26/2017 897.94 - - 20.85 877.09
Z4-X55 12/11/2017 897.94 - - 24.48 873.46
Z4-X55 7/9/2018 897.94 - - 23.70 874.24
Z4-X55 12/12/2018 897.94 - - 19.73 878.21
Z4-X55 6/10/2019 897.94 - - 17.19 880.75
Z4-X55 12/9/2019 897.94 - - 20.91 877.03
Z4-X55 6/11/2020 897.94 - - 16.89 881.05
Page 19 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z4-X55 12/14/2020 897.94 - - 16.58 881.36
Z4-X55 6/14/2021 897.94 - - 18.41 879.53
Z4-X55 6/20/2022 897.94 - - 22.47 875.47
Z4-X55 7/17/2023 897.94 - - 21.51 876.43
Z4-X63 12/20/2012 898.33 24.30 0.06 24.36 874.02
Z4-X63 2/28/2013 898.33 22.95 0.55 23.50 875.24
Z4-X63 4/16/2013 898.33 21.20 0.25 21.45 877.07
Z4-X63 8/6/2013 898.33 19.54 0.22 19.76 878.74
Z4-X63 10/26/2015 898.68 - - 25.76 872.92
Z4-X63 7/11/2016 898.68 - - 21.11 877.57
Z4-X63 7/12/2016 898.68 - - 21.11 877.57
Z4-X63 7/13/2016 898.68 - - 21.20 877.48
Z4-X63 11/28/2016 898.68 - - 25.75 872.93
Z4-X63 12/14/2016 898.68 - - 26.45 872.23
Z4-X63 6/26/2017 898.68 - - 22.98 875.70
Z4-X63 12/11/2017 898.68 - - 27.65 871.03
Z4-X63 7/9/2018 898.68 - - 24.63 874.05
Z4-X63 12/12/2018 898.68 - - 21.08 877.60
Z4-X63 6/10/2019 898.68 - - 19.22 879.46
Z4-X63 12/9/2019 898.68 - - 22.01 876.67
Z4-X63 6/11/2020 898.68 - - 17.46 881.22
Z4-X63 12/14/2020 898.68 - - 18.49 880.19
Z4-X63 6/14/2021 898.68 - - 19.27 879.41
Z4-X63 6/20/2022 898.68 - - 23.20 875.48
Z4-X63 7/17/2023 898.68 - - 22.32 876.36
Z4-X68 12/20/2012 898.27 - - 23.49 874.78
Z4-X68 2/28/2013 898.27 - - 20.68 877.59
Z4-X68 4/16/2013 898.27 - - 19.15 879.12
Z4-X68 10/26/2015 898.27 - - 24.10 874.17
Z4-X68 7/11/2016 898.27 - - 19.70 878.57
Z4-X68 7/12/2016 898.27 - - 19.70 878.57
Z4-X68 7/14/2016 898.27 - - 19.78 878.49
Z4-X68 11/28/2016 898.27 - - 24.45 873.82
Z4-X68 12/14/2016 898.27 - - 24.88 873.39
Z4-X68 6/26/2017 898.27 - - 20.90 877.37
Z4-X68 12/11/2017 898.27 - - 26.47 871.80
Page 20 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z4-X68 7/9/2018 898.27 - - 23.37 874.90
Z4-X68 12/12/2018 898.27 - - 19.24 879.03
Z4-X68 6/10/2019 898.27 - - 17.46 880.81
Z4-X68 12/9/2019 898.27 - - 20.44 877.83
Z4-X68 6/11/2020 898.27 - - 15.84 882.43
Z4-X68 12/14/2020 898.27 - - 16.80 881.47
Z4-X68 6/14/2021 898.27 - - 17.96 880.31
Z4-X68 6/20/2022 898.27 - - 21.86 876.41
Z4-X68 7/17/2023 898.27 - - 21.03 877.24
Z4-X70 12/20/2012 898.06 - - 24.25 873.81
Z4-X70 2/28/2013 898.06 - - 21.60 876.46
Z4-X70 4/16/2013 898.06 - - 20.40 877.66
Z4-X70 10/26/2015 898.06 - -24.21 873.85
Z4-X70 7/11/2016 898.06 - - 20.65 877.41
Z4-X70 7/12/2016 898.06 - - 20.65 877.41
Z4-X70 7/19/2016 898.06 - - 22.38 875.68
Z4-X70 11/28/2016 898.06 - - 25.23 872.83
Z4-X70 12/16/2016 898.06 - - 25.59 872.47
Z4-X70 6/26/2017 898.06 - - 22.37 875.69
Z4-X70 12/11/2017 898.06 - - 27.19 870.87
Z4-X70 7/9/2018 898.06 - - 24.25 873.81
Z4-X70 12/12/2018 898.06 - - 20.67 877.39
Z4-X70 6/10/2019 898.06 - - 18.73 879.33
Z4-X70 12/9/2019 898.06 - - 21.70 876.36
Z4-X70 6/11/2020 898.06 - - 17.16 880.90
Z4-X70 12/14/2020 898.06 - - 18.17 879.89
Z4-X70 6/14/2021 898.06 - - 18.83 879.23
Z4-X70 6/20/2022 898.06 - - 22.81 875.25
Z4-X70 7/17/2023 898.06 - - 21.89 876.17
Z4-X72 12/20/2012 897.98 - - 24.12 873.86
Z4-X72 2/28/2013 897.98 - - 20.95 877.03
Z4-X72 4/16/2013 897.98 - - 19.45 878.53
Z4-X72 10/26/2015 897.98 - -24.17 873.81
Z4-X72 7/11/2016 897.98 - - 19.68 878.30
Z4-X72 7/12/2016 897.98 - - 19.68 878.30
Z4-X72 7/19/2016 897.98 - - 20.03 877.95
Page 21 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Z4-X72 11/28/2016 897.98 - - 24.45 873.53
Z4-X72 12/16/2016 897.98 - - 24.84 873.14
Z4-X72 6/26/2017 897.98 - - 21.06 876.92
Z4-X72 12/11/2017 897.98 - - 26.44 871.54
Z4-X72 7/9/2018 897.98 - - 23.40 874.58
Z4-X72 12/12/2018 897.98 - - 19.41 878.57
Z4-X72 6/10/2019 897.98 - - 17.41 880.57
Z4-X72 12/9/2019 897.98 - - 20.35 877.63
Z4-X72 6/11/2020 897.98 - - 16.02 881.96
Z4-X72 12/14/2020 897.98 - - 15.59 882.39
Z4-X72 6/14/2021 897.98 - - 17.94 880.04
Z4-X72 6/20/2022 897.98 - - 21.92 876.06
Z4-X72 7/17/2023 897.98 - - 21.02 876.96
Z4-X89 12/20/2012 NA - - 24.06 NA
Z4-X89 2/28/2013 NA - - 21.20 NA
Z4-X89 4/16/2013 NA - - 20.60 NA
Z4-X89 10/26/2015 901.77 - -25.19 876.58
Z4-X89 7/11/2016 901.77 - - 20.71 881.06
Z4-X89 7/12/2016 901.77 - - 20.71 881.06
Z4-X89 7/19/2016 901.77 - - 20.98 880.79
Z4-X89 11/28/2016 901.77 - - 25.30 876.47
Z4-X89 12/28/2016 901.77 - - 26.06 875.71
Z4-X89 6/26/2017 901.77 - - 22.41 879.36
Z4-X89 12/11/2017 901.77 - - 27.30 874.47
Z4-X89 7/9/2018 901.77 - - 24.27 877.50
Z4-X89 12/12/2018 901.77 - - 20.51 881.26
Z4-X89 6/10/2019 901.77 - - 18.43 883.34
Z4-X89 12/9/2019 901.77 - - 21.39 880.38
Z4-X89 6/11/2020 901.77 - - 16.80 884.97
Z4-X89 12/14/2020 901.77 - - 17.67 884.10
Z4-X89 6/14/2021 901.77 - - 19.42 882.35
Z4-X89 6/20/2022 901.77 - - 20.71 881.06
Z4-X89 7/17/2023 901.77 - - 21.74 880.03
MW-A-I 10/26/2015 902.43 - -23.34 879.09
MW-A-I 7/11/2016 902.43 - - 18.71 883.72
MW-A-I 7/12/2016 902.43 - - 18.71 883.72
Page 22 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-A-I 7/19/2016 902.43 - - 19.13 883.30
MW-A-I 11/28/2016 902.43 - - 23.66 878.77
MW-A-I 12/14/2016 902.43 - - 24.10 878.33
MW-A-I 6/26/2017 902.43 - - 20.03 882.40
MW-A-I 12/11/2017 902.43 - - 25.97 876.46
MW-A-I 7/9/2018 902.43 - - 22.55 879.88
MW-A-I 12/12/2018 902.43 - - 17.94 884.49
MW-A-I 6/10/2019 902.43 - - 16.58 885.85
MW-A-I 12/9/2019 902.43 - - 19.40 883.03
MW-A-I 6/11/2020 902.43 - - 13.77 888.66
MW-A-I 12/14/2020 902.43 - - 15.19 887.24
MW-A-I 6/14/2021 902.43 - - 16.38 886.05
MW-A-I 6/20/2022 902.43 - - 20.77 881.66
MW-A-I 7/17/2023 902.43 - - 19.62 882.81
MW-A-D 10/26/2015 902.71 - - 23.85 878.86
MW-A-D 7/11/2016 902.71 - - 19.23 883.48
MW-A-D 7/12/2016 902.71 - - 19.23 883.48
MW-A-D 7/19/2016 902.71 - - 19.59 883.48
MW-A-D 11/28/2016 902.71 - - 24.17 878.54
MW-A-D 12/13/2016 902.71 - - 24.53 878.18
MW-A-D 6/26/2017 902.71 - - 20.49 882.22
MW-A-D 12/11/2017 902.71 - - 26.41 876.30
MW-A-D 7/9/2018 902.71 - - 23.06 879.65
MW-A-D 12/12/2018 902.71 - - 18.55 884.16
MW-A-D 6/10/2019 902.71 - - 17.11 885.60
MW-A-D 12/9/2019 902.71 - - 19.93 882.78
MW-A-D 6/11/2020 902.71 - - 14.46 888.25
MW-A-D 12/14/2020 902.71 - - 15.85 886.86
MW-A-D 6/14/2021 902.71 - - 16.95 885.76
MW-A-D 6/20/2022 902.71 - - 21.28 881.43
MW-A-D 7/17/2023 902.71 - - 20.13 882.58
MW-A-B 12/1/2015 899.96 - -19.36 880.60
MW-A-B 7/11/2016 899.96 - - 16.41 883.55
MW-A-B 7/12/2016 899.96 - - 16.41 883.55
MW-A-B 7/19/2016 899.96 - - 16.95 883.55
MW-A-B 11/28/2016 899.96 - - 21.52 878.44
Page 23 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-A-B 12/14/2016 899.96 - - 22.00 877.96
MW-A-B 6/26/2017 899.96 - - 17.83 882.13
MW-A-B 12/11/2017 899.96 - - 23.66 876.30
MW-A-B 7/9/2018 899.96 - - 20.45 879.51
MW-A-B 12/12/2018 899.96 - - 16.10 883.86
MW-A-B 6/10/2019 899.96 - - 14.57 885.39
MW-A-B 12/9/2019 899.96 - - 17.39 882.57
MW-A-B 6/11/2020 899.96 - - 16.82 883.14
MW-A-B 12/14/2020 899.96 - - 13.33 886.63
MW-A-B 6/14/2021 899.96 - - 14.38 885.58
MW-A-B 6/20/2022 899.96 - - 18.72 881.24
MW-A-B 7/17/2023 899.96 - - 17.52 882.44
MW-B-I 10/26/2015 901.28 - - 24.58 876.70
MW-B-I 7/11/2016 901.28 - - 20.19 881.09
MW-B-I 7/12/2016 901.28 - - 20.19 881.09
MW-B-I 7/19/2016 901.28 - - 20.29 881.09
MW-B-I 11/28/2016 901.28 - - 24.79 876.49
MW-B-I 12/13/2016 901.28 - - 25.18 876.10
MW-B-I 6/26/2017 901.28 - - 21.73 879.55
MW-B-I 12/11/2017 901.28 - - 26.85 874.43
MW-B-I 7/9/2018 901.28 - - 23.72 877.56
MW-B-I 12/12/2018 901.28 - - 19.71 881.57
MW-B-I 6/10/2019 901.28 - - 17.84 883.44
MW-B-I 12/9/2019 901.28 - - 20.70 880.58
MW-B-I 6/11/2020 901.28 - - 16.01 885.27
MW-B-I 12/14/2020 901.28 - - 17.11 884.17
MW-B-I 6/14/2021 901.28 - - 17.99 883.29
MW-B-I 6/20/2022 901.28 - - 22.23 879.05
MW-B-I 7/17/2023 901.28 - - 21.17 880.11
MW-B-D 10/26/2015 901.18 - -24.57 876.61
MW-B-D 7/11/2016 901.18 - - 20.18 881.00
MW-B-D 7/12/2016 901.18 - - 20.18 881.00
MW-B-D 7/20/2016 901.18 - - 20.44 881.00
MW-B-D 11/28/2016 901.18 - - 24.85 876.33
MW-B-D 12/13/2016 901.18 - - 25.14 876.04
MW-B-D 6/26/2017 901.18 - - 21.62 879.56
Page 24 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-B-D 12/11/2017 901.18 - - 26.80 874.38
MW-B-D 7/9/2018 901.18 - - 23.77 877.41
MW-B-D 12/12/2018 901.18 - - 19.83 881.35
MW-B-D 6/10/2019 901.18 - - 15.81 885.37
MW-B-D 12/9/2019 901.18 - - 20.80 880.38
MW-B-D 6/11/2020 901.18 - - 16.23 884.95
MW-B-D 12/14/2020 901.18 - - 17.29 883.89
MW-B-D 6/14/2021 901.18 - - 18.17 883.01
MW-B-D 6/20/2022 901.18 - - 22.51 878.67
MW-B-D 7/17/2023 901.18 - - 21.29 879.89
MW-B-B 12/1/2015 898.57 - - 20.65 877.92
MW-B-B 7/11/2016 898.57 - - 17.92 880.65
MW-B-B 7/12/2016 898.57 - - 17.92 880.65
MW-B-B 7/20/2016 898.57 - - 18.22 880.65
MW-B-B 11/28/2016 898.57 - - 22.55 876.02
MW-B-B 12/14/2016 898.57 - - 22.88 875.69
MW-B-B 6/26/2017 898.57 - - 19.22 879.35
MW-B-B 12/11/2017 898.57 - - 23.51 875.06
MW-B-B 7/9/2018 898.57 - - 21.54 877.03
MW-B-B 12/12/2018 898.57 - - 17.71 880.86
MW-B-B 6/10/2019 898.57 - - 15.81 882.76
MW-B-B 12/9/2019 898.57 - - 18.65 879.92
MW-B-B 6/11/2020 898.57 - - 14.13 884.44
MW-B-B 12/14/2020 898.57 - - 15.13 883.44
MW-B-B 6/14/2021 898.57 - - 15.94 882.63
MW-B-B 6/20/2022 898.57 - - 20.68 877.89
MW-B-B 12/5/2022 898.57 - - 21.73 876.84
MW-B-B 7/17/2023 898.57 - - 19.00 879.57
MW-B-B 12/6/2023 898.57 - - 23.33 875.24
MW-C-I 10/26/2015 900.29 - -24.71 875.58
MW-C-I 7/11/2016 900.29 - - 19.95 880.34
MW-C-I 7/12/2016 900.29 - - 19.95 880.34
MW-C-I 7/20/2016 900.29 - - 19.38 880.34
MW-C-I 11/28/2016 900.29 - - 24.55 875.74
MW-C-I 12/13/2016 900.29 - - 24.88 875.41
MW-C-I 6/26/2017 900.29 - - 21.53 878.76
Page 25 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-C-I 12/11/2017 900.29 - - 26.58 873.71
MW-C-I 7/9/2018 900.29 - - 23.50 876.79
MW-C-I 12/12/2018 900.29 - - 19.71 880.58
MW-C-I 6/10/2019 900.29 - - 17.70 882.59
MW-C-I 12/9/2019 900.29 - - 20.55 879.74
MW-C-I 6/11/2020 900.29 - - 16.04 884.25
MW-C-I 12/14/2020 900.29 - - 16.90 883.39
MW-C-I 6/14/2021 900.29 - - 17.96 882.33
MW-C-I 6/20/2022 900.29 - - 22.62 877.67
MW-C-I 7/17/2023 900.29 - - 20.98 879.31
MW-C-D 10/26/2015 900.35 - - 24.45 875.90
MW-C-D 7/11/2016 900.35 - - 20.22 880.13
MW-C-D 7/12/2016 900.35 - - 20.22 880.13
MW-C-D 7/20/2016 900.35 - - 20.58 879.77
MW-C-D 11/28/2016 900.35 - - 24.86 875.49
MW-C-D 12/13/2016 900.35 - - 25.16 875.19
MW-C-D 6/26/2017 900.35 - - 21.86 878.49
MW-C-D 12/11/2017 900.35 - - 26.84 873.51
MW-C-D 7/9/2018 900.35 - - 23.88 876.47
MW-C-D 12/12/2018 900.35 - - 20.19 880.16
MW-C-D 6/10/2019 900.35 - - 18.19 882.16
MW-C-D 12/9/2019 900.35 - - 21.05 879.30
MW-C-D 6/11/2020 900.35 - - 16.65 883.70
MW-C-D 12/14/2020 900.35 - - 17.53 882.82
MW-C-D 6/14/2021 900.35 - - 18.47 881.88
MW-C-D 6/20/2022 900.35 - - 22.56 877.79
MW-C-D 7/17/2023 900.35 - - 21.49 878.86
MW-C-B 12/1/2015 897.68 - -20.69 876.99
MW-C-B 7/11/2016 897.68 - - 18.20 879.48
MW-C-B 7/12/2016 897.68 - - 18.20 879.48
MW-C-B 7/20/2016 897.68 - - 18.61 879.07
MW-C-B 11/28/2016 897.68 - - 22.85 874.83
MW-C-B 12/13/2016 897.68 - - 23.12 874.56
MW-C-B 6/26/2017 897.68 - - 19.83 877.85
MW-C-B 12/11/2017 897.68 - - 24.71 872.97
MW-C-B 7/9/2018 897.68 - - 20.91 876.77
Page 26 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-C-B 12/12/2018 897.68 - - 18.33 879.35
MW-C-B 6/10/2019 897.68 - - 16.48 881.20
MW-C-B 12/9/2019 897.68 - - 19.30 878.38
MW-C-B 6/11/2020 897.68 - - 15.03 882.65
MW-C-B 12/14/2020 897.68 - - 15.98 881.70
MW-C-B 6/14/2021 897.68 - - 16.52 881.16
MW-C-B 6/20/2022 897.68 - - 22.65 875.03
MW-C-B 7/17/2023 897.68 - - 19.70 877.98
MW-D-I 10/26/2015 901.15 - - 23.79 877.36
MW-D-I 7/11/2016 901.15 - - 19.38 881.77
MW-D-I 7/12/2016 901.15 - - 19.38 881.77
MW-D-I 7/19/2016 901.15 - - 19.78 881.37
MW-D-I 11/28/2016 901.15 - - 24.10 877.05
MW-D-I 12/14/2016 901.15 - - 24.48 876.67
MW-D-I 6/26/2017 901.15 - - 20.79 880.36
MW-D-I 12/11/2017 901.15 - - 26.14 875.01
MW-D-I 7/9/2018 901.15 - - 23.02 878.13
MW-D-I 12/12/2018 901.15 - - 18.76 882.39
MW-D-I 6/10/2019 901.15 - - 17.16 883.99
MW-D-I 12/9/2019 901.15 - - 19.90 881.25
MW-D-I 6/11/2020 901.15 - - 15.09 886.06
MW-D-I 12/14/2020 901.15 - - 16.28 884.87
MW-D-I 6/14/2021 901.15 - - 17.29 883.86
MW-D-I 6/20/2022 901.15 - - 22.49 878.66
MW-D-I 7/17/2023 901.15 - - 20.31 880.84
MW-D-D 10/26/2015 901.06 - -23.93 877.13
MW-D-D 7/11/2016 901.06 - - 19.45 881.61
MW-D-D 7/12/2016 901.06 - - 19.45 881.61
MW-D-D 7/19/2016 901.06 - - 19.94 881.12
MW-D-D 11/28/2016 901.06 - - 24.29 876.77
MW-D-D 12/13/2016 901.06 - - 24.66 876.40
MW-D-D 6/26/2017 901.06 - - 20.68 880.38
MW-D-D 12/11/2017 901.06 - - 26.35 874.71
MW-D-D 7/9/2018 901.06 - - 23.20 877.86
MW-D-D 12/12/2018 901.06 - - 19.04 882.02
Page 27 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-D-D 6/10/2019 901.06 - - 17.41 883.65
MW-D-D 12/9/2019 901.06 - - 20.10 880.96
MW-D-D 6/11/2020 901.06 - - 15.53 885.53
MW-D-D 12/14/2020 901.06 - - 16.55 884.51
MW-D-D 6/14/2021 901.06 - - 17.81 883.25
MW-D-D 6/20/2022 901.06 - - 22.70 878.36
MW-D-D 7/17/2023 901.06 - - 20.62 880.44
MW-D-B 12/1/2015 898.81 - - 19.76 879.05
MW-D-B 7/11/2016 898.81 - - 17.22 881.59
MW-D-B 7/12/2016 898.81 - - 17.22 881.59
MW-D-B 7/20/2016 898.81 - - 17.67 881.14
MW-D-B 11/28/2016 898.81 - - 21.96 876.85
MW-D-B 12/13/2016 898.81 - - 22.36 876.45
MW-D-B 6/26/2017 898.81 - - 18.45 880.36
MW-D-B 12/11/2017 898.81 - - 24.10 874.71
MW-D-B 7/9/2018 898.81 - - 20.93 877.88
MW-D-B 12/12/2018 898.81 - - 16.81 882.00
MW-D-B 6/10/2019 898.81 - - 14.41 884.40
MW-D-B 12/9/2019 898.81 - - 17.90 880.91
MW-D-B 6/11/2020 898.81 - - 13.15 885.66
MW-D-B 12/14/2020 898.81 - - 14.31 884.50
MW-D-B 6/14/2021 898.81 - - 14.81 884.00
MW-D-B 6/20/2022 898.81 - - 19.46 879.35
MW-D-B 7/17/2023 898.81 - - 18.39 880.42
MW-E-I 10/26/2015 896.94 - -22.28 874.66
MW-E-I 7/11/2016 896.94 - - 17.86 879.08
MW-E-I 7/12/2016 896.94 - - 17.86 879.08
MW-E-I 7/21/2016 896.94 - - 17.93 879.01
MW-E-I 11/28/2016 896.94 - - 22.45 874.49
MW-E-I 12/12/2016 896.94 - - 27.71 869.23
MW-E-I 6/26/2017 896.94 - - 19.47 877.47
MW-E-I 12/11/2017 896.94 - - 24.43 872.51
MW-E-I 7/9/2018 896.94 - - 21.52 875.42
MW-E-I 12/12/2018 896.94 - - 17.78 879.16
MW-E-I 6/10/2019 896.94 - - 15.97 880.97
Page 28 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-E-I 12/9/2019 896.94 - - 18.89 878.05
MW-E-I 6/11/2020 896.94 - - 14.73 882.21
MW-E-I 12/14/2020 896.94 - - 15.52 881.42
MW-E-I 6/14/2021 896.94 - - 16.30 880.64
MW-E-I 6/20/2022 896.94 - - 20.21 876.73
MW-E-I 7/17/2023 896.94 - - 19.28 877.66
MW-E-D 10/26/2015 897.11 - - 22.80 874.31
MW-E-D 7/11/2016 897.11 - - 18.21 878.90
MW-E-D 7/12/2016 897.11 - - 18.21 878.90
MW-E-D 8/15/2016 897.11 - - 18.26 878.85
MW-E-D 11/28/2016 897.11 - - 22.87 874.24
MW-E-D 12/12/2016 897.11 - - 23.08 874.03
MW-E-D 6/26/2017 897.11 - - 19.73 877.38
MW-E-D 12/11/2017 897.11 - - 24.66 872.45
MW-E-D 7/9/2018 897.11 - - 21.98 875.13
MW-E-D 12/12/2018 897.11 - - 18.41 878.70
MW-E-D 6/10/2019 897.11 - - 16.75 880.36
MW-E-D 12/9/2019 897.11 - - 19.40 877.71
MW-E-D 6/11/2020 897.11 - - 15.22 881.89
MW-E-D 12/14/2020 897.11 - - 16.18 880.93
MW-E-D 6/14/2021 897.11 - - 16.73 880.38
MW-E-D 6/20/2022 897.11 - - 20.89 876.22
MW-E-D 7/17/2023 897.11 - - 19.66 877.45
MW-E-B 12/1/2015 894.89 - -18.41 876.48
MW-E-B 7/11/2016 894.89 - - 15.98 878.91
MW-E-B 7/12/2016 894.89 - - 15.98 878.91
MW-E-B 7/21/2016 894.89 - - 16.03 878.86
MW-E-B 11/28/2016 894.89 - - 20.60 874.29
MW-E-B 12/12/2016 894.89 - - 20.88 874.01
MW-E-B 6/26/2017 894.89 - - 17.49 877.40
MW-E-B 12/11/2017 894.89 - - 24.71 870.18
MW-E-B 7/9/2018 894.89 - - 19.71 875.18
MW-E-B 12/12/2018 894.89 - - 16.18 878.71
MW-E-B 6/10/2019 894.89 - - 14.61 880.28
MW-E-B 12/9/2019 894.89 - - 17.15 877.74
Page 29 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-E-B 6/11/2020 894.89 - - 12.98 881.91
MW-E-B 12/14/2020 894.89 - - 13.93 880.96
MW-E-B 6/14/2021 894.89 - - 14.47 880.42
MW-E-B 6/20/2022 894.89 - - 18.51 876.38
MW-E-B 7/17/2023 894.89 - - 17.69 877.20
MW-F-I 10/26/2015 896.86 - - 21.30 875.56
MW-F-I 7/11/2016 896.86 - - 16.73 880.13
MW-F-I 7/12/2016 896.86 - - 16.73 880.13
MW-F-I 7/20/2016 896.86 - - 17.18 879.68
MW-F-I 11/28/2016 896.86 - - 21.50 875.36
MW-F-I 12/12/2016 896.86 - - 21.79 875.07
MW-F-I 6/26/2017 896.86 - - 18.05 878.81
MW-F-I 12/11/2017 896.86 - - 23.45 873.41
MW-F-I 7/9/2018 896.86 - - 20.48 876.38
MW-F-I 12/12/2018 896.86 - - 16.52 880.34
MW-F-I 6/10/2019 896.86 - - 14.56 882.30
MW-F-I 12/9/2019 896.86 - - 17.46 879.40
MW-F-I 6/11/2020 896.86 - - 13.33 883.53
MW-F-I 12/14/2020 896.86 - - 14.08 882.78
MW-F-I 6/14/2021 896.86 - - 15.14 881.72
MW-F-I 6/20/2022 896.86 - - 19.07 877.79
MW-F-I 7/17/2023 896.86 - - 18.11 878.75
MW-F-D 10/26/2015 896.94 - -21.81 875.13
MW-F-D 7/11/2016 896.94 - - 17.49 879.45
MW-F-D 7/12/2016 896.94 - - 17.49 879.45
MW-F-D 7/20/2016 896.94 - - 17.72 879.22
MW-F-D 11/28/2016 896.94 - - 22.08 874.86
MW-F-D 12/12/2016 896.94 - - 22.37 874.57
MW-F-D 6/26/2017 896.94 - - 18.47 878.47
MW-F-D 12/11/2017 896.94 - - 23.93 873.01
MW-F-D 7/9/2018 896.94 - - 21.09 875.85
MW-F-D 12/12/2018 896.94 - - 17.43 879.51
MW-F-D 6/10/2019 896.94 - - 15.70 881.24
MW-F-D 12/9/2019 896.94 - - 18.52 878.42
MW-F-D 6/11/2020 896.94 - - 14.19 882.75
Page 30 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-F-D 12/14/2020 896.94 - - 15.09 881.85
MW-F-D 6/14/2021 896.94 - - 15.84 881.10
MW-F-D 6/20/2022 896.94 - - 24.81 872.13
MW-F-D 7/17/2023 896.94 - - 18.78 878.16
MW-F-B 12/1/2015 895.34 - - 18.44 876.90
MW-F-B 7/11/2016 895.34 - - 15.91 879.43
MW-F-B 7/12/2016 895.34 - - 15.91 879.43
MW-F-B 7/21/2016 895.34 - - 16.02 879.32
MW-F-B 11/28/2016 895.34 - - 20.50 874.84
MW-F-B 12/15/2016 895.34 - - 20.80 874.54
MW-F-B 6/26/2017 895.34 - - 17.43 877.91
MW-F-B 12/11/2017 895.34 - - 22.49 872.85
MW-F-B 7/9/2018 895.34 - - 19.59 875.75
MW-F-B 12/12/2018 895.34 - - 16.01 879.33
MW-F-B 6/10/2019 895.34 - - 14.12 881.22
MW-F-B 12/9/2019 895.34 - - 17.00 878.34
MW-F-B 6/11/2020 895.34 - - 13.19 882.15
MW-F-B 12/14/2020 895.34 - - 13.75 881.59
MW-F-B 6/14/2021 895.34 - - 14.26 881.08
MW-F-B 6/20/2022 895.34 - - 19.03 876.31
MW-F-B 7/17/2023 895.34 - - 17.22 878.12
MW-G-I 10/26/2015 898.12 - -21.59 876.53
MW-G-I 7/11/2016 898.12 - - 17.16 880.96
MW-G-I 7/12/2016 898.12 - - 17.16 880.96
MW-G-I 7/21/2016 898.12 - - 17.76 880.36
MW-G-I 11/28/2016 898.12 - - 21.92 876.20
MW-G-I 12/13/2016 898.12 - - 22.26 875.86
MW-G-I 6/26/2017 898.12 - - 18.38 879.74
MW-G-I 12/11/2017 898.12 - - 23.94 874.18
MW-G-I 7/9/2018 898.12 - - 20.84 877.28
MW-G-I 12/12/2018 898.12 - - 16.74 881.38
MW-G-I 6/10/2019 898.12 - - 16.96 881.16
MW-G-I 12/9/2019 898.12 - - 17.80 880.32
MW-G-I 6/11/2020 898.12 - - 13.37 884.75
MW-G-I 12/14/2020 898.12 - - 14.46 883.66
Page 31 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-G-I 6/14/2021 898.12 - - 16.41 881.71
MW-G-I 6/20/2022 898.12 - - 19.51 878.61
MW-G-I 7/17/2023 898.12 - - 18.32 879.80
MW-G-D 10/26/2015 898.40 - - 22.03 876.37
MW-G-D 7/11/2016 898.40 - - 16.43 881.97
MW-G-D 7/12/2016 898.40 - - 16.43 881.97
MW-G-D 7/21/2016 898.40 - - 18.16 880.24
MW-G-D 11/28/2016 898.40 - - 22.35 876.05
MW-G-D 12/13/2016 898.40 - - 22.69 875.71
MW-G-D 6/26/2017 898.40 - - 18.84 879.56
MW-G-D 12/11/2017 898.40 - - 24.57 873.83
MW-G-D 7/9/2018 898.40 - - 21.29 877.11
MW-G-D 12/12/2018 898.40 - - 17.31 881.09
MW-G-D 6/10/2019 898.40 - - 15.60 882.80
MW-G-D 12/9/2019 898.40 - - 13.50 884.90
MW-G-D 6/11/2020 898.40 - - 13.95 884.45
MW-G-D 12/14/2020 898.40 - - 14.85 883.55
MW-G-D 6/14/2021 898.40 - - 15.94 882.46
MW-G-D 6/20/2022 898.40 - - 20.95 877.45
MW-G-D 7/17/2023 898.40 - - 18.76 879.64
MW-G-B 12/1/2015 896.78 - -18.42 878.36
MW-G-B 7/11/2016 896.78 - - 15.94 880.84
MW-G-B 7/12/2016 896.78 - - 15.94 880.84
MW-G-B 7/21/2016 896.78 - - 16.50 880.28
MW-G-B 11/28/2016 896.78 - - 20.69 876.09
MW-G-B 12/13/2016 896.78 - - 21.05 875.73
MW-G-B 6/26/2017 896.78 - - 17.18 879.60
MW-G-B 12/11/2017 896.78 - - 22.76 874.02
MW-G-B 7/9/2018 896.78 - - 19.86 876.92
MW-G-B 12/12/2018 896.78 - - 15.69 881.09
MW-G-B 6/10/2019 896.78 - - 13.95 882.83
MW-G-B 12/9/2019 896.78 - - 16.79 879.99
MW-G-B 6/11/2020 896.78 - - 12.35 884.43
MW-G-B 12/14/2020 896.78 - - 13.30 883.48
MW-G-B 6/14/2021 896.78 - - 14.30 882.48
Page 32 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-G-B 6/20/2022 896.78 - - 20.73 876.05
MW-G-B 7/17/2023 896.78 - - 17.20 879.58
MW-H-I 10/26/2015 899.78 - - 21.60 878.18
MW-H-I 7/11/2016 899.78 - - 17.04 882.74
MW-H-I 7/12/2016 899.78 - - 17.04 882.74
MW-H-I 7/20/2016 899.78 - - 17.78 882.00
MW-H-I 11/28/2016 899.78 - - 22.38 877.40
MW-H-I 12/13/2016 899.78 - - 22.74 877.04
MW-H-I 6/26/2017 899.78 - - 17.04 882.74
MW-H-I 12/11/2017 899.78 - - 24.48 875.30
MW-H-I 7/9/2018 899.78 - - 21.06 878.72
MW-H-I 12/12/2018 899.78 - - 16.28 883.50
MW-H-I 6/10/2019 899.78 - - 15.16 884.62
MW-H-I 12/9/2019 899.78 - - 17.60 882.18
MW-H-I 6/11/2020 899.78 - - 13.20 886.58
MW-H-I 12/14/2020 899.78 - - 13.75 886.03
MW-H-I 6/14/2021 899.78 - - 15.91 883.87
MW-H-I 6/20/2022 899.78 - - 19.62 880.16
MW-H-I 7/17/2023 899.78 - - 19.35 880.43
MW-H-D 10/26/2015 899.54 - -21.46 878.08
MW-H-D 7/11/2016 899.54 - - 15.89 883.65
MW-H-D 7/12/2016 899.54 - - 15.89 883.65
MW-H-D 7/20/2016 899.54 - - 17.64 881.90
MW-H-D 11/28/2016 899.54 - - 22.25 877.29
MW-H-D 12/13/2016 899.54 - - 22.63 876.91
MW-H-D 6/26/2017 899.54 - - 16.91 882.63
MW-H-D 12/11/2017 899.54 - - 24.29 875.25
MW-H-D 7/9/2018 899.54 - - 20.95 878.59
MW-H-D 12/12/2018 899.54 - - 16.16 883.38
MW-H-D 6/10/2019 899.54 - - 14.98 884.56
MW-H-D 12/9/2019 899.54 - - 17.51 882.03
MW-H-D 6/11/2020 899.54 - - 13.19 886.35
MW-H-D 12/14/2020 899.54 - - 13.74 885.80
MW-H-D 6/14/2021 899.54 - - 15.76 883.78
MW-H-D 6/20/2022 899.54 - - 19.61 879.93
Page 33 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-H-D 7/17/2023 899.54 - - 15.83 883.71
MW-H-B 12/1/2015 897.00 - - 15.99 881.01
MW-H-B 7/11/2016 897.00 - - 13.91 883.09
MW-H-B 7/12/2016 897.00 - - 13.91 883.09
MW-H-B 7/21/2016 897.00 - - 15.20 881.80
MW-H-B 11/28/2016 897.00 - - 19.70 877.30
MW-H-B 12/13/2016 897.00 - - 19.77 877.23
MW-H-B 6/26/2017 897.00 - - 14.56 882.44
MW-H-B 12/11/2017 897.00 - - 21.84 875.16
MW-H-B 7/9/2018 897.00 - - 18.43 878.57
MW-H-B 12/12/2018 897.00 - - 13.72 883.28
MW-H-B 6/10/2019 897.00 - - 12.51 884.49
MW-H-B 12/9/2019 897.00 - - 15.10 881.90
MW-H-B 6/11/2020 897.00 - - 10.67 886.33
MW-H-B 12/14/2020 897.00 - - 12.32 884.68
MW-H-B 6/14/2021 897.00 - - 13.39 883.61
MW-H-B 6/20/2022 897.00 - - 17.02 879.98
MW-H-B 7/17/2023 897.00 - - 18.31 878.69
MW-I-I 10/26/2015 900.21 - -21.24 878.97
MW-I-I 7/11/2016 900.21 - - 16.65 883.56
MW-I-I 7/12/2016 900.21 - - 16.65 883.56
MW-I-I 7/20/2016 900.21 - - 17.56 882.65
MW-I-I 11/28/2016 900.21 - - 22.35 877.86
MW-I-I 12/13/2016 900.21 - - 22.70 877.51
MW-I-I 6/26/2017 900.21 - - 15.88 884.33
MW-I-I 12/11/2017 900.21 - - 24.39 875.82
MW-I-I 7/9/2018 900.21 - - 20.89 879.32
MW-I-I 12/12/2018 900.21 - - 15.63 884.58
MW-I-I 6/10/2019 900.21 - - 14.38 885.83
MW-I-I 12/9/2019 900.21 - - 17.15 883.06
MW-I-I 6/11/2020 900.21 - - 12.80 887.41
MW-I-I 12/14/2020 900.21 - - 12.26 887.95
MW-I-I 6/14/2021 900.21 - - 15.37 884.84
MW-I-I 6/20/2022 900.21 - - 19.40 880.81
MW-I-I 7/17/2023 900.21 - - 18.57 881.64
Page 34 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-I-D 10/26/2015 900.11 - - 21.41 878.70
MW-I-D 7/11/2016 900.11 - - 16.92 883.19
MW-I-D 7/12/2016 900.11 - - 16.92 883.19
MW-I-D 7/20/2016 900.11 - - 17.77 882.34
MW-I-D 11/28/2016 900.11 - - 22.48 877.63
MW-I-D 12/13/2016 900.11 - - 22.84 877.27
MW-I-D 6/26/2017 900.11 - - 16.22 883.89
MW-I-D 12/11/2017 900.11 - - 24.57 875.54
MW-I-D 7/9/2018 900.11 - - 21.07 879.04
MW-I-D 12/12/2018 900.11 - - 16.00 884.11
MW-I-D 6/10/2019 900.11 - - 14.81 885.30
MW-I-D 12/9/2019 900.11 - - 17.44 882.67
MW-I-D 6/11/2020 900.11 - - 13.22 886.89
MW-I-D 12/14/2020 900.11 - - 13.40 886.71
MW-I-D 6/14/2021 900.11 - - 15.68 884.43
MW-I-D 6/20/2022 900.11 - - 20.90 879.21
MW-I-D 7/17/2023 900.11 - - 18.56 881.55
MW-I-B 12/1/2015 897.56 - -15.12 882.44
MW-I-B 7/11/2016 897.56 - - 14.43 883.13
MW-I-B 7/12/2016 897.56 - - 14.43 883.13
MW-I-B 7/20/2016 897.56 - - 15.18 882.38
MW-I-B 11/28/2016 897.56 - - 19.95 877.61
MW-I-B 12/13/2016 897.56 - - 20.30 877.26
MW-I-B 6/26/2017 897.56 - - 13.95 883.61
MW-I-B 12/11/2017 897.56 - - 22.03 875.53
MW-I-B 7/9/2018 897.56 - - 18.55 879.01
MW-I-B 12/12/2018 897.56 - - 13.50 884.06
MW-I-B 6/10/2019 897.56 - - 12.38 885.18
MW-I-B 12/9/2019 897.56 - - 15.00 882.56
MW-I-B 6/11/2020 897.56 - - 10.70 886.86
MW-I-B 12/14/2020 897.56 - - 10.90 886.66
Page 35 of 36
Table 2
Historical Groundwater Elevation Data - Onsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
MW-I-B 6/14/2021 897.56 - - 13.12 884.44
MW-I-B 6/20/2022 897.56 - - 17.94 879.62
MW-I-B 7/17/2023 897.56 - - 15.93 881.63
Notes:
ft - feet
NA - not applicable
Page 36 of 36
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
Units - ft ft ft ft ft
AMW-8S 8/5/2003 889.93 - - 10.46 879.47
AMW-8S 8/5/2003 889.93 - - 10.46 879.47
AMW-8S 8/20/2003 889.93 9.26 0.01 9.27 880.67
AMW-8S 11/10/2003 889.93 - - 12.60 877.33
AMW-8S 11/10/2003 889.93 - - 12.60 877.33
AMW-8S 12/23/2003 889.93 - - 12.00 877.93
AMW-8S 1/29/2004 889.93 - - 13.68 876.25
AMW-8S 3/30/2004 889.93 - - 13.08 876.85
AMW-8S 4/23/2004 889.93 - - 13.26 876.67
AMW-8S 5/20/2004 889.93 - - 14.40 875.53
AMW-8S 6/28/2004 889.93 - - 15.65 874.28
AMW-8S 8/30/2004 889.93 - - 18.52 871.41
AMW-8S 1/26/2005 889.93 - - 14.44 875.49
AMW-8S 2/18/2005 889.93 - - 14.19 875.74
AMW-8S 3/29/2005 889.93 - - 13.68 876.25
AMW-8S 11/5/2010 889.93 - - 17.37 872.56
AMW-8S 10/26/2015 889.93 - -18.61 871.32
AMW-8S 7/11/2016 889.93 - - 14.12 875.81
AMW-8S 7/12/2016 889.93 - - 14.12 875.81
AMW-8S 8/2/2016 889.93 - - 15.35 874.58
AMW-8S 11/29/2016 889.93 - - 18.75 871.18
AMW-8S 12/13/2016 889.93 - - 18.95 870.98
AMW-8S 6/26/2017 889.93 - - 14.63 875.30
AMW-8S 12/11/2017 889.93 - - 20.31 869.62
AMW-8S 7/9/2018 889.93 - - 19.93 870.00
AMW-8S 12/12/2018 889.93 - - 14.11 875.82
AMW-8S 6/10/2019 889.93 - - 13.07 876.86
AMW-8S 12/9/2019 889.93 - - 15.57 874.36
AMW-8S 6/11/2020 889.93 - - 11.72 878.21
AMW-8S 12/14/2020 889.93 - - 12.72 877.21
AMW-8S 6/14/2021 889.93 - - 14.36 875.57
AMW-8S 6/20/2022 889.93 - - 16.59 873.34
AMW-8S 7/17/2023 889.93 - - 15.45 874.48
AMW-9S 8/5/2003 889.74 - - 7.85 881.89
AMW-9S 8/20/2003 889.74 6.25 0.01 6.26 883.49
Page 1 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-9S 11/10/2003 889.74 - - 9.11 880.63
AMW-9S 12/23/2003 889.74 - - 8.80 880.94
AMW-9S 1/29/2004 889.74 - - 10.40 879.34
AMW-9S 3/30/2004 889.74 - - 9.48 880.26
AMW-9S 4/23/2004 889.74 - - 9.86 879.88
AMW-9S 5/20/2004 889.74 - - 10.93 878.81
AMW-9S 6/28/2004 889.74 - - 12.38 877.36
AMW-9S 8/30/2004 889.74 - - 13.28 876.46
AMW-9S 1/26/2005 889.74 - - 11.20 878.54
AMW-9S 2/18/2005 889.74 - - 10.77 878.97
AMW-9S 3/29/2005 889.74 - - 10.05 879.69
AMW-9S 11/5/2010 889.74 - - 14.13 875.61
AMW-9S 10/26/2015 889.74 - -15.95 873.79
AMW-9S 7/11/2016 889.74 - - 11.39 878.35
AMW-9S 7/12/2016 889.74 - - 11.39 878.35
AMW-9S 7/25/2016 889.74 - - 11.98 877.76
AMW-9S 11/29/2016 889.74 - - 16.01 873.73
AMW-9S 12/13/2016 889.74 - - 16.26 873.48
AMW-9S 6/26/2017 889.74 - - 11.32 878.42
AMW-9S 12/11/2017 889.74 - - 17.68 872.06
AMW-9S 7/9/2018 889.74 - - 15.00 874.74
AMW-9S 12/12/2018 889.74 - - 11.55 878.19
AMW-9S 6/10/2019 889.74 - - 8.26 881.48
AMW-9S 12/9/2019 889.74 - - 12.66 877.08
AMW-9S 6/11/2020 889.74 - - 8.56 881.18
AMW-9S 12/14/2020 889.74 - - 8.41 881.33
AMW-9S 6/14/2021 889.74 - - 10.08 879.66
AMW-9S 6/20/2022 889.74 - - 13.22 876.52
AMW-9S 7/17/2023 889.74 - - 12.76 876.98
AMW-10S 8/5/2003 892.90 - - 5.00 887.90
AMW-10S 8/20/2003 892.90 - - 4.22 888.68
AMW-10S 11/10/2003 892.90 - - 8.37 884.53
AMW-10S 12/23/2003 892.90 - - 6.67 886.23
AMW-10S 1/29/2004 892.90 - - 8.40 884.50
AMW-10S 3/30/2004 892.90 - - 8.10 884.80
AMW-10S 4/23/2004 892.90 - - 8.01 884.89
Page 2 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-10S 5/20/2004 892.90 - - 10.14 882.76
AMW-10S 6/28/2004 892.90 - - 12.18 880.72
AMW-10S 8/30/2004 892.90 - - 12.34 880.56
AMW-10S 1/26/2005 892.90 - - 9.36 883.54
AMW-10S 2/18/2005 892.90 - - 7.70 885.20
AMW-10S 3/29/2005 892.90 - - 6.33 886.57
AMW-10S 11/5/2010 892.90 - - 13.68 879.22
AMW-10S 10/26/2015 892.90 - -13.91 878.99
AMW-10S 7/11/2016 892.90 - - 8.52 884.38
AMW-10S 7/12/2016 892.90 - - 8.52 884.38
AMW-10S 8/2/2016 892.90 - - 11.62 881.28
AMW-10S 11/29/2016 892.90 - - 15.50 877.40
AMW-10S 12/13/2016 892.90 - - 16.16 876.74
AMW-10S 6/26/2017 892.90 - - 7.84 885.06
AMW-10S 12/11/2017 892.90 - - 21.86 871.04
MW-10S 7/9/2018 892.90 - - 13.95 878.95
AMW-10S 12/12/2018 892.90 - - 7.75 885.15
AMW-10S 6/10/2019 892.90 - - 8.34 884.56
AMW-10S 12/9/2019 892.90 - - 9.81 883.09
AMW-10S 6/11/2020 892.90 - - 6.77 886.13
AMW-10S 12/14/2020 892.90 - - 6.11 886.79
AMW-10S 6/14/2021 892.90 - - 9.14 883.76
AMW-10S 6/20/2022 892.90 - - 12.77 880.13
AMW-10S 7/17/2023 892.90 - - 11.53 881.37
AMW-11S 8/5/2003 884.86 - - 6.85 878.01
AMW-11S 8/20/2003 884.86 - - 5.90 878.96
AMW-11S 11/10/2003 884.86 - - 8.65 876.21
AMW-11S 12/23/2003 884.86 - - 8.10 876.76
AMW-11S 1/29/2004 884.86 - - 9.42 875.44
AMW-11S 3/30/2004 884.86 - - 8.98 875.88
AMW-11S 4/23/2004 884.86 - - 9.23 875.63
AMW-11S 5/20/2004 884.86 - - 10.30 874.56
AMW-11S 6/28/2004 884.86 - - 11.56 873.30
AMW-11S 8/30/2004 884.86 - - 12.36 872.50
AMW-11S 1/26/2005 884.86 - - 10.23 874.63
AMW-11S 2/18/2005 884.86 - - 9.65 875.21
Page 3 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-11S 3/29/2005 884.86 - - 8.81 876.05
AMW-11S 6/2/2006 884.86 - - 13.30 871.56
AMW-11S 6/16/2006 884.86 - - 12.39 872.47
AMW-11S 1/11/2008 884.86 - - 14.88 869.98
AMW-11S 11/5/2010 884.86 - - 13.00 871.86
AMW-11S 1/10/2014 884.86 - - 10.36 874.50
AMW-11S 1/17/2014 884.86 - - 9.86 875.00
AMW-11S 1/24/2014 884.86 - - 9.97 874.89
AMW-11S 1/31/2014 884.86 - - 10.15 874.71
AMW-11S 2/7/2014 884.86 - - 9.81 875.05
AMW-11S 2/14/2014 884.86 - - 9.48 875.38
AMW-11S 2/21/2014 884.86 - - 8.98 875.88
AMW-11S 2/28/2014 884.86 - - 9.55 875.31
AMW-11S 3/7/2014 884.86 - - 9.02 875.84
AMW-11S 3/14/2014 884.86 - - 9.11 875.75
AMW-11S 3/21/2014 884.86 - - 9.02 875.84
AMW-11S 3/28/2014 884.86 - - 9.12 875.74
AMW-11S 4/4/2014 884.86 - - 8.78 876.08
AMW-11S 4/11/2014 884.86 - - 8.35 876.51
AMW-11S 4/18/2014 884.86 - - 8.09 876.77
AMW-11S 4/25/2014 884.86 - - 8.47 876.39
AMW-11S 5/2/2014 884.86 - - 8.81 876.05
AMW-11S 5/9/2014 884.86 - - 9.13 875.73
AMW-11S 5/16/2014 884.86 - - 8.83 876.03
AMW-11S 5/23/2014 884.86 - - 9.28 875.58
AMW-11S 5/30/2014 884.86 - - 9.63 875.23
AMW-11S 6/6/2014 884.86 - - 9.89 874.97
AMW-11S 6/13/2014 884.86 - - 10.29 874.57
AMW-11S 6/20/2014 884.86 - - 10.53 874.33
AMW-11S 6/27/2014 884.86 - - 10.26 874.60
AMW-11S 7/5/2014 884.86 - - 10.82 874.04
AMW-11S 7/11/2014 884.86 - - 11.52 873.34
AMW-11S 3/5/2015 884.86 - -12.21 872.65
AMW-11S 5/27/2015 884.86 - -12.15 872.71
AMW-11S 6/29/2015 884.86 - -13.68 871.18
AMW-11S 7/30/2015 884.86 - -15.00 869.86
AMW-11S 8/20/2015 884.86 - -15.23 869.63
Page 4 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-11S 9/9/2015 884.86 - -15.70 869.16
AMW-11S 10/15/2015 884.86 - -13.95 870.91
AMW-11S 10/26/2015 884.86 - -14.24 870.62
AMW-11S 12/4/2015 884.86 - -10.87 873.99
AMW-11S 1/12/2016 884.86 - - 9.26 875.60
AMW-11S 5/26/2016 884.86 - - 8.21 876.65
AMW-11S 7/11/2016 884.86 - - 10.18 874.68
AMW-11S 7/12/2016 884.86 - - 10.18 874.68
AMW-11S 7/25/2016 884.86 - - 10.90 873.96
AMW-11S 9/28/2016 884.86 - - 13.44 871.42
AMW-11S 11/29/2016 884.86 - - 14.50 870.36
AMW-11S 12/14/2016 884.86 - - 17.56 867.30
AMW-11S 5/17/2017 884.86 - - 12.92 871.94
AMW-11S 6/26/2017 884.86 - - 10.48 874.38
AMW-11S 8/8/2017 884.86 - - 12.70 872.16
AMW-11S 11/28/2017 884.86 - - 15.74 869.12
AMW-11S 12/11/2017 884.86 - - 15.91 868.95
AMW-11S 1/25/2018 884.86 - - 15.54 869.32
AMW-11S 5/21/2018 884.86 - - 12.49 872.37
AMW-11S 7/9/2018 884.86 - - 13.78 871.08
AMW-11S 8/16/2018 884.86 - - 12.71 872.15
AMW-11S 11/29/2018 884.86 - - 10.32 874.54
AMW-11S 12/12/2018 884.86 - - 9.94 874.92
AMW-11S 3/27/2019 884.86 - - 7.23 877.63
AMW-11S 5/29/2019 884.86 - - 9.40 875.46
AMW-11S 6/10/2019 884.86 - - 9.22 875.64
AMW-11S 8/6/2019 884.86 - - 10.10 874.76
AMW-11S 11/8/2019 884.86 - - 12.36 872.50
AMW-11S 12/9/2019 884.86 - - 11.30 873.56
AMW-11S 3/6/2020 884.86 - - 7.32 877.54
AMW-11S 6/11/2020 884.86 - - 4.34 880.52
AMW-11S 8/24/2020 884.86 - - 10.75 874.11
AMW-11S 11/30/2020 884.86 - - 9.14 875.72
AMW-11S 12/14/2020 884.86 - - 8.79 876.07
AMW-11S 3/29/2021 884.86 - - 6.26 878.60
AMW-11S 6/14/2021 884.86 - - 9.55 875.31
AMW-11S 9/28/2021 884.86 - - 12.64 872.22
Page 5 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-11S 12/28/2021 884.86 - - 14.22 870.64
AMW-11S 4/1/2022 884.86 - - 10.63 874.23
AMW-11S 6/20/2022 884.86 - - 12.74 872.12
AMW-11S 9/22/2022 884.86 - - 14.36 870.50
AMW-11S 12/5/2022 884.86 - - 14.65 870.21
AMW-11S 4/10/2023 884.86 - - 8.93 875.93
AMW-11S 7/17/2023 884.86 - - 11.14 873.72
AMW-11S 9/18/2023 884.86 - - 13.70 871.16
AMW-11S 12/6/2023 884.86 - - 16.30 868.56
AMW-11S 3/1/2024 884.86 - - 11.79 873.07
AMW-12S 8/5/2003 897.26 - - 9.45 887.81
AMW-12S 8/20/2003 897.26 - - 7.65 889.61
AMW-12S 11/10/2003 897.26 - - 12.27 884.99
AMW-12S 12/23/2003 897.26 - - 10.50 886.76
AMW-12S 1/29/2004 897.26 - - 12.75 884.51
AMW-12S 3/30/2004 897.26 - - 11.68 885.58
AMW-12S 4/23/2004 897.26 - - 11.68 885.58
AMW-12S 5/20/2004 897.26 - - 13.53 883.73
AMW-12S 6/28/2004 897.26 - - 15.57 881.69
AMW-12S 8/30/2004 897.26 - - 15.55 881.71
AMW-12S 1/26/2005 897.26 - - 12.68 884.58
AMW-12S 2/18/2005 897.26 - - 12.34 884.92
AMW-12S 3/29/2005 897.26 - - 10.12 887.14
AMW-12S 11/5/2010 897.26 - - 16.71 880.55
AMW-12S 10/26/2015 897.26 - -16.18 881.08
AMW-12S 7/11/2016 897.26 - - 12.76 884.50
AMW-12S 7/12/2016 897.26 - - 12.76 884.50
AMW-12S 8/2/2016 897.26 - - 14.85 882.41
AMW-12S 11/29/2016 897.26 - - 18.39 878.87
AMW-12S 6/26/2017 897.26 - - 10.52 886.74
AMW-12S 12/11/2017 897.26 - - 20.21 877.05
AMW-12S 7/9/2018 897.26 - - 16.59 880.67
AMW-12S 12/12/2018 897.26 - - 10.85 886.41
AMW-12S 6/10/2019 897.26 - - 12.10 885.16
AMW-12S 12/9/2019 897.26 - - 12.82 884.44
AMW-12S 6/11/2020 897.26 - - 10.55 886.71
Page 6 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-12S 12/14/2020 897.26 - - 8.83 888.43
AMW-12S 6/14/2021 897.26 - - 13.03 884.23
AMW-12S 6/20/2022 897.26 - - 15.95 881.31
AMW-12S 7/17/2023 897.26 - - 14.57 882.69
AMW-13B 5/20/2004 883.77 - - 9.27 874.50
AMW-13B 6/28/2004 883.77 - - 10.52 873.25
AMW-13B 8/30/2004 883.77 - - 11.30 872.47
AMW-13B 1/26/2005 883.77 - - 9.22 874.55
AMW-13B 2/18/2005 883.77 - - 8.98 874.79
AMW-13B 3/29/2005 883.77 - - 8.17 875.60
AMW-13B 10/26/2015 883.77 - -12.61 871.16
AMW-13B 7/11/2016 883.77 - - 9.09 874.68
AMW-13B 7/12/2016 883.77 - - 9.09 874.68
AMW-13B 7/26/2016 883.77 - - 9.93 873.84
AMW-13B 11/29/2016 883.77 - - 13.41 870.36
AMW-13B 12/16/2016 883.77 - - 13.59 870.18
AMW-13B 6/26/2017 883.77 - - 9.41 874.36
AMW-13B 12/11/2017 883.77 - - 14.78 868.99
AMW-13B 7/9/2018 883.77 - - 12.70 871.07
AMW-13B 12/12/2018 883.77 - - 8.88 874.89
AMW-13B 6/10/2019 883.77 - - 8.18 875.59
AMW-13B 12/9/2019 883.77 - - 10.21 873.56
AMW-13B 6/11/2020 883.77 - - 7.02 876.75
AMW-13B 12/14/2020 883.77 - - 7.85 875.92
AMW-13B 6/14/2021 883.77 - - 8.50 875.27
AMW-13B 6/20/2022 883.77 - - 11.69 872.08
AMW-13B 12/5/2022 883.77 - - 12.40 871.37
AMW-13B 7/17/2023 883.77 - - 13.13 870.64
AMW-13B 12/6/2023 883.77 - - 14.29 869.48
AMW-13D 5/20/2004 883.19 - - 8.84 874.35
AMW-13D 6/28/2004 883.19 - - 10.05 873.14
AMW-13D 8/30/2004 883.19 - - 10.80 872.39
AMW-13D 1/26/2005 883.19 - - 8.70 874.49
AMW-13D 2/18/2005 883.19 - - 8.59 874.60
AMW-13D 3/29/2005 883.19 - - 7.89 875.30
Page 7 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-13D 10/26/2015 883.19 - -12.97 870.22
AMW-13D 7/11/2016 883.19 - - 8.62 874.57
AMW-13D 7/12/2016 883.19 - - 8.62 874.57
AMW-13D 7/26/2016 883.19 - - 9.41 873.78
AMW-13D 11/29/2016 883.19 - - 12.90 870.29
AMW-13D 12/15/2016 883.19 - - 13.02 870.17
AMW-13D 6/26/2017 883.19 - - 8.93 874.26
AMW-13D 12/11/2017 883.19 - - 14.25 868.94
AMW-13D 7/9/2018 883.19 - - 12.20 870.99
AMW-13D 12/12/2018 883.19 - - 8.34 874.85
AMW-13D 6/11/2019 883.19 - - 7.70 875.49
AMW-13D 12/9/2019 883.19 - - 9.69 873.50
AMW-13D 6/11/2020 883.19 - - 6.52 876.67
AMW-13D 12/14/2020 883.19 - - 7.21 875.98
AMW-13D 6/14/2021 883.19 - - 8.02 875.17
AMW-13D 6/20/2022 883.19 - - 11.18 872.01
AMW-13D 7/17/2023 883.19 - - 10.45 872.74
AMW-13I 5/20/2004 882.35 - - 8.02 874.33
AMW-13I 6/28/2004 882.35 - - 9.27 873.08
AMW-13I 8/30/2004 882.35 - - 10.05 872.30
AMW-13I 1/26/2005 882.35 - - 7.93 874.42
AMW-13I 2/18/2005 882.35 - - 7.71 874.64
AMW-13I 3/29/2005 882.35 - - 6.98 875.37
AMW-13I 10/26/2015 882.35 - -12.09 870.26
AMW-13I 7/11/2016 882.35 - - 7.83 874.52
AMW-13I 7/12/2016 882.35 - - 7.83 874.52
AMW-13I 7/26/2016 882.35 - - 8.65 873.70
AMW-13I 11/29/2016 882.35 - - 12.10 870.25
AMW-13I 12/15/2016 882.35 - - 12.23 870.12
AMW-13I 6/26/2017 882.35 - - 8.14 874.21
AMW-13I 12/11/2017 882.35 - - 13.44 868.91
AMW-13I 7/9/2018 882.35 - - 11.37 870.98
AMW-13I 12/12/2018 882.35 - - 7.55 874.80
AMW-13I 6/10/2019 882.35 - - 6.96 875.39
AMW-13I 12/9/2019 882.35 - - 8.91 873.44
AMW-13I 6/11/2020 882.35 - - 5.85 876.50
Page 8 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-13I 12/14/2020 882.35 - - 6.54 875.81
AMW-13I 6/14/2021 882.35 - - 7.25 875.10
AMW-13I 6/20/2022 882.35 - - 10.39 871.96
AMW-13I 7/17/2023 882.35 - - 9.51 872.84
AMW-13S 8/5/2003 883.17 - - 5.65 877.52
AMW-13S 8/20/2003 883.17 - - 4.86 878.31
AMW-13S 11/10/2003 883.17 - - 7.30 875.87
AMW-13S 12/23/2003 883.17 - - 6.72 876.45
AMW-13S 1/29/2004 883.17 - - 7.93 875.24
AMW-13S 3/30/2004 883.17 - - 7.58 875.59
AMW-13S 4/23/2004 883.17 - - 7.83 875.34
AMW-13S 5/20/2004 883.17 - - 8.80 874.37
AMW-13S 6/28/2004 883.17 - - 10.12 873.05
AMW-13S 8/30/2004 883.17 - - 10.96 872.21
AMW-13S 1/26/2005 883.17 - - 8.81 874.36
AMW-13S 2/18/2005 883.17 - - 8.20 874.97
AMW-13S 3/29/2005 883.17 - - 7.44 875.73
AMW-13S 6/2/2006 883.17 - - 11.71 871.46
AMW-13S 6/16/2006 883.17 - - 10.75 872.42
AMW-13S 1/11/2008 883.17 - - 13.24 869.93
AMW-13S 11/5/2010 883.17 - - 11.50 871.67
AMW-13S 1/10/2014 883.17 - - 8.89 874.28
AMW-13S 1/17/2014 883.17 - - 8.47 874.70
AMW-13S 1/24/2014 883.17 - - 8.59 874.58
AMW-13S 1/31/2014 883.17 - - 8.77 874.40
AMW-13S 2/7/2014 883.17 - - 8.56 874.61
AMW-13S 2/14/2014 883.17 - - 8.21 874.96
AMW-13S 2/21/2014 883.17 - - 7.91 875.26
AMW-13S 2/28/2014 883.17 - - 8.14 875.03
AMW-13S 3/7/2014 883.17 - - 7.21 875.96
AMW-13S 3/14/2014 883.17 - - 7.28 875.89
AMW-13S 3/21/2014 883.17 - - 7.21 875.96
AMW-13S 3/28/2014 883.17 - - 7.33 875.84
AMW-13S 4/4/2014 883.17 - - 7.42 875.75
AMW-13S 4/11/2014 883.17 - - 7.18 875.99
AMW-13S 4/18/2014 883.17 - - 6.93 876.24
Page 9 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-13S 4/25/2014 883.17 - - 7.21 875.96
AMW-13S 5/2/2014 883.17 - - 7.56 875.61
AMW-13S 5/9/2014 883.17 - - 7.73 875.44
AMW-13S 5/16/2014 883.17 - - 7.55 875.62
AMW-13S 5/23/2014 883.17 - - 7.97 875.20
AMW-13S 5/30/2014 883.17 - - 8.21 874.96
AMW-13S 6/6/2014 883.17 - - 8.57 874.60
AMW-13S 6/13/2014 883.17 - - 8.91 874.26
AMW-13S 6/20/2014 883.17 - - 9.23 873.94
AMW-13S 6/27/2014 883.17 - - 9.44 873.73
AMW-13S 7/5/2014 883.17 - - 9.87 873.30
AMW-13S 7/11/2014 883.17 - - 10.26 872.91
AMW-13S 3/5/2015 883.17 - -13.50 869.67
AMW-13S 5/27/2015 883.17 - -10.67 872.50
AMW-13S 6/29/2015 883.17 - -12.26 870.91
AMW-13S 7/30/2015 883.17 - -13.62 869.55
AMW-13S 8/20/2015 883.17 - -13.70 869.47
AMW-13S 9/9/2015 883.17 - -14.31 868.86
AMW-13S 10/15/2015 883.17 - -12.50 870.67
AMW-13S 10/26/2015 883.17 - -12.77 870.40
AMW-13S 12/4/2015 883.17 - -9.66 873.51
AMW-13S 1/12/2016 883.17 - - 7.99 875.18
AMW-13S 5/26/2016 883.17 - - 6.74 876.43
AMW-13S 7/11/2016 883.17 - - 8.71 874.46
AMW-13S 7/12/2016 883.17 - - 8.71 874.46
AMW-13S 7/26/2016 883.17 - - 9.65 873.52
AMW-13S 9/28/2016 883.17 - - 12.10 871.07
AMW-13S 11/29/2016 883.17 - - 13.07 870.10
AMW-13S 12/15/2016 883.17 - - 13.15 870.02
AMW-13S 12/27/2016 883.17 - - 13.30 869.87
AMW-13S 5/17/2017 883.17 - - 11.44 871.73
AMW-13S 6/26/2017 883.17 - - 9.12 874.05
AMW-13S 8/8/2017 883.17 - - 11.38 871.79
AMW-13S 11/28/2017 883.17 - - 14.25 868.92
AMW-13S 12/11/2017 883.17 - - 14.30 868.87
AMW-13S 1/25/2018 883.17 - - 13.89 869.28
AMW-13S 5/21/2018 883.17 - - 10.99 872.18
Page 10 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-13S 7/9/2018 883.17 - - 12.35 870.82
AMW-13S 8/16/2018 883.17 - - 11.29 871.88
AMW-13S 11/29/2018 883.17 - - 8.99 874.18
AMW-13S 12/12/2018 883.17 - - 8.45 874.72
AMW-13S 3/27/2019 883.17 - - 5.97 877.20
AMW-13S 5/29/2019 883.17 - - 8.08 875.09
AMW-13S 6/10/2019 883.17 - - 7.88 875.29
AMW-13S 8/6/2019 883.17 - - 8.79 874.38
AMW-13S 11/8/2019 883.17 - - 10.88 872.29
AMW-13S 12/9/2019 883.17 - - 10.83 872.34
AMW-13S 3/6/2020 883.17 - - 6.07 877.10
AMW-13S 6/11/2020 883.17 - - 6.90 876.27
AMW-13S 8/24/2020 883.17 - - 6.39 876.78
AMW-13S 11/30/2020 883.17 - - 7.43 875.74
AMW-13S 12/14/2020 883.17 - - 7.06 876.11
AMW-13S 3/29/2021 883.17 - - 5.14 878.03
AMW-13S 6/14/2021 883.17 - - 8.20 874.97
AMW-13S 9/28/2021 883.17 - - 11.25 871.92
AMW-13S 12/28/2021 883.17 - - 11.78 871.39
AMW-13S 4/1/2022 883.17 - - 9.14 874.03
AMW-13S 6/20/2022 883.17 - - 11.32 871.85
AMW-13S 9/22/2022 883.17 - - 12.94 870.23
AMW-13S 12/5/2022 883.17 - - 11.95 871.22
AMW-13S 4/10/2023 883.17 - - 7.48 875.69
AMW-13S 7/17/2023 883.17 - - 9.82 873.35
AMW-13S 9/18/2023 883.17 - - 12.26 870.91
AMW-13S 12/6/2023 883.17 - - 13.90 869.27
AMW-13S 3/1/2024 883.17 - - 10.20 872.97
AMW-14S 8/5/2003 890.35 - - 8.04 882.31
AMW-14S 8/20/2003 890.35 - - 7.02 883.33
AMW-14S 11/10/2003 890.35 - - 9.64 880.71
AMW-14S 12/23/2003 890.35 - - 9.05 881.30
AMW-14S 1/29/2004 890.35 - - 10.55 879.80
AMW-14S 3/30/2004 890.35 - - 9.40 880.95
AMW-14S 4/23/2004 890.35 - - 9.83 880.52
AMW-14S 5/20/2004 890.35 - - 11.10 879.25
Page 11 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-14S 6/28/2004 890.35 - - 13.00 877.35
AMW-14S 8/30/2004 890.35 - - 13.75 876.60
AMW-14S 1/26/2005 890.35 - - 11.08 879.27
AMW-14S 2/18/2005 890.35 - - 10.74 879.61
AMW-14S 3/29/2005 890.35 - - 9.57 880.78
AMW-14S 11/5/2010 890.35 - - 14.91 875.44
AMW-14S 3/5/2015 890.35 - -13.35 877.00
AMW-14S 5/27/2015 890.35 - -13.25 877.10
AMW-14S 6/29/2015 890.35 - -15.13 875.22
AMW-14S 7/30/2015 890.35 - -17.86 872.49
AMW-14S 8/20/2015 890.35 - -17.15 873.20
AMW-14S 9/9/2015 890.35 - -17.52 872.83
AMW-14S 10/15/2015 890.35 - -15.64 874.71
AMW-14S 10/26/2015 890.35 - -15.78 874.57
AMW-14S 12/4/2015 890.35 - -13.08 877.27
AMW-14S 1/12/2016 890.35 - - 11.31 879.04
AMW-14S 5/26/2016 890.35 - - 9.91 880.44
AMW-14S 7/11/2016 890.35 - - 11.68 878.67
AMW-14S 7/12/2016 890.35 - - 11.68 878.67
AMW-14S 7/22/2016 890.35 - - 12.11 878.24
AMW-14S 9/28/2016 890.35 - - 15.45 874.90
AMW-14S 11/29/2016 890.35 - - 16.25 874.10
AMW-14S 12/13/2016 890.35 - - 16.45 873.90
AMW-14S 5/17/2017 890.35 - - 14.50 875.85
AMW-14S 6/26/2017 890.35 - - 12.30 878.05
AMW-14S 8/8/2017 890.35 - - 14.49 875.86
AMW-14S 11/28/2017 890.35 - - 17.65 872.70
AMW-14S 12/11/2017 890.35 - - 17.82 872.53
AMW-14S 1/25/2018 890.35 17.29 0.02 17.31 873.06
AMW-14S 5/21/2018 890.35 - - 13.76 876.59
AMW-14S 7/9/2018 890.35 - - 15.09 875.26
AMW-14S 8/16/2018 890.35 - - 14.02 876.33
AMW-14S 11/29/2018 890.35 - - 11.65 878.70
AMW-14S 12/12/2018 890.35 - - 11.30 879.05
AMW-14S 3/27/2019 890.35 - - 8.13 882.22
AMW-14S 5/29/2019 890.35 - - 10.25 880.10
AMW-14S 6/10/2019 890.35 - - 10.45 879.90
Page 12 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-14S 8/6/2019 890.35 - - 11.06 879.29
AMW-14S 11/8/2019 890.35 - - 13.70 876.65
AMW-14S 12/9/2019 890.35 - - 12.53 877.82
AMW-14S 3/6/2020 890.35 - - 7.79 882.56
AMW-14S 6/11/2020 890.35 - - 5.66 884.69
AMW-14S 8/24/2020 890.35 - - 11.86 878.49
AMW-14S 11/30/2020 890.35 - - 9.73 880.62
AMW-14S 12/14/2020 890.35 - - 10.12 880.23
AMW-14S 3/29/2021 890.35 - - 6.82 883.53
AMW-14S 6/14/2021 890.35 - - 10.56 879.79
AMW-14S 9/28/2021 890.35 - - 13.89 876.46
AMW-14S 12/28/2021 890.35 - - 15.56 874.79
AMW-14S 4/1/2022 890.35 - - 11.51 878.84
AMW-14S 6/20/2022 890.35 - - 13.90 876.45
AMW-14S 9/22/2022 890.35 - - 15.73 874.62
AMW-14S 12/5/2022 890.35 - - 14.84 875.51
AMW-14S 4/10/2023 890.35 - - 10.05 880.30
AMW-14S 7/17/2023 890.35 - - 12.87 877.48
AMW-14S 9/18/2023 890.35 - - 15.18 875.17
AMW-14S 12/6/2023 890.35 - - 16.92 873.43
AMW-14S 3/1/2024 890.35 - - 12.99 877.36
AMW-15S 8/5/2003 881.42 - - 6.24 875.18
AMW-15S 8/20/2003 881.42 - - 5.48 875.94
AMW-15S 11/10/2003 881.42 - - 7.28 874.14
AMW-15S 12/23/2003 881.42 - - 6.64 874.78
AMW-15S 1/29/2004 881.42 - - 7.74 873.68
AMW-15S 3/30/2004 881.42 - - 7.15 874.27
AMW-15S 4/23/2004 881.42 - - 7.52 873.90
AMW-15S 5/20/2004 881.42 - - 8.50 872.92
AMW-15S 6/28/2004 881.42 - - 9.90 871.52
AMW-15S 8/30/2004 881.42 - - 10.45 870.97
AMW-15S 1/26/2005 881.42 - - 8.16 873.26
AMW-15S 2/18/2005 881.42 - - 7.89 873.53
AMW-15S 3/29/2005 881.42 - - 7.00 874.42
AMW-15S 6/2/2006 881.42 - - 10.88 870.54
AMW-15S 6/16/2006 881.42 - - 9.95 871.47
Page 13 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-15S 1/11/2008 881.42 - - 12.10 869.32
AMW-15S 11/5/2010 881.42 - - 10.75 870.67
AMW-15S 1/10/2014 881.42 - - 8.15 873.27
AMW-15S 1/17/2014 881.42 - - 7.93 873.49
AMW-15S 1/24/2014 881.42 - - 8.11 873.31
AMW-15S 1/31/2014 881.42 - - 8.25 873.17
AMW-15S 2/7/2014 881.42 - - 7.91 873.51
AMW-15S 2/14/2014 881.42 - - 7.63 873.79
AMW-15S 2/21/2014 881.42 - - 7.44 873.98
AMW-15S 2/28/2014 881.42 - - 7.68 873.74
AMW-15S 3/7/2014 881.42 - - 7.13 874.29
AMW-15S 3/14/2014 881.42 - - 7.23 874.19
AMW-15S 3/21/2014 881.42 - - 7.13 874.29
AMW-15S 3/28/2014 881.42 - - 7.13 874.29
AMW-15S 4/4/2014 881.42 - - 7.09 874.33
AMW-15S 4/11/2014 881.42 - - 6.89 874.53
AMW-15S 4/18/2014 881.42 - - 6.71 874.71
AMW-15S 4/25/2014 881.42 - - 6.98 874.44
AMW-15S 5/2/2014 881.42 - - 7.25 874.17
AMW-15S 5/9/2014 881.42 - - 7.59 873.83
AMW-15S 5/16/2014 881.42 - - 7.39 874.03
AMW-15S 5/23/2014 881.42 - - 7.83 873.59
AMW-15S 5/30/2014 881.42 - - 8.37 873.05
AMW-15S 6/6/2014 881.42 - - 8.53 872.89
AMW-15S 6/13/2014 881.42 - - 8.89 872.53
AMW-15S 6/20/2014 881.42 - - 9.16 872.26
AMW-15S 6/27/2014 881.42 - - 9.48 871.94
AMW-15S 7/5/2014 881.42 - - 9.83 871.59
AMW-15S 7/11/2014 881.42 - - 10.38 871.04
AMW-15S 3/5/2015 881.42 - -9.45 871.97
AMW-15S 5/27/2015 881.42 - -10.10 871.32
AMW-15S 6/29/2015 881.42 - -12.08 869.34
AMW-15S 7/30/2015 881.42 - -13.39 868.03
AMW-15S 8/20/2015 881.42 - -18.78 862.64
AMW-15S 9/9/2015 881.42 - -13.80 867.62
AMW-15S 10/15/2015 881.42 - -11.81 869.61
AMW-15S 10/26/2015 881.42 - -11.95 869.47
Page 14 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-15S 12/4/2015 881.42 - -9.05 872.37
AMW-15S 1/12/2016 881.42 - - 7.67 873.75
AMW-15S 5/26/2016 881.42 - - 6.93 874.49
AMW-15S 7/11/2016 881.42 - - 8.72 872.70
AMW-15S 7/12/2016 881.42 - - 8.72 872.70
AMW-15S 8/3/2016 881.42 - - 10.11 871.31
AMW-15S 9/28/2016 881.42 - - 11.90 869.52
AMW-15S 11/29/2016 881.42 - - 12.42 869.00
AMW-15S 12/14/2016 881.42 - - 12.34 869.08
AMW-15S 5/17/2017 881.42 - - 10.62 870.80
AMW-15S 6/26/2017 881.42 - - 8.82 872.60
AMW-15S 8/8/2017 881.42 - - 11.41 870.01
AMW-15S 11/28/2017 881.42 - - 13.42 868.00
AMW-15S 12/11/2017 881.42 - - 13.48 867.94
AMW-15S 1/25/2018 881.42 - - 12.69 868.73
AMW-15S 5/21/2018 881.42 - - 10.30 871.12
AMW-15S 7/9/2018 881.42 - - 11.97 869.45
AMW-15S 8/16/2018 881.42 - - 10.75 870.67
AMW-15S 11/29/2018 881.42 - - 8.55 872.87
AMW-15S 12/12/2018 881.42 - - 8.10 873.32
AMW-15S 3/27/2019 881.42 - - 6.06 875.36
AMW-15S 5/29/2019 881.42 - - 8.57 872.85
AMW-15S 6/10/2019 881.42 - - 7.93 873.49
AMW-15S 8/6/2019 881.42 - - 5.76 875.66
AMW-15S 11/8/2019 881.42 - - 10.19 871.23
AMW-15S 12/9/2019 881.42 - - 9.14 872.28
AMW-15S 3/6/2020 881.42 - - 5.92 875.50
AMW-15S 6/11/2020 881.42 - - 6.47 874.95
AMW-15S 8/24/2020 881.42 - - 9.09 872.33
AMW-15S 11/30/2020 881.42 - - 7.27 874.15
AMW-15S 12/14/2020 881.42 - - 7.88 873.54
AMW-15S 3/29/2021 881.42 - - 5.30 876.12
AMW-15S 6/14/2021 881.42 - - 7.95 873.47
AMW-15S 9/28/2021 881.42 - - 10.79 870.63
AMW-15S 12/28/2021 881.42 - - 11.81 869.61
AMW-15S 4/1/2022 881.42 - - 8.36 873.06
AMW-15S 6/20/2022 881.42 - - 10.40 871.02
Page 15 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-15S 12/5/2022 881.42 - - 10.96 870.46
AMW-15S 4/10/2023 881.42 - - 7.23 874.19
AMW-15S 7/17/2023 881.42 - - 9.83 871.59
AMW-15S 9/18/2023 881.42 - - 11.65 869.77
AMW-15S 12/6/2023 881.42 - - 13.02 868.40
AMW-15S 3/1/2024 881.42 - - 9.56 871.86
AMW-16S 8/5/2003 880.34 - - 4.93 875.41
AMW-16S 8/20/2003 880.34 - - 4.16 876.18
AMW-16S 11/10/2003 880.34 - - 6.00 874.34
AMW-16S 12/23/2003 880.34 - - 5.41 874.93
AMW-16S 1/29/2004 880.34 - - 6.31 874.03
AMW-16S 3/30/2004 880.34 - - 5.91 874.43
AMW-16S 4/23/2004 880.34 - - 6.27 874.07
AMW-16S 5/20/2004 880.34 - - 7.25 873.09
AMW-16S 6/28/2004 880.34 - - 8.60 871.74
AMW-16S 8/30/2004 880.34 - - 9.17 871.17
AMW-16S 1/26/2005 880.34 - - 6.92 873.42
AMW-16S 2/18/2005 880.34 - - 6.38 873.96
AMW-16S 3/29/2005 880.34 - - 5.72 874.62
AMW-16S 6/2/2006 880.34 - - 9.64 870.70
AMW-16S 6/16/2006 880.34 - - 8.67 871.67
AMW-16S 1/11/2008 880.34 - - 10.94 869.40
AMW-16S 11/5/2010 880.34 - - 9.45 870.89
AMW-16S 1/10/2014 880.34 - - 6.89 873.45
AMW-16S 1/17/2014 880.34 - - 6.69 873.65
AMW-16S 1/24/2014 880.34 - - 6.78 873.56
AMW-16S 1/31/2014 880.34 - - 6.99 873.35
AMW-16S 2/7/2014 880.34 - - 6.81 873.53
AMW-16S 2/14/2014 880.34 - - 6.48 873.86
AMW-16S 2/21/2014 880.34 - - 6.15 874.19
AMW-16S 2/28/2014 880.34 - - 6.42 873.92
AMW-16S 3/7/2014 880.34 - - 5.82 874.52
AMW-16S 3/14/2014 880.34 - - 5.97 874.37
AMW-16S 3/21/2014 880.34 - - 5.82 874.52
AMW-16S 3/28/2014 880.34 - - 5.76 874.58
AMW-16S 4/4/2014 880.34 - - 5.83 874.51
Page 16 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-16S 4/11/2014 880.34 - - 5.61 874.73
AMW-16S 4/18/2014 880.34 - - 5.47 874.87
AMW-16S 4/25/2014 880.34 - - 5.73 874.61
AMW-16S 5/2/2014 880.34 - - 6.03 874.31
AMW-16S 5/9/2014 880.34 - - 6.28 874.06
AMW-16S 5/16/2014 880.34 - - 6.09 874.25
AMW-16S 5/23/2014 880.34 - - 6.54 873.80
AMW-16S 5/30/2014 880.34 - - 6.89 873.45
AMW-16S 6/6/2014 880.34 - - 7.22 873.12
AMW-16S 6/13/2014 880.34 - - 7.53 872.81
AMW-16S 6/20/2014 880.34 - - 7.91 872.43
AMW-16S 6/27/2014 880.34 - - 8.14 872.20
AMW-16S 7/5/2014 880.34 - - 8.63 871.71
AMW-16S 7/11/2014 880.34 - - 9.02 871.32
AMW-16S 3/5/2015 880.34 - -8.11 872.23
AMW-16S 5/27/2015 880.34 - -8.85 871.49
AMW-16S 6/29/2015 880.34 - -10.74 869.60
AMW-16S 7/30/2015 880.34 - -11.99 868.35
AMW-16S 8/20/2015 880.34 - -11.89 868.45
AMW-16S 9/9/2015 880.34 - -12.80 867.54
AMW-16S 10/15/2015 880.34 - -10.35 869.99
AMW-16S 10/26/2015 880.34 - -10.68 869.66
AMW-16S 12/4/2015 880.34 - -7.75 872.59
AMW-16S 1/12/2016 880.34 - - 6.38 873.96
AMW-16S 5/26/2016 880.34 - - 5.62 874.72
AMW-16S 7/11/2016 880.34 - - 7.31 873.03
AMW-16S 7/12/2016 880.34 - - 7.31 873.03
AMW-16S 7/27/2016 880.34 - - 8.38 871.96
AMW-16S 9/28/2016 880.34 - - 10.55 869.79
AMW-16S 11/29/2016 880.34 - - 11.16 869.18
AMW-16S 12/15/2016 880.34 - - 11.11 869.23
AMW-16S 5/17/2017 880.34 - - 9.35 870.99
AMW-16S 6/26/2017 880.34 - - 7.48 872.86
AMW-16S 8/8/2017 880.34 - - 10.07 870.27
AMW-16S 11/28/2017 880.34 - - 12.16 868.18
AMW-16S 12/11/2017 880.34 - - 12.23 868.11
AMW-16S 1/25/2018 880.34 - - 11.41 868.93
Page 17 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-16S 5/21/2018 880.34 - - 9.03 871.31
AMW-16S 7/9/2018 880.34 - - 10.65 869.69
AMW-16S 8/16/2018 880.34 - - 9.44 870.90
AMW-16S 11/29/2018 880.34 - - 7.27 873.07
AMW-16S 12/12/2018 880.34 - - 6.84 873.50
AMW-16S 3/27/2019 880.34 - - 4.78 875.56
AMW-16S 5/29/2019 880.34 - - 8.65 871.69
AMW-16S 6/10/2019 880.34 - - 6.57 873.77
AMW-16S 8/6/2019 880.34 - - 7.42 872.92
AMW-16S 11/8/2019 880.34 - - 8.91 871.43
AMW-16S 12/9/2019 880.34 - - 7.88 872.46
AMW-16S 3/6/2020 880.34 - - 4.66 875.68
AMW-16S 6/11/2020 880.34 - - 5.65 874.69
AMW-16S 8/24/2020 880.34 - - 7.78 872.56
AMW-16S 11/30/2020 880.34 - - 5.98 874.36
AMW-16S 12/14/2020 880.34 - - 5.96 874.38
AMW-16S 3/29/2021 880.34 - - 4.04 876.30
AMW-16S 6/14/2021 880.34 - - 7.58 872.76
AMW-16S 9/28/2021 880.34 - - 9.51 870.83
AMW-16S 12/28/2021 880.34 - - 10.55 869.79
AMW-16S 4/1/2022 880.34 - - 7.09 873.25
AMW-16S 6/20/2022 880.34 - - 8.92 871.42
AMW-16S 9/22/2022 880.34 - - 10.93 869.41
AMW-16S 12/5/2022 880.34 - - 9.69 870.65
AMW-16S 4/10/2023 880.34 - - 5.97 874.37
AMW-16S 7/17/2023 880.34 - - 9.18 871.16
AMW-16S 9/18/2023 880.34 - - 10.30 870.04
AMW-16S 12/6/2023 880.34 - - 11.76 868.58
AMW-16S 3/1/2024 880.34 - - 8.29 872.05
AMW-17S 8/5/2003 879.81 - - 4.20 875.61
AMW-17S 8/20/2003 879.81 - - 3.40 876.41
AMW-17S 11/10/2003 879.81 - - 5.30 874.51
AMW-17S 12/23/2003 879.81 - - 4.73 875.08
AMW-17S 1/29/2004 879.81 - - 5.70 874.11
AMW-17S 3/30/2004 879.81 - - 5.26 874.55
AMW-17S 4/23/2004 879.81 - - 5.60 874.21
Page 18 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-17S 5/20/2004 879.81 - - 6.60 873.21
AMW-17S 6/28/2004 879.81 - - 7.92 871.89
AMW-17S 8/30/2004 879.81 - - 8.50 871.31
AMW-17S 1/26/2005 879.81 - - 6.28 873.53
AMW-17S 2/18/2005 879.81 - - 5.71 874.10
AMW-17S 3/29/2005 879.81 - - 4.99 874.82
AMW-17S 6/2/2006 879.81 - - 8.98 870.83
AMW-17S 6/16/2006 879.81 - - 8.08 871.73
AMW-17S 1/11/2008 879.81 - - 10.29 869.52
AMW-17S 11/5/2010 879.81 - - 8.81 871.00
AMW-17S 1/10/2014 879.81 - - 6.41 873.40
AMW-17S 1/17/2014 879.81 - - 6.07 873.74
AMW-17S 1/24/2014 879.81 - - 6.18 873.63
AMW-17S 1/31/2014 879.81 - - 6.35 873.46
AMW-17S 2/7/2014 879.81 - - 6.18 873.63
AMW-17S 2/14/2014 879.81 - - 5.89 873.92
AMW-17S 2/21/2014 879.81 - - 5.59 874.22
AMW-17S 2/28/2014 879.81 - - 5.78 874.03
AMW-17S 3/7/2014 879.81 - - 5.23 874.58
AMW-17S 3/14/2014 879.81 - - 5.34 874.47
AMW-17S 3/21/2014 879.81 - - 5.34 874.47
AMW-17S 3/28/2014 879.81 - - 5.10 874.71
AMW-17S 4/4/2014 879.81 - - 5.17 874.64
AMW-17S 4/11/2014 879.81 - - 4.91 874.90
AMW-17S 4/18/2014 879.81 - - 4.76 875.05
AMW-17S 4/25/2014 879.81 - - 5.21 874.60
AMW-17S 5/2/2014 879.81 - - 5.47 874.34
AMW-17S 5/9/2014 879.81 - - 5.73 874.08
AMW-17S 5/16/2014 879.81 - - 5.43 874.38
AMW-17S 5/23/2014 879.81 - - 5.86 873.95
AMW-17S 5/30/2014 879.81 - - 6.26 873.55
AMW-17S 6/6/2014 879.81 - - 6.52 873.29
AMW-17S 6/13/2014 879.81 - - 6.87 872.94
AMW-17S 6/20/2014 879.81 - - 7.14 872.67
AMW-17S 6/27/2014 879.81 - - 7.42 872.39
AMW-17S 7/5/2014 879.81 - - 7.92 871.89
AMW-17S 7/11/2014 879.81 - - 8.28 871.53
Page 19 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-17S 3/5/2015 879.81 - -7.68 872.13
AMW-17S 5/27/2015 879.81 - -8.20 871.61
AMW-17S 6/29/2015 879.81 - -10.04 869.77
AMW-17S 7/30/2015 879.81 - -11.29 868.52
AMW-17S 8/20/2015 879.81 - -11.19 868.62
AMW-17S 9/9/2015 879.81 - -11.80 868.01
AMW-17S 10/15/2015 879.81 - -9.74 870.07
AMW-17S 10/26/2015 879.81 - -10.05 869.76
AMW-17S 12/4/2015 879.81 - -7.16 872.65
AMW-17S 1/12/2016 879.81 - - 5.75 874.06
AMW-17S 5/26/2016 879.81 - - 4.91 874.90
AMW-17S 7/11/2016 879.81 - - 6.67 873.14
AMW-17S 7/12/2016 879.81 - - 6.67 873.14
AMW-17S 7/27/2016 879.81 - - 7.67 872.14
AMW-17S 9/28/2016 879.81 - - 9.89 869.92
AMW-17S 11/29/2016 879.81 - - 10.49 869.32
AMW-17S 12/14/2016 879.81 - - 10.43 869.38
AMW-17S 5/17/2017 879.81 - - 8.74 871.07
AMW-17S 6/26/2017 879.81 - - 6.85 872.96
AMW-17S 8/8/2017 879.81 - - 9.32 870.49
AMW-17S 11/28/2017 879.81 - - 11.51 868.30
AMW-17S 12/11/2017 879.81 - - 11.59 868.22
AMW-17S 1/25/2018 879.81 - - 10.89 868.92
AMW-17S 5/21/2018 879.81 - - 8.39 871.42
AMW-17S 7/9/2018 879.81 - - 9.96 869.85
AMW-17S 8/16/2018 879.81 - - 8.80 871.01
AMW-17S 11/29/2018 879.81 - - 6.61 873.20
AMW-17S 12/12/2018 879.81 - - 6.21 873.60
AMW-17S 3/27/2019 879.81 - - 4.07 875.74
AMW-17S 5/29/2019 879.81 - - 6.13 873.68
AMW-17S 6/10/2019 879.81 - - 5.91 873.90
AMW-17S 8/6/2019 879.81 - - 6.71 873.10
AMW-17S 11/8/2019 879.81 - - 8.27 871.54
AMW-17S 12/9/2019 879.81 - - 7.24 872.57
AMW-17S 3/6/2020 879.81 - - 3.98 875.83
AMW-17S 6/11/2020 879.81 - - 4.92 874.89
AMW-17S 8/24/2020 879.81 - - 7.14 872.67
Page 20 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-17S 11/30/2020 879.81 - - 5.34 874.47
AMW-17S 12/14/2020 879.81 - - 6.80 873.01
AMW-17S 3/29/2021 879.81 - - 3.32 876.49
AMW-17S 6/14/2021 879.81 - - 5.97 873.84
AMW-17S 9/28/2021 879.81 - - 8.94 870.87
AMW-17S 12/28/2021 879.81 - - 9.94 869.87
AMW-17S 4/1/2022 879.81 - - 6.51 873.30
AMW-17S 6/20/2022 879.81 - - 6.94 872.87
AMW-17S 9/22/2022 879.81 - - 10.28 869.53
AMW-17S 12/5/2022 879.81 - - 9.13 870.68
AMW-17S 4/10/2023 879.81 - - 5.37 874.44
AMW-17S 7/17/2023 879.81 - - 7.12 872.69
AMW-17S 9/18/2023 879.81 - - 9.69 870.12
AMW-17S 12/6/2023 879.81 - - 11.14 868.67
AMW-17S 3/1/2024 879.81 - - 7.70 872.11
AMW-18S 8/5/2003 879.96 - - 4.26 875.70
AMW-18S 8/20/2003 879.96 3.49 0.01 3.50 876.47
AMW-18S 11/10/2003 879.96 - - 5.40 874.56
AMW-18S 12/23/2003 879.96 - - 4.90 875.06
AMW-18S 1/29/2004 879.96 - - 5.75 874.21
AMW-18S 3/30/2004 879.96 - - 5.40 874.56
AMW-18S 4/23/2004 879.96 - - 5.72 874.24
AMW-18S 5/20/2004 879.96 - - 6.70 873.26
AMW-18S 6/28/2004 879.96 - - 8.00 871.96
AMW-18S 8/30/2004 879.96 - - 8.60 871.36
AMW-18S 1/26/2005 879.96 - - 6.43 873.53
AMW-18S 2/18/2005 879.96 - - 5.85 874.11
AMW-18S 3/29/2005 879.96 - - 5.15 874.81
AMW-18S 6/2/2006 879.96 - - 9.12 870.84
AMW-18S 6/16/2006 879.96 - - 7.98 871.98
AMW-18S 1/11/2008 879.96 - - 10.40 869.56
AMW-18S 11/5/2010 879.96 - - 8.89 871.07
AMW-18S 1/10/2014 879.96 - - 6.28 873.68
AMW-18S 1/17/2014 879.96 - - 5.99 873.97
AMW-18S 1/24/2014 879.96 - - 6.15 873.81
AMW-18S 1/31/2014 879.96 - - 6.47 873.49
Page 21 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-18S 2/7/2014 879.96 - - 6.14 873.82
AMW-18S 2/14/2014 879.96 - - 5.80 874.16
AMW-18S 2/21/2014 879.96 - - 5.41 874.55
AMW-18S 2/28/2014 879.96 - - 5.89 874.07
AMW-18S 3/7/2014 879.96 - - 4.56 875.40
AMW-18S 3/14/2014 879.96 - - 4.67 875.29
AMW-18S 3/21/2014 879.96 - - 4.56 875.40
AMW-18S 3/28/2014 879.96 - - 4.99 874.97
AMW-18S 4/4/2014 879.96 - - 5.31 874.65
AMW-18S 4/11/2014 879.96 - - 4.89 875.07
AMW-18S 4/18/2014 879.96 - - 4.71 875.25
AMW-18S 4/25/2014 879.96 - - 5.18 874.78
AMW-18S 5/2/2014 879.96 - - 5.43 874.53
AMW-18S 5/9/2014 879.96 - - 5.67 874.29
AMW-18S 5/16/2014 879.96 - - 5.48 874.48
AMW-18S 5/23/2014 879.96 - - 5.96 874.00
AMW-18S 5/30/2014 879.96 - - 6.31 873.65
AMW-18S 6/6/2014 879.96 - - 6.61 873.35
AMW-18S 6/13/2014 879.96 - - 6.84 873.12
AMW-18S 6/20/2014 879.96 - - 7.21 872.75
AMW-18S 6/27/2014 879.96 - - 7.51 872.45
AMW-18S 7/5/2014 879.96 - - 7.96 872.00
AMW-18S 7/11/2014 879.96 - - 8.35 871.61
AMW-18S 3/5/2015 879.96 - -7.48 872.48
AMW-18S 5/27/2015 879.96 - -8.30 871.66
AMW-18S 6/29/2015 879.96 - -10.10 869.86
AMW-18S 7/30/2015 879.96 - -11.37 868.59
AMW-18S 8/20/2015 879.96 - -11.28 868.68
AMW-18S 9/9/2015 879.96 - -11.90 868.06
AMW-18S 10/15/2015 879.96 - -9.83 870.13
AMW-18S 10/26/2015 879.96 - -10.21 869.75
AMW-18S 12/4/2015 879.96 - -7.10 872.86
AMW-18S 1/12/2016 879.96 - - 5.81 874.15
AMW-18S 5/26/2016 879.96 - - 5.02 874.94
AMW-18S 7/11/2016 879.96 - - 6.75 873.21
AMW-18S 7/12/2016 879.96 - - 6.75 873.21
AMW-18S 7/27/2016 879.96 - - 7.76 872.20
Page 22 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
AMW-18S 9/28/2016 879.96 - - 9.95 870.01
AMW-18S 11/29/2016 879.96 - - 10.60 869.36
AMW-18S 12/16/2016 879.96 - - 10.90 869.06
AMW-18S 5/17/2017 879.96 - - 8.83 871.13
AMW-18S 6/26/2017 879.96 - - 6.83 873.13
AMW-18S 8/8/2017 879.96 - - 9.37 870.59
AMW-18S 11/28/2017 879.96 - - 11.65 868.31
AMW-18S 12/11/2017 879.96 - - 11.75 868.21
AMW-18S 1/25/2018 879.96 - - 10.81 869.15
AMW-18S 5/21/2018 879.96 - - 8.51 871.45
AMW-18S 7/9/2018 879.96 - - 10.05 869.91
AMW-18S 8/16/2018 879.96 - - 8.86 871.10
AMW-18S 11/29/2018 879.96 - - 6.68 873.28
AMW-18S 12/12/2018 879.96 - - 6.21 873.75
AMW-18S 3/27/2019 879.96 - - 4.24 875.72
AMW-18S 5/29/2019 879.96 - - 6.32 873.64
AMW-18S 6/10/2019 879.96 - - 5.86 874.10
AMW-18S 8/6/2019 879.96 - - 6.87 873.09
AMW-18S 11/8/2019 879.96 - - 8.32 871.64
AMW-18S 12/9/2019 879.96 - - 7.31 872.65
AMW-18S 3/6/2020 879.96 - - 4.14 875.82
AMW-18S 6/11/2020 879.96 - - 4.92 875.04
AMW-18S 8/24/2020 879.96 - - 7.34 872.62
AMW-18S 11/30/2020 879.96 - - 6.05 873.91
AMW-18S 12/14/2020 879.96 - - 6.77 873.19
AMW-18S 3/29/2021 879.96 - - 3.53 876.43
AMW-18S 6/14/2021 879.96 - - 5.19 874.77
AMW-18S 9/28/2021 879.96 - - 8.91 871.05
AMW-18S 12/28/2021 879.96 - - 10.06 869.90
AMW-18S 6/20/2022 879.96 - - 8.99 870.97
AMW-18S 9/22/2022 879.96 - - 10.38 869.58
AMW-18S 12/5/2022 879.96 - - 9.07 870.89
AMW-18S 4/10/2023 879.96 - - 5.41 874.55
AMW-18S 7/17/2023 879.96 - - 8.64 871.32
AMW-18S 9/18/2023 879.96 - - 9.64 870.32
AMW-18S 12/6/2023 879.96 - - 11.27 868.69
AMW-18S 3/1/2024 879.96 - - 7.82 872.14
Page 23 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
DEM-MW6D 11/10/2003 891.12 - - 11.25 879.87
DEM-MW6D 1/29/2004 891.12 - - 12.30 878.82
DEM-MW6D 3/30/2004 891.12 - - 11.22 879.90
DEM-MW6D 4/23/2004 891.12 - - 11.68 879.44
DEM-MW6D 5/20/2004 891.12 - - 12.73 878.39
DEM-MW6D 6/28/2004 891.12 - - 13.35 877.77
DEM-MW6D 8/30/2004 891.12 - - 15.18 875.94
DEM-MW6D 1/26/2005 891.12 - - 12.86 878.26
DEM-MW6D 2/18/2005 891.12 - - 12.26 878.86
DEM-MW6D 3/29/2005 891.12 - - 11.74 879.38
DEM-MW6D 10/26/2015 891.12 - -17.59 873.53
DEM-MW6D 7/11/2016 891.12 - - 15.60 875.52
DEM-MW6D 7/12/2016 891.12 - - 15.60 875.52
DEM-MW6D 7/20/2016 891.12 - - 13.95 877.17
DEM-MW6D 11/29/2016 891.12 - - 17.83 873.29
DEM-MW6D 12/16/2016 891.12 - - 18.57 872.55
DEM-MW6D 6/26/2017 891.12 - - 14.60 876.52
DEM-MW6D 12/11/2017 891.12 - - 19.36 871.76
DEM-MW6D 7/9/2018 891.12 - - 16.83 874.29
DEM-MW6D 12/12/2018 891.12 - - 13.51 877.61
DEM-MW6D 6/10/2019 891.12 - - 12.35 878.77
DEM-MW6D 12/9/2019 891.12 - - 14.48 876.64
DEM-MW6D 6/11/2020 891.12 - - 10.66 880.46
DEM-MW6D 12/14/2020 891.12 - - 11.31 879.81
DEM-MW6D 6/14/2021 891.12 - - 12.33 878.79
DEM-MW6D 6/20/2022 891.12 - - 15.65 875.47
DEM-MW6D 7/17/2023 891.12 - - 14.68 876.44
DEM-MW6I 11/10/2003 891.02 - - 10.97 880.05
DEM-MW6I 1/29/2004 891.02 - - 12.10 878.92
DEM-MW6I 3/30/2004 891.02 - - 11.00 880.02
DEM-MW6I 4/23/2004 891.02 - - 11.43 879.59
DEM-MW6I 5/20/2004 891.02 - - 12.50 878.52
DEM-MW6I 6/28/2004 891.02 - - 14.13 876.89
DEM-MW6I 8/30/2004 891.02 - - 14.95 876.07
DEM-MW6I 1/26/2005 891.02 - - 12.67 878.35
Page 24 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
DEM-MW6I 2/18/2005 891.02 - - 12.17 878.85
DEM-MW6I 3/29/2005 891.02 - - 11.57 879.45
DEM-MW6I 10/26/2015 891.02 - - 17.40 873.62
DEM-MW6I 7/11/2016 891.02 - - 13.35 877.67
DEM-MW6I 7/12/2016 891.02 - - 13.35 877.67
DEM-MW6I 7/20/2016 891.02 - - 13.69 877.33
DEM-MW6I 11/29/2016 891.02 - - 17.62 873.40
DEM-MW6I 12/16/2016 891.02 - - 17.89 873.13
DEM-MW6I 6/26/2017 891.02 - - 14.43 876.59
DEM-MW6I 12/11/2017 891.02 - - 19.16 871.86
DEM-MW6I 7/9/2018 891.02 - - 16.57 874.45
DEM-MW6I 12/12/2018 891.02 - - 13.33 877.69
DEM-MW6I 6/10/2019 891.02 - - 12.10 878.92
DEM-MW6I 12/9/2019 891.02 - - 14.28 876.74
DEM-MW6I 6/11/2020 891.02 - - 10.40 880.62
DEM-MW6I 12/14/2020 891.02 - - 11.22 879.80
DEM-MW6I 6/14/2021 891.02 - - 12.10 878.92
DEM-MW6I 6/20/2022 891.02 - - 15.36 875.66
DEM-MW6I 7/17/2023 891.02 - - 14.41 876.61
DEM-MW6R 8/5/2003 892.77 - - 11.91 880.86
DEM-MW6R 8/20/2003 893.77 10.49 0.01 10.50 882.28
DEM-MW6R 11/10/2003 894.77 - - 12.75 880.02
DEM-MW6R 12/23/2003 895.77 - -12.46 880.31
DEM-MW6R 1/29/2004 896.77 - -13.90 878.87
DEM-MW6R 3/30/2004 896.77 - - 12.78 879.99
DEM-MW6R 4/23/2004 896.77 - - 13.23 879.54
DEM-MW6R 5/20/2004 896.77 - - 14.27 878.50
DEM-MW6R 6/28/2004 896.77 - - 15.90 876.87
DEM-MW6R 8/30/2004 896.77 - - 16.75 876.02
DEM-MW6R 1/26/2005 896.77 - - 14.45 878.32
DEM-MW6R 2/18/2005 896.77 - - 13.98 878.79
DEM-MW6R 3/29/2005 896.77 - - 13.37 879.40
DEM-MW6R 6/2/2006 896.77 - - 17.83 874.94
DEM-MW6R 6/16/2006 896.77 - - 17.52 875.25
DEM-MW6R 1/11/2008 896.77 - - 19.82 872.95
DEM-MW6R 11/5/2010 896.77 - - 18.12 874.65
Page 25 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
DEM-MW6R 1/10/2014 896.77 - - 15.78 876.99
DEM-MW6R 1/17/2014 896.77 - - 15.58 877.19
DEM-MW6R 1/24/2014 896.77 - - 15.27 877.50
DEM-MW6R 1/31/2014 896.77 - - 15.08 877.69
DEM-MW6R 2/7/2014 896.77 - - 14.99 877.78
DEM-MW6R 2/14/2014 896.77 - - 14.89 877.88
DEM-MW6R 2/21/2014 896.77 - - 14.77 878.00
DEM-MW6R 2/28/2014 896.77 - - 14.55 878.22
DEM-MW6R 3/7/2014 896.77 - - 14.34 878.43
DEM-MW6R 3/14/2014 896.77 - - 14.48 878.29
DEM-MW6R 3/21/2014 896.77 - - 14.34 878.43
DEM-MW6R 3/28/2014 896.77 - - 13.98 878.79
DEM-MW6R 4/4/2014 896.77 - - 13.72 879.05
DEM-MW6R 4/11/2014 896.77 - - 13.59 879.18
DEM-MW6R 4/18/2014 896.77 - - 13.38 879.39
DEM-MW6R 4/25/2014 896.77 - - 13.51 879.26
DEM-MW6R 5/2/2014 896.77 - - 13.75 879.02
DEM-MW6R 5/9/2014 896.77 - - 14.03 878.74
DEM-MW6R 5/16/2014 896.77 - - 13.81 878.96
DEM-MW6R 5/23/2014 896.77 - - 13.96 878.81
DEM-MW6R 5/30/2014 896.77 - - 14.19 878.58
DEM-MW6R 6/6/2014 896.77 - - 14.87 877.90
DEM-MW6R 6/13/2014 896.77 - - 14.96 877.81
DEM-MW6R 6/20/2014 896.77 - - 15.19 877.58
DEM-MW6R 6/27/2014 896.77 - - 15.46 877.31
DEM-MW6R 7/5/2014 896.77 - - 15.91 876.86
DEM-MW6R 7/11/2014 896.77 - - 16.22 876.55
DEM-MW6R 3/5/2015 896.77 - -17.49 875.28
DEM-MW6R 5/27/2015 896.77 - -16.65 876.12
DEM-MW6R 6/29/2015 896.77 - -17.42 875.35
DEM-MW6R 7/30/2015 896.77 - -19.77 873.00
DEM-MW6R 8/20/2015 896.77 - -20.20 872.57
DEM-MW6R 9/9/2015 896.77 - -20.58 872.19
DEM-MW6R 10/15/2015 896.77 - -19.15 873.62
DEM-MW6R 10/26/2015 896.77 - -19.18 873.59
DEM-MW6R 12/4/2015 896.77 - -17.06 875.71
DEM-MW6R 1/12/2016 892.77 - - 15.17 877.60
Page 26 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
DEM-MW6R 5/26/2016 892.77 - - 13.66 879.11
DEM-MW6R 7/11/2016 892.77 - - 15.11 877.66
DEM-MW6R 7/12/2016 892.77 - - 15.11 877.66
DEM-MW6R 7/20/2016 892.77 - - 15.40 877.37
DEM-MW6R 9/28/2016 892.77 - - 18.45 874.32
DEM-MW6R 11/29/2016 892.77 - - 19.36 873.41
DEM-MW6R 12/16/2016 892.77 - - 19.62 873.15
DEM-MW6R 5/17/2017 892.77 - - 17.98 874.79
DEM-MW6R 6/26/2017 892.77 - - 16.26 876.51
DEM-MW6R 8/8/2017 892.77 - - 17.67 875.10
DEM-MW6R 11/28/2017 892.77 - - 20.77 872.00
DEM-MW6R 12/11/2017 892.77 - - 11.91 880.86
DEM-MW6R 1/25/2018 892.77 - - 20.82 871.95
DEM-MW6R 5/21/2018 892.77 - - 17.11 875.66
DEM-MW6R 7/9/2018 892.77 - - 18.33 874.44
DEM-MW6R 8/16/2018 892.77 - - 17.65 875.12
DEM-MW6R 11/29/2018 892.77 - - 15.45 877.32
DEM-MW6R 12/12/2018 892.77 - - 15.13 877.64
DEM-MW6R 3/27/2019 892.77 - - 11.78 880.99
DEM-MW6R 5/29/2019 892.77 - - 13.57 879.20
DEM-MW6R 6/10/2019 892.77 - - 13.88 878.89
DEM-MW6R 8/6/2019 892.77 - - 14.55 878.22
DEM-MW6R 11/8/2019 892.77 - - 17.09 875.68
DEM-MW6R 12/9/2019 892.77 - - 16.08 876.69
DEM-MW6R 3/6/2020 892.77 - - 11.53 881.24
DEM-MW6R 6/11/2020 892.77 - - 12.17 880.60
DEM-MW6R 8/24/2020 892.77 - - 16.17 876.60
DEM-MW6R 11/30/2020 892.77 - - 13.46 879.31
DEM-MW6R 12/14/2020 892.77 - - 13.04 879.73
DEM-MW6R 3/29/2021 892.77 - - 10.62 882.15
DEM-MW6R 6/14/2021 892.77 - - 13.80 878.97
DEM-MW6R 9/28/2021 892.77 - - 17.06 875.71
DEM-MW6R 12/28/2021 892.77 - - 18.70 874.07
DEM-MW6R 4/1/2022 892.77 - - 15.20 877.57
DEM-MW6R 6/20/2022 892.77 - - 17.11 875.66
DEM-MW6R 9/22/2022 892.77 - - 18.96 873.81
DEM-MW6R 12/5/2022 892.77 - - 18.52 874.25
Page 27 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
DEM-MW6R 4/10/2023 892.77 - - 13.95 878.82
DEM-MW6R 7/17/2023 892.77 - - 16.14 876.63
DEM-MW6R 9/18/2023 892.77 - - 18.47 874.30
DEM-MW6R 12/6/2023 892.77 - - 20.04 872.73
DEM-MW6R 3/1/2024 892.77 - - 16.49 876.28
FMW-15 6/26/1995 902.95 - - 22.26 880.69
FMW-15 8/20/2003 902.95 - - 15.50 887.26
FMW-15 11/13/2003 902.95 - - 9.97 892.79
FMW-15 12/23/2003 902.95 - - 18.16 884.79
FMW-15 1/29/2004 902.95 - - 19.03 883.92
FMW-15 3/30/2004 902.95 - - 17.92 885.03
FMW-15 4/23/2004 902.95 - - 18.08 884.87
FMW-15 5/20/2004 902.95 - - 19.70 883.25
FMW-15 6/28/2004 902.95 - - 21.66 881.29
FMW-15 8/30/2004 902.95 - - 22.61 880.34
FMW-15 1/26/2005 902.95 - - 19.65 883.30
FMW-15 2/18/2005 902.95 - - 18.78 884.17
FMW-15 3/29/2005 902.95 - - 18.30 884.65
FMW-15 11/5/2010 902.95 - - 24.68 878.08
FMW-15 10/26/2015 902.95 - -24.39 878.37
FMW-15 11/28/2016 902.76 - - 26.42 876.34
FMW-15 12/15/2016 902.76 - - 26.19 876.57
FMW-15 6/26/2017 902.76 - - Dry NA
FMW-15 12/11/2017 902.76 - - 26.60 876.16
FMW-15 1/25/2018 902.76 - - Dry NA
FMW-15 7/9/2018 902.76 - - Dry NA
FMW-15 12/12/2018 902.76 - - 22.18 880.58
FMW-15 6/10/2019 902.76 - - 19.52 883.24
FMW-15 12/9/2019 902.76 - - 24.49 878.27
FMW-15 6/11/2020 902.76 - - 17.86 884.90
FMW-15 12/14/2020 902.76 - - 18.86 883.90
FMW-15 6/14/2021 902.76 - - 19.36 883.40
FMW-15 6/20/2022 902.76 - - 23.63 879.13
FMW-15 7/17/2023 902.76 - - 22.70 880.06
FMW-19 6/26/1995 890.61 - - 17.83 872.78
Page 28 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-19 5/21/1997 890.61 - - 12.33 878.28
FMW-19 12/26/1998 890.61 - - 18.02 872.59
FMW-19 8/26/1999 890.61 - - 18.50 872.11
FMW-19 9/22/1999 890.61 - - 17.61 873.00
FMW-19 10/7/1999 890.61 - - 17.61 873.00
FMW-19 10/18/2002 890.61 - - 19.83 870.78
FMW-19 3/20/2003 890.61 - - 10.16 880.45
FMW-19 4/23/2003 890.61 - - 11.03 879.58
FMW-19 5/30/2003 890.61 - - 10.40 880.21
FMW-19 6/30/2003 890.61 - - 11.60 879.01
FMW-19 7/29/2003 890.61 - - 13.04 877.57
FMW-19 8/20/2003 890.61 - - 10.02 880.51
FMW-19 11/10/2003 890.61 - - 13.40 877.13
FMW-19 12/23/2003 890.61 - - 12.80 877.81
FMW-19 1/29/2004 890.61 - - 14.50 876.11
FMW-19 3/30/2004 890.61 - - 13.95 876.66
FMW-19 4/23/2004 890.61 - - 14.11 876.50
FMW-19 5/20/2004 890.61 - - 15.24 875.37
FMW-19 6/28/2004 890.61 - -16.50 874.11
FMW-19 8/30/2004 890.61 - -17.35 873.26
FMW-19 1/26/2005 890.61 - - 15.26 875.35
FMW-19 2/18/2005 890.61 - - 14.02 876.59
FMW-19 3/29/2005 890.61 - - 13.87 876.74
FMW-19 3/5/2015 890.61 - -17.81 872.80
FMW-19 5/27/2015 890.61 - -17.22 873.39
FMW-19 6/29/2015 890.61 - -18.69 871.92
FMW-19 7/30/2015 890.61 - -20.03 870.58
FMW-19 8/20/2015 890.61 - -20.41 870.20
FMW-19 9/9/2015 890.61 - -20.80 869.81
FMW-19 10/15/2015 890.61 - -19.11 871.50
FMW-19 10/26/2015 890.61 - - 19.38 871.23
FMW-19 12/4/2015 890.61 - - 16.21 874.40
FMW-19 1/12/2016 890.61 - - 14.20 876.41
FMW-19 5/26/2016 890.61 - - 12.72 877.89
FMW-19 7/11/2016 890.61 - - 14.92 875.69
FMW-19 7/12/2016 890.61 - - 14.92 875.69
FMW-19 8/2/2016 890.61 - - 16.14 874.47
Page 29 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-19 9/28/2016 890.61 - - 18.37 872.24
FMW-19 11/29/2016 890.61 - - 20.55 870.06
FMW-19 12/14/2016 890.61 - - 19.74 870.87
FMW-19 5/17/2017 890.61 - - 10.98 879.63
FMW-19 6/26/2017 890.61 - - 15.28 875.33
FMW-19 8/8/2017 890.61 - - 17.58 873.03
FMW-19 11/28/2017 890.61 - - 20.88 869.73
FMW-19 12/11/2017 890.61 - - 21.07 869.54
FMW-19 1/25/2018
FMW-19 7/9/2018
FMW-19
FMW-20 6/26/1995 889.46 - - 17.65 871.81
FMW-20 5/21/1997 889.46 - - 12.54 876.92
FMW-20 12/26/1998 889.46 - - 17.46 882.00
FMW-20 8/26/1999 889.46 - - 18.07 881.39
FMW-20 9/22/1999 889.46 - - 17.24 882.22
FMW-20 10/7/1999 889.46 - - 17.24 882.22
FMW-20 10/18/2002 889.46 - - 19.09 880.37
FMW-20 3/20/2003 889.46 - - 9.83 879.63
FMW-20 4/23/2003 889.46 - - 11.25 878.21
FMW-20 5/30/2003 889.46 - - 10.85 878.61
FMW-20 6/30/2003 889.46 - - 11.81 877.65
FMW-20 7/29/2003 889.46 - - 13.17 876.29
FMW-20 8/20/2003 889.46 - - 10.65 878.75
FMW-20 11/10/2003 889.46 - - 13.51 875.89
FMW-20 12/23/2003 889.46 - - 13.00 876.46
FMW-20 1/29/2004 889.46 - - 14.41 875.05
FMW-20 3/30/2004 889.46 - - 14.00 875.46
FMW-20 4/23/2004 889.46 - - 14.21 875.25
FMW-20 5/20/2004 889.46 - - 15.20 874.26
FMW-20 6/28/2004 889.46 - - 16.44 873.02
FMW-20 8/30/2004 889.46 - - 17.25 872.21
FMW-20 1/26/2005 889.46 - - 15.18 874.28
FMW-20 2/18/2005 889.46 - - 14.58 874.88
FMW-20 3/29/2005 889.46 - - 13.75 875.71
FMW-19 was damaged and unable to be measured
FMW-19 was damaged and unable to be measured
FMW-19 was abandoned in December 2018
Page 30 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-20 6/2/2006 889.46 - - 18.26 871.20
FMW-20 6/16/2006 889.46 - - 17.43 872.03
FMW-20 1/11/2008 889.46 - - 19.87 869.59
FMW-20 11/5/2010 889.46 - - 17.96 871.50
FMW-20 1/10/2014 889.46 - -15.12 874.34
FMW-20 1/17/2014 889.46 - -14.92 874.54
FMW-20 1/24/2014 889.46 - - 14.92 874.54
FMW-20 1/31/2014 889.46 - - 14.98 874.48
FMW-20 2/7/2014 889.46 - - 14.89 874.57
FMW-20 2/14/2014 889.46 - - 14.51 874.95
FMW-20 2/21/2014 889.46 - - 14.26 875.20
FMW-20 2/28/2014 889.46 - - 14.38 875.08
FMW-20 3/7/2014 889.46 - - 13.29 876.17
FMW-20 3/14/2014 889.46 - - 13.87 875.59
FMW-20 3/21/2014 889.46 - - 13.79 875.67
FMW-20 3/28/2014 889.46 - - 13.69 875.77
FMW-20 4/4/2014 889.46 - - 13.59 875.87
FMW-20 4/11/2014 889.46 - - 13.26 876.20
FMW-20 4/18/2014 889.46 - - 13.18 876.28
FMW-20 4/25/2014 889.46 - - 13.41 876.05
FMW-20 5/2/2014 889.46 - - 14.63 874.83
FMW-20 5/9/2014 889.46 - - 13.91 875.55
FMW-20 5/16/2014 889.46 - - 13.65 875.81
FMW-20 5/23/2014 889.46 - - 14.07 875.39
FMW-20 5/30/2014 889.46 - - 14.41 875.05
FMW-20 6/6/2014 889.46 - - 14.71 874.75
FMW-20 6/13/2014 889.46 - - 14.93 874.53
FMW-20 6/20/2014 889.46 - - 15.26 874.20
FMW-20 6/27/2014 889.46 - - 15.57 873.89
FMW-20 7/5/2014 889.46 - - 15.95 873.51
FMW-20 7/11/2014 889.46 - - 16.22 873.24
FMW-20 3/5/2015 889.46 - -17.30 872.16
FMW-20 5/27/2015 889.46 - -17.18 872.28
FMW-20 6/29/2015 889.46 - -18.47 870.99
FMW-20 7/30/2015 889.46 - -19.80 869.66
FMW-20 8/20/2015 889.46 - -20.11 869.35
FMW-20 9/9/2015 889.46 - -20.50 868.96
Page 31 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-20 10/15/2015 889.46 - -18.78 870.68
FMW-20 10/26/2015 889.46 - -19.09 870.37
FMW-20 12/4/2015 889.46 - -15.80 873.66
FMW-20 1/12/2016 889.46 - - 14.05 875.41
FMW-20 5/26/2016 889.46 - - 12.94 876.52
FMW-20 7/11/2016 889.46 - - 14.97 874.49
FMW-20 7/12/2016 889.46 - - 14.97 874.49
FMW-20 8/3/2016 889.46 - - 16.29 873.17
FMW-20 9/28/2016 889.46 - - 18.23 871.23
FMW-20 11/29/2016 889.46 - - 19.30 870.16
FMW-20 12/14/2016 889.46 - - 19.44 870.02
FMW-20 6/26/2017 889.46 - - 15.13 874.33
FMW-20 8/8/2017 889.46 - - 17.36 872.10
FMW-20 11/28/2017 889.46 - - 10.53 878.93
FMW-20 12/11/2017 889.46 - - 20.71 868.75
FMW-20 1/25/2018 889.46 - - 20.55 868.91
FMW-20 5/21/2018 889.46 - - 17.25 872.21
FMW-20 7/9/2018 889.46 - - 18.55 870.91
FMW-20 8/16/2018 889.46 - - 17.47 871.99
FMW-20 11/29/2018 889.46 - - 15.05 874.41
FMW-20 12/12/2018 889.46 - - 14.72 874.74
FMW-20 3/27/2019 889.46 - - 11.91 877.55
FMW-20 5/29/2019 889.46 - - 11.63 877.83
FMW-20 6/10/2019 889.46 - - 14.06 875.40
FMW-20 8/6/2019 889.46 - - 14.92 874.54
FMW-20 11/8/2019 889.46 - - 17.26 872.20
FMW-20 12/9/2019 889.46 - - 16.19 873.27
FMW-20 3/6/2020 889.46 - - 12.22 877.24
FMW-20 6/11/2020 889.46 - - 12.80 876.66
FMW-20 8/24/2020 889.46 - - 15.62 873.84
FMW-20 11/30/2020 889.46 - - 13.99 875.47
FMW-20 12/14/2020 889.46 - - 14.28 875.18
FMW-20 3/29/2021 889.46 - - 10.93 878.53
FMW-20 6/14/2021 889.46 - - 13.48 875.98
FMW-20 9/28/2021 889.46 - - 17.50 871.96
FMW-20 12/28/2021 889.46 - - 19.11 870.35
FMW-20 4/1/2022 889.46 - - 15.59 873.87
Page 32 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-20 6/20/2022 889.46 - - 13.99 875.47
FMW-20 9/22/2022 889.46 - - 19.22 870.24
FMW-20 12/5/2022 889.46 - - 18.48 870.98
FMW-20 4/10/2023 889.46 - - 13.98 875.48
FMW-20 7/17/2023 889.46 - - 12.06 877.40
FMW-20 9/18/2023 889.46 - - 18.53 870.93
FMW-20 12/6/2023 889.46 - - 20.22 869.24
FMW-20 3/1/2024 889.46 - - 16.61 872.85
FMW-21 6/26/1995 884.52 - - 13.17 871.35
FMW-21 4/16/1997 884.52 - - 8.74 875.78
FMW-21 5/21/1997 884.52 - - 9.17 875.35
FMW-21 7/10/1997 884.52 - - 11.55 872.97
FMW-21 7/25/1997 884.52 - - 12.47 872.05
FMW-21 9/14/1997 884.52 - - 13.67 870.85
FMW-21 10/3/1997 884.52 - -13.98 870.54
FMW-21 11/14/1997 884.52 - -13.85 870.67
FMW-21 3/6/1998 884.52 - - 8.97 875.55
FMW-21 4/28/1998 884.52 - - 8.59 875.93
FMW-21 12/26/1998 884.52 - - 12.67 871.85
FMW-21 8/26/1999 884.52 - - 13.65 870.87
FMW-21 9/22/1999 884.52 - - 12.39 872.13
FMW-21 10/7/1999 884.52 - - 12.39 872.13
FMW-21 10/12/2000 884.52 - - 10.95 873.57
FMW-21 10/15/2001 884.52 - - 15.13 869.39
FMW-21 10/18/2002 884.52 - - 14.05 870.47
FMW-21 3/20/2003 884.52 - - 8.22 876.30
FMW-21 4/23/2003 884.52 - - 7.85 876.67
FMW-21 5/30/2003 884.52 - - 7.65 876.87
FMW-21 6/30/2003 884.52 - - 7.57 876.95
FMW-21 7/29/2003 884.52 - - 9.68 874.84
FMW-21 8/20/2003 884.52 - - 7.77 876.72
FMW-21 11/10/2003 884.52 - - 9.58 874.91
FMW-21 12/23/2003 884.52 - - 8.99 875.53
FMW-21 1/29/2004 884.52 - - 10.00 874.52
FMW-21 3/30/2004 884.52 - - 9.32 875.20
FMW-21 4/23/2004 884.52 - - 9.73 874.79
Page 33 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-21 5/20/2004 884.52 - - 10.80 873.72
FMW-21 6/28/2004 884.52 - - 12.32 872.20
FMW-21 8/30/2004 884.52 - - 12.95 871.57
FMW-21 1/26/2005 884.52 - - 10.47 874.05
FMW-21 2/18/2005 884.52 - - 9.95 874.57
FMW-21 3/29/2005 884.52 - - 9.38 875.14
FMW-21 6/2/2006 884.52 - - 13.35 871.17
FMW-21 6/16/2006 884.52 - - 12.71 871.81
FMW-21 1/11/2008 884.52 - - 14.65 869.87
FMW-21 11/5/2010 884.52 - - 13.39 871.13
FMW-21 1/10/2014 884.52 - - 10.86 873.66
FMW-21 1/17/2014 884.52 - - 10.47 874.05
FMW-21 1/24/2014 884.52 - - 10.55 873.97
FMW-21 1/31/2014 884.52 - - 10.63 873.89
FMW-21 2/7/2014 884.52 - - 10.49 874.03
FMW-21 2/14/2014 884.52 - - 10.21 874.31
FMW-21 2/21/2014 884.52 - - 10.02 874.50
FMW-21 2/28/2014 884.52 - - 10.07 874.45
FMW-21 3/7/2014 884.52 - - 9.73 874.79
FMW-21 3/14/2014 884.52 - - 9.84 874.68
FMW-21 3/21/2014 884.52 - -9.73 874.79
FMW-21 3/28/2014 884.52 - -9.53 874.99
FMW-21 4/4/2014 884.52 - - 9.38 875.14
FMW-21 4/11/2014 884.52 - - 9.11 875.41
FMW-21 4/18/2014 884.52 - - 8.98 875.54
FMW-21 4/25/2014 884.52 - - 9.35 875.17
FMW-21 5/2/2014 884.52 - - 9.71 874.81
FMW-21 5/9/2014 884.52 - - 10.01 874.51
FMW-21 5/16/2014 884.52 - - 8.79 875.73
FMW-21 5/23/2014 884.52 - - 10.18 874.34
FMW-21 5/30/2014 884.52 - - 10.52 874.00
FMW-21 6/6/2014 884.52 - - 10.93 873.59
FMW-21 6/13/2014 884.52 - - 11.31 873.21
FMW-21 6/20/2014 884.52 - - 11.59 872.93
FMW-21 6/27/2014 884.52 - - 11.92 872.60
FMW-21 7/5/2014 884.52 - - 12.89 871.63
FMW-21 7/11/2014 884.52 - - 14.02 870.50
Page 34 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-21 3/5/2015 884.52 - -12.22 872.30
FMW-21 5/27/2015 884.52 - -12.50 872.02
FMW-21 6/29/2015 884.52 - -14.31 870.21
FMW-21 7/30/2015 884.52 - -15.85 868.67
FMW-21 8/20/2015 884.52 - -15.86 868.66
FMW-21 9/9/2015 884.52 - -16.31 868.21
FMW-21 10/15/2015 884.52 - -14.18 870.34
FMW-21 10/26/2015 884.52 - -14.45 870.07
FMW-21 12/4/2015 884.52 - -11.80 872.72
FMW-21 1/12/2016 884.52 - - 10.26 874.26
FMW-21 5/26/2016 884.52 - - 9.40 875.12
FMW-21 7/11/2016 884.52 - - 11.22 873.30
FMW-21 7/12/2016 884.52 - - 11.22 873.30
FMW-21 8/3/2016 884.52 - - 12.62 871.90
FMW-21 9/28/2016 884.52 - - 14.55 869.97
FMW-21 11/29/2016 884.52 - - 14.98 869.54
FMW-21 12/15/2016 884.52 - - 14.95 869.57
FMW-21 5/17/2017 884.52 - - 13.11 871.41
FMW-21 6/26/2017 884.52 - - 11.48 873.04
FMW-21 8/8/2017 884.52 - - 14.02 870.50
FMW-21 12/11/2017 884.52 - - 16.08 868.44
FMW-21 1/25/2018 884.52 - - 15.38 869.14
FMW-21 5/21/2018 884.52 - - 12.71 871.81
FMW-21 7/9/2018 884.52 - - 14.49 870.03
FMW-21 8/16/2018 884.52 - - 13.30 871.22
FMW-21 11/29/2018 884.52 - - 11.14 873.38
FMW-21 12/12/2018 884.52 - - 10.80 873.72
FMW-21 3/27/2019 884.52 - - 8.23 876.29
FMW-21 5/29/2019 884.52 - - 14.09 870.43
FMW-21 6/10/2019 884.52 - - 10.44 874.08
FMW-21 8/6/2019 884.52 - - 11.29 873.23
FMW-21 11/8/2019 884.52 - - 12.79 871.73
FMW-21 12/9/2019 884.52 - - 11.66 872.86
FMW-21 3/6/2020 884.52 - - 8.04 876.48
FMW-21 6/11/2020 884.52 - - 9.20 875.32
FMW-21 8/24/2020 884.52 - - 11.55 872.97
FMW-21 11/30/2020 884.52 - - 9.81 874.71
Page 35 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-21 12/14/2020 884.52 - - 9.39 875.13
FMW-21 3/29/2021 884.52 - - 7.44 877.08
FMW-21 6/14/2021 884.52 - - 10.34 874.18
FMW-21 9/28/2021 884.52 - - 13.24 871.28
FMW-21 12/28/2021 884.52 - - 14.32 870.20
FMW-21 4/1/2022 884.52 - - 10.77 873.75
FMW-21 6/20/2022 884.52 - - 13.35 871.17
FMW-21 9/22/2022 884.52 - - 14.73 869.79
FMW-21 12/5/2022 884.52 - - 13.76 870.76
FMW-21 4/10/2023 884.52 - - 4.71 879.81
FMW-21 7/17/2023 884.52 - - 12.58 871.94
FMW-21 9/18/2023 884.52 - - 14.30 870.22
FMW-21 12/6/2023 884.52 - - 15.56 868.96
FMW-21 3/1/2024 884.52 - - 12.05 872.47
FMW-22 6/26/1995 888.28 - - 13.21 875.07
FMW-22 10/18/2002 888.28 - - 14.45 873.83
FMW-22 3/20/2003 888.28 - - 6.61 881.67
FMW-22 4/23/2003 888.28 - - 6.65 881.63
FMW-22 5/30/2003 888.28 - - 6.51 881.77
FMW-22 6/30/2003 888.28 - - 8.14 880.14
FMW-22 7/29/2003 888.28 - - 9.75 878.53
FMW-22 8/20/2003 888.28 - - 6.87 881.43
FMW-22 11/10/2003 888.28 - - 9.63 878.67
FMW-22 12/23/2003 888.28 - - 8.36 879.92
FMW-22 1/29/2004 888.28 - - 9.78 878.50
FMW-22 3/30/2004 888.28 - - 8.60 879.68
FMW-22 4/23/2004 888.28 - - 8.87 879.41
FMW-22 5/20/2004 888.28 - - 10.60 877.68
FMW-22 6/28/2004 888.28 - - 12.73 875.55
FMW-22 8/30/2004 888.28 - - 13.42 874.86
FMW-22 1/26/2005 888.28 - -9.85 878.43
FMW-22 2/18/2005 888.28 - -9.03 879.25
FMW-22 3/29/2005 888.28 - - 8.13 880.15
FMW-22 11/5/2010 888.28 - - 13.92 874.38
FMW-22 10/26/2015 888.28 - -14.20 874.10
FMW-22 7/11/2016 888.28 - - 11.06 877.24
Page 36 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-22 7/12/2016 888.28 - - 11.06 877.24
FMW-22 8/3/2016 888.28 - - 12.77 875.51
FMW-22 11/29/2016 888.28 - - 15.54 872.76
FMW-22 12/13/2016 888.28 - - 15.17 873.13
FMW-22 6/26/2017 888.28 - - 10.26 878.02
FMW-22 12/11/2017 888.28 - - 17.18 871.10
FMW-22 1/25/2018 888.28 - - 15.70 872.58
FMW-22 7/9/2018 888.28 - - 14.34 873.94
FMW-22 12/12/2018 888.28 - - 9.64 878.64
FMW-22 6/10/2019 888.28 - - 10.45 877.83
FMW-22 12/9/2019 888.28 - - 11.50 876.78
FMW-22 6/11/2020 888.28 - - 8.24 880.04
FMW-22 12/14/2020 888.28 - - 11.01 877.27
FMW-22 6/14/2021 888.28 - - 10.26 878.02
FMW-22 6/20/2022 888.28 - - 13.09 875.19
FMW-22 7/17/2023 888.28 - - 12.06 876.22
FMW-23R 8/5/2003 887.45 - - 9.66 877.79
FMW-23R 8/20/2003 887.45 - - 8.59 878.86
FMW-23R 11/10/2003 887.45 - - 11.15 876.30
FMW-23R 12/23/2003 887.45 - - 10.67 876.78
FMW-23R 1/29/2004 887.45 - - 12.05 875.40
FMW-23R 3/30/2004 887.45 - - 11.37 876.08
FMW-23R 4/23/2004 887.45 - - 11.70 875.75
FMW-23R 5/20/2004 887.45 - - 12.72 874.73
FMW-23R 6/28/2004 887.45 - - 14.00 873.45
FMW-23R 8/30/2004 887.45 - - 14.80 872.65
FMW-23R 1/26/2005 887.45 - - 12.68 874.77
FMW-23R 2/18/2005 887.45 - - 12.17 875.28
FMW-23R 3/29/2005 887.45 - - 11.72 875.73
FMW-23R 6/2/2006 887.45 - - 15.68 871.77
FMW-23R 6/16/2006 887.45 - - 14.93 872.52
FMW-23R 1/11/2008 887.45 - - 17.40 870.05
FMW-23R 11/5/2010 887.45 - - 15.53 871.92
FMW-23R 1/10/2014 887.45 - - 12.98 874.47
FMW-23R 1/17/2014 887.45 - - 12.83 874.62
FMW-23R 1/24/2014 887.45 - - 12.58 874.87
Page 37 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-23R 1/31/2014 887.45 - - 12.64 874.81
FMW-23R 2/7/2014 887.45 - - 12.48 874.97
FMW-23R 2/14/2014 887.45 - - 12.19 875.26
FMW-23R 2/21/2014 887.45 - - 12.02 875.43
FMW-23R 2/28/2014 887.45 - - 12.02 875.43
FMW-23R 3/7/2014 887.45 - - 11.59 875.86
FMW-23R 3/14/2014 887.45 - - 11.69 875.76
FMW-23R 3/21/2014 887.45 - - 11.59 875.86
FMW-23R 3/28/2014 887.45 - - 11.41 876.04
FMW-23R 4/4/2014 887.45 - - 11.29 876.16
FMW-23R 4/11/2014 887.45 - - 11.03 876.42
FMW-23R 4/18/2014 887.45 - - 10.89 876.56
FMW-23R 4/25/2014 887.45 - - 11.18 876.27
FMW-23R 5/2/2014 887.45 - - 11.39 876.06
FMW-23R 5/9/2014 887.45 - - 11.57 875.88
FMW-23R 5/16/2014 887.45 - - 11.36 876.09
FMW-23R 5/23/2014 887.45 - - 11.74 875.71
FMW-23R 5/30/2014 887.45 - -12.09 875.36
FMW-23R 6/6/2014 887.45 - -12.36 875.09
FMW-23R 6/13/2014 887.45 - - 12.71 874.74
FMW-23R 6/20/2014 887.45 - - 12.93 874.52
FMW-23R 6/27/2014 887.45 - - 13.24 874.21
FMW-23R 7/5/2014 887.45 - - 12.65 874.80
FMW-23R 7/11/2014 887.45 - - 12.85 874.60
FMW-23R 3/5/2015 887.45 - -14.90 872.55
FMW-23R 5/27/2015 887.45 - -14.54 872.91
FMW-23R 6/29/2015 887.45 - -16.13 871.32
FMW-23R 7/30/2015 887.45 - -17.50 869.95
FMW-23R 8/20/2015 887.45 - -17.71 869.74
FMW-23R 9/9/2015 887.45 - - 18.19 869.26
FMW-23R 10/15/2015 887.45 - - 16.36 871.09
FMW-23R 10/26/2015 887.45 - -16.72 870.73
FMW-23R 12/4/2015 887.45 - -13.82 873.63
FMW-23R 1/12/2016 887.45 - - 11.88 875.57
FMW-23R 5/26/2016 887.45 - - 10.67 876.78
FMW-23R 7/11/2016 887.45 - - 12.71 874.74
FMW-23R 7/12/2016 887.45 - - 12.71 874.74
Page 38 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-23R 7/26/2016 887.45 - - 13.40 874.05
FMW-23R 9/28/2016 887.45 - - 15.98 871.47
FMW-23R 11/29/2016 887.45 - - 16.96 870.49
FMW-23R 12/16/2016 887.45 - - 17.16 870.29
FMW-23R 5/17/2017 887.45 - - 15.39 872.06
FMW-23R 6/26/2017 887.45 - - 13.09 874.36
FMW-23R 8/8/2017 887.45 - - 15.21 872.24
FMW-23R 11/28/2017 887.45 - - 13.20 874.25
FMW-23R 12/11/2017 887.45 - - 18.38 869.07
FMW-23R 1/25/2018 887.45 - - 18.08 869.37
FMW-23R 5/21/2018 887.45 - - 14.86 872.59
FMW-23R 7/9/2018 887.45 - - 16.18 871.27
FMW-23R 8/16/2018 887.45 - - 15.20 872.25
FMW-23R 11/29/2018 887.45 - - 12.88 874.57
FMW-23R 12/12/2018 887.45 - - 12.48 874.97
FMW-23R 3/27/2019 887.45 - - 9.75 877.70
FMW-23R 5/29/2019 887.45 - - 11.77 875.68
FMW-23R 6/10/2019 887.45 - - 11.82 875.63
FMW-23R 8/6/2019 887.45 - - 12.61 874.84
FMW-23R 11/8/2019 887.45 - - 14.84 872.61
FMW-23R 12/9/2019 887.45 - - 13.79 873.66
FMW-23R 3/6/2020 887.45 - - 9.80 877.65
FMW-23R 6/11/2020 887.45 - - 10.63 876.82
FMW-23R 8/24/2020 887.45 - - 13.22 874.23
FMW-23R 11/30/2020 887.45 - - 11.66 875.79
FMW-23R 12/15/2020 887.45 - - 12.64 874.81
FMW-23R 3/29/2021 887.45 - - 8.86 878.59
FMW-23R 6/14/2021 887.45 - - 12.00 875.45
FMW-23R 9/28/2021 887.45 - - 15.09 872.36
FMW-23R 4/1/2022 887.45 - - 13.08 874.37
FMW-23R 12/28/2021 887.45 - - 16.65 870.80
FMW-23R 6/20/2022 887.45 - - 15.15 872.30
FMW-23R 9/22/2022 887.45 - - 16.82 870.63
FMW-23R 12/5/2022 887.45 - - 16.03 871.42
FMW-23R 4/10/2023 887.45 - - 11.57 875.88
FMW-23R 7/17/2023 887.45 - - 14.28 873.17
FMW-23R 9/18/2023 887.45 - - 16.17 871.28
Page 39 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-23R 12/6/2023 887.45 - - 17.82 869.63
FMW-23R 3/1/2024 887.45 - - 14.26 873.19
FMW-24 6/26/1995 888.02 15.02 0.21 15.23 872.95
FMW-24 4/16/1997 888.02 9.83 0.81 10.64 877.99
FMW-24 5/21/1997 888.02 9.86 0.83 10.69 877.95
FMW-24 7/18/1997 888.02 14.06 0.85 14.91 873.75
FMW-24 10/3/1997 888.02 15.95 0.89 16.84 871.85
FMW-24 11/14/1997 888.02 15.67 1.00 16.67 872.10
FMW-24 3/6/1998 888.02 10.16 1.67 11.83 877.44
FMW-24 4/28/1998 888.02 9.33 0.01 9.34 878.69
FMW-24 12/26/1998 888.02 15.03 0.89 15.92 872.77
FMW-24 8/26/1999 888.02 15.64 0.82 16.46 872.18
FMW-24 9/22/1999 888.02 14.78 0.10 14.88 873.22
FMW-24 10/7/1999 888.02 14.78 0.10 14.88 873.22
FMW-24 4/24/2002 888.02 15.84 1.06 16.90 871.92
FMW-24 10/18/2002 888.02 16.85 0.61 17.46 871.02
FMW-24 3/20/2003 888.02 - - 9.60 878.42
FMW-24 4/23/2003 888.02 - - 8.75 879.27
FMW-24 5/30/2003 888.02 - - 8.20 879.82
FMW-24 6/30/2003 888.02 - - 9.30 878.72
FMW-24 7/29/2003 888.02 - - 10.60 877.42
FMW-24 8/20/2003 888.02 - - 7.95 880.07
FMW-24 11/10/2003 888.02 - - 10.91 877.11
FMW-24 12/23/2003 888.02 - - 10.40 877.62
FMW-24 1/29/2004 888.02 - - 11.93 876.09
FMW-24 3/30/2004 888.02 - - 11.30 876.72
FMW-24 4/23/2004 888.02 - - 11.55 876.47
FMW-24 5/20/2004 888.02 - - 12.66 875.36
FMW-24 6/28/2004 888.02 - -13.90 874.12
FMW-24 8/30/2004 888.02 14.72 0.06 14.78 873.29
FMW-24 1/26/2005 888.02 - - 12.65 875.37
FMW-24 2/18/2005 888.02 - - 11.98 876.04
FMW-24 3/29/2005 888.02 - - 11.38 876.64
FMW-24 10/26/2015 888.02 - -16.75 871.27
FMW-24 7/11/2016 888.02 - - 12.48 875.54
FMW-24 7/12/2016 888.02 - - 12.48 875.54
Page 40 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-24 7/25/2016 888.02 - - 13.19 874.83
FMW-24 11/29/2016 888.02 - - 16.94 871.08
FMW-24 12/27/2016 888.02 - - 17.44 870.58
FMW-24 6/26/2017 888.02 - - 12.91 875.11
FMW-24 12/11/2017 888.02 18.41 0.19 18.60 869.56
FMW-24 1/25/2018 888.02 18.30 0.21 18.51 869.67
FMW-24 7/9/2018 888.02 - - 16.25 871.77
FMW-24 12/12/2018 888.02 - - 12.52 875.50
FMW-24 6/10/2019 888.02 - - 11.64 876.38
FMW-24 12/9/2019 888.02 - - 13.73 874.29
FMW-24 6/11/2020 888.02 - - 10.22 877.80
FMW-24 12/14/2020 888.02 - - 12.81 875.21
FMW-24 6/14/2021 888.02 - - 11.80 876.22
FMW-24 6/20/2022 888.02 - - 15.11 872.91
FMW-24 12/12/2022 888.02 - - 15.73 872.29
FMW-24 7/17/2023 888.02 - - 14.17 873.85
FMW-24 12/6/2023 888.02 - - 17.86 870.16
FMW-24D 11/10/2003 888.11 - - 11.35 876.76
FMW-24D 1/29/2004 888.11 - - 12.23 875.88
FMW-24D 3/30/2004 888.11 - - 11.70 876.41
FMW-24D 4/23/2004 888.11 - - 11.90 876.21
FMW-24D 5/20/2004 888.11 - - 13.00 875.11
FMW-24D 6/28/2004 888.11 - - 14.25 873.86
FMW-24D 8/30/2004 888.11 - - 15.10 873.01
FMW-24D 1/26/2005 888.11 - - 13.00 875.11
FMW-24D 2/18/2005 888.11 - - 12.41 875.70
FMW-24D 3/29/2005 888.11 - - 11.83 876.28
FMW-24D 10/26/2015 888.11 - -17.05 871.06
FMW-24D 7/11/2016 888.11 - - 12.75 875.36
FMW-24D 7/12/2016 888.11 - - 12.75 875.36
FMW-24D 7/25/2016 888.11 - - 13.52 NA
FMW-24D 11/29/2016 888.11 - - 17.25 870.86
FMW-24D 12/16/2016 888.11 - - 17.49 870.62
FMW-24D 6/26/2017 888.11 - - 13.10 875.01
FMW-24D 12/11/2017 888.11 - - 18.73 869.38
FMW-24D 7/9/2018 888.11 - - 16.48 871.63
Page 41 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FMW-24D 12/12/2018 888.11 - - 12.64 875.47
FMW-24D 6/10/2019 888.11 - - 11.77 876.34
FMW-24D 12/9/2019 888.11 - - 14.00 874.11
FMW-24D 6/11/2020 888.11 - - 10.46 877.65
FMW-24D 12/14/2020 888.11 - - 11.42 876.69
FMW-24D 6/14/2021 888.11 - - 12.19 875.92
FMW-24D 6/20/2022 888.11 - - 15.49 872.62
FMW-24D 7/17/2023 888.11 - - 14.55 873.56
FMW-24I 11/10/2003 888.25 - - 11.80 876.45
FMW-24I 1/29/2004 888.25 - - 12.30 875.95
FMW-24I 3/30/2004 888.25 - - 11.72 876.53
FMW-24I 4/23/2004 888.25 - - 11.96 876.29
FMW-24I 5/20/2004 888.25 - - 13.10 875.15
FMW-24I 6/28/2004 888.25 - - 14.35 873.90
FMW-24I 8/30/2004 888.25 - - 15.15 873.10
FMW-24I 1/26/2005 888.25 - - 13.08 875.17
FMW-24I 2/18/2005 888.25 - - 12.33 875.92
FMW-24I 3/29/2005 888.25 - - 11.51 876.74
FMW-24I 10/26/2015 888.25 - -16.78 871.47
FMW-24I 7/11/2016 888.25 - - 12.88 875.37
FMW-24I 7/12/2016 888.25 - - 12.88 875.37
FMW-24I 7/25/2016 888.25 - - 13.63 NA
FMW-24I 11/29/2016 888.25 - - 17.34 870.91
FMW-24I 12/14/2016 888.25 - - 17.52 870.73
FMW-24I 6/26/2017 888.25 - - 13.22 875.03
FMW-24I 12/11/2017 888.25 - - 18.84 869.41
FMW-24I 7/9/2018 888.25 - - 16.54 871.71
FMW-24I 12/12/2018 888.25 - - 12.26 875.99
FMW-24I 6/10/2019 888.25 - - 11.87 876.38
FMW-24I 12/9/2019 888.25 - - 14.08 874.17
FMW-24I 6/11/2020 888.25 - - 10.52 877.73
FMW-24I 12/14/2020 888.25 - - 11.38 876.87
FMW-24I 6/14/2021 888.25 - - 12.21 876.04
FMW-24I 6/20/2022 888.25 - - 15.54 872.71
FMW-24I 7/17/2023 888.25 - - 14.57 873.68
Page 42 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-5 6/26/1995 874.79 - -4.25 870.54
FPZ-5 5/21/1997 874.79 - -1.21 873.58
FPZ-5 7/18/1997 874.79 - -4.28 870.51
FPZ-5 10/3/1997 874.79 - -5.15 869.64
FPZ-5 11/14/1997 874.79 - -5.12 869.67
FPZ-5 12/31/1997 874.79 - -3.96 870.83
FPZ-5 1/23/1998 874.79 - -1.58 873.21
FPZ-5 2/17/1998 874.79 - -1.18 873.61
FPZ-5 4/28/1998 874.79 - -8.50 866.29
FPZ-5 9/22/1999 874.79 - -2.46 872.33
FPZ-5 10/12/2000 874.79 - -2.51 872.28
FPZ-5 10/15/2001 874.79 - -6.29 868.50
FPZ-5 10/18/2002 874.79 - -4.82 869.97
FPZ-5 3/20/2003 874.79 - -0.40 874.39
FPZ-5 4/23/2003 874.79 - -0.35 874.44
FPZ-5 5/30/2003 874.79 - -0.43 874.36
FPZ-5 6/30/2003 874.79 - -1.10 873.69
FPZ-5 7/29/2003 874.79 - -1.70 873.09
FPZ-5 8/20/2003 874.79 - -0.60 874.19
FPZ-5 11/10/2003 874.79 - -1.55 873.24
FPZ-5 12/23/2003 874.79 - -1.15 873.64
FPZ-5 1/29/2004 874.79 - -1.50 873.29
FPZ-5 3/30/2004 874.79 - -1.36 873.43
FPZ-5 4/23/2004 874.79 - -1.68 873.11
FPZ-5 5/20/2004 874.79 - -2.52 872.27
FPZ-5 6/28/2004 874.79 - -3.80 870.99
FPZ-5 8/30/2004 874.79 - - 4.15 870.64
FPZ-5 1/26/2005 874.79 - - 2.10 872.69
FPZ-5 2/18/2005 874.79 - -1.54 873.25
FPZ-5 3/29/2005 874.79 - -1.06 873.73
FPZ-5 6/2/2006 874.79 - -4.29 870.50
FPZ-5 6/16/2006 874.79 - -3.44 871.35
FPZ-5 1/11/2008 874.79 - -5.51 869.28
FPZ-5 11/5/2010 874.79 - -3.20 871.59
FPZ-5 1/10/2014 874.79 - -2.01 872.78
FPZ-5 1/17/2014 874.79 - -1.88 872.91
FPZ-5 1/24/2014 874.79 - -1.99 872.80
Page 43 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-5 1/31/2014 874.79 - -2.15 872.64
FPZ-5 2/7/2014 874.79 - -2.01 872.78
FPZ-5 2/14/2014 874.79 - -1.56 873.23
FPZ-5 2/21/2014 874.79 - -1.45 873.34
FPZ-5 2/28/2014 874.79 - -1.67 873.12
FPZ-5 3/7/2014 874.79 - -1.16 873.63
FPZ-5 3/14/2014 874.79 - -1.21 873.58
FPZ-5 3/21/2014 874.79 - -1.16 873.63
FPZ-5 3/28/2014 874.79 - -1.20 873.59
FPZ-5 4/4/2014 874.79 - -1.25 873.54
FPZ-5 4/11/2014 874.79 - -1.15 873.64
FPZ-5 4/18/2014 874.79 - -1.09 873.70
FPZ-5 4/25/2014 874.79 - -1.31 873.48
FPZ-5 5/2/2014 874.79 - -1.53 873.26
FPZ-5 5/9/2014 874.79 - -1.71 873.08
FPZ-5 5/16/2014 874.79 - -1.51 873.28
FPZ-5 5/23/2014 874.79 - -1.97 872.82
FPZ-5 5/30/2014 874.79 - -2.21 872.58
FPZ-5 6/6/2014 874.79 - -2.59 872.20
FPZ-5 6/13/2014 874.79 - - 2.89 871.90
FPZ-5 6/20/2014 874.79 - - 3.15 871.64
FPZ-5 6/27/2014 874.79 - -3.47 871.32
FPZ-5 7/5/2014 874.79 - -4.02 870.77
FPZ-5 7/11/2014 874.79 - -4.52 870.27
FPZ-5 3/5/2015 874.79 - - 3.25 871.54
FPZ-5 5/27/2015 874.79 - - 4.00 870.79
FPZ-5 6/29/2015 874.79 - - 8.08 866.71
FPZ-5 7/30/2015 874.79 - - 7.27 867.52
FPZ-5 8/20/2015 874.79 - - 6.81 867.98
FPZ-5 9/9/2015 874.79 - - 7.54 867.25
FPZ-5 10/15/2015 874.79 - - 5.24 869.55
FPZ-5 10/26/2015 874.79 - - 5.56 869.23
FPZ-5 12/4/2015 874.79 - - 2.86 871.93
FPZ-5 1/12/2016 874.79 - - 1.61 873.18
FPZ-5 5/26/2016 874.79 - - 1.31 873.48
FPZ-5 7/11/2016 874.79 - - 2.68 872.11
FPZ-5 7/12/2016 874.79 - - 2.68 872.11
Page 44 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-5 7/21/2016 874.79 - - 3.48 871.31
FPZ-5 9/28/2016 874.79 - - 5.67 869.12
FPZ-5 11/29/2016 874.79 - - 6.05 868.74
FPZ-5 12/14/2016 874.79 - - 5.90 868.89
FPZ-5 5/17/2017 874.79 - - 4.41 870.38
FPZ-5 6/26/2017 874.79 - - 2.91 871.88
FPZ-5 8/8/2017 874.79 - - 5.28 869.51
FPZ-5 11/28/2017 874.79 - - 7.01 867.78
FPZ-5 12/11/2017 874.79 - - 6.98 867.81
FPZ-5 1/25/2018 874.79 - - 6.28 868.51
FPZ-5 5/21/2018 874.79 - - 4.16 870.63
FPZ-5 7/9/2018 874.79 - - 5.90 868.89
FPZ-5 8/16/2018 874.79 - - 4.52 870.27
FPZ-5 11/29/2018 874.79 - - 2.40 872.39
FPZ-5 12/12/2018 874.79 - - 1.98 872.81
FPZ-5 3/27/2019 874.79 - - 0.77 874.02
FPZ-5 5/29/2019 874.79 - - 0.58 874.21
FPZ-5 6/10/2019 874.79 - - 1.87 872.92
FPZ-5 8/6/2019 874.79 - - 2.81 871.98
FPZ-5 11/8/2019 874.79 - - 3.76 871.03
FPZ-5 12/9/2019 874.79 - - 2.88 871.91
FPZ-5 3/6/2020 874.79 - - 0.29 874.50
FPZ-5 6/11/2020 874.79 - - 1.42 873.37
FPZ-5 8/24/2020 874.79 - - 2.49 872.30
FPZ-5 11/30/2020 874.79 - - 1.33 873.46
FPZ-5 12/14/2020 874.79 - - 1.86 872.93
FPZ-5 3/29/2021 874.79 - - 0.51 874.28
FPZ-5 6/14/2021 874.79 - - 2.49 872.30
FPZ-5 9/28/2021 874.79 - - 4.57 870.22
FPZ-5 12/28/2021 874.79 - - 5.44 869.35
FPZ-5 4/1/2022 874.79 - - 2.23 872.56
FPZ-5 6/20/2022 874.79 - - 3.84 870.95
FPZ-5 9/22/2022 874.79 - - 5.82 868.97
FPZ-5 12/5/2022 874.79 - - 4.57 870.22
FPZ-5 4/10/2023 874.79 - - 1.32 873.47
FPZ-5 7/17/2023 874.79 - - 4.24 870.55
FPZ-5 9/18/2023 874.79 - - 5.31 869.48
Page 45 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-5 12/6/2023 874.79 - - 6.55 868.24
FPZ-5 3/1/2024 874.79 - - 3.30 871.49
FPZ-6 5/21/1997 881.55 - -5.57 875.98
FPZ-6 7/10/1997 881.55 - -8.00 873.55
FPZ-6 7/25/1997 881.55 - -8.55 873.00
FPZ-6 8/24/1997 881.55 - -9.58 871.97
FPZ-6 9/14/1997 881.55 - -10.17 871.38
FPZ-6 10/3/1997 881.55 - -10.42 871.13
FPZ-6 11/14/1997 881.55 - -10.36 871.19
FPZ-6 12/31/1997 881.55 - -9.39 872.16
FPZ-6 1/23/1998 881.55 - -6.88 874.67
FPZ-6 2/17/1998 881.55 - -5.27 876.28
FPZ-6 3/6/1998 881.55 - -5.81 875.74
FPZ-6 4/28/1998 881.55 - -5.24 876.31
FPZ-6 12/26/1998 881.55 - -9.38 872.17
FPZ-6 8/26/1999 881.55 - -10.23 871.32
FPZ-6 9/22/1999 881.55 - -8.08 873.47
FPZ-6 10/7/1999 881.55 - -8.08 873.47
FPZ-6 4/24/2002 881.55 - -10.53 871.02
FPZ-6 9/27/2002 881.55 - -12.64 868.91
FPZ-6 10/3/2002 881.55 - -12.08 869.47
FPZ-6 10/18/2002 881.55 - -10.83 870.72
FPZ-6 10/30/2002 881.55 - -9.99 871.56
FPZ-6 12/4/2002 881.55 - -9.29 872.26
FPZ-6 12/11/2002 881.55 - -8.00 873.55
FPZ-6 12/16/2002 881.55 - -7.73 873.82
FPZ-6 1/2/2003 881.55 - -6.98 874.57
FPZ-6 1/9/2003 881.55 - -6.74 874.81
FPZ-6 1/14/2003 881.55 - -7.10 874.45
FPZ-6 1/21/2003 881.55 - -7.33 874.22
FPZ-6 1/30/2003 881.55 - - 7.40 874.15
FPZ-6 2/6/2003 881.55 - - 7.87 873.68
FPZ-6 2/14/2003 881.55 - -8.02 873.53
FPZ-6 2/21/2003 881.55 - -7.43 874.12
FPZ-6 2/24/2003 881.55 - -7.44 874.11
FPZ-6 3/20/2003 881.55 - -4.95 876.60
Page 46 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-6 4/23/2003 881.55 - -4.45 877.10
FPZ-6 5/30/2003 881.55 - -4.10 877.45
FPZ-6 6/30/2003 881.55 - -5.07 876.48
FPZ-6 7/29/2003 881.55 - -6.18 875.37
FPZ-6 8/20/2003 881.55 - -4.30 877.30
FPZ-6 11/10/2003 881.55 - -6.28 875.32
FPZ-6 12/23/2003 881.55 - - 5.68 875.87
FPZ-6 1/29/2004 881.55 - - 6.80 874.75
FPZ-6 3/30/2004 881.55 - -6.38 875.17
FPZ-6 4/23/2004 881.55 - -6.73 874.82
FPZ-6 5/20/2004 881.55 - -7.68 873.87
FPZ-6 6/28/2004 881.55 - -8.97 872.58
FPZ-6 8/30/2004 881.55 - -9.72 871.83
FPZ-6 1/26/2005 881.55 - -7.55 874.00
FPZ-6 2/18/2005 881.55 - -6.95 874.60
FPZ-6 3/29/2005 881.55 - -6.19 875.36
FPZ-6 6/2/2006 881.55 - -10.30 871.25
FPZ-6 6/16/2006 881.55 - -9.37 872.18
FPZ-6 6/30/2006 881.55 - -8.47 873.08
FPZ-6 7/5/2006 881.55 - -8.77 872.78
FPZ-6 7/13/2006 881.55 - -8.95 872.60
FPZ-6 7/19/2006 881.55 - -9.20 872.35
FPZ-6 7/28/2006 881.55 - -8.91 872.64
FPZ-6 7/31/2006 881.55 - -8.94 872.61
FPZ-6 8/15/2006 881.55 - -9.73 871.82
FPZ-6 8/24/2006 881.55 - -9.52 872.03
FPZ-6 8/30/2006 881.55 - -9.87 871.68
FPZ-6 9/6/2006 881.55 - -7.97 873.58
FPZ-6 9/14/2006 881.55 - -7.48 874.07
FPZ-6 9/22/2006 881.55 - -7.87 873.68
FPZ-6 9/28/2006 881.55 - -7.95 873.60
FPZ-6 10/9/2006 881.55 - -8.18 873.37
FPZ-6 10/12/2006 881.55 - -8.18 873.37
FPZ-6 10/20/2006 881.55 - -7.89 873.66
FPZ-6 10/27/2006 881.55 - -8.25 873.30
FPZ-6 11/1/2006 881.55 - -8.04 873.51
FPZ-6 11/10/2006 881.55 - - 7.95 873.60
Page 47 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-6 11/15/2006 881.55 - - 7.70 873.85
FPZ-6 11/20/2006 881.55 - -7.38 874.17
FPZ-6 11/30/2006 881.55 - -6.97 874.58
FPZ-6 12/4/2006 881.55 - -7.23 874.32
FPZ-6 12/15/2006 881.55 - -7.53 874.02
FPZ-6 12/18/2006 881.55 - -7.76 873.79
FPZ-6 12/29/2006 881.55 - -7.48 874.07
FPZ-6 1/2/2007 881.55 - -7.22 874.33
FPZ-6 1/10/2007 881.55 - -6.71 874.84
FPZ-6 1/19/2007 881.55 - -6.83 874.72
FPZ-6 1/26/2007 881.55 - -6.85 874.70
FPZ-6 2/8/2007 881.55 - - 7.32 874.23
FPZ-6 2/21/2007 881.55 - - 7.13 874.42
FPZ-6 3/2/2007 881.55 - -6.67 874.88
FPZ-6 3/8/2007 881.55 - -6.85 874.70
FPZ-6 3/15/2007 881.55 - -7.08 874.47
FPZ-6 3/22/2007 881.55 - -6.73 874.82
FPZ-6 3/27/2007 881.55 - -6.96 874.59
FPZ-6 4/5/2007 881.55 - -7.26 874.29
FPZ-6 4/12/2007 881.55 - -7.03 874.52
FPZ-6 4/19/2007 881.55 - -6.54 875.01
FPZ-6 4/26/2007 881.55 - -6.92 874.63
FPZ-6 5/4/2007 881.55 - -7.11 874.44
FPZ-6 5/10/2007 881.55 - -7.45 874.10
FPZ-6 5/23/2007 881.55 - -8.62 872.93
FPZ-6 5/31/2007 881.55 - -8.62 872.93
FPZ-6 6/8/2007 881.55 - -8.78 872.77
FPZ-6 6/14/2007 881.55 - -9.08 872.47
FPZ-6 6/21/2007 881.55 - -9.41 872.14
FPZ-6 6/28/2007 881.55 - -9.72 871.83
FPZ-6 7/5/2007 881.55 - -10.11 871.44
FPZ-6 7/12/2007 881.55 - -10.29 871.26
FPZ-6 7/19/2007 881.55 - -10.58 870.97
FPZ-6 7/26/2007 881.55 - -10.86 870.69
FPZ-6 8/3/2007 881.55 - -11.23 870.32
FPZ-6 8/9/2007 881.55 - -11.48 870.07
FPZ-6 8/15/2007 881.55 - -11.81 869.74
Page 48 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-6 8/22/2007 881.55 - -12.13 869.42
FPZ-6 8/31/2007 881.55 - -12.23 869.32
FPZ-6 9/7/2007 881.55 - -12.65 868.90
FPZ-6 9/13/2007 881.55 - -12.92 868.63
FPZ-6 9/21/2007 881.55 - - 12.65 868.90
FPZ-6 9/26/2007 881.55 - - 13.14 868.41
FPZ-6 10/5/2007 881.55 - -13.36 868.19
FPZ-6 10/12/2007 881.55 - -13.60 867.95
FPZ-6 10/19/2007 881.55 - -13.76 867.79
FPZ-6 10/26/2007 881.55 - -12.33 869.22
FPZ-6 11/2/2007 881.55 - -12.15 869.40
FPZ-6 11/9/2007 881.55 - -12.43 869.12
FPZ-6 11/17/2007 881.55 - -12.47 869.08
FPZ-6 11/30/2007 881.55 - -12.82 868.73
FPZ-6 12/8/2007 881.55 - -13.04 868.51
FPZ-6 12/17/2007 881.55 - -12.90 868.65
FPZ-6 12/21/2007 881.55 - - 12.96 868.59
FPZ-6 12/27/2007 881.55 - - 12.42 869.13
FPZ-6 1/4/2008 881.55 - -11.63 869.92
FPZ-6 1/11/2008 881.55 - -11.76 869.79
FPZ-6 1/18/2008 881.55 - -11.61 869.94
FPZ-6 1/26/2008 881.55 - -11.71 869.84
FPZ-6 2/8/2008 881.55 - -11.01 870.54
FPZ-6 2/22/2008 881.55 - -10.98 870.57
FPZ-6 3/1/2008 881.55 - -10.89 870.66
FPZ-6 3/10/2008 881.55 - -9.88 871.67
FPZ-6 3/14/2008 881.55 - -9.97 871.58
FPZ-6 3/28/2008 881.55 - -9.97 871.58
FPZ-6 4/18/2008 881.55 - -9.20 872.35
FPZ-6 4/30/2008 881.55 - -8.15 873.40
FPZ-6 5/2/2008 881.55 - -8.26 873.29
FPZ-6 5/9/2008 881.55 - -8.55 873.00
FPZ-6 5/16/2008 881.55 - -8.70 872.85
FPZ-6 5/24/2008 881.55 - -9.13 872.42
FPZ-6 6/6/2008 881.55 - -9.70 871.85
FPZ-6 6/13/2008 881.55 - -10.10 871.45
FPZ-6 6/20/2008 881.55 - -10.48 871.07
Page 49 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-6 6/27/2008 881.55 - -10.65 870.90
FPZ-6 7/11/2008 881.55 - -10.75 870.80
FPZ-6 7/18/2008 881.55 - -11.20 870.35
FPZ-6 7/25/2008 881.55 - -11.45 870.10
FPZ-6 8/1/2008 881.55 - -11.88 869.67
FPZ-6 8/8/2008 881.55 - -12.28 869.27
FPZ-6 8/15/2008 881.55 - -12.63 868.92
FPZ-6 8/22/2008 881.55 - -12.99 868.56
FPZ-6 9/5/2008 881.55 - -11.92 869.63
FPZ-6 9/12/2008 881.55 - - 11.24 870.31
FPZ-6 9/19/2008 881.55 - - 10.68 870.87
FPZ-6 10/10/2008 881.55 - -10.99 870.56
FPZ-6 11/7/2008 881.55 - -11.48 870.07
FPZ-6 11/14/2008 881.55 - -11.92 869.63
FPZ-6 11/21/2008 881.55 - -11.48 870.07
FPZ-6 12/5/2008 881.55 - -11.37 870.18
FPZ-6 12/12/2008 881.55 - -11.29 870.26
FPZ-6 1/2/2009 881.55 - -11.31 870.24
FPZ-6 1/9/2009 881.55 - -11.27 870.28
FPZ-6 1/23/2009 881.55 - -11.21 870.34
FPZ-6 2/13/2009 881.55 - -11.18 870.37
FPZ-6 2/27/2009 881.55 - - 11.28 870.27
FPZ-6 3/6/2009 881.55 - - 11.39 870.16
FPZ-6 3/30/2009 881.55 - -7.88 873.67
FPZ-6 4/30/2009 881.55 - -8.16 873.39
FPZ-6 5/15/2009 881.55 - -7.85 873.70
FPZ-6 5/22/2009 881.55 - -7.81 873.74
FPZ-6 5/29/2009 881.55 - -8.01 873.54
FPZ-6 6/6/2009 881.55 - -7.22 874.33
FPZ-6 6/12/2009 881.55 - -7.31 874.24
FPZ-6 6/22/2009 881.55 - -7.45 874.10
FPZ-6 6/27/2009 881.55 - -7.66 873.89
FPZ-6 7/6/2009 881.55 - -8.08 873.47
FPZ-6 7/10/2009 881.55 - -8.37 873.18
FPZ-6 7/17/2009 881.55 - -8.88 872.67
FPZ-6 7/24/2009 881.55 - -9.32 872.23
FPZ-6 7/31/2009 881.55 - -9.54 872.01
Page 50 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-6 8/6/2009 881.55 - -9.74 871.81
FPZ-6 8/14/2009 881.55 - -10.21 871.34
FPZ-6 8/21/2009 881.55 - -10.35 871.20
FPZ-6 8/28/2009 881.55 - -10.66 870.89
FPZ-6 9/4/2009 881.55 - -10.85 870.70
FPZ-6 9/11/2009 881.55 - -10.93 870.62
FPZ-6 9/25/2009 881.55 - -11.05 870.50
FPZ-6 10/2/2009 881.55 - -11.01 870.54
FPZ-6 10/9/2009 881.55 - -10.91 870.64
FPZ-6 10/16/2009 881.55 - -11.11 870.44
FPZ-6 10/23/2009 881.55 - -11.23 870.32
FPZ-6 11/6/2009 881.55 - -10.18 871.37
FPZ-6 11/13/2009 881.55 - -10.27 871.28
FPZ-6 11/20/2009 881.55 - -10.20 871.35
FPZ-6 12/4/2009 881.55 - - 10.50 871.05
FPZ-6 12/11/2009 881.55 - - 10.57 870.98
FPZ-6 12/17/2009 881.55 - -10.59 870.96
FPZ-6 1/7/2010 881.55 - -7.03 874.52
FPZ-6 1/7/2010 881.55 - -6.93 874.62
FPZ-6 1/22/2010 881.55 - -6.92 874.63
FPZ-6 1/28/2010 881.55 - -6.97 874.58
FPZ-6 2/4/2010 881.55 - -5.93 875.62
FPZ-6 2/12/2010 881.55 - -5.26 876.29
FPZ-6 11/5/2010 881.55 - -10.09 871.46
FPZ-6 1/10/2014 881.55 - -7.71 873.84
FPZ-6 1/17/2014 881.55 - -7.46 874.09
FPZ-6 1/24/2014 881.55 - - 7.51 874.04
FPZ-6 1/31/2014 881.55 - - 7.58 873.97
FPZ-6 2/7/2014 881.55 - -7.28 874.27
FPZ-6 2/14/2014 881.55 - -6.91 874.64
FPZ-6 2/21/2014 881.55 - -6.76 874.79
FPZ-6 2/28/2014 881.55 - -6.97 874.58
FPZ-6 3/7/2014 881.55 - -6.34 875.21
FPZ-6 3/14/2014 881.55 - -6.39 875.16
FPZ-6 3/21/2014 881.55 - -6.31 875.24
FPZ-6 3/28/2014 881.55 - -6.22 875.33
FPZ-6 4/4/2014 881.55 - -6.33 875.22
Page 51 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-6 4/11/2014 881.55 - -6.12 875.43
FPZ-6 4/18/2014 881.55 - -5.97 875.58
FPZ-6 4/25/2014 881.55 - -6.09 875.46
FPZ-6 5/2/2014 881.55 - -6.28 875.27
FPZ-6 5/9/2014 881.55 - -6.59 874.96
FPZ-6 5/16/2014 881.55 - -6.44 875.11
FPZ-6 5/23/2014 881.55 - -6.91 874.64
FPZ-6 5/30/2014 881.55 - -7.15 874.40
FPZ-6 6/6/2014 881.55 - -7.49 874.06
FPZ-6 6/13/2014 881.55 - -7.79 873.76
FPZ-6 6/20/2014 881.55 - -8.11 873.44
FPZ-6 6/27/2014 881.55 - -8.39 873.16
FPZ-6 7/5/2014 881.55 - -8.81 872.74
FPZ-6 7/11/2014 881.55 - -9.27 872.28
FPZ-6 3/5/2015 881.55 - - 9.15 872.40
FPZ-6 5/27/2015 881.55 - - 9.48 872.07
FPZ-6 6/29/2015 881.55 - - 11.11 870.44
FPZ-6 7/30/2015 881.55 - - 12.41 869.14
FPZ-6 8/20/2015 881.55 - - 12.35 869.20
FPZ-6 9/9/2015 881.55 - - 13.10 868.45
FPZ-6 10/15/2015 881.55 - - 11.14 870.41
FPZ-6 10/26/2015 881.55 - - 11.48 870.07
FPZ-6 12/4/2015 881.55 - - 8.39 873.16
FPZ-6 1/12/2016 881.55 - - 6.87 874.68
FPZ-6 5/26/2016 881.55 - - 5.41 876.14
FPZ-6 7/11/2016 881.55 - - 7.80 873.75
FPZ-6 7/12/2016 881.55 - - 7.80 873.75
FPZ-6 7/22/2016 881.55 - - 8.29 873.26
FPZ-6 9/28/2016 881.55 - - 10.85 870.70
FPZ-6 11/29/2016 881.55 - - 11.84 869.71
FPZ-6 12/15/2016 881.55 - - 11.79 869.76
FPZ-6 5/17/2017 881.55 - - 10.14 871.41
FPZ-6 6/26/2017 881.55 - - 7.94 873.61
FPZ-6 8/8/2017 881.55 - - 10.18 871.37
FPZ-6 11/28/2017 881.55 - - 12.84 868.71
FPZ-6 12/11/2017 881.55 - - 12.91 868.64
FPZ-6 1/25/2018 881.55 - - 12.38 869.17
Page 52 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-6 5/21/2018 881.55 - - 9.70 871.85
FPZ-6 7/9/2018 881.55 - - 7.14 874.41
FPZ-6 8/16/2018 881.55 - - 10.05 871.50
FPZ-6 11/29/2018 881.55 - - 7.74 873.81
FPZ-6 12/12/2018 881.55 - - 7.32 874.23
FPZ-6 3/27/2019 881.55 - - 5.02 876.53
FPZ-6 5/29/2019 881.55 - - 7.11 874.44
FPZ-6 6/10/2019 881.55 - - 6.84 874.71
FPZ-6 8/6/2019 881.55 - - 7.72 873.83
FPZ-6 11/8/2019 881.55 - - 9.56 871.99
FPZ-6 12/9/2019 881.55 - - 8.53 873.02
FPZ-6 3/6/2020 881.55 - - 5.05 876.50
FPZ-6 6/11/2020 881.55 - - 5.87 875.68
FPZ-6 8/24/2020 881.55 - - 8.22 873.33
FPZ-6 11/30/2020 881.55 - - 6.43 875.12
FPZ-6 12/14/2020 881.55 - - 7.85 873.70
FPZ-6 3/29/2021 881.55 - - 4.23 877.32
FPZ-6 6/14/2021 881.55 - - 7.03 874.52
FPZ-6 9/28/2021 881.55 - - 10.04 871.51
FPZ-6 12/28/2021 881.55 - - 11.39 870.16
FPZ-6 4/1/2022 881.55 - - 7.86 873.69
FPZ-6 6/20/2022 881.55 - - 8.21 873.34
FPZ-6 9/22/2022 881.55 - - 11.66 869.89
FPZ-6 12/5/2022 881.55 - - 10.58 870.97
FPZ-6 4/10/2023 881.55 - - 6.51 875.04
FPZ-6 7/17/2023 881.55 - - 9.33 872.22
FPZ-6 9/18/2023 881.55 - - 10.94 870.61
FPZ-6 12/6/2023 881.55 - - 12.52 869.03
FPZ-6 3/1/2024 881.55 - - 9.02 872.53
FPZ-7 5/21/1997 878.84 - -3.76 875.08
FPZ-7 7/10/1997 878.84 - -6.05 872.79
FPZ-7 7/25/1997 878.84 - -6.56 872.28
FPZ-7 8/24/1997 878.84 - -7.27 871.57
FPZ-7 9/14/1997 878.84 - -7.91 870.93
FPZ-7 10/3/1997 878.84 - -8.06 870.78
FPZ-7 11/14/1997 878.84 - -7.91 870.93
Page 53 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-7 12/31/1997 878.84 - -7.09 871.75
FPZ-7 1/23/1998 878.84 - - 2.41 876.43
FPZ-7 2/17/1998 878.84 - - 2.31 876.53
FPZ-7 3/6/1998 878.84 - -3.77 875.07
FPZ-7 4/28/1998 878.84 - -3.45 875.39
FPZ-7 12/26/1998 878.84 - -6.64 872.20
FPZ-7 8/26/1999 878.84 - -7.89 870.95
FPZ-7 9/22/1999 878.84 - -5.73 873.11
FPZ-7 10/7/1999 878.84 - -5.73 873.11
FPZ-7 4/24/2002 878.84 - -7.99 870.85
FPZ-7 9/27/2002 878.84 - -9.97 868.87
FPZ-7 10/3/2002 878.84 - -9.67 869.17
FPZ-7 10/18/2002 878.84 - -8.06 870.78
FPZ-7 10/30/2002 878.84 - -4.15 874.69
FPZ-7 12/4/2002 878.84 - -6.87 871.97
FPZ-7 12/11/2002 878.84 - -2.55 876.29
FPZ-7 12/16/2002 878.84 - -4.46 874.38
FPZ-7 1/2/2003 878.84 - -3.27 875.57
FPZ-7 1/9/2003 878.84 - -4.03 874.81
FPZ-7 1/14/2003 878.84 - -4.70 874.14
FPZ-7 1/21/2003 878.84 - -4.97 873.87
FPZ-7 1/30/2003 878.84 - -2.41 876.43
FPZ-7 2/6/2003 878.84 - -4.13 874.71
FPZ-7 2/14/2003 878.84 - -4.21 874.63
FPZ-7 2/21/2003 878.84 - -3.89 874.95
FPZ-7 2/24/2003 878.84 - -4.09 874.75
FPZ-7 3/20/2003 878.84 - -3.37 875.47
FPZ-7 4/23/2003 878.84 - -3.03 875.81
FPZ-7 5/30/2003 878.84 - -2.65 876.19
FPZ-7 6/30/2003 878.84 - -3.52 875.32
FPZ-7 7/29/2003 878.84 - -4.13 874.71
FPZ-7 8/20/2003 878.84 - - 2.70 876.12
FPZ-7 11/10/2003 878.84 - - 4.10 874.72
FPZ-7 12/23/2003 878.84 - -3.62 875.22
FPZ-7 1/29/2004 878.84 - -3.53 875.31
FPZ-7 3/30/2004 878.84 - -4.15 874.69
FPZ-7 4/23/2004 878.84 - -5.48 873.36
Page 54 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-7 5/20/2004 878.84 - -5.42 873.42
FPZ-7 6/28/2004 878.84 - -6.72 872.12
FPZ-7 8/30/2004 878.84 - -7.34 871.50
FPZ-7 1/26/2005 878.84 - -5.18 873.66
FPZ-7 2/18/2005 878.84 - -4.43 874.41
FPZ-7 3/29/2005 878.84 - -2.82 876.02
FPZ-7 6/2/2006 878.84 - - 7.86 870.98
FPZ-7 6/16/2006 878.84 - - 6.72 872.12
FPZ-7 6/30/2006 878.84 - -5.98 872.86
FPZ-7 7/5/2006 878.84 - -6.39 872.45
FPZ-7 7/13/2006 878.84 - -6.53 872.31
FPZ-7 7/19/2006 878.84 - -6.81 872.03
FPZ-7 7/28/2006 878.84 - -6.51 872.33
FPZ-7 7/31/2006 878.84 - -6.58 872.26
FPZ-7 8/15/2006 878.84 - -7.35 871.49
FPZ-7 8/24/2006 878.84 - -7.10 871.74
FPZ-7 8/30/2006 878.84 - -7.46 871.38
FPZ-7 9/6/2006 878.84 - -4.01 874.83
FPZ-7 9/14/2006 878.84 - -2.68 876.16
FPZ-7 9/22/2006 878.84 - -5.53 873.31
FPZ-7 9/28/2006 878.84 - -5.64 873.20
FPZ-7 10/9/2006 878.84 - -5.80 873.04
FPZ-7 10/12/2006 878.84 - -5.79 873.05
FPZ-7 10/20/2006 878.84 - -4.96 873.88
FPZ-7 10/27/2006 878.84 - -5.84 873.00
FPZ-7 11/1/2006 878.84 - -5.58 873.26
FPZ-7 11/10/2006 878.84 - -5.18 873.66
FPZ-7 11/15/2006 878.84 - -5.16 873.68
FPZ-7 11/20/2006 878.84 - -4.88 873.96
FPZ-7 11/30/2006 878.84 - -4.53 874.31
FPZ-7 12/4/2006 878.84 - -4.82 874.02
FPZ-7 12/15/2006 878.84 - -5.18 873.66
FPZ-7 12/18/2006 878.84 - -5.40 873.44
FPZ-7 12/29/2006 878.84 - -4.90 873.94
FPZ-7 1/2/2007 878.84 - -3.63 875.21
FPZ-7 1/10/2007 878.84 - -3.78 875.06
FPZ-7 1/19/2007 878.84 - - 4.37 874.47
Page 55 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-7 1/26/2007 878.84 - - 4.11 874.73
FPZ-7 2/8/2007 878.84 - -4.92 873.92
FPZ-7 2/21/2007 878.84 - -4.71 874.13
FPZ-7 3/2/2007 878.84 - -2.57 876.27
FPZ-7 3/8/2007 878.84 - -4.49 874.35
FPZ-7 3/15/2007 878.84 - -4.73 874.11
FPZ-7 3/22/2007 878.84 - -4.38 874.46
FPZ-7 3/27/2007 878.84 - -4.64 874.20
FPZ-7 4/5/2007 878.84 - -4.95 873.89
FPZ-7 4/12/2007 878.84 - -2.52 876.32
FPZ-7 4/19/2007 878.84 - -4.10 874.74
FPZ-7 4/26/2007 878.84 - - 4.68 874.16
FPZ-7 5/4/2007 878.84 - - 5.07 873.77
FPZ-7 5/10/2007 878.84 - -5.17 873.67
FPZ-7 5/23/2007 878.84 - -6.37 872.47
FPZ-7 5/31/2007 878.84 - -6.37 872.47
FPZ-7 6/8/2007 878.84 - -6.55 872.29
FPZ-7 6/14/2007 878.84 - -6.81 872.03
FPZ-7 6/21/2007 878.84 - -7.15 871.69
FPZ-7 6/28/2007 878.84 - -7.48 871.36
FPZ-7 7/5/2007 878.84 - -7.89 870.95
FPZ-7 7/12/2007 878.84 - -8.13 870.71
FPZ-7 7/19/2007 878.84 - -8.42 870.42
FPZ-7 7/26/2007 878.84 - -8.67 870.17
FPZ-7 8/3/2007 878.84 - -9.01 869.83
FPZ-7 8/9/2007 878.84 - -9.28 869.56
FPZ-7 8/15/2007 878.84 - -9.67 869.17
FPZ-7 8/22/2007 878.84 - -9.93 868.91
FPZ-7 8/31/2007 878.84 - -10.08 868.76
FPZ-7 9/7/2007 878.84 - -10.47 868.37
FPZ-7 9/13/2007 878.84 - -10.69 868.15
FPZ-7 9/21/2007 878.84 - -10.63 868.21
FPZ-7 9/26/2007 878.84 - -10.86 867.98
FPZ-7 10/5/2007 878.84 - -11.06 867.78
FPZ-7 10/12/2007 878.84 - -11.32 867.52
FPZ-7 10/19/2007 878.84 - -9.55 869.29
FPZ-7 10/26/2007 878.84 - -7.48 871.36
Page 56 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-7 11/2/2007 878.84 - -9.62 869.22
FPZ-7 11/9/2007 878.84 - -9.93 868.91
FPZ-7 11/17/2007 878.84 - -9.98 868.86
FPZ-7 11/30/2007 878.84 - -10.29 868.55
FPZ-7 12/8/2007 878.84 - - 10.48 868.36
FPZ-7 12/17/2007 878.84 - - 10.37 868.47
FPZ-7 12/21/2007 878.84 - -10.43 868.41
FPZ-7 12/27/2007 878.84 - -8.83 870.01
FPZ-7 1/4/2008 878.84 - -8.95 869.89
FPZ-7 1/11/2008 878.84 - -9.13 869.71
FPZ-7 1/18/2008 878.84 - -7.31 871.53
FPZ-7 1/26/2008 878.84 - -9.06 869.78
FPZ-7 2/8/2008 878.84 - -8.32 870.52
FPZ-7 2/22/2008 878.84 - -8.33 870.51
FPZ-7 3/1/2008 878.84 - -8.24 870.60
FPZ-7 3/10/2008 878.84 - -7.07 871.77
FPZ-7 3/14/2008 878.84 - - 7.36 871.48
FPZ-7 3/28/2008 878.84 - - 7.38 871.46
FPZ-7 4/18/2008 878.84 - -6.66 872.18
FPZ-7 4/30/2008 878.84 - -5.20 873.64
FPZ-7 5/2/2008 878.84 - -5.73 873.11
FPZ-7 5/9/2008 878.84 - -6.12 872.72
FPZ-7 5/16/2008 878.84 - -6.31 872.53
FPZ-7 5/24/2008 878.84 - -6.74 872.10
FPZ-7 6/6/2008 878.84 - -7.31 871.53
FPZ-7 6/13/2008 878.84 - -7.75 871.09
FPZ-7 6/20/2008 878.84 - -8.16 870.68
FPZ-7 6/27/2008 878.84 - -8.34 870.50
FPZ-7 7/11/2008 878.84 - -8.44 870.40
FPZ-7 7/18/2008 878.84 - -11.81 867.03
FPZ-7 7/25/2008 878.84 - -9.13 869.71
FPZ-7 8/1/2008 878.84 - -9.54 869.30
FPZ-7 8/8/2008 878.84 - -9.95 868.89
FPZ-7 8/15/2008 878.84 - -10.31 868.53
FPZ-7 8/22/2008 878.84 - -10.67 868.17
FPZ-7 9/5/2008 878.84 - -9.45 869.39
FPZ-7 9/12/2008 878.84 - -8.69 870.15
Page 57 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-7 9/19/2008 878.84 - -8.14 870.70
FPZ-7 10/10/2008 878.84 - -8.51 870.33
FPZ-7 11/7/2008 878.84 - -8.93 869.91
FPZ-7 11/14/2008 878.84 - -9.09 869.75
FPZ-7 11/21/2008 878.84 - -8.93 869.91
FPZ-7 12/5/2008 878.84 - -8.74 870.10
FPZ-7 12/12/2008 878.84 - -8.56 870.28
FPZ-7 1/2/2009 878.84 - -8.52 870.32
FPZ-7 1/9/2009 878.84 - -8.51 870.33
FPZ-7 1/23/2009 878.84 - - 8.44 870.40
FPZ-7 2/13/2009 878.84 - - 8.40 870.44
FPZ-7 2/27/2009 878.84 - -8.32 870.52
FPZ-7 3/6/2009 878.84 - -8.44 870.40
FPZ-7 3/30/2009 878.84 - -4.40 874.44
FPZ-7 4/30/2009 878.84 - -5.75 873.09
FPZ-7 5/15/2009 878.84 - -5.46 873.38
FPZ-7 5/22/2009 878.84 - -5.42 873.42
FPZ-7 5/29/2009 878.84 - -5.66 873.18
FPZ-7 6/6/2009 878.84 - -3.56 875.28
FPZ-7 6/12/2009 878.84 - -4.09 874.75
FPZ-7 6/22/2009 878.84 - -5.12 873.72
FPZ-7 6/27/2009 878.84 - - 5.61 873.23
FPZ-7 7/6/2009 878.84 - - 5.92 872.92
FPZ-7 7/10/2009 878.84 - -6.22 872.62
FPZ-7 7/17/2009 878.84 - -6.60 872.24
FPZ-7 7/24/2009 878.84 - -7.02 871.82
FPZ-7 7/31/2009 878.84 - -7.31 871.53
FPZ-7 8/6/2009 878.84 - -7.55 871.29
FPZ-7 8/14/2009 878.84 - -7.98 870.86
FPZ-7 8/21/2009 878.84 - -8.17 870.67
FPZ-7 8/28/2009 878.84 - -8.37 870.47
FPZ-7 9/4/2009 878.84 - -8.54 870.30
FPZ-7 9/11/2009 878.84 - -8.61 870.23
FPZ-7 9/25/2009 878.84 - -8.88 869.96
FPZ-7 10/2/2009 878.84 - -8.50 870.34
FPZ-7 10/9/2009 878.84 - -8.33 870.51
FPZ-7 10/16/2009 878.84 - -8.59 870.25
Page 58 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-7 10/23/2009 878.84 - -8.66 870.18
FPZ-7 11/6/2009 878.84 - -7.60 871.24
FPZ-7 11/13/2009 878.84 - -7.64 871.20
FPZ-7 11/20/2009 878.84 - -7.54 871.30
FPZ-7 12/4/2009 878.84 - -7.78 871.06
FPZ-7 12/11/2009 878.84 - -7.84 871.00
FPZ-7 12/17/2009 878.84 - -7.83 871.01
FPZ-7 1/7/2010 878.84 - -4.50 874.34
FPZ-7 1/7/2010 878.84 - -4.36 874.48
FPZ-7 1/22/2010 878.84 - -4.44 874.40
FPZ-7 1/28/2010 878.84 - -4.39 874.45
FPZ-7 2/4/2010 878.84 - -3.64 875.20
FPZ-7 2/12/2010 878.84 - -2.97 875.87
FPZ-7 11/5/2010 878.84 - -7.28 871.56
FPZ-7 1/10/2014 878.84 - - 4.01 874.83
FPZ-7 1/17/2014 878.84 - - 3.84 875.00
FPZ-7 1/24/2014 878.84 - -4.65 874.19
FPZ-7 1/31/2014 878.84 - -5.11 873.73
FPZ-7 2/7/2014 878.84 - -4.38 874.46
FPZ-7 2/14/2014 878.84 - -3.18 875.66
FPZ-7 2/21/2014 878.84 - -2.92 875.92
FPZ-7 2/28/2014 878.84 - -4.45 874.39
FPZ-7 3/7/2014 878.84 - -2.31 876.53
FPZ-7 3/14/2014 878.84 - -2.36 876.48
FPZ-7 3/21/2014 878.84 - -2.31 876.53
FPZ-7 3/28/2014 878.84 - -3.12 875.72
FPZ-7 4/4/2014 878.84 - - 3.98 874.86
FPZ-7 4/11/2014 878.84 - - 3.72 875.12
FPZ-7 4/18/2014 878.84 - -3.58 875.26
FPZ-7 4/25/2014 878.84 - -3.81 875.03
FPZ-7 5/2/2014 878.84 - -4.12 874.72
FPZ-7 5/9/2014 878.84 - -4.50 874.34
FPZ-7 5/16/2014 878.84 - -4.04 874.80
FPZ-7 5/23/2014 878.84 - -4.65 874.19
FPZ-7 5/30/2014 878.84 - -4.93 873.91
FPZ-7 6/6/2014 878.84 - -5.26 873.58
FPZ-7 6/13/2014 878.84 - -5.59 873.25
Page 59 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-7 6/20/2014 878.84 - -5.87 872.97
FPZ-7 6/27/2014 878.84 - -6.13 872.71
FPZ-7 7/5/2014 878.84 - -6.52 872.32
FPZ-7 7/11/2014 878.84 - -6.99 871.85
FPZ-7 3/5/2015 878.84 - - 2.58 876.26
FPZ-7 5/27/2015 878.84 - - 7.01 871.83
FPZ-7 6/29/2015 878.84 - - 8.74 870.10
FPZ-7 7/30/2015 878.84 - - 10.07 868.77
FPZ-7 8/20/2015 878.84 - - 9.86 868.98
FPZ-7 9/9/2015 878.84 - - 10.60 868.24
FPZ-7 1/12/2016 878.84 - - 3.85 874.99
FPZ-7 5/26/2016 878.84 - - 3.93 874.91
FPZ-7 7/11/2016 878.84 - - 5.35 873.49
FPZ-7 7/12/2016 878.84 - - 5.35 873.49
FPZ-7 7/26/2016 878.84 - - 6.35 872.49
FPZ-7 9/28/2016 878.84 - - 8.59 870.25
FPZ-7 11/29/2016 878.84 - - 9.35 869.49
FPZ-7 12/14/2016 878.84 - - 9.32 869.52
FPZ-7 5/17/2017 878.84 - - 7.59 871.25
FPZ-7 6/26/2017 878.84 - - 5.44 873.40
FPZ-7 8/8/2017 878.84 - - 7.98 870.86
FPZ-7 11/28/2017 878.84 - - 10.41 868.43
FPZ-7 12/11/2017 878.84 - - 10.48 868.36
FPZ-7 1/25/2018 878.84 - - 9.48 869.36
FPZ-7 5/21/2018 878.84 - - 7.23 871.61
FPZ-7 7/9/2018 878.84 - - 8.75 870.09
FPZ-7 8/16/2018 878.84 - - 7.58 871.26
FPZ-7 11/29/2018 878.84 - - 6.00 872.84
FPZ-7 12/12/2018 878.84 - - 3.23 875.61
FPZ-7 3/27/2019 878.84 - - 3.29 875.55
FPZ-7 5/29/2019 878.84 - - 4.93 873.91
FPZ-7 6/10/2019 878.84 - - 3.42 875.42
FPZ-7 8/6/2019 878.84 - - 5.43 873.41
FPZ-7 11/8/2019 878.84 - - 7.02 871.82
FPZ-7 12/9/2019 878.84 - - 6.03 872.81
FPZ-7 3/6/2020 878.84 - - 3.07 875.77
FPZ-7 6/11/2020 878.84 - - 4.75 874.09
Page 60 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-7 8/24/2020 878.84 - - 5.90 872.94
FPZ-7 11/30/2020 878.84 - - 4.29 874.55
FPZ-7 12/14/2020 878.84 - - 5.71 873.13
FPZ-7 3/29/2021 878.84 - - 2.50 876.34
FPZ-7 6/14/2021 878.84 - - 4.52 874.32
FPZ-7 9/28/2021 878.84 - - 7.60 871.24
FPZ-7 12/28/2021 878.84 - - 8.81 870.03
FPZ-7 4/1/2022 878.84 - - 3.96 874.88
FPZ-7 6/20/2022 878.84 - - 6.04 872.80
FPZ-7 9/22/2022 878.84 - - 9.12 869.72
FPZ-7 12/5/2022 878.84 - - 7.59 871.25
FPZ-7 4/10/2023 878.84 - - 3.01 875.83
FPZ-7 7/17/2023 878.84 - - 6.91 871.93
FPZ-7 9/18/2023 878.84 - - 8.38 870.46
FPZ-7 12/6/2023 878.84 - - 9.98 868.86
FPZ-7 3/1/2024 878.84 - - 6.23 872.61
FPZ-8 5/21/1997 879.30 - -4.92 874.38
FPZ-8 7/10/1997 879.30 - -7.27 872.03
FPZ-8 7/25/1997 879.30 - -7.43 871.87
FPZ-8 8/24/1997 879.30 - -8.30 871.00
FPZ-8 9/14/1997 879.30 - -8.74 870.56
FPZ-8 10/3/1997 879.30 - -9.01 870.29
FPZ-8 11/14/1997 879.30 - -8.90 870.40
FPZ-8 12/31/1997 879.30 - -8.01 871.29
FPZ-8 1/23/1998 879.30 - -4.98 874.32
FPZ-8 2/17/1998 879.30 - - 3.95 875.35
FPZ-8 3/6/1998 879.30 - - 4.70 874.60
FPZ-8 4/28/1998 879.30 - -4.32 874.98
FPZ-8 12/26/1998 879.30 - -7.84 871.46
FPZ-8 8/26/1999 879.30 - -8.94 870.36
FPZ-8 9/22/1999 879.30 - -6.66 872.64
FPZ-8 10/7/1999 879.30 - -6.66 872.64
FPZ-8 10/18/2002 879.30 8.92 0.84 9.76 870.17
FPZ-8 10/30/2002 879.30 8.08 0.27 8.35 871.15
FPZ-8 12/4/2002 879.30 7.63 0.20 7.83 871.62
FPZ-8 12/11/2002 879.30 6.15 0.10 6.25 873.13
Page 61 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-8 12/16/2002 879.30 6.16 0.01 6.17 873.14
FPZ-8 1/2/2003 879.30 - - 6.17 873.13
FPZ-8 1/9/2003 879.30 5.35 0.01 5.36 873.95
FPZ-8 1/14/2003 879.30 - - 5.73 873.57
FPZ-8 1/21/2003 879.30 - - 5.93 873.37
FPZ-8 1/30/2003 879.30 - - 5.82 873.48
FPZ-8 2/6/2003 879.30 - - 5.70 873.60
FPZ-8 2/14/2003 879.30 - - 5.50 873.80
FPZ-8 2/21/2003 879.30 - - 5.21 874.09
FPZ-8 2/24/2003 879.30 - - 5.18 874.12
FPZ-8 3/20/2003 879.30 - - 4.93 874.37
FPZ-8 4/23/2003 879.30 - - 3.62 875.68
FPZ-8 5/30/2003 879.30 - - 3.42 875.88
FPZ-8 6/30/2003 879.30 - - 4.40 874.90
FPZ-8 7/29/2003 879.30 - - 5.33 873.97
FPZ-8 8/20/2003 879.30 3.53 0.02 3.55 875.77
FPZ-8 11/10/2003 879.30 - - 5.23 874.06
FPZ-8 12/23/2003 879.30 - - 4.60 874.70
FPZ-8 1/29/2004 879.30 - - 5.47 873.83
FPZ-8 3/30/2004 879.30 - - 5.10 874.20
FPZ-8 4/23/2004 879.30 - - 5.45 873.85
FPZ-8 5/20/2004 879.30 - - 6.44 872.86
FPZ-8 6/28/2004 879.30 - - 7.82 871.48
FPZ-8 8/30/2004 879.30 - - 8.33 870.97
FPZ-8 1/26/2005 879.30 - - 6.05 873.25
FPZ-8 2/18/2005 879.30 - - 5.52 873.78
FPZ-8 3/29/2005 879.30 - - 4.84 874.46
FPZ-8 6/2/2006 879.30 - - 8.75 870.55
FPZ-8 6/16/2006 879.30 - - 7.79 871.51
FPZ-8 1/11/2008 879.30 - - 9.92 869.38
FPZ-8 11/5/2010 879.30 - - 8.57 870.73
FPZ-8 1/10/2014 879.30 - - 6.21 873.09
FPZ-8 1/17/2014 879.30 - - 5.89 873.41
FPZ-8 1/24/2014 879.30 - - 6.01 873.29
FPZ-8 1/31/2014 879.30 - - 6.14 873.16
FPZ-8 2/7/2014 879.30 - - 5.81 873.49
FPZ-8 2/14/2014 879.30 - - 5.49 873.81
Page 62 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-8 2/21/2014 879.30 - - 5.29 874.01
FPZ-8 2/28/2014 879.30 - - 5.57 873.73
FPZ-8 3/7/2014 879.30 - - 4.91 874.39
FPZ-8 3/14/2014 879.30 - - 4.98 874.32
FPZ-8 3/21/2014 879.30 - - 4.91 874.39
FPZ-8 3/28/2014 879.30 - - 4.95 874.35
FPZ-8 4/4/2014 879.30 - - 5.02 874.28
FPZ-8 4/11/2014 879.30 - - 4.89 874.41
FPZ-8 4/18/2014 879.30 - - 4.65 874.65
FPZ-8 4/25/2014 879.30 - - 4.98 874.32
FPZ-8 5/2/2014 879.30 - - 4.19 875.11
FPZ-8 5/9/2014 879.30 - - 5.57 873.73
FPZ-8 5/16/2014 879.30 - - 6.32 872.98
FPZ-8 5/23/2014 879.30 - - 5.78 873.52
FPZ-8 5/30/2014 879.30 - - 6.14 873.16
FPZ-8 6/6/2014 879.30 - - 6.48 872.82
FPZ-8 6/13/2014 879.30 - - 6.83 872.47
FPZ-8 6/20/2014 879.30 - - 7.19 872.11
FPZ-8 6/27/2014 879.30 - - 7.41 871.89
FPZ-8 7/5/2014 879.30 - - 7.97 871.33
FPZ-8 7/11/2014 879.30 - - 8.34 870.96
FPZ-8 3/5/2015 879.30 - -6.60 872.70
FPZ-8 5/27/2015 879.30 - -8.00 871.30
FPZ-8 6/29/2015 879.30 - -9.95 869.35
FPZ-8 7/30/2015 879.30 - -11.25 868.05
FPZ-8 8/20/2015 879.30 - -11.05 868.25
FPZ-8 9/9/2015 879.30 - -11.46 867.84
FPZ-8 10/15/2015 879.30 - -9.48 869.82
FPZ-8 10/26/2015 879.30 - -9.84 869.46
FPZ-8 12/4/2015 879.30 - -6.90 872.40
FPZ-8 1/12/2016 879.30 - - 5.55 873.75
FPZ-8 5/26/2016 879.30 - - 4.86 874.44
FPZ-8 7/11/2016 879.30 - - 6.61 872.69
FPZ-8 7/12/2016 879.30 - - 6.61 872.69
FPZ-8 7/22/2016 879.30 - - 7.45 871.85
FPZ-8 9/28/2016 879.30 - - 9.82 869.48
FPZ-8 11/29/2016 879.30 - - 10.31 868.99
Page 63 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-8 12/14/2016 879.30 - - 10.21 869.09
FPZ-8 5/17/2017 879.30 - - 8.49 870.81
FPZ-8 6/26/2017 879.30 - - 6.70 872.60
FPZ-8 8/8/2017 879.30 - - 9.38 869.92
FPZ-8 11/28/2017 879.30 - - 11.31 867.99
FPZ-8 12/11/2017 879.30 - - 11.33 867.97
FPZ-8 1/25/2018 879.30 - - 10.49 868.81
FPZ-8 5/21/2018 879.30 - - 8.18 871.12
FPZ-8 7/9/2018 879.30 - - 9.92 869.38
FPZ-8 8/16/2018 879.30 - - 8.63 870.67
FPZ-8 11/29/2018 879.30 - - 6.45 872.85
FPZ-8 12/12/2018 879.30 - - 5.92 873.38
FPZ-8 3/27/2019 879.30 - - 4.02 875.28
FPZ-8 5/29/2019 879.30 - - 6.13 873.17
FPZ-8 6/10/2019 879.30 - - 5.82 873.48
FPZ-8 8/6/2019 879.30 - - 6.69 872.61
FPZ-8 11/8/2019 879.30 - - 8.06 871.24
FPZ-8 12/9/2019 879.30 - - 7.04 872.26
FPZ-8 3/6/2020 879.30 - - 3.90 875.40
FPZ-8 6/11/2020 879.30 - - 4.94 874.36
FPZ-8 8/24/2020 879.30 - - 7.01 872.29
FPZ-8 11/30/2020 879.30 - - 4.29 875.01
FPZ-8 12/14/2020 879.30 - - 6.85 872.45
FPZ-8 3/29/2021 879.30 - - 3.30 876.00
FPZ-8 6/14/2021 879.30 - - 5.84 873.46
FPZ-8 9/28/2021 879.30 - - 8.69 870.61
FPZ-8 12/28/2021 879.30 - - 9.69 869.61
FPZ-8 4/1/2022 879.30 - - 6.28 873.02
FPZ-8 6/20/2022 879.30 - - 7.08 872.22
FPZ-8 9/22/2022 879.30 - - 10.11 869.19
FPZ-8 12/5/2022 879.30 - - 8.81 870.49
FPZ-8 4/10/2023 879.30 - - 5.14 874.16
FPZ-8 7/17/2023 879.30 - - 8.14 871.16
FPZ-8 9/18/2023 879.30 - - 9.48 869.82
FPZ-8 12/6/2023 879.30 - - 10.89 868.41
FPZ-8 3/1/2024 879.30 - - 7.44 871.86
Page 64 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-10 5/21/1997 880.01 - - 5.12 874.89
FPZ-10 7/10/1997 880.01 - - 7.48 872.53
FPZ-10 7/25/1997 880.01 7.82 0.05 7.87 872.18
FPZ-10 8/24/1997 880.01 8.50 0.12 8.62 871.48
FPZ-10 9/14/1997 880.01 8.82 0.45 9.27 871.08
FPZ-10 10/3/1997 880.01 9.05 2.27 11.32 870.39
FPZ-10 11/14/1997 880.01 9.02 2.25 11.27 870.43
FPZ-10 12/31/1997 880.01 8.18 1.45 9.63 871.47
FPZ-10 1/23/1998 880.01 5.58 0.65 6.23 874.27
FPZ-10 2/17/1998 880.01 4.18 0.86 5.04 875.62
FPZ-10 3/6/1998 880.01 4.90 0.54 5.44 874.98
FPZ-10 4/28/1998 880.01 4.52 0.53 5.05 875.36
FPZ-10 12/26/1998 880.01 8.05 1.25 9.30 871.65
FPZ-10 8/26/1999 880.01 8.97 1.85 10.82 870.58
FPZ-10 9/22/1999 880.01 6.98 0.50 7.48 872.91
FPZ-10 10/7/1999 880.01 6.98 0.50 7.48 872.91
FPZ-10 4/24/2002 880.01 9.07 0.85 9.92 870.73
FPZ-10 9/27/2002 880.01 10.87 1.45 12.32 868.78
FPZ-10 10/3/2002 880.01 10.21 2.22 12.43 869.25
FPZ-10 10/18/2002 880.01 9.52 0.82 10.34 870.29
FPZ-10 10/30/2002 880.01 8.68 0.38 9.06 871.24
FPZ-10 12/4/2002 880.01 8.09 0.29 8.38 871.85
FPZ-10 12/11/2002 880.01 6.72 0.27 6.99 873.22
FPZ-10 12/16/2002 880.01 6.66 0.21 6.87 873.30
FPZ-10 1/2/2003 880.01 5.98 0.02 6.00 874.03
FPZ-10 1/9/2003 880.01 - - 5.80 874.21
FPZ-10 1/14/2003 880.01 - - 6.11 873.90
FPZ-10 1/21/2003 880.01 - - 6.35 873.66
FPZ-10 1/30/2003 880.01 - - 6.35 873.66
FPZ-10 2/6/2003 880.01 - - 6.14 873.87
FPZ-10 2/14/2003 880.01 - - 6.34 873.67
FPZ-10 2/21/2003 880.01 - - 5.76 874.25
FPZ-10 2/24/2003 880.01 - - 6.08 873.93
FPZ-10 3/20/2003 880.01 - - 4.25 875.76
FPZ-10 4/23/2003 880.01 - - 3.88 876.13
FPZ-10 5/30/2003 880.01 - - 5.61 874.40
FPZ-10 6/30/2003 880.01 - - 4.90 875.11
Page 65 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-10 7/29/2003 880.01 - - 5.91 874.10
FPZ-10 8/20/2003 880.01 - - 3.99 875.98
FPZ-10 11/10/2003 880.01 - - 5.50 874.47
FPZ-10 12/23/2003 880.01 - - 4.95 875.06
FPZ-10 1/29/2004 880.01 - - 5.92 874.09
FPZ-10 3/30/2004 880.01 - - 5.45 874.56
FPZ-10 4/23/2004 880.01 - - 5.82 874.19
FPZ-10 5/20/2004 880.01 - - 6.80 873.21
FPZ-10 6/28/2004 880.01 - - 8.17 871.84
FPZ-10 8/30/2004 880.01 8.70 0.18 8.88 871.27
FPZ-10 1/26/2005 880.01 6.47 0.01 6.48 873.54
FPZ-10 2/18/2005 880.01 5.93 0.02 5.95 874.08
FPZ-10 3/29/2005 880.01 4.40 0.06 4.46 875.60
FPZ-10 6/2/2006 880.01 9.58 0.02 9.60 870.43
FPZ-10 6/16/2006 880.01 8.73 0.03 8.76 871.27
FPZ-10 6/30/2006 880.01 - - 7.87 872.14
FPZ-10 7/5/2006 880.01 - - 8.40 871.61
FPZ-10 7/13/2006 880.01 - - 8.55 871.46
FPZ-10 7/19/2006 880.01 - - 8.58 871.43
FPZ-10 7/28/2006 880.01 - - 8.34 871.67
FPZ-10 7/31/2006 880.01 - - 8.80 871.21
FPZ-10 8/15/2006 880.01 - - 9.38 870.63
FPZ-10 8/24/2006 880.01 - - 9.29 870.72
FPZ-10 8/30/2006 880.01 - - 9.51 870.50
FPZ-10 9/6/2006 880.01 - - 7.50 872.51
FPZ-10 9/14/2006 880.01 - - 6.85 873.16
FPZ-10 9/22/2006 880.01 - - 9.17 870.84
FPZ-10 9/28/2006 880.01 - - 7.38 872.63
FPZ-10 10/9/2006 880.01 - - 7.68 872.33
FPZ-10 10/12/2006 880.01 - - 7.54 872.47
FPZ-10 10/20/2006 880.01 - - 7.33 872.68
FPZ-10 10/27/2006 880.01 - - 7.67 872.34
FPZ-10 11/1/2006 880.01 - - 7.43 872.58
FPZ-10 11/10/2006 880.01 - - 7.33 872.68
FPZ-10 11/15/2006 880.01 - - 7.11 872.90
FPZ-10 11/20/2006 880.01 - - 6.86 873.15
FPZ-10 11/30/2006 880.01 - - 6.63 873.38
Page 66 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-10 12/4/2006 880.01 - - 7.78 872.23
FPZ-10 12/15/2006 880.01 - - 7.07 872.94
FPZ-10 12/18/2006 880.01 - - 7.28 872.73
FPZ-10 12/29/2006 880.01 - - 6.88 873.13
FPZ-10 1/2/2007 880.01 - - 6.70 873.31
FPZ-10 1/10/2007 880.01 - - 6.22 873.79
FPZ-10 1/19/2007 880.01 - - 6.40 873.61
FPZ-10 1/26/2007 880.01 - - 6.42 873.59
FPZ-10 2/8/2007 880.01 - - 6.74 873.27
FPZ-10 2/21/2007 880.01 - - 6.83 873.18
FPZ-10 3/2/2007 880.01 - - 6.09 873.92
FPZ-10 3/8/2007 880.01 - - 6.41 873.60
FPZ-10 3/15/2007 880.01 - - 6.75 873.26
FPZ-10 3/22/2007 880.01 - - 6.30 873.71
FPZ-10 3/27/2007 880.01 - - 6.68 873.33
FPZ-10 4/5/2007 880.01 - - 6.83 873.18
FPZ-10 4/12/2007 880.01 - - 6.47 873.54
FPZ-10 4/19/2007 880.01 - - 6.25 873.76
FPZ-10 4/26/2007 880.01 - - 8.84 871.17
FPZ-10 5/4/2007 880.01 - - 7.00 873.01
FPZ-10 5/10/2007 880.01 - - 9.12 870.89
FPZ-10 5/23/2007 880.01 - - 8.63 871.38
FPZ-10 5/31/2007 880.01 - - 8.63 871.38
FPZ-10 6/8/2007 880.01 - - 9.20 870.81
FPZ-10 6/14/2007 880.01 - - 9.02 870.99
FPZ-10 6/21/2007 880.01 - - 9.20 870.81
FPZ-10 6/28/2007 880.01 - - 9.70 870.31
FPZ-10 7/5/2007 880.01 - - 9.41 870.60
FPZ-10 7/12/2007 880.01 - - 9.64 870.37
FPZ-10 7/19/2007 880.01 - - 9.92 870.09
FPZ-10 7/26/2007 880.01 - - 10.15 869.86
FPZ-10 8/3/2007 880.01 - - 10.40 869.61
FPZ-10 8/9/2007 880.01 - - 10.73 869.28
FPZ-10 8/15/2007 880.01 - - 11.63 868.38
FPZ-10 8/22/2007 880.01 - - 11.91 868.10
FPZ-10 8/31/2007 880.01 - - 12.01 868.00
FPZ-10 9/7/2007 880.01 - - 12.02 867.99
Page 67 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-10 9/13/2007 880.01 - - 12.15 867.86
FPZ-10 9/21/2007 880.01 - - 12.30 867.71
FPZ-10 9/26/2007 880.01 - - 12.32 867.69
FPZ-10 10/5/2007 880.01 - - 12.38 867.63
FPZ-10 10/12/2007 880.01 - - 12.68 867.33
FPZ-10 10/19/2007 880.01 - - 12.69 867.32
FPZ-10 10/26/2007 880.01 - - 10.09 869.92
FPZ-10 11/2/2007 880.01 - - 11.14 868.87
FPZ-10 11/9/2007 880.01 - - 11.58 868.43
FPZ-10 11/17/2007 880.01 - - 11.83 868.18
FPZ-10 11/30/2007 880.01 - - 11.94 868.07
FPZ-10 12/8/2007 880.01 - - 11.89 868.12
FPZ-10 12/17/2007 880.01 - - 12.90 867.11
FPZ-10 12/21/2007 880.01 - - 11.84 868.17
FPZ-10 12/27/2007 880.01 - - 11.34 868.67
FPZ-10 1/4/2008 880.01 - - 10.85 869.16
FPZ-10 1/11/2008 880.01 10.88 0.56 11.44 868.99
FPZ-10 1/18/2008 880.01 - - 10.69 869.32
FPZ-10 1/26/2008 880.01 - - 10.90 869.11
FPZ-10 2/8/2008 880.01 - - 10.13 869.88
FPZ-10 2/22/2008 880.01 - - 10.03 869.98
FPZ-10 3/1/2008 880.01 - - 9.90 870.11
FPZ-10 3/10/2008 880.01 - - 9.31 870.70
FPZ-10 3/14/2008 880.01 - - 9.33 870.68
FPZ-10 3/28/2008 880.01 - - 9.45 870.56
FPZ-10 4/18/2008 880.01 - - 9.85 870.16
FPZ-10 4/30/2008 880.01 - - 7.50 872.51
FPZ-10 5/2/2008 880.01 - - 7.53 872.48
FPZ-10 5/9/2008 880.01 - - 7.97 872.04
FPZ-10 5/16/2008 880.01 - - 8.20 871.81
FPZ-10 5/24/2008 880.01 - - 8.97 871.04
FPZ-10 6/6/2008 880.01 - - 9.53 870.48
FPZ-10 6/13/2008 880.01 - - 9.80 870.21
FPZ-10 6/20/2008 880.01 - - 10.15 869.86
FPZ-10 6/27/2008 880.01 - - 10.60 869.41
FPZ-10 7/11/2008 880.01 - - 10.60 869.41
FPZ-10 7/18/2008 880.01 - - 11.02 868.99
Page 68 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-10 7/25/2008 880.01 - - 11.32 868.69
FPZ-10 8/1/2008 880.01 - - 11.60 868.41
FPZ-10 8/8/2008 880.01 - - 11.93 868.08
FPZ-10 8/15/2008 880.01 - - 12.34 867.67
FPZ-10 8/22/2008 880.01 - - 12.63 867.38
FPZ-10 9/5/2008 880.01 - - 11.14 868.87
FPZ-10 9/12/2008 880.01 - - 10.78 869.23
FPZ-10 9/19/2008 880.01 - - 10.25 869.76
FPZ-10 10/10/2008 880.01 - - 10.70 869.31
FPZ-10 11/7/2008 880.01 - - 11.27 868.74
FPZ-10 11/14/2008 880.01 - - 11.25 868.76
FPZ-10 11/21/2008 880.01 - - 11.45 868.56
FPZ-10 12/5/2008 880.01 - - 11.05 868.96
FPZ-10 12/12/2008 880.01 - - 10.95 869.06
FPZ-10 1/2/2009 880.01 - - 10.97 869.04
FPZ-10 1/9/2009 880.01 - - 10.99 869.02
FPZ-10 1/23/2009 880.01 - - 10.94 869.07
FPZ-10 2/13/2009 880.01 - - 10.90 869.11
FPZ-10 2/27/2009 880.01 - - 10.92 869.09
FPZ-10 3/6/2009 880.01 - - 11.24 868.77
FPZ-10 3/30/2009 880.01 - - 7.16 872.85
FPZ-10 4/30/2009 880.01 - - 7.65 872.36
FPZ-10 5/15/2009 880.01 - - 7.43 872.58
FPZ-10 5/22/2009 880.01 - - 7.38 872.63
FPZ-10 5/29/2009 880.01 - - 7.66 872.35
FPZ-10 6/6/2009 880.01 - - 6.86 873.15
FPZ-10 6/12/2009 880.01 - - 7.07 872.94
FPZ-10 6/22/2009 880.01 - - 7.66 872.35
FPZ-10 6/27/2009 880.01 - - 7.92 872.09
FPZ-10 7/6/2009 880.01 - - 8.44 871.57
FPZ-10 7/10/2009 880.01 - - 8.78 871.23
FPZ-10 7/17/2009 880.01 - - 9.30 870.71
FPZ-10 7/24/2009 880.01 - - 9.50 870.51
FPZ-10 7/31/2009 880.01 - - 9.62 870.39
FPZ-10 8/6/2009 880.01 - - 9.91 870.10
FPZ-10 8/14/2009 880.01 - - 10.01 870.00
FPZ-10 8/21/2009 880.01 - - 10.28 869.73
Page 69 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-10 8/28/2009 880.01 - - 10.85 869.16
FPZ-10 9/4/2009 880.01 - - 10.64 869.37
FPZ-10 9/11/2009 880.01 - - 10.92 869.09
FPZ-10 9/25/2009 880.01 - - 11.01 869.00
FPZ-10 10/2/2009 880.01 - - 10.83 869.18
FPZ-10 10/9/2009 880.01 - - 10.80 869.21
FPZ-10 10/16/2009 880.01 - - 10.90 869.11
FPZ-10 10/23/2009 880.01 - - 10.99 869.02
FPZ-10 11/6/2009 880.01 - - 9.64 870.37
FPZ-10 11/13/2009 880.01 - - 9.71 870.30
FPZ-10 11/20/2009 880.01 - - 9.62 870.39
FPZ-10 12/4/2009 880.01 - - 9.84 870.17
FPZ-10 12/11/2009 880.01 - - 9.90 870.11
FPZ-10 12/17/2009 880.01 - - 9.92 870.09
FPZ-10 1/7/2010 880.01 - - 6.93 873.08
FPZ-10 1/7/2010 880.01 - - 7.06 872.95
FPZ-10 1/22/2010 880.01 - - 7.00 873.01
FPZ-10 1/28/2010 880.01 - - 6.94 873.07
FPZ-10 2/4/2010 880.01 - - 5.57 874.44
FPZ-10 2/12/2010 880.01 - - 4.96 875.05
FPZ-10 11/5/2010 880.01 - - 9.70 870.31
FPZ-10 1/10/2014 880.01 - - 6.98 873.03
FPZ-10 1/17/2014 880.01 - - 6.73 873.28
FPZ-10 1/24/2014 880.01 - - 7.48 872.53
FPZ-10 1/31/2014 880.01 - - 7.03 872.98
FPZ-10 2/7/2014 880.01 - - 6.81 873.20
FPZ-10 2/14/2014 880.01 - - 6.48 873.53
FPZ-10 2/21/2014 880.01 - - 6.11 873.90
FPZ-10 2/28/2014 880.01 - - 6.39 873.62
FPZ-10 3/7/2014 880.01 - - 5.06 874.95
FPZ-10 3/14/2014 880.01 - - 5.96 874.05
FPZ-10 3/21/2014 880.01 - - 5.86 874.15
FPZ-10 3/28/2014 880.01 - - 5.96 874.05
FPZ-10 4/4/2014 880.01 - - 5.76 874.25
FPZ-10 4/11/2014 880.01 - - 5.53 874.48
FPZ-10 4/18/2014 880.01 - - 5.31 874.70
FPZ-10 4/25/2014 880.01 - - 5.63 874.38
Page 70 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-10 5/2/2014 880.01 - - 5.98 874.03
FPZ-10 5/9/2014 880.01 - - 6.35 873.66
FPZ-10 5/16/2014 880.01 - - 6.06 873.95
FPZ-10 5/23/2014 880.01 - - 6.72 873.29
FPZ-10 5/30/2014 880.01 - - 7.38 872.63
FPZ-10 6/6/2014 880.01 - - 7.76 872.25
FPZ-10 6/13/2014 880.01 - - 8.09 871.92
FPZ-10 6/20/2014 880.01 - - 8.51 871.50
FPZ-10 6/27/2014 880.01 - - 8.83 871.18
FPZ-10 7/5/2014 880.01 - - 9.12 870.89
FPZ-10 7/11/2014 880.01 - - 9.34 870.67
FPZ-10 3/5/2015 880.01 - -8.30 871.71
FPZ-10 5/27/2015 880.01 - -9.30 870.71
FPZ-10 6/29/2015 880.01 - -10.25 869.76
FPZ-10 7/30/2015 880.01 11.50 0.17 11.67 868.47
FPZ-10 8/20/2015 880.01 11.45 0.06 11.51 868.55
FPZ-10 9/9/2015 880.01 11.95 0.50 12.45 867.94
FPZ-10 10/15/2015 880.01 9.89 0.55 10.44 869.98
FPZ-10 10/26/2015 880.01 10.06 0.96 11.02 869.71
FPZ-10 12/1/2015 880.01 7.25 1.13 8.38 872.48
FPZ-10 12/2/2015 880.01 7.42 0.43 7.85 872.48
FPZ-10 12/3/2015 880.01 7.26 0.05 7.31 872.74
FPZ-10 12/4/2015 880.01 7.33 0.52 7.85 872.55
FPZ-10 12/10/2015 880.01 - - 7.86 872.15
FPZ-10 12/28/2015 880.01 6.32 0.18 6.50 873.64
FPZ-10 1/12/2016 880.01 6.94 0.02 6.96 873.07
FPZ-10 5/26/2016 880.01 5.12 0.01 5.13 874.89
FPZ-10 7/11/2016 880.01 - - 6.92 873.09
FPZ-10 7/12/2016 880.01 - - 6.92 873.09
FPZ-10 9/28/2016 880.01 10.09 0.09 10.18 869.90
FPZ-10 11/29/2016 880.01 - - 11.89 868.12
FPZ-10 12/16/2016 880.01 - - 11.14 868.87
FPZ-10 12/28/2016 880.01 - - 10.90 869.11
FPZ-10 5/17/2017 880.01 9.23 0.02 9.25 870.78
FPZ-10 6/26/2017 880.01 - - 7.21 872.80
FPZ-10 8/8/2017 880.01 - - 9.61 870.40
FPZ-10 11/28/2017 880.01 11.71 0.21 11.92 868.25
Page 71 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-10 12/11/2017 880.01 11.73 0.26 11.99 868.22
FPZ-10 1/25/2018 880.01 11.21 0.20 11.41 868.75
FPZ-10 5/21/2018 880.01 9.04 0.11 9.15 870.94
FPZ-10 7/9/2018 880.01 - - 10.49 869.52
FPZ-10 8/16/2018 880.01 - - 9.34 870.67
FPZ-10 11/29/2018 880.01 - - 6.93 873.08
FPZ-10 12/12/2018 880.01 - - 6.43 873.58
FPZ-10 3/27/2019 880.01 - - 4.31 875.70
FPZ-10 5/29/2019 880.01 - - 6.37 873.64
FPZ-10 6/10/2019 880.01 - - 6.12 873.89
FPZ-10 8/6/2019 880.01 - - 6.96 873.05
FPZ-10 11/8/2019 880.01 - - 8.56 871.45
FPZ-10 12/9/2019 880.01 - - 7.46 872.55
FPZ-10 3/6/2020 880.01 - - 4.21 875.80
FPZ-10 6/11/2020 880.01 - - 5.14 874.87
FPZ-10 8/24/2020 880.01 - - 7.35 872.66
FPZ-10 11/30/2020 880.01 - - 5.39 874.62
FPZ-10 12/15/2020 880.01 - - 7.04 872.97
FPZ-10 3/29/2021 880.01 - - 3.50 876.51
FPZ-10 6/14/2021 880.01 - - 6.79 873.22
FPZ-10 9/28/2021 880.01 - - 9.07 870.94
FPZ-10 12/28/2021 880.01 - - 10.16 869.85
FPZ-10 4/1/2022 880.01 - - 6.67 873.34
FPZ-10 6/20/2022 880.01 - - 9.02 870.99
FPZ-10 9/22/2022 880.01 - - 10.53 869.48
FPZ-10 12/5/2022 880.01 - - 9.35 870.66
FPZ-10 4/10/2023 880.01 - - 5.55 874.46
FPZ-10 7/17/2023 880.01 - - 8.16 871.85
FPZ-10 9/18/2023 880.01 - - 9.92 870.09
FPZ-10 12/6/2023 880.01 11.35 0.07 11.42 868.59
FPZ-10 3/1/2024 880.01 - - 7.98 872.03
FPZ-10I 11/10/2003 880.45 - - 5.88 874.57
FPZ-10I 1/29/2004 880.45 - - 6.30 874.15
FPZ-10I 3/30/2004 880.45 - - 5.85 874.60
FPZ-10I 4/23/2004 880.45 - - 6.22 874.23
FPZ-10I 5/20/2004 880.45 - - 7.21 873.24
Page 72 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-10I 6/28/2004 880.45 - - 8.53 871.92
FPZ-10I 8/30/2004 880.45 - - 9.12 871.33
FPZ-10I 1/26/2005 880.45 - - 6.90 873.55
FPZ-10I 2/18/2005 880.45 - - 6.34 874.11
FPZ-10I 3/29/2005 880.45 - - 5.73 874.72
FPZ-10I 10/26/2015 880.45 - -10.66 869.79
FPZ-10I 7/11/2016 880.45 - - 7.33 873.12
FPZ-10I 7/12/2016 880.45 - - 7.33 873.12
FPZ-10I 7/27/2016 880.45 - - 8.30 872.15
FPZ-10I 11/29/2016 880.45 - - 11.10 869.35
FPZ-10I 5/17/2017 880.45 9.25 871.20
FPZ-10I 6/26/2017 880.45 - - 7.53 872.92
FPZ-10I 8/8/2017 880.45 - - 9.61 870.84
FPZ-10I 11/28/2017 880.45 - - 12.16 868.29
FPZ-10I 12/11/2017 880.45 - - 12.23 868.22
FPZ-10I 1/25/2018 880.45 - - 11.41 869.04
FPZ-10I 7/9/2018 880.45 - - 10.62 869.83
FPZ-10I 12/12/2018 880.45 - - 6.87 873.58
FPZ-10I 6/10/2019 880.45 - - 6.55 873.90
FPZ-10I 12/9/2019 880.45 - - 7.88 872.57
FPZ-10I 6/11/2020 880.45 - - 5.53 874.92
FPZ-10I 12/15/2020 880.45 - - 7.21 873.24
FPZ-10I 6/14/2021 880.45 - - 6.59 873.86
FPZ-10I 6/20/2022 880.45 - - 9.53 870.92
FPZ-10I 7/17/2023 880.45 - - 9.26 871.19
FPZ-11 5/21/1997 880.95 - - 4.47 876.48
FPZ-11 7/10/1997 880.95 - - 6.86 874.09
FPZ-11 7/25/1997 880.95 - - 7.47 873.48
FPZ-11 8/24/1997 880.95 - - 8.18 872.77
FPZ-11 9/14/1997 880.95 - - 8.55 872.40
FPZ-11 10/3/1997 880.95 - - 8.84 872.11
FPZ-11 11/14/1997 880.95 - - 8.72 872.23
FPZ-11 4/28/1998 880.95 - - 3.97 876.98
FPZ-11 12/26/1998 880.95 - - 8.06 872.89
FPZ-11 8/26/1999 880.95 - - 8.84 872.11
FPZ-11 9/22/1999 880.95 - - 7.02 873.93
Page 73 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-11 10/7/1999 880.95 - - 7.02 873.93
FPZ-11 10/12/2000 880.95 - - 6.92 874.03
FPZ-11 10/15/2001 880.95 - - 11.00 869.95
FPZ-11 4/24/2002 880.95 - - 9.72 871.23
FPZ-11 9/27/2002 880.95 - - 11.81 869.14
FPZ-11 10/3/2002 880.95 - - 11.32 869.63
FPZ-11 10/18/2002 880.95 - - 9.70 871.25
FPZ-11 10/30/2002 880.95 - - 9.56 871.39
FPZ-11 12/4/2002 880.95 - - 8.36 872.59
FPZ-11 12/11/2002 880.95 - - 6.55 874.40
FPZ-11 12/16/2002 880.95 - - 6.60 874.35
FPZ-11 1/2/2003 880.95 - - 5.70 875.25
FPZ-11 1/9/2003 880.95 - - 5.67 875.28
FPZ-11 1/14/2003 880.95 - - 6.05 874.90
FPZ-11 1/21/2003 880.95 - - 6.36 874.59
FPZ-11 1/30/2003 880.95 - - 5.84 875.11
FPZ-11 2/6/2003 880.95 - - 6.34 874.61
FPZ-11 2/14/2003 880.95 - - 6.45 874.50
FPZ-11 2/21/2003 880.95 - - 6.12 874.83
FPZ-11 2/24/2003 880.95 - - 6.34 874.61
FPZ-11 3/20/2003 880.95 - - 3.79 877.16
FPZ-11 4/23/2003 880.95 - - 3.29 877.66
FPZ-11 5/30/2003 880.95 - - 2.95 878.00
FPZ-11 6/30/2003 880.95 - - 3.80 877.15
FPZ-11 7/29/2003 880.95 - - 5.00 875.95
FPZ-11 8/20/2003 880.95 - - 2.90 878.02
FPZ-11 11/10/2003 880.95 - - 5.15 875.77
FPZ-11 12/23/2003 880.95 - - 4.55 876.40
FPZ-11 1/29/2004 880.95 - - 5.55 875.40
FPZ-11 3/30/2004 880.95 - - 5.40 875.55
FPZ-11 4/23/2004 880.95 - - 5.68 875.27
FPZ-11 5/20/2004 880.95 - - 6.72 874.23
FPZ-11 6/28/2004 880.95 - - 8.00 872.95
FPZ-11 8/30/2004 880.95 - - 8.78 872.17
FPZ-11 1/26/2005 880.95 - - 6.61 874.34
FPZ-11 2/18/2005 880.95 - - 5.88 875.07
FPZ-11 3/29/2005 880.95 - - 4.83 876.12
Page 74 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-11 6/2/2006 880.95 - - 9.53 871.42
FPZ-11 6/16/2006 880.95 - - 8.13 872.82
FPZ-11 6/30/2006 880.95 - - 7.22 873.73
FPZ-11 7/5/2006 880.95 - - 7.79 873.16
FPZ-11 7/13/2006 880.95 - - 7.97 872.98
FPZ-11 7/19/2006 880.95 - - 8.24 872.71
FPZ-11 7/28/2006 880.95 - - 7.84 873.11
FPZ-11 7/31/2006 880.95 - - 7.98 872.97
FPZ-11 8/15/2006 880.95 - - 8.77 872.18
FPZ-11 8/24/2006 880.95 - - 8.93 872.02
FPZ-11 8/30/2006 880.95 - - 8.90 872.05
FPZ-11 9/6/2006 880.95 - - 6.19 874.76
FPZ-11 9/14/2006 880.95 - - 5.29 875.66
FPZ-11 9/22/2006 880.95 - - 6.79 874.16
FPZ-11 9/28/2006 880.95 - - 6.93 874.02
FPZ-11 10/9/2006 880.95 - - 7.22 873.73
FPZ-11 10/12/2006 880.95 - - 7.22 873.73
FPZ-11 10/20/2006 880.95 - - 6.69 874.26
FPZ-11 10/27/2006 880.95 - - 7.27 873.68
FPZ-11 11/1/2006 880.95 - - 6.98 873.97
FPZ-11 11/10/2006 880.95 - - 6.83 874.12
FPZ-11 11/15/2006 880.95 - - 6.53 874.42
FPZ-11 11/20/2006 880.95 - - 6.18 874.77
FPZ-11 11/30/2006 880.95 - - 5.87 875.08
FPZ-11 12/4/2006 880.95 - - 6.19 874.76
FPZ-11 12/15/2006 880.95 - - 6.53 874.42
FPZ-11 12/18/2006 880.95 - - 6.77 874.18
FPZ-11 12/29/2006 880.95 - - 6.33 874.62
FPZ-11 1/2/2007 880.95 - - 5.78 875.17
FPZ-11 1/10/2007 880.95 - - 5.42 875.53
FPZ-11 1/19/2007 880.95 - - 5.78 875.17
FPZ-11 1/26/2007 880.95 - - 5.70 875.25
FPZ-11 2/8/2007 880.95 - - 6.32 874.63
FPZ-11 2/21/2007 880.95 - - 6.08 874.87
FPZ-11 3/2/2007 880.95 - - 4.85 876.10
FPZ-11 3/8/2007 880.95 - - 5.77 875.18
FPZ-11 3/15/2007 880.95 - - 6.05 874.90
Page 75 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-11 3/22/2007 880.95 - - 5.64 875.31
FPZ-11 3/27/2007 880.95 - - 5.92 875.03
FPZ-11 4/5/2007 880.95 - - 6.25 874.70
FPZ-11 4/12/2007 880.95 - - 5.42 875.53
FPZ-11 4/19/2007 880.95 - - 5.34 875.61
FPZ-11 4/26/2007 880.95 - - 5.83 875.12
FPZ-11 5/4/2007 880.95 - - 6.28 874.67
FPZ-11 5/10/2007 880.95 - - 6.42 874.53
FPZ-11 5/23/2007 880.95 - - 7.55 873.40
FPZ-11 5/31/2007 880.95 - - 7.55 873.40
FPZ-11 6/8/2007 880.95 - - 7.74 873.21
FPZ-11 6/14/2007 880.95 - - 8.04 872.91
FPZ-11 6/21/2007 880.95 - - 8.38 872.57
FPZ-11 6/28/2007 880.95 - - 8.68 872.27
FPZ-11 7/5/2007 880.95 - - 9.08 871.87
FPZ-11 7/12/2007 880.95 - - 9.33 871.62
FPZ-11 7/19/2007 880.95 - - 9.58 871.37
FPZ-11 7/26/2007 880.95 - - 9.83 871.12
FPZ-11 8/3/2007 880.95 - - 10.20 870.75
FPZ-11 8/9/2007 880.95 - - 10.45 870.50
FPZ-11 8/15/2007 880.95 - - 10.77 870.18
FPZ-11 8/22/2007 880.95 - - 11.08 869.87
FPZ-11 8/31/2007 880.95 - - 11.25 869.70
FPZ-11 9/7/2007 880.95 - - 11.62 869.33
FPZ-11 9/13/2007 880.95 - - 11.87 869.08
FPZ-11 9/21/2007 880.95 - - 11.85 869.10
FPZ-11 9/26/2007 880.95 - - 12.13 868.82
FPZ-11 10/5/2007 880.95 - - 12.35 868.60
FPZ-11 10/12/2007 880.95 - - 12.54 868.41
FPZ-11 10/19/2007 880.95 - - 12.68 868.27
FPZ-11 10/26/2007 880.95 - - 5.36 875.59
FPZ-11 11/2/2007 880.95 - - 12.15 868.80
FPZ-11 11/9/2007 880.95 - - 11.60 869.35
FPZ-11 11/17/2007 880.95 - - 11.70 869.25
FPZ-11 11/30/2007 880.95 - - 12.02 868.93
FPZ-11 12/8/2007 880.95 - - 12.22 868.73
FPZ-11 12/17/2007 880.95 - - 12.17 868.78
Page 76 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-11 12/21/2007 880.95 - - 12.21 868.74
FPZ-11 12/27/2007 880.95 - - 11.62 869.33
FPZ-11 1/4/2008 880.95 - - 10.69 870.26
FPZ-11 1/11/2008 880.95 - - 10.98 869.97
FPZ-11 1/18/2008 880.95 - - 10.78 870.17
FPZ-11 1/26/2008 880.95 - - 10.95 870.00
FPZ-11 2/8/2008 880.95 - - 10.09 870.86
FPZ-11 2/22/2008 880.95 - - 10.17 870.78
FPZ-11 3/1/2008 880.95 - - 10.08 870.87
FPZ-11 3/10/2008 880.95 - - 8.62 872.33
FPZ-11 3/14/2008 880.95 - - 9.08 871.87
FPZ-11 3/28/2008 880.95 - - 9.12 871.83
FPZ-11 4/18/2008 880.95 - - 8.29 872.66
FPZ-11 4/30/2008 880.95 - - 6.77 874.18
FPZ-11 5/2/2008 880.95 - - 7.12 873.83
FPZ-11 5/9/2008 880.95 - - 7.64 873.31
FPZ-11 5/16/2008 880.95 - - 7.79 873.16
FPZ-11 5/24/2008 880.95 - - 8.20 872.75
FPZ-11 6/6/2008 880.95 - - 8.72 872.23
FPZ-11 6/13/2008 880.95 - - 9.08 871.87
FPZ-11 6/20/2008 880.95 - - 9.46 871.49
FPZ-11 6/27/2008 880.95 - - 9.62 871.33
FPZ-11 7/11/2008 880.95 - - 9.80 871.15
FPZ-11 7/18/2008 880.95 - - 10.18 870.77
FPZ-11 7/25/2008 880.95 - - 10.50 870.45
FPZ-11 8/1/2008 880.95 - - 10.88 870.07
FPZ-11 8/8/2008 880.95 - - 11.26 869.69
FPZ-11 8/15/2008 880.95 - - 11.61 869.34
FPZ-11 8/22/2008 880.95 - - 11.96 868.99
FPZ-11 9/5/2008 880.95 - - 10.94 870.01
FPZ-11 9/12/2008 880.95 - - 10.11 870.84
FPZ-11 9/19/2008 880.95 - - 9.52 871.43
FPZ-11 10/10/2008 880.95 - - 10.02 870.93
FPZ-11 11/7/2008 880.95 - - 10.61 870.34
FPZ-11 11/14/2008 880.95 - - 10.70 870.25
FPZ-11 11/21/2008 880.95 - - 10.61 870.34
FPZ-11 12/5/2008 880.95 - - 10.53 870.42
Page 77 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-11 12/12/2008 880.95 - - 10.49 870.46
FPZ-11 1/2/2009 880.95 - - 10.45 870.50
FPZ-11 1/9/2009 880.95 - - 10.42 870.53
FPZ-11 1/23/2009 880.95 - - 10.37 870.58
FPZ-11 2/13/2009 880.95 - - 10.34 870.61
FPZ-11 2/27/2009 880.95 - - 10.40 870.55
FPZ-11 3/6/2009 880.95 - - 10.48 870.47
FPZ-11 3/30/2009 880.95 - - 6.14 874.81
FPZ-11 4/30/2009 880.95 - - 7.16 873.79
FPZ-11 5/15/2009 880.95 - - 6.76 874.19
FPZ-11 5/22/2009 880.95 - - 6.74 874.21
FPZ-11 5/29/2009 880.95 - - 7.03 873.92
FPZ-11 6/6/2009 880.95 - - 5.03 875.92
FPZ-11 6/12/2009 880.95 - - 5.56 875.39
FPZ-11 6/22/2009 880.95 - - 6.29 874.66
FPZ-11 6/27/2009 880.95 - - 7.09 873.86
FPZ-11 7/6/2009 880.95 - - 7.23 873.72
FPZ-11 7/10/2009 880.95 - - 7.56 873.39
FPZ-11 7/17/2009 880.95 - - 7.79 873.16
FPZ-11 7/24/2009 880.95 - - 8.24 872.71
FPZ-11 7/31/2009 880.95 - - 8.49 872.46
FPZ-11 8/6/2009 880.95 - - 8.76 872.19
FPZ-11 8/14/2009 880.95 - - 9.22 871.73
FPZ-11 8/21/2009 880.95 - - 9.41 871.54
FPZ-11 8/28/2009 880.95 - - 9.65 871.30
FPZ-11 9/4/2009 880.95 - - 9.85 871.10
FPZ-11 9/11/2009 880.95 - - 9.98 870.97
FPZ-11 9/25/2009 880.95 - - 10.06 870.89
FPZ-11 10/2/2009 880.95 - - 10.04 870.91
FPZ-11 10/9/2009 880.95 - - 9.93 871.02
FPZ-11 10/16/2009 880.95 - - 10.31 870.64
FPZ-11 10/23/2009 880.95 - - 10.42 870.53
FPZ-11 11/6/2009 880.95 - - 9.18 871.77
FPZ-11 11/13/2009 880.95 - - 9.44 871.51
FPZ-11 11/20/2009 880.95 - - 9.39 871.56
FPZ-11 12/4/2009 880.95 - - 9.64 871.31
FPZ-11 12/11/2009 880.95 - - 9.71 871.24
Page 78 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-11 12/17/2009 880.95 - - 9.69 871.26
FPZ-11 1/7/2010 880.95 - - 5.94 875.01
FPZ-11 1/7/2010 880.95 - - 5.89 875.06
FPZ-11 1/22/2010 880.95 - - 5.85 875.10
FPZ-11 1/28/2010 880.95 - - 5.77 875.18
FPZ-11 2/4/2010 880.95 - - 4.44 876.51
FPZ-11 2/12/2010 880.95 - - 3.82 877.13
FPZ-11 11/5/2010 880.95 - - 9.23 871.72
FPZ-11 1/10/2014 880.95 - - 6.34 874.61
FPZ-11 1/17/2014 880.95 - - 6.18 874.77
FPZ-11 1/24/2014 880.95 - - 6.30 874.65
FPZ-11 1/31/2014 880.95 - - 6.51 874.44
FPZ-11 2/7/2014 880.95 - - 6.28 874.67
FPZ-11 2/14/2014 880.95 - - 4.98 875.97
FPZ-11 2/21/2014 880.95 - - 4.75 876.20
FPZ-11 2/28/2014 880.95 - - 5.88 875.07
FPZ-11 3/7/2014 880.95 - - 3.61 877.34
FPZ-11 3/14/2014 880.95 - - 3.68 877.27
FPZ-11 3/21/2014 880.95 - - 3.61 877.34
FPZ-11 3/28/2014 880.95 - - 3.68 877.27
FPZ-11 4/4/2014 880.95 - - 5.18 875.77
FPZ-11 4/11/2014 880.95 - - 4.83 876.12
FPZ-11 4/18/2014 880.95 - - 4.69 876.26
FPZ-11 4/25/2014 880.95 - - 5.17 875.78
FPZ-11 5/2/2014 880.95 - - 5.39 875.56
FPZ-11 5/9/2014 880.95 - - 5.68 875.27
FPZ-11 5/16/2014 880.95 - - 5.18 875.77
FPZ-11 5/23/2014 880.95 - - 5.45 875.50
FPZ-11 5/30/2014 880.95 - - 5.93 875.02
FPZ-11 6/6/2014 880.95 - - 6.37 874.58
FPZ-11 6/13/2014 880.95 - - 6.73 874.22
FPZ-11 6/20/2014 880.95 - - 7.03 873.92
FPZ-11 6/27/2014 880.95 - - 7.26 873.69
FPZ-11 7/5/2014 880.95 - - 7.73 873.22
FPZ-11 7/11/2014 880.95 - - 8.11 872.84
FPZ-11 3/5/2015 880.95 - -4.91 876.04
FPZ-11 5/27/2015 880.95 - -8.50 872.45
Page 79 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-11 6/29/2015 880.95 - -10.10 870.85
FPZ-11 7/30/2015 880.95 - -11.45 869.50
FPZ-11 8/20/2015 880.95 - -11.55 869.40
FPZ-11 9/9/2015 880.95 - -12.10 868.85
FPZ-11 10/15/2015 880.95 - -10.16 870.79
FPZ-11 10/26/2015 880.95 - -10.55 870.40
FPZ-11 12/4/2015 880.95 - -5.54 875.41
FPZ-11 1/12/2016 880.95 - - 4.87 876.08
FPZ-11 5/26/2016 880.95 - - 4.51 876.44
FPZ-11 7/11/2016 880.95 - - 6.52 874.43
FPZ-11 7/12/2016 880.95 - - 6.52 874.43
FPZ-11 7/25/2016 880.95 - - 7.44 873.51
FPZ-11 9/28/2016 880.95 - - 9.82 871.13
FPZ-11 11/29/2016 880.95 - - 10.85 870.10
FPZ-11 12/14/2016 880.95 - - 10.90 870.05
FPZ-11 5/17/2017 880.95 - - 9.14 871.81
FPZ-11 6/26/2017 880.95 - - 6.50 874.45
FPZ-11 8/8/2017 880.95 - - 9.10 871.85
FPZ-11 11/28/2017 880.95 - - 12.04 868.91
FPZ-11 12/11/2017 880.95 - - 12.22 868.73
FPZ-11 1/25/2018 880.95 - - 11.26 869.69
FPZ-11 5/21/2018 880.95 - - 8.75 872.20
FPZ-11 7/9/2018 880.95 - - 10.11 870.84
FPZ-11 8/16/2018 880.95 - - 8.99 871.96
FPZ-11 11/29/2018 880.95 - - 6.09 874.86
FPZ-11 12/12/2018 880.95 - - 3.98 876.97
FPZ-11 3/27/2019 880.95 - - 3.62 877.33
FPZ-11 5/29/2019 880.95 - - 5.93 875.02
FPZ-11 6/10/2019 880.95 - - 4.42 876.53
FPZ-11 8/6/2019 880.95 - - 6.48 874.47
FPZ-11 11/8/2019 880.95 - - 8.53 872.42
FPZ-11 12/9/2019 880.95 - - 7.48 873.47
FPZ-11 3/6/2020 880.95 - - 3.66 877.29
FPZ-11 6/11/2020 880.95 - - 4.71 876.24
FPZ-11 8/24/2020 880.95 - - 7.13 873.82
FPZ-11 11/30/2020 880.95 - - 2.75 878.20
FPZ-11 12/14/2020 880.95 - - 6.58 874.37
Page 80 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-11 3/29/2021 880.95 - - 2.75 878.20
FPZ-11 6/14/2021 880.95 - - 7.41 873.54
FPZ-11 9/28/2021 880.95 - - 9.03 871.92
FPZ-11 12/28/2021 880.95 - - 10.48 870.47
FPZ-11 4/1/2022 880.95 - - 6.54 874.41
FPZ-11 6/20/2022 880.95 - - 8.66 872.29
FPZ-11 9/22/2022 880.95 - - 10.83 870.12
FPZ-11 12/5/2022 880.95 - - 8.87 872.08
FPZ-11 4/10/2023 880.95 - - 3.62 877.33
FPZ-11 7/17/2023 880.95 - - 8.34 872.61
FPZ-11 9/18/2023 880.95 - - 9.99 870.96
FPZ-11 12/6/2023 880.95 - - 11.67 869.28
FPZ-11 3/1/2024 880.95 - - 7.08 873.87
FPZ-12 1/2/2003 877.68 - - 3.81 873.87
FPZ-12 1/9/2003 877.68 - - 3.95 873.73
FPZ-12 1/14/2003 877.68 - - 4.26 873.42
FPZ-12 1/21/2003 877.68 - - 4.47 873.21
FPZ-12 1/30/2003 877.68 - - 4.53 873.15
FPZ-12 2/6/2003 877.68 - - 5.65 872.03
FPZ-12 2/14/2003 877.68 - - 5.36 872.32
FPZ-12 2/21/2003 877.68 - - 5.08 872.60
FPZ-12 2/24/2003 877.68 - - 5.44 872.24
FPZ-12 3/20/2003 877.68 - - 2.66 875.02
FPZ-12 4/23/2003 877.68 - - 2.40 875.28
FPZ-12 5/30/2003 877.68 - - 2.16 875.52
FPZ-12 6/30/2003 877.68 - - 3.30 874.38
FPZ-12 7/29/2003 877.68 - - 4.20 873.48
FPZ-12 8/20/2003 877.68 - - 2.46 875.20
FPZ-12 11/10/2003 877.68 - - 3.85 873.81
FPZ-12 12/23/2003 877.68 - - 3.38 874.30
FPZ-12 1/29/2004 877.68 - - 4.15 873.53
FPZ-12 3/30/2004 877.68 - - 3.90 873.78
FPZ-12 4/23/2004 877.68 - - 4.35 873.33
FPZ-12 5/20/2004 877.68 - - 5.05 872.63
FPZ-12 6/28/2004 877.68 - - 6.20 871.48
FPZ-12 8/30/2004 877.68 - - 6.71 870.97
Page 81 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-12 1/26/2005 877.68 - - 4.67 873.01
FPZ-12 2/18/2005 877.68 - - 4.02 873.66
FPZ-12 3/29/2005 877.68 - - 3.55 874.13
FPZ-12 6/2/2006 877.68 - - 7.05 870.63
FPZ-12 6/16/2006 877.68 - - 6.05 871.63
FPZ-12 1/11/2008 877.68 - - 8.17 869.51
FPZ-12 11/5/2010 877.68 - - 6.64 871.04
FPZ-12 1/10/2014 877.68 - - 4.43 873.25
FPZ-12 1/17/2014 877.68 - - 4.28 873.40
FPZ-12 1/24/2014 877.68 - - 4.48 873.20
FPZ-12 1/31/2014 877.68 - - 4.63 873.05
FPZ-12 2/7/2014 877.68 - - 4.48 873.20
FPZ-12 2/14/2014 877.68 - - 4.15 873.53
FPZ-12 2/21/2014 877.68 - - 3.91 873.77
FPZ-12 2/28/2014 877.68 - - 4.18 873.50
FPZ-12 3/7/2014 877.68 - - 3.55 874.13
FPZ-12 3/14/2014 877.68 - - 3.61 874.07
FPZ-12 3/21/2014 877.68 - - 3.55 874.13
FPZ-12 3/28/2014 877.68 - - 3.63 874.05
FPZ-12 4/4/2014 877.68 - - 3.81 873.87
FPZ-12 4/11/2014 877.68 - - 3.12 874.56
FPZ-12 4/18/2014 877.68 - - 2.91 874.77
FPZ-12 4/25/2014 877.68 - - 3.31 874.37
FPZ-12 5/2/2014 877.68 - - 3.71 873.97
FPZ-12 5/9/2014 877.68 - - 4.18 873.50
FPZ-12 5/16/2014 877.68 - - 3.94 873.74
FPZ-12 5/23/2014 877.68 - - 4.41 873.27
FPZ-12 5/30/2014 877.68 - - 4.57 873.11
FPZ-12 6/6/2014 877.68 - - 4.89 872.79
FPZ-12 6/13/2014 877.68 - - 5.19 872.49
FPZ-12 6/20/2014 877.68 - - 5.43 872.25
FPZ-12 6/27/2014 877.68 - - 5.64 872.04
FPZ-12 7/5/2014 877.68 - - 5.07 872.61
FPZ-12 7/11/2014 877.68 - - 6.43 871.25
FPZ-12 3/5/2015 877.68 - -5.60 872.08
FPZ-12 5/27/2015 877.68 - -6.48 871.20
FPZ-12 6/29/2015 877.68 - -8.00 869.68
Page 82 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-12 7/30/2015 877.68 - -9.21 868.47
FPZ-12 8/20/2015 877.68 - -8.78 868.90
FPZ-12 9/9/2015 877.68 - -9.75 867.93
FPZ-12 10/15/2015 877.68 - -7.70 869.98
FPZ-12 10/26/2015 877.68 - -8.07 869.61
FPZ-12 12/4/2015 877.68 - -5.06 872.62
FPZ-12 1/12/2016 877.68 - - 3.94 873.74
FPZ-12 5/26/2016 877.68 - - 3.68 874.00
FPZ-12 7/11/2016 877.68 - - 4.89 872.79
FPZ-12 7/12/2016 877.68 - - 4.89 872.79
FPZ-12 7/21/2016 877.68 - - 5.50 872.18
FPZ-12 9/28/2016 877.68 - - 7.75 869.93
FPZ-12 11/29/2016 877.68 - - 8.50 869.18
FPZ-12 12/14/2016 877.68 - - 8.74 868.94
FPZ-12 5/17/2017 877.68 - - 6.78 870.90
FPZ-12 6/26/2017 877.68 - - 4.82 872.86
FPZ-12 8/8/2017 877.68 - - 7.12 870.56
FPZ-12 11/28/2017 877.68 - - 9.51 868.17
FPZ-12 12/11/2017 877.68 - - 9.43 868.25
FPZ-12 1/25/2018 877.68 - - 8.61 869.07
FPZ-12 5/21/2018 877.68 - - 6.48 871.20
FPZ-12 7/9/2018 877.68 - - 7.88 869.80
FPZ-12 8/16/2018 877.68 - - 6.78 870.90
FPZ-12 11/29/2018 877.68 - - 4.70 872.98
FPZ-12 12/12/2018 877.68 - - 4.24 873.44
FPZ-12 3/27/2019 877.68 - - 3.04 874.64
FPZ-12 5/29/2019 877.68 - - 4.70 872.98
FPZ-12 6/10/2019 877.68 - - 4.05 873.63
FPZ-12 8/6/2019 877.68 - - 4.87 872.81
FPZ-12 11/8/2019 877.68 - - 6.11 871.57
FPZ-12 12/9/2019 877.68 - - 5.21 872.47
FPZ-12 3/6/2020 877.68 - - 3.07 874.61
FPZ-12 6/11/2020 877.68 - - 3.75 873.93
FPZ-12 8/24/2020 877.68 - - 5.31 872.37
FPZ-12 11/30/2020 877.68 - - 3.57 874.11
FPZ-12 12/14/2020 877.68 - - 4.94 872.74
FPZ-12 3/29/2021 877.68 - - 2.78 874.90
Page 83 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-12 6/14/2021 877.68 - - 4.43 873.25
FPZ-12 9/28/2021 877.68 - - 6.80 870.88
FPZ-12 12/28/2021 877.68 - - 8.01 869.67
FPZ-12 4/1/2022 877.68 - - 4.51 873.17
FPZ-12 6/20/2022 877.68 - - 5.12 872.56
FPZ-12 9/22/2022 877.68 - - 8.16 869.52
FPZ-12 12/5/2022 877.68 - - 6.91 870.77
FPZ-12 4/10/2023 877.68 - - 3.77 873.91
FPZ-12 7/17/2023 877.68 - - 6.27 871.41
FPZ-12 9/18/2023 877.68 - - 7.49 870.19
FPZ-12 12/6/2023 877.68 - - 9.04 868.64
FPZ-12 3/1/2024 877.68 - - 5.72 871.96
FPZ-12I 11/10/2003 877.63 - - 3.80 873.83
FPZ-12I 1/29/2004 877.63 - - 4.20 873.43
FPZ-12I 3/30/2004 877.63 - - 3.90 873.73
FPZ-12I 4/23/2004 877.63 - - 4.30 873.33
FPZ-12I 5/20/2004 877.63 - - 5.07 872.56
FPZ-12I 6/28/2004 877.63 - - 6.22 871.41
FPZ-12I 8/30/2004 877.63 - - 6.71 870.92
FPZ-12I 1/26/2005 877.63 - - 4.71 872.92
FPZ-12I 2/18/2005 877.63 - - 4.17 873.46
FPZ-12I 3/29/2005 877.63 - - 3.68 873.95
FPZ-12I 10/26/2015 877.63 - -8.15 869.48
FPZ-12I 7/11/2016 877.63 - - 4.91 872.72
FPZ-12I 7/12/2016 877.63 - - 4.91 872.72
FPZ-12I 7/21/2016 877.63 - - 5.49 872.14
FPZ-12I 11/29/2016 877.63 - - 8.56 869.07
FPZ-12I 12/14/2016 877.63 - - 8.62 869.01
FPZ-12I 6/26/2017 877.63 - - 4.87 872.76
FPZ-12I 12/11/2017 877.63 - - 9.53 868.10
FPZ-12I 7/9/2018 877.63 - - 7.96 869.67
FPZ-12I 12/12/2018 877.63 - - 4.38 873.25
FPZ-12I 6/10/2019 877.63 - - 4.11 873.52
FPZ-12I 12/9/2019 877.63 - - 5.37 872.26
FPZ-12I 6/11/2020 877.63 - - 3.54 874.09
FPZ-12I 12/14/2020 877.63 - - 4.89 872.74
Page 84 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-12I 6/14/2021 877.63 - - 4.44 873.19
FPZ-12I 6/20/2022 877.63 - - 6.04 871.59
FPZ-12I 7/17/2023 877.63 - - 6.98 870.65
FPZ-13 1/2/2003 880.15 - - 5.53 874.62
FPZ-13 1/9/2003 880.15 - - 6.27 873.88
FPZ-13 1/14/2003 880.15 - - 6.58 873.57
FPZ-13 1/21/2003 880.15 - - 6.85 873.30
FPZ-13 1/30/2003 880.15 - - 6.87 873.28
FPZ-13 2/6/2003 880.15 - - 6.87 873.28
FPZ-13 2/14/2003 880.15 - - 7.02 873.13
FPZ-13 2/21/2003 880.15 - - 6.76 873.39
FPZ-13 2/24/2003 880.15 - - 6.95 873.20
FPZ-13 3/20/2003 880.15 - - 4.88 875.27
FPZ-13 4/23/2003 880.15 - - 4.58 875.57
FPZ-13 5/30/2003 880.15 - - 4.38 875.77
FPZ-13 6/30/2003 880.15 - - 5.44 874.71
FPZ-13 7/29/2003 880.15 - - 6.47 873.68
FPZ-13 8/20/2003 880.15 - - 4.54 875.63
FPZ-13 11/10/2003 880.15 - - 6.26 873.91
FPZ-13 12/23/2003 880.15 - - 5.58 874.57
FPZ-13 1/29/2004 880.15 - - 6.39 873.76
FPZ-13 3/30/2004 880.15 - - 6.80 873.35
FPZ-13 4/23/2004 880.15 - - 6.39 873.76
FPZ-13 5/20/2004 880.15 - - 7.35 872.80
FPZ-13 6/28/2004 880.15 - - 8.68 871.47
FPZ-13 8/30/2004 880.15 - - 9.21 870.94
FPZ-13 1/26/2005 880.15 - - 6.97 873.18
FPZ-13 2/18/2005 880.15 - - 6.43 873.72
FPZ-13 3/29/2005 880.15 - - 5.78 874.37
FPZ-13 6/2/2006 880.15 - - 9.63 870.52
FPZ-13 6/16/2006 880.15 - - 8.70 871.45
FPZ-13 1/11/2008 880.15 - - 11.00 869.15
FPZ-13 11/5/2010 880.15 - - 9.81 870.34
FPZ-13 1/10/2014 880.15 - - 7.43 872.72
FPZ-13 1/17/2014 880.15 - - 7.21 872.94
FPZ-13 1/24/2014 880.15 - - 7.31 872.84
Page 85 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-13 1/31/2014 880.15 - - 7.31 872.84
FPZ-13 2/7/2014 880.15 - - 7.18 872.97
FPZ-13 2/14/2014 880.15 - - 6.79 873.36
FPZ-13 2/21/2014 880.15 - - 6.55 873.60
FPZ-13 2/28/2014 880.15 - - 6.77 873.38
FPZ-13 3/7/2014 880.15 - - 6.18 873.97
FPZ-13 3/14/2014 880.15 - - 6.27 873.88
FPZ-13 3/21/2014 880.15 - - 6.18 873.97
FPZ-13 3/28/2014 880.15 - - 6.26 873.89
FPZ-13 4/4/2014 880.15 - - 6.31 873.84
FPZ-13 4/11/2014 880.15 - - 6.18 873.97
FPZ-13 4/18/2014 880.15 - - 6.01 874.14
FPZ-13 4/25/2014 880.15 - - 6.57 873.58
FPZ-13 5/2/2014 880.15 - - 7.31 872.84
FPZ-13 5/9/2014 880.15 - - 8.10 872.05
FPZ-13 5/16/2014 880.15 - - 7.83 872.32
FPZ-13 5/23/2014 880.15 - - 7.23 872.92
FPZ-13 5/30/2014 880.15 - - 7.61 872.54
FPZ-13 6/6/2014 880.15 - - 7.86 872.29
FPZ-13 6/13/2014 880.15 - - 8.15 872.00
FPZ-13 6/20/2014 880.15 - - 8.49 871.66
FPZ-13 6/27/2014 880.15 - - 8.66 871.49
FPZ-13 7/5/2014 880.15 - - 9.11 871.04
FPZ-13 7/11/2014 880.15 - - 9.47 870.68
FPZ-13 3/5/2015 880.15 - -8.21 871.94
FPZ-13 5/27/2015 880.15 - -9.39 870.76
FPZ-13 6/29/2015 880.15 - -10.80 869.35
FPZ-13 7/30/2015 880.15 - -12.08 868.07
FPZ-13 8/20/2015 880.15 - - 11.87 868.28
FPZ-13 9/9/2015 880.15 - - 12.50 867.65
FPZ-13 10/15/2015 880.15 - -10.34 869.81
FPZ-13 10/26/2015 880.15 - -10.68 869.47
FPZ-13 12/4/2015 880.15 - -7.80 872.35
FPZ-13 1/12/2016 880.15 - - 6.45 873.70
FPZ-13 5/26/2016 880.15 - - 5.79 874.36
FPZ-13 7/11/2016 880.15 - - 7.48 872.67
FPZ-13 7/12/2016 880.15 - - 7.48 872.67
Page 86 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-13 7/22/2016 880.15 - - 8.30 871.85
FPZ-13 9/28/2016 880.15 - - 10.63 869.52
FPZ-13 11/29/2016 880.15 - - 11.15 869.00
FPZ-13 12/14/2016 880.15 - - 11.06 869.09
FPZ-13 5/17/2017 880.15 - - 9.37 870.78
FPZ-13 6/26/2017 880.15 - - 7.61 872.54
FPZ-13 8/8/2017 880.15 - - 10.16 869.99
FPZ-13 11/28/2017 880.15 - - 12.14 868.01
FPZ-13 12/11/2017 880.15 - - 12.18 867.97
FPZ-13 1/25/2018 880.15 - - 11.36 868.79
FPZ-13 5/21/2018 880.15 - - 9.07 871.08
FPZ-13 7/9/2018 880.15 - - 10.78 869.37
FPZ-13 8/16/2018 880.15 - - 9.49 870.66
FPZ-13 11/29/2018 880.15 - - 7.35 872.80
FPZ-13 12/12/2018 880.15 - - 6.88 873.27
FPZ-13 3/27/2019 880.15 - - 4.95 875.20
FPZ-13 5/29/2019 880.15 - - 7.06 873.09
FPZ-13 6/10/2019 880.15 - - 6.72 873.43
FPZ-13 8/6/2019 880.15 - - 7.56 872.59
FPZ-13 11/8/2019 880.15 - - 8.93 871.22
FPZ-13 12/9/2019 880.15 - - 7.94 872.21
FPZ-13 3/6/2020 880.15 - - 4.83 875.32
FPZ-13 6/11/2020 880.15 - - 5.85 874.30
FPZ-13 8/24/2020 880.15 - - 7.87 872.28
FPZ-13 11/30/2020 880.15 - - 5.86 874.29
FPZ-13 12/14/2020 880.15 - - 7.28 872.87
FPZ-13 3/29/2021 880.15 - - 4.24 875.91
FPZ-13 6/14/2021 880.15 - - 6.25 873.90
FPZ-13 9/28/2021 880.15 - - 9.75 870.40
FPZ-13 12/28/2021 880.15 - - 10.55 869.60
FPZ-13 4/1/2022 880.15 - - 7.09 873.06
FPZ-13 6/20/2022 880.15 - - 7.27 872.88
FPZ-13 9/22/2022 880.15 - - 10.94 869.21
FPZ-13 12/5/2022 880.15 - - 9.69 870.46
FPZ-13 4/10/2023 880.15 - - 6.05 874.10
FPZ-13 7/17/2023 880.15 - - 8.95 871.20
FPZ-13 9/18/2023 880.15 - - 9.79 870.36
Page 87 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-13 12/6/2023 880.15 - - 11.73 868.42
FPZ-13 3/1/2024 880.15 - - 8.31 871.84
FPZ-14 1/2/2003 879.87 - - 5.81 874.06
FPZ-14 1/9/2003 879.87 - - 5.81 874.06
FPZ-14 1/14/2003 879.87 - - 6.16 873.71
FPZ-14 1/21/2003 879.87 - - 6.32 873.55
FPZ-14 1/30/2003 879.87 - - 6.10 873.77
FPZ-14 2/6/2003 879.87 - - 6.09 873.78
FPZ-14 2/14/2003 879.87 - - 6.25 873.62
FPZ-14 2/21/2003 879.87 - - 6.11 873.76
FPZ-14 2/24/2003 879.87 - - 6.21 873.66
FPZ-14 3/20/2003 879.87 - - 4.34 875.53
FPZ-14 4/23/2003 879.87 - - 4.02 875.85
FPZ-14 5/30/2003 879.87 - - 3.81 876.06
FPZ-14 6/30/2003 879.87 - - 4.85 875.02
FPZ-14 7/29/2003 879.87 - - 5.82 874.05
FPZ-14 8/20/2003 879.87 - - 3.98 875.93
FPZ-14 11/10/2003 879.87 - - 5.58 874.33
FPZ-14 12/23/2003 879.87 - - 5.04 874.83
FPZ-14 1/29/2004 879.87 - - 5.86 874.01
FPZ-14 3/30/2004 879.87 - - 5.56 874.31
FPZ-14 4/23/2004 879.87 - - 5.90 873.97
FPZ-14 5/20/2004 879.87 - - 6.85 873.02
FPZ-14 6/28/2004 879.87 - - 8.17 871.70
FPZ-14 8/30/2004 879.87 - - 8.73 871.14
FPZ-14 1/26/2005 879.87 - - 6.53 873.34
FPZ-14 2/18/2005 879.87 - - 5.97 873.90
FPZ-14 3/29/2005 879.87 - - 5.27 874.60
FPZ-14 6/2/2006 879.87 - - 9.18 870.69
FPZ-14 6/16/2006 879.87 - - 8.08 871.79
FPZ-14 1/11/2008 879.87 - - 10.43 869.44
FPZ-14 11/5/2010 879.87 - - 8.96 870.95
FPZ-14 1/10/2014 879.87 - - 6.43 873.44
FPZ-14 1/17/2014 879.87 - - 6.17 873.70
FPZ-14 1/24/2014 879.87 - - 6.33 873.54
FPZ-14 1/31/2014 879.87 - - 6.61 873.26
Page 88 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-14 2/7/2014 879.87 - - 6.49 873.38
FPZ-14 2/14/2014 879.87 - - 5.78 874.09
FPZ-14 2/21/2014 879.87 - - 5.69 874.18
FPZ-14 2/28/2014 879.87 - - 6.04 873.83
FPZ-14 3/7/2014 879.87 - - 5.31 874.56
FPZ-14 3/14/2014 879.87 - - 5.38 874.49
FPZ-14 3/21/2014 879.87 - - 5.31 874.56
FPZ-14 3/28/2014 879.87 - - 5.39 874.48
FPZ-14 4/4/2014 879.87 - - 5.48 874.39
FPZ-14 4/11/2014 879.87 - - 5.13 874.74
FPZ-14 4/18/2014 879.87 - - 4.89 874.98
FPZ-14 4/25/2014 879.87 - - 5.31 874.56
FPZ-14 5/2/2014 879.87 - - 5.78 874.09
FPZ-14 5/9/2014 879.87 - - 6.05 873.82
FPZ-14 5/16/2014 879.87 - - 5.71 874.16
FPZ-14 5/23/2014 879.87 - - 6.18 873.69
FPZ-14 5/30/2014 879.87 - - 6.49 873.38
FPZ-14 6/6/2014 879.87 - - 6.84 873.03
FPZ-14 6/13/2014 879.87 - - 7.19 872.68
FPZ-14 6/20/2014 879.87 - - 7.51 872.36
FPZ-14 6/27/2014 879.87 - - 7.73 872.14
FPZ-14 7/5/2014 879.87 - - 8.19 871.68
FPZ-14 7/11/2014 879.87 - - 8.61 871.26
FPZ-14 3/5/2015 879.87 - -7.38 872.49
FPZ-14 5/27/2015 879.87 - -8.48 871.39
FPZ-14 6/29/2015 879.87 - -10.30 869.57
FPZ-14 7/30/2015 879.87 - -11.55 868.32
FPZ-14 8/20/2015 879.87 - -11.39 868.48
FPZ-14 9/9/2015 879.87 - -12.08 867.79
FPZ-14 10/15/2015 879.87 - -9.15 870.72
FPZ-14 10/26/2015 879.87 - -10.31 869.56
FPZ-14 12/4/2015 879.87 - -7.22 872.65
FPZ-14 1/12/2016 879.87 - - 5.98 873.89
FPZ-14 5/26/2016 879.87 - - 5.28 874.59
FPZ-14 7/11/2016 879.87 - - 7.00 872.87
FPZ-14 7/12/2016 879.87 - - 7.00 872.87
FPZ-14 7/22/2016 879.87 - - 7.75 872.12
Page 89 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-14 9/28/2016 879.87 - - 10.12 869.75
FPZ-14 11/29/2016 879.87 - - 11.76 868.11
FPZ-14 12/14/2016 879.87 - - 10.69 869.18
FPZ-14 5/17/2017 879.87 - - 8.96 870.91
FPZ-14 6/26/2017 879.87 - - 7.01 872.86
FPZ-14 8/8/2017 879.87 - - 9.59 870.28
FPZ-14 11/28/2017 879.87 - - 11.75 868.12
FPZ-14 12/11/2017 879.87 - - 11.82 868.05
FPZ-14 1/25/2018 879.87 - - 10.88 868.99
FPZ-14 5/21/2018 879.87 - - 8.64 871.23
FPZ-14 7/9/2018 879.87 - - 10.23 869.64
FPZ-14 8/16/2018 879.87 - - 9.01 870.86
FPZ-14 11/29/2018 879.87 - - 6.83 873.04
FPZ-14 12/12/2018 879.87 - - 6.31 873.56
FPZ-14 3/27/2019 879.87 - - 4.43 875.44
FPZ-14 5/29/2019 879.87 - - 6.53 873.34
FPZ-14 6/10/2019 879.87 - - 6.08 873.79
FPZ-14 8/6/2019 879.87 - - 6.98 872.89
FPZ-14 11/8/2019 879.87 - - 8.46 871.41
FPZ-14 12/9/2019 879.87 - - 7.48 872.39
FPZ-14 3/6/2020 879.87 - - 4.39 875.48
FPZ-14 6/11/2020 879.87 - - 5.33 874.54
FPZ-14 8/24/2020 879.87 - - 7.39 872.48
FPZ-14 11/30/2020 879.87 - - 5.13 874.74
FPZ-14 12/14/2020 879.87 - - 7.01 872.86
FPZ-14 3/29/2021 879.87 - - 3.87 876.00
FPZ-14 6/14/2021 879.87 - - 4.33 875.54
FPZ-14 9/28/2021 879.87 - - 9.11 870.76
FPZ-14 12/28/2021 879.87 - - 10.16 869.71
FPZ-14 4/1/2022 879.87 - - 6.62 873.25
FPZ-14 6/20/2022 879.87 - - 5.94 873.93
FPZ-14 9/22/2022 879.87 - - 10.50 869.37
FPZ-14 12/5/2022 879.87 - - 9.20 870.67
FPZ-14 4/10/2023 879.87 - - 5.57 874.30
FPZ-14 7/17/2023 879.87 - - 8.46 871.41
FPZ-14 9/18/2023 879.87 - - 10.34 869.53
FPZ-14 12/6/2023 879.87 - - 11.34 868.53
Page 90 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-14 3/1/2024 879.87 - - 7.88 871.99
FPZ-15 1/2/2003 881.16 5.66 0.04 5.70 875.49
FPZ-15 1/9/2003 881.16 7.13 0.02 7.15 874.03
FPZ-15 1/14/2003 881.16 - - 7.52 873.64
FPZ-15 1/21/2003 881.16 - - 7.69 873.47
FPZ-15 1/30/2003 881.16 - - 6.12 875.04
FPZ-15 2/6/2003 881.16 - - 7.50 873.66
FPZ-15 2/14/2003 881.16 - - 7.26 873.90
FPZ-15 2/21/2003 881.16 - - 6.54 874.62
FPZ-15 2/24/2003 881.16 - - 6.84 874.32
FPZ-15 3/20/2003 881.16 - - 5.57 875.59
FPZ-15 4/23/2003 881.16 - - 5.42 875.74
FPZ-15 5/30/2003 881.16 - - 5.23 875.93
FPZ-15 6/30/2003 881.16 - - 6.48 874.68
FPZ-15 7/29/2003 881.16 7.42 0.02 7.44 873.74
FPZ-15 8/20/2003 881.16 - - 5.20 876.01
FPZ-15 11/10/2003 881.16 - - 6.93 874.28
FPZ-15 12/23/2003 881.16 6.73 0.03 6.76 874.42
FPZ-15 1/29/2004 881.16 7.25 0.08 7.33 873.89
FPZ-15 3/30/2004 881.16 - - 6.88 874.28
FPZ-15 4/23/2004 881.16 - - 7.23 873.93
FPZ-15 5/20/2004 881.16 8.82 0.10 8.92 872.32
FPZ-15 6/28/2004 881.16 - - 9.81 871.35
FPZ-15 8/30/2004 881.16 10.11 0.07 10.18 871.03
FPZ-15 1/26/2005 881.16 - - 7.87 873.29
FPZ-15 2/18/2005 881.16 - - 7.30 873.86
FPZ-15 3/29/2005 881.16 - - 6.93 874.23
FPZ-15 6/2/2006 881.16 - - 10.53 870.63
FPZ-15 6/16/2006 881.16 - - 9.57 871.59
FPZ-15 1/11/2008 881.16 - - 12.23 868.93
FPZ-15 11/5/2010 881.16 10.92 0.02 10.94 870.24
FPZ-15 1/10/2014 881.16 - - 8.69 872.47
FPZ-15 1/17/2014 881.16 - - 8.54 872.62
FPZ-15 1/24/2014 881.16 - - 8.63 872.53
FPZ-15 1/31/2014 881.16 - - 8.79 872.37
FPZ-15 2/7/2014 881.16 - - 8.53 872.63
Page 91 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-15 2/14/2014 881.16 - - 8.01 873.15
FPZ-15 2/21/2014 881.16 - - 7.72 873.44
FPZ-15 2/28/2014 881.16 - - 8.06 873.10
FPZ-15 3/7/2014 881.16 - - 7.18 873.98
FPZ-15 3/14/2014 881.16 - - 7.31 873.85
FPZ-15 3/21/2014 881.16 - - 7.18 873.98
FPZ-15 3/28/2014 881.16 - - 7.28 873.88
FPZ-15 4/4/2014 881.16 - - 7.39 873.77
FPZ-15 4/11/2014 881.16 - - 7.11 874.05
FPZ-15 4/18/2014 881.16 - - 6.73 874.43
FPZ-15 4/25/2014 881.16 - - 6.89 874.27
FPZ-15 5/2/2014 881.16 - - 7.01 874.15
FPZ-15 5/9/2014 881.16 - - 7.15 874.01
FPZ-15 5/16/2014 881.16 - - 6.57 874.59
FPZ-15 5/23/2014 881.16 - - 8.61 872.55
FPZ-15 5/30/2014 881.16 - - 9.27 871.89
FPZ-15 6/6/2014 881.16 - - 9.56 871.60
FPZ-15 6/13/2014 881.16 - - 9.87 871.29
FPZ-15 6/20/2014 881.16 - - 10.11 871.05
FPZ-15 6/27/2014 881.16 - - 10.45 870.71
FPZ-15 7/5/2014 881.16 - - 10.63 870.53
FPZ-15 7/11/2014 881.16 - - 10.81 870.35
FPZ-15 3/5/2015 881.16 - -8.90 872.26
FPZ-15 5/27/2015 881.16 - -10.75 870.41
FPZ-15 6/29/2015 881.16 - -11.71 869.45
FPZ-15 7/30/2015 881.16 12.92 0.18 13.10 868.20
FPZ-15 8/20/2015 881.16 12.82 0.04 12.86 868.33
FPZ-15 9/9/2015 881.16 13.35 0.50 13.85 867.69
FPZ-15 10/15/2015 881.16 11.25 0.05 11.30 869.90
FPZ-15 10/26/2015 881.16 11.80 0.01 11.81 869.36
FPZ-15 12/1/2015 881.16 - - 8.05 873.11
FPZ-15 12/2/2015 881.16 8.43 0.02 8.45 872.72
FPZ-15 12/3/2015 881.16 - - 8.55 872.61
FPZ-15 12/4/2015 881.16 - - 8.63 872.53
FPZ-15 12/10/2015 881.16 - - 8.59 872.57
FPZ-15 12/28/2015 881.16 - - 7.69 873.47
FPZ-15 1/12/2016 881.16 - - 7.31 873.85
Page 92 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-15 5/26/2016 881.16 - - 6.59 874.57
FPZ-15 7/11/2016 881.16 - - 8.34 872.82
FPZ-15 7/12/2016 881.16 - - 8.34 872.82
FPZ-15 8/3/2016 881.16 - - 9.85 871.31
FPZ-15 9/28/2016 881.16 - - 11.52 869.64
FPZ-15 11/29/2016 881.16 - - 12.15 869.01
FPZ-15 12/28/2016 881.16 - - 12.30 868.86
FPZ-15 5/17/2017 881.16 - - 10.49 870.67
FPZ-15 6/26/2017 881.16 - - 8.60 872.56
FPZ-15 8/8/2017 881.16 - - 11.15 870.01
FPZ-15 11/28/2017 881.16 13.09 0.02 13.11 868.07
FPZ-15 12/11/2017 881.16 - - 13.03 868.13
FPZ-15 1/25/2018 881.16 - - 12.31 868.85
FPZ-15 5/21/2018 881.16 - - 9.97 871.19
FPZ-15 7/9/2018 881.16 - - 11.65 869.51
FPZ-15 8/16/2018 881.16 - - 10.40 870.76
FPZ-15 11/29/2018 881.16 - - 8.31 872.85
FPZ-15 12/12/2018 881.16 - - 7.90 873.26
FPZ-15 3/27/2019 881.16 - - 5.77 875.39
FPZ-15 5/29/2019 881.16 - - 8.89 872.27
FPZ-15 6/10/2019 881.16 - - 17.48 863.68
FPZ-15 8/6/2019 881.16 - - 8.44 872.72
FPZ-15 11/8/2019 881.16 - - 9.93 871.23
FPZ-15 12/9/2019 881.16 - - 8.88 872.28
FPZ-15 3/6/2020 881.16 - - 5.71 875.45
FPZ-15 6/11/2020 881.16 - - 6.62 874.54
FPZ-15 8/24/2020 881.16 - - 8.79 872.37
FPZ-15 11/30/2020 881.16 - - 7.03 874.13
FPZ-15 12/14/2020 881.16 - - 8.11 873.05
FPZ-15 3/29/2021 881.16 - - 5.16 876.00
FPZ-15 6/14/2021 881.16 - - 6.73 874.43
FPZ-15 9/28/2021 881.16 - - 10.49 870.67
FPZ-15 12/28/2021 881.16 - - 11.48 869.68
FPZ-15 4/1/2022 881.16 - - 8.06 873.10
FPZ-15 6/20/2022 881.16 - - 8.03 873.13
FPZ-15 9/22/2022 881.16 - - 10.88 870.28
FPZ-15 12/5/2022 881.16 - - 10.62 870.54
Page 93 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
FPZ-15 4/10/2023 881.16 - - 6.92 874.24
FPZ-15 7/17/2023 881.16 - - 9.83 871.33
FPZ-15 9/18/2023 881.16 - - 11.24 869.92
FPZ-15 12/6/2023 881.16 - - 12.69 868.47
FPZ-15 3/1/2024 881.16 - - 9.23 871.93
OW-1 7/25/1997 883.49 - - 10.27 873.22
OW-1 8/24/1997 883.49 - - 10.56 872.93
OW-1 9/14/1997 883.49 - - 10.34 873.15
OW-1 10/3/1997 883.49 - - 9.93 873.56
OW-1 11/14/1997 883.49 - - 7.42 876.07
OW-1 12/31/1997 883.49 - - 5.63 877.86
OW-1 1/23/1998 883.49 - - 5.15 878.34
OW-1 2/17/1998 883.49 - - 4.90 878.59
OW-1 3/6/1998 883.49 6.73 0.01 6.74 876.76
OW-1 4/28/1998 883.49 - - 5.61 877.88
OW-1 12/26/1998 883.49 - - 6.53 876.96
OW-1 8/26/1999 883.49 - - 7.30 876.19
OW-1 9/22/1999 883.49 - - 8.74 874.75
OW-1 10/7/1999 883.49 - - 8.74 874.75
OW-1 4/24/2002 883.49 8.70 0.79 9.49 874.59
OW-1 10/18/2002 883.49 - - 6.61 876.88
OW-1 1/30/2003 883.49 - - 5.41 878.08
OW-1 2/6/2003 883.49 - - 6.54 876.95
OW-1 2/14/2003 883.49 - - 7.34 876.15
OW-1 2/21/2003 883.49 - - 6.89 876.60
OW-1 2/24/2003 883.49 - - 7.05 876.44
OW-1 3/20/2003 883.49 - - 5.80 877.69
OW-1 4/23/2003 883.49 - - 5.57 877.92
OW-1 5/30/2003 883.49 - - 5.50 877.99
OW-1 6/30/2003 883.49 - - 6.40 877.09
OW-1 7/29/2003 883.49 - - 7.53 875.96
OW-1 8/20/2003 883.49 - - 5.91 877.56
OW-1 11/10/2003 883.49 - - 7.20 876.27
OW-1 12/23/2003 883.49 - - 6.27 877.22
OW-1 1/29/2004 883.49 - - 5.72 877.77
OW-1 3/30/2004 883.49 - - 7.53 875.96
Page 94 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-1 4/23/2004 883.49 - - 7.64 875.85
OW-1 5/20/2004 883.49 - - 8.75 874.74
OW-1 6/28/2004 883.49 - - 9.78 873.71
OW-1 8/30/2004 883.49 - - 11.03 872.46
OW-1 1/26/2005 883.49 - - 8.79 874.70
OW-1 2/18/2005 883.49 - - 7.05 876.44
OW-1 3/29/2005 883.49 - - 5.51 877.98
OW-1 6/2/2006 883.49 - - 10.64 872.85
OW-1 6/16/2006 883.49 - - 6.47 877.02
OW-1 1/11/2008 883.49 - - 11.20 872.29
OW-1 11/5/2010 883.49 - - 10.88 872.59
OW-1 1/10/2014 883.49 - - 6.18 877.31
OW-1 1/17/2014 883.49 - - 5.97 877.52
OW-1 1/24/2014 883.49 - - 7.21 876.28
OW-1 1/31/2014 883.49 - - 8.57 874.92
OW-1 2/7/2014 883.49 - - 7.89 875.60
OW-1 2/14/2014 883.49 - - 6.48 877.01
OW-1 2/21/2014 883.49 - - 5.91 877.58
OW-1 2/28/2014 883.49 - - 7.71 875.78
OW-1 3/7/2014 883.49 - - 5.21 878.28
OW-1 3/14/2014 883.49 - - 5.31 878.18
OW-1 3/21/2014 883.49 - - 5.21 878.28
OW-1 3/28/2014 883.49 - - 6.01 877.48
OW-1 4/4/2014 883.49 - - 6.99 876.50
OW-1 4/11/2014 883.49 - - 6.38 877.11
OW-1 4/18/2014 883.49 - - 5.98 877.51
OW-1 4/25/2014 883.49 - - 6.11 877.38
OW-1 5/2/2014 883.49 - - 6.48 877.01
OW-1 5/9/2014 883.49 - - 6.78 876.71
OW-1 5/16/2014 883.49 - - 6.45 877.04
OW-1 5/23/2014 883.49 - - 7.77 875.72
OW-1 5/30/2014 883.49 - - 7.87 875.62
OW-1 6/6/2014 883.49 - - 7.99 875.50
OW-1 6/13/2014 883.49 - - 8.34 875.15
OW-1 6/20/2014 883.49 - - 8.91 874.58
OW-1 6/27/2014 883.49 - - 9.22 874.27
OW-1 7/5/2014 883.49 - - 9.79 873.70
Page 95 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-1 7/11/2014 883.49 - - 10.21 873.28
OW-1 3/5/2015 883.49 - - 6.91 876.58
OW-1 5/27/2015 883.49 - -10.16 873.33
OW-1 6/29/2015 883.49 - -11.15 872.34
OW-1 7/30/2015 883.49 - -13.05 870.44
OW-1 8/20/2015 883.49 - -20.11 863.38
OW-1 9/9/2015 883.49 - -14.05 869.44
OW-1 10/15/2015 883.49 - -10.92 872.57
OW-1 10/26/2015 883.49 - -12.21 871.28
OW-1 12/4/2015 883.49 - -6.27 877.22
OW-1 1/12/2016 883.49 - - 7.02 876.47
OW-1 5/26/2016 883.49 - - 6.21 877.28
OW-1 7/11/2016 883.49 - - 8.59 874.90
OW-1 7/12/2016 883.49 - - 8.59 874.90
OW-1 8/3/2016 883.49 - - 9.64 873.85
OW-1 9/28/2016 883.49 - - 10.09 873.40
OW-1 11/29/2016 883.49 - - 13.01 870.48
OW-1 12/14/2016 883.49 - - 20.80 862.69
OW-1 5/17/2017 883.49 - - 10.40 873.09
OW-1 6/26/2017 883.49 - - 6.81 876.68
OW-1 8/8/2017 883.49 - - 9.51 873.98
OW-1 11/28/2017 883.49 - - 13.67 869.82
OW-1 12/11/2017 883.49 - - 10.36 873.13
OW-1 1/25/2018 883.49 - - 7.95 875.54
OW-1 5/21/2018 883.49 - - 9.60 873.89
OW-1 7/9/2018 883.49 - - 10.92 872.57
OW-1 8/16/2018 883.49 - - 10.03 873.46
OW-1 11/29/2018 883.49 - - 7.01 876.48
OW-1 12/12/2018 883.49 - - 5.68 877.81
OW-1 3/27/2019 883.49 - - 5.71 877.78
OW-1 5/29/2019 883.49 - - 7.84 875.65
OW-1 6/10/2019 883.49 - - 6.49 877.00
OW-1 8/6/2019 883.49 - - 7.45 876.04
OW-1 11/8/2019 883.49 - - 8.40 875.09
OW-1 12/9/2019 883.49 - - 8.45 875.04
OW-1 3/6/2020 883.49 - - 5.87 877.62
OW-1 6/11/2020 883.49 - - 6.49 877.00
Page 96 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-1 8/24/2020 883.49 - - 8.63 874.86
OW-1 11/30/2020 883.49 - - 5.90 877.59
OW-1 12/14/2020 883.49 - - 5.39 878.10
OW-1 3/29/2021 883.49 - - 5.06 878.43
OW-1 6/14/2021 883.49 - - 7.55 875.94
OW-1 9/28/2021 883.49 - - 10.87 872.62
OW-1 12/28/2021 883.49 - - 12.03 871.46
OW-1 4/1/2022 883.49 - - 8.66 874.83
OW-1 6/20/2022 883.49 - - 9.99 873.50
OW-1 9/22/2022 883.49 - - 12.56 870.93
OW-1 12/5/2022 883.49 - - 9.98 873.51
OW-1 4/10/2023 883.49 - - 5.40 878.09
OW-1 7/17/2023 883.49 - - 10.13 873.36
OW-1 9/18/2023 883.49 - - 10.97 872.52
OW-1 12/6/2023 883.49 - - 10.61 872.88
OW-1 3/1/2024 883.49 - - 9.48 874.01
OW-2 7/25/1997 879.64 - - 6.86 872.78
OW-2 8/24/1997 879.64 - - 8.45 871.19
OW-2 9/14/1997 879.64 - - 8.66 870.98
OW-2 10/3/1997 879.64 - - 9.05 870.59
OW-2 11/14/1997 879.64 - - 8.87 870.77
OW-2 12/31/1997 879.64 - - 8.18 871.46
OW-2 1/23/1998 879.64 3.56 0.06 3.62 876.07
OW-2 2/17/1998 879.64 3.29 0.12 3.41 876.32
OW-2 3/6/1998 879.64 4.72 0.14 4.86 874.89
OW-2 4/28/1998 879.64 - - 4.50 875.14
OW-2 12/26/1998 879.64 7.76 0.08 7.84 871.86
OW-2 8/26/1999 879.64 8.98 0.07 9.05 870.64
OW-2 9/22/1999 879.64 6.70 0.05 6.75 872.93
OW-2 10/7/1999 879.64 6.70 0.05 6.75 872.93
OW-2 9/27/2002 879.64 10.65 0.14 10.79 868.96
OW-2 10/3/2002 879.64 10.12 0.07 10.19 869.50
OW-2 10/18/2002 879.64 7.93 0.72 8.65 871.53
OW-2 10/30/2002 879.64 5.57 0.54 6.11 873.94
OW-2 12/4/2002 879.64 7.56 0.54 8.10 871.95
OW-2 12/11/2002 879.64 3.33 0.45 3.78 876.20
Page 97 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-2 12/16/2002 879.64 5.44 0.47 5.91 874.08
OW-2 1/2/2003 879.64 4.35 0.20 4.55 875.24
OW-2 1/9/2003 879.64 5.24 0.19 5.43 874.35
OW-2 1/14/2003 879.64 5.65 0.25 5.90 873.93
OW-2 1/21/2003 879.64 5.88 0.28 6.16 873.69
OW-2 1/30/2003 879.64 3.58 0.27 3.85 875.99
OW-2 2/6/2003 879.64 5.21 0.07 5.28 874.41
OW-2 2/14/2003 879.64 5.33 0.08 5.41 874.29
OW-2 2/21/2003 879.64 5.01 0.09 5.10 874.61
OW-2 2/24/2003 879.64 5.14 0.06 5.20 874.49
OW-2 3/20/2003 879.64 3.78 0.01 3.79 875.86
OW-2 4/23/2003 879.64 - - 3.45 876.16
OW-2 5/30/2003 879.64 - - 3.31 876.30
OW-2 6/30/2003 879.64 - - 4.13 875.48
OW-2 7/29/2003 879.64 5.09 0.01 5.10 874.55
OW-2 8/20/2003 879.64 3.33 0.01 3.34 876.31
OW-2 11/10/2003 879.64 - - 5.15 874.47
OW-2 12/23/2003 879.64 - - 4.66 874.95
OW-2 1/29/2004 879.64 - - 5.03 874.58
OW-2 3/30/2004 879.64 - - 5.15 874.46
OW-2 4/23/2004 879.64 - - 5.33 874.28
OW-2 5/20/2004 879.64 - - 6.35 873.26
OW-2 6/28/2004 879.64 - - 7.67 871.94
OW-2 8/30/2004 879.64 - - 8.25 871.36
OW-2 1/26/2005 879.64 - - 6.15 873.46
OW-2 2/18/2005 879.64 - - 5.31 874.30
OW-2 3/29/2005 879.64 - - 4.21 875.40
OW-2 6/2/2006 879.64 - - 8.70 870.91
OW-2 6/16/2006 879.64 - - 6.49 873.12
OW-2 6/30/2006 879.64 - - 6.00 873.61
OW-2 7/5/2006 879.64 - - 6.97 872.64
OW-2 7/13/2006 879.64 - - 7.20 872.41
OW-2 7/19/2006 879.64 - - 7.55 872.06
OW-2 7/28/2006 879.64 - - 6.97 872.64
OW-2 7/31/2006 879.64 - - 9.25 870.36
OW-2 8/15/2006 879.64 - - 8.20 871.41
OW-2 8/24/2006 879.64 - - 7.77 871.84
Page 98 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-2 8/30/2006 879.64 - - 8.21 871.40
OW-2 9/6/2006 879.64 - - 5.18 874.43
OW-2 9/14/2006 879.64 - - 3.55 876.06
OW-2 9/22/2006 879.64 - - 6.18 873.43
OW-2 9/28/2006 879.64 - - 6.55 873.06
OW-2 10/9/2006 879.64 - - 6.68 872.93
OW-2 10/12/2006 879.64 - - 6.76 872.85
OW-2 10/20/2006 879.64 - - 5.46 874.15
OW-2 10/27/2006 879.64 - - 6.58 873.03
OW-2 11/1/2006 879.64 - - 6.02 873.59
OW-2 11/10/2006 879.64 - - 6.42 873.19
OW-2 11/15/2006 879.64 - - 5.61 874.00
OW-2 11/20/2006 879.64 - - 5.52 874.09
OW-2 11/30/2006 879.64 - - 5.55 874.06
OW-2 12/4/2006 879.64 - - 5.74 873.87
OW-2 12/15/2006 879.64 - - 6.18 873.43
OW-2 12/18/2006 879.64 - - 6.30 873.31
OW-2 12/29/2006 879.64 - - 5.53 874.08
OW-2 1/2/2007 879.64 - - 4.48 875.13
OW-2 1/10/2007 879.64 - - 4.64 874.97
OW-2 1/19/2007 879.64 - - 5.47 874.14
OW-2 1/26/2007 879.64 - - 5.05 874.56
OW-2 2/8/2007 879.64 - - 5.84 873.77
OW-2 2/21/2007 879.64 - - 5.61 874.00
OW-2 3/2/2007 879.64 - - 3.36 876.25
OW-2 3/8/2007 879.64 - - 5.34 874.27
OW-2 3/15/2007 879.64 - - 5.68 873.93
OW-2 3/22/2007 879.64 - - 5.29 874.32
OW-2 3/27/2007 879.64 - - 5.57 874.04
OW-2 4/5/2007 879.64 - - 5.82 873.79
OW-2 4/12/2007 879.64 - - 3.38 876.23
OW-2 4/19/2007 879.64 - - 4.82 874.79
OW-2 4/26/2007 879.64 - - 7.77 871.84
OW-2 5/4/2007 879.64 - - 5.91 873.70
OW-2 5/10/2007 879.64 - - 8.91 870.70
OW-2 5/23/2007 879.64 - - 7.22 872.39
OW-2 5/31/2007 879.64 - - 7.22 872.39
Page 99 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-2 6/8/2007 879.64 - - 7.80 871.81
OW-2 6/14/2007 879.64 - - 7.74 871.87
OW-2 6/21/2007 879.64 - - 8.03 871.58
OW-2 6/28/2007 879.64 - - 8.41 871.20
OW-2 7/5/2007 879.64 - - 8.79 870.82
OW-2 7/12/2007 879.64 - - 9.09 870.52
OW-2 7/19/2007 879.64 - - 9.41 870.20
OW-2 7/26/2007 879.64 - - 9.68 869.93
OW-2 8/3/2007 879.64 - - 9.95 869.66
OW-2 8/9/2007 879.64 - - 10.19 869.42
OW-2 8/15/2007 879.64 - - 10.51 869.10
OW-2 8/22/2007 879.64 - - 10.86 868.75
OW-2 8/31/2007 879.64 - - 11.17 868.44
OW-2 9/7/2007 879.64 - - 11.42 868.19
OW-2 9/13/2007 879.64 - - 11.63 867.98
OW-2 9/21/2007 879.64 - - 11.66 867.95
OW-2 9/26/2007 879.64 - - 11.93 867.68
OW-2 10/5/2007 879.64 - - 12.03 867.58
OW-2 10/12/2007 879.64 - - 12.22 867.39
OW-2 10/19/2007 879.64 - - 12.36 867.25
OW-2 10/26/2007 879.64 - - 6.42 873.22
OW-2 11/2/2007 879.64 - - 10.07 869.57
OW-2 11/9/2007 879.64 - - 10.67 868.97
OW-2 11/17/2007 879.64 - - 10.89 868.75
OW-2 11/30/2007 879.64 - - 11.15 868.49
OW-2 12/8/2007 879.64 - - 11.30 868.34
OW-2 12/17/2007 879.64 - - 11.23 868.41
OW-2 12/21/2007 879.64 - - 11.30 868.34
OW-2 12/27/2007 879.64 - - 9.56 870.08
OW-2 1/4/2008 879.64 - - 9.07 870.57
OW-2 1/11/2008 879.64 - - 9.81 869.80
OW-2 1/18/2008 879.64 - - 8.66 870.98
OW-2 1/26/2008 879.64 - - 9.63 870.01
OW-2 2/8/2008 879.64 - - 8.57 871.07
OW-2 2/22/2008 879.64 - - 8.93 870.71
OW-2 3/1/2008 879.64 - - 8.78 870.86
OW-2 3/10/2008 879.64 - - 7.15 872.49
Page 100 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-2 3/14/2008 879.64 - - 7.90 871.74
OW-2 3/28/2008 879.64 - - 8.04 871.60
OW-2 4/18/2008 879.64 - - 7.27 872.37
OW-2 4/30/2008 879.64 - - 5.42 874.22
OW-2 5/2/2008 879.64 - - 5.98 873.66
OW-2 5/9/2008 879.64 - - 6.74 872.90
OW-2 5/16/2008 879.64 - - 7.15 872.49
OW-2 5/24/2008 879.64 - - 7.47 872.17
OW-2 6/6/2008 879.64 - - 8.04 871.60
OW-2 6/13/2008 879.64 - - 8.45 871.19
OW-2 6/20/2008 879.64 - - 8.84 870.80
OW-2 6/27/2008 879.64 - - 9.17 870.47
OW-2 7/11/2008 879.64 - - 9.33 870.31
OW-2 7/18/2008 879.64 - - 9.65 869.99
OW-2 7/25/2008 879.64 - - 9.99 869.65
OW-2 8/1/2008 879.64 - - 10.37 869.27
OW-2 8/8/2008 879.64 - - 10.75 868.89
OW-2 8/15/2008 879.64 - - 11.15 868.49
OW-2 8/22/2008 879.64 - - 11.05 868.59
OW-2 9/5/2008 879.64 - - 10.12 869.52
OW-2 9/12/2008 879.64 - - 9.49 870.15
OW-2 9/19/2008 879.64 - - 8.08 871.56
OW-2 10/10/2008 879.64 - - 9.23 870.41
OW-2 11/7/2008 879.64 - - 9.57 870.07
OW-2 11/14/2008 879.64 - - 9.66 869.98
OW-2 11/21/2008 879.64 - - 9.44 870.20
OW-2 12/5/2008 879.64 - - 9.26 870.38
OW-2 12/12/2008 879.64 - - 9.19 870.45
OW-2 1/2/2009 879.64 - - 9.23 870.41
OW-2 1/9/2009 879.64 - - 9.19 870.45
OW-2 1/23/2009 879.64 - - 9.15 870.49
OW-2 2/13/2009 879.64 - - 9.22 870.42
OW-2 2/27/2009 879.64 - - 9.19 870.45
OW-2 3/6/2009 879.64 - - 9.32 870.32
OW-2 3/30/2009 879.64 - - 4.70 874.94
OW-2 4/30/2009 879.64 - - 6.60 873.04
OW-2 5/15/2009 879.64 - - 6.10 873.54
Page 101 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-2 5/22/2009 879.64 - - 6.06 873.58
OW-2 5/29/2009 879.64 - - 6.52 873.12
OW-2 6/6/2009 879.64 - - 4.08 875.56
OW-2 6/12/2009 879.64 - - 5.09 874.55
OW-2 6/22/2009 879.64 - - 5.67 873.97
OW-2 6/27/2009 879.64 - - 6.09 873.55
OW-2 7/6/2009 879.64 - - 6.77 872.87
OW-2 7/10/2009 879.64 - - 7.07 872.57
OW-2 7/17/2009 879.64 - - 7.57 872.07
OW-2 7/24/2009 879.64 - - 7.96 871.68
OW-2 7/31/2009 879.64 - - 8.21 871.43
OW-2 8/6/2009 879.64 - - 8.57 871.07
OW-2 8/14/2009 879.64 - - 8.92 870.72
OW-2 8/21/2009 879.64 - - 9.22 870.42
OW-2 8/28/2009 879.64 - - 9.38 870.26
OW-2 9/4/2009 879.64 - - 9.54 870.10
OW-2 9/11/2009 879.64 - - 10.69 868.95
OW-2 9/25/2009 879.64 - - 9.89 869.75
OW-2 10/2/2009 879.64 - - 9.68 869.96
OW-2 10/9/2009 879.64 - - 9.57 870.07
OW-2 10/16/2009 879.64 - - 9.74 869.90
OW-2 10/23/2009 879.64 - - 9.82 869.82
OW-2 11/6/2009 879.64 - - 7.85 871.79
OW-2 11/13/2009 879.64 - - 7.91 871.73
OW-2 11/20/2009 879.64 - - 7.83 871.81
OW-2 12/4/2009 879.64 - - 8.09 871.55
OW-2 12/11/2009 879.64 - - 8.16 871.48
OW-2 12/17/2009 879.64 - - 8.16 871.48
OW-2 1/7/2010 879.64 - - 5.36 874.28
OW-2 1/7/2010 879.64 - - 5.29 874.35
OW-2 1/22/2010 879.64 - - 5.28 874.36
OW-2 1/28/2010 879.64 - - 5.19 874.45
OW-2 2/4/2010 879.64 - - 4.78 874.86
OW-2 2/12/2010 879.64 - - 3.72 875.92
OW-2 11/5/2010 879.64 - - 8.19 871.42
OW-2 1/10/2014 879.64 - - 4.69 874.92
OW-2 1/17/2014 879.64 - - 4.49 875.12
Page 102 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-2 1/24/2014 879.64 - - 4.98 874.63
OW-2 1/31/2014 879.64 - - 5.97 873.64
OW-2 2/7/2014 879.64 - - 5.38 874.23
OW-2 2/14/2014 879.64 - - 4.31 875.30
OW-2 2/21/2014 879.64 - - 3.86 875.75
OW-2 2/28/2014 879.64 - - 5.22 874.39
OW-2 3/7/2014 879.64 - - 3.27 876.34
OW-2 3/14/2014 879.64 - - 3.39 876.22
OW-2 3/21/2014 879.64 - - 3.27 876.34
OW-2 3/28/2014 879.64 - - 4.12 875.49
OW-2 4/4/2014 879.64 - - 4.68 874.93
OW-2 4/11/2014 879.64 - - 4.35 875.26
OW-2 4/18/2014 879.64 - - 4.05 875.56
OW-2 4/25/2014 879.64 - - 4.25 875.36
OW-2 5/2/2014 879.64 - - 4.57 875.04
OW-2 5/9/2014 879.64 - - 4.76 874.85
OW-2 5/16/2014 879.64 - - 4.51 875.10
OW-2 5/23/2014 879.64 - - 5.42 874.19
OW-2 5/30/2014 879.64 - - 5.87 873.74
OW-2 6/6/2014 879.64 - - 6.18 873.43
OW-2 6/13/2014 879.64 - - 6.43 873.18
OW-2 6/20/2014 879.64 - - 6.89 872.72
OW-2 6/27/2014 879.64 - - 7.08 872.53
OW-2 7/5/2014 879.64 - - 7.53 872.08
OW-2 7/11/2014 879.64 - - 7.91 871.70
OW-2 3/5/2015 879.64 - -3.22 876.39
OW-2 5/27/2015 879.64 - -7.79 871.82
OW-2 6/29/2015 879.64 - -9.55 870.06
OW-2 7/30/2015 879.64 - -10.90 868.71
OW-2 8/20/2015 879.64 - -10.90 868.71
OW-2 9/9/2015 879.64 - -11.51 868.10
OW-2 10/15/2015 879.64 - -8.74 870.87
OW-2 10/26/2015 879.64 - -9.55 870.06
OW-2 12/4/2015 879.64 - -4.70 874.91
OW-2 1/12/2016 879.61 - - 4.71 874.90
OW-2 5/26/2016 879.61 - - 4.27 875.34
OW-2 7/11/2016 879.61 - - 5.14 874.47
Page 103 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-2 7/12/2016 879.61 - - 5.14 874.47
OW-2 7/27/2016 879.61 - - 7.10 872.51
OW-2 9/28/2016 879.61 - - 9.69 869.92
OW-2 11/29/2016 879.61 - - 10.25 869.36
OW-2 12/14/2016 879.61 - - 10.21 869.40
OW-2 5/17/2017 879.61 - - 7.85 871.76
OW-2 6/26/2017 879.61 - - 5.18 874.43
OW-2 8/8/2017 879.61 - - 8.91 870.70
OW-2 11/28/2017 879.61 - - 11.19 868.42
OW-2 12/11/2017 879.61 - - 11.38 868.23
OW-2 1/25/2018 879.61 - - 7.67 871.94
OW-2 5/21/2018 879.61 - - 7.82 871.79
OW-2 7/9/2018 879.61 - - 9.39 870.22
OW-2 8/16/2018 879.61 - - 7.68 871.93
OW-2 11/29/2018 879.61 - - 5.13 874.48
OW-2 12/12/2018 879.61 - - 3.96 875.65
OW-2 3/27/2019 879.61 - - 3.79 875.82
OW-2 5/29/2019 879.61 - - 5.65 873.96
OW-2 6/10/2019 879.61 - - 3.91 875.70
OW-2 8/6/2019 879.61 - - 5.40 874.21
OW-2 11/8/2019 879.61 - - 6.96 872.65
OW-2 12/9/2019 879.61 - - 6.22 873.39
OW-2 3/6/2020 879.61 - - 3.73 875.88
OW-2 6/11/2020 879.61 - - 4.55 875.06
OW-2 8/24/2020 879.61 - - 6.25 873.36
OW-2 11/30/2020 879.61 - - 3.26 876.35
OW-2 12/14/2020 879.61 - - 6.07 873.54
OW-2 3/29/2021 879.61 - - 5.06 874.55
OW-2 6/14/2021 879.61 - - 4.54 875.07
OW-2 9/28/2021 879.61 - - 8.00 871.61
OW-2 12/28/2021 879.61 - - 8.81 870.80
OW-2 4/1/2022 879.61 - - 4.68 874.93
OW-2 6/20/2022 879.61 - - 7.04 872.57
OW-2 9/22/2022 879.61 - - 9.53 870.08
OW-2 12/5/2022 879.61 - - 6.61 873.00
OW-2 4/10/2023 879.61 - - 3.74 875.87
OW-2 7/17/2023 879.61 - - 7.14 872.47
Page 104 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-2 9/18/2023 879.61 - - 7.30 872.31
OW-2 12/6/2023 879.61 - - 10.61 869.00
OW-2 3/1/2024 879.61 - - 6.45 873.16
OW-3 7/25/1997 882.42 - - 9.67 872.75
OW-3 8/24/1997 882.42 - - 11.21 871.21
OW-3 9/14/1997 882.42 - - 11.44 870.98
OW-3 10/3/1997 882.42 - - 11.81 870.61
OW-3 11/14/1997 882.42 - - 11.67 870.75
OW-3 12/31/1997 882.42 10.92 0.18 11.10 871.46
OW-3 1/23/1998 882.42 6.34 0.18 6.52 876.04
OW-3 2/17/1998 882.42 6.07 0.15 6.22 876.31
OW-3 3/6/1998 882.42 7.50 0.15 7.65 874.88
OW-3 4/28/1998 882.42 7.08 0.11 7.19 875.31
OW-3 12/26/1998 882.42 10.56 0.11 10.67 871.83
OW-3 8/26/1999 882.42 11.75 0.07 11.82 870.65
OW-3 9/22/1999 882.42 9.48 0.05 9.53 872.93
OW-3 10/7/1999 882.42 9.48 0.05 9.53 872.93
OW-3 10/18/2002 882.42 10.73 0.68 11.41 871.52
OW-3 1/30/2003 882.42 6.31 0.44 6.75 876.00
OW-3 2/6/2003 882.42 7.93 0.36 8.29 874.40
OW-3 2/14/2003 882.42 8.06 0.33 8.39 874.28
OW-3 2/21/2003 882.42 7.77 0.17 7.94 874.61
OW-3 2/24/2003 882.42 8.01 0.19 8.20 874.36
OW-3 3/20/2003 882.42 6.54 0.37 6.91 875.79
OW-3 4/23/2003 882.42 6.16 0.20 6.36 876.21
OW-3 5/30/2003 882.42 6.05 0.15 6.20 876.33
OW-3 6/30/2003 882.42 6.88 0.10 6.98 875.52
OW-3 7/29/2003 882.42 7.85 0.07 7.92 874.55
OW-3 8/20/2003 882.42 6.05 0.05 6.10 876.36
OW-3 11/10/2003 882.42 - - 7.92 874.48
OW-3 12/23/2003 882.42 7.41 0.01 7.42 875.01
OW-3 1/29/2004 882.42 - - 7.81 874.59
OW-3 3/30/2004 882.42 7.92 0.02 7.94 874.50
OW-3 4/23/2004 882.42 - - 8.11 874.29
OW-3 5/20/2004 882.42 9.12 0.01 9.13 873.30
OW-3 6/28/2004 882.42 - - 10.48 871.92
Page 105 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-3 8/30/2004 882.42 - - 11.03 871.37
OW-3 1/26/2005 882.42 - - 8.92 873.48
OW-3 2/18/2005 882.42 - - 8.09 874.31
OW-3 3/29/2005 882.42 - - 7.23 875.17
OW-3 6/2/2006 882.42 - - 11.48 870.92
OW-3 6/16/2006 882.42 - - 9.28 873.12
OW-3 1/11/2008 882.42 - - 12.60 869.80
OW-3 11/5/2010 882.42 - - 10.97 871.43
OW-3 1/10/2014 882.42 - - 7.44 874.96
OW-3 1/17/2014 882.42 - - 7.17 875.23
OW-3 1/24/2014 882.42 - - 7.91 874.49
OW-3 1/31/2014 882.42 - - 8.74 873.66
OW-3 2/7/2014 882.42 - - 7.98 874.42
OW-3 2/14/2014 882.42 - - 6.99 875.41
OW-3 2/21/2014 882.42 - - 6.64 875.76
OW-3 2/28/2014 882.42 - - 7.99 874.41
OW-3 3/7/2014 882.42 - - 6.06 876.34
OW-3 3/14/2014 882.42 - - 6.15 876.25
OW-3 3/21/2014 882.42 - - 6.06 876.34
OW-3 3/28/2014 882.42 - - 6.89 875.51
OW-3 4/4/2014 882.42 - - 7.47 874.93
OW-3 4/11/2014 882.42 - - 7.13 875.27
OW-3 4/18/2014 882.42 - - 6.89 875.51
OW-3 4/25/2014 882.42 - - 7.05 875.35
OW-3 5/2/2014 882.42 - - 7.21 875.19
OW-3 5/9/2014 882.42 - - 7.51 874.89
OW-3 5/16/2014 882.42 - - 7.28 875.12
OW-3 5/23/2014 882.42 - - 8.19 874.21
OW-3 5/30/2014 882.42 - - 8.53 873.87
OW-3 6/6/2014 882.42 - - 8.97 873.43
OW-3 6/13/2014 882.42 - - 9.25 873.15
OW-3 6/20/2014 882.42 - - 9.53 872.87
OW-3 6/27/2014 882.42 - - 9.87 872.53
OW-3 7/5/2014 882.42 - - 10.23 872.17
OW-3 7/11/2014 882.42 - - 10.69 871.71
OW-3 3/5/2015 882.42 - -6.03 876.37
OW-3 5/27/2015 882.42 - -10.58 871.82
Page 106 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-3 6/29/2015 882.42 - -12.35 870.05
OW-3 7/30/2015 882.42 - -13.68 868.72
OW-3 8/20/2015 882.42 - -13.71 868.69
OW-3 9/9/2015 882.42 - -14.27 868.13
OW-3 10/15/2015 882.42 - -11.50 870.90
OW-3 10/26/2015 882.42 - -12.32 870.08
OW-3 12/4/2015 882.42 - -7.49 874.91
OW-3 1/12/2016 882.42 - - 5.43 876.97
OW-3 5/26/2016 882.42 - - 7.03 875.37
OW-3 7/11/2016 882.42 - - 7.85 874.55
OW-3 7/12/2016 882.42 - - 7.85 874.55
OW-3 8/3/2016 882.42 - - 10.39 872.03
OW-3 9/28/2016 882.42 - - 12.46 869.94
OW-3 11/29/2016 882.42 - - 13.00 869.40
OW-3 12/14/2016 882.42 - - 13.00 869.40
OW-3 5/17/2017 882.42 - - 10.62 871.80
OW-3 6/26/2017 882.42 - - 7.98 874.44
OW-3 8/8/2017 882.42 - - 11.70 870.72
OW-3 11/28/2017 882.42 - - 13.98 868.44
OW-3 12/11/2017 882.42 - - 14.16 868.26
OW-3 1/25/2018 882.42 - - 10.44 871.98
OW-3 5/21/2018 882.42 - - 10.61 871.81
OW-3 7/9/2018 882.42 - - 12.20 870.22
OW-3 8/16/2018 882.42 - - 10.44 871.98
OW-3 11/29/2018 882.42 - - 7.91 874.51
OW-3 12/12/2018 882.42 - - 6.74 875.68
OW-3 3/27/2019 882.42 - - 6.56 875.86
OW-3 5/29/2019 882.42 - - 8.40 874.02
OW-3 6/10/2019 882.42 - - 6.70 875.72
OW-3 8/6/2019 882.42 - - 8.16 874.26
OW-3 11/8/2019 882.42 - - 9.73 872.69
OW-3 12/9/2019 882.42 - - 8.99 873.43
OW-3 3/6/2020 882.42 - - 6.51 875.91
OW-3 6/11/2020 882.42 - - 7.33 875.09
OW-3 8/24/2020 882.42 - - 9.03 873.39
OW-3 11/30/2020 882.42 - - 6.06 876.36
OW-3 12/14/2020 882.42 - - 8.84 873.58
Page 107 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-3 3/29/2021 882.42 - - 6.07 876.35
OW-3 6/14/2021 882.42 - - 7.30 875.12
OW-3 9/28/2021 882.42 - - 10.82 871.60
OW-3 12/28/2021 882.42 - - 11.58 870.84
OW-3 4/1/2022 882.42 - - 7.36 875.06
OW-3 6/20/2022 882.42 - - 8.94 873.48
OW-3 9/22/2022 882.42 - - 12.34 870.08
OW-3 12/5/2022 882.42 - - 9.38 873.04
OW-3 4/10/2023 882.42 - - 6.51 875.91
OW-3 7/17/2023 882.42 - - 9.47 872.95
OW-3 9/18/2023 882.42 - - 10.08 872.34
OW-3 12/6/2023 882.42 - - 13.39 869.03
OW-3 3/1/2024 882.42 - - 9.22 873.20
OW-4 8/5/2003 879.85 - - 4.18 875.67
OW-4 8/20/2003 879.85 - - 3.55 876.30
OW-4 11/10/2003 879.85 - - 5.35 874.50
OW-4 12/23/2003 879.85 - - 4.85 875.00
OW-4 1/29/2004 879.85 5.22 0.02 5.24 874.62
OW-4 3/30/2004 879.85 5.33 0.02 5.35 874.51
OW-4 4/23/2004 879.85 5.51 0.03 5.54 874.33
OW-4 5/20/2004 879.85 - - 6.55 873.30
OW-4 6/28/2004 879.85 - - 7.86 871.99
OW-4 8/30/2004 879.85 - - 8.43 871.42
OW-4 1/26/2005 879.85 - - 6.32 873.53
OW-4 2/18/2005 879.85 - - 5.49 874.36
OW-4 3/29/2005 879.85 - - 4.38 875.47
OW-4 6/2/2006 879.85 - - 8.85 871.00
OW-4 6/16/2006 879.85 - - 6.64 873.21
OW-4 1/11/2008 879.85 - - 9.95 869.90
OW-4 11/5/2010 879.85 - - 8.32 871.53
OW-4 1/10/2014 879.85 - - 4.81 875.04
OW-4 1/17/2014 879.85 - - 4.59 875.26
OW-4 1/24/2014 879.85 - - 5.41 874.44
OW-4 1/31/2014 879.85 - - 6.12 873.73
OW-4 2/7/2014 879.85 - - 5.69 874.16
OW-4 2/14/2014 879.85 - - 4.49 875.36
Page 108 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-4 2/21/2014 879.85 - - 4.03 875.82
OW-4 2/28/2014 879.85 - - 5.38 874.47
OW-4 3/7/2014 879.85 - - 3.44 876.41
OW-4 3/14/2014 879.85 - - 3.57 876.28
OW-4 3/21/2014 879.85 - - 3.44 876.41
OW-4 3/28/2014 879.85 - - 4.10 875.75
OW-4 4/4/2014 879.85 - - 4.85 875.00
OW-4 4/11/2014 879.85 - - 4.63 875.22
OW-4 4/18/2014 879.85 - - 4.38 875.47
OW-4 4/25/2014 879.85 - - 4.51 875.34
OW-4 5/2/2014 879.85 - - 4.73 875.12
OW-4 5/9/2014 879.85 - - 4.91 874.94
OW-4 5/16/2014 879.85 - - 4.66 875.19
OW-4 5/23/2014 879.85 - - 5.56 874.29
OW-4 5/30/2014 879.85 - - 6.02 873.83
OW-4 6/6/2014 879.85 - - 6.32 873.53
OW-4 6/13/2014 879.85 - - 6.61 873.24
OW-4 6/20/2014 879.85 - - 7.04 872.81
OW-4 6/27/2014 879.85 - - 7.25 872.60
OW-4 7/5/2014 879.85 - - 7.64 872.21
OW-4 7/11/2014 879.85 - - 8.05 871.80
OW-4 3/5/2015 879.85 - -3.46 876.39
OW-4 5/27/2015 879.85 - -7.91 871.94
OW-4 6/29/2015 879.85 - -9.74 870.11
OW-4 7/30/2015 879.85 - -11.05 868.80
OW-4 8/20/2015 879.85 - -11.05 868.80
OW-4 9/9/2015 879.85 - -11.65 868.20
OW-4 10/15/2015 879.85 - -8.85 871.00
OW-4 10/26/2015 879.85 - -9.68 870.17
OW-4 12/4/2015 879.85 - -4.82 875.03
OW-4 1/12/2016 879.85 - - 4.84 875.01
OW-4 5/26/2016 879.85 - - 4.46 875.39
OW-4 7/11/2016 879.85 - - 5.27 874.58
OW-4 7/12/2016 879.85 - - 5.27 874.58
OW-4 7/26/2016 879.85 - - 7.20 872.65
OW-4 9/28/2016 879.85 - - 9.85 870.00
OW-4 11/29/2016 879.85 - - 10.38 869.47
Page 109 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-4 12/14/2016 879.85 - - 10.33 869.52
OW-4 5/17/2017 879.85 - - 8.00 871.85
OW-4 6/26/2017 879.85 - - 5.32 874.53
OW-4 8/8/2017 879.85 - - 9.08 870.77
OW-4 11/28/2017 879.85 - - 11.33 868.52
OW-4 12/11/2017 879.85 - - 11.53 868.32
OW-4 1/25/2018 879.85 - - 7.83 872.02
OW-4 5/21/2018 879.85 - - 7.96 871.89
OW-4 7/9/2018 879.85 - - 9.43 870.42
OW-4 8/16/2018 879.85 - - 7.81 872.04
OW-4 11/29/2018 879.85 - - 5.29 874.56
OW-4 12/12/2018 879.85 - - 4.10 875.75
OW-4 3/27/2019 879.85 - - 3.93 875.92
OW-4 5/29/2019 879.85 - - 8.79 871.06
OW-4 6/10/2019 879.85 - - 4.06 875.79
OW-4 8/6/2019 879.85 - - 5.54 874.31
OW-4 11/8/2019 879.85 - - 7.10 872.75
OW-4 12/9/2019 879.85 - - 6.35 873.50
OW-4 3/6/2020 879.85 - - 3.88 875.97
OW-4 6/11/2020 879.85 - - 4.70 875.15
OW-4 8/24/2020 879.85 - - 6.41 873.44
OW-4 11/30/2020 879.85 - - 3.42 876.43
OW-4 12/16/2020 879.85 - - 6.17 873.68
OW-4 3/29/2021 879.85 - - 3.45 876.40
OW-4 6/14/2021 879.85 - - 4.68 875.17
OW-4 9/28/2021 879.85 - - 8.16 871.69
OW-4 12/28/2021 879.85 - - 8.93 870.92
OW-4 4/1/2022 879.85 - - 4.74 875.11
OW-4 6/20/2022 879.85 - - 8.39 871.46
OW-4 9/22/2022 879.85 - - 9.66 870.19
OW-4 12/5/2022 879.85 - - 6.74 873.11
OW-4 4/10/2023 879.85 - - 3.88 875.97
OW-4 7/17/2023 879.85 - - 8.17 871.68
OW-4 9/18/2023 879.85 - - 7.42 872.43
OW-4 12/6/2023 879.85 - - 10.76 869.09
OW-4 3/1/2024 879.85 - - 6.60 873.25
Page 110 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-5 8/5/2003 879.50 - - 3.82 875.68
OW-5 8/20/2003 879.50 - - 3.20 876.30
OW-5 11/10/2003 879.50 - - 5.00 874.50
OW-5 12/23/2003 879.50 - - 4.52 874.98
OW-5 1/29/2004 879.50 4.89 0.01 4.90 874.61
OW-5 3/30/2004 879.50 - - 5.00 874.50
OW-5 4/23/2004 879.50 - - 5.18 874.32
OW-5 5/20/2004 879.50 - - 6.21 873.29
OW-5 6/28/2004 879.50 - - 7.53 871.97
OW-5 8/30/2004 879.50 - - 8.14 871.36
OW-5 1/26/2005 879.50 - - 5.98 873.52
OW-5 2/18/2005 879.50 - - 5.16 874.34
OW-5 3/29/2005 879.50 - - 4.05 875.45
OW-5 6/2/2006 879.50 - - 8.50 871.00
OW-5 6/16/2006 879.50 - - 6.30 873.20
OW-5 1/11/2008 879.50 - - 9.59 869.91
OW-5 11/5/2010 879.50 - - 7.94 871.56
OW-5 1/10/2014 879.50 - - 4.38 875.12
OW-5 1/17/2014 879.50 - - 4.08 875.42
OW-5 1/24/2014 879.50 - - 5.01 874.49
OW-5 1/31/2014 879.50 - - 5.75 873.75
OW-5 2/7/2014 879.50 - - 5.13 874.37
OW-5 2/14/2014 879.50 - - 4.21 875.29
OW-5 2/21/2014 879.50 - - 3.65 875.85
OW-5 2/28/2014 879.50 - - 5.01 874.49
OW-5 3/7/2014 879.50 - - 3.06 876.44
OW-5 3/14/2014 879.50 - - 3.21 876.29
OW-5 3/21/2014 879.50 - - 3.06 876.44
OW-5 3/28/2014 879.50 - - 5.07 874.43
OW-5 4/4/2014 879.50 - - 4.47 875.03
OW-5 4/11/2014 879.50 - - 4.41 875.09
OW-5 4/18/2014 879.50 - - 4.18 875.32
OW-5 4/25/2014 879.50 - - 4.39 875.11
OW-5 5/2/2014 879.50 - - 4.51 874.99
OW-5 5/9/2014 879.50 - - 4.73 874.77
OW-5 5/16/2014 879.50 - - 4.28 875.22
OW-5 5/23/2014 879.50 - - 5.19 874.31
Page 111 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-5 5/30/2014 879.50 - - 5.58 873.92
OW-5 6/6/2014 879.50 - - 5.95 873.55
OW-5 6/13/2014 879.50 - - 6.33 873.17
OW-5 6/20/2014 879.50 - - 6.59 872.91
OW-5 6/27/2014 879.50 - - 6.87 872.63
OW-5 7/5/2014 879.50 - - 7.28 872.22
OW-5 7/11/2014 879.50 - - 7.68 871.82
OW-5 3/5/2015 879.50 - -3.02 876.48
OW-5 5/27/2015 879.50 - -7.55 871.95
OW-5 6/29/2015 879.50 - -9.35 870.15
OW-5 7/30/2015 879.50 - -10.65 868.85
OW-5 8/20/2015 879.50 - -10.67 868.83
OW-5 9/9/2015 879.50 - -11.25 868.25
OW-5 10/15/2015 879.50 - -8.45 871.05
OW-5 10/26/2015 879.50 - -9.31 870.19
OW-5 12/4/2015 879.50 - -4.46 875.04
OW-5 1/12/2016 879.50 - - 4.46 875.04
OW-5 5/26/2016 879.50 - - 4.08 875.42
OW-5 7/11/2016 879.50 - - 4.89 874.61
OW-5 7/12/2016 879.50 - - 4.89 874.61
OW-5 7/27/2016 879.50 - - 6.90 872.60
OW-5 9/28/2016 879.50 - - 9.45 870.05
OW-5 11/29/2016 879.50 - - 9.98 869.52
OW-5 12/14/2016 879.50 - - 7.99 871.51
OW-5 5/17/2017 879.50 - - 7.62 871.88
OW-5 6/26/2017 879.50 - - 4.94 874.56
OW-5 8/8/2017 879.50 - - 8.68 870.82
OW-5 11/28/2017
OW-5 12/11/2017 879.50 - - Dry NA
OW-5 1/25/2018 879.50 - - 7.49 872.01
OW-5 5/21/2018 879.50 - - 7.63 871.87
OW-5 7/9/2018 879.50 - - 9.18 870.32
OW-5 8/16/2018 879.50 - - 7.46 872.04
OW-5 11/29/2018 879.50 - - 4.93 874.57
OW-5 12/12/2018 879.50 - - 3.74 875.76
OW-5
OW-5 was damaged and unable to be measured
OW-5 was abandoned in December 2018
Page 112 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-6 8/5/2003 879.45 - - 3.78 875.67
OW-6 8/20/2003 879.45 - - 3.15 876.30
OW-6 11/10/2003 879.45 - - 4.95 874.50
OW-6 12/23/2003 879.45 - - 4.50 874.95
OW-6 1/29/2004 879.45 - - 4.86 874.59
OW-6 3/30/2004 879.45 - - 4.98 874.47
OW-6 4/23/2004 879.45 - - 5.17 874.28
OW-6 5/20/2004 879.45 - - 6.20 873.25
OW-6 6/28/2004 879.45 - - 7.50 871.95
OW-6 8/30/2004 879.45 - - 8.05 871.40
OW-6 1/26/2005 879.45 - - 5.97 873.48
OW-6 2/18/2005 879.45 - - 5.14 874.31
OW-6 3/29/2005 879.45 - - 4.03 875.42
OW-6 6/2/2006 879.45 - - 8.53 870.92
OW-6 6/16/2006 879.45 - - 6.33 873.12
OW-6 3/5/2015 879.45 - -2.97 876.48
OW-6 5/27/2015 879.45 - -7.55 871.90
OW-6 6/29/2015 879.45 - -9.30 870.15
OW-6 7/30/2015 879.45 - -10.85 868.60
OW-6 8/20/2015 879.45 - -10.65 868.80
OW-6 9/9/2015 879.45 - -11.24 868.21
OW-6 10/15/2015 879.45 - -8.48 870.97
OW-6 10/26/2015 879.45 - -9.36 870.09
OW-6 12/4/2015 879.45 - -4.46 874.99
OW-6 1/12/2016 879.45 - - 4.48 874.97
OW-6 5/26/2016 879.45 - - 4.11 875.34
OW-6 7/11/2016 879.45 - - 4.92 874.53
OW-6 7/12/2016 879.45 - - 4.92 874.53
OW-6 8/2/2016 879.45 - - 7.36 872.09
OW-6 9/28/2016 879.45 - - 9.47 869.98
OW-6 11/29/2016 879.45 - - 10.05 869.40
OW-6 12/27/2016 879.45 - - 10.20 869.25
OW-6 5/17/2017 879.45 - - 7.63 871.82
OW-6 6/26/2017 879.45 - - 4.98 874.47
OW-6 8/8/2017 879.45 - - 8.69 870.76
OW-6 11/28/2017 879.45 - - 10.98 868.47
Page 113 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-6 12/11/2017 879.45 - - 11.16 868.29
OW-6 1/25/2018 879.45 - - 7.46 871.99
OW-6 5/21/2018 879.45 - - 7.61 871.84
OW-6 7/9/2018 879.45 - - 9.16 870.29
OW-6 8/16/2018 879.45 - - 7.44 872.01
OW-6 11/29/2018 879.45 - - 4.92 874.53
OW-6 12/12/2018 879.45 - - 3.72 875.73
OW-6 3/27/2019 879.45 - - 3.58 875.87
OW-6 5/29/2019 879.45 - - 5.43 874.02
OW-6 6/10/2019 879.45 - - 3.70 875.75
OW-6 8/6/2019 879.45 - - 5.18 874.27
OW-6 11/8/2019 879.45 - - 6.73 872.72
OW-6 12/9/2019 879.45 - - 4.26 875.19
OW-6 3/6/2020 879.45 - - 3.51 875.94
OW-6 6/11/2020 879.45 - - 4.34 875.11
OW-6 8/24/2020 879.45 - - 6.03 873.42
OW-6 11/30/2020 879.45 - - 3.06 876.39
OW-6 12/14/2020 879.45 - - 5.88 873.57
OW-6 3/29/2021 879.45 - - 3.07 876.38
OW-6 6/14/2021 879.45 - - 6.02 873.43
OW-6 9/28/2021 879.45 - - 7.80 871.65
OW-6 12/28/2021 879.45 - - 8.60 870.85
OW-6 4/1/2022 879.45 - - 4.41 875.04
OW-6 6/20/2022 879.45 - - 8.92 870.53
OW-6 9/22/2022 879.45 - - 9.31 870.14
OW-6 12/5/2022 879.45 - - 6.39 873.06
OW-6 4/10/2023 879.45 - - 3.52 875.93
OW-6 7/17/2023 879.45 - - 6.92 872.53
OW-6 9/18/2023 879.45 - - 7.08 872.37
OW-6 12/6/2023 879.45 - - 10.39 869.06
OW-6 3/1/2024 879.45 - - 6.24 873.21
OW-7 8/5/2003 887.09 - - 8.98 878.11
OW-7 8/20/2003 887.09 - - 8.05 879.04
OW-7 11/10/2003 887.09 - - 11.00 876.09
OW-7 12/23/2003 887.09 - - 10.45 876.64
OW-7 1/29/2004 887.09 - - 11.85 875.24
Page 114 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-7 3/30/2004 887.09 - - 11.47 875.62
OW-7 4/23/2004 887.09 - - 11.68 875.41
OW-7 5/20/2004 887.09 - - 12.74 874.35
OW-7 6/28/2004 887.09 - - 13.98 873.11
OW-7 8/30/2004 887.09 - - 14.77 872.32
OW-7 1/26/2005 887.09 - - 12.67 874.42
OW-7 2/18/2005 887.09 - - 12.02 875.07
OW-7 3/29/2005 887.09 - - 11.14 875.95
OW-7 3/5/2015 887.09 - -14.74 872.35
OW-7 5/27/2015 887.09 - -14.58 872.51
OW-7 6/29/2015 887.09 - -16.05 871.04
OW-7 7/30/2015 887.09 - -17.40 869.69
OW-7 8/20/2015 887.09 - -17.66 869.43
OW-7 9/9/2015 887.09 - - 18.10 868.99
OW-7 10/15/2015 887.09 - - 16.34 870.75
OW-7 10/26/2015 887.09 - -16.64 870.45
OW-7 12/4/2015 887.09 - -13.31 873.78
OW-7 1/12/2016 887.09 - - 11.61 875.48
OW-7 5/26/2016 887.09 - - 10.41 876.68
OW-7 7/11/2016 887.09 - - 12.47 874.62
OW-7 7/12/2016 887.09 - - 12.47 874.62
OW-7 8/3/2016 887.09 - - 13.83 873.26
OW-7 9/28/2016 887.09 - - 15.80 871.29
OW-7 11/29/2016 887.09 - - 16.84 870.25
OW-7 12/15/2016 887.09 - - 17.02 870.07
OW-7 5/17/2017 887.09 - - 15.25 871.84
OW-7 6/26/2017 887.09 - - 12.63 874.46
OW-7 8/8/2017 887.09 - - 14.94 872.15
OW-7 11/28/2017 887.09 - - 18.10 868.99
OW-7 12/11/2017 887.09 - - 18.29 868.80
OW-7 1/25/2018 887.09 - - 18.03 869.06
OW-7 5/21/2018 887.09 - - 14.81 872.28
OW-7 7/9/2018 887.09 - - 16.11 870.98
OW-7 8/16/2018 887.09 - - 15.01 872.08
OW-7 11/29/2018 887.09 - - 12.59 874.50
OW-7 12/12/2018 887.09 - - 12.20 874.89
OW-7 3/27/2019 887.09 - - 9.44 877.65
Page 115 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-7 5/29/2019 887.09 - - 11.63 875.46
OW-7 6/10/2019 887.09 - - 11.50 875.59
OW-7 8/6/2019 887.09 - - 12.43 874.66
OW-7 11/8/2019 887.09 - - 14.76 872.33
OW-7 12/9/2019 887.09 - - 13.64 873.45
OW-7 3/6/2020 887.09 - - 9.72 877.37
OW-7 6/11/2020 887.09 - - 10.34 876.75
OW-7 8/24/2020 887.09 - - 13.11 873.98
OW-7 11/30/2020 887.09 - - 11.35 875.74
OW-7 12/14/2020 887.09 - - 12.64 874.45
OW-7 3/29/2021 887.09 - - 8.32 878.77
OW-7 6/14/2021 887.09 - - 11.97 875.12
OW-7 9/28/2021 887.09 - - 15.02 872.07
OW-7 12/28/2021 887.09 - - 16.64 870.45
OW-7 4/1/2022 887.09 - - 13.08 874.01
OW-7 6/20/2022 887.09 - - 14.08 873.01
OW-7 9/22/2022 887.09 - - 16.79 870.30
OW-7 12/5/2022 887.09 - - 14.95 872.14
OW-7 4/10/2023 887.09 - - 11.34 875.75
OW-7 7/17/2023 887.09 - - 14.23 872.86
OW-7 9/18/2023 887.09 - - 16.10 870.99
OW-7 12/6/2023 887.09 - - 17.79 869.30
OW-7 3/1/2024 887.09 - - 14.12 872.97
OW-8 8/5/2003 887.97 - - 13.37 874.60
OW-8 8/20/2003 887.97 - - 9.34 878.63
OW-8 11/10/2003 887.97 - - 11.27 876.70
OW-8 12/23/2003 887.97 - - 10.68 877.29
OW-8 1/29/2004 887.97 - - 11.82 876.15
OW-8 3/30/2004 887.97 - - 10.85 877.12
OW-8 4/23/2004 887.97 - - 11.30 876.67
OW-8 5/20/2004 887.97 - - 12.50 875.47
OW-8 6/28/2004 887.97 - - 14.30 873.67
OW-8 8/30/2004 887.97 - - 15.00 872.97
OW-8 1/26/2005 887.97 - - 12.32 875.65
OW-8 2/18/2005 887.97 - - 11.71 876.26
OW-8 3/29/2005 887.97 - - 10.98 876.99
Page 116 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-8 3/5/2015 887.97 - -14.35 873.62
OW-8 5/27/2015 887.97 - -14.29 873.68
OW-8 6/29/2015 887.97 - -15.63 872.34
OW-8 7/30/2015 887.97 - -17.92 870.05
OW-8 8/20/2015 887.97 - -18.11 869.86
OW-8 9/9/2015 887.97 - -18.50 869.47
OW-8 10/15/2015 887.97 - -16.25 871.72
OW-8 10/26/2015 887.97 - -16.50 871.47
OW-8 12/4/2015 887.97 - -14.21 873.76
OW-8 1/12/2016 887.97 - - 12.27 875.70
OW-8 5/26/2016 887.97 - - 11.21 876.76
OW-8 7/11/2016 887.97 - - 13.25 874.72
OW-8 7/12/2016 887.97 - - 13.25 874.72
OW-8 7/22/2016 887.97 - - 13.75 874.22
OW-8 9/28/2016 887.97 - - 16.74 871.23
OW-8 11/29/2016 887.97 - - 17.13 870.84
OW-8 12/14/2016 887.97 - - 17.15 870.82
OW-8 5/17/2017 887.97 - - 15.13 872.84
OW-8 6/26/2017 887.97 - - 13.67 874.30
OW-8 8/8/2017 887.97 - - 16.12 871.85
OW-8 11/28/2017 887.97 - - 18.19 869.78
OW-8 12/11/2017 887.97 - - 18.31 869.66
OW-8 1/25/2018 887.97 - - 20.55 867.42
OW-8 5/21/2018 887.97 - - 14.56 873.41
OW-8 7/9/2018 887.97 - - 16.41 871.56
OW-8 8/16/2018 887.97 - - 15.32 872.65
OW-8 11/29/2018 887.97 - - 13.17 874.80
OW-8 12/12/2018 887.97 - - 12.79 875.18
OW-8 3/27/2019 887.97 - - 9.72 878.25
OW-8 5/29/2019 887.97 - - 10.06 877.91
OW-8 6/10/2019 887.97 - - 12.33 875.64
OW-8 8/6/2019 887.97 - - 13.20 874.77
OW-8 11/8/2019 887.97 - - 14.92 873.05
OW-8 12/9/2019 887.97 - - 13.74 874.23
OW-8 3/6/2020 887.97 - - 9.49 878.48
OW-8 6/11/2020 887.97 - - 10.71 877.26
OW-8 8/24/2020 887.97 - - 13.47 874.50
Page 117 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
OW-8 11/30/2020 887.97 - - 11.63 876.34
OW-8 12/14/2020 887.97 - - 11.27 876.70
OW-8 3/29/2021 887.97 - - 8.97 879.00
OW-8 6/14/2021 887.97 - - 12.16 875.81
OW-8 9/28/2021 887.97 - - 15.30 872.67
OW-8 12/28/2021 887.97 - - 16.37 871.60
OW-8 4/1/2022 887.97 - - 12.63 875.34
OW-8 6/20/2022 887.97 - - 15.26 872.71
OW-8 9/22/2022 887.97 - - 16.73 871.24
OW-8 12/5/2022 887.97 - - 15.77 872.20
OW-8 4/10/2023 887.97 - - 11.57 876.40
OW-8 7/17/2023 887.97 - - 14.37 873.60
OW-8 9/18/2023 887.97 - - 16.42 871.55
OW-8 12/6/2023 887.97 - - 17.66 870.31
OW-8 3/1/2024 887.97 - - 17.60 870.37
RW-1 7/25/1997 882.24 - - 9.01 873.23
RW-1 8/24/1997 882.24 - - 9.26 872.98
RW-1 9/14/1997 882.24 - - 9.07 873.17
RW-1 10/3/1997 882.24 - - 8.69 873.55
RW-1 11/14/1997 882.24 - - 6.15 876.09
RW-1 12/31/1997 882.24 - - 4.35 877.89
RW-1 1/23/1998 882.24 - - 3.90 878.34
RW-1 2/17/1998 882.24 - - 3.63 878.61
RW-1 12/26/1998 882.24 - - 6.53 875.71
RW-1 8/26/1999 882.24 - - 6.05 876.19
RW-1 9/22/1999 882.24 - - 7.44 874.80
RW-1 10/7/1999 882.24 - - 7.44 874.80
RW-1 4/24/2002 882.24 - - 10.09 872.15
RW-1 9/27/2002 882.24 - - 10.24 872.00
RW-1 10/3/2002 882.24 - - 10.35 871.89
RW-1 10/18/2002 882.24 - - 5.35 876.89
RW-1 10/30/2002 882.24 - - 4.35 877.89
RW-1 12/4/2002 882.24 - - 9.10 873.14
RW-1 12/11/2002 882.24 - - 4.00 878.24
RW-1 12/16/2002 882.24 - - 4.41 877.83
RW-1 1/2/2003 882.24 - - 4.30 877.94
Page 118 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-1 1/9/2003 882.24 - - 4.81 877.43
RW-1 1/14/2003 882.24 - - 6.34 875.90
RW-1 1/21/2003 882.24 - - 7.13 875.11
RW-1 1/30/2003 882.24 - - 4.15 878.09
RW-1 2/6/2003 882.24 - - 6.22 876.02
RW-1 2/14/2003 882.24 - - 6.65 875.59
RW-1 2/21/2003 882.24 - - 6.02 876.22
RW-1 2/24/2003 882.24 - - 6.21 876.03
RW-1 3/20/2003 882.24 - - 4.52 877.70
RW-1 4/23/2003 882.24 - - 4.35 877.87
RW-1 5/30/2003 882.24 - - 4.20 878.02
RW-1 6/30/2003 882.24 - - 4.70 877.52
RW-1 7/29/2003 882.24 - - 5.98 876.24
RW-1 8/20/2003 882.24 - - 4.20 878.04
RW-1 11/10/2003 882.24 - - 6.00 876.24
RW-1 12/23/2003 882.24 - - 5.00 877.22
RW-1 1/29/2004 882.24 - - 4.45 877.77
RW-1 3/30/2004 882.24 - - 6.30 875.92
RW-1 4/23/2004 882.24 - - 6.37 875.85
RW-1 5/20/2004 882.24 - - 7.50 874.72
RW-1 6/28/2004 882.24 - - 8.53 873.69
RW-1 8/30/2004 882.24 - - 9.80 872.42
RW-1 1/26/2005 882.24 - - 6.99 875.23
RW-1 2/18/2005 882.24 - - 5.78 876.44
RW-1 3/29/2005 882.24 - - 4.26 877.96
RW-1 6/2/2006 882.24 - - 9.36 872.86
RW-1 6/16/2006 882.24 - - 6.21 876.01
RW-1 6/30/2006 882.24 - - 5.67 876.55
RW-1 7/5/2006 882.24 - - 7.79 874.43
RW-1 7/13/2006 882.24 - - 8.62 873.60
RW-1 7/19/2006 882.24 - - 9.03 873.19
RW-1 7/28/2006 882.24 - - 7.67 874.55
RW-1 7/31/2006 882.24 - - 8.33 873.89
RW-1 8/15/2006 882.24 - - 9.67 872.55
RW-1 8/24/2006 882.24 - - 8.98 873.24
RW-1 8/30/2006 882.24 - - 9.73 872.49
RW-1 9/6/2006 882.24 - - 4.11 878.11
Page 119 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-1 9/14/2006 882.24 - - 3.91 878.31
RW-1 9/22/2006 882.24 - - 9.03 873.19
RW-1 9/28/2006 882.24 - - 7.81 874.41
RW-1 10/9/2006 882.24 - - 7.73 874.49
RW-1 10/12/2006 882.24 - - 7.80 874.42
RW-1 10/20/2006 882.24 - - 6.28 875.94
RW-1 10/27/2006 882.24 - - 7.94 874.28
RW-1 11/1/2006 882.24 - - 7.24 874.98
RW-1 11/10/2006 882.24 - - 6.63 875.59
RW-1 11/15/2006 882.24 - - 6.08 876.14
RW-1 11/20/2006 882.24 - - 5.83 876.39
RW-1 11/30/2006 882.24 - - 6.37 875.85
RW-1 12/4/2006 882.24 - - 6.83 875.39
RW-1 12/15/2006 882.24 - - 7.57 874.65
RW-1 12/18/2006 882.24 - - 7.73 874.49
RW-1 12/29/2006 882.24 - - 5.88 876.34
RW-1 1/2/2007 882.24 - - 4.56 877.66
RW-1 1/10/2007 882.24 - - 4.77 877.45
RW-1 1/19/2007 882.24 - - 6.60 875.62
RW-1 1/26/2007 882.24 - - 5.90 876.32
RW-1 2/8/2007 882.24 - - 7.22 875.00
RW-1 2/21/2007 882.24 - - 6.67 875.55
RW-1 3/2/2007 882.24 - - 3.85 878.37
RW-1 3/8/2007 882.24 - - 6.23 875.99
RW-1 3/15/2007 882.24 - - 6.97 875.25
RW-1 3/22/2007 882.24 - - 6.23 875.99
RW-1 3/27/2007 882.24 - - 6.76 875.46
RW-1 4/5/2007 882.24 - - 7.13 875.09
RW-1 4/12/2007 882.24 - - 4.11 878.11
RW-1 4/19/2007 882.24 - - 5.14 877.08
RW-1 4/26/2007 882.24 - - 6.62 875.60
RW-1 5/4/2007 882.24 - - 7.11 875.11
RW-1 5/10/2007 882.24 - - 7.33 874.89
RW-1 5/23/2007 882.24 - - 8.45 873.77
RW-1 5/31/2007 882.24 - - 8.45 873.77
RW-1 6/8/2007 882.24 - - 8.18 874.04
RW-1 6/14/2007 882.24 - - 8.86 873.36
Page 120 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-1 6/21/2007 882.24 - - 9.27 872.95
RW-1 6/28/2007 882.24 - - 9.40 872.82
RW-1 7/5/2007 882.24 - - 9.93 872.29
RW-1 7/12/2007 882.24 - - 9.83 872.39
RW-1 7/19/2007 882.24 - - 9.68 872.54
RW-1 7/26/2007 882.24 - - 9.78 872.44
RW-1 8/3/2007 882.24 - - 10.66 871.56
RW-1 8/9/2007 882.24 - - 11.88 870.34
RW-1 8/15/2007 882.24 - - 11.43 870.79
RW-1 8/22/2007 882.24 - - 11.67 870.55
RW-1 8/31/2007 882.24 - - 10.62 871.60
RW-1 9/7/2007 882.24 - - 10.62 871.60
RW-1 9/13/2007 882.24 - - 12.66 869.56
RW-1 9/21/2007 882.24 - - 12.66 869.56
RW-1 9/26/2007 882.24 - - 12.66 869.56
RW-1 10/5/2007 882.24 - - 12.66 869.56
RW-1 10/12/2007 882.24 - - 12.66 869.56
RW-1 10/19/2007 882.24 - - 12.66 869.56
RW-1 10/26/2007 882.24 - - 12.66 869.58
RW-1 11/2/2007 882.24 - - 12.66 869.58
RW-1 11/9/2007 882.24 - - 12.66 869.58
RW-1 11/17/2007 882.24 - - 12.66 869.58
RW-1 11/30/2007 882.24 - - 12.66 869.58
RW-1 12/8/2007 882.24 - - 12.66 869.58
RW-1 12/17/2007 882.24 - - 12.66 869.58
RW-1 12/21/2007 882.24 - - 12.66 869.58
RW-1 12/27/2007 882.24 - - 12.66 869.58
RW-1 1/4/2008 882.24 - - 8.00 874.24
RW-1 1/11/2008 882.24 - - 9.93 872.29
RW-1 1/18/2008 882.24 - - 9.46 872.78
RW-1 1/26/2008 882.24 - - 10.37 871.87
RW-1 2/8/2008 882.24 - - 7.49 874.75
RW-1 2/22/2008 882.24 - - 9.64 872.60
RW-1 3/1/2008 882.24 - - 9.21 873.03
RW-1 3/10/2008 882.24 - - 5.75 876.49
RW-1 3/14/2008 882.24 - - 7.97 874.27
RW-1 3/28/2008 882.24 - - 9.27 872.97
Page 121 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-1 4/18/2008 882.24 - - 8.70 873.54
RW-1 4/30/2008 882.24 - - 4.84 877.40
RW-1 5/2/2008 882.24 - - 6.06 876.18
RW-1 5/9/2008 882.24 - - 7.53 874.71
RW-1 5/16/2008 882.24 - - 7.99 874.25
RW-1 5/24/2008 882.24 - - 8.72 873.52
RW-1 6/6/2008 882.24 - - 9.57 872.67
RW-1 6/13/2008 882.24 - - 9.99 872.25
RW-1 6/20/2008 882.24 - - 10.25 871.99
RW-1 6/27/2008 882.24 - - 9.52 872.72
RW-1 7/11/2008 882.24 - - 9.25 872.99
RW-1 7/18/2008 882.24 - - 10.74 871.50
RW-1 7/25/2008 882.24 - - 10.78 871.46
RW-1 8/1/2008 882.24 - - 11.60 870.64
RW-1 8/8/2008 882.24 - - 12.15 870.09
RW-1 8/15/2008 882.24 - - 12.64 869.60
RW-1 8/22/2008 882.24 - - 13.05 869.19
RW-1 9/5/2008 882.24 - - 10.43 871.81
RW-1 9/12/2008 882.24 - - 9.47 872.77
RW-1 9/19/2008 882.24 - - 6.87 875.37
RW-1 10/10/2008 882.24 - - 10.48 871.76
RW-1 11/7/2008 882.24 - - 10.42 871.82
RW-1 11/14/2008 882.24 - - 10.33 871.91
RW-1 11/21/2008 882.24 - - 10.25 871.99
RW-1 12/5/2008 882.24 - - 10.07 872.17
RW-1 12/12/2008 882.24 - - 9.89 872.35
RW-1 1/2/2009 882.24 - - 9.92 872.32
RW-1 1/9/2009 882.24 - - 9.84 872.40
RW-1 1/23/2009 882.24 - - 9.78 872.46
RW-1 2/13/2009 882.24 - - 9.82 872.42
RW-1 2/27/2009 882.24 - - 9.93 872.31
RW-1 3/6/2009 882.24 - - 10.04 872.20
RW-1 3/30/2009 882.24 - - 4.79 877.45
RW-1 4/30/2009 882.24 - - 8.00 874.24
RW-1 5/15/2009 882.24 - - 6.90 875.34
RW-1 5/22/2009 882.24 - - 7.01 875.23
RW-1 5/29/2009 882.24 - - 7.43 874.81
Page 122 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-1 6/6/2009 882.24 - - 4.15 878.09
RW-1 6/12/2009 882.24 - - 5.50 876.74
RW-1 6/22/2009 882.24 - - 6.45 875.79
RW-1 6/27/2009 882.24 - - 7.41 874.83
RW-1 7/6/2009 882.24 - - 6.34 875.90
RW-1 7/10/2009 882.24 - - 5.99 876.25
RW-1 7/17/2009 882.24 - - 5.65 876.59
RW-1 7/24/2009 882.24 - - 9.11 873.13
RW-1 7/31/2009 882.24 - - 9.17 873.07
RW-1 8/6/2009 882.24 - - 9.33 872.91
RW-1 8/14/2009 882.24 - - 10.02 872.22
RW-1 8/21/2009 882.24 - - 10.28 871.96
RW-1 8/28/2009 882.24 - - 10.03 872.21
RW-1 9/4/2009 882.24 - - 10.21 872.03
RW-1 9/11/2009 882.24 - - 10.43 871.81
RW-1 9/25/2009 882.24 - - 10.66 871.58
RW-1 10/2/2009 882.24 - - 10.29 871.95
RW-1 10/9/2009 882.24 - - 10.14 872.10
RW-1 10/16/2009 882.24 - - 10.33 871.91
RW-1 10/23/2009 882.24 - - 10.41 871.83
RW-1 11/6/2009 882.24 - - 7.94 874.30
RW-1 11/13/2009 882.24 - - 8.02 874.22
RW-1 11/20/2009 882.24 - - 7.90 874.34
RW-1 12/4/2009 882.24 - - 8.11 874.13
RW-1 12/11/2009 882.24 - - 8.16 874.08
RW-1 12/17/2009 882.24 - - 8.18 874.06
RW-1 1/7/2010 882.24 - - 6.52 875.72
RW-1 1/7/2010 882.24 - - 6.43 875.81
RW-1 1/22/2010 882.24 - - 6.41 875.83
RW-1 1/28/2010 882.24 - - 6.35 875.89
RW-1 2/4/2010 882.24 - - 5.57 876.67
RW-1 2/12/2010 882.24 - - 4.41 877.83
RW-1 11/5/2010 882.24 - - 9.66 872.58
RW-1 1/10/2014 882.24 - - 4.87 877.35
RW-1 1/17/2014 882.24 - - 4.61 877.61
RW-1 1/24/2014 882.24 - - 6.51 875.71
RW-1 1/31/2014 882.24 - - 7.29 874.93
Page 123 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-1 2/7/2014 882.24 - - 6.83 875.39
RW-1 2/14/2014 882.24 - - 5.18 877.04
RW-1 2/21/2014 882.24 - - 4.65 877.57
RW-1 2/28/2014 882.24 - - 6.42 875.80
RW-1 3/7/2014 882.24 - - 3.97 878.25
RW-1 3/14/2014 882.24 - - 4.16 878.06
RW-1 3/21/2014 882.24 - - 3.97 878.25
RW-1 3/28/2014 882.24 - - 4.91 877.31
RW-1 4/4/2014 882.24 - - 5.73 876.49
RW-1 4/11/2014 882.24 - - 5.39 876.83
RW-1 4/18/2014 882.24 - - 4.89 877.33
RW-1 4/25/2014 882.24 - - 5.05 877.17
RW-1 5/2/2014 882.24 - - 5.21 877.01
RW-1 5/9/2014 882.24 - - 5.41 876.81
RW-1 5/16/2014 882.24 - - 5.17 877.05
RW-1 5/23/2014 882.24 - - 6.51 875.71
RW-1 5/30/2014 882.24 - - 6.61 875.61
RW-1 6/6/2014 882.24 - - 6.72 875.50
RW-1 6/13/2014 882.24 - - 7.18 875.04
RW-1 6/20/2014 882.24 - - 7.56 874.66
RW-1 6/27/2014 882.24 - - 7.99 874.23
RW-1 7/5/2014 882.24 - - 8.49 873.73
RW-1 7/11/2014 882.24 - - 8.93 873.29
RW-1 3/5/2015 882.24 - -5.55 878.12
RW-1 5/27/2015 882.24 - -8.90 873.32
RW-1 6/29/2015 882.24 - -9.90 872.32
RW-1 7/30/2015 882.24 - -11.38 870.84
RW-1 8/20/2015 882.24 - -10.71 871.51
RW-1 9/9/2015 882.24 - -12.10 870.12
RW-1 10/15/2015 882.24 - -9.68 872.54
RW-1 10/26/2015 882.24 - -10.95 871.27
RW-1 12/4/2015 882.24 - -5.02 877.20
RW-1 1/12/2016 882.22 - - 5.80 876.42
RW-1 5/26/2016 882.22 - - 5.12 877.10
RW-1 7/11/2016 882.22 - - 6.89 875.33
RW-1 7/12/2016 882.22 - - 6.89 875.33
RW-1 7/25/2016 882.22 - - 8.09 874.13
Page 124 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-1 9/28/2016 882.22 - - 8.82 873.40
RW-1 11/29/2016 882.22 - - 11.80 870.42
RW-1 12/14/2016 882.22 - - 10.53 871.69
RW-1 5/17/2017 882.22 - - 9.11 873.11
RW-1 6/26/2017 882.22 - - 5.58 876.64
RW-1 8/8/2017 882.22 - - 8.29 873.93
RW-1 11/28/2017 882.22 - - 12.24 869.98
RW-1 12/11/2017 882.22 - - 8.94 873.28
RW-1 1/25/2018 882.22 - - 6.69 875.53
RW-1 5/21/2018 882.22 - - 8.34 873.88
RW-1 7/9/2018 882.22 - - 9.69 872.53
RW-1 8/16/2018 882.22 - - 8.77 873.45
RW-1 11/29/2018 882.22 - - 5.76 876.46
RW-1 12/12/2018 882.22 - - 4.43 877.79
RW-1 3/27/2019 882.22 - - 4.46 877.76
RW-1 5/29/2019 882.22 - - 6.60 875.62
RW-1 6/10/2019 882.22 - - 5.25 876.97
RW-1 8/6/2019 882.22 - - 6.22 876.00
RW-1 11/8/2019 882.22 - - 7.13 875.09
RW-1 12/9/2019 882.22 - - 7.11 875.11
RW-1 3/6/2020 882.22 - - 4.62 877.60
RW-1 6/11/2020 882.22 - - 5.23 876.99
RW-1 8/24/2020 882.22 - - 7.40 874.82
RW-1 11/30/2020 882.22 - - 4.64 877.58
RW-1 12/15/2020 882.22 - - 6.25 875.97
RW-1 3/29/2021 882.22 - - 3.81 878.41
RW-1 6/14/2021 882.22 - - 6.30 875.92
RW-1 9/28/2021 882.22 - - 9.62 872.60
RW-1 12/28/2021 882.22 - - 10.74 871.48
RW-1 4/1/2022 882.22 - - 7.41 874.81
RW-1 6/20/2022 882.22 - - 7.46 874.76
RW-1 9/22/2022 882.22 - - 11.28 870.94
RW-1 12/5/2022 882.22 - - 8.74 873.48
RW-1 4/10/2023 882.22 - - 4.18 878.04
RW-1 7/17/2023 882.22 - - 8.89 873.33
RW-1 9/18/2023 882.22 - - 9.71 872.51
RW-1 12/6/2023 882.22 - - 11.44 870.78
Page 125 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-1
RW-2 7/25/1997 880.48 - - 7.72 872.76
RW-2 8/24/1997 880.48 - - 9.27 871.21
RW-2 9/14/1997 880.48 - - 9.49 870.99
RW-2 10/3/1997 880.48 - - 9.90 870.58
RW-2 11/14/1997 880.48 9.70 0.01 9.71 870.78
RW-2 12/31/1997 880.48 9.00 0.14 9.14 871.45
RW-2 1/23/1998 880.48 4.42 0.14 4.56 876.03
RW-2 2/17/1998 880.48 4.11 0.13 4.24 876.34
RW-2 12/26/1998 880.48 8.58 0.10 8.68 871.88
RW-2 8/26/1999 880.48 9.82 0.08 9.90 870.64
RW-2 9/22/1999 880.48 7.54 0.09 7.63 872.92
RW-2 10/7/1999 880.48 7.54 0.09 7.63 872.92
RW-2 4/24/2002 880.48 9.55 0.79 10.34 870.73
RW-2 9/27/2002 880.48 11.78 0.76 12.54 868.51
RW-2 10/3/2002 880.48 11.54 0.78 12.32 868.75
RW-2 10/18/2002 880.48 8.78 0.74 9.52 871.52
RW-2 10/30/2002 880.48 6.42 0.60 7.02 873.91
RW-2 12/4/2002 880.48 8.43 0.49 8.92 871.93
RW-2 12/11/2002 880.48 4.17 0.49 4.66 876.19
RW-2 12/16/2002 880.48 6.30 0.46 6.76 874.07
RW-2 1/2/2003 880.48 5.13 0.45 5.58 875.24
RW-2 1/9/2003 880.48 6.05 0.40 6.45 874.33
RW-2 1/14/2003 880.48 6.46 0.42 6.88 873.92
RW-2 1/21/2003 880.48 6.80 0.08 6.88 873.66
RW-2 1/30/2003 880.48 4.45 0.11 4.56 876.00
RW-2 2/6/2003 880.48 6.05 0.08 6.13 874.41
RW-2 2/14/2003 880.48 6.12 0.08 6.20 874.34
RW-2 2/21/2003 880.48 5.56 0.06 5.62 874.91
RW-2 2/24/2003 880.48 5.68 0.07 5.75 874.78
RW-2 3/20/2003 880.48 6.50 0.08 6.58 873.96
RW-2 4/23/2003 880.48 - - 4.29 876.15
RW-2 5/30/2003 880.48 - - 16.16 864.28
RW-2 6/30/2003 880.48 4.95 0.05 5.00 875.52
RW-2 7/29/2003 880.48 - - 5.93 874.51
RW-2 8/20/2003 880.48 - - 4.20 876.28
RW-1 was abandoned in February 2024
Page 126 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-2 11/10/2003 880.48 - - 5.98 874.50
RW-2 12/23/2003 880.48 5.48 0.02 5.50 875.00
RW-2 1/29/2004 880.48 5.85 0.02 5.87 874.63
RW-2 3/30/2004 880.48 - - 6.01 874.43
RW-2 4/23/2004 880.48 - - 6.18 874.26
RW-2 5/20/2004 880.48 - - 7.20 873.24
RW-2 6/28/2004 880.48 - - 8.52 871.92
RW-2 8/30/2004 880.48 - - 9.03 871.41
RW-2 1/26/2005 880.48 - - 7.51 872.93
RW-2 2/18/2005 880.48 - - 6.17 874.27
RW-2 3/29/2005 880.48 - - 5.05 875.39
RW-2 6/2/2006 880.48 - - 9.55 870.89
RW-2 6/16/2006 880.48 - - 7.34 873.10
RW-2 6/30/2006 880.48 - - 6.83 873.61
RW-2 7/5/2006 880.48 - - 7.81 872.63
RW-2 7/13/2006 880.48 - - 8.02 872.42
RW-2 7/19/2006 880.48 - - 8.40 872.04
RW-2 7/28/2006 880.48 - - 7.82 872.62
RW-2 7/31/2006 880.48 - - 8.09 872.35
RW-2 8/15/2006 880.48 - - 9.04 871.40
RW-2 8/24/2006 880.48 - - 8.61 871.83
RW-2 8/30/2006 880.48 - - 9.06 871.38
RW-2 9/6/2006 880.48 - - 6.02 874.42
RW-2 9/14/2006 880.48 - - 4.31 876.13
RW-2 9/22/2006 880.48 - - 9.11 871.33
RW-2 9/28/2006 880.48 - - 7.41 873.03
RW-2 10/9/2006 880.48 - - 7.53 872.91
RW-2 10/12/2006 880.48 - - 7.60 872.84
RW-2 10/20/2006 880.48 - - 6.31 874.13
RW-2 10/27/2006 880.48 - - 7.43 873.01
RW-2 11/1/2006 880.48 - - 6.86 873.58
RW-2 11/10/2006 880.48 - - 6.26 874.18
RW-2 11/15/2006 880.48 - - 6.43 874.01
RW-2 11/20/2006 880.48 - - 6.36 874.08
RW-2 11/30/2006 880.48 - - 6.41 874.03
RW-2 12/4/2006 880.48 - - 6.60 873.84
RW-2 12/15/2006 880.48 - - 7.01 873.43
Page 127 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-2 12/18/2006 880.48 - - 7.15 873.29
RW-2 12/29/2006 880.48 - - 6.37 874.07
RW-2 1/2/2007 880.48 - - 5.32 875.12
RW-2 1/10/2007 880.48 - - 5.50 874.94
RW-2 1/19/2007 880.48 - - 6.31 874.13
RW-2 1/26/2007 880.48 - - 5.89 874.55
RW-2 2/8/2007 880.48 - - 6.68 873.76
RW-2 2/21/2007 880.48 - - 6.46 873.98
RW-2 3/2/2007 880.48 - - 4.19 876.25
RW-2 3/8/2007 880.48 - - 6.19 874.25
RW-2 3/15/2007 880.48 - - 6.53 873.91
RW-2 3/22/2007 880.48 - - 6.13 874.31
RW-2 3/27/2007 880.48 - - 6.41 874.03
RW-2 4/5/2007 880.48 - - 6.67 873.77
RW-2 4/12/2007 880.48 - - 4.23 876.21
RW-2 4/19/2007 880.48 - - 5.65 874.79
RW-2 4/26/2007 880.48 - - 6.38 874.06
RW-2 5/4/2007 880.48 - - 6.75 873.69
RW-2 5/10/2007 880.48 - - 6.97 873.47
RW-2 5/23/2007 880.48 - - 8.04 872.40
RW-2 5/31/2007 880.48 - - 8.04 872.40
RW-2 6/8/2007 880.48 - - 8.35 872.09
RW-2 6/14/2007 880.48 - - 8.59 871.85
RW-2 6/21/2007 880.48 - - 8.88 871.56
RW-2 6/28/2007 880.48 - - 9.26 871.18
RW-2 7/5/2007 880.48 - - 9.64 870.80
RW-2 7/12/2007 880.48 - - 9.94 870.50
RW-2 7/19/2007 880.48 - - 10.26 870.18
RW-2 7/26/2007 880.48 - - 10.54 869.90
RW-2 8/3/2007 880.48 - - 10.80 869.64
RW-2 8/9/2007 880.48 - - 11.04 869.40
RW-2 8/15/2007 880.48 - - 11.34 869.10
RW-2 8/22/2007 880.48 - - 11.71 868.73
RW-2 8/31/2007 880.48 - - 12.02 868.42
RW-2 9/7/2007 880.48 - - 12.02 868.42
RW-2 9/13/2007 880.48 - - 12.49 867.95
RW-2 9/21/2007 880.48 - - 12.49 867.95
Page 128 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-2 9/26/2007 880.48 - - 12.49 867.95
RW-2 10/5/2007 880.48 - - 12.49 867.95
RW-2 10/12/2007 880.48 - - 12.49 867.95
RW-2 10/19/2007 880.48 - - 12.49 867.95
RW-2 10/26/2007 880.48 - - 12.49 867.99
RW-2 11/2/2007 880.48 - - 12.49 867.99
RW-2 11/9/2007 880.48 - - 12.49 867.99
RW-2 11/17/2007 880.48 - - 12.49 867.99
RW-2 11/30/2007 880.48 - - 12.49 867.99
RW-2 12/8/2007 880.48 - - 12.49 867.99
RW-2 12/17/2007 880.48 - - 12.49 867.99
RW-2 12/21/2007 880.48 - - 12.49 867.99
RW-2 12/27/2007 880.48 - - 12.49 867.99
RW-2 1/4/2008 880.48 - - 9.93 870.55
RW-2 1/11/2008 880.48 - - 10.66 869.78
RW-2 1/18/2008 880.48 - - 9.57 870.91
RW-2 1/26/2008 880.48 - - 10.48 870.00
RW-2 2/8/2008 880.48 - - 9.42 871.06
RW-2 2/22/2008 880.48 - - 9.78 870.70
RW-2 3/1/2008 880.48 - - 9.63 870.85
RW-2 3/10/2008 880.48 - - 8.00 872.48
RW-2 3/14/2008 880.48 - - 8.75 871.73
RW-2 3/28/2008 880.48 - - 8.89 871.59
RW-2 4/18/2008 880.48 - - 8.12 872.36
RW-2 4/30/2008 880.48 - - 6.26 874.22
RW-2 5/2/2008 880.48 - - 6.82 873.66
RW-2 5/9/2008 880.48 - - 7.59 872.89
RW-2 5/16/2008 880.48 - - 7.99 872.49
RW-2 5/24/2008 880.48 - - 8.33 872.15
RW-2 6/6/2008 880.48 - - 8.88 871.60
RW-2 6/13/2008 880.48 - - 9.30 871.18
RW-2 6/20/2008 880.48 - - 9.68 870.80
RW-2 6/27/2008 880.48 - - 10.01 870.47
RW-2 7/11/2008 880.48 - - 10.23 870.25
RW-2 7/18/2008 880.48 - - 10.50 869.98
RW-2 7/25/2008 880.48 - - 10.84 869.64
RW-2 8/1/2008 880.48 - - 11.22 869.26
Page 129 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-2 8/8/2008 880.48 - - 11.60 868.88
RW-2 8/15/2008 880.48 - - 11.99 868.49
RW-2 8/22/2008 880.48 - - 12.35 868.13
RW-2 9/5/2008 880.48 - - 10.97 869.51
RW-2 9/12/2008 880.48 - - 9.89 870.59
RW-2 9/19/2008 880.48 - - 8.93 871.55
RW-2 10/10/2008 880.48 - - 10.07 870.41
RW-2 11/7/2008 880.48 - - 10.11 870.37
RW-2 11/14/2008 880.48 - - 10.54 869.94
RW-2 11/21/2008 880.48 - - 10.25 870.23
RW-2 12/5/2008 880.48 - - 10.09 870.39
RW-2 12/12/2008 880.48 - - 9.99 870.49
RW-2 1/2/2009 880.48 - - 10.00 870.48
RW-2 1/9/2009 880.48 - - 9.99 870.49
RW-2 1/23/2009 880.48 - - 9.94 870.54
RW-2 2/13/2009 880.48 - - 9.99 870.49
RW-2 2/27/2009 880.48 - - 10.04 870.44
RW-2 3/6/2009 880.48 - - 10.19 870.29
RW-2 3/30/2009 880.48 - - 5.54 874.94
RW-2 4/30/2009 880.48 - - 7.44 873.04
RW-2 5/15/2009 880.48 - - 6.94 873.54
RW-2 5/22/2009 880.48 - - 6.90 873.58
RW-2 5/29/2009 880.48 - - 7.36 873.12
RW-2 6/6/2009 880.48 - - 4.83 875.65
RW-2 6/12/2009 880.48 - - 5.99 874.49
RW-2 6/22/2009 880.48 - - 6.51 873.97
RW-2 6/27/2009 880.48 - - 7.12 873.36
RW-2 7/6/2009 880.48 - - 7.56 872.92
RW-2 7/10/2009 880.48 - - 8.12 872.36
RW-2 7/17/2009 880.48 - - 8.41 872.07
RW-2 7/24/2009 880.48 - - 8.80 871.68
RW-2 7/31/2009 880.48 - - 9.10 871.38
RW-2 8/6/2009 880.48 - - 9.38 871.10
RW-2 8/14/2009 880.48 - - 9.76 870.72
RW-2 8/21/2009 880.48 - - 9.99 870.49
RW-2 8/28/2009 880.48 - - 10.23 870.25
RW-2 9/4/2009 880.48 - - 10.40 870.08
Page 130 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-2 9/11/2009 880.48 - - 10.64 869.84
RW-2 9/25/2009 880.48 - - 10.79 869.69
RW-2 10/2/2009 880.48 - - 10.41 870.07
RW-2 10/9/2009 880.48 - - 10.34 870.14
RW-2 10/16/2009 880.48 - - 10.59 869.89
RW-2 10/23/2009 880.48 - - 10.66 869.82
RW-2 11/6/2009 880.48 - - 8.69 871.79
RW-2 11/13/2009 880.48 - - 8.74 871.74
RW-2 11/20/2009 880.48 - - 8.67 871.81
RW-2 12/4/2009 880.48 - - 8.84 871.64
RW-2 12/11/2009 880.48 - - 8.92 871.56
RW-2 12/17/2009 880.48 - - 8.97 871.51
RW-2 1/7/2010 880.48 - - 6.22 874.26
RW-2 1/7/2010 880.48 - - 6.14 874.34
RW-2 1/22/2010 880.48 - - 6.15 874.33
RW-2 1/28/2010 880.48 - - 6.08 874.40
RW-2 2/4/2010 880.48 - - 5.02 875.46
RW-2 2/12/2010 880.48 - - 4.55 875.93
RW-2 11/5/2010 880.48 - - 9.00 871.48
RW-2 1/10/2014 880.48 - - 5.43 875.01
RW-2 1/17/2014 880.48 - - 5.16 875.28
RW-2 1/24/2014 880.48 - - 6.13 874.31
RW-2 1/31/2014 880.48 - - 6.81 873.63
RW-2 2/7/2014 880.48 - - 6.18 874.26
RW-2 2/14/2014 880.48 - - 5.32 875.12
RW-2 2/21/2014 880.48 - - 4.72 875.72
RW-2 2/28/2014 880.48 - - 6.07 874.37
RW-2 3/7/2014 880.48 - - 4.12 876.32
RW-2 3/14/2014 880.48 - - 4.31 876.13
RW-2 3/21/2014 880.48 - - 4.12 876.32
RW-2 3/28/2014 880.48 - - 4.69 875.75
RW-2 4/4/2014 880.48 - - 5.52 874.92
RW-2 4/11/2014 880.48 - - 5.19 875.25
RW-2 4/18/2014 880.48 - - 4.76 875.68
RW-2 4/25/2014 880.48 - - 4.98 875.46
RW-2 5/2/2014 880.48 - - 5.39 875.05
RW-2 5/9/2014 880.48 - - 5.61 874.83
Page 131 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-2 5/16/2014 880.48 - - 5.34 875.10
RW-2 5/23/2014 880.48 - - 6.26 874.18
RW-2 5/30/2014 880.48 - - 6.76 873.68
RW-2 6/6/2014 880.48 - - 7.03 873.41
RW-2 6/13/2014 880.48 - - 7.37 873.07
RW-2 6/20/2014 880.48 - - 7.69 872.75
RW-2 6/27/2014 880.48 - - 7.93 872.51
RW-2 7/5/2014 880.48 - - 8.43 872.01
RW-2 7/11/2014 880.48 - - 8.76 871.68
RW-2 3/5/2015 880.48 - - 4.10 862.63
RW-2 5/27/2015 880.48 - -8.70 871.74
RW-2 6/29/2015 880.48 - -10.32 870.12
RW-2 7/30/2015 880.48 - -11.78 868.66
RW-2 8/20/2015 880.48 - -11.80 868.64
RW-2 9/9/2015 880.48 - -12.38 868.06
RW-2 10/15/2015 880.48 - -9.74 870.70
RW-2 10/26/2015 880.48 - -10.39 870.05
RW-2 12/4/2015 880.48 - -5.55 874.89
RW-2 1/12/2016 880.44 - - 5.53 874.91
RW-2 5/26/2016 880.44 - - 5.21 875.23
RW-2 7/11/2016 880.44 - - 6.06 874.38
RW-2 7/12/2016 880.44 - - 6.06 874.38
RW-2 7/27/2016 880.44 - - 7.94 872.50
RW-2 9/28/2016 880.44 - - 10.55 869.89
RW-2 11/29/2016 880.44 - - 11.09 869.35
RW-2 12/14/2016 880.44 - - 11.05 869.39
RW-2 5/17/2017 880.44 - - 8.70 871.74
RW-2 6/26/2017 880.44 - - 6.04 874.40
RW-2 8/8/2017 880.44 - - 9.77 870.67
RW-2 11/28/2017 880.44 - - 12.04 868.40
RW-2 12/11/2017 880.44 - - 12.23 868.21
RW-2 1/25/2018 880.44 - - 5.85 874.59
RW-2 5/21/2018 880.44 - - 8.67 871.77
RW-2 7/9/2018 880.44 - - 10.28 870.16
RW-2 8/16/2018 880.44 - - 8.51 871.93
RW-2 11/29/2018 880.44 - - 5.98 874.46
RW-2 12/12/2018 880.44 - - 4.81 875.63
Page 132 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
RW-2 3/27/2019 880.44 - - 4.64 875.80
RW-2 5/29/2019 880.44 - - 6.49 873.95
RW-2 6/10/2019 880.44 - - 4.76 875.68
RW-2 8/6/2019 880.44 - - 6.34 874.10
RW-2 11/8/2019 880.44 - - 7.80 872.64
RW-2 12/9/2019 880.44 - - 7.03 873.41
RW-2 3/6/2020 880.44 - - 4.57 875.87
RW-2 6/11/2020 880.44 - - 5.39 875.05
RW-2 8/24/2020 880.44 - - 7.10 873.34
RW-2 11/30/2020 880.44 - - 4.13 876.31
RW-2 12/14/2020 880.44 - - 6.44 874.00
RW-2 3/29/2021 880.44 - - 4.14 876.30
RW-2 6/14/2021 880.44 - - 5.44 875.00
RW-2 9/28/2021 880.44 - - 9.62 870.82
RW-2 12/28/2021 880.44 - - 9.64 870.80
RW-2 4/1/2022 880.44 - - 5.50 874.94
RW-2 6/20/2022 880.44 - - 6.04 874.40
RW-2 9/22/2022 880.44 - - 10.36 870.08
RW-2 12/5/2022 880.44 - - 7.45 872.99
RW-2 4/10/2023 880.44 - - 4.58 875.86
RW-2 7/17/2023 880.44 - - 7.87 872.57
RW-2 9/18/2023 880.44 - - 8.13 872.31
RW-2 12/6/2023 880.44 - - 9.88 870.56
RW-2
SBMW-1R 8/5/2003 893.18 - - 9.62 883.56
SBMW-1R 8/20/2003 893.18 - - 8.10 885.08
SBMW-1R 11/10/2003 893.18 - - 11.05 882.13
SBMW-1R 12/23/2003 893.18 - - 10.45 882.73
SBMW-1R 1/29/2004 893.18 - - 12.10 881.08
SBMW-1R 3/30/2004 893.18 - - 10.99 882.19
SBMW-1R 4/23/2004 893.18 - - 11.29 881.89
SBMW-1R 5/20/2004 893.18 - - 12.66 880.52
SBMW-1R 6/28/2004 893.18 - - 14.57 878.61
SBMW-1R 8/30/2004 893.18 - - 15.25 877.93
SBMW-1R 1/26/2005 893.18 - - 12.65 880.53
SBMW-1R 2/18/2005 893.18 - - 12.03 881.15
RW-2 was aboandoned in February 2024
Page 133 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
SBMW-1R 3/29/2005 893.18 - - 11.08 882.10
SBMW-1R 11/5/2010 893.18 - - 16.68 876.50
SBMW-1R 10/26/2015 893.18 - - 17.50 875.68
SBMW-1R 7/11/2016 893.18 - - 13.21 879.97
SBMW-1R 7/12/2016 893.18 - - 13.21 879.97
SBMW-1R 8/2/2016 893.18 - - 14.36 878.82
SBMW-1R 11/29/2016 893.18 - - 17.93 875.25
SBMW-1R 12/28/2016 893.18 - - 18.52 874.66
SBMW-1R 6/26/2017 893.18 - - 13.85 879.33
SBMW-1R 12/11/2017 893.18 - - 19.68 873.50
SBMW-1R 7/9/2018 893.18 - - 16.69 876.49
SBMW-1R 12/12/2018 893.18 - - 12.88 880.30
SBMW-1R 6/10/2019 893.18 - - 11.91 881.27
SBMW-1R 12/9/2019 893.18 - - 14.05 879.13
SBMW-1R 6/11/2020 893.18 - - 10.07 883.11
SBMW-1R 12/14/2020 893.18 - - 11.00 882.18
SBMW-1R 6/14/2021 893.18 - - 11.95 881.23
SBMW-1R 6/20/2022 893.18 - - 15.47 877.71
SBMW-1R 7/17/2023 893.18 - - 14.39 878.79
SBMW-2R 8/5/2003 891.54 - - 9.28 882.26
SBMW-2R 8/20/2003 892.54 7.59 0.01 7.60 884.95
SBMW-2R 11/10/2003 893.54 - - 10.20 881.34
SBMW-2R 12/23/2003 894.54 - - 10.10 881.44
SBMW-2R 1/29/2004 895.54 - - 11.58 879.96
SBMW-2R 3/30/2004 896.54 - - 10.55 880.99
SBMW-2R 4/23/2004 897.54 - - 10.98 880.56
SBMW-2R 5/20/2004 898.54 - - 12.00 879.54
SBMW-2R 6/28/2004 899.54 - - 13.53 878.01
SBMW-2R 8/30/2004 900.54 - - 14.40 877.14
SBMW-2R 1/26/2005 901.54 - - 12.31 879.23
SBMW-2R 2/18/2005 902.54 - - 11.73 879.81
SBMW-2R 3/29/2005 903.54 - - 11.25 880.29
SBMW-2R 11/5/2010 904.54 - - 15.84 875.70
SBMW-2R 10/26/2015 905.54 - -17.10 874.44
SBMW-2R 10/26/2015 891.54 - - 17.10 874.44
SBMW-2R 7/11/2016 891.54 - - 13.08 878.46
Page 134 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
SBMW-2R 7/12/2016 891.54 - - 13.08 878.46
SBMW-2R 8/2/2016 891.54 - - 13.69 877.85
SBMW-2R 11/29/2016 891.54 - - 17.15 874.39
SBMW-2R 12/14/2016 891.54 - - 17.41 874.13
SBMW-2R 6/26/2017 891.54 - - 14.16 877.38
SBMW-2R 12/11/2017 891.54 - - 18.88 872.66
SBMW-2R 7/9/2018 891.54 - - 16.19 875.35
SBMW-2R 12/12/2018 891.54 - - 12.90 878.64
SBMW-2R 6/10/2019 891.54 - - 11.14 880.40
SBMW-2R 12/9/2019 891.54 - - 13.80 877.74
SBMW-2R 6/11/2020 891.54 - - 9.65 881.89
SBMW-2R 12/14/2020 891.54 - - 10.77 880.77
SBMW-2R 6/14/2021 891.54 - - 11.18 880.36
SBMW-2R 6/20/2022 891.54 - - 14.89 876.65
SBMW-2R 7/17/2023 891.54 - - 14.83 876.71
SBMW-2I 11/10/2003 891.18 - - 9.75 881.43
SBMW-2I 1/29/2004 891.18 - - 11.10 880.08
SBMW-2I 3/30/2004 891.18 - - 10.08 881.10
SBMW-2I 4/23/2004 891.18 - - 10.46 880.72
SBMW-2I 5/20/2004 891.18 - - 11.54 879.64
SBMW-2I 6/28/2004 891.18 - - 13.10 878.08
SBMW-2I 8/30/2004 891.18 - - 13.97 877.21
SBMW-2I 1/26/2005 891.18 - - 11.82 879.36
SBMW-2I 2/18/2005 891.18 - - 11.43 879.75
SBMW-2I 3/29/2005 891.18 - - 10.71 880.47
SBMW-2I 10/26/2015 891.18 - - 16.70 874.48
SBMW-2I 7/11/2016 891.18 - - 12.84 878.34
SBMW-2I 7/12/2016 891.18 - - 12.84 878.34
SBMW-2I 7/28/2016 891.18 - - 12.94 878.24
SBMW-2I 11/29/2016 891.18 - - 16.72 874.46
SBMW-2I 12/16/2016 891.18 - - 17.04 874.14
SBMW-2I 6/26/2017 891.18 - - 13.71 877.47
SBMW-2I 12/11/2017 891.18 - - 18.43 872.75
SBMW-2I 7/9/2018 891.18 - - 15.73 875.45
SBMW-2I 12/12/2018 891.18 - - 12.44 878.74
SBMW-2I 6/10/2019 891.18 - - 10.84 880.34
Page 135 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
SBMW-2I 12/9/2019 891.18 - - 13.35 877.83
SBMW-2I 6/11/2020 891.18 - - 9.22 881.96
SBMW-2I 12/14/2020 891.18 - - 10.30 880.88
SBMW-2I 6/14/2021 891.18 - - 10.76 880.42
SBMW-2I 6/20/2022 891.18 - - 14.42 876.76
SBMW-2I 7/17/2023 891.18 - - 13.39 877.79
SBMW-2D 11/10/2003 890.80 - - 9.48 881.32
SBMW-2D 1/29/2004 890.80 - - 10.80 88-4618
SBMW-2D 3/30/2004 890.80 - - 9.85 880.95
SBMW-2D 4/23/2004 890.80 - - 10.24 880.56
SBMW-2D 5/20/2004 890.80 - - 11.30 879.50
SBMW-2D 6/28/2004 890.80 - - 12.82 877.98
SBMW-2D 8/30/2004 890.80 - - 13.70 877.10
SBMW-2D 1/26/2005 890.80 - - 11.57 879.23
SBMW-2D 2/18/2005 890.80 - - 10.93 879.87
SBMW-2D 3/29/2005 890.80 - - 10.47 880.33
SBMW-2D 10/26/2015 890.80 - -16.39 874.41
SBMW-2D 7/11/2016 890.80 - - 12.65 878.15
SBMW-2D 7/12/2016 890.80 - - 12.65 878.15
SBMW-2D 7/28/2016 890.80 - - 12.68 878.12
SBMW-2D 11/29/2016 890.80 - - 16.47 874.33
SBMW-2D 12/14/2016 890.80 - - 16.71 874.09
SBMW-2D 6/26/2017 890.80 - - 13.33 877.47
SBMW-2D 12/11/2017 890.80 - - 18.19 872.61
SBMW-2D 7/9/2018 890.80 - - 15.51 875.29
SBMW-2D 12/12/2018 890.80 - - 12.10 878.70
SBMW-2D 6/10/2019 890.80 - - 10.52 880.28
SBMW-2D 12/9/2019 890.80 - - 15.01 875.79
SBMW-2D 6/11/2020 890.80 - - 8.96 881.84
SBMW-2D 12/14/2020 890.80 - - 9.99 880.81
SBMW-2D 6/14/2021 890.80 - - 10.50 880.30
SBMW-2D 6/20/2022 890.80 - - 14.23 876.57
SBMW-2D 7/17/2023 890.80 - - 13.18 877.62
SBMW-2B 5/20/2004 892.06 - - 12.53 879.53
SBMW-2B 6/28/2004 892.06 - - 14.10 877.96
Page 136 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
SBMW-2B 8/30/2004 892.06 - - 14.96 877.10
SBMW-2B 1/26/2005 892.06 - - 12.77 879.29
SBMW-2B 2/18/2005 892.06 - - 12.32 879.74
SBMW-2B 3/29/2005 892.06 - - 11.80 880.26
SBMW-2B 10/26/2015 892.06 - -17.62 874.44
SBMW-2B 7/11/2016 892.06 - - 13.21 878.85
SBMW-2B 7/12/2016 892.06 - - 13.21 878.85
SBMW-2B 7/28/2016 892.06 - - 13.88 878.18
SBMW-2B 11/29/2016 892.06 - - 17.72 874.34
SBMW-2B 12/27/2016 892.06 - - 18.24 873.82
SBMW-2B 6/26/2017 892.06 - - 14.51 877.55
SBMW-2B 12/11/2017 892.06 - - 19.40 872.66
SBMW-2B 7/9/2018 892.06 - - 16.72 875.34
SBMW-2B 12/12/2018 892.06 - - 13.30 878.76
SBMW-2B 6/10/2019 892.06 - - 11.74 880.32
SBMW-2B 12/9/2019 892.06 - - 15.20 876.86
SBMW-2B 6/11/2020 892.06 - - 10.17 881.89
SBMW-2B 12/14/2020 892.06 - - 11.20 880.86
SBMW-2B 6/14/2021 892.06 - - 11.71 880.35
SBMW-2B 6/20/2022 892.06 - - 15.41 876.65
SBMW-2B 7/17/2023 892.06 - - 14.39 877.67
PMW-J-I 2/17/2017 888.45 - - 17.45 871.00
PMW-J-I 6/26/2017 888.45 - - 13.91 874.54
PMW-J-I 12/11/2017 888.45 - - 19.69 868.76
PMW-J-I 7/9/2018 888.45 - - 17.35 871.10
PMW-J-I 12/12/2018 888.45 - - 13.48 874.97
PMW-J-I 6/10/2019 888.45 - - 12.48 875.97
PMW-J-I 12/9/2019 888.45 - - 14.85 873.60
PMW-J-I 6/11/2020 888.45 - - 11.11 877.34
PMW-J-I 12/14/2020 888.45 - - 12.12 876.33
PMW-J-I 6/14/2021 888.45 - - 12.82 875.63
PMW-J-I 6/20/2022 888.45 - - 16.29 872.16
PMW-J-I 7/17/2023 888.45 - - 15.32 873.13
PMW-J-D 2/17/2017 888.35 - - 17.36 870.99
PMW-J-D 6/26/2017 888.35 - - 13.85 874.50
Page 137 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-J-D 12/11/2017 888.35 - - 19.54 868.81
PMW-J-D 7/9/2018 888.35 - - 17.68 870.67
PMW-J-D 12/12/2018 888.35 - - 13.39 874.96
PMW-J-D 6/10/2019 888.35 - - 12.39 875.96
PMW-J-D 12/9/2019 888.35 - - 14.79 873.56
PMW-J-D 6/11/2020 888.35 - - 11.03 877.32
PMW-J-D 12/14/2020 888.35 - - 12.00 876.35
PMW-J-D 6/14/2021 888.35 - - 12.98 875.37
PMW-J-D 6/20/2022 888.35 - - 16.24 872.11
PMW-J-D 7/17/2023 888.35 - - 15.38 872.97
PMW-J-B 2/17/2017 885.57 - - 14.55 871.02
PMW-J-B 6/26/2017 885.57 - - 10.96 874.61
PMW-J-B 12/11/2017 885.57 - - 16.94 868.63
PMW-J-B 7/9/2018 885.57 - - 14.46 871.11
PMW-J-B 12/12/2018 885.57 - - 10.56 875.01
PMW-J-B 6/10/2019 885.57 - - 4.58 880.99
PMW-J-B 12/9/2019 885.57 - - 12.00 873.57
PMW-J-B 6/11/2020 885.57 - - 8.20 877.37
PMW-J-B 12/14/2020 885.57 - - 9.20 876.37
PMW-J-B 6/14/2021 885.57 - - 9.96 875.61
PMW-J-B 6/20/2022 885.57 - - 13.40 872.17
PMW-J-B 7/17/2023 885.57 - - 12.47 873.10
PMW-K-I 2/16/2017 891.75 - - 16.75 875.00
PMW-K-I 6/26/2017 891.75 - - 13.60 878.15
PMW-K-I 12/11/2017 891.75 - - 19.20 872.55
PMW-K-I 7/9/2018 891.75 - - 16.40 875.35
PMW-K-I 12/12/2018 891.75 - - 12.58 879.17
PMW-K-I 6/10/2019 891.75 - - 11.46 880.29
PMW-K-I 12/9/2019 891.75 - - 13.65 878.10
PMW-K-I 6/11/2020 891.75 - - 9.73 882.02
PMW-K-I 12/14/2020 891.75 - - 10.63 881.12
PMW-K-I 6/14/2021 891.75 - - 11.51 880.24
PMW-K-I 6/20/2022 891.75 - - 15.05 876.70
PMW-K-I 7/17/2023 891.75 - - 14.00 877.75
Page 138 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-K-D 2/16/2017 892.16 - - 17.20 874.96
PMW-K-D 6/26/2017 892.16 - - 13.96 878.20
PMW-K-D 12/11/2017 892.16 - - 19.62 872.54
PMW-K-D 7/9/2018 892.16 - - 16.76 875.40
PMW-K-D 12/12/2018 892.16 - - 12.96 879.20
PMW-K-D 6/10/2019 892.16 - - 11.84 880.32
PMW-K-D 12/9/2019 892.16 - - 14.50 877.66
PMW-K-D 6/11/2020 892.16 - - 10.14 882.02
PMW-K-D 12/14/2020 892.16 - - 11.02 881.14
PMW-K-D 6/14/2021 892.16 - - 11.94 880.22
PMW-K-D 6/20/2022 892.16 - - 15.50 876.66
PMW-K-D 7/17/2023 892.16 - - 14.44 877.72
PMW-K-B 2/16/2017 889.07 - - 14.04 875.03
PMW-K-B 6/26/2017 889.07 - - 10.91 878.16
PMW-K-B 12/11/2017 889.07 - - 16.53 872.54
PMW-K-B 7/9/2018 889.07 - - 13.70 875.37
PMW-K-B 12/12/2018 889.07 - - 9.85 879.22
PMW-K-B 6/10/2019 889.07 - - 8.73 880.34
PMW-K-B 12/9/2019 889.07 - - 10.99 878.08
PMW-K-B 6/11/2020 889.07 - - 7.07 882.00
PMW-K-B 12/14/2020 889.07 - - 7.90 881.17
PMW-K-B 6/14/2021 889.07 - - 8.83 880.24
PMW-K-B 6/20/2022 889.07 - - 12.37 876.70
PMW-K-B 7/17/2023 889.07 - - 11.35 877.72
PMW-L-I 2/16/2017 891.23 - - 13.27 877.96
PMW-L-I 6/26/2017 891.23 - - 7.37 883.86
PMW-L-I 12/11/2017 891.23 - - 16.63 874.60
PMW-L-I 7/9/2018 891.23 - - 13.21 878.02
PMW-L-I 12/12/2018 891.23 - - 7.63 883.60
PMW-L-I 6/10/2019 891.23 - - 7.65 883.58
PMW-L-I 12/9/2019 891.23 - - 9.20 882.03
PMW-L-I 6/11/2020 891.23 - - 6.05 885.18
PMW-L-I 12/14/2020 891.23 - - 6.40 884.83
PMW-L-I 6/14/2021 891.23 - - 8.36 882.87
PMW-L-I 6/20/2022 891.23 - - 12.02 879.21
Page 139 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-L-I 7/17/2023 891.23 - - 10.78 880.45
PMW-L-D 2/16/2017 891.57 - - 13.69 877.88
PMW-L-D 6/26/2017 891.57 - - 7.95 883.62
PMW-L-D 12/11/2017 891.57 - - 17.04 874.53
PMW-L-D 7/9/2018 891.57 - - 13.64 877.93
PMW-L-D 12/12/2018 891.57 - - 8.17 883.40
PMW-L-D 6/10/2019 891.57 - - 8.05 883.52
PMW-L-D 12/9/2019 891.57 - - 9.70 881.87
PMW-L-D 6/11/2020 891.57 - - 6.51 885.06
PMW-L-D 12/14/2020 891.57 - - 6.84 884.73
PMW-L-D 6/14/2021 891.57 - - 8.79 882.78
PMW-L-D 6/20/2022 891.57 - - 12.51 879.06
PMW-L-D 7/17/2023 891.57 - - 11.22 880.35
PMW-L-B 2/16/2017 888.56 - - 11.10 877.46
PMW-L-B 6/26/2017 888.56 - - 7.87 880.69
PMW-L-B 12/11/2017 888.56 - - 14.02 874.54
PMW-L-B 7/9/2018 888.56 - - 10.65 877.91
PMW-L-B 12/12/2018 888.56 - - 5.48 883.08
PMW-L-B 6/10/2019 888.56 - - 4.80 883.76
PMW-L-B 12/9/2019 888.56 - - 7.00 881.56
PMW-L-B 6/11/2020 888.56 - - 3.76 884.80
PMW-L-B 12/14/2020 888.56 - - 3.80 884.76
PMW-L-B 6/14/2021 888.56 - - 5.55 883.01
PMW-L-B 6/20/2022 888.56 - - 9.32 879.24
PMW-L-B 7/17/2023 888.56 - - 8.20 880.36
PMW-M-I 2/16/2017 888.48 - - 17.80 870.68
PMW-M-I 6/26/2017 888.48 - - 15.03 873.45
PMW-M-I 12/11/2017 888.48 - - 20.08 868.40
PMW-M-I 7/9/2018 888.48 - - 15.05 873.43
PMW-M-I 12/12/2018 888.48 - - 14.36 874.12
PMW-M-I 6/10/2019 888.48 - - 13.76 874.72
PMW-M-I 12/9/2019 888.48 - - 15.49 872.99
PMW-M-I 6/11/2020 888.48 - - 12.49 875.99
PMW-M-I 12/15/2020 888.48 - - 12.76 875.72
Page 140 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-M-I 6/14/2021 888.48 - - 13.89 874.59
PMW-M-I 6/20/2022 888.48 - - 16.95 871.53
PMW-M-I 7/17/2023 888.48 - - 16.09 872.39
PMW-M-D 2/17/2017 888.10 - - 17.55 870.55
PMW-M-D 6/26/2017 888.10 - - 14.54 873.56
PMW-M-D 12/11/2017 888.10 - - 19.73 868.37
PMW-M-D 7/9/2018 888.10 - - 17.70 870.40
PMW-M-D 12/12/2018 888.10 - - 13.89 874.21
PMW-M-D 6/10/2019 888.10 - - 13.16 874.94
PMW-M-D 12/9/2019 888.10 - - 15.11 872.99
PMW-M-D 6/11/2020 888.10 - - 12.03 876.07
PMW-M-D 12/15/2020 888.10 - - 12.25 875.85
PMW-M-D 6/14/2021 888.10 - - 13.54 874.56
PMW-M-D 6/20/2022 888.10 - - 16.69 871.41
PMW-M-D 12/5/2022 888.10 - - 17.34 870.76
PMW-M-D 7/17/2023 888.10 - - 15.74 872.36
PMW-M-D 12/6/2023 888.10 - - 19.18 868.92
PMW-M-B 2/17/2017 885.06 - - 14.44 870.62
PMW-M-B 6/26/2017 885.06 - - 11.27 873.79
PMW-M-B 12/11/2017 885.06 - - 15.18 869.88
PMW-M-B 7/9/2018 885.06 - - 14.44 870.62
PMW-M-B 12/12/2018 885.06 - - 8.27 876.79
PMW-M-B 6/10/2019 885.06 - - 6.50 878.56
PMW-M-B 12/9/2019 885.06 - - 10.63 874.43
PMW-M-B 6/11/2020 885.06 - - 5.22 879.84
PMW-M-B 12/15/2020 885.06 - - 11.98 873.08
PMW-M-B 6/14/2021 885.06 - - 7.16 877.90
PMW-M-B 6/20/2022 885.06 - - 11.99 873.07
PMW-M-B 7/17/2023 885.06 - - 2.02 883.04
PMW-N-I 2/16/2017 888.48 - - 15.35 873.13
PMW-N-I 6/26/2017 888.48 - - 12.27 876.21
PMW-N-I 12/11/2017 888.48 - - 17.90 870.58
PMW-N-I 7/9/2018 888.48 - - 15.55 872.93
PMW-N-I 12/12/2018 888.48 - - 11.93 876.55
Page 141 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-N-I 6/10/2019 888.48 - - 11.10 877.38
PMW-N-I 12/9/2019 888.48 - - 12.96 875.52
PMW-N-I 6/11/2020 888.48 - - 4.44 884.04
PMW-N-I 12/15/2020 888.48 - - 10.03 878.45
PMW-N-I 6/14/2021 888.48 - - 11.20 877.28
PMW-N-I 6/20/2022 888.48 - - 14.32 874.16
PMW-N-I 7/17/2023 888.48 - - 13.38 875.10
PMW-N-D 2/16/2017 888.26 - - 14.89 873.37
PMW-N-D 6/26/2017 888.26 - - 12.87 875.39
PMW-N-D 12/11/2017 888.26 - - 17.42 870.84
PMW-N-D 7/9/2018 888.26 - - 14.95 873.31
PMW-N-D 12/12/2018 888.26 - - 11.33 876.93
PMW-N-D 6/10/2019 888.26 - - 10.51 877.75
PMW-N-D 12/9/2019 888.26 - - 12.36 875.90
PMW-N-D 6/11/2020 888.26 - - 5.81 882.45
PMW-N-D 12/15/2020 888.26 - - 9.36 878.90
PMW-N-D 6/14/2021 888.26 - - 10.57 877.69
PMW-N-D 6/20/2022 888.26 - - 13.81 874.45
PMW-N-D 7/17/2023 888.26 - - 12.84 875.42
PMW-N-B 2/16/2017 885.18 - - 11.60 873.58
PMW-N-B 6/26/2017 885.18 - - 8.90 876.28
PMW-N-B 12/11/2017 885.18 - - 13.71 871.47
PMW-N-B 7/9/2018 885.18 - - 10.97 874.21
PMW-N-B 12/12/2018 885.18 - - 0.00 885.18
PMW-N-B 6/10/2019 885.18 - - 0.50 884.68
PMW-N-B 12/9/2019 885.18 - - 4.25 880.93
PMW-N-B 6/11/2020 885.18 - - 2.50 882.68
PMW-N-B 12/15/2020 885.18 - - 8.42 876.76
PMW-N-B 6/14/2021 885.18 - - 3.51 881.67
PMW-N-B 6/20/2022 885.18 - - 8.28 876.90
PMW-N-B 7/17/2023 885.18 - - 4.56 880.62
PMW-O-I 2/17/2017 880.66 - - 10.43 870.23
PMW-O-I 6/26/2017 880.66 - - 7.21 873.45
PMW-O-I 12/11/2017 880.66 - - 12.64 868.02
Page 142 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-O-I 7/9/2018 880.66 - - 10.60 870.06
PMW-O-I 12/12/2018 880.66 - - 6.71 873.95
PMW-O-I 6/10/2019 880.66 - - 6.08 874.58
PMW-O-I 12/9/2019 880.66 - - 8.10 872.56
PMW-O-I 6/11/2020 880.66 - - 5.00 875.66
PMW-O-I 12/15/2020 880.66 - - 5.19 875.47
PMW-O-I 6/14/2021 880.66 - - 6.50 874.16
PMW-O-I 6/20/2022 880.66 - - 9.56 871.10
PMW-O-I 7/17/2023 880.66 - - 8.03 872.63
PMW-O-D 2/17/2017 880.10 - - 9.95 870.15
PMW-O-D 6/26/2017 880.10 - - 6.76 873.34
PMW-O-D 12/11/2017 880.10 - - 12.14 867.96
PMW-O-D 7/9/2018 880.10 - - 10.11 869.99
PMW-O-D 12/12/2018 880.10 - - 6.24 873.86
PMW-O-D 6/10/2019 880.10 - - 5.63 874.47
PMW-O-D 12/9/2019 880.10 - - 7.60 872.50
PMW-O-D 6/11/2020 880.10 - - 4.55 875.55
PMW-O-D 12/15/2020 880.10 - - 6.21 873.89
PMW-O-D 6/14/2021 880.10 - - 6.24 873.86
PMW-O-D 6/20/2022 880.10 - - 9.09 871.01
PMW-O-D 7/17/2023 880.10 - - 8.73 871.37
PMW-O-B 2/17/2017 877.39 - - 7.10 870.29
PMW-O-B 6/26/2017 877.39 - - 3.92 873.47
PMW-O-B 12/11/2017 877.39 - - 8.83 868.56
PMW-O-B 7/9/2018 877.39 - - 7.26 870.13
PMW-O-B 12/12/2018 877.39 - - 3.56 873.83
PMW-O-B 6/10/2019 877.39 - - 2.86 874.53
PMW-O-B 12/9/2019 877.39 - - 4.89 872.50
PMW-O-B 6/11/2020 877.39 - - 1.61 875.78
PMW-O-B 12/15/2020 877.39 - - 4.27 873.12
PMW-O-B 6/14/2021 877.39 - - 3.10 874.29
PMW-O-B 6/20/2022 877.39 - - 6.24 871.15
PMW-O-B 7/17/2023 877.39 - - 6.21 871.18
PMW-P-S 1/25/2018 883.26 - - 20.97 862.29
Page 143 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-P-S 7/9/2018 883.26 - - 19.24 864.02
PMW-P-S 12/12/2018 883.26 - - 16.72 866.54
PMW-P-S 6/10/2019 883.26 - - 16.82 866.44
PMW-P-S 12/9/2019 883.26 - - 17.94 865.32
PMW-P-S 6/11/2020 883.26 - - 15.77 867.49
PMW-P-S 12/15/2020 883.26 - - 16.28 866.98
PMW-P-S 6/14/2021 883.26 - - 17.04 866.22
PMW-P-S 6/20/2022 883.26 - - 18.98 864.28
PMW-P-S 7/17/2023 883.26 - - 18.35 864.91
PMW-P-I 1/25/2018 883.38 - - 23.20 860.18
PMW-P-I 7/9/2018 883.38 - - 19.00 864.38
PMW-P-I 12/12/2018 883.38 - - 15.77 867.61
PMW-P-I 6/10/2019 883.38 - - 15.74 867.64
PMW-P-I 12/9/2019 883.38 - - 17.45 865.93
PMW-P-I 6/11/2020 883.38 - - 15.23 868.15
PMW-P-I 12/15/2020 883.38 - - 5.57 877.81
PMW-P-I 6/14/2021 883.38 - - 16.82 866.56
PMW-P-I 6/20/2022 883.38 - - 18.98 864.40
PMW-P-I 7/17/2023 883.38 - - 18.15 865.23
PMW-P-D 1/25/2018 883.36 - - 20.48 862.88
PMW-P-D 7/9/2018 883.36 - - 19.81 863.55
PMW-P-D 12/12/2018 883.36 - - 17.17 866.19
PMW-P-D 6/10/2019 883.36 - - 17.70 865.66
PMW-P-D 12/9/2019 883.36 - - 19.28 864.08
PMW-P-D 6/11/2020 883.36 - - 17.43 865.93
PMW-P-D 12/15/2020 883.36 - - 17.46 865.90
PMW-P-D 6/14/2021 883.36 - - 18.57 864.79
PMW-P-D 6/20/2022 883.36 - - 21.91 861.45
PMW-P-D 7/17/2023 883.36 - - 19.20 864.16
PMW-P-B 1/25/2018 879.84 - - 62.73 817.11
PMW-P-B 7/9/2018 879.84 - - 12.95 866.89
PMW-P-B 12/12/2018 879.84 - - 10.41 869.43
PMW-P-B 6/10/2019 879.84 - - 7.79 872.05
PMW-P-B 12/9/2019 879.84 - - 11.39 868.45
Page 144 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-P-B 6/11/2020 879.84 - - 7.98 871.86
PMW-P-B 12/15/2020 879.84 - - 7.64 872.20
PMW-P-B 6/14/2021 879.84 - - 8.12 871.72
PMW-P-B 6/20/2022 879.84 - - 10.50 869.34
PMW-P-B 7/17/2023 879.84 - - 13.50 866.34
PMW-Q-S 1/25/2018 878.60 - - 19.72 858.88
PMW-Q-S 7/9/2018 878.60 - - 18.72 859.88
PMW-Q-S 12/12/2018 878.60 - - 11.11 867.49
PMW-Q-S 6/10/2019 878.60 - - 10.03 868.57
PMW-Q-S 12/9/2019 878.60 - - 17.01 861.59
PMW-Q-S 6/11/2020 878.60 - - 15.60 863.00
PMW-Q-S 12/15/2020 878.60 - - 8.34 870.26
PMW-Q-S 6/14/2021 878.60 - - 13.31 865.29
PMW-Q-S 6/20/2022 878.60 - - 18.34 860.26
PMW-Q-S 7/17/2023 878.60 - - 16.72 861.88
PMW-Q-I 1/25/2018 878.29 - - 18.54 859.75
PMW-Q-I 7/9/2018 878.29 - - 18.32 859.97
PMW-Q-I 12/12/2018 878.29 - - 15.64 862.65
PMW-Q-I 6/10/2019 878.29 - - 15.92 862.37
PMW-Q-I 12/9/2019 878.29 - - 16.79 861.50
PMW-Q-I 6/11/2020 878.29 - - 15.26 863.03
PMW-Q-I 12/15/2020 878.29 - - 15.27 863.02
PMW-Q-I 6/14/2021 878.29 - - 16.27 862.02
PMW-Q-I 6/20/2022 878.29 - - 18.19 860.10
PMW-Q-I 7/17/2023 878.29 - - 17.56 860.73
PMW-Q-D 1/25/2018 878.28 - - 19.39 858.89
PMW-Q-D 7/9/2018 878.28 - - 18.89 859.39
PMW-Q-D 12/12/2018 878.28 - - 16.33 861.95
PMW-Q-D 6/10/2019 878.28 - - 16.73 861.55
PMW-Q-D 12/9/2019 878.28 - - 17.59 860.69
PMW-Q-D 6/11/2020 878.28 - - 16.21 862.07
PMW-Q-D 12/15/2020 878.28 - - 16.11 862.17
PMW-Q-D 6/14/2021 878.28 - - 17.07 861.21
PMW-Q-D 6/20/2022 878.28 - - 18.93 859.35
Page 145 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-Q-D 7/17/2023 878.28 - - 18.30 859.98
PMW-Q-B 1/25/2018 874.95 - - 15.55 859.40
PMW-Q-B 7/9/2018 874.95 - - 14.51 860.44
PMW-Q-B 12/12/2018 874.95 - - 12.30 862.65
PMW-Q-B 6/10/2019 874.95 - - 12.50 862.45
PMW-Q-B 12/9/2019 874.95 - - 13.45 861.50
PMW-Q-B 6/11/2020 874.95 - - 11.85 863.10
PMW-Q-B 12/15/2020 874.95 - - 11.70 863.25
PMW-Q-B 6/14/2021 874.95 - - 12.84 862.11
PMW-Q-B 6/20/2022 874.95 - - 14.75 860.20
PMW-Q-B 7/17/2023 874.95 - - 14.13 860.82
PMW-R-S 1/25/2018 877.23 - - 20.71 856.52
PMW-R-S 7/9/2018 877.23 - - 21.12 856.11
PMW-R-S 12/12/2018 877.23 - - 17.87 859.36
PMW-R-S 6/10/2019 877.23 - - 17.62 859.61
PMW-R-S 12/9/2019 877.23 - - 18.66 858.57
PMW-R-S 6/11/2020 877.23 - - 17.66 859.57
PMW-R-S 12/15/2020 877.23 - - 17.25 859.98
PMW-R-S 6/14/2021 877.23 - - 17.78 859.45
PMW-R-S 6/20/2022 877.23 - - 19.61 857.62
PMW-R-S 7/17/2023 877.23 - - 19.09 858.14
PMW-R-I 1/25/2018 877.03 - - 19.61 857.42
PMW-R-I 7/9/2018 877.03 - - 19.23 857.80
PMW-R-I 12/12/2018 877.03 - - 16.51 860.52
PMW-R-I 6/10/2019 877.03 - - 16.69 860.34
PMW-R-I 12/9/2019 877.03 - - 17.45 859.58
PMW-R-I 6/11/2020 877.03 - - 16.11 860.92
PMW-R-I 12/15/2020 877.03 - - 15.95 861.08
PMW-R-I 6/14/2021 877.03 - - 16.84 860.19
PMW-R-I 6/20/2022 877.03 - - 18.88 858.15
PMW-R-I 7/17/2023 877.03 - - 18.34 858.69
PMW-R-D 1/25/2018 877.20 - - 19.41 857.79
PMW-R-D 7/9/2018 877.20 - - 19.01 858.19
Page 146 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
PMW-R-D 12/12/2018 877.20 - - 16.28 860.92
PMW-R-D 6/10/2019 877.20 - - 17.14 860.06
PMW-R-D 12/9/2019 877.20 - - 17.27 859.93
PMW-R-D 6/11/2020 877.20 - - 16.06 861.14
PMW-R-D 12/15/2020 877.20 - - 15.83 861.37
PMW-R-D 6/14/2021 877.20 - - 16.79 860.41
PMW-R-D 6/20/2022 877.20 - - 18.81 858.39
PMW-R-D 7/17/2023 877.20 - - 19.01 858.19
PMW-R-B 1/25/2018 873.47 - - 16.73 856.74
PMW-R-B 7/9/2018 873.47 - - 16.32 857.15
PMW-R-B 12/12/2018 873.47 - - 13.29 860.18
PMW-R-B 6/10/2019 873.47 - - 14.16 859.31
PMW-R-B 12/9/2019 873.47 - - 15.55 857.92
PMW-R-B 6/11/2020 873.47 - - 13.69 859.78
PMW-R-B 12/15/2020 873.47 - - 13.25 860.22
PMW-R-B 6/14/2021 873.47 - - 13.99 859.48
PMW-R-B 6/20/2022 873.47 - - 16.23 857.24
PMW-R-B 7/17/2023 873.47 - - 16.35 857.12
SG-1 5/21/2018 871.49 - - 0.41 871.08
SG-1 7/9/2018 871.49 - - 0.00 871.49
SG-1 8/16/2018 871.49 - - 0.95 870.54
SG-1 11/29/2018 871.49 - - 0.60 870.89
SG-1 12/13/2018 871.49 - - 0.66 870.83
SG-1 3/27/2019 871.49 - - 0.56 870.93
SG-1 5/30/2019 871.49 - - 0.00 871.49
SG-1 6/14/2019 871.49 - - 0.46 871.03
SG-1 8/6/2019 871.49 - - 0.87 870.62
SG-1 12/9/2019 871.49 - - 0.61 870.88
SG-1 3/6/2020 871.49 - - 0.60 870.89
SG-1 6/11/2020 871.49 - - 0.38 871.11
SG-1 8/24/2020 871.49 - - 0.66 870.83
SG-1 11/30/2020 871.49 - - 1.06 870.43
SG-1 12/14/2020 871.49 - - 0.88 870.61
SG-1 3/29/2021 871.49 - - 0.67 870.82
SG-1 6/14/2021 871.49 - - 0.26 871.23
Page 147 of 148
Table 3
Historical Groundwater Elevation Data - Offsite Wells
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Top of Casing
Elevation
Depth to
Product
Product
Thickness
Depth to
Water
Groundwater
Elevation
SG-1 9/28/2021 871.49 - - 0.00 871.49
SG-1 12/28/2021 871.49 - - 0.00 871.49
SG-1 4/1/2022 871.49 - - 0.40 871.09
SG-1 6/20/2022 871.49 - - 0.12 871.37
SG-1 9/22/2022 871.49 - - 0.60 870.89
SG-1 12/5/2022 871.49 - - 0.78 870.71
SG-1 7/17/2023 871.49 - - 0.08 871.41
SG-1 9/18/2023 871.49 - - 0.16 871.33
SG-1 12/6/2023 871.49 - - 0.40 871.09
SG-1 3/1/2024 871.49 - - 0.74 870.75
Notes:
ft - feet
NA - not applicable
Page 148 of 148
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
Units - °C mg/L mV NTU mg/L mg/L mg/L mg/L mg/L ug/mg/L
Z1-X01 11/3/2015 18.49 0.62 37.9 4.92 NA NA NA NA NA NA NA
Z1-X01 7/15/2016 21.42 0.35 107 1.62 NA NA NA NA NA NA NA
Z1-X01 12/15/2016 13.37 0.63 53.1 6.71 NA NA NA NA NA NA NA
Z1-X01 6/29/2017 19.94 0.30 211.5 4.32 NA NA NA NA NA NA NA
Z1-X01 12/12/2017 17.15 0.17 56.6 5.32 NA NA NA NA NA NA NA
Z1-X01 7/9/2018 21.99 0.21 121.1 7.02 NA NA NA NA NA NA NA
Z1-X01 12/17/2018 19.05 1.80 20.1 4.43 NA NA NA NA NA NA NA
Z1-X01 6/10/2019 19.90 0.90 15.9 3.79 NA NA NA NA NA NA NA
Z1-X01 12/9/2019 19.84 0.25 198.5 5.29 NA NA NA NA NA NA NA
Z1-X01 6/15/2020 18.80 0.16 25.1 8.18 NA NA NA NA NA NA NA
Z1-X01 12/15/2020 12.60 0.62 47.3 58.09 NA NA NA NA NA NA NA
Z1-X01 6/14/2021 20.40 0.52 66.3 10.31 NA NA NA NA NA NA NA
Z1-X01 6/20/2022 19.40 0.18 30.9 9.08 NA NA NA NA NA NA NA
Z1-X01 7/18/2023 17.50 0.44 94.8 4.59 NA NA NA NA NA NA NA
Z1-X25 11/3/2015 24.19 0.48 204.8 3.02 NA NA NA NA NA NA NA
Z1-X25 7/15/2016 26.41 0.31 129.1 0.63 NA NA NA NA NA NA NA
Z1-X25 12/15/2016 16.53 0.53 32.6 4.9 NA NA NA NA NA NA NA
Z1-X25 6/29/2017 25.21 0.50 218.6 1.14 NA NA NA NA NA NA NA
Z1-X25 12/12/2017 23.77 0.21 34.1 1.28 NA NA NA NA NA NA NA
Z1-X25 7/9/2018 23.21 0.31 92.2 7.76 NA NA NA NA NA NA NA
Z1-X25 12/17/2018 22.90 2.30 38.8 1.79 NA NA NA NA NA NA NA
Z1-X25 6/10/2019 22.89 0.60 50.1 1.17 NA NA NA NA NA NA NA
Z1-X25 12/9/2019 23.17 0.15 176.8 3.22 NA NA NA NA NA NA NA
Z1-X27 11/3/2015 22.75 0.52 91.5 6.78 NA NA NA NA NA NA NA
Z1-X27 7/18/2016 23.52 0.29 23.1 4.03 1.61 0.116 3.21 2.50 HF <1.00 42 113
Z1-X27 12/15/2016 20.64 0.32 44.2 6.53 1.49 <0.0400 3.51 1.63 HF <1.00 58.5 155
Z1-X27 6/27/2017 23.52 0.32 23.3 7.0 0.94 <0.0300 > 3.57 E 2.48 0.93 25.8 165
Z1-X27 12/13/2017 20.59 0.23 45.2 2.89 3.30 <0.0300 > 2.51 E 1.03 1.26 33.2 196
Z1-X27 7/9/2018 NA NA 25.7 2.47 1.12 <0.0300 2.68 1.76 0.902 94.1 194
Z1-X27 12/19/2018 21.37 0.14 34.6 6.31 3.39 0.0850 J 3.63 3.61 1.54 14.3 121
Z1-X27 6/10/2019 19.90 0.10 84.7 6.13 0.00 0.410 J 3.1 1.29 0.538 119 110
Z1-X27 12/9/2019 17.62 1.07 147.3 5.98 0.00 <0.0600 3.98 3.09 0.440 J 79.2 169
Z1-X27 6/15/2020 19.70 0.19 50.7 6.82 0.03 <0.150 3.88 1.45 1.26 50.1 105
Z1-X27 12/17/2020 18.90 0.49 52.0 9.4 0.93 <0.150 3.52 3.00 0.941 64.4 105
Z1-X27 6/14/2021 30.40 1.09 34.6 7.12 0.00 <0.150 2.74 1.48 0.751 28.3 90.3
Z1-X27 6/20/2022 20.50 0.08 57.9 5.41 0.14 0.230 J 3.25 4.63 0.911 86.5 148
Z1-X27 7/18/2023 19.00 1.24 9.2 3.78 0.04 <0.300 3.21 2.16 0.778 93.4 152
Z1-X28 11/5/2015 22.65 0.65 77.4 9.92 NA NA NA NA NA NA NA
Z1-X28 7/18/2016 25.3 0.35 -100 4.04 0.85 <0.0400 14 53.1 ^ HF <1.00 29.6 295
Z1-X28 12/12/2016 20.73 0.31 -40.9 9.7 2.16 <0.0400 12.2 21.7 HF <1.00 154 200
Z1-X28 6/26/2017 25.27 0.80 -82.8 4.33 1.22 0.669 J 11.7 21.5 0.469 J 234 257
Z1-X28 7/9/2018 26.19 0.61 -40.1 7.4 0.12 1.16 9.37 58.7 1.35 228 221
Z1-X28 12/19/2018 22.80 0.19 -122.2 13.1 4.98 0.0950 J 11.5 33.6 0.543 31.1 418
Z1-X28 6/10/2019 24.21 0.38 -94.0 16.7 3.3 0.254 J 12.5 51.8 <0.200 812 255
Z1-X28 12/9/2019 16.06 2.99 89.8 6.49 0.12 <0.0600 13.1 22.3 <0.200 489 268
Z1-X28 6/15/2020 18.50 0.32 -102.9 4.39 3.30 <0.150 17.2 33.8 <0.200 396 266
Z1-X28 12/17/2020 17.80 0.49 -114.2 6.21 0.22 1.02 10.6 33.0 1.40 606 271
Z1-X28 6/14/2021 21.80 0.51 -89.9 0.48 0.75 <0.150 11.9 37.7 0.358 J 436 219
Z1-X28 6/20/2022 24.10 0.44 -43.9 5.83 0.03 0.232 J 12.0 21.2 0.286 J 1,040 181
Z1-X28 7/18/2023 27.80 2.62 -80.4 9.56 0.12 <0.300 13.2 216 7.45 1,270 247
Z2-PZ-06 11/3/2015 18.25 0.99 71.8 5.08 NA NA NA NA NA NA NA
Z2-PZ-06 7/15/2016 24.03 0.59 122 37.0 NA NA NA NA NA NA NA
Z2-PZ-06 6/28/2017 22.52 1.91 60.7 141 NA NA NA NA NA NA NA
Z2-PZ-06 12/14/2017 14.92 1.86 72.8 NA NA NA NA NA NA NA NA
Z2-PZ-06 7/9/2018 NA NA NA NA NA NA NA
Z2-PZ-06 12/19/2018 18.46 10.98 154.70 76.0 NA NA NA NA NA NA NA
Z2-PZ-06 6/12/2019 17.48 5.84 30.50 21.6 NA NA NA NA NA NA NA
Z2-PZ-06 12/11/2019 16.05 0.90 105.40 5.6 NA NA NA NA NA NA NA
Z2-PZ-06 6/21/2020 21.00 1.63 271.30 35.3 NA NA NA NA NA NA NA
Z2-PZ-06 12/17/2020 17.30 1.52 178.30 9.90 NA NA NA NA NA NA NA
Z2-PZ-06 6/16/2021 20.60 0.43 -13.40 98.24 NA NA NA NA NA NA NA
Z2-PZ-06 6/20/202 23.00 0.27 179.30 25.37 NA NA NA NA NA NA NA
Z2-PZ-06 7/19/202 22.80 1.38 -115.10 4.80 NA NA NA NA NA NA NA
Onsite Wells
an insuffient water level, parameters were not able to b
Page 1 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
Z2-PZ-08 11/3/2015 18.3 7.57 -13.5 6.42 NA NA NA NA NA NA NA
Z2-PZ-08 7/19/2016 22.16 1.18 -61.3 9.8 NA NA NA NA NA NA NA
Z2-PZ-08 6/28/2017 18.65 2.43 -15.8 30.3 NA NA NA NA NA NA NA
Z2-PZ-08 7/9/2018 NA NA NA NA NA NA NA
Z2-PZ-08 12/19/2018 NA NA NA NA NA NA NA
Z2-PZ-08 6/12/2019 17.50 6.84 59.20 30.10 NA NA NA NA NA NA NA
Z2-PZ-08 12/11/2019 11.60 5.14 2.20 NA NA NA NA NA NA NA NA
Z2-PZ-08 6/21/2020 NA NA NA NA NA NA NA
Z2-PZ-08 12/17/2020 16.2 0.94 66.4 8.90 NA NA NA NA NA NA NA
Z2-PZ-08 6/16/2021 19.7 0.48 105.1 45.02 NA NA NA NA NA NA NA
Z2-PZ-08 6/21/2022 21.6 0.55 139.5 5.65 NA NA NA NA NA NA NA
Z2-PZ-08 7/19/2023 20.8 0.21 -93.4 4.60 NA NA NA NA NA NA NA
Z2-PZ-09 11/4/2015 20.29 5.41 -9.6 10.1 NA NA NA NA NA NA NA
Z2-PZ-09 7/18/2016 27.46 0.16 -82.4 194 NA NA NA NA NA NA NA
Z2-PZ-09 7/7/2017 25.00 0.44 -97.2 232 NA NA NA NA NA NA NA
Z2-PZ-09 12/15/2017 17.59 1.80 -148.5 NA NA NA NA NA NA NA NA
Z2-PZ-09 7/9/2018 NA NA NA NA NA NA NA
Z2-PZ-09 12/19/2018 14.44 0.30 -79.80 32.1 NA NA NA NA NA NA NA
Z2-PZ-09 6/11/2019 21.20 0.24 12.70 14.9 NA NA NA NA NA NA NA
Z2-PZ-09 12/11/2019 16.45 1.21 -61.60 25.5 NA NA NA NA NA NA NA
Z2-PZ-09 6/21/2020 20.60 0.39 -105.10 9.8 NA NA NA NA NA NA NA
Z2-PZ-09 12/17/2020 16.90 0.47 -68.80 7.9 NA NA NA NA NA NA NA
Z2-PZ-09 6/16/2021 21.10 0.35 -106.70 28.14 NA NA NA NA NA NA NA
Z2-PZ-09 6/21/2022 21.00 0.24 76.80 10.19 NA NA NA NA NA NA NA
Z2-PZ-09 12/12/2022 NA NA NA NA NA NA NA
Z2-PZ-09 7/19/2023 22.10 0.17 168.40 7.57 NA NA NA NA NA NA NA
Z2-PZ-09 2/2/2024 17.98 1.42 -261.20 192.00 NA NA NA NA NA NA NA
Z2-PZ-10 11/5/2015 23.24 1.18 78.4 70.8 NA NA NA NA NA NA NA
Z2-PZ-10 7/18/2016 27.53 0.15 -59.2 8.97 NA NA NA NA NA NA NA
Z2-PZ-10 7/7/2017 24.98 0.50 -98.4 202 NA NA NA NA NA NA NA
Z2-PZ-10 12/15/2017 20.13 0.29 -80.5 68.7 NA NA NA NA NA NA NA
Z2-PZ-10 7/9/2018 23.21 0.11 -33.1 64.3 NA NA NA NA NA NA NA
Z2-PZ-10 12/19/2018 17.21 1.68 -43.9 9.23 NA NA NA NA NA NA NA
Z2-PZ-10 6/11/2019 21.72 0.16 25.4 15.5 NA NA NA NA NA NA NA
Z2-PZ-10 12/11/2019 16.24 1.70 214.2 25.0 NA NA NA NA NA NA NA
Z2-PZ-10 6/21/2020 21.90 0.19 -83.2 133.6 NA NA NA NA NA NA NA
Z2-PZ-10 12/17/2020 18.70 1.48 -66.0 11.3 NA NA NA NA NA NA NA
Z2-PZ-10 6/16/2021 21.40 0.61 -62.7 21.76 NA NA NA NA NA NA NA
Z2-PZ-10 6/21/2022 23.60 0.25 13.5 12.14 NA NA NA NA NA NA NA
Z2-PZ-10 7/19/2023 21.00 1.12 77.0 2.84 NA NA NA NA NA NA NA
Z2-X03 11/3/2015 22.75 0.52 91.5 6.78 NA NA NA NA NA NA NA
Z2-X03 7/15/2016 23.86 0.25 32.9 3.86 NA NA NA NA NA NA NA
Z2-X03 12/15/2016 18.90 0.51 26.7 6.9 NA NA NA NA NA NA NA
Z2-X03 6/29/2017 23.64 0.21 184.0 2.47 NA NA NA NA NA NA NA
Z2-X03 12/12/2017 17.98 0.42 15.4 8.73 NA NA NA NA NA NA NA
Z2-X03 7/9/2018 24.17 0.24 63.5 9.5 NA NA NA NA NA NA NA
Z2-X03 12/17/2018 21.24 0.80 63.5 9.94 NA NA NA NA NA NA NA
Z2-X03 6/10/2019 23.04 0.44 88.2 12.8 NA NA NA NA NA NA NA
Z2-X03 12/9/2019 19.05 1.51 261.7 2.9 NA NA NA NA NA NA NA
Z2-X16 11/3/2015 26.61 0.37 -7.6 5.32 NA NA NA NA NA NA NA
Z2-X16 7/13/2016 28.15 0.32 66.7 1.15 NA NA NA NA NA NA NA
Z2-X16 12/15/2016 23.22 0.31 -26.3 9.7 NA NA NA NA NA NA NA
Z2-X16 6/29/2017 27.76 0.25 13.3 1.36 NA NA NA NA NA NA NA
Z2-X16 12/12/2017 25.67 0.14 -36.9 16.4 NA NA NA NA NA NA NA
Z2-X16 7/9/2018 27.90 0.09 -56.0 11.02 NA NA NA NA NA NA NA
Z2-X16 12/17/2018 20.62 0.92 42.2 19.0 NA NA NA NA NA NA NA
Z2-X16 6/10/2019 24.99 0.33 46.7 9.5 NA NA NA NA NA NA NA
Z2-X16 12/9/2019 18.90 1.94 111.5 9.9 NA NA NA NA NA NA NA
Z2-X16 6/15/2020 21.80 1.00 102.7 23.36 NA NA NA NA NA NA NA
Z2-X16 12/15/2020 18.00 0.51 77.3 8.13 NA NA NA NA NA NA NA
Z2-X16 6/14/2021 25.60 0.42 -19.8 50.94 NA NA NA NA NA NA NA
Z2-X16 6/20/2022 22.90 0.48 50.7 8.77 NA NA NA NA NA NA NA
Z2-X16 7/18/2023 21.00 0.15 -74.7 2.85 NA NA NA NA NA NA NA
Z2-X18 11/3/2015 19.84 1.7 165.4 3.4 NA NA NA NA NA NA NA
Z2-X18 7/14/2016 23.29 1.64 41.8 6.24 NA NA NA NA NA NA NA
o an insuffient water level, parameters were not able to b
an insuffient water level, parameters were not able to b
an insuffient water level, parameters were not able to b
an insuffient water level, parameters were not able to b
an insuffient water level, parameters were not able to b
Page 2 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
Z2-X18 12/15/2016 16.45 0.54 61.6 6.9 NA NA NA NA NA NA NA
Z2-X18 6/29/2017 22.15 1.14 207.7 1.66 NA NA NA NA NA NA NA
Z2-X18 12/11/2017 18.45 2.72 67.5 4.1 NA NA NA NA NA NA NA
Z2-X18 7/10/2018 23.87 0.79 55.7 5.93 NA NA NA NA NA NA NA
Z2-X18 12/17/2018 16.36 3.34 108.3 8.12 NA NA NA NA NA NA NA
Z2-X18 6/10/2019 20.50 1.85 61.5 11.8 NA NA NA NA NA NA NA
Z2-X18 12/9/2019 16.13 5.34 328.1 5.92 NA NA NA NA NA NA NA
Z2-X20 11/3/2015 25.92 0.24 16.8 2.84 NA NA NA NA NA NA NA
Z2-X20 7/18/2016 28.45 0.36 44.9 3.71 0.39 0.469 4.36 1.85 HF 5.73 50.9 121
Z2-X20 12/12/2016 24.91 0.21 14 6.74 1.96 <0.0400 4.64 8.20 HF <1.00 209 117
Z2-X20 6/29/2017 27.89 0.57 -28.7 8.27 2.92 <0.0300 > 4.34 E 12.1 0.303 J 139 150
Z2-X20 12/13/2017 27.17 0.16 -62.0 3.26 3.30 <0.0300 > 4.09 E 13.2 1.03 231 146
Z2-X20 7/10/2018 NA 3.08 -13.7 2.09 1.16 <0.0300 4.39 9.92 1.18 90 158
Z2-X20 12/19/2018 25.20 0.19 -35.2 10.66 4.79 <0.0300 4.45 6.35 2.80 14.1 192
Z2-X20 6/10/2019 25.19 0.09 67.2 8.62 0.00 3.03 4.05 0.687 12.20 36.7 223
Z2-X20 12/10/2019 21.46 2.08 96.6 7.68 2.43 <0.0600 3.72 2.76 2.88 28.9 180
Z2-X20 6/22/2020 23.00 0.24 7.3 10.32 0.44 <0.150 5.33 1.84 4.53 70.9 221
Z2-X20 12/17/2020 14.20 0.63 2.0 26.38 3.30 0.538 J 5.32 3.91 5.48 155 202
Z2-X20 6/15/2021 22.50 0.60 -11.9 5.23 1.00 <0.150 5.34 7.89 11.70 221 194
Z2-X20 6/20/2022 23.80 0.39 -80.2 3.5 0.21 0.520 J 6.66 8.5 3.02 305 210
Z2-X20 7/19/2023 21.10 4.19 -48.1 9.21 1.21 <0.300 4.84 11.8 6.73 450 219
Z2-X29 11/3/2015 19.23 1.27 227.7 18.4 NA NA NA NA NA NA NA
Z2-X29 7/14/2016 23.84 0.33 152.4 4.89 NA NA NA NA NA NA NA
Z2-X29 12/13/2016 17.67 0.34 74.5 9.8 NA NA NA NA NA NA NA
Z2-X29 6/27/2017 21.17 0.29 77.0 15.0 NA NA NA NA NA NA NA
Z2-X29 12/12/2017 14.81 0.62 -63.4 8.7 NA NA NA NA NA NA NA
Z2-X29 7/10/2018 22.71 0.23 66.1 9.03 NA NA NA NA NA NA NA
Z2-X29 12/17/2018 16.91 4.49 172.9 8.2 NA NA NA NA NA NA NA
Z2-X29 6/11/2019 18.69 1.69 56.0 10.5 NA NA NA NA NA NA NA
Z2-X29 12/10/2019 16.83 3.24 246.9 32.5 NA NA NA NA NA NA NA
Z2-X29 6/15/2020 18.70 0.50 245.8 4.71 NA NA NA NA NA NA NA
Z2-X29 12/15/2020 14.30 3.15 240.0 52.97 NA NA NA NA NA NA NA
Z2-X29 6/16/2021 20.80 1.17 190.7 22.0 NA NA NA NA NA NA NA
Z2-X29 6/21/2022 21.70 0.67 150.5 27.4 NA NA NA NA NA NA NA
Z2-X29 7/17/2023 19.00 0.14 78.0 25.4 NA NA NA NA NA NA NA
Z2-X31 11/4/2015 28.67 0.26 -74.5 4.24 NA NA NA NA NA NA NA
Z2-X31 7/13/2016 29.8 0.19 -37.4 3.58 NA NA NA NA NA NA NA
Z2-X31 12/14/2016 25.94 0.28 -8.4 3.8 NA NA NA NA NA NA NA
Z2-X31 6/27/2017 30.17 0.21 -25.7 9.0 NA NA NA NA NA NA NA
Z2-X31 12/13/2017 23.85 0.31 3.2 1.11 NA NA NA NA NA NA NA
Z2-X31 7/10/2018 30.04 1.07 -48.3 3.42 NA NA NA NA NA NA NA
Z2-X31 12/17/2018 26.07 0.16 -132.7 5.83 NA NA NA NA NA NA NA
Z2-X31 6/11/2019 25.07 0.45 -143.9 2.7 NA NA NA NA NA NA NA
Z2-X31 12/10/2019 22.43 1.06 137.4 1.62 NA NA NA NA NA NA NA
Z2-X31 6/15/2020 23.20 0.16 -118.0 2.05 NA NA NA NA NA NA NA
Z2-X31 12/15/2020 20.00 0.27 -143.7 8.6 NA NA NA NA NA NA NA
Z2-X31 6/14/2021 24.40 0.36 -92.0 7.69 NA NA NA NA NA NA NA
Z2-X31 6/22/2022 24.50 0.09 -28.7 2.98 NA NA NA NA NA NA NA
Z2-X31 7/18/2023 23.10 0.35 -90.3 13.55 NA NA NA NA NA NA NA
Z2-X35 11/4/2015 22.79 0.46 154.5 82.3 NA NA NA NA NA NA NA
Z2-X35 7/14/2016 26.2 0.41 -3 7.24 NA NA NA NA NA NA NA
Z2-X35 6/27/2017 24.47 0.27 73.4 41.0 NA NA NA NA NA NA NA
Z2-X35 12/17/2018 22.17 0.15 -13.2 2.91 NA NA NA NA NA NA NA
Z2-X35 6/11/2019 21.12 2.21 149.2 6.89 NA NA NA NA NA NA NA
Z2-X35 12/10/2019 20.21 2.48 248.9 9.80 NA NA NA NA NA NA NA
Z2-X35 6/22/2020 20.80 0.59 6.58 9.50 NA NA NA NA NA NA NA
Z2-X35 12/15/2020 20.52 0.98 12.80 5.42 NA NA NA NA NA NA NA
Z2-X35 6/14/2021 20.90 0.71 46.00 8.51 NA NA NA NA NA NA NA
Z2-X35 6/20/2022 24.10 0.24 45.10 2.74 NA NA NA NA NA NA NA
Z2-X35 7/19/2023 24.10 1.47 28.70 6.63 NA NA NA NA NA NA NA
Z3-X80 11/5/2015 33.18 0.77 161 11.7 NA NA NA NA NA NA NA
Z3-X80 7/19/2016 31.74 0.24 -15.5 4.76 0.12 0.122 5.61 0.408 HF 3.84 8.64 158
Z3-X80 12/10/2016 25.55 0.65 -13.4 40.5 2.01 <0.0400 6.25 0.626 HF <1.00 24 165
Z3-X80 6/28/2017 30.99 0.19 -0.4 1.12 1.19 <0.0300 > 6.76 E 1.07 1.78 10.1 232
Z3-X80 12/13/2017 29.54 0.14 -0.6 1.63 1.12 <0.0300 > 5.99 E 1.22 0.634 21 233
Page 3 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
Z3-X80 7/10/2018 31.06 0.19 2.2 7.91 0.00 <0.0300 4.12 2.61 10.3 18.9 207
Z3-X80 12/18/2018 18.16 0.18 -3.4 10.7 0.21 0.317 4.37 1.26 3.96 8.28 237
Z3-X80 6/11/2019 27.36 1.98 96.7 0.9 0.00 0.766 J 3.34 0.0350 J 2.9 12.5 188
Z3-X80 12/10/2019 24.02 1.62 151.9 5.24 0.00 <0.0600 4.61 0.174 2.31 10.2 198
Z3-X80 6/22/2020 25.90 0.24 131.2 0.98 0.00 <0.150 3.24 0.0350 J 1.98 4.0 164
Z3-X80 12/17/2020 20.60 0.65 31.4 8.3 0.60 1.19 5.90 2.40 2.26 4.6 173
Z3-X80 6/16/2021 25.00 0.33 -9.6 8.04 1.19 <0.150 4.99 1.92 1.52 9.29 183
Z3-X80 6/21/2022 26.00 0.42 11.5 9.2 0.17 0.280 J 6.46 0.910 1.14 12.00 220
Z3-X80 7/18/2023 20.70 0.08 -16.8 6.44 0.00 <0.300 4.12 1.840 1.21 12.20 204
Z3-X82 11/5/2015 29.32 1.28 137.8 10.8 NA NA NA NA NA NA NA
Z3-X82 7/13/2016 29.83 0.22 5.7 3.06 NA NA NA NA NA NA NA
Z3-X82 12/14/2016 23.08 0.56 11.7 14.7 NA NA NA NA NA NA NA
Z3-X82 6/27/2017 18.10 0.48 14.7 6.0 NA NA NA NA NA NA NA
Z3-X82 12/12/2017 26.54 0.13 -14.6 16.4 NA NA NA NA NA NA NA
Z3-X82 7/10/2018 28.10 0.89 -4.7 6.02 NA NA NA NA NA NA NA
Z3-X82 12/17/2018 26.54 0.06 12.1 8.88 NA NA NA NA NA NA NA
Z3-X82 6/11/2019 25.85 0.32 25.8 14.3 NA NA NA NA NA NA NA
Z3-X82 12/9/2019 25.90 2.40 56.9 9.45 NA NA NA NA NA NA NA
Z3-X82 6/15/2020 23.30 0.19 -2.2 14.61 NA NA NA NA NA NA NA
Z3-X82 12/15/2020 20.30 1.52 71.9 8.44 NA NA NA NA NA NA NA
Z3-X82 6/15/2021 23.80 0.43 -13.4 8.94 NA NA NA NA NA NA NA
Z3-X82 6/22/2022 24.50 0.91 4.9 5.04 NA NA NA NA NA NA NA
Z3-X82 7/18/2023 22.70 1.25 -12.7 8.07 NA NA NA NA NA NA NA
Z4-PZ04 11/4/2015 25.02 0.17 -84.8 44 NA NA NA NA NA NA NA
Z4-PZ04 7/19/2016 26.66 0.45 -23.9 32.6 NA NA NA NA NA NA NA
Z4-PZ04 12/13/2016 19.77 0.75 6.4 116 NA NA NA NA NA NA NA
Z4-PZ04 7/7/2017 25.34 1.27 71.5 343 NA NA NA NA NA NA NA
Z4-PZ04 12/15/2017 19.02 1.53 -10.1 32.5 NA NA NA NA NA NA NA
Z4-PZ04 7/9/2018 23.50 6.54 -4.1 122.2 NA NA NA NA NA NA NA
Z4-PZ04 12/19/2018 18.78 3.81 169.6 110.0 NA NA NA NA NA NA NA
Z4-PZ04 6/10/2019 22.94 0.52 67.9 20.1 NA NA NA NA NA NA NA
Z4-PZ04 12/11/2019 17.66 1.29 80.4 11.6 NA NA NA NA NA NA NA
Z4-PZ04 6/21/2020 21.90 0.30 -6.9 35.5 NA NA NA NA NA NA NA
Z4-PZ04 12/17/2020 18.20 3.99 154.1 12.6 NA NA NA NA NA NA NA
Z4-PZ04 6/16/2021 22.40 2.57 -57.1 114.05 NA NA NA NA NA NA NA
Z4-PZ04 6/21/2022 21.20 0.32 -60.1 30.91 NA NA NA NA NA NA NA
Z4-PZ04 7/19/2023 21.90 1.08 -133.4 2.99 NA NA NA NA NA NA NA
Z4-PZ07 11/4/2015 23.18 2.66 89.3 5.08 NA NA NA NA NA NA NA
Z4-PZ07 7/14/2016 25.19 2.19 27.9 125 NA NA NA NA NA NA NA
Z4-PZ07 12/13/2016 20.58 0.39 625 8.7 NA NA NA NA NA NA NA
Z4-PZ07 7/7/2017 23.97 1.50 68.3 53 NA NA NA NA NA NA NA
Z4-PZ07 12/12/2017 19.76 0.86 22.1 10.1 NA NA NA NA NA NA NA
Z4-PZ07 7/10/2018 22.76 1.55 61.0 52.1 NA NA NA NA NA NA NA
Z4-PZ07 12/19/2018 18.90 0.86 44.4 4.28 NA NA NA NA NA NA NA
Z4-PZ07 6/10/2019 21.24 0.27 88.1 10.4 NA NA NA NA NA NA NA
Z4-PZ07 12/11/2019 17.19 1.73 58.2 8.32 NA NA NA NA NA NA NA
Z4-PZ07 6/21/2020 21.60 0.64 -1.8 10.3 NA NA NA NA NA NA NA
Z4-PZ07 12/17/2020 16.30 0.69 -18.0 5.3 NA NA NA NA NA NA NA
Z4-PZ07 6/16/2021 19.10 1.11 -11.6 1.36 NA NA NA NA NA NA NA
Z4-PZ07 6/21/2022 20.10 0.41 10.1 8.18 NA NA NA NA NA NA NA
Z4-PZ07 7/19/2023 21.50 1.24 -47.5 8.61 NA NA NA NA NA NA NA
Z4-PZ09 11/4/2015 20.74 0.87 41.8 10.2 NA NA NA NA NA NA NA
Z4-PZ09 7/18/2016 25.52 0.38 -27.3 29 NA NA NA NA NA NA NA
Z4-PZ09 12/13/2016 11.6 2.35 35.9 20.2 NA NA NA NA NA NA NA
Z4-PZ09 6/28/2017 22.26 1.98 19.8 16.5 NA NA NA NA NA NA NA
Z4-PZ09 7/10/2018 NA NA NA NA NA NA NA
Z4-PZ09 12/18/2018 18.19 0.47 30.9 2.69 NA NA NA NA NA NA NA
Z4-PZ09 6/10/201 NA NA NA NA NA NA NA
Z4-PZ09 12/10/201 18.40 1.71 32.10 6.01 NA NA NA NA NA NA NA
Z4-PZ09 6/21/202 21.90 0.45 20.90 23.7 NA NA NA NA NA NA NA
Z4-PZ09 12/17/202 12.90 2.54 63.30 7.40 NA NA NA NA NA NA NA
Z4-PZ09 6/16/2021 18.50 0.69 12.80 1.26 NA NA NA NA NA NA NA
Z4-PZ09 6/21/202 18.80 0.61 9.80 14.20 NA NA NA NA NA NA NA
Z4-PZ09 7/19/202 20.20 1.24 -33.40 6.88 NA NA NA NA NA NA NA
Z4-X21 11/4/2015 27.39 0.71 30.1 24.2 NA NA NA NA NA NA NA
o an insuffient water level, parameters were not able to b
an insuffient water level, parameters were not able to b
Page 4 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
Z4-X21 7/13/2016 30.07 0.21 -9 5.08 NA NA NA NA NA NA NA
Z4-X21 12/14/2016 24.77 0.33 46.9 18.4 NA NA NA NA NA NA NA
Z4-X21 6/27/2017 28.39 15.90 6.0 12.8 NA NA NA NA NA NA NA
Z4-X21 12/11/2017 27.41 0.16 33.3 9.2 NA NA NA NA NA NA NA
Z4-X21 7/10/2018 25.81 0.27 16.2 9.48 NA NA NA NA NA NA NA
Z4-X21 12/18/2018 23.36 0.53 -26.4 30.5 NA NA NA NA NA NA NA
Z4-X21 6/11/2019 22.60 1.60 -293.7 15.3 NA NA NA NA NA NA NA
Z4-X21 12/9/2019 20.99 1.06 89.9 9.91 NA NA NA NA NA NA NA
Z4-X21 6/15/2020 21.60 0.18 -25.5 10.17 NA NA NA NA NA NA NA
Z4-X21 12/15/2020 19.70 0.94 46.1 7.80 NA NA NA NA NA NA NA
Z4-X21 6/15/2021 21.80 0.44 -14.2 6.51 NA NA NA NA NA NA NA
Z4-X21 6/21/2022 21.20 0.39 65.2 8.7 NA NA NA NA NA NA NA
Z4-X21 7/18/2023 20.20 0.16 -8.1 10.02 NA NA NA NA NA NA NA
Z4-X30 11/4/2015 28.75 0.21 306 41.1 NA NA NA NA NA NA NA
Z4-X30 7/14/2016 29.59 0.23 37.4 4.46 NA NA NA NA NA NA NA
Z4-X30 12/14/2016 23.22 0.48 36.1 12.4 NA NA NA NA NA NA NA
Z4-X30 6/29/2017 28.47 0.67 -5.6 26.6 NA NA NA NA NA NA NA
Z4-X30 12/13/2017 21.18 0.34 39.3 10.9 NA NA NA NA NA NA NA
Z4-X30 7/10/2018 NA 7.27 -10.2 1.57 NA NA NA NA NA NA NA
Z4-X30 12/18/2018 17.82 3.45 112.9 27.1 NA NA NA NA NA NA NA
Z4-X30 6/11/2019 25.30 1.62 57.8 11.4 NA NA NA NA NA NA NA
Z4-X30 12/10/2019 22.14 0.41 232.3 13.4 NA NA NA NA NA NA NA
Z4-X30 6/15/2020 22.50 0.25 83.4 9.29 NA NA NA NA NA NA NA
Z4-X30 12/15/2020 16.30 1.39 128.4 9.8 NA NA NA NA NA NA NA
Z4-X30 6/15/2021 23.00 1.01 18.8 7.04 NA NA NA NA NA NA NA
Z4-X30 6/21/2022 23.60 0.30 8.0 8.7 NA NA NA NA NA NA NA
Z4-X30 7/19/2023 22.30 3.20 -16.8 8.55 NA NA NA NA NA NA NA
Z4-X35 11/4/2015 35.63 0.52 -85.5 4.94 NA NA NA NA NA NA NA
Z4-X35 7/13/2016 36.97 0.11 -14.7 4.45 NA NA NA NA NA NA NA
Z4-X35 12/14/2016 28.06 0.48 -43.2 6.2 NA NA NA NA NA NA NA
Z4-X35 6/27/2017 31.93 0.54 -1.6 4.86 NA NA NA NA NA NA NA
Z4-X35 12/13/2017 23.23 0.28 59.9 3.67 NA NA NA NA NA NA NA
Z4-X35 7/10/2018 NA 4.10 -210.1 2.56 NA NA NA NA NA NA NA
Z4-X35 12/17/2018 30.08 0.34 -99.8 10.2 NA NA NA NA NA NA NA
Z4-X35 6/11/2019 26.51 1.70 -296.4 21.2 NA NA NA NA NA NA NA
Z4-X35 12/10/2019 23.51 0.55 100.0 5.3 NA NA NA NA NA NA NA
Z4-X35 6/15/2020 23.00 0.23 -75.6 10.21 NA NA NA NA NA NA NA
Z4-X35 12/17/2020 17.60 0.43 -87.9 3.91 NA NA NA NA NA NA NA
Z4-X35 6/15/2021 26.60 0.71 -62.9 8.17 NA NA NA NA NA NA NA
Z4-X35 6/21/2022 25.00 0.40 40.0 4.9 NA NA NA NA NA NA NA
Z4-X35 7/18/2023 24.10 1.21 -82.9 4.27 NA NA NA NA NA NA NA
Z4-X47 11/4/2015 28.53 0.35 -99.5 5.73 NA NA NA NA NA NA NA
Z4-X47 7/13/2016 30.05 0.21 -63.1 3.02 NA NA NA NA NA NA NA
Z4-X47 12/14/2016 23.3 0.28 -56.3 10.1 NA NA NA NA NA NA NA
Z4-X47 6/27/2017 29.39 0.20 -67.7 8.0 NA NA NA NA NA NA NA
Z4-X47 12/11/2017 27.11 0.19 -83.7 1.25 NA NA NA NA NA NA NA
Z4-X47 7/10/2018 NA 9.55 -87.8 1.07 NA NA NA NA NA NA NA
Z4-X47 12/18/2018 18.90 2.05 -55.1 7.14 NA NA NA NA NA NA NA
Z4-X47 6/11/2019 24.38 0.14 -23.1 2.47 NA NA NA NA NA NA NA
Z4-X47 12/10/2019 23.98 5.29 -58.0 2.44 NA NA NA NA NA NA NA
Z4-X47 6/15/2020 22.10 0.23 -92.6 99.03 NA NA NA NA NA NA NA
Z4-X47 12/17/2020 20.10 0.95 -99.1 16.21 NA NA NA NA NA NA NA
Z4-X47 6/16/2021 23.20 0.33 -89.3 6.77 NA NA NA NA NA NA NA
Z4-X47 6/21/202 24.50 1.01 -79.5 7.8 NA NA NA NA NA NA NA
Z4-X47 7/18/202 23.10 0.04 -104.4 102.13 NA NA NA NA NA NA NA
Z4-X55 11/4/2015 23.61 9.61 71.2 34.4 NA NA NA NA NA NA NA
Z4-X55 7/13/2016 26.59 0.78 37 3.29 NA NA NA NA NA NA NA
Z4-X55 12/14/2016 19.17 0.62 87.5 19.8 NA NA NA NA NA NA NA
Z4-X55 6/28/2017 25.01 0.57 74.3 15.0 NA NA NA NA NA NA NA
Z4-X55 12/11/2017 24.39 0.30 12.9 5.42 NA NA NA NA NA NA NA
Z4-X55 7/10/2018 24.26 0.24 34.5 14.1 NA NA NA NA NA NA NA
Z4-X55 12/18/2018 18.68 22.90 40.0 7.21 NA NA NA NA NA NA NA
Z4-X55 6/11/2019 20.70 3.80 -23.6 40.8 NA NA NA NA NA NA NA
Z4-X55 12/10/2019 21.67 0.59 29.0 12.06 NA NA NA NA NA NA NA
Z4-X63 11/5/2015 34.49 0.34 -42.1 38.2 NA NA NA NA NA NA NA
Page 5 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
Z4-X63 7/13/2016 33.44 0.15 -49.7 3.73 NA NA NA NA NA NA NA
Z4-X63 12/14/2016 24.87 0.51 -32.1 8.4 NA NA NA NA NA NA NA
Z4-X63 6/28/2017 29.21 0.14 -36.5 12.3 NA NA NA NA NA NA NA
Z4-X63 12/11/2017 31.56 0.19 -57.2 7.12 NA NA NA NA NA NA NA
Z4-X63 7/10/2018 30.00 0.10 -57.8 13.2 NA NA NA NA NA NA NA
Z4-X63 12/18/2018 13.14 0.80 -20.6 5.93 NA NA NA NA NA NA NA
Z4-X63 6/11/2019 27.34 0.09 -41.4 6.78 NA NA NA NA NA NA NA
Z4-X63 12/10/2019 26.21 0.18 -106.7 5.49 NA NA NA NA NA NA NA
Z4-X63 6/15/2020 20.30 1.21 88.7 9.58 NA NA NA NA NA NA NA
Z4-X63 12/17/2020 17.70 0.64 -113.21 8.77 NA NA NA NA NA NA NA
Z4-X63 6/15/2021 24.90 0.30 -104.9 4.04 NA NA NA NA NA NA NA
Z4-X63 6/22/2022 24.90 0.13 -65.1 3.49 NA NA NA NA NA NA NA
Z4-X63 7/19/2023 22.80 0.40 -94.6 3.84 NA NA NA NA NA NA NA
Z4-X68 11/4/2015 30.12 0.47 -42.8 2.55 NA NA NA NA NA NA NA
Z4-X68 7/14/2016 32.33 0.22 -42.1 6.32 NA NA NA NA NA NA NA
Z4-X68 12/14/2016 26.08 0.36 -17.3 6.4 NA NA NA NA NA NA NA
Z4-X68 6/28/2017 26.37 0.71 -6.1 8.42 NA NA NA NA NA NA NA
Z4-X68 12/12/2017 23.24 0.35 48.9 10.12 NA NA NA NA NA NA NA
Z4-X68 7/10/2018 29.52 0.17 -27.6 5.44 NA NA NA NA NA NA NA
Z4-X68 12/18/2018 21.71 2.60 -19.7 5.31 NA NA NA NA NA NA NA
Z4-X68 6/11/2019 25.40 0.94 -29.0 6.4 NA NA NA NA NA NA NA
Z4-X68 12/10/2019 21.87 1.15 -27.3 3.09 NA NA NA NA NA NA NA
Z4-X68 6/15/2020 23.00 1.04 -74.9 9.60 NA NA NA NA NA NA NA
Z4-X68 12/17/2020 21.90 0.52 -153.8 9.60 NA NA NA NA NA NA NA
Z4-X68 6/16/2021 23.60 0.30 -95.6 4.23 NA NA NA NA NA NA NA
Z4-X68 6/22/2022 24.20 0.07 -66.1 4.76 NA NA NA NA NA NA NA
Z4-X68 7/19/2023 21.70 5.44 -77.0 2.42 NA NA NA NA NA NA NA
Z4-X70 11/4/2015 35.19 0.4 -82.3 4.83 NA NA NA NA NA NA NA
Z4-X70 7/19/2016 36.31 0.12 -87.3 3.89 1.00 <0.0400 7.53 5.32 HF <1.00 508 228
Z4-X70 12/14/2016 27.93 0.48 -61.3 21.2 1.65 <0.0400 7.00 2.51 HF <1.00 200 226
Z4-X70 6/28/2017 34.43 0.10 -74.1 12.9 1.23 <0.0300 > 6.85 E 4.3 0.439 J 580 270
Z4-X70 12/14/2017 32.93 0.87 -54.1 11.1 2.36 <0.0300 > 6.84 E 3.04 0.450 J 38.2 254
Z4-X70 7/10/2018 33.79 0.02 -141.9 6.32 0.04 0.0520 J 7.45 3.98 0.904 79.6 293
Z4-X70 12/18/2018 19.27 0.97 -100.2 6.92 0.64 0.0790 J 9.5 6.58 1.9 509 303
Z4-X70 6/11/2019 29.61 0.02 -51.5 9.09 0.00 0.243 J 10.9 15.2 1.51 552 336
Z4-X70 12/10/2019 26.46 0.92 -95.0 8.41 1.01 <0.0600 10.2 0.876 10.6 1,990 317
Z4-X70 6/22/2020 27.80 0.20 -152.1 3.48 1.30 <0.150 11.8 17.4 0.639 1,720 383
Z4-X70 12/17/2020 23.40 0.47 -99.1 2.3 3.24 0.922 J 11.6 6.17 0.830 1,280 355
Z4-X70 6/15/2021 27.00 0.26 -117.1 6.7 1.04 <0.150 10.7 15.4 1.74 1,090 374
Z4-X70 6/21/2022 27.10 0.06 -91.4 3.08 1.05 0.302 13.9 7.6 1.64 566 386
Z4-X70 7/18/2023 24.50 0.16 -100.8 13.91 +++ <0.300 15.4 19 1.12 2,090 424
Z4-X72 11/4/2015 33.56 0.46 -25.8 1.83 NA NA NA NA NA NA NA
Z4-X72 7/19/2016 35.89 0.20 -17.5 4.07 1.49 0.116 3.76 2.56 HF <1.00 585 181
Z4-X72 12/16/2016 28.2 0.45 -37.5 0.93 2.34 <0.0400 3.33 2.10 HF <1.00 760 174
Z4-X72 6/28/2017 33.29 0.17 -26.2 1.08 1.38 0.345 J 3.84 E 2.15 1.96 168 196
Z4-X72 12/14/2017 33.95 0.13 -49.6 13.1 1.93 <0.0300 2.71 E 2.2 0.451 J 319 213
Z4-X72 7/10/2018 32.83 0.16 -62.9 9.21 0.00 <0.0300 3.81 14 4.28 165 203
Z4-X72 12/18/2018 23.47 0.24 30.9 9.27 0.87 0.121 J 4.5 0.50 3.26 11.6 171
Z4-X72 6/10/2019 28.96 0.09 11.2 10.5 2.37 0.338 J 5.51 6.99 0.666 113 219
Z4-X72 12/10/2019 26.14 0.31 -26.8 3.58 0.00 <0.0600 5.17 2.29 1.29 168 220
Z4-X72 6/15/2020 25.80 1.17 -57.4 4.32 0.32 <0.150 5.68 5.00 1.73 178 211
Z4-X72 12/17/2020 19.70 0.52 56.5 8.2 0.00 1.89 4.53 0.641 3.01 213 134
Z4-X72 6/15/2021 27.20 0.26 -108.5 0.95 0.80 <0.150 11.5 16.2 1.88 2,010 370
Z4-X72 6/21/2022 28.10 0.30 -70.0 45.88 0.11 0.214 J 8.25 6.9 0.63 1,610 265
Z4-X72 7/18/2023 20.20 0.08 -96.1 6.55 0.00 <0.300 7.96 9.7 0.703 2,200 261
Z4-X89 11/4/2015 37.4 0.26 -55.6 30.7 NA NA NA NA NA NA NA
Z4-X89 7/19/2016 37.72 0.16 -35.5 8.66 1.39 0.123 7.05 13.6 ^ HF <1.00 401 163
Z4-X89 12/28/2016 31.56 0.38 10.0 4.9 2.09 <0.0400 5.81 8.89 HF <1.00 455 106
Z4-X89 6/28/2017 35.52 0.55 8.70 4.33 2.66 <0.0300 <6.33 E 12.1 0.605 132 183
Z4-X89 12/11/2017 26.44 1.85 28.6 51.4 3.10 <0.0300 <4.25 E 8.12 0.386 J 159 95.8
Z4-X89 7/10/2018 33.99 0.10 -14.8 2.97 3.30 <0.0300 7.14 14.6 0.266 J 93.7 171
Z4-X89 12/19/2018 27.12 0.20 0.7 5.75 0.61 0.0790 J 3.13 0.142 5.36 6.26 333
Z4-X89 6/10/2019 30.36 0.04 21.1 9.37 3.06 0.320 J 5.50 7.54 4.44 814 257
Z4-X89 12/10/2019 26.55 1.21 52.7 5.61 0.00 <0.0600 4.33 2.55 8.42 1,140 238
Z4-X89 6/22/2020 28.00 0.23 -26.6 9.64 0.60 <0.150 4.93 4.58 3.76 987 266
Z4-X89 12/17/2020 23.80 0.33 -12.3 46.76 2.17 <0.150 2.25 2.98 4.33 346 209
Page 6 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
Z4-X89 6/14/2021 27.80 0.53 -47.8 8.07 0.06 <0.150 6.53 7.65 1.96 2,390 280
Z4-X89 6/21/2022 25.50 0.46 66.4 9.6 1.60 0.232 J 10.30 10.1 0.578 1,260 228
Z4-X89 7/18/2023 24.20 0.15 -92.0 34.63 +++ <0.300 10.10 15.1 0.785 1,890 260
MW-A-I 10/27/2015 31 0.44 55.1 3.82 NA NA NA NA NA NA NA
MW-A-I 7/19/2016 31.23 0.1 39.8 7.5 0.90 0.104 1.25 0.668 HF <1.00 35.7 132
MW-A-I 12/14/2016 29.73 0.19 -75.3 50 1.85 <0.0400 1.7 4.71 HF <1.00 38.6 128
MW-A-I 6/26/2017 28.21 0.37 95.0 11.71 2.70 <0.0300 0.674 0.479 1.7 8.81 130
MW-A-I 12/11/2017 27.61 0.15 10.0 10.0 0.50 <0.0300 0.739 1.01 1.67 9.33 123
MW-A-I 7/9/2018 28.85 0.25 13.3 10.0 0.33 <0.0300 0.669 0.798 1.38 6.86 116
MW-A-I 12/17/2018 21.43 3.00 47.0 21.4 0.00 0.0780 J 0.531 0.793 1.41 3.17 107
MW-A-I 6/10/2019 27.39 0.61 50.1 12.7 0.00 0.445 J 0.385 0.314 1.87 5.81 101
MW-A-I 12/10/2019 20.69 1.50 69.3 9.8 0.64 <0.0600 0.546 0.918 1.49 3.89 93.5
MW-A-I 6/15/2020 20.00 3.14 104.1 3.75 0.00 <0.150 0.564 0.093 1.61 3.50 91.4
MW-A-I 12/14/2020 21.10 0.48 43.3 9.75 0.24 <0.150 0.341 0.175 1.48 2.84 85.5
MW-A-I 6/14/2021 25.20 0.45 45.7 15.38 0.00 <0.150 0.323 0.592 1.60 3.22 93.5
MW-A-I 6/20/2022 28.30 1.52 88.6 9.60 0.02 0.253 J 0.552 0.965 0.869 1.65 92.4
MW-A-I 7/18/2023 26.10 0.60 43.2 7.62 0.04 <0.300 0.496 1.74 0.919 4.02 116
MW-A-D 10/27/2015 29.64 0.16 -31.7 22.7 NA NA NA NA NA NA NA
MW-A-D 7/19/2016 30.41 0.09 -34.9 9.6 1.88 0.108 4.08 3.24 HF <1.00 125 263
MW-A-D 12/13/2016 29.2 0.1 -134.8 23.2 2.06 <0.0400 4.86 3.98 HF <1.00 131 243
MW-A-D 6/26/2017 28.95 0.11 20.0 2.88 3.30 0.523 J > 4.94 E 1.52 0.708 46.3 240
MW-A-D 12/11/2017 27.79 0.07 -21.0 0.86 0.99 <0.0300 > 4.00 E 2.49 0.549 28.4 241
MW-A-D 7/9/2018 28.21 0.07 -32.1 26.7 NA <0.0300 3.47 3 0.429 38.6 239
MW-A-D 12/17/2018 22.97 10.1 27.9 62.3 2.09 0.0810 J 4.91 3.2 0.592 0.399 J 217
MW-A-D 6/10/2019 26.44 1.87 -28.2 2.04 0.74 0.328 J 4.36 1.9 <0.200 53.9 192
MW-A-D 12/10/2019 21.93 2.83 165.3 9.02 0.82 <0.0600 3.57 1.5 0.273 J 22.9 182
MW-A-D 6/15/2020 23.80 0.10 -23.6 1.57 1.15 <0.150 4.44 1.29 0.686 34.1 166
MW-A-D 12/14/2020 21.50 0.36 -52.6 3.82 0.26 <0.150 3.93 0.935 0.593 14.9 160
MW-A-D 6/14/2021 25.10 0.48 10.4 9.3 0.00 <0.150 2.97 1.28 0.616 15.5 156
MW-A-D 6/20/2022 25.20 0.60 4.7 5.6 0.57 0.254 J 3.21 0.538 0.470 J 11.3 172
MW-A-D 7/18/2023 23.10 1.19 -23.9 5.60 0.00 <0.300 2.96 1.22 0.746 14.3 149
MW-A-B 12/2/2015 28.09 2.9 182.5 11.0 NA NA NA NA NA NA NA
MW-A-B 7/19/2016 29.03 0.19 6.3 4.92 NA <0.0400 3.88 0.111 HF <1.00 57.7 307
MW-A-B 12/14/2016 27.88 0.18 -132.1 5.47 1.09 <0.0400 3.39 0.277 HF 4.54 52 318
MW-A-B 6/27/2017 27.93 2.49 -8.6 8.80 0.04 1.09 0.0737 0.0210 J 14 0.796 191
MW-A-B 12/11/2017 26.78 0.13 29.6 2.09 0.15 <0.0300 > 3.41 E 0.248 1.97 29.7 354
MW-A-B 7/9/2018 27.93 3.80 78.4 8.4 0.00 0.423 0.0254 <0.0200 12.6 0.768 150
MW-A-B 12/17/2018 24.14 38.10 34.6 28.9 0.00 0.241 0.0152 <0.0200 5.34 3.23 97.9
MW-A-B 6/10/2019 28.25 0.68 57.3 71 0.00 0.710 J 0.0409 1.17 3.08 1.79 76.5
MW-A-B 12/11/2019 19.27 2.20 25.4 10.4 0.00 <0.0600 0.0187 0.243 3.99 1.2 74.7
MW-A-B 6/15/2020 22.90 0.17 111.8 26.94 0.26 <0.150 0.167 0.65 1.97 2.35 65.9
MW-A-B 12/14/2020 19.80 1.02 68.4 105.38 0.00 1.04 0.185 0.185 3.92 1.67 53.9
MW-A-B 6/14/2021 25.00 0.33 44.2 95.47 0.12 <0.150 0.160 0.578 2.06 1.86 47.1
MW-A-B 6/20/2022 23.60 1.50 71.9 7.8 0.03 0.238 J 0.026 0.717 3.02 1.74 52.6
MW-A-B 7/18/2023 22.60 1.19 -12.6 7.21 0.00 <0.300 0.024 1.64 1.7 1.07 58.4
MW-B-I 10/27/2015 33.97 1.27 -33.3 9.7 NA NA NA NA NA NA NA
MW-B-I 7/19/2016 36.47 1.65 -4.1 6.79 1.71 0.111 2.65 1.22 HF <1.00 46.4 311
MW-B-I 12/13/2016 33.26 1.42 0.3 -21 2.05 <0.0400 2.57 3.47 HF <1.00 109 305
MW-B-I 6/28/2017 33.13 0.32 19.5 25.6 2.11 <0.0300 > 3.16 E 1.71 1.66 50.2 372
MW-B-I 12/13/2017 20.45 0.31 116.7 9.84 0.10 <0.0300 > 2.58 E 0.785 0.796 61.1 H 383
MW-B-I 7/10/2018 32.44 0.18 -28.4 34.3 0.08 0.0350 J 2.99 1.26 0.578 39.8 372
MW-B-I 12/17/2018 26.69 0.66 15.8 23.4 0.85 <0.0300 3.24 0.756 0.821 5.3 352
MW-B-I 6/10/2019 30.65 57.50 3.4 10.1 0.12 1.4 2.4 0.943 1 30.5 334
MW-B-I 12/12/2019 25.31 3.86 50.9 5.89 0.00 <0.0600 2.22 0.341 1.44 16.2 315
MW-B-I 6/15/2020 21.30 1.81 20.3 13.01 1.09 <0.150 3.12 0.56 2.13 33.8 304
MW-B-I 12/14/2020 19.20 3.43 0.8 6.10 0.00 1.17 2.05 2.55 1.72 49.1 301
MW-B-I 6/14/2021 33.10 0.50 68.9 7.52 0.11 <0.150 1.71 1.68 1.70 20.0 274
MW-B-I 6/20/2022 25.80 0.82 75.0 6..76 0.06 0.350 J 2.17 1.16 3.01 23.8 285
MW-B-I 7/19/2023 28.50 1.44 -30.1 7.44 0.00 <0.300 1.90 0.509 1.46 33.4 285
MW-B-D 10/27/2015 30.39 0.59 -20.1 9.1 NA NA NA NA NA NA NA
MW-B-D 7/20/2016 31.56 0.16 -18.3 7.21 0.0 <0.0400 3.89 0.580 HF <1.00 292 309
MW-B-D 12/13/2016 30.18 0.24 -12.0 10.0 0.62 <0.0400 4.29 0.884 HF <1.00 300 334
MW-B-D 6/28/2017 31.80 0.33 38.3 13.3 0.37 <0.0300 > 4.74 E 0.84 0.605 150 406
MW-B-D 12/13/2017 23.95 0.41 58.0 1.12 0.00 <0.0300 1.52 0.627 25 178 H 250
MW-B-D 7/9/2018 30.35 0.49 -3.8 19.7 1.21 0.0470 J 2.33 0.929 0.662 120 396
Page 7 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
MW-B-D 12/17/2018 27.58 0.76 43.3 1.08 0.00 <0.0300 1.1 0.0390 J 29.4 66.2 247
MW-B-D 6/11/2019 28.40 0.33 57.0 1.15 0.00 0.342 J 4.96 1.19 2.42 114 426
MW-B-D 12/12/2019 27.07 0.90 34.5 2.47 0.00 <0.0600 0.0722 0.0270 J 6.69 1.7 395
MW-B-D 6/15/2020 24.60 0.42 -54.1 0.19 0.00 <0.150 0.144 0.0300 J 5.5 6.65 327
MW-B-D 12/14/2020 27.20 2.78 -8.3 5.4 0.00 <0.150 6.05 1.14 0.722 109 456
MW-B-D 6/14/2021 28.40 0.39 -8.4 7.65 0.00 <0.150 4.09 0.99 0.849 78.7 429
MW-B-D 6/20/2022 26.10 0.97 43.7 9.21 0.00 0.290 J 0.38 0.181 3.89 2.76 196
MW-B-D 7/19/2023 25.40 3.63 0.8 4.68 0.00 <0.300 5.37 1.12 0.778 101 450
MW-B-B 12/2/2015 30.99 1.59 119.9 2.65 NA NA NA NA NA NA NA
MW-B-B 7/20/2016 30.56 0.33 -188.9 8.59 0.00 <0.0400 0.0741 0.104 HF <1.00 70.6 265
MW-B-B 12/14/2016 30.22 0.27 39.2 2.58 NA <0.0400 0.0665 <0.0600 HF 6.03 66.3 273
MW-B-B 6/29/2017 30.30 0.56 -28.7 3.04 0.00 <0.0300 0.0193 <0.0200 4.22 24.5 215
MW-B-B 12/13/2017 28.31 0.16 -22.5 0.81 0.03 <0.0300 0.00599 <0.0200 4.38 <0.107 205
MW-B-B 7/9/2018 30.79 0.07 85.6 1.56 0.00 <0.0300 0.00441 <0.0200 4.58 4.34 60.8
MW-B-B 12/17/2018 24.18 0.29 -60.8 1.42 0.00 <0.0300 0.00405 J <0.0200 3.02 3.09 166
MW-B-B 6/10/2019 27.21 3.34 -29.3 1.83 0.00 0.606 J 0.00250 J 0.0290 J 3.33 9.85 178
MW-B-B 12/12/2019 26.67 3.47 -64.0 1.42 0.00 <0.0600 0.00375 J 0.0210 J 5.03 1.17 143
MW-B-B 6/15/2020 20.20 1.85 100.3 0.38 0.00 <0.150 0.006 0.0410 J 0.594 9.12 123
MW-B-B 12/14/2020 26.20 0.52 -126.1 2.6 0.06 <0.150 0.00328 J <0.0200 3.47 3.27 105
MW-B-B 6/14/2021 26.20 0.37 -53.1 6.37 0.20 <0.150 0.0123 <0.0200 3.44 J 9.03 119
MW-B-B 12/28/2021 26.20 0.67 -56.2 4.02 0.12 0.390 J 0.0043 <0.0200 3.39 5.4 87
MW-B-B 6/20/2022 26.40 0.41 -93.0 7.4 0.02 0.228 J 0.0353 0.0200 J 3.34 3.45 79.4
MW-B-B 12/5/2022 19.18 0.00 -132.0 6.6 0.00 <0.150 0.00313 J 0.0410 J 0.208 J 2.94 74.7
MW-B-B 2/27/2023 23.90 0.10 -443.6 3 0.00 NA 0.003 <0.02 NA 3.27 23.1
MW-B-B 7/19/2023 26.20 3.45 -153.0 5.03 0.00 <0.300 0.00743 0.051 3.53 3.45 71
MW-B-B 12/6/2023 19.70 0.30 -8.9 3.38 0.01 <0.300 0.00463 J 0.0210 J 3.08 2.25 64
MW-C-I 10/27/2015 39.77 0.78 31.7 13.7 NA NA NA NA NA NA NA
MW-C-I 7/20/2016 40.07 0.16 47.4 7.56 1.42 <0.0400 1.37 2.45 HF <1.00 94.7 131
MW-C-I 12/13/2016 39.2 0.09 -124.1 5.24 2.34 <0.0400 1.53 3.70 HF <1.00 138 144
MW-C-I 6/28/2017 38.16 0.25 40.3 5.16 0.69 <0.0300 1.66 1.08 <0.200 30.2 154
MW-C-I 12/11/2017 22.06 3.91 -11.9 241 3.20 <0.0300 1.65 8.3 1.22 37.8 168
MW-C-I 7/9/2018 35.22 0.41 -46.7 8.18 0.88 0.0560 J 1.63 1.91 0.766 45.7 170
MW-C-I 12/17/2018 22.43 0.16 -64.7 5.02 0.95 0.0810 J 2.03 1.42 0.744 6.97 168
MW-C-I 6/11/2019 29.86 0.57 19.2 1.78 0.00 0.363 J 1.88 0.709 0.434 J 5.76 154
MW-C-I 12/11/2019 22.37 1.10 -16.6 9.80 0.81 <0.0600 2.07 2.97 0.348 J 24.3 162
MW-C-I 6/22/2020 29.70 0.72 35.2 7.70 0.00 <0.150 1.78 0.287 0.637 22.8 148
MW-C-I 12/15/2020 21.80 0.47 -7.2 8.59 0.05 <0.150 2.21 0.345 0.62 25.4 147
MW-C-I 6/14/2021 29.50 0.44 67.2 9.50 0.00 <0.150 1.82 0.510 0.447 J 23.3 141
MW-C-I 6/21/2022 26.80 0.45 108.2 4.50 0.03 0.232 J 2.16 0.339 0.447 J 21.3 142
MW-C-I 7/17/2023 25.50 0.18 -84.6 2.93 1.76 0.326 J 1.93 0.270 0.253 J 26.8 146
MW-C-D 10/27/2015 32.97 0.7 -32.7 9.1 NA NA NA NA NA NA NA
MW-C-D 7/20/2016 34.55 0.12 18.3 7.29 1.96 <0.0400 5.78 3.15 HF <1.00 370 331
MW-C-D 12/13/2016 32.96 0.06 -187.1 8.62 2.35 <0.0400 5.86 4.04 HF <1.00 423 350
MW-C-D 6/28/2017 36.40 2.91 17.9 2.46 0.00 0.318 J 0.722 0.077 27.9 4.59 275
MW-C-D 12/11/2017 26.43 3.85 -10.4 > 1000 3.20 <0.0300 > 4.80 E 6.5 1.22 179 399
MW-C-D 7/9/2018 31.89 0.12 -25.4 8.6 0.05 0.0550 J 4.83 3.52 0.626 123 400
MW-C-D 12/17/2018 29.68 0.51 -110.9 1.11 12.35 0.0800 J 0.0392 0.0290 J 25.6 13.4 129
MW-C-D 6/11/2019 29.28 0.51 -17.6 1.71 3.30 0.279 J 4.95 6.75 4.56 97 346
MW-C-D 12/12/2019 19.98 5.76 34.9 2.34 0.00 <0.0600 0.110 0.0200 J 51.4 9.16 70.7
MW-C-D 6/22/2020 30.20 0.89 -36.7 0.10 0.00 <0.150 0.0198 0.0280 J 56.6 10.6 47.3
MW-C-D 12/15/2020 24.90 0.79 -44.0 1.49 0.00 <0.150 0.00554 0.0320 J 53.0 8.95 58.1
MW-C-D 6/14/2021 24.20 1.72 -49.3 7.44 0.00 <0.150 3.73 4.41 9.67 71.0 287
MW-C-D 6/21/2022 27.60 0.40 -59.6 5.80 0.05 0.234 J 0.0125 0.134 29.6 3.8 179
MW-C-D 7/17/2023 26.30 0.32 99.9 5.69 2.08 0.407 J 4.7100 6.48 0.771 123.0 309
MW-C-B 12/2/2015 37.73 2.99 149 2.07 NA NA NA NA NA NA NA
MW-C-B 7/20/2016 34.46 0.18 60.9 4.53 0.0 <0.0400 0.818 <0.0600 HF <1.00 180 342
MW-C-B 12/13/2016 37.85 3.34 -184.4 8.59 0.31 0.105 0.0271 <0.0600 HF 5.82 17.1 548
MW-C-B 6/28/2017 36.57 2.15 -39.0 11.8 0.00 0.619 J 0.013 <0.0200 6.54 5.65 525
MW-C-B 12/11/2017 30.52 0.81 50.2 3.25 0.00 0.842 J 0.232 0.068 4.93 31.8 276
MW-C-B 7/9/2018 30.07 0.25 -6.8 1.95 0.00 0.0530 J 1.29 0.057 1.61 84 409
MW-C-B 12/17/2018 27.35 5.46 -85.0 2.21 0.00 0.233 0.00394 J 0.06 4.68 3.25 343
MW-C-B 6/10/2019 30.34 1.32 -65.7 1.16 0.00 0.512 J 0.0035 <0.0200 5.74 8.93 268
MW-C-B 12/12/2019 26.28 2.08 -57.9 1.98 0.00 <0.0600 0.00439 J 0.0350 J 5.91 3.69 219
MW-C-B 6/22/2020 29.30 0.47 -48.9 5.00 0.00 <0.150 0.012 0.0300 J 6.17 3.03 192
MW-C-B 12/15/2020 23.60 0.98 15.8 4.21 0.00 1.53 0.00273 J 0.062 5.55 3.09 160
MW-C-B 6/14/2021 28.50 5.21 3.5 1.72 0.13 0.718 J 0.0156 <0.0200 5.36 1.89 148
Page 8 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
MW-C-B 6/21/2022 26.10 6.10 5.3 8.30 0.00 1.33 0.00268 J 0.0230 J 5.3 3.03 131
MW-C-B 7/17/2023 25.10 5.27 -5.3 8.62 0.23 1.63 J .00423 J 0.0490 J 5.17 <0.107 134
MW-D-I 10/27/2015 34.23 0.25 -21.5 21.0 NA NA NA NA NA NA NA
MW-D-I 7/19/2016 36.49 0.17 -39.2 27.9 NA NA NA NA NA NA NA
MW-D-I 12/14/2016 26.8 0.83 120.5 74.5 NA NA NA NA NA NA NA
MW-D-I 6/28/2017 31.05 0.30 -10.9 19.4 NA NA NA NA NA NA NA
MW-D-I 12/12/2017 28.75 5.60 9.7 28.0 NA NA NA NA NA NA NA
MW-D-I 7/10/2018 31.60 0.39 11.1 15.9 NA NA NA NA NA NA NA
MW-D-I 12/17/2018 28.89 0.13 -28.1 35.6 NA NA NA NA NA NA NA
MW-D-I 6/11/2019 20.36 8.53 52.1 11.7 NA NA NA NA NA NA NA
MW-D-I 12/11/2019 23.52 0.40 180.8 9.79 NA NA NA NA NA NA NA
MW-D-I 6/22/2020 26.60 1.18 26.1 9.90 NA NA NA NA NA NA NA
MW-D-I 12/15/2020 20.60 0.64 71.9 7.60 NA NA NA NA NA NA NA
MW-D-I 6/15/2021 33.70 0.64 76.7 12.90 NA NA NA NA NA NA NA
MW-D-I 6/21/2022 26.70 5.10 92.1 9.60 NA NA NA NA NA NA NA
MW-D-I 7/18/2023 25.90 0.92 18.7 184.60 NA NA NA NA NA NA NA
MW-D-D 10/27/2015 32.25 0.14 -18.5 0.80 NA NA NA NA NA NA NA
MW-D-D 7/19/2016 32.84 0.16 6.4 8.71 0.71 0.1 2.69 0.623 HF <1.00 478 358
MW-D-D 12/13/2016 31.61 0.44 -82.7 10.11 0.12 <0.0400 1.66 0.110 HF <1.00 340 352
MW-D-D 6/29/2017 91.71 1.05 -18.5 1.91 0.00 0.680 J > 2.85 E 0.122 0.693 54 372
MW-D-D 12/13/2017 30.21 0.26 -4.0 1.23 0.00 <0.0300 > 3.07 E 0.419 0.849 345 460
MW-D-D 7/10/2018 30.97 0.14 -28.4 2.01 0.78 0.247 2.70 0.259 1.16 10.3 443
MW-D-D 12/19/2018 24.33 0.15 -27.8 1.89 0.12 0.0780 J 3.16 0.34 1.1 11.9 418
MW-D-D 6/11/2019 28.74 2.13 17.5 6.07 0.00 0.404 J 3.49 0.451 0.380 J 150 485
MW-D-D 12/12/2019 24.85 0.64 -36.7 3.15 0.24 <0.0600 3.14 0.284 7.77 3.14 485
MW-D-D 6/22/2020 28.00 0.15 -118.2 7.80 0.21 <0.150 3.34 0.179 1.19 86.3 467
MW-D-D 12/15/2020 16.20 0.50 -78.0 8.79 0.81 1.24 0.0122 <0.0200 2.16 23.8 152
MW-D-D 6/15/2021 29.20 0.45 -76.7 54.20 0.005 <0.150 4.72 0.246 0.525 79.9 511
MW-D-D 6/21/2022 25.00 4.15 -76.1 9.50 0.000 0.820 J 0.02 0.0210 J 6.69 3.61 108
MW-D-D 7/18/2023 25.30 0.39 -71.2 2.19 0.180 <0.300 0.01 <0.0200 3.79 14.9 213
MW-D-B 12/2/2015 30.9 1.4 151.9 10.31 NA NA NA NA NA NA NA
MW-D-B 7/20/2016 30.86 0.72 -31.6 9.26 0.0 <0.0400 0.866 0.149 HF 2 42.2 203
MW-D-B 12/13/2016 29.49 2.15 76.4 9.81 0.09 0.254 <0.00500 <0.0600 HF 4.82 0.796 J 140
MW-D-B 7/5/2017 30.38 3.94 -4.2 2.90 0.64 1.19 0.0189 <0.0200 5.36 0.806 141
MW-D-B 12/13/2017 30.50 5.70 50.3 1.32 0.00 1.14 0.00336 J <0.0200 5.62 0.805 147
MW-D-B 7/10/2018 30.48 4.78 62.7 1.10 0.00 0.526 0.00302 J <0.0200 6.15 1.08 152
MW-D-B 12/17/2018 27.99 6.56 39.1 2.33 0.00 0.474 0.00594 0.0380 J 4.2 3.41 153
MW-D-B 6/11/2019 27.34 7.68 28.5 1.11 0.00 0.869 J 0.0261 0.0300 J 4.95 2.32 174
MW-D-B 12/12/2019 19.03 4.01 -23.7 5.05 0.38 <0.0600 0.0129 0.0210 J 4.71 5.81 206
MW-D-B 6/23/2020 25.30 3.41 -46.2 5.80 0.00 <0.150 0.0167 <0.0200 4.6 15.4 176
MW-D-B 12/15/2020 24.50 1.17 -31.0 1.28 0.08 1.7 0.000701 J 0.0210 J 4.27 4.72 168
MW-D-B 6/15/2021 27.50 6.51 -62.9 3.50 0.014 0.380 J 0.00352 J <0.0200 4.35 J 4.50 220
MW-D-B 6/21/2022 26.20 4.37 70.1 8.60 0.000 0.648 J 0.00119 <0.0200 4.81 4.13 170
MW-D-B 7/18/2023 27.10 7.45 -70.8 2.94 0.310 <0.300 <0.000700 <0.0200 5.29 3.49 164
MW-E-I 10/27/2015 33.26 0.08 -67.8 1.99 NA NA NA NA NA NA NA
MW-E-I 7/21/2016 35.7 0.52 5.2 4.89 0.64 <0.0400 0.971 0.972 HF 13.6 203 106
MW-E-I 12/12/2016 31.00 0.82 -19.8 9.67 0.44 <0.0400 0.898 0.718 HF 19.8 113 110
MW-E-I 6/26/2017 29.77 0.73 64.8 1.50 0.00 <0.0300 0.789 <0.0200 20.1 3.87 130
MW-E-I 12/13/2017 28.46 0.27 101.9 7.87 0.00 <0.0300 0.674 0.114 15.7 3.33 139
MW-E-I 7/10/2018 29.56 0.17 10.0 0.49 0.62 <0.0300 0.702 0.568 11.3 23.9 134
MW-E-I 12/18/2018 23.68 1.13 42.4 8.41 0.00 0.0800 J 0.671 0.266 9.77 5.86 138
MW-E-I 6/10/2019 25.77 1.56 32.0 4.00 0.00 1.46 0.682 0.323 15.1 16.7 139
MW-E-I 12/11/2019 24.73 0.44 -157.8 6.25 0.00 <0.0600 0.674 0.311 14.8 2.28 143
MW-E-I 6/22/2020 26.30 0.17 -61.0 1.34 0.81 <0.150 0.605 0.675 18.1 31.7 147
MW-E-I 12/17/2020 19.70 1.00 -28.9 1.32 0.16 0.937 J 0.714 0.363 20.3 33.1 147
MW-E-I 6/15/2021 26.20 0.46 185.6 4.03 0.03 <0.150 0.681 0.139 26.0 15.3 155
MW-E-I 6/21/2022 25.70 0.26 82.6 3.37 0.00 0.224 J 0.731 0.0240 J 31.0 11.5 169
MW-E-I 7/18/2023 24.50 0.19 -5.2 5.56 0.11 <0.300 0.649 0.167 31.1 65.1 162
MW-E-D 10/27/2015 27.99 0.1 -29.6 6.80 NA NA NA NA NA NA NA
MW-E-D 7/21/2016 28.8 0.1 32.5 6.39 0.50 <0.0400 0.437 1.21 HF 3.61 77.2 119
MW-E-D 12/12/2016 27.3 0.22 11 93.8 0.82 <0.0400 0.381 0.852 HF 2.35 85.2 115
MW-E-D 6/26/2017 29.17 0.43 67.7 5.80 0.00 <0.0300 0.196 0.068 3.4 18.1 128
MW-E-D 12/11/2017 29.22 1.81 87.0 1.94 0.71 <0.0300 0.0526 0.0300 J 3.98 0.480 J 144
MW-E-D 7/10/2018 26.14 0.19 35.4 9.82 0.00 0.0780 J 0.321 1.01 1.43 29.6 134
MW-E-D 12/18/2018 25.97 1.21 90.1 1.35 0.00 0.0780 J 0.0608 <0.0200 2.21 2.73 153
Page 9 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
MW-E-D 6/10/2019 26.86 0.40 81.4 1.85 0.00 0.394 J 0.0984 0.055 2.43 3.91 156
MW-E-D 12/11/2019 25.16 0.64 114.5 2.46 0.21 <0.0600 0.112 0.158 2.03 28.5 129
MW-E-D 6/22/2020 24.80 0.10 29.1 0.27 0.25 <0.150 0.174 0.208 2.19 34 126
MW-E-D 12/17/2020 22.10 0.39 15.6 2.47 0.31 <0.150 0.264 0.178 2.84 7.36 121
MW-E-D 6/15/2021 25.80 0.45 158.6 3.66 0.07 <0.150 0.0804 0.116 2.62 31.7 119
MW-E-D 6/21/2022 26.00 0.09 83.0 3.09 0.00 0.219 J 0.0901 0.079 3.4 28.2 113
MW-E-D 7/18/2023 22.90 0.05 3.3 1.08 0.10 <0.300 0.184 0.172 2.9 42.2 114
MW-E-B 12/2/2015 31.38 0.95 98.6 2.14 NA NA NA NA NA NA NA
MW-E-B 7/21/2016 32.74 2.01 7.7 4.51 0.00 0.292 <0.00500 <0.0600 HF 31.9 0.748 J 92.8
MW-E-B 12/12/2016 29.08 0.88 -2.5 4.47 0.12 0.363 <0.00500 <0.0600 HF 17.9 0.595 J 110
MW-E-B 6/26/2017 31.66 4.67 80.9 6.30 0.00 0.991 J 0.00841 <0.0200 37.1 0.419 J 98.6
MW-E-B 12/11/2017 27.39 4.44 136.0 1.02 0.00 1.29 0.00435 J 0.0420 J 32.2 1.08 102
MW-E-B 7/10/2018 29.74 7.96 63.5 1.20 0.01 0.997 0.00331 J <0.0200 26.6 0.695 101
MW-E-B 12/19/2018 17.74 5.05 180.5 2.43 0.00 1.03 0.00360 J 0.0240 J 16.8 3.65 81.8
MW-E-B 6/10/2019 26.00 5.13 32.7 2.74 0.00 0.946 0.00963 0.067 9.81 1.84 64.3
MW-E-B 12/12/2019 25.50 5.17 50.9 1.07 0.00 <0.0600 0.00142 J 0.0300 J 6.26 0.632 54.7
MW-E-B 6/22/2020 25.10 0.61 50.7 0.19 0.00 <0.150 0.0145 <0.0200 4.6 3.92 187
MW-E-B 12/15/2020 23.90 7.17 58.9 3.30 0.44 1.80 0.00281 J 0.0230 J 3.79 1.64 44.0
MW-E-B 6/15/2021 26.90 6.17 182.5 1.84 0.12 0.903 J 0.000736 J <0.0200 3.93 1.32 45.4
MW-E-B 6/21/2022 24.90 7.44 97.1 3.84 0.00 1.22 0.00329 J <0.0200 3.71 3.31 44.6
MW-E-B 7/18/2023 22.70 6.38 62.8 2.85 0.08 0.568 J 0.00152 J 0.0370 J 4.16 0.549 46.8
MW-F-I 10/27/2015 33.67 1.01 13.7 8.50 NA NA NA NA NA NA NA
MW-F-I 7/20/2016 33.36 0.2 16.8 6.90 NA NA NA NA NA NA NA
MW-F-I 12/12/2016 32.30 0.16 -194.4 36.4 0.76 NA NA NA NA NA NA
MW-F-I 6/28/2017 28.89 0.37 -46.6 3.66 NA NA NA NA NA NA NA
MW-F-I 12/12/2017 22.19 1.58 43.1 2.37 NA NA NA NA NA NA NA
MW-F-I 7/10/2018 29.61 0.22 -2.7 5.51 NA NA NA NA NA NA NA
MW-F-I 12/18/2018 24.93 3.20 10.5 9.8 NA NA NA NA NA NA NA
MW-F-I 6/11/2019 27.63 0.16 -370.6 0.93 NA NA NA NA NA NA NA
MW-F-I 12/10/2019 25.95 0.65 16.0 3.39 NA NA NA NA NA NA NA
MW-F-I 6/22/2020 24.60 0.13 -43.1 4.60 NA NA NA NA NA NA NA
MW-F-I 12/15/2020 19.10 0.44 10.3 3.50 NA NA NA NA NA NA NA
MW-F-I 6/15/2021 27.40 0.66 -11.7 6.60 NA NA NA NA NA NA NA
MW-F-I 6/21/2022 26.80 0.30 18.4 7.75 NA NA NA NA NA NA NA
MW-F-I 7/18/2023 20.50 0.06 4.8 24.33 NA NA NA NA NA NA NA
MW-F-D 10/27/2015 27.88 1.01 8.2 7.40 NA NA NA NA NA NA NA
MW-F-D 7/20/2016 29.02 0.21 9.6 7.42 0.00 <0.0400 2.9 0.344 HF <1.00 140 308
MW-F-D 12/12/2016 27.28 0.42 -192.7 3.55 0.28 <0.0400 2.77 0.403 HF <1.00 166 320
MW-F-D 6/26/2017 30.60 0.08 16.4 2.70 0.19 <0.0300 > 2.63 E 0.333 3.35 61.9 344
MW-F-D 12/13/2017 24.31 1.14 15.4 34.0 0.36 <0.0300 > 2.59 E 0.676 1.19 42.3 H 356
MW-F-D 7/10/2018 29.00 0.44 8.40 0.80 0.24 <0.0300 2.19 0.278 1.68 49.4 354
MW-F-D 12/18/2018 23.38 2.70 1.60 2.32 0.00 0.0780 J 2.52 0.28 1.09 10.4 368
MW-F-D 6/11/2019 27.41 0.13 -347.30 0.92 0.00 0.317 J 0.314 0.097 4.51 57.5 65.3
MW-F-D 12/11/2019 23.01 3.61 -8.90 9.60 0.00 <0.0600 1.65 0.093 2.11 4.08 268
MW-F-D 6/22/2020 25.60 0.16 16.40 1.54 0.26 <0.150 2.3 0.267 0.726 44.8 334
MW-F-D 12/15/2020 22.60 2.91 -118.80 2.00 0.07 0.856 J 0.0227 <0.0200 3.41 38.1 141
MW-F-D 6/15/2021 25.90 4.63 -87.70 2.39 0.71 <0.150 0.113 <0.0200 3.60 J 19.5 154
MW-F-D 6/21/2022 26.80 0.55 3.40 6.09 0.11 0.231 J 1.73 1.48 0.802 346 212
MW-F-D 7/18/2023 21.30 4.30 -32.70 0.75 0.00 <0.300 2.13 0.262 0.834 36.3 287
MW-F-B 12/2/2015 33.07 1.67 108.6 15.2 NA NA NA NA NA NA NA
MW-F-B 7/21/2016 32.92 0.18 18.3 4.86 0.00 <0.0400 0.538 0.134 HF <1.00 3.06 J 273
MW-F-B 12/12/2016 30.23 0.13 -234.9 7.66 0.33 <0.0400 0.471 0.214 HF <1.00 F1 8.37 271
MW-F-B 6/27/2017 31.78 2.13 22.8 1.31 0.22 0.942 J 0.0523 0.0250 J 2.65 0.643 210
MW-F-B 12/14/2017 28.59 1.12 -32.4 8.29 0.00 0.986 J 0.0986 <0.0200 2.81 1.26 H 226
MW-F-B 7/10/2018 30.54 4.69 47.1 1.02 0.07 0.207 0.00992 <0.0200 2.85 1.28 207
MW-F-B 12/18/2018 25.04 5.40 0.1 5.46 0.00 0.0770 J 1.32 0.163 1.44 29.5 382
MW-F-B 6/11/2019 27.38 0.62 -236.6 0.72 0.00 0.662 J 0.416 <0.0200 2.28 2.03 217
MW-F-B 12/11/2019 24.01 0.34 11.0 4.86 0.00 <0.0600 0.0186 <0.0200 2.88 3.78 219
MW-F-B 6/23/2020 27.30 5.35 144.9 2.39 0.04 <0.150 0.00414 J <0.0200 1.85 1.89 163
MW-F-B 12/15/2020 22.00 6.41 37.8 2.6 0.00 1.63 0.0145 <0.0200 1.67 2.31 121
MW-F-B 6/15/2021 25.80 7.44 40.4 2.64 0.00 0.392 J 0.0100 <0.0200 J 1.54 1.01 105
MW-F-B 6/21/2022 25.70 6.60 53.7 6.18 0.00 0.780 J 0.0191 0.0320 J 1.50 1.81 79
MW-F-B 7/18/2023 20.70 1.59 50.2 2.55 0.00 <0.300 0.00221 J 0.0320 J 1.38 0.514 64.3
MW-G-I 11/2/2015 33.39 0.28 60.9 22 NA NA NA NA NA NA NA
MW-G-I 7/21/2016 33.8 0.11 -8.2 7.8 0.99 <0.0400 1.57 1.73 HF <1.00 178 153
Page 10 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
MW-G-I 12/13/2016 29.09 0.62 67.5 57.4 0.00 <0.0400 1.82 1.50 HF <1.00 117 164
MW-G-I 6/27/2017 30.65 0.58 -12.9 23.8 0.59 <0.0300 > 1.84 E 1.38 1.01 69.5 187
MW-G-I 12/12/2017 21.51 0.33 62.0 5.44 0.00 <0.0300 1.61 0.47 1.64 13.4 187
MW-G-I 7/10/2018 31.28 0.29 -131.0 10.4 0.87 <0.0300 1.92 2.12 10.3 66.9 185
MW-G-I 12/19/2018 23.48 0.43 61.3 4.39 0.00 0.0780 J 2.6 0.62 21 14.5 182
MW-G-I 6/11/2019 27.80 0.37 -14.6 0.62 0.19 0.402 J 2.35 0.992 28.2 87.1 169
MW-G-I 12/11/2019 18.01 1.00 29.9 10.31 0.00 <0.0600 2.63 0.494 26.6 37 166
MW-G-I 6/22/2020 27.60 0.24 35.2 6.01 0.29 <0.150 2.21 0.636 20.3 28.5 159
MW-G-I 12/17/2020 14.40 1.15 33.7 5.54 0.00 1.18 2.6 0.144 13.2 34.4 149
MW-G-I 6/15/2021 27.10 0.73 79.2 9.38 0.00 <0.150 2.82 0.850 9.96 8.89 152
MW-G-I 6/21/2022 30.10 1.70 63.1 8.71 0.04 0.410 J 3.18 0.579 6.84 13.3 155
MW-G-I 7/17/2023 20.70 0.10 40.6 4.85 0.21 <0.300 2.76 0.263 4.56 16.7 165
MW-G-D 11/2/2015 29.45 0.11 -333.2 1000 NA NA NA NA NA NA NA
MW-G-D 7/21/2016 31.3 0.05 -21.1 2.9 NA NA NA NA NA NA NA
MW-G-D 12/13/2016 29.4 2.18 35 194 NA NA NA NA NA NA NA
MW-G-D 6/28/2017 29.76 0.16 -52.7 0.52 NA NA NA NA NA NA NA
MW-G-D 12/12/2017 21.40 0.42 -14.1 3.38 NA NA NA NA NA NA NA
MW-G-D 7/10/2018 28.92 1.29 11.3 6.21 NA NA NA NA NA NA NA
MW-G-D 12/19/2018 26.30 0.61 126.2 12.97 NA NA NA NA NA NA NA
MW-G-D 6/11/2019 27.39 0.24 67.8 79.6 NA NA NA NA NA NA NA
MW-G-D 12/10/2019 26.03 0.74 -24.0 8.94 NA NA NA NA NA NA NA
MW-G-D 6/22/2020 25.80 0.11 -44.1 11.7 NA NA NA NA NA NA NA
MW-G-D 12/15/2020 22.80 0.37 -56.9 11.8 NA NA NA NA NA NA NA
MW-G-D 6/15/2021 26.10 0.21 -81.0 36.51 NA NA NA NA NA NA NA
MW-G-D 6/21/2022 29.80 1.07 28.9 1.92 NA NA NA NA NA NA NA
MW-G-D 2/27/2023 22.20 0.09 -67.9 20.54 3.3 NA 1.01 3.60 NA 160 164
MW-G-D 7/17/2023 21.00 0.09 17.9 6.16 NA NA NA NA NA NA NA
MW-G-B 12/3/2015 31.85 1.51 93.5 4.79 NA NA NA NA NA NA NA
MW-G-B 7/21/2016 27.39 0.37 45.2 8.45 NA NA NA NA NA NA NA
MW-G-B 7/21/2016 31.33 0.19 -14.2 3.29 0.00 <0.0400 2.35 0.591 HF <1.00 170 265
MW-G-B 12/13/2016 30 0.68 40.1 9.47 0.00 <0.0400 1.98 0.328 HF <1.00 76 258
MW-G-B 7/5/2007 30.59 0.15 -94.9 1.41 3.30 <0.0300 1.12 0.267 2.55 20.5 301
MW-G-B 12/12/2017 20.98 0.36 95.4 3.16 0.00 <0.0300 0.288 0.133 3.21 6.62 299
MW-G-B 7/11/2018 28.85 4.33 14.4 1.37 NA <0.0300 2.25 0.888 1.22 150 319
MW-G-B 12/19/2018 25.44 0.67 83.2 0.69 0.00 0.105 J 0.0377 0.0230 J 3.39 3.11 300
MW-G-B 6/11/2019 26.99 3.07 64.7 0.57 0.00 0.480 J 0.00749 <0.0200 2.97 1.26 302
MW-G-B 12/11/2019 25.20 4.37 134.1 0.96 0.04 <0.0600 0.0601 <0.0200 3.6 1.81 259
MW-G-B 6/23/2020 25.50 0.13 -55.0 0.79 0.71 <0.150 3.08 0.779 1.06 95.3 352
MW-G-B 12/17/2020 21.00 6.30 53.0 3.42 0.00 1.28 0.042 <0.0200 3.44 2.27 241
MW-G-B 6/15/2021 25.20 7.03 -8.5 3.57 0.00 0.336 J 0.0137 <0.0200 3.00 0.975 222
MW-G-B 6/22/2022 24.60 7.15 95.2 3.1 0.00 0.582 J 0.0113 <0.0200 3.02 1.57 220
MW-G-B 7/17/2023 19.80 5.67 98.8 0.00 1.20 0.345 J 0.00612 <0.0200 2.75 0.545 233
MW-H-I 11/2/2015 28.28 0.24 -3.9 36 NA NA NA NA NA NA NA
MW-H-I 7/20/2016 30.24 0.39 -31.7 8.47 2.21 <0.0400 7.72 3.02 HF <1.00 661 189
MW-H-I 12/13/2016 27.59 1.13 -80.3 163 1.96 <0.0400 6.3 5.61 HF <1.00 819 176
MW-H-I 6/27/2017 25.90 0.30 84.1 76.3 1.85 <0.0300 <5.99 E 2.59 <0.200 185 205
MW-H-I 12/13/2017 16.12 0.21 3.7 12.5 0.16 <0.0300 <4.92 E 1.95 0.616 46.5 H 209
MW-H-I 7/10/2018 28.78 0.58 7.1 8.41 0.11 <0.0300 2.38 0.0440 J 2.74 3.53 206
MW-H-I 12/19/2018 17.31 4.50 -23.5 104.8 2.01 0.0770 J 7.23 2.86 0.587 14.6 215
MW-H-I 6/11/2019 25.43 0.84 -21.6 23.5 1.37 0.336 J 4.48 3.45 0.250 J 35.5 214
MW-H-I 12/10/2019 20.07 0.51 222.9 24.6 0.00 <0.0600 4.92 0.442 0.328 J 11.4 236
MW-H-I 6/22/2020 26.00 0.58 119.1 17.01 0.11 <0.150 5.09 0.08 0.487 J 2.26 247
MW-H-I 12/17/2020 19.80 0.51 -65.8 9.9 3.30 0.848 J 8.14 0.794 0.878 202 259
MW-H-I 6/16/2021 21.50 0.51 15.2 9.08 0.19 <0.150 6.24 0.972 0.5 34.7 266
MW-H-I 6/21/2022 27.70 0.35 -33.3 9.7 0.12 0.222 J 7.51 4.41 0.434 J 111 292
MW-H-I 7/17/2023 21.70 2.94 -58.3 10.13 0.12 0.338 J 6.17 6.38 0.396 J 182 297
MW-H-D 11/2/2015 28.05 0.34 -40 25.2 NA NA NA NA NA NA NA
MW-H-D 7/20/2016 28.73 0.15 8 9.2 2.26 <0.0400 2.1 3.15 HF 4.81 1290 217
MW-H-D 12/13/2016 26.38 0.29 2.2 10 1.60 <0.0400 1.73 2.08 HF 2.55 1570 217
MW-H-D 6/27/2017 26.47 0.36 95.2 17.9 0.16 <0.0300 1.44 0.572 2.34 165 H 257
MW-H-D 12/13/2017 21.79 0.24 119.0 2.12 0.20 <0.0300 1.07 0.611 1.8 158 H 223
MW-H-D 7/11/2018 27.37 0.08 23.1 21.7 0.00 0.139 J 1.57 1.92 1.09 338 219
MW-H-D 12/19/2018 19.79 28.60 -3.2 7.78 0.00 0.0780 J 1.28 0.591 1.09 76.2 199
MW-H-D 6/11/2019 25.26 0.48 -6.2 7.08 0.08 0.357 J 1.44 3.12 0.51 306 183
MW-H-D 12/10/2019 22.35 0.32 252.4 4.23 0.03 <0.0600 1.15 0.334 0.621 121 166
MW-H-D 6/22/2020 25.40 0.20 28.3 2.82 0.22 <0.150 1.1 0.215 0.608 77 152
Page 11 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
MW-H-D 12/17/2020 21.10 0.64 37.7 2.22 0.05 1.17 1.09 0.177 1.08 67.3 140
MW-H-D 6/16/2021 23.60 0.35 54.8 7.45 0.00 <0.150 0.917 0.912 0.505 62.7 135
MW-H-D 6/21/2022 25.60 0.18 55.7 6.13 0.06 0.216 J 3.21 0.775 0.569 24 135
MW-H-D 7/17/2023 21.30 6.16 -60.7 3.46 0.13 0.793 J 0.00462 J 0.0380 J 5.43 2.46 79.7
MW-H-B 12/3/2015 27.73 1.2 115.7 18.3 NA NA NA NA NA NA NA
MW-H-B 7/21/2016 27.89 0.37 45.2 8.45 0.00 <0.0400 2.29 <0.0600 HF <1.00 125 236
MW-H-B 12/13/2016 26.11 0.35 28.6 10 0.00 <0.0400 1.92 <0.0600 HF <1.00 129 232
MW-H-B 6/27/2017 27.13 5.54 127.5 4.12 1.63 0.608 J 0.0442 0.0380 J 10.2 0.508 188
MW-H-B 12/13/2017 20.38 4.35 137.7 2.55 0.00 4.91 0.047 0.0430 J 10.9 1.11 H 192
MW-H-B 7/11/2018 26.39 10.05 48.9 4.41 0.03 0.264 0.0155 0.0450 J 10.2 1.24 178
MW-H-B 12/19/2018 22.31 3.40 -9.2 1.74 2.81 <0.0300 1.74 0.151 1.48 13.4 244
MW-H-B 6/11/2019 24.95 0.64 63.6 1.54 0.00 0.442 J 0.644 0.101 6.11 8.91 206
MW-H-B 12/10/2019 22.53 4.12 206.7 2.42 0.00 0.936 0.0296 0.0220 J 7.28 1.45 70.5
MW-H-B 6/22/2020 25.00 5.49 85.7 2.76 0.05 <0.150 0.00162 J <0.0200 5.6 2.13 59.7
MW-H-B 12/17/2020 21.80 3.39 -32.4 1.12 0.05 2.02 0.00911 0.0320 J 5.2 2.61 68.2
MW-H-B 6/16/2021 23.10 6.33 -50.4 0.39 0.00 0.660 J 0.00846 0.0320 J 5.29 3.52 81.4
MW-H-B 6/21/2022 23.40 6.91 -10.1 5.07 0.11 0.960 J 0.0111 0.051 4.98 3.56 64.2
MW-H-B 7/17/2023 22.30 0.05 3.2 3.45 0.15 0.330 J 1.12 0.369 0.385 J 61.3 131
MW-I-I 11/2/2015 22.84 1.83 126.9 18.6 NA NA NA NA NA NA NA
MW-I-I 7/20/2016 27.63 0.24 11.5 11.4 NA NA NA NA NA NA NA
MW-I-I 12/13/2016 21.98 0.39 130.9 6.92 NA NA NA NA NA NA NA
MW-I-I 6/28/2017 22.44 0.25 128.9 1.10 NA NA NA NA NA NA NA
MW-I-I 12/11/2017 20.29 0.93 35.5 10.8 NA NA NA NA NA NA NA
MW-I-I 7/10/2018 NA 19.29 16.8 1.34 NA NA NA NA NA NA NA
MW-I-I 12/19/2018 15.08 1.92 117.8 1.39 NA NA NA NA NA NA NA
MW-I-I 6/11/2019 23.05 0.63 -252.4 1.76 NA NA NA NA NA NA NA
MW-I-I 12/10/2019 21.06 0.30 -45.2 2.16 NA NA NA NA NA NA NA
MW-I-I 6/15/2020 17.90 0.43 43.7 3.92 NA NA NA NA NA NA NA
MW-I-I 12/15/2020 12.40 0.64 -3.5 2.6 NA NA NA NA NA NA NA
MW-I-I 6/16/2021 22.20 0.41 -13.2 45.71 NA NA NA NA NA NA NA
MW-I-I 6/21/2022 26.90 2.02 49.0 7.9 NA NA NA NA NA NA NA
MW-I-I 7/17/2023 20.20 0.13 -17.6 14.55 NA NA NA NA NA NA NA
MW-I-D 11/4/2015 22.48 0.63 1.4 4.84 NA NA NA NA NA NA NA
MW-I-D 7/20/2016 24.68 0.06 -29.6 34.8 NA NA NA NA NA NA NA
MW-I-D 6/28/2017 21.98 0.25 96.6 20.7 NA NA NA NA NA NA NA
MW-I-D 12/11/2017 20.93 3.15 57.0 3.63 NA NA NA NA NA NA NA
MW-I-D 7/10/2018 NA 3.24 -34.7 1.79 NA NA NA NA NA NA NA
MW-I-D 12/19/2018 17.78 1.00 108.6 16.6 NA NA NA NA NA NA NA
MW-I-D 6/11/2019 22.78 0.08 -208.4 5.79 NA NA NA NA NA NA NA
MW-I-D 12/10/2019 21.24 0.23 -71.8 2.68 NA NA NA NA NA NA NA
MW-I-D 6/15/2020 20.50 0.60 44.9 2.13 NA NA NA NA NA NA NA
MW-I-D 12/15/2020 17.60 0.51 -7.1 3.2 NA NA NA NA NA NA NA
MW-I-D 6/16/2021 23.30 0.69 81.2 11.3 NA NA NA NA NA NA NA
MW-I-D 6/21/2022 22.30 0.24 52.7 3.3 NA NA NA NA NA NA NA
MW-I-D 7/17/2023 19.80 0.05 44.2 9.43 NA NA NA NA NA NA NA
MW-I-B 12/3/2015 24.28 1.68 165.3 14.7 NA NA NA NA NA NA NA
MW-I-B 7/20/2016 24.4 0.39 -1.4 7.05 0.0 <0.0400 2.57 0.568 HF <1.00 107 223
MW-I-B 12/13/2016 23.95 4.96 197.0 8.09 0.0 <0.0400 0.145 <0.0600 HF 6.42 <0.218 221
MW-I-B 6/27/2017 23.10 5.52 159.3 5.27 2.59 0.247 J 0.113 <0.0200 5.84 0.265 J 234
MW-I-B 12/11/2017 22.80 5.87 26.5 1.06 0.0 0.901 J 0.0207 0.0370 J 8.57 1.34 240
MW-I-B 7/10/2018 NA 19.93 53.1 1.31 0.09 0.122 J 0.034 <0.0200 4.96 1.15 246
MW-I-B 12/19/2018 14.79 5.01 137.2 1.74 0.00 0.222 0.0128 <0.0200 5.27 2.73 220
MW-I-B 6/11/2019 20.60 6.13 -192.4 3.72 0.00 1.47 0.00498 J <0.0200 4.85 1.66 205
MW-I-B 12/10/2019 20.81 5.68 -13.7 1.39 0.00 1.11 0.00913 <0.0200 4.52 1.75 212
MW-I-B 6/15/2020 20.10 6.50 78.4 1.52 0.00 <0.150 0.0301 0.0250 J 4.09 2.55 201
MW-I-B 12/15/2020 20.20 6.51 50.4 4.2 0.41 1.24 0.0264 <0.0200 4.55 2.95 193
MW-I-B 6/16/2021 20.90 6.10 10.5 5.43 0.00 0.298 J 0.024 <0.0200 3.31 1.46 200
MW-I-B 6/21/2022 29.10 6.15 71.7 6.76 0.00 0.263 J 2.78 0.262 1.27 2.92 182
MW-I-B 7/17/2023 19.40 7.63 68.1 2.05 0.37 <0.300 0.00304 J <0.0200 3.36 <0.107 200
Offsite Well
AMW-8S 11/10/2015 20.21 4.04 31 47.9 NA NA NA NA NA NA NA
AMW-8S 8/2/2016 23.89 1.5 79.7 10 NA NA NA NA NA NA NA
AMW-8S 12/14/2016 16.7 0.65 47.2 16.9 NA NA NA NA NA NA NA
AMW-8S 6/29/2017 15.51 0.48 58.3 5.77 NA NA NA NA NA NA NA
AMW-8S 12/12/2017 18.02 0.19 9.7 12.8 NA NA NA NA NA NA NA
Page 12 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
AMW-8S 7/10/2018 19.70 0.30 53.9 6.11 NA NA NA NA NA NA NA
AMW-8S 1/10/2019 11.67 0.54 47.5 18.9 NA NA NA NA NA NA NA
AMW-8S 6/12/2019 20.50 4.63 139.0 5.87 NA NA NA NA NA NA NA
AMW-8S 12/12/2019 16.80 1.39 69.8 11.9 NA NA NA NA NA NA NA
AMW-8S 6/23/2020 21.20 0.40 77.2 5.73 NA NA NA NA NA NA NA
AMW-8S 12/29/2020 17.50 0.44 58.8 9.37 NA NA NA NA NA NA NA
AMW-8S 6/15/2021 21.90 0.62 48.3 29.2 NA NA NA NA NA NA NA
AMW-8S 6/21/2022 22.70 0.93 136.5 49.7 NA NA NA NA NA NA NA
AMW-8S 7/19/2023 18.10 0.42 -56.9 20.5 NA NA NA NA NA NA NA
AMW-9S 10/28/2015 20.33 0.15 53.2 24.4 NA NA NA NA NA NA NA
AMW-9S 7/25/2016 22.93 0.48 34.2 24.5 NA NA NA NA NA NA NA
AMW-9S 12/13/2016 14.22 0.94 57.1 58.1 NA NA NA NA NA NA NA
AMW-9S 6/29/2017 19.38 0.35 53.2 7.81 NA NA NA NA NA NA NA
AMW-9S 12/12/2017 18.46 0.50 59.9 7.2 NA NA NA NA NA NA NA
AMW-9S 7/10/2018 19.91 0.22 18.6 6.3 NA NA NA NA NA NA NA
AMW-9S 1/11/2019 16.28 0.20 11.7 16.1 NA NA NA NA NA NA NA
AMW-9S 6/14/2019 24.20 2.11 351.1 26.0 NA NA NA NA NA NA NA
AMW-9S 12/17/2019 19.35 1.31 -97.2 9.6 NA NA NA NA NA NA NA
AMW-9S 6/23/2020 19.90 0.26 13.2 8.9 NA NA NA NA NA NA NA
AMW-9S 12/29/2020 16.10 0.56 -19.2 8.49 NA NA NA NA NA NA NA
AMW-9S 6/17/2021 22.70 0.34 -138.6 45.3 NA NA NA NA NA NA NA
AMW-9S 6/21/2022 21.20 0.59 -16.5 52.1 NA NA NA NA NA NA NA
AMW-9S 7/19/2023 18.90 0.53 -114.9 19.02 NA NA NA NA NA NA NA
AMW-10S 10/29/2015 20.21 1.83 -20.4 26.8 NA NA NA NA NA NA NA
AMW-10S 8/2/2016 22.99 0.96 -7.3 63.6 NA <0.0400 2.96 53.5 HF <1.00 8740 104
AMW-10S 12/28/2016 18.03 0.24 -7.1 7.3 2.98 <0.0400 5.99 22.9 HF <1.00 4920 58.2
AMW-10S 7/6/2017 17.85 0.99 -25.0 27.0 NA <0.0300 > 2.73 E 10.5 <0.200 765 53.4
AMW-10S 12/13/2017 14.94 2.19 -10.9 334 NA <0.0300 > 7.31 E 22.5 0.606 2070 H 99.2
AMW-10S 7/12/2018 17.48 0.27 81.8 2.02 1.65 <0.0300 8.03 24.8 <0.200 279 78.6
AMW-10S 1/8/2019 17.22 0.68 98.4 10.09 0.00 0.0840 J 0.174 2.68 0.732 0.174 11.9
AMW-10S 6/13/2019 22.01 3.16 178.7 29.7 0.07 <0.150 0.0594 0.223 1.57 50.9 11.6
AMW-10S 12/17/2019 17.54 5.53 354.6 9.7 0.11 <0.0600 0.0174 0.171 0.974 5.19 6.31
AMW-10S 6/23/2020 20.00 0.20 104.9 10.2 2.15 <0.150 0.601 2.93 0.735 235 13.8
AMW-10S 12/29/2020 17.60 2.34 172.2 9.04 0.26 <0.150 0.0730 0.163 0.592 24.1 8.46
AMW-10S 6/17/2021 20.10 0.28 -75.0 18.74 +++ 0.174 J 1.59 23.9 0.572 974 43.2
AMW-10S 6/20/2022 22.10 1.15 27.8 9.5 +++ 0.085 23.4 1.36 82.4 8.5 13.6
AMW-10S 7/19/2023 20.40 1.56 104.5 8.16 0.05 0.948 J 1.50 10.9 1.5 62.2 <5.00
AMW-11S 11/10/2015 20.23 0.37 0.8 27.1 NA NA NA NA NA NA NA
AMW-11S 7/25/2016 24.72 0.36 55.3 8.6 NA NA NA NA NA NA NA
AMW-11S 12/14/2016 17.83 1.02 -30.1 12.4 NA NA NA NA NA NA NA
AMW-11S 6/29/2017 16.70 1.35 64.2 21.0 NA NA NA NA NA NA NA
AMW-11S 12/12/2017 18.27 0.40 21.5 18.4 NA NA NA NA NA NA NA
AMW-11S 7/11/2018 20.75 0.28 20.3 14.1 NA NA NA NA NA NA NA
AMW-11S 1/11/2019 15.07 0.34 45.1 15.7 NA NA NA NA NA NA NA
AMW-11S 6/12/2019 20.23 0.53 -29.6 2.11 NA NA NA NA NA NA NA
AMW-11S 12/18/2019 14.21 1.09 51.8 1.2 NA NA NA NA NA NA NA
AMW-11S 6/24/2020 22.00 0.26 -11.7 0.51 NA NA NA NA NA NA NA
AMW-11S 12/29/2020 15.90 0.52 6.9 9.09 NA NA NA NA NA NA NA
AMW-11S 6/16/2021 21.80 0.48 5.7 41.13 NA NA NA NA NA NA NA
AMW-11S 12/28/2021 19.70 0.95 -61.2 9.77 NA NA NA NA NA NA NA
AMW-11S 6/23/2022 20.20 1.27 -84.7 9.5 NA NA NA NA NA NA NA
AMW-11S 12/5/2022 17.00 0.12 -2.0 17.3 NA NA NA NA NA NA NA
AMW-11S 7/19/2023 14.20 0.20 -50.2 6.01 NA NA NA NA NA NA NA
AMW-11S 12/6/2023 14.40 0.53 -77.0 37.84 NA NA NA NA NA NA NA
AMW-12S 11/5/2015 18.27 6.2 67.5 41.2 NA NA NA NA NA NA NA
AMW-12S 8/2/2016 19.27 2.84 118.2 9.03 NA NA NA NA NA NA NA
AMW-12S 6/29/2017 18.02 5.60 48.8 11.2 NA NA NA NA NA NA NA
AMW-12S 12/12/2017 18.02 1.13 63.2 11.0 NA NA NA NA NA NA NA
AMW-12S 7/12/2018 17.57 4.09 60.0 16.98 NA NA NA NA NA NA NA
AMW-12S 1/8/2019 16.63 3.06 73.4 51.70 NA NA NA NA NA NA NA
AMW-12S 6/13/2019 19.37 1.64 117.9 63.70 NA NA NA NA NA NA NA
AMW-12S 12/18/2019 13.09 4.56 163.2 3.28 NA NA NA NA NA NA NA
AMW-12S 6/24/2020 22.10 2.20 74.1 9.39 NA NA NA NA NA NA NA
AMW-12S 12/17/2020 14.10 7.07 134.1 43.69 NA NA NA NA NA NA NA
AMW-12S 6/15/2021 22.80 3.38 83.5 126.87 NA NA NA NA NA NA NA
AMW-12S 6/20/2022 23.40 1.36 82.4 8.50 NA NA NA NA NA NA NA
Page 13 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
AMW-12S 7/18/2023 17.20 0.29 -28.9 8.23 NA NA NA NA NA NA NA
AMW-13S 10/29/2015 20.55 0.22 -13.3 42.1 NA NA NA NA NA NA NA
AMW-13S 7/26/2016 22.32 0.21 -29 26.6 3.30 <0.0400 2.51 9.13 ^ HF <1.00 5,120 B 354
AMW-13S 12/15/2016 17.96 0.44 -175.7 11.8 3.36 NA NA NA NA NA NA
AMW-13S 12/27/2016 20.75 0.19 -48.8 11.1 3.30 <0.0400 3.43 12.6 HF <1.00 F1 F2 4,060 62.5
AMW-13S 6/29/2017 19.30 3.62 -39.4 16.8 1.08 <0.0300 > 2.61 E 9.18 <0.200 140 285
AMW-13S 12/13/2017 18.25 0.21 -53.8 4.78 3.30 <0.0300 > 4.41 E 17.7 0.841 1,130 351
AMW-13S 7/11/2018 23.12 0.12 -28.4 8.67 3.30 <0.0300 4.9 15.2 0.244 J 793 446
AMW-13S 1/8/2019 17.58 1.13 31.1 8.57 2.00 <0.0300 2.71 9.02 10.2 272 620
AMW-13S 6/12/2019 18.85 0.04 9.1 9.8 2.49 <0.150 1.49 7.1 6.51 1,170 394
AMW-13S 12/18/2019 18.13 0.68 -15.1 2.79 2.18 <0.0600 0.699 5.41 6.56 510 242
AMW-13S 6/23/2020 20.20 0.46 -80.4 13.01 0.41 <0.150 0.957 0.438 0.336 J 748 332
AMW-13S 12/28/2020 14.50 0.53 -100.2 11.5 2.94 <0.150 0.504 5.26 17.9 470 492
AMW-13S 6/17/2021 19.40 0.36 -101.6 0.61 2.56 <0.150 1.76 5.32 7.76 1,230 623
AMW-13S 6/22/2022 20.70 0.87 90.1 9.2 0.32 0.290 J 5.1 15 0.396 J 1,070 486
AMW-13S 7/19/2023 14.60 0.21 -68.7 10.23 0.11 <0.300 1.52 0.659 0.629 1,730 421
AMW-13I 10/29/2015 18.23 1.41 11.1 19.6 NA NA NA NA NA NA NA
AMW-13I 7/26/2016 23.04 1.32 46.6 11.9 NA NA NA NA NA NA NA
AMW-13I 12/15/2016 9.29 1.05 40.2 9.4 NA NA NA NA NA NA NA
AMW-13I 6/30/2017 17.50 4.00 222.6 5.21 NA NA NA NA NA NA NA
AMW-13I 12/12/2017 17.41 3.30 71.0 2.25 NA NA NA NA NA NA NA
AMW-13I 7/12/2018 18.65 4.69 23.3 3.88 NA NA NA NA NA NA NA
AMW-13I 12/18/2018 16.87 0.22 30.8 5.55 NA NA NA NA NA NA NA
AMW-13I 6/12/2019 18.20 5.59 31.7 4.81 NA NA NA NA NA NA NA
AMW-13I 12/18/2019 13.90 1.41 51.6 2.78 NA NA NA NA NA NA NA
AMW-13I 6/24/2020 25.70 4.76 124.9 4.62 NA NA NA NA NA NA NA
AMW-13I 12/28/2020 16.70 0.52 20.6 7.9 NA NA NA NA NA NA NA
AMW-13I 6/17/2021 18.20 4.73 81.0 2.85 NA NA NA NA NA NA NA
AMW-13I 6/22/2022 20.70 6.04 89.7 9.9 NA NA NA NA NA NA NA
AMW-13I 7/19/2023 14.50 0.09 63.1 4.77 NA NA NA NA NA NA NA
AMW-13D 11/11/2015 18.07 0.58 7.5 11.5 NA NA NA NA NA NA NA
AMW-13D 7/26/2016 26.47 1.54 52.8 8.92 NA NA NA NA NA NA NA
AMW-13D 12/15/2016 12.97 1.18 36.7 6.9 NA NA NA NA NA NA NA
AMW-13D 6/30/2017 17.65 2.30 141.2 3.79 NA NA NA NA NA NA NA
AMW-13D 12/12/2017 16.81 3.11 70.9 4.69 NA NA NA NA NA NA NA
AMW-13D 7/11/2018 18.12 0.69 30.1 4.54 NA NA NA NA NA NA NA
AMW-13D 12/18/2018 18.73 3.33 -28.5 4.99 NA NA NA NA NA NA NA
AMW-13D 6/12/2019 19.01 3.51 28.4 4.19 NA NA NA NA NA NA NA
AMW-13D 12/17/2019 17.37 2.25 127.0 2.70 NA NA NA NA NA NA NA
AMW-13D 6/24/2020 18.20 1.32 56.1 8.16 NA NA NA NA NA NA NA
AMW-13D 12/28/2020 14.80 0.82 20.6 4.50 NA NA NA NA NA NA NA
AMW-13D 6/17/2021 18.10 1.53 58.1 4.95 NA NA NA NA NA NA NA
AMW-13D 6/22/2022 22.10 3.31 18.4 8 NA NA NA NA NA NA NA
AMW-13D 7/19/2023 16.30 0.98 63.7 6.15 NA NA NA NA NA NA NA
AMW-13B 11/11/2015 16.69 0.63 -18.2 2.64 NA NA NA NA NA NA NA
AMW-13B 7/26/2016 17.96 0.34 62.7 3.98 0.0 0.145 0.104 0.244 HF 2.49 9.90 B 179
AMW-13B 12/16/2016 16.37 0.29 -122.1 7.6 0.15 <0.0400 0.0758 0.208 HF <1.00 173 171
AMW-13B 6/29/2017 17.75 2.88 -9.2 5.21 NA 0.669 J 0.0995 0.0280 J 1.7 27.1 210
AMW-13B 12/13/2017 16.17 0.25 35.4 0.81 0.00 <0.0300 0.0775 0.0210 J 1.81 48.4 214
AMW-13B 7/11/2018 17.96 0.37 18.9 1.4 0.03 0.0790 J 0.091 0.0360 J 1.69 14.1 230
AMW-13B 1/8/2019 16.84 0.23 -155.8 0.64 0.00 0.263 0.0941 0.0290 J 3.02 2.55 197
AMW-13B 6/12/2019 17.35 4.02 50.0 1.72 0.00 1.12 0.0657 <0.0200 1.85 19.6 212
AMW-13B 12/18/2019 13.50 1.29 38.7 1.16 0.02 <0.0600 0.0723 <0.0200 1.82 3.39 235
AMW-13B 6/23/2020 17.50 0.45 -25.1 1.21 0.00 <0.150 0.0567 0.0270 J 2.07 23.4 220
AMW-13B 12/28/2020 14.80 0.74 -50.3 1.1 0.00 <0.150 0.125 0.103 1.60 10.1 213
AMW-13B 6/17/2021 16.50 0.41 21.7 5.55 0.00 0.254 J 0.0694 <0.0200 2.04 15.7 217
AMW-13B 12/28/2021 18.70 0.65 -81.1 2.65 0.00 0.501 J 0.0538 0.056 1.53 199 220
AMW-13B 6/22/2022 18.00 2.10 -13.0 3.5 0.00 0.264 J 0.0581 0.0470 J 1.46 77.2 220
AMW-13B 12/5/2022 16.91 0.01 -176.0 5.5 0.00 <0.150 0.0891 0.571 1.26 197 238
AMW-13B 7/19/2023 13.60 0.05 7.1 0.46 0.00 <0.300 0.0757 <0.0200 1.89 77.2 242
AMW-13B 12/6/2023 14.30 0.23 5.8 0.94 0.15 <0.300 0.0749 0.052 1.8 25.2 210
AMW-14S 11/10/2015 17.94 1.92 72.8 54.1 NA NA NA NA NA NA NA
AMW-14S 7/22/2016 19.59 0.48 82.9 12.8 NA NA NA NA NA NA NA
AMW-14S 12/13/2016 15.25 0.67 15.7 116 NA NA NA NA NA NA NA
AMW-14S 6/29/2017 19.75 1.76 -9.5 3.72 NA NA NA NA NA NA NA
Page 14 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
AMW-14S 12/12/2017 15.21 0.28 59.4 26.6 NA NA NA NA NA NA NA
AMW-14S 7/12/2018 16.90 0.24 2.1 0.56 NA NA NA NA NA NA NA
AMW-14S 1/8/2019 16.72 0.27 73.2 7.78 NA NA NA NA NA NA NA
AMW-14S 6/13/2019 17.93 4.35 49.6 9.49 NA NA NA NA NA NA NA
AMW-14S 12/18/2019 18.03 0.29 13.3 4.64 NA NA NA NA NA NA NA
AMW-14S 6/22/2020 18.30 0.18 -69.7 6.18 NA NA NA NA NA NA NA
AMW-14S 12/29/2020 12.00 1.33 49.9 9.9 NA NA NA NA NA NA NA
AMW-14S 6/15/2021 21.30 0.81 95.7 17.45 NA NA NA NA NA NA NA
AMW-14S 12/28/2021 19.30 1.05 64.5 10.12 NA NA NA NA NA NA NA
AMW-14S 6/22/2022 22.30 0.48 75.4 6.32 NA NA NA NA NA NA NA
AMW-14S 12/5/2022 15.88 0.14 -18.0 37.8 NA NA NA NA NA NA NA
AMW-14S 7/18/2023 14.40 0.26 -17.6 6.88 NA NA NA NA NA NA NA
AMW-14S 12/6/2023 16.20 0.30 -21.6 10.5 NA NA NA NA NA NA NA
AMW-15S 10/29/2015 19.24 2.18 -33.3 9.2 NA NA NA NA NA NA NA
AMW-15S 8/3/2016 20.16 0.58 28.3 21.9 NA NA NA NA NA NA NA
AMW-15S 12/14/2016 15.7 0.66 63.9 19.4 NA NA NA NA NA NA NA
AMW-15S 6/27/2017 18.77 1.11 46.3 15.1 NA NA NA NA NA NA NA
AMW-15S 12/12/2017 17.72 0.25 6.0 6.9 NA NA NA NA NA NA NA
AMW-15S 7/12/2018 20.05 0.35 -6.6 2.24 NA NA NA NA NA NA NA
AMW-15S 1/1/019 14.24 3.39 126.4 11.1 NA NA NA NA NA NA NA
AMW-15S 6/13/2019 18.35 7.86 53.1 12.5 NA NA NA NA NA NA NA
AMW-15S 12/16/2019 21.90 2.12 102.3 7.6 NA NA NA NA NA NA NA
AMW-15S 6/23/2020 19.50 0.19 -66.9 8.3 NA NA NA NA NA NA NA
AMW-15S 12/29/2020 9.20 3.87 56.0 8.49 NA NA NA NA NA NA NA
AMW-15S 6/17/2021 20.30 0.75 -117.1 26.1 NA NA NA NA NA NA NA
AMW-15S 6/23/2022 17.90 0.78 -42.8 22.1 NA NA NA NA NA NA NA
AMW-15S 7/20/2023 17.30 0.28 -64.7 23.28 NA NA NA NA NA NA NA
AMW-16S 10/28/2015 19.31 1.97 -47.6 9.4 NA NA NA NA NA NA NA
AMW-16S 7/27/2016 21.51 0.23 2.9 9.4 2.17 <0.0400 2.69 2.27 HF <1.00 1880 B 246
AMW-16S 12/15/2016 15.18 0.83 13.6 21.9 0.94 <0.0400 3.72 2.80 HF <1.00 4970 304
AMW-16S 6/28/2017 22.21 2.48 66.9 0.28 0.70 <0.0300 0.164 0.082 6.31 66.8 237
AMW-16S 12/14/2017 18.36 0.22 18.4 7.1 1.45 <0.0300 > 4.09 E 3.29 0.594 515 380
AMW-16S 7/12/2018 23.17 2.94 3.6 2.58 NA 0.0700 J 1.06 2.23 0.73 595 220
AMW-16S 1/11/2019 14.94 0.73 32.8 12 0.00 <0.0300 1.01 0.354 8.47 99.9 269
AMW-16S 6/13/2019 23.00 2.05 24.4 9.93 0.00 <0.150 1.55 1.25 15 413 318
AMW-16S 12/16/2019 20.81 0.35 -36.2 9.4 2.77 <0.0600 2.12 1.31 5.42 822 332
AMW-16S 6/23/2020 20.10 0.16 -141.9 6.34 2.56 <0.150 3.03 2.34 4.53 1,140 319
AMW-16S 12/28/2020 15.70 0.75 -45.6 4.81 0.00 <0.150 1.59 2.65 8.52 881 321
AMW-16S 6/17/2021 26.80 0.70 -112.9 3.6 0.031 <0.150 4.42 3.31 2.62 1,110 379
AMW-16S 6/22/2022 20.70 1.28 -11.4 9.8 0.820 0.240 J 4.43 1.65 2.39 37 387
AMW-16S 7/19/2023 14.90 0.38 18.6 8.27 0.094 <0.300 0.729 2.56 1.79 472 234
AMW-17S 10/28/2015 19.11 2.07 -52.7 8.6 NA NA NA NA NA NA NA
AMW-17S 7/27/2016 22.59 1.63 -19.2 29.4 NA NA NA NA NA NA NA
AMW-17S 12/14/2016 18.76 0.36 -132.2 8.81 NA NA NA NA NA NA NA
AMW-17S 6/27/2017 21.00 1.69 49.2 39.2 NA NA NA NA NA NA NA
AMW-17S 12/14/2017 18.96 0.99 3.2 12.2 NA NA NA NA NA NA NA
AMW-17S 8/15/2018 19.21 0.38 -16.7 6.03 NA NA NA NA NA NA NA
AMW-17S 1/11/2019 13.09 2.90 111.9 9.25 NA NA NA NA NA NA NA
AMW-17S 6/13/2019 21.45 1.45 24.5 38.8 NA NA NA NA NA NA NA
AMW-17S 12/19/2019 17.73 0.29 240.4 9.83 NA NA NA NA NA NA NA
AMW-17S 6/23/2020 19.50 0.32 -25.8 8.41 NA NA NA NA NA NA NA
AMW-17S 12/29/2020 16.60 0.95 -26.2 21.3 NA NA NA NA NA NA NA
AMW-17S 6/17/2021 26.00 0.57 -77.0 4.7 NA NA NA NA NA NA NA
AMW-18S 10/28/2015 20.09 5.13 57.6 25.7 NA NA NA NA NA NA NA
AMW-18S 7/27/2016 24.28 0.27 9.4 20.1 2.03 <0.0400 0.542 2.60 HF 2.02 3090 B 163
AMW-18S 12/16/2016 16.08 0.53 20.6 8.7 1.26 <0.0400 1.03 2.10 HF <1.00 2130 157
AMW-18S 6/28/2017 21.49 1.10 -67.7 21.8 2.17 <0.0300 0.238 2.82 0.644 82.7 166
AMW-18S 12/14/2017 16.43 0.20 76.7 15.4 3.30 0.879 J 1.36 4.39 1.59 1600 203
AMW-18S 7/12/2018 23.36 0.58 -38.4 9.96 0.19 <0.0300 0.354 2.44 0.377 J 102 177
AMW-18S 1/11/2019 13.78 1.61 75.5 13.7 1.10 <0.0300 0.453 1.64 0.346 J 149 213
AMW-18S 6/13/2019 20.87 0.16 16.6 10 3.03 <0.150 0.682 3.05 3.37 398 259
AMW-18S 12/16/2019 17.52 0.35 137.2 5.41 0.28 <0.0600 0.157 0.368 3.97 182 190
AMW-18S 6/23/2020 21.60 0.19 -134.2 7.21 2.41 <0.150 1.35 2.69 0.586 2,110 287
AMW-18S 12/28/2020 15.30 0.49 -58.7 27.9 1.34 <0.150 1.01 2.15 2.52 1,110 284
AMW-18S 6/17/2021 19.30 0.78 -83.2 6.44 3.27 <0.150 1.82 4.33 1.12 1,090 317
AMW-18S 6/22/2022 23.70 0.53 -49.4 29.7 +++ 0.232 J 1.58 4.01 0.294 1,710 297
Page 15 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
AMW-18S 7/19/2023 15.30 0.04 -40.1 1.10 0.30 <0.300 2.06 7.00 0.892 2,870 337
DEM-MW6R 10/29/2015 20.07 2.23 4.9 11.02 NA NA NA NA NA NA NA
DEM-MW6R 7/20/2016 19.18 0.4 -19.9 6.53 1.67 <0.0400 3.61 4.03 HF <1.00 1380 444
DEM-MW6R 12/16/2016 14.14 0.91 -19.9 19.1 0.15 <0.0400 3.34 4.22 HF <1.00 1120 473
DEM-MW6R 6/28/2017 20.31 0.73 -12.6 5.54 0.29 <0.0300 > 1.99 E 2.87 0.433 J 156 486
DEM-MW6R 12/14/2017 17.29 0.21 111.4 14.2 2.92 <0.0300 > 2.96 E 3.98 0.348 J 710 534
DEM-MW6R 7/12/2018 18.54 0.19 -11.6 4.12 1.28 <0.0300 3.42 5.08 0.254J 120 542
DEM-MW6R 1/8/2019 18.61 0.12 -80.1 6.51 1.93 0.0870 J 1.71 0.188 0.475 J 30.7 468
DEM-MW6R 6/12/2019 16.94 0.15 50.8 3.39 1.43 <0.150 3.26 8.0 <0.200 706 499
DEM-MW6R 12/17/2019 18.74 1.18 -29.8 4.97 0.39 <0.0600 1.81 2.67 <0.200 467 508
DEM-MW6R 6/23/2020 20.20 0.14 -32.1 2.08 0.06 <0.150 2.36 4.72 0.260 J 541 516
DEM-MW6R 12/28/2020 18.20 0.48 -35.3 8.82 1.15 <0.150 2.65 4.05 0.708 582 485
DEM-MW6R 6/16/2021 22.80 0.54 -58.0 9.5 0.02 <0.150 2.92 5.14 <0.200 876 500
DEM-MW6R 6/22/2022 20.90 0.15 -25.2 3.82 1.79 0.241 J 3.88 5.34 0.204 J 1370 532
DEM-MW6R 7/19/2023 17.60 0.20 -84.3 6.62 2.76 <0.3000 3.76 10.4 <0.200 1,610 532
DEM-MW6I 10/29/2015 17.57 0.81 78.7 1.95 NA NA NA NA NA NA NA
DEM-MW6I 7/20/2016 18.85 0.68 52.2 3.58 0.00 <0.0400 <0.00500 <0.0600 HF <1.00 304 250
DEM-MW6I 12/16/2016 15.5 0.61 47.3 11 0.12 <0.0400 0.0254 0.180 HF <1.00 307 256
DEM-MW6I 7/6/2017 17.56 0.98 -11.2 NA NA <0.0300 0.0102 0.0430 J 0.450 J 135 289
DEM-MW6I 12/14/2017 16.42 0.29 122.4 1.01 0.00 <0.0300 0.0105 0.087 1.2 158 300
DEM-MW6I 7/12/2018 20.50 1.25 39.5 1.31 0.95 <0.0300 0.00842 0.139 1.79 153 303
DEM-MW6I 1/7/2019 17.33 0.53 -101.5 1.19 0.00 0.0800 J 0.00982 0.0280 J 1.24 51.8 294
DEM-MW6I 6/12/2019 18.05 2.21 51.1 2.34 0.00 1.57 0.00606 <0.0200 0.728 91.4 303
DEM-MW6I 12/16/2019 19.29 0.81 -106.3 0.52 0.00 <0.0600 0.0105 0.113 0.843 68.4 324
DEM-MW6I 6/23/2020 17.70 0.11 40.0 1.5 0.00 <0.150 0.0125 <0.0200 0.919 111 313
DEM-MW6I 12/28/2020 17.20 0.46 15.2 0.45 1.03 <0.150 0.0101 0.0240 J 1.38 104 297
DEM-MW6I 6/16/2021 19.20 0.97 31.2 1.4 0.009 <0.150 0.00977 <0.0200 0.882 104 296
DEM-MW6I 6/22/2022 18.70 2.00 8.6 2.54 0.000 0.234 J 0.00781 <0.0200 0.809 137 293
DEM-MW6I 7/19/2023 16.80 0.51 -61.8 4.08 0.00 <0.300 0.00783 0.055 1.3 142 298
DEM-MW6D 10/29/2015 17.23 3.29 52.7 35.2 NA NA NA NA NA NA NA
DEM-MW6D 7/20/2016 18.98 0.56 -72.1 5.54 0.00 <0.0400 0.0218 <0.0600 HF <1.00 <0.218 115
DEM-MW6D 12/16/2016 13.72 0.91 60.3 10.5 0.23 <0.0400 0.182 0.300 HF <1.00 155 263
DEM-MW6D 7/6/2017 19.71 5.27 25.4 NA NA 0.658 J 0.047 0.122 1.52 1.07 129
DEM-MW6D 12/14/2017 15.97 0.48 122.3 1.11 0.00 <0.0300 0.0493 0.487 2.86 5.2 143
DEM-MW6D 7/12/2018 20.96 2.70 41.8 1.12 0.26 0.129 J 0.0356 0.336 2.35 4.27 142
DEM-MW6D 1/8/2019 16.02 1.20 40.2 3.46 0.00 0.112 J 0.0811 0.097 2.33 2.08 170
DEM-MW6D 6/12/2019 20.03 2.62 39.9 3.29 0.00 0.432 J 0.137 <0.0200 1.81 8.28 199
DEM-MW6D 12/16/2019 19.33 1.11 -85.3 1.47 0.00 <0.0600 0.116 0.272 0.89 38.4 324
DEM-MW6D 6/23/2020 19.50 0.49 -27.6 4.15 0.00 <0.150 0.139 0.15 0.845 37.9 321
DEM-MW6D 12/28/2020 17.10 0.60 -0.1 1.97 NA <0.150 45.1 0.174 1.60 45.1 282
DEM-MW6D 6/16/2021 28.00 0.74 19.3 2.9 0.017 <0.150 0.839 0.071 0.871 4.50 312
DEM-MW6D 6/22/2022 22.00 3.15 11.7 2.98 1.620 0.238 J 0.483 0.116 0.481 J 7.82 308
DEM-MW6D 7/19/2023 17.80 0.58 15.3 2.67 0.360 <0.300 0.222 0.279 0.555 15.60 329
FMW-15 7/7/2017 17.77 1.34 177.5 4.0 NA NA NA NA NA NA NA
FMW-15 12/8/2018 13.83 1.17 58.3 4.0 NA NA NA NA NA NA NA
FMW-15 6/13/2019 15.12 3.79 56.6 5.51 NA NA NA NA NA NA NA
FMW-15 12/12/2019 14.42 1.12 3.7 5.44 NA NA NA NA NA NA NA
FMW-15 6/24/2020 19.40 1.03 171.9 13.71 NA NA NA NA NA NA NA
FMW-15 12/17/2020 14.80 1.76 71.8 4.05 NA NA NA NA NA NA NA
FMW-15 6/16/2021 14.70 1.65 122.8 3.86 NA NA NA NA NA NA NA
FMW-15 6/22/2022 15.20 0.58 73.5 3.50 NA NA NA NA NA NA NA
FMW-15 2/27/2023 15.20 5.30 183.8 6.21 0 NA 0.08 0.04 NA 1.65 32.0
FMW-15 7/20/2023 15.90 0.41 94.1 3.52 NA NA NA NA NA NA NA
FMW-19 11/10/2015 20.88 5.57 34.1 51.0 NA NA NA NA NA NA NA
FMW-19 8/2/2016 23.62 5.83 127.4 150 NA NA NA NA NA NA NA
FMW-19 12/14/2016 16.18 4.94 145.7 82.6 NA NA NA NA NA NA NA
FMW-19 6/30/2017 17.85 5.92 181.1 28.1 NA NA NA NA NA NA NA
FMW-19 12/12/2017 17.45 5.47 118.6 35.4 NA NA NA NA NA NA NA
FMW-19
FMW-20 10/30/2015 16.66 7.7 209.1 19.8 NA NA NA NA NA NA NA
FMW-20 8/3/2016 20.49 6.82 95 7.50 NA NA NA NA NA NA NA
FMW-20 12/14/2016 15.15 5.81 158.1 40.4 NA NA NA NA NA NA NA
FMW-20 7/5/2017 20.02 6.72 69.6 9.32 NA NA NA NA NA NA NA
FMW-20 12/14/2017 15.26 4.03 13.8 75.0 NA NA NA NA NA NA NA
FMW-19 was abandonded in December 201
Page 16 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
FMW-20 7/12/2018 19.55 11.94 106.7 10.0 NA NA NA NA NA NA NA
FMW-20 1/10/2019 17.02 17.02 112.1 9.17 NA NA NA NA NA NA NA
FMW-20 6/14/2019 17.53 6.91 132.8 10.20 NA NA NA NA NA NA NA
FMW-20 12/18/2019 18.16 4.91 63.1 11.10 NA NA NA NA NA NA NA
FMW-21 10/29/2015 20.78 1.27 15.9 9.10 NA NA NA NA NA NA NA
FMW-21 8/3/2016 20.72 0.41 42.5 12.1 NA <0.0400 1.72 1.11 HF <1.00 1120 275
FMW-21 12/15/2016 13.90 1.89 85.2 94.0 1.21 <0.0400 1.58 0.913 HF <1.00 1160 290
FMW-21 7/6/2017 20.69 0.15 21.4 8.84 1.21 <0.0300 1.7 1.18 <0.200 387 298
FMW-21 12/15/2017 14.75 1.35 117.7 69.3 NA <0.0300 1.2 1.10 H 0.474 J 216 330
FMW-21 7/12/2018 24.37 0.29 31.4 7.99 0.11 <0.0300 2.46 1.77 6.72 292 321
FMW-21 1/10/2019 18.20 0.07 49.7 8.59 0.11 0.0800 J 1.38 2.13 8.02 160 316
FMW-21 6/13/2019 17.23 0.18 246.2 4.80 0.86 0.404 J 2.14 1.83 <0.200 428 338
FMW-21 12/18/2019 17.91 0.69 -1.6 8.24 0.40 <0.0600 2.07 2.86 <0.200 462 363
FMW-21 6/23/2020 19.30 0.12 -13.6 40.3 1.68 <0.150 2.01 2.50 0.356 J 363 331
FMW-21 12/28/2020 18.60 0.47 -20.8 7.9 1.20 0.346 J 2.47 3.30 0.374 J 518 319
FMW-21 6/16/2021 23.90 0.63 -57.3 57.2 0.048 <0.150 2.47 8.14 <0.200 174 323
FMW-21 12/28/2021 23.30 0.58 -59.1 31.7 0.50 0.644 J 2.64 7.10 <0.200 189 307
FMW-21 6/22/2022 26.70 0.59 10.0 8.8 +++ 0.414 J 2.21 1.87 <0.200 240 308
FMW-21 12/5/2022 19.14 0.00 -40.0 50.9 2.45 <0.150 2.81 2.24 <0.200 135 346
FMW-21 2/27/2023 15.80 3.82 21.1 14.5 1.64 NA 1.95 1.59 NA 311 313
FMW-21 7/19/2023 20.50 0.46 -18.6 65.9 0.86 <0.300 2.78 3.7 0.77 348 308
FMW-21 12/6/2023 17.00 3.92 -27.3 36.03 0.61 <0.300 0.677 1.42 0.98 348 268
FMW-22 11/10/2015 18.44 6.3 113.5 37.4 NA NA NA NA NA NA NA
FMW-22 8/3/2016 22.07 7.56 90 19.3 NA NA NA NA NA NA NA
FMW-22 12/13/2016 16.42 5.13 115.8 147 NA NA NA NA NA NA NA
FMW-22 6/29/2017 21.84 6.93 54.6 7.66 NA NA NA NA NA NA NA
FMW-22 1/26/2018 NA NA NA NA NA NA
FMW-22 7/13/2018 NA NA NA NA NA NA
FMW-22 1/10/2019 14.17 10.86 143.60 13.7 NA NA NA NA NA NA NA
FMW-22 6/12/2019 17.52 4.68 326.70 174.0 NA NA NA NA NA NA NA
FMW-22 12/19/2019 15.59 4.01 48.70 3.17 NA NA NA NA NA NA NA
FMW-22 6/22/2020 22.30 4.34 105.60 57.0 NA NA NA NA NA NA NA
FMW-22 12/29/2020 16.60 4.66 36.00 11.1 NA NA NA NA NA NA NA
FMW-22 6/17/2021 20.40 3.24 42.30 81.9 NA NA NA NA NA NA NA
FMW-22 6/22/2022 44.20 6.02 55.20 148.2 NA NA NA NA NA NA NA
FMW-22 7/19/2023 20.70 8.48 27.50 18.1 NA NA NA NA NA NA NA
FMW-23R 11/11/2015 15.63 2.36 -61.3 18.9 NA NA NA NA NA NA NA
FMW-23R 7/26/2016 23.51 0.97 -47.9 5.85 2.16 <0.0400 4.17 8.64 ^ HF <1.00 1,160 B 381
FMW-23R 12/16/2016 13.79 0.94 10.4 12.4 0.54 <0.0400 4.95 9.16 HF <1.00 3,730 411
FMW-23R 7/6/2017 21.30 0.24 -59.1 3.21 3.27 <0.0300 > 4.31 E 11.60 <0.200 907 472
FMW-23R 12/14/2017 15.87 2.01 -70.2 51.8 NA <0.0300 > 5.15 E 9.32 0.425 J 1,220 H 524
FMW-23R 7/12/2018 18.15 0.60 29.5 2.12 1.99 <0.0300 7.03 5.54 <0.200 256 565
FMW-23R 1/9/2019 13.83 7.43 90.1 9.62 0.00 0.0970 J 0.412 0.0250 J 1.96 18.2 287
FMW-23R 6/13/2019 24.00 1.72 -49.5 9.37 2.33 0.776 J 4.07 5.5 3.22 385 374
FMW-23R 12/17/2019 18.16 0.56 -54.1 2.34 +++ <0.0600 5.34 8.76 <0.200 1,150 505
FMW-23R 6/23/2020 23.70 0.63 -69.6 10.1 0.97 <0.150 1.12 1.92 13.4 221 324
FMW-23R 12/28/2020 18.20 4.91 -51.1 9.4 1.07 <0.150 0.927 1.54 7.25 498 258
FMW-23R 6/17/2021 23.90 0.43 -133.7 26.12 +++ <0.150 1.78 6.92 3.01 234 327
FMW-23R 6/22/2022 23.50 0.95 -43.7 7.6 1.20 0.234 J 3.61 6.9 0.626 1080 347
FMW-23R 7/19/2023 15.30 0.48 -37.6 14.37 0.18 <0.300 0.939 0.530 1.23 381 181
FMW-24 11/10/2015 20.27 0.23 -64.2 29.1 NA NA NA NA NA NA NA
FMW-24 7/25/2016 20.17 0.28 -6.6 9.7 2.23 <0.0400 7.12 3.66 ^ HF <1.00 11,100 457
FMW-24 12/27/2016 20.4 0.2 -38 8.43 2.18 <0.0400 5.64 15.7 HF <1.00 13,900 454
FMW-24 7/6/2017 18.39 0.09 -85.2 15.7 1.51 <0.0300 > 4.62 E 15.9 <0.200 4,910 464
FMW-24 7/13/2018 0.0600 J 5.22 12.1 <0.200 1,510 426
FMW-24 1/9/2019 17.02 0.16 -47.90 8.37 1.74 0.0820 J 5.83 19.3 0.345 J 1,090 460
FMW-24 6/12/2019 17.73 0.27 -53.20 3.07 3.30 0.404 J 7.98 26 <0.200 1,640 493
FMW-24 12/17/2019 18.48 0.33 -55.20 3.27 2.74 <0.0600 3.94 9.32 <0.200 3,090 454
FMW-24 6/23/2020 19.20 0.23 -65.80 39.56 0.99 <0.150 7.11 14.0 <0.200 2,700 480
FMW-24 12/29/2020 17.60 0.43 -78.20 17.30 +++ <0.150 5.57 16.1 0.355 J 2,520 460
FMW-24 6/16/2021 21.40 0.40 18.30 38.90 +++ <0.150 5.79 13.8 <0.200 2,410 469
FMW-24 12/28/2021 21.50 0.66 -63.40 7.59 1.92 0.608 J 5.33 17.9 0.632 2,970 501
FMW-24 6/21/2022 20.50 0.76 -45.70 60.30 +++ 0.216 J 6.93 13.4 <0.200 2,470 462
FMW-24 12/12/2022 17.37 0.01 -9.70 3.02 +++ 0.272 J 3.68 15.0 <0.200 3,950 360
FMW-24 2/27/2023 15.70 3.26 -68.00 33.85 +++ NA 3.72 16.0 NA 4,120 423
FMW-24 7/19/2023 17.80 0.34 -116.90 239.4 2.24 0.899 J 9.96 20.0 <0.200 2,470 444
Due to an insuffient water level, parameters were not able to be tak
ue to an insuffient water level, parameters were not able to be tak
ue to an insuffient water level, parameters were not able to be tak
Page 17 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
FMW-24 12/6/2023 16.30 0.30 -120.60 215.8 1.01 <0.300 33.9 33.4 13.1 1,610 404
FMW-24I 11/2/2015 17.33 8.15 61.5 17.0 NA NA NA NA NA NA NA
FMW-24I 11/10/2015 - - - - NA NA NA NA NA NA NA
FMW-24I 7/25/2016 21.02 1.4 21 18.7 NA NA NA NA NA NA NA
FMW-24I 12/14/2016 15.62 0.94 52.8 13.6 NA NA NA NA NA NA NA
FMW-24I 7/5/2017 18.46 0.87 79.2 5.67 NA NA NA NA NA NA NA
FMW-24I 12/14/2017 15.64 2.61 -20.6 44.8 NA NA NA NA NA NA NA
FMW-24I 7/12/2018 18.42 1.31 46.8 1.90 NA NA NA NA NA NA NA
FMW-24I 1/10/2019 12.69 7.65 37.2 8.50 NA NA NA NA NA NA NA
FMW-24I 6/12/2019 20.05 5.82 60.5 3.61 NA NA NA NA NA NA NA
FMW-24I 12/19/2019 17.31 5.81 338.6 9.13 NA NA NA NA NA NA NA
FMW-24I 6/23/2020 17.70 1.01 -3.2 8.31 NA NA NA NA NA NA NA
FMW-24I 12/29/2020 14.90 9.05 15.3 8.70 NA NA NA NA NA NA NA
FMW-24I 6/16/2021 21.20 4.71 43.4 5.65 NA NA NA NA NA NA NA
FMW-24I 6/21/2022 24.20 5.77 99.7 8.20 NA NA NA NA NA NA NA
FMW-24I 7/19/2023 17.50 3.20 121.2 7.87 NA NA NA NA NA NA NA
FMW-24D 11/2/2015 16.64 0.81 60.7 17 NA NA NA NA NA NA NA
FMW-24D 7/25/2016 19.6 0.66 39.5 8.75 0.40 <0.0400 0.5 0.523 HF <1.00 U F1 3.24 J 302
FMW-24D 12/16/2016 15.47 0.36 96.5 4.47 0.00 <0.0400 0.348 0.165 HF <1.00 0.544 J 238
FMW-24D 7/6/2017 17.90 0.18 -15.7 19.7 0.91 <0.0300 0.416 0.602 1.61 1.73 351
FMW-24D 12/14/2017 15.92 1.38 -22.3 54.2 +++ <0.0300 0.567 0.735 2.03 4.25 H 366
FMW-24D 7/12/2018 18.46 0.16 33.3 0.99 0.18 <0.0300 0.324 0.191 1.82 0.794 349
FMW-24D 1/10/2019 15.92 4.92 15.0 1.48 0.34 0.134 J 0.0143 <0.0200 1.2 3.67 365
FMW-24D 6/12/2019 18.53 3.16 -36.9 0.99 0.00 <0.150 0.34 0.231 1.64 5.62 428
FMW-24D 12/17/2019 16.94 0.81 54.5 0.85 0.22 <0.0600 0.268 0.198 1.65 2.94 405
FMW-24D 6/23/2020 17.60 0.99 76.2 0.53 0.00 <0.150 0.275 0.217 1.87 2.35 370
FMW-24D 12/29/2020 16.50 0.34 49.3 2.59 0.00 <0.150 0.259 0.256 2.04 1.36 354
FMW-24D 6/16/2021 19.00 6.82 176.6 3.61 0.07 <0.150 0.24 0.257 1.75 2.55 358
FMW-24D 6/21/2022 21.20 6.51 100.5 9.8 --- 0.252 J 0.0715 0.0390 J 1.84 2.31 384
FMW-24D 7/19/2023 17.90 4.84 34.7 3.02 0.02 <0.300 0.0864 0.0340 J 2.13 0.696 389
FPZ-10 12/28/2016 16.93 0.36 23.9 4.18 0.04 NA NA NA NA NA NA
FPZ-10 6/27/2017 20.19 2.25 21.2 32.0 NA NA NA NA NA NA NA
FPZ-10 7/13/2018 20.92 0.14 -5.0 11.5 NA NA NA NA NA NA NA
FPZ-10 1/11/2019 14.63 0.12 10.2 13.3 NA NA NA NA NA NA NA
FPZ-10 6/12/2019 23.26 0.19 292.9 UR NA NA NA NA NA NA NA
FPZ-10 12/17/2019 16.27 0.35 126.8 19.5 NA NA NA NA NA NA NA
FPZ-10 6/24/2020 20.00 0.14 -91.2 7.21 NA NA NA NA NA NA NA
FPZ-10 12/29/2020 14.80 0.48 -17.8 12.31 NA NA NA NA NA NA NA
FPZ-10 6/17/2021 23.50 0.55 -50.5 22.00 NA NA NA NA NA NA NA
FPZ-10 6/22/2022 22.40 0.70 -73.9 2.10 NA NA NA NA NA NA NA
FPZ-10 7/20/2023 20.00 0.10 -87.6 24.50 NA NA NA NA NA NA NA
FPZ-10I 10/29/2015 17.08 2.09 29.3 8.1 NA NA NA NA NA NA NA
FPZ-10I 7/27/2016 18.46 0.5 40.2 11.4 0.10 <0.0400 0.102 0.140 HF <1.00 F1 20.3 B 301
FPZ-10I 12/16/2016 16.46 0.58 -114.3 14 +++ <0.0400 0.0937 0.211 HF <1.00 20.6 320
FPZ-10I 6/28/2017 17.60 11.22 19.8 11.22 1.88 <0.0300 0.0755 0.104 1.46 7.11 368
FPZ-10I 12/15/2017 15.08 0.55 170.9 2.10 0.0 <0.0300 0.104 0.207 H 1.93 9.58 354
FPZ-10I 7/12/2018 21.76 8.35 65.1 2.47 1.07 0.0880 J 0.0334 0.102 2.81 0.865 334
FPZ-10I 1/11/2019 15.62 1.55 31.0 2.11 0.00 <0.0300 0.129 0.065 1.29 7.06 380
FPZ-10I 6/12/2019 19.65 3.24 292.4 UR 0.00 <0.150 0.0167 <0.0200 1.52 2.3 364
FPZ-10I 12/16/2019 16.84 1.33 160.9 2.79 0.16 <0.0600 0.0565 0.101 1.38 16.9 403
FPZ-10I 6/23/2020 23.80 1.74 -7.1 3.00 0.00 <0.150 0.0501 0.0370 J 1.62 9.12 378
FPZ-10I 12/28/2020 16.90 0.46 28.5 5.24 0.82 <0.150 0.0482 0.101 1.43 17.7 371
FPZ-10I 6/17/2021 20.90 4.62 23.4 1.90 0.001 <0.150 0.00794 <0.0200 1.67 8.18 367
FPZ-10I 6/22/2022 20.40 3.29 117.3 9.80 0.000 0.263 J 0.0236 <0.0200 1.37 2.11 361
FPZ-10I 7/19/2023 17.80 3.35 51.4 10.32 0.000 <0.300 0.00493 J 0.0350 J 1.44 0.829 367
FPZ-11 10/30/2015 19.86 5.62 130.5 32.4 NA NA NA NA NA NA NA
FPZ-11 7/25/2016 25.91 0.48 53.4 19.4 NA NA NA NA NA NA NA
FPZ-11 12/15/2016 14.3 1.65 77.8 264 NA NA NA NA NA NA NA
FPZ-11 7/6/2017 21.85 2.60 119.5 11.38 NA NA NA NA NA NA NA
FPZ-11 12/14/2017 17.23 1.06 -1.1 158 NA NA NA NA NA NA NA
FPZ-11 7/13/2018 20.78 0.45 -7.1 2.07 NA NA NA NA NA NA NA
FPZ-11 1/9/2019 13.72 5.81 100.2 16.9 NA NA NA NA NA NA NA
FPZ-11 6/14/2019 22.67 3.65 232.6 31.5 NA NA NA NA NA NA NA
FPZ-11 12/19/2019 16.22 7.07 305.1 10.8 NA NA NA NA NA NA NA
Page 18 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
FPZ-12 11/12/2015 20.07 2.8 132.6 793 NA NA NA NA NA NA NA
FPZ-12 7/21/2016 21.15 0.72 29.3 7.8 NA NA NA NA NA NA NA
FPZ-12 12/14/2016 18 0.79 27.2 15.1 NA NA NA NA NA NA NA
FPZ-12 6/28/2017 19.69 2.93 61.8 91.3 NA NA NA NA NA NA NA
FPZ-12 12/14/2017 18.06 0.25 44.9 27.7 NA NA NA NA NA NA NA
FPZ-12 7/11/2018 20.18 0.37 51.3 3.96 NA NA NA NA NA NA NA
FPZ-12 1/10/2019 16.96 0.92 115.2 10.2 NA NA NA NA NA NA NA
FPZ-12 6/14/2019 18.84 2.72 45.3 14.3 NA NA NA NA NA NA NA
FPZ-12 12/19/2019 15.29 1.08 92.3 8.32 NA NA NA NA NA NA NA
FPZ-12I 11/12/2015 18.18 0.35 163.8 7.54 NA NA NA NA NA NA NA
FPZ-12I 7/21/2016 17.67 0.7 19.3 0.3 NA NA NA NA NA NA NA
FPZ-12I 12/14/2016 16.48 0.46 16.1 7.2 NA NA NA NA NA NA NA
FPZ-12I 6/29/2017 19.15 5.12 4.7 7.01 NA NA NA NA NA NA NA
FPZ-12I 12/14/2017 15.11 1.33 -57.6 1.93 NA NA NA NA NA NA NA
FPZ-12I 7/11/2018 18.33 1.85 10.9 0.48 NA NA NA NA NA NA NA
FPZ-12I 1/10/2019 11.74 7.99 128.5 0.94 NA NA NA NA NA NA NA
FPZ-12I 6/14/2019 18.15 9.03 29.4 1.24 NA NA NA NA NA NA NA
FPZ-12I 12/19/2019 14.98 0.48 -26.1 2.48 NA NA NA NA NA NA NA
FPZ-13 10/29/2015 17.57 1.39 -1.9 15.6 NA NA NA NA NA NA NA
FPZ-13 7/22/2016 21.87 0.35 -16.4 46.7 NA NA NA NA NA NA NA
FPZ-13 12/14/2016 16.92 0.54 -14.8 272 NA NA NA NA NA NA NA
FPZ-13 6/27/2017 19.62 0.77 17.9 9.80 NA NA NA NA NA NA NA
FPZ-13 12/14/2017 17.31 0.16 22.2 14.3 NA NA NA NA NA NA NA
FPZ-13 7/12/2018 17.81 0.69 49.1 2.93 NA NA NA NA NA NA NA
FPZ-13 1/10/2019 15.32 0.17 55.0 7.80 NA NA NA NA NA NA NA
FPZ-13 6/13/2019 17.65 0.50 57.3 7.84 NA NA NA NA NA NA NA
FPZ-13 12/17/2019 15.62 0.66 46.8 3.87 NA NA NA NA NA NA NA
FPZ-13 6/24/2020 17.20 0.11 -59.1 9.21 NA NA NA NA NA NA NA
FPZ-13 12/29/2020 16.50 6.80 -19.0 10.60 NA NA NA NA NA NA NA
FPZ-13 6/17/2021 16.80 0.39 -38.7 8.48 NA NA NA NA NA NA NA
FPZ-14 10/28/2015 19.07 2.94 -17.4 11.2 NA NA NA NA NA NA NA
FPZ-14 7/22/2016 18.38 0.41 -63.4 26 NA NA NA NA NA NA NA
FPZ-14 12/14/2016 18.35 0.44 -98.4 7.82 NA NA NA NA NA NA NA
FPZ-14 6/27/2017 18.37 0.45 27.8 6.30 NA NA NA NA NA NA NA
FPZ-14 12/14/2017 17.70 1.43 94.7 19.9 NA NA NA NA NA NA NA
FPZ-14 7/13/2018 16.63 0.53 -41.3 5.21 NA NA NA NA NA NA NA
FPZ-14 1/10/2019 11.81 0.72 34.0 31.3 NA NA NA NA NA NA NA
FPZ-14 6/13/2019 21.10 2.99 42.7 19.1 NA NA NA NA NA NA NA
FPZ-14 12/17/2019 15.88 2.77 90.0 6.24 NA NA NA NA NA NA NA
FPZ-15 11/11/2015 - - - - NA NA NA NA NA NA NA
FPZ-15 8/3/2016 21.49 1.06 -22.8 32.0 NA NA NA NA NA NA NA
FPZ-15 12/28/2016 17.62 0.19 39.8 18.4 NA NA NA NA NA NA NA
FPZ-15 6/29/2017 20.64 2.40 21.3 32.4 NA NA NA NA NA NA NA
FPZ-15 12/14/2017 18.36 0.46 37.4 29.0 NA NA NA NA NA NA NA
FPZ-15 7/12/2018 18.00 0.59 -4.2 2.42 NA NA NA NA NA NA NA
FPZ-15 1/11/2019 12.64 1.72 16.3 21.8 NA NA NA NA NA NA NA
FPZ-15 6/13/2019 19.62 1.04 23.5 723 AU NA NA NA NA NA NA NA
FPZ-15 12/16/2019 20.51 0.55 -14.2 7.60 NA NA NA NA NA NA NA
FPZ-15 6/23/2020 21.20 0.96 -62.8 26.5 NA NA NA NA NA NA NA
FPZ-15 12/29/2020 13.40 0.57 -10.3 9.94 NA NA NA NA NA NA NA
FPZ-15 6/17/2021 17.70 0.42 -65.0 4.28 NA NA NA NA NA NA NA
FPZ-5 11/12/2015 20.98 2.71 98.3 23.6 NA NA NA NA NA NA NA
FPZ-5 7/21/2016 26.02 1.12 25.7 9.7 NA NA NA NA NA NA NA
FPZ-5 12/14/2016 16.25 3.7 87.3 35.4 NA NA NA NA NA NA NA
FPZ-5 6/27/2017 21.49 1.45 7.6 6.22 NA NA NA NA NA NA NA
FPZ-5 12/14/2017 19.24 1.07 89.2 8.03 NA NA NA NA NA NA NA
FPZ-5 7/11/2018 23.57 0.67 3.5 37.8 NA NA NA NA NA NA NA
FPZ-5 1/11/2019 12.53 2.10 51.9 2.92 NA NA NA NA NA NA NA
FPZ-5 6/14/2019 18.80 0.65 145.3 UR NA NA NA NA NA NA NA
FPZ-5 12/19/2019 15.41 1.55 61.8 3.74 NA NA NA NA NA NA NA
FPZ-6 11/12/2015 20 4.15 10.9 43.7 NA NA NA NA NA NA NA
FPZ-6 7/22/2016 18.81 3.03 56.6 50.5 NA NA NA NA NA NA NA
FPZ-6 12/15/2016 17.87 1.22 -144.1 39.2 NA NA NA NA NA NA NA
FPZ-6 7/6/2017 18.68 1.45 142.8 16.2 NA NA NA NA NA NA NA
Page 19 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
FPZ-6 12/13/2017 18.40 0.79 72.3 39.5 NA NA NA NA NA NA NA
FPZ-6 7/13/2018 17.93 1.63 12.1 9.6 NA NA NA NA NA NA NA
FPZ-6 1/11/2019 0.55 16.35 97.2 20.7 NA NA NA NA NA NA NA
FPZ-6 6/14/2019 18.00 1.89 331.8 10.5 NA NA NA NA NA NA NA
FPZ-6 12/16/2019 17.24 2.38 270.8 5.39 NA NA NA NA NA NA NA
FPZ-7 7/26/2016 26.44 0.31 66.8 27.4 NA NA NA NA NA NA NA
FPZ-7 12/14/2016 16.69 3.53 -626 750.0 > NA NA NA NA NA NA NA
FPZ-7 6/27/2017 20.74 1.16 53.6 95.9 NA NA NA NA NA NA NA
FPZ-7 12/13/2017 15.38 2.81 34.5 1195 NA NA NA NA NA NA NA
FPZ-7 7/13/2018 20.27 1.02 7.8 91.9 NA NA NA NA NA NA NA
FPZ-7 1/11/2019 12.86 1.06 21.1 38.5 NA NA NA NA NA NA NA
FPZ-7 6/13/2019 23.02 0.50 48.5 6.81 NA NA NA NA NA NA NA
FPZ-7 12/18/2019 11.48 3.62 166.3 2.74 NA NA NA NA NA NA NA
FPZ-8 10/29/2015 19.55 2.03 10.9 9.80 NA NA NA NA NA NA NA
FPZ-8 7/22/2016 25.93 0.27 14.1 29.4 NA NA NA NA NA NA NA
FPZ-8 12/14/2016 18.16 0.35 -10.5 7.90 NA NA NA NA NA NA NA
FPZ-8 6/27/2017 20.16 0.48 30.8 14.9 NA NA NA NA NA NA NA
FPZ-8 7/12/2018 22.70 3.06 14.0 2.43 NA NA NA NA NA NA NA
FPZ-8 1/10/2019 12.83 0.19 47.5 12.0 NA NA NA NA NA NA NA
FPZ-8 6/13/2019 22.32 3.62 48.5 12.6 NA NA NA NA NA NA NA
FPZ-8 12/16/2019 19.65 2.00 106.8 15.7 NA NA NA NA NA NA NA
OW-1 10/30/2015 19.31 3.53 129.9 16.8 NA NA NA NA NA NA NA
OW-1 8/3/2016 21.83 4.07 26.1 9.12 NA NA NA NA NA NA NA
OW-1 12/14/2016 18.29 1.28 -1.5 13.3 NA NA NA NA NA NA NA
OW-1 7/7/2017 18.77 2.20 -37.1 NA NA NA NA NA NA NA NA
OW-1 12/13/2017 14.40 3.60 -36.8 11.8 NA NA NA NA NA NA NA
OW-1 7/11/2018 18.96 0.51 -1.3 8.9 NA NA NA NA NA NA NA
OW-1 1/9/2019 14.29 1.19 43.4 6.04 NA NA NA NA NA NA NA
OW-1 6/14/2019 18.61 0.80 -27.7 5.72 NA NA NA NA NA NA NA
OW-1 12/18/2019 14.31 2.26 21.6 8.16 NA NA NA NA NA NA NA
OW-2 10/28/2015 18.56 3.31 57.7 11.2 NA NA NA NA NA NA NA
OW-2 7/27/2016 21.57 0.21 -14.3 14.3 NA NA NA NA NA NA NA
OW-2 12/14/2016 17.89 0.38 -157 5.81 NA NA NA NA NA NA NA
OW-2 6/27/2017 19.47 2.89 -117.9 5.42 NA NA NA NA NA NA NA
OW-2 12/13/2017 15.40 0.19 9.1 11.8 NA NA NA NA NA NA NA
OW-2 7/11/2018 17.98 0.28 -56.2 2.24 NA NA NA NA NA NA NA
OW-2 1/10/2019 10.85 0.70 44.9 19.3 NA NA NA NA NA NA NA
OW-2 6/12/2019 18.56 0.19 306.8 UR NA NA NA NA NA NA NA
OW-2 12/16/2019 11.97 0.37 198.2 2.6 NA NA NA NA NA NA NA
OW-3 10/28/2015 19.78 2.61 -103.7 9.9 NA NA NA NA NA NA NA
OW-3 8/3/2016 20.45 0.34 -37.1 11.5 NA NA NA NA NA NA NA
OW-3 12/14/2016 18 0.66 -2.9 8.21 NA NA NA NA NA NA NA
OW-3 7/6/2017 19.52 0.90 -60.4 NA NA NA NA NA NA NA NA
OW-3 12/13/2017 17.88 0.25 -32.1 7.0 NA NA NA NA NA NA NA
OW-3 7/12/2018 19.80 0.91 -56.1 4.71 NA NA NA NA NA NA NA
OW-3 1/10/2019 14.24 0.57 85.6 6.77 NA NA NA NA NA NA NA
OW-3 6/12/2019 17.90 0.10 287.7 0.00 NA NA NA NA NA NA NA
OW-3 12/16/2019 17.31 0.79 127.4 2.46 NA NA NA NA NA NA NA
OW-4 10/28/2015 19.89 4.17 -148.3 9.1 NA NA NA NA NA NA NA
OW-4 7/26/2016 24.71 0.27 -12.9 7.9 NA NA NA NA NA NA NA
OW-4 12/14/2016 18.11 0.66 -196.1 3.17 NA NA NA NA NA NA NA
OW-4 6/27/2017 22.70 1.38 -32.1 10.9 NA NA NA NA NA NA NA
OW-4 12/13/2017 17.75 0.23 -59.9 1.25 NA NA NA NA NA NA NA
OW-4 7/12/2018 NA NA NA NA NA NA NA
OW-4 1/11/2019 12 2.18 74.9 10.15 NA NA NA NA NA NA NA
OW-4 6/12/2019 17.9 0.12 30.6 5.26 NA NA NA NA NA NA NA
OW-4 12/16/2019 12.44 0.22 164.3 1.13 NA NA NA NA NA NA NA
OW-4 6/23/2022 19.1 2.89 74.5 8.7 NA NA NA NA NA NA NA
OW-4 7/19/2023 19.4 0.51 -8.3 30.18 NA NA NA NA NA NA NA
OW-5 10/28/2015 20.24 3.17 -106.3 7.7 NA NA NA NA NA NA NA
OW-5 7/27/2016 24.48 0.25 -13.2 12.4 NA NA NA NA NA NA NA
OW-5 12/14/2016 18.12 0.32 -208.6 7.26 NA NA NA NA NA NA NA
OW-5 6/27/2017 20.69 1.47 -125.0 20.6 NA NA NA NA NA NA NA
o an insuffient water level, parameters were not able to b
Page 20 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
OW-5 7/12/2018 18.32 0.16 -17.6 NA NA NA NA NA NA NA
OW-5
OW-6 11/12/2015 17.35 2.64 93 14.8 NA NA NA NA NA NA NA
OW-6 8/2/2016 19.98 0.54 -40.2 8.49 NA NA NA NA NA NA NA
OW-6 12/27/2016 17.03 0.32 -27.2 9.8 NA NA NA NA NA NA NA
OW-6 7/6/2017 19.78 1.51 -43.5 6.0 NA NA NA NA NA NA NA
OW-6 7/12/2018 NA NA NA NA NA NA NA
OW-6 1/10/2019 11.14 0.55 36.8 13.8 NA NA NA NA NA NA NA
OW-6 6/12/2019 19.58 0.09 269.4 UR NA NA NA NA NA NA NA
OW-6 12/16/2019 14.35 2.34 288.9 2.31 NA NA NA NA NA NA NA
OW-7 10/30/2015 18.46 9.24 120.6 28 NA NA NA NA NA NA NA
OW-7 8/3/2016 20.91 6.55 95 11.4 NA NA NA NA NA NA NA
OW-7 12/15/2016 17.55 5.85 -64.4 17.4 NA NA NA NA NA NA NA
OW-7 7/5/2017 12.11 6.84 50.1 10.21 NA NA NA NA NA NA NA
OW-7 12/13/2017 15.11 4.10 22.3 11.9 NA NA NA NA NA NA NA
OW-7 7/12/2018 18.39 11.92 107.8 10.41 NA NA NA NA NA NA NA
OW-7 1/9/2019 18.15 6.64 120.1 8.49 NA NA NA NA NA NA NA
OW-7 6/14/2019 18.16 6.52 123.2 9.78 NA NA NA NA NA NA NA
OW-7 12/18/2019 17.56 5.28 46.9 3.75 NA NA NA NA NA NA NA
OW-8 10/29/2015 19.88 5 19.7 14.6 NA NA NA NA NA NA NA
OW-8 7/22/2016 25.23 4.06 12.6 20.2 NA NA NA NA NA NA NA
OW-8 12/14/2016 15.91 1.74 159.1 99.7 NA NA NA NA NA NA NA
OW-8 6/27/2017 22.70 1.36 -0.9 5.71 NA NA NA NA NA NA NA
OW-8 12/14/2017 16.32 1.07 -122.6 76.6 NA NA NA NA NA NA NA
OW-8 7/12/2018 22.33 0.99 54.7 8.72 NA NA NA NA NA NA NA
OW-8 1/10/2019 13.72 0.31 70.2 9.16 NA NA NA NA NA NA NA
OW-8 6/12/2019 20.04 0.81 308.9 2.26 NA NA NA NA NA NA NA
OW-8 12/18/2019 16.89 0.46 5.2 3.98 NA NA NA NA NA NA NA
OW-8 6/24/2020 17.60 0.51 -19.3 37.47 NA NA NA NA NA NA NA
OW-8 12/28/2020 13.90 0.73 52.4 10.49 NA NA NA NA NA NA NA
OW-8 6/17/2021 22.00 1.00 -52.0 21.0 NA NA NA NA NA NA NA
OW-8 6/23/2022 21.50 1.12 19.8 5.3 NA NA NA NA NA NA NA
OW-8 7/19/2023 25.40 7.91 -33.7 5.4 NA NA NA NA NA NA NA
RW-1 10/30/2015 18.43 2.45 129.8 41.2 NA NA NA NA NA NA NA
RW-1 7/25/2016 21.55 0.33 34.8 26.3 NA NA NA NA NA NA NA
RW-1 12/14/2016 16.12 0.7 28.1 40.6 NA NA NA NA NA NA NA
RW-1 7/7/2017 19.94 0.96 -47.1 NA NA NA NA NA NA NA NA
RW-1 12/13/2017 11.28 4.88 57.8 23.6 NA NA NA NA NA NA NA
RW-1 7/11/2018 24.63 3.07 -6.2 75.7 NA NA NA NA NA NA NA
RW-1 1/9/2019 11.28 18.50 87.8 21.2 NA NA NA NA NA NA NA
RW-1 6/14/2019 17.43 0.49 233.9 UR NA NA NA NA NA NA NA
RW-1 12/20/2019 8.48 3.29 277.5 28.9 NA NA NA NA NA NA NA
RW-2 10/29/2015 18.55 2.67 -89.1 8.1 NA NA NA NA NA NA NA
RW-2 7/26/2016 20.25 0.19 -65.8 11.9 NA NA NA NA NA NA NA
RW-2 12/14/2016 16.99 1.27 -33.3 15.7 NA NA NA NA NA NA NA
RW-2 6/27/2017 18.95 0.59 7.4 7.1 NA NA NA NA NA NA NA
RW-2 12/13/2017 16.64 0.14 -56.1 6.52 NA NA NA NA NA NA NA
RW-2 7/12/2018 16.39 0.56 -146.7 1.86 NA NA NA NA NA NA NA
RW-2 1/11/2019 12.62 1.75 27.8 12.9 NA NA NA NA NA NA NA
RW-2 6/13/2019 20.64 0.46 -46.4 8.45 NA NA NA NA NA NA NA
RW-2 12/17/2019 14.72 0.56 48.4 4.87 NA NA NA NA NA NA NA
SBMW-1R 11/10/2015 19.76 0.3 -55.8 28.5 NA NA NA NA NA NA NA
SBMW-1R 8/2/2016 25.46 2.39 10.3 38.4 +++ <0.0400 6.37 7.92 HF <1.00 5900 411
SBMW-1R 12/28/2016 18.4 0.55 28.2 10 1.94 <0.0400 6.7 8.63 HF <1.00 1700 544
SBMW-1R 7/7/2017 18.71 0.96 -33.5 17.0 3.30 <0.0300 > 7.86 E 6.05 <0.200 572 606
SBMW-1R 12/13/2017 15.45 2.02 -10.2 436 +++ 0.899 J > 7.58 E 7.08 0.253 J 405 H 628
SBMW-1R 7/11/2018 23.80 0.51 -1.9 9.1 1.12 <0.0300 8.06 8.88 0.286 451 627
SBMW-1R 1/8/2019 18.64 0.23 -139.1 5.22 +++ <0.0300 6.9 5.28 0.879 286 601
SBMW-1R 6/13/2019 21.98 0.36 -32.3 17.5 3.3 0.960 J 8.14 6.9 1.96 2480 487
SBMW-1R 12/12/2019 18.53 3.24 -83.9 53.9 3.16 <0.0600 6.66 5.12 <0.200 907 610
SBMW-1R 6/23/2020 20.40 0.17 -69.1 19.44 2.33 <0.150 5.50 7.64 1.05 1,460 424
SBMW-1R 12/28/2020 17.50 1.37 23.9 7.31 2.29 0.527 J 0.505 4.59 0.652 663 24.2
SBMW-1R 6/16/2021 22.10 0.26 -84.3 61.33 +++ <0.150 7.14 11.4 <0.200 1,960 566
SBMW-1R 6/20/2022 21.30 0.69 24.2 8.9 2.29 0.309 J 10.20 10.0 0.213 J 2,080 580
OW-5 was abandoned in Decmeber 2018
an insuffient water level, parameters were not able to b
Page 21 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
SBMW-1R 7/18/2023 17.10 0.11 -98.6 120.23 +++ <0.300 9.95 7.5 <0.200 1,200 567
SBMW-2R 10/28/2015 20.27 0.21 -12.1 15.2 NA NA NA NA NA NA NA
SBMW-2R 8/2/2016 19.01 0.55 37.9 6.33 NA NA NA NA NA NA NA
SBMW-2R 12/14/2016 18.09 3.02 27.4 11 NA NA NA NA NA NA NA
SBMW-2R 6/28/2017 21.43 1.13 119.2 15.7 NA NA NA NA NA NA NA
SBMW-2R 12/12/2017 17.73 0.3 97.2 5.11 NA NA NA NA NA NA NA
SBMW-2R 7/11/2018 27.41 0.26 13.1 68.1 NA NA NA NA NA NA NA
SBMW-2R 12/18/2018 17.71 1.97 59.1 12..2 NA NA NA NA NA NA NA
SBMW-2R 6/11/2019 19.13 4.81 136.4 17.4 NA NA NA NA NA NA NA
SBMW-2R 12/17/2019 19.82 0.66 28.2 7.87 NA NA NA NA NA NA NA
SBMW-2R 6/23/2020 21.2 0.17 115.1 5.64 NA NA NA NA NA NA NA
SBMW-2R 12/28/2020 17.2 0.33 27.2 6.21 NA NA NA NA NA NA NA
SBMW-2R 6/16/2021 22.4 0.31 -4.5 63.81 NA NA NA NA NA NA NA
SBMW-2R 6/22/2022 23.5 0.91 -7.4 10.8 NA NA NA NA NA NA NA
SBMW-2R 7/18/2023 22.7 0.23 -3.3 60.92 NA NA NA NA NA NA NA
SBMW-2I 10/28/2015 18.19 1.45 8.0 5.89 NA NA NA NA NA NA NA
SBMW-2I 7/28/2016 22.46 1.04 41.2 8.34 0.57 <0.0400 0.392 0.738 HF <1.00 231 311
SBMW-2I 12/16/2016 17.56 0.06 -122.2 5.28 0.23 <0.0400 0.252 0.238 HF <1.00 216 348
SBMW-2I 7/7/2017 18.35 3.20 12.9 2.11 1.92 <0.0300 0.968 1.6 6.34 137 361
SBMW-2I 12/13/2017 18.26 0.29 16.0 0.69 0.16 <0.0300 0.595 1.1 7.06 174 375
SBMW-2I 7/11/2018 19.95 0.43 22.9 0.80 0.92 <0.0300 0.428 0.781 6.56 69.8 395
SBMW-2I 1/7/2019 19.17 0.19 88.4 1.34 0.72 <0.0300 0.853 1.1 6.16 32.1 378
SBMW-2I 6/12/2019 21.50 5.95 104.1 2.32 0.00 0.326 J 0.604 <0.0200 6.31 2.07 396
SBMW-2I 12/17/2019 18.70 1.30 -21.3 1.24 0.14 <0.0600 0.458 0.782 5.92 99.9 391
SBMW-2I 6/23/2020 22.20 5.58 160.9 3.98 0.01 <0.150 0.214 <0.0200 6.82 2.03 388
SBMW-2I 12/28/2020 18.10 0.32 -5.1 2.43 1.42 <0.150 0.542 1.39 6.68 103 361
SBMW-2I 6/16/2021 23.10 6.59 50.0 2.91 0.00 <0.150 0.0963 <0.0200 6.98 1.73 377
SBMW-2I 6/22/2022 26.10 7.22 47.6 3.40 0.00 0.266 J 0.0312 <0.0200 6.21 1.71 379
SBMW-2I 7/18/2023 17.60 0.91 -30.6 2.18 0.03 <0.300 0.191 0.264 5.73 58.9 389
SBMW-2D 10/28/2015 18.31 2.47 -40.9 68.5 NA NA NA NA NA NA NA
SBMW-2D 7/28/2016 23.14 0.68 -24.3 6.2 NA NA NA NA NA NA NA
SBMW-2D 12/14/2016 13.01 1.02 -25.5 12.5 NA NA NA NA NA NA NA
SBMW-2D 6/28/2017 20.67 2.79 89.7 2.43 NA NA NA NA NA NA NA
SBMW-2D 12/12/2017 16.28 4.37 18.4 1.79 NA NA NA NA NA NA NA
SBMW-2D 7/10/2018 19.59 0.22 -29.5 5.67 NA NA NA NA NA NA NA
SBMW-2D 12/18/2018 16.58 6.41 74.1 1.45 NA NA NA NA NA NA NA
SBMW-2D 6/11/2019 19.01 1.11 -33.8 1.08 NA NA NA NA NA NA NA
SBMW-2D 12/17/2019 19.08 1.01 -88.2 0.96 NA NA NA NA NA NA NA
SBMW-2D 6/23/2020 20.70 6.51 109.2 2.68 NA NA NA NA NA NA NA
SBMW-2D 12/28/2020 16.20 0.44 -66.5 2.78 NA NA NA NA NA NA NA
SBMW-2D 6/16/2021 21.00 6.98 19.9 4.06 NA NA NA NA NA NA NA
SBMW-2D 6/22/2022 27.00 7.60 14.4 5.6 NA NA NA NA NA NA NA
SBMW-2D 7/18/2023 17.60 7.33 15.4 4.04 NA NA NA NA NA NA NA
SBMW-2B 10/28/2015 17.01 0.23 34 2.05 NA NA NA NA NA NA NA
SBMW-2B 7/28/2016 18.57 0.57 32.5 9.8 0.15 <0.0400 1.20 0.542 HF <1.00 207 314
SBMW-2B 12/27/2016 17.26 0.79 28.6 6.4 0.52 <0.0400 1.29 0.758 HF <1.00 308 337
SBMW-2B 7/7/2017 17.54 1.38 -71.3 7.03 0.86 <0.0300 1.00 0.708 0.313 J 1,010 361
SBMW-2B 12/13/2017 16.87 0.24 13.8 1.43 0.00 <0.0300 0.948 0.292 0.230 J 1,130 374
SBMW-2B 7/12/2018 19.34 1.25 26.4 1.02 0.96 <0.0300 1.07 0.088 1.47 64.6 368
SBMW-2B 1/7/2019 17.39 0.15 30.7 1.55 0.00 <0.0300 1.33 0.141 0.768 310 369
SBMW-2B 6/12/2019 19.50 0.81 -36.1 0.68 0.00 <0.150 1.25 0.093 0.608 744 367
SBMW-2B 12/17/2019 17.84 0.91 -133.0 0.65 0.00 <0.0600 1.19 0.0420 J 1.15 283 382
SBMW-2B 6/23/2020 18.10 0.08 -138.0 2.11 0.08 <0.150 1.12 0.0390 J 0.994 535 373
SBMW-2B 12/28/2020 17.20 0.57 -31.2 3.43 0.23 <0.150 1.13 0.0260 J 1.58 212 362
SBMW-2B 6/16/2021 21.30 0.33 -124.5 2.85 0.00 <0.150 1.09 0.091 0.508 498 359
SBMW-2B 6/22/2022 24.50 0.70 -35.9 3.9 0.00 0.235 J 1.41 0.102 0.655 118 360
SBMW-2B 2/27/2023 16.20 4.81 -166.7 1.42 0.00 NA 1.12 0.126 NA 2420 362
SBMW-2B 7/18/2023 17.00 0.09 -117.1 4.39 0.36 <0.3000 1.03 0.135 1.21 32.8 367
PMW-J-I 12/15/2016 17.71 0.93 23.3 28.4 NA NA NA NA NA NA NA
PMW-J-I 2/17/2017 17.71 0.93 23.3 28.4 NA NA NA NA NA NA NA
PMW-J-I 6/30/2017 18.97 0.82 -57.7 21.0 NA NA NA NA NA NA NA
PMW-J-I 12/12/207 13.30 0.28 -118.4 1.64 NA NA NA NA NA NA NA
PMW-J-I 7/12/2018 18.26 0.68 52.4 6.96 NA NA NA NA NA NA NA
PMW-J-I 1/9/2019 18.14 0.90 119.0 0.9 NA NA NA NA NA NA NA
PMW-J-I 6/12/2019 17.57 2.87 120.6 0.91 NA NA NA NA NA NA NA
Page 22 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
PMW-J-I 12/12/2019 13.98 3.74 43.3 2.37 NA NA NA NA NA NA NA
PMW-J-I 6/23/2020 18.20 0.58 117.1 0.74 NA NA NA NA NA NA NA
PMW-J-I 12/17/2020 14.50 0.72 16.5 1.21 NA NA NA NA NA NA NA
PMW-J-I 6/15/2021 19.30 1.97 96.4 17.1 NA NA NA NA NA NA NA
PMW-J-I 6/21/2022 24.90 7.35 90.2 3.8 NA NA NA NA NA NA NA
PMW-J-I 7/19/2023 18.30 1.79 30.5 2.87 NA NA NA NA NA NA NA
PMW-J-D 12/15/2016 17.19 0.59 -3.6 53.0 NA NA NA NA NA NA NA
PMW-J-D 2/17/2017 17.19 0.59 -3.6 83.0 NA NA NA NA NA NA NA
PMW-J-D 6/30/2017 17.61 1.09 -94.1 82.0 NA NA NA NA NA NA NA
PMW-J-D 12/12/2017 14.51 0.23 -114.7 1.85 NA NA NA NA NA NA NA
PMW-J-D 7/12/2018 18.52 0.01 10.3 6.11 NA NA NA NA NA NA NA
PMW-J-D 1/9/2019 16.99 0.22 103.6 1.01 NA NA NA NA NA NA NA
PMW-J-D 6/12/2019 18.43 1.49 107.0 0.51 NA NA NA NA NA NA NA
PMW-J-D 12/12/2019 13.25 3.13 10.5 1.56 NA NA NA NA NA NA NA
PMW-J-D 6/23/2020 18.80 0.29 81.7 0.07 NA NA NA NA NA NA NA
PMW-J-D 12/17/2020 18.30 1.02 19.9 1.34 NA NA NA NA NA NA NA
PMW-J-D 6/15/2021 19.40 0.92 67.2 5.00 NA NA NA NA NA NA NA
PMW-J-D 6/21/2022 23.20 6.89 71.7 3.40 NA NA NA NA NA NA NA
PMW-J-D 7/19/2023 17.50 1.08 -14.9 2.78 NA NA NA NA NA NA NA
PMW-J-B 12/15/2016 16.9 1.46 4.7 8.91 NA NA NA NA NA NA NA
PMW-J-B 2/17/2017 16.9 1.46 4.7 8.91 NA NA NA NA NA NA NA
PMW-J-B 6/30/2017 17.09 1.83 -77.7 16.0 NA NA NA NA NA NA NA
PMW-J-B 12/12/2017 14.11 2.12 -91.3 0.89 NA NA NA NA NA NA NA
PMW-J-B 7/12/2018 17.74 16.20 59.0 4.42 NA NA NA NA NA NA NA
PMW-J-B 1/9/2019 16.62 0.64 85.1 1.02 NA NA NA NA NA NA NA
PMW-J-B 6/12/2019 17.60 4.13 36.9 0.8 NA NA NA NA NA NA NA
PMW-J-B 12/12/2019 15.02 1.18 -24.1 0.92 NA NA NA NA NA NA NA
PMW-J-B 6/23/2020 20.10 5.03 -35.2 0.45 NA NA NA NA NA NA NA
PMW-J-B 12/17/2020 19.70 1.44 -80.4 1.21 NA NA NA NA NA NA NA
PMW-J-B 6/15/2021 19.80 5.81 -2.0 1.5 NA NA NA NA NA NA NA
PMW-J-B 6/21/2022 20.20 5.96 43.8 3.1 NA NA NA NA NA NA NA
PMW-J-B 7/19/2023 18.60 6.33 -74.1 3.13 NA NA NA NA NA NA NA
PMW-K-I 12/15/2016 17.17 1.17 18.6 9.4 NA NA NA NA NA NA NA
PMW-K-I 2/16/2017 17.17 1.17 18.6 9.4 NA NA NA NA NA NA NA
PMW-K-I 6/28/2017 18.73 0.92 -25.2 3.33 NA NA NA NA NA NA NA
PMW-K-I 12/12/2017 15.91 0.77 -75.7 619 NA NA NA NA NA NA NA
PMW-K-I 7/12/2018 18.50 0.28 -11.8 1.92 NA NA NA NA NA NA NA
PMW-K-I 1/8/2019 18.04 0.37 -69.7 2.22 NA NA NA NA NA NA NA
PMW-K-I 6/12/2019 18.55 0.54 -24.9 1.35 NA NA NA NA NA NA NA
PMW-K-I 12/12/2019 13.99 0.79 -70.4 4.39 NA NA NA NA NA NA NA
PMW-K-I 6/23/2020 20.20 3.26 91.9 23.06 NA NA NA NA NA NA NA
PMW-K-I 12/17/2020 16.90 0.52 -78.0 1.16 NA NA NA NA NA NA NA
PMW-K-I 6/16/2021 19.70 0.60 -50.2 3.59 NA NA NA NA NA NA NA
PMW-K-I 6/20/2022 21.40 5.84 60.9 9.4 NA NA NA NA NA NA NA
PMW-K-I 7/18/2023 20.10 0.83 -42.6 330.68 NA NA NA NA NA NA NA
PMW-K-D 12/15/2016 16.94 0.64 26.1 12.4 NA NA NA NA NA NA NA
PMW-K-D 2/16/2017 16.94 0.64 26.1 12.4 NA NA NA NA NA NA NA
PMW-K-D 6/28/2017 17.45 0.72 10.3 3.08 NA NA NA NA NA NA NA
PMW-K-D 12/12/2017 13.18 3.89 19.8 10.6 NA NA NA NA NA NA NA
PMW-K-D 7/12/2018 17.16 0.22 36.7 1.01 NA NA NA NA NA NA NA
PMW-K-D 1/8/2019 16.67 0.79 -122.9 1.00 NA NA NA NA NA NA NA
PMW-K-D 6/12/2019 18.91 1.04 22.3 0.67 NA NA NA NA NA NA NA
PMW-K-D 12/12/2019 14.10 3.07 32.8 1.48 NA NA NA NA NA NA NA
PMW-K-D 6/23/2020 18.80 1.27 10.4 2.15 NA NA NA NA NA NA NA
PMW-K-D 12/17/2020 16.20 0.51 -5.0 0.16 NA NA NA NA NA NA NA
PMW-K-D 6/16/2021 19.30 0.90 -55.1 2.22 NA NA NA NA NA NA NA
PMW-K-D 6/20/2022 22.10 7.05 66.3 4.00 NA NA NA NA NA NA NA
PMW-K-D 7/18/2023 17.90 6.70 20.1 2.36 NA NA NA NA NA NA NA
PMW-K-B 12/15/2016 16.34 0.74 41.2 5.84 NA NA NA NA NA NA NA
PMW-K-B 2/16/2017 16.34 0.74 41.2 5.84 NA NA NA NA NA NA NA
PMW-K-B 6/28/2017 17.33 0.75 64.8 2.11 NA NA NA NA NA NA NA
PMW-K-B 12/12/2017 13.51 1.88 19.5 10.6 NA NA NA NA NA NA NA
PMW-K-B 7/12/2018 17.36 4.15 84.4 0.98 NA NA NA NA NA NA NA
PMW-K-B 1/8/2019 16.66 0.80 99.8 2.28 NA NA NA NA NA NA NA
PMW-K-B 6/12/2019 19.09 4.33 -38.5 0.96 NA NA NA NA NA NA NA
Page 23 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
PMW-K-B 12/12/2019 16.54 2.98 -30.0 1.27 NA NA NA NA NA NA NA
PMW-K-B 6/24/2020 17.70 5.55 15.3 2.23 NA NA NA NA NA NA NA
PMW-K-B 12/17/2020 16.10 1.41 -69.2 2.01 NA NA NA NA NA NA NA
PMW-K-B 6/16/2021 19.00 2.72 -103.1 3.33 NA NA NA NA NA NA NA
PMW-K-B 6/20/2022 21.40 2.43 72.7 4.6 NA NA NA NA NA NA NA
PMW-K-B 7/18/2023 17.70 2.67 -57.4 2.53 NA NA NA NA NA NA NA
PMW-L-I 12/15/2016 17.12 0.12 -18.4 13.3 NA NA NA NA NA NA NA
PMW-L-I 2/16/2017 17.12 0.12 -19.4 13.3 NA NA NA NA NA NA NA
PMW-L-I 6/28/2017 17.86 2.63 38.2 24.2 NA NA NA NA NA NA NA
PMW-L-I 12/12/2017 15.35 2.86 -16.1 1143 NA NA NA NA NA NA NA
PMW-L-I 7/10/2018 17.78 0.17 -6.8 9.26 NA NA NA NA NA NA NA
PMW-L-I 12/19/2018 13.57 1.50 -43.0 708 NA NA NA NA NA NA NA
PMW-L-I 6/11/2019 18.96 0.53 -3.7 28.7 NA NA NA NA NA NA NA
PMW-L-I 12/11/2019 16.57 1.33 14.7 1.08 NA NA NA NA NA NA NA
PMW-L-I 6/23/2020 19.00 0.18 -40.8 5.2 NA NA NA NA NA NA NA
PMW-L-I 12/17/2020 11.30 1.75 -23.0 4.55 NA NA NA NA NA NA NA
PMW-L-I 6/15/2021 19.10 0.54 -10.6 9.13 NA NA NA NA NA NA NA
PMW-L-I 6/20/2022 21.60 0.54 10.2 8.2 NA NA NA NA NA NA NA
PMW-L-I 7/18/2023 17.20 1.94 1.6 1.77 NA NA NA NA NA NA NA
PMW-L-D 12/15/2016 17.02 0.18 -1.1 11.7 NA NA NA NA NA NA NA
PMW-L-D 2/16/2017 19.02 0.18 -1.1 11.7 NA NA NA NA NA NA NA
PMW-L-D 6/28/2017 18.64 1.60 56.1 1.08 NA NA NA NA NA NA NA
PMW-L-D 12/12/2017 15.39 2.97 -1.2 101 NA NA NA NA NA NA NA
PMW-L-D 7/10/2018 17.94 0.34 38.5 1.28 NA NA NA NA NA NA NA
PMW-L-D 12/19/2018 12.49 31.60 -37.6 1.91 NA NA NA NA NA NA NA
PMW-L-D 6/11/2019 19.03 3.18 58.1 44.6 NA NA NA NA NA NA NA
PMW-L-D 12/11/2019 16.64 1.16 33.7 0.44 NA NA NA NA NA NA NA
PMW-L-D 6/23/2020 18.60 0.20 31.5 8.4 NA NA NA NA NA NA NA
PMW-L-D 12/17/2020 16.50 0.80 10.2 2.19 NA NA NA NA NA NA NA
PMW-L-D 6/15/2021 17.60 0.42 -3.1 2.61 NA NA NA NA NA NA NA
PMW-L-D 6/20/2022 20.20 2.48 16.2 4.5 NA NA NA NA NA NA NA
PMW-L-D 7/18/2023 16.80 0.02 -1.7 1.74 NA NA NA NA NA NA NA
PMW-L-B 12/15/2016 16.91 1.18 92.2 6.26 NA NA NA NA NA NA NA
PMW-L-B 2/16/2017 16.91 1.18 92.2 6.26 NA NA NA NA NA NA NA
PMW-L-B 7/7/2017 17.44 0.15 -580.6 9.86 NA NA NA NA NA NA NA
PMW-L-B 12/12/2017 13.60 3.09 -193.0 24.6 NA NA NA NA NA NA NA
PMW-L-B 7/11/2018 17.79 0.24 126.5 6.32 NA NA NA NA NA NA NA
PMW-L-B 12/19/2018 13.69 4.40 -50.8 11.16 NA NA NA NA NA NA NA
PMW-L-B 6/11/2019 19.19 0.70 -89.2 3.24 NA NA NA NA NA NA NA
PMW-L-B 12/11/2019 14.00 0.93 -16.8 1.49 NA NA NA NA NA NA NA
PMW-L-B 6/23/2020 19.50 3.61 77.3 1.3 NA NA NA NA NA NA NA
PMW-L-B 12/17/2020 9.60 3.12 12.6 2.15 NA NA NA NA NA NA NA
PMW-L-B 6/15/2021 19.60 5.39 -22.3 1.89 NA NA NA NA NA NA NA
PMW-L-B 6/20/2022 21.80 6.23 44.3 2.9 NA NA NA NA NA NA NA
PMW-L-B 7/18/2023 16.80 6.23 -33.7 15.94 NA NA NA NA NA NA NA
PMW-M-I 12/15/2016 16.48 1.6 1.5 9.3 NA NA NA NA NA NA NA
PMW-M-I 2/17/2017 16.48 1.6 1.5 9.5 NA NA NA NA NA NA NA
PMW-M-I 6/28/2017 17.76 0.60 18.9 3.06 NA NA NA NA NA NA NA
PMW-M-I 12/13/2017 11.95 4.42 -20.2 67.3 NA NA NA NA NA NA NA
PMW-M-I 7/12/2018 18.51 0.14 7.5 11.2 NA NA NA NA NA NA NA
PMW-M-I 1/9/2019 16.33 0.27 98.3 1.08 NA NA NA NA NA NA NA
PMW-M-I 6/12/2019 18.83 1.30 22.1 0.88 NA NA NA NA NA NA NA
PMW-M-I 12/12/2019 17.57 0.64 -16.8 1.64 NA NA NA NA NA NA NA
PMW-M-I 6/22/2020 18.00 0.29 -35.1 4.61 NA NA NA NA NA NA NA
PMW-M-I 12/28/2020 16.60 0.47 0.7 1.2 NA NA NA NA NA NA NA
PMW-M-I 6/17/2021 19.00 0.33 -67.0 11.19 NA NA NA NA NA NA NA
PMW-M-I 6/21/2022 22.00 7.47 106.8 4.8 NA NA NA NA NA NA NA
PMW-M-I 7/18/2023 16.80 0.36 -52.7 3.47 NA NA NA NA NA NA NA
PMW-M-D 12/15/2016 16.65 0.32 -80.8 38.4 NA NA NA NA NA NA NA
PMW-M-D 2/16/2017 16.65 0.32 -80.8 38.9 NA NA NA NA NA NA NA
PMW-M-D 6/28/2017 19.82 0.70 36.0 3.40 NA NA NA NA NA NA NA
PMW-M-D 12/13/2017 14.23 0.49 -91.5 55.6 NA NA NA NA NA NA NA
PMW-M-D 7/12/2018 18.61 0.74 52.1 65.9 NA NA NA NA NA NA NA
PMW-M-D 1/9/2019 16.47 0.39 -246.1 1.75 NA NA NA NA NA NA NA
PMW-M-D 6/12/2019 18.97 0.18 -287.8 1.18 NA NA NA NA NA NA NA
Page 24 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
PMW-M-D 12/12/2019 13.08 0.39 -113.2 2.25 NA NA NA NA NA NA NA
PMW-M-D 6/22/2020 19.60 0.22 -137.0 3.62 NA NA NA NA NA NA NA
PMW-M-D 12/28/2020 16.20 0.51 -121.1 1.2 NA NA NA NA NA NA NA
PMW-M-D 6/17/2021 18.50 0.51 -141.8 5.94 NA NA NA NA NA NA NA
PMW-M-D 12/28/2021 18.70 0.69 -90.4 7.48 NA NA NA NA NA NA NA
PMW-M-D 6/21/2022 22.60 5.49 82.1 3.8 NA NA NA NA NA NA NA
PMW-M-D 7/18/2023 17.30 0.08 -115.1 2.98 NA NA NA NA NA NA NA
PMW-M-D 12/6/2023 16.00 0.25 -66.4 10.21 NA NA NA NA NA NA NA
PMW-M-B 12/15/2016 17.51 0.11 -69.7 13.2 NA NA NA NA NA NA NA
PMW-M-B 2/17/2017 17.51 0.11 -69.7 13.2 NA NA NA NA NA NA NA
PMW-M-B 6/28/2017 22.67 0.61 -37.4 1.47 NA NA NA NA NA NA NA
PMW-M-B 12/13/2017 12.81 1.01 -132.8 15.9 NA NA NA NA NA NA NA
PMW-M-B 8/15/2018 19.36 0.47 -110.5 7.66 NA NA NA NA NA NA NA
PMW-M-B 1/8/2019 17.40 5.87 -93.8 7.27 NA NA NA NA NA NA NA
PMW-M-B 6/12/2019 19.00 4.63 -93.7 2.95 NA NA NA NA NA NA NA
PMW-M-B 12/12/2019 10.38 6.94 -34.4 3.14 NA NA NA NA NA NA NA
PMW-M-B 6/22/2020 20.30 4.61 41.9 8.64 NA NA NA NA NA NA NA
PMW-M-B 12/28/2020 14.50 1.97 -150.0 10.2 NA NA NA NA NA NA NA
PMW-M-B 6/17/2021 21.80 3.79 -64.8 18.61 NA NA NA NA NA NA NA
PMW-M-B 6/21/2022 24.20 4.44 23.1 13.7 NA NA NA NA NA NA NA
PMW-M-B 12/5/2022 16.90 0.38 -133.0 6.1 NA NA NA NA NA NA NA
PMW-M-B 7/18/2023 17.90 0.19 -175.3 19.46 NA NA NA NA NA NA NA
PMW-N-I 12/15/2016 14.11 0.41 -12.4 28.7 NA NA NA NA NA NA NA
PMW-N-I 2/16/2017 14.11 0.41 -12.4 28.7 NA NA NA NA NA NA NA
PMW-N-I 6/29/2017 17.68 0.50 29.3 3.55 NA NA NA NA NA NA NA
PMW-N-I 12/13/2017 16.01 0.85 -67.4 29.4 NA NA NA NA NA NA NA
PMW-N-I 7/12/2018 18.77 1.05 7.2 19.8 NA NA NA NA NA NA NA
PMW-N-I 1/8/2019 17.56 2.54 -57.0 1.08 NA NA NA NA NA NA NA
PMW-N-I 6/12/2019 17.41 4.01 10.4 2.01 NA NA NA NA NA NA NA
PMW-N-I 12/16/2019 18.09 1.89 -82.1 2.45 NA NA NA NA NA NA NA
PMW-N-I 6/22/2020 17.70 0.23 -45.7 6.3 NA NA NA NA NA NA NA
PMW-N-I 12/28/2020 16.20 0.53 -22.6 0.73 NA NA NA NA NA NA NA
PMW-N-I 6/15/2021 19.90 5.90 46.3 2.39 NA NA NA NA NA NA NA
PMW-N-I 6/21/2022 20.90 7.22 10.6 2.02 NA NA NA NA NA NA NA
PMW-N-I 7/18/2023 14.00 0.22 2.9 0.69 NA NA NA NA NA NA NA
PMW-N-D 12/15/2016 15.94 0.2 57.0 8.7 NA NA NA NA NA NA NA
PMW-N-D 2/16/2017 15.94 0.2 57.0 8.9 NA NA NA NA NA NA NA
PMW-N-D 6/29/2017 18.23 2.78 166.0 3.89 NA NA NA NA NA NA NA
PMW-N-D 12/12/2017 14.66 1.02 -3.2 116 NA NA NA NA NA NA NA
PMW-N-D 7/12/2018 18.45 0.23 36.9 14.3 NA NA NA NA NA NA NA
PMW-N-D 1/8/2019 16.77 0.33 73.2 1.61 NA NA NA NA NA NA NA
PMW-N-D 6/12/2019 16.31 0.10 37.5 0.72 NA NA NA NA NA NA NA
PMW-N-D 12/16/2019 16.58 1.97 -59.5 0.97 NA NA NA NA NA NA NA
PMW-N-D 6/22/2020 17.20 0.12 28.0 6.02 NA NA NA NA NA NA NA
PMW-N-D 12/28/2020 15.90 0.50 27.0 0.07 NA NA NA NA NA NA NA
PMW-N-D 6/15/2021 18.10 7.98 170.3 2.10 NA NA NA NA NA NA NA
PMW-N-D 6/21/2022 19.00 7.28 102.8 1.49 NA NA NA NA NA NA NA
PMW-N-D 7/18/2023 13.80 0.46 26.8 0.50 NA NA NA NA NA NA NA
PMW-N-B 12/15/2016 15.86 0.16 -130.0 733 NA NA NA NA NA NA NA
PMW-N-B 2/17/2017 15.86 0.16 -130.0 733 NA NA NA NA NA NA NA
PMW-N-B 7/7/2017 19.25 0.25 -255.1 6.66 NA NA NA NA NA NA NA
PMW-N-B 12/12/2017 12.88 1.10 -94.8 9.46 NA NA NA NA NA NA NA
PMW-N-B 7/12/2018 20.15 1.98 65.9 1.01 NA NA NA NA NA NA NA
PMW-N-B 1/8/2019 14.83 5.50 -3.1 2.84 NA NA NA NA NA NA NA
PMW-N-B 6/12/2019 17.61 4.80 22.0 3.45 NA NA NA NA NA NA NA
PMW-N-B 12/16/2019 17.72 3.22 -28.0 2.36 NA NA NA NA NA NA NA
PMW-N-B 6/22/2020 17.10 0.44 -62.5 9.43 NA NA NA NA NA NA NA
PMW-N-B 12/28/2020 11.40 3.54 53.0 1.91 NA NA NA NA NA NA NA
PMW-N-B 6/15/2021 19.00 0.59 106.5 3.97 NA NA NA NA NA NA NA
PMW-N-B 6/21/2022 19.70 1.84 83.4 4.21 NA NA NA NA NA NA NA
PMW-N-B 7/18/2023 13.90 0.09 23.6 3.6 NA NA NA NA NA NA NA
PMW-O-I 12/15/2016 17.15 0.11 -360.9 11.6 NA NA NA NA NA NA NA
PMW-O-I 2/17/2017 17.15 0.11 -360.9 11.5 NA NA NA NA NA NA NA
PMW-O-I 7/6/2017 17.73 0.12 -62.0 7.54 NA NA NA NA NA NA NA
PMW-O-I 12/14/2017 13.62 0.61 -82.4 3.76 NA NA NA NA NA NA NA
Page 25 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
PMW-O-I 7/11/2018 16.62 0.60 10.6 4.27 NA NA NA NA NA NA NA
PMW-O-I 1/9/2019 16.65 0.61 63.3 1.92 NA NA NA NA NA NA NA
PMW-O-I 6/12/2019 20.08 0.61 297.3 0.00 NA NA NA NA NA NA NA
PMW-O-I 12/20/2019 16.13 0.30 189.3 0.95 NA NA NA NA NA NA NA
PMW-O-I 6/24/2020 16.40 0.11 -14.8 10.1 NA NA NA NA NA NA NA
PMW-O-I 12/28/2020 15.90 0.33 -6.4 7.24 NA NA NA NA NA NA NA
PMW-O-I 6/16/2021 18.40 4.63 182.2 3.24 NA NA NA NA NA NA NA
PMW-O-I 6/21/2022 20.60 6.11 89.9 3.7 NA NA NA NA NA NA NA
PMW-O-I 7/19/2023 13.50 0.41 -10.2 3.05 NA NA NA NA NA NA NA
PMW-O-D 12/15/2016 16.61 0.15 -68.0 4.28 NA NA NA NA NA NA NA
PMW-O-D 2/17/2017 16.61 0.15 -68.0 4.28 NA NA NA NA NA NA NA
PMW-O-D 7/6/2017 17.27 0.16 -51.7 11.93 NA NA NA NA NA NA NA
PMW-O-D 12/14/2017 16.16 0.68 -3.4 4.84 NA NA NA NA NA NA NA
PMW-O-D 7/11/2018 18.94 3.81 51.7 2.39 NA NA NA NA NA NA NA
PMW-O-D 1/9/2019 15.57 0.60 46.3 1.82 NA NA NA NA NA NA NA
PMW-O-D 6/12/2019 17.79 0.13 300.2 0.00 NA NA NA NA NA NA NA
PMW-O-D 12/20/2019 16.39 0.22 213.5 0.20 NA NA NA NA NA NA NA
PMW-O-D 6/24/2020 18.20 1.11 103.5 2.10 NA NA NA NA NA NA NA
PMW-O-D 12/28/2020 16.10 0.35 39.1 2.09 NA NA NA NA NA NA NA
PMW-O-D 6/16/2021 18.00 4.05 191.8 3.00 NA NA NA NA NA NA NA
PMW-O-D 6/21/2022 20.60 5.24 88.5 2.70 NA NA NA NA NA NA NA
PMW-O-D 7/19/2023 13.50 0.38 57.2 0.00 NA NA NA NA NA NA NA
PMW-O-B 12/15/2016 17.76 0.24 14.5 11.4 NA NA NA NA NA NA NA
PMW-O-B 2/16/2017 17.76 0.24 14.5 11.4 NA NA NA NA NA NA NA
PMW-O-B 7/7/2017 17.01 0.96 -59.3 NA NA NA NA NA NA NA NA
PMW-O-B 12/14/2017 12.90 0.36 -110.9 4.24 NA NA NA NA NA NA NA
PMW-O-B 7/11/2018 20.83 2.78 -78.4 1.31 NA NA NA NA NA NA NA
PMW-O-B 1/9/2019 14.26 6.24 36.1 5.03 NA NA NA NA NA NA NA
PMW-O-B 6/12/2019 19.95 3.14 258.9 UR NA NA NA NA NA NA NA
PMW-O-B 12/20/2019 16.98 6.96 242.6 7.41 NA NA NA NA NA NA NA
PMW-O-B 6/24/2020 22.30 0.86 86.1 5.8 NA NA NA NA NA NA NA
PMW-O-B 12/28/2020 15.10 0.95 9.2 6.88 NA NA NA NA NA NA NA
PMW-O-B 6/16/2021 20.50 0.56 165.0 3.85 NA NA NA NA NA NA NA
PMW-O-B 6/21/2022 21.10 0.69 123.1 4.8 NA NA NA NA NA NA NA
PMW-O-B 7/19/2023 13.20 0.03 -14.2 10.23 NA NA NA NA NA NA NA
PMW-P-S 1/26/2018 NA NA NA NA NA NA NA
PMW-P-S 7/11/2018 NA NA NA NA NA NA NA
PMW-P-S 1/7/2019 13.67 5.44 42.50 1426.00 NA NA NA NA NA NA NA
PMW-P-S 6/12/2019 19.48 3.64 46.80 198.70 NA NA NA NA NA NA NA
PMW-P-S 12/11/2019 21.00 3.87 306.20 70.10 NA NA NA NA NA NA NA
PMW-P-S 6/21/2020 23.80 4.26 151.1 19.71 NA NA NA NA NA NA NA
PMW-P-S 12/18/2020 NA NA NA NA NA NA NA
PMW-P-S 6/16/2021 NA NA NA NA NA NA NA
PMW-P-S 6/23/2022 23.1 4.05 57.3 9.1 NA NA NA NA NA NA NA
PMW-P-S 7/19/2023 19.90 2.97 84.6 15.5 NA NA NA NA NA NA NA
PMW-P-I 1/26/2018 17.91 2.55 -34.6 2.41 NA NA NA NA NA NA NA
PMW-P-I 7/11/2018 20.23 5.00 43.1 1.13 NA NA NA NA NA NA NA
PMW-P-I 1/7/2019 16.55 5.22 23.9 3.63 NA NA NA NA NA NA NA
PMW-P-I 6/12/2019 18.60 8.24 57.3 1.20 NA NA NA NA NA NA NA
PMW-P-I 12/11/2019 16.41 5.49 336.8 1.54 NA NA NA NA NA NA NA
PMW-P-I 6/21/2020 19.90 5.82 138.9 3.00 NA NA NA NA NA NA NA
PMW-P-I 12/18/2020 16.70 5.49 106.8 0.47 NA NA NA NA NA NA NA
PMW-P-I 6/16/2021 20.30 6.50 84.3 2.00 NA NA NA NA NA NA NA
PMW-P-I 6/22/2022 20.30 8.25 42.1 4.80 NA NA NA NA NA NA NA
PMW-P-I 7/19/2023 19.90 7.66 66.5 13.55 NA NA NA NA NA NA NA
PMW-P-D 1/26/2018 18.53 2.79 -23.8 5.84 NA NA NA NA NA NA NA
PMW-P-D 7/11/2018 20.47 3.60 45.3 1.98 NA NA NA NA NA NA NA
PMW-P-D 1/7/2019 17.76 2.76 124.3 3.56 NA NA NA NA NA NA NA
PMW-P-D 6/12/2019 18.33 7.49 77.4 0.43 NA NA NA NA NA NA NA
PMW-P-D 12/11/2019 18.82 4.35 317.7 0.77 NA NA NA NA NA NA NA
PMW-P-D 6/21/2020 19.50 4.97 181.9 1.81 NA NA NA NA NA NA NA
PMW-P-D 12/18/2020 17.20 3.70 92.0 1.48 NA NA NA NA NA NA NA
PMW-P-D 6/16/2021 19.10 5.18 70.1 2.1 NA NA NA NA NA NA NA
PMW-P-D 6/22/2022 21.60 7.68 39.1 4.1 NA NA NA NA NA NA NA
PMW-P-D 2/27/2023 16.30 3.44 54.4 1.27 NA NA 0.008 <0.02 NA 1.87 89.4
o an insuffient water level, parameters were not able to b
an insuffient water level, parameters were not able to b
an insuffient water level, parameters were not able to b
an insuffient water level, parameters were not able to b
Page 26 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
PMW-P-D 7/19/2023 17.40 4.20 59.3 4.24 NA NA NA NA NA NA NA
PMW-P-B 1/26/2018 17.88 3.09 -55.5 1.24 NA NA NA NA NA NA NA
PMW-P-B 7/11/2018 18.67 1.36 -19.2 1.45 NA NA NA NA NA NA NA
PMW-P-B 1/7/2019 15.49 0.99 -49.5 1.46 NA NA NA NA NA NA NA
PMW-P-B 6/13/2019 17.20 6.11 -7.8 0.96 NA NA NA NA NA NA NA
PMW-P-B 12/11/2019 16.19 4.49 101.2 1.34 NA NA NA NA NA NA NA
PMW-P-B 6/21/2020 17.30 0.61 -51.7 2.04 NA NA NA NA NA NA NA
PMW-P-B 12/18/2020 16.30 7.45 -35.4 9.3 NA NA NA NA NA NA NA
PMW-P-B 6/16/2021 22.70 7.26 -15.2 6.4 NA NA NA NA NA NA NA
PMW-P-B 6/22/2022 26.50 7.54 35.1 8.9 NA NA NA NA NA NA NA
PMW-P-B 7/19/2023 16.80 7.75 -4.6 5.67 NA NA NA NA NA NA NA
PMW-Q-S 1/25/2018 NA NA NA NA NA NA NA
PMW-Q-S 7/11/2018 NA NA NA NA NA NA NA
PMW-Q-S 1/7/2019 16.43 7.68 36.70 96.70 NA NA NA NA NA NA NA
PMW-Q-S 6/13/2019 18.54 9.36 -7.20 81.50 NA NA NA NA NA NA NA
PMW-Q-S 12/12/2019 NA NA NA NA NA NA NA
PMW-Q-S 6/22/2020 18.50 0.80 57.40 872.64 NA NA NA NA NA NA NA
PMW-Q-S 12/18/2020 11.50 4.35 98.60 9.60 NA NA NA NA NA NA NA
PMW-Q-S 6/17/2021 19.00 3.29 98.00 2618.44 NA NA NA NA NA NA NA
PMW-Q-S 6/22/2022 NA NA NA NA NA NA NA
PMW-Q-S 7/19/2023 NA NA NA NA NA NA NA
PMW-Q-I 1/25/2018 16.74 2.63 34.9 4.76 NA NA NA NA NA NA NA
PMW-Q-I 7/11/2018 27.57 4.61 55.5 5.11 NA NA NA NA NA NA NA
PMW-Q-I 1/7/2019 15.99 8.59 130.6 1.66 NA NA NA NA NA NA NA
PMW-Q-I 6/13/2019 20.31 4.45 73.3 1.67 NA NA NA NA NA NA NA
PMW-Q-I 12/12/2019 14.31 3.70 61.9 5.99 NA NA NA NA NA NA NA
PMW-Q-I 6/22/2020 21.20 4.36 113.9 1.95 NA NA NA NA NA NA NA
PMW-Q-I 12/18/2020 16.40 3.40 89.6 2.17 NA NA NA NA NA NA NA
PMW-Q-I 6/17/2021 19.00 4.43 170.8 7.24 NA NA NA NA NA NA NA
PMW-Q-I 6/22/2022 28.10 5.08 100.3 15.65 NA NA NA NA NA NA NA
PMW-Q-I 7/19/2023 17.60 6.54 88.2 9.87 NA NA NA NA NA NA NA
PMW-Q-D 1/26/2018 17.21 3.23 -20.2 76.8 NA NA NA NA NA NA NA
PMW-Q-D 7/11/2018 20.41 8.76 43.6 1.52 NA NA NA NA NA NA NA
PMW-Q-D 1/7/2019 18.11 1.79 100.2 1.09 NA NA NA NA NA NA NA
PMW-Q-D 6/13/2019 18.45 2.76 38.7 0.1 NA NA NA NA NA NA NA
PMW-Q-D 12/12/2019 17.55 1.97 30.7 2.3 NA NA NA NA NA NA NA
PMW-Q-D 6/22/2020 18.20 2.99 104.3 2.46 NA NA NA NA NA NA NA
PMW-Q-D 12/18/2020 17.60 2.52 77.8 6.87 NA NA NA NA NA NA NA
PMW-Q-D 6/17/2021 19.00 7.50 176.8 2.72 NA NA NA NA NA NA NA
PMW-Q-D 6/22/2022 18.30 7.27 99.8 3.52 NA NA NA NA NA NA NA
PMW-Q-D 7/19/2023 17.10 5.95 80.3 4.22 NA NA NA NA NA NA NA
PMW-Q-B 1/25/2018 16.71 5.07 36.9 8.4 NA NA NA NA NA NA NA
PMW-Q-B 7/11/2018 18.68 12.26 29.1 1.41 NA NA NA NA NA NA NA
PMW-Q-B 1/7/2019 16.26 1.75 52.2 3.47 NA NA NA NA NA NA NA
PMW-Q-B 6/13/2019 18.86 6.69 40.4 2.77 NA NA NA NA NA NA NA
PMW-Q-B 12/12/2019 16.80 1.30 -6.4 5.09 NA NA NA NA NA NA NA
PMW-Q-B 6/22/2020 19.00 5.50 -5.4 2.61 NA NA NA NA NA NA NA
PMW-Q-B 12/18/2020 15.80 1.94 -58.8 5.00 NA NA NA NA NA NA NA
PMW-Q-B 6/17/2021 18.60 5.84 17.8 5.05 NA NA NA NA NA NA NA
PMW-Q-B 6/22/2022 20.80 6.09 -9.5 7.01 NA NA NA NA NA NA NA
PMW-Q-B 7/19/2023 16.80 5.29 -63.8 8.15 NA NA NA NA NA NA NA
PMW-R-S 1/25/2018 NA NA NA NA NA NA NA
PMW-R-S 7/11/2018 NA NA NA NA NA NA NA
PMW-R-S 1/7/2019 NA NA NA NA NA NA NA
PMW-R-S 6/13/2019 18.42 0.76 159.70 69.20 NA NA NA NA NA NA NA
PMW-R-S 12/12/2019 NA NA NA NA NA NA NA
PMW-R-S 6/22/2020 20.70 1.33 153.40 84.75 NA NA NA NA NA NA
PMW-R-S 12/18/2020 NA NA NA NA NA NA NA
PMW-R-S 6/17/2021 NA NA NA NA NA NA NA
PMW-R-S 6/22/2022 NA NA NA NA NA NA NA
PMW-R-S 7/19/2023 16.20 1.19 101.50 9.11 NA NA NA NA NA NA NA
PMW-R-I 1/25/2018 15.91 0.73 -0.5 50.4 NA NA NA NA NA NA NA
PMW-R-I 7/11/2018 23.19 0.56 14.7 10.8 NA NA NA NA NA NA NA
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Due to an insuffient water level, parameters were not ab
Page 27 of 28
Table 4
Groundwater Geochemical Field Parameters
Total Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
Well ID Date Temperature Dissolved Oxygen ORP Turbitiy Field
Ferrous
Iron
Nitrogen
(Nitrate +
Nitrite)
Manganese Ferrous Iron Sulfate as
SO4 Methane Alkalinity, Total
(CaCO3)
PMW-R-I 1/7/2019 16.76 0.57 15.5 71.1 NA NA NA NA NA NA NA
PMW-R-I 6/13/2019 17.94 0.91 262.6 41.8 NA NA NA NA NA NA NA
PMW-R-I 12/11/2019 18.19 3.20 66.2 53.1 NA NA NA NA NA NA NA
PMW-R-I 6/21/2020 22.20 0.87 65.4 86.34 NA NA NA NA NA NA NA
PMW-R-I 12/18/2020 13.70 0.54 179.3 77.1 NA NA NA NA NA NA NA
PMW-R-I 6/17/2021 21.80 1.87 103.7 17.23 NA NA NA NA NA NA NA
PMW-R-I 6/22/2022 22.20 1.45 78.7 7.8 NA NA NA NA NA NA NA
PMW-R-I 7/19/2023 17.30 1.05 25.4 9.19 NA NA NA NA NA NA NA
PMW-R-D 1/25/2018 17.73 0.62 -59.3 14.1 NA NA NA NA NA NA NA
PMW-R-D 7/11/2018 19.47 1.01 47.1 5.32 NA NA NA NA NA NA NA
PMW-R-D 1/7/2019 17.65 0.36 99.7 3.35 NA NA NA NA NA NA NA
PMW-R-D 6/13/2019 17.76 4.79 329.3 2.54 NA NA NA NA NA NA NA
PMW-R-D 12/11/2019 16.89 0.63 45.0 3.43 NA NA NA NA NA NA NA
PMW-R-D 6/21/2020 19.60 1.33 96.0 1.94 NA NA NA NA NA NA NA
PMW-R-D 12/18/2020 13.70 0.67 102.7 4.33 NA NA NA NA NA NA NA
PMW-R-D 6/17/2021 19.60 7.20 155.4 10.34 NA NA NA NA NA NA NA
PMW-R-D 6/22/2022 19.90 0.47 105.2 3.3 NA NA NA NA NA NA NA
PMW-R-D 7/19/2023 17.50 0.05 65.3 10.14 NA NA NA NA NA NA NA
PMW-R-B 1/25/2018 17.18 2.39 -34.8 2.17 NA NA NA NA NA NA NA
PMW-R-B 7/11/2018 19.55 0.89 -131.4 0.61 NA NA NA NA NA NA NA
PMW-R-B 1/7/2019 16.38 0.20 -438.1 6.54 NA NA NA NA NA NA NA
PMW-R-B 6/13/2019 17.13 0.27 382.9 1.2 NA NA NA NA NA NA NA
PMW-R-B 12/11/2019 16.60 0.57 -164.0 1.74 NA NA NA NA NA NA NA
PMW-R-B 6/21/2020 20.70 0.86 -72.4 0.01 NA NA NA NA NA NA NA
PMW-R-B 12/18/2020 13.70 0.98 -130.0 2.78 NA NA NA NA NA NA NA
PMW-R-B 6/17/2021 21.80 2.88 -11.9 3.79 NA NA NA NA NA NA NA
PMW-R-B 6/22/2022 17.70 2.13 -75.2 4.1 NA NA NA NA NA NA NA
PMW-R-B 7/19/2023 16.20 1.10 -126.6 5.24 NA NA NA NA NA NA NA
Notes:
PID - photoionization detector
ppm - parts per million
mScm - millisiemens per centimeter
°C - degrees Celsius
mg/L - milligram per liter
ORP - oxydation reduction potential
mV - millivolt
NTU - nephelometric turbidity unit
AU = Attenuation turbidity unit
UR = Under Range for turbidity meter
Page 28 of 28
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
MW-A-I 10/27/2015 2.1 < 0.0199* 2.67 <10 <1.0 <1.0 6.65 <1.0 NA 3.45 <5.0 <5.0 425 <1.0 <3.0
MW-A-I 7/19/2016 <1.0 <0.019 1.26 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 237 <1.0 <3.0
MW-A-I 12/14/2016 <1.0 < 0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 144 <1.0 <3.0
MW-A-I 6/26/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 4.12 <0.20 <1.0 <0.30 110 <0.20 <0.30
MW-A-I 12/11/2017 0.51 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 2.9 <10 <0.20 <0.30
MW-A-I 7/9/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-I 12/17/2018 <0.30 0.011 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 30.0 <0.20 <0.30
MW-A-I 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.722 J <0.20 <1.0 <0.30 19.0 <0.20 <0.30
MW-A-I 12/10/2019 <0.30 0.0065 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-I 6/15/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-I 12/14/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-I 6/14/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.465 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-I 6/20/2022 <0.30 0.12 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.465 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-I 7/18/2023 <0.30 0.020 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 < 1.0 <0.30 <10 <0.20 <0.30
MW-A-D 10/27/2015 72.7 < 0.0203 *184 <10 <1.0 <1.0 <1.0 1.08 NA <1.0 <5.0 7.14 753 <1.0 23.2
MW-A-D 7/19/2016 <1.0 <0.0206 170 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 791 <1.0 <3.0
MW-A-D 12/13/2016 <1.0 < 0.0199 161 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 438 <1.0 <3.0
MW-A-D 6/26/2017 <0.30 <0.20 81.0 <1.0 <0.30 <0.20 <0.20 <0.30 1.53 <0.20 <1.0 <0.30 370 <0.20 <0.30
MW-A-D 12/11/2017 <0.30 <0.20 66.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.661 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-D 7/9/2018 <0.30 <0.0026 74.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 110 <0.20 <0.30
MW-A-D 12/17/2018 <0.30 0.015 J 34.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 150 <0.20 <0.30
MW-A-D 6/10/2019 <0.30 <0.0031 18.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 96.0 <0.20 <0.30
MW-A-D 12/10/2019 <0.30 <0.0031 11.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 55.0 <0.20 <0.30
MW-A-D 6/15/2020 <0.30 <0.0030 8.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-D 12/14/2020 <0.30 <0.0031 5.9 <1.0 <0.30 <0.20 <0.20 0.32 J <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-D 6/14/2021 <0.30 <0.0032 2.7 <1.0 <0.30 <0.20 <0.20 <0.30 0.381 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-D 6/20/2022 <0.30 0.024 1.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-D 7/18/2023 <0.30 <0.0032 4.0 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 < 1.0 <0.30 <10 <0.20 <0.30
MW-A-B 12/2/2015 <1.0 <0.0198 438 <10 <1.0 <1.0 <5.0 <1.0 NA <1.0 <5.0 <5.0 313 <1.0 <3.0
MW-A-B 7/19/2016 <1.0 <0.0207 347 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 587 <1.0 <3.0
MW-A-B 12/14/2016 <1.0 <0.0202 285 F1 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 308 <1.0 <3.0
MW-A-B 6/27/2017 <0.30 <0.20 61.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-B 12/11/2017 <0.30 <0.20 190 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-B 7/9/2018 <0.30 0.031 31.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-B 12/17/2018 <0.30 <0.0032 9.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-B 6/10/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.576 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-B 12/11/2019 <0.30 <0.0032 0.94 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-B 6/15/2020 <0.30 <0.0030 0.80 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <1.0 <0.30 <0.20 <10 <0.30 <0.0900
Analyte
Unit
Page 1 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-A-B 12/14/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-B 6/14/2021 <0.30 <0.0031 0.54 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-B 6/20/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-A-B 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-B-I 10/27/2015 61.1 <0.020 54.9 <10 <1.0 22.5 5.74 3.45 NA 28.6 <5.0 <5.0 144,000 <1.0 <3.0
MW-B-I 7/19/2016 <100 <0.0208 <100 <1,000 <100 <100 <100 <100 4.34 J <100 <500 <500 130,000 <100 <300
MW-B-I 12/13/2016 <50 <200 <50 <500 <50 <50 <50 <50 1.87 J <50 <50 <50 50,900 <50 1<50
MW-B-I 6/28/2017 <1.5 <1.0 21.0 <5.0 <1.5 7.0 <1.0 <1.5 1,180 23.0 <5.0 <1.5 68,000 <1.0 <1.5
MW-B-I 12/13/2017 <3.0 <2.0 <2.0 <10 <3.0 <2.0 <2.0 <3.0 485 17.0 <10 <3.0 32,000 <2.0 <3.0
MW-B-I 7/10/2018 3.0 <0.0026 7.6 <5.0 <1.5 1.9 <1.0 <1.5 229 20.0 <5.0 <1.5 29,000 <1.0 <1.5
MW-B-I 12/17/2018 <1.5 <0.0031 3.5 J <5.0 <1.5 <1.0 <1.0 <1.5 13.9 24.0 <5.0 <1.5 59,000 <1.0 <1.5
MW-B-I 6/10/2019 <0.30 <0.0031 3.3 <1.0 <0.30 <0.20 <0.20 <0.30 9.18 10.0 <1.0 <0.30 21,000 <0.20 <0.30
MW-B-I 12/12/2019 <0.30 <0.0031 1.7 <1.0 <0.30 <0.20 <0.20 <0.30 3.08 7.1 <1.0 <0.30 <10 <0.20 <0.30
MW-B-I 6/15/2020 <0.30 <0.0032 1.9 1.3 <0.30 <0.20 <0.20 <0.30 2.07 6.7 <1.0 <0.30 9,400 <0.20 <0.30
MW-B-I 12/14/2020 <0.30 <0.0032 0.82 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 2.3 <1.0 <0.30 2,500 <0.20 <0.30
MW-B-I 6/14/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 2.5 <1.0 <0.30 3,100 <0.20 <0.30
MW-B-I 6/20/2022 <0.30 0.041 P <0.20 <1.0 <0.30 0.34 J <0.20 <0.30 1.80 <0.20 <1.0 <0.30 340 0.31 J <0.30
MW-B-I 7/19/2023 <0.30 <0.0031 < 0.20 U <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 < 1.0 <0.30 400 <0.20 <0.30
MW-B-D 10/27/2015 <1.0 <0.019 114 <10 <1.0 6.4 <10 <1.0 NA 406 <50 <5.0 316,000 <1.0 <3.0
MW-B-D 7/20/2016 <100 <0.0198 483 <1,000 <100 <100 <100 <100 6.88 5,280 <500 <500 252,000 <100 <300
MW-B-D 12/13/2016 <50 <0.0202 74.0 < 500 <50 <50 <50 <50 1.47 J 361 <50 <50 68,400 <50 <50
MW-B-D 6/28/2017 <1.5 <1.0 20.0 <5.0 <1.5 <1.0 <1.0 <1.5 31.7 380 <5.0 <1.5 130,000 <1.0 <1.5
MW-B-D 12/13/2017 <3.0 <2.0 8.0 <10 <3.0 <2.0 <2.0 <3.0 68.1 130 <10 <3.0 5,700 <2.0 <3.0
MW-B-D 7/9/2018 <1.5 <0.0026 21.0 <5.0 <1.5 <1.0 <1.0 <1.5 26.8 450 <5.0 <1.5 57,000 <1.0 <1.5
MW-B-D 12/17/2018 <0.30 <0.0032 3.0 <1.0 <0.30 0.88 <0.20 <0.30 16.0 180 <1.0 <0.30 57,000 <0.20 <0.30
MW-B-D 6/11/2019 <0.30 <0.0031 15.0 <1.0 <0.30 <0.20 <0.20 <0.30 32.6 260 <1.0 <0.30 82,000 <0.20 <0.30
MW-B-D 12/12/2019 <0.30 <0.0032 <1.0 <5.0 <1.5 <1.0 <1.0 <1.5 <0.0900 140 <5.0 <1.5 85,000 <1.0 <1.5
MW-B-D 6/15/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 3.92 95.0 <1.0 <0.30 40,000 <0.20 <0.30
MW-B-D 12/14/2020 <3.0 <0.0031 12.0 <10 <3.0 <2.0 <2.0 <3.0 3.51 170 <10 <3.0 65,000 <2.0 <3.0
MW-B-D 6/14/2021 <3.0 <0.0031 15.0 <10 <3.0 <2.0 <2.0 <3.0 5.31 140 <10 <3.0 92,000 <2.0 <3.0
MW-B-D 6/20/2022 <3.0 0.0086 J <2.0 <10 <3.0 <2.0 <2.0 <3.0 3.66 79 <10 <3.0 20,000 <2.0 <3.0
MW-B-D 7/19/2023 <0.30 <0.0031 4.0 <1.0 <0.30 <0.20 <0.20 <0.30 NA 180 < 1.0 <0.30 30,000 <0.20 1.7 J
MW-B-B 12/2/2015 <1.0 <0.020 86.2 <10 <1.0 <1.0 <10 <1.0 NA 197 <50 <5.0 6,050 <1.0 <3.0
MW-B-B 7/20/2016 32.3 <0.0206 62.0 <100 <10 <10 <10 14.1 5.69 174 <50 <50 103,000 11.5 86.1
MW-B-B 12/14/2016 29 <0.020 81.6 <50 <5.0 7.17 <5.0 14.2 10.3 151 <5.0 <5.0 73,700 9.75 86.6
MW-B-B 6/26/2017 7.8 <1.0 44.0 <5.0 <1.5 6.2 <1.0 10.0 672 100 <5.0 <1.5 110,000 6.8 63.0
MW-B-B 12/13/2017 <3.0 <2.0 28.0 <10 <3.0 2.6 <2.0 <3.0 237 75.0 <10 <3.0 150,000 <2.0 8.5
Page 2 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-B-B 7/9/2018 <1.5 <0.0026 36.0 <5.0 <1.5 2.4 <1.0 <1.5 148 76.0 <5.0 <1.5 59,000 <1.0 8.2
MW-B-B 12/17/2018 <0.30 <0.20 17.0 <1.0 <0.30 1.7 <0.20 0.85 J 38.4 55.0 <1.0 <0.30 56,000 0.53 J 4.8
MW-B-B 6/10/2019 5.3 <0.0031 29.0 2.6 <0.30 3.4 <0.20 1.8 524 33.0 <1.0 0.73 J 150,000 0.76 J 11.0
MW-B-B 12/12/2019 4.4 J <0.0031 20.0 <5.0 <1.5 2.3 J <1.0 1.5 J 155 45.0 <5.0 <1.5 120,000 <1.0 8.6
MW-B-B 6/15/2020 3.0 <0.0031 14.0 <1.0 <0.30 1.3 <0.20 1.0 174 45.0 <1.0 <0.30 110,000 0.45 J 6.0
MW-B-B 12/14/2020 1.1 <0.0031 9.2 <1.0 <0.30 0.96 J <0.20 1.2 80.7 29.0 <1.0 0.56 J 430,000 0.43 J 6.1
MW-B-B 6/14/2021 3.1 J <0.0031 7.0 J <10.0 <3.0 <2.0 <2.0 <3.0 130 34.0 <10.0 <3.0 130,000 <2.0 <3.0
MW-B-B 12/28/2021 <7.5 <0.0031 <5.0 <25.0 <7.5 <5.0 <5.0 <7.5 84.0 14.0 J <25.0 <7.5 170,000 <5.0 <7.5
MW-B-B 6/20/2022 <3.0 <0.0032 <2.0 <10 <3.0 <2.0 <2.0 <3.0 49.4 100 <10 <3.0 5,500 <2.0 <3.0
MW-B-B 12/5/2022 1.6 <0.0031 2.6 <1.0 <0.30 0.27 J <0.20 0.44 J NA 19 <1.0 <0.30 59,000 <0.20 2.6
MW-B-B 2/27/2023 <3.0 <0.0031 <2.0 <10 <3.0 <2.0 <2.0 <3.0 NA 30 <10 <3.0 94,000 <2.0 <3.0
MW-B-B 7/19/2023 0.81 J <0.0032 1.8 <1.0 <0.30 <0.20 <0.20 0.39 J NA <0.20 <1.0 <0.30 100,000 <0.20 1.7 J
MW-B-B 12/6/2023 <15 <0.0032 <10 <50 <15 <10 <10 <15 NA <10 <50 <15 150,000 <10 <15
MW-C-I 10/27/2015 184 <0.0204 7.55 <10 <1.0 2.55 2.05 23.1 NA 34.0 <5.0 <5.0 14,600 <1.0 20.1
MW-C-I 7/20/2016 <50 <200 <50 <500 <50 <50 <50 <50 2.99 J <50 <50 <50 16,100 <50 <50
MW-C-I 12/13/2016 19.6 < 0.0199 <10 <100 <10 <10 <10 <10 <5.0 11.3 <50 <50 11,500 <10 <30.0
MW-C-I 6/28/2017 0.64 <0.20 <0.20 <1.0 <0.30 1.0 <0.20 <0.30 1,190 3.1 <1.0 <0.30 17,000 <0.20 <0.30
MW-C-I 12/11/2017 <0.30 <0.20 0.7 <1.0 <0.30 0.68 <0.20 <0.30 190 1.7 <1.0 <0.30 3,200 <0.20 <0.30
MW-C-I 7/9/2018 2.3 <0.0027 <0.20 <1.0 <0.30 0.83 <0.20 <0.30 334 1.8 <1.0 0.68 5,800 0.89 <0.30
MW-C-I 12/17/2018 0.31 J <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 23.6 0.87 J <1.0 <0.30 5,800 <0.20 0.46 J
MW-C-I 6/11/2019 0.56 J <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 9.53 1.7 <1.0 2.7 4,900 <0.20 <0.30
MW-C-I 12/11/2019 0.35 J 0.0071 JP <0.20 <1.0 <0.30 0.43 J <0.20 <0.30 23.9 1.6 <1.0 <0.30 8,700 0.66 J <0.30
MW-C-I 6/22/2020 1.1 <0.0030 <0.20 <1.0 <0.30 0.34 J <0.20 <0.30 20.2 0.91 J <1.0 <0.30 2,900 <0.20 <0.30
MW-C-I 12/15/2020 1.4 <0.0032 <0.20 1.9 <0.30 0.24 J <0.20 <0.30 12.1 0.32 J <1.0 <0.30 2,500 <0.20 <0.30
MW-C-I 6/14/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 6.62 <0.20 <1.0 <0.30 3,100 <0.20 <0.30
MW-C-I 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 6.98 <0.20 <1.0 <0.30 2,700 <0.20 <0.30
MW-C-I 7/17/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 1,300 <0.20 <0.30
MW-C-D 10/27/2015 <1.0 <200 267 <10 <1.0 62.2 <10 <1.0 NA 270 <50 <5.0 151,000 <1.0 <3.0
MW-C-D 7/20/2016 <100 <0.0202 237 <1,000 <100 <100 <100 <100 5.02 301 <500 <500 61,100 <100 <300
MW-C-D 12/13/2016 <20 <0.0198 252 <200 <20 <20 <20 <20 <5.0 280 <100 <100 30,600 <20 <60.0
MW-C-D 6/28/2017 <0.30 <0.20 1.6 <1.0 <0.30 <0.20 <0.20 <0.30 8.56 41 <1.0 <0.30 350 <0.20 <0.30
MW-C-D 12/11/2017 <0.30 <0.20 150 <1.0 <0.30 0.79 <0.20 <0.30 <0.30 270 <1.0 <0.30 28,000 <0.20 <0.30
MW-C-D 7/9/2018 <1.5 <0.0026 190 <5.0 <1.5 <1.0 <1.0 4.3 528 350 <5.0 <1.5 15,000 <1.0 <1.5
MW-C-D 12/17/2018 52.0 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 235 2.4 <1.0 <0.30 2,500 <0.20 <0.30
MW-C-D 6/11/2019 16.0 <0.0031 16.0 2.5 0.58 J 1.1 <0.20 0.88 J 697 280 <1.0 <0.30 14,000 <0.20 <0.30
MW-C-D 12/12/2019 66.0 <0.0031 1.1 <1.0 1.5 0.44 J 0.44 J 0.80 J 62.5 12.0 <1.0 <0.30 18,000 <0.20 <0.30
MW-C-D 6/22/2020 27.0 <0.0031 27.0 <1.0 <0.30 0.26 J 0.82 J 0.89 J 39.7 12.0 <1.0 <0.30 19,000 <0.20 <0.30
MW-C-D 12/15/2020 <0.30 <0.0032 <0.20 1.8 0.64 J 0.24 J <0.20 0.66 J 26.0 6.9 <1.0 <0.30 9,500 <0.20 <0.30
Page 3 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-C-D 6/14/2021 <1.5 <0.0031 <1.0 <5.0 <1.5 <1.0 <1.0 <1.5 25.0 190 <1.0 <0.30 19,000 <0.20 <0.30
MW-C-D 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 1.0 <0.20 <0.30 1.15 52 <1.0 <0.30 6,000 <0.20 <0.30
MW-C-D 7/17/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA 200 <1.0 <0.30 7,600 <0.20 <0.30
MW-C-B 12/2/2015 <1.0 <0.020 89.5 <10 <1.0 <1.0 <50 <1.0 NA 275 <50 <5.0 33,600 <1.0 <3.0
MW-C-B 7/20/2016 <50 <0.0198 79.3 <500 <50 <50 <50 <50 5.16 409 <50 <50 73,300 <50 <50
MW-C-B 12/13/2016 <20 < 0.0199 <20 <200 <20 <20 <20 <20 1.51 J 136 <100 <100 25,600 <20 <60.0
MW-C-B 6/28/2017 <0.30 <0.20 5.9 <1.0 <0.30 <0.20 <0.20 <0.30 7.82 78.0 <1.0 <0.30 17,000 <0.20 <0.30
MW-C-B 12/11/2017 <0.30 <0.20 38.0 <1.0 <0.30 <0.20 <0.20 <0.30 7.57 260 <1.0 <0.30 210,000 0.48 <0.30
MW-C-B 7/9/2018 <0.30 <0.20 54.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 340 <1.0 <0.30 29,000 <0.20 <0.30
MW-C-B 12/17/2018 <0.30 <0.0032 3.8 <1.0 <0.30 <0.20 <0.20 <0.30 7.20 83.0 <1.0 <0.30 10,000 <0.20 <0.30
MW-C-B 6/10/2019 <0.30 <0.0031 7.6 <1.0 <0.30 <0.20 <0.20 <0.30 15.5 100 <1.0 <0.30 18,000 <0.20 <0.30
MW-C-B 12/12/2019 <0.30 <0.0032 7.0 <1.0 <0.30 <0.20 <0.20 <0.30 6.24 93.0 <1.0 <0.30 15,000 <0.20 <0.30
MW-C-B 6/22/2020 <0.30 <0.0030 3.3 <1.0 <0.30 <0.20 <0.20 <0.30 7.17 44.0 <1.0 <0.30 1,400 <0.20 <0.30
MW-C-B 12/15/2020 <0.30 <0.0030 2.2 <1.0 <0.30 <0.20 <0.20 <0.30 15.0 16.0 <1.0 <0.30 <10 <0.20 <0.30
MW-C-B 6/14/2021 <0.30 <0.0031 1.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 6.3 <1.0 <0.30 <10 <0.20 <0.30
MW-C-B 6/21/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 2.53 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-C-B 7/17/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-D-I 10/27/2015 7.5 <0.020* <1.0 <10 <1.0 50.3 5.12 <1.0 NA 6.33 <5.0 <5.0 781 <1.0 <3.0
MW-D-I 7/19/2016 <1.0 <0.020 1.42 <10 <1.0 <1.0 <1.0 <1.0 <5.0 3.35 <5.0 <5.0 894 <1.0 <3.0
MW-D-I 12/14/2016 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 2.47 <5.0 <5.0 607 <1.0 <3.0
MW-D-I 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.576 2.4 <1.0 <0.30 1,200 <0.20 <0.30
MW-D-I 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 13.9 <0.20 <1.0 <0.30 700 <0.20 <0.30
MW-D-I 7/10/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 5.93 1.6 <1.0 <0.30 710 <0.20 <0.30
MW-D-I 12/17/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 36.8 1.2 <1.0 <0.30 520 <0.20 <0.30
MW-D-I 6/11/2019 <0.30 <0.0031 <0.20 3 <0.30 <0.20 <0.20 <0.30 4.9 1.0 <1.0 <0.30 750 <0.20 <0.30
MW-D-I 12/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.4 0.90 J <1.0 <0.30 750 <0.20 <0.30
MW-D-I 6/22/2020 <0.30 <0.0031 0.36 J <1.0 <0.30 0.21 J <0.20 <0.30 <0.0900 1.0 <1.0 <0.30 430 <0.20 <0.30
MW-D-I 12/15/2020 <0.30 <0.0032 <0.20 3.2 <0.30 <0.20 0.63 J <0.30 <0.0900 1.1 <1.0 1.4 440 <0.20 <0.30
MW-D-I 6/15/2021 <0.30 <0.0031 0.33 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.1 1.7 J <0.30 330 <0.20 <0.30
MW-D-I 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-D-I 7/18/2023 <0.30 0.038 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 380 <0.20 <0.30
MW-D-D 10/27/2015 <1.0 <0.0198*335 <10 <1.0 <1.0 <10 <1.0 NA 830 <50 <5.0 15,900 <1.0 <3.0
MW-D-D 7/19/2016 <10 <0.020 216 <100 <10 <10 <10 <10 1.2 J 1,200 <50 <50 43,300 <10 <30.0
MW-D-D 12/13/2016 <10 < 0.0199 11.4 <100 <10 <10 <10 <10 7.13 1,320 <50 <50 39,200 <10 <30.0
MW-D-D 6/26/2017 <1.5 <1.0 110 <5.0 <1.5 <1.0 <1.0 <1.5 3.04 1,200 <5.0 <1.5 43,000 <1.0 <1.5
MW-D-D 12/13/2017 <0.30 <0.20 66.0 <1.0 <0.30 <0.20 <0.20 <0.30 4.58 930 <1.0 <0.30 19,000 <0.20 <0.30
MW-D-D 7/10/2018 <0.30 <0.0026 9.6 <1.0 <0.30 <0.20 <0.20 <0.30 7.55 1,200 <1.0 <0.30 19,000 <0.20 <0.30
Page 4 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-D-D 12/19/2018 <0.30 <0.0032 69.0 <1.0 <0.30 <0.20 <0.20 <0.30 1.59 1,500 <1.0 <0.30 41,000 <0.20 <0.30
MW-D-D 6/11/2019 3.6 <0.0031 22.0 2.5 <0.30 <0.20 <0.20 2.7 58.0 940 <1.0 <0.30 12,000 <0.20 <0.30
MW-D-D 12/12/2019 0.70 J <0.0032 8.1 3.2 <0.30 0.31 J 0.75 J 0.60 J 17.4 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-D-D 6/22/2020 2.6 <0.0030 19.0 <1.0 <0.30 0.57 J <0.20 1.4 32.5 1,000 2.7 1.8 11,000 <0.20 0.85 J
MW-D-D 12/15/2020 14.0 <0.0031 2.1 3.4 <0.30 <0.20 0.78 J 0.92 J 92.5 400 <1.0 <0.30 1,600 0.64 J 1.5
MW-D-D 6/15/2021 <1.5 <0.0032 11.0 <5.0 <1.5 <1.0 <1.0 <1.5 10.9 960 <5.0 <1.5 5,200 <1.0 <1.5
MW-D-D 6/21/2022 5.5 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 0.98 J 4.12 170 <1.0 <0.30 800 <0.20 <0.30
MW-D-D 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA 230 <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 12/2/2015 <1.0 <0.0202 152 <10 <1.0 <1.0 <1.0 <1.0 NA 68.9 <5.0 <5.0 713 <1.0 <3.0
MW-D-B 7/20/2016 <1.0 <0.0209 87.3 <10 <1.0 <1.0 <1.0 <1.0 <5.0 43.5 <5.0 <5.0 159 <1.0 <3.0
MW-D-B 12/13/2016 <1.0 <0.020 34.9 <10 <1.0 <1.0 <1.0 <1.0 <5.0 32.0 <5.0 <5.0 <10 <1.0 <3.0
MW-D-B 7/5/2017 <0.30 <0.20 8.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 12/13/2017 <0.30 <0.20 4.3 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.5 <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 7/10/2018 <0.30 <0.0027 2.8 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 12/17/2018 <0.30 <0.0032 0.59 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.61 J <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 3.45 1.3 <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 12/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 4.75 2.4 <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 6/23/2020 0.33 J <0.0031 0.48 J <1.0 <0.30 <0.20 <0.20 <0.30 0.648 J 9.3 <1.0 1.4 <10 <0.20 <0.30
MW-D-B 12/15/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.3 <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 6/15/2021 <0.30 <0.0031 0.30 J <1.0 <0.30 <0.20 <0.20 <0.30 1.08 1.8 <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-D-B 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 10/27/2015 <1.0 <0.0204*12.3 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 192 <1.0 <3.0
MW-E-I 7/21/2016 <1.0 <0.0208 3.55 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 27.7 <1.0 <3.0
MW-E-I 12/12/2016 <1.0 < 0.0199 4.53 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-E-I 6/26/2017 <0.30 <0.20 1.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 12/11/2017 0.36 <0.20 1.6 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 7/10/2018 <0.30 <0.0026 4.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 12/18/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.875 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 12/11/2019 <0.30 <0.0031 2.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 6/22/2020 <0.30 <0.0032 2.1 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 12/17/2020 <0.30 <0.0031 1.4 1.7 <0.30 <0.20 <0.20 0.45 J <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 6/15/2021 <0.30 <0.0032 1.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-I 7/18/2023 <0.30 <0.0031 <0.21 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 < 1.0 2.4 <10 <0.20 <0.30
MW-E-D 10/27/2015 <1.0 <0.020*17.1 <10 <1.0 <1.0 <1.0 <1.0 NA 1.74 <5.0 <5.0 248 <1.0 <3.0
Page 5 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-E-D 7/21/2016 <1.0 <0.0204 25.9 <10 <1.0 <1.0 <1.0 <1.0 <5.0 1.57 <5.0 <5.0 287 <1.0 <3.0
MW-E-D 12/12/2016 <1.0 <0.0198 28.3 <10 <1.0 <1.0 <1.0 <1.0 <5.0 1.44 <5.0 <5.0 196 <1.0 <3.0
MW-E-D 6/26/2017 <0.30 <0.20 29.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.2 <1.0 <0.30 190 <0.20 <0.30
MW-E-D 12/11/2017 0.62 <0.20 17.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.99 <1.0 <0.30 <10 <0.20 <0.30
MW-E-D 7/10/2018 <0.30 <0.0027 26.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.2 <1.0 <0.30 130 <0.20 <0.30
MW-E-D 12/18/2018 <0.30 0.013 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.95 J <1.0 <0.30 <10 <0.20 <0.30
MW-E-D 6/10/2019 <0.30 <0.0031 21.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.72 <1.0 <0.30 <10 <0.20 <0.30
MW-E-D 12/11/2019 <0.30 0.0081 JP 21.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.67 J <1.0 <0.30 54.0 <0.20 <0.30
MW-E-D 6/22/2020 <0.30 <0.0031 14.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.63 J <1.0 <0.30 32.0 <0.20 <0.30
MW-E-D 12/17/2020 <0.30 <0.0031 18.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-D 6/15/2021 <0.30 <0.0032 15.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-D 6/21/2022 <0.30 <0.0031 9.3 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-D 7/18/2023 <0.30 <0.0031 12 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 < 1.0 <0.30 <10 <0.20 <0.30
MW-E-B 12/2/2015 <1.0 <0.0204 5.44 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 339 <1.0 <3.0
MW-E-B 7/21/2016 <1.0 <0.020 4.74 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 30.3 <1.0 <3.0
MW-E-B 12/12/2016 <1.0 < 0.0199 5.34 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 27.3 <1.0 <3.0
MW-E-B 6/26/2017 <0.30 <0.20 2.5 <1.0 <0.30 <0.20 0.35 <0.30 <0.0900 0.34 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 12/11/2017 <0.30 <0.20 1.6 <1.0 <0.30 <0.20 0.25 <0.30 <0.0900 0.2 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 7/10/2018 <0.30 <0.0026 1.1 <1.0 <0.30 <0.20 0.25 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 12/19/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 12/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 6/22/2020 <0.30 <0.0031 2.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.5 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 12/15/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 6/15/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-E-B 7/18/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 < 1.0 <0.30 <10 <0.20 <0.30
MW-F-I 10/27/2015 8.68 <0.020 <1.0 <10 1.48 2.26 <1.0 <1.0 NA <1.0 <5.0 <5.0 529 <1.0 <3.0
MW-F-I 7/20/2016 <1.0 <0.0197 <1.0 <10 <1.0 2.72 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 892 <1.0 <3.0
MW-F-I 12/12/2016 <1.0 <0.0198 <1.0 <10 <1.0 1.74 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 602 <1.0 <3.0
MW-F-I 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 0.93 <0.20 <0.30 69 <0.20 <1.0 <0.30 720 <0.20 <0.30
MW-F-I 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 3.94 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-F-I 7/10/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 0.6 <0.20 <0.30 2.92 <0.20 <1.0 0.65 610 <0.20 <0.30
MW-F-I 12/18/2018 <0.30 <0.0031 <0.20 <1.0 <0.30 0.38 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 330 <0.20 <0.30
MW-F-I 6/11/2019 9 <0.0031 <0.20 <1.0 <0.30 0.93 J <0.20 0.76 J 14.9 <0.20 <1.0 <0.30 250 <0.20 9.0
MW-F-I 12/10/2019 <0.30 <0.0031 <0.20 <1.0 1.8 1.2 <0.20 <0.30 0.698 J <0.20 <1.0 <0.30 160 <0.20 <0.30
MW-F-I 6/22/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 0.57 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 60.0 <0.20 <0.30
MW-F-I 12/15/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 0.95 J <0.20 0.31 J 1.2 <0.20 <1.0 <0.30 53.0 <0.20 <0.30
Page 6 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-F-I 6/15/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 0.27 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 60.0 <0.20 <0.30
MW-F-I 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.35 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-F-I 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 0.42 J <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-F-D 10/27/2015 <1.0 <0.0202 42.8 <10 <1.0 <1.0 <1.0 <1.0 NA 61.0 <5.0 <5.0 35,100 <1.0 <3.0
MW-F-D 7/20/2016 <200 <0.0206 <200 <2,000 <200 <200 <200 <200 <5.0 <200 <1,000 <1,000 28,900 <200 <600
MW-F-D 12/12/2016 <10 <0.020 54.4 <100 <10 <10 <10 <10 <5.0 63.9 <50 <50 15,400 <10 <30.0
MW-F-D 6/26/2017 <0.30 <0.20 29.0 <1.0 <0.30 <0.20 <0.20 <0.30 3.1 54.0 <1.0 <0.30 30,000 <0.20 <0.30
MW-F-D 12/13/2017 <0.30 <0.20 40.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 57.0 <1.0 <0.30 28,000 <0.20 <0.30
MW-F-D 7/10/2018 <0.30 <0.0027 26.0 <1.0 <0.30 <0.20 <0.20 <0.30 2.69 41.0 <1.0 <0.30 8,700 <0.20 <0.30
MW-F-D 12/18/2018 <0.30 <0.0032 16.0 <1.0 <0.30 1.0 <0.20 17.0 2.0 45.0 <1.0 <0.30 11,000 <0.20 1.8
MW-F-D 6/11/2019 88.0 <0.0031 4.4 9.6 2.6 14.0 <0.20 110 133 11.0 <1.0 30.0 3,500 1.2 38.0
MW-F-D 12/11/2019 <0.30 <0.0031 13.0 <1.0 <0.30 0.42 J <0.20 <0.30 1.17 30.0 <1.0 <0.30 9,800 <0.20 <0.30
MW-F-D 6/22/2020 0.53 J 0.013 JP 22.0 <1.0 <0.30 <0.20 <0.20 0.72 J 1.38 55.0 <1.0 <0.30 15,000 <0.20 <0.30
MW-F-D 12/15/2020 17 <0.0032 3.6 3.8 <0.30 3.6 <0.20 1.2 64.7 9.1 <1.0 9.0 36.0 0.33 J 7.9
MW-F-D 6/15/2021 11 <0.0031 3.1 4.1 <0.30 1.4 <0.20 2.2 34.7 12.0 <1.0 7.2 870.0 <0.20 4.0
MW-F-D 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-F-D 7/18/2023 <0.30 <0.0031 10 <1.0 <0.30 <0.20 <0.20 <0.30 NA 44 <1.0 <0.30 2,900 <0.20 <0.30
MW-F-B 12/2/2015 <1.0 <0.020 141 <10 <1.0 <1.0 <10 <1.0 NA 676 <50 <5.0 195,000 <1.0 <3.0
MW-F-B 7/21/2016 <5.0 <0.020 84.0 <50 <5.0 <5.0 <5.0 <5.0 3.41 J 519 <5.0 <5.0 52,300 <5.0 <75.0
MW-F-B 12/13/2016 <20 <200 86.9 <200 <20 <20 <20 <20 3.70 J 488 <100 <100 49,700 <20 <60.0
MW-F-B 6/27/2017 <0.30 <0.20 11.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 140 <1.0 <0.30 83.0 <0.20 <0.30
MW-F-B 12/14/2017 <0.30 <0.20 4.6 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 140 <1.0 <0.30 2,100 <0.20 <0.30
MW-F-B 7/10/2018 <0.30 <0.0026 1.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 84.0 <1.0 <0.30 89.0 <0.20 <0.30
MW-F-B 12/18/2018 <0.30 <0.0032 65.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.669 J 820.0 <5.0 <1.5 66,000 <1.0 <1.5
MW-F-B 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.0 <1.0 <0.30 <10 <0.20 <0.30
MW-F-B 12/11/2019 1.9 <0.0031 <0.20 <1.0 <0.30 0.22 J <0.20 <0.30 3.8 38.0 <1.0 <0.30 2,200 <0.20 0.96 J
MW-F-B 6/23/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.724 J <0.20 <1.0 2.0 <10 <0.20 <0.30
MW-F-B 12/15/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-F-B 6/15/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-F-B 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-F-B 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-G-I 11/2/2015 6.24 <0.0202* 11.9 11.0 <1.0 1.77 1.68 <1.0 NA 307 <5.0 <5.0 147,000 <1.0 <3.0
MW-G-I 7/21/2016 <20 <0.0197 <20 <200 <20 <20 <20 <20 1.68 J 342 <100 <100 36,700 <20 <60.0
MW-G-I 12/13/2016 <10 <0.0202 <10 <100 <10 <10 <10 <10 <5.0 216 <50 <50 19,800 <10 <30.0
MW-G-I 6/27/2017 <0.30 <0.20 2.1 <1.0 <0.30 <0.20 <0.20 <0.30 7.2 100 <1.0 <0.30 39,000 <0.20 <0.30
MW-G-I 12/12/2017 <0.30 <0.20 1.6 <1.0 <0.30 <0.20 <0.20 <0.30 0.809 120 <1.0 <0.30 2,000 <0.20 <0.30
MW-G-I 7/10/2018 1.7 <0.0026 2.7 <1.0 <0.30 <0.20 <0.20 <0.30 4.67 96.0 <1.0 <0.30 8,400 <0.20 0.6
Page 7 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-G-I 12/19/2018 <0.30 <0.0032 1.3 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 64.0 <1.0 <0.30 7,800 <0.20 0.6
MW-G-I 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.867 J 50.0 <1.0 <0.30 3,200 <0.20 <0.30
MW-G-I 12/11/2019 <0.30 <0.0031 1.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 44.0 <1.0 <0.30 2,000 <0.20 <0.30
MW-G-I 6/22/2020 <0.30 <0.0031 0.51 J <1.0 <0.30 0.26 J <0.20 <0.30 <0.0900 20.0 <1.0 <0.30 330 <0.20 <0.30
MW-G-I 12/17/2020 <0.30 <0.0032 0.43 J 6.4 <0.30 <0.20 <0.20 0.97 J <0.0900 16.0 <1.0 3.2 420 <0.20 <0.30
MW-G-I 6/15/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 0.20 J <0.20 <0.30 <0.0900 11.0 <1.0 <0.30 270 0.38 J <0.30
MW-G-I 6/22/2022 <0.30 0.043 <0.20 <1.0 <0.30 0.20 J <0.20 <0.30 <0.0900 6.8 <1.0 <0.30 <10 <0.20 <0.30
MW-G-I 7/17/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA 3.5 <1.0 <0.30 <10 <0.20 <0.30
MW-G-D 11/2/2015 <1.0 <0.0198*59.4 238 <1.0 1.27 <1.0 <1.0 NA 1,100 <5.0 <5.0 99,200 <1.0 <3.0
MW-G-D 7/21/2016 <5.0 <0.0197 39.3 <50 <5.0 <5.0 <5.0 <5.0 5.68 1,390 <5.0 <5.0 69,400 <5.0 <75.0
MW-G-D 12/13/2016 <50 <0.020 <50 <500 <50 <50 <50 <50 <5.0 1,100 <50 <50 57,300 <50 1<50
MW-G-D 6/28/2017 <1.5 <1.0 25.0 <5.0 <1.5 <1.0 <1.0 <1.5 225 710 <5.0 <1.5 59,000 <1.0 <1.5
MW-G-D 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.68 410 <1.0 <0.30 29,000 <0.20 <0.30
MW-G-D 7/10/2018 4.0 <0.0026 24.0 <5.0 <1.5 <1.0 <1.0 <1.5 118 960 <5.0 <1.5 50,000 <1.0 <1.5
MW-G-D 12/19/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 53.0 <1.0 <0.30 1,800 <0.20 <0.30
MW-G-D 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 6.8 350 <1.0 <0.30 25,000 <0.20 <0.30
MW-G-D 12/10/2019 0.91 J <0.0032 1.8 6.2 <0.30 <0.20 <0.20 <0.30 1.81 130 <1.0 <0.30 13,000 <0.20 <0.30
MW-G-D 6/22/2020 <0.30 <0.0030 7.0 <1.0 <0.30 <0.20 <0.20 <0.30 7.82 870 <1.0 <0.30 99,000 <0.20 <0.30
MW-G-D 12/15/2020 <0.30 <0.0031 1.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 94.0 <1.0 <0.30 13,000 <0.20 <0.30
MW-G-D 6/15/2021 <3.0 <0.0031 <2.0 <10 <3.0 <2.0 <2.0 <3.0 <0.0900 400 <10 <3.0 39,000 <2.0 <3.0
MW-G-D 6/22/2022 <0.30 <0.0031 1.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 200 <1.0 <0.30 <10 <0.20 <0.30
MW-G-D 2/27/2023 <0.30 <0.0031 4.8 <1.0 <0.30 <0.20 <0.20 <0.30 NA 450 <1.0 <0.30 27,000 <0.20 <0.30
MW-G-D 7/17/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA 480 <1.0 <0.30 23,000 <0.20 <0.30
MW-G-B 12/3/2015 <1.0 <0.0197 58.7 <10 <1.0 <1.0 <10 <1.0 NA 1,570 <50 <5.0 132,000 <1.0 <3.0
MW-G-B 7/21/2016 <20 < 0.0199 36.7 <200 <20 <20 <20 <20 5.08 1,440 <100 <100 55,300 <20 <60.0
MW-G-B 12/13/2016 <5.0 <0.020 <5.0 <50 <5.0 <5.0 <5.0 <5.0 3.83 J 1,100 <5.0 <5.0 42,900 <5.0 <75.0
MW-G-B 7/5/2017 <1.5 <1.0 5.5 <5.0 <1.5 0.93 <1.0 <1.5 3.31 820 <5.0 <1.5 87,000 <1.0 <1.5
MW-G-B 12/12/2017 <0.30 <0.20 1.4 <1.0 <0.30 <0.20 <0.20 <0.30 3.85 580 <1.0 <0.30 10,000 <0.20 <0.30
MW-G-B 7/11/2018 <0.30 <0.0026 11 <1.0 <0.30 <0.20 <0.20 <0.30 4.00 1,100 <1.0 <0.30 23,000 <0.20 <0.30
MW-G-B 12/19/2018 <0.30 0.049 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 18.0 <1.0 <0.30 <10 <0.20 <0.30
MW-G-B 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 2.1 <1.0 <0.30 <10 <0.20 <0.30
MW-G-B 12/11/2019 <0.30 <0.0031 0.57 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.75 J <1.0 <0.30 <10 <0.20 <0.30
MW-G-B 6/23/2020 <0.30 <0.0031 5.9 <1.0 <0.30 <0.20 <0.20 <0.30 2.02 720 <1.0 <0.30 12,000 <0.20 <0.30
MW-G-B 12/17/2020 <0.30 <0.0032 0.65 J 4.9 <0.30 <0.20 <0.20 <0.30 <0.0900 3.8 <1.0 2.8 <10 <0.20 <0.30
MW-G-B 6/15/2021 <0.30 <0.0031 0.35 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.55 J <1.0 <0.30 <10 <0.20 <0.30
MW-G-B 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-G-B 7/17/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 8 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-H-I 11/2/2015 136 <0.0199*1.57 46.7 4.09 <1.0 10.4 4.57 NA 19.0 <5.0 71.8 371 <1.0 13.7
MW-H-I 7/20/2016 <1.0 0.0<200 2.31 <10 <1.0 <1.0 <1.0 <1.0 <5.0 33.0 <5.0 <5.0 1,100 <1.0 <3.0
MW-H-I 12/13/2016 <1.0 <0.0199 2.23 <10* <1.0 <1.0 <1.0 <1.0 <5.0 30.4 <5.0 <5.0 803 <1.0 <3.0
MW-H-I 6/29/2017 <0.30 <0.20 1.1 <1.0 <0.30 <0.20 <0.20 <0.30 0.975 20.0 <1.0 <0.30 850 <0.20 <0.30
MW-H-I 12/13/2017 <0.30 <0.20 0.74 <1.0 <0.30 <0.20 <0.20 <0.30 1.27 15.0 <1.0 <0.30 390 <0.20 <0.30
MW-H-I 7/10/2018 <0.30 <0.0027 0.63 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 14.0 <1.0 <0.30 <10 <0.20 <0.30
MW-H-I 12/19/2018 <0.30 <0.0032 0.77 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 12.0 <1.0 <0.30 320 <0.20 <0.30
MW-H-I 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 2.07 5.9 <1.0 <0.30 120 <0.20 <0.30
MW-H-I 12/10/2019 <0.30 0.026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 2.6 <1.0 <0.30 <10 <0.20 <0.30
MW-H-I 6/22/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.57 J <1.0 <0.30 <10 <0.20 <0.30
MW-H-I 12/17/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.85 J <1.0 <0.30 <10 <0.20 <0.30
MW-H-I 6/16/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-H-I 6/21/2022 <0.30 0.11 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-H-I 7/17/2023 2.0 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 29 <0.20 <0.30
MW-H-D 11/2/2015 4.75 <0.020 83.4 <50 <1.0 8.72 1.79 <1.0 NA 453 <5.0 5.11 1,650 <1.0 <3.0
MW-H-D 7/20/2016 <1.0 <0.0197 57.1 <10 <1.0 1.96 <1.0 <1.0 <5.0 418 <5.0 <5.0 3,210 <1.0 <3.0
MW-H-D 12/13/2016 <1.0 <200 55.0 <10 <1.0 2.26 <1.0 <1.0 <5.0 348 <5.0 <5.0 1,680 <1.0 <3.0
MW-H-D 6/29/2017 <0.30 <0.20 22.0 <1.0 <0.30 <0.20 <0.20 <0.30 2.04 200 <1.0 <0.30 620 <0.20 <0.30
MW-H-D 12/13/2017 <0.30 <0.20 7.1 <1.0 <0.30 <0.20 <0.20 <0.30 2.57 120 <1.0 <0.30 1,400 <0.20 <0.30
MW-H-D 7/11/2018 <0.30 <0.0026 29.0 <1.0 <0.30 0.22 <0.20 <0.30 4.2 190 <1.0 <0.30 1,200 <0.20 <0.30
MW-H-D 12/19/2018 <0.30 <0.0031 12.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.180 110 <1.0 <0.30 1,100 <0.20 <0.30
MW-H-D 6/11/2019 <0.30 <0.0031 9.3 <1.0 <0.30 <0.20 <0.20 <0.30 1.37 100 <1.0 <0.30 750 <0.20 <0.30
MW-H-D 12/10/2019 <0.30 <0.0031 3.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 41.0 <1.0 <0.30 360 <0.20 <0.30
MW-H-D 6/22/2020 <0.30 <0.0030 2.3 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 21.0 <1.0 <0.30 140 <0.20 <0.30
MW-H-D 12/17/2020 <0.30 <0.0031 1.3 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 14.0 <1.0 <0.30 85.0 <0.20 <0.30
MW-H-D 6/16/2021 <0.30 <0.0032 1.00 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 14.0 <1.0 <0.30 39.0 <0.20 <0.30
MW-H-D 6/21/2022 <0.30 0.10 0.39 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 8.2 <1.0 <0.30 <10 <0.20 <0.30
MW-H-D 7/17/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 < 1.0 <0.30 <10 <0.20 <0.30
MW-H-B 12/3/2015 <1.0 <0.020 19.5 <10 <1.0 <1.0 <1.0 <1.0 NA 71.3 <5.0 <5.0 699 <1.0 <3.0
MW-H-B 7/21/2016 <1.0 <0.0196 35.1 <10 <1.0 <1.0 <1.0 <1.0 <5.0 96.1 <5.0 <5.0 353 <1.0 <3.0
MW-H-B 12/13/2016 <1.0 <0.0197 59.7 <10* <1.0 <1.0 <1.0 <1.0 <5.0 123.0 <5.0 <5.0 519 <1.0 <3.0
MW-H-B 6/29/2017 <0.30 <0.20 8.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 65.0 <1.0 <0.30 27.0 <0.20 <0.30
MW-H-B 12/13/2017 <0.30 <0.20 4.6 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 48.0 <1.0 <0.30 <10 <0.20 <0.30
MW-H-B 7/11/2018 <0.30 <0.0026 3.1 <1.0 <0.30 <0.20 <0.20 <0.30 6.84 31.0 <1.0 <0.30 <10 <0.20 <0.30
MW-H-B 12/19/2018 <0.30 0.022 19.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 74.0 <1.0 <0.30 <20 <0.20 <0.30
MW-H-B 6/11/2019 <0.30 <0.0031 9.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 38.0 <1.0 <0.30 37.0 <0.20 <0.30
MW-H-B 12/10/2019 <0.30 <0.0031 1.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.99 J <1.0 <0.30 <10 <0.20 <0.30
MW-H-B 6/22/2020 <0.30 <0.0030 0.83 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.55 J <1.0 <0.30 <10 <0.20 <0.30
Page 9 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-H-B 12/17/2020 <0.30 <0.0031 0.54 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.87 J <1.0 <0.30 <10 <0.20 <0.30
MW-H-B 6/16/2021 <0.30 <0.0032 1.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 4.9 <1.0 <0.30 <10 <0.20 <0.30
MW-H-B 6/21/2022 <0.30 <0.0031 1.8 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 2.6 <1.0 <0.30 <10 <0.20 <0.30
MW-H-B 7/17/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA 11 <1.0 <0.30 75 <0.20 <0.30
MW-I-I 11/2/2015 <1.0 <200* <1.0 <10 <1.0 <1.0 1.02 <1.0 NA <1.0 <5.0 <5.0 40.4 <1.0 <3.0
MW-I-I 7/20/2016 <1.0 <0.0204 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 29.2 <1.0 <3.0
MW-I-I 12/13/2016 <1.0 <0.0202 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-I-I 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-I 12/11/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-I 7/10/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-I 12/19/2018 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-I 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-I 12/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-I 6/15/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-I 12/15/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 17.0 <0.20 <0.30
MW-I-I 6/16/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-I 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-I 7/17/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 11/4/2015 <1.0 <0.020* <1.0 <10 <1.0 <1.0 1.43 <1.0 NA <1.0 <5.0 <5.0 205 <1.0 <3.0
MW-I-D 7/20/2016 <1.0 <0.0208 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 263 <1.0 <3.0
MW-I-D 12/13/2016 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 21.6 <1.0 <3.0
MW-I-D 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 12/11/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 7/10/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 12/19/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 12/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 6/15/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 12/15/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-D 7/17/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 12/3/2015 <1.0 <0.02 9.76 <10 <1.0 <1.0 <1.0 <1.0 NA 13.4 <5.0 <5.0 151 <1.0 <3.0
MW-I-B 7/20/2016 <1.0 <0.0198 6.78 <10 <1.0 <1.0 <1.0 <1.0 <5.0 15.1 <5.0 <5.0 437 <1.0 <3.0
MW-I-B 12/13/2016 <1.0 <0.0202 5.4 <10 <1.0 <1.0 <1.0 <1.0 <5.0 12.9 <5.0 <5.0 <10 <1.0 <3.0
MW-I-B 6/30/2017 <0.30 <0.20 2.6 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 11.0 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 12/11/2017 <0.30 <0.20 2.1 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 9.3 <1.0 <0.30 <10 <0.20 <0.30
Page 10 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
MW-I-B 7/10/2018 <0.30 <0.0026 1.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 8.4 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 12/19/2018 <0.30 0.042 1.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 7.3 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 6/11/2019 <0.30 <0.0031 0.74 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 12/10/2019 <0.30 0.0052 JP <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 6/15/2020 <0.30 0.013 JP <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 12/15/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 6/21/2022 <0.30 0.051 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-I-B 7/17/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X01 5/9/2006 670 <0.009 <50 <100 <50 180 NA 1,600 NA <50 NA 360 <1,000 <50 2,000
Z1-X01 4/10/2007 1,300 NA <50 <500 <50 230 J <50 1,000 NA <50 <500 690 <5,000 41.0 J 2,600
Z1-X01 5/8/2007 2,300 NA <5.0 320 4.0 J 46.0 <5.0 1,100 NA <5.0 <10 960 <100 6.9 2,400
Z1-X01 6/19/2007 2,600 <5.0 <5.0 1,300 11.0 62.0 <5.0 950 NA <5.0 <10 940 <100 12.0 1,900
Z1-X01 7/19/2007 2,200 <50 <50 820 <50 210 J <50 930 NA <50 <500 810 <5,000 110 J 1,800
Z1-X01 9/18/2007 2,300 <5.0 <5.0 740 21.0 4.6 J <5.0 550 NA <5.0 <10 1,200 <100 5.9 1,400
Z1-X01 5/24/2011 190 <1.0 <1.0 93.0 5.0 3.1 <1.0 64.0 NA <1.0 <2.0 76.0 20.0 0.75 J 95.0
Z1-X01 4/16/2013 55.0 <5.0 <5.0 81.0 14.0 <5.0 <5.0 26.0 NA <5.0 <10 47.0 <50 <5.0 23.0
Z1-X01 11/3/2015 70.0 <0.0199* <1.0 41.9 1.6 <1.0 <1.0 23.9 NA <1.0 <5.0 42.6 39.6 <1.0 12.8
Z1-X01 7/15/2016 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z1-X01 12/15/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 1.17 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z1-X01 6/29/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X01 12/11/2017 63.0 <0.20 <0.20 33.0 <0.30 <0.20 <0.20 18.0 3.31 <0.20 <1.0 14.0 <10 <0.20 7.9
Z1-X01 7/9/2018 12.0 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 1.4 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 1.0
Z1-X01 12/17/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X01 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X01 12/9/2019 1.8 0.0064 J <0.20 <1.0 1.0 J <0.20 <0.20 0.62 J <0.0900 <0.20 <1.0 <0.30 <10 0.33 J <0.30
Z1-X01 6/15/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X01 12/15/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X01 6/14/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X01 6/20/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X01 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 < 1.0 <0.30 <10 <0.20 <0.30
Z1-X25 5/16/2006 700 18.0 <5.0 66.0 <5.0 25,000 NA 800 NA <5.0 NA 330 540 1,500 3,300
Z1-X25 4/10/2007 2,300 NA <5.0 160 10.0 J 7,500 <5.0 2,600 NA <5.0 <50 630 <500 13,000 12,000
Z1-X25 5/8/2007 3,400 NA <5.0 420 18.0 J 8,100 <5.0 2,400 NA <5.0 <50 980 680 10,000 13,000
Z1-X25 6/19/2007 1,800 <5.0 110 650 10.0 J 6,500 <5.0 1,500 NA <5.0 <50 880 <500 7,300 8,200
Z1-X25 7/19/2007 900 <5.0 <5.0 770 5.5 J 4,300 <5.0 600 NA <5.0 <50 850 <500 2,200 2,900
Z1-X25 9/18/2007 760 <50 290 400 18 J 6,900 <50 310 NA <50 <100 640 <1,000 850 1,500
Z1-X25 5/24/2011 1.5 <1.0 1.9 <1.0 2.5 0.3 J <1.0 15 NA <1.0 <2.0 <1.0 88.0 0.81 J 1.7 J
Page 11 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z1-X25 4/16/2013 0.29 J <1.0 0.41 J <1.0 2.1 <1.0 <1.0 <1.0 NA <1.0 <2.0 <1.0 30.0 <1.0 <1.0
Z1-X25 11/3/2015 <1.0 <0.020* <1.0 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 91.6 <1.0* <3.0*
Z1-X25 7/15/2016 <1.0 0.511 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 12.1 <1.0 <3.0
Z1-X25 12/15/2016 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 14.3 <1.0 <3.0
Z1-X25 6/29/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X25 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X25 7/9/2018 1.4 0.014 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X25 12/17/2018 <0.30 0.053 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X25 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X25 12/9/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X27 5/17/2006 300 120 <5.0 55.0 <5.0 30,000 NA 230 NA <5.0 NA 200 3,800 4,300 2,100
Z1-X27 4/9/2007 1,900 NA <5.0 370 9.3 J 7,400 <5.0 3,200 NA <5.0 14.0 J 1,200 660 16,000 16,000
Z1-X27 5/8/2007 3,700 NA <5.0 360 25.0 J 6,700 <5.0 3,300 NA <5.0 <50 900 1,000 13,000 17,000
Z1-X27 6/18/2007 2,400 <5.0 <5.0 1,200 14 J 1,800 <5.0 1,600 NA <5.0 <50 1,900 <500 4,300 8,300
Z1-X27 7/19/2007 1,000 0.2 J <1.0 1,300 6.5 990 <1.0 320 NA <1.0 <2.0 1,500 160 1,400 1,800
Z1-X27 9/18/2007 570 <1.0 76 340 5.6 1,700 <1.0 470 NA <1.0 <2.0 79.0 340 1,500 2,100
Z1-X27 5/24/2011 12.0 <1.0 8.1 3.7 4.5 0.64 J <1.0 8.2 NA <1.0 <2.0 <1.0 140 <1.0 0.36 J
Z1-X27 4/16/2013 0.75 J <1.0 6.0 3.0 2.4 0.58 J <1.0 0.43 J NA <1.0 <2.0 1.8 80 <1.0 <1.0
Z1-X27 11/3/2015 <1.0 <200*3.96 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 20.3 <1.0 <3.0
Z1-X27 7/18/2016 <1.0 <0.020 2.16 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 32.2 <1.0 <3.0
Z1-X27 12/12/2016 <1.0 <0.0199 2.95 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 62.7 <1.0 <3.0
Z1-X27 6/27/2017 <0.30 <0.20 2.4 <1.0 <0.30 0.69 <0.20 <0.30 <0.50 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X27 12/13/2017 <0.30 <0.20 1.7 <1.0 <0.30 0.4 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X27 7/9/2018 0.78 <0.0027 1.6 7.2 0.44 0.61 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X27 12/18/2018 <0.30 <0.0031 0.84 J <1.0 <0.30 0.38 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X27 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.494 J <0.20 <1.0 <0.30 25.0 <0.20 <0.30
Z1-X27 12/9/2019 0.45 J <0.0031 0.84 J <1.0 <0.30 0.90 J <0.20 0.71 J <0.360 <0.20 <1.0 <0.30 29.0 <0.20 <0.30
Z1-X27 6/15/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X27 12/17/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 0.53 J <0.20 0.39 J <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X27 6/14/2021 0.51 J <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 20.0 <0.20 <0.30
Z1-X27 6/20/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 0.72 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z1-X27 7/18/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 0.82 J <0.20 <0.30 NA <0.20 < 1.0 <0.30 <10 <0.20 <0.30
Z1-X28 5/12/2006 1,400 3.6 <5.0 110 <5.0 11,000 NA 1,600 NA <5.0 NA 480 <500 670 6,700
Z1-X28 4/10/2007 2,300 NA <5.0 310 9.5 J 5,500 <5.0 2,800 NA <5.0 <50 940 <500 1,600 13,000
Z1-X28 5/7/2007 3,500 NA <5.0 450 14.0 J 5,400 <5.0 4,100 NA <5.0 <50 1,200 520 1,800 18,000
Z1-X28 6/26/2007 4,100 <5.0 <5.0 220 19.0 3,700 <5.0 3,600 NA <5.0 <10 1,300 <100 1,400 17,000
Z1-X28 7/19/2007 3,200 <5.0 <5.0 740 17.0 J 3,600 <5.0 3,000 NA <5.0 <50 1,300 <500 840 13,000
Z1-X28 9/18/2007 3,800 <5.0 <5.0 420 34.0 520 <5.0 2,500 NA <5.0 <10 1,100 <100 480.0 13,000
Page 12 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z1-X28 5/24/2011 1,400 <1.0 <1.0 350 47.0 38.0 <1.0 450.0 NA <1.0 <2.0 190 160 1.7 820
Z1-X28 4/16/2013 320 <5.0 28 130 15.0 10.0 <5.0 170.0 NA <5.0 <10 100 150 <5.0 300
Z1-X28 11/5/2015 100 <0.020 16.1 10.3 1.17 <1.0 <1.0 35.3 NA <1.0 <5.0 13.7 162 <1.0 71.4
Z1-X28 7/18/2016 59.3 <0.0198 8.15 15.6 2.06 <1.0 <1.0 72.1 <5.0 <1.0 <5.0 29.2 180 <1.0 86.6
Z1-X28 12/12/2016 58.9 <0.0198 11.8 <10 <1.0 <1.0 <1.0 76.5 <5.0 <1.0 <5.0 42.1 112 <1.0 131
Z1-X28 6/26/2017 120 <0.20 9.1 28.0 <0.30 0.99 <0.20 170.0 53.5 <0.20 <1.0 61.0 140 <0.20 210
Z1-X28 7/9/2018 130 <0.0026 2.7 52.0 5.2 <0.20 <0.20 21.0 <0.0900 <0.20 <1.0 40.0 60.0 <0.20 88.0
Z1-X28 12/19/2018 300 <0.0031 6.7 56.0 <1.5 3.9 J <1.0 <1.5 1.63 <1.0 <5.0 39.0 <50 <50 140
Z1-X28 6/10/2019 48.0 <0.0031 1.1 56.0 0.72 J <0.20 <0.20 <0.30 23.0 <0.20 <1.0 63.0 57.0 <0.20 26.0
Z1-X28 12/9/2019 320 <0.0031 1.5 65.0 <0.30 <0.20 <0.20 68.0 15.9 <0.20 <1.0 83.0 49.0 <0.20 62.0
Z1-X28 6/15/2020 250 0.0087 JP 2.5 28.0 <0.30 <0.20 <0.20 38.0 18.4 <0.20 <1.0 12.0 38.0 <0.20 120
Z1-X28 12/17/2020 26.0 <0.0031 2.0 36.0 <0.30 <0.20 <0.20 85.0 16.7 <0.20 <1.0 42.0 27.0 <0.20 40.0
Z1-X28 6/15/2021 10.0 <0.0031 <2.0 35.0 <3.0 <2.0 <2.0 <3.0 14.2 <2.0 <10.0 30.0 <100 <2.0 35.0
Z1-X28 6/20/2022 <3.0 <0.0032 <2.0 <10 <3.0 <2.0 <2.0 <3.0 4.36 <2.0 <10 <3.0 <100 <2.0 <3.0
Z1-X28 7/18/2023 6.3 <0.0031 1.9 6.6 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 5.5 <10 <0.20 3.9
Z2-PZ-06 11/3/2015 <1.0 <0.020<2.0* <1.0 <10 <1.0 <1.0 <1.0 1.82 NA <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z2-PZ-06 7/15/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z2-PZ-06 12/13/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z2-PZ-06 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 2.4 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-PZ-06 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-PZ-06 7/9/2018 1.4 <0.0027 <0.20 24.0 3.5 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 45.0 <10 <0.20 3.7
Z2-PZ-06 6/12/2019 59.0 <0.0031 <0.20 52.0 5.3 <0.20 <0.20 39.0 1.54 <0.20 <1.0 100 <10 <0.20 3.7
Z2-PZ-06 12/11/2019 3.6 <0.0031 <0.20 4.7 <0.30 2.6 <0.20 2.8 <0.0900 <0.20 <1.0 2.1 <10 <0.20 2.0
Z2-PZ-06 6/21/2020 1.4 0.0085 JP <0.20 6.9 <0.30 3.3 <0.20 3.1 <0.0900 <0.20 <1.0 2.9 <10 <0.20 2.9
Z2-PZ-06 12/17/2020 2.0 <0.0031 <0.20 4.7 <0.30 3.4 <0.20 8.5 1.17 <0.20 <1.0 6.6 <10 <0.20 7.7
Z2-PZ-06 6/16/2021 24.0 <0.0032 <1.0 31.0 2.0 J 6.3 <1.0 39.0 1.45 <1.0 <5.0 44.0 <50 2.1 J 10.0
Z2-PZ-06 6/20/2022 <0.30 0.0060 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-PZ-06 7/19/2023 5.3 <0.0031 <0.20 19 <0.30 11 <0.20 22 NA <0.20 <1.0 19 <10 0.62 J 6.7
Z2-PZ-08 11/3/2015 179 NA <1.0 83.9 1.41 2.64 <1.0 350 NA <1.0 <5.0 207 49.2 1.28 32.2
Z2-PZ-08 7/19/2016 435 <0.0199 <5.0 90.8 <5.0 <5.0 <5.0 911 <5.0 <5.0 <5.0 410 <50 <5.0 74.3
Z2-PZ-08 12/13/2016 36.8 <0.020 <1.0 70.4 1.16 3.56 <1.0 181 <5.0 <1.0 <5.0 155 <10 1.34 8.07
Z2-PZ-08 6/28/2017 25.0 <0.20 <0.20 130 2.3 2.0 <0.20 750 71.8 <0.20 <1.0 380 <10 1.5 62.0
Z2-PZ-08 12/14/2017 54.0 <0.20 <0.20 13.0 <0.30 2.0 0.89 44 49.8 <0.20 <1.0 40.0 27.0 1.5 8.2
Z2-PZ-08 7/9/2018 <0.30 0.11 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-PZ-08 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-PZ-08 12/11/2019 72.0 <0.0031 <0.20 22.0 <0.30 69.0 <0.20 <0.30 2.35 <0.20 <1.0 31.0 <10 <2.0 77.0
Z2-PZ-08 12/17/2020 3.3 <0.0031 <0.20 11.0 <0.30 8.2 <0.20 8.7 1.72 <0.20 <1.0 13.0 <10 <2.0 12.0
Z2-PZ-08 6/16/2021 15.0 <0.0032 <0.20 9.2 0.64 J 8.5 0.42 J 19.0 2.14 <0.20 <1.0 12.0 <10 <0.20 13.0
Page 13 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z2-PZ-08 6/21/2022 7.5 <0.0031 <0.20 10.0 <0.30 12.0 <0.20 9.6 5.06 <0.20 <1.0 13.0 <10 <0.20 7.0
Z2-PZ-08 7/19/2023 5.5 <0.0031 <0.20 87 <0.30 <0.20 <0.20 54 NA <0.20 <1.0 110 <10 <0.20 1.3 J
Z2-PZ-09 11/4/2015 59.8 <0.0198* <1.0 57.2 1.44 469 <1.0 348 NA <1.0 <5.0 110 148 23.2 254
Z2-PZ-09 7/18/2016 367 <0.020 <1.0 169 4.03 2,470 <1.0 1,020 <5.0 <1.0 <5.0 374 <10 45.0 838
Z2-PZ-09 12/13/2016 31.8 <0.0199 <1.0 55.6 5.33 13.2 <1.0 53.5 <5.0 <1.0 <5.0 41.2 <10 23.0 650
Z2-PZ-09 7/7/2017 33.0 <0.20 <0.20 130 3.7 1,300 <0.20 39.0 40.1 <0.20 <1.0 320 <10 22.0 46.0
Z2-PZ-09 12/15/2017 52.0 <1.0 <1.0 48.0 <1.5 600 <1.0 170 56.0 <1.0 <5.0 32.0 <50 9.9 96.0
Z2-PZ-09 12/19/2018 270 <1.0 <1.0 55.0 3.2 J 1,500 <1.0 610 6.79 <1.0 <5.0 260 <0.50 30.0 640
Z2-PZ-09 6/11/2019 380 <0.0031 <1.0 140 6.1 1,500 <1.0 330 21.4 <1.0 <5.0 430 <50 24.0 890
Z2-PZ-09 12/11/2019 140 <0.0031 <2.0 150 <3.0 790 <2.0 220 38.0 <2.0 <10 210 <100 16.0 330
Z2-PZ-09 6/21/2020 220 <0.0030 <1.0 140 5.9 1,100 2.5 J 2.0 J 6.89 <1.0 <5.0 380 <50 11.0 730
Z2-PZ-09 12/17/2020 85.0 <0.0032 <1.0 220 3.8 J 940 <1.0 140 27.0 <1.0 <5.0 450 <50 9.6 360
Z2-PZ-09 6/16/2021 290.0 <0.0031 <1.0 100 <1.5 870 <1.0 <1.5 35.7 <1.0 <5.0 240 <50 3.1 J 250
Z2-PZ-09 6/21/2022 0.78 J <0.0031 <0.20 <1.0 <0.30 12.0 <0.20 0.64 J 8.25 <0.20 <1.0 3.5 <10 <0.20 4.4
Z2-PZ-09 12/12/2022 190.0 <0.0031 <1.0 38 <1.5 460 <1.0 190 NA <1.0 <5.0 81.0 <50 2.5 J 260
Z2-PZ-09 7/19/2023 1.4 <0.0031 <0.20 7.4 <0.30 <0.20 <0.20 4.8 NA <0.20 <1.0 8.5 <10 <0.20 1.5 J
Z2-PZ-09 2/2/2024 <1.5 <1.0 <1.0 75 <1.5 490 <1.0 <1.5 NA <1.0 <5.0 130 <50 1.9 J 280
Z2-PZ-10 11/5/2015 3.94 <0.0198 <1.0 <10 <1.0 59.4 <1.0 6.01 NA <1.0 <5.0 <5.0 30.4 <1.0 3.35
Z2-PZ-10 7/18/2016 38.5 <0.0198 <1.0 64.0 5.53 11.9 <1.0 60.6 <5.0 <1.0 <5.0 52.1 <10 <1.0 7.2
Z2-PZ-10 12/28/2016 69.5 <0.020 <1.0 139 23.1 10.1 <1.0 68.7 <5.0 <1.0 <5.0 58.5 <10 <1.0 8.35
Z2-PZ-10 7/7/2017 3.4 <0.20 <0.30 77.0 6.0 14.0 <0.20 54.0 112 <0.20 <1.0 44.0 <10 <0.79 9.2
Z2-PZ-10 12/15/2017 13.0 <1.0 <1.0 67.0 <1.5 25.0 <1.0 52.0 135 <1.0 <5.0 32.0 <50 <1.0 2.8
Z2-PZ-10 7/9/2018 28.0 <0.0026 <0.20 130 12.0 9.7 <0.20 37.0 71.5 <0.20 <1.0 53.0 <10 0.52 5.7
Z2-PZ-10 12/19/2018 26.0 <0.0032 <0.20 <1.0 6.9 7.2 <0.20 35.0 12.6 <0.20 <1.0 42.0 <10 0.62 J 4.7
Z2-PZ-10 6/11/2019 0.90 J <0.0031 <0.20 19.0 5.9 5.4 <0.20 0.95 J 77.6 <0.20 <1.0 26.0 14.0 <0.20 3.1
Z2-PZ-10 12/11/2019 4.6 <0.0031 <0.20 6.0 0.40 J 3.9 <0.20 4.6 <0.0900 <0.20 <1.0 2.8 <10 <0.20 <0.20
Z2-PZ-10 6/21/2020 4.9 <0.0031 <0.20 41.0 5.1 3.8 <0.20 1.2 33.3 <0.20 <1.0 24.0 <10 <0.20 3.3
Z2-PZ-10 12/17/2020 4.0 <0.0032 <0.20 68.0 4.9 2.7 0.55 J 9.7 37.1 <0.20 <1.0 35.0 <10 <0.20 4.4
Z2-PZ-10 6/16/2021 1.8 <0.0032 <0.20 26.0 3.9 3.8 <0.20 1.6 37.0 <0.20 <1.0 20.0 <10 <0.20 8.8
Z2-PZ-10 6/21/2022 63.0 <0.0031 <0.20 100.0 5.7 580.0 <0.20 8.7 44.9 <0.20 <1.0 85.0 <1.0 2.1 35
Z2-PZ-10 7/19/2023 1.7 <0.0031 <0.20 6.8 <0.30 0.58 J <0.20 3.1 NA <0.20 <1.0 6.3 <10 <0.20 2.0 J
Z2-X03 6/30/2006 19.0 <0.009 <10 <20 <10 3,600 NA 71 NA <10 NA 28.0 <200 59.0 190
Z2-X03 2/20/2008 47.0 <10 77.0 130 5.7 J 2,700 <10 300 NA <10 <20 270 <200 97.0 280
Z2-X03 3/18/2008 2,300 <10 200 590 26.0 2,400 <10 910 NA <10 <20 700 1,200 580 4,000
Z2-X03 4/15/2008 1,600 <10 <10 490 13.0 1,300 <10 530 NA <10 <20 660 1,000 160 2,200
Z2-X03 5/20/2008 1,100 <10 82.0 480 10.0 390 <10 330 NA <10 3.2 J 740 1,500 91.0 1,600
Z2-X03 7/9/2008 92.0 <10 <10 280 3.2 J 13.0 <10 22 NA <10 <20 130 290 7.0 J 110
Page 14 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z2-X03 9/3/2008 480 <10 47.0 93.0 15.0 130 <10 130 NA <10 <20 83.0 1,100 29.0 510
Z2-X03 5/24/2011 0.81 J <1.0 <1.0 <1.0 <1.0 0.16 J <1.0 <1.0 NA <1.0 <2.0 <1.0 330 <1.0 <3.0
Z2-X03 4/16/2013 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <2.0 <1.0 14.0 <1.0 <1.0
Z2-X03 11/3/2015 <1.0 <0.0197* <1.0 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 12.7 <1.0 <3.0
Z2-X03 7/15/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 26.6 <1.0 <3.0
Z2-X03 12/15/2016 <1.0 <0.0194 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 57.5 <1.0 <3.0
Z2-X03 6/29/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.452 <0.20 <1.0 <0.30 21 <0.20 <0.30
Z2-X03 12/17/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X03 7/9/2018 <0.30 <0.017 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X03 12/17/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X03 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X03 12/9/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X16 6/29/2006 310 0.35 <10 <20 <10 17,000 NA 660 NA 79.0 NA 280 <200 2,000 4,000
Z2-X16 2/19/2008 99.0 <10 <10 61.0 4.2 J 14,000 <10 480 NA 41.0 <20 340 670 160 1,000
Z2-X16 3/18/2008 590 <50 290 90.0 J <50 12,000 <50 230 NA 240 <100 270 19,000 720 4,700
Z2-X16 4/15/2008 4,400 26 J <50 430 28.0 J 9,300 <50 3,600 NA 400 <100 1,100 17,000 14,000 16,000
Z2-X16 5/20/2008 2,900 <50 <50 330 18.0 J 9,300 30 J 4,900 NA 610 <100 700 29,000 28,000 22,000
Z2-X16 7/8/2008 5,100 <50 <50 1,000 21.0 J 3,300 <50 6,300 NA 37.0 J <100 3,400 4,000 12,000 34,000
Z2-X16 9/2/2008 890 <50 6.4 J 480 48.0 J 1,100 <50 250 NA 1,400 <100 770 110,000 330 1,400
Z2-X16 4/18/2013 12.0 <1.0 <1.0 7.7 2.3 0.23 J <1.0 4.2 NA 2.4 <2.0 1.5 3,000 <1.0 8.2
Z2-X16 11/3/2015 <1.0 <0.0199* <1.0 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 944 1.05 <3.0*
Z2-X16 7/13/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 1,940 <1.0 <3.0
Z2-X16 12/15/2016 <1.0 <0.019 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 1,190 <1.0 <3.0
Z2-X16 6/29/2017 1.4 <0.20 <0.20 6.4 0.65 <0.20 <0.20 <0.30 0.529 <0.20 <1.0 <0.30 2,000 <0.20 <0.30
Z2-X16 12/12/2017 1.7 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 900 <0.20 <0.30
Z2-X16 7/9/2018 4.6 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.296 <0.20 <1.0 <0.30 1,200 <0.20 <0.30
Z2-X16 12/17/2018 <0.30 0.011 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 23 0.58 <1.0 <0.30 940 <0.20 <0.30
Z2-X16 6/10/2019 0.63 J <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 1,200 <0.20 <0.30
Z2-X16 12/9/2019 0.71 J 0.0088 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 1,300 <0.20 <0.30
Z2-X16 6/15/2020 0.33 J <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 540 <0.20 <0.30
Z2-X16 12/15/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 250 <0.20 <0.30
Z2-X16 6/14/2021 <0.30 <0.0032 <0.20 3.4 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 220 <0.20 <0.30
Z2-X16 6/20/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X16 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 < 1.0 <0.30 <10 <0.20 <0.30
Z2-X18 6/27/2006 560 0.13 <10 130 <10 900 NA 2,300 NA <10 NA 580 <200 130 6,200
Z2-X18 2/20/2008 750 <10 <10 220 9.7 J 2,800 <10 1,100 NA <10 <20 610 <200 76.0 1,900
Z2-X18 3/18/2008 1,300 <5.0 23.0 210 9.5 800 <5.0 1,000 NA <5.0 9.5 J 550 820 56.0 3,400
Z2-X18 4/15/2008 1,800 <5.0 <5.0 290 7.7 250 <5.0 1,200 NA 5.4 <10 1,200 2,900 33.0 4,200
Page 15 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z2-X18 5/20/2008 830 <5.0 <5.0 350 3.6 J 6.4 <5.0 390 NA <5.0 <10 460 3,500 5.1 1,200
Z2-X18 7/9/2008 NA <5.0 <5.0 1,000 29.0 290 <5.0 2,700 NA <5.0 <10 1,700 1,100 240 9,200 H
Z2-X18 9/3/2008 3,900 <5.0 <5.0 470 53.0 160 <5.0 1,200 NA <5.0 <50 1,100 2,500 20.0 J 3,800
Z2-X18 5/24/2011 0.25 J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <2.0 <1.0 <10 <1.0 <3.0
Z2-X18 4/16/2013 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <2.0 <1.0 <10 <1.0 <1.0
Z2-X18 11/3/2015 <1.0 <0.020* <1.0 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 <10 <1.0* <3.0*
Z2-X18 7/14/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z2-X18 12/15/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z2-X18 6/29/2017 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X18 12/11/2017 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X18 7/10/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X18 12/17/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 18.7 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X18 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X18 12/9/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X20 6/29/2006 1,300 0.27 <10 220 13.0 26,000 NA 2,800 NA 14,000 NA 670 19,000 27,000 12,000
Z2-X20 2/20/2008 1,800 <10 <10 310 11.0 26,000 <10 2,900 NA 9,600 <20 900 20,000 30,000 14,000
Z2-X20 3/18/2008 3,400 <50 <50 900 120 20,000 <50 5,500 NA 8,000 <100 1,400 21,000 47,000 25,000
Z2-X20 4/15/2008 3,300 <50 930 530 21.0 J 10,000 <50 3,300 NA 700 <100 1,200 10,000 24,000 13,000
Z2-X20 5/20/2008 2,300 24.0 J 1,000 240 27.0 J 16,000 17.0 J 5,400 NA 2,500 <100 440 22,000 52,000 26,000
Z2-X20 7/8/2008 4,600 <50 <50 870 36.0 J 7,000 <50 2,100 NA 1,600 <100 2,300 12,000 8,400 12,000
Z2-X20 9/3/2008 1,400 <50 <50 590 14.0 J 4,600 <50 900 NA 1,100 19.0 J 1,000 14,000 4,300 4,300
Z2-X20 5/24/2011 1,100 <1.0 <1.0 180 22.0 160 <1.0 160 NA 200 <2.0 61.0 13,000 110 1,600
Z2-X20 4/17/2013 77.0 <5.0 <5.0 22.0 15.0 3.5 J <5.0 21.0 NA 13.0 <10 11.0 770 <5.0 13.0
Z2-X20 11/3/2015 6.46 <0.0199*1.68 <10 <1.0 <1.0 <1.0 <1.0 NA 7.46 <5.0 <5.0 1,340 <1.0* <3.0*
Z2-X20 7/18/2016 <1.0 <0.0198 2.13 <10 <1.0 <1.0 <1.0 <1.0 <5.0 3.72 <5.0 <5.0 917 <1.0 <3.0
Z2-X20 12/12/2016 <1.0 <0.0199 3.53 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 729 <1.0 <3.0
Z2-X20 6/29/2017 <0.30 <0.0026 4.3 <1.0 <0.30 0.56 <0.20 <0.30 <0.0900 9.6 <1.0 <0.30 1,300 <0.20 <0.30
Z2-X20 12/13/2017 <0.30 <0.0026 5.0 <1.0 <0.30 0.26 <0.20 <0.30 48.6 0.59 <1.0 <0.30 960 0.32 <0.30
Z2-X20 7/10/2018 <0.30 <0.0025 3.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.38 <1.0 <0.30 490 <0.20 <0.30
Z2-X20 12/18/2018 <0.30 <0.0032 2.1 <1.0 <0.30 0.30 J <0.20 <0.30 0.521 J 3.3 <1.0 <0.30 1400 <0.20 <0.30
Z2-X20 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.574 J <0.20 <1.0 <0.30 410 <0.20 <0.30
Z2-X20 12/10/2019 <0.30 <0.0031 2.7 <1.0 <0.30 0.22 J <0.20 <0.30 <0.0900 0.94 J <1.0 <0.30 760 <0.20 <0.30
Z2-X20 6/22/2020 <0.30 0.0085 JP 2.0 <1.0 <0.30 0.30 J <0.20 <0.30 <0.0900 0.67 J <1.0 <0.30 420 <0.20 <0.30
Z2-X20 12/17/2020 <0.30 <0.0031 2.0 5.3 <0.30 <0.20 <0.20 <0.30 <0.0900 3.8 <1.0 2.9 410 <0.20 <0.30
Z2-X20 6/15/2021 <0.30 <0.0031 1.1 2.4 <0.30 0.53 J 0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 610 <0.20 <0.30
Z2-X20 6/20/2022 <0.30 <0.0031 1.1 <1.0 <0.30 0.42 J <0.20 <0.30 <0.0900 1.6 <1.0 <0.30 240 <0.20 <0.30
Z2-X20 7/19/2023 <0.30 <0.0032 1.2 <1.0 <0.30 0.57 J <0.20 <0.30 NA <0.20 < 1.0 <0.30 630 <0.20 <0.30
Z2-X29 6/28/2006 1,500 0.07 85.0 100 <10 2,400 NA 3,000 NA <10 NA 590 <200 230 9,400
Page 16 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z2-X29 2/20/2008 550 <10 <10 260 8.3 J 1,500 <10 1,200 NA <10 <20 890 <200 150 1,900
Z2-X29 3/18/2008 400 <5.0 <5.0 130 3.3 J 1,800 <5.0 940 NA <5.0 <10 380 830 61 3,000
Z2-X29 4/15/2008 1,200 <5.0 32.0 190 7.4 1,400 2.2 J 830 NA <5.0 3.0 J 460 1,100 76.0 3,900
Z2-X29 5/20/2008 1,800 <5.0 20.0 470 18.0 880 <5.0 1,000 NA <5.0 <10 760 1,100 53.0 3,600
Z2-X29 7/9/2008 2,700 <5.0 4.0 J 620 13.0 940 <5.0 970 NA <5.0 <10 780 530 49.0 4,200
Z2-X29 9/3/2008 2,400 <5.0 <5.0 260 21.0 1,000 <5.0 890 NA <5.0 <10 640 830 35.0 3,400
Z2-X29 5/24/2011 2.3 <1.0 <1.0 4.7 0.49 J 0.24 J <1.0 <1.0 NA <1.0 <2.0 <1.0 11.0 <1.0 0.38 J
Z2-X29 4/16/2013 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <2.0 <1.0 <10 <1.0 <1.0
Z2-X29 11/3/2015 <1.0 <0.0198* <1.0 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 <10 <1.0* <3.0*
Z2-X29 7/14/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z2-X29 12/13/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 47.9 <1.0 <3.0
Z2-X29 6/27/2017 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X29 12/12/2017 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X29 7/10/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X29 12/17/2018 <0.30 <0.00320 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 14 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X29 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X29 12/10/2019 <0.30 0.0064 JP <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X29 6/15/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X29 12/15/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X29 6/15/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X29 6/21/2022 7.0 <0.0031 <0.20 <1.0 <0.30 0.58 J <0.20 1.5 1.66 <0.20 <1.0 4.1 <10 <0.20 4.5
Z2-X29 7/17/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X31 6/28/2006 120 <0.009 <10 <20 <10 21,000 NA 210 NA 100 NA 270 4,900 91.0 840
Z2-X31 2/19/2008 44.0 <10 <10 230 2.6 J 17,000 <10 150 NA 43.0 <20 610 6,700 48.0 220
Z2-X31 3/18/2008 1,700 <50 <50 150 15.0 J 12,000 <50 2,600 NA <50 <100 560 2,100 7,600 12,000
Z2-X31 4/15/2008 1,400 <50 250 280 33.0 J 4,800 <50 700 NA 120 <100 570 5,000 540 3,400
Z2-X31 5/20/2008 840 <5.0 <5.0 230 6.8 4,100 <5.0 950 NA <5.0 <10 470 560 47.0 3,600
Z2-X31 7/8/2008 3,600 <5.0 <5.0 310 27.0 2,200 <5.0 1,900 NA 53.0 <10 1,300 2,800 2,400 9,500
Z2-X31 9/3/2008 5,000 <50 <50 220 110 2,100 <50 4,600 NA 120 13.0 J 540 <1,000 6,200 24,000
Z2-X31 5/24/2011 490 <1.0 <1.0 210 9.1 34.0 <1.0 120 NA <1.0 <2.0 250 910 160 1,300
Z2-X31 4/17/2013 750 <5.0 <5.0 53.0 5.5 1.8 J <5.0 180 NA <5.0 <10 21.0 500 6.0 460
Z2-X31 11/4/2015 28.9 <0.0204 <1.0 15.7 <1.0 <1.0 <1.0 1.81 NA 3.92 <5.0 <5.0 1,030 3.32 18.6
Z2-X31 7/13/2016 394 <0.0198 <1.0 16.6 2.26 <1.0 <1.0 86.8 <5.0 2.53 <5.0 <5.0 586 57.9 516
Z2-X31 12/14/2016 57.8 <0.0199 <1.0 10.6 1.01 <1.0 <1.0 16.4 <5.0 3.65 <5.0 5.27 744 9.83 58.0
Z2-X31 6/27/2017 1.2 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 10.2 1.6 <1.0 <0.30 330 <0.20 16.0
Z2-X31 12/13/2017 290 <0.20 <0.20 27.0 <0.30 0.51 <0.20 28.0 14.9 3.0 <1.0 6.5 410 0.94 170
Z2-X31 7/10/2018 500 <0.0027 <0.20 13.0 2.7 0.43 <0.20 17.0 3.51 1.2 <1.0 3.8 160 1.8 400
Z2-X31 12/17/2018 450 <0.0031 <1.0 <5.0 <1.5 <1.0 <1.0 89.0 4.41 <1.0 <5.0 <1.5 <50 1.8 110
Z2-X31 6/11/2019 <0.30 <0.0031 <0.20 <1.0 1.9 <0.20 <0.20 4.1 4.45 <0.20 <1.0 <0.30 96.0 0.59 J 85.0
Page 17 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z2-X31 12/10/2019 16.0 <0.0031 <0.20 6.1 <0.30 0.44 J <0.20 2.3 3.18 0.46 J <1.0 <0.30 81.0 <0.20 18.0
Z2-X31 6/15/2020 43.0 0.0059 JP <0.20 <1.0 <0.30 0.25 J <0.20 55.0 1.32 <0.20 <1.0 1.2 44.0 1.1 75.0
Z2-X31 12/15/2020 2.8 <0.0031 <0.20 3.1 <0.30 <0.20 <0.20 3.1 1.10 <0.20 <1.0 1.4 88.0 <0.20 13.0
Z2-X31 6/14/2021 <1.5 <0.0031 <1.0 <5.0 <1.5 <1.0 <1.0 3.5 J 2.26 <1.0 <5.0 <1.5 99.0 <1.0 88.0
Z2-X31 6/22/2022 5.4 <0.0031 <0.20 <1.0 0.87 J 0.45 J <0.20 2.7 4.50 <0.20 <1.0 <0.30 <10 0.34 J 3.9
Z2-X31 7/18/2023 12.0 <0.0032 <0.20 <1.0 <0.30 0.41 J <0.20 5.8 NA <0.20 <1.0 2.6 110 <0.20 5.2
Z2-X35 6/27/2006 46.0 0.025 <10 <20 <10 10,000 NA 57.0 NA <10 NA 82.0 990 1,800 930
Z2-X35 2/20/2008 12.0 <10 <10 24.0 <10 8,700 <10 44.0 NA <10 <20 65.0 1,100 37.0 93.0
Z2-X35 3/18/2008 2,300 <100 <100 270 <100 9,300 <100 3,000 NA 120 <200 590 <2,000 13,000 14,000
Z2-X35 4/15/2008 2,000 <10 34.0 320 16.0 6,100 <10 1,900 NA 120 <20 700 1,800 7,300 9,800
Z2-X35 5/20/2008 1,300 <10 <10 950 42.0 5,700 <10 1,500 NA 290 <20 720 4,000 3,700 6,000
Z2-X35 7/9/2008 3,000 <10 <10 820 24.0 3,900 <10 1,800 NA 45.0 <20 1,500 780 4,900 8,600
Z2-X35 9/3/2008 870 <10 28.0 160 19.0 2,300 <10 420 NA 120 3.2 J 650 1,200 1,400 2,100
Z2-X35 4/17/2013 0.27 J <1.0 <1.0 <1.0 2.1 <1.0 <1.0 <1.0 NA <1.0 <2.0 <1.0 <10 <1.0 <1.0
Z2-X35 11/4/2015 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 <10 <1.0* <3.0*
Z2-X35 7/14/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z2-X35 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X35 7/10/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X35 12/17/2018 <0.30 0.012 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 6.58 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X35 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 68.0 <0.20 <0.30
Z2-X35 12/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 12.0 <0.20 <0.30
Z2-X35 6/22/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X35 12/15/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X35 6/14/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 29.0 <0.20 <0.30
Z2-X35 6/20/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z2-X35 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z3-X80 12/30/2009 1,000 0.082 610 530 <50 11,000 <50 770 NA 34.0 J <100 950 65,000 960 3,800
Z3-X80 3/31/2010 1,100 <50 <50 550 <50 10,000 <50 630 NA 50.0 <100 910 96,000 380 3,000
Z3-X80 5/26/2011 170 <1.0 <1.0 180 3.8 83.0 <1.0 3.3 NA 0.77 J <2.0 120 8,500 12.0 330
Z3-X80 4/18/2013 47.0 <1.0 <1.0 <1.0 3.3 1.1 <1.0 10 NA <1.0 <2.0 <1.0 330 0.32 J 30.0
Z3-X80 11/5/2015 3.99 <200 <1.0 22.1 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 1,320 <1.0 <3.0
Z3-X80 7/19/2016 1.01 <0.0208 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 500 <1.0 <3.0
Z3-X80 12/16/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 1,380 <1.0 <3.0
Z3-X80 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 1.0 <0.20 <0.30 142 <0.20 <1.0 <0.30 2,800 <0.20 <0.30
Z3-X80 12/13/2017 0.59 <0.20 <0.20 1.1 <0.30 0.26 <0.20 <0.30 99.5 1.0 <1.0 <0.30 9,500 <0.20 <0.30
Z3-X80 7/10/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 0.55 <0.20 <0.30 7.9 <0.20 <1.0 <0.30 780 <0.49 <0.30
Z3-X80 12/18/2018 <0.30 <0.0031 <0.20 <1.0 <0.30 0.26 J <0.20 <0.30 1.84 <0.20 <1.0 <0.30 650 <0.20 <0.30
Z3-X80 6/11/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.886 J <0.20 <1.0 <0.30 68.0 <0.20 <0.30
Page 18 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z3-X80 12/10/2019 0.31 J <0.0031 <0.20 <1.0 <0.30 0.30 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 140 <0.20 <0.30
Z3-X80 6/22/2020 0.30 J <0.0030 <0.20 <1.0 <0.30 0.25 J <0.20 0.50 J <0.0900 <0.20 <1.0 1.4 <10 <0.20 <0.30
Z3-X80 12/17/2020 <0.30 <0.0031 <0.20 5.6 <0.30 <0.20 <0.20 0.51 J <0.0900 <0.20 <1.0 2.9 45.0 <0.20 <0.30
Z3-X80 6/16/2021 0.31 J <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 0.70 J <0.0900 <0.20 <1.0 <0.30 83.0 <0.20 <0.30
Z3-X80 6/21/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 0.43 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z3-X80 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 89 <0.20 <0.30
Z3-X82 12/29/2009 2,100 0.65 1,100 460 17.0 J 16,000 <50 1,400 NA 210 <100 910 7,900 1,400 5,100
Z3-X82 4/1/2010 280 <50 <50 210 17.0 J 19,000 <50 230 NA 230 <100 750 16,000 350 970
Z3-X82 11/5/2015 6.95 <200 <1.0 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 753 3.6 <3.0
Z3-X82 7/13/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 560 <1.0 <3.0
Z3-X82 12/14/2016 <1.0 <200 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 752 <1.0 <3.0
Z3-X82 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 0.74 <0.20 <0.30 23.1 <0.20 <1.0 <0.30 560 <0.20 <0.30
Z3-X82 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 0.78 <0.20 0.31 17.5 <0.20 <1.0 <0.30 830 0.51 <0.30
Z3-X82 7/10/2018 0.58 <0.0027 <0.20 <1.0 <0.30 0.68 <0.20 <0.30 4.26 <0.20 <1.0 <0.30 440 0.51 <0.30
Z3-X82 12/17/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 46.3 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z3-X82 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.94 <0.20 <1.0 <0.30 170 <0.20 <0.30
Z3-X82 12/9/2019 0.36 J 0.0071 J <0.20 <1.0 <0.30 0.56 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 280 0.37 J <0.30
Z3-X82 6/15/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 0.28 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 23.0 <0.20 <0.30
Z3-X82 12/15/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 34.0 <0.20 <0.30
Z3-X82 6/15/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 130 <0.20 <0.30
Z3-X82 6/22/2022 0.41 J <0.0032 <0.20 <1.0 <0.30 0.53 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z3-X82 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 0.61 J <0.20 <0.30 NA <0.20 <1.0 <0.30 74 <0.20 <0.30
Z4-PZ04 10/26/2011 790 <5.0 <5.0 83.0 7.7 1,300 <5.0 760 NA <5.0 <10 150 38.0 J 120 2,300
Z4-PZ04 3/7/2012 17.0 <5.0 <5.0 20.0 <5.0 1,900 <5.0 23.0 NA <5.0 2.2 J 28.0 380 28.0 36.0
Z4-PZ04 8/27/2012 150 <5.0 <5.0 79.0 3.9 J 2,000 <5.0 220 NA <5.0 <10 120 99.0 23.0 170
Z4-PZ04 4/18/2013 68.0 <5.0 <5.0 53.0 <5.0 11.0 <5.0 110 NA <5.0 16.0 130 <50 <5.0 19.0
Z4-PZ04 11/4/2015 65.6 <0.0199* <1.0 69.6 6.42 13.1 <1.0 88.4 NA <1.0 <5.0 84.9 27.4 <1.0 17.1
Z4-PZ04 7/19/2016 47.6 <0.0198 <1.0 <10 <1.0 564 <1.0 142 1.40 J <1.0 <5.0 30.5 103 3.49 44.0
Z4-PZ04 12/13/2016 10.4 <0.0202 <5.0 <50* <5.0 434 <5.0 60.9 1.87 J <5.0 <5.0 <5.0 399 5.37 18.8
Z4-PZ04 7/7/2017 2.5 <0.20 <0.20 <1.0 <0.30 19 <0.20 2.1 29.4 <0.20 <1.0 <0.30 <10 <0.53 5.0
Z4-PZ04 12/15/2017 1.4 <0.20 <0.20 8.1 0.69 120 <0.20 10.0 455 <0.20 <1.0 2.7 3110 1.9 3.1
Z4-PZ04 7/9/2018 <0.30 <0.0027 <0.20 <1.0 4.3 480 <0.20 <0.30 329 <0.20 <1.0 <0.30 270 3.5 7.9
Z4-PZ04 12/19/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 0.32 J <0.20 <0.30 0.418 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-PZ04 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 170 <0.30 2.8 127 <0.20 <1.0 <0.30 73.0 0.50 J 1.5
Z4-PZ04 12/11/2019 8.0 <0.0031 <1.0 56.0 7.8 3.6 J <1.0 <1.5 44.8 <1.0 <5.0 24.0 <50 <1.0 2.2 J
Z4-PZ04 6/21/2020 0.37 J <0.0031 <0.20 <1.0 0.41 J 46.0 <0.20 2.8 38.2 <0.20 <1.0 1.5 11.0 0.65 J 12.0
Z4-PZ04 12/17/2020 13.0 <0.0032 <0.20 6.2 <0.30 15.0 <0.20 19.0 50.8 <0.20 <1.0 6.7 <10 <0.20 16.0
Z4-PZ04 6/16/2021 <3.0 <0.0032 <2.0 <2.0 <10 250 <2.0 <3.0 101 <2.0 <10 <3.0 120 4.8 J 14.0
Page 19 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z4-PZ04 6/21/2022 <3.0 <0.0031 <2.0 <10 4.6 J 5.5 J <2.0 13.0 60.2 <2.0 <10 <3.0 <100 <2.0 <3.0
Z4-PZ04 7/19/2023 2.8 <0.0031 <0.20 68 5.4 3.2 <0.20 9.2 NA <0.20 <1.0 32 <10 0.39 J 6.5
Z4-PZ07 10/27/2011 0.59 J <1.0 <1.0 2.2 <1.0 3.6 <1.0 1.2 NA <1.0 <2.0 3.7 29.0 0.59 J 1.3 J
Z4-PZ07 3/7/2012 6.2 <1.0 2.4 11.0 0.24 J 260 <1.0 18.0 NA <1.0 <2.0 16.0 96.0 130 61.0
Z4-PZ07 8/27/2012 0.79 J <1.0 <1.0 26.0 <1.0 14.0 <1.0 6.9 NA <1.0 <2.0 8.9 110 0.62 J 2.7 J
Z4-PZ07 4/16/2013 84 <5.0 70.0 14.0 <5.0 2,300 <5.0 260 NA <5.0 13.0 97.0 310 44.0 220
Z4-PZ07 11/4/2015 1.17 NA <1.0 <10 <1.0 3.86 <1.0 3.83 NA <1.0 <5.0 <5.0 52.2 <1.0 <3.0
Z4-PZ07 7/14/2016 <1.0 <0.020 <1.0 <10 <1.0 1.89 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z4-PZ07 12/13/2016 <1.0 <0.020 <1.0 <10* <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 69.6 <1.0 <3.0
Z4-PZ07 7/7/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-PZ07 12/15/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 72.0 <0.20 <0.30
Z4-PZ07 7/9/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 26.0 <0.20 <0.30
Z4-PZ07 12/19/2018 <0.30 <0.0031 <0.20 <1.0 <0.30 0.50 J <0.20 <0.30 1.62 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-PZ07 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 5.4 <0.20 1.5 28.9 <0.20 <1.0 <0.30 26.0 <0.20 <0.30
Z4-PZ07 12/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 7.3 <0.20 1.6 44.8 <0.20 <1.0 <0.30 63.0 0.33 J <0.30
Z4-PZ07 6/21/2020 1.3 <0.0031 <0.20 <1.0 <0.30 12.0 <0.20 6.0 47.1 <0.20 <1.0 2.9 21.0 0.40 J 1.8
Z4-PZ07 12/17/2020 1.3 <0.0031 <0.20 7.9 <0.30 7.0 <0.20 2.5 29.6 <0.20 <1.0 10.0 <10 0.41 J 1.8
Z4-PZ07 6/16/2021 7.9 <0.0032 <0.20 3.3 <0.30 8.6 <0.20 8.4 99.5 <0.20 <1.0 3.9 <10 <0.20 8.4
Z4-PZ07 6/21/2022 4.9 <0.0031 <0.20 <1.0 0.36 J 14.0 <0.20 35.0 117 <0.20 <1.0 12.0 45 0.98 J 9.9
Z4-PZ07 7/19/2023 5.8 <0.0031 <0.20 9.8 <0.30 18 <0.20 47 NA <0.20 <1.0 27 <10 1.1 8.5
Z4-PZ09 4/18/2013 80.0 <5.0 <5.0 28.0 <5.0 570 <5.0 80 NA <5.0 7.7 J 120 <50 140 240
Z4-PZ09 11/4/2015 13.5 <0.020 <1.0 <50 1.94 325 <1.0 72.9 NA <1.0 <5.0 103 59.8 18.1 35.3
Z4-PZ09 7/18/2016 64.0 <0.020 <1.0 <10 <1.0 422 <1.0 116 8.36 <1.0 <5.0 66.4 <10 36.4 213
Z4-PZ09 12/13/2016 13.0 <0.020 <5.0 109 <5.0 411 <5.0 24.1 12.9 <5.0 <5.0 173 15.7 49.9
Z4-PZ09 6/28/2017 15.0 <0.20 <0.20 82.0 7.0 280 <0.20 110 176 <0.20 <1.0 140 50.0 22.0 46.0
Z4-PZ09 7/9/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 1.5 <0.20 <0.30 <0.50 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-PZ09 12/18/2018 80.0 <0.0032 <0.20 64 <0.30 270 <0.20 210 90.2 <0.20 <1.0 14.0 <10 29.0 160
Z4-PZ09 6/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 678 <0.20 <1.0 <0.30 17.0 <0.20 <0.30
Z4-PZ09 12/10/2019 60.0 0.0052 J <1.0 24.0 <1.5 150 2.4 J 110 37.8 <1.0 7.2 J 67.0 <50 12.0 140
Z4-PZ09 6/21/2020 75.0 <0.0031 <0.20 37.0 2.1 65.0 2.2 8.2 188 <0.20 <1.0 110 <10 5.3 140
Z4-PZ09 12/17/2020 58.0 <0.0031 <0.20 16.0 1.1 53.0 <0.20 75.0 151 <0.20 <1.0 61.0 <10 3.4 82.0
Z4-PZ09 6/16/2021 61.0 <0.0032 <1.0 <5.0 2.5 J 27.0 <1.0 80.0 587 <1.0 <5.0 <1.5 <50 4.0 J 130
Z4-PZ09 6/21/2022 70.0 <0.0031 <1.0 <5.0 2.9 J 160.0 <1.0 40.0 515 <1.0 <5.0 110.0 <50 13.0 170
Z4-PZ09 7/19/2023 25.0 <0.0031 <0.20 51 <0.30 180 <0.20 290 NA <0.20 <1.0 96 <10 13 110
Z4-X21 10/5/2010 0.91 J <1.0 <1.0 96.0 2.6 96.0 <1.0 150 NA <1.0 <2.0 190 74.0 100 240
Z4-X21 3/23/2011 340 <5.0 <5.0 480 24.0 1,200 0.75 J 790 NA <5.0 39.0 890 350 350 3,500
Z4-X21 5/11/2011 510 <10 <10 460 14.0 1,400 5.0 J 110 NA <10 <20 580 840 220 1,600
Page 20 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z4-X21 7/26/2011 970 <5.0 <5.0 350 14.0 1,800 <5.0 1,300 NA <5.0 <10 1,100 350 920 3,000
Z4-X21 9/19/2011 440 <5.0 <5.0 290 15.0 320 <5.0 670 NA <5.0 <10 300 300 320 1,700
Z4-X21 10/26/2011 860 <1.0 <1.0 670 25.0 260 <5.0 790 NA <5.0 <10 1,100 150 670 1,700
Z4-X21 1/18/2012 1,400 <1.0 <1.0 710 47.0 130 0.41 J 150 NA <1.0 <2.0 280 620 36.0 660
Z4-X21 3/7/2012 1,700 <5.0 4.7 J 220 40.0 23.0 <5.0 110 NA 4.8 J <10 130 570 9.6 680
Z4-X21 4/17/2013 390 <5.0 <5.0 35.0 5.6 8.4 <5.0 76 NA <5.0 <10 44.0 440 14.0 340
Z4-X21 11/4/2015 253 <0.020 <1.0 <10 7.84 4.27 <1.0 33.7 NA <1.0 <5.0 <5.0 489 6.54 35.6
Z4-X21 7/13/2016 1.46 <0.0198 <1.0 <10 1.09 <1.0 <1.0 1.79 <5.0 <1.0 <5.0 <5.0 61.6 <1.0 3.17
Z4-X21 12/14/2016 4.04 <0.0199 <1.0 <10 1.62 1.73 <1.0 1.57 <5.0 <1.0 <5.0 <5.0 268 <1.0 <3.0
Z4-X21 6/27/2017 19.0 <0.20 <0.20 9.4 <0.30 1.0 <0.20 11.0 57.3 <0.20 <1.0 <0.30 89.0 <0.20 18.0
Z4-X21 12/11/2017 890 <0.20 <0.20 55.0 12.0 5.0 <0.20 92 282 <0.20 <1.0 17.0 530 <0.31 170
Z4-X21 7/10/2018 20.0 <0.0026 <0.20 8.7 1.4 1.5 <0.20 11.0 <69.3 <0.20 <1.0 2.7 130 <0.20 3.2
Z4-X21 12/18/2018 110 <0.0032 <0.20 6.6 <0.30 0.95 J <0.20 1.2 2.81 <0.20 <1.0 3.0 <10 <0.20 8.0
Z4-X21 6/11/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 4.25 <0.20 <1.0 <0.30 15.0 <0.20 <0.30
Z4-X21 12/9/2019 12 <0.0031 <0.20 8.0 <0.30 <0.20 <0.20 8.7 <0.0900 <0.20 <1.0 2.4 50.0 <0.20 1.8
Z4-X21 6/15/2020 0.96 J <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 3.74 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X21 12/15/2020 0.71 J <0.0032 <0.20 3.9 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 1.6 11.0 <0.20 <0.30
Z4-X21 6/15/2021 2.6 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 2.32 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X21 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 0.30 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X21 7/18/2023 5.9 <0.0031 < 0.20 <1.0 <0.30 <0.30 <0.30 <0.30 NA < 0.20 < 1.0 <0.30 <10 <0.20 <0.30
Z4-X30 9/30/2010 1,100 <10 <10 270 <10 78.0 <10 1,400 NA <10 <20 520 <200 18.0 96.0
Z4-X30 3/23/2011 1.5 <1.0 <1.0 5.7 0.63 J 760 <1.0 8.6 NA 0.26 J <2.0 31.0 190 7.0 20.0
Z4-X30 5/12/2011 13.0 <5.0 <5.0 63.0 0.72 J 160 <5.0 47.0 NA <5.0 <10 54.0 380 11.0 62.0
Z4-X30 7/27/2011 360 <1.0 <1.0 230 6.6 430 <1.0 210 NA 6.1 <2.0 280 1,800 51.0 770
Z4-X30 9/19/2011 43.0 <1.0 <1.0 95.0 1.0 300 <1.0 39.0 NA <1.0 <2.0 140 340 7.5 58.0
Z4-X30 10/27/2011 25.0 <10 <10 180 2.0 J 17.0 <10 33.0 NA <10 5.6 J 170 820 3.4 J 30.0
Z4-X30 1/18/2012 18.0 <5.0 <5.0 34.0 <5.0 31.0 <5.0 8.1 NA <5.0 2.5 J 39.0 650 3.2 J 15.0
Z4-X30 3/8/2012 26.0 <1.0 <1.0 42.0 0.9 J 1.8 <1.0 11.0 NA <1.0 <2.0 28.0 360 1.3 25.0
Z4-X30 4/17/2013 19.0 <1.0 <1.0 52.0 2.2 3.3 <1.0 9.5 NA <1.0 <2.0 65.0 140 3.5 52.0
Z4-X30 11/4/2015 3.96 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 1.03 NA <1.0 <5.0 <5.0 <10 1.93 <3.0
Z4-X30 7/14/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z4-X30 12/14/2016 <1.0 <0.0202 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 398 <1.0 <3.0
Z4-X30 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X30 12/13/2017 1.2 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.32 <1.0 <0.30 28.0 <0.20 <0.30
Z4-X30 7/10/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X30 12/18/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X30 6/11/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.502 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X30 12/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X30 6/15/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 21 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z4-X30 12/15/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X30 6/15/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X30 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X30 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X35 10/6/2010 110 8.8 1,600 78.0 J <100 26,000 <100 410 NA <100 <200 250 14,000 990 2,700
Z4-X35 3/23/2011 1,800 <50 <50 380 13.0 J 21,000 <50 2,000 NA <50 <100 770 13,000 4,500 10,000
Z4-X35 5/11/2011 3,300 150 <100 360 42.0 J 20,000 <100 4,800 NA <100 <200 880 8,000 40,000 25,000
Z4-X35 7/27/2011 790 <50 250 680 27.0 J 6,000 <50 810 NA <50 13.0 J 1,500 7,000 3,000 4,700
Z4-X35 9/19/2011 790 <10 <10 700 16.0 5,000 <10 510 NA <10 7.4 J 930 3,600 1,200 2,700
Z4-X35 11/15/2011 990 <10 <10 2,500 7.7 J 120 <10 250 NA <10 4.2 J 3,200 840 410 1,600
Z4-X35 1/18/2012 160 <5.0 <5.0 650 5.5 250 <5.0 56.0 NA <5.0 <10 460 830 120 360
Z4-X35 3/7/2012 450 <5.0 270 820 1.3 J 3,700 <5.0 47.0 NA <5.0 <10 420 7,500 89.0 270
Z4-X35 5/21/2012 7.7 <1.0 18.0 45.0 <1.0 370 <1.0 2.5 NA <1.0 <2.0 80 1,400 5.1 16.0
Z4-X35 7/24/2012 2.8 <1.0 6.7 91.0 <1.0 69.0 <1.0 0.56 J NA <1.0 <2.0 18.0 340 0.7 J 3.4
Z4-X35 4/17/2013 62.0 <5.0 42.0 79.0 <5.0 220 <5.0 17.0 NA 3.5 J <10 270 2,400 23.0 100
Z4-X35 11/4/2015 6.43 <0.020 <1.0 11.8 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 358 1.95 <3.0
Z4-X35 7/13/2016 6.01 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 367 <1.0 <3.0
Z4-X35 12/14/2016 4.17 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 241 <1.0 <3.0
Z4-X35 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 33.7 <0.20 <1.0 <0.30 270 <0.20 <0.30
Z4-X35 12/13/2017 0.85 <0.20 <0.20 5.8 <0.30 <0.20 <0.20 <0.30 42.3 0.28 <1.0 3.0 310 0.3 <0.30
Z4-X35 7/10/2018 1.5 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 29.6 <0.20 <1.0 <0.30 120 0.44 1.1
Z4-X35 12/17/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 0.27 J <0.20 <0.30 11.9 <0.20 <1.0 <0.30 90.0 0.59 J <0.30
Z4-X35 6/11/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 16.3 <0.20 <1.0 <0.30 75.0 <0.20 <0.30
Z4-X35 12/10/2019 3.4 <0.0031 <0.20 7.6 <0.30 0.37 J <0.20 <0.30 15.6 7.6 <1.0 <0.30 76.0 1.2 0.62 J
Z4-X35 6/15/2020 0.97 J <0.0032 <0.20 1.8 <0.30 <0.20 <0.20 <0.30 11.6 <0.20 <1.0 <0.30 13.0 0.52 J <0.30
Z4-X35 12/17/2020 <0.30 <0.0031 <0.20 3.5 <0.30 <0.20 <0.20 <0.30 6.62 <0.20 <1.0 <0.30 14.0 0.53 J <0.30
Z4-X35 6/15/2021 <0.30 <0.0032 <0.20 4.0 0.94 J <0.20 <0.20 <0.30 6.18 <0.20 <1.0 3.2 29.0 0.81 J <0.30
Z4-X35 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 0.31 J <0.20 <0.30 1.29 <0.20 <1.0 <0.30 <10 0.83 J <0.30
Z4-X35 7/18/2023 <0.30 <0.0031 < 0.20 <1.0 <0.30 <0.30 <0.30 <0.30 NA < 0.20 < 1.0 <0.30 <10 0.95 J <0.30
Z4-X47 9/29/2010 310 <100 590 210 <100 30,000 <100 1,800 NA 45.0 J <200 510 18,000 6,800 10,000
Z4-X47 3/23/2011 4,100 15 J 1,200 730 36.0 J 23,000 <50 4,500 NA 11.0 J <100 960 5,900 20,000 16,000
Z4-X47 5/12/2011 4,400 <50 <50 1,500 83 3,300 <50 3,200 NA <50 30.0 J 1,600 2,400 10,000 30,000
Z4-X47 7/27/2011 470 <50 440 610 21.0 J 5,100 <50 600 NA <50 14.0 J 980 7,000 1,700 3,300
Z4-X47 9/19/2011 560 <5.0 <5.0 430 12.0 760 <5.0 280 NA <5.0 <10 320 570 1,000 1,700
Z4-X47 11/9/2011 660 <50 57 320 11.0 J 890 <50 220 NA <50 <100 250 1,200 730 1,400
Z4-X47 1/17/2012 790 <1.0 <1.0 390 16.0 940 <1.0 360 NA 1.5 <2.0 450 950 1,400 2,100
Z4-X47 3/7/2012 1,300 <5.0 100 420 <5.0 1,500 <5.0 720 NA 3.0 J <10 520 1,900 2,000 4,000
Z4-X47 5/22/2012 180 <5.0 <5.0 240 3.5 J 340 <5.0 130 NA <5.0 <10 180 530 690 730
Page 22 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z4-X47 4/18/2013 64.0 <5.0 48 21.0 <5.0 200 <5.0 46.0 NA 1.8 J <10 25.0 1,200 160 180
Z4-X47 11/4/2015 31.9 <0.0204 2.4 16.7 <1.0 106 <1.0 50.8 NA <1.0 <5.0 14.7 475 40.0 88.5
Z4-X47 7/13/2016 86.9 <0.0198 4.78 22.0 <1.0 64.6 <1.0 51.0 1.43 J <1.0 <5.0 14.9 497 88.4 238
Z4-X47 12/14/2016 12.1 <0.0198 <1.0 <10 <1.0 26.5 <1.0 14.9 1.66 J <1.0 <5.0 6.89 275 <1.0 8.56
Z4-X47 6/27/2017 1.4 <0.20 2.7 9.9 <0.30 <0.20 <0.20 <0.30 131 <0.20 <1.0 12.0 380 <0.20 94.0
Z4-X47 12/11/2017 130 <0.20 <0.20 39.0 <0.30 40.0 <0.20 63.0 129 <0.20 <1.0 14.0 300 1.7 220
Z4-X47 7/10/2018 61.0 <0.0027 1.0 14.0 <0.30 <0.20 <0.20 <0.30 116 <0.20 <1.0 6.0 170 <0.20 160
Z4-X47 12/18/2018 <0.30 <0.0031 1.0 9.0 <0.30 <0.20 <0.20 4.1 12.4 <0.20 <1.0 0.81 J 300 <0.20 15.0
Z4-X47 6/11/2019 13.0 <0.0031 <0.20 12.0 0.94 J <0.20 <0.20 <0.30 112 <0.20 <1.0 7.4 170 <0.20 62.0
Z4-X47 12/10/2019 12.0 <0.0031 0.54 J 7.6 <0.30 <0.20 <0.20 4.6 161 <0.20 <1.0 4.2 140 <0.20 36.0
Z4-X47 6/15/2020 2.3 <0.0032 <0.20 28.0 <0.30 34.0 <0.20 67.0 58.5 <0.20 <1.0 11.0 33.0 1.4 17.0
Z4-X47 12/17/2020 1.8 <0.0031 0.48 J 21.0 <0.30 14.0 <0.20 90.0 42.2 3.3 <1.0 9.4 41.0 0.47 J 15.0
Z4-X47 6/16/2021 0.72 J <0.0032 <0.20 25.0 <0.30 19.0 <0.20 53.0 51.0 <0.20 <1.0 8.4 57.0 <0.20 6.6
Z4-X47 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 39.4 <0.20 <1.0 <0.30 <10 <0.20 0.71 J
Z4-X47 7/18/2023 <0.30 <0.0031 <0.20 7.5 <0.30 8.2 <0.30 0.74 J NA <0.20 <1.0 4.3 <10 <0.20 1.4 J
Z4-X55 10/1/2010 180 <10 100 130 <10 5,400 <10 1,100 NA <10 <20 520 470 4,300 5,300
Z4-X55 3/23/2011 140 <1.0 <1.0 170 5.2 1,500 <1.0 120 NA <1.0 <2.0 270 470 260 510
Z4-X55 5/11/2011 260 <5.0 <5.0 150 9.7 270 <5.0 62.0 NA <5.0 <10 170 200 240 1,100
Z4-X55 7/27/2011 120 <1.0 <1.0 130 6.9 650 <1.0 150 NA <1.0 8.4 210 340 98.0 360
Z4-X55 9/19/2011 200 <5.0 <5.0 140 15.0 260 <5.0 180 NA <5.0 <10 130 280 63.0 490
Z4-X55 10/26/2011 160 <5.0 <5.0 120 10.0 200 0.9 J 87.0 NA <5.0 <10 85.0 440 44.0 300
Z4-X55 1/18/2012 84.0 <1.0 <1.0 22.0 3.1 10.0 <1.0 38.0 NA <1.0 <2.0 13.0 240 3.3 56.0
Z4-X55 3/7/2012 52.0 <1.0 <1.0 66.0 0.32 J 3.7 <1.0 5.8 NA <1.0 <2.0 13.0 190 1.6 31.0
Z4-X55 4/18/2013 100 <1.0 <1.0 11.0 5.5 0.4 J <1.0 0.78 J NA <1.0 <2.0 5.6 220 0.46 J 20.0
Z4-X55 11/4/2015 1.11 <200 <1.0 <10 <1.0 1.41 <1.0 3.36 NA <1.0 <5.0 <5.0 <10 1.82 <3.0
Z4-X55 7/13/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
Z4-X55 12/14/2016 <1.0 <0.0202 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 66.5 <1.0 <3.0
Z4-X55 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.886 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X55 12/11/2017 0.48 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.883 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X55 7/10/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X55 12/18/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X55 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.20 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X55 12/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.20 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X63 1/17/2012 2,200 <10 <10 740 53.0 2,900 <10 1,400 NA 33.0 9.0 J 1,100 1,600 650 5,500
Z4-X63 3/7/2012 1,900 <5.0 <5.0 800 1.7 J 2,200 <5.0 700 NA 36.0 <10 720 2,700 220 3,200
Z4-X63 5/21/2012 1,100 <5.0 <5.0 990 27.0 880 <5.0 390 NA 37.0 <10 280 790 98.0 1,600
Z4-X63 7/24/2012 730 <1.0 <1.0 1,300 7.7 120 <1.0 300 NA 4.1 <2.0 280 200 20.0 840
Z4-X63 8/27/2012 460 <5.0 <5.0 570 13.0 28.0 <5.0 130 NA 2.7 J <10 820 240 7.1 380
Page 23 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z4-X63 11/5/2015 164 <0.020 <1.0 30.6 1.99 18.2 <1.0 84.5 NA <1.0 <5.0 <5.0 545 6.02 203
Z4-X63 7/13/2016 80.2 <0.020 <1.0 89 <1.0 14.2 <1.0 34.3 1.37 J 1.45 <5.0 7.96 512 1.08 47.2
Z4-X63 12/14/2016 147 <200 <1.0 18.6 <1.0 13.4 <1.0 55.5 <5.0 <1.0 <5.0 <5.0 337 1.61 177
Z4-X63 6/28/2017 53.0 <0.20 <0.20 28.0 <0.30 5.1 <0.20 45.0 412 3.8 <1.0 <0.30 600 0.62 100
Z4-X63 12/11/2017 740 <0.20 <0.20 100 4.7 19.0 <0.20 230 273 0.7 <1.0 7.7 420 2.3 400
Z4-X63 7/10/2018 350 <0.0027 <0.20 28.0 2.1 6.5 <0.20 21.0 127 0.46 <1.0 <0.30 190 0.44 130
Z4-X63 12/18/2018 3.9 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 42.8 2.6 <1.0 <0.30 310 <0.20 7.0
Z4-X63 6/11/2019 100 <0.0030 <0.20 8.7 1.4 1.3 <0.20 <0.30 123 <0.20 <1.0 2.1 110 <0.20 28.0
Z4-X63 12/10/2019 190 <0.0031 <0.20 13.0 <0.30 1.3 <0.20 5.9 171 <0.20 <1.0 <0.30 180 <0.20 17.0
Z4-X63 6/15/2020 48.0 <0.0031 <0.20 3.3 <0.30 0.92 J <0.20 0.53 J 35.6 0.60 J <1.0 <0.30 110 <0.20 3.3
Z4-X63 12/17/2020 60.0 <0.0032 <0.20 12.0 2.3 1.9 <0.20 2.0 44.7 3.7 1.9 J 4.4 100 <0.20 4.7
Z4-X63 6/15/2021 4.9 <0.0032 <0.20 <1.0 2.1 <0.20 <0.20 <0.30 41.5 <0.20 <1.0 <0.30 100 <0.20 3.0
Z4-X63 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X63 7/19/2023 23.0 <0.0031 <0.20 <1.0 <0.30 1.1 <0.20 2.4 NA <0.20 <1.0 4.1 <10 <0.20 2.4 J
Z4-X68 1/17/2012 590 <10 <10 530 <10 4,800 <10 310 NA 3.2 J 15.0 J 840 3,200 330 2,400
Z4-X68 3/8/2012 200 <10 <10 240 2.6 J 5,300 <10 63.0 NA 13.0 <20 330 9,900 65.0 550
Z4-X68 5/21/2012 48 <5.0 <5.0 130 <5.0 1,600 <5.0 9.8 NA 50.0 <10 190 13,000 11.0 140
Z4-X68 7/25/2012 140 <1.0 27.0 93.0 2.9 2,000 <1.0 75.0 NA 180 <2.0 330 16,000 81.0 1,000
Z4-X68 8/27/2012 170 <5.0 <5.0 200 2.0 J 1,400 <5.0 55.0 NA 290 <10 200 35,000 82.0 690
Z4-X68 11/29/2012 NA NA NA NA NA NA NA NA NA NA NA NA 8,000 NA NA
Z4-X68 4/15/2013 57 <5.0 42.0 33.0 <5.0 12.0 <5.0 14 NA 710 8.5 J 36.0 79,000 3.6 J 170
Z4-X68 11/4/2015 57.8 <0.020 <1.0 <10 <1.0 1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 671 1.85 <3.0*
Z4-X68 7/14/2016 8.9 <0.020 <1.0 <10 <1.0 1.23 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 260 2.05 <3.0
Z4-X68 12/14/2016 4.15 <0.0198 <1.0 <10 <1.0 1.01 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 458 1.21 <3.0
Z4-X68 6/28/2017 <0.30 <0.20 <0.20 7.7 <0.30 <0.20 <0.20 <0.30 39.2 1.8 <1.0 <0.30 9,100 <0.20 2.0
Z4-X68 12/12/2017 1.2 <0.20 <0.20 <1.0 <0.30 0.84 <0.20 <0.30 6.01 0.54 <1.0 <0.30 440 0.91 <0.30
Z4-X68 7/10/2018 1.9 <0.0026 <0.20 <1.0 <0.30 0.59 <0.20 <0.30 3.95 <0.20 <1.0 <0.30 210 0.39 0.72
Z4-X68 12/18/2018 0.88 J <0.0032 <0.20 <1.0 <0.30 0.30 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 130 <0.20 0.74 J
Z4-X68 6/11/2019 <0.30 <0.0031 <0.20 2.7 <0.30 <0.20 <0.20 <0.30 1.69 <0.20 <1.0 <0.30 76.0 <0.20 0.76 J
Z4-X68 12/10/2019 0.94 J <0.0031 <0.20 6.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 60.0 <0.20 <0.30
Z4-X68 6/15/2020 0.87 J 0.0076 <0.20 3.6 <0.30 0.73 J <0.20 0.49 J <0.0900 <0.20 <1.0 0.60 J <10 <0.20 <0.30
Z4-X68 12/17/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 0.98 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X68 6/16/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X68 6/22/2022 91 <0.0031 <0.20 <1.0 2.5 1.5 <0.20 1.9 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 4.9
Z4-X68 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
Z4-X70 1/18/2012 760 <5.0 <5.0 490 1.1 J 43.0 <5.0 54 NA <5.0 <10 810 890 48.0 400
Z4-X70 2/9/2012 250 <1.0 37.0 57.0 <1.0 730 <1.0 140 NA 8.3 <2.0 59.0 12,000 130 520
Z4-X70 3/7/2012 330 <1.0 35.0 180 0.3 J 250 <1.0 93 NA 2.8 <2.0 77.0 7,500 45.0 450
Page 24 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z4-X70 5/22/2012 95 <5.0 <5.0 1,400 5.8 <5.0 <5.0 5.1 NA <5.0 <10 86.0 240 5.6 38.0
Z4-X70 7/25/2012 200 <1.0 17.0 40.0 7.1 240 <1.0 130 NA 5.3 <2.0 210 3,400 69.0 1,100
Z4-X70 4/16/2013 130 <5.0 200 20.0 <5.0 7.1 <5.0 <5.0 NA 22.0 3.6 J 24.0 24,000 <5.0 120
Z4-X70 11/4/2015 32.1 <200 <1.0 26.4 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 1,010 1.8 <3.0
Z4-X70 7/19/2016 27.4 <0.0198 <1.0 22.9 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 1,270 <1.0 <3.0
Z4-X70 12/16/2016 26.4 <0.0202 <1.0 18.9 <1.0 <1.0 <1.0 <1.0 1.52 J <1.0 <5.0 <5.0 534 <1.0 <3.0
Z4-X70 6/28/2017 3.6 <0.20 <0.20 32.0 <0.30 <0.20 <0.20 <0.30 59.4 <0.20 <1.0 <0.30 780 <0.20 1.5
Z4-X70 12/14/2017 7.5 <0.20 <0.20 12.0 <0.30 <0.20 <0.20 <0.30 30.4 <0.20 <1.0 <0.30 320 <0.20 <0.30
Z4-X70 7/10/2018 3.6 <0.0026 <0.20 13.0 <0.30 0.29 <0.20 <0.30 17.2 <0.20 <1.0 <0.30 280 <0.65 <0.30
Z4-X70 12/18/2018 1.9 <0.0032 <0.20 13.0 <0.30 <0.20 <0.20 <0.30 3.06 <0.20 <1.0 <0.30 <10 0.60 J <0.30
Z4-X70 6/11/2019 7.6 <0.0031 <0.20 13.0 <0.30 <0.20 <0.20 <0.30 5.77 <0.20 <1.0 6.1 210 0.84 J 2.1
Z4-X70 12/10/2019 5.8 <0.0031 <0.20 6.2 <0.30 0.24 J <0.20 <0.30 6.2 <0.20 <1.0 <0.30 150 0.75 J 1.1
Z4-X70 6/22/2020 6.7 <0.0031 <0.20 19.0 <0.30 0.22 J <0.20 0.38 J <0.0900 <0.20 <1.0 11.0 47.0 0.93 J 2.9
Z4-X70 12/17/2020 5.0 <0.0032 <0.20 12.0 <0.30 0.26 J <0.20 0.38 J <0.0900 3.3 <1.0 5.2 64.0 1.1 2.2
Z4-X70 6/15/2021 2.1 <0.0032 <0.20 3.4 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 41.0 0.58 J 1.9
Z4-X70 6/21/2022 2.6 <0.0032 <0.20 <1.0 <0.30 0.28 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 49.0 1.4 1.4
Z4-X70 7/18/2023 1.5 <0.0032 < 0.20 <1.0 <0.30 0.45 J <0.20 0.47 J NA <0.20 <1.0 <0.30 51 1.7 1.1 J
Z4-X72 1/18/2012 370 <5.0 96 700 15.0 22.0 <5.0 21.0 NA 92 <10 670 53,000 2.7 J 90.0
Z4-X72 2/9/2012 76.0 <1.0 54 280 0.37 J 210 <1.0 40.0 NA 56 <2.0 360 35,000 7.6 63.0
Z4-X72 3/8/2012 11.0 <1.0 18 160 0.15 J 5.5 <1.0 3.0 NA 15 <2.0 19.0 7,400 0.77 J 8.5
Z4-X72 5/22/2012 21.0 <5.0 19 170 <5.0 5.5 <5.0 2.2 J NA 30 <10 39.0 15,000 <5.0 8.6 J
Z4-X72 7/25/2012 100 <1.0 <1.0 1,200 3.3 47.0 <1.0 43.0 NA 1.1 <2.0 1,200 1,900 4.8 120
Z4-X72 4/16/2013 30.0 <5.0 45.0 74.0 <5.0 130 <5.0 6.9 NA 56.0 3.4 J 87.0 26,000 4.5 J 31.0
Z4-X72 11/4/2015 21.5 <0.0199 <1.0 <10 <1.0 6.38 <1.0 <1.0 NA 1.12 <5.0 <5.0 18,100 3.27 3.66 *
Z4-X72 7/19/2016 <10 <0.0198 <10 <100 <10 <10 <10 <10 <5.0 <10 <50 <50 16,200 <10 <30
Z4-X72 12/16/2016 5.32 <0.020 <1.0 <10 <1.0 2.76 <1.0 <1.0 <5.0 3.43 <5.0 <5.0 12,800 1.77 <3.0
Z4-X72 6/28/2017 <0.30 <0.20 <0.20 6.2 <0.30 <0.20 <0.20 <0.30 31.4 <0.20 <1.0 <0.30 9,000 <0.20 1.2
Page 25 of 26
Table 5
Groundwater Analytical Data - Onsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane 1,2-DCA 2-
Methylnaphthalene
4-
Isopropylt
oluene
Benzene Chloroform Ethyl-
benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
Z4-X72 12/14/2014 1.1 <0.20 <0.20 <1.0 <0.30 0.9 <0.20 <0.30 75.9 3.9 <1.0 <0.30 15,000 <0.20 <0.30
Z4-X72 7/10/2018 1.4 <0.0027 <0.20 8.6 <0.30 1.1 <0.20 <0.30 30.7 3.5 <1.0 <0.30 8,000 0.36 <0.30
Z4-X72 12/18/2018 1.1 <0.20 <0.20 1.4 <0.30 <0.20 <0.20 <0.30 <0.0900 1.0 <1.0 <0.30 3,900 <0.20 0.74 J
Z4-X72 6/10/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 3.01 1.9 <1.0 <0.30 5,800 <0.20 <0.30
Z4-X72 12/10/2019 0.47 J 0.0085 JP <0.20 <1.0 <0.30 0.54 J <0.20 <0.30 1.46 2.2 <1.0 <0.30 5,200 <0.20 <0.30
Z4-X72 6/15/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 0.44 J <0.20 <0.30 <0.0900 2.3 <1.0 <0.30 2,600 <0.20 <0.30
Z4-X72 12/17/2020 <0.30 <0.0031 <0.20 5.4 <0.30 0.30 J <0.20 <0.30 <0.0900 3.7 <1.0 <0.30 500 <0.20 <0.30
Z4-X72 6/15/2021 3.6 <0.0032 <0.20 38.0 <0.30 0.23 J <0.20 0.31 J <0.0900 <0.20 <1.0 11.0 80.0 1.0 2.2
Z4-X72 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 290.0 <0.20 <0.30
Z4-X72 7/18/2023 <0.30 <0.0031 <0.20 4.3 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 140 <0.20 <0.30
Z4-X89 5/21/2012 1,600 <5.0 18.0 690 <5.0 2,500 <5.0 560 NA <5.0 <10 1,500 810 650 3,700
Z4-X89 8/9/2012 80.0 <5.0 26.0 110 1.6 J 570 <5.0 70.0 NA <5.0 <10 26.0 2,200 61.0 420
Z4-X89 8/27/2012 750 <5.0 72.0 650 9.5 1,500 <5.0 240 NA 32.0 <10 710 3,100 73.0 1,200
Z4-X89 4/18/2013 1,300 <5.0 <5.0 170 4.8 J 600 <5.0 490 NA 1.5 J <10 1,200 1,100 100 2,500
Z4-X89 11/4/2015 1,020 <0.020 <1.0 47.9 7.36 11.6 <1.0 41.9 NA <1.0 <5.0 25.1 1,470 3.75 356
Z4-X89 7/19/2016 1,200 <0.0197 <10 <100 <10 12.9 <10 57.9 <5.0 <10 <50 <50 1,410 <10 280
Z4-X89 12/28/2016 767 <0.0202 <1.0 <10 5.99 9.01 <1.0 45.1 <5.0 <1.0 <5.0 <5.0 1,770 1.53 70.1
Z4-X89 6/28/2017 59.0 <0.20 <0.20 9.7 8.6 6.0 <0.20 45.0 128 1.3 <1.0 1.1 1,700 0.7 49.0
Z4-X89 12/11/2017 130 <0.20 <0.20 7.1 16.0 3.4 <0.20 1.8 145 0.29 <1.0 3.7 2,100 <0.20 1.5
Z4-X89 7/10/2018 56.0 <0.20 <0.20 7.8 <0.30 4.8 <0.20 1.9 92.9 <0.20 <1.0 1.4 1,100 0.63 9.0
Z4-X89 12/19/2018 33.0 <0.0032 <0.20 <1.0 <0.30 0.89 J <0.20 1.1 1.4 <0.20 <1.0 <0.30 340 <0.20 4.2
Z4-X89 6/10/2019 110 <0.0031 <0.20 3.0 1.4 2.2 <0.20 1.5 18.5 <0.20 <1.0 3.7 490 <0.20 6.0
Z4-X89 12/10/2019 27.0 <0.0031 <0.20 6.3 0.41 J 1.2 <0.20 2.3 15.8 <0.20 <1.0 2.4 430 <0.20 3.0
Z4-X89 6/22/2020 31.0 0.015 JP <0.20 4.4 <0.30 0.70 J <0.20 2.8 4.82 <0.20 <1.0 3.5 190 0.59 J 3.6
Z4-X89 12/17/2020 1.4 <0.0031 <0.20 5.5 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 3.1 <10 <0.20 <0.30
Z4-X89 6/14/2021 0.91 J <0.0031 <0.20 2.8 <0.30 0.60 J <0.20 0.59 J 1.60 <0.20 <1.0 4.3 130 0.45 J 1.3
Z4-X89 6/21/2022 0.70 J <0.0031 <0.20 <1.0 <0.30 0.74 J <0.20 0.76 J 3.44 <0.20 <1.0 <0.30 110 0.69 J 2.1
Z4-X89 7/18/2023 <0.30 <0.0031 <0.20 4.9 <0.30 0.59 J <0.20 <0.30 NA <0.20 <1.0 4.0 <10 0.68 J <0.30
Notes
MTBE - Methyl tert-butyl ether
TBA - Tert-butyl alcohol
NA - Not Available
J - Analyte detected below quantitation limits.
ug/l - microgram per liter
mg/l - milligram per liter
Exceeds NCAC 2L standard
Exceeds IMAC standard
1,2-DCA - 1,2-Dichloroethane
Page 26 of 26
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
AMW-8S 8/6/2003 NA NA <2.0 11.0 NA 230 9.0 84.0 NA NA <5.0 25.0 NA 41.0 219
AMW-8S 9/1/2004 NA <10 <10 NA NA 1,510 <10 178 NA <10 <5.0 NA 417 6.6 J 79
AMW-8S 11/20/2007 0.22 J <0.009 <1.0 1.5 J <1.0 3.7 <1.0 0.37 J NA <1.0 <2.0 1.2 280 0.16 J 0.52 J
AMW-8S 11/6/2008 <1.0 <1.0 <1.0 <2.0 <1.0 15.0 <1.0 0.52 J NA 2.0 1.8 J 0.94 J 390 0.21 J 0.61 J
AMW-8S 11/24/2009 0.19 J <1.0 <1.0 <2.0 <1.0 1.5 <1.0 <1.0 NA 0.12 J <2.0 0.18 J 23.0 <1.0 <3.0
AMW-8S 3/10/2011 <1.0 <1.0 0.28 J <2.0 <1.0 0.71 J <1.0 0.24 J NA 0.35 J <2.0 <1.0 110 0.15 J <3.0
AMW-8S 11/8/2011 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <2.0 <1.0 120 <1.0 <3.0
AMW-8S 11/30/2012 <1.0 <1.0 0.57 J <1.0 <1.0 <1.0 <1.0 <1.0 NA 0.93 J 1.6 J <1.0 210 0.6 J <3.0
AMW-8S 11/10/2015 3.28 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 NA <1.0 <5.0 <5.0 <10 <1.0 3.73
AMW-8S 8/2/2016 <1.0 <0.0206 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 12.7 <1.0 <3.0
AMW-8S 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 99.8 <1.0 <3.0
AMW-8S 6/29/2017 <0.30 <0.20 <0.20 <1.0 <0.30 0.96 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 47.0 <0.20 <0.30
AMW-8S 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-8S 7/10/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 74.0 <0.20 <0.30
AMW-8S 1/10/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-8S 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-8S 12/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 24.0 <0.20 <0.30
AMW-8S 6/23/2020 <0.30 0.0081 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.49 <0.20 <1.0 <0.30 37.0 <0.20 <0.30
AMW-8S 12/29/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-8S 6/15/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 0.44 J <0.20 0.68 J 1.13 0.24 J <1.0 <0.30 62.0 <0.20 <0.30
AMW-8S 6/21/2022 <0.30 0.049 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-8S 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-9S 8/5/2003 N N <100 10 N 2,710 <100 281 N N <50 24.0 N 1,030 1,650
AMW-9S 9/1/2004 N <100 67.6 J N N 3,760 <100 325 N <100 <50 N <1,000 483 1,340
AMW-9S 11/20/2007 120 <0.0094 <1.0 14 1.5 740 <1.0 130 N <1.0 <2.0 34.0 730 29 270
MW-9S 11/6/2008 90.0 <1.0 3.4 5.7 1.8 320 <1.0 130 N <1.0 <2.0 11.0 120 25 220
MW-9S 11/24/2009 28.0 <1.0 3.0 0.87 J 0.86 J 110 3.4 60 N 0.13 J 16.0 1.6 <20 19 110
MW-9S 3/10/2011 0.57 J <1.0 <1.0 <2.0 <1.0 3.0 <1.0 2.2 N <1.0 <2.0 0.76 J 12 J 0.48 J 2.1 J
MW-9S 11/8/2011 2.9 <1.0 <1.0 <2.0 <1.0 14.0 <1.0 5.4 N <1.0 <2.0 <1.0 <10 1.6 5.4
MW-9S 11/30/2012 25.0 <1.0 <1.0 <1.0 1.6 180 <1.0 62.0 N <1.0 <2.0 7.8 <10 15.0 69.0
MW-9S 10/28/2015 6.53 <0.0199* <1.0 <10 <1.0 14.2 <1.0 1.8 N <1.0 <5.0 <5.0 <10 <1.0 3.43
MW-9S 7/25/2016 <1.0 <0.020 <1.0 <10 <1.0 1.7 <1.0 1.6 <5.0 <1.0 <5.0 <5.0 25.4 1.94 <3.0
MW-9S 12/13/2016 2.02 <0.020 <1.0 <10* <1.0 2.5 <1.0 3.14 <5.0 <1.0 <5.0 <5.0 <10 2.83 <3.0
MW-9S 6/29/2017 <0.30 <0.20 <0.20 <1.0 <0.30 1.2 <0.20 <0.30 2.15 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-9S 12/12/2017 0.69 <0.20 <0.20 <1.0 <0.30 1.2 <0.20 0.81 5.73 <0.20 <1.0 <0.30 <10 0.68 0.76
MW-9S 7/10/2018 <0.30 <0.0025 <0.20 <1.0 <0.30 0.62 <0.20 <0.30 21.4 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-9S 1/11/2019 <0.30 0.0080 J <0.20 <1.0 <0.30 56.0 <0.20 11.0 14.7 <0.20 <1.0 1.4 <10 4.0 8
MW-9S 6/14/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-9S 12/17/2019 0.64 J <0.0031 <0.20 <1.0 <0.30 1.1 <0.20 0.84 J 41.1 <0.20 <1.0 <0.30 <10 <0.20 1.4
AMW-9S 6/23/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 4.81 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Analyte
Unit
Page 1 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
AMW-9S 12/29/2020 11.0 <0.0032 <0.20 <1.0 <0.30 74.0 <0.20 20.0 45.1 <0.20 <1.0 3.8 <10 4.2 20.0
AMW-9S 6/17/2021 6.5 <0.0031 <0.20 2.7 0.67 J 63.0 <0.20 4.9 85.8 <0.20 <1.0 2.2 <10 2.9 9.8
AMW-9S 6/21/2022 79.00 <0.0031 <0.20 34.0 <0.30 110 <0.20 24 46 <0.20 <1.0 36.0 <10 4.4 68
AMW-9S 7/19/2023 1.4 <0.0031 <0.20 <1.0 <0.30 12.0 <0.20 4.5 NM <0.20 <1.0 2.4 <10 0.44 J 3.5
MW-10S 8/5/2003 N N <2.0 73.0 N 3,860 11.0 846 N N <5.0 172 N 373 4,230
AMW-10S 8/31/2004 N <100 <100 N N 2,710 <100 436 N <100 <50 N <1,000 89.3 J 2,290
AMW-10S 10/29/2015 306 <0.0198 <1.0 62.3 <1.0 31.7 <1.0 324 N <1.0 <5.0 160 <10 1.51 205
MW-10S 8/2/2016 257 <0.0199 <10 <100 <10 17.0 <10 398 <5.0 <10 <50 125 <100 <10 322
MW-10S 12/28/2016 56.7 <0.020 <1.0 15.3 1.07 60.8 <1.0 35.2 <5.0 <1.0 <5.0 33.4 <10 <1.0 11
MW-10S 7/6/2017 1.8 <0.20 1.9 7.9 1.1 7.0 <0.20 57.0 74.6 <0.20 <1.0 13.0 0.58 43 322
MW-10S 12/13/2017 61.0 <0.20 1.9 7.9 1.1 63.0 0.73 46.0 160.0 <0.20 <1.0 20.0 <10 0.48 21
MW-10S 7/12/2018 61.0 <0.0026 <0.20 8.8 <0.30 21.0 <0.20 52.0 158.0 <0.20 <1.0 36.0 <10 0.49 36
MW-10S 1/8/2019 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-10S 6/13/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-10S 12/17/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 0.27 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 0.63 J
AMW-10S 6/23/2020 33.0 <0.0031 <0.20 <1.0 0.44 J 0.41 J <0.20 17.0 13.2 <0.20 <1.0 6.8 <10 <0.20 17.0
AMW-10S 12/29/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 0.59 J 1.71 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-10S 6/17/2021 130 <0.0032 <0.20 12.0 <0.30 4.2 <0.20 180 51.5 <0.20 <1.0 42.0 <10 0.42 J 130
AMW-10S 6/20/2022 12.0 <0.0031 <0.20 <1.0 0.31 J 1.4 <0.20 11.0 8.22 <0.20 <1.0 7.0 <10 <0.20 18
AMW-10S 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-11S 8/5/2003 N N <100 42.0 N 1,670 <100 163 N N <50 103 N 613 1,110
AMW-11S 9/7/2012 1.1 <1.0 <1.0 <1.0 <1.0 12.0 <1.0 1.2 N <1.0 <2.0 3.7 <10 <1.0 <3.0
MW-11S 11/10/2015 <1.0 <0.020 <1.0 <10 <1.0 2.24 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-11S 7/25/2016 2.22 <0.0199 <1.0 <10 <1.0 25.2 <1.0 1.99 <5.0 <1.0 <5.0 <5.0 <10 1.07 5.87
MW-11S 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-11S 6/29/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.722 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-11S 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.878 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-11S 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-11S 1/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-11S 6/12/2019 <0.30 <0.0031 0.66 J <1.0 <0.30 <0.20 <0.20 <0.30 4.36 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-11S 12/18/2019 <0.30 0.0053 J <0.20 <1.0 <0.30 2.2 <0.20 <0.30 65.3 <0.20 <1.0 <0.30 <10 <0.20 0.61 J
AMW-11S 6/24/2020 <0.30 <0.0031 0.39 J <1.0 <0.30 1.3 <0.20 <0.30 10.4 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-11S 12/29/2020 2.1 <0.0032 <0.20 <1.0 <0.30 58.0 <0.20 3.2 114 <0.20 <1.0 3.0 <10 1.1 5.2
AMW-11S 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 11.3 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-11S 12/28/2021 <3.0 <0.0031 <2.0 <10.0 <3.0 70.0 <2.0 <3.0 170 <2.0 <10.0 <3.0 <100 <2.0 <3.0
AMW-11S 6/23/2022 0.85 J <0.0030 <0.20 <1.0 <0.30 56.0 <0.20 0.64 J 47.1 <0.20 <1.0 <0.30 <10 0.66 J 2.9
AMW-11S 12/5/2022 <0.30 <0.0030 <0.20 <1.0 <0.30 6.3 <0.20 <0.30 11.3 <0.20 <1.0 <0.30 <10 0.42 J <0.30
AMW-11S 7/19/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 2.6 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-11S 12/6/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 36 <0.20 <0.30
Page 2 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
AMW-12S 8/5/2003 N N <2.0 <5.0 N <1.0 15.0 <2.0 N N <5.0 <5.0 N <2.0 <6.0
MW-12S 11/5/2015 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 65.5 2.22 <3.0
MW-12S 8/2/2016 <1.0 <0.0200 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 F1 <1.0 <3.0
MW-12S 6/29/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-12S 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-12S 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-12S 1/8/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-12S 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-12S 12/18/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-12S 6/24/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-12S 12/17/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-12S 6/15/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-12S 6/20/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-12S 7/18/2023 43.0 <0.0031 <0.20 5.9 <0.30 1.0 <0.20 50 NM <0.20 <1.0 20.0 <10 <0.20 28.0
MW-13B 5/5/2004 N <2.0 48.0 <5.0 N <1.0 <2.0 <2.0 N 3.1 <5.0 <5.0 1,620 <2.0 <6.0
MW-13B 3/8/2006 <2.0 <1.0 87.9 <5.0 <1.0 <1.0 <1.0 <1.0 N 7.3 <5.0 <2.0 2,900 <1.0 <3.0
MW-13B 5/23/2011 <1.0 <1.0 20.0 <1.0 <1.0 <1.0 <1.0 <1.0 N 2.2 <2.0 <1.0 <10 <1.0 <3.0
MW-13B 11/11/2015 <1.0 <0.020 22.5 <10 <1.0 <1.0 <1.0 <1.0 N 4.28 <5.0 <5.0 363 <1.0 <3.0
MW-13B 7/26/2016 <1.0 <0.0198 10.9 <10 <1.0 <1.0 <1.0 <1.0 <5.0 2.9 <5.0 <5.0 725 <1.0* <3.0
MW-13B 12/16/2016 <1.0 <0.0194 11.1 <10 <1.0 <1.0 <1.0 <1.0 <5.0 3.75 <5.0 <5.0 839 <1.0 <3.0
MW-13B 6/29/2017 <0.30 <0.20 9.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 3.6 <1.0 <0.30 1,100 <0.20 <0.30
MW-13B 12/12/2017 <0.30 <0.20 9.1 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 3.2 <1.0 <0.30 960 <0.20 <0.30
MW-13B 7/11/2018 <0.30 <0.0027 21.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 8.1 <1.0 0.55 980 <0.20 <0.30
MW-13B 1/8/2019 <0.30 <0.0032 11.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 4.1 <1.0 <0.30 800 <0.20 <0.30
MW-13B 6/12/2019 <0.30 <0.0031 6.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 3.4 <1.0 <0.30 680 <0.20 <0.30
AMW-13B 12/18/2019 <0.30 <0.0031 13.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 7.3 <1.0 <0.30 <10 <0.20 <0.30
AMW-13B 6/23/2020 <0.30 <0.0030 9.4 <1.0 <0.30 0.21 J <0.20 <0.30 <0.0900 5.1 <1.0 <0.30 770 <0.20 <0.30
AMW-13B 12/28/2020 <0.30 <0.0032 5.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 4.6 <1.0 <0.30 670 <0.20 <0.30
AMW-13B 6/17/2021 <0.30 <0.0033 10.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 7.1 <1.0 <0.30 940 <0.20 <0.30
AMW-13B 12/28/2021 <0.30 <0.0031 1.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 7.3 <1.0 <0.30 1,500 <0.20 <0.30
AMW-13B 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 3.7 <1.0 <0.30 580 <0.20 <0.30
AMW-13B 12/5/2022 <0.30 <0.0031 8.9 <1.0 <0.30 <0.20 <0.20 <0.30 NA 13 <1.0 <0.30 1,800 <0.20 <0.30
AMW-13B 7/19/2023 <0.30 <0.0032 22.0 <1.0 <0.30 <0.20 <0.20 <0.30 NM 17 <1.0 2.5 1,900 <0.20 <0.30
AMW-13B 12/6/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-13D 5/5/2004 N <4.0 8.3 29.5 N 136 <4.0 42.6 N <4.0 <10 34.7 255 36.3 306
MW-13D 3/8/2006 <2.0 <1.0 9.7 <5.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <2.0 194 <1.0 <3.0
MW-13D 5/23/2011 <1.0 <1.0 1.2 <1.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <2.0 <1.0 17.0 <1.0 <3.0
MW-13D 11/11/2015 <1.0 <0.0198 7.99 <10 <1.0 <1.0 <1.0 <1.0 N 1.3 <5.0 <5.0 103 <1.0 <3.0
Page 3 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
AMW-13D 7/26/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 1.95 <5.0 <5.0 <10 <1.0* <3.0
MW-13D 12/15/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 2.85 <5.0 <5.0 697 <1.0 <3.0
MW-13D 6/30/2017 <0.30 <0.20 7.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.6 <1.0 <0.30 340 <0.20 <0.30
MW-13D 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-13D 7/11/2018 <0.30 <0.0026 26.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 2.6 <1.0 <0.30 590 <0.20 <0.30
AMW-13D 12/18/2018 <0.30 0.014 J 9.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.5 <1.0 <0.30 160 <0.20 <0.30
MW-13D 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.76 J <1.0 <0.30 <10 <0.20 <0.30
AMW-13D 12/17/2019 <0.30 <0.0031 13.0 <1.0 <0.30 0.24 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 220 <0.20 <0.30
AMW-13D 6/24/2020 <0.30 <0.0030 2.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-13D 12/28/2020 <0.30 0.023 11.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 180 <0.20 <0.30
AMW-13D 6/17/2021 <0.30 <0.0032 4.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-13D 6/22/2022 <0.30 0.15 4.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 53 <0.20 <0.30
AMW-13D 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-13I 5/6/2004 N <4.0 4.1 10.5 N 116 <4.0 21.8 N <4.0 <10 11.6 <40 27.6 101
MW-13I 3/8/2006 <2.0 <1.0 2.8 <5.0 <1.0 1.5 <1.0 <1.0 N <1.0 <5.0 <2.0 98.6 <1.0 <3.0
MW-13I 5/23/2011 <1.0 <1.0 0.11 J <1.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <2.0 <1.0 <10 <1.0 <3.0
MW-13I 10/29/2015 <1.0 <0.0199 <1.0 <10 <1.0 1.02 <1.0 <1.0 N <1.0 <5.0 <5.0 21.6 <1.0 <3.0
MW-13I 7/26/2016 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10* <1.0* <3.0
MW-13I 12/15/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 28.9 <1.0 <3.0
MW-13I 6/29/2017 <0.30 <0.20 0.99 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 3.6 <1.0 <0.30 38.0 <0.20 <0.30
MW-13I 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-13I 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-13I 12/18/2018 <0.30 0.027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-13I 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-13I 12/18/2019 0.31 J 0.013 JP <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-13I 6/24/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-13I 12/28/2020 <0.30 0.019 JP <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-13I 6/17/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-13I 6/22/2022 <0.30 0.035 <0.20 <1.0 <0.30 0.32 J <0.20 0.39 J <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-13I 7/19/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-13S 9/2/2004 N <40 <40 33.3 N 1,780 <40 231 N <40 <100 102 <400 145 370
MW-13S 3/7/2006 98.4 <20 <20 <100 <20 1,710 <20 123 N <20 <100 46.4 <400 81.8 211
MW-13S 5/23/2011 20.0 <1.0 <1.0 9.5 2.2 590 1.3 35.0 N <1.0 <2.0 20.0 <10 15.0 31.0
MW-13S 9/7/2012 38.0 <1.0 <1.0 7.8 3.4 1,000 <1.0 53.0 N <1.0 <2.0 25.0 <10 16.0 50.0
MW-13S 10/29/2015 24.2 <0.0206 5.57 <10 1.18 205 <1.0 36.3 N <1.0 <5.0 7.27 <10 2.76 29.2
MW-13S 7/26/2016 7.45 <0.020 <1.0 <10 <1.0 158 <1.0 8.57 1.56 J <1.0 <5.0 8.27 <10* 3.14 13.0
MW-13S 12/15/2016 13.8 <0.020 <1.0 <10 <1.0 194 <1.0 10.4 2.03 J <1.0 <5.0 5.69 <10 3.15 23.1
MW-13S 12/27/2016 7.38 <0.020 <1.0 <10 <1.0 305 <1.0 7.87 7.21 <1.0 <5.0 9.05 <10 3.81 17.2
MW-13S 6/29/2017 3.1 <0.20 <0.20 <1.0 0.67 130 <0.20 3.3 61.4 <0.20 <1.0 2.8 <10 1.6 7.9
Page 4 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
AMW-13S 12/13/2017 9.1 <0.20 <0.20 9.0 0.81 440 <0.20 17.0 1,190 <0.20 <1.0 17.0 <10 5.2 25.0
MW-13S 7/11/2018 8.5 <0.0027 <0.20 <1.0 <0.30 890 <0.20 11.0 412 <0.20 <1.0 12.0 <10 6.0 32.0
MW-13S 1/8/2019 2.6 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 1.6 1.5 J <0.20 <1.0 2.6 <10 <0.20 2.0
AMW-13S 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 1.6 <0.20 <0.30 294 <0.20 <1.0 <0.30 <10 <0.20 1.5
AMW-13S 12/18/2019 0.97 J <0.0031 <0.20 <1.0 <0.30 34.0 <0.20 2.2 139 <0.20 <1.0 1.2 <10 0.54 J 3.3
AMW-13S 6/23/2020 2.7 <0.0030 <0.20 2.1 0.30 J 120 <0.20 5.5 359 <0.20 <1.0 5.8 <10 2.3 6.9
AMW-13S 12/28/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 7.0 <0.20 <0.30 3.41 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-13S 6/17/2021 0.59 J <0.0032 <0.20 2.4 <0.30 130 <0.20 2.5 296 <0.20 <1.0 2.0 <10 2.0 3.2
AMW-13S 6/22/2022 2.8 <0.0031 <0.20 <1.0 <0.30 300 <0.20 7.7 606 <0.20 <1.0 20.0 <10 2.9 9.4
AMW-13S 7/19/2023 0.90 J <0.0031 <0.20 8.3 <0.30 260 <0.20 4.5 NM <0.20 <1.0 13.0 <10 3.6 5.4
MW-14S 8/6/2003 N N 4.0 <5.0 N 102 4.0 53.0 N N <5.0 <5.0 N 1.0 J 33.0
MW-14S 9/1/2004 N <2.0 4.5 N N 101 <2.0 30.9 N <2.0 <5.0 N 275 <2.0 1.1 J
MW-14S 3/8/2006 <2.0 <1.0 4.7 <5.0 <1.0 6.9 <1.0 1.8 N 1.6 <5.0 1.2 J 338 <1.0 <3.0
MW-14S 11/10/2015 <1.0 <0.0228 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-14S 7/22/2016 <1.0 <0.0200 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-14S 12/13/2016 <1.0 <0.020 4.75 <10 <1.0 <1.0 <1.0 <1.0 <5.0 1.82 <5.0 <5.0 255 <1.0 <3.0
MW-14S 6/29/2017 <0.30 <0.20 0.99 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <0.20 <0.30 <10 <0.20 <0.30
MW-14S 12/12/2017 <0.30 <0.20 11.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.724 4.3 4.3 <0.30 <10 <0.20 <0.30
MW-14S 7/12/2018 <0.30 <0.0026 3.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.835 1.0 <1.0 <0.30 100 <0.20 <0.30
MW-14S 1/8/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <0.20 <0.30 <10 <0.20 <0.30
MW-14S 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.497 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-14S 12/18/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.11 <0.20 <1.0 <0.30 21.0 <0.20 <0.30
AMW-14S 6/22/2020 <0.30 <0.0030 1.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.56 J <1.0 <0.30 53.0 <0.20 <0.30
AMW-14S 12/29/2020 <0.30 <0.0031 13.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 5.5 <1.0 <0.30 240 <0.20 <0.30
AMW-14S 6/15/2021 <0.30 <0.0032 4.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 2.3 <1.0 <0.30 72.0 <0.20 <0.30
AMW-14S 12/28/2021 <0.30 <0.0031 19.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 9.4 <1.0 <0.30 410 <0.20 <0.30
AMW-14S 6/22/2022 <0.30 <0.0031 9.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 6.0 <1.0 <0.30 230 <0.20 <0.30
AMW-14S 12/5/2022 <0.30 <0.0031 13.0 <1.0 <0.30 <0.20 <0.20 <0.30 NA 7.6 <1.0 <0.30 350 <0.20 <0.30
AMW-14S 7/18/2023 <0.30 <0.0031 7.4 <1.0 <0.30 <0.20 <0.20 <0.30 NM 3.9 <1.0 <0.30 110 <0.20 <0.30
AMW-14S 12/6/2023 7.0 <0.0032 6.1 15 <0.30 <0.20 <0.20 <0.30 NM 7.9 <1.0 5.9 <10 <0.20 0.93 J
MW-15S 10/29/2015 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-15S 8/3/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 4.3 <10* <1.0 <3.0
MW-15S 12/14/2016 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-15S 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 0.59 <0.20 <0.30 2.67 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-15S 12/12/2017 <0.30 <0.20 11.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.745 <0.20 <1.0 <0.30 16.0 <0.20 <0.30
MW-15S 7/12/2018 <3.0 <0.0026 <2.0 <10 <3.0 <2.0 <2.0 <3.0 45.9 <2.0 <10 <3.0 <100 <2.0 <3.0
MW-15S 1/10/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-15S 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.378 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-15S 12/16/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.76 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 5 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
AMW-15S 6/23/2020 1.1 <0.0030 <0.20 <1.0 <0.30 1.1 <0.20 <0.30 6.58 <0.20 <1.0 2.4 <10 <0.20 1.1
AMW-15S 12/29/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 2.5 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-15S 6/17/2021 0.64 J <0.0032 <0.20 <1.0 <0.30 2.2 <0.20 <0.30 6.56 <0.20 <1.0 1.3 <10 <0.20 1.1
AMW-15S 6/23/2022 4.7 <0.0031 <0.20 <1.0 <0.30 5.1 <0.20 0.43 J 28.1 <0.20 <1.0 <0.30 <10 <0.20 4.9
AMW-15S 7/20/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-16S 10/28/2015 4.57 <0.0199 <1.0 <10 <1.0 117 <1.0 2.26 N <1.0 <5.0 <5.0 <10 1.26 3.23
MW-16S 7/27/2016 15.1 <0.0208 <1.0 <10 1.06 219 <1.0 16.9 <5.0 <1.0 <5.0 10.7 13.9 2.88 9.65
MW-16S 12/15/2016 54.8 <0.0199 <5.0 <50 <5.0 241 <5.0 14.8 <5.0 <5.0 <25.0 26.9 2,470 5.97 38.4
MW-16S 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 26.0 <0.20 <0.30 17.9 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-16S 12/14/2017 13 <0.20 <0.20 6.7 <0.30 100 1.1 2.0 214 <0.20 2.9 3.2 <10 1.3 5.8
MW-16S 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 46.0 <0.20 2.2 116 <0.20 <1.0 2.8 <10 0.32 5.9
MW-16S 1/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 6.8 <0.20 <0.30 25.8 <0.20 <1.0 1.3 <10 <0.20 <0.30
MW-16S 6/13/2019 0.97 J <0.0031 <0.20 <1.0 <0.30 1.3 <0.20 <0.30 90 <0.20 <1.0 <0.30 <10 <0.20 0.69 J
AMW-16S 12/16/2019 7.4 <0.0031 <0.20 4.8 0.84 J 140 <0.20 3.3 224 <0.20 <1.0 6.0 19.0 1.7 9.5
AMW-16S 6/23/2020 3.2 <0.0031 <0.20 6.6 1.1 36.0 <0.20 1.7 191 <0.20 <1.0 7.4 12.0 0.66 J 7.5
AMW-16S 12/28/2020 <0.30 <0.0032 <0.20 <1.0 3.4 <0.20 <0.20 <0.30 132 <0.20 <1.0 4.7 28.0 <0.20 0.68 J
AMW-16S 6/17/2021 8.6 <0.0032 <0.20 5.5 <0.30 190 <0.20 3.1 173 <0.20 <1.0 11.0 <10 2.3 9.4
AMW-16S 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 8.5 <0.20 0.36 J 6.95 2.1 <1.0 <0.30 <10 <0.20 0.77 J
AMW-16S 7/19/2023 11.0 <0.0031 <0.20 4.4 <0.30 250 <0.20 6.7 NM <0.20 <1.0 22.0 <10 4.7 9.4
MW-17S 10/28/2015 <1.0 <0.020 <1.0 <10 <1.0 18.0 <1.0 1.42 N <1.0 <5.0 <5.0 15.1 <1.0 <3.0
MW-17S 7/27/2016 <1.0 <0.0196 <1.0 <10 <1.0 6.34 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-17S 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
MW-17S 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 6.2 <0.20 <0.30 12.3 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-17S 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 5.4 <0.20 <0.30 6.2 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-17S 8/15/2018 < 0.30 < 0.20 < 0.20 < 1.0 < 0.30 1.2 < 0.20 < 0.30 1.14 < 0.20 < 1.0 < 0.30 < 10 < 0.20 < 0.30
MW-17S 1/11/2019 <0.30 0.021 J <0.20 <1.0 <0.30 1.3 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
MW-17S 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.21 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-17S 12/19/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 14.8 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-17S 6/23/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.09 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-17S 12/29/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.55 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-17S 6/17/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 2.3 <0.20 <0.30 6.96 <0.20 <1.0 <0.30 <10 <0.20 0.62 J
MW-18S 10/28/2015 18.6 <0.02 <1.0 <10 <1.0 110 <1.0 26.5 N <1.0 <5.0 12.7 <10 1.85 20.8
MW-18S 7/27/2016 59.0 <0.0196 <1.0 <10 <1.0 253 <1.0 28.3 <5.0 <1.0 <5.0 37.2 12.2 5.28 110
MW-18S 12/16/2016 4.68 <0.020 <1.0 <10 <1.0 8.0 <1.0 <1.0 <5.0 <1.0 <5.0 10.0 293 <1.0 6.56
MW-18S 6/28/2017 1.6 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 1.2 4.64 <0.20 <1.0 3.3 <10 <0.20 3.4
MW-18S 12/14/2017 30.0 <0.20 <0.20 9.5 <0.30 160 2.3 17 344 <0.20 8.0 25.0 <10 2.2 28.0
MW-18S 7/12/2018 1.5 <0.0026 <0.20 7.4 <0.30 1.5 <0.20 <0.30 181 <0.20 <1.0 11.0 <10 <0.20 21.0
MW-18S 1/11/2019 5.7 <0.0032 <0.20 4.4 <0.30 12.0 <0.20 1.3 15.8 <0.20 <1.0 5.1 <10 0.25 J 10.0
Page 6 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
AMW-18S 6/13/2019 <0.30 <0.0031 <0.20 2.7 0.65 J <0.20 <0.20 <0.30 102 <0.20 <1.0 4.7 <10 <0.20 2.0
AMW-18S 12/16/2019 <0.30 0.016 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 22 <0.20 <1.0 <0.30 <10 <0.20 <0.30
AMW-18S 6/23/2020 <0.30 <0.0030 <0.20 6.2 1.2 <0.20 0.51 J <0.30 177 <0.20 <1.0 18.0 26.0 <0.20 3.5
AMW-18S 12/28/2020 2.1 <0.0031 <0.20 12.0 1.2 0.67 J <0.20 16.0 103 <0.20 3.2 9.0 <10 <0.20 14.0
AMW-18S 6/17/2021 2.6 <0.0032 <0.20 4.0 <0.30 130 <0.20 0.58 J 132 <0.20 <1.0 11.0 <10 0.88 J 31.0
AMW-18S 6/22/2022 180 <0.0031 <0.20 68.0 5.2 1,700 <0.20 0.64 J 211 <0.20 <1.0 180 <10 21 340
AMW-18S 7/19/2023 4.3 <0.0032 <0.20 9.2 <0.30 870 <0.20 6.7 NM <0.20 <1.0 56.0 <10 2.4 57.0
DEM-MW6D 11/4/2003 N N 345 N N <1.0 <2.0 0.62 J N N <5.0 N N 0.62 J 2.7 J
DEM-MW6D 9/1/2004 N <2.0 262 J N N 3.0 <2.0 <2.0 N 281 <5.0 N 47,700 <2.0 <6.0
DEM-MW6D 3/8/2006 <200 <100 252 <500 <100 <100 <100 <100 N 214 <500 <200 45,100 <100 <300
DEM-MW6D 5/26/2011 <10 <10 140 <10 <10 <10 <10 <10 N 300 <20 <10 53,000 <10 <30
DEM-MW6D 9/6/2012 <1.0 <1.0 1.3 <1.0 <1.0 <1.0 <1.0 <1.0 N 5.1 <2.0 4.1 290 <1.0 <3.0
DEM-MW6D 11/29/2012 N N N N N N N N N N N N 57900 F N N
DEM-MW6D 10/29/2015 <1.0 <0.0204 6.76 <10 <1.0 <1.0 <1.0 <1.0 N 24.7 <5.0 <5.0 1,670 <1.0 <3.0
DEM-MW6D 7/20/2016 <1.0 <0.0207 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 2.64 <5.0 <5.0 <10 <1.0 <3.0
DEM-MW6D 12/16/2016 <1.0 <0.0194 71.2 <10 <1.0 <1.0 <1.0 <1.0 1.96 J 374 <5.0 <5.0 26,600 <1.0 <3.0
DEM-MW6D 7/6/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 2.2 <1.0 <0.30 <10 <0.20 <0.30
DEM-MW6D 12/14/2017 <0.30 <0.20 1.4 <1.0 <0.30 <0.20 <0.20 <0.30 34.4 16.0 <1.0 <0.30 420 <0.20 <0.30
DEM-MW6D 7/9/2018 <0.30 <0.0026 2.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 17.0 <1.0 <0.30 <10 <0.20 <0.30
DEM-MW6D 1/8/2019 <0.30 <0.0031 3.6 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 32.0 <1.0 <0.30 2,000 <0.20 <0.30
DEM-MW6D 6/12/2019 <0.30 <0.0031 3.7 <1.0 <0.30 <0.20 <0.20 <0.30 9.61 1.4 <1.0 <0.30 <10 <0.20 <0.30
DEM-MW6D 12/16/2019 <0.30 <0.0031 52.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.944 J 480 <1.0 <0.30 27,000 0.94 J 0.82 J
DEM-MW6D 6/23/2020 0.87 J <0.0031 34.0 <1.0 <0.30 0.36 J <0.20 0.41 J 2.83 480 <1.0 <0.30 18,000 <0.20 1.6
DEM-MW6D 12/28/2020 <0.30 <0.0032 29.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 470 <1.0 <0.30 47,000 <0.20 <0.30
DEM-MW6D 6/16/2021 <1.5 <0.0030 9.1 <5.0 <1.5 <1.0 <1.0 <1.5 1.02 310 <5.0 <1.5 9,000 <1.0 <1.5
DEM-MW6D 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 3.16 320 <1.0 <0.30 6,900 <0.20 <0.30
DEM-MW6D 7/19/2023 <0.30 <0.0032 <0.20 5.2 <0.30 <0.20 <0.20 <0.30 NM 400 <1.0 3.1 15,000 <0.20 <0.30
DEM-MW6I 11/7/2003 N N 118 N N <2.0 <2.0 <2.0 N N <5.0 N N <2.0 <6.0
DEM-MW6I 9/1/2004 N <2.0 99.3 J N N <1.0 <2.0 <2.0 N 54.1 <5.0 N 12,400 <2.0 <6.0
DEM-MW6I 2/22/2005 N <50 154 N N <50 N <50 N 58.1 N N 17,300 <50 <3.0
DEM-MW6I 3/8/2006 <2.0 <1.0 121 <5.0 <1.0 <1.0 <1.0 <1.0 N 67.7 <5.0 <2.0 19,400 <1.0 <3.0
DEM-MW6I 5/26/2011 <5.0 <5.0 130 <5.0 <5.0 <5.0 <5.0 <5.0 N 150 <10 <5.0 31,000 <5.0 1<5.0
DEM-MW6I 9/6/2012 1.2 <1.0 14 <1.0 <1.0 <1.0 <1.0 0.36 J N 0.88 J <2.0 3.5 500 <1.0 1.7 J
DEM-MW6I 10/29/2015 <1.0 N 118 <10 <1.0 <1.0 <1.0 <1.0 N 131 <5.0 <5.0 17,400 <1.0 <3.0
DEM-MW6I 7/20/2016 <20 <0.020 106 <200 <20 <20 <20 <20 <5.0 142 <100 <100 30,900 <20 60.0 U
DEM-MW6I 12/16/2016 <10 <0.0197 119 <100 <10 <10 <10 <10 2.80 J 124 <50 <50 16,300 <10 30.0 U
DEM-MW6I 7/6/2017 <0.30 <0.20 96 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 130 <1.0 <0.30 21,000 <0.20 <30
DEM-MW6I 12/14/2017 <1.5 <1.0 120 <5.0 <1.5 <1.0 <1.0 <1.5 <0.0900 140 <5.0 <1.5 18,000 <1.0 <1.5
DEM-MW6I 7/12/2018 <1.5 <0.0026 140 <5.0 <1.5 <1.0 <1.0 <1.5 1.89 190 <5.0 <1.5 14,000 <1.0 <1.5
Page 7 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
DEM-MW6I 1/7/2019 <0.30 <0.0032 120 <1.0 <0.30 <0.20 <0.20 <0.30 <0.180 230 <1.0 <0.30 14,000 <0.20 <0.30
DEM-MW6I 6/12/2019 0.98 J <0.0031 79 2.9 <0.30 <0.20 <0.20 <0.30 3.42 170 <1.0 <0.30 20,000 <0.20 1.1
DEM-MW6I 12/16/2019 <0.30 <0.0032 92 <1.0 <0.30 <0.20 <0.20 <0.30 1.04 280 <1.0 <0.30 27,000 <0.20 <0.30
DEM-MW6I 6/23/2020 <0.30 <0.0031 100 <1.0 <0.30 <0.20 <0.20 <0.30 1.78 210 <1.0 1.7 25,000 <0.20 <0.30
DEM-MW6I 12/28/2020 <0.30 <0.0032 90 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 260 <1.0 <0.30 35,000 <0.20 <0.30
DEM-MW6I 6/16/2021 <3.0 <0.0030 100 <10.0 <3.0 <2.0 <2.0 <3.0 8.13 230 <10.0 <3.0 30,000 <2.0 <3.0
DEM-MW6I 6/22/2022 <0.30 <0.0031 110 <1.0 <0.30 <0.20 <0.20 <0.30 2.74 160 <1.0 <0.30 3,400 <0.20 <0.30
DEM-MW6I 7/19/2023 <0.30 <0.0032 140 <1.0 <0.30 <0.20 <0.20 <0.30 NM 260 <1.0 <0.30 27,000 <0.20 <0.30
DEM-MW6R 8/5/2003 N N <100 23.0 N 2,820 <100 488 N N <50 101 N 530 2,260
DEM-MW6R 9/1/2004 N <40 11.7 J N N 876 <40 154 N <40 <50 N <400 54.8 401
DEM-MW6R 3/8/2006 136 <10 <10 31.4 J <10 295 <10 97.1 N <10 12.4 J 105 1,820 15.4 294
DEM-MW6R 5/26/2011 21.0 <1.0 <1.0 19.0 1.9 82.0 <1.0 18.0 N 7.1 <2.0 27 4,800 2.9 17.0
DEM-MW6R 9/6/2012 9.1 <1.0 <1.0 17.0 <1.0 56.0 <1.0 15.0 N <1.0 <2.0 27 2,300 1.4 7.3
DEM-MW6R 10/29/2015 <1.0 <0.020 2.29 <10 <1.0 6.58 <1.0 <1.0 N 7.88 <5.0 6.43 3,060 <1.0 <3.0
DEM-MW6R 7/20/2016 <5.0 <0.0196 <5.0 <50 <5.0 32.1 <5.0 <5.0 <5.0 10.2 <25.0 <25.0 5,160 5.46 15.0 U
DEM-MW6R 12/16/2016 <5.0 <0.0196 <5.0 <50 <5.0 22.4 <5.0 <5.0 <5.0 9.74 <25.0 <25.0 5,820 <5.0 15.0 U
DEM-MW6R 6/28/2017 2.1 <0.20 4.0 <1.0 <0.30 3.4 <0.20 <0.30 173 10.0 <1.0 2.9 4,000 <0.20 <0.30
DEM-MW6R 12/14/2017 <0.30 <0.20 1.5 8.0 <0.30 7.3 <0.20 1.4 1,010 6.4 4.7 9.6 1,900 <0.20 <0.30
DEM-MW6R 7/12/2018 3.3 <0.0026 <0.20 <1.0 <0.30 34.0 <0.20 2.3 389 8.5 <1.0 7.5 2,000 1.0 14.0
DEM-MW6R 1/8/2019 0.39 J <0.0031 5.9 1.8 <0.30 2.7 <0.20 0.54 J 17.3 14.0 <1.0 3.5 3,300 <0.20 0.38 J
DEM-MW6R 6/12/2019 7.1 <0.0031 3.3 14.0 0.86 J 15.0 <0.20 3.9 242 19.0 <1.0 28.0 3,400 0.79 J 17.0
DEM-MW6R 12/17/2019 0.57 J <0.0031 4.6 8.3 <0.30 8.8 <0.20 <0.30 194 17.0 <1.0 10.0 3,900 0.42 J 2.8
DEM-MW6R 6/23/2020 1.3 <0.0031 3.6 11.0 0.55 J 8.2 <0.20 6.5 270 15.0 <1.0 15.0 2,800 0.49 J 2.2
DEM-MW6R 12/28/2020 0.88 J <0.0032 5.1 15.0 4.2 8.4 0.86 J 8.4 293 20.0 <1.0 16.0 4,000 0.31 J 1.6
DEM-MW6R 6/16/2021 27.0 <0.0030 5.0 J 25.0 <3.0 5.6 J <2.0 6.1 J 396 17.0 <10.0 5.9 J 5,300 3.9 J <3.0
DEM-MW6R 6/22/2022 11.0 <0.0031 <0.20 <1.0 1.8 42.0 <0.20 26 397 24 <1.0 46.0 2,800 0.81 J 10.0
DEM-MW6R 7/19/2023 0.97 J <0.0032 < 0.20 17.0 <0.30 14.0 <0.20 0.63 J NM 31 <1.0 19.0 5,800 <0.20 1.4 J
FMW-15 6/26/1995 N N N N N 0.0 N 0.0 N 0.0 N 0.0 N 0.0 0.0
FMW-15 3/25/1999 N N N N N 0.0 N N N N N N N N N
FMW-15 7/15/1999 N N N N N 0.0 N N N N N N N N N
FMW-15 1/17/2000 N N N N N 0.0 N N N N N N N N N
FMW-15 3/28/2000 N N N N N 0.0 N N N N N N N N N
FMW-15 8/11/2000 N N N N N 0.0 N N N N N N N N N
FMW-15 10/29/2001 N N N N N 0.0 N N N N N N N N N
FMW-15 3/21/2003 N N N N N 0.0 N N N N N N N N N
FMW-15 11/2/2015 1.65 <0.0200* <1.0 10.9 <1.0 <1.0 <1.0 1.62 N <1.0 <5.0 9.02 <10 <1.0 5.16
FMW-15 12/15/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FMW-15 12/18/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 0.93 J <0.20 <0.30 <0.0900 <0.20 <1.0 0.88 J <10 <0.20 <0.30
FMW-15 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 8 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
FMW-15 12/12/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-15 6/24/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-15 12/17/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-15 6/16/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-15 6/22/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-15 2/27/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-15 7/20/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-19 6/26/1995 N N N N N 0.0 N 0.0 N 0.0 N 0.0 N 0.0 0.0
FMW-19 8/6/2003 N N <2.0 <5.0 N <1.0 <2.0 <2.0 N N <5.0 <5.0 N 1.0 J <6.0
FMW-19 11/10/2015 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
FMW-19 8/2/2016 <1.0 <0.0194 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FMW-19 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FMW-19 6/30/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.20 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-19 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.20 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-19
FMW-20 6/26/1995 N N N N N 0.0 N 0.0 N 0.0 N 0.0 N 0.0 0.0
FMW-20 8/6/2003 N N <2.0 <5.0 N <1.0 <2.0 <2.0 N N <5.0 <5.0 N <2.0 <6.0
FMW-20 3/7/2006 <2.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <2.0 <20 <1.0 <3.0
FMW-20 10/30/2015 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 86.9 <1.0 <3.0
FMW-20 8/3/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FMW-20 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FMW-20 6/30/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.20 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-20 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.20 <0.0900 <0.20 <1.0 <0.30 51 <0.20 <0.30
FMW-20 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.20 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-20 1/9/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 0.70 J <0.20 <0.20 0.439 J <0.20 <1.0 <0.30 <10 <0.20 0.38 J
FMW-20 6/14/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-20 12/18/2019 <0.30 0.042 P <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-21 6/26/1995 N N N N N 0.0 N 0.0 N 0.0 N 1.8 N 5.8 0.0
FMW-21 12/30/1998 0.0 N 8.2 0.0 N 0.0 N 0.0 N 1.1 N 3.1 N 0.0 N
FMW-21 10/13/1999 0.0 N 14.9 N N 0.0 N 0.0 N 1.4 N 16.4 N 0.0 N
FMW-21 10/13/2000 0.0 N 17 N 3.7 0.0 N 0.0 N 0.0 N 10.1 N 0.0 N
FMW-21 10/18/2001 0.0 N 18.2 N 0.0 N N 0.0 N 1.6 N 0.0 N 0.0 N
FMW-21 10/29/2015 <1.0 N <1.0 <10 <1.0 <1.0 <50 <1.0 N 34.7 <50 <5.0 11,300 <1.0 <3.0
FMW-21 8/3/2016 <1.0 <0.020 5.45 <10 <1.0 <1.0 <1.0 <1.0 <5.0 33.2 <5.0 <5.0 8,290 <1.0 <3.0
FMW-21 12/15/2016 <1.0 <0.020 3.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 41.7 <5.0 <5.0 5,590 F1 <1.0 <3.0
FMW-21 7/6/2017 <0.30 <0.20 17.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 24.0 <1.0 <0.30 6,300 <0.20 <0.30
FMW-21 12/15/2017 <0.30 <0.20 1.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 35.0 <1.0 <0.30 12,000 <0.20 <0.30
FMW-21 7/12/2018 <0.30 <0.0027 2.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 32.0 <1.0 <0.30 7,000 <0.20 <0.30
FMW-21 1/10/2019 <0.30 <0.0031 4.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.450 59.0 <1.0 <0.30 7,500 <0.20 <0.30
Abandonded in December 2018
Page 9 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
FMW-21 6/13/2019 0.51 J <0.0031 3.6 <1.0 <0.30 <0.20 <0.20 <0.30 2.75 42.0 <1.0 <0.30 11,000 <0.20 0.77 J
FMW-21 12/18/2019 <0.30 <0.0031 1.8 <1.0 <0.30 <0.20 <0.20 <0.30 0.571 J 48.0 <1.0 <0.30 <10 <0.20 <0.30
FMW-21 6/23/2020 <0.30 <0.0031 3.1 <1.0 <0.30 <0.20 <0.20 <0.30 0.589 J 47.0 <1.0 <0.30 9,600 <0.20 <0.30
FMW-21 12/28/2020 <0.30 <0.0032 2.2 <1.0 3.6 1.8 <0.20 <0.30 <0.0900 59.0 <1.0 <0.30 16,000 <0.20 <0.30
FMW-21 6/16/2021 <1.5 <0.0030 2.8 J <5.0 <1.5 <1.0 <1.0 <1.5 <0.0900 57.0 <5.0 <1.5 9,400 <1.0 <1.5
FMW-21 12/28/2021 <3.0 <0.0031 <2.0 <10.0 <3.0 <2.0 <2.0 <3.0 <0.0900 77.0 <10.0 <3.0 14,000 <2.0 <3.0
FMW-21 6/22/2022 <0.30 <0.0032 1.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 67.0 <1.0 <0.30 3,800 <0.20 <0.30
FMW-21 12/5/2022 <0.30 <0.0031 2.2 <1.0 <0.30 <0.20 <0.20 <0.30 NA 82.0 <1.0 <0.30 3,900 <0.20 <0.30
FMW-21 2/27/2023 <0.30 <0.0031 2.1 <1.0 <0.30 <0.20 <0.20 <0.30 NA 59 <1.0 <0.30 4,500 <0.20 <0.30
FMW-21 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM 95 <1.0 <0.30 7,200 <0.20 <0.30
FMW-21 12/6/2023 270 <0.0031 9.8 110 <0.30 14 <0.20 100 260 29 <1.0 73 1,100 3.8 370
FMW-22 6/26/1995 N N N N N <5.0 N <1.0 N <1.0 N <5.0 N <1.0 <3.0
FMW-22 11/10/2015 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
FMW-22 8/3/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FMW-22 12/13/2016 <1.0 <0.020 <1.0 <10* <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FMW-22 6/29/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 1/26/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 7/13/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 1/10/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 12/19/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 6/22/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 12/29/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 6/17/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 6/22/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-22 7/19/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-23R 8/6/2003 N N <100 68.0 N 5,830 <100 934 N N <50 213 N 1,940 4,080
FMW-23R 3/8/2006 324 <10 <10 60.2 <10 5,280 <10 304 N <10 <50 201 <200 134 1,370
FMW-23R 9/7/2012 170 <5.0 <5.0 41.0 <5.0 1,800 <5.0 270 N <5.0 <10 71.0 <50 32.0 200
FMW-23R 11/11/2015 143 <0.020 <1.0 <100 2.11 1,850 <1.0 223 N <1.0 <5.0 80.5 <100 23.2 199
FMW-23R 7/26/2016 77.6 <0.0200 <1.0 <10 <1.0 204 <1.0 186 <5.0 <1.0 <5.0 45.3 <10*22.9 *84.9
FMW-23R 12/16/2016 72.1 <0.020 <1.0 12.4 1.53 702 F1 <1.0 <1.0 3.21 J <1.0 <5.0 56.1 <10 3.45 94.7
FMW-23R 7/6/2017 37 <1.0 <1.0 <5.0 3.5 1,800 <1.0 140 1,830 <1.0 <5.0 56.0 <50 16.0 160
FMW-23R 12/14/2017 16 <1.0 <1.0 <5.0 <1.5 970 <1.0 97.0 2,060 <1.0 <5.0 35.0 <50 14.0 110
FMW-23R 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 35.0 <0.20 <0.30 153 <0.20 <1.0 2.2 <10 1.2 4.9
FMW-23R 1/9/2019 1.8 <0.0032 <0.20 7.3 1.0 9.2 <0.20 1.5 11.3 <0.20 <1.0 10.0 <10 0.68 J 12.0
FMW-23R 6/13/2019 10.0 <0.0031 <0.20 2.6 0.74 J 24.0 <0.20 19 119.0 <0.20 <1.0 7.5 <10 0.62 J 7.1
FMW-23R 12/17/2019 7.8 <0.0031 <1.0 <5.0 <1.5 1,100 <1.0 8.8 1,260 <1.0 <5.0 21.0 <50 9.4 23.0
FMW-23R 6/23/2020 5.2 <0.0031 <0.20 <1.0 0.33 J 85.0 <0.20 13.0 101 <0.20 <1.0 4.4 <10 1.2 5.2
Page 10 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
FMW-23R 12/28/2020 0.62 J <0.0031 5.6 <1.0 <0.30 190 <0.20 8.1 590 <0.20 <1.0 4.7 <10 1.5 9.0
FMW-23R 6/17/2021 3.0 <0.0032 <0.20 2.4 <0.30 29.0 <0.20 37.0 90.6 <0.20 <1.0 3.4 <10 0.90 J 5.8
FMW-23R 6/22/2022 1.0 <0.0030 <0.20 2.3 <0.30 200 <0.20 17.0 347 <0.20 <1.0 21.0 <10 4.3 11.0
FMW-23R 7/19/2023 <0.30 <0.0032 <0.20 4.4 <0.30 4.9 <0.20 9.8 NM <0.20 <1.0 6.1 <10 <0.20 2.1 J
FMW-24 6/26/1995 N N N N N 22,000 N 3,000 N 0.0 N 1,900 N 23,000 14,300
FMW-24 8/6/2003 N N <100 146 N 9,600 <100 2,090 N N <50 435 N 5,010 9,670
FMW-24 9/1/2004 N <400 <400 N N 12,300 <400 1,620 N <400 <1,000 N 4000 U 3,590 7,110
FMW-24 5/25/2011 1,600 <50 190 200 28 J 7,700 <50 1,300 N <50 <100 290 420 J 560 8,000
FMW-24 9/6/2012 1,600 <5.0 <5.0 140 <5.0 8,400 <5.0 1,600 N <5.0 <10 480 1,000 590 8,100
FMW-24 11/10/2015 1,690 <0.0198 <1.0 <500 13 6,300 <1.0 1,410 NA 2.03 <5.0 479 <500 318 7,260
FMW-24 7/25/2016 1,670 <0.0200 <1.0 280 12.7 4,240 <1.0 969 63.9 <1.0 <5.0 604 1,390 349 6,630
FMW-24 12/27/2016 1,360 <0.0197 <5.0 430 36.3 6,120 <5.0 1,430 147 <5.0 <25.0 747 <50 373 6,070
FMW-24 7/6/2017 490 <1.0 <1.0 230 14.0 3,900 <1.0 940 2,230 <1.0 <5.0 460 1,200 300 7,300
FMW-24 7/13/2018 1,900 <0.0026 <3.0 560 <0.30 6,800 <2.0 1,100 6,130 <2.0 <10 790 <100 400 9,700
FMW-24 1/9/2019 2,400 <0.0032 <2.0 240 15 7,700 <2.0 1,600 489 <2.0 <10 750 1,700 410 8,400
FMW-24 6/12/2019 2,300 <0.0031 <0.20 140 9.6 5,200 <0.20 220 852 <0.20 <1.0 750 660 300 7,900
FMW-24 12/17/2019 1,800 <0.0031 <2.0 440 12 5,100 <2.0 1,500 1,740 <2.0 <10 650 <100 340 9,300
FMW-24 6/23/2020 1,200 <0.0031 110 170 8.8 4,600 <0.20 1,100 1,670 <0.20 <1.0 390 770 240 4,200
FMW-24 12/29/2020 2,100 <0.0032 <0.20 360 14.0 6,100 6.0 1,400 1,250 4.4 <1.0 550 840 340 5,900
FMW-24 6/16/2021 1,300 <0.0032 <0.20 150 <3.0 4,700 <2.0 610 1,500 <2.0 <10 560 1,100 300 4,400
FMW-24 12/28/2021 1,900 <0.0031 <2.0 840 20.0 8,000 <2.0 1,700 1,580 <2.0 <10.0 1,300 <100 340 5,000
FMW-24 6/21/2022 1,600 <0.0031 120 270 <3.0 4,500 <2.0 1,300 897 <2.0 <10 580 2,200 180 3,800
FMW-24 12/12/2022 1,100 < 0.0031 <10 95 < 15.0 5,500 <10 1,200 NA <10 <50 340 <500 91 3,100
FMW-24 2/27/2023 1,600 < 0.0031 <2.0 230 <3.0 3,600 <2.0 1,200 NA 22 <10.0 510 <100 130 3,900
FMW-24 7/19/2023 2,700 <0.0030 <0.20 560 33.0 7,100 <0.20 1,200 NM 3.3 <1.0 800 <10 250 5,100
FMW-24 12/6/2023 2,200 <0.0032 <4.0 370 <6.0 6,600 <4.0 1,400 NM <4.0 <20 680 <200 230 5,400
FMW-24D 11/5/2003 N N 21.0 N N 1.0 <2.0 3.1 N N <5.0 N N 0.95 J 16.0
FMW-24D 9/1/2004 N <2.0 24.1 4.8 U N <1.0 <2.0 <2.0 N 0.73 J <5.0 4.8 U 382 <2.0 <6.0
FMW-24D 5/25/2011 <1.0 <1.0 17.0 <1.0 <1.0 0.14 J <1.0 <1.0 N 0.79 J <2.0 <1.0 520 <1.0 <3.0
FMW-24D 9/6/2012 0.25 J <1.0 130 <1.0 <1.0 <1.0 <1.0 <1.0 N 290 <2.0 3.6 42,000 <1.0 <3.0
FMW-24D 11/2/2015 <1.0 <0.0198*12.8 <10 <1.0 <1.0 <1.0 <1.0 N 1.19 <5.0 <5.0 522 <1.0 <3.0
FMW-24D 7/25/2016 <1.0 <0.020 10.7 <10 <1.0 <1.0 <1.0 <1.0 <5.0 1.11 <5.0 <5.0 864 <1.0 <3.0
FMW-24D 12/16/2016 <1.0 <0.020 8.58 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 341 <1.0 <3.0
FMW-24D 7/6/2017 <0.30 <0.20 8.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.88 <1.0 <0.30 390 <0.20 <0.30
FMW-24D 12/14/2017 <0.30 <0.20 10.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.87 <1.0 <0.30 330 <0.20 <0.30
FMW-24D 7/12/2018 <0.30 <0.0026 11.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.0 <1.0 <0.30 310 <0.20 <0.30
FMW-24D 1/10/2019 2.0 <0.0031 2.1 <1.0 <0.30 7.6 <0.20 0.91 J 2.85 0.33 J <1.0 1.6 50.0 0.26J 3.7
FMW-24D 6/12/2019 <0.30 <0.0031 6.8 <1.0 <0.30 <0.20 <0.20 <0.30 8.28 0.93 J <1.0 <0.30 <10 <0.20 <0.30
FMW-24D 12/17/2019 <0.30 <0.0032 7.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 320 <0.20 <0.30
Page 11 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
FMW-24D 6/23/2020 <0.30 <0.0031 7.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.99 J <1.0 <0.30 250 <0.20 <0.30
FMW-24D 12/29/2020 <0.30 <0.0032 6.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.97 J <1.0 <0.30 240 <0.20 <0.30
FMW-24D 6/16/2021 <0.30 <0.0032 6.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.95 J <1.0 <0.30 270 <0.20 <0.30
FMW-24D 6/21/2022 <0.30 0.045 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 26 <0.20 <0.30
FMW-24D 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-24I 11/7/2003 N N 42.0 N N <1.0 <2.0 <2.0 N N <5.0 N N <2.0 <6.0
FMW-24I 9/1/2004 N <2.0 55.1 4.8 U N <1.0 <2.0 <2.0 N <2.0 <5.0 4.8 U 237 <2.0 <6.0
FMW-24I 5/25/2011 <1.0 <1.0 46.0 <1.0 <1.0 <1.0 <1.0 <1.0 N 0.5 J <2.0 <1.0 450 <1.0 <3.0
FMW-24I 11/2/2015 <1.0 N 5.11 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 101 <1.0 <3.0
FMW-24I 7/25/2016 <1.0 <0.0198 10.6 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 162 <1.0 <3.0
FMW-24I 12/14/2016 <1.0 <0.020 19.5 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 233 <1.0 <3.0
FMW-24I 6/30/2017 <0.30 <0.20 15.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 230 <0.20 <0.30
FMW-24I 12/14/2017 <0.30 <0.20 32.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.51 1.1 <1.0 <0.30 390 <0.20 <0.30
FMW-24I 7/12/2018 <0.30 <0.0027 21.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.78 <1.0 <0.30 240 <0.20 <0.30
FMW-24I 1/10/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-24I 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.338 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-24I 12/19/2019 <0.30 0.010 JP 1.1 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-24I 6/23/2020 <0.30 <0.0031 5.8 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.34 J <1.0 1.8 16.0 <0.20 <0.30
FMW-24I 12/29/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-24I 6/16/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 0.68 J <0.20 0.33 J 1.48 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-24I 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FMW-24I 7/19/2023 120 <0.0031 <0.20 37.0 <0.30 5.6 <0.20 12 NM <0.20 <1.0 53.0 <10 0.54 J 43.0
FPZ-5 6/26/1995 N N N N N 0.0 N 0.0 N 0.0 N 0.0 N 0.0 0.0
FPZ-5 12/30/1998 0.0 N 0.0 0.0 N 0.0 N 0.0 N 0.0 N 0.0 N 0.0 N
FPZ-5 8/6/2003 N N <2.0 <5.0 N <1.0 <2.0 <2.0 N N <5.0 <5.0 N <2.0 <6.0
FPZ-5 3/6/2006 <2.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <2.0 <20 <1.0 <3.0
FPZ-5 11/12/2015 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-5 7/21/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-5 12/14/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-5 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.325 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-5 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-5 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-5 1/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-5 6/14/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-5 12/19/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-6 8/25/1997 N N N N N 0.0 N 0.0 N N N N N 0.0 0.0
FPZ-6 3/7/2006 <2.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <2.0 <20 <1.0 <3.0
FPZ-6 11/11/2015 <1.0 <0.0200 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
Page 12 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
FPZ-6 7/22/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 126 <1.0 <3.0
FPZ-6 12/15/2016 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-6 6/29/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-6 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-6 7/13/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-6 1/11/2019 0.98 J <0.0031 <0.20 3.6 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 1.1 <10 <0.20 <0.30
FPZ-6 6/14/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-6 12/16/2019 <0.30 0.0059 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-7 9/2/2004 N <2.0 <2.0 N N <1.0 <2.0 <2.0 N <2.0 <5.0 N <20 <2.0 <6.0
FPZ-7 7/26/2016 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10* <1.0* <3.0
FPZ-7 12/14/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-7 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.33 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-7 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.01 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-7 7/13/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-7 1/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-7 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.603 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-7 12/18/2019 0.75 J <0.0031 <0.20 3.7 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 0.54 J <10 <0.20 0.65 J
FPZ-8 8/25/1997 N N N N N 0.9 N 0.0 N N N N N 0.0 0.0
FPZ-8 8/6/2003 N N <5.0 45.0 N 36.0 <5.0 91 N N <3.0 68.0 N 84.0 410
FPZ-8 9/2/2004 N <10 <10 N N 409 <10 295 N <10 <5.0 N <100 252 964
FPZ-8 3/6/2006 483 <10 <10 104 7.4 J 42.1 <10 156 N <10 <50 163 <200 36.3 611
FPZ-8 9/7/2012 55 <1.0 <1.0 34.0 <1.0 1.2 <1.0 10 N <1.0 <2.0 16.0 <10 0.36 J 20
FPZ-8 10/29/2015 7.51 <1.0 <1.0 <10 <1.0 <1.0 <1.0 1.14 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-8 7/22/2016 <1.0 <0.0198 <1.0 <10 1.26 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 19.1 <1.0 <3.0
FPZ-8 12/14/2016 2.87 <0.020 <1.0 <10 1.13 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 273 <1.0 <3.0
FPZ-8 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.909 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-8 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-8 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.291 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-8 1/10/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-8 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.592 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-8 12/16/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-10 5/25/2011 <1.0 <1.0 64.0 <1.0 <1.0 <1.0 <1.0 <1.0 N 19.0 <2.0 <1.0 5,100 <1.0 <3.0
FPZ-10 9/7/2012 320 <1.0 <1.0 200 9.8 120 <1.0 140 N <1.0 <2.0 190 <10 1.2 340
FPZ-10 12/28/2016 353 <0.0199 <1.0 119 7.97 147 <1.0 266 <5.0 <1.0 <5.0 345 <10 6.44 478
FPZ-10 6/27/2017 580 <2.0 <2.0 110 <0.30 57.0 <2.0 140 654 <2.0 <10 210 <100 <2.0 470
FPZ-10 7/13/2018 350 <0.0026 <0.20 110 9.7 1,200 <0.20 48.0 914 <0.20 <1.0 350 <10 20.0 620
FPZ-10 1/11/2019 120 <0.0032 <0.20 29.0 6.6 3.2 <0.20 <0.30 20.3 <0.20 <1.0 45.0 <10 <0.20 85.0
FPZ-10 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 1.8 <0.20 <0.30 101 <0.20 <1.0 <0.30 <10 <0.20 1.4
FPZ-10 12/17/2019 <3.0 <0.0031 120 <10.0 <3.0 <2.0 <2.0 <3.0 <0.450 <2.0 <10.0 <3.0 1,200 <2.0 <3.0
Page 13 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
FPZ-10 6/24/2020 4.9 <0.0031 <0.20 5.6 <0.30 4.7 <0.20 0.47 J 148 <0.20 <1.0 3.9 <10 <0.20 29.0
FPZ-10 12/29/2020 100 <0.0032 <0.20 35.0 9.6 5.7 2.1 0.52 J 68.6 <0.20 <1.0 30.0 <10 <0.20 39.0
FPZ-10 6/17/2021 2.9 <0.0032 <0.20 3.3 <0.30 5.3 <0.20 0.88 J 89.2 <0.20 <1.0 6.3 <10 <0.20 18.0
FPZ-10 6/22/2022 72.0 <0.0031 <0.20 <1.0 11 12.0 <0.20 13 298 <0.20 <1.0 24.0 <10 <0.20 41.0
FPZ-10 7/20/2023 20.0 <0.0031 <0.20 6.4 <0.30 4.1 <0.20 1.5 NM <0.20 <1.0 8.1 <10 <0.20 4.1
FPZ-10I 11/7/2003 N N 54.0 N N <1.0 <2.0 <2.0 N N <5.0 N N <2.0 <6.0
FPZ-10I 9/1/2004 N <2.0 68.6 N N <1.0 <2.0 <2.0 N <2.0 <5.0 N 3,780 <2.0 <6.0
FPZ-10I 3/7/2006 <10 <5.0 55.0 <5.0 <5.0 <5.0 <5.0 <5.0 N 12.2 5.6 J <10 4,660 <5.0 1<5.0
FPZ-10I 5/25/2011 500 <10 <10 78.0 19.0 290 <10 260 N <10 <20 230 <100 5.8 J 610
FPZ-10I 9/7/2012 3.5 <1.0 60.0 <1.0 <1.0 <1.0 <1.0 0.47 J NA 21.0 <2.0 4.0 5,400 <1.0 1.4 J
FPZ-10I 10/29/2015 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <20 <1.0 N 21.3 <100 <5.0 3,900 <1.0 <3.0
FPZ-10I 7/27/2016 <1.0 <0.0196 56.2 <10 <1.0 <1.0 <1.0 <1.0 <5.0 19.3 <5.0 <5.0 3,750 <1.0 <3.0
FPZ-10I 12/16/2016 <1.0 <0.0194 62.3 <10 <1.0 <1.0 <1.0 <1.0 <5.0 23.5 <5.0 <5.0 5,320 <1.0 <3.0
FPZ-10I 6/28/2017 <0.30 <0.20 72.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.428 25.0 <1.0 <0.30 6,000 <0.20 <0.30
FPZ-10I 12/15/2017 <0.30 <0.20 37.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 12.0 <1.0 <0.30 2,800 <0.20 <0.30
FPZ-10I 7/12/2018 <0.30 <0.0026 5.3 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-10I 1/11/2019 <0.30 <0.0031 54.0 2.7 <0.30 <0.20 <0.20 <0.30 <0.0900 19.0 <1.0 0.83 J 3,800 <0.20 <0.30
FPZ-10I 6/12/2019 <0.30 <0.0031 22.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.3 <1.0 <0.30 <10 <0.20 <0.30
FPZ-10I 12/16/2019 <0.30 0.0085 JP 60.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 27.0 <1.0 <0.30 3,300 <0.20 <0.30
FPZ-10I 6/23/2020 <0.30 <0.0030 37.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.838 J 13.0 <1.0 <0.30 2,200 <0.20 <0.30
FPZ-10I 12/28/2020 <0.30 <0.0032 63.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 33.0 <1.0 <0.30 7,400 <0.20 <0.30
FPZ-10I 6/17/2021 1.3 <0.0032 9.7 <1.0 <0.30 <0.20 <0.20 0.73 J <0.0900 0.58 J <1.0 0.92 J <10 <0.20 1.0
FPZ-10I 6/22/2022 <0.30 0.024 19 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-10I 7/19/2023 <0.30 <0.0032 4.2 <1.0 <0.30 <0.20 <0.20 <0.30 NM 1.8 <1.0 <0.30 190 <0.20 <0.30
FPZ-11 12/30/1998 0.0 N 0.0 0.0 N 0.0 N 0.0 N 0.0 N 0.0 N 0.0 N
FPZ-11 9/1/2004 N <2.0 <2.0 4.8 U N 2.8 <2.0 <2.0 N <2.0 <5.0 4.8 U <20 0.69 J 1.5 J
FPZ-11 3/7/2006 <2.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <2.0 <20 <1.0 <3.0
FPZ-11 5/25/2011 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <2.0 <1.0 <10 <1.0 <3.0
FPZ-11 10/30/2015 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-11 7/25/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-11 12/15/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 109 <1.0 <3.0
FPZ-11 7/6/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-11 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-11 7/13/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-11 1/9/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-11 6/14/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-11 12/19/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12 8/6/2003 N N <2.0 <5.0 N <1.0 <2.0 <2.0 N N <5.0 <5.0 N <2.0 <6.0
Page 14 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
FPZ-12 9/1/2004 N <2.0 <2.0 4.8 U N <1.0 <2.0 <2.0 N <2.0 <5.0 4.8 U <20 <2.0 <6.0
FPZ-12 3/6/2006 <2.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <2.0 <20 <1.0 <3.0
FPZ-12 5/25/2011 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <2.0 <1.0 <10 <1.0 <3.0
FPZ-12 11/12/2015 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-12 7/21/2016 <1.0 <0.019 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-12 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-12 6/26/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12 7/11/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12 1/10/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12 6/14/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12 12/19/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12I 11/7/2003 N N <2.0 N N <1.0 <2.0 <2.0 N N <5.0 N N <2.0 <6.0
FPZ-12I 9/1/2004 N <2.0 <2.0 4.8 U N <1.0 <2.0 <2.0 N <2.0 <5.0 4.8 U <20 <2.0 <6.0
FPZ-12I 3/7/2006 <2.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <2.0 <20 <1.0 <3.0
FPZ-12I 5/25/2011 0.2 J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <2.0 <1.0 99 <1.0 <3.0
FPZ-12I 11/11/2015 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-12I 7/21/2016 <1.0 <0.0194 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-12I 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-12I 6/26/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12I 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12I 7/11/2018 <0.30 <0.021 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12I 1/10/2019 <0.30 0.027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12I 6/14/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-12I 12/19/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-13 9/2/2004 N <2.0 <2.0 N N 476.0 <2.0 171 N <2.0 <5.0 N <20 156 432
FPZ-13 3/6/2006 104 <5.0 <5.0 10.9 J 2.7 J 240.0 <5.0 80.7 N <5.0 7.0 J 51.6 <100 59.1 240
FPZ-13 10/29/2015 4.5 <1.0 <1.0 <10 <1.0 1.42 <1.0 3.35 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-13 7/22/2016 <1.0 <0.0200 <1.0 <10 <1.0 2.3 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-13 12/14/2016 4.86 <0.0198 <1.0 <10 <1.0 6.62 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 15.9
FPZ-13 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 1.0 <0.20 <0.30 7.46 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-13 12/14/2017 2.9 <0.20 <0.20 <1.0 <0.30 1.5 <0.20 3.5 23.5 <0.20 <1.0 <0.30 <10 <0.20 2.7
FPZ-13 7/12/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 11.0 <0.20 <0.30 53.0 <0.20 <1.0 <0.30 <10 <0.20 1.6
FPZ-13 1/10/2019 0.69 J <0.0031 <0.20 <1.0 <0.30 2.5 <0.20 1.1 1.78 <0.20 <1.0 1.0 <10 <0.20 <0.30
FPZ-13 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 5.75 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-13 12/17/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 0.43 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-13 6/24/2020 3.0 <0.0031 <0.20 1.3 0.75 J 8.9 <0.20 1.9 37.2 <0.20 <1.0 5.6 <10 <0.20 8.1
FPZ-13 12/29/2020 1.9 <0.0032 <0.20 3.7 <0.30 4.2 <0.20 1.4 13.6 <0.20 <1.0 3.0 <10 <0.20 1.8
FPZ-13 6/17/2021 3.0 <0.0032 <0.20 <1.0 0.51 J 1.9 <0.20 1.2 31.3 <0.20 <1.0 <0.30 <10 <0.20 4.5
Page 15 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
FPZ-14 8/6/2003 N N <2.0 <5.0 N 0 J <2.0 <2.0 N N <5.0 <5.0 N <2.0 <6.0
FPZ-14 9/2/2004 N <2.0 <2.0 N N <1.0 <2.0 <2.0 N <2.0 <5.0 N 14.9 J <2.0 <6.0
FPZ-14 3/6/2006 <2.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <2.0 16.5 J <1.0 <3.0
FPZ-14 10/28/2015 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-14 7/22/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-14 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-14 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-14 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.78 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-14 7/13/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-14 1/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-14 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.407 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-14 12/17/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-15 8/3/2016 9.39 <0.020 <1.0 <10 1.47 3.77 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-15 12/28/2016 <1.0 <0.0200 <1.0 15.4 1.07 1.92 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
FPZ-15 6/26/2017 0.92 <0.20 <0.20 <1.0 <0.30 0.67 <0.20 <0.30 9.34 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-15 12/14/2017 46 <1.0 <1.0 32.0 6.2 5.9 <1.0 4.7 23.2 <1.0 <5.0 <1.5 <50 <1.0 14
FPZ-15 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 4.5 1.2 <0.30 34.1 <0.20 <1.0 <0.30 <10 <0.20 2.3
FPZ-15 1/11/2019 0.88 J <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-15 6/13/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 2.15 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-15 12/16/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 1.8 <0.20 <0.30 7.20 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-15 6/23/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 2.98 <0.20 <1.0 <0.30 <10 <0.20 <0.30
FPZ-15 12/29/2020 2.4 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.67 <0.20 <1.0 <0.30 <10 <0.20 1.3
FPZ-15 6/17/2021 0.59 J <0.0032 <0.20 <1.0 0.69 J 2.1 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 0.72 J
OW-1 3/7/2006 <2.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <2.0 <20 <1.0 <3.0
OW-1 10/30/2015 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-1 8/3/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-1 12/14/2016 <1.0 <0.0200 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-1 7/7/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-1 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-1 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-1 1/9/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-1 6/14/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-1 12/18/2019 <0.30 0.014 JP <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-2 3/7/2006 150 <5.0 <5.0 26.6 10.2 7.6 <5.0 9.6 NA <5.0 6.2 J 11.2 <100 4.1 J 93.9
OW-2 10/28/2015 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-2 7/27/2016 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 1.2 <3.0
OW-2 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-2 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.09 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-2 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.13 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
Page 16 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
OW-2 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-2 1/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-2 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-2 12/16/2019 <0.30 0.0058 JP <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-3 3/7/2006 94.8 <1.0 <1.0 45.3 3.4 18.2 <1.0 38.0 N <1.0 <5.0 27.1 <20 2.8 141
OW-3 10/28/2015 <1.0 <0.0197 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-3 8/3/2016 <1.0 <0.0196 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10* <1.0 <3.0
OW-3 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 235 <1.0 <3.0
OW-3 7/6/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.338 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-3 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-3 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-3 1/10/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-3 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-3 12/16/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-4 3/7/2006 770 <10 <10 175 12.1 46.1 <10 130 N <10 <50 154 <200 34.5 806
OW-4 10/28/2015 <1.0 <0.0199* <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-4 7/26/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10* <1.0* <3.0
OW-4 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 1.23 J <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-4 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 119 <0.20 <1.0 <1.0 <0.10 <0.20 <0.30
OW-4 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.465 <0.20 <1.0 <0.30 100 <0.20 <0.30
OW-4 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-4 1/11/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-4 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-4 12/16/2019 <0.30 0.0067 JP <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-4 6/23/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 0.49 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 0.56 J <0.30
OW-4 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-5 3/7/2006 854 <10 <10 159 11.9 32.9 <10 165 N <10 <50 194 <200 30.0 990
OW-5 10/28/2015 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-5 7/27/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 1.67 <3.0
OW-5 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 1.26 J <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-5 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.775 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-5 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.542 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-5 7/12/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 0.36 <0.30
OW-5
OW-6 11/12/2015 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-6 8/2/2016 <1.0 <0.0198 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-6 12/27/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 40.8 <1.0 <3.0
OW-6 7/6/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
Abandonded in December 2018
Page 17 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
OW-6 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-6 7/12/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-6 1/10/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-6 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-6 12/16/2019 <0.30 0.0053 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-7 8/6/2003 N N <2.0 <5.0 N <1.0 5.0 <2.0 N N <5.0 <5.0 N <2.0 <6.0
OW-7 10/30/2015 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-7 8/3/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-7 12/15/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
OW-7 6/30/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <1.0 <0.10 <0.20 <0.30
OW-7 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 21.5 <0.20 <1.0 <0.30 <0.10 <0.20 <0.30
OW-7 7/12/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <1.0 <0.10 <0.20 <0.30
OW-7 1/9/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <1.0 <0.10 <0.20 <0.30
OW-7 6/14/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-7 12/18/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
OW-8 8/6/2003 N N 13.0 <5.0 N <1.0 2.0 <2.0 N N <5.0 <5.0 N <2.0 <6.0
OW-8 9/1/2004 N <2.0 14.9 N N <1.0 <2.0 <2.0 N 9.1 <5.0 N 2,220 <2.0 1.6 J
OW-8 3/7/2006 <2.0 <2.0 9.0 <5.0 <1.0 <1.0 <1.0 <1.0 N 4.9 <5.0 <2.0 1,320 <1.0 <3.0
OW-8 10/29/2015 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N 10.7 <5.0 <5.0 658 <1.0 <3.0
OW-8 7/22/2016 <1.0 <1.0 10.5 <10 <1.0 <1.0 <1.0 <1.0 <5.0 13.5 <5.0 <5.0 1,480 <1.0 <3.0
OW-8 12/14/2016 <1.0 <1.0 18 <10 <1.0 <1.0 <1.0 <1.0 1.29 J 17.9 <5.0 <5.0 1,310 <1.0 <3.0
OW-8 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.02 7.5 <1.0 <0.30 560 <0.20 <0.30
OW-8 12/14/2017 <0.30 <0.20 9.3 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 13.0 <1.0 <0.30 460 <0.20 <0.30
OW-8 7/12/2018 <0.30 <0.0026 6.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 9.2 <1.0 <0.30 790 <0.20 <0.30
OW-8 1/10/2019 <0.30 <0.0031 6.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 9.3 <1.0 <0.30 680 <0.20 <0.30
OW-8 6/12/2019 <0.30 <0.0031 1.7 <1.0 <0.30 <0.20 <0.20 <0.30 1.62 4.7 <1.0 <0.30 400 <0.20 <0.30
OW-8 12/18/2019 <0.30 <0.0031 9.1 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 17.0 <1.0 <0.30 1,600 <0.20 <0.30
OW-8 6/24/2020 <0.30 <0.0030 3.8 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 6.1 <1.0 <0.30 500 <0.20 <0.30
OW-8 12/28/2020 <0.30 <0.0031 4.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 8.2 <1.0 <0.30 170 <0.20 <0.30
OW-8 6/17/2021 <0.30 <0.0032 2.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 4.4 <1.0 <0.30 370 <0.20 <0.30
OW-8 6/23/2022 <0.30 <0.20 <0.20 <1.0 <0.30 0.54 J <0.20 <0.30 <0.0900 16 <1.0 <0.30 460.0 <0.20 <0.30
OW-8 7/19/2023 <0.30 <0.0031 5.7 <1.0 <0.30 <0.20 <0.20 <0.30 NM 16.0 <1.0 <0.30 930 <0.20 <0.30
RW-1 10/30/2015 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
RW-1 7/25/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
RW-1 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
RW-1 7/7/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-1 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-1 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-1 1/9/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 18 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
RW-1 6/14/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-1 12/20/2019 <0.30 0.0071 JP <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-2 10/29/2015 <1.0 <1.0 <1.0 <10 <1.0 <1.0 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
RW-2 7/27/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
RW-2 12/14/2016 <1.0 <0.0199 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
RW-2 6/27/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-2 12/13/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-2 7/12/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-2 1/11/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-2 6/13/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
RW-2 12/17/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-1R 8/5/2003 NA NA <40 153 NA 955 <40 201 NA NA <100 300 NA 556 635
SBMW-1R 8/31/2004 N <20 <20 N N 567 <20 67.7 N <20 <50 N <200 13 J 135
SBMW-1R 5/26/2011 9.5 <1.0 <1.0 150 3.0 200 <1.0 41.0 N <1.0 <2.0 140 <10 1.2 8.3
SBMW-1R 9/7/2012 4.3 <1.0 <1.0 150 5.3 150 <1.0 20.0 N <1.0 <2.0 85.0 <10 0.43 J 3.1
SBMW-1R 11/10/2015 3.66 <0.0200 <1.0 12.4 2.37 87.5 <1.0 14.2 N <1.0 <5.0 20.5 <10 <1.0 11.5
SBMW-1R 8/2/2016 3.88 <0.019 2.22 13.9 1.55 55.3 <1.0 <1.0 <5.0 <1.0 <5.0 28.8 <10 <1.0 6.9
SBMW-1R 12/28/2016 1.65 <0.020 <1.0 80.3 1.44 28.9 <1.0 1.37 <5.0 <1.0 <5.0 14.7 <10 <1.0 <3.0
SBMW-1R 7/7/2017 <0.30 <0.20 <0.20 10.0 <0.30 24.0 <0.20 1.1 70.0 <0.20 <1.0 9.7 <10 <0.20 1.6
SBMW-1R 12/13/2017 0.87 <0.20 2.6 16.0 1.3 35.0 <0.20 0.66 82.9 <0.20 <1.0 12.0 160 0.36 1.1
SBMW-1R 7/11/2018 <0.30 <0.0025 <0.20 <1.0 <0.30 42.0 <0.20 <0.30 40.2 <0.20 <1.0 <0.30 <10 <0.20 0.77
SBMW-1R 1/8/2019 0.57 J <0.0031 <0.20 2.1 <0.30 29.0 <0.20 1.2 18.5 <0.20 <1.0 5.1 34.0 <0.20 <0.30
SBMW-1R 6/13/2019 0.76 J <0.0031 <0.20 3.3 <0.30 <0.20 <0.20 <0.30 43.7 <0.20 <1.0 7.3 22.0 <0.20 2.1
SBMW-1R 12/12/2019 0.86 J <0.0031 1.4 8.4 0.86 J 10.0 <0.20 <0.30 49.9 <0.20 <1.0 5.8 87.0 0.32 J 1.00 J
SBMW-1R 6/23/2020 3.1 <0.0032 <0.20 12.0 0.68 J 17.0 <0.20 0.52 J 24.6 <0.20 <1.0 21.0 11.0 0.52 J 5.2
SBMW-1R 12/28/2020 210 <0.0031 <0.20 11.0 4.3 3.1 <0.20 120 33.0 <0.20 <1.0 31.0 <10 <0.20 100
SBMW-1R 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 1.8 <0.20 <0.30 23.0 <0.20 <1.0 1.0 <10 <0.20 1.7
SBMW-1R 6/20/2022 2.1 <0.20 <0.20 9.9 0.83 J 37.0 <0.20 2.2 57.3 <0.20 <1.0 22.0 <10 0.51 J 6.7
SBMW-1R 7/18/2023 <0.30 <0.0031 <0.20 14.0 <0.30 38.0 <0.20 1.8 NM <0.20 <1.0 26.0 <10 0.38 J 2.6 J
.
SBMW-2R 8/5/2003 N N <200 111 N 5,120 <200 649 N N <500 244 N 514 2,900
SBMW-2R 11/19/2007 120 0.15 <1.0 87.0 7.4 660 <1.0 130 N <1.0 <2.0 130 110 28.0 190
SBMW-2R 11/6/2008 61.0 <1.0 0.64 J 20.0 4.0 650 <1.0 130 N <1.0 <2.0 24.0 49.0 61.0 220
SBMW-2R 11/24/2009 46.0 <1.0 11.0 2.3 1.4 550 0.21 J 150 N <1.0 11.0 4.5 <20 62.0 200
SBMW-2R 3/10/2011 0.47 J <1.0 0.17 J 1.8 J 0.3 J 27.0 <1.0 4.2 N <1.0 <2.0 0.81 J <20 0.53 J 2.0 J
SBMW-2R 11/8/2011 2.2 <1.0 <1.0 <2.0 <1.0 82.0 <1.0 5.8 N <1.0 <2.0 <1.0 <10 2.6 5.7
SBMW-2R 9/6/2012 0.72 J <1.0 <1.0 <1.0 <1.0 80.0 <1.0 1.0 N <1.0 <2.0 <1.0 <10 1.2 <3.0
SBMW-2R 11/30/2012 1.1 <1.0 <1.0 <1.0 0.44 J <1.0 <1.0 6.5 N <1.0 <2.0 <1.0 <10 4.8 2.8 J
SBMW-2R 10/28/2015 <1.0 <0.020 <1.0 <10 <1.0 4.48 <1.0 <1.0 N <1.0 <5.0 <5.0 <10 <1.0 <3.0
SBMW-2R 8/2/2016 <1.0 <0.0198 <1.0 <10 <1.0 39.5 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 1.01 3.97
Page 19 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
SBMW-2R 12/14/2016 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 <10 <1.0 <3.0
SBMW-2R 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2R 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 0.82 <0.20 <0.30 0.344 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2R 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 2.87 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2R 12/18/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2R 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.67 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2R 12/17/2019 0.51 J <0.0031 <0.20 <1.0 <0.30 0.79 J <0.20 0.35 J <0.0900 <0.20 <1.0 <0.30 <10 <0.20 0.81 J
SBMW-2R 6/23/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.552 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2R 12/28/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 11 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2R 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 10.1 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2R 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 16.0 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2R 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2I 11/7/2003 N N 6.0 N N 16.0 <2.0 5.0 N N <5.0 N N 27.0 21.0
SBMW-2I 11/19/2007 <1.0 <0.0094 9.4 <2.0 <1.0 0.48 J <1.0 <1.0 N 0.46 J <2.0 <1.0 570 <1.0 <3.0
SBMW-2I 11/5/2008 <1.0 <1.0 11.0 <2.0 <1.0 0.69 J <1.0 <1.0 N 0.67 J <2.0 0.83 J 550 0.16 J <3.0
SBMW-2I 11/24/2009 0.16 J <1.0 10.0 0.2 J <1.0 1.6 <1.0 <1.0 N 0.52 J <2.0 0.4 J 520 0.15 J 0.4 J
SBMW-2I 3/9/2011 <1.0 <1.0 11.0 <2.0 <1.0 1.7 <1.0 <1.0 N 0.42 J <2.0 <1.0 630 0.15 J <3.0
SBMW-2I 11/8/2011 <1.0 <1.0 8.9 <2.0 <1.0 3.1 <1.0 <1.0 N <1.0 <2.0 <1.0 700 <1.0 <3.0
SBMW-2I 11/29/2012 <1.0 <1.0 8.3 <1.0 <1.0 0.23 J <1.0 <1.0 N 0.48 J <2.0 <1.0 520 2.7 <3.0
SBMW-2I 10/28/2015 <1.0 <0.0198*8.99 <10 <1.0 <1.0 <1.0 <1.0 N 1.84 <5.0 <5.0 760 <1.0 <3.0
SBMW-2I 7/28/2016 <1.0 <0.019 9.55 <10 <1.0 1.08 <1.0 <1.0 <5.0 1.04 <5.0 <5.0 509 <1.0 <3.0
SBMW-2I 12/16/2016 3.51 <0.020 9.69 <10 2.38 1.79 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 478 <1.0 <3.0
SBMW-2I 7/7/2017 <0.30 <0.20 8.8 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.77 <1.0 <0.30 490 <0.20 <0.30
SBMW-2I 12/12/2017 <0.30 <0.20 9.5 <1.0 <0.30 0.23 <0.20 <0.30 0.465 1.1 <1.0 <0.30 720 <0.20 <0.30
SBMW-2I 7/11/2018 <0.30 <0.0026 12.0 <1.0 <0.30 1.2 <0.20 <0.30 <0.0900 0.85 <1.0 <0.30 460 <0.20 <0.30
SBMW-2I 1/7/2019 <0.30 <0.0031 9.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.1 <1.0 <0.30 300 <0.20 <0.30
SBMW-2I 6/12/2019 <0.30 <0.0031 6.1 <1.0 <0.30 <0.20 <0.20 <0.30 0.851 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2I 12/17/2019 1.3 <0.0032 11.0 <1.0 <0.30 1.1 <0.20 0.71 J <0.0900 <0.20 <1.0 1.6 920 <0.20 2.8
SBMW-2I 6/23/2020 <0.30 <0.0030 5.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 16.0 <0.20 <0.30
SBMW-2I 12/28/2020 <0.30 <0.0032 13.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 5.2 <1.0 3.6 570 <0.20 <0.30
SBMW-2I 6/16/2021 <0.30 <0.0030 4.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.39 J <1.0 <0.30 <10 0.31 J <0.30
SBMW-2I 6/22/2022 <0.30 <0.0030 0.73 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2I 7/18/2023 <0.30 <0.0031 8.8 <1.0 <0.30 0.49 J <0.20 <0.30 NM <0.20 <1.0 <0.30 420 <0.20 <0.30
SBMW-2D 11/4/2003 N N 10.8 N N 62.3 <2.0 57.1 N N <5.0 N N 74.9 241
SBMW-2D 11/19/2007 4.3 <0.0094 5.7 5.3 0.89 J 1.6 <1.0 2.1 N <1.0 <2.0 3.4 600 0.68 J 3.6
SBMW-2D 11/6/2008 8.3 <1.0 3.0 1.9 J 1.4 2.4 <1.0 3.5 N 0.46 J <2.0 1.1 360 0.27 J 1.3 J
SBMW-2D 11/24/2009 0.64 J <1.0 8.6 0.42 J <1.0 0.39 J <1.0 0.37 J N 1.2 <2.0 <1.0 720 0.21 J 0.51 J
SBMW-2D 3/9/2011 <1.0 <1.0 7.0 <2.0 <1.0 0.25 J <1.0 <1.0 N 1.1 <2.0 0.52 J 1,100 0.27 J <3.0
SBMW-2D 11/8/2011 <1.0 <1.0 6.8 <2.0 <1.0 <1.0 <1.0 <1.0 N 1.0 <2.0 <1.0 <10 <1.0 <3.0
Page 20 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
SBMW-2D 11/29/2012 <1.0 <1.0 130 <1.0 <1.0 <1.0 <1.0 <1.0 N 310 <2.0 <1.0 680 <1.0 <3.0
SBMW-2D 10/28/2015 <1.0 <0.020 7.72 <10 <1.0 <1.0 <1.0 <1.0 N 1.43 <5.0 <5.0 607 <1.0 <3.0
SBMW-2D 7/28/2016 <1.0 <0.0197 8.96 <10 <1.0 <1.0 <1.0 <1.0 <5.0 1.48 <5.0 <5.0 493 <1.0 <3.0
SBMW-2D 12/14/2016 <1.0 <0.020 8.79 <10 <1.0 <1.0 <1.0 <1.0 <5.0 1.08 <5.0 <5.0 585 <1.0 <3.0
SBMW-2D 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2D 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2D 7/10/2018 <0.30 <0.0026 14.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.2 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2D 12/18/2018 <0.30 <0.0900 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2D 6/11/2019 <0.30 <0.0032 12.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.5 <1.0 <0.30 1,100 <0.20 <0.30
SBMW-2D 12/17/2019 0.39 J <0.0031 12.0 <1.0 <0.30 0.50 J <0.20 <0.30 <0.0900 1.9 <1.0 <0.30 1,000 <0.20 0.66 J
SBMW-2D 6/23/2020 <0.30 <0.0031 1.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.30 J <1.0 <0.30 <10 <0.20 <0.30
SBMW-2D 12/28/2020 <0.30 <0.0031 19.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 5.2 <1.0 <0.30 760 <0.20 <0.30
SBMW-2D 6/16/2021 <0.30 <0.0030 3.3 4.4 <0.30 <0.20 <0.20 <0.30 <0.0900 0.50 J <1.0 0.99 J <10 <0.20 <0.30
SBMW-2D 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2D 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 8.5 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
SBMW-2B 5/6/2004 N <10 327 <2.0 N <5.0 <10 <10 N 50.0 <5.0 <2.0 59,500 <10 <30
SBMW-2B 11/19/2007 0.29 J <0.009 210 4.1 <1.0 0.65 J <1.0 0.28 J N 89.0 <2.0 3.2 <20 0.16 J 0.97 J
SBMW-2B 11/5/2008 <1.0 <1.0 250 <2.0 <1.0 <1.0 <1.0 <1.0 N 89.0 <2.0 <1.0 37,000 0.13 J 0.47 J
SBMW-2B 11/24/2009 0.56 J <5.0 210 <10 <5.0 <5.0 <5.0 1.2 J N 100 <10 <5.0 41,000 <5.0 1<5.0
SBMW-2B 3/9/2011 <1.0 <1.0 190 <2.0 <1.0 <1.0 <1.0 <1.0 N 210 <2.0 <1.0 85,000 0.18 J <3.0
SBMW-2B 11/9/2011 2 J <5.0 160 27.0 <5.0 3.0 J <5.0 1.1 J N 230 <10 15.0 75,000 1.2 J 5 J
SBMW-2B 9/6/2012 <1.0 <1.0 110 <1.0 <1.0 <1.0 <1.0 <1.0 N 140 <2.0 <1.0 20,000 <1.0 <3.0
SBMW-2B 11/29/2012 <1.0 <1.0 5.8 <1.0 <1.0 <1.0 <1.0 <1.0 N 0.99 J <2.0 <1.0 46,000 12 <3.0
SBMW-2B 10/28/2015 <1.0 <0.0200*57.2 <10 <1.0 <1.0 <10 <1.0 N 378 <50 <5.0 160,000 <1.0 <3.0
SBMW-2B 7/28/2016 <1.0 <0.0198 49.1 <10 <1.0 <1.0 <1.0 <1.0 1.26 J 351 <5.0 <5.0 32,200 <1.0 <3.0
SBMW-2B 12/27/2016 <25.0 <0.0199 62.9 <50 <25.0 <25.0 <25.0 <25.0 <5.0 394 <5.0 <5.0 39,000 <25.0 <75
SBMW-2B 7/7/2017 <0.30 <0.20 2.1 <1.0 <0.30 <0.20 <0.20 <0.30 3.89 160 <1.0 <0.30 29,000 <0.20 <0.30
SBMW-2B 12/12/2017 <1.5 <1.0 2.9 <5.0 <1.5 <1.0 <1.0 <1.5 2.0 590 <5.0 <1.5 55,000 <1.0 <1.5
SBMW-2B 7/12/2018 <0.30 <0.0026 41.0 <1.0 <0.30 <0.20 <0.20 <0.30 2.06 410 <1.0 <0.30 19,000 <0.20 <0.30
SBMW-2B 1/7/2019 <0.30 <0.0031 22.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 410 <1.0 <0.30 20,000 <0.20 <0.30
SBMW-2B 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.65 430 <1.0 <0.30 33,000 <0.20 <0.30
SBMW-2B 12/17/2019 0.81 J <0.0031 23.0 <1.0 <0.30 0.72 J <0.20 0.42 J 0.761 J 330 <1.0 <0.30 14,000 <0.20 1.6
SBMW-2B 6/23/2020 <0.30 <0.0031 1.0 <1.0 <0.30 <0.20 <0.20 <0.30 2.17 270 <1.0 <0.30 28,000 <0.20 <0.30
SBMW-2B 12/28/2020 <0.30 <0.0031 33.0 <1.0 <0.30 <0.20 <0.20 <0.30 1.02 230 <1.0 <0.30 12,000 <0.20 <0.30
SBMW-2B 6/16/2021 <1.5 <0.0030 <1.0 <5.0 <1.5 <1.0 <1.0 <1.5 1.64 260 <5.0 <1.5 14,000 <1.0 <1.5
SBMW-2B 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 140 <1.0 <0.30 4,500 <0.20 <0.30
SBMW-2B 2/27/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA 180 <1.0 <0.30 18,000 <0.20 <0.30
SBMW-2B 7/18/2023 <0.30 <0.0031 18.0 <1.0 <0.30 <0.20 <0.20 <0.30 NM 250 <1.0 <0.30 15,000 <0.20 <0.30
PMW-J-I 2/17/2017 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 486 <1.0 <3.0
Page 21 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
PMW-J-I 6/30/2017 <0.30 <0.20 0.87 <1.0 <0.30 0.69 0.78 <0.30 0.537 <0.20 <1.0 <0.30 560 <0.20 0.67
PMW-J-I 12/12/2017 <0.30 <0.20 0.59 <1.0 <0.30 0.79 1.3 <0.30 4.7 1.1 <1.0 <0.30 300 <0.20 <0.30
PMW-J-I 7/12/2018 <0.30 <0.0026 1.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.45 <1.0 <0.30 310 <0.20 <0.30
PMW-J-I 1/9/2019 <0.30 0.011 J 0.41 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.49 J <1.0 <0.30 430 <0.20 <0.30
PMW-J-I 6/12/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-J-I 12/12/2019 <0.30 <0.0032 0.83 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.49 J <1.0 <0.30 380 <0.20 <0.30
PMW-J-I 6/23/2020 <0.30 <0.0030 0.78 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 210 <0.20 <0.30
PMW-J-I 12/17/2020 <0.30 <0.0031 0.65 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 61.0 <0.20 <0.30
PMW-J-I 6/15/2021 <0.30 <0.0031 0.74 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.42 J <1.0 <0.30 87.0 <0.20 <0.30
PMW-J-I 6/21/2022 <0.30 0.018 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-J-I 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-J-D 2/17/2017 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 1.55 <5.0 <5.0 900 <1.0 <3.0
PMW-J-D 6/30/2017 <0.30 <0.20 1.1 <1.0 <0.30 <0.20 <0.20 <0.30 0.722 1.3 <1.0 <0.30 1,700 <0.20 <0.30
PMW-J-D 12/12/2017 0.51 <0.20 <0.20 <1.0 <0.30 1.0 3.3 1.5 1.24 <0.20 2.6 2.7 530 0.2 2.8
PMW-J-D 7/12/2018 <0.30 <0.0027 1.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.3 <1.0 <0.30 400 <0.20 <0.30
PMW-J-D 1/9/2019 <0.30 <0.0032 0.49 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.8 <1.0 <0.30 1,400 <0.20 <0.30
PMW-J-D 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.613 J 1.5 <1.0 <0.30 <10 <0.20 <0.30
PMW-J-D 12/12/2019 <0.30 <0.0032 0.52 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.3 <1.0 <0.30 810 <0.20 <0.30
PMW-J-D 6/23/2020 <0.30 <0.0030 0.60 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.4 <1.0 <0.30 480 <0.20 <0.30
PMW-J-D 12/17/2020 <0.30 <0.0031 0.49 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.0 <1.0 <0.30 680 <0.20 <0.30
PMW-J-D 6/15/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.3 <1.0 <0.30 200 <0.20 <0.30
PMW-J-D 6/21/2022 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-J-D 7/19/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-J-B 2/17/2017 <1.0 <0.020 2.46 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 455 <1.0 <3.0
PMW-J-B 6/30/2017 <0.30 <0.20 1.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-J-B 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-J-B 7/12/2018 <0.30 <0.0026 1.6 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-J-B 1/9/2019 <0.30 <0.0031 0.45 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.40 J <1.0 <0.30 <10 <0.20 <0.30
PMW-J-B 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 2.9 <0.20 <0.30 4.47 <0.20 <1.0 <0.30 <10 <0.20 0.88 J
PMW-J-B 12/12/2019 <0.30 <0.0031 1.6 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.88 J <1.0 <0.30 <10 <0.20 <0.30
PMW-J-B 6/23/2020 0.78 J <0.0030 0.78 J <1.0 <0.30 0.22 J <0.20 1.6 6.9 <0.20 <1.0 0.74 J <10 <0.20 4.9
PMW-J-B 12/17/2020 3.2 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 0.58 J 4.18 <0.20 <1.0 <0.30 <10 <0.20 4.4
PMW-J-B 6/15/2021 1.5 <0.0032 <0.20 <1.0 <0.30 0.39 J <0.20 0.37 J 4.21 0.33 J <1.0 3.0 <10 <0.20 3.2
PMW-J-B 6/21/2022 <0.30 <0.20 <0.20 <1.0 <0.30 3.7 <0.20 0.45 J 3.33 <0.20 <1.0 <0.30 <10 0.31 J 3.1
PMW-J-B 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-K-I 2/16/2017 47.3 <0.0196 5.59 35.8 2.51 28.5 <1.0 20.2 1.57 J <1.0 <5.0 56.7 21.4 14.6 79.2
PMW-K-I 6/28/2017 1.4 <0.20 5.2 12.0 <0.30 6.7 <0.20 1.1 18.8 <0.20 <1.0 18.0 53.0 <0.20 1.3
PMW-K-I 12/12/2017 0.6 <0.20 4.0 10.0 <0.30 5.9 <0.20 1.2 6.24 0.45 <1.0 17.0 78.0 0.32 <0.30
Page 22 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
PMW-K-I 7/12/2018 <0.30 <0.0027 4.7 <1.0 <0.30 4.2 <0.20 <0.30 1.10 <0.20 <1.0 4.2 <10 <0.20 <0.30
PMW-K-I 1/8/2019 <0.30 <0.0031 5.7 <1.0 <0.30 2.1 <0.20 <0.30 <0.0900 1.6 <1.0 2.8 59.0 <0.20 <0.30
PMW-K-I 6/12/2019 <0.30 <0.0031 4.9 <1.0 <0.30 0.86 J <0.20 <0.30 7.23 1.0 <1.0 <0.30 46.0 <0.20 <0.30
PMW-K-I 12/12/2019 0.74 J <0.0031 5.6 4.2 <0.30 20.0 <0.20 1.6 12.8 1.4 <1.0 1.1 54.0 5.2 6.1
PMW-K-I 6/23/2020 <0.30 <0.0030 2.8 <1.0 <0.30 <0.20 <0.20 <0.30 5.45 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-K-I 12/17/2020 <0.30 <0.0031 6.4 <1.0 <0.30 2.9 <0.20 <0.30 3.77 0.82 J <1.0 <0.30 27.0 0.45 J <0.30
PMW-K-I 6/16/2021 <0.30 <0.0032 4.7 <1.0 <0.30 1.3 <0.20 <0.30 9.77 <0.20 <1.0 <0.30 16.0 <0.20 <0.30
PMW-K-I 6/20/2022 <0.30 0.087 2.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-K-I 7/18/2023 <0.30 <0.0031 7.2 4.2 <0.30 2.4 <0.20 <0.30 NM <0.20 <1.0 3.8 <10 <0.20 <0.30
PMW-K-D 2/16/2017 <1.0 <0.020 7.3 <10 <1.0 <1.0 <1.0 <1.0 <5.0 84.5 <5.0 <5.0 1,660 <1.0 <3.0
PMW-K-D 6/28/2017 <0.30 <0.20 4.6 <1.0 <0.30 <0.20 <0.20 <0.30 0.315 72.0 <1.0 <0.30 2,300 <0.20 <0.30
PMW-K-D 12/12/2017 <0.30 <0.20 3.4 <1.0 <0.30 <0.20 <0.20 <0.30 1.29 41.0 <1.0 <0.30 1,300 <0.20 <0.30
PMW-K-D 7/12/2018 <0.30 <0.0026 6.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 68.0 <1.0 <0.30 1,200 <0.20 <0.30
PMW-K-D 1/8/2019 <0.30 <0.0031 1.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 36.0 <1.0 <0.30 690 <0.20 <0.30
PMW-K-D 6/12/2019 <0.30 <0.0031 1.8 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 39.0 <1.0 <0.30 530 <0.20 <0.30
PMW-K-D 12/12/2019 <0.30 <0.0031 1.8 <1.0 <0.30 <0.20 <0.20 <0.30 0.280 J 37.0 <1.0 <0.30 600 <0.20 <0.30
PMW-K-D 6/23/2020 <0.30 <0.0031 4.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 59.0 <1.0 <0.30 670 <0.20 <0.30
PMW-K-D 12/17/2020 <0.30 <0.0031 2.1 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 38.0 <1.0 <0.30 420 <0.20 <0.30
PMW-K-D 6/16/2021 <0.30 <0.0031 2.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 43.0 <1.0 <0.30 430 <0.20 <0.30
PMW-K-D 6/20/2022 <0.30 0.067 0.85 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-K-D 7/18/2023 <0.30 <0.0031 1.6 <1.0 <0.30 <0.20 <0.20 <0.30 NM 37 <1.0 <0.30 <10 <0.20 <0.30
PMW-K-B 2/16/2017 <1.0 <0.020 6.97 <10 <1.0 <1.0 <1.0 <1.0 <5.0 178 <5.0 <5.0 1,980 <1.0 <3.0
PMW-K-B 6/28/2017 <0.30 <0.20 4.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 140 <1.0 <0.30 2,500 <0.20 <0.30
PMW-K-B 12/12/2017 <0.30 <0.20 6.4 <1.0 <0.30 <0.20 <0.20 <0.30 2.42 160 <1.0 <0.30 1,500 <0.20 <0.30
PMW-K-B 7/12/2018 <0.30 <0.0026 1.1 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 35.0 <1.0 <0.30 <10 <0.20 <0.30
PMW-K-B 1/8/2019 <0.30 0.014 J 0.45 J <1.0 <0.30 1.9 <0.20 <0.30 1.52 30.0 <1.0 <0.30 <10 <0.20 <0.30
PMW-K-B 6/12/2019 1.9 <0.0031 0.52 J 4.5 <0.30 13.0 <0.20 1.3 25.3 13.0 <1.0 7.1 29.0 <0.20 1.6
PMW-K-B 12/12/2019 3.1 <0.0032 <0.20 4.6 <0.30 17.0 <0.20 1.2 48.0 15.0 <1.0 12.0 <10 <0.20 2.9
PMW-K-B 6/24/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 4.3 <0.20 0.36 J 17.4 6.9 <1.0 5.7 <10 <0.20 <0.30
PMW-K-B 12/17/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 3.2 <0.20 <0.30 12.9 4.9 <1.0 4.0 <10 <0.20 <0.30
PMW-K-B 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 2.3 <0.20 <0.30 6.37 4.8 <1.0 <0.30 <10 <0.20 <0.30
PMW-K-B 6/20/2022 <0.30 <0.0031 0.45 J <1.0 <0.30 0.43 J <0.20 <0.30 2.27 14.0 <1.0 <0.30 <10 <0.20 <0.30
PMW-K-B 7/18/2023 <0.30 <0.0031 0.61 J <1.0 <0.30 <0.20 <0.20 <0.30 NM 14 <1.0 <0.30 <10 <0.20 <0.30
PMW-L-I 2/16/2017 <1.0 <0.0206 <1.0 <10 <1.0 31.6 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 62.7 <1.0 <3.0
PMW-L-I 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 23.0 <0.20 <0.30 3.69 <0.20 <1.0 <0.30 42.0 <0.20 <0.30
PMW-L-I 12/12/2017 <0.30 <0.20 <0.20 <1.0 <0.30 1.6 <0.20 <0.30 0.817 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-L-I 7/10/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 3.7 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 24.0 <0.20 <0.30
PMW-L-I 12/19/2018 <0.30 <0.0031 <0.20 <1.0 <0.30 5.1 <0.20 <0.30 1.33 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 23 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
PMW-L-I 6/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 1.3 <0.20 <0.30 0.394 J <0.20 <1.0 <0.30 36.0 <0.20 <0.30
PMW-L-I 12/11/2019 <0.30 <0.0031 <0.20 3.9 <0.30 5.8 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 34.0 <0.20 <0.30
PMW-L-I 6/23/2020 <0.30 0.0098 JP <0.20 <1.0 <0.30 0.65 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-L-I 12/17/2020 <0.30 <0.0031 <0.20 5.1 <0.30 0.44 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 18.0 <0.20 <0.30
PMW-L-I 6/15/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 38.0 <0.20 <0.30
PMW-L-I 6/20/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 0.65 J <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-L-I 7/18/2023 <0.30 <0.0032 1.3 <1.0 <0.30 <0.20 <0.20 <0.30 NM 13 <1.0 <0.30 120 <0.20 <0.30
PMW-L-D 2/16/2017 <1.0 <0.0200 1.84 <10 <1.0 <1.0 <1.0 <1.0 1.79 J 9.22 <5.0 <5.0 319 <1.0 <3.0
PMW-L-D 6/28/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.278 <0.20 <1.0 <0.30 170 <0.20 <0.30
PMW-L-D 12/12/2017 <0.30 <0.20 0.94 <1.0 <0.30 <0.20 <0.20 <0.30 1.12 6.3 <1.0 <0.30 270 <0.20 <0.30
PMW-L-D 7/10/2018 <0.30 <0.0026 1.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 6.1 <1.0 <0.30 140 <0.20 <0.30
PMW-L-D 12/19/2018 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 100 <0.20 <0.30
PMW-L-D 6/11/2019 <0.30 <0.0031 1.6 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 21.0 <1.0 <0.30 260 <0.20 <0.30
PMW-L-D 12/11/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.21 J <1.0 <0.30 110 <0.20 <0.30
PMW-L-D 6/23/2020 <0.30 0.012 JP 0.49 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 1.3 <1.0 <0.30 83.0 <0.20 <0.30
PMW-L-D 12/17/2020 <0.30 <0.0032 <0.20 4.9 <0.30 <0.20 <0.20 <0.30 <0.0900 3.4 <1.0 2.9 43.0 <0.20 <0.30
PMW-L-D 6/15/2021 <0.30 <0.0031 1.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 26.0 <1.0 <0.30 280 <0.20 <0.30
PMW-L-D 6/20/2022 <0.30 <0.20 <0.20 <1.0 <0.30 0.34 J <0.20 <0.30 0.278 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-L-D 7/18/2023 <0.30 <0.0031 3.9 <1.0 <0.30 <0.20 <0.20 <0.30 NM 43 <1.0 <0.30 240 <0.20 <0.30
PMW-L-B 2/16/2017 <1.0 <0.020 10.1 <10 <1.0 <1.0 <1.0 <1.0 <5.0 248 <5.0 <5.0 1,720 <1.0 <3.0
PMW-L-B 7/7/2017 <0.30 <0.20 9.2 7.1 <0.30 <0.20 <0.20 <0.30 0.777 270 <1.0 <0.30 2,300 <0.20 <0.30
PMW-L-B 12/12/2017 0.73 <0.20 6.7 <1.0 <0.30 0.55 <0.20 0.43 0.73 200 <1.0 <0.30 1,900 0.2 0.56
PMW-L-B 7/11/2018 <0.30 <0.0026 5.9 <1.0 <0.30 0.21 <0.20 <0.30 <0.0900 160 <1.0 <0.30 1,500 <0.20 <0.30
PMW-L-B 12/19/2018 <0.30 <0.0032 11.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 420 <1.0 <0.30 2,900 <0.20 <0.30
PMW-L-B 6/11/2019 <0.30 <0.0031 10.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 330 <1.0 <0.30 2,400 <0.20 <0.30
PMW-L-B 12/11/2019 <0.30 <0.0031 2.7 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 130 <1.0 <0.30 25.0 <0.20 <0.30
PMW-L-B 6/23/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 63.0 <1.0 <0.30 36.0 <0.20 <0.30
PMW-L-B 12/17/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 55.0 <1.0 <0.30 170 <0.20 <0.30
PMW-L-B 6/15/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 56.0 <1.0 <0.30 <10 <0.20 <0.30
PMW-L-B 6/20/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 38.0 <1.0 <0.30 250 <0.20 <0.30
PMW-L-B 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-M-I 2/16/2017 <1.0 <0.0197 97.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 14.5 <5.0 <5.0 2,290 <1.0 <3.0
PMW-M-I 6/28/2017 <0.30 <0.20 82.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.476 16.0 <1.0 <0.30 3,700 <0.20 <0.30
PMW-M-I 12/13/2017 <0.30 <0.20 98.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 20.0 <1.0 <0.30 4,200 <0.20 <0.30
PMW-M-I 7/12/2018 <0.30 0.024 110 <1.0 <0.30 <0.20 <0.20 <0.30 0.378 19.0 <1.0 <0.30 2,900 <0.20 <0.30
PMW-M-I 1/9/2019 <0.30 <0.0032 98.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 20.0 <1.0 <0.30 3,300 <0.20 <0.30
PMW-M-I 6/12/2019 <0.30 <0.0031 80.0 <1.0 <0.30 <0.20 <0.20 <0.30 1.03 21.0 <1.0 <0.30 3,200 <0.20 <0.30
PMW-M-I 12/12/2019 <0.30 <0.0032 85.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 28.0 <1.0 <0.30 <10 <0.20 <0.30
Page 24 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
PMW-M-I 6/22/2020 <0.30 <0.0031 78.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 27.0 <1.0 <0.30 3,300 <0.20 <0.30
PMW-M-I 12/28/2020 <0.30 <0.0032 90.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 35.0 <1.0 <0.30 5,300 <0.20 <0.30
PMW-M-I 6/17/2021 <0.30 <0.0032 74.0 <1.0 <0.30 <0.20 <0.20 <0.30 1.16 35.0 <1.0 <0.30 4,200 <0.20 <0.30
PMW-M-I 6/21/2022 <0.30 0.037 12.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.73 J <1.0 <0.30 32.0 <0.20 <0.30
PMW-M-I 7/18/2023 <0.30 <0.0032 74.0 <1.0 <0.30 <0.20 <0.20 <0.30 NM 48 <1.0 <0.30 4,500 <0.20 <0.30
PMW-M-D 2/17/2017 6.87 <0.020 147 <10 <1.0 2.85 <1.0 <1.0 <5.0 21.8 <5.0 <5.0 3,710 <1.0 7.09
PMW-M-D 6/28/2017 1.6 <0.20 89.0 <1.0 <0.30 36.0 <0.20 2.3 7.13 17.0 <1.0 <0.30 4,300 2.1 22.0
PMW-M-D 12/13/2017 2.5 <0.20 110 <1.0 <0.30 5.5 <0.20 1.2 3.86 19.0 <1.0 2.9 4,800 <0.20 11.0
PMW-M-D 7/12/2018 3.0 <0.0027 100 <1.0 <0.30 30.0 <0.20 1.3 3.53 19.0 <1.0 0.56 3,200 1.6 13.0
PMW-M-D 1/9/2019 360 <0.0031 <0.20 14.0 2.2 6,500 <0.20 250 34.4 6.4 <1.0 82.0 2,700 290 1,900
PMW-M-D 6/12/2019 110 <0.0031 <2.0 <10 <3.0 3,700 <2.0 37.0 88.8 6.2 J <10.0 33.0 1,100 78.0 750
PMW-M-D 12/12/2019 61.0 <0.0032 <2.0 <10 <3.0 2,400 <2.0 14.0 52.3 9.7 J <10.0 6.4 J 2,000 47.0 510
PMW-M-D 6/22/2020 0.77 J <0.0030 31.0 <1.0 <0.30 41.0 <2.0 0.44 J 2.58 21.0 <1.0 <0.30 2,900 0.46 J 6.7
PMW-M-D 12/28/2020 <0.30 <0.0032 18.0 <1.0 <0.30 28.0 <2.0 0.51 J 3.18 28.0 <1.0 <0.30 4,600 <0.20 0.78 J
PMW-M-D 6/17/2021 0.60 J <0.0031 56.0 <1.0 <0.30 28.0 <2.0 0.91 J 4.85 28.0 <1.0 <0.30 3,900 0.62 J 3.8
PMW-M-D 12/28/2021 <1.5 <0.0031 <1.0 <5.0 <1.5 300 <1.0 3.9 J 68.4 12.0 <5.0 <1.5 3,700 <1.0 16.0
PMW-M-D 6/21/2022 <0.30 <0.0031 28.0 <1.0 <0.30 <0.20 <0.20 <0.30 3.40 25.0 <1.0 <0.30 2,300 <0.20 <0.30
PMW-M-D 12/5/2022 <0.30 <0.0031 70.0 <1.0 <0.30 1.0 <0.20 <0.30 NA 40.0 <1.0 <0.30 5,900 <0.20 <0.30
PMW-M-D 7/18/2023 <0.30 <0.0031 66.0 <1.0 <0.30 <0.20 <0.20 0.59 J NM 47 <1.0 <0.30 3,900 <0.20 0.98 J
PMW-M-D 12/6/2023 <0.30 <0.0032 90.0 <1.0 <0.30 3.5 <0.20 <0.30 NM 47 <1.0 <0.30 6,900 0.45 J <0.30
PMW-M-B 2/17/2017 29.2 <0.020 24.4 <10 <1.0 18.3 <1.0 15.2 <5.0 3.32 <5.0 13.4 818 1.56 89.2
PMW-M-B 6/28/2017 15.0 <0.20 17.0 6.4 0.51 24.0 <0.20 20.0 18.1 3.4 <1.0 15.0 1,400 2.2 110
PMW-M-B 12/13/2017 48.0 <0.20 20.0 8.7 <0.30 25.0 <0.20 25.0 19.2 3.7 <1.0 13.0 970 2.4 150
PMW-M-B 8/15/2018 36.0 <0.20 19.0 <1.0 <1.0 1.2 <0.20 1.3 91.0 2.9 <1.0 8.3 870 <1.0 91.0
PMW-M-B 1/8/2019 0.62 J <0.0031 <0.20 <1.0 <0.30 1.3 <0.20 <0.20 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 2.0
PMW-M-B 6/12/2019 1.6 <0.0031 <0.20 2.5 <0.30 18.0 <0.20 <0.30 2.18 <0.20 <1.0 <0.30 14.0 0.67 J 7.0
PMW-M-B 12/12/2019 3.5 <0.0031 <0.20 <1.0 <0.30 68.0 <0.20 0.72 J 3.11 <0.20 <1.0 0.70 J 16.0 2.4 29.0
PMW-M-B 6/22/2020 <0.30 <0.0029 <0.20 <1.0 <0.30 1.4 <0.20 <0.20 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 1.4
PMW-M-B 12/28/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-M-B 6/17/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 1.1 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-M-B 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-M-B 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-N-I 2/16/2017 <1.0 <0.020 25.5 <10 <1.0 <1.0 <1.0 <1.0 1.73 J 35.1 <5.0 <5.0 1,920 <1.0 <3.0
PMW-N-I 6/29/2017 <0.30 <0.20 23.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.92 59.0 <1.0 <0.30 4,400 <0.20 <0.30
PMW-N-I 12/13/2017 <0.30 <0.20 43.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 75.0 <1.0 <0.30 6,400 0.21 <0.30
PMW-N-I 7/12/2018 <0.30 <0.0026 19.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 14.0 <1.0 <0.30 1,400 <0.20 <0.30
PMW-N-I 1/8/2019 <0.30 0.016 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-N-I 6/12/2019 <0.30 <0.0031 15.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 12.0 <1.0 <0.30 1,100 <0.20 <0.30
Page 25 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
PMW-N-I 12/16/2019 <0.30 <0.0031 16.0 5.8 <0.30 <0.20 <0.20 <0.30 0.835 J 56.0 <1.0 <0.30 2,000 <0.20 <0.30
PMW-N-I 6/22/2020 <0.30 <0.0031 20.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 26.0 <1.0 <0.30 1,300 <0.20 <0.30
PMW-N-I 12/28/2020 <0.30 <0.0032 19.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 64.0 <1.0 <0.30 2,100 <0.20 <0.30
PMW-N-I 6/15/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 63.0 <0.20 <0.30
PMW-N-I 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-N-I 7/18/2023 <0.30 <0.0031 22.0 <1.0 <0.30 <0.20 <0.20 <0.30 NM 34 <1.0 <0.30 2,200 <0.20 <0.30
PMW-N-D 2/16/2017 <1.0 <0.0199 6.33 <10 <1.0 <1.0 <1.0 <1.0 <5.0 81.6 <5.0 <5.0 757 <1.0 <3.0
PMW-N-D 6/29/2017 <0.30 <0.20 1.3 6.1 <0.30 <0.20 12.0 <0.30 0.782 24.0 <1.0 <0.30 <10 <0.20 <0.30
PMW-N-D 12/12/2017 <0.30 <0.20 6.1 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 110.0 <1.0 <0.30 1400 <0.20 <0.30
PMW-N-D 7/12/2018 <0.30 0.038 6.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 79.0 <1.0 <0.30 720 <0.20 <0.30
PMW-N-D 1/8/2019 <0.30 <0.0032 4.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 46.0 <1.0 <0.30 150 <0.20 <0.30
PMW-N-D 6/12/2019 <0.30 <0.0031 4.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 80.0 <1.0 <0.30 550 <0.20 <0.30
PMW-N-D 12/16/2019 <0.30 <0.0031 4.5 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 96.0 <1.0 <0.30 750 <0.20 <0.30
PMW-N-D 6/22/2020 <0.30 0.028 4.9 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 97.0 <1.0 <0.30 660 <0.20 <0.30
PMW-N-D 12/28/2020 <0.30 <0.0031 4.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 110.0 <1.0 <0.30 560 <0.20 <0.30
PMW-N-D 6/15/2021 <0.30 <0.0032 3.2 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 46.0 <1.0 <0.30 150 <0.20 <0.30
PMW-N-D 6/21/2022 <0.30 0.055 3.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 47.0 <1.0 <0.30 110 <0.20 <0.30
PMW-N-D 7/18/2023 <0.30 <0.0032 4.0 <1.0 <0.30 <0.20 <0.20 <0.30 NM 99 <1.0 <0.30 280 <0.20 <0.30
PMW-N-B 2/16/2017 <1.0 <0.0199 77.5 <10 <1.0 <1.0 <1.0 <1.0 <5.0 80.7 <5.0 <5.0 3,960 <1.0 <3.0
PMW-N-B 7/7/2017 <0.30 <0.20 56.0 <1.0 <0.30 <0.20 <0.20 <0.30 1.17 60.0 <1.0 <0.30 7,500 <0.20 <0.30
PMW-N-B 12/12/2017 <0.30 <0.20 54.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.642 64.0 <1.0 <0.30 4,700 <0.20 <0.30
PMW-N-B 7/12/2018 <0.30 <0.0027 21.0 <1.0 <0.30 <0.20 <0.20 <0.30 0.428 26.0 <1.0 <0.30 2,200 <0.20 <0.30
PMW-N-B 1/8/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.22 J <1.0 <0.30 20.0 <0.20 <0.30
PMW-N-B 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-N-B 12/16/2019 <0.30 0.0072 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-N-B 6/22/2020 <0.30 0.014 JP 1.0 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.63 J <1.0 <0.30 22.0 <0.20 <0.30
PMW-N-B 12/28/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-N-B 6/15/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-N-B 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-N-B 7/18/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-I 2/17/2017 <1.0 <0.020 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 87.0 <1.0 <3.0
PMW-O-I 7/6/2017 <0.30 <0.20 0.76 <1.0 <0.30 <0.20 <0.20 <0.30 0.301 0.2 <1.0 <0.30 56.0 <0.20 <0.30
PMW-O-I 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.441 0.23 <1.0 1.4 96.0 <0.20 <0.30
PMW-O-I 7/11/2018 <0.30 <0.0026 0.90 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 66.0 <0.20 <0.30
PMW-O-I 1/9/2019 <0.30 <0.0032 0.63 J <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 16.0 <0.20 <0.30
PMW-O-I 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-I 12/20/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 36.0 <0.20 <0.30
PMW-O-I 6/24/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 26 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
PMW-O-I 12/28/2020 <0.30 <0.0032 <0.20 <1.0 <0.30 1.7 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 41.0 <0.20 <0.30
PMW-O-I 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-I 6/21/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-I 7/19/2023 <0.30 <0.0031 6.7 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 3.6 220 <0.20 <0.30
PMW-O-D 2/17/2017 <1.0 <0.0200 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 198 <1.0 <3.0
PMW-O-D 7/6/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 270 <0.20 <0.30
PMW-O-D 12/14/2017 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.57 <1.0 <0.30 190 <0.20 <0.30
PMW-O-D 7/11/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.6 <1.0 <0.30 240 <0.20 <0.30
PMW-O-D 1/9/2019 <0.30 <0.0032 0.87 J <1.0 <0.30 0.96 J <0.20 <0.30 <0.0900 0.83 J <1.0 <0.30 590 <0.20 <0.30
PMW-O-D 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 190 <0.20 <0.30
PMW-O-D 12/20/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.69 J <1.0 <0.30 350 <0.20 <0.30
PMW-O-D 6/24/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.85 J <1.0 <0.30 280 <0.20 <0.30
PMW-O-D 12/28/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.93 J <1.0 <0.30 320 <0.20 <0.30
PMW-O-D 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 0.55 J <1.0 <0.30 <10 <0.20 <0.30
PMW-O-D 6/21/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-D 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 560 <0.20 <0.30
PMW-O-B 2/17/2017 <1.0 <0.0199 5.08 <10 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <5.0 <5.0 309 <1.0 <3.0
PMW-O-B 7/7/2017 <0.30 <0.20 3.4 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-B 12/14/2017 <0.30 <0.20 3.4 <1.0 <0.30 <0.20 <0.20 <0.30 1.92 0.89 <1.0 <0.30 190 <0.20 <0.30
PMW-O-B 7/11/2018 <0.30 <0.0027 1.1 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-B 1/9/2019 <0.30 <0.0032 0.68 J <1.0 <0.30 4.0 <0.20 <0.30 <0.0900 <0.20 <1.0 0.89 J <10 <0.20 2.3
PMW-O-B 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-B 12/20/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-B 6/24/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-B 12/28/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 1.8 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-B 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-B 6/21/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-O-B 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-S 1/26/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 8.8 <0.30 3.72 <0.20 <1.0 <0.30 <10 4.8 <0.30
PMW-P-S 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 1.3 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-S 1/7/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 0.25 J <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-S 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-S 12/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-S 6/21/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-S 12/18/2020 <0.21 <0.0032 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 1.6 J <2.7 <0.23 <0.39
PMW-P-S 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-S 6/23/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-S 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 27 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
PMW-P-I 1/26/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.761 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-I 7/11/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-I 1/7/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-I 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-I 12/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-I 6/21/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-I 12/18/2020 0.24 J <0.0031 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 1.9 J <2.7 <0.23 <0.39
PMW-P-I 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-I 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-I 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 1/26/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.270 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 7/11/2018 <0.30 0.018 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 1/7/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 6/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 12/11/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 6/21/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 12/18/2020 <0.21 <0.0031 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 1.8 J <2.7 <0.23 <0.39
PMW-P-D 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 6/22/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 2/27/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NA <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-D 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-B 1/26/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 0.44 <0.30 0.391 <0.20 <1.0 <0.30 <10 0.93 <0.30
PMW-P-B 7/11/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 0.57 J <0.30
PMW-P-B 1/7/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 0.43 J <0.30
PMW-P-B 6/13/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-B 12/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-B 6/21/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 0.37 J <0.30
PMW-P-B 12/18/2020 <0.21 <0.0031 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 0.88 J <2.7 <0.23 <0.39
PMW-P-B 6/16/2021 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-B 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-P-B 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-S 1/25/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 7.0 <0.30 4.97 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-S 7/11/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-S 1/7/2019 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-S 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-S 12/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-S 6/22/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 28 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
PMW-Q-S 12/18/2020 <0.21 <0.0031 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 <0.30 <2.7 <0.23 <0.39
PMW-Q-S 6/17/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-S 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-S 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-I 1/25/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 0.93 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-I 7/11/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 0.93 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-I 1/7/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 0.93 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-I 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-I 12/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-I 6/22/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-I 12/18/2020 <0.21 <0.0030 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 <0.30 <2.7 <0.23 <0.39
PMW-Q-I 6/17/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-I 6/22/2022 <0.30 0.0100 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-I 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-D 1/26/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-D 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-D 1/7/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-D 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-D 12/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-D 6/22/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-D 12/18/2020 <0.21 <0.0031 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 <0.30 <2.7 <0.23 <0.39
PMW-Q-D 6/17/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-D 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-D 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-B 1/25/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.19 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-B 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.468 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-B 1/7/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-B 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-B 12/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-B 6/22/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-B 12/18/2020 <0.21 <0.0031 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 1.2 J <2.7 <0.23 <0.39
PMW-Q-B 6/17/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-B 6/22/2022 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-Q-B 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-S 1/25/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 3.6 <0.30 1.72 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-S 7/11/2018 <0.30 0.055 <0.20 <1.0 <0.30 <0.20 4.88 <0.30 4.88 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-S 1/7/2019 <0.30 0.020 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 29 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
PMW-R-S 6/13/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-S 12/12/2019 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-S 6/22/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-S 12/18/2020 <0.21 <0.0032 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 1.4 J <2.7 <0.23 <0.39
PMW-R-S 6/17/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-S 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-S 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-I 1/25/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.49 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-I 7/11/2018 <0.30 0.035 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-I 1/7/2019 <0.30 0.011 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-I 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-I 12/12/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-I 6/21/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-I 12/18/2020 <0.21 <0.0031 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 <0.30 <2.7 <0.23 <0.39
PMW-R-I 6/17/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-I 6/22/2022 <0.30 0.041 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-I 7/19/2023 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-D 1/25/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.58 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-D 7/11/2018 <0.30 <0.0026 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-D 1/7/2019 <0.30 0.0095 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-D 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-D 12/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-D 6/21/2020 <0.30 <0.0030 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-D 12/18/2020 <0.21 <0.0031 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 <0.30 <2.7 <0.23 <0.39
PMW-R-D 6/17/2021 <0.30 <0.0032 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-D 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-D 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-B 1/25/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.65 <0.20 <1.0 <0.30 <10 0.34 <0.30
PMW-R-B 7/11/2018 <0.30 <0.0027 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-B 1/7/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-B 6/13/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-B 12/11/2019 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.77 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-B 6/21/2020 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.02 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-B 12/18/2020 <0.21 <0.0031 <0.41 <1.0 <0.26 <0.23 <0.26 <0.23 <0.0900 <0.21 <0.27 1.0 J 8.5 J <0.23 <0.39
PMW-R-B 6/17/2021 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 1.64 <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-B 6/22/2022 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 0.846 J <0.20 <1.0 <0.30 <10 <0.20 <0.30
PMW-R-B 7/19/2023 <0.30 <0.0031 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 NM <0.20 <1.0 <0.30 <10 <0.20 <0.30
Page 30 of 31
Table 6
Groundwater Analytical Data - Offsite Wells
Total Petrochemicals Refind USA, Inc.
Facility #1760
Greensboro, North Carolina
1,2,4-
Trimethylbenzene
1,2-
Dibromoethane
1,2-
DCA
2-
Methylnaphthalene 4-Isopropyltoluene Benzene Chloroform Ethyl-benzene Isobutylene MTBE Methylene
chloride Naphthalene TBA Toluene Xylene
(Total)
ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l
NCAC 2L / IMAC 400 0.0200 0.4 30 25 1 70 600 NA 20 5 6 10 600 500
Analyte
Unit
SG-1 7/12/2018 <0.30 <0.20 <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
SG-1 8/24/2020 <0.30 0.011 J <0.20 <1.0 <0.30 <0.20 <0.20 <0.30 <0.0900 <0.20 <1.0 <0.30 <10 <0.20 <0.30
Notes:
1,2-DCA - 1,2-Dichloroethan
MTBE - Methyl tert-butyl ethe
TBA - Tert-butyl alcoho
NA - Not Availabl
- Analyte detected below quanitation limits
ug/l - microgram per lite
mg/l - milligram per lite
Exceeds NCAC 2L standar
xceeds IMAC standard
Page 31 of 31
Table 7July 2023 Cluster Head Evaluations
TotalEnergies Petrochemicals and Refining USA, Inc.Facility #1760Greensboro, North Carolina
Well ID TOC DTW Head Vertical
Gradient Direction Mass Flux
Transect
Screen
Interval
Nearest
shallow well Comments
MW-A-S 903.92 20.16 883.76 none 5-35 Z1-X25 5 - 25
MW-A-I 902.43 16.92 885.51 0.18 up 37-47 37 - 47
MW-A-D 902.71 20.13 882.58 0.161 down 57-67 57 - 67
MW-A-B 899.96 17.52 882.44 0.104 down 82-92 82 - 92
MW-B-S 902.87 22.12 880.75 A(2)5-35 Z3-X80 5 - 35
MW-B-I 901.28 21.17 880.11 0.004 down 35-45 35 - 45
MW-B-D 901.18 21.29 879.89 0.0006 down 66-76 67 - 77
MW-B-B 898.57 19.00 879.57 0.009 down 96-111 96 - 111 shows upward gradient from berock to deep saprolite if ground surface elevations are used versus TOC
MW-C-S 901.77 21.74 880.03 A(1)8-38 Z4-X89 8 - 38
MW-C-I 900.29 20.98 879.31 0.041 down 41-51 41 - 51
MW-C-D 900.35 21.49 878.86 0.019 down 69-79 69 - 79
MW-C-B 897.68 19.70 877.98 0.021 down 96-130 96 - 130
MW-D-S 902.94 21.38 881.56 A(3)5-35 Z2-X31 5 - 35 historical LNAPL
MW-D-I 901.15 20.31 880.84 0.075 down 31-41 31 - 41
MW-D-D 901.06 20.62 880.44 0.011 down 67-77 67 - 77
MW-D-B 898.81 18.39 880.42 0.0006 none 96-106 96 - 106 nearly identical gradients in deep saprolite and bedrock zones, very slight downward gradient
MW-E-S 896.98 19.55 877.43 B(1)8-43 Z4-X47 8 - 43
MW-E-I 896.94 19.28 877.66 0.015 up 42-52 42 - 52
MW-E-D 897.11 19.66 877.45 0.007 down 72-82 72 - 82
MW-E-B 894.89 17.69 877.20 0.008 down 100-110 100 - 110
MW-F-S 897.55 19.54 878.01 B(2)8-43 Z4-X30 8 - 43
MW-F-I 896.86 18.11 878.75 0.065 up 37-47 37 - 47
MW-F-D 896.94 18.78 878.16 0.013 down 81-91 81 - 91
MW-F-B 895.34 17.22 878.12 0.0015 down 106-116 106 - 116
MW-G-S 898.27 21.03 877.24 B(3)18-38 Z4-X68 18 - 38
MW-G-I 898.12 18.32 879.80 0.335 up 32-42 32 - 42
MW-G-D 898.40 18.76 879.64 0.011 down 47-57 47 - 57
MW-G-B 896.78 17.20 879.58 0.002 down 74-84 74 - 84
MW-H-S 900.96 18.43 882.53 B(4)5-35 Z2-X35 5 - 35
MW-H-I 899.78 19.35 880.43 0.156 down 34-44 34 - 44
MW-H-D 899.54 15.83 883.71 0.162 up 54-64 54 - 64
MW-H-B 897.00 18.31 878.69 0.170 down 81-91 81 - 91
MW-I-S 900.96 17.85 883.11 B(5)5-35 Z2-X29 5 - 35
MW-I-I 900.21 18.57 881.64 0.069 down 42-52 42- 52
MW-I-D 900.11 18.56 881.55 0.004 down 67-77 67 - 77
MW-I-B 897.56 15.93 881.63 0.003 up 94-104 94 - 104
PMW-J-S 889.93 15.45 874.48 C(1)5-25 AMW-8S 5 - 25
PMW-J-I 888.45 15.32 873.13 0.035 down 52-62 52 - 62
PMW-J-D 888.35 15.38 872.97 0.004 down 89-99 89 - 99
PMW-J-B 885.57 12.47 873.10 0.002 down 114-126 114 - 126
PMW-K-S 893.18 14.39 878.79 C(3)3-23 SBMW-1R 3 - 23
PMW-K-I 891.75 14.00 877.75 0.050 down 33-43 33- 43
PMW-K-D 892.16 14.44 877.72 0.002 down 52-62 52 - 62
PMW-K-B 889.07 11.35 877.72 0.0 none 77-87 77 - 87 virtually identical heads in intermediate, deep and bedrock zones
PMW-L-S 892.90 11.53 881.37 C(4)3-23 AMW-10S 3 - 23
PMW-L-I 891.23 10.78 880.45 0.064 down 25-35 25 - 35
PMW-L-D 891.57 11.22 880.35 0.004 down 50-60 50 - 60
PMW-L-B 888.56 8.20 880.36 0.00036 up 75-85 75 - 85 negligible head difference from deep saprolite to bedrock
Table 7July 2023 Cluster Head Evaluations
TotalEnergies Petrochemicals and Refining USA, Inc.Facility #1760Greensboro, North Carolina
14.28 873.17 D(2)3-18 FMW-23R 3 - 18
PMW-M-I 888.48 16.09 872.39 0.028 down 40-50 40 - 50
PMW-M-D 888.10 15.74 872.36 0.0009 down 73-83 73 - 83
PMW-M-B 885.06 2.02 883.04 0.230 up 98-145 98 - 145 most shallow water depth reading ever from this bedrock well
FMW-24 888.02 14.17 873.85 D(1)5.5-20 included 5.5 - 20
FMW-24I 888.25 14.57 873.68 0.007 down 40.5-45.5 40.5 - 45.5
FMW-24D 888.11 14.55 873.56 0.005 down 60-70 60 - 70
PMW-N-S 890.35 12.99 877.36 D(4)5-25 AMW-14S 5 - 25
PMW-N-I 888.48 13.38 875.10 0.081 down 40-50 40 - 50
PMW-N-D 888.26 12.84 875.42 0.012 up 66-76 66 - 76
PMW-N-B 885.18 4.56 880.62 0.157 up 91-111 91 - 111
PMW-O-S 880.95 12.22 868.73 none 1.5-15 FPZ-11 1.5 - 15
PMW-O-I 880.66 8.03 872.63 0.094 up 50-60 50 - 60
PMW-O-D 880.10 8.73 871.37 0.030 down 92-102 92 - 102
PMW-O-B 877.39 6.21 871.18 0.005 down 116-145 116 - 145
DEM-MW-6-R 892.77 16.14 876.63 D(3)5-30 included 5 - 30
DEM-MW-6-I 891.02 14.41 876.61 0.0009 down 40.5-45.5 40.5 - 45.5
DEM-MW-6-D 891.12 14.68 876.44 0.007 down 64.5-69.5 64.5 - 69.5 not 100% certain this is constructed in bedrock
SBMW-2R 891.54 14.83 876.71 C(2)3-23 included 3 - 23
SBMW-2I 891.18 13.39 877.79 0.045 up 40-45 40 - 45
SBMW-2D 890.80 13.18 877.62 0.007 down 65-70 65 - 70
SBMW-2B 892.06 14.39 877.67 0.0018 up 93.5-98.5 93.5 - 98.5 negligible head difference from deep saprolite to bedrock
PMW-P-S 883.26 18.35 864.91 E(1)3-18 included 3 - 18
PMW-P-I 883.38 18.15 865.23 0.015 down 50-60 50 - 60
PMW-P-D 883.36 19.20 864.16 0.036 down 80-90 80 - 90
PMW-P-B 879.84 13.50 866.34 0.118 up 95-105 95 - 105
PMW-Q-S 878.60 16.72 861.88 E(2)3-18 included 3 - 18
PMW-Q-I 878.29 17.56 860.73 0.089 down 25-35 25 - 35
PMW-Q-D 878.28 18.30 859.98 0.031 down 49-59 49 - 59 negligible head difference from shallow to deep saprolite zones
PMW-Q-B 874.95 14.13 860.82 0.028 up 75.5-85 75 - 85
PMW-R-S 877.23 19.09 858.14 E(3)3-18 included 3 - 18
PMW-R-I 877.03 18.34 858.69 0.066 up 20-30 20 - 30
PMW-R-D 877.20 19.01 858.19 0.025 down 40-50 40 - 50
PMW-R-B 873.47 16.35 857.12 0.010 down 147-157 147 - 157 negligible head difference from shallow saprolite to bedrock zones
AMW-13S 883.17 9.82 873.35 none 3-18 included 3- 18
AMW-13I 882.35 9.51 872.84 0.017 down 40-45 40 - 45
AMW-13D 883.19 10.45 872.74 0.007 down 56-61 56 - 61
AMW-13B 883.77 13.13 870.64 0.074 down 85-90 85 - 90
Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendices

Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendix A – Mass Flux Figures and Tables

Appendix A
Cell# thickness (width (ft)area (ft2)K (cm/sec) Gradient TBA (mg/L) Flux (g/day) Cell# thickness (width (ft)area (ft2)K (cm/sec) Gradient TBA (mg/L) Flux (g/day)
A(1)S 19.46 85 1654.1 0.00001 0.015 0.005 0.000 C(1)S 12.45 146.1 1818.95 0.000569 0.015 0.005 0.006
A(1)I 20.89 85 1775.65 0.00009 0.012 1.300 0.21 C(1)I 37.95 146.1 5544.5 0.00961 0.012 0.005 0.257
A(1)D 19.05 85 1619.25 0.000961 0.013 7.60 12.346 C(1)D 23.50 146.1 3433.35 0.00175 0.013 0.005 0.031
A(1)B 50.80 85 4318.0 0.000475 0.013 0.005 0.011 C(1)B 27.00 146.1 3944.7 0.001043 0.013 0.005 0.021
A(2)S 16.28 80 1302.4 0.000059 0.015 0.089 0.008 C(2)S 11.27 262.1 2953.87 0.000569 0.015 0.005 0.010
A(2)I 17.45 80 1396.0 0.000019 0.012 0.40 0.010 C(2)I 23.50 262.1 6159.35 0.00022 0.012 0.420 0.566
A(2)D 20.95 80 1676.0 0.00151 0.013 30.00 79.676 C(2)D 18.59 262.1 4872.4 0.00013 0.013 0.005 0.003
A(2)B 33.7 80 2696.0 0.00070 0.013 100.00 198.975 C(2)B 24.50 262.1 6421.45 0.009615 0.013 15.00 966.791
A(3)S 17.32 74.9 1297.27 0.000569 0.015 0.110 0.098 C(3)S 11.71 208.2440.3 0.000025 0.015 0.005 0.000
A(3)I 24.8 74.9 1860.52 0.00124 0.012 0.380 0.847 C(3)I 19.91 208.4149.2 0.00025 0.012 0.005 0.005
A(3)D 23.05 74.9 1726.45 0.00211 0.013 0.005 0.019 C(3)D 14.50 208.3021.8 0.006643 0.013 0.005 0.105
A(3)B 28.60 74.9 2142.1 0.00075 0.013 0.005 0.008 C(3)B 25.00 208.5210.0 0.02376 0.013 0.005 0.646
23463.7 Transect total: 292.212 16.7% C(4)S 14.57 247.7 3608.99 0.00004 0.015 0.005 0.001
B(1)S 25.15 175.0 4401.25 0.00006 0.015 0.005 0.002 C(4)I 19.03 247.7 4713.73 0.00124 0.012 0.120 0.678
B(1)I 19.97 175.0 3494.75 0.00124 0.012 0.005 0.021 C(4)D 17.50 247.7 4334.75 0.00183 0.013 0.240 1.987
B(1)D 20.00 175.0 3500.0 0.003672 0.013 0.005 0.067 C(4)B 25.00 247.7 6192.5 0.01760 0.013 0.005 0.569
B(1)B 27.20 175.0 4760.0 0.000711 0.013 0.005 0.018 68819.9 Transect total: 971.67 55.6%
B(2)S 25.06 140.0 3508.4 0.00002 0.015 0.005 0.000 D(1)S 8.23 123.1015.5 0.000569 0.015 0.005 0.003
B(2)I 24.59 140.0 3442.6 0.000145 0.012 0.005 0.002 D(1)I 21.95 123.2708.63 0.00124 0.012 0.005 0.016
B(2)D 26.95 140.0 3773.0 0.00073 0.013 2.900 8.38 D(1)D 17.75 123.2190.35 0.00211 0.013 0.005 0.02
B(2)B 24.20 140.0 3388.0 0.00147 0.013 0.005 0.026 D(2)S 6.72 157.7 1059.7 0.000022 0.015 0.005 0.000
B(3)S 16.97 109.5 1858.22 0.000151 0.015 0.005 0.002 D(2)I 31.96 157.7 5040.09 0.00147 0.012 4.500 32.28
B(3)I 10.65 109.5 1166.1 0.00008 0.012 0.005 0.000 D(2)D 21.50 157.7 3390.55 0.00024 0.013 3.900 3.409
B(3)D 12.50 109.5 1368.75 0.010375 0.013 23.00 340.95 D(2)B 62.00 157.7 9777.4 0.000002 0.013 0.005 0.000
B(3)B 26.00 109.5 2847.0 0.019449 0.013 0.005 0.289 D(3)S 17.36 177.7 3084.87 0.00048 0.015 5.800 10.47
B(4)S 19.77 96.9 1915.71 0.000569 0.015 0.005 0.007 D(3)I 19.87 177.7 3530.9 0.00064 0.012 27.00 59.528
B(4)I 14.92 96.9 1445.75 0.000025 0.012 0.029 0.001 D(3)D 14.27 177.7 2535.7 0.00003 0.013 15.00 1.429
B(4)D 15.1 96.9 1463.19 0.00032 0.013 0.005 0.003 D(4)S 15.51 270.0 4187.7 0.000569 0.015 0.110 0.316
B(4)B 26.5 96.9 2567.85 0.003069 0.013 0.075 0.617 D(4)I 26.2 270.0 7084.8 0.00124 0.012 2.200 18.68
B(5)S 20.05 79.6 1595.9 0.000569 0.015 0.005 0.005 D(4)D 18.00 270.0 4860.0 0.00435 0.013 0.280 6.179
B(5)I 21.1 79.6 1682.7 0.00124 0.012 0.005 0.010 D(4)B 35.00 270.0 9450.0 0.000003 0.013 0.005 0.000
B(5)D 17.45 79.6 1389.02 0.00211 0.013 0.005 0.015 59916.4 Transect total: 132.34 7.6%
B(5)B 29.7 79.6 2364.12 0.00968 0.013 0.005 0.119
51932.51 Transect total: 350.545 20.1% All 4 transects total: 1746.779
denotes average value for zone
denotes non‐detect lab value, entered at one‐half detection limi
denotes low head zone per cluste
Areas for water table cells change for each distinct gauging even
No recent data ‐ used average of last 5 sampling event
TBA Flux by Cell ‐ Transect A: 292.21 g/da Transect B: 350.55 g/da Transect C: 971.68 g/da Transect D: 132.34 g/day 
change from upgradient transect: NA change from upgradient transect: 20.0% change from upgradient transect: 177.2% change from upgradient transect:‐86.4%
A (1) A (2) A (3) B (1) B (2) B (3) B (4) B (5) C (1) C (2) C (3) C (4) D (1) D (2) D (3) D (4)
shallow * ** 10.47
interm.32.28 59.528 18.68 *
deep 12.346 79.676 8.38 340.95 * * * * * * * 6.179
bedrock * 198.98 * * * * * 966.791 * NA NA
95.4% of transect flux in 2 cells ‐ one is low head 97.3% of transect flux in 1 cell which equals 2.5% of transect are 99.5% in 1 cell which equal 9.3% of transect total are
99.6% of transect flux in 3 of 12 cell 99.7% of transect flux in 2 cells ‐ neither is a low head featur
Legend:
< 0.01 g * denotes low head zone per cluste Transect‐to‐transect mass changes: TBA (g/day
0.01 ‐ 1 g Moving through A 292.212
1 ‐ 10 g Change A to B: 58.333 20% increase
10 ‐ 100 g Moving through B 350.545
100 ‐ 1000 g Change B to C: 621.133 177% increase
NA not analyzed Moving through C: 971.68
Change C to D:‐839.335 ‐86% decrease 
Moving through D 132.34  leaving system
Appendix A
Cell# Well thickness ( width (ft)area (ft2)K (cm/sec) Gradient 1,2 DCA (mg/L) Flux (g/day) Cell# thickness ( width (ft)area (ft2)K (cm/sec) Gradient 1,2 DCA (mg/L) Flux (g/day)
A(1)S 19.46 85 1654.10 0.000018 0.015 0.0001 0.0000 C(1)S 12.45 146.1 1818.95 0.000569 0.015 0.0001 0.0000
A(1)I 20.89 85 1775.65 0.000096 0.012 0.0001 0.0000 C(1)I 37.95 146.1 5544.50 0.009610 0.012 0.0001 0.0001
A(1)D 19.05 85 1619.25 0.000961 0.013 0.0001 0.0000 C(1)D 23.50 146.1 3433.35 0.001756 0.013 0.0001 0.0000
A(1)B 50.80 85 4318.00 0.000475 0.013 0.0001 0.0000 C(1)B 27.00 146.1 3944.70 0.001043 0.013 0.0001 0.0000
A(2)S 16.28 80 1302.40 0.000059 0.015 0.0001 0.0000 C(2)S 11.27 262.1 2953.87 0.000569 0.015 0.0001 0.0000
A(2)I 17.45 80 1396.00 0.000019 0.012 0.0001 0.0000 C(2)I 23.50 262.1 6159.35 0.000227 0.012 0.0088 0.0001
A(2)D 20.95 80 1676.00 0.001518 0.013 0.004 0.0001 C(2)D 18.59 262.1 4872.44 0.000137 0.013 0.0001 0.0000
A(2)B 33.7 80 2696.00 0.000707 0.013 0.0018 0.0000 C(2)B 24.50 262.1 6421.45 0.009615 0.013 0.018 0.0144
A(3)S 17.32 74.9 1297.27 0.000569 0.015 0.0001 0.0000 C(3)S 11.71 208.4 2440.36 0.000025 0.015 0.0001 0.0000
A(3)I 24.84 74.9 1860.52 0.001244 0.012 0.0001 0.0000 C(3)I 19.91 208.4 4149.24 0.000256 0.012 0.0072 0.0001
A(3)D 23.05 74.9 1726.45 0.002117 0.013 0.0001 0.0000 C(3)D 14.50 208.4 3021.80 0.006643 0.013 0.0016 0.0004
A(3)B 28.60 74.9 2142.14 0.000758 0.013 0.0001 0.0000 C(3)B 25.00 208.4 5210.00 0.023767 0.013 0.0006 0.0010
Transect total: 0.0002 0.6% C(4)S 14.57 247.7 3608.99 0.000044 0.015 0.0001 0.0000
B(1)S 25.15 175.0 4401.25 0.000066 0.015 0.0001 0.0000 C(4)I 19.03 247.7 4713.73 0.001244 0.012 0.0013 0.0001
B(1)I 19.97 175.0 3494.75 0.001244 0.012 0.0001 0.0000 C(4)D 17.50 247.7 4334.75 0.001830 0.013 0.0039 0.0004
B(1)D 20.00 175.0 3500.00 0.003672 0.013 0.012 0.0020 C(4)B 25.00 247.7 6192.50 0.017604 0.013 0.0001 0.0001
B(1)B 27.20 175.0 4760.00 0.000711 0.013 0.0001 0.0000 Transect total: 0.0168 48.9%
B(2)S 25.06 140.0 3508.40 0.000020 0.015 0.0001 0.0000 D(1)S 8.23 123.4 1015.58 0.000569 0.015 0.0001 0.0000
B(2)I 24.59 140.0 3442.60 0.000145 0.012 0.0001 0.0000 D(1)I 21.95 123.4 2708.63 0.001244 0.012 0.0001 0.0000
B(2)D 26.95 140.0 3773.00 0.000734 0.013 0.010 0.0004 D(1)D 17.75 123.4 2190.35 0.002117 0.013 0.0001 0.0000
B(2)B 24.20 140.0 3388.00 0.001476 0.013 0.0001 0.0000 D(2)S 6.72 157.7 1059.74 0.000022 0.015 0.0001 0.0000
B(3)S 16.97 109.5 1858.22 0.000151 0.015 0.0001 0.0000 D(2)I 31.96 157.7 5040.09 0.001477 0.012 0.074 0.0066
B(3)I 10.65 109.5 1166.18 0.000086 0.012 0.0001 0.0000 D(2)D 21.50 157.7 3390.55 0.000247 0.013 0.066 0.0007
B(3)D 12.50 109.5 1368.75 0.010375 0.013 0.0001 0.0000 D(2)B 62.00 157.7 9777.40 0.000002 0.013 0.0001 0.0000
B(3)B 26.00 109.5 2847.00 0.019449 0.013 0.0001 0.0001 D(3)S 17.36 177.7 3084.87 0.000486 0.015 0.0001 0.0000
B(4)S 19.77 96.9 1915.71 0.000569 0.015 0.0001 0.0000 D(3)I 19.87 177.7 3530.90 0.000648 0.012 0.140 0.0038
B(4)I 14.92 96.9 1445.75 0.000025 0.012 0.0001 0.0000 D(3)D 14.27 177.7 2535.78 0.000036 0.013 0.0001 0.0000
B(4)D 15.1 96.9 1463.19 0.000328 0.013 0.0001 0.0000 D(4)S 15.51 270.0 4187.70 0.000569 0.015 0.0074 0.0003
B(4)B 26.5 96.9 2567.85 0.003069 0.013 0.0001 0.0000 D(4)I 26.24 270.0 7084.80 0.001244 0.012 0.022 0.0023
B(5)S 20.05 79.6 1595.98 0.000569 0.015 0.0001 0.0000 D(4)D 18.00 270.0 4860.00 0.004350 0.013 0.0040 0.0011
B(5)I 21.14 79.6 1682.74 0.001244 0.012 0.0001 0.0000 D(4)B 35.00 270.0 9450.00 0.000003 0.013 0.0001 0.0000
B(5)D 17.45 79.6 1389.02 0.002117 0.013 0.0001 0.0000 Transect total: 0.0149 43.3%
B(5)B 29.7 79.6 2364.12 0.009680 0.013 0.0001 0.0000
Transect total: 0.0025 7.3%All 4 transects total: 0.034
denotes average value for zone
denotes non‐detect lab value, entered at one‐half detection limit Unlike the petroleum compounds, the 1,2 DCA fluxes across alll 4 transects are of the same order of magnitude ‐ and all quite low
denotes low head zone per cluster This coupled with the correlation between detectable flux and low head zones in the off‐site transects (C & D) suggests a regional, 
Areas for water table cells change for each distinct gauging event low level presence of this compound.
1,2 DCA Flux by Cell ‐ Transect A (0.0002 g/day total) Transect B (0.0025 g/day total) Transect C (0.0168 g/day total) Transect D (0.0149 g/day total)
change from upgradient transect: NA change from upgradient transect: 1209.2% change from upgradient transect: 566.0% change from upgradient transect:‐11.5%
A (1) A (2) A (3) B (1) B (2) B (3) B (4) B (5) C (1) C (2) C (3) C (4) D (1) D (2) D (3) D (4)
shallow * * * *
interm.*
deep * * * * * *
bedrock * * * * * * NA NA
Legend:
no flux some flux measured in 19 of 62 cells (31%), 15 of these 19 cells (79%) are in the off‐site wells ‐ C & D transects. 11 of the total flux detections (58%) are deep or bedrock zones,  
any detection but most align with low head flow as 4 of 6 detections in transect D are in shallow or intermediate zones
NA not analyzed Some detectable 1,2 DCA mass flux is found in 5 of 9 off‐site low head zones ‐ suggesting a regional source?  This was not the case for TBA.
1,2‐DCA flux is within one order of magnitude across all transects, and is primarily measured off site. 
*  denotes low head zone in cluster Transect‐to‐transect mass changes: 1,2 DCA (g/day)
Moving through A: 0.0002
Change A to B: 0.0023 1209% increase
Moving through B: 0.0025
Change B to C: 0.014281 566% increase
Moving through C: 0.0168
Change C to D:‐0.00193 ‐11% decrease
Moving through D: 0.0149  leaving system
Appendix A
Cell# Well thickness (width (ft)area (ft2)K (cm/sec) Gradient MTBE (mg/L) Flux (g/day) Cell# Well thickness (width (ft)area (ft2)K (cm/sec) Gradient MTBE (mg/L) Flux (g/day)
A(1)S Z4‐X89 19.46 85 1654.10 0.000018 0.015 0.0001 0.0000 C(1)S 12.45 146.1 1818.95 0.000569 0.015 0.0001 0.0000
A(1)I C‐I 20.89 85 1775.65 0.000096 0.012 0.0001 0.0000 C(1)I 37.95 146.1 5544.50 0.009610 0.012 0.0001 0.0001
A(1)D C‐D 19.05 85 1619.25 0.000961 0.013 0.200 0.0040 C(1)D 23.50 146.1 3433.35 0.001756 0.013 0.0001 0.0000
A(1)B C‐B 50.80 85 4318.00 0.000475 0.013 0.0001 0.0000 C(1)B 27.00 146.1 3944.70 0.001043 0.013 0.0001 0.0000
A(2)S Z3‐X80 16.28 80 1302.40 0.000059 0.015 0.0001 0.0000 C(2)S 11.27 262.1 2953.87 0.000569 0.015 0.0001 0.0000
A(2)I B‐I 17.45 80 1396.00 0.000019 0.012 0.0001 0.0000 C(2)I 23.50 262.1 6159.35 0.000227 0.012 0.0001 0.0000
A(2)D B‐D 20.95 80 1676.00 0.001518 0.013 0.180 0.0060 C(2)D 18.59 262.1 4872.44 0.000137 0.013 0.0001 0.0000
A(2)B B‐B 33.7 80 2696.00 0.000707 0.013 0.0001 0.0000 C(2)B 24.50 262.1 6421.45 0.009615 0.013 0.250 0.2007
A(3)S Z2‐X31 17.32 74.9 1297.27 0.000569 0.015 0.0001 0.0000 C(3)S 11.71 208.4 2440.36 0.000025 0.015 0.0001 0.0000
A(3)I D‐I 24.84 74.9 1860.52 0.001244 0.012 0.0001 0.0000 C(3)I 19.91 208.4 4149.24 0.000256 0.012 0.0001 0.0000
A(3)D D‐D 23.05 74.9 1726.45 0.002117 0.013 0.230 0.0109 C(3)D 14.50 208.4 3021.80 0.006643 0.013 0.037 0.0097
A(3)B D‐B 28.60 74.9 2142.14 0.000758 0.013 0.0001 0.0000 C(3)B 25.00 208.4 5210.00 0.023767 0.013 0.014 0.0225
Transect total: 0.021 5.30% C(4)S 14.57 247.7 3608.99 0.000044 0.015 0.0001 0.0000
B(1)S Z4‐X47 25.15 175.0 4401.25 0.000066 0.015 0.0001 0.0000 C(4)I 19.03 247.7 4713.73 0.001244 0.012 0.013 0.0009
B(1)I E‐I 19.97 175.0 3494.75 0.001244 0.012 0.0001 0.0000 C(4)D 17.50 247.7 4334.75 0.001830 0.013 0.043 0.0044
B(1)D E‐D 20.00 175.0 3500.00 0.003672 0.013 0.0001 0.0000 C(4)B 25.00 247.7 6192.50 0.017604 0.013 0.0001 0.0001
B(1)B E‐B 27.20 175.0 4760.00 0.000711 0.013 0.0001 0.0000 Transect total: 0.2384 60.37%
B(2)S Z4‐X30 25.06 140.0 3508.40 0.000020 0.015 0.0001 0.0000 D(1)S 8.23 123.4 1015.58 0.000569 0.015 0.0033 0.0000
B(2)I F‐I 24.59 140.0 3442.60 0.000145 0.012 0.0001 0.0000 D(1)I 21.95 123.4 2708.63 0.001244 0.012 0.0001 0.0000
B(2)D F‐D 26.95 140.0 3773.00 0.000734 0.013 0.044 0.0016 D(1)D 17.75 123.4 2190.35 0.002117 0.013 0.0001 0.0000
B(2)B F‐B 24.20 140.0 3388.00 0.001476 0.013 0.0001 0.0000 D(2)S 6.72 157.7 1059.74 0.000022 0.015 0.0001 0.0000
B(3)S Z4‐X68 16.97 109.5 1858.22 0.000151 0.015 0.0001 0.0000 D(2)I 31.96 157.7 5040.09 0.001477 0.012 0.048 0.0043
B(3)I G‐I 10.65 109.5 1166.18 0.000086 0.012 0.0035 0.0000 D(2)D 21.50 157.7 3390.55 0.000247 0.013 0.047 0.0005
B(3)D G‐D 12.50 109.5 1368.75 0.010375 0.013 0.480 0.0886 D(2)B 62.00 157.7 9777.40 0.000002 0.013 0.0001 0.0000
B(3)B G‐B 26.00 109.5 2847.00 0.019449 0.013 0.0001 0.0001 D(3)S 17.36 177.7 3084.87 0.000486 0.015 0.031 0.0007
B(4)S Z2‐X35 19.77 96.9 1915.71 0.000569 0.015 0.0001 0.0000 D(3)I 19.87 177.7 3530.90 0.000648 0.012 0.260 0.0071
B(4)I H‐I 14.92 96.9 1445.75 0.000025 0.012 0.0001 0.0000 D(3)D 14.27 177.7 2535.78 0.000036 0.013 0.400 0.0005
B(4)D H‐D 15.1 96.9 1463.19 0.000328 0.013 0.0001 0.0000 D(4)S 15.51 270.0 4187.70 0.000569 0.015 0.0039 0.0001
B(4)B H‐B 26.5 96.9 2567.85 0.003069 0.013 0.011 0.0011 D(4)I 26.24 270.0 7084.80 0.001244 0.012 0.034 0.0036
B(5)S Z2‐X29 20.05 79.6 1595.98 0.000569 0.015 0.0001 0.0000 D(4)D 18.00 270.0 4860.00 0.004350 0.013 0.099 0.0272
B(5)I I‐I 21.14 79.6 1682.74 0.001244 0.012 0.0001 0.0000 D(4)B 35.00 270.0 9450.00 0.000003 0.013 0.0001 0.0000
B(5)D I‐D 17.45 79.6 1389.02 0.002117 0.013 0.0001 0.0000 Transect total: 0.0441 11.16%
B(5)B I‐B 29.7 79.6 2364.12 0.009680 0.013 0.0001 0.0000
Transect total: 0.0915 23.16%All 4 transects total: 0.395
denotes average value for zon
denotes non‐detect lab value, entered at one‐half detection limi
denotes low head zone per cluste Detectable flux in 22 of 62 cells (35%), but only one cell has a value greater than 0.1 g/da
Areas for water table cells change for each distinct gauging even Site‐wide, 60% of total crosses transect C, suggesting the source is primarily downgradient of the 
former Total terminal ‐ beneath the RR tracks and highway. Low flux via low head zone
MTBE Flux by Cell ‐ Transect A (0.021 g/day total) Transect B (0.0915 g/day total) Transect C (0.2384 g/day total) Transect D (0.0441 g/day total)
change from upgradient transect: NA change from upgradient transect: 336.9% reduction from upgradient transect: 160.7% reduction from upgradient transect:‐81.5%
A (1) A (2) A (3) B (1) B (2) B (3) B (4) B (5) C (1) C (2) C (3) C (4) D (1) D (2) D (3) D (4)
shallow * * * *
interm.*
deep 0.0886 * * * * * *
bedrock * * * * * 0.2007 * NA NA
Legend:
< 0.001 g
0.001 ‐ 0.01 g *  denotes low head zone in cluste Transect‐to‐transect mass changes: MTBE (g/day)
0.01 ‐ 0.1 g Moving through A: 0.021
0.1 ‐ 1.0 g Change A to B: 0.0705 337% increase 
NA not analyzed Moving through B: 0.0915
Change B to C: 0.147 161% increase 
Moving through C: 0.238
Change C to D:‐0.194 ‐82% decrease 
Moving through D: 0.0441  leaving the system
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
A'A
A(1)S
A(1)I
A(1)D
A(1)B*
A(2)S
A(2)I
A(2)D
A(2)B*
A(3)S
A(3)I
A(3)D*
A(3)B
MW
-
D
-
D
MW
-
D
-
B
MW
-
D
-
I
MW
-
B
-
I
MW
-
B
-
D
MW
-
B
-
B
MW
-
C
-
D
MW
-
C
-
B
MW
-
C
-
I
Z4
-
X
8
9
Z3
-
X
8
0
Z2
-
X
3
1
05/15/24
Designed
Date
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
D.B.
R.E.J.
Appendix AFigure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.
LEGEND
WELL
SCREEN
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
75'
GROUNDWATER ELEVATION
A(2)B MASS FLUX CELL IDENTIFICATION
TBA MASS FLUX
CROSS SECTION A-A'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
TBA FLUX (g/day)
0
0.01
10
100
1
1
1,000
10,000
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

A
-
A
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
B'B
B(1)S
B(1)I
B(1)D*
B(1)B
B(2)S*
B(2)I
B(2)D
B(2)B
B(3)S*
B(3)I
B(3)D
B(3)B
B(4)S
B(4)I
B(4)D
B(5)B*
B(5)S
B(5)I
B(5)D*
B(5)B
Z4
-
X
3
0
MW
-
E
-
D
MW
-
E
-
B
MW
-
E
-
I
Z4
-
X
4
7
Z4
-
X
6
8
MW
-
F
-
I
MW
-
F
-
B
MW
-
F
-
D
MW
-
G
-
I
MW
-
G
-
B
MW
-
G
-
D
MW
-
H
-
I
MW
-
H
-
B
MW
-
H
-
D
Z2
-
X
3
5
MW
-
I
-
I
MW
-
I
-
B
MW
-
I
-
D
Z2
-
X
2
9
Designed
Date
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
D.B.Appendix AFigure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
50'
TBA MASS FLUX
CROSS SECTION B-B'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
LEGEND
WELL
SCREEN
GROUNDWATER ELEVATION
B(2)B MASS FLUX CELL IDENTIFICATION
TBA FLUX (g/day)
0
0.01
10
100
1
1
1,000
10,000
05/15/24R.E.J.
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

B
-
B
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
C'C
C(1)S
C(1)I
C(1)D*
C(1)B
C(2)S
C(2)I
C(2)D*
C(2)B
C(3)S
C(3)I
C(3)D*
C(3)B
C(4)S
C(4)I
C(4)D*
C(4)B
AM
W
-
1
2
S
PM
W
-
J
-
B
PM
W
-
J
-
I
PM
W
-
J
-
D
AM
W
-
8
S
SB
M
W
-
2
B
SB
M
W
-
2
I
SB
M
W
-
2
D
SB
M
W
-
2
R
SB
M
W
-
1
R
PM
W
-
K
-
B
PM
W
-
K
-
D
PM
W
-
K
-
I
AM
W
-
1
0
S
PM
W
-
L
-
B
PM
W
-
L
-
D
PM
W
-
L
-
I
Designed
Date
SITE A
GREENSBORO, NORTH CAROLINA
D.B.
Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
TBA MASS FLUX
CROSS SECTION C-C'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
3. ARROW ACROSS VERTICALLY ADJACENT ZONES
DEPICTS VERTICAL HYDRAULIC GRADIENT
WHERE ARROW LENGTH IS PROPORTIONAL TO
MAGNITUDE
LEGEND
WELL
SCREEN
GROUNDWATER ELEVATION
C(2)B MASS FLUX CELL IDENTIFICATION
TBA FLUX (g/day)
0
0.01
10
100
1
1
1,000
10,000
05/15/24R.E.J.
Appendix A
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

C
-
C
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
900
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
D'D
D(2)S
D(2)I
D(2)D*
D(2)B
D(3)S
D(3)I
D(3)D*
D(4)S
D(4)I*
D(4)D
D(4)B
D(1)S
D(1)I
D(1)D*
FM
W
-
2
3
R
AM
W
-
1
4
S
FM
W
-
2
2
FM
W
-
2
4
D
FM
W
-
2
4
FM
W
-
2
4
I
PM
W
-
M
-
I
PM
W
-
M
-
D
PM
W
-
M
-
B
PM
W
-
N
-
I
PM
W
-
N
-
B
PM
W
-
N
-
D
DE
M
-
M
W
6
R
DE
M
-
M
W
6
D
DE
M
-
M
W
6
I
NA
NA
Designed
Date
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
D.B.
Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
TBA MASS FLUX
CROSS SECTION D-D'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
TBA MASS FLUX
CROSS SECTION C-C'
LEGEND
WELL
SCREEN
GROUNDWATER ELEVATION
D(2)B MASS FLUX CELL IDENTIFICATION
TBA FLUX (g/day)
0
0.01
10
100
1
1
1,000
10,000
05/15/24R.E.J.
Appendix A
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

D
-
D
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
A'A
A(1)S
A(1)I
A(1)D
A(1)B*
A(2)S
A(2)I
A(2)D
A(2)B*
A(3)S
A(3)I
A(3)D*
A(3)B
MW
-
D
-
D
MW
-
D
-
B
MW
-
D
-
I
MW
-
B
-
I
MW
-
B
-
D
MW
-
B
-
B
MW
-
C
-
D
MW
-
C
-
B
MW
-
C
-
I
Z4
-
X
8
9
Z3
-
X
8
0
Z2
-
X
3
1
05/15/24
Designed
Date
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
D.B.
R.E.J.
Appendix AFigure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.
LEGEND
WELL
SCREEN
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
75'
GROUNDWATER ELEVATION
A(2)B MASS FLUX CELL IDENTIFICATION
1,2 DCA MASS FLUX
CROSS SECTION A-A'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
1,2-DCA FLUX (g/day)
NO FLUX
ANY DETECTION
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

A
-
A
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
B'B
B(1)S
B(1)I
B(1)D*
B(1)B
B(2)S*
B(2)I
B(2)D
B(2)B
B(3)S*
B(3)I
B(3)D
B(3)B
B(4)S
B(4)I
B(4)D
B(5)B*
B(5)S
B(5)I
B(5)D*
B(5)B
Z4
-
X
3
0
MW
-
E
-
D
MW
-
E
-
B
MW
-
E
-
I
Z4
-
X
4
7
Z4
-
X
6
8
MW
-
F
-
I
MW
-
F
-
B
MW
-
F
-
D
MW
-
G
-
I
MW
-
G
-
B
MW
-
G
-
D
MW
-
H
-
I
MW
-
H
-
B
MW
-
H
-
D
Z2
-
X
3
5
MW
-
I
-
I
MW
-
I
-
B
MW
-
I
-
D
Z2
-
X
2
9
Designed
Date
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
D.B.Appendix AFigure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
50'
1,2 DCA MASS FLUX
CROSS SECTION B-B'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
LEGEND
WELL
SCREEN
GROUNDWATER ELEVATION
B(2)B MASS FLUX CELL IDENTIFICATION
05/15/24R.E.J.
1,2-DCA FLUX (g/day)
NO FLUX
ANY DETECTION
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

B
-
B
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
C'C
C(1)S
C(1)I
C(1)D*
C(1)B
C(2)S
C(2)I
C(2)D*
C(2)B
C(3)S
C(3)I
C(3)D*
C(3)B
C(4)S
C(4)I
C(4)D*
C(4)B
AM
W
-
1
2
S
PM
W
-
J
-
B
PM
W
-
J
-
I
PM
W
-
J
-
D
AM
W
-
8
S
SB
M
W
-
2
B
SB
M
W
-
2
I
SB
M
W
-
2
D
SB
M
W
-
2
R
SB
M
W
-
1
R
PM
W
-
K
-
B
PM
W
-
K
-
D
PM
W
-
K
-
I
AM
W
-
1
0
S
PM
W
-
L
-
B
PM
W
-
L
-
D
PM
W
-
L
-
I
Designed
Date
SITE A
GREENSBORO, NORTH CAROLINA
D.B.
Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
1,2 DCA MASS FLUX
CROSS SECTION C-C'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
3. ARROW ACROSS VERTICALLY ADJACENT ZONES
DEPICTS VERTICAL HYDRAULIC GRADIENT
WHERE ARROW LENGTH IS PROPORTIONAL TO
MAGNITUDE
LEGEND
WELL
SCREEN
GROUNDWATER ELEVATION
C(2)B MASS FLUX CELL IDENTIFICATION
05/15/24R.E.J.
1,2-DCA FLUX (g/day)
NO FLUX
ANY DETECTION
Appendix A
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

C
-
C
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
900
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
D'D
D(2)S
D(2)I
D(2)D*
D(2)B
D(3)S
D(3)I
D(3)D*
D(4)S
D(4)I*
D(4)D
D(4)B
D(1)S
D(1)I
D(1)D*
FM
W
-
2
3
R
AM
W
-
1
4
S
FM
W
-
2
2
FM
W
-
2
4
D
FM
W
-
2
4
FM
W
-
2
4
I
PM
W
-
M
-
I
PM
W
-
M
-
D
PM
W
-
M
-
B
PM
W
-
N
-
I
PM
W
-
N
-
B
PM
W
-
N
-
D
DE
M
-
M
W
6
R
DE
M
-
M
W
6
D
DE
M
-
M
W
6
I
NA
NA
Designed
Date
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
D.B.
Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
1,2 DCA MASS FLUX
CROSS SECTION D-D'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
LEGEND
WELL
SCREEN
GROUNDWATER ELEVATION
D(2)B MASS FLUX CELL IDENTIFICATION
05/15/24R.E.J.
1,2-DCA FLUX (g/day)
NO FLUX
ANY DETECTION
Appendix A
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

D
-
D
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
A'A
A(1)S
A(1)I
A(1)D
A(1)B*
A(2)S
A(2)I
A(2)D
A(2)B*
A(3)S
A(3)I
A(3)D*
A(3)B
MW
-
D
-
D
MW
-
D
-
B
MW
-
D
-
I
MW
-
B
-
I
MW
-
B
-
D
MW
-
B
-
B
MW
-
C
-
D
MW
-
C
-
B
MW
-
C
-
I
Z4
-
X
8
9
Z3
-
X
8
0
Z2
-
X
3
1
05/15/24
Designed
Date
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
D.B.
R.E.J.
Appendix AFigure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.
LEGEND
WELL
SCREEN
SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
75'
GROUNDWATER ELEVATION
A(2)B MASS FLUX CELL IDENTIFICATION
MTBE MASS FLUX
CROSS SECTION A-A'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
MTBE FLUX (g/day)
0
0.001
0.01
0.1
1
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

A
-
A
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
B'B
B(1)S
B(1)I
B(1)D*
B(1)B
B(2)S*
B(2)I
B(2)D
B(2)B
B(3)S*
B(3)I
B(3)D
B(3)B
B(4)S
B(4)I
B(4)D
B(5)B*
B(5)S
B(5)I
B(5)D*
B(5)B
Z4
-
X
3
0
MW
-
E
-
D
MW
-
E
-
B
MW
-
E
-
I
Z4
-
X
4
7
Z4
-
X
6
8
MW
-
F
-
I
MW
-
F
-
B
MW
-
F
-
D
MW
-
G
-
I
MW
-
G
-
B
MW
-
G
-
D
MW
-
H
-
I
MW
-
H
-
B
MW
-
H
-
D
Z2
-
X
3
5
MW
-
I
-
I
MW
-
I
-
B
MW
-
I
-
D
Z2
-
X
2
9
Designed
Date
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
D.B.Appendix AFigure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
50'
MTBE MASS FLUX
CROSS SECTION B-B'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
LEGEND
WELL
SCREEN
GROUNDWATER ELEVATION
B(2)B MASS FLUX CELL IDENTIFICATION
05/15/24R.E.J.
MTBE FLUX (g/day)
0
0.001
0.01
0.1
1
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

B
-
B
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
C'C
C(1)S
C(1)I
C(1)D*
C(1)B
C(2)S
C(2)I
C(2)D*
C(2)B
C(3)S
C(3)I
C(3)D*
C(3)B
C(4)S
C(4)I
C(4)D*
C(4)B
AM
W
-
1
2
S
PM
W
-
J
-
B
PM
W
-
J
-
I
PM
W
-
J
-
D
AM
W
-
8
S
SB
M
W
-
2
B
SB
M
W
-
2
I
SB
M
W
-
2
D
SB
M
W
-
2
R
SB
M
W
-
1
R
PM
W
-
K
-
B
PM
W
-
K
-
D
PM
W
-
K
-
I
AM
W
-
1
0
S
PM
W
-
L
-
B
PM
W
-
L
-
D
PM
W
-
L
-
I
Designed
Date
SITE A
GREENSBORO, NORTH CAROLINA
D.B.
Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
MTBE MASS FLUX
CROSS SECTION C-C'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
3. ARROW ACROSS VERTICALLY ADJACENT ZONES
DEPICTS VERTICAL HYDRAULIC GRADIENT
WHERE ARROW LENGTH IS PROPORTIONAL TO
MAGNITUDE
LEGEND
WELL
SCREEN
GROUNDWATER ELEVATION
C(2)B MASS FLUX CELL IDENTIFICATION
05/15/24R.E.J.
MTBE FLUX (g/day)
0
0.001
0.01
0.1
1
Appendix A
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

C
-
C
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
900
720
740
760
720
740
760
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
920
880
860
840
820
800
780
El
e
v
a
t
i
o
n

i
n

F
e
e
t

M
S
L
900
920
880
860
840
820
800
D'D
D(2)S
D(2)I
D(2)D*
D(2)B
D(3)S
D(3)I
D(3)D*
D(4)S
D(4)I*
D(4)D
D(4)B
D(1)S
D(1)I
D(1)D*
FM
W
-
2
3
R
AM
W
-
1
4
S
FM
W
-
2
2
FM
W
-
2
4
D
FM
W
-
2
4
FM
W
-
2
4
I
PM
W
-
M
-
I
PM
W
-
M
-
D
PM
W
-
M
-
B
PM
W
-
N
-
I
PM
W
-
N
-
B
PM
W
-
N
-
D
DE
M
-
M
W
6
R
DE
M
-
M
W
6
D
DE
M
-
M
W
6
I
NA
NA
Designed
Date
TOTAL PETROCHEMICALS USA, INC.
FACILITY #1760
GREENSBORO, NORTH CAROLINA
D.B.
Figure
Drawn
Groundwater & Environmental Services, Inc.
Approved
C.M.SCALE IN FEET
HORIZONTAL
VERTICAL
1" =
1" =
150'
25'
MTBE MASS FLUX
CROSS SECTION D-D'
NOTES:
1. VERTICAL EXAGGERATION = 2X
2. ASTERISK (*) DENOTES THE LOW HEAD CELL IN
EACH CLUSTER
LEGEND
WELL
SCREEN
GROUNDWATER ELEVATION
D(2)B MASS FLUX CELL IDENTIFICATION
05/15/24R.E.J.
MTBE FLUX (g/day)
0
0.001
0.01
0.1
1
Appendix A
N:\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
C
A
D
\
2
0
2
4
\
2
0
2
4
-
0
5
\
T
P
U
_
G
r
e
e
n
s
b
o
r
o
_
m
a
s
s
_
f
l
u
x
_
s
e
c
t
i
o
n
s
.
d
w
g
,

D
-
D
'
,

r
a
j
o
n
e
s
,

D
W
G

T
o

P
D
F
.
p
c
3
,

A
N
S
I

f
u
l
l

b
l
e
e
d

B

(
1
7
.
0
0

x

1
1
.
0
0

I
n
c
h
e
s
)
,

1
:
1
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
T
r
a
n
s
e
c
t
s
_
C
r
o
s
s
_
S
e
c
t
i
o
n
s
_
J
u
n
e
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
1
,
1
7
7

-

5
/
1
5
/
2
0
2
4

8
:
4
6
:
2
1

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

M
i
c
h
i
g
a
n

C
e
n
t
r
a
l

F
I
P
S

2
1
1
2

F
e
e
t
Legend
Transects
A - A'B -B'
C - C'
D - D'
+/+/+/+/+/+/Railroad
Ground SurfaceAbove Mass Flux
W. MARKET STR
E
E
T
DCA Flux (g/day)
Note:Vertical profiles extend to a depth of 120 feet.Oblique projection.
Drawn 5/15/24
Mass Flux Profiles for 1,2-DichloroethaneJune 2023
Designed
Approved
FigureAppendix A
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
Any Detection
No Flux
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
T
r
a
n
s
e
c
t
s
_
C
r
o
s
s
_
S
e
c
t
i
o
n
s
_
J
u
n
e
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
1
,
1
7
7

-

5
/
1
5
/
2
0
2
4

8
:
2
4
:
0
8

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

M
i
c
h
i
g
a
n

C
e
n
t
r
a
l

F
I
P
S

2
1
1
2

F
e
e
t
Legend
Transects
A - A'
B -B'C - C'D - D'
+/+/+/+/+/+/Railroad
Ground SurfaceAbove Mass Flux
W. MARKET STR
E
E
T
MTBE Flux (g/day)
Note:Vertical profiles extend to a depth of 120 feet.Oblique projection.
Drawn 5/15/24
Mass Flux Profiles for Methyl Tert Butyl EtherJune 2023
Designed
Approved
FigureAppendix A
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
< 0.0001
N:
\
B
l
a
c
k
s
b
u
r
g
\
P
r
o
j
e
c
t
s
\
T
P
U
\
G
r
e
e
n
s
b
o
r
o
N
C
\
G
I
S
\
G
r
e
e
n
s
b
o
r
o
_
T
r
a
n
s
e
c
t
s
_
C
r
o
s
s
_
S
e
c
t
i
o
n
s
_
J
u
n
e
2
0
2
3
.
m
x
d

-

S
c
a
l
e

1
:
1
,
1
7
7

-

5
/
1
5
/
2
0
2
4

7
:
5
0
:
5
3

A
M

-

G
S
t
e
w
a
r
t

-

N
A
D

1
9
8
3

S
t
a
t
e
P
l
a
n
e

M
i
c
h
i
g
a
n

C
e
n
t
r
a
l

F
I
P
S

2
1
1
2

F
e
e
t
Legend
Transects
A - A'B -B'
C - C'
D - D'
+/+/+/+/+/+/Railroad
Ground SurfaceAbove Mass Flux
W. MARKET STR
E
E
T
TBA Flux (g/day)
Note:Vertical profiles extend to a depth of 120 feet.Oblique projection.
Drawn 5/15/24
Mass Flux Profiles for Tert Butyl AlcoholJune 2023
Designed
Approved
FigureAppendix A
GKS
DMC
DB
Date
Groundwater & Environmental Services, Inc.
< 0.01
Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendix B – Historical Plume Delineation Map

Groundwater & Environmental Services, Inc.
P:\TPU\GreensboroNC\GIS\Greensboro_FID.mxd - Scale 1:3,000 - 10/25/2013 10:39:08 AM - rbannister - NAD 1983 StatePlane North Carolina FIPS 3200 Feet
Existing Recovery System
FID Responseat 880 ft MSL
Existing Recovery System
FID Responseat 875 ft MSL
Existing Recovery System
FID Responseat 865 ft MSL
MIPs response at P-11 not utilized since not part of ATOFINA plume
Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendix C – Groundwater Sampling Forms (July
2023)

Pump had too much interference to collect
accurate DTW's
Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendix D – Groundwater Sampling Forms
(December 2023/February 2024)

Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendix E – Laboratory Analytical Report –
Groundwater (July 2023)

July 31, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 11 sample(s) on Jul 18, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23070922
Project Manager
Generated By: DAYNA.FISHER
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 41
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23070922
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23070922-01 17-Jul-2023 11:32 18-Jul-2023 09:25Z2-X29 Groundwater
HS23070922-02 17-Jul-2023 12:15 18-Jul-2023 09:25MW-I-I Groundwater
HS23070922-03 17-Jul-2023 12:45 18-Jul-2023 09:25MW-I-D Groundwater
HS23070922-04 17-Jul-2023 13:35 18-Jul-2023 09:25MW-I-B Groundwater
HS23070922-05 17-Jul-2023 14:42 18-Jul-2023 09:25MW-C-I Groundwater
HS23070922-06 17-Jul-2023 15:40 18-Jul-2023 09:25MW-C-D Groundwater
HS23070922-07 17-Jul-2023 15:27 18-Jul-2023 09:25MW-C-B Groundwater
HS23070922-08 17-Jul-2023 15:15 18-Jul-2023 09:25Field Blank #1 Water
HS23070922-09 17-Jul-2023 15:25 18-Jul-2023 09:25Equipment Blank #1 Water
HS23070922-10 17-Jul-2023 00:00 18-Jul-2023 09:25Trip Blank Water
HS23070922-11 17-Jul-2023 14:50 18-Jul-2023 09:25Field Dup #1 Groundwater
ALS Houston, US 31-Jul-23Date:
Page 2 of 41
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23070922
Work Order Comments
Login notes:
Sample #9 - ID = Equip. Blank - 2 x voa neat Vials rec'd Broken. ! remains for analysis
•
Per client email on July 20, 2023 add the MNA parameters to samples MW-C-D, Equipment Blank #1, and Field Blank #1. Ferrous
Iron will be performed outside the holding time and will be "H" flagged. Data for this should be considered estimated.
•
ECD Organics by Method SW8011
Batch ID: 197842
Sample ID: MBLK-197842
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R442316
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R441892
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R441787
Sample ID: Z2-X29 (HS23070922-01MS)
MS and/or MSD recovered outside control limits for multiple compounds•
Metals by Method SW6020A
Batch ID: 198234
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Wet Chemistry by Method E300
Batch ID: R442693
Sample ID: HS23071518-01MS
MS and MSD are for an unrelated sample•
WetChemistry by Method SM2320B
Batch ID: R442736
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 31-Jul-23Date:
Page 3 of 41
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23070922
WetChemistry by Method E300
Batch ID: R441876
Sample ID: Equipment Blank #1 (HS23070922-09)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Field Blank #1 (HS23070922-08)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Field Dup #1 (HS23070922-11)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-C-B (HS23070922-07)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-C-D (HS23070922-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-C-I (HS23070922-05)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-I-B (HS23070922-04)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441843
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 31-Jul-23Date:
Page 4 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-X29
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-01
17-Jul-2023 11:32 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 19-Jul-2023 23:160.301,2,4-Trimethylbenzene 1.0U
1ug/L 19-Jul-2023 23:160.201,2-Dibromoethane 1.0U
1ug/L 19-Jul-2023 23:160.201,2-Dichloroethane 1.0U
1ug/L 19-Jul-2023 23:161.02-Methylnaphthalene 1.0U
1ug/L 19-Jul-2023 23:160.304-Isopropyltoluene 1.0U
1ug/L 19-Jul-2023 23:160.20Benzene 1.0U
1ug/L 19-Jul-2023 23:160.20Chloroform 1.0U
1ug/L 19-Jul-2023 23:160.30Ethylbenzene 1.0U
1ug/L 19-Jul-2023 23:160.50m,p-Xylene 2.0U
1ug/L 19-Jul-2023 23:160.20Methyl tert-butyl ether 1.0U
1ug/L 19-Jul-2023 23:161.0Methylene chloride 2.0U
1ug/L 19-Jul-2023 23:160.30Naphthalene 1.0U
1ug/L 19-Jul-2023 23:160.30o-Xylene 1.0U
1ug/L 19-Jul-2023 23:1610Tert-butyl alcohol 10U
1ug/L 19-Jul-2023 23:160.20Toluene 1.0U
1ug/L 19-Jul-2023 23:160.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 19-Jul-2023 23:1697.7 70-126
Surr: 4-Bromofluorobenzene 1%REC 19-Jul-2023 23:1694.1 77-113
Surr: Dibromofluoromethane 1%REC 19-Jul-2023 23:1610077-123
Surr: Toluene-d8 1%REC 19-Jul-2023 23:1698.3 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 23-Jul-2023 23:310.00311,2-Dibromoethane 0.021U
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-I-I
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-02
17-Jul-2023 12:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 00:190.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 00:190.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 00:190.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 00:191.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 00:190.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 00:190.20Benzene 1.0U
1ug/L 20-Jul-2023 00:190.20Chloroform 1.0U
1ug/L 20-Jul-2023 00:190.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 00:190.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 00:190.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 00:191.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 00:190.30Naphthalene 1.0U
1ug/L 20-Jul-2023 00:190.30o-Xylene 1.0U
1ug/L 20-Jul-2023 00:1910Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 00:190.20Toluene 1.0U
1ug/L 20-Jul-2023 00:190.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 00:1910070-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 00:1991.6 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 00:1910577-123
Surr: Toluene-d8 1%REC 20-Jul-2023 00:1910282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 23-Jul-2023 23:550.00321,2-Dibromoethane 0.021U
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-I-D
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-03
17-Jul-2023 12:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 00:400.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 00:400.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 00:400.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 00:401.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 00:400.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 00:400.20Benzene 1.0U
1ug/L 20-Jul-2023 00:400.20Chloroform 1.0U
1ug/L 20-Jul-2023 00:400.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 00:400.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 00:400.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 00:401.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 00:400.30Naphthalene 1.0U
1ug/L 20-Jul-2023 00:400.30o-Xylene 1.0U
1ug/L 20-Jul-2023 00:4010Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 00:400.20Toluene 1.0U
1ug/L 20-Jul-2023 00:400.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 00:4099.3 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 00:4090.4 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 00:4010577-123
Surr: Toluene-d8 1%REC 20-Jul-2023 00:4010282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 00:180.00321,2-Dibromoethane 0.021U
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-I-B
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-04
17-Jul-2023 13:35 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 01:010.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 01:010.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 01:010.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 01:011.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 01:010.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 01:010.20Benzene 1.0U
1ug/L 20-Jul-2023 01:010.20Chloroform 1.0U
1ug/L 20-Jul-2023 01:010.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 01:010.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 01:010.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 01:011.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 01:010.30Naphthalene 1.0U
1ug/L 20-Jul-2023 01:010.30o-Xylene 1.0U
1ug/L 20-Jul-2023 01:0110Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 01:010.20Toluene 1.0U
1ug/L 20-Jul-2023 01:010.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 01:0199.0 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 01:0192.1 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 01:0110377-123
Surr: Toluene-d8 1%REC 20-Jul-2023 01:0199.3 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 08:420.107Methane 0.500U
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 00:420.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:130.0120Iron 0.200U
1mg/L 28-Jul-2023 22:13J0.000700Manganese 0.005000.00304
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 11:490.200Sulfate 0.5003.36
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 14:350.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00197
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00200
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:590.0200Ferrous Iron 0.0500U
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-C-I
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-05
17-Jul-2023 14:42 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 01:220.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 01:220.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 01:220.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 01:221.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 01:220.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 01:220.20Benzene 1.0U
1ug/L 20-Jul-2023 01:220.20Chloroform 1.0U
1ug/L 20-Jul-2023 01:220.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 01:220.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 01:220.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 01:221.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 01:220.30Naphthalene 1.0U
1ug/L 20-Jul-2023 01:220.30o-Xylene 1.0U
1ug/L 20-Jul-2023 01:2210Tert-butyl alcohol 101,300
1ug/L 20-Jul-2023 01:220.20Toluene 1.0U
1ug/L 20-Jul-2023 01:220.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 01:2297.8 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 01:2291.0 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 01:2210477-123
Surr: Toluene-d8 1%REC 20-Jul-2023 01:2210182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 08:570.107Methane 0.50026.8
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 03:020.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:150.0120Iron 0.2000.476
20mg/L 31-Jul-2023 11:490.0140Manganese 0.1001.93
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 12:06J0.200Sulfate 0.5000.253
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 14:52J0.300Nitrate/Nitrite (as N)2.000.326
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00146
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00146
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:590.0200Ferrous Iron 0.05000.270
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-C-D
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-06
17-Jul-2023 15:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 01:430.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 01:430.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 01:430.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 01:431.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 01:430.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 01:430.20Benzene 1.0U
1ug/L 20-Jul-2023 01:430.20Chloroform 1.0U
1ug/L 20-Jul-2023 01:430.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 01:430.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 01:430.20Methyl tert-butyl ether 1.0200
1ug/L 20-Jul-2023 01:431.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 01:430.30Naphthalene 1.0U
1ug/L 20-Jul-2023 01:430.30o-Xylene 1.0U
20ug/L 20-Jul-2023 13:42200Tert-butyl alcohol 2007,600
1ug/L 20-Jul-2023 01:430.20Toluene 1.0U
1ug/L 20-Jul-2023 01:430.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 01:4395.4 70-126
Surr: 1,2-Dichloroethane-d4 20%REC 20-Jul-2023 13:4296.7 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 01:4394.9 77-113
Surr: 4-Bromofluorobenzene 20%REC 20-Jul-2023 13:4296.6 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 01:4310177-123
Surr: Dibromofluoromethane 20%REC 20-Jul-2023 13:4298.8 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 01:4310082-127
Surr: Toluene-d8 20%REC 20-Jul-2023 13:4210182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
5ug/L 22-Jul-2023 10:320.535Methane 2.50123
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 03:260.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:170.0120Iron 0.2005.13
50mg/L 31-Jul-2023 11:510.0350Manganese 0.2504.71
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 12:120.200Sulfate 0.5000.771
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 17:42J0.300Nitrate/Nitrite (as N)2.000.407
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-C-D
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-06
17-Jul-2023 15:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00309
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00309
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
5mg/L 19-Jul-2023 10:590.100Ferrous Iron 0.2506.48
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-C-B
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-07
17-Jul-2023 15:27 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 02:040.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 02:040.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 02:040.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 02:041.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 02:040.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 02:040.20Benzene 1.0U
1ug/L 20-Jul-2023 02:040.20Chloroform 1.0U
1ug/L 20-Jul-2023 02:040.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 02:040.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 02:040.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 02:041.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 02:040.30Naphthalene 1.0U
1ug/L 20-Jul-2023 02:040.30o-Xylene 1.0U
1ug/L 20-Jul-2023 02:0410Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 02:040.20Toluene 1.0U
1ug/L 20-Jul-2023 02:040.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 02:0410070-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 02:0489.7 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 02:0410577-123
Surr: Toluene-d8 1%REC 20-Jul-2023 02:0410482-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 09:260.107Methane 0.500U
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 03:490.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:19J0.0120Iron 0.2000.0331
1mg/L 28-Jul-2023 22:19J0.000700Manganese 0.005000.00423
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 12:170.200Sulfate 0.5005.17
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 14:58J0.300Nitrate/Nitrite (as N)2.001.63
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00116
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.0018.2
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00134
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:59J0.0200Ferrous Iron 0.05000.0490
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Field Blank #1
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-08
17-Jul-2023 15:15 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 19-Jul-2023 21:520.301,2,4-Trimethylbenzene 1.0U
1ug/L 19-Jul-2023 21:520.201,2-Dibromoethane 1.0U
1ug/L 19-Jul-2023 21:520.201,2-Dichloroethane 1.0U
1ug/L 19-Jul-2023 21:521.02-Methylnaphthalene 1.0U
1ug/L 19-Jul-2023 21:520.304-Isopropyltoluene 1.0U
1ug/L 19-Jul-2023 21:520.20Benzene 1.0U
1ug/L 19-Jul-2023 21:520.20Chloroform 1.0U
1ug/L 19-Jul-2023 21:520.30Ethylbenzene 1.0U
1ug/L 19-Jul-2023 21:520.50m,p-Xylene 2.0U
1ug/L 19-Jul-2023 21:520.20Methyl tert-butyl ether 1.0U
1ug/L 19-Jul-2023 21:521.0Methylene chloride 2.011
1ug/L 19-Jul-2023 21:520.30Naphthalene 1.0U
1ug/L 19-Jul-2023 21:520.30o-Xylene 1.0U
1ug/L 19-Jul-2023 21:5210Tert-butyl alcohol 10U
1ug/L 19-Jul-2023 21:520.20Toluene 1.0U
1ug/L 19-Jul-2023 21:520.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 19-Jul-2023 21:5210270-126
Surr: 4-Bromofluorobenzene 1%REC 19-Jul-2023 21:5292.6 77-113
Surr: Dibromofluoromethane 1%REC 19-Jul-2023 21:5210677-123
Surr: Toluene-d8 1%REC 19-Jul-2023 21:5297.6 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 09:350.107Methane 0.500U
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 04:130.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:210.0120Iron 0.200U
1mg/L 28-Jul-2023 22:210.000700Manganese 0.00500U
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 12:230.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 17:480.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:590.0200Ferrous Iron 0.0500U
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Equipment Blank #1
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-09
17-Jul-2023 15:25 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 19-Jul-2023 22:130.301,2,4-Trimethylbenzene 1.0U
1ug/L 19-Jul-2023 22:130.201,2-Dibromoethane 1.0U
1ug/L 19-Jul-2023 22:130.201,2-Dichloroethane 1.0U
1ug/L 19-Jul-2023 22:131.02-Methylnaphthalene 1.0U
1ug/L 19-Jul-2023 22:130.304-Isopropyltoluene 1.0U
1ug/L 19-Jul-2023 22:130.20Benzene 1.0U
1ug/L 19-Jul-2023 22:130.20Chloroform 1.0U
1ug/L 19-Jul-2023 22:130.30Ethylbenzene 1.0U
1ug/L 19-Jul-2023 22:130.50m,p-Xylene 2.0U
1ug/L 19-Jul-2023 22:130.20Methyl tert-butyl ether 1.0U
1ug/L 19-Jul-2023 22:131.0Methylene chloride 2.09.4
1ug/L 19-Jul-2023 22:130.30Naphthalene 1.0U
1ug/L 19-Jul-2023 22:130.30o-Xylene 1.0U
1ug/L 19-Jul-2023 22:1310Tert-butyl alcohol 10U
1ug/L 19-Jul-2023 22:130.20Toluene 1.0U
1ug/L 19-Jul-2023 22:130.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 19-Jul-2023 22:1398.9 70-126
Surr: 4-Bromofluorobenzene 1%REC 19-Jul-2023 22:1391.0 77-113
Surr: Dibromofluoromethane 1%REC 19-Jul-2023 22:1399.3 77-123
Surr: Toluene-d8 1%REC 19-Jul-2023 22:1310282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 09:500.107Methane 0.500U
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 04:360.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:240.0120Iron 0.200U
1mg/L 28-Jul-2023 22:240.000700Manganese 0.00500U
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 12:290.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 17:540.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:590.0200Ferrous Iron 0.0500U
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-10
17-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 19-Jul-2023 22:550.301,2,4-Trimethylbenzene 1.0U
1ug/L 19-Jul-2023 22:550.201,2-Dibromoethane 1.0U
1ug/L 19-Jul-2023 22:550.201,2-Dichloroethane 1.0U
1ug/L 19-Jul-2023 22:551.02-Methylnaphthalene 1.0U
1ug/L 19-Jul-2023 22:550.304-Isopropyltoluene 1.0U
1ug/L 19-Jul-2023 22:550.20Benzene 1.0U
1ug/L 19-Jul-2023 22:550.20Chloroform 1.0U
1ug/L 19-Jul-2023 22:550.30Ethylbenzene 1.0U
1ug/L 19-Jul-2023 22:550.50m,p-Xylene 2.0U
1ug/L 19-Jul-2023 22:550.20Methyl tert-butyl ether 1.0U
1ug/L 19-Jul-2023 22:551.0Methylene chloride 2.0U
1ug/L 19-Jul-2023 22:550.30Naphthalene 1.0U
1ug/L 19-Jul-2023 22:550.30o-Xylene 1.0U
1ug/L 19-Jul-2023 22:5510Tert-butyl alcohol 10U
1ug/L 19-Jul-2023 22:550.20Toluene 1.0U
1ug/L 19-Jul-2023 22:550.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 19-Jul-2023 22:5598.5 70-126
Surr: 4-Bromofluorobenzene 1%REC 19-Jul-2023 22:5592.2 77-113
Surr: Dibromofluoromethane 1%REC 19-Jul-2023 22:5510577-123
Surr: Toluene-d8 1%REC 19-Jul-2023 22:5510382-127
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Field Dup #1
WorkOrder:
Lab ID:
Collection Date:
HS23070922
HS23070922-11
17-Jul-2023 14:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 02:250.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 02:250.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 02:250.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 02:251.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 02:250.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 02:250.20Benzene 1.0U
1ug/L 20-Jul-2023 02:250.20Chloroform 1.0U
1ug/L 20-Jul-2023 02:250.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 02:250.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 02:250.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 02:251.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 02:250.30Naphthalene 1.0U
1ug/L 20-Jul-2023 02:250.30o-Xylene 1.0U
1ug/L 20-Jul-2023 02:2510Tert-butyl alcohol 101,400
1ug/L 20-Jul-2023 02:250.20Toluene 1.0U
1ug/L 20-Jul-2023 02:250.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 02:2599.9 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 02:2593.8 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 02:2510277-123
Surr: Toluene-d8 1%REC 20-Jul-2023 02:2510082-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 10:150.107Methane 0.50012.7
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 05:000.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:260.0120Iron 0.2003.41
20mg/L 31-Jul-2023 11:530.0140Manganese 0.1001.82
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 12:35J0.200Sulfate 0.5000.376
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 15:04J0.300Nitrate/Nitrite (as N)2.000.339
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00146
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00146
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:590.0200Ferrous Iron 0.05000.321
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 16 of 41
Weight / Prep Log
HS23070922
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197842
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:26 End Date: 21 Jul 2023 09:26
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23070922-01 35 (mL)40 mL VOA w/ HCL36.63 (mL)1.047
HS23070922-02 35 (mL)40 mL VOA w/ HCL37.41 (mL)1.069
HS23070922-03 35 (mL)40 mL VOA w/ HCL37.05 (mL)1.059
HS23070922-04 35 (mL)40 mL VOA w/ HCL36.36 (mL)1.039
HS23070922-05 35 (mL)40 mL VOA w/ HCL36.12 (mL)1.032
HS23070922-06 35 (mL)40 mL VOA w/ HCL36.96 (mL)1.056
HS23070922-07 35 (mL)40 mL VOA w/ HCL36.75 (mL)1.05
HS23070922-08 35 (mL)40 mL VOA w/ HCL36.27 (mL)1.036
HS23070922-09 35 (mL)40 mL VOA w/ HCL36.09 (mL)1.031
HS23070922-11 35 (mL)40 mL VOA w/ HCL36.63 (mL)1.047
Batch ID:198234
Method:WATER - SW3010A 3010APrep Code:
Start Date: 28 Jul 2023 13:30 End Date: 28 Jul 2023 13:30
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23070922-04 10 (mL)120 plastic HNO310 (mL)1
HS23070922-05 10 (mL)120 plastic HNO310 (mL)1
HS23070922-06 10 (mL)120 plastic HNO310 (mL)1
HS23070922-07 10 (mL)120 plastic HNO310 (mL)1
HS23070922-08 10 (mL)120 plastic HNO310 (mL)1
HS23070922-09 10 (mL)120 plastic HNO310 (mL)1
HS23070922-11 10 (mL)120 plastic HNO310 (mL)1
31-Jul-23Date: ALS Houston, US
Page 17 of 41
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23070922
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197842 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Water
21 Jul 2023 09:26 24 Jul 2023 04:13HS23070922-08 17 Jul 2023 15:15 1Field Blank #1
21 Jul 2023 09:26 24 Jul 2023 04:36HS23070922-09 17 Jul 2023 15:25 1Equipment Blank #1
Batch ID:197842 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:26 23 Jul 2023 23:31HS23070922-01 17 Jul 2023 11:32 1Z2-X29
21 Jul 2023 09:26 23 Jul 2023 23:55HS23070922-02 17 Jul 2023 12:15 1MW-I-I
21 Jul 2023 09:26 24 Jul 2023 00:18HS23070922-03 17 Jul 2023 12:45 1MW-I-D
21 Jul 2023 09:26 24 Jul 2023 00:42HS23070922-04 17 Jul 2023 13:35 1MW-I-B
21 Jul 2023 09:26 24 Jul 2023 03:02HS23070922-05 17 Jul 2023 14:42 1MW-C-I
21 Jul 2023 09:26 24 Jul 2023 03:26HS23070922-06 17 Jul 2023 15:40 1MW-C-D
21 Jul 2023 09:26 24 Jul 2023 03:49HS23070922-07 17 Jul 2023 15:27 1MW-C-B
21 Jul 2023 09:26 24 Jul 2023 05:00HS23070922-11 17 Jul 2023 14:50 1Field Dup #1
Batch ID:198234 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Water
28 Jul 2023 13:30 28 Jul 2023 22:21HS23070922-08 17 Jul 2023 15:15 1Field Blank #1
28 Jul 2023 13:30 28 Jul 2023 22:24HS23070922-09 17 Jul 2023 15:25 1Equipment Blank #1
Batch ID:198234 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
28 Jul 2023 13:30 28 Jul 2023 22:13HS23070922-04 17 Jul 2023 13:35 1MW-I-B
28 Jul 2023 13:30 31 Jul 2023 11:49HS23070922-05 17 Jul 2023 14:42 20MW-C-I
28 Jul 2023 13:30 28 Jul 2023 22:15HS23070922-05 17 Jul 2023 14:42 1MW-C-I
28 Jul 2023 13:30 31 Jul 2023 11:51HS23070922-06 17 Jul 2023 15:40 50MW-C-D
28 Jul 2023 13:30 28 Jul 2023 22:17HS23070922-06 17 Jul 2023 15:40 1MW-C-D
28 Jul 2023 13:30 28 Jul 2023 22:19HS23070922-07 17 Jul 2023 15:27 1MW-C-B
28 Jul 2023 13:30 31 Jul 2023 11:53HS23070922-11 17 Jul 2023 14:50 20Field Dup #1
28 Jul 2023 13:30 28 Jul 2023 22:26HS23070922-11 17 Jul 2023 14:50 1Field Dup #1
Batch ID:R441787 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
19 Jul 2023 21:52HS23070922-08 17 Jul 2023 15:15 1Field Blank #1
19 Jul 2023 22:13HS23070922-09 17 Jul 2023 15:25 1Equipment Blank #1
19 Jul 2023 22:55HS23070922-10 17 Jul 2023 00:00 1Trip Blank
Batch ID:R441787 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
19 Jul 2023 23:16HS23070922-01 17 Jul 2023 11:32 1Z2-X29
20 Jul 2023 00:19HS23070922-02 17 Jul 2023 12:15 1MW-I-I
20 Jul 2023 00:40HS23070922-03 17 Jul 2023 12:45 1MW-I-D
20 Jul 2023 01:01HS23070922-04 17 Jul 2023 13:35 1MW-I-B
20 Jul 2023 01:22HS23070922-05 17 Jul 2023 14:42 1MW-C-I
20 Jul 2023 01:43HS23070922-06 17 Jul 2023 15:40 1MW-C-D
20 Jul 2023 02:04HS23070922-07 17 Jul 2023 15:27 1MW-C-B
20 Jul 2023 02:25HS23070922-11 17 Jul 2023 14:50 1Field Dup #1
31-Jul-23Date: ALS Houston, US
Page 18 of 41
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23070922
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R441843 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Water
19 Jul 2023 10:59HS23070922-08 17 Jul 2023 15:15 1Field Blank #1
19 Jul 2023 10:59HS23070922-09 17 Jul 2023 15:25 1Equipment Blank #1
Batch ID:R441843 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
19 Jul 2023 10:59HS23070922-04 17 Jul 2023 13:35 1MW-I-B
19 Jul 2023 10:59HS23070922-05 17 Jul 2023 14:42 1MW-C-I
19 Jul 2023 10:59HS23070922-06 17 Jul 2023 15:40 5MW-C-D
19 Jul 2023 10:59HS23070922-07 17 Jul 2023 15:27 1MW-C-B
19 Jul 2023 10:59HS23070922-11 17 Jul 2023 14:50 1Field Dup #1
Batch ID:R441876 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Water
20 Jul 2023 17:48HS23070922-08 17 Jul 2023 15:15 10Field Blank #1
20 Jul 2023 17:54HS23070922-09 17 Jul 2023 15:25 10Equipment Blank #1
Batch ID:R441876 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
20 Jul 2023 14:35HS23070922-04 17 Jul 2023 13:35 10MW-I-B
20 Jul 2023 14:52HS23070922-05 17 Jul 2023 14:42 10MW-C-I
20 Jul 2023 17:42HS23070922-06 17 Jul 2023 15:40 10MW-C-D
20 Jul 2023 14:58HS23070922-07 17 Jul 2023 15:27 10MW-C-B
20 Jul 2023 15:04HS23070922-11 17 Jul 2023 14:50 10Field Dup #1
Batch ID:R441892 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
20 Jul 2023 13:42HS23070922-06 17 Jul 2023 15:40 20MW-C-D
Batch ID:R442316 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Water
22 Jul 2023 09:35HS23070922-08 17 Jul 2023 15:15 1Field Blank #1
22 Jul 2023 09:50HS23070922-09 17 Jul 2023 15:25 1Equipment Blank #1
Batch ID:R442316 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
22 Jul 2023 08:42HS23070922-04 17 Jul 2023 13:35 1MW-I-B
22 Jul 2023 08:57HS23070922-05 17 Jul 2023 14:42 1MW-C-I
22 Jul 2023 10:32HS23070922-06 17 Jul 2023 15:40 5MW-C-D
22 Jul 2023 09:26HS23070922-07 17 Jul 2023 15:27 1MW-C-B
22 Jul 2023 10:15HS23070922-11 17 Jul 2023 14:50 1Field Dup #1
Batch ID:R442693 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Water
28 Jul 2023 12:23HS23070922-08 17 Jul 2023 15:15 1Field Blank #1
28 Jul 2023 12:29HS23070922-09 17 Jul 2023 15:25 1Equipment Blank #1
31-Jul-23Date: ALS Houston, US
Page 19 of 41
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23070922
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442693 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
28 Jul 2023 11:49HS23070922-04 17 Jul 2023 13:35 1MW-I-B
28 Jul 2023 12:06HS23070922-05 17 Jul 2023 14:42 1MW-C-I
28 Jul 2023 12:12HS23070922-06 17 Jul 2023 15:40 1MW-C-D
28 Jul 2023 12:17HS23070922-07 17 Jul 2023 15:27 1MW-C-B
28 Jul 2023 12:35HS23070922-11 17 Jul 2023 14:50 1Field Dup #1
Batch ID:R442736 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Water
29 Jul 2023 12:25HS23070922-08 17 Jul 2023 15:15 1Field Blank #1
29 Jul 2023 12:25HS23070922-09 17 Jul 2023 15:25 1Equipment Blank #1
Batch ID:R442736 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
29 Jul 2023 12:25HS23070922-04 17 Jul 2023 13:35 1MW-I-B
29 Jul 2023 12:25HS23070922-05 17 Jul 2023 14:42 1MW-C-I
29 Jul 2023 12:25HS23070922-06 17 Jul 2023 15:40 1MW-C-D
29 Jul 2023 12:25HS23070922-07 17 Jul 2023 15:27 1MW-C-B
29 Jul 2023 12:25HS23070922-11 17 Jul 2023 14:50 1Field Dup #1
31-Jul-23Date: ALS Houston, US
Page 20 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:197842 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197842 Units:ug/L Analysis Date:23-Jul-2023 22:21
Run ID:ECD_13_442222 SeqNo:7448736 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197842 Units:ug/L Analysis Date:23-Jul-2023 22:44
Run ID:ECD_13_442222 SeqNo:7448737 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.2266 0.25 0 90.6 60 - 1400.020
Sample ID:LCSD-197842 Units:ug/L Analysis Date:23-Jul-2023 23:08
Run ID:ECD_13_442222 SeqNo:7448738 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.2303 0.25 0 92.1 60 - 140 0.2266 1.63 200.020
The following samples were analyzed in this batch:HS23070922-01 HS23070922-02 HS23070922-03 HS23070922-04
HS23070922-05 HS23070922-06 HS23070922-07 HS23070922-08
HS23070922-09 HS23070922-11
ALS Houston, US Date: 31-Jul-23
Page 21 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R442316 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230722 Units:ug/L Analysis Date:22-Jul-2023 08:11
Run ID:FID-4_442316 SeqNo:7450987 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230722 Units:ug/L Analysis Date:22-Jul-2023 08:21
Run ID:FID-4_442316 SeqNo:7450988 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 8.179 9.647 0 84.8 75 - 1250.500
Sample ID:LCSD-230722 Units:ug/L Analysis Date:22-Jul-2023 08:33
Run ID:FID-4_442316 SeqNo:7450989 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 7.869 9.647 0 81.6 75 - 125 8.179 3.86 300.500
Sample ID:HS23070922-11DUP Units:ug/L Analysis Date:22-Jul-2023 10:23
Run ID:FID-4_442316 SeqNo:7450998 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:Field Dup #1
Methane 14.19 12.65 11.4 300.500
The following samples were analyzed in this batch:HS23070922-04 HS23070922-05 HS23070922-06 HS23070922-07
HS23070922-08 HS23070922-09 HS23070922-11
ALS Houston, US Date: 31-Jul-23
Page 22 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:198234 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198234 Units:mg/L Analysis Date:28-Jul-2023 21:54
Run ID:ICPMS05_442602 SeqNo:7460488 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese 0.001726 J 0.00500
Sample ID:LCS-198234 Units:mg/L Analysis Date:28-Jul-2023 21:56
Run ID:ICPMS05_442602 SeqNo:7460489 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.76 5 0 95.2 80 - 1200.200
Manganese 0.04489 0.05 0 89.8 80 - 1200.00500
Sample ID:HS23071175-03MS Units:mg/L Analysis Date:28-Jul-2023 22:02
Run ID:ICPMS05_442602 SeqNo:7460459 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.08 5 0.1716 98.2 80 - 1200.200
Manganese 0.1304 0.05 0.08299 94.9 80 - 1200.00500
Sample ID:HS23071175-03MSD Units:mg/L Analysis Date:28-Jul-2023 22:04
Run ID:ICPMS05_442602 SeqNo:7460460 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.043 5 0.1716 97.4 80 - 120 5.08 0.73 200.200
Manganese 0.1299 0.05 0.08299 93.9 80 - 120 0.1304 0.4 200.00500
Sample ID:HS23071175-03PDS Units:mg/L Analysis Date:28-Jul-2023 22:06
Run ID:ICPMS05_442602 SeqNo:7460461 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 9.974 10 0.1716 98.0 75 - 1250.200
Manganese 0.176 0.1 0.08299 93.0 75 - 1250.00500
ALS Houston, US Date: 31-Jul-23
Page 23 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:198234 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23071175-03SD Units:mg/L Analysis Date:28-Jul-2023 22:00
Run ID:ICPMS05_442602 SeqNo:7460458 PrepDate:28-Jul-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron 0.1575 0.1716 0 10 J 1.00
Manganese 0.08327 0.08299 0.345 100.0250
The following samples were analyzed in this batch:HS23070922-04 HS23070922-05 HS23070922-06 HS23070922-07
HS23070922-08 HS23070922-09 HS23070922-11
ALS Houston, US Date: 31-Jul-23
Page 24 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R441787 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230719 Units:ug/L Analysis Date:19-Jul-2023 21:10
Run ID:VOA11_441787 SeqNo:7438803 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
48.5 50 0 97.0 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.57 50 0 93.1 77 - 1131.0Surr: 4-Bromofluorobenzene
48.94 50 0 97.9 73 - 1261.0Surr: Dibromofluoromethane
51.03 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 31-Jul-23
Page 25 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R441787 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230719 Units:ug/L Analysis Date:19-Jul-2023 20:28
Run ID:VOA11_441787 SeqNo:7438802 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 20.94 20 0 105 73 - 1211.0
1,2-Dibromoethane 18.66 20 0 93.3 76 - 1231.0
1,2-Dichloroethane 18.02 20 0 90.1 70 - 1241.0
2-Methylnaphthalene 17.09 20 0 85.5 55 - 1401.0
4-Isopropyltoluene 21.01 20 0 105 74 - 1261.0
Benzene 18.65 20 0 93.3 74 - 1201.0
Chloroform 19.17 20 0 95.8 71 - 1211.0
Ethylbenzene 20.13 20 0 101 77 - 1171.0
m,p-Xylene 40.29 40 0 101 77 - 1222.0
Methyl tert-butyl ether 17.35 20 0 86.8 70 - 1301.0
Methylene chloride 22.49 20 0 112 70 - 1272.0
Naphthalene 18.74 20 0 93.7 70 - 1301.0
o-Xylene 21.01 20 0 105 75 - 1191.0
Tert-butyl alcohol 301.8 400 0 75.4 70 - 13010
Toluene 19.28 20 0 96.4 77 - 1181.0
Xylenes, Total 61.3 60 0 102 75 - 1223.0
45.68 50 0 91.4 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.86 50 0 95.7 77 - 1131.0Surr: 4-Bromofluorobenzene
48.7 50 0 97.4 73 - 1261.0Surr: Dibromofluoromethane
51.24 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 31-Jul-23
Page 26 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R441787 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23070922-01MS Units:ug/L Analysis Date:19-Jul-2023 23:37
Run ID:VOA11_441787 SeqNo:7438810 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:Z2-X29
1,2,4-Trimethylbenzene 13.6 20 0 68.0 70 - 125 S1.0
1,2-Dibromoethane 11.73 20 0 58.6 70 - 124 S1.0
1,2-Dichloroethane 12.62 20 0 63.1 70 - 127 S1.0
2-Methylnaphthalene 11.09 20 0 55.5 55 - 1401.0
4-Isopropyltoluene 13.28 20 0 66.4 70 - 130 S1.0
Benzene 13.8 20 0 69.0 70 - 127 S1.0
Chloroform 14.55 20 0 72.7 70 - 1251.0
Ethylbenzene 14.71 20 0 73.6 70 - 1241.0
m,p-Xylene 28.67 40 0 71.7 70 - 1302.0
Methyl tert-butyl ether 11.06 20 0 55.3 70 - 130 S1.0
Methylene chloride 14.51 20 0 72.5 70 - 1282.0
Naphthalene 11.11 20 0 55.5 70 - 130 S1.0
o-Xylene 14.25 20 0 71.2 70 - 1241.0
Tert-butyl alcohol 200 400 0 50.0 70 - 130 S10
Toluene 13.86 20 0 69.3 70 - 123 S1.0
Xylenes, Total 42.91 60 0 71.5 70 - 1303.0
46.47 50 0 92.9 70 - 1261.0Surr: 1,2-Dichloroethane-d4
46.79 50 0 93.6 77 - 1131.0Surr: 4-Bromofluorobenzene
50.07 50 0 100 77 - 1231.0Surr: Dibromofluoromethane
50.81 50 0 102 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 31-Jul-23
Page 27 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R441787 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23070922-01MSD Units:ug/L Analysis Date:19-Jul-2023 23:58
Run ID:VOA11_441787 SeqNo:7438811 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:Z2-X29
1,2,4-Trimethylbenzene 12.5 20 0 62.5 70 - 125 13.6 8.46 20 S1.0
1,2-Dibromoethane 11.39 20 0 56.9 70 - 124 11.73 2.94 20 S1.0
1,2-Dichloroethane 12.28 20 0 61.4 70 - 127 12.62 2.76 20 S1.0
2-Methylnaphthalene 11.58 20 0 57.9 55 - 140 11.09 4.34 201.0
4-Isopropyltoluene 12.71 20 0 63.6 70 - 130 13.28 4.34 20 S1.0
Benzene 12.88 20 0 64.4 70 - 127 13.8 6.9 20 S1.0
Chloroform 13.15 20 0 65.8 70 - 125 14.55 10 20 S1.0
Ethylbenzene 12.79 20 0 64.0 70 - 124 14.71 13.9 20 S1.0
m,p-Xylene 26.34 40 0 65.8 70 - 130 28.67 8.48 20 S2.0
Methyl tert-butyl ether 10.26 20 0 51.3 70 - 130 11.06 7.54 20 S1.0
Methylene chloride 13.93 20 0 69.7 70 - 128 14.51 4.05 20 S2.0
Naphthalene 11.6 20 0 58.0 70 - 130 11.11 4.32 20 S1.0
o-Xylene 12.54 20 0 62.7 70 - 124 14.25 12.7 20 S1.0
Tert-butyl alcohol 203.3 400 0 50.8 70 - 130 200 1.63 20 S10
Toluene 12.43 20 0 62.1 70 - 123 13.86 10.9 20 S1.0
Xylenes, Total 38.88 60 0 64.8 70 - 130 42.91 9.86 20 S3.0
45.79 50 0 91.6 70 - 126 46.47 1.47 201.0Surr: 1,2-Dichloroethane-d4
47.18 50 0 94.4 77 - 113 46.79 0.841 201.0Surr: 4-Bromofluorobenzene
49.21 50 0 98.4 77 - 123 50.07 1.73 201.0Surr: Dibromofluoromethane
49.04 50 0 98.1 82 - 127 50.81 3.53 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23070922-01 HS23070922-02 HS23070922-03 HS23070922-04
HS23070922-05 HS23070922-06 HS23070922-07 HS23070922-08
HS23070922-09 HS23070922-10 HS23070922-11
ALS Houston, US Date: 31-Jul-23
Page 28 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R441892 ( 0 )Instrument:VOA7 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230720 Units:ug/L Analysis Date:20-Jul-2023 10:25
Run ID:VOA7_441892 SeqNo:7441393 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Tert-butyl alcohol U 10
48.46 50 0 96.9 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.31 50 0 96.6 77 - 1131.0Surr: 4-Bromofluorobenzene
49.32 50 0 98.6 73 - 1261.0Surr: Dibromofluoromethane
50 50 0 100.0 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230720 Units:ug/L Analysis Date:20-Jul-2023 09:42
Run ID:VOA7_441892 SeqNo:7441392 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Tert-butyl alcohol 328 400 0 82.0 70 - 13010
48.76 50 0 97.5 70 - 1231.0Surr: 1,2-Dichloroethane-d4
49.13 50 0 98.3 77 - 1131.0Surr: 4-Bromofluorobenzene
50.24 50 0 100 73 - 1261.0Surr: Dibromofluoromethane
50.1 50 0 100 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23070946-01MS Units:ug/L Analysis Date:20-Jul-2023 11:31
Run ID:VOA7_441892 SeqNo:7441396 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Tert-butyl alcohol 290.4 400 0 72.6 70 - 13010
47.53 50 0 95.1 70 - 1261.0Surr: 1,2-Dichloroethane-d4
49.23 50 0 98.5 77 - 1131.0Surr: 4-Bromofluorobenzene
48.84 50 0 97.7 77 - 1231.0Surr: Dibromofluoromethane
49.94 50 0 99.9 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 31-Jul-23
Page 29 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R441892 ( 0 )Instrument:VOA7 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23070946-01MSD Units:ug/L Analysis Date:20-Jul-2023 11:53
Run ID:VOA7_441892 SeqNo:7441397 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Tert-butyl alcohol 344.6 400 0 86.2 70 - 130 290.4 17.1 2010
48.7 50 0 97.4 70 - 126 47.53 2.43 201.0Surr: 1,2-Dichloroethane-d4
49.05 50 0 98.1 77 - 113 49.23 0.362 201.0Surr: 4-Bromofluorobenzene
49.57 50 0 99.1 77 - 123 48.84 1.49 201.0Surr: Dibromofluoromethane
50.05 50 0 100 82 - 127 49.94 0.233 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23070922-06
ALS Houston, US Date: 31-Jul-23
Page 30 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R441843 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441843 Units:mg/L Analysis Date:19-Jul-2023 10:59
Run ID:UV-2450_441843 SeqNo:7440150 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441843 Units:mg/L Analysis Date:19-Jul-2023 10:59
Run ID:UV-2450_441843 SeqNo:7440149 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.256 0.25 0 102 80 - 1200.0500
Sample ID:HS23070935-01MS Units:mg/L Analysis Date:19-Jul-2023 10:59
Run ID:UV-2450_441843 SeqNo:7440151 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.262 0.25 0.012 100 75 - 1250.0500
The following samples were analyzed in this batch:HS23070922-04 HS23070922-05 HS23070922-06 HS23070922-07
HS23070922-08 HS23070922-09 HS23070922-11
ALS Houston, US Date: 31-Jul-23
Page 31 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R441876 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:20-Jul-2023 12:28
Run ID:ICS-Integrion_441876 SeqNo:7440828 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:20-Jul-2023 12:34
Run ID:ICS-Integrion_441876 SeqNo:7440829 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.055 8 0 101 90 - 1100.200
Sample ID:HS23070922-04MS Units:mg/L Analysis Date:20-Jul-2023 14:41
Run ID:ICS-Integrion_441876 SeqNo:7440843 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-I-B
Nitrate/Nitrite (as N)35.93 40 0 89.8 80 - 1202.00
Sample ID:HS23070339-01MS Units:mg/L Analysis Date:20-Jul-2023 13:14
Run ID:ICS-Integrion_441876 SeqNo:7440831 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)35.84 40 2.793 82.6 80 - 1202.00
Sample ID:HS23070922-04MSD Units:mg/L Analysis Date:20-Jul-2023 14:46
Run ID:ICS-Integrion_441876 SeqNo:7440844 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:MW-I-B
Nitrate/Nitrite (as N)36.38 40 0 91.0 80 - 120 35.93 1.25 202.00
Sample ID:HS23070339-01MSD Units:mg/L Analysis Date:20-Jul-2023 13:20
Run ID:ICS-Integrion_441876 SeqNo:7440832 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)36.85 40 2.793 85.1 80 - 120 35.84 2.77 202.00
The following samples were analyzed in this batch:HS23070922-04 HS23070922-05 HS23070922-06 HS23070922-07
HS23070922-08 HS23070922-09 HS23070922-11
ALS Houston, US Date: 31-Jul-23
Page 32 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R442693 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:28-Jul-2023 09:59
Run ID:ICS-Integrion_442693 SeqNo:7459857 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:28-Jul-2023 10:16
Run ID:ICS-Integrion_442693 SeqNo:7459858 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.65 20 0 98.3 90 - 1100.500
Sample ID:HS23071760-02MS Units:mg/L Analysis Date:28-Jul-2023 10:33
Run ID:ICS-Integrion_442693 SeqNo:7459860 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 12.28 10 2.936 93.4 80 - 1200.500
Sample ID:HS23071518-01MS Units:mg/L Analysis Date:28-Jul-2023 13:39
Run ID:ICS-Integrion_442693 SeqNo:7459885 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 149.4 100 71 78.4 80 - 120 S 5.00
Sample ID:HS23070922-04MS Units:mg/L Analysis Date:28-Jul-2023 11:54
Run ID:ICS-Integrion_442693 SeqNo:7459870 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-I-B
Sulfate 13.28 10 3.357 99.2 80 - 1200.500
Sample ID:HS23071760-02MSD Units:mg/L Analysis Date:28-Jul-2023 10:39
Run ID:ICS-Integrion_442693 SeqNo:7459861 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 12.29 10 2.936 93.6 80 - 120 12.28 0.112 200.500
ALS Houston, US Date: 31-Jul-23
Page 33 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R442693 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:HS23071518-01MSD Units:mg/L Analysis Date:28-Jul-2023 13:45
Run ID:ICS-Integrion_442693 SeqNo:7459886 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 150 100 71 79.0 80 - 120 149.4 0.421 20 S 5.00
Sample ID:HS23070922-04MSD Units:mg/L Analysis Date:28-Jul-2023 12:00
Run ID:ICS-Integrion_442693 SeqNo:7459871 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:MW-I-B
Sulfate 13.32 10 3.357 99.6 80 - 120 13.28 0.337 200.500
The following samples were analyzed in this batch:HS23070922-04 HS23070922-05 HS23070922-06 HS23070922-07
HS23070922-08 HS23070922-09 HS23070922-11
ALS Houston, US Date: 31-Jul-23
Page 34 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070922
QC BATCH REPORT
Batch ID:R442736 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:MBLK-R442736 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442736 SeqNo:7461095 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-R442736 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442736 SeqNo:7461094 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)968.6 1000 0 96.9 85 - 1155.00
Alkalinity, Total (As CaCO3)1009 1000 0 101 85 - 1155.00
Sample ID:LCSD-R442736 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442736 SeqNo:7461093 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)986.3 1000 0 98.6 85 - 115 968.6 1.81 205.00
Alkalinity, Total (As CaCO3)1008 1000 0 101 85 - 115 1009 0.157 205.00
Sample ID:HS23070912-01DUP Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442736 SeqNo:7461096 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)345.2 358.4 3.76 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)345.2 358.4 3.76 205.00
The following samples were analyzed in this batch:HS23070922-04 HS23070922-05 HS23070922-06 HS23070922-07
HS23070922-08 HS23070922-09 HS23070922-11
ALS Houston, US Date: 31-Jul-23
Page 35 of 41
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23070922
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 31-Jul-23
Page 36 of 41
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
31-Jul-23Date: ALS Houston, US
Page 37 of 41
Malcolm Burleson
18-Jul-2023 09:25Date/Time Received:HS23070922
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
2.5C/2.4C UC/C IR 31
47146
07/18/2023 13:30
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Sample #9 - ID = Equip. Blank - 2 x voa neat Vials rec'd Broken
Completed By:/S/ Nilesh D. Ranchod
Date/TimeeSignatureDate/TimeeSignature
19-Jul-2023 07:2718-Jul-2023 12:54
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241109/241117
ALS Houston, US 31-Jul-23Date:
Page 38 of 41
Page 39 of 41
Page 40 of 41
Page 41 of 41
July 31, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 7 sample(s) on Jul 18, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23070935
Project Manager
Generated By: DAYNA.FISHER
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 34
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23070935
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23070935-01 17-Jul-2023 15:40 18-Jul-2023 09:25MW-G-B Groundwater
HS23070935-02 17-Jul-2023 15:10 18-Jul-2023 09:25MW-G-I Groundwater
HS23070935-03 17-Jul-2023 14:30 18-Jul-2023 09:25MW-G-D Groundwater
HS23070935-04 17-Jul-2023 14:27 18-Jul-2023 09:25MW-H-B Groundwater
HS23070935-05 17-Jul-2023 15:05 18-Jul-2023 09:25MW-H-I Groundwater
HS23070935-06 17-Jul-2023 15:45 18-Jul-2023 09:25MW-H-D Groundwater
HS23070935-07 17-Jul-2023 00:00 18-Jul-2023 09:25Trip Blank Water
ALS Houston, US 31-Jul-23Date:
Page 2 of 34
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23070935
ECD Organics by Method SW8011
Batch ID: 197842
Sample ID: MBLK-197842
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R441986
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R441892
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R441787
Sample ID: HS23070922-01MS
MS and MSD are for an unrelated sample•
Metals by Method SW6020A
Batch ID: 198234
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Wet Chemistry by Method E300
Batch ID: R442693
Sample ID: HS23071518-01MS
MS and MSD are for an unrelated sample•
WetChemistry by Method SM2320B
Batch ID: R442736
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 31-Jul-23Date:
Page 3 of 34
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23070935
WetChemistry by Method E300
Batch ID: R441876
Sample ID: MW-G-B (HS23070935-01)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-G-I (HS23070935-02)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-H-B (HS23070935-04)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-H-D (HS23070935-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-H-I (HS23070935-05)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441843
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 31-Jul-23Date:
Page 4 of 34
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-G-B
WorkOrder:
Lab ID:
Collection Date:
HS23070935
HS23070935-01
17-Jul-2023 15:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 02:460.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 02:460.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 02:460.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 02:461.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 02:460.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 02:460.20Benzene 1.0U
1ug/L 20-Jul-2023 02:460.20Chloroform 1.0U
1ug/L 20-Jul-2023 02:460.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 02:460.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 02:460.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 02:461.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 02:460.30Naphthalene 1.0U
1ug/L 20-Jul-2023 02:460.30o-Xylene 1.0U
1ug/L 20-Jul-2023 02:4610Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 02:460.20Toluene 1.0U
1ug/L 20-Jul-2023 02:460.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 02:4610270-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 02:4692.0 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 02:4610277-123
Surr: Toluene-d8 1%REC 20-Jul-2023 02:4610282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 08:380.107Methane 0.5000.545
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 05:230.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:280.0120Iron 0.200U
1mg/L 28-Jul-2023 22:280.000700Manganese 0.005000.00612
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 13:500.200Sulfate 0.5002.75
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 15:10J0.300Nitrate/Nitrite (as N)2.000.345
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00233
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00233
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:590.0200Ferrous Iron 0.0500U
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 34
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-G-I
WorkOrder:
Lab ID:
Collection Date:
HS23070935
HS23070935-02
17-Jul-2023 15:10 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 03:070.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 03:070.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 03:070.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 03:071.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 03:070.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 03:070.20Benzene 1.0U
1ug/L 20-Jul-2023 03:070.20Chloroform 1.0U
1ug/L 20-Jul-2023 03:070.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 03:070.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 03:070.20Methyl tert-butyl ether 1.03.5
1ug/L 20-Jul-2023 03:071.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 03:070.30Naphthalene 1.0U
1ug/L 20-Jul-2023 03:070.30o-Xylene 1.0U
1ug/L 20-Jul-2023 03:0710Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 03:070.20Toluene 1.0U
1ug/L 20-Jul-2023 03:070.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 03:0710370-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 03:0790.6 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 03:0710777-123
Surr: Toluene-d8 1%REC 20-Jul-2023 03:0710082-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 08:560.107Methane 0.50016.7
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 05:470.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:300.0120Iron 0.20011.8
20mg/L 31-Jul-2023 11:550.0140Manganese 0.1002.76
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 13:560.200Sulfate 0.5004.56
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 15:150.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00165
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00165
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:590.0200Ferrous Iron 0.05000.263
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 34
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-G-D
WorkOrder:
Lab ID:
Collection Date:
HS23070935
HS23070935-03
17-Jul-2023 14:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 03:280.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 03:280.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 03:280.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 03:281.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 03:280.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 03:280.20Benzene 1.0U
1ug/L 20-Jul-2023 03:280.20Chloroform 1.0U
1ug/L 20-Jul-2023 03:280.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 03:280.50m,p-Xylene 2.0U
50ug/L 20-Jul-2023 14:0410Methyl tert-butyl ether 50480
1ug/L 20-Jul-2023 03:281.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 03:280.30Naphthalene 1.0U
1ug/L 20-Jul-2023 03:280.30o-Xylene 1.0U
50ug/L 20-Jul-2023 14:04500Tert-butyl alcohol 50023,000
1ug/L 20-Jul-2023 03:280.20Toluene 1.0U
1ug/L 20-Jul-2023 03:280.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 03:2897.3 70-126
Surr: 1,2-Dichloroethane-d4 50%REC 20-Jul-2023 14:0495.9 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 03:2892.5 77-113
Surr: 4-Bromofluorobenzene 50%REC 20-Jul-2023 14:0495.5 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 03:2898.7 77-123
Surr: Dibromofluoromethane 50%REC 20-Jul-2023 14:0498.3 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 03:2810282-127
Surr: Toluene-d8 50%REC 20-Jul-2023 14:0499.6 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 06:110.00311,2-Dibromoethane 0.021U
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 34
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-H-B
WorkOrder:
Lab ID:
Collection Date:
HS23070935
HS23070935-04
17-Jul-2023 14:27 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 03:490.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 03:490.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 03:490.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 03:491.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 03:490.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 03:490.20Benzene 1.0U
1ug/L 20-Jul-2023 03:490.20Chloroform 1.0U
1ug/L 20-Jul-2023 03:490.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 03:490.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 03:490.20Methyl tert-butyl ether 1.011
1ug/L 20-Jul-2023 03:491.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 03:490.30Naphthalene 1.0U
1ug/L 20-Jul-2023 03:490.30o-Xylene 1.0U
1ug/L 20-Jul-2023 03:4910Tert-butyl alcohol 1075
1ug/L 20-Jul-2023 03:490.20Toluene 1.0U
1ug/L 20-Jul-2023 03:490.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 03:4910170-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 03:4988.4 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 03:4910577-123
Surr: Toluene-d8 1%REC 20-Jul-2023 03:4910082-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
2ug/L 21-Jul-2023 10:040.214Methane 1.0061.3
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 07:450.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:320.0120Iron 0.2000.323
1mg/L 28-Jul-2023 22:320.000700Manganese 0.005001.12
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 14:02J0.200Sulfate 0.5000.385
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 15:50J0.300Nitrate/Nitrite (as N)2.000.330
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00131
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00131
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:590.0200Ferrous Iron 0.05000.369
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 34
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-H-I
WorkOrder:
Lab ID:
Collection Date:
HS23070935
HS23070935-05
17-Jul-2023 15:05 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 04:100.301,2,4-Trimethylbenzene 1.02.0
1ug/L 20-Jul-2023 04:100.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 04:100.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 04:101.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 04:100.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 04:100.20Benzene 1.0U
1ug/L 20-Jul-2023 04:100.20Chloroform 1.0U
1ug/L 20-Jul-2023 04:100.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 04:100.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 04:100.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 04:101.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 04:100.30Naphthalene 1.0U
1ug/L 20-Jul-2023 04:100.30o-Xylene 1.0U
1ug/L 20-Jul-2023 04:1010Tert-butyl alcohol 1029
1ug/L 20-Jul-2023 04:100.20Toluene 1.0U
1ug/L 20-Jul-2023 04:100.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 04:1010070-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 04:1093.1 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 04:1010477-123
Surr: Toluene-d8 1%REC 20-Jul-2023 04:1010282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
5ug/L 21-Jul-2023 10:140.535Methane 2.50182
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 08:080.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:390.0120Iron 0.20021.2
50mg/L 31-Jul-2023 11:570.0350Manganese 0.2506.17
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 14:08J0.200Sulfate 0.5000.396
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 15:56J0.300Nitrate/Nitrite (as N)2.000.338
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00297
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00297
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
5mg/L 19-Jul-2023 10:590.100Ferrous Iron 0.2506.38
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 34
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-H-D
WorkOrder:
Lab ID:
Collection Date:
HS23070935
HS23070935-06
17-Jul-2023 15:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 04:320.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 04:320.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 04:320.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 04:321.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 04:320.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 04:320.20Benzene 1.0U
1ug/L 20-Jul-2023 04:320.20Chloroform 1.0U
1ug/L 20-Jul-2023 04:320.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 04:320.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 04:320.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 04:321.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 04:320.30Naphthalene 1.0U
1ug/L 20-Jul-2023 04:320.30o-Xylene 1.0U
1ug/L 20-Jul-2023 04:3210Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 04:320.20Toluene 1.0U
1ug/L 20-Jul-2023 04:320.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 04:3210270-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 04:3289.4 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 04:3210577-123
Surr: Toluene-d8 1%REC 20-Jul-2023 04:3297.8 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 09:270.107Methane 0.5002.46
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 08:320.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 28-Jul-2023
1mg/L 28-Jul-2023 22:41J0.0120Iron 0.2000.0317
1mg/L 28-Jul-2023 22:41J0.000700Manganese 0.005000.00462
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 28-Jul-2023 14:490.200Sulfate 0.5005.43
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 20-Jul-2023 16:02J0.300Nitrate/Nitrite (as N)2.000.793
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: TH
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.0062.4
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.0017.3
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.0079.7
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 19-Jul-2023 10:59J0.0200Ferrous Iron 0.05000.0380
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 34
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23070935
HS23070935-07
17-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 19-Jul-2023 22:340.301,2,4-Trimethylbenzene 1.0U
1ug/L 19-Jul-2023 22:340.201,2-Dibromoethane 1.0U
1ug/L 19-Jul-2023 22:340.201,2-Dichloroethane 1.0U
1ug/L 19-Jul-2023 22:341.02-Methylnaphthalene 1.0U
1ug/L 19-Jul-2023 22:340.304-Isopropyltoluene 1.0U
1ug/L 19-Jul-2023 22:340.20Benzene 1.0U
1ug/L 19-Jul-2023 22:340.20Chloroform 1.0U
1ug/L 19-Jul-2023 22:340.30Ethylbenzene 1.0U
1ug/L 19-Jul-2023 22:340.50m,p-Xylene 2.0U
1ug/L 19-Jul-2023 22:340.20Methyl tert-butyl ether 1.0U
1ug/L 19-Jul-2023 22:341.0Methylene chloride 2.0U
1ug/L 19-Jul-2023 22:340.30Naphthalene 1.0U
1ug/L 19-Jul-2023 22:340.30o-Xylene 1.0U
1ug/L 19-Jul-2023 22:3410Tert-butyl alcohol 10U
1ug/L 19-Jul-2023 22:340.20Toluene 1.0U
1ug/L 19-Jul-2023 22:340.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 19-Jul-2023 22:3410070-126
Surr: 4-Bromofluorobenzene 1%REC 19-Jul-2023 22:3490.9 77-113
Surr: Dibromofluoromethane 1%REC 19-Jul-2023 22:3410477-123
Surr: Toluene-d8 1%REC 19-Jul-2023 22:3410382-127
31-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 34
Weight / Prep Log
HS23070935
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197842
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:26 End Date: 21 Jul 2023 09:26
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23070935-01 35 (mL)40 mL VOA w/ HCL36.23 (mL)1.035
HS23070935-02 35 (mL)40 mL VOA w/ HCL36.84 (mL)1.053
HS23070935-03 35 (mL)40 mL VOA w/ HCL36.13 (mL)1.032
HS23070935-04 35 (mL)40 mL VOA w/ HCL36.44 (mL)1.041
HS23070935-05 35 (mL)40 mL VOA w/ HCL37.22 (mL)1.063
HS23070935-06 35 (mL)40 mL VOA w/ HCL37.27 (mL)1.065
Batch ID:198234
Method:WATER - SW3010A 3010APrep Code:
Start Date: 28 Jul 2023 13:30 End Date: 28 Jul 2023 13:30
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23070935-01 10 (mL)120 plastic HNO310 (mL)1
HS23070935-02 10 (mL)120 plastic HNO310 (mL)1
HS23070935-04 10 (mL)120 plastic HNO310 (mL)1
HS23070935-05 10 (mL)120 plastic HNO310 (mL)1
HS23070935-06 10 (mL)120 plastic HNO310 (mL)1
31-Jul-23Date: ALS Houston, US
Page 12 of 34
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23070935
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197842 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:26 24 Jul 2023 05:23HS23070935-01 17 Jul 2023 15:40 1MW-G-B
21 Jul 2023 09:26 24 Jul 2023 05:47HS23070935-02 17 Jul 2023 15:10 1MW-G-I
21 Jul 2023 09:26 24 Jul 2023 06:11HS23070935-03 17 Jul 2023 14:30 1MW-G-D
21 Jul 2023 09:26 24 Jul 2023 07:45HS23070935-04 17 Jul 2023 14:27 1MW-H-B
21 Jul 2023 09:26 24 Jul 2023 08:08HS23070935-05 17 Jul 2023 15:05 1MW-H-I
21 Jul 2023 09:26 24 Jul 2023 08:32HS23070935-06 17 Jul 2023 15:45 1MW-H-D
Batch ID:198234 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
28 Jul 2023 13:30 28 Jul 2023 22:28HS23070935-01 17 Jul 2023 15:40 1MW-G-B
28 Jul 2023 13:30 31 Jul 2023 11:55HS23070935-02 17 Jul 2023 15:10 20MW-G-I
28 Jul 2023 13:30 28 Jul 2023 22:30HS23070935-02 17 Jul 2023 15:10 1MW-G-I
28 Jul 2023 13:30 28 Jul 2023 22:32HS23070935-04 17 Jul 2023 14:27 1MW-H-B
28 Jul 2023 13:30 31 Jul 2023 11:57HS23070935-05 17 Jul 2023 15:05 50MW-H-I
28 Jul 2023 13:30 28 Jul 2023 22:39HS23070935-05 17 Jul 2023 15:05 1MW-H-I
28 Jul 2023 13:30 28 Jul 2023 22:41HS23070935-06 17 Jul 2023 15:45 1MW-H-D
Batch ID:R441787 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
19 Jul 2023 22:34HS23070935-07 17 Jul 2023 00:00 1Trip Blank
Batch ID:R441787 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
20 Jul 2023 02:46HS23070935-01 17 Jul 2023 15:40 1MW-G-B
20 Jul 2023 03:07HS23070935-02 17 Jul 2023 15:10 1MW-G-I
20 Jul 2023 03:28HS23070935-03 17 Jul 2023 14:30 1MW-G-D
20 Jul 2023 03:49HS23070935-04 17 Jul 2023 14:27 1MW-H-B
20 Jul 2023 04:10HS23070935-05 17 Jul 2023 15:05 1MW-H-I
20 Jul 2023 04:32HS23070935-06 17 Jul 2023 15:45 1MW-H-D
Batch ID:R441843 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
19 Jul 2023 10:59HS23070935-01 17 Jul 2023 15:40 1MW-G-B
19 Jul 2023 10:59HS23070935-02 17 Jul 2023 15:10 1MW-G-I
19 Jul 2023 10:59HS23070935-04 17 Jul 2023 14:27 1MW-H-B
19 Jul 2023 10:59HS23070935-05 17 Jul 2023 15:05 5MW-H-I
19 Jul 2023 10:59HS23070935-06 17 Jul 2023 15:45 1MW-H-D
Batch ID:R441876 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
20 Jul 2023 15:10HS23070935-01 17 Jul 2023 15:40 10MW-G-B
20 Jul 2023 15:15HS23070935-02 17 Jul 2023 15:10 10MW-G-I
20 Jul 2023 15:50HS23070935-04 17 Jul 2023 14:27 10MW-H-B
20 Jul 2023 15:56HS23070935-05 17 Jul 2023 15:05 10MW-H-I
20 Jul 2023 16:02HS23070935-06 17 Jul 2023 15:45 10MW-H-D
Batch ID:R441892 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
20 Jul 2023 14:04HS23070935-03 17 Jul 2023 14:30 50MW-G-D
31-Jul-23Date: ALS Houston, US
Page 13 of 34
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23070935
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R441986 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
21 Jul 2023 08:38HS23070935-01 17 Jul 2023 15:40 1MW-G-B
21 Jul 2023 08:56HS23070935-02 17 Jul 2023 15:10 1MW-G-I
21 Jul 2023 10:04HS23070935-04 17 Jul 2023 14:27 2MW-H-B
21 Jul 2023 10:14HS23070935-05 17 Jul 2023 15:05 5MW-H-I
21 Jul 2023 09:27HS23070935-06 17 Jul 2023 15:45 1MW-H-D
Batch ID:R442693 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
28 Jul 2023 13:50HS23070935-01 17 Jul 2023 15:40 1MW-G-B
28 Jul 2023 13:56HS23070935-02 17 Jul 2023 15:10 1MW-G-I
28 Jul 2023 14:02HS23070935-04 17 Jul 2023 14:27 1MW-H-B
28 Jul 2023 14:08HS23070935-05 17 Jul 2023 15:05 1MW-H-I
28 Jul 2023 14:49HS23070935-06 17 Jul 2023 15:45 1MW-H-D
Batch ID:R442736 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
29 Jul 2023 12:25HS23070935-01 17 Jul 2023 15:40 1MW-G-B
29 Jul 2023 12:25HS23070935-02 17 Jul 2023 15:10 1MW-G-I
29 Jul 2023 12:25HS23070935-04 17 Jul 2023 14:27 1MW-H-B
29 Jul 2023 12:25HS23070935-05 17 Jul 2023 15:05 1MW-H-I
29 Jul 2023 12:25HS23070935-06 17 Jul 2023 15:45 1MW-H-D
31-Jul-23Date: ALS Houston, US
Page 14 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:197842 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197842 Units:ug/L Analysis Date:23-Jul-2023 22:21
Run ID:ECD_13_442222 SeqNo:7448736 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197842 Units:ug/L Analysis Date:23-Jul-2023 22:44
Run ID:ECD_13_442222 SeqNo:7448737 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.2266 0.25 0 90.6 60 - 1400.020
Sample ID:LCSD-197842 Units:ug/L Analysis Date:23-Jul-2023 23:08
Run ID:ECD_13_442222 SeqNo:7448738 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.2303 0.25 0 92.1 60 - 140 0.2266 1.63 200.020
The following samples were analyzed in this batch:HS23070935-01 HS23070935-02 HS23070935-03 HS23070935-04
HS23070935-05 HS23070935-06
ALS Houston, US Date: 31-Jul-23
Page 15 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R441986 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230721 Units:ug/L Analysis Date:21-Jul-2023 07:07
Run ID:FID-4_441986 SeqNo:7443383 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230721 Units:ug/L Analysis Date:21-Jul-2023 07:40
Run ID:FID-4_441986 SeqNo:7443384 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.855 9.647 0 81.4 75 - 1250.500
Sample ID:LCSD-230721 Units:ug/L Analysis Date:21-Jul-2023 08:01
Run ID:FID-4_441986 SeqNo:7443385 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 7.797 9.647 0 80.8 75 - 125 7.855 0.747 300.500
Sample ID:HS23070935-02DUP Units:ug/L Analysis Date:21-Jul-2023 09:44
Run ID:FID-4_441986 SeqNo:7443391 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:MW-G-I
Methane 16.97 16.73 1.42 300.500
The following samples were analyzed in this batch:HS23070935-01 HS23070935-02 HS23070935-04 HS23070935-05
HS23070935-06
ALS Houston, US Date: 31-Jul-23
Page 16 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:198234 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198234 Units:mg/L Analysis Date:28-Jul-2023 21:54
Run ID:ICPMS05_442602 SeqNo:7460488 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese 0.001726 J 0.00500
Sample ID:LCS-198234 Units:mg/L Analysis Date:28-Jul-2023 21:56
Run ID:ICPMS05_442602 SeqNo:7460489 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.76 5 0 95.2 80 - 1200.200
Manganese 0.04489 0.05 0 89.8 80 - 1200.00500
Sample ID:HS23071175-03MS Units:mg/L Analysis Date:28-Jul-2023 22:02
Run ID:ICPMS05_442602 SeqNo:7460459 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.08 5 0.1716 98.2 80 - 1200.200
Manganese 0.1304 0.05 0.08299 94.9 80 - 1200.00500
Sample ID:HS23071175-03MSD Units:mg/L Analysis Date:28-Jul-2023 22:04
Run ID:ICPMS05_442602 SeqNo:7460460 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.043 5 0.1716 97.4 80 - 120 5.08 0.73 200.200
Manganese 0.1299 0.05 0.08299 93.9 80 - 120 0.1304 0.4 200.00500
Sample ID:HS23071175-03PDS Units:mg/L Analysis Date:28-Jul-2023 22:06
Run ID:ICPMS05_442602 SeqNo:7460461 PrepDate:28-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 9.974 10 0.1716 98.0 75 - 1250.200
Manganese 0.176 0.1 0.08299 93.0 75 - 1250.00500
ALS Houston, US Date: 31-Jul-23
Page 17 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:198234 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23071175-03SD Units:mg/L Analysis Date:28-Jul-2023 22:00
Run ID:ICPMS05_442602 SeqNo:7460458 PrepDate:28-Jul-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron 0.1575 0.1716 0 10 J 1.00
Manganese 0.08327 0.08299 0.345 100.0250
The following samples were analyzed in this batch:HS23070935-01 HS23070935-02 HS23070935-04 HS23070935-05
HS23070935-06
ALS Houston, US Date: 31-Jul-23
Page 18 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R441787 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230719 Units:ug/L Analysis Date:19-Jul-2023 21:10
Run ID:VOA11_441787 SeqNo:7438803 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
48.5 50 0 97.0 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.57 50 0 93.1 77 - 1131.0Surr: 4-Bromofluorobenzene
48.94 50 0 97.9 73 - 1261.0Surr: Dibromofluoromethane
51.03 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 31-Jul-23
Page 19 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R441787 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230719 Units:ug/L Analysis Date:19-Jul-2023 20:28
Run ID:VOA11_441787 SeqNo:7438802 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 20.94 20 0 105 73 - 1211.0
1,2-Dibromoethane 18.66 20 0 93.3 76 - 1231.0
1,2-Dichloroethane 18.02 20 0 90.1 70 - 1241.0
2-Methylnaphthalene 17.09 20 0 85.5 55 - 1401.0
4-Isopropyltoluene 21.01 20 0 105 74 - 1261.0
Benzene 18.65 20 0 93.3 74 - 1201.0
Chloroform 19.17 20 0 95.8 71 - 1211.0
Ethylbenzene 20.13 20 0 101 77 - 1171.0
m,p-Xylene 40.29 40 0 101 77 - 1222.0
Methyl tert-butyl ether 17.35 20 0 86.8 70 - 1301.0
Methylene chloride 22.49 20 0 112 70 - 1272.0
Naphthalene 18.74 20 0 93.7 70 - 1301.0
o-Xylene 21.01 20 0 105 75 - 1191.0
Tert-butyl alcohol 301.8 400 0 75.4 70 - 13010
Toluene 19.28 20 0 96.4 77 - 1181.0
Xylenes, Total 61.3 60 0 102 75 - 1223.0
45.68 50 0 91.4 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.86 50 0 95.7 77 - 1131.0Surr: 4-Bromofluorobenzene
48.7 50 0 97.4 73 - 1261.0Surr: Dibromofluoromethane
51.24 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 31-Jul-23
Page 20 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R441787 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23070922-01MS Units:ug/L Analysis Date:19-Jul-2023 23:37
Run ID:VOA11_441787 SeqNo:7438810 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 13.6 20 0 68.0 70 - 125 S1.0
1,2-Dibromoethane 11.73 20 0 58.6 70 - 124 S1.0
1,2-Dichloroethane 12.62 20 0 63.1 70 - 127 S1.0
2-Methylnaphthalene 11.09 20 0 55.5 55 - 1401.0
4-Isopropyltoluene 13.28 20 0 66.4 70 - 130 S1.0
Benzene 13.8 20 0 69.0 70 - 127 S1.0
Chloroform 14.55 20 0 72.7 70 - 1251.0
Ethylbenzene 14.71 20 0 73.6 70 - 1241.0
m,p-Xylene 28.67 40 0 71.7 70 - 1302.0
Methyl tert-butyl ether 11.06 20 0 55.3 70 - 130 S1.0
Methylene chloride 14.51 20 0 72.5 70 - 1282.0
Naphthalene 11.11 20 0 55.5 70 - 130 S1.0
o-Xylene 14.25 20 0 71.2 70 - 1241.0
Tert-butyl alcohol 200 400 0 50.0 70 - 130 S10
Toluene 13.86 20 0 69.3 70 - 123 S1.0
Xylenes, Total 42.91 60 0 71.5 70 - 1303.0
46.47 50 0 92.9 70 - 1261.0Surr: 1,2-Dichloroethane-d4
46.79 50 0 93.6 77 - 1131.0Surr: 4-Bromofluorobenzene
50.07 50 0 100 77 - 1231.0Surr: Dibromofluoromethane
50.81 50 0 102 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 31-Jul-23
Page 21 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R441787 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23070922-01MSD Units:ug/L Analysis Date:19-Jul-2023 23:58
Run ID:VOA11_441787 SeqNo:7438811 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 12.5 20 0 62.5 70 - 125 13.6 8.46 20 S1.0
1,2-Dibromoethane 11.39 20 0 56.9 70 - 124 11.73 2.94 20 S1.0
1,2-Dichloroethane 12.28 20 0 61.4 70 - 127 12.62 2.76 20 S1.0
2-Methylnaphthalene 11.58 20 0 57.9 55 - 140 11.09 4.34 201.0
4-Isopropyltoluene 12.71 20 0 63.6 70 - 130 13.28 4.34 20 S1.0
Benzene 12.88 20 0 64.4 70 - 127 13.8 6.9 20 S1.0
Chloroform 13.15 20 0 65.8 70 - 125 14.55 10 20 S1.0
Ethylbenzene 12.79 20 0 64.0 70 - 124 14.71 13.9 20 S1.0
m,p-Xylene 26.34 40 0 65.8 70 - 130 28.67 8.48 20 S2.0
Methyl tert-butyl ether 10.26 20 0 51.3 70 - 130 11.06 7.54 20 S1.0
Methylene chloride 13.93 20 0 69.7 70 - 128 14.51 4.05 20 S2.0
Naphthalene 11.6 20 0 58.0 70 - 130 11.11 4.32 20 S1.0
o-Xylene 12.54 20 0 62.7 70 - 124 14.25 12.7 20 S1.0
Tert-butyl alcohol 203.3 400 0 50.8 70 - 130 200 1.63 20 S10
Toluene 12.43 20 0 62.1 70 - 123 13.86 10.9 20 S1.0
Xylenes, Total 38.88 60 0 64.8 70 - 130 42.91 9.86 20 S3.0
45.79 50 0 91.6 70 - 126 46.47 1.47 201.0Surr: 1,2-Dichloroethane-d4
47.18 50 0 94.4 77 - 113 46.79 0.841 201.0Surr: 4-Bromofluorobenzene
49.21 50 0 98.4 77 - 123 50.07 1.73 201.0Surr: Dibromofluoromethane
49.04 50 0 98.1 82 - 127 50.81 3.53 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23070935-01 HS23070935-02 HS23070935-03 HS23070935-04
HS23070935-05 HS23070935-06 HS23070935-07
ALS Houston, US Date: 31-Jul-23
Page 22 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R441892 ( 0 )Instrument:VOA7 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230720 Units:ug/L Analysis Date:20-Jul-2023 10:25
Run ID:VOA7_441892 SeqNo:7441393 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methyl tert-butyl ether U 1.0
Tert-butyl alcohol U 10
48.46 50 0 96.9 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.31 50 0 96.6 77 - 1131.0Surr: 4-Bromofluorobenzene
49.32 50 0 98.6 73 - 1261.0Surr: Dibromofluoromethane
50 50 0 100.0 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230720 Units:ug/L Analysis Date:20-Jul-2023 09:42
Run ID:VOA7_441892 SeqNo:7441392 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methyl tert-butyl ether 19.6 20 0 98.0 70 - 1301.0
Tert-butyl alcohol 328 400 0 82.0 70 - 13010
48.76 50 0 97.5 70 - 1231.0Surr: 1,2-Dichloroethane-d4
49.13 50 0 98.3 77 - 1131.0Surr: 4-Bromofluorobenzene
50.24 50 0 100 73 - 1261.0Surr: Dibromofluoromethane
50.1 50 0 100 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23070946-01MS Units:ug/L Analysis Date:20-Jul-2023 11:31
Run ID:VOA7_441892 SeqNo:7441396 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Methyl tert-butyl ether 19.93 20 0 99.6 70 - 1301.0
Tert-butyl alcohol 290.4 400 0 72.6 70 - 13010
47.53 50 0 95.1 70 - 1261.0Surr: 1,2-Dichloroethane-d4
49.23 50 0 98.5 77 - 1131.0Surr: 4-Bromofluorobenzene
48.84 50 0 97.7 77 - 1231.0Surr: Dibromofluoromethane
49.94 50 0 99.9 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 31-Jul-23
Page 23 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R441892 ( 0 )Instrument:VOA7 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23070946-01MSD Units:ug/L Analysis Date:20-Jul-2023 11:53
Run ID:VOA7_441892 SeqNo:7441397 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Methyl tert-butyl ether 22.1 20 0 110 70 - 130 19.93 10.3 201.0
Tert-butyl alcohol 344.6 400 0 86.2 70 - 130 290.4 17.1 2010
48.7 50 0 97.4 70 - 126 47.53 2.43 201.0Surr: 1,2-Dichloroethane-d4
49.05 50 0 98.1 77 - 113 49.23 0.362 201.0Surr: 4-Bromofluorobenzene
49.57 50 0 99.1 77 - 123 48.84 1.49 201.0Surr: Dibromofluoromethane
50.05 50 0 100 82 - 127 49.94 0.233 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23070935-03
ALS Houston, US Date: 31-Jul-23
Page 24 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R441843 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441843 Units:mg/L Analysis Date:19-Jul-2023 10:59
Run ID:UV-2450_441843 SeqNo:7440150 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441843 Units:mg/L Analysis Date:19-Jul-2023 10:59
Run ID:UV-2450_441843 SeqNo:7440149 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.256 0.25 0 102 80 - 1200.0500
Sample ID:HS23070935-01MS Units:mg/L Analysis Date:19-Jul-2023 10:59
Run ID:UV-2450_441843 SeqNo:7440151 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-G-B
Ferrous Iron 0.262 0.25 0.012 100 75 - 1250.0500
The following samples were analyzed in this batch:HS23070935-01 HS23070935-02 HS23070935-04 HS23070935-05
HS23070935-06
ALS Houston, US Date: 31-Jul-23
Page 25 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R441876 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:20-Jul-2023 12:28
Run ID:ICS-Integrion_441876 SeqNo:7440828 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:20-Jul-2023 12:34
Run ID:ICS-Integrion_441876 SeqNo:7440829 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.055 8 0 101 90 - 1100.200
Sample ID:HS23070922-04MS Units:mg/L Analysis Date:20-Jul-2023 14:41
Run ID:ICS-Integrion_441876 SeqNo:7440843 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)35.93 40 0 89.8 80 - 1202.00
Sample ID:HS23070339-01MS Units:mg/L Analysis Date:20-Jul-2023 13:14
Run ID:ICS-Integrion_441876 SeqNo:7440831 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)35.84 40 2.793 82.6 80 - 1202.00
Sample ID:HS23070922-04MSD Units:mg/L Analysis Date:20-Jul-2023 14:46
Run ID:ICS-Integrion_441876 SeqNo:7440844 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)36.38 40 0 91.0 80 - 120 35.93 1.25 202.00
Sample ID:HS23070339-01MSD Units:mg/L Analysis Date:20-Jul-2023 13:20
Run ID:ICS-Integrion_441876 SeqNo:7440832 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)36.85 40 2.793 85.1 80 - 120 35.84 2.77 202.00
The following samples were analyzed in this batch:HS23070935-01 HS23070935-02 HS23070935-04 HS23070935-05
HS23070935-06
ALS Houston, US Date: 31-Jul-23
Page 26 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R442693 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:28-Jul-2023 09:59
Run ID:ICS-Integrion_442693 SeqNo:7459857 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:28-Jul-2023 10:16
Run ID:ICS-Integrion_442693 SeqNo:7459858 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.65 20 0 98.3 90 - 1100.500
Sample ID:HS23071760-02MS Units:mg/L Analysis Date:28-Jul-2023 10:33
Run ID:ICS-Integrion_442693 SeqNo:7459860 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 12.28 10 2.936 93.4 80 - 1200.500
Sample ID:HS23071518-01MS Units:mg/L Analysis Date:28-Jul-2023 13:39
Run ID:ICS-Integrion_442693 SeqNo:7459885 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 149.4 100 71 78.4 80 - 120 S 5.00
Sample ID:HS23070922-04MS Units:mg/L Analysis Date:28-Jul-2023 11:54
Run ID:ICS-Integrion_442693 SeqNo:7459870 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 13.28 10 3.357 99.2 80 - 1200.500
Sample ID:HS23071760-02MSD Units:mg/L Analysis Date:28-Jul-2023 10:39
Run ID:ICS-Integrion_442693 SeqNo:7459861 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 12.29 10 2.936 93.6 80 - 120 12.28 0.112 200.500
ALS Houston, US Date: 31-Jul-23
Page 27 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R442693 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:HS23071518-01MSD Units:mg/L Analysis Date:28-Jul-2023 13:45
Run ID:ICS-Integrion_442693 SeqNo:7459886 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 150 100 71 79.0 80 - 120 149.4 0.421 20 S 5.00
Sample ID:HS23070922-04MSD Units:mg/L Analysis Date:28-Jul-2023 12:00
Run ID:ICS-Integrion_442693 SeqNo:7459871 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 13.32 10 3.357 99.6 80 - 120 13.28 0.337 200.500
The following samples were analyzed in this batch:HS23070935-01 HS23070935-02 HS23070935-04 HS23070935-05
HS23070935-06
ALS Houston, US Date: 31-Jul-23
Page 28 of 34
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23070935
QC BATCH REPORT
Batch ID:R442736 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:MBLK-R442736 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442736 SeqNo:7461095 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-R442736 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442736 SeqNo:7461094 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)968.6 1000 0 96.9 85 - 1155.00
Alkalinity, Total (As CaCO3)1009 1000 0 101 85 - 1155.00
Sample ID:LCSD-R442736 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442736 SeqNo:7461093 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)986.3 1000 0 98.6 85 - 115 968.6 1.81 205.00
Alkalinity, Total (As CaCO3)1008 1000 0 101 85 - 115 1009 0.157 205.00
Sample ID:HS23070912-01DUP Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442736 SeqNo:7461096 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)345.2 358.4 3.76 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)345.2 358.4 3.76 205.00
The following samples were analyzed in this batch:HS23070935-01 HS23070935-02 HS23070935-04 HS23070935-05
HS23070935-06
ALS Houston, US Date: 31-Jul-23
Page 29 of 34
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23070935
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 31-Jul-23
Page 30 of 34
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
31-Jul-23Date: ALS Houston, US
Page 31 of 34
Malcolm Burleson
18-Jul-2023 09:25Date/Time Received:HS23070935
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
5.3C/5.2C UC/C IR 31
47692
07/18/2023 15:00
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Nilesh D. Ranchod
Date/TimeeSignatureDate/TimeeSignature
18-Jul-2023 12:54
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241116
ALS Houston, US 31-Jul-23Date:
Page 32 of 34
Page 33 of 34
Page 34 of 34
August 01, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 8 sample(s) on Jul 19, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071014
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 36
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071014
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071014-01 18-Jul-2023 09:55 19-Jul-2023 13:35PMW-K-I Groundwater
HS23071014-02 18-Jul-2023 10:50 19-Jul-2023 13:35PMW-K-D Groundwater
HS23071014-03 18-Jul-2023 11:35 19-Jul-2023 13:35PMW-K-B Groundwater
HS23071014-04 18-Jul-2023 12:35 19-Jul-2023 13:35Z2-X31 Groundwater
HS23071014-05 18-Jul-2023 13:35 19-Jul-2023 13:35MW-D-I Groundwater
HS23071014-06 18-Jul-2023 14:35 19-Jul-2023 13:35MW-D-D Groundwater
HS23071014-07 18-Jul-2023 15:45 19-Jul-2023 13:35MW-D-B Groundwater
HS23071014-08 18-Jul-2023 00:00 19-Jul-2023 13:35Trip Blank Water
ALS Houston, US 01-Aug-23Date:
Page 2 of 36
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071014
ECD Organics by Method SW8011
Batch ID: 197843
Sample ID: MBLK-197843
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
Batch ID: 197842
Sample ID: MBLK-197842
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R441986
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R441822
Sample ID: PMW-K-I (HS23071014-01MS)
MS/MSD/RPD failed QC limit for some compounds•
Batch ID: R441923
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Metals by Method SW6020A
Batch ID: 198311
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R442749
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442827
Sample ID: HS23071023-05MS
MS and MSD are for an unrelated sample (Sulfate)•
Batch ID: R442705
Sample ID: MW-D-B (HS23071014-07)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-D-D (HS23071014-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
ALS Houston, US 01-Aug-23Date:
Page 3 of 36
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071014
WetChemistry by Method E300
WetChemistry by Method SM3500FED
Batch ID: R441813
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 01-Aug-23Date:
Page 4 of 36
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-K-I
WorkOrder:
Lab ID:
Collection Date:
HS23071014
HS23071014-01
18-Jul-2023 09:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 10:490.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 10:490.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 10:490.201,2-Dichloroethane 1.07.2
1ug/L 20-Jul-2023 10:491.02-Methylnaphthalene 1.04.2
1ug/L 20-Jul-2023 10:490.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 10:490.20Benzene 1.02.4
1ug/L 20-Jul-2023 10:490.20Chloroform 1.0U
1ug/L 20-Jul-2023 10:490.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 10:490.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 10:490.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 10:491.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 10:490.30Naphthalene 1.03.8
1ug/L 20-Jul-2023 10:490.30o-Xylene 1.0U
1ug/L 20-Jul-2023 10:4910Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 10:490.20Toluene 1.0U
1ug/L 20-Jul-2023 10:490.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 10:4910070-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 10:4992.2 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 10:4910377-123
Surr: Toluene-d8 1%REC 20-Jul-2023 10:4910182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 08:550.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 36
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-K-D
WorkOrder:
Lab ID:
Collection Date:
HS23071014
HS23071014-02
18-Jul-2023 10:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 14:400.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 14:400.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 14:400.201,2-Dichloroethane 1.01.6
1ug/L 20-Jul-2023 14:401.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 14:400.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 14:400.20Benzene 1.0U
1ug/L 20-Jul-2023 14:400.20Chloroform 1.0U
1ug/L 20-Jul-2023 14:400.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 14:400.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 14:400.20Methyl tert-butyl ether 1.037
1ug/L 20-Jul-2023 14:401.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 14:400.30Naphthalene 1.0U
1ug/L 20-Jul-2023 14:400.30o-Xylene 1.0U
1ug/L 20-Jul-2023 14:4010Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 14:400.20Toluene 1.0U
1ug/L 20-Jul-2023 14:400.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 14:4097.8 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 14:4093.7 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 14:4010177-123
Surr: Toluene-d8 1%REC 20-Jul-2023 14:4010282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 09:190.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 36
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-K-B
WorkOrder:
Lab ID:
Collection Date:
HS23071014
HS23071014-03
18-Jul-2023 11:35 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 15:010.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 15:010.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 15:01J0.201,2-Dichloroethane 1.00.61
1ug/L 20-Jul-2023 15:011.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 15:010.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 15:010.20Benzene 1.0U
1ug/L 20-Jul-2023 15:010.20Chloroform 1.0U
1ug/L 20-Jul-2023 15:010.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 15:010.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 15:010.20Methyl tert-butyl ether 1.014
1ug/L 20-Jul-2023 15:011.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 15:010.30Naphthalene 1.0U
1ug/L 20-Jul-2023 15:010.30o-Xylene 1.0U
1ug/L 20-Jul-2023 15:0110Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 15:010.20Toluene 1.0U
1ug/L 20-Jul-2023 15:010.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 15:0195.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 15:0191.4 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 15:0110277-123
Surr: Toluene-d8 1%REC 20-Jul-2023 15:0110282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 09:430.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 36
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-X31
WorkOrder:
Lab ID:
Collection Date:
HS23071014
HS23071014-04
18-Jul-2023 12:35 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 15:220.301,2,4-Trimethylbenzene 1.012
1ug/L 20-Jul-2023 15:220.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 15:220.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 15:221.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 15:220.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 15:22J0.20Benzene 1.00.41
1ug/L 20-Jul-2023 15:220.20Chloroform 1.0U
1ug/L 20-Jul-2023 15:220.30Ethylbenzene 1.05.8
1ug/L 20-Jul-2023 15:220.50m,p-Xylene 2.03.8
1ug/L 20-Jul-2023 15:220.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 15:221.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 15:220.30Naphthalene 1.02.6
1ug/L 20-Jul-2023 15:220.30o-Xylene 1.01.5
1ug/L 20-Jul-2023 15:2210Tert-butyl alcohol 10110
1ug/L 20-Jul-2023 15:220.20Toluene 1.0U
1ug/L 20-Jul-2023 15:220.30Xylenes, Total 3.05.2
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 15:2297.6 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 15:2293.9 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 15:2210477-123
Surr: Toluene-d8 1%REC 20-Jul-2023 15:2299.8 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 10:060.00321,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 36
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-D-I
WorkOrder:
Lab ID:
Collection Date:
HS23071014
HS23071014-05
18-Jul-2023 13:35 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 15:430.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 15:430.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 15:430.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 15:431.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 15:430.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 15:430.20Benzene 1.0U
1ug/L 20-Jul-2023 15:430.20Chloroform 1.0U
1ug/L 20-Jul-2023 15:430.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 15:430.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 15:430.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 15:431.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 15:430.30Naphthalene 1.0U
1ug/L 20-Jul-2023 15:430.30o-Xylene 1.0U
1ug/L 20-Jul-2023 15:4310Tert-butyl alcohol 10380
1ug/L 20-Jul-2023 15:430.20Toluene 1.0U
1ug/L 20-Jul-2023 15:430.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 15:4395.9 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 15:4393.6 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 15:4399.2 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 15:4310282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 10:300.00321,2-Dibromoethane 0.0210.038
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 36
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-D-D
WorkOrder:
Lab ID:
Collection Date:
HS23071014
HS23071014-06
18-Jul-2023 14:35 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 16:040.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 16:040.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 16:040.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 16:041.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 16:040.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 16:040.20Benzene 1.0U
1ug/L 20-Jul-2023 16:040.20Chloroform 1.0U
1ug/L 20-Jul-2023 16:040.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 16:040.50m,p-Xylene 2.0U
10ug/L 21-Jul-2023 12:032.0Methyl tert-butyl ether 10230
1ug/L 20-Jul-2023 16:041.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 16:040.30Naphthalene 1.0U
1ug/L 20-Jul-2023 16:040.30o-Xylene 1.0U
1ug/L 20-Jul-2023 16:0410Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 16:040.20Toluene 1.0U
1ug/L 20-Jul-2023 16:040.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 16:0494.0 70-126
Surr: 1,2-Dichloroethane-d4 10%REC 21-Jul-2023 12:0394.3 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 16:0493.2 77-113
Surr: 4-Bromofluorobenzene 10%REC 21-Jul-2023 12:0395.2 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 16:0489.9 77-123
Surr: Dibromofluoromethane 10%REC 21-Jul-2023 12:0310277-123
Surr: Toluene-d8 1%REC 20-Jul-2023 16:0410282-127
Surr: Toluene-d8 10%REC 21-Jul-2023 12:0310282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 10:230.107Methane 0.50014.9
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 10:540.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:200.0120Iron 0.200U
1mg/L 01-Aug-2023 14:200.000700Manganese 0.005000.00684
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 21:330.200Sulfate 0.5003.79
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 00:160.300Nitrate/Nitrite (as N)2.00U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 36
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-D-D
WorkOrder:
Lab ID:
Collection Date:
HS23071014
HS23071014-06
18-Jul-2023 14:35 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.0046.3
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00167
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00213
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.0500U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 36
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-D-B
WorkOrder:
Lab ID:
Collection Date:
HS23071014
HS23071014-07
18-Jul-2023 15:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 16:250.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 16:250.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 16:250.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 16:251.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 16:250.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 16:250.20Benzene 1.0U
1ug/L 20-Jul-2023 16:250.20Chloroform 1.0U
1ug/L 20-Jul-2023 16:250.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 16:250.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 16:250.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 16:251.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 16:250.30Naphthalene 1.0U
1ug/L 20-Jul-2023 16:250.30o-Xylene 1.0U
1ug/L 20-Jul-2023 16:2510Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 16:250.20Toluene 1.0U
1ug/L 20-Jul-2023 16:250.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 16:2595.3 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 16:2594.9 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 16:2595.2 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 16:2510282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 10:340.107Methane 0.5003.49
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 12:280.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:230.0120Iron 0.200U
1mg/L 01-Aug-2023 14:230.000700Manganese 0.00500U
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 21:560.200Sulfate 0.5005.29
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 00:330.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00101
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.0062.9
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00164
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.0500U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 36
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071014
HS23071014-08
18-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 13:370.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 13:370.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 13:370.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 13:371.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 13:370.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 13:370.20Benzene 1.0U
1ug/L 20-Jul-2023 13:370.20Chloroform 1.0U
1ug/L 20-Jul-2023 13:370.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 13:370.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 13:370.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 13:371.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 13:370.30Naphthalene 1.0U
1ug/L 20-Jul-2023 13:370.30o-Xylene 1.0U
1ug/L 20-Jul-2023 13:3710Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 13:370.20Toluene 1.0U
1ug/L 20-Jul-2023 13:370.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 13:3794.2 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 13:3794.5 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 13:3797.9 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 13:3710282-127
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 36
Weight / Prep Log
HS23071014
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197842
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:26 End Date: 21 Jul 2023 09:26
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071014-01 35 (mL)40 mL VOA w/ HCL36.25 (mL)1.036
HS23071014-02 35 (mL)40 mL VOA w/ HCL36.63 (mL)1.047
HS23071014-03 35 (mL)40 mL VOA w/ HCL36.05 (mL)1.03
HS23071014-04 35 (mL)40 mL VOA w/ HCL36.79 (mL)1.051
Batch ID:197843
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:45 End Date: 21 Jul 2023 09:45
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071014-05 35 (mL)40 mL VOA w/ HCL36.87 (mL)1.053
HS23071014-06 35 (mL)40 mL VOA w/ HCL36.34 (mL)1.038
HS23071014-07 35 (mL)40 mL VOA w/ HCL36.63 (mL)1.047
Batch ID:198311
Method:WATER - SW3010A 3010APrep Code:
Start Date: 31 Jul 2023 11:00 End Date: 31 Jul 2023 11:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071014-06 10 (mL)120 plastic HNO310 (mL)1
HS23071014-07 10 (mL)120 plastic HNO310 (mL)1
01-Aug-23Date: ALS Houston, US
Page 14 of 36
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071014
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197842 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:26 24 Jul 2023 08:55HS23071014-01 18 Jul 2023 09:55 1PMW-K-I
21 Jul 2023 09:26 24 Jul 2023 09:19HS23071014-02 18 Jul 2023 10:50 1PMW-K-D
21 Jul 2023 09:26 24 Jul 2023 09:43HS23071014-03 18 Jul 2023 11:35 1PMW-K-B
21 Jul 2023 09:26 24 Jul 2023 10:06HS23071014-04 18 Jul 2023 12:35 1Z2-X31
Batch ID:197843 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:45 24 Jul 2023 10:30HS23071014-05 18 Jul 2023 13:35 1MW-D-I
21 Jul 2023 09:45 24 Jul 2023 10:54HS23071014-06 18 Jul 2023 14:35 1MW-D-D
21 Jul 2023 09:45 24 Jul 2023 12:28HS23071014-07 18 Jul 2023 15:45 1MW-D-B
Batch ID:198311 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
31 Jul 2023 11:00 01 Aug 2023 14:20HS23071014-06 18 Jul 2023 14:35 1MW-D-D
31 Jul 2023 11:00 01 Aug 2023 14:23HS23071014-07 18 Jul 2023 15:45 1MW-D-B
Batch ID:R441813 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
20 Jul 2023 10:02HS23071014-06 18 Jul 2023 14:35 1MW-D-D
20 Jul 2023 10:02HS23071014-07 18 Jul 2023 15:45 1MW-D-B
Batch ID:R441822 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
20 Jul 2023 13:37HS23071014-08 18 Jul 2023 00:00 1Trip Blank
Batch ID:R441822 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
20 Jul 2023 10:49HS23071014-01 18 Jul 2023 09:55 1PMW-K-I
20 Jul 2023 14:40HS23071014-02 18 Jul 2023 10:50 1PMW-K-D
20 Jul 2023 15:01HS23071014-03 18 Jul 2023 11:35 1PMW-K-B
20 Jul 2023 15:22HS23071014-04 18 Jul 2023 12:35 1Z2-X31
20 Jul 2023 15:43HS23071014-05 18 Jul 2023 13:35 1MW-D-I
20 Jul 2023 16:04HS23071014-06 18 Jul 2023 14:35 1MW-D-D
20 Jul 2023 16:25HS23071014-07 18 Jul 2023 15:45 1MW-D-B
Batch ID:R441923 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 12:03HS23071014-06 18 Jul 2023 14:35 10MW-D-D
Batch ID:R441986 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
21 Jul 2023 10:23HS23071014-06 18 Jul 2023 14:35 1MW-D-D
21 Jul 2023 10:34HS23071014-07 18 Jul 2023 15:45 1MW-D-B
Batch ID:R442705 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
29 Jul 2023 00:16HS23071014-06 18 Jul 2023 14:35 10MW-D-D
29 Jul 2023 00:33HS23071014-07 18 Jul 2023 15:45 10MW-D-B
Batch ID:R442749 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
29 Jul 2023 12:25HS23071014-06 18 Jul 2023 14:35 1MW-D-D
29 Jul 2023 12:25HS23071014-07 18 Jul 2023 15:45 1MW-D-B
01-Aug-23Date: ALS Houston, US
Page 15 of 36
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071014
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442827 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
31 Jul 2023 21:33HS23071014-06 18 Jul 2023 14:35 1MW-D-D
31 Jul 2023 21:56HS23071014-07 18 Jul 2023 15:45 1MW-D-B
01-Aug-23Date: ALS Houston, US
Page 16 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:197842 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197842 Units:ug/L Analysis Date:23-Jul-2023 22:21
Run ID:ECD_13_442222 SeqNo:7448736 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197842 Units:ug/L Analysis Date:23-Jul-2023 22:44
Run ID:ECD_13_442222 SeqNo:7448737 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.2266 0.25 0 90.6 60 - 1400.020
Sample ID:LCSD-197842 Units:ug/L Analysis Date:23-Jul-2023 23:08
Run ID:ECD_13_442222 SeqNo:7448738 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.2303 0.25 0 92.1 60 - 140 0.2266 1.63 200.020
The following samples were analyzed in this batch:HS23071014-01 HS23071014-02 HS23071014-03 HS23071014-04
ALS Houston, US Date: 01-Aug-23
Page 17 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:197843 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197843 Units:ug/L Analysis Date:24-Jul-2023 01:05
Run ID:ECD_13_442223 SeqNo:7448785 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197843 Units:ug/L Analysis Date:24-Jul-2023 01:28
Run ID:ECD_13_442223 SeqNo:7448786 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.2347 0.25 0 93.9 60 - 1400.020
Sample ID:LCSD-197843 Units:ug/L Analysis Date:24-Jul-2023 01:52
Run ID:ECD_13_442223 SeqNo:7448787 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.213 0.25 0 85.2 60 - 140 0.2347 9.7 200.020
The following samples were analyzed in this batch:HS23071014-05 HS23071014-06 HS23071014-07
ALS Houston, US Date: 01-Aug-23
Page 18 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R441986 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230721 Units:ug/L Analysis Date:21-Jul-2023 07:07
Run ID:FID-4_441986 SeqNo:7443383 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230721 Units:ug/L Analysis Date:21-Jul-2023 07:40
Run ID:FID-4_441986 SeqNo:7443384 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.855 9.647 0 81.4 75 - 1250.500
Sample ID:LCSD-230721 Units:ug/L Analysis Date:21-Jul-2023 08:01
Run ID:FID-4_441986 SeqNo:7443385 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 7.797 9.647 0 80.8 75 - 125 7.855 0.747 300.500
Sample ID:HS23070935-02DUP Units:ug/L Analysis Date:21-Jul-2023 09:44
Run ID:FID-4_441986 SeqNo:7443391 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Methane 16.97 16.73 1.42 300.500
The following samples were analyzed in this batch:HS23071014-06 HS23071014-07
ALS Houston, US Date: 01-Aug-23
Page 19 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:198311 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198311 Units:mg/L Analysis Date:01-Aug-2023 13:49
Run ID:ICPMS06_442867 SeqNo:7464813 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese 0.000794 J 0.00500
Sample ID:LCS-198311 Units:mg/L Analysis Date:01-Aug-2023 13:52
Run ID:ICPMS06_442867 SeqNo:7464814 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.563 5 0 91.3 80 - 1200.200
Manganese 0.04482 0.05 0 89.6 80 - 1200.00500
Sample ID:HS23070892-01MS Units:mg/L Analysis Date:01-Aug-2023 13:59
Run ID:ICPMS06_442867 SeqNo:7464817 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.048 5 0.02657 100 80 - 1200.200
Manganese 0.1484 0.05 0.09528 106 80 - 1200.00500
Sample ID:HS23070892-01MSD Units:mg/L Analysis Date:01-Aug-2023 14:01
Run ID:ICPMS06_442867 SeqNo:7464818 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.293 5 0.02657 105 80 - 120 5.048 4.74 200.200
Manganese 0.1545 0.05 0.09528 118 80 - 120 0.1484 4.01 200.00500
Sample ID:HS23070892-01PDS Units:mg/L Analysis Date:01-Aug-2023 14:03
Run ID:ICPMS06_442867 SeqNo:7464819 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 10.48 10 0.02657 104 75 - 1250.200
Manganese 0.2032 0.1 0.09528 108 75 - 1250.00500
ALS Houston, US Date: 01-Aug-23
Page 20 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:198311 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23070892-01SD Units:mg/L Analysis Date:01-Aug-2023 13:57
Run ID:ICPMS06_442867 SeqNo:7464816 PrepDate:31-Jul-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron U 0.02657 0 101.00
Manganese 0.09742 0.09528 2.25 100.0250
The following samples were analyzed in this batch:HS23071014-06 HS23071014-07
ALS Houston, US Date: 01-Aug-23
Page 21 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230720 Units:ug/L Analysis Date:20-Jul-2023 10:28
Run ID:VOA11_441822 SeqNo:7439640 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
48.56 50 0 97.1 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.86 50 0 91.7 77 - 1131.0Surr: 4-Bromofluorobenzene
49.8 50 0 99.6 73 - 1261.0Surr: Dibromofluoromethane
51.28 50 0 103 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 22 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230720 Units:ug/L Analysis Date:20-Jul-2023 09:46
Run ID:VOA11_441822 SeqNo:7439639 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.89 20 0 94.5 73 - 1211.0
1,2-Dibromoethane 17.19 20 0 86.0 76 - 1231.0
1,2-Dichloroethane 16.7 20 0 83.5 70 - 1241.0
2-Methylnaphthalene 15.22 20 0 76.1 55 - 1401.0
4-Isopropyltoluene 18.8 20 0 94.0 74 - 1261.0
Benzene 18.3 20 0 91.5 74 - 1201.0
Chloroform 18.88 20 0 94.4 71 - 1211.0
Ethylbenzene 18.52 20 0 92.6 77 - 1171.0
m,p-Xylene 37.54 40 0 93.9 77 - 1222.0
Methyl tert-butyl ether 15.44 20 0 77.2 70 - 1301.0
Methylene chloride 21.16 20 0 106 70 - 1272.0
Naphthalene 16.52 20 0 82.6 70 - 1301.0
o-Xylene 19.2 20 0 96.0 75 - 1191.0
Tert-butyl alcohol 293.5 400 0 73.4 70 - 13010
Toluene 17.51 20 0 87.6 77 - 1181.0
Xylenes, Total 56.75 60 0 94.6 75 - 1223.0
44.62 50 0 89.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.02 50 0 96.0 77 - 1131.0Surr: 4-Bromofluorobenzene
49.25 50 0 98.5 73 - 1261.0Surr: Dibromofluoromethane
49.36 50 0 98.7 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 23 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071014-01MS Units:ug/L Analysis Date:20-Jul-2023 11:31
Run ID:VOA11_441822 SeqNo:7439643 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:PMW-K-I
1,2,4-Trimethylbenzene 17.04 20 0 85.2 70 - 1251.0
1,2-Dibromoethane 13.88 20 0 69.4 70 - 124 S1.0
1,2-Dichloroethane 21.28 20 7.19 70.5 70 - 1271.0
2-Methylnaphthalene 17.4 20 4.153 66.2 55 - 1401.0
4-Isopropyltoluene 17.45 20 0 87.3 70 - 1301.0
Benzene 19.04 20 2.396 83.2 70 - 1271.0
Chloroform 16.55 20 0 82.7 70 - 1251.0
Ethylbenzene 16.66 20 0 83.3 70 - 1241.0
m,p-Xylene 33.2 40 0 83.0 70 - 1302.0
Methyl tert-butyl ether 13.81 20 0 69.0 70 - 130 S1.0
Methylene chloride 17.79 20 0 89.0 70 - 1282.0
Naphthalene 19.21 20 3.823 76.9 70 - 1301.0
o-Xylene 16.77 20 0 83.8 70 - 1241.0
Tert-butyl alcohol 234.8 400 0 58.7 70 - 130 S10
Toluene 15.96 20 0 79.8 70 - 1231.0
Xylenes, Total 49.96 60 0 83.3 70 - 1303.0
46.11 50 0 92.2 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.26 50 0 94.5 77 - 1131.0Surr: 4-Bromofluorobenzene
48.94 50 0 97.9 77 - 1231.0Surr: Dibromofluoromethane
48.78 50 0 97.6 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 24 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071014-01MSD Units:ug/L Analysis Date:20-Jul-2023 11:52
Run ID:VOA11_441822 SeqNo:7439644 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:PMW-K-I
1,2,4-Trimethylbenzene 19.33 20 0 96.6 70 - 125 17.04 12.6 201.0
1,2-Dibromoethane 16.63 20 0 83.1 70 - 124 13.88 18 201.0
1,2-Dichloroethane 24.06 20 7.19 84.4 70 - 127 21.28 12.3 201.0
2-Methylnaphthalene 20.41 20 4.153 81.3 55 - 140 17.4 15.9 201.0
4-Isopropyltoluene 18.84 20 0 94.2 70 - 130 17.45 7.66 201.0
Benzene 20.72 20 2.396 91.6 70 - 127 19.04 8.43 201.0
Chloroform 19.37 20 0 96.9 70 - 125 16.55 15.7 201.0
Ethylbenzene 19.99 20 0 99.9 70 - 124 16.66 18.2 201.0
m,p-Xylene 38.35 40 0 95.9 70 - 130 33.2 14.4 202.0
Methyl tert-butyl ether 16.26 20 0 81.3 70 - 130 13.81 16.3 201.0
Methylene chloride 20.63 20 0 103 70 - 128 17.79 14.8 202.0
Naphthalene 21.54 20 3.823 88.6 70 - 130 19.21 11.4 201.0
o-Xylene 20.15 20 0 101 70 - 124 16.77 18.3 201.0
Tert-butyl alcohol 324.9 400 0 81.2 70 - 130 234.8 32.2 20 R10
Toluene 18.16 20 0 90.8 70 - 123 15.96 12.9 201.0
Xylenes, Total 58.5 60 0 97.5 70 - 130 49.96 15.7 203.0
44.31 50 0 88.6 70 - 126 46.11 4 201.0Surr: 1,2-Dichloroethane-d4
49.8 50 0 99.6 77 - 113 47.26 5.23 201.0Surr: 4-Bromofluorobenzene
48.4 50 0 96.8 77 - 123 48.94 1.12 201.0Surr: Dibromofluoromethane
50.45 50 0 101 82 - 127 48.78 3.37 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071014-01 HS23071014-02 HS23071014-03 HS23071014-04
HS23071014-05 HS23071014-06 HS23071014-07 HS23071014-08
ALS Houston, US Date: 01-Aug-23
Page 25 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 10:39
Run ID:VOA11_441923 SeqNo:7441986 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methyl tert-butyl ether U 1.0
48.67 50 0 97.3 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.77 50 0 91.5 77 - 1131.0Surr: 4-Bromofluorobenzene
52.19 50 0 104 73 - 1261.0Surr: Dibromofluoromethane
50.07 50 0 100 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 09:57
Run ID:VOA11_441923 SeqNo:7441985 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methyl tert-butyl ether 15.97 20 0 79.8 70 - 1301.0
45.12 50 0 90.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.21 50 0 94.4 77 - 1131.0Surr: 4-Bromofluorobenzene
50.13 50 0 100 73 - 1261.0Surr: Dibromofluoromethane
48.96 50 0 97.9 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23071018-01MS Units:ug/L Analysis Date:21-Jul-2023 11:21
Run ID:VOA11_441923 SeqNo:7441988 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Methyl tert-butyl ether 14.39 20 0 72.0 70 - 1301.0
46.03 50 0 92.1 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.95 50 0 95.9 77 - 1131.0Surr: 4-Bromofluorobenzene
48.45 50 0 96.9 77 - 1231.0Surr: Dibromofluoromethane
49.45 50 0 98.9 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 26 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071018-01MSD Units:ug/L Analysis Date:21-Jul-2023 11:42
Run ID:VOA11_441923 SeqNo:7441989 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Methyl tert-butyl ether 14.33 20 0 71.7 70 - 130 14.39 0.403 201.0
46.07 50 0 92.1 70 - 126 46.03 0.0777 201.0Surr: 1,2-Dichloroethane-d4
48.18 50 0 96.4 77 - 113 47.95 0.479 201.0Surr: 4-Bromofluorobenzene
48.66 50 0 97.3 77 - 123 48.45 0.431 201.0Surr: Dibromofluoromethane
49.15 50 0 98.3 82 - 127 49.45 0.619 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071014-06
ALS Houston, US Date: 01-Aug-23
Page 27 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R441813 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439509 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439508 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.241 0.25 0 96.4 80 - 1200.0500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439511 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-D-D
Ferrous Iron 0.241 0.25 0.008 93.2 75 - 1250.0500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439510 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:MW-D-D
Ferrous Iron 0.242 0.25 0.008 93.6 75 - 125 0.241 0.414 200.0500
The following samples were analyzed in this batch:HS23071014-06 HS23071014-07
ALS Houston, US Date: 01-Aug-23
Page 28 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R442705 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 00:04
Run ID:ICS-Integrion_442705 SeqNo:7460135 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 00:10
Run ID:ICS-Integrion_442705 SeqNo:7460136 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.068 8 0 101 90 - 1100.200
Sample ID:HS23071018-09MS Units:mg/L Analysis Date:29-Jul-2023 02:00
Run ID:ICS-Integrion_442705 SeqNo:7460167 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)39.02 40 0 97.6 80 - 1202.00
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:29-Jul-2023 00:22
Run ID:ICS-Integrion_442705 SeqNo:7460138 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-D-D
Nitrate/Nitrite (as N)38.78 40 0 97.0 80 - 1202.00
Sample ID:HS23071018-09MSD Units:mg/L Analysis Date:29-Jul-2023 02:06
Run ID:ICS-Integrion_442705 SeqNo:7460168 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)40.1 40 0 100 80 - 120 39.02 2.71 202.00
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:29-Jul-2023 00:27
Run ID:ICS-Integrion_442705 SeqNo:7460139 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:MW-D-D
Nitrate/Nitrite (as N)39.88 40 0 99.7 80 - 120 38.78 2.79 202.00
The following samples were analyzed in this batch:HS23071014-06 HS23071014-07
ALS Houston, US Date: 01-Aug-23
Page 29 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R442749 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:MBLK-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461284 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461283 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)991.4 1000 0 99.1 85 - 1155.00
Alkalinity, Total (As CaCO3)997.4 1000 0 99.7 85 - 1155.00
Sample ID:LCSD-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461282 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)997.2 1000 0 99.7 85 - 115 991.4 0.579 205.00
Alkalinity, Total (As CaCO3)1028 1000 0 103 85 - 115 997.4 3 205.00
Sample ID:HS23071235-03DUP Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461285 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)132.5 135.4 2.16 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)132.5 135.4 2.16 205.00
The following samples were analyzed in this batch:HS23071014-06 HS23071014-07
ALS Houston, US Date: 01-Aug-23
Page 30 of 36
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071014
QC BATCH REPORT
Batch ID:R442827 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:31-Jul-2023 21:16
Run ID:ICS-Integrion_442827 SeqNo:7463012 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:31-Jul-2023 21:27
Run ID:ICS-Integrion_442827 SeqNo:7463013 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.97 20 0 99.9 90 - 1100.500
Sample ID:HS23071023-05MS Units:mg/L Analysis Date:01-Aug-2023 00:27
Run ID:ICS-Integrion_442827 SeqNo:7463003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 38.1 10 31.05 70.5 80 - 120 S 0.500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:31-Jul-2023 21:39
Run ID:ICS-Integrion_442827 SeqNo:7463015 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-D-D
Sulfate 13.5 10 3.787 97.1 80 - 1200.500
Sample ID:HS23071023-05MSD Units:mg/L Analysis Date:01-Aug-2023 00:33
Run ID:ICS-Integrion_442827 SeqNo:7463004 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 38.67 10 31.05 76.2 80 - 120 38.1 1.47 20 S 0.500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:31-Jul-2023 21:45
Run ID:ICS-Integrion_442827 SeqNo:7463016 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:MW-D-D
Sulfate 13.36 10 3.787 95.8 80 - 120 13.5 1.02 200.500
The following samples were analyzed in this batch:HS23071014-06 HS23071014-07
ALS Houston, US Date: 01-Aug-23
Page 31 of 36
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071014
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 01-Aug-23
Page 32 of 36
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
01-Aug-23Date: ALS Houston, US
Page 33 of 36
Nelson D. Dusara
19-Jul-2023 13:35Date/Time Received:HS23071014
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.9C/3.8C UC/C IR 31
50651
07/19/2023 16:00
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Nilesh D. Ranchod
Date/TimeeSignatureDate/TimeeSignature
20-Jul-2023 08:0718-Jul-2023 12:54
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241094
ALS Houston, US 01-Aug-23Date:
Page 34 of 36
Page 35 of 36
Page 36 of 36
August 01, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 10 sample(s) on Jul 19, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071017
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 41
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071017
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071017-01 18-Jul-2023 09:10 19-Jul-2023 13:35PMW-N-D Groundwater
HS23071017-02 18-Jul-2023 09:40 19-Jul-2023 13:35PMW-N-I Groundwater
HS23071017-03 18-Jul-2023 10:30 19-Jul-2023 13:35PMW-N-B Groundwater
HS23071017-04 18-Jul-2023 11:15 19-Jul-2023 13:35AMW-14S Groundwater
HS23071017-05 18-Jul-2023 13:00 19-Jul-2023 13:35MW-F-I Groundwater
HS23071017-06 18-Jul-2023 13:30 19-Jul-2023 13:35MW-F-D Groundwater
HS23071017-07 18-Jul-2023 14:10 19-Jul-2023 13:35MW-F-B Groundwater
HS23071017-08 18-Jul-2023 14:50 19-Jul-2023 13:35Z4-X72 Groundwater
HS23071017-09 18-Jul-2023 15:50 19-Jul-2023 13:35Z3-X80 Groundwater
HS23071017-10 18-Jul-2023 00:00 19-Jul-2023 13:35Trip Blank Water
ALS Houston, US 01-Aug-23Date:
Page 2 of 41
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071017
ECD Organics by Method SW8011
Batch ID: 197843
Sample ID: MBLK-197843
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R441986
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R441822
Sample ID: HS23071014-01MS
MS/MSD was performed on an unrelated sample.•
Batch ID: R441888
Sample ID: MW-F-D (HS23071017-06MS)
The recovery of the Matrix Spike (MS) associated to this analyte was outside of the established control limits. However, the LCS was
within control limits. The recovery of the MS may be due to sample matrix interference. Tert-butyl alcohol
•
Sample ID: MW-F-D (HS23071017-06MSD)
The recovery of the Matrix Spike Duplicate (MSD) associated to this analyte was outside of the established control limits. However,
the LCS was within control limits. The failed recovery of the MSD may be due to sample matrix interference. Tert-butyl alcohol
•
Batch ID: R441939
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Metals by Method SW6020A
Batch ID: 198283
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R442749
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 01-Aug-23Date:
Page 3 of 41
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071017
WetChemistry by Method E300
Batch ID: R442705
Sample ID: MW-F-B (HS23071017-07)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-F-D (HS23071017-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Z3-X80 (HS23071017-09)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Z4-X72 (HS23071017-08)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Batch ID: R442827
Sample ID: HS23071023-05MS
MS and MSD are for an unrelated sample •
WetChemistry by Method SM3500FED
Batch ID: R441813
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 01-Aug-23Date:
Page 4 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-N-D
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-01
18-Jul-2023 09:10 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 16:460.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 16:460.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 16:460.201,2-Dichloroethane 1.04.0
1ug/L 20-Jul-2023 16:461.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 16:460.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 16:460.20Benzene 1.0U
1ug/L 20-Jul-2023 16:460.20Chloroform 1.0U
1ug/L 20-Jul-2023 16:460.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 16:460.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 16:460.20Methyl tert-butyl ether 1.099
1ug/L 20-Jul-2023 16:461.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 16:460.30Naphthalene 1.0U
1ug/L 20-Jul-2023 16:460.30o-Xylene 1.0U
1ug/L 20-Jul-2023 16:4610Tert-butyl alcohol 10280
1ug/L 20-Jul-2023 16:460.20Toluene 1.0U
1ug/L 20-Jul-2023 16:460.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 16:4694.7 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 16:4694.9 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 16:4699.1 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 16:4610382-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 12:520.00321,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-N-I
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-02
18-Jul-2023 09:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 17:070.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 17:070.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 17:070.201,2-Dichloroethane 1.022
1ug/L 20-Jul-2023 17:071.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 17:070.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 17:070.20Benzene 1.0U
1ug/L 20-Jul-2023 17:070.20Chloroform 1.0U
1ug/L 20-Jul-2023 17:070.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 17:070.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 17:070.20Methyl tert-butyl ether 1.034
1ug/L 20-Jul-2023 17:071.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 17:070.30Naphthalene 1.0U
1ug/L 20-Jul-2023 17:070.30o-Xylene 1.0U
1ug/L 20-Jul-2023 17:0710Tert-butyl alcohol 102,200
1ug/L 20-Jul-2023 17:070.20Toluene 1.0U
1ug/L 20-Jul-2023 17:070.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 17:0797.5 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 17:0789.4 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 17:0710177-123
Surr: Toluene-d8 1%REC 20-Jul-2023 17:0795.2 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 13:160.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-N-B
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-03
18-Jul-2023 10:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 17:280.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 17:280.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 17:280.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 17:281.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 17:280.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 17:280.20Benzene 1.0U
1ug/L 20-Jul-2023 17:280.20Chloroform 1.0U
1ug/L 20-Jul-2023 17:280.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 17:280.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 17:280.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 17:281.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 17:280.30Naphthalene 1.0U
1ug/L 20-Jul-2023 17:280.30o-Xylene 1.0U
1ug/L 20-Jul-2023 17:2810Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 17:280.20Toluene 1.0U
1ug/L 20-Jul-2023 17:280.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 17:2898.9 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 17:2892.0 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 17:2810377-123
Surr: Toluene-d8 1%REC 20-Jul-2023 17:2810482-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 13:390.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-14S
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-04
18-Jul-2023 11:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 17:490.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 17:490.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 17:490.201,2-Dichloroethane 1.07.4
1ug/L 20-Jul-2023 17:491.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 17:490.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 17:490.20Benzene 1.0U
1ug/L 20-Jul-2023 17:490.20Chloroform 1.0U
1ug/L 20-Jul-2023 17:490.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 17:490.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 17:490.20Methyl tert-butyl ether 1.03.9
1ug/L 20-Jul-2023 17:491.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 17:490.30Naphthalene 1.0U
1ug/L 20-Jul-2023 17:490.30o-Xylene 1.0U
1ug/L 20-Jul-2023 17:4910Tert-butyl alcohol 10110
1ug/L 20-Jul-2023 17:490.20Toluene 1.0U
1ug/L 20-Jul-2023 17:490.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 17:4910070-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 17:4993.1 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 17:4910377-123
Surr: Toluene-d8 1%REC 20-Jul-2023 17:4910382-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 14:030.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-F-I
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-05
18-Jul-2023 13:00 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 05:040.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 05:040.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 05:040.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 05:041.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 05:040.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 05:04J0.20Benzene 1.00.42
1ug/L 21-Jul-2023 05:040.20Chloroform 1.0U
1ug/L 21-Jul-2023 05:040.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 05:040.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 05:040.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 05:041.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 05:040.30Naphthalene 1.0U
1ug/L 21-Jul-2023 05:040.30o-Xylene 1.0U
1ug/L 21-Jul-2023 05:0410Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 05:040.20Toluene 1.0U
1ug/L 21-Jul-2023 05:040.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 05:0499.1 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 05:0493.3 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 05:0410377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 05:0410182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 14:270.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-F-D
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-06
18-Jul-2023 13:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 21:430.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 21:430.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 21:430.201,2-Dichloroethane 1.010
1ug/L 20-Jul-2023 21:431.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 21:430.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 21:430.20Benzene 1.0U
1ug/L 20-Jul-2023 21:430.20Chloroform 1.0U
1ug/L 20-Jul-2023 21:430.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 21:430.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 21:430.20Methyl tert-butyl ether 1.044
1ug/L 20-Jul-2023 21:431.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 21:430.30Naphthalene 1.0U
1ug/L 20-Jul-2023 21:430.30o-Xylene 1.0U
10ug/L 21-Jul-2023 13:24100Tert-butyl alcohol 1002,900
1ug/L 20-Jul-2023 21:430.20Toluene 1.0U
1ug/L 20-Jul-2023 21:430.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 21:4399.1 70-126
Surr: 1,2-Dichloroethane-d4 10%REC 21-Jul-2023 13:2496.5 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 21:4393.2 77-113
Surr: 4-Bromofluorobenzene 10%REC 21-Jul-2023 13:2496.5 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 21:4310577-123
Surr: Dibromofluoromethane 10%REC 21-Jul-2023 13:2498.0 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 21:4310282-127
Surr: Toluene-d8 10%REC 21-Jul-2023 13:2499.9 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 10:420.107Methane 0.50036.3
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 14:500.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 31-Jul-2023
1mg/L 31-Jul-2023 18:420.0120Iron 0.2000.212
20mg/L 01-Aug-2023 12:050.0140Manganese 0.1002.13
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 22:020.200Sulfate 0.5000.834
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 00:390.300Nitrate/Nitrite (as N)2.00U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-F-D
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-06
18-Jul-2023 13:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00287
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05000.262
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-F-B
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-07
18-Jul-2023 14:10 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 22:460.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 22:460.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 22:460.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 22:461.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 22:460.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 22:460.20Benzene 1.0U
1ug/L 20-Jul-2023 22:460.20Chloroform 1.0U
1ug/L 20-Jul-2023 22:460.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 22:460.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 22:460.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 22:461.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 22:460.30Naphthalene 1.0U
1ug/L 20-Jul-2023 22:460.30o-Xylene 1.0U
1ug/L 20-Jul-2023 22:4610Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 22:460.20Toluene 1.0U
1ug/L 20-Jul-2023 22:460.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 22:4695.8 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 22:4693.4 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 22:4610277-123
Surr: Toluene-d8 1%REC 20-Jul-2023 22:4610282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 10:590.107Methane 0.5000.514
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 15:140.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 31-Jul-2023
1mg/L 31-Jul-2023 19:14J0.0120Iron 0.2000.0196
1mg/L 31-Jul-2023 19:14J0.000700Manganese 0.005000.00221
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 22:080.200Sulfate 0.5001.38
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 00:450.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.0064.3
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.0064.3
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:02J0.0200Ferrous Iron 0.05000.0320
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-X72
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-08
18-Jul-2023 14:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 23:070.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 23:070.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 23:070.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 23:071.02-Methylnaphthalene 1.04.3
1ug/L 20-Jul-2023 23:070.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 23:070.20Benzene 1.0U
1ug/L 20-Jul-2023 23:070.20Chloroform 1.0U
1ug/L 20-Jul-2023 23:070.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 23:070.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 23:070.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 23:071.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 23:070.30Naphthalene 1.0U
1ug/L 20-Jul-2023 23:070.30o-Xylene 1.0U
1ug/L 20-Jul-2023 23:0710Tert-butyl alcohol 10140
1ug/L 20-Jul-2023 23:070.20Toluene 1.0U
1ug/L 20-Jul-2023 23:070.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 23:0798.6 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 23:0791.1 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 23:0710377-123
Surr: Toluene-d8 1%REC 20-Jul-2023 23:0710282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
100ug/L 21-Jul-2023 11:3510.7Methane 50.02,200
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 15:380.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 31-Jul-2023
1mg/L 31-Jul-2023 19:160.0120Iron 0.2008.75
100mg/L 01-Aug-2023 12:070.0700Manganese 0.5007.96
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 22:140.200Sulfate 0.5000.703
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 00:500.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00261
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00261
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
5mg/L 20-Jul-2023 10:020.100Ferrous Iron 0.2509.74
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z3-X80
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-09
18-Jul-2023 15:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 23:280.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 23:280.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 23:280.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 23:281.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 23:280.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 23:280.20Benzene 1.0U
1ug/L 20-Jul-2023 23:280.20Chloroform 1.0U
1ug/L 20-Jul-2023 23:280.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 23:280.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 23:280.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 23:281.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 23:280.30Naphthalene 1.0U
1ug/L 20-Jul-2023 23:280.30o-Xylene 1.0U
1ug/L 20-Jul-2023 23:2810Tert-butyl alcohol 1089
1ug/L 20-Jul-2023 23:280.20Toluene 1.0U
1ug/L 20-Jul-2023 23:280.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 23:2899.5 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 23:2894.9 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 23:2899.9 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 23:2899.9 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 11:240.107Methane 0.50012.2
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 17:130.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 31-Jul-2023
1mg/L 31-Jul-2023 19:180.0120Iron 0.2002.12
50mg/L 01-Aug-2023 12:090.0350Manganese 0.2504.12
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 22:490.200Sulfate 0.5001.21
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 00:560.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00204
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00204
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05001.84
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 41
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071017
HS23071017-10
18-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 13:580.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 13:580.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 13:580.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 13:581.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 13:580.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 13:580.20Benzene 1.0U
1ug/L 20-Jul-2023 13:580.20Chloroform 1.0U
1ug/L 20-Jul-2023 13:580.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 13:580.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 13:580.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 13:581.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 13:580.30Naphthalene 1.0U
1ug/L 20-Jul-2023 13:580.30o-Xylene 1.0U
1ug/L 20-Jul-2023 13:5810Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 13:580.20Toluene 1.0U
1ug/L 20-Jul-2023 13:580.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 13:5896.9 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 13:5895.0 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 13:5898.2 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 13:5810382-127
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of 41
Weight / Prep Log
HS23071017
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197843
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:45 End Date: 21 Jul 2023 09:45
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071017-01 35 (mL)40 mL VOA w/ HCL36.85 (mL)1.053
HS23071017-02 35 (mL)40 mL VOA w/ HCL36.38 (mL)1.039
HS23071017-03 35 (mL)40 mL VOA w/ HCL36.17 (mL)1.033
HS23071017-04 35 (mL)40 mL VOA w/ HCL36.49 (mL)1.043
HS23071017-05 35 (mL)40 mL VOA w/ HCL36.55 (mL)1.044
HS23071017-06 35 (mL)40 mL VOA w/ HCL36.61 (mL)1.046
HS23071017-07 35 (mL)40 mL VOA w/ HCL36.71 (mL)1.049
HS23071017-08 35 (mL)40 mL VOA w/ HCL36.35 (mL)1.039
HS23071017-09 35 (mL)40 mL VOA w/ HCL36.33 (mL)1.038
Batch ID:198283
Method:WATER - SW3010A 3010APrep Code:
Start Date: 31 Jul 2023 08:00 End Date: 31 Jul 2023 08:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071017-06 10 (mL)120 plastic HNO310 (mL)1
HS23071017-07 10 (mL)120 plastic HNO310 (mL)1
HS23071017-08 10 (mL)120 plastic HNO310 (mL)1
HS23071017-09 10 (mL)120 plastic HNO310 (mL)1
01-Aug-23Date: ALS Houston, US
Page 16 of 41
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071017
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197843 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:45 24 Jul 2023 12:52HS23071017-01 18 Jul 2023 09:10 1PMW-N-D
21 Jul 2023 09:45 24 Jul 2023 13:16HS23071017-02 18 Jul 2023 09:40 1PMW-N-I
21 Jul 2023 09:45 24 Jul 2023 13:39HS23071017-03 18 Jul 2023 10:30 1PMW-N-B
21 Jul 2023 09:45 24 Jul 2023 14:03HS23071017-04 18 Jul 2023 11:15 1AMW-14S
21 Jul 2023 09:45 24 Jul 2023 14:27HS23071017-05 18 Jul 2023 13:00 1MW-F-I
21 Jul 2023 09:45 24 Jul 2023 14:50HS23071017-06 18 Jul 2023 13:30 1MW-F-D
21 Jul 2023 09:45 24 Jul 2023 15:14HS23071017-07 18 Jul 2023 14:10 1MW-F-B
21 Jul 2023 09:45 24 Jul 2023 15:38HS23071017-08 18 Jul 2023 14:50 1Z4-X72
21 Jul 2023 09:45 24 Jul 2023 17:13HS23071017-09 18 Jul 2023 15:50 1Z3-X80
Batch ID:198283 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
31 Jul 2023 08:00 31 Jul 2023 18:42HS23071017-06 18 Jul 2023 13:30 1MW-F-D
31 Jul 2023 08:00 01 Aug 2023 12:05HS23071017-06 18 Jul 2023 13:30 20MW-F-D
31 Jul 2023 08:00 31 Jul 2023 19:14HS23071017-07 18 Jul 2023 14:10 1MW-F-B
31 Jul 2023 08:00 31 Jul 2023 19:16HS23071017-08 18 Jul 2023 14:50 1Z4-X72
31 Jul 2023 08:00 01 Aug 2023 12:07HS23071017-08 18 Jul 2023 14:50 100Z4-X72
31 Jul 2023 08:00 31 Jul 2023 19:18HS23071017-09 18 Jul 2023 15:50 1Z3-X80
31 Jul 2023 08:00 01 Aug 2023 12:09HS23071017-09 18 Jul 2023 15:50 50Z3-X80
Batch ID:R441813 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
20 Jul 2023 10:02HS23071017-06 18 Jul 2023 13:30 1MW-F-D
20 Jul 2023 10:02HS23071017-07 18 Jul 2023 14:10 1MW-F-B
20 Jul 2023 10:02HS23071017-08 18 Jul 2023 14:50 5Z4-X72
20 Jul 2023 10:02HS23071017-09 18 Jul 2023 15:50 1Z3-X80
Batch ID:R441822 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
20 Jul 2023 13:58HS23071017-10 18 Jul 2023 00:00 1Trip Blank
Batch ID:R441822 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
20 Jul 2023 16:46HS23071017-01 18 Jul 2023 09:10 1PMW-N-D
20 Jul 2023 17:07HS23071017-02 18 Jul 2023 09:40 1PMW-N-I
20 Jul 2023 17:28HS23071017-03 18 Jul 2023 10:30 1PMW-N-B
20 Jul 2023 17:49HS23071017-04 18 Jul 2023 11:15 1AMW-14S
Batch ID:R441888 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 05:04HS23071017-05 18 Jul 2023 13:00 1MW-F-I
20 Jul 2023 21:43HS23071017-06 18 Jul 2023 13:30 1MW-F-D
20 Jul 2023 22:46HS23071017-07 18 Jul 2023 14:10 1MW-F-B
20 Jul 2023 23:07HS23071017-08 18 Jul 2023 14:50 1Z4-X72
20 Jul 2023 23:28HS23071017-09 18 Jul 2023 15:50 1Z3-X80
Batch ID:R441939 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 13:24HS23071017-06 18 Jul 2023 13:30 10MW-F-D
01-Aug-23Date: ALS Houston, US
Page 17 of 41
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071017
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R441986 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
21 Jul 2023 10:42HS23071017-06 18 Jul 2023 13:30 1MW-F-D
21 Jul 2023 10:59HS23071017-07 18 Jul 2023 14:10 1MW-F-B
21 Jul 2023 11:35HS23071017-08 18 Jul 2023 14:50 100Z4-X72
21 Jul 2023 11:24HS23071017-09 18 Jul 2023 15:50 1Z3-X80
Batch ID:R442705 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
29 Jul 2023 00:39HS23071017-06 18 Jul 2023 13:30 10MW-F-D
29 Jul 2023 00:45HS23071017-07 18 Jul 2023 14:10 10MW-F-B
29 Jul 2023 00:50HS23071017-08 18 Jul 2023 14:50 10Z4-X72
29 Jul 2023 00:56HS23071017-09 18 Jul 2023 15:50 10Z3-X80
Batch ID:R442749 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
29 Jul 2023 12:25HS23071017-06 18 Jul 2023 13:30 1MW-F-D
29 Jul 2023 12:25HS23071017-07 18 Jul 2023 14:10 1MW-F-B
29 Jul 2023 12:25HS23071017-08 18 Jul 2023 14:50 1Z4-X72
29 Jul 2023 12:25HS23071017-09 18 Jul 2023 15:50 1Z3-X80
Batch ID:R442827 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
31 Jul 2023 22:02HS23071017-06 18 Jul 2023 13:30 1MW-F-D
31 Jul 2023 22:08HS23071017-07 18 Jul 2023 14:10 1MW-F-B
31 Jul 2023 22:14HS23071017-08 18 Jul 2023 14:50 1Z4-X72
31 Jul 2023 22:49HS23071017-09 18 Jul 2023 15:50 1Z3-X80
01-Aug-23Date: ALS Houston, US
Page 18 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:197843 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197843 Units:ug/L Analysis Date:24-Jul-2023 01:05
Run ID:ECD_13_442223 SeqNo:7448785 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197843 Units:ug/L Analysis Date:24-Jul-2023 01:28
Run ID:ECD_13_442223 SeqNo:7448786 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.2347 0.25 0 93.9 60 - 1400.020
Sample ID:LCSD-197843 Units:ug/L Analysis Date:24-Jul-2023 01:52
Run ID:ECD_13_442223 SeqNo:7448787 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.213 0.25 0 85.2 60 - 140 0.2347 9.7 200.020
The following samples were analyzed in this batch:HS23071017-01 HS23071017-02 HS23071017-03 HS23071017-04
HS23071017-05 HS23071017-06 HS23071017-07 HS23071017-08
HS23071017-09
ALS Houston, US Date: 01-Aug-23
Page 19 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441986 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230721 Units:ug/L Analysis Date:21-Jul-2023 07:07
Run ID:FID-4_441986 SeqNo:7443383 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230721 Units:ug/L Analysis Date:21-Jul-2023 07:40
Run ID:FID-4_441986 SeqNo:7443384 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.855 9.647 0 81.4 75 - 1250.500
Sample ID:LCSD-230721 Units:ug/L Analysis Date:21-Jul-2023 08:01
Run ID:FID-4_441986 SeqNo:7443385 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 7.797 9.647 0 80.8 75 - 125 7.855 0.747 300.500
Sample ID:HS23070935-02DUP Units:ug/L Analysis Date:21-Jul-2023 09:44
Run ID:FID-4_441986 SeqNo:7443391 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Methane 16.97 16.73 1.42 300.500
The following samples were analyzed in this batch:HS23071017-06 HS23071017-07 HS23071017-08 HS23071017-09
ALS Houston, US Date: 01-Aug-23
Page 20 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:198283 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198283 Units:mg/L Analysis Date:31-Jul-2023 18:02
Run ID:ICPMS05_442748 SeqNo:7462763 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese 0.001622 J 0.00500
Sample ID:MBLK-198283 Units:mg/L Analysis Date:01-Aug-2023 11:59
Run ID:ICPMS05_442868 SeqNo:7464141 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:LCS-198283 Units:mg/L Analysis Date:31-Jul-2023 18:04
Run ID:ICPMS05_442748 SeqNo:7462764 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 5.418 5 0 108 80 - 1200.200
Manganese 0.05078 0.05 0 102 80 - 1200.00500
Sample ID:HS23071368-01MS Units:mg/L Analysis Date:31-Jul-2023 18:54
Run ID:ICPMS05_442748 SeqNo:7463072 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.207 5 0.005617 104 80 - 1200.200
Manganese 0.04901 0.05 0.000804 96.4 80 - 1200.00500
Sample ID:HS23071368-01MSD Units:mg/L Analysis Date:01-Aug-2023 12:03
Run ID:ICPMS05_442868 SeqNo:7464143 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.311 5 0.005617 106 80 - 120 5.207 1.98 200.200
Manganese 0.05318 0.05 0.000804 105 80 - 120 0.04901 8.16 200.00500
ALS Houston, US Date: 01-Aug-23
Page 21 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:198283 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23071368-01PDS Units:mg/L Analysis Date:31-Jul-2023 18:58
Run ID:ICPMS05_442748 SeqNo:7463074 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 11.29 10 0.005617 113 75 - 1250.200
Manganese 0.1084 0.1 0.000804 108 75 - 1250.00500
Sample ID:HS23071368-01SD Units:mg/L Analysis Date:31-Jul-2023 18:52
Run ID:ICPMS05_442748 SeqNo:7463071 PrepDate:31-Jul-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron U 0.005617 0 101.00
Manganese U 0.000804 0 100.0250
The following samples were analyzed in this batch:HS23071017-06 HS23071017-07 HS23071017-08 HS23071017-09
ALS Houston, US Date: 01-Aug-23
Page 22 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230720 Units:ug/L Analysis Date:20-Jul-2023 10:28
Run ID:VOA11_441822 SeqNo:7439640 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
48.56 50 0 97.1 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.86 50 0 91.7 77 - 1131.0Surr: 4-Bromofluorobenzene
49.8 50 0 99.6 73 - 1261.0Surr: Dibromofluoromethane
51.28 50 0 103 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 23 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230720 Units:ug/L Analysis Date:20-Jul-2023 09:46
Run ID:VOA11_441822 SeqNo:7439639 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.89 20 0 94.5 73 - 1211.0
1,2-Dibromoethane 17.19 20 0 86.0 76 - 1231.0
1,2-Dichloroethane 16.7 20 0 83.5 70 - 1241.0
2-Methylnaphthalene 15.22 20 0 76.1 55 - 1401.0
4-Isopropyltoluene 18.8 20 0 94.0 74 - 1261.0
Benzene 18.3 20 0 91.5 74 - 1201.0
Chloroform 18.88 20 0 94.4 71 - 1211.0
Ethylbenzene 18.52 20 0 92.6 77 - 1171.0
m,p-Xylene 37.54 40 0 93.9 77 - 1222.0
Methyl tert-butyl ether 15.44 20 0 77.2 70 - 1301.0
Methylene chloride 21.16 20 0 106 70 - 1272.0
Naphthalene 16.52 20 0 82.6 70 - 1301.0
o-Xylene 19.2 20 0 96.0 75 - 1191.0
Tert-butyl alcohol 293.5 400 0 73.4 70 - 13010
Toluene 17.51 20 0 87.6 77 - 1181.0
Xylenes, Total 56.75 60 0 94.6 75 - 1223.0
44.62 50 0 89.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.02 50 0 96.0 77 - 1131.0Surr: 4-Bromofluorobenzene
49.25 50 0 98.5 73 - 1261.0Surr: Dibromofluoromethane
49.36 50 0 98.7 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 24 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071014-01MS Units:ug/L Analysis Date:20-Jul-2023 11:31
Run ID:VOA11_441822 SeqNo:7439643 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 17.04 20 0 85.2 70 - 1251.0
1,2-Dibromoethane 13.88 20 0 69.4 70 - 124 S1.0
1,2-Dichloroethane 21.28 20 7.19 70.5 70 - 1271.0
2-Methylnaphthalene 17.4 20 4.153 66.2 55 - 1401.0
4-Isopropyltoluene 17.45 20 0 87.3 70 - 1301.0
Benzene 19.04 20 2.396 83.2 70 - 1271.0
Chloroform 16.55 20 0 82.7 70 - 1251.0
Ethylbenzene 16.66 20 0 83.3 70 - 1241.0
m,p-Xylene 33.2 40 0 83.0 70 - 1302.0
Methyl tert-butyl ether 13.81 20 0 69.0 70 - 130 S1.0
Methylene chloride 17.79 20 0 89.0 70 - 1282.0
Naphthalene 19.21 20 3.823 76.9 70 - 1301.0
o-Xylene 16.77 20 0 83.8 70 - 1241.0
Tert-butyl alcohol 234.8 400 0 58.7 70 - 130 S10
Toluene 15.96 20 0 79.8 70 - 1231.0
Xylenes, Total 49.96 60 0 83.3 70 - 1303.0
46.11 50 0 92.2 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.26 50 0 94.5 77 - 1131.0Surr: 4-Bromofluorobenzene
48.94 50 0 97.9 77 - 1231.0Surr: Dibromofluoromethane
48.78 50 0 97.6 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 25 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071014-01MSD Units:ug/L Analysis Date:20-Jul-2023 11:52
Run ID:VOA11_441822 SeqNo:7439644 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 19.33 20 0 96.6 70 - 125 17.04 12.6 201.0
1,2-Dibromoethane 16.63 20 0 83.1 70 - 124 13.88 18 201.0
1,2-Dichloroethane 24.06 20 7.19 84.4 70 - 127 21.28 12.3 201.0
2-Methylnaphthalene 20.41 20 4.153 81.3 55 - 140 17.4 15.9 201.0
4-Isopropyltoluene 18.84 20 0 94.2 70 - 130 17.45 7.66 201.0
Benzene 20.72 20 2.396 91.6 70 - 127 19.04 8.43 201.0
Chloroform 19.37 20 0 96.9 70 - 125 16.55 15.7 201.0
Ethylbenzene 19.99 20 0 99.9 70 - 124 16.66 18.2 201.0
m,p-Xylene 38.35 40 0 95.9 70 - 130 33.2 14.4 202.0
Methyl tert-butyl ether 16.26 20 0 81.3 70 - 130 13.81 16.3 201.0
Methylene chloride 20.63 20 0 103 70 - 128 17.79 14.8 202.0
Naphthalene 21.54 20 3.823 88.6 70 - 130 19.21 11.4 201.0
o-Xylene 20.15 20 0 101 70 - 124 16.77 18.3 201.0
Tert-butyl alcohol 324.9 400 0 81.2 70 - 130 234.8 32.2 20 R10
Toluene 18.16 20 0 90.8 70 - 123 15.96 12.9 201.0
Xylenes, Total 58.5 60 0 97.5 70 - 130 49.96 15.7 203.0
44.31 50 0 88.6 70 - 126 46.11 4 201.0Surr: 1,2-Dichloroethane-d4
49.8 50 0 99.6 77 - 113 47.26 5.23 201.0Surr: 4-Bromofluorobenzene
48.4 50 0 96.8 77 - 123 48.94 1.12 201.0Surr: Dibromofluoromethane
50.45 50 0 101 82 - 127 48.78 3.37 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071017-01 HS23071017-02 HS23071017-03 HS23071017-04
HS23071017-10
ALS Houston, US Date: 01-Aug-23
Page 26 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230720 Units:ug/L Analysis Date:20-Jul-2023 21:22
Run ID:VOA11_441888 SeqNo:7441300 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
49.7 50 0 99.4 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.15 50 0 94.3 77 - 1131.0Surr: 4-Bromofluorobenzene
51.74 50 0 103 73 - 1261.0Surr: Dibromofluoromethane
51.05 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 27 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230720 Units:ug/L Analysis Date:20-Jul-2023 20:39
Run ID:VOA11_441888 SeqNo:7441299 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.85 20 0 94.3 73 - 1211.0
1,2-Dibromoethane 16.69 20 0 83.4 76 - 1231.0
1,2-Dichloroethane 18.37 20 0 91.9 70 - 1241.0
2-Methylnaphthalene 15.38 20 0 76.9 55 - 1401.0
4-Isopropyltoluene 19.21 20 0 96.0 74 - 1261.0
Benzene 19.67 20 0 98.4 74 - 1201.0
Chloroform 19.17 20 0 95.9 71 - 1211.0
Ethylbenzene 19.46 20 0 97.3 77 - 1171.0
m,p-Xylene 39.54 40 0 98.8 77 - 1222.0
Methyl tert-butyl ether 16.6 20 0 83.0 70 - 1301.0
Methylene chloride 19.17 20 0 95.9 70 - 1272.0
Naphthalene 17.44 20 0 87.2 70 - 1301.0
o-Xylene 20.86 20 0 104 75 - 1191.0
Tert-butyl alcohol 322.5 400 0 80.6 70 - 13010
Toluene 19.02 20 0 95.1 77 - 1181.0
Xylenes, Total 60.4 60 0 101 75 - 1223.0
45.02 50 0 90.0 70 - 1231.0Surr: 1,2-Dichloroethane-d4
49.81 50 0 99.6 77 - 1131.0Surr: 4-Bromofluorobenzene
47.91 50 0 95.8 73 - 1261.0Surr: Dibromofluoromethane
49.98 50 0 100.0 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 28 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071017-06MS Units:ug/L Analysis Date:20-Jul-2023 22:04
Run ID:VOA11_441888 SeqNo:7441302 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-F-D
1,2,4-Trimethylbenzene 21.59 20 0 108 70 - 1251.0
1,2-Dibromoethane 19.33 20 0 96.6 70 - 1241.0
1,2-Dichloroethane 28.75 20 10.27 92.4 70 - 1271.0
2-Methylnaphthalene 17.71 20 0 88.6 55 - 1401.0
4-Isopropyltoluene 21.08 20 0 105 70 - 1301.0
Benzene 20.81 20 0 104 70 - 1271.0
Chloroform 20.27 20 0 101 70 - 1251.0
Ethylbenzene 20.95 20 0 105 70 - 1241.0
m,p-Xylene 44 40 0 110 70 - 1302.0
Methyl tert-butyl ether 58.33 20 44.28 70.2 70 - 1301.0
Methylene chloride 22.86 20 0 114 70 - 1282.0
Naphthalene 19.39 20 0 97.0 70 - 1301.0
o-Xylene 22.02 20 0 110 70 - 1241.0
Tert-butyl alcohol 4274 400 4174 25.1 70 - 130 SEO10
Toluene 20.18 20 0 101 70 - 1231.0
Xylenes, Total 66.02 60 0 110 70 - 1303.0
45.12 50 0 90.2 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.49 50 0 95.0 77 - 1131.0Surr: 4-Bromofluorobenzene
48.78 50 0 97.6 77 - 1231.0Surr: Dibromofluoromethane
49.94 50 0 99.9 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 29 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071017-06MSD Units:ug/L Analysis Date:20-Jul-2023 22:25
Run ID:VOA11_441888 SeqNo:7441303 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:MW-F-D
1,2,4-Trimethylbenzene 20.18 20 0 101 70 - 125 21.59 6.72 201.0
1,2-Dibromoethane 18.57 20 0 92.8 70 - 124 19.33 4.01 201.0
1,2-Dichloroethane 29.6 20 10.27 96.7 70 - 127 28.75 2.92 201.0
2-Methylnaphthalene 18.29 20 0 91.4 55 - 140 17.71 3.2 201.0
4-Isopropyltoluene 20.24 20 0 101 70 - 130 21.08 4.04 201.0
Benzene 20.73 20 0 104 70 - 127 20.81 0.383 201.0
Chloroform 21.16 20 0 106 70 - 125 20.27 4.32 201.0
Ethylbenzene 19.76 20 0 98.8 70 - 124 20.95 5.83 201.0
m,p-Xylene 41.81 40 0 105 70 - 130 44 5.09 202.0
Methyl tert-butyl ether 60.84 20 44.28 82.8 70 - 130 58.33 4.22 201.0
Methylene chloride 21.69 20 0 108 70 - 128 22.86 5.22 202.0
Naphthalene 19.51 20 0 97.6 70 - 130 19.39 0.62 201.0
o-Xylene 21.6 20 0 108 70 - 124 22.02 1.96 201.0
Tert-butyl alcohol 4774 400 4174 150 70 - 130 4274 11 20 SEO10
Toluene 19.38 20 0 96.9 70 - 123 20.18 4.06 201.0
Xylenes, Total 63.41 60 0 106 70 - 130 66.02 4.04 203.0
46.43 50 0 92.9 70 - 126 45.12 2.86 201.0Surr: 1,2-Dichloroethane-d4
49.16 50 0 98.3 77 - 113 47.49 3.46 201.0Surr: 4-Bromofluorobenzene
49.36 50 0 98.7 77 - 123 48.78 1.17 201.0Surr: Dibromofluoromethane
48.82 50 0 97.6 82 - 127 49.94 2.26 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071017-05 HS23071017-06 HS23071017-07 HS23071017-08
HS23071017-09
ALS Houston, US Date: 01-Aug-23
Page 30 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441939 ( 0 )Instrument:VOA7 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 10:27
Run ID:VOA7_441939 SeqNo:7442286 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Tert-butyl alcohol U 10
47.73 50 0 95.5 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.75 50 0 95.5 77 - 1131.0Surr: 4-Bromofluorobenzene
49.39 50 0 98.8 73 - 1261.0Surr: Dibromofluoromethane
50.17 50 0 100 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 09:44
Run ID:VOA7_441939 SeqNo:7442285 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Tert-butyl alcohol 286.6 400 0 71.6 70 - 13010
47.9 50 0 95.8 70 - 1231.0Surr: 1,2-Dichloroethane-d4
49.4 50 0 98.8 77 - 1131.0Surr: 4-Bromofluorobenzene
49.23 50 0 98.5 73 - 1261.0Surr: Dibromofluoromethane
50.12 50 0 100 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23071095-02MS Units:ug/L Analysis Date:21-Jul-2023 11:59
Run ID:VOA7_441939 SeqNo:7442290 PrepDate:DF:100
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Tert-butyl alcohol 33100 40000 0 82.8 70 - 1301000
4937 5000 0 98.7 70 - 126100Surr: 1,2-Dichloroethane-d4
4915 5000 0 98.3 77 - 113100Surr: 4-Bromofluorobenzene
4937 5000 0 98.7 77 - 123100Surr: Dibromofluoromethane
5030 5000 0 101 82 - 127100Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 31 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441939 ( 0 )Instrument:VOA7 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071095-02MSD Units:ug/L Analysis Date:21-Jul-2023 12:20
Run ID:VOA7_441939 SeqNo:7442291 PrepDate:DF:100
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Tert-butyl alcohol 31000 40000 0 77.5 70 - 130 33100 6.57 201000
4838 5000 0 96.8 70 - 126 4937 2.02 20100Surr: 1,2-Dichloroethane-d4
4902 5000 0 98.0 77 - 113 4915 0.266 20100Surr: 4-Bromofluorobenzene
4919 5000 0 98.4 77 - 123 4937 0.367 20100Surr: Dibromofluoromethane
4971 5000 0 99.4 82 - 127 5030 1.18 20100Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071017-06
ALS Houston, US Date: 01-Aug-23
Page 32 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R441813 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439509 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439508 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.241 0.25 0 96.4 80 - 1200.0500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439511 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.241 0.25 0.008 93.2 75 - 1250.0500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439510 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.242 0.25 0.008 93.6 75 - 125 0.241 0.414 200.0500
The following samples were analyzed in this batch:HS23071017-06 HS23071017-07 HS23071017-08 HS23071017-09
ALS Houston, US Date: 01-Aug-23
Page 33 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R442705 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 00:04
Run ID:ICS-Integrion_442705 SeqNo:7460135 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 00:10
Run ID:ICS-Integrion_442705 SeqNo:7460136 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.068 8 0 101 90 - 1100.200
Sample ID:HS23071018-09MS Units:mg/L Analysis Date:29-Jul-2023 02:00
Run ID:ICS-Integrion_442705 SeqNo:7460167 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)39.02 40 0 97.6 80 - 1202.00
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:29-Jul-2023 00:22
Run ID:ICS-Integrion_442705 SeqNo:7460138 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)38.78 40 0 97.0 80 - 1202.00
Sample ID:HS23071018-09MSD Units:mg/L Analysis Date:29-Jul-2023 02:06
Run ID:ICS-Integrion_442705 SeqNo:7460168 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)40.1 40 0 100 80 - 120 39.02 2.71 202.00
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:29-Jul-2023 00:27
Run ID:ICS-Integrion_442705 SeqNo:7460139 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)39.88 40 0 99.7 80 - 120 38.78 2.79 202.00
The following samples were analyzed in this batch:HS23071017-06 HS23071017-07 HS23071017-08 HS23071017-09
ALS Houston, US Date: 01-Aug-23
Page 34 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R442749 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:MBLK-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461284 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461283 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)991.4 1000 0 99.1 85 - 1155.00
Alkalinity, Total (As CaCO3)997.4 1000 0 99.7 85 - 1155.00
Sample ID:LCSD-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461282 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)997.2 1000 0 99.7 85 - 115 991.4 0.579 205.00
Alkalinity, Total (As CaCO3)1028 1000 0 103 85 - 115 997.4 3 205.00
Sample ID:HS23071235-03DUP Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461285 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)132.5 135.4 2.16 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)132.5 135.4 2.16 205.00
The following samples were analyzed in this batch:HS23071017-06 HS23071017-07 HS23071017-08 HS23071017-09
ALS Houston, US Date: 01-Aug-23
Page 35 of 41
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071017
QC BATCH REPORT
Batch ID:R442827 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:31-Jul-2023 21:16
Run ID:ICS-Integrion_442827 SeqNo:7463012 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:31-Jul-2023 21:27
Run ID:ICS-Integrion_442827 SeqNo:7463013 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.97 20 0 99.9 90 - 1100.500
Sample ID:HS23071023-05MS Units:mg/L Analysis Date:01-Aug-2023 00:27
Run ID:ICS-Integrion_442827 SeqNo:7463003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 38.1 10 31.05 70.5 80 - 120 S 0.500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:31-Jul-2023 21:39
Run ID:ICS-Integrion_442827 SeqNo:7463015 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 13.5 10 3.787 97.1 80 - 1200.500
Sample ID:HS23071023-05MSD Units:mg/L Analysis Date:01-Aug-2023 00:33
Run ID:ICS-Integrion_442827 SeqNo:7463004 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 38.67 10 31.05 76.2 80 - 120 38.1 1.47 20 S 0.500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:31-Jul-2023 21:45
Run ID:ICS-Integrion_442827 SeqNo:7463016 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 13.36 10 3.787 95.8 80 - 120 13.5 1.02 200.500
The following samples were analyzed in this batch:HS23071017-06 HS23071017-07 HS23071017-08 HS23071017-09
ALS Houston, US Date: 01-Aug-23
Page 36 of 41
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071017
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 01-Aug-23
Page 37 of 41
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
01-Aug-23Date: ALS Houston, US
Page 38 of 41
Nelson D. Dusara
19-Jul-2023 13:35Date/Time Received:HS23071017
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.4C/3.3C UC/C IR 31
50966
07/19/2023 16:00
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Nilesh D. Ranchod
Date/TimeeSignatureDate/TimeeSignature
20-Jul-2023 07:5618-Jul-2023 12:54
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241112
ALS Houston, US 01-Aug-23Date:
Page 39 of 41
Page 40 of 41
Page 41 of 41
August 01, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 10 sample(s) on Jul 19, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071018
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 35
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071018
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071018-01 18-Jul-2023 09:05 19-Jul-2023 13:35Z1-X1 Groundwater
HS23071018-02 18-Jul-2023 09:35 19-Jul-2023 13:35Z2-X16 Groundwater
HS23071018-03 18-Jul-2023 10:10 19-Jul-2023 13:35Z4-X21 Groundwater
HS23071018-04 18-Jul-2023 10:50 19-Jul-2023 13:35Z4-X35 Groundwater
HS23071018-05 18-Jul-2023 11:30 19-Jul-2023 13:35Z3-X82 Groundwater
HS23071018-06 18-Jul-2023 12:05 19-Jul-2023 13:35Z1-X28 Groundwater
HS23071018-07 18-Jul-2023 12:45 19-Jul-2023 13:35MW-A-I Groundwater
HS23071018-08 18-Jul-2023 13:20 19-Jul-2023 13:35MW-A-D Groundwater
HS23071018-09 18-Jul-2023 13:50 19-Jul-2023 13:35MW-A-B Groundwater
HS23071018-10 18-Jul-2023 00:00 19-Jul-2023 13:35Trip Blank Water
ALS Houston, US 01-Aug-23Date:
Page 2 of 35
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071018
ECD Organics by Method SW8011
Batch ID: 197843
Sample ID: MBLK-197843
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
Batch ID: 197845
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GC Semivolatiles by Method RSK-175
Batch ID: R442316
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R441923
Sample ID: Z1-X1(HS23071018-01MS)
The recovery of the Matrix Spike (MS) associated to this analyte was outside of the established control limits. However, the LCS was
within control limits. The recovery of the MS may be due to sample matrix interference. Tert-butyl alcohol.
•
Sample ID: Z1-X1 (HS23071018-01MSD)
The recovery of the Matrix Spike Duplicate (MSD) associated to this analyte was outside of the established control limits. However,
the LCS was within control limits. The failed recovery of the MSD may be due to sample matrix interference. Tert-butyl alcohol
•
Metals by Method SW6020A
Batch ID: 198283
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R442749
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442827
Sample ID: HS23071023-05MS
MS and MSD are for an unrelated sample •
ALS Houston, US 01-Aug-23Date:
Page 3 of 35
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071018
WetChemistry by Method E300
Batch ID: R442705
Sample ID: MW-A-B (HS23071018-09)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-A-D (HS23071018-08)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-A-I (HS23071018-07)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Z1-X28 (HS23071018-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441813
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 01-Aug-23Date:
Page 4 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z1-X1
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-01
18-Jul-2023 09:05 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 11:000.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 11:000.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 11:000.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 11:001.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 11:000.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 11:000.20Benzene 1.0U
1ug/L 21-Jul-2023 11:000.20Chloroform 1.0U
1ug/L 21-Jul-2023 11:000.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 11:000.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 11:000.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 11:001.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 11:000.30Naphthalene 1.0U
1ug/L 21-Jul-2023 11:000.30o-Xylene 1.0U
1ug/L 21-Jul-2023 11:0010Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 11:000.20Toluene 1.0U
1ug/L 21-Jul-2023 11:000.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 11:0097.8 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 11:0091.8 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 11:0010277-123
Surr: Toluene-d8 1%REC 21-Jul-2023 11:0010182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 17:360.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-X16
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-02
18-Jul-2023 09:35 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 14:300.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 14:300.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 14:300.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 14:301.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 14:300.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 14:300.20Benzene 1.0U
1ug/L 21-Jul-2023 14:300.20Chloroform 1.0U
1ug/L 21-Jul-2023 14:300.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 14:300.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 14:300.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 14:301.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 14:300.30Naphthalene 1.0U
1ug/L 21-Jul-2023 14:300.30o-Xylene 1.0U
1ug/L 21-Jul-2023 14:3010Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 14:300.20Toluene 1.0U
1ug/L 21-Jul-2023 14:300.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 14:3098.3 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 14:3091.1 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 14:3010377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 14:3098.9 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 18:000.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-X21
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-03
18-Jul-2023 10:10 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 14:510.301,2,4-Trimethylbenzene 1.05.9
1ug/L 21-Jul-2023 14:510.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 14:510.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 14:511.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 14:510.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 14:510.20Benzene 1.0U
1ug/L 21-Jul-2023 14:510.20Chloroform 1.0U
1ug/L 21-Jul-2023 14:510.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 14:510.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 14:510.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 14:511.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 14:510.30Naphthalene 1.0U
1ug/L 21-Jul-2023 14:510.30o-Xylene 1.0U
1ug/L 21-Jul-2023 14:5110Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 14:510.20Toluene 1.0U
1ug/L 21-Jul-2023 14:510.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 14:5196.2 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 14:5191.1 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 14:5110377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 14:5110182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 18:240.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-X35
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-04
18-Jul-2023 10:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 15:120.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 15:120.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 15:120.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 15:121.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 15:120.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 15:120.20Benzene 1.0U
1ug/L 21-Jul-2023 15:120.20Chloroform 1.0U
1ug/L 21-Jul-2023 15:120.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 15:120.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 15:120.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 15:121.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 15:120.30Naphthalene 1.0U
1ug/L 21-Jul-2023 15:120.30o-Xylene 1.0U
1ug/L 21-Jul-2023 15:1210Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 15:12J0.20Toluene 1.00.95
1ug/L 21-Jul-2023 15:120.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 15:1297.2 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 15:1297.0 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 15:1210477-123
Surr: Toluene-d8 1%REC 21-Jul-2023 15:1210382-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 18:470.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z3-X82
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-05
18-Jul-2023 11:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 15:330.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 15:330.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 15:330.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 15:331.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 15:330.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 15:33J0.20Benzene 1.00.61
1ug/L 21-Jul-2023 15:330.20Chloroform 1.0U
1ug/L 21-Jul-2023 15:330.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 15:330.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 15:330.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 15:331.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 15:330.30Naphthalene 1.0U
1ug/L 21-Jul-2023 15:330.30o-Xylene 1.0U
1ug/L 21-Jul-2023 15:3310Tert-butyl alcohol 1074
1ug/L 21-Jul-2023 15:330.20Toluene 1.0U
1ug/L 21-Jul-2023 15:330.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 15:3397.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 15:3398.5 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 15:3398.2 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 15:3310282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 19:110.00311,2-Dibromoethane 0.021U
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z1-X28
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-06
18-Jul-2023 12:05 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 15:540.301,2,4-Trimethylbenzene 1.06.3
1ug/L 21-Jul-2023 15:540.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 15:540.201,2-Dichloroethane 1.01.9
1ug/L 21-Jul-2023 15:541.02-Methylnaphthalene 1.06.6
1ug/L 21-Jul-2023 15:540.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 15:540.20Benzene 1.0U
1ug/L 21-Jul-2023 15:540.20Chloroform 1.0U
1ug/L 21-Jul-2023 15:540.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 15:540.50m,p-Xylene 2.02.8
1ug/L 21-Jul-2023 15:540.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 15:541.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 15:540.30Naphthalene 1.05.5
1ug/L 21-Jul-2023 15:540.30o-Xylene 1.01.1
1ug/L 21-Jul-2023 15:5410Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 15:540.20Toluene 1.0U
1ug/L 21-Jul-2023 15:540.30Xylenes, Total 3.03.9
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 15:5493.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 15:5495.6 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 15:5499.0 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 15:5410182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
50ug/L 22-Jul-2023 11:355.35Methane 25.01,270
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 19:350.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 31-Jul-2023
1mg/L 31-Jul-2023 19:200.0120Iron 0.20029.0
100mg/L 01-Aug-2023 12:110.0700Manganese 0.50013.2
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 22:540.200Sulfate 0.5007.45
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 01:310.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00247
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00247
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
250mg/L 20-Jul-2023 10:025.00Ferrous Iron 12.5216
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-A-I
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-07
18-Jul-2023 12:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 16:150.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 16:150.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 16:150.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 16:151.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 16:150.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 16:150.20Benzene 1.0U
1ug/L 21-Jul-2023 16:150.20Chloroform 1.0U
1ug/L 21-Jul-2023 16:150.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 16:150.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 16:150.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 16:151.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 16:150.30Naphthalene 1.0U
1ug/L 21-Jul-2023 16:150.30o-Xylene 1.0U
1ug/L 21-Jul-2023 16:1510Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 16:150.20Toluene 1.0U
1ug/L 21-Jul-2023 16:150.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 16:1592.2 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 16:1593.4 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 16:1510177-123
Surr: Toluene-d8 1%REC 21-Jul-2023 16:1599.7 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 10:560.107Methane 0.5004.02
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 19:59J0.00321,2-Dibromoethane 0.0210.020
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 31-Jul-2023
1mg/L 31-Jul-2023 19:220.0120Iron 0.20013.1
1mg/L 31-Jul-2023 19:220.000700Manganese 0.005000.496
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 23:000.200Sulfate 0.5000.919
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 01:370.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00116
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00116
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05001.74
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-A-D
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-08
18-Jul-2023 13:20 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 16:360.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 16:360.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 16:360.201,2-Dichloroethane 1.04.0
1ug/L 21-Jul-2023 16:361.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 16:360.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 16:360.20Benzene 1.0U
1ug/L 21-Jul-2023 16:360.20Chloroform 1.0U
1ug/L 21-Jul-2023 16:360.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 16:360.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 16:360.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 16:361.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 16:360.30Naphthalene 1.0U
1ug/L 21-Jul-2023 16:360.30o-Xylene 1.0U
1ug/L 21-Jul-2023 16:3610Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 16:360.20Toluene 1.0U
1ug/L 21-Jul-2023 16:360.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 16:3695.9 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 16:3695.1 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 16:3610077-123
Surr: Toluene-d8 1%REC 21-Jul-2023 16:3610282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 11:050.107Methane 0.50014.3
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 20:220.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 31-Jul-2023
1mg/L 31-Jul-2023 19:240.0120Iron 0.2006.10
20mg/L 01-Aug-2023 12:130.0140Manganese 0.1002.96
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 23:060.200Sulfate 0.5000.746
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 01:420.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00149
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00149
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05001.22
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-A-B
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-09
18-Jul-2023 13:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 16:570.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 16:570.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 16:570.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 16:571.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 16:570.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 16:570.20Benzene 1.0U
1ug/L 21-Jul-2023 16:570.20Chloroform 1.0U
1ug/L 21-Jul-2023 16:570.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 16:570.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 16:570.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 16:571.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 16:570.30Naphthalene 1.0U
1ug/L 21-Jul-2023 16:570.30o-Xylene 1.0U
1ug/L 21-Jul-2023 16:5710Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 16:570.20Toluene 1.0U
1ug/L 21-Jul-2023 16:570.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 16:5797.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 16:5792.5 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 16:5710177-123
Surr: Toluene-d8 1%REC 21-Jul-2023 16:5710182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 11:230.107Methane 0.5001.07
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 23:080.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 31-Jul-2023
1mg/L 31-Jul-2023 19:260.0120Iron 0.2002.49
1mg/L 31-Jul-2023 19:260.000700Manganese 0.005000.0238
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 23:120.200Sulfate 0.5001.70
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 01:480.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.0058.4
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.0058.4
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05001.64
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071018
HS23071018-10
18-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 12:240.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 12:240.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 12:240.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 12:241.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 12:240.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 12:240.20Benzene 1.0U
1ug/L 21-Jul-2023 12:240.20Chloroform 1.0U
1ug/L 21-Jul-2023 12:240.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 12:240.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 12:240.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 12:241.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 12:240.30Naphthalene 1.0U
1ug/L 21-Jul-2023 12:240.30o-Xylene 1.0U
1ug/L 21-Jul-2023 12:2410Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 12:240.20Toluene 1.0U
1ug/L 21-Jul-2023 12:240.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 12:2496.7 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 12:2491.5 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 12:2410377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 12:2410182-127
01-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 35
Weight / Prep Log
HS23071018
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197843
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:45 End Date: 21 Jul 2023 09:45
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071018-01 35 (mL)40 mL VOA w/ HCL36.26 (mL)1.036
HS23071018-02 35 (mL)40 mL VOA w/ HCL36.11 (mL)1.032
HS23071018-03 35 (mL)40 mL VOA w/ HCL36.2 (mL)1.034
HS23071018-04 35 (mL)40 mL VOA w/ HCL36.28 (mL)1.037
HS23071018-05 35 (mL)40 mL VOA w/ HCL36.31 (mL)1.037
HS23071018-06 35 (mL)40 mL VOA w/ HCL36.69 (mL)1.048
HS23071018-07 35 (mL)40 mL VOA w/ HCL37.16 (mL)1.062
HS23071018-08 35 (mL)40 mL VOA w/ HCL37.4 (mL)1.069
Batch ID:197845
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:48 End Date: 21 Jul 2023 09:48
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071018-09 35 (mL)40 mL VOA w/ HCL36.33 (mL)1.038
Batch ID:198283
Method:WATER - SW3010A 3010APrep Code:
Start Date: 31 Jul 2023 08:00 End Date: 31 Jul 2023 08:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071018-06 10 (mL)120 plastic HNO310 (mL)1
HS23071018-07 10 (mL)120 plastic HNO310 (mL)1
HS23071018-08 10 (mL)120 plastic HNO310 (mL)1
HS23071018-09 10 (mL)120 plastic HNO310 (mL)1
01-Aug-23Date: ALS Houston, US
Page 15 of 35
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071018
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197843 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:45 24 Jul 2023 17:36HS23071018-01 18 Jul 2023 09:05 1Z1-X1
21 Jul 2023 09:45 24 Jul 2023 18:00HS23071018-02 18 Jul 2023 09:35 1Z2-X16
21 Jul 2023 09:45 24 Jul 2023 18:24HS23071018-03 18 Jul 2023 10:10 1Z4-X21
21 Jul 2023 09:45 24 Jul 2023 18:47HS23071018-04 18 Jul 2023 10:50 1Z4-X35
21 Jul 2023 09:45 24 Jul 2023 19:11HS23071018-05 18 Jul 2023 11:30 1Z3-X82
21 Jul 2023 09:45 24 Jul 2023 19:35HS23071018-06 18 Jul 2023 12:05 1Z1-X28
21 Jul 2023 09:45 24 Jul 2023 19:59HS23071018-07 18 Jul 2023 12:45 1MW-A-I
21 Jul 2023 09:45 24 Jul 2023 20:22HS23071018-08 18 Jul 2023 13:20 1MW-A-D
Batch ID:197845 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:48 24 Jul 2023 23:08HS23071018-09 18 Jul 2023 13:50 1MW-A-B
Batch ID:198283 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
31 Jul 2023 08:00 31 Jul 2023 19:20HS23071018-06 18 Jul 2023 12:05 1Z1-X28
31 Jul 2023 08:00 01 Aug 2023 12:11HS23071018-06 18 Jul 2023 12:05 100Z1-X28
31 Jul 2023 08:00 31 Jul 2023 19:22HS23071018-07 18 Jul 2023 12:45 1MW-A-I
31 Jul 2023 08:00 31 Jul 2023 19:24HS23071018-08 18 Jul 2023 13:20 1MW-A-D
31 Jul 2023 08:00 01 Aug 2023 12:13HS23071018-08 18 Jul 2023 13:20 20MW-A-D
31 Jul 2023 08:00 31 Jul 2023 19:26HS23071018-09 18 Jul 2023 13:50 1MW-A-B
Batch ID:R441813 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
20 Jul 2023 10:02HS23071018-06 18 Jul 2023 12:05 250Z1-X28
20 Jul 2023 10:02HS23071018-07 18 Jul 2023 12:45 1MW-A-I
20 Jul 2023 10:02HS23071018-08 18 Jul 2023 13:20 1MW-A-D
20 Jul 2023 10:02HS23071018-09 18 Jul 2023 13:50 1MW-A-B
Batch ID:R441923 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
21 Jul 2023 12:24HS23071018-10 18 Jul 2023 00:00 1Trip Blank
Batch ID:R441923 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 11:00HS23071018-01 18 Jul 2023 09:05 1Z1-X1
21 Jul 2023 14:30HS23071018-02 18 Jul 2023 09:35 1Z2-X16
21 Jul 2023 14:51HS23071018-03 18 Jul 2023 10:10 1Z4-X21
21 Jul 2023 15:12HS23071018-04 18 Jul 2023 10:50 1Z4-X35
21 Jul 2023 15:33HS23071018-05 18 Jul 2023 11:30 1Z3-X82
21 Jul 2023 15:54HS23071018-06 18 Jul 2023 12:05 1Z1-X28
21 Jul 2023 16:15HS23071018-07 18 Jul 2023 12:45 1MW-A-I
21 Jul 2023 16:36HS23071018-08 18 Jul 2023 13:20 1MW-A-D
21 Jul 2023 16:57HS23071018-09 18 Jul 2023 13:50 1MW-A-B
01-Aug-23Date: ALS Houston, US
Page 16 of 35
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071018
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442316 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
22 Jul 2023 11:35HS23071018-06 18 Jul 2023 12:05 50Z1-X28
22 Jul 2023 10:56HS23071018-07 18 Jul 2023 12:45 1MW-A-I
22 Jul 2023 11:05HS23071018-08 18 Jul 2023 13:20 1MW-A-D
22 Jul 2023 11:23HS23071018-09 18 Jul 2023 13:50 1MW-A-B
Batch ID:R442705 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
29 Jul 2023 01:31HS23071018-06 18 Jul 2023 12:05 10Z1-X28
29 Jul 2023 01:37HS23071018-07 18 Jul 2023 12:45 10MW-A-I
29 Jul 2023 01:42HS23071018-08 18 Jul 2023 13:20 10MW-A-D
29 Jul 2023 01:48HS23071018-09 18 Jul 2023 13:50 10MW-A-B
Batch ID:R442749 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
29 Jul 2023 12:25HS23071018-06 18 Jul 2023 12:05 1Z1-X28
29 Jul 2023 12:25HS23071018-07 18 Jul 2023 12:45 1MW-A-I
29 Jul 2023 12:25HS23071018-08 18 Jul 2023 13:20 1MW-A-D
29 Jul 2023 12:25HS23071018-09 18 Jul 2023 13:50 1MW-A-B
Batch ID:R442827 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
31 Jul 2023 22:54HS23071018-06 18 Jul 2023 12:05 1Z1-X28
31 Jul 2023 23:00HS23071018-07 18 Jul 2023 12:45 1MW-A-I
31 Jul 2023 23:06HS23071018-08 18 Jul 2023 13:20 1MW-A-D
31 Jul 2023 23:12HS23071018-09 18 Jul 2023 13:50 1MW-A-B
01-Aug-23Date: ALS Houston, US
Page 17 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:197843 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197843 Units:ug/L Analysis Date:24-Jul-2023 01:05
Run ID:ECD_13_442223 SeqNo:7448785 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197843 Units:ug/L Analysis Date:24-Jul-2023 01:28
Run ID:ECD_13_442223 SeqNo:7448786 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.2347 0.25 0 93.9 60 - 1400.020
Sample ID:LCSD-197843 Units:ug/L Analysis Date:24-Jul-2023 01:52
Run ID:ECD_13_442223 SeqNo:7448787 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.213 0.25 0 85.2 60 - 140 0.2347 9.7 200.020
The following samples were analyzed in this batch:HS23071018-01 HS23071018-02 HS23071018-03 HS23071018-04
HS23071018-05 HS23071018-06 HS23071018-07 HS23071018-08
ALS Houston, US Date: 01-Aug-23
Page 18 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:197845 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197845 Units:ug/L Analysis Date:24-Jul-2023 21:57
Run ID:ECD_13_442224 SeqNo:7448808 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197845 Units:ug/L Analysis Date:24-Jul-2023 22:21
Run ID:ECD_13_442224 SeqNo:7448809 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1917 0.25 0 76.7 60 - 1400.020
Sample ID:LCSD-197845 Units:ug/L Analysis Date:25-Jul-2023 01:29
Run ID:ECD_13_442418 SeqNo:7453268 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1962 0.25 0 78.5 60 - 140 0.1917 2.33 200.020
Sample ID:LCSD-197845 Units:ug/L Analysis Date:24-Jul-2023 22:44
Run ID:ECD_13_442224 SeqNo:7448810 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1835 0.25 0 73.4 60 - 140 0.1917 4.39 200.020
The following samples were analyzed in this batch:HS23071018-09
ALS Houston, US Date: 01-Aug-23
Page 19 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:R442316 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230722 Units:ug/L Analysis Date:22-Jul-2023 08:11
Run ID:FID-4_442316 SeqNo:7450987 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230722 Units:ug/L Analysis Date:22-Jul-2023 08:21
Run ID:FID-4_442316 SeqNo:7450988 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 8.179 9.647 0 84.8 75 - 1250.500
Sample ID:LCSD-230722 Units:ug/L Analysis Date:22-Jul-2023 08:33
Run ID:FID-4_442316 SeqNo:7450989 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 7.869 9.647 0 81.6 75 - 125 8.179 3.86 300.500
Sample ID:HS23070922-11DUP Units:ug/L Analysis Date:22-Jul-2023 10:23
Run ID:FID-4_442316 SeqNo:7450998 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Methane 14.19 12.65 11.4 300.500
The following samples were analyzed in this batch:HS23071018-06 HS23071018-07 HS23071018-08 HS23071018-09
ALS Houston, US Date: 01-Aug-23
Page 20 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:198283 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198283 Units:mg/L Analysis Date:01-Aug-2023 11:59
Run ID:ICPMS05_442868 SeqNo:7464141 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:MBLK-198283 Units:mg/L Analysis Date:31-Jul-2023 18:02
Run ID:ICPMS05_442748 SeqNo:7462763 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese 0.001622 J 0.00500
Sample ID:LCS-198283 Units:mg/L Analysis Date:31-Jul-2023 18:04
Run ID:ICPMS05_442748 SeqNo:7462764 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 5.418 5 0 108 80 - 1200.200
Manganese 0.05078 0.05 0 102 80 - 1200.00500
Sample ID:HS23071368-01MS Units:mg/L Analysis Date:31-Jul-2023 18:54
Run ID:ICPMS05_442748 SeqNo:7463072 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.207 5 0.005617 104 80 - 1200.200
Manganese 0.04901 0.05 0.000804 96.4 80 - 1200.00500
Sample ID:HS23071368-01MSD Units:mg/L Analysis Date:01-Aug-2023 12:03
Run ID:ICPMS05_442868 SeqNo:7464143 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.311 5 0.005617 106 80 - 120 5.207 1.98 200.200
Manganese 0.05318 0.05 0.000804 105 80 - 120 0.04901 8.16 200.00500
ALS Houston, US Date: 01-Aug-23
Page 21 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:198283 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23071368-01PDS Units:mg/L Analysis Date:31-Jul-2023 18:58
Run ID:ICPMS05_442748 SeqNo:7463074 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 11.29 10 0.005617 113 75 - 1250.200
Manganese 0.1084 0.1 0.000804 108 75 - 1250.00500
Sample ID:HS23071368-01SD Units:mg/L Analysis Date:31-Jul-2023 18:52
Run ID:ICPMS05_442748 SeqNo:7463071 PrepDate:31-Jul-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron U 0.005617 0 101.00
Manganese U 0.000804 0 100.0250
The following samples were analyzed in this batch:HS23071018-06 HS23071018-07 HS23071018-08 HS23071018-09
ALS Houston, US Date: 01-Aug-23
Page 22 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 10:39
Run ID:VOA11_441923 SeqNo:7441986 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
48.67 50 0 97.3 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.77 50 0 91.5 77 - 1131.0Surr: 4-Bromofluorobenzene
52.19 50 0 104 73 - 1261.0Surr: Dibromofluoromethane
50.07 50 0 100 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 23 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 09:57
Run ID:VOA11_441923 SeqNo:7441985 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 19.18 20 0 95.9 73 - 1211.0
1,2-Dibromoethane 17.67 20 0 88.3 76 - 1231.0
1,2-Dichloroethane 17.63 20 0 88.2 70 - 1241.0
2-Methylnaphthalene 15.83 20 0 79.2 55 - 1401.0
4-Isopropyltoluene 19.51 20 0 97.6 74 - 1261.0
Benzene 18.81 20 0 94.0 74 - 1201.0
Chloroform 19.9 20 0 99.5 71 - 1211.0
Ethylbenzene 20.17 20 0 101 77 - 1171.0
m,p-Xylene 38.64 40 0 96.6 77 - 1222.0
Methyl tert-butyl ether 15.97 20 0 79.8 70 - 1301.0
Methylene chloride 20.48 20 0 102 70 - 1272.0
Naphthalene 17.38 20 0 86.9 70 - 1301.0
o-Xylene 20.04 20 0 100 75 - 1191.0
Tert-butyl alcohol 327.3 400 0 81.8 70 - 13010
Toluene 17.8 20 0 89.0 77 - 1181.0
Xylenes, Total 58.68 60 0 97.8 75 - 1223.0
45.12 50 0 90.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.21 50 0 94.4 77 - 1131.0Surr: 4-Bromofluorobenzene
50.13 50 0 100 73 - 1261.0Surr: Dibromofluoromethane
48.96 50 0 97.9 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 24 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071018-01MS Units:ug/L Analysis Date:21-Jul-2023 11:21
Run ID:VOA11_441923 SeqNo:7441988 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:Z1-X1
1,2,4-Trimethylbenzene 17.95 20 0 89.7 70 - 1251.0
1,2-Dibromoethane 16.3 20 0 81.5 70 - 1241.0
1,2-Dichloroethane 16.58 20 0 82.9 70 - 1271.0
2-Methylnaphthalene 14.77 20 0 73.9 55 - 1401.0
4-Isopropyltoluene 18.13 20 0 90.6 70 - 1301.0
Benzene 17.83 20 0 89.1 70 - 1271.0
Chloroform 17.92 20 0 89.6 70 - 1251.0
Ethylbenzene 17.93 20 0 89.7 70 - 1241.0
m,p-Xylene 36.54 40 0 91.3 70 - 1302.0
Methyl tert-butyl ether 14.39 20 0 72.0 70 - 1301.0
Methylene chloride 18.88 20 0 94.4 70 - 1282.0
Naphthalene 16.23 20 0 81.1 70 - 1301.0
o-Xylene 18 20 0 90.0 70 - 1241.0
Tert-butyl alcohol 274.5 400 0 68.6 70 - 130 S10
Toluene 17.38 20 0 86.9 70 - 1231.0
Xylenes, Total 54.54 60 0 90.9 70 - 1303.0
46.03 50 0 92.1 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.95 50 0 95.9 77 - 1131.0Surr: 4-Bromofluorobenzene
48.45 50 0 96.9 77 - 1231.0Surr: Dibromofluoromethane
49.45 50 0 98.9 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 01-Aug-23
Page 25 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071018-01MSD Units:ug/L Analysis Date:21-Jul-2023 11:42
Run ID:VOA11_441923 SeqNo:7441989 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:Z1-X1
1,2,4-Trimethylbenzene 16.5 20 0 82.5 70 - 125 17.95 8.4 201.0
1,2-Dibromoethane 15.15 20 0 75.8 70 - 124 16.3 7.29 201.0
1,2-Dichloroethane 14.99 20 0 74.9 70 - 127 16.58 10.1 201.0
2-Methylnaphthalene 15.61 20 0 78.0 55 - 140 14.77 5.48 201.0
4-Isopropyltoluene 16.91 20 0 84.6 70 - 130 18.13 6.94 201.0
Benzene 16.46 20 0 82.3 70 - 127 17.83 7.98 201.0
Chloroform 16.73 20 0 83.7 70 - 125 17.92 6.87 201.0
Ethylbenzene 16.47 20 0 82.4 70 - 124 17.93 8.48 201.0
m,p-Xylene 33.7 40 0 84.3 70 - 130 36.54 8.07 202.0
Methyl tert-butyl ether 14.33 20 0 71.7 70 - 130 14.39 0.403 201.0
Methylene chloride 17.96 20 0 89.8 70 - 128 18.88 5.01 202.0
Naphthalene 15.8 20 0 79.0 70 - 130 16.23 2.66 201.0
o-Xylene 16.44 20 0 82.2 70 - 124 18 9.05 201.0
Tert-butyl alcohol 264.7 400 0 66.2 70 - 130 274.5 3.62 20 S10
Toluene 16.1 20 0 80.5 70 - 123 17.38 7.67 201.0
Xylenes, Total 50.15 60 0 83.6 70 - 130 54.54 8.39 203.0
46.07 50 0 92.1 70 - 126 46.03 0.0777 201.0Surr: 1,2-Dichloroethane-d4
48.18 50 0 96.4 77 - 113 47.95 0.479 201.0Surr: 4-Bromofluorobenzene
48.66 50 0 97.3 77 - 123 48.45 0.431 201.0Surr: Dibromofluoromethane
49.15 50 0 98.3 82 - 127 49.45 0.619 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071018-01 HS23071018-02 HS23071018-03 HS23071018-04
HS23071018-05 HS23071018-06 HS23071018-07 HS23071018-08
HS23071018-09 HS23071018-10
ALS Houston, US Date: 01-Aug-23
Page 26 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:R441813 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439509 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439508 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.241 0.25 0 96.4 80 - 1200.0500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439511 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.241 0.25 0.008 93.2 75 - 1250.0500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439510 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.242 0.25 0.008 93.6 75 - 125 0.241 0.414 200.0500
The following samples were analyzed in this batch:HS23071018-06 HS23071018-07 HS23071018-08 HS23071018-09
ALS Houston, US Date: 01-Aug-23
Page 27 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:R442705 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 00:04
Run ID:ICS-Integrion_442705 SeqNo:7460135 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 00:10
Run ID:ICS-Integrion_442705 SeqNo:7460136 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.068 8 0 101 90 - 1100.200
Sample ID:HS23071018-09MS Units:mg/L Analysis Date:29-Jul-2023 02:00
Run ID:ICS-Integrion_442705 SeqNo:7460167 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-A-B
Nitrate/Nitrite (as N)39.02 40 0 97.6 80 - 1202.00
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:29-Jul-2023 00:22
Run ID:ICS-Integrion_442705 SeqNo:7460138 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)38.78 40 0 97.0 80 - 1202.00
Sample ID:HS23071018-09MSD Units:mg/L Analysis Date:29-Jul-2023 02:06
Run ID:ICS-Integrion_442705 SeqNo:7460168 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:MW-A-B
Nitrate/Nitrite (as N)40.1 40 0 100 80 - 120 39.02 2.71 202.00
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:29-Jul-2023 00:27
Run ID:ICS-Integrion_442705 SeqNo:7460139 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)39.88 40 0 99.7 80 - 120 38.78 2.79 202.00
The following samples were analyzed in this batch:HS23071018-06 HS23071018-07 HS23071018-08 HS23071018-09
ALS Houston, US Date: 01-Aug-23
Page 28 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:R442749 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:MBLK-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461284 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461283 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)991.4 1000 0 99.1 85 - 1155.00
Alkalinity, Total (As CaCO3)997.4 1000 0 99.7 85 - 1155.00
Sample ID:LCSD-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461282 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)997.2 1000 0 99.7 85 - 115 991.4 0.579 205.00
Alkalinity, Total (As CaCO3)1028 1000 0 103 85 - 115 997.4 3 205.00
Sample ID:HS23071235-03DUP Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461285 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)132.5 135.4 2.16 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)132.5 135.4 2.16 205.00
The following samples were analyzed in this batch:HS23071018-06 HS23071018-07 HS23071018-08 HS23071018-09
ALS Houston, US Date: 01-Aug-23
Page 29 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071018
QC BATCH REPORT
Batch ID:R442827 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:31-Jul-2023 21:16
Run ID:ICS-Integrion_442827 SeqNo:7463012 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:31-Jul-2023 21:27
Run ID:ICS-Integrion_442827 SeqNo:7463013 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.97 20 0 99.9 90 - 1100.500
Sample ID:HS23071023-05MS Units:mg/L Analysis Date:01-Aug-2023 00:27
Run ID:ICS-Integrion_442827 SeqNo:7463003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 38.1 10 31.05 70.5 80 - 120 S 0.500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:31-Jul-2023 21:39
Run ID:ICS-Integrion_442827 SeqNo:7463015 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 13.5 10 3.787 97.1 80 - 1200.500
Sample ID:HS23071023-05MSD Units:mg/L Analysis Date:01-Aug-2023 00:33
Run ID:ICS-Integrion_442827 SeqNo:7463004 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 38.67 10 31.05 76.2 80 - 120 38.1 1.47 20 S 0.500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:31-Jul-2023 21:45
Run ID:ICS-Integrion_442827 SeqNo:7463016 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 13.36 10 3.787 95.8 80 - 120 13.5 1.02 200.500
The following samples were analyzed in this batch:HS23071018-06 HS23071018-07 HS23071018-08 HS23071018-09
ALS Houston, US Date: 01-Aug-23
Page 30 of 35
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071018
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 01-Aug-23
Page 31 of 35
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
01-Aug-23Date: ALS Houston, US
Page 32 of 35
Nelson D. Dusara
19-Jul-2023 13:35Date/Time Received:HS23071018
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
4.1C/4.0C UC/C IR 31
50356
07/19/2023 16:00
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Nilesh D. Ranchod
Date/TimeeSignatureDate/TimeeSignature
20-Jul-2023 08:0118-Jul-2023 12:54
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241095
ALS Houston, US 01-Aug-23Date:
Page 33 of 35
Page 34 of 35
Page 35 of 35
August 03, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 6 sample(s) on Jul 19, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071020
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 33
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071020
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071020-01 18-Jul-2023 14:00 19-Jul-2023 13:35Field Blank (FB) #2 Water
HS23071020-02 18-Jul-2023 14:10 19-Jul-2023 13:35Equipment Blank (EB) #2 Water
HS23071020-03 18-Jul-2023 13:55 19-Jul-2023 13:35DUP #2 Groundwater
HS23071020-04 18-Jul-2023 14:45 19-Jul-2023 13:35Z1-X27 Groundwater
HS23071020-05 18-Jul-2023 15:30 19-Jul-2023 13:35Z4-X70 Groundwater
HS23071020-06 18-Jul-2023 00:00 19-Jul-2023 13:35Trip Blank Water
ALS Houston, US 03-Aug-23Date:
Page 2 of 33
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071020
ECD Organics by Method SW8011
Batch ID: 197845
Sample ID: MBLK-197845
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GC Semivolatiles by Method RSK-175
Batch ID: R442316
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R441923
Sample ID: HS23071018-01MS
MS and MSD are for an unrelated sample•
Metals by Method SW6020A
Batch ID: 198283,198311
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R442749,R443018
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442827
Sample ID: HS23071023-05MS
MS and MSD are for an unrelated sample (Sulfate)•
ALS Houston, US 03-Aug-23Date:
Page 3 of 33
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071020
WetChemistry by Method E300
Batch ID: R442705
Sample ID: DUP #2 (HS23071020-03)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Equipment Blank (EB) #2 (HS23071020-02)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Field Blank (FB) #2 (HS23071020-01)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Z1-X27 (HS23071020-04)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Z4-X70 (HS23071020-05)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441813
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 4 of 33
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Field Blank (FB) #2
WorkOrder:
Lab ID:
Collection Date:
HS23071020
HS23071020-01
18-Jul-2023 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 12:450.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 12:450.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 12:450.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 12:451.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 12:450.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 12:450.20Benzene 1.0U
1ug/L 21-Jul-2023 12:450.20Chloroform 1.0U
1ug/L 21-Jul-2023 12:450.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 12:450.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 12:450.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 12:451.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 12:450.30Naphthalene 1.0U
1ug/L 21-Jul-2023 12:450.30o-Xylene 1.0U
1ug/L 21-Jul-2023 12:4510Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 12:450.20Toluene 1.0U
1ug/L 21-Jul-2023 12:450.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 12:4599.3 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 12:4590.9 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 12:4510377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 12:4510482-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 11:500.107Methane 0.500U
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 23:310.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 31-Jul-2023
1mg/L 31-Jul-2023 19:280.0120Iron 0.200U
1mg/L 31-Jul-2023 19:280.000700Manganese 0.00500U
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 23:180.200Sulfate 0.5000.554
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 01:540.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.0500U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 33
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Equipment Blank (EB) #2
WorkOrder:
Lab ID:
Collection Date:
HS23071020
HS23071020-02
18-Jul-2023 14:10 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 13:060.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 13:060.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 13:060.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 13:061.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 13:060.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 13:060.20Benzene 1.0U
1ug/L 21-Jul-2023 13:060.20Chloroform 1.0U
1ug/L 21-Jul-2023 13:060.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 13:060.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 13:060.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 13:061.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 13:060.30Naphthalene 1.0U
1ug/L 21-Jul-2023 13:060.30o-Xylene 1.0U
1ug/L 21-Jul-2023 13:0610Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 13:060.20Toluene 1.0U
1ug/L 21-Jul-2023 13:060.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 13:0699.0 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 13:0693.9 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 13:0610777-123
Surr: Toluene-d8 1%REC 21-Jul-2023 13:0610082-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 11:580.107Methane 0.500U
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 24-Jul-2023 23:550.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:250.0120Iron 0.200U
1mg/L 01-Aug-2023 14:250.000700Manganese 0.00500U
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 23:230.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 02:110.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.0500U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 33
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DUP #2
WorkOrder:
Lab ID:
Collection Date:
HS23071020
HS23071020-03
18-Jul-2023 13:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 17:180.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 17:180.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 17:180.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 17:181.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 17:180.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 17:180.20Benzene 1.0U
1ug/L 21-Jul-2023 17:180.20Chloroform 1.0U
1ug/L 21-Jul-2023 17:180.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 17:180.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 17:180.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 17:181.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 17:180.30Naphthalene 1.0U
1ug/L 21-Jul-2023 17:180.30o-Xylene 1.0U
1ug/L 21-Jul-2023 17:1810Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 17:180.20Toluene 1.0U
1ug/L 21-Jul-2023 17:180.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 17:1894.6 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 17:1891.3 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 17:1899.8 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 17:1810182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 12:240.107Methane 0.5001.03
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 00:190.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:270.0120Iron 0.2002.72
1mg/L 01-Aug-2023 14:270.000700Manganese 0.005000.0235
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 23:290.200Sulfate 0.5001.76
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 02:170.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 29-Jul-2023 12:255.00Alkalinity, Bicarbonate (As
CaCO3)5.0058.3
1mg/L 29-Jul-2023 12:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 29-Jul-2023 12:25a5.00Alkalinity, Total (As CaCO3)5.0058.3
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05001.83
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 33
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z1-X27
WorkOrder:
Lab ID:
Collection Date:
HS23071020
HS23071020-04
18-Jul-2023 14:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 17:390.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 17:390.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 17:390.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 17:391.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 17:390.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 17:39J0.20Benzene 1.00.82
1ug/L 21-Jul-2023 17:390.20Chloroform 1.0U
1ug/L 21-Jul-2023 17:390.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 17:390.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 17:390.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 17:391.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 17:390.30Naphthalene 1.0U
1ug/L 21-Jul-2023 17:390.30o-Xylene 1.0U
1ug/L 21-Jul-2023 17:3910Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 17:390.20Toluene 1.0U
1ug/L 21-Jul-2023 17:390.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 17:3910370-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 17:3991.7 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 17:3910777-123
Surr: Toluene-d8 1%REC 21-Jul-2023 17:3998.3 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
5ug/L 22-Jul-2023 12:540.535Methane 2.5093.4
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 02:400.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:290.0120Iron 0.2002.11
20mg/L 01-Aug-2023 16:440.0140Manganese 0.1003.21
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 23:350.200Sulfate 0.5000.778
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 02:230.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 01-Aug-2023 18:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00152
1mg/L 01-Aug-2023 18:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:25a5.00Alkalinity, Total (As CaCO3)5.00152
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
5mg/L 20-Jul-2023 10:020.100Ferrous Iron 0.2502.16
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 33
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-X70
WorkOrder:
Lab ID:
Collection Date:
HS23071020
HS23071020-05
18-Jul-2023 15:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 18:000.301,2,4-Trimethylbenzene 1.01.5
1ug/L 21-Jul-2023 18:000.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 18:000.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 18:001.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 18:000.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 18:00J0.20Benzene 1.00.45
1ug/L 21-Jul-2023 18:000.20Chloroform 1.0U
1ug/L 21-Jul-2023 18:00J0.30Ethylbenzene 1.00.47
1ug/L 21-Jul-2023 18:00J0.50m,p-Xylene 2.01.1
1ug/L 21-Jul-2023 18:000.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 18:001.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 18:000.30Naphthalene 1.0U
1ug/L 21-Jul-2023 18:000.30o-Xylene 1.0U
1ug/L 21-Jul-2023 18:0010Tert-butyl alcohol 1051
1ug/L 21-Jul-2023 18:000.20Toluene 1.01.7
1ug/L 21-Jul-2023 18:00J0.30Xylenes, Total 3.01.1
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 18:0094.9 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 18:0095.7 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 18:0010077-123
Surr: Toluene-d8 1%REC 21-Jul-2023 18:00100.0 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
100ug/L 22-Jul-2023 13:1210.7Methane 50.02,090
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 03:040.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:310.0120Iron 0.2009.33
100mg/L 01-Aug-2023 16:460.0700Manganese 0.50015.4
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 31-Jul-2023 23:410.200Sulfate 0.5001.12
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 02:580.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 01-Aug-2023 18:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00424
1mg/L 01-Aug-2023 18:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:25a5.00Alkalinity, Total (As CaCO3)5.00424
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
10mg/L 20-Jul-2023 10:020.200Ferrous Iron 0.50019.0
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 33
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071020
HS23071020-06
18-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 13:270.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 13:270.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 13:270.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 13:271.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 13:270.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 13:270.20Benzene 1.0U
1ug/L 21-Jul-2023 13:270.20Chloroform 1.0U
1ug/L 21-Jul-2023 13:270.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 13:270.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 13:270.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 13:271.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 13:270.30Naphthalene 1.0U
1ug/L 21-Jul-2023 13:270.30o-Xylene 1.0U
1ug/L 21-Jul-2023 13:2710Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 13:270.20Toluene 1.0U
1ug/L 21-Jul-2023 13:270.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 13:2710270-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 13:2796.1 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 13:2710777-123
Surr: Toluene-d8 1%REC 21-Jul-2023 13:2710082-127
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 33
Weight / Prep Log
HS23071020
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197845
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:48 End Date: 21 Jul 2023 09:48
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071020-01 35 (mL)40 mL VOA w/ HCL36.17 (mL)1.033
HS23071020-02 35 (mL)40 mL VOA w/ HCL36.37 (mL)1.039
HS23071020-03 35 (mL)40 mL VOA w/ HCL36.95 (mL)1.056
HS23071020-04 35 (mL)40 mL VOA w/ HCL36.99 (mL)1.057
HS23071020-05 35 (mL)40 mL VOA w/ HCL36.9 (mL)1.054
Batch ID:198283
Method:WATER - SW3010A 3010APrep Code:
Start Date: 31 Jul 2023 08:00 End Date: 31 Jul 2023 08:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071020-01 10 (mL)120 plastic HNO310 (mL)1
Batch ID:198311
Method:WATER - SW3010A 3010APrep Code:
Start Date: 31 Jul 2023 11:00 End Date: 31 Jul 2023 11:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071020-02 10 (mL)120 plastic HNO310 (mL)1
HS23071020-03 10 (mL)120 plastic HNO310 (mL)1
HS23071020-04 10 (mL)120 plastic HNO310 (mL)1
HS23071020-05 10 (mL)120 plastic HNO310 (mL)1
03-Aug-23Date: ALS Houston, US
Page 11 of 33
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071020
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197845 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:48 25 Jul 2023 00:19HS23071020-03 18 Jul 2023 13:55 1DUP #2
21 Jul 2023 09:48 25 Jul 2023 02:40HS23071020-04 18 Jul 2023 14:45 1Z1-X27
21 Jul 2023 09:48 25 Jul 2023 03:04HS23071020-05 18 Jul 2023 15:30 1Z4-X70
Batch ID:197845 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Water
21 Jul 2023 09:48 24 Jul 2023 23:31HS23071020-01 18 Jul 2023 14:00 1Field Blank (FB) #2
21 Jul 2023 09:48 24 Jul 2023 23:55HS23071020-02 18 Jul 2023 14:10 1Equipment Blank (EB) #2
Batch ID:198283 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Water
31 Jul 2023 08:00 31 Jul 2023 19:28HS23071020-01 18 Jul 2023 14:00 1Field Blank (FB) #2
Batch ID:198311 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
31 Jul 2023 11:00 01 Aug 2023 14:27HS23071020-03 18 Jul 2023 13:55 1DUP #2
31 Jul 2023 11:00 01 Aug 2023 16:44HS23071020-04 18 Jul 2023 14:45 20Z1-X27
31 Jul 2023 11:00 01 Aug 2023 14:29HS23071020-04 18 Jul 2023 14:45 1Z1-X27
31 Jul 2023 11:00 01 Aug 2023 16:46HS23071020-05 18 Jul 2023 15:30 100Z4-X70
31 Jul 2023 11:00 01 Aug 2023 14:31HS23071020-05 18 Jul 2023 15:30 1Z4-X70
Batch ID:198311 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Water
31 Jul 2023 11:00 01 Aug 2023 14:25HS23071020-02 18 Jul 2023 14:10 1Equipment Blank (EB) #2
Batch ID:R441813 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
20 Jul 2023 10:02HS23071020-03 18 Jul 2023 13:55 1DUP #2
20 Jul 2023 10:02HS23071020-04 18 Jul 2023 14:45 5Z1-X27
20 Jul 2023 10:02HS23071020-05 18 Jul 2023 15:30 10Z4-X70
Batch ID:R441813 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Water
20 Jul 2023 10:02HS23071020-01 18 Jul 2023 14:00 1Field Blank (FB) #2
20 Jul 2023 10:02HS23071020-02 18 Jul 2023 14:10 1Equipment Blank (EB) #2
Batch ID:R441923 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 17:18HS23071020-03 18 Jul 2023 13:55 1DUP #2
21 Jul 2023 17:39HS23071020-04 18 Jul 2023 14:45 1Z1-X27
21 Jul 2023 18:00HS23071020-05 18 Jul 2023 15:30 1Z4-X70
Batch ID:R441923 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
21 Jul 2023 12:45HS23071020-01 18 Jul 2023 14:00 1Field Blank (FB) #2
21 Jul 2023 13:06HS23071020-02 18 Jul 2023 14:10 1Equipment Blank (EB) #2
21 Jul 2023 13:27HS23071020-06 18 Jul 2023 00:00 1Trip Blank
Batch ID:R442316 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
22 Jul 2023 12:24HS23071020-03 18 Jul 2023 13:55 1DUP #2
22 Jul 2023 12:54HS23071020-04 18 Jul 2023 14:45 5Z1-X27
22 Jul 2023 13:12HS23071020-05 18 Jul 2023 15:30 100Z4-X70
03-Aug-23Date: ALS Houston, US
Page 12 of 33
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071020
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442316 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Water
22 Jul 2023 11:50HS23071020-01 18 Jul 2023 14:00 1Field Blank (FB) #2
22 Jul 2023 11:58HS23071020-02 18 Jul 2023 14:10 1Equipment Blank (EB) #2
Batch ID:R442705 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
29 Jul 2023 02:17HS23071020-03 18 Jul 2023 13:55 10DUP #2
29 Jul 2023 02:23HS23071020-04 18 Jul 2023 14:45 10Z1-X27
29 Jul 2023 02:58HS23071020-05 18 Jul 2023 15:30 10Z4-X70
Batch ID:R442705 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Water
29 Jul 2023 01:54HS23071020-01 18 Jul 2023 14:00 10Field Blank (FB) #2
29 Jul 2023 02:11HS23071020-02 18 Jul 2023 14:10 10Equipment Blank (EB) #2
Batch ID:R442749 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
29 Jul 2023 12:25HS23071020-03 18 Jul 2023 13:55 1DUP #2
Batch ID:R442749 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Water
29 Jul 2023 12:25HS23071020-01 18 Jul 2023 14:00 1Field Blank (FB) #2
29 Jul 2023 12:25HS23071020-02 18 Jul 2023 14:10 1Equipment Blank (EB) #2
Batch ID:R442827 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
31 Jul 2023 23:29HS23071020-03 18 Jul 2023 13:55 1DUP #2
31 Jul 2023 23:35HS23071020-04 18 Jul 2023 14:45 1Z1-X27
31 Jul 2023 23:41HS23071020-05 18 Jul 2023 15:30 1Z4-X70
Batch ID:R442827 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Water
31 Jul 2023 23:18HS23071020-01 18 Jul 2023 14:00 1Field Blank (FB) #2
31 Jul 2023 23:23HS23071020-02 18 Jul 2023 14:10 1Equipment Blank (EB) #2
Batch ID:R443018 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
01 Aug 2023 18:25HS23071020-04 18 Jul 2023 14:45 1Z1-X27
01 Aug 2023 18:25HS23071020-05 18 Jul 2023 15:30 1Z4-X70
03-Aug-23Date: ALS Houston, US
Page 13 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:197845 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197845 Units:ug/L Analysis Date:24-Jul-2023 21:57
Run ID:ECD_13_442224 SeqNo:7448808 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197845 Units:ug/L Analysis Date:24-Jul-2023 22:21
Run ID:ECD_13_442224 SeqNo:7448809 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1917 0.25 0 76.7 60 - 1400.020
Sample ID:LCSD-197845 Units:ug/L Analysis Date:25-Jul-2023 01:29
Run ID:ECD_13_442418 SeqNo:7453268 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1962 0.25 0 78.5 60 - 140 0.1917 2.33 200.020
Sample ID:LCSD-197845 Units:ug/L Analysis Date:24-Jul-2023 22:44
Run ID:ECD_13_442224 SeqNo:7448810 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1835 0.25 0 73.4 60 - 140 0.1917 4.39 200.020
The following samples were analyzed in this batch:HS23071020-01 HS23071020-02 HS23071020-03 HS23071020-04
HS23071020-05
ALS Houston, US Date: 03-Aug-23
Page 14 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R442316 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230722 Units:ug/L Analysis Date:22-Jul-2023 08:11
Run ID:FID-4_442316 SeqNo:7450987 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230722 Units:ug/L Analysis Date:22-Jul-2023 08:21
Run ID:FID-4_442316 SeqNo:7450988 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 8.179 9.647 0 84.8 75 - 1250.500
Sample ID:LCSD-230722 Units:ug/L Analysis Date:22-Jul-2023 08:33
Run ID:FID-4_442316 SeqNo:7450989 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 7.869 9.647 0 81.6 75 - 125 8.179 3.86 300.500
Sample ID:HS23070922-11DUP Units:ug/L Analysis Date:22-Jul-2023 10:23
Run ID:FID-4_442316 SeqNo:7450998 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Methane 14.19 12.65 11.4 300.500
The following samples were analyzed in this batch:HS23071020-01 HS23071020-02 HS23071020-03 HS23071020-04
HS23071020-05
ALS Houston, US Date: 03-Aug-23
Page 15 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:198283 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198283 Units:mg/L Analysis Date:01-Aug-2023 11:59
Run ID:ICPMS05_442868 SeqNo:7464141 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:MBLK-198283 Units:mg/L Analysis Date:31-Jul-2023 18:02
Run ID:ICPMS05_442748 SeqNo:7462763 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese 0.001622 J 0.00500
Sample ID:LCS-198283 Units:mg/L Analysis Date:31-Jul-2023 18:04
Run ID:ICPMS05_442748 SeqNo:7462764 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 5.418 5 0 108 80 - 1200.200
Manganese 0.05078 0.05 0 102 80 - 1200.00500
Sample ID:HS23071368-01MS Units:mg/L Analysis Date:31-Jul-2023 18:54
Run ID:ICPMS05_442748 SeqNo:7463072 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.207 5 0.005617 104 80 - 1200.200
Manganese 0.04901 0.05 0.000804 96.4 80 - 1200.00500
Sample ID:HS23071368-01MSD Units:mg/L Analysis Date:01-Aug-2023 12:03
Run ID:ICPMS05_442868 SeqNo:7464143 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.311 5 0.005617 106 80 - 120 5.207 1.98 200.200
Manganese 0.05318 0.05 0.000804 105 80 - 120 0.04901 8.16 200.00500
ALS Houston, US Date: 03-Aug-23
Page 16 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:198283 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23071368-01PDS Units:mg/L Analysis Date:31-Jul-2023 18:58
Run ID:ICPMS05_442748 SeqNo:7463074 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 11.29 10 0.005617 113 75 - 1250.200
Manganese 0.1084 0.1 0.000804 108 75 - 1250.00500
Sample ID:HS23071368-01SD Units:mg/L Analysis Date:31-Jul-2023 18:52
Run ID:ICPMS05_442748 SeqNo:7463071 PrepDate:31-Jul-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron U 0.005617 0 101.00
Manganese U 0.000804 0 100.0250
The following samples were analyzed in this batch:HS23071020-01
ALS Houston, US Date: 03-Aug-23
Page 17 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:198311 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198311 Units:mg/L Analysis Date:01-Aug-2023 13:49
Run ID:ICPMS06_442867 SeqNo:7464813 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese 0.000794 J 0.00500
Sample ID:LCS-198311 Units:mg/L Analysis Date:01-Aug-2023 13:52
Run ID:ICPMS06_442867 SeqNo:7464814 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.563 5 0 91.3 80 - 1200.200
Manganese 0.04482 0.05 0 89.6 80 - 1200.00500
Sample ID:HS23070892-01MS Units:mg/L Analysis Date:01-Aug-2023 13:59
Run ID:ICPMS06_442867 SeqNo:7464817 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.048 5 0.02657 100 80 - 1200.200
Manganese 0.1484 0.05 0.09528 106 80 - 1200.00500
Sample ID:HS23070892-01MSD Units:mg/L Analysis Date:01-Aug-2023 14:01
Run ID:ICPMS06_442867 SeqNo:7464818 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.293 5 0.02657 105 80 - 120 5.048 4.74 200.200
Manganese 0.1545 0.05 0.09528 118 80 - 120 0.1484 4.01 200.00500
Sample ID:HS23070892-01PDS Units:mg/L Analysis Date:01-Aug-2023 14:03
Run ID:ICPMS06_442867 SeqNo:7464819 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 10.48 10 0.02657 104 75 - 1250.200
Manganese 0.2032 0.1 0.09528 108 75 - 1250.00500
ALS Houston, US Date: 03-Aug-23
Page 18 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:198311 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23070892-01SD Units:mg/L Analysis Date:01-Aug-2023 13:57
Run ID:ICPMS06_442867 SeqNo:7464816 PrepDate:31-Jul-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron U 0.02657 0 101.00
Manganese 0.09742 0.09528 2.25 100.0250
The following samples were analyzed in this batch:HS23071020-02 HS23071020-03 HS23071020-04 HS23071020-05
ALS Houston, US Date: 03-Aug-23
Page 19 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 10:39
Run ID:VOA11_441923 SeqNo:7441986 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
48.67 50 0 97.3 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.77 50 0 91.5 77 - 1131.0Surr: 4-Bromofluorobenzene
52.19 50 0 104 73 - 1261.0Surr: Dibromofluoromethane
50.07 50 0 100 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 20 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 09:57
Run ID:VOA11_441923 SeqNo:7441985 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 19.18 20 0 95.9 73 - 1211.0
1,2-Dibromoethane 17.67 20 0 88.3 76 - 1231.0
1,2-Dichloroethane 17.63 20 0 88.2 70 - 1241.0
2-Methylnaphthalene 15.83 20 0 79.2 55 - 1401.0
4-Isopropyltoluene 19.51 20 0 97.6 74 - 1261.0
Benzene 18.81 20 0 94.0 74 - 1201.0
Chloroform 19.9 20 0 99.5 71 - 1211.0
Ethylbenzene 20.17 20 0 101 77 - 1171.0
m,p-Xylene 38.64 40 0 96.6 77 - 1222.0
Methyl tert-butyl ether 15.97 20 0 79.8 70 - 1301.0
Methylene chloride 20.48 20 0 102 70 - 1272.0
Naphthalene 17.38 20 0 86.9 70 - 1301.0
o-Xylene 20.04 20 0 100 75 - 1191.0
Tert-butyl alcohol 327.3 400 0 81.8 70 - 13010
Toluene 17.8 20 0 89.0 77 - 1181.0
Xylenes, Total 58.68 60 0 97.8 75 - 1223.0
45.12 50 0 90.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.21 50 0 94.4 77 - 1131.0Surr: 4-Bromofluorobenzene
50.13 50 0 100 73 - 1261.0Surr: Dibromofluoromethane
48.96 50 0 97.9 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 21 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071018-01MS Units:ug/L Analysis Date:21-Jul-2023 11:21
Run ID:VOA11_441923 SeqNo:7441988 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 17.95 20 0 89.7 70 - 1251.0
1,2-Dibromoethane 16.3 20 0 81.5 70 - 1241.0
1,2-Dichloroethane 16.58 20 0 82.9 70 - 1271.0
2-Methylnaphthalene 14.77 20 0 73.9 55 - 1401.0
4-Isopropyltoluene 18.13 20 0 90.6 70 - 1301.0
Benzene 17.83 20 0 89.1 70 - 1271.0
Chloroform 17.92 20 0 89.6 70 - 1251.0
Ethylbenzene 17.93 20 0 89.7 70 - 1241.0
m,p-Xylene 36.54 40 0 91.3 70 - 1302.0
Methyl tert-butyl ether 14.39 20 0 72.0 70 - 1301.0
Methylene chloride 18.88 20 0 94.4 70 - 1282.0
Naphthalene 16.23 20 0 81.1 70 - 1301.0
o-Xylene 18 20 0 90.0 70 - 1241.0
Tert-butyl alcohol 274.5 400 0 68.6 70 - 130 S10
Toluene 17.38 20 0 86.9 70 - 1231.0
Xylenes, Total 54.54 60 0 90.9 70 - 1303.0
46.03 50 0 92.1 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.95 50 0 95.9 77 - 1131.0Surr: 4-Bromofluorobenzene
48.45 50 0 96.9 77 - 1231.0Surr: Dibromofluoromethane
49.45 50 0 98.9 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 22 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071018-01MSD Units:ug/L Analysis Date:21-Jul-2023 11:42
Run ID:VOA11_441923 SeqNo:7441989 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 16.5 20 0 82.5 70 - 125 17.95 8.4 201.0
1,2-Dibromoethane 15.15 20 0 75.8 70 - 124 16.3 7.29 201.0
1,2-Dichloroethane 14.99 20 0 74.9 70 - 127 16.58 10.1 201.0
2-Methylnaphthalene 15.61 20 0 78.0 55 - 140 14.77 5.48 201.0
4-Isopropyltoluene 16.91 20 0 84.6 70 - 130 18.13 6.94 201.0
Benzene 16.46 20 0 82.3 70 - 127 17.83 7.98 201.0
Chloroform 16.73 20 0 83.7 70 - 125 17.92 6.87 201.0
Ethylbenzene 16.47 20 0 82.4 70 - 124 17.93 8.48 201.0
m,p-Xylene 33.7 40 0 84.3 70 - 130 36.54 8.07 202.0
Methyl tert-butyl ether 14.33 20 0 71.7 70 - 130 14.39 0.403 201.0
Methylene chloride 17.96 20 0 89.8 70 - 128 18.88 5.01 202.0
Naphthalene 15.8 20 0 79.0 70 - 130 16.23 2.66 201.0
o-Xylene 16.44 20 0 82.2 70 - 124 18 9.05 201.0
Tert-butyl alcohol 264.7 400 0 66.2 70 - 130 274.5 3.62 20 S10
Toluene 16.1 20 0 80.5 70 - 123 17.38 7.67 201.0
Xylenes, Total 50.15 60 0 83.6 70 - 130 54.54 8.39 203.0
46.07 50 0 92.1 70 - 126 46.03 0.0777 201.0Surr: 1,2-Dichloroethane-d4
48.18 50 0 96.4 77 - 113 47.95 0.479 201.0Surr: 4-Bromofluorobenzene
48.66 50 0 97.3 77 - 123 48.45 0.431 201.0Surr: Dibromofluoromethane
49.15 50 0 98.3 82 - 127 49.45 0.619 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071020-01 HS23071020-02 HS23071020-03 HS23071020-04
HS23071020-05 HS23071020-06
ALS Houston, US Date: 03-Aug-23
Page 23 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R441813 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439509 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439508 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.241 0.25 0 96.4 80 - 1200.0500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439511 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.241 0.25 0.008 93.2 75 - 1250.0500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439510 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.242 0.25 0.008 93.6 75 - 125 0.241 0.414 200.0500
The following samples were analyzed in this batch:HS23071020-01 HS23071020-02 HS23071020-03 HS23071020-04
HS23071020-05
ALS Houston, US Date: 03-Aug-23
Page 24 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R442705 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 00:04
Run ID:ICS-Integrion_442705 SeqNo:7460135 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 00:10
Run ID:ICS-Integrion_442705 SeqNo:7460136 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.068 8 0 101 90 - 1100.200
Sample ID:HS23071018-09MS Units:mg/L Analysis Date:29-Jul-2023 02:00
Run ID:ICS-Integrion_442705 SeqNo:7460167 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)39.02 40 0 97.6 80 - 1202.00
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:29-Jul-2023 00:22
Run ID:ICS-Integrion_442705 SeqNo:7460138 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)38.78 40 0 97.0 80 - 1202.00
Sample ID:HS23071018-09MSD Units:mg/L Analysis Date:29-Jul-2023 02:06
Run ID:ICS-Integrion_442705 SeqNo:7460168 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)40.1 40 0 100 80 - 120 39.02 2.71 202.00
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:29-Jul-2023 00:27
Run ID:ICS-Integrion_442705 SeqNo:7460139 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)39.88 40 0 99.7 80 - 120 38.78 2.79 202.00
The following samples were analyzed in this batch:HS23071020-01 HS23071020-02 HS23071020-03 HS23071020-04
HS23071020-05
ALS Houston, US Date: 03-Aug-23
Page 25 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R442749 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:MBLK-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461284 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461283 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)991.4 1000 0 99.1 85 - 1155.00
Alkalinity, Total (As CaCO3)997.4 1000 0 99.7 85 - 1155.00
Sample ID:LCSD-R442749 Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461282 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)997.2 1000 0 99.7 85 - 115 991.4 0.579 205.00
Alkalinity, Total (As CaCO3)1028 1000 0 103 85 - 115 997.4 3 205.00
Sample ID:HS23071235-03DUP Units:mg/L Analysis Date:29-Jul-2023 12:25
Run ID:ManTech01_442749 SeqNo:7461285 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)132.5 135.4 2.16 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)132.5 135.4 2.16 205.00
The following samples were analyzed in this batch:HS23071020-01 HS23071020-02 HS23071020-03
ALS Houston, US Date: 03-Aug-23
Page 26 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R442827 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:31-Jul-2023 21:16
Run ID:ICS-Integrion_442827 SeqNo:7463012 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:31-Jul-2023 21:27
Run ID:ICS-Integrion_442827 SeqNo:7463013 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.97 20 0 99.9 90 - 1100.500
Sample ID:HS23071023-05MS Units:mg/L Analysis Date:01-Aug-2023 00:27
Run ID:ICS-Integrion_442827 SeqNo:7463003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 38.1 10 31.05 70.5 80 - 120 S 0.500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:31-Jul-2023 21:39
Run ID:ICS-Integrion_442827 SeqNo:7463015 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 13.5 10 3.787 97.1 80 - 1200.500
Sample ID:HS23071023-05MSD Units:mg/L Analysis Date:01-Aug-2023 00:33
Run ID:ICS-Integrion_442827 SeqNo:7463004 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 38.67 10 31.05 76.2 80 - 120 38.1 1.47 20 S 0.500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:31-Jul-2023 21:45
Run ID:ICS-Integrion_442827 SeqNo:7463016 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 13.36 10 3.787 95.8 80 - 120 13.5 1.02 200.500
The following samples were analyzed in this batch:HS23071020-01 HS23071020-02 HS23071020-03 HS23071020-04
HS23071020-05
ALS Houston, US Date: 03-Aug-23
Page 27 of 33
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071020
QC BATCH REPORT
Batch ID:R443018 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:MBLK-R443018 Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467806 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-R443018 Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467805 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)1005 1000 0 100 85 - 1155.00
Alkalinity, Total (As CaCO3)1008 1000 0 101 85 - 1155.00
Sample ID:LCSD-R443018 Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467837 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)997.3 1000 0 99.7 85 - 115 1005 0.724 205.00
Alkalinity, Total (As CaCO3)1001 1000 0 100 85 - 115 1008 0.682 205.00
Sample ID:HS23071020-04DUP Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467807 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:Z1-X27
Alkalinity, Bicarbonate (As CaCO3)167.9 152 9.94 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)167.9 152 9.94 205.00
The following samples were analyzed in this batch:HS23071020-04 HS23071020-05
ALS Houston, US Date: 03-Aug-23
Page 28 of 33
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071020
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 03-Aug-23
Page 29 of 33
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
03-Aug-23Date: ALS Houston, US
Page 30 of 33
Nelson D. Dusara
19-Jul-2023 13:35Date/Time Received:HS23071020
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.8C/3.7C UC/C IR 31
Blue
07/19/2023 16:00
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Ragen Giga
Date/TimeeSignatureDate/TimeeSignature
20-Jul-2023 07:5518-Jul-2023 12:54
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241115
ALS Houston, US 03-Aug-23Date:
Page 31 of 33
Page 32 of 33
Page 33 of 33
August 03, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 9 sample(s) on Jul 19, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071023
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 37
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071023
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071023-01 18-Jul-2023 09:00 19-Jul-2023 13:35PMW-L-I Groundwater
HS23071023-02 18-Jul-2023 11:25 19-Jul-2023 13:35PMW-L-D Groundwater
HS23071023-03 18-Jul-2023 10:35 19-Jul-2023 13:35PMW-L-B Groundwater
HS23071023-04 18-Jul-2023 09:40 19-Jul-2023 13:35AMW-12S Groundwater
HS23071023-05 18-Jul-2023 13:55 19-Jul-2023 13:35MW-E-I Groundwater
HS23071023-06 18-Jul-2023 13:10 19-Jul-2023 13:35MW-E-D Groundwater
HS23071023-07 18-Jul-2023 14:50 19-Jul-2023 13:35MW-E-B Groundwater
HS23071023-08 18-Jul-2023 15:40 19-Jul-2023 13:35Z4-X47 Groundwater
HS23071023-09 18-Jul-2023 00:00 19-Jul-2023 13:35Trip Blank Water
ALS Houston, US 03-Aug-23Date:
Page 2 of 37
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071023
ECD Organics by Method SW8011
Batch ID: 197845
Sample ID: MBLK-197845
The recovery of the Matrix Spike (MS) associated to this analyte was outside of the established control limits. However, the LCS was
within control limits. The recovery of the MS may be due to sample matrix interference.
•
GC Semivolatiles by Method RSK-175
Batch ID: R441986
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R441822
Sample ID: HS23071014-01MS
MS and MSD are for an unrelated sample•
Batch ID: R441888
Sample ID: HS23071017-06MS
MS and MSD are for an unrelated sample•
Metals by Method SW6020A
Batch ID: 198311
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R443018
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442827
Sample ID: MW-E-I (HS23071023-05MS)
The recovery of the Matrix Spike (MS) and/or Matrix Spike Duplicate (MSD) associated with this analyte was outside of the
established control limits. However, the LCS was within control limits. The recovery of the MS/MSD may be due to sample matrix
interference. (Sulfate)
•
ALS Houston, US 03-Aug-23Date:
Page 3 of 37
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071023
WetChemistry by Method E300
Batch ID: R442705
Sample ID: MW-E-B (HS23071023-07)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-E-D (HS23071023-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-E-I (HS23071023-05)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441813
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 4 of 37
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-L-I
WorkOrder:
Lab ID:
Collection Date:
HS23071023
HS23071023-01
18-Jul-2023 09:00 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 23:490.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 23:490.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 23:490.201,2-Dichloroethane 1.01.3
1ug/L 20-Jul-2023 23:491.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 23:490.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 23:490.20Benzene 1.0U
1ug/L 20-Jul-2023 23:490.20Chloroform 1.0U
1ug/L 20-Jul-2023 23:490.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 23:490.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 23:490.20Methyl tert-butyl ether 1.013
1ug/L 20-Jul-2023 23:491.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 23:490.30Naphthalene 1.0U
1ug/L 20-Jul-2023 23:490.30o-Xylene 1.0U
1ug/L 20-Jul-2023 23:4910Tert-butyl alcohol 10120
1ug/L 20-Jul-2023 23:490.20Toluene 1.0U
1ug/L 20-Jul-2023 23:490.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 23:4995.9 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 23:4997.3 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 23:4998.9 77-123
Surr: Toluene-d8 1%REC 20-Jul-2023 23:4996.9 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 03:270.00321,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 37
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-L-D
WorkOrder:
Lab ID:
Collection Date:
HS23071023
HS23071023-02
18-Jul-2023 11:25 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 00:100.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 00:100.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 00:100.201,2-Dichloroethane 1.03.9
1ug/L 21-Jul-2023 00:101.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 00:100.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 00:100.20Benzene 1.0U
1ug/L 21-Jul-2023 00:100.20Chloroform 1.0U
1ug/L 21-Jul-2023 00:100.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 00:100.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 00:100.20Methyl tert-butyl ether 1.043
1ug/L 21-Jul-2023 00:101.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 00:100.30Naphthalene 1.0U
1ug/L 21-Jul-2023 00:100.30o-Xylene 1.0U
1ug/L 21-Jul-2023 00:1010Tert-butyl alcohol 10240
1ug/L 21-Jul-2023 00:100.20Toluene 1.0U
1ug/L 21-Jul-2023 00:100.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 00:1098.8 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 00:1092.4 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 00:1010577-123
Surr: Toluene-d8 1%REC 21-Jul-2023 00:1010282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 03:510.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 37
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-L-B
WorkOrder:
Lab ID:
Collection Date:
HS23071023
HS23071023-03
18-Jul-2023 10:35 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 00:310.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 00:310.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 00:310.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 00:311.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 00:310.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 00:310.20Benzene 1.0U
1ug/L 21-Jul-2023 00:310.20Chloroform 1.0U
1ug/L 21-Jul-2023 00:310.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 00:310.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 00:310.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 00:311.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 00:310.30Naphthalene 1.0U
1ug/L 21-Jul-2023 00:310.30o-Xylene 1.0U
1ug/L 21-Jul-2023 00:3110Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 00:310.20Toluene 1.0U
1ug/L 21-Jul-2023 00:310.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 00:3199.3 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 00:3193.5 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 00:3110577-123
Surr: Toluene-d8 1%REC 21-Jul-2023 00:3110282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 04:140.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 37
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-12S
WorkOrder:
Lab ID:
Collection Date:
HS23071023
HS23071023-04
18-Jul-2023 09:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 00:520.301,2,4-Trimethylbenzene 1.043
1ug/L 21-Jul-2023 00:520.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 00:520.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 00:521.02-Methylnaphthalene 1.05.9
1ug/L 21-Jul-2023 00:520.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 00:520.20Benzene 1.01.0
1ug/L 21-Jul-2023 00:520.20Chloroform 1.0U
1ug/L 21-Jul-2023 00:520.30Ethylbenzene 1.050
1ug/L 21-Jul-2023 00:520.50m,p-Xylene 2.028
1ug/L 21-Jul-2023 00:520.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 00:521.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 00:520.30Naphthalene 1.020
1ug/L 21-Jul-2023 00:520.30o-Xylene 1.0U
1ug/L 21-Jul-2023 00:5210Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 00:520.20Toluene 1.0U
1ug/L 21-Jul-2023 00:520.30Xylenes, Total 3.028
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 00:5295.5 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 00:5295.3 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 00:5298.4 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 00:5299.9 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 04:380.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 37
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-E-I
WorkOrder:
Lab ID:
Collection Date:
HS23071023
HS23071023-05
18-Jul-2023 13:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 01:130.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 01:130.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 01:130.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 01:131.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 01:130.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 01:130.20Benzene 1.0U
1ug/L 21-Jul-2023 01:130.20Chloroform 1.0U
1ug/L 21-Jul-2023 01:130.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 01:130.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 01:130.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 01:131.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 01:130.30Naphthalene 1.02.4
1ug/L 21-Jul-2023 01:130.30o-Xylene 1.0U
1ug/L 21-Jul-2023 01:1310Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 01:130.20Toluene 1.0U
1ug/L 21-Jul-2023 01:130.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 01:1399.3 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 01:1392.9 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 01:1310477-123
Surr: Toluene-d8 1%REC 21-Jul-2023 01:1310182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
2ug/L 21-Jul-2023 12:350.214Methane 1.0065.1
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 05:010.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:330.0120Iron 0.2000.219
1mg/L 01-Aug-2023 14:330.000700Manganese 0.005000.649
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 00:220.200Sulfate 0.50031.1
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 03:030.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 01-Aug-2023 18:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00162
1mg/L 01-Aug-2023 18:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:25a5.00Alkalinity, Total (As CaCO3)5.00162
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05000.167
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 37
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-E-D
WorkOrder:
Lab ID:
Collection Date:
HS23071023
HS23071023-06
18-Jul-2023 13:10 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 01:340.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 01:340.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 01:340.201,2-Dichloroethane 1.012
1ug/L 21-Jul-2023 01:341.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 01:340.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 01:340.20Benzene 1.0U
1ug/L 21-Jul-2023 01:340.20Chloroform 1.0U
1ug/L 21-Jul-2023 01:340.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 01:340.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 01:340.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 01:341.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 01:340.30Naphthalene 1.0U
1ug/L 21-Jul-2023 01:340.30o-Xylene 1.0U
1ug/L 21-Jul-2023 01:3410Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 01:340.20Toluene 1.0U
1ug/L 21-Jul-2023 01:340.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 01:3499.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 01:3496.5 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 01:3410277-123
Surr: Toluene-d8 1%REC 21-Jul-2023 01:3410182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
2ug/L 21-Jul-2023 12:430.214Methane 1.0042.2
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 05:250.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:35J0.0120Iron 0.2000.155
1mg/L 01-Aug-2023 14:350.000700Manganese 0.005000.184
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 00:450.200Sulfate 0.5002.90
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 03:090.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 01-Aug-2023 18:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00114
1mg/L 01-Aug-2023 18:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:25a5.00Alkalinity, Total (As CaCO3)5.00114
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05000.172
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 37
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-E-B
WorkOrder:
Lab ID:
Collection Date:
HS23071023
HS23071023-07
18-Jul-2023 14:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 01:550.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 01:550.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 01:550.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 01:551.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 01:550.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 01:550.20Benzene 1.0U
1ug/L 21-Jul-2023 01:550.20Chloroform 1.0U
1ug/L 21-Jul-2023 01:550.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 01:550.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 01:550.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 01:551.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 01:550.30Naphthalene 1.0U
1ug/L 21-Jul-2023 01:550.30o-Xylene 1.0U
1ug/L 21-Jul-2023 01:5510Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 01:550.20Toluene 1.0U
1ug/L 21-Jul-2023 01:550.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 01:5510170-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 01:5593.0 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 01:5510477-123
Surr: Toluene-d8 1%REC 21-Jul-2023 01:5599.5 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 12:260.107Methane 0.5000.549
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 05:490.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:41J0.0120Iron 0.2000.0131
1mg/L 01-Aug-2023 14:41J0.000700Manganese 0.005000.00152
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 00:510.200Sulfate 0.5004.16
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 03:15J0.300Nitrate/Nitrite (as N)2.000.568
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 01-Aug-2023 18:255.00Alkalinity, Bicarbonate (As
CaCO3)5.0046.8
1mg/L 01-Aug-2023 18:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:25a5.00Alkalinity, Total (As CaCO3)5.0046.8
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:02J0.0200Ferrous Iron 0.05000.0370
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 37
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-X47
WorkOrder:
Lab ID:
Collection Date:
HS23071023
HS23071023-08
18-Jul-2023 15:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 02:160.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 02:160.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 02:160.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 02:161.02-Methylnaphthalene 1.07.5
1ug/L 21-Jul-2023 02:160.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 02:160.20Benzene 1.08.2
1ug/L 21-Jul-2023 02:160.20Chloroform 1.0U
1ug/L 21-Jul-2023 02:16J0.30Ethylbenzene 1.00.74
1ug/L 21-Jul-2023 02:16J0.50m,p-Xylene 2.01.0
1ug/L 21-Jul-2023 02:160.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 02:161.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 02:160.30Naphthalene 1.04.3
1ug/L 21-Jul-2023 02:16J0.30o-Xylene 1.00.40
1ug/L 21-Jul-2023 02:1610Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 02:160.20Toluene 1.0U
1ug/L 21-Jul-2023 02:16J0.30Xylenes, Total 3.01.4
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 02:1699.2 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 02:1693.9 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 02:1610177-123
Surr: Toluene-d8 1%REC 21-Jul-2023 02:1699.6 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 07:220.00311,2-Dibromoethane 0.020U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 37
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071023
HS23071023-09
18-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 20-Jul-2023 14:190.301,2,4-Trimethylbenzene 1.0U
1ug/L 20-Jul-2023 14:190.201,2-Dibromoethane 1.0U
1ug/L 20-Jul-2023 14:190.201,2-Dichloroethane 1.0U
1ug/L 20-Jul-2023 14:191.02-Methylnaphthalene 1.0U
1ug/L 20-Jul-2023 14:190.304-Isopropyltoluene 1.0U
1ug/L 20-Jul-2023 14:190.20Benzene 1.0U
1ug/L 20-Jul-2023 14:190.20Chloroform 1.0U
1ug/L 20-Jul-2023 14:190.30Ethylbenzene 1.0U
1ug/L 20-Jul-2023 14:190.50m,p-Xylene 2.0U
1ug/L 20-Jul-2023 14:190.20Methyl tert-butyl ether 1.0U
1ug/L 20-Jul-2023 14:191.0Methylene chloride 2.0U
1ug/L 20-Jul-2023 14:190.30Naphthalene 1.0U
1ug/L 20-Jul-2023 14:190.30o-Xylene 1.0U
1ug/L 20-Jul-2023 14:1910Tert-butyl alcohol 10U
1ug/L 20-Jul-2023 14:190.20Toluene 1.0U
1ug/L 20-Jul-2023 14:190.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 20-Jul-2023 14:1996.6 70-126
Surr: 4-Bromofluorobenzene 1%REC 20-Jul-2023 14:1993.7 77-113
Surr: Dibromofluoromethane 1%REC 20-Jul-2023 14:1910177-123
Surr: Toluene-d8 1%REC 20-Jul-2023 14:1910382-127
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 37
Weight / Prep Log
HS23071023
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197845
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:48 End Date: 21 Jul 2023 09:48
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071023-01 35 (mL)40 mL VOA w/ HCL36.87 (mL)1.053
HS23071023-02 35 (mL)40 mL VOA w/ HCL36.53 (mL)1.044
HS23071023-03 35 (mL)40 mL VOA w/ HCL36.48 (mL)1.042
HS23071023-04 35 (mL)40 mL VOA w/ HCL36.68 (mL)1.048
HS23071023-05 35 (mL)40 mL VOA w/ HCL36.56 (mL)1.045
HS23071023-06 35 (mL)40 mL VOA w/ HCL36.08 (mL)1.031
HS23071023-07 35 (mL)40 mL VOA w/ HCL36.76 (mL)1.05
HS23071023-08 35 (mL)40 mL VOA w/ HCL35.81 (mL)1.023
Batch ID:198311
Method:WATER - SW3010A 3010APrep Code:
Start Date: 31 Jul 2023 11:00 End Date: 31 Jul 2023 11:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071023-05 10 (mL)120 plastic HNO310 (mL)1
HS23071023-06 10 (mL)120 plastic HNO310 (mL)1
HS23071023-07 10 (mL)120 plastic HNO310 (mL)1
03-Aug-23Date: ALS Houston, US
Page 14 of 37
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071023
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197845 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:48 25 Jul 2023 03:27HS23071023-01 18 Jul 2023 09:00 1PMW-L-I
21 Jul 2023 09:48 25 Jul 2023 03:51HS23071023-02 18 Jul 2023 11:25 1PMW-L-D
21 Jul 2023 09:48 25 Jul 2023 04:14HS23071023-03 18 Jul 2023 10:35 1PMW-L-B
21 Jul 2023 09:48 25 Jul 2023 04:38HS23071023-04 18 Jul 2023 09:40 1AMW-12S
21 Jul 2023 09:48 25 Jul 2023 05:01HS23071023-05 18 Jul 2023 13:55 1MW-E-I
21 Jul 2023 09:48 25 Jul 2023 05:25HS23071023-06 18 Jul 2023 13:10 1MW-E-D
21 Jul 2023 09:48 25 Jul 2023 05:49HS23071023-07 18 Jul 2023 14:50 1MW-E-B
21 Jul 2023 09:48 25 Jul 2023 07:22HS23071023-08 18 Jul 2023 15:40 1Z4-X47
Batch ID:198311 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
31 Jul 2023 11:00 01 Aug 2023 14:33HS23071023-05 18 Jul 2023 13:55 1MW-E-I
31 Jul 2023 11:00 01 Aug 2023 14:35HS23071023-06 18 Jul 2023 13:10 1MW-E-D
31 Jul 2023 11:00 01 Aug 2023 14:41HS23071023-07 18 Jul 2023 14:50 1MW-E-B
Batch ID:R441813 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
20 Jul 2023 10:02HS23071023-05 18 Jul 2023 13:55 1MW-E-I
20 Jul 2023 10:02HS23071023-06 18 Jul 2023 13:10 1MW-E-D
20 Jul 2023 10:02HS23071023-07 18 Jul 2023 14:50 1MW-E-B
Batch ID:R441822 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
20 Jul 2023 14:19HS23071023-09 18 Jul 2023 00:00 1Trip Blank
Batch ID:R441888 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
20 Jul 2023 23:49HS23071023-01 18 Jul 2023 09:00 1PMW-L-I
21 Jul 2023 00:10HS23071023-02 18 Jul 2023 11:25 1PMW-L-D
21 Jul 2023 00:31HS23071023-03 18 Jul 2023 10:35 1PMW-L-B
21 Jul 2023 00:52HS23071023-04 18 Jul 2023 09:40 1AMW-12S
21 Jul 2023 01:13HS23071023-05 18 Jul 2023 13:55 1MW-E-I
21 Jul 2023 01:34HS23071023-06 18 Jul 2023 13:10 1MW-E-D
21 Jul 2023 01:55HS23071023-07 18 Jul 2023 14:50 1MW-E-B
21 Jul 2023 02:16HS23071023-08 18 Jul 2023 15:40 1Z4-X47
Batch ID:R441986 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
21 Jul 2023 12:35HS23071023-05 18 Jul 2023 13:55 2MW-E-I
21 Jul 2023 12:43HS23071023-06 18 Jul 2023 13:10 2MW-E-D
21 Jul 2023 12:26HS23071023-07 18 Jul 2023 14:50 1MW-E-B
Batch ID:R442705 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
29 Jul 2023 03:03HS23071023-05 18 Jul 2023 13:55 10MW-E-I
29 Jul 2023 03:09HS23071023-06 18 Jul 2023 13:10 10MW-E-D
29 Jul 2023 03:15HS23071023-07 18 Jul 2023 14:50 10MW-E-B
03-Aug-23Date: ALS Houston, US
Page 15 of 37
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071023
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442827 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
01 Aug 2023 00:22HS23071023-05 18 Jul 2023 13:55 1MW-E-I
01 Aug 2023 00:45HS23071023-06 18 Jul 2023 13:10 1MW-E-D
01 Aug 2023 00:51HS23071023-07 18 Jul 2023 14:50 1MW-E-B
Batch ID:R443018 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
01 Aug 2023 18:25HS23071023-05 18 Jul 2023 13:55 1MW-E-I
01 Aug 2023 18:25HS23071023-06 18 Jul 2023 13:10 1MW-E-D
01 Aug 2023 18:25HS23071023-07 18 Jul 2023 14:50 1MW-E-B
03-Aug-23Date: ALS Houston, US
Page 16 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:197845 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197845 Units:ug/L Analysis Date:24-Jul-2023 21:57
Run ID:ECD_13_442224 SeqNo:7448808 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197845 Units:ug/L Analysis Date:24-Jul-2023 22:21
Run ID:ECD_13_442224 SeqNo:7448809 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1917 0.25 0 76.7 60 - 1400.020
Sample ID:LCSD-197845 Units:ug/L Analysis Date:25-Jul-2023 01:29
Run ID:ECD_13_442418 SeqNo:7453268 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1962 0.25 0 78.5 60 - 140 0.1917 2.33 200.020
Sample ID:LCSD-197845 Units:ug/L Analysis Date:24-Jul-2023 22:44
Run ID:ECD_13_442224 SeqNo:7448810 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1835 0.25 0 73.4 60 - 140 0.1917 4.39 200.020
The following samples were analyzed in this batch:HS23071023-01 HS23071023-02 HS23071023-03 HS23071023-04
HS23071023-05 HS23071023-06 HS23071023-07 HS23071023-08
ALS Houston, US Date: 03-Aug-23
Page 17 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441986 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230721 Units:ug/L Analysis Date:21-Jul-2023 07:07
Run ID:FID-4_441986 SeqNo:7443383 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230721 Units:ug/L Analysis Date:21-Jul-2023 07:40
Run ID:FID-4_441986 SeqNo:7443384 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.855 9.647 0 81.4 75 - 1250.500
Sample ID:LCSD-230721 Units:ug/L Analysis Date:21-Jul-2023 08:01
Run ID:FID-4_441986 SeqNo:7443385 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 7.797 9.647 0 80.8 75 - 125 7.855 0.747 300.500
Sample ID:HS23070935-02DUP Units:ug/L Analysis Date:21-Jul-2023 09:44
Run ID:FID-4_441986 SeqNo:7443391 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Methane 16.97 16.73 1.42 300.500
The following samples were analyzed in this batch:HS23071023-05 HS23071023-06 HS23071023-07
ALS Houston, US Date: 03-Aug-23
Page 18 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:198311 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198311 Units:mg/L Analysis Date:01-Aug-2023 13:49
Run ID:ICPMS06_442867 SeqNo:7464813 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese 0.000794 J 0.00500
Sample ID:LCS-198311 Units:mg/L Analysis Date:01-Aug-2023 13:52
Run ID:ICPMS06_442867 SeqNo:7464814 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.563 5 0 91.3 80 - 1200.200
Manganese 0.04482 0.05 0 89.6 80 - 1200.00500
Sample ID:HS23070892-01MS Units:mg/L Analysis Date:01-Aug-2023 13:59
Run ID:ICPMS06_442867 SeqNo:7464817 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.048 5 0.02657 100 80 - 1200.200
Manganese 0.1484 0.05 0.09528 106 80 - 1200.00500
Sample ID:HS23070892-01MSD Units:mg/L Analysis Date:01-Aug-2023 14:01
Run ID:ICPMS06_442867 SeqNo:7464818 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.293 5 0.02657 105 80 - 120 5.048 4.74 200.200
Manganese 0.1545 0.05 0.09528 118 80 - 120 0.1484 4.01 200.00500
Sample ID:HS23070892-01PDS Units:mg/L Analysis Date:01-Aug-2023 14:03
Run ID:ICPMS06_442867 SeqNo:7464819 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 10.48 10 0.02657 104 75 - 1250.200
Manganese 0.2032 0.1 0.09528 108 75 - 1250.00500
ALS Houston, US Date: 03-Aug-23
Page 19 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:198311 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23070892-01SD Units:mg/L Analysis Date:01-Aug-2023 13:57
Run ID:ICPMS06_442867 SeqNo:7464816 PrepDate:31-Jul-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron U 0.02657 0 101.00
Manganese 0.09742 0.09528 2.25 100.0250
The following samples were analyzed in this batch:HS23071023-05 HS23071023-06 HS23071023-07
ALS Houston, US Date: 03-Aug-23
Page 20 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230720 Units:ug/L Analysis Date:20-Jul-2023 10:28
Run ID:VOA11_441822 SeqNo:7439640 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
48.56 50 0 97.1 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.86 50 0 91.7 77 - 1131.0Surr: 4-Bromofluorobenzene
49.8 50 0 99.6 73 - 1261.0Surr: Dibromofluoromethane
51.28 50 0 103 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 21 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230720 Units:ug/L Analysis Date:20-Jul-2023 09:46
Run ID:VOA11_441822 SeqNo:7439639 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.89 20 0 94.5 73 - 1211.0
1,2-Dibromoethane 17.19 20 0 86.0 76 - 1231.0
1,2-Dichloroethane 16.7 20 0 83.5 70 - 1241.0
2-Methylnaphthalene 15.22 20 0 76.1 55 - 1401.0
4-Isopropyltoluene 18.8 20 0 94.0 74 - 1261.0
Benzene 18.3 20 0 91.5 74 - 1201.0
Chloroform 18.88 20 0 94.4 71 - 1211.0
Ethylbenzene 18.52 20 0 92.6 77 - 1171.0
m,p-Xylene 37.54 40 0 93.9 77 - 1222.0
Methyl tert-butyl ether 15.44 20 0 77.2 70 - 1301.0
Methylene chloride 21.16 20 0 106 70 - 1272.0
Naphthalene 16.52 20 0 82.6 70 - 1301.0
o-Xylene 19.2 20 0 96.0 75 - 1191.0
Tert-butyl alcohol 293.5 400 0 73.4 70 - 13010
Toluene 17.51 20 0 87.6 77 - 1181.0
Xylenes, Total 56.75 60 0 94.6 75 - 1223.0
44.62 50 0 89.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.02 50 0 96.0 77 - 1131.0Surr: 4-Bromofluorobenzene
49.25 50 0 98.5 73 - 1261.0Surr: Dibromofluoromethane
49.36 50 0 98.7 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 22 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071014-01MS Units:ug/L Analysis Date:20-Jul-2023 11:31
Run ID:VOA11_441822 SeqNo:7439643 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 17.04 20 0 85.2 70 - 1251.0
1,2-Dibromoethane 13.88 20 0 69.4 70 - 124 S1.0
1,2-Dichloroethane 21.28 20 7.19 70.5 70 - 1271.0
2-Methylnaphthalene 17.4 20 4.153 66.2 55 - 1401.0
4-Isopropyltoluene 17.45 20 0 87.3 70 - 1301.0
Benzene 19.04 20 2.396 83.2 70 - 1271.0
Chloroform 16.55 20 0 82.7 70 - 1251.0
Ethylbenzene 16.66 20 0 83.3 70 - 1241.0
m,p-Xylene 33.2 40 0 83.0 70 - 1302.0
Methyl tert-butyl ether 13.81 20 0 69.0 70 - 130 S1.0
Methylene chloride 17.79 20 0 89.0 70 - 1282.0
Naphthalene 19.21 20 3.823 76.9 70 - 1301.0
o-Xylene 16.77 20 0 83.8 70 - 1241.0
Tert-butyl alcohol 234.8 400 0 58.7 70 - 130 S10
Toluene 15.96 20 0 79.8 70 - 1231.0
Xylenes, Total 49.96 60 0 83.3 70 - 1303.0
46.11 50 0 92.2 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.26 50 0 94.5 77 - 1131.0Surr: 4-Bromofluorobenzene
48.94 50 0 97.9 77 - 1231.0Surr: Dibromofluoromethane
48.78 50 0 97.6 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 23 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441822 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071014-01MSD Units:ug/L Analysis Date:20-Jul-2023 11:52
Run ID:VOA11_441822 SeqNo:7439644 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 19.33 20 0 96.6 70 - 125 17.04 12.6 201.0
1,2-Dibromoethane 16.63 20 0 83.1 70 - 124 13.88 18 201.0
1,2-Dichloroethane 24.06 20 7.19 84.4 70 - 127 21.28 12.3 201.0
2-Methylnaphthalene 20.41 20 4.153 81.3 55 - 140 17.4 15.9 201.0
4-Isopropyltoluene 18.84 20 0 94.2 70 - 130 17.45 7.66 201.0
Benzene 20.72 20 2.396 91.6 70 - 127 19.04 8.43 201.0
Chloroform 19.37 20 0 96.9 70 - 125 16.55 15.7 201.0
Ethylbenzene 19.99 20 0 99.9 70 - 124 16.66 18.2 201.0
m,p-Xylene 38.35 40 0 95.9 70 - 130 33.2 14.4 202.0
Methyl tert-butyl ether 16.26 20 0 81.3 70 - 130 13.81 16.3 201.0
Methylene chloride 20.63 20 0 103 70 - 128 17.79 14.8 202.0
Naphthalene 21.54 20 3.823 88.6 70 - 130 19.21 11.4 201.0
o-Xylene 20.15 20 0 101 70 - 124 16.77 18.3 201.0
Tert-butyl alcohol 324.9 400 0 81.2 70 - 130 234.8 32.2 20 R10
Toluene 18.16 20 0 90.8 70 - 123 15.96 12.9 201.0
Xylenes, Total 58.5 60 0 97.5 70 - 130 49.96 15.7 203.0
44.31 50 0 88.6 70 - 126 46.11 4 201.0Surr: 1,2-Dichloroethane-d4
49.8 50 0 99.6 77 - 113 47.26 5.23 201.0Surr: 4-Bromofluorobenzene
48.4 50 0 96.8 77 - 123 48.94 1.12 201.0Surr: Dibromofluoromethane
50.45 50 0 101 82 - 127 48.78 3.37 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071023-09
ALS Houston, US Date: 03-Aug-23
Page 24 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230720 Units:ug/L Analysis Date:20-Jul-2023 21:22
Run ID:VOA11_441888 SeqNo:7441300 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
49.7 50 0 99.4 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.15 50 0 94.3 77 - 1131.0Surr: 4-Bromofluorobenzene
51.74 50 0 103 73 - 1261.0Surr: Dibromofluoromethane
51.05 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 25 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230720 Units:ug/L Analysis Date:20-Jul-2023 20:39
Run ID:VOA11_441888 SeqNo:7441299 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.85 20 0 94.3 73 - 1211.0
1,2-Dibromoethane 16.69 20 0 83.4 76 - 1231.0
1,2-Dichloroethane 18.37 20 0 91.9 70 - 1241.0
2-Methylnaphthalene 15.38 20 0 76.9 55 - 1401.0
4-Isopropyltoluene 19.21 20 0 96.0 74 - 1261.0
Benzene 19.67 20 0 98.4 74 - 1201.0
Chloroform 19.17 20 0 95.9 71 - 1211.0
Ethylbenzene 19.46 20 0 97.3 77 - 1171.0
m,p-Xylene 39.54 40 0 98.8 77 - 1222.0
Methyl tert-butyl ether 16.6 20 0 83.0 70 - 1301.0
Methylene chloride 19.17 20 0 95.9 70 - 1272.0
Naphthalene 17.44 20 0 87.2 70 - 1301.0
o-Xylene 20.86 20 0 104 75 - 1191.0
Tert-butyl alcohol 322.5 400 0 80.6 70 - 13010
Toluene 19.02 20 0 95.1 77 - 1181.0
Xylenes, Total 60.4 60 0 101 75 - 1223.0
45.02 50 0 90.0 70 - 1231.0Surr: 1,2-Dichloroethane-d4
49.81 50 0 99.6 77 - 1131.0Surr: 4-Bromofluorobenzene
47.91 50 0 95.8 73 - 1261.0Surr: Dibromofluoromethane
49.98 50 0 100.0 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 26 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071017-06MS Units:ug/L Analysis Date:20-Jul-2023 22:04
Run ID:VOA11_441888 SeqNo:7441302 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 21.59 20 0 108 70 - 1251.0
1,2-Dibromoethane 19.33 20 0 96.6 70 - 1241.0
1,2-Dichloroethane 28.75 20 10.27 92.4 70 - 1271.0
2-Methylnaphthalene 17.71 20 0 88.6 55 - 1401.0
4-Isopropyltoluene 21.08 20 0 105 70 - 1301.0
Benzene 20.81 20 0 104 70 - 1271.0
Chloroform 20.27 20 0 101 70 - 1251.0
Ethylbenzene 20.95 20 0 105 70 - 1241.0
m,p-Xylene 44 40 0 110 70 - 1302.0
Methyl tert-butyl ether 58.33 20 44.28 70.2 70 - 1301.0
Methylene chloride 22.86 20 0 114 70 - 1282.0
Naphthalene 19.39 20 0 97.0 70 - 1301.0
o-Xylene 22.02 20 0 110 70 - 1241.0
Tert-butyl alcohol 4274 400 4174 25.1 70 - 130 SEO10
Toluene 20.18 20 0 101 70 - 1231.0
Xylenes, Total 66.02 60 0 110 70 - 1303.0
45.12 50 0 90.2 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.49 50 0 95.0 77 - 1131.0Surr: 4-Bromofluorobenzene
48.78 50 0 97.6 77 - 1231.0Surr: Dibromofluoromethane
49.94 50 0 99.9 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 27 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071017-06MSD Units:ug/L Analysis Date:20-Jul-2023 22:25
Run ID:VOA11_441888 SeqNo:7441303 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 20.18 20 0 101 70 - 125 21.59 6.72 201.0
1,2-Dibromoethane 18.57 20 0 92.8 70 - 124 19.33 4.01 201.0
1,2-Dichloroethane 29.6 20 10.27 96.7 70 - 127 28.75 2.92 201.0
2-Methylnaphthalene 18.29 20 0 91.4 55 - 140 17.71 3.2 201.0
4-Isopropyltoluene 20.24 20 0 101 70 - 130 21.08 4.04 201.0
Benzene 20.73 20 0 104 70 - 127 20.81 0.383 201.0
Chloroform 21.16 20 0 106 70 - 125 20.27 4.32 201.0
Ethylbenzene 19.76 20 0 98.8 70 - 124 20.95 5.83 201.0
m,p-Xylene 41.81 40 0 105 70 - 130 44 5.09 202.0
Methyl tert-butyl ether 60.84 20 44.28 82.8 70 - 130 58.33 4.22 201.0
Methylene chloride 21.69 20 0 108 70 - 128 22.86 5.22 202.0
Naphthalene 19.51 20 0 97.6 70 - 130 19.39 0.62 201.0
o-Xylene 21.6 20 0 108 70 - 124 22.02 1.96 201.0
Tert-butyl alcohol 4774 400 4174 150 70 - 130 4274 11 20 SEO10
Toluene 19.38 20 0 96.9 70 - 123 20.18 4.06 201.0
Xylenes, Total 63.41 60 0 106 70 - 130 66.02 4.04 203.0
46.43 50 0 92.9 70 - 126 45.12 2.86 201.0Surr: 1,2-Dichloroethane-d4
49.16 50 0 98.3 77 - 113 47.49 3.46 201.0Surr: 4-Bromofluorobenzene
49.36 50 0 98.7 77 - 123 48.78 1.17 201.0Surr: Dibromofluoromethane
48.82 50 0 97.6 82 - 127 49.94 2.26 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071023-01 HS23071023-02 HS23071023-03 HS23071023-04
HS23071023-05 HS23071023-06 HS23071023-07 HS23071023-08
ALS Houston, US Date: 03-Aug-23
Page 28 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R441813 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439509 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439508 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.241 0.25 0 96.4 80 - 1200.0500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439511 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.241 0.25 0.008 93.2 75 - 1250.0500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439510 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.242 0.25 0.008 93.6 75 - 125 0.241 0.414 200.0500
The following samples were analyzed in this batch:HS23071023-05 HS23071023-06 HS23071023-07
ALS Houston, US Date: 03-Aug-23
Page 29 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R442705 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 00:04
Run ID:ICS-Integrion_442705 SeqNo:7460135 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 00:10
Run ID:ICS-Integrion_442705 SeqNo:7460136 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.068 8 0 101 90 - 1100.200
Sample ID:HS23071018-09MS Units:mg/L Analysis Date:29-Jul-2023 02:00
Run ID:ICS-Integrion_442705 SeqNo:7460167 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)39.02 40 0 97.6 80 - 1202.00
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:29-Jul-2023 00:22
Run ID:ICS-Integrion_442705 SeqNo:7460138 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)38.78 40 0 97.0 80 - 1202.00
Sample ID:HS23071018-09MSD Units:mg/L Analysis Date:29-Jul-2023 02:06
Run ID:ICS-Integrion_442705 SeqNo:7460168 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)40.1 40 0 100 80 - 120 39.02 2.71 202.00
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:29-Jul-2023 00:27
Run ID:ICS-Integrion_442705 SeqNo:7460139 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)39.88 40 0 99.7 80 - 120 38.78 2.79 202.00
The following samples were analyzed in this batch:HS23071023-05 HS23071023-06 HS23071023-07
ALS Houston, US Date: 03-Aug-23
Page 30 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R442827 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:31-Jul-2023 21:16
Run ID:ICS-Integrion_442827 SeqNo:7463012 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:31-Jul-2023 21:27
Run ID:ICS-Integrion_442827 SeqNo:7463013 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.97 20 0 99.9 90 - 1100.500
Sample ID:HS23071023-05MS Units:mg/L Analysis Date:01-Aug-2023 00:27
Run ID:ICS-Integrion_442827 SeqNo:7463003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-E-I
Sulfate 38.1 10 31.05 70.5 80 - 120 S 0.500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:31-Jul-2023 21:39
Run ID:ICS-Integrion_442827 SeqNo:7463015 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 13.5 10 3.787 97.1 80 - 1200.500
Sample ID:HS23071023-05MSD Units:mg/L Analysis Date:01-Aug-2023 00:33
Run ID:ICS-Integrion_442827 SeqNo:7463004 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:MW-E-I
Sulfate 38.67 10 31.05 76.2 80 - 120 38.1 1.47 20 S 0.500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:31-Jul-2023 21:45
Run ID:ICS-Integrion_442827 SeqNo:7463016 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 13.36 10 3.787 95.8 80 - 120 13.5 1.02 200.500
The following samples were analyzed in this batch:HS23071023-05 HS23071023-06 HS23071023-07
ALS Houston, US Date: 03-Aug-23
Page 31 of 37
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071023
QC BATCH REPORT
Batch ID:R443018 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:MBLK-R443018 Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467806 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-R443018 Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467805 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)1005 1000 0 100 85 - 1155.00
Alkalinity, Total (As CaCO3)1008 1000 0 101 85 - 1155.00
Sample ID:LCSD-R443018 Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467837 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)997.3 1000 0 99.7 85 - 115 1005 0.724 205.00
Alkalinity, Total (As CaCO3)1001 1000 0 100 85 - 115 1008 0.682 205.00
Sample ID:HS23071020-04DUP Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467807 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)167.9 152 9.94 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)167.9 152 9.94 205.00
The following samples were analyzed in this batch:HS23071023-05 HS23071023-06 HS23071023-07
ALS Houston, US Date: 03-Aug-23
Page 32 of 37
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071023
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 03-Aug-23
Page 33 of 37
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
03-Aug-23Date: ALS Houston, US
Page 34 of 37
Nelson D. Dusara
19-Jul-2023 13:35Date/Time Received:HS23071023
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
2.9C/2.8C UC/C IR 31
49127
07/19/2023 16:00
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Ragen Giga
Date/TimeeSignatureDate/TimeeSignature
20-Jul-2023 08:0418-Jul-2023 12:54
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241113
ALS Houston, US 03-Aug-23Date:
Page 35 of 37
Page 36 of 37
Page 37 of 37
August 03, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 10 sample(s) on Jul 19, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071029
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 44
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071029
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071029-01 18-Jul-2023 09:20 19-Jul-2023 13:35PMW-M-I Groundwater
HS23071029-02 18-Jul-2023 09:45 19-Jul-2023 13:35PMW-M-D Groundwater
HS23071029-03 18-Jul-2023 10:10 19-Jul-2023 13:35PMW-M-B Groundwater
HS23071029-04 18-Jul-2023 11:00 19-Jul-2023 13:35SBMW-2R Groundwater
HS23071029-05 18-Jul-2023 11:25 19-Jul-2023 13:35SBMW-2D Groundwater
HS23071029-06 18-Jul-2023 12:02 19-Jul-2023 13:35SBMW-2I Groundwater
HS23071029-07 18-Jul-2023 12:45 19-Jul-2023 13:35SBMW-2B Groundwater
HS23071029-08 18-Jul-2023 13:15 19-Jul-2023 13:35SBMW-1R Groundwater
HS23071029-09 18-Jul-2023 14:55 19-Jul-2023 13:35Z4-X89 Groundwater
HS23071029-10 18-Jul-2023 00:00 19-Jul-2023 13:35Trip Blank Water
ALS Houston, US 03-Aug-23Date:
Page 2 of 44
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071029
ECD Organics by Method SW8011
Batch ID: 197845
Sample ID: MBLK-197845
The recovery of the Matrix Spike (MS) associated to this analyte was outside of the established control limits. However, the LCS was
within control limits. The recovery of the MS may be due to sample matrix interference.
•
Batch ID: 197847
Sample ID: MBLK-197847
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R442303
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R441923
Sample ID: HS23071018-01MS
MS and MSD are for an unrelated sample•
Batch ID: R441888
Sample ID: HS23071017-06MS
MS and MSD are for an unrelated sample•
Batch ID: R441939
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Metals by Method SW6020A
Batch ID: 198311
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R443018
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442963
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 3 of 44
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071029
WetChemistry by Method E300
Batch ID: R442706
Sample ID: SBMW-1R (HS23071029-08)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Z4-X89 (HS23071029-09)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Batch ID: R442705
Sample ID: SBMW-2B (HS23071029-07)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: SBMW-2I (HS23071029-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441813,R441819
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 4 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-M-I
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-01
18-Jul-2023 09:20 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 02:370.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 02:370.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 02:370.201,2-Dichloroethane 1.074
1ug/L 21-Jul-2023 02:371.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 02:370.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 02:370.20Benzene 1.0U
1ug/L 21-Jul-2023 02:370.20Chloroform 1.0U
1ug/L 21-Jul-2023 02:370.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 02:370.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 02:370.20Methyl tert-butyl ether 1.048
1ug/L 21-Jul-2023 02:371.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 02:370.30Naphthalene 1.0U
1ug/L 21-Jul-2023 02:370.30o-Xylene 1.0U
10ug/L 21-Jul-2023 13:46100Tert-butyl alcohol 1004,500
1ug/L 21-Jul-2023 02:370.20Toluene 1.0U
1ug/L 21-Jul-2023 02:370.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 02:3796.0 70-126
Surr: 1,2-Dichloroethane-d4 10%REC 21-Jul-2023 13:4695.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 02:3792.8 77-113
Surr: 4-Bromofluorobenzene 10%REC 21-Jul-2023 13:4696.1 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 02:3798.7 77-123
Surr: Dibromofluoromethane 10%REC 21-Jul-2023 13:4698.3 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 02:3798.0 82-127
Surr: Toluene-d8 10%REC 21-Jul-2023 13:4610182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 07:460.00321,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-M-D
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-02
18-Jul-2023 09:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 02:580.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 02:580.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 02:580.201,2-Dichloroethane 1.066
1ug/L 21-Jul-2023 02:581.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 02:580.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 02:580.20Benzene 1.0U
1ug/L 21-Jul-2023 02:580.20Chloroform 1.0U
1ug/L 21-Jul-2023 02:58J0.30Ethylbenzene 1.00.59
1ug/L 21-Jul-2023 02:58J0.50m,p-Xylene 2.00.98
1ug/L 21-Jul-2023 02:580.20Methyl tert-butyl ether 1.047
1ug/L 21-Jul-2023 02:581.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 02:580.30Naphthalene 1.0U
1ug/L 21-Jul-2023 02:580.30o-Xylene 1.0U
10ug/L 21-Jul-2023 14:29100Tert-butyl alcohol 1003,900
1ug/L 21-Jul-2023 02:580.20Toluene 1.0U
1ug/L 21-Jul-2023 02:58J0.30Xylenes, Total 3.00.98
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 02:5896.8 70-126
Surr: 1,2-Dichloroethane-d4 10%REC 21-Jul-2023 14:2995.6 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 02:5889.2 77-113
Surr: 4-Bromofluorobenzene 10%REC 21-Jul-2023 14:2996.1 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 02:5810177-123
Surr: Dibromofluoromethane 10%REC 21-Jul-2023 14:2997.4 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 02:5810182-127
Surr: Toluene-d8 10%REC 21-Jul-2023 14:2998.7 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 08:090.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-M-B
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-03
18-Jul-2023 10:10 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 03:190.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 03:190.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 03:190.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 03:191.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 03:190.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 03:190.20Benzene 1.0U
1ug/L 21-Jul-2023 03:190.20Chloroform 1.0U
1ug/L 21-Jul-2023 03:190.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 03:190.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 03:190.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 03:191.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 03:190.30Naphthalene 1.0U
1ug/L 21-Jul-2023 03:190.30o-Xylene 1.0U
1ug/L 21-Jul-2023 03:1910Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 03:190.20Toluene 1.0U
1ug/L 21-Jul-2023 03:190.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 03:1997.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 03:1988.8 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 03:1910177-123
Surr: Toluene-d8 1%REC 21-Jul-2023 03:1999.1 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 08:330.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
SBMW-2R
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-04
18-Jul-2023 11:00 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 03:400.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 03:400.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 03:400.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 03:401.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 03:400.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 03:400.20Benzene 1.0U
1ug/L 21-Jul-2023 03:400.20Chloroform 1.0U
1ug/L 21-Jul-2023 03:400.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 03:400.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 03:400.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 03:401.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 03:400.30Naphthalene 1.0U
1ug/L 21-Jul-2023 03:400.30o-Xylene 1.0U
1ug/L 21-Jul-2023 03:4010Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 03:400.20Toluene 1.0U
1ug/L 21-Jul-2023 03:400.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 03:4010170-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 03:4095.5 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 03:4010177-123
Surr: Toluene-d8 1%REC 21-Jul-2023 03:4098.6 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 08:560.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
SBMW-2D
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-05
18-Jul-2023 11:25 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
5ug/L 21-Jul-2023 04:011.51,2,4-Trimethylbenzene 5.0U
5ug/L 21-Jul-2023 04:011.01,2-Dibromoethane 5.0U
5ug/L 21-Jul-2023 04:011.01,2-Dichloroethane 5.0U
5ug/L 21-Jul-2023 04:015.02-Methylnaphthalene 5.0U
5ug/L 21-Jul-2023 04:011.54-Isopropyltoluene 5.0U
5ug/L 21-Jul-2023 04:011.0Benzene 5.08.5
5ug/L 21-Jul-2023 04:011.0Chloroform 5.0U
5ug/L 21-Jul-2023 04:011.5Ethylbenzene 5.0U
5ug/L 21-Jul-2023 04:012.5m,p-Xylene 10U
5ug/L 21-Jul-2023 04:011.0Methyl tert-butyl ether 5.0U
5ug/L 21-Jul-2023 04:015.0Methylene chloride 10U
5ug/L 21-Jul-2023 04:011.5Naphthalene 5.0U
5ug/L 21-Jul-2023 04:011.5o-Xylene 5.0U
5ug/L 21-Jul-2023 04:0150Tert-butyl alcohol 50U
5ug/L 21-Jul-2023 04:011.0Toluene 5.0U
5ug/L 21-Jul-2023 04:011.5Xylenes, Total 15U
Surr: 1,2-Dichloroethane-d4 5%REC 21-Jul-2023 04:0110170-126
Surr: 4-Bromofluorobenzene 5%REC 21-Jul-2023 04:0190.2 77-113
Surr: Dibromofluoromethane 5%REC 21-Jul-2023 04:0110377-123
Surr: Toluene-d8 5%REC 21-Jul-2023 04:0110082-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 09:200.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
SBMW-2I
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-06
18-Jul-2023 12:02 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 04:220.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 04:220.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 04:220.201,2-Dichloroethane 1.08.8
1ug/L 21-Jul-2023 04:221.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 04:220.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 04:22J0.20Benzene 1.00.49
1ug/L 21-Jul-2023 04:220.20Chloroform 1.0U
1ug/L 21-Jul-2023 04:220.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 04:220.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 04:220.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 04:221.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 04:220.30Naphthalene 1.0U
1ug/L 21-Jul-2023 04:220.30o-Xylene 1.0U
1ug/L 21-Jul-2023 04:2210Tert-butyl alcohol 10420
1ug/L 21-Jul-2023 04:220.20Toluene 1.0U
1ug/L 21-Jul-2023 04:220.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 04:2210270-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 04:2290.9 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 04:2298.7 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 04:2298.1 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
2ug/L 21-Jul-2023 18:070.214Methane 1.0058.9
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 09:430.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:500.0120Iron 0.2000.212
1mg/L 01-Aug-2023 14:500.000700Manganese 0.005000.191
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 08:290.200Sulfate 0.5005.73
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 03:210.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 01-Aug-2023 18:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00389
1mg/L 01-Aug-2023 18:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:25a5.00Alkalinity, Total (As CaCO3)5.00389
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05000.264
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
SBMW-2B
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-07
18-Jul-2023 12:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 04:430.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 04:430.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 04:430.201,2-Dichloroethane 1.018
1ug/L 21-Jul-2023 04:431.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 04:430.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 04:430.20Benzene 1.0U
1ug/L 21-Jul-2023 04:430.20Chloroform 1.0U
1ug/L 21-Jul-2023 04:430.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 04:430.50m,p-Xylene 2.0U
50ug/L 21-Jul-2023 14:0710Methyl tert-butyl ether 50250
1ug/L 21-Jul-2023 04:431.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 04:430.30Naphthalene 1.0U
1ug/L 21-Jul-2023 04:430.30o-Xylene 1.0U
50ug/L 21-Jul-2023 14:07500Tert-butyl alcohol 50015,000
1ug/L 21-Jul-2023 04:430.20Toluene 1.0U
1ug/L 21-Jul-2023 04:430.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 04:4398.6 70-126
Surr: 1,2-Dichloroethane-d4 50%REC 21-Jul-2023 14:0795.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 04:4392.6 77-113
Surr: 4-Bromofluorobenzene 50%REC 21-Jul-2023 14:0795.0 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 04:4310077-123
Surr: Dibromofluoromethane 50%REC 21-Jul-2023 14:0796.1 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 04:4310382-127
Surr: Toluene-d8 50%REC 21-Jul-2023 14:0799.5 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 17:330.107Methane 0.50032.8
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 10:070.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:52J0.0120Iron 0.2000.0721
1mg/L 01-Aug-2023 14:520.000700Manganese 0.005001.03
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 08:460.200Sulfate 0.5001.21
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 03:260.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
SBMW-2B
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-07
18-Jul-2023 12:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 01-Aug-2023 18:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00367
1mg/L 01-Aug-2023 18:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:25a5.00Alkalinity, Total (As CaCO3)5.00367
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 20-Jul-2023 10:020.0200Ferrous Iron 0.05000.135
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
SBMW-1R
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-08
18-Jul-2023 13:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 18:210.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 18:210.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 18:210.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 18:211.02-Methylnaphthalene 1.014
1ug/L 21-Jul-2023 18:210.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 18:210.20Benzene 1.038
1ug/L 21-Jul-2023 18:210.20Chloroform 1.0U
1ug/L 21-Jul-2023 18:210.30Ethylbenzene 1.01.8
1ug/L 21-Jul-2023 18:210.50m,p-Xylene 2.02.6
1ug/L 21-Jul-2023 18:210.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 18:211.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 18:210.30Naphthalene 1.026
1ug/L 21-Jul-2023 18:210.30o-Xylene 1.0U
1ug/L 21-Jul-2023 18:2110Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 18:21J0.20Toluene 1.00.38
1ug/L 21-Jul-2023 18:21J0.30Xylenes, Total 3.02.6
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 18:2193.7 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 18:2196.2 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 18:2197.8 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 18:2110082-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
50ug/L 21-Jul-2023 18:275.35Methane 25.01,200
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 10:300.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:540.0120Iron 0.2008.75
100mg/L 01-Aug-2023 16:480.0700Manganese 0.5009.95
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 08:520.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 03:320.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 01-Aug-2023 18:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00567
1mg/L 01-Aug-2023 18:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:25a5.00Alkalinity, Total (As CaCO3)5.00567
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
50mg/L 20-Jul-2023 11:151.00Ferrous Iron 2.507.45
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-X89
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-09
18-Jul-2023 14:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 14:090.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 14:090.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 14:090.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 14:091.02-Methylnaphthalene 1.04.9
1ug/L 21-Jul-2023 14:090.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 14:09J0.20Benzene 1.00.59
1ug/L 21-Jul-2023 14:090.20Chloroform 1.0U
1ug/L 21-Jul-2023 14:090.30Ethylbenzene 1.01.1
1ug/L 21-Jul-2023 14:090.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 14:090.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 14:091.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 14:090.30Naphthalene 1.04.0
1ug/L 21-Jul-2023 14:090.30o-Xylene 1.0U
1ug/L 21-Jul-2023 14:0910Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 14:09J0.20Toluene 1.00.68
1ug/L 21-Jul-2023 14:090.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 14:0910270-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 14:0994.9 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 14:0910677-123
Surr: Toluene-d8 1%REC 21-Jul-2023 14:0999.6 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
50ug/L 21-Jul-2023 18:355.35Methane 25.01,890
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 12:050.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 31-Jul-2023
1mg/L 01-Aug-2023 14:560.0120Iron 0.20014.6
100mg/L 01-Aug-2023 16:500.0700Manganese 0.50010.1
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 08:580.200Sulfate 0.5000.785
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 03:380.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 01-Aug-2023 18:255.00Alkalinity, Bicarbonate (As
CaCO3)5.00260
1mg/L 01-Aug-2023 18:255.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:255.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 01-Aug-2023 18:25a5.00Alkalinity, Total (As CaCO3)5.00260
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
100mg/L 20-Jul-2023 11:152.00Ferrous Iron 5.0015.1
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 44
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071029
HS23071029-10
18-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 13:480.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 13:480.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 13:480.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 13:481.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 13:480.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 13:480.20Benzene 1.0U
1ug/L 21-Jul-2023 13:480.20Chloroform 1.0U
1ug/L 21-Jul-2023 13:480.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 13:480.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 13:480.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 13:481.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 13:480.30Naphthalene 1.0U
1ug/L 21-Jul-2023 13:480.30o-Xylene 1.0U
1ug/L 21-Jul-2023 13:4810Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 13:480.20Toluene 1.0U
1ug/L 21-Jul-2023 13:480.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 13:4810470-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 13:4890.4 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 13:4811077-123
Surr: Toluene-d8 1%REC 21-Jul-2023 13:4897.4 82-127
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of 44
Weight / Prep Log
HS23071029
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197845
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:48 End Date: 21 Jul 2023 09:48
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071029-01 35 (mL)40 mL VOA w/ HCL36.79 (mL)1.051
HS23071029-02 35 (mL)40 mL VOA w/ HCL36.23 (mL)1.035
HS23071029-03 35 (mL)40 mL VOA w/ HCL36.43 (mL)1.041
HS23071029-04 35 (mL)40 mL VOA w/ HCL36.56 (mL)1.045
HS23071029-05 35 (mL)40 mL VOA w/ HCL36.71 (mL)1.049
HS23071029-06 35 (mL)40 mL VOA w/ HCL36.65 (mL)1.047
Batch ID:197847
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:56 End Date: 21 Jul 2023 09:56
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071029-07 35 (mL)40 mL VOA w/ HCL36.71 (mL)1.049
HS23071029-08 35 (mL)40 mL VOA w/ HCL36.21 (mL)1.035
HS23071029-09 35 (mL)40 mL VOA w/ HCL36.39 (mL)1.04
Batch ID:198311
Method:WATER - SW3010A 3010APrep Code:
Start Date: 31 Jul 2023 11:00 End Date: 31 Jul 2023 11:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071029-06 10 (mL)120 plastic HNO310 (mL)1
HS23071029-07 10 (mL)120 plastic HNO310 (mL)1
HS23071029-08 10 (mL)120 plastic HNO310 (mL)1
HS23071029-09 10 (mL)120 plastic HNO310 (mL)1
03-Aug-23Date: ALS Houston, US
Page 16 of 44
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071029
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197845 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:48 25 Jul 2023 07:46HS23071029-01 18 Jul 2023 09:20 1PMW-M-I
21 Jul 2023 09:48 25 Jul 2023 08:09HS23071029-02 18 Jul 2023 09:45 1PMW-M-D
21 Jul 2023 09:48 25 Jul 2023 08:33HS23071029-03 18 Jul 2023 10:10 1PMW-M-B
21 Jul 2023 09:48 25 Jul 2023 08:56HS23071029-04 18 Jul 2023 11:00 1SBMW-2R
21 Jul 2023 09:48 25 Jul 2023 09:20HS23071029-05 18 Jul 2023 11:25 1SBMW-2D
21 Jul 2023 09:48 25 Jul 2023 09:43HS23071029-06 18 Jul 2023 12:02 1SBMW-2I
Batch ID:197847 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:56 25 Jul 2023 10:07HS23071029-07 18 Jul 2023 12:45 1SBMW-2B
21 Jul 2023 09:56 25 Jul 2023 10:30HS23071029-08 18 Jul 2023 13:15 1SBMW-1R
21 Jul 2023 09:56 25 Jul 2023 12:05HS23071029-09 18 Jul 2023 14:55 1Z4-X89
Batch ID:198311 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
31 Jul 2023 11:00 01 Aug 2023 14:50HS23071029-06 18 Jul 2023 12:02 1SBMW-2I
31 Jul 2023 11:00 01 Aug 2023 14:52HS23071029-07 18 Jul 2023 12:45 1SBMW-2B
31 Jul 2023 11:00 01 Aug 2023 16:48HS23071029-08 18 Jul 2023 13:15 100SBMW-1R
31 Jul 2023 11:00 01 Aug 2023 14:54HS23071029-08 18 Jul 2023 13:15 1SBMW-1R
31 Jul 2023 11:00 01 Aug 2023 16:50HS23071029-09 18 Jul 2023 14:55 100Z4-X89
31 Jul 2023 11:00 01 Aug 2023 14:56HS23071029-09 18 Jul 2023 14:55 1Z4-X89
Batch ID:R441813 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
20 Jul 2023 10:02HS23071029-06 18 Jul 2023 12:02 1SBMW-2I
20 Jul 2023 10:02HS23071029-07 18 Jul 2023 12:45 1SBMW-2B
Batch ID:R441819 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
20 Jul 2023 11:15HS23071029-08 18 Jul 2023 13:15 50SBMW-1R
20 Jul 2023 11:15HS23071029-09 18 Jul 2023 14:55 100Z4-X89
Batch ID:R441888 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 02:37HS23071029-01 18 Jul 2023 09:20 1PMW-M-I
21 Jul 2023 02:58HS23071029-02 18 Jul 2023 09:45 1PMW-M-D
21 Jul 2023 03:19HS23071029-03 18 Jul 2023 10:10 1PMW-M-B
21 Jul 2023 03:40HS23071029-04 18 Jul 2023 11:00 1SBMW-2R
21 Jul 2023 04:01HS23071029-05 18 Jul 2023 11:25 5SBMW-2D
21 Jul 2023 04:22HS23071029-06 18 Jul 2023 12:02 1SBMW-2I
21 Jul 2023 04:43HS23071029-07 18 Jul 2023 12:45 1SBMW-2B
Batch ID:R441923 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
21 Jul 2023 13:48HS23071029-10 18 Jul 2023 00:00 1Trip Blank
Batch ID:R441923 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 18:21HS23071029-08 18 Jul 2023 13:15 1SBMW-1R
21 Jul 2023 14:09HS23071029-09 18 Jul 2023 14:55 1Z4-X89
03-Aug-23Date: ALS Houston, US
Page 17 of 44
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071029
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R441939 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 13:46HS23071029-01 18 Jul 2023 09:20 10PMW-M-I
21 Jul 2023 14:29HS23071029-02 18 Jul 2023 09:45 10PMW-M-D
21 Jul 2023 14:07HS23071029-07 18 Jul 2023 12:45 50SBMW-2B
Batch ID:R442303 ( 1 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
21 Jul 2023 18:07HS23071029-06 18 Jul 2023 12:02 2SBMW-2I
21 Jul 2023 17:33HS23071029-07 18 Jul 2023 12:45 1SBMW-2B
21 Jul 2023 18:27HS23071029-08 18 Jul 2023 13:15 50SBMW-1R
21 Jul 2023 18:35HS23071029-09 18 Jul 2023 14:55 50Z4-X89
Batch ID:R442705 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
29 Jul 2023 03:21HS23071029-06 18 Jul 2023 12:02 10SBMW-2I
29 Jul 2023 03:26HS23071029-07 18 Jul 2023 12:45 10SBMW-2B
Batch ID:R442706 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
29 Jul 2023 03:32HS23071029-08 18 Jul 2023 13:15 10SBMW-1R
29 Jul 2023 03:38HS23071029-09 18 Jul 2023 14:55 10Z4-X89
Batch ID:R442963 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
01 Aug 2023 08:29HS23071029-06 18 Jul 2023 12:02 1SBMW-2I
01 Aug 2023 08:46HS23071029-07 18 Jul 2023 12:45 1SBMW-2B
01 Aug 2023 08:52HS23071029-08 18 Jul 2023 13:15 1SBMW-1R
01 Aug 2023 08:58HS23071029-09 18 Jul 2023 14:55 1Z4-X89
Batch ID:R443018 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
01 Aug 2023 18:25HS23071029-06 18 Jul 2023 12:02 1SBMW-2I
01 Aug 2023 18:25HS23071029-07 18 Jul 2023 12:45 1SBMW-2B
01 Aug 2023 18:25HS23071029-08 18 Jul 2023 13:15 1SBMW-1R
01 Aug 2023 18:25HS23071029-09 18 Jul 2023 14:55 1Z4-X89
03-Aug-23Date: ALS Houston, US
Page 18 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:197845 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197845 Units:ug/L Analysis Date:24-Jul-2023 21:57
Run ID:ECD_13_442224 SeqNo:7448808 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197845 Units:ug/L Analysis Date:24-Jul-2023 22:21
Run ID:ECD_13_442224 SeqNo:7448809 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1917 0.25 0 76.7 60 - 1400.020
Sample ID:LCSD-197845 Units:ug/L Analysis Date:24-Jul-2023 22:44
Run ID:ECD_13_442224 SeqNo:7448810 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1835 0.25 0 73.4 60 - 140 0.1917 4.39 200.020
The following samples were analyzed in this batch:HS23071029-01 HS23071029-02 HS23071029-03 HS23071029-04
HS23071029-05 HS23071029-06
ALS Houston, US Date: 03-Aug-23
Page 19 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:197847 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197847 Units:ug/L Analysis Date:25-Jul-2023 00:42
Run ID:ECD_13_442418 SeqNo:7453266 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197847 Units:ug/L Analysis Date:25-Jul-2023 01:06
Run ID:ECD_13_442418 SeqNo:7453267 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1954 0.25 0 78.2 60 - 1400.020
Sample ID:LCSD-197847 Units:ug/L Analysis Date:25-Jul-2023 01:29
Run ID:ECD_13_442418 SeqNo:7453268 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1962 0.25 0 78.5 60 - 140 0.1954 0.406 200.020
The following samples were analyzed in this batch:HS23071029-07 HS23071029-08 HS23071029-09
ALS Houston, US Date: 03-Aug-23
Page 20 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R442303 ( 1 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230721 Units:ug/L Analysis Date:21-Jul-2023 14:22
Run ID:FID-4_442303 SeqNo:7450742 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230721 Units:ug/L Analysis Date:21-Jul-2023 14:32
Run ID:FID-4_442303 SeqNo:7450743 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.86 9.647 0 81.5 75 - 1250.500
Sample ID:LCSD-230721 Units:ug/L Analysis Date:21-Jul-2023 14:47
Run ID:FID-4_442303 SeqNo:7450744 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 8.056 9.647 0 83.5 75 - 125 7.86 2.47 300.500
Sample ID:HS23071069-04DUP Units:ug/L Analysis Date:21-Jul-2023 19:32
Run ID:FID-4_442303 SeqNo:7450769 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Methane 15.63 15.58 0.335 300.500
The following samples were analyzed in this batch:HS23071029-06 HS23071029-07 HS23071029-08 HS23071029-09
ALS Houston, US Date: 03-Aug-23
Page 21 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:198311 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198311 Units:mg/L Analysis Date:01-Aug-2023 13:49
Run ID:ICPMS06_442867 SeqNo:7464813 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese 0.000794 J 0.00500
Sample ID:LCS-198311 Units:mg/L Analysis Date:01-Aug-2023 13:52
Run ID:ICPMS06_442867 SeqNo:7464814 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.563 5 0 91.3 80 - 1200.200
Manganese 0.04482 0.05 0 89.6 80 - 1200.00500
Sample ID:HS23070892-01MS Units:mg/L Analysis Date:01-Aug-2023 13:59
Run ID:ICPMS06_442867 SeqNo:7464817 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.048 5 0.02657 100 80 - 1200.200
Manganese 0.1484 0.05 0.09528 106 80 - 1200.00500
Sample ID:HS23070892-01MSD Units:mg/L Analysis Date:01-Aug-2023 14:01
Run ID:ICPMS06_442867 SeqNo:7464818 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.293 5 0.02657 105 80 - 120 5.048 4.74 200.200
Manganese 0.1545 0.05 0.09528 118 80 - 120 0.1484 4.01 200.00500
Sample ID:HS23070892-01PDS Units:mg/L Analysis Date:01-Aug-2023 14:03
Run ID:ICPMS06_442867 SeqNo:7464819 PrepDate:31-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 10.48 10 0.02657 104 75 - 1250.200
Manganese 0.2032 0.1 0.09528 108 75 - 1250.00500
ALS Houston, US Date: 03-Aug-23
Page 22 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:198311 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23070892-01SD Units:mg/L Analysis Date:01-Aug-2023 13:57
Run ID:ICPMS06_442867 SeqNo:7464816 PrepDate:31-Jul-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron U 0.02657 0 101.00
Manganese 0.09742 0.09528 2.25 100.0250
The following samples were analyzed in this batch:HS23071029-06 HS23071029-07 HS23071029-08 HS23071029-09
ALS Houston, US Date: 03-Aug-23
Page 23 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230720 Units:ug/L Analysis Date:20-Jul-2023 21:22
Run ID:VOA11_441888 SeqNo:7441300 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
49.7 50 0 99.4 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.15 50 0 94.3 77 - 1131.0Surr: 4-Bromofluorobenzene
51.74 50 0 103 73 - 1261.0Surr: Dibromofluoromethane
51.05 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 24 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230720 Units:ug/L Analysis Date:20-Jul-2023 20:39
Run ID:VOA11_441888 SeqNo:7441299 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.85 20 0 94.3 73 - 1211.0
1,2-Dibromoethane 16.69 20 0 83.4 76 - 1231.0
1,2-Dichloroethane 18.37 20 0 91.9 70 - 1241.0
2-Methylnaphthalene 15.38 20 0 76.9 55 - 1401.0
4-Isopropyltoluene 19.21 20 0 96.0 74 - 1261.0
Benzene 19.67 20 0 98.4 74 - 1201.0
Chloroform 19.17 20 0 95.9 71 - 1211.0
Ethylbenzene 19.46 20 0 97.3 77 - 1171.0
m,p-Xylene 39.54 40 0 98.8 77 - 1222.0
Methyl tert-butyl ether 16.6 20 0 83.0 70 - 1301.0
Methylene chloride 19.17 20 0 95.9 70 - 1272.0
Naphthalene 17.44 20 0 87.2 70 - 1301.0
o-Xylene 20.86 20 0 104 75 - 1191.0
Tert-butyl alcohol 322.5 400 0 80.6 70 - 13010
Toluene 19.02 20 0 95.1 77 - 1181.0
Xylenes, Total 60.4 60 0 101 75 - 1223.0
45.02 50 0 90.0 70 - 1231.0Surr: 1,2-Dichloroethane-d4
49.81 50 0 99.6 77 - 1131.0Surr: 4-Bromofluorobenzene
47.91 50 0 95.8 73 - 1261.0Surr: Dibromofluoromethane
49.98 50 0 100.0 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 25 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071017-06MS Units:ug/L Analysis Date:20-Jul-2023 22:04
Run ID:VOA11_441888 SeqNo:7441302 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 21.59 20 0 108 70 - 1251.0
1,2-Dibromoethane 19.33 20 0 96.6 70 - 1241.0
1,2-Dichloroethane 28.75 20 10.27 92.4 70 - 1271.0
2-Methylnaphthalene 17.71 20 0 88.6 55 - 1401.0
4-Isopropyltoluene 21.08 20 0 105 70 - 1301.0
Benzene 20.81 20 0 104 70 - 1271.0
Chloroform 20.27 20 0 101 70 - 1251.0
Ethylbenzene 20.95 20 0 105 70 - 1241.0
m,p-Xylene 44 40 0 110 70 - 1302.0
Methyl tert-butyl ether 58.33 20 44.28 70.2 70 - 1301.0
Methylene chloride 22.86 20 0 114 70 - 1282.0
Naphthalene 19.39 20 0 97.0 70 - 1301.0
o-Xylene 22.02 20 0 110 70 - 1241.0
Tert-butyl alcohol 4274 400 4174 25.1 70 - 130 SEO10
Toluene 20.18 20 0 101 70 - 1231.0
Xylenes, Total 66.02 60 0 110 70 - 1303.0
45.12 50 0 90.2 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.49 50 0 95.0 77 - 1131.0Surr: 4-Bromofluorobenzene
48.78 50 0 97.6 77 - 1231.0Surr: Dibromofluoromethane
49.94 50 0 99.9 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 26 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441888 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071017-06MSD Units:ug/L Analysis Date:20-Jul-2023 22:25
Run ID:VOA11_441888 SeqNo:7441303 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 20.18 20 0 101 70 - 125 21.59 6.72 201.0
1,2-Dibromoethane 18.57 20 0 92.8 70 - 124 19.33 4.01 201.0
1,2-Dichloroethane 29.6 20 10.27 96.7 70 - 127 28.75 2.92 201.0
2-Methylnaphthalene 18.29 20 0 91.4 55 - 140 17.71 3.2 201.0
4-Isopropyltoluene 20.24 20 0 101 70 - 130 21.08 4.04 201.0
Benzene 20.73 20 0 104 70 - 127 20.81 0.383 201.0
Chloroform 21.16 20 0 106 70 - 125 20.27 4.32 201.0
Ethylbenzene 19.76 20 0 98.8 70 - 124 20.95 5.83 201.0
m,p-Xylene 41.81 40 0 105 70 - 130 44 5.09 202.0
Methyl tert-butyl ether 60.84 20 44.28 82.8 70 - 130 58.33 4.22 201.0
Methylene chloride 21.69 20 0 108 70 - 128 22.86 5.22 202.0
Naphthalene 19.51 20 0 97.6 70 - 130 19.39 0.62 201.0
o-Xylene 21.6 20 0 108 70 - 124 22.02 1.96 201.0
Tert-butyl alcohol 4774 400 4174 150 70 - 130 4274 11 20 SEO10
Toluene 19.38 20 0 96.9 70 - 123 20.18 4.06 201.0
Xylenes, Total 63.41 60 0 106 70 - 130 66.02 4.04 203.0
46.43 50 0 92.9 70 - 126 45.12 2.86 201.0Surr: 1,2-Dichloroethane-d4
49.16 50 0 98.3 77 - 113 47.49 3.46 201.0Surr: 4-Bromofluorobenzene
49.36 50 0 98.7 77 - 123 48.78 1.17 201.0Surr: Dibromofluoromethane
48.82 50 0 97.6 82 - 127 49.94 2.26 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071029-01 HS23071029-02 HS23071029-03 HS23071029-04
HS23071029-05 HS23071029-06 HS23071029-07
ALS Houston, US Date: 03-Aug-23
Page 27 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 10:39
Run ID:VOA11_441923 SeqNo:7441986 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
48.67 50 0 97.3 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.77 50 0 91.5 77 - 1131.0Surr: 4-Bromofluorobenzene
52.19 50 0 104 73 - 1261.0Surr: Dibromofluoromethane
50.07 50 0 100 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 28 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 09:57
Run ID:VOA11_441923 SeqNo:7441985 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 19.18 20 0 95.9 73 - 1211.0
1,2-Dibromoethane 17.67 20 0 88.3 76 - 1231.0
1,2-Dichloroethane 17.63 20 0 88.2 70 - 1241.0
2-Methylnaphthalene 15.83 20 0 79.2 55 - 1401.0
4-Isopropyltoluene 19.51 20 0 97.6 74 - 1261.0
Benzene 18.81 20 0 94.0 74 - 1201.0
Chloroform 19.9 20 0 99.5 71 - 1211.0
Ethylbenzene 20.17 20 0 101 77 - 1171.0
m,p-Xylene 38.64 40 0 96.6 77 - 1222.0
Methyl tert-butyl ether 15.97 20 0 79.8 70 - 1301.0
Methylene chloride 20.48 20 0 102 70 - 1272.0
Naphthalene 17.38 20 0 86.9 70 - 1301.0
o-Xylene 20.04 20 0 100 75 - 1191.0
Tert-butyl alcohol 327.3 400 0 81.8 70 - 13010
Toluene 17.8 20 0 89.0 77 - 1181.0
Xylenes, Total 58.68 60 0 97.8 75 - 1223.0
45.12 50 0 90.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.21 50 0 94.4 77 - 1131.0Surr: 4-Bromofluorobenzene
50.13 50 0 100 73 - 1261.0Surr: Dibromofluoromethane
48.96 50 0 97.9 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 29 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071018-01MS Units:ug/L Analysis Date:21-Jul-2023 11:21
Run ID:VOA11_441923 SeqNo:7441988 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 17.95 20 0 89.7 70 - 1251.0
1,2-Dibromoethane 16.3 20 0 81.5 70 - 1241.0
1,2-Dichloroethane 16.58 20 0 82.9 70 - 1271.0
2-Methylnaphthalene 14.77 20 0 73.9 55 - 1401.0
4-Isopropyltoluene 18.13 20 0 90.6 70 - 1301.0
Benzene 17.83 20 0 89.1 70 - 1271.0
Chloroform 17.92 20 0 89.6 70 - 1251.0
Ethylbenzene 17.93 20 0 89.7 70 - 1241.0
m,p-Xylene 36.54 40 0 91.3 70 - 1302.0
Methyl tert-butyl ether 14.39 20 0 72.0 70 - 1301.0
Methylene chloride 18.88 20 0 94.4 70 - 1282.0
Naphthalene 16.23 20 0 81.1 70 - 1301.0
o-Xylene 18 20 0 90.0 70 - 1241.0
Tert-butyl alcohol 274.5 400 0 68.6 70 - 130 S10
Toluene 17.38 20 0 86.9 70 - 1231.0
Xylenes, Total 54.54 60 0 90.9 70 - 1303.0
46.03 50 0 92.1 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.95 50 0 95.9 77 - 1131.0Surr: 4-Bromofluorobenzene
48.45 50 0 96.9 77 - 1231.0Surr: Dibromofluoromethane
49.45 50 0 98.9 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 30 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441923 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071018-01MSD Units:ug/L Analysis Date:21-Jul-2023 11:42
Run ID:VOA11_441923 SeqNo:7441989 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 16.5 20 0 82.5 70 - 125 17.95 8.4 201.0
1,2-Dibromoethane 15.15 20 0 75.8 70 - 124 16.3 7.29 201.0
1,2-Dichloroethane 14.99 20 0 74.9 70 - 127 16.58 10.1 201.0
2-Methylnaphthalene 15.61 20 0 78.0 55 - 140 14.77 5.48 201.0
4-Isopropyltoluene 16.91 20 0 84.6 70 - 130 18.13 6.94 201.0
Benzene 16.46 20 0 82.3 70 - 127 17.83 7.98 201.0
Chloroform 16.73 20 0 83.7 70 - 125 17.92 6.87 201.0
Ethylbenzene 16.47 20 0 82.4 70 - 124 17.93 8.48 201.0
m,p-Xylene 33.7 40 0 84.3 70 - 130 36.54 8.07 202.0
Methyl tert-butyl ether 14.33 20 0 71.7 70 - 130 14.39 0.403 201.0
Methylene chloride 17.96 20 0 89.8 70 - 128 18.88 5.01 202.0
Naphthalene 15.8 20 0 79.0 70 - 130 16.23 2.66 201.0
o-Xylene 16.44 20 0 82.2 70 - 124 18 9.05 201.0
Tert-butyl alcohol 264.7 400 0 66.2 70 - 130 274.5 3.62 20 S10
Toluene 16.1 20 0 80.5 70 - 123 17.38 7.67 201.0
Xylenes, Total 50.15 60 0 83.6 70 - 130 54.54 8.39 203.0
46.07 50 0 92.1 70 - 126 46.03 0.0777 201.0Surr: 1,2-Dichloroethane-d4
48.18 50 0 96.4 77 - 113 47.95 0.479 201.0Surr: 4-Bromofluorobenzene
48.66 50 0 97.3 77 - 123 48.45 0.431 201.0Surr: Dibromofluoromethane
49.15 50 0 98.3 82 - 127 49.45 0.619 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071029-08 HS23071029-09 HS23071029-10
ALS Houston, US Date: 03-Aug-23
Page 31 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441939 ( 0 )Instrument:VOA7 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 10:27
Run ID:VOA7_441939 SeqNo:7442286 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methyl tert-butyl ether U 1.0
Tert-butyl alcohol U 10
47.73 50 0 95.5 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.75 50 0 95.5 77 - 1131.0Surr: 4-Bromofluorobenzene
49.39 50 0 98.8 73 - 1261.0Surr: Dibromofluoromethane
50.17 50 0 100 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 09:44
Run ID:VOA7_441939 SeqNo:7442285 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methyl tert-butyl ether 18.71 20 0 93.6 70 - 1301.0
Tert-butyl alcohol 286.6 400 0 71.6 70 - 13010
47.9 50 0 95.8 70 - 1231.0Surr: 1,2-Dichloroethane-d4
49.4 50 0 98.8 77 - 1131.0Surr: 4-Bromofluorobenzene
49.23 50 0 98.5 73 - 1261.0Surr: Dibromofluoromethane
50.12 50 0 100 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23071095-02MS Units:ug/L Analysis Date:21-Jul-2023 11:59
Run ID:VOA7_441939 SeqNo:7442290 PrepDate:DF:100
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Methyl tert-butyl ether 1808 2000 0 90.4 70 - 130100
Tert-butyl alcohol 33100 40000 0 82.8 70 - 1301000
4937 5000 0 98.7 70 - 126100Surr: 1,2-Dichloroethane-d4
4915 5000 0 98.3 77 - 113100Surr: 4-Bromofluorobenzene
4937 5000 0 98.7 77 - 123100Surr: Dibromofluoromethane
5030 5000 0 101 82 - 127100Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 32 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441939 ( 0 )Instrument:VOA7 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071095-02MSD Units:ug/L Analysis Date:21-Jul-2023 12:20
Run ID:VOA7_441939 SeqNo:7442291 PrepDate:DF:100
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Methyl tert-butyl ether 1698 2000 0 84.9 70 - 130 1808 6.26 20100
Tert-butyl alcohol 31000 40000 0 77.5 70 - 130 33100 6.57 201000
4838 5000 0 96.8 70 - 126 4937 2.02 20100Surr: 1,2-Dichloroethane-d4
4902 5000 0 98.0 77 - 113 4915 0.266 20100Surr: 4-Bromofluorobenzene
4919 5000 0 98.4 77 - 123 4937 0.367 20100Surr: Dibromofluoromethane
4971 5000 0 99.4 82 - 127 5030 1.18 20100Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071029-01 HS23071029-02 HS23071029-07
ALS Houston, US Date: 03-Aug-23
Page 33 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441813 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439509 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441813 Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439508 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.241 0.25 0 96.4 80 - 1200.0500
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439511 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.241 0.25 0.008 93.2 75 - 1250.0500
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:20-Jul-2023 10:02
Run ID:UV-2450_441813 SeqNo:7439510 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.242 0.25 0.008 93.6 75 - 125 0.241 0.414 200.0500
The following samples were analyzed in this batch:HS23071029-06 HS23071029-07
ALS Houston, US Date: 03-Aug-23
Page 34 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R441819 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441819 Units:mg/L Analysis Date:20-Jul-2023 11:15
Run ID:UV-2450_441819 SeqNo:7439573 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441819 Units:mg/L Analysis Date:20-Jul-2023 11:15
Run ID:UV-2450_441819 SeqNo:7439572 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.229 0.25 0 91.6 80 - 1200.0500
Sample ID:HS23071038-18MS Units:mg/L Analysis Date:20-Jul-2023 11:15
Run ID:UV-2450_441819 SeqNo:7439575 PrepDate:DF:250
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 94.5 62.5 32.75 98.8 75 - 12512.5
Sample ID:HS23071038-18MSD Units:mg/L Analysis Date:20-Jul-2023 11:15
Run ID:UV-2450_441819 SeqNo:7439574 PrepDate:DF:250
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 95.5 62.5 32.75 100 75 - 125 94.5 1.05 2012.5
The following samples were analyzed in this batch:HS23071029-08 HS23071029-09
ALS Houston, US Date: 03-Aug-23
Page 35 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R442705 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 00:04
Run ID:ICS-Integrion_442705 SeqNo:7460135 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 00:10
Run ID:ICS-Integrion_442705 SeqNo:7460136 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.068 8 0 101 90 - 1100.200
Sample ID:HS23071018-09MS Units:mg/L Analysis Date:29-Jul-2023 02:00
Run ID:ICS-Integrion_442705 SeqNo:7460167 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)39.02 40 0 97.6 80 - 1202.00
Sample ID:HS23071014-06MS Units:mg/L Analysis Date:29-Jul-2023 00:22
Run ID:ICS-Integrion_442705 SeqNo:7460138 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)38.78 40 0 97.0 80 - 1202.00
Sample ID:HS23071018-09MSD Units:mg/L Analysis Date:29-Jul-2023 02:06
Run ID:ICS-Integrion_442705 SeqNo:7460168 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)40.1 40 0 100 80 - 120 39.02 2.71 202.00
Sample ID:HS23071014-06MSD Units:mg/L Analysis Date:29-Jul-2023 00:27
Run ID:ICS-Integrion_442705 SeqNo:7460139 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)39.88 40 0 99.7 80 - 120 38.78 2.79 202.00
The following samples were analyzed in this batch:HS23071029-06 HS23071029-07
ALS Houston, US Date: 03-Aug-23
Page 36 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R442706 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 04:19
Run ID:ICS-Integrion_442706 SeqNo:7460175 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 04:24
Run ID:ICS-Integrion_442706 SeqNo:7460176 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)7.902 8 0 98.8 90 - 1100.200
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:29-Jul-2023 05:51
Run ID:ICS-Integrion_442706 SeqNo:7460188 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.68 40 0 94.2 80 - 1202.00
Sample ID:HS23071063-01MS Units:mg/L Analysis Date:29-Jul-2023 04:36
Run ID:ICS-Integrion_442706 SeqNo:7460178 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.84 40 0 94.6 80 - 1202.00
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:29-Jul-2023 05:57
Run ID:ICS-Integrion_442706 SeqNo:7460189 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.69 40 0 96.7 80 - 120 37.68 2.64 202.00
Sample ID:HS23071063-01MSD Units:mg/L Analysis Date:29-Jul-2023 04:42
Run ID:ICS-Integrion_442706 SeqNo:7460179 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.8 40 0 97.0 80 - 120 37.84 2.51 202.00
The following samples were analyzed in this batch:HS23071029-08 HS23071029-09
ALS Houston, US Date: 03-Aug-23
Page 37 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R442963 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:01-Aug-2023 08:11
Run ID:ICS-Integrion_442963 SeqNo:7466487 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:01-Aug-2023 08:17
Run ID:ICS-Integrion_442963 SeqNo:7466488 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.49 20 0 97.5 90 - 1100.500
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:01-Aug-2023 09:50
Run ID:ICS-Integrion_442963 SeqNo:7466500 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 11.56 10 1.444 101 80 - 1200.500
Sample ID:HS23071029-06MS Units:mg/L Analysis Date:01-Aug-2023 08:34
Run ID:ICS-Integrion_442963 SeqNo:7466490 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:SBMW-2I
Sulfate 15.91 10 5.729 102 80 - 1200.500
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:01-Aug-2023 09:56
Run ID:ICS-Integrion_442963 SeqNo:7466501 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 11.99 10 1.444 105 80 - 120 11.56 3.66 200.500
Sample ID:HS23071029-06MSD Units:mg/L Analysis Date:01-Aug-2023 08:40
Run ID:ICS-Integrion_442963 SeqNo:7466491 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:SBMW-2I
Sulfate 15.86 10 5.729 101 80 - 120 15.91 0.28 200.500
The following samples were analyzed in this batch:HS23071029-06 HS23071029-07 HS23071029-08 HS23071029-09
ALS Houston, US Date: 03-Aug-23
Page 38 of 44
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071029
QC BATCH REPORT
Batch ID:R443018 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:MBLK-R443018 Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467806 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-R443018 Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467805 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)1005 1000 0 100 85 - 1155.00
Alkalinity, Total (As CaCO3)1008 1000 0 101 85 - 1155.00
Sample ID:LCSD-R443018 Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467837 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)997.3 1000 0 99.7 85 - 115 1005 0.724 205.00
Alkalinity, Total (As CaCO3)1001 1000 0 100 85 - 115 1008 0.682 205.00
Sample ID:HS23071020-04DUP Units:mg/L Analysis Date:01-Aug-2023 18:25
Run ID:ManTech01_443018 SeqNo:7467807 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)167.9 152 9.94 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)167.9 152 9.94 205.00
The following samples were analyzed in this batch:HS23071029-06 HS23071029-07 HS23071029-08 HS23071029-09
ALS Houston, US Date: 03-Aug-23
Page 39 of 44
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071029
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 03-Aug-23
Page 40 of 44
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
03-Aug-23Date: ALS Houston, US
Page 41 of 44
Nelson D. Dusara
19-Jul-2023 13:35Date/Time Received:HS23071029
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.8C/3.7C UC/C IR 31
black
07/19/2023 16:00
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Nilesh D. Ranchod
Date/TimeeSignatureDate/TimeeSignature
20-Jul-2023 07:3818-Jul-2023 12:54
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241110
ALS Houston, US 03-Aug-23Date:
Page 42 of 44
Page 43 of 44
Page 44 of 44
August 04, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 9 sample(s) on Jul 20, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071061
Project Manager
Generated By: DAYNA.FISHER
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 31
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071061
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071061-01 19-Jul-2023 10:20 20-Jul-2023 09:40PMW-R-S Groundwater
HS23071061-02 19-Jul-2023 09:40 20-Jul-2023 09:40PMW-R-I Groundwater
HS23071061-03 19-Jul-2023 10:50 20-Jul-2023 09:40PMW-R-D Groundwater
HS23071061-04 19-Jul-2023 08:40 20-Jul-2023 09:40PMW-R-B Groundwater
HS23071061-05 19-Jul-2023 12:50 20-Jul-2023 09:40FMW-22 Groundwater
HS23071061-06 19-Jul-2023 14:25 20-Jul-2023 09:40AMW-10S Groundwater
HS23071061-07 19-Jul-2023 12:15 20-Jul-2023 09:40OW-4 Groundwater
HS23071061-08 19-Jul-2023 11:55 20-Jul-2023 09:40OW-8 Groundwater
HS23071061-09 19-Jul-2023 00:00 20-Jul-2023 09:40Trip Blank Water
ALS Houston, US 04-Aug-23Date:
Page 2 of 31
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071061
Work Order Comments
Login notes:
Sample ID - COC = AMW-10 , Label = AMW-10S.
1 X Trip Blank Vial received broken
•
Login Notes: Sample ID - COC = 10 , Label = 10S.
1 X Trip Blank Vial received broken
•
ECD Organics by Method SW8011
Batch ID: 197847
Sample ID: MBLK-197847
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R442303
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R442011
Sample ID: PMW-R-S (HS23071061-01MS)
MS is for an unrelated sample•
Metals by Method SW6020A
Batch ID: 198376
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R443058
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R443157
Sample ID: AMW-10S (HS23071061-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Batch ID: R442963
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM3500FED
Batch ID: R441924
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 04-Aug-23Date:
Page 3 of 31
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-R-S
WorkOrder:
Lab ID:
Collection Date:
HS23071061
HS23071061-01
19-Jul-2023 10:20 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 22:330.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 22:330.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 22:330.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 22:331.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 22:330.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 22:330.20Benzene 1.0U
1ug/L 21-Jul-2023 22:330.20Chloroform 1.0U
1ug/L 21-Jul-2023 22:330.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 22:330.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 22:330.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 22:331.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 22:330.30Naphthalene 1.0U
1ug/L 21-Jul-2023 22:330.30o-Xylene 1.0U
1ug/L 21-Jul-2023 22:3310Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 22:330.20Toluene 1.0U
1ug/L 21-Jul-2023 22:330.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 22:3310070-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 22:3389.3 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 22:3310677-123
Surr: Toluene-d8 1%REC 21-Jul-2023 22:3399.0 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 12:280.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of 31
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-R-I
WorkOrder:
Lab ID:
Collection Date:
HS23071061
HS23071061-02
19-Jul-2023 09:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 23:360.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 23:360.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 23:360.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 23:361.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 23:360.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 23:360.20Benzene 1.0U
1ug/L 21-Jul-2023 23:360.20Chloroform 1.0U
1ug/L 21-Jul-2023 23:360.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 23:360.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 23:360.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 23:361.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 23:360.30Naphthalene 1.0U
1ug/L 21-Jul-2023 23:360.30o-Xylene 1.0U
1ug/L 21-Jul-2023 23:3610Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 23:360.20Toluene 1.0U
1ug/L 21-Jul-2023 23:360.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 23:3698.5 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 23:3693.2 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 23:3610377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 23:3610282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 14:190.00321,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 31
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-R-D
WorkOrder:
Lab ID:
Collection Date:
HS23071061
HS23071061-03
19-Jul-2023 10:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 23:570.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 23:570.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 23:570.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 23:571.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 23:570.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 23:570.20Benzene 1.0U
1ug/L 21-Jul-2023 23:570.20Chloroform 1.0U
1ug/L 21-Jul-2023 23:570.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 23:570.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 23:570.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 23:571.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 23:570.30Naphthalene 1.0U
1ug/L 21-Jul-2023 23:570.30o-Xylene 1.0U
1ug/L 21-Jul-2023 23:5710Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 23:570.20Toluene 1.0U
1ug/L 21-Jul-2023 23:570.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 23:5799.7 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 23:5794.2 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 23:5710777-123
Surr: Toluene-d8 1%REC 21-Jul-2023 23:5799.7 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 15:070.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 31
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-R-B
WorkOrder:
Lab ID:
Collection Date:
HS23071061
HS23071061-04
19-Jul-2023 08:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 00:180.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 00:180.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 00:180.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 00:181.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 00:180.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 00:180.20Benzene 1.0U
1ug/L 22-Jul-2023 00:180.20Chloroform 1.0U
1ug/L 22-Jul-2023 00:180.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 00:180.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 00:180.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 00:181.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 00:180.30Naphthalene 1.0U
1ug/L 22-Jul-2023 00:180.30o-Xylene 1.0U
1ug/L 22-Jul-2023 00:1810Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 00:180.20Toluene 1.0U
1ug/L 22-Jul-2023 00:180.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 00:1810370-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 00:1893.9 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 00:1896.7 77-123
Surr: Toluene-d8 1%REC 22-Jul-2023 00:1898.2 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 15:300.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 31
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-22
WorkOrder:
Lab ID:
Collection Date:
HS23071061
HS23071061-05
19-Jul-2023 12:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 00:390.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 00:390.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 00:390.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 00:391.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 00:390.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 00:390.20Benzene 1.0U
1ug/L 22-Jul-2023 00:390.20Chloroform 1.0U
1ug/L 22-Jul-2023 00:390.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 00:390.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 00:390.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 00:391.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 00:390.30Naphthalene 1.0U
1ug/L 22-Jul-2023 00:390.30o-Xylene 1.0U
1ug/L 22-Jul-2023 00:3910Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 00:390.20Toluene 1.0U
1ug/L 22-Jul-2023 00:390.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 00:3910270-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 00:3992.1 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 00:3910877-123
Surr: Toluene-d8 1%REC 22-Jul-2023 00:3910182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 15:540.00321,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 31
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-10S
WorkOrder:
Lab ID:
Collection Date:
HS23071061
HS23071061-06
19-Jul-2023 14:25 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 05:130.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 05:130.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 05:130.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 05:131.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 05:130.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 05:130.20Benzene 1.0U
1ug/L 22-Jul-2023 05:130.20Chloroform 1.0U
1ug/L 22-Jul-2023 05:130.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 05:130.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 05:130.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 05:131.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 05:130.30Naphthalene 1.0U
1ug/L 22-Jul-2023 05:130.30o-Xylene 1.0U
1ug/L 22-Jul-2023 05:1310Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 05:130.20Toluene 1.0U
1ug/L 22-Jul-2023 05:130.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 05:1392.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 05:1399.4 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 05:1393.8 77-123
Surr: Toluene-d8 1%REC 22-Jul-2023 05:1310282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
2ug/L 21-Jul-2023 15:390.214Methane 1.0062.2
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 16:180.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 01-Aug-2023
1mg/L 01-Aug-2023 21:190.0120Iron 0.20021.1
1mg/L 01-Aug-2023 21:190.000700Manganese 0.005001.50
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 10:360.200Sulfate 0.5001.50
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 03-Aug-2023 22:50J0.300Nitrate/Nitrite (as N)2.000.948
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 16:265.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:265.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:265.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:26a5.00Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
10mg/L 21-Jul-2023 10:400.200Ferrous Iron 0.50010.9
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 31
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
OW-4
WorkOrder:
Lab ID:
Collection Date:
HS23071061
HS23071061-07
19-Jul-2023 12:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 01:000.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 01:000.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 01:000.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 01:001.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 01:000.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 01:000.20Benzene 1.0U
1ug/L 22-Jul-2023 01:000.20Chloroform 1.0U
1ug/L 22-Jul-2023 01:000.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 01:000.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 01:000.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 01:001.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 01:000.30Naphthalene 1.0U
1ug/L 22-Jul-2023 01:000.30o-Xylene 1.0U
1ug/L 22-Jul-2023 01:0010Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 01:000.20Toluene 1.0U
1ug/L 22-Jul-2023 01:000.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 01:0010470-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 01:0090.7 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 01:0010677-123
Surr: Toluene-d8 1%REC 22-Jul-2023 01:0098.2 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 16:420.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 31
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
OW-8
WorkOrder:
Lab ID:
Collection Date:
HS23071061
HS23071061-08
19-Jul-2023 11:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 01:210.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 01:210.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 01:210.201,2-Dichloroethane 1.05.7
1ug/L 22-Jul-2023 01:211.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 01:210.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 01:210.20Benzene 1.0U
1ug/L 22-Jul-2023 01:210.20Chloroform 1.0U
1ug/L 22-Jul-2023 01:210.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 01:210.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 01:210.20Methyl tert-butyl ether 1.016
1ug/L 22-Jul-2023 01:211.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 01:210.30Naphthalene 1.0U
1ug/L 22-Jul-2023 01:210.30o-Xylene 1.0U
1ug/L 22-Jul-2023 01:2110Tert-butyl alcohol 10930
1ug/L 22-Jul-2023 01:210.20Toluene 1.0U
1ug/L 22-Jul-2023 01:210.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 01:2110470-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 01:2194.5 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 01:2110677-123
Surr: Toluene-d8 1%REC 22-Jul-2023 01:2110182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 17:050.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 31
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071061
HS23071061-09
19-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 22:120.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 22:120.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 22:120.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 22:121.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 22:120.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 22:120.20Benzene 1.0U
1ug/L 21-Jul-2023 22:120.20Chloroform 1.0U
1ug/L 21-Jul-2023 22:120.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 22:120.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 22:120.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 22:121.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 22:120.30Naphthalene 1.0U
1ug/L 21-Jul-2023 22:120.30o-Xylene 1.0U
1ug/L 21-Jul-2023 22:1210Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 22:120.20Toluene 1.0U
1ug/L 21-Jul-2023 22:120.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 22:1210070-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 22:1293.7 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 22:1210277-123
Surr: Toluene-d8 1%REC 21-Jul-2023 22:1210282-127
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 31
Weight / Prep Log
HS23071061
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197847
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:56 End Date: 21 Jul 2023 09:56
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071061-01 35 (mL)40 mL VOA w/ HCL36.18 (mL)1.034
HS23071061-02 35 (mL)40 mL VOA w/ HCL36.76 (mL)1.05
HS23071061-03 35 (mL)40 mL VOA w/ HCL36.43 (mL)1.041
HS23071061-04 35 (mL)40 mL VOA w/ HCL36.69 (mL)1.048
HS23071061-05 35 (mL)40 mL VOA w/ HCL37.28 (mL)1.065
HS23071061-06 35 (mL)40 mL VOA w/ HCL36.55 (mL)1.044
HS23071061-07 35 (mL)40 mL VOA w/ HCL36.5 (mL)1.043
HS23071061-08 35 (mL)40 mL VOA w/ HCL36.55 (mL)1.044
Batch ID:198376
Method:WATER - SW3010A 3010APrep Code:
Start Date: 01 Aug 2023 12:00 End Date: 01 Aug 2023 12:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071061-06 10 (mL)120 plastic HNO310 (mL)1
04-Aug-23Date: ALS Houston, US
Page 13 of 31
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071061
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197847 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:56 25 Jul 2023 12:28HS23071061-01 19 Jul 2023 10:20 1PMW-R-S
21 Jul 2023 09:56 25 Jul 2023 14:19HS23071061-02 19 Jul 2023 09:40 1PMW-R-I
21 Jul 2023 09:56 25 Jul 2023 15:07HS23071061-03 19 Jul 2023 10:50 1PMW-R-D
21 Jul 2023 09:56 25 Jul 2023 15:30HS23071061-04 19 Jul 2023 08:40 1PMW-R-B
21 Jul 2023 09:56 25 Jul 2023 15:54HS23071061-05 19 Jul 2023 12:50 1FMW-22
21 Jul 2023 09:56 25 Jul 2023 16:18HS23071061-06 19 Jul 2023 14:25 1AMW-10S
21 Jul 2023 09:56 25 Jul 2023 16:42HS23071061-07 19 Jul 2023 12:15 1OW-4
21 Jul 2023 09:56 25 Jul 2023 17:05HS23071061-08 19 Jul 2023 11:55 1OW-8
Batch ID:198376 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
01 Aug 2023 12:00 01 Aug 2023 21:19HS23071061-06 19 Jul 2023 14:25 1AMW-10S
Batch ID:R441924 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
21 Jul 2023 10:40HS23071061-06 19 Jul 2023 14:25 10AMW-10S
Batch ID:R442011 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
21 Jul 2023 22:12HS23071061-09 19 Jul 2023 00:00 1Trip Blank
Batch ID:R442011 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 22:33HS23071061-01 19 Jul 2023 10:20 1PMW-R-S
21 Jul 2023 23:36HS23071061-02 19 Jul 2023 09:40 1PMW-R-I
21 Jul 2023 23:57HS23071061-03 19 Jul 2023 10:50 1PMW-R-D
22 Jul 2023 00:18HS23071061-04 19 Jul 2023 08:40 1PMW-R-B
22 Jul 2023 00:39HS23071061-05 19 Jul 2023 12:50 1FMW-22
22 Jul 2023 05:13HS23071061-06 19 Jul 2023 14:25 1AMW-10S
22 Jul 2023 01:00HS23071061-07 19 Jul 2023 12:15 1OW-4
22 Jul 2023 01:21HS23071061-08 19 Jul 2023 11:55 1OW-8
Batch ID:R442303 ( 1 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
21 Jul 2023 15:39HS23071061-06 19 Jul 2023 14:25 2AMW-10S
21 Jul 2023 15:26HS23071061-06 19 Jul 2023 14:25 1AMW-10S
Batch ID:R442963 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
01 Aug 2023 10:36HS23071061-06 19 Jul 2023 14:25 1AMW-10S
Batch ID:R443058 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
02 Aug 2023 16:26HS23071061-06 19 Jul 2023 14:25 1AMW-10S
Batch ID:R443157 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
03 Aug 2023 22:50HS23071061-06 19 Jul 2023 14:25 10AMW-10S
04-Aug-23Date: ALS Houston, US
Page 14 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:197847 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197847 Units:ug/L Analysis Date:25-Jul-2023 00:42
Run ID:ECD_13_442418 SeqNo:7453266 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197847 Units:ug/L Analysis Date:25-Jul-2023 01:06
Run ID:ECD_13_442418 SeqNo:7453267 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1954 0.25 0 78.2 60 - 1400.020
Sample ID:LCSD-197847 Units:ug/L Analysis Date:25-Jul-2023 01:29
Run ID:ECD_13_442418 SeqNo:7453268 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1962 0.25 0 78.5 60 - 140 0.1954 0.406 200.020
The following samples were analyzed in this batch:HS23071061-01 HS23071061-02 HS23071061-03 HS23071061-04
HS23071061-05 HS23071061-06 HS23071061-07 HS23071061-08
ALS Houston, US Date: 04-Aug-23
Page 15 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:R442303 ( 1 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230721 Units:ug/L Analysis Date:21-Jul-2023 14:22
Run ID:FID-4_442303 SeqNo:7450742 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ethane U 1.00
Ethene U 1.00
Methane U 0.500
Sample ID:LCS-230721 Units:ug/L Analysis Date:21-Jul-2023 14:32
Run ID:FID-4_442303 SeqNo:7450743 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ethane 20.41 18.04 0 113 75 - 1251.00
Ethene 18.1 16.8 0 108 75 - 1251.00
Methane 7.86 9.647 0 81.5 75 - 1250.500
Sample ID:LCSD-230721 Units:ug/L Analysis Date:21-Jul-2023 14:47
Run ID:FID-4_442303 SeqNo:7450744 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Ethane 20.46 18.04 0 113 75 - 125 20.41 0.245 301.00
Ethene 18.5 16.8 0 110 75 - 125 18.1 2.18 301.00
Methane 8.056 9.647 0 83.5 75 - 125 7.86 2.47 300.500
Sample ID:HS23071069-04DUP Units:ug/L Analysis Date:21-Jul-2023 19:32
Run ID:FID-4_442303 SeqNo:7450769 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Ethane U 0 0 301.00
Ethene U 0 0 301.00
Methane 15.63 15.58 0.335 300.500
The following samples were analyzed in this batch:HS23071061-06
ALS Houston, US Date: 04-Aug-23
Page 16 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:198376 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198376 Units:mg/L Analysis Date:01-Aug-2023 20:53
Run ID:ICPMS05_442868 SeqNo:7465463 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:LCS-198376 Units:mg/L Analysis Date:01-Aug-2023 20:55
Run ID:ICPMS05_442868 SeqNo:7465464 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.799 5 0 96.0 80 - 1200.200
Manganese 0.04714 0.05 0 94.3 80 - 1200.00500
Sample ID:HS23071590-01MS Units:mg/L Analysis Date:01-Aug-2023 21:01
Run ID:ICPMS05_442868 SeqNo:7465467 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 4.853 5 0.09242 95.2 80 - 1200.200
Manganese 0.05012 0.05 0.006256 87.7 80 - 1200.00500
Sample ID:HS23071590-01MSD Units:mg/L Analysis Date:01-Aug-2023 21:03
Run ID:ICPMS05_442868 SeqNo:7465468 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 4.83 5 0.09242 94.8 80 - 120 4.853 0.457 200.200
Manganese 0.04956 0.05 0.006256 86.6 80 - 120 0.05012 1.14 200.00500
Sample ID:HS23071590-01PDS Units:mg/L Analysis Date:01-Aug-2023 21:05
Run ID:ICPMS05_442868 SeqNo:7465469 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 9.302 10 0.09242 92.1 75 - 1250.200
Manganese 0.0962 0.1 0.006256 89.9 75 - 1250.00500
ALS Houston, US Date: 04-Aug-23
Page 17 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:198376 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23071590-01SD Units:mg/L Analysis Date:01-Aug-2023 20:59
Run ID:ICPMS05_442868 SeqNo:7465466 PrepDate:01-Aug-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron 0.1269 0.09242 0 10 J 1.00
Manganese 0.006381 0.006256 0 10 J 0.0250
The following samples were analyzed in this batch:HS23071061-06
ALS Houston, US Date: 04-Aug-23
Page 18 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 21:30
Run ID:VOA11_442011 SeqNo:7443881 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
47.84 50 0 95.7 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.54 50 0 93.1 77 - 1131.0Surr: 4-Bromofluorobenzene
50.49 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
49.22 50 0 98.4 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Page 19 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 20:48
Run ID:VOA11_442011 SeqNo:7443880 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.12 20 0 90.6 73 - 1211.0
1,2-Dibromoethane 16.74 20 0 83.7 76 - 1231.0
1,2-Dichloroethane 16.44 20 0 82.2 70 - 1241.0
2-Methylnaphthalene 17.3 20 0 86.5 55 - 1401.0
4-Isopropyltoluene 17.68 20 0 88.4 74 - 1261.0
Benzene 17.13 20 0 85.7 74 - 1201.0
Chloroform 17.62 20 0 88.1 71 - 1211.0
Ethylbenzene 18.39 20 0 92.0 77 - 1171.0
m,p-Xylene 35.54 40 0 88.8 77 - 1222.0
Methyl tert-butyl ether 15.44 20 0 77.2 70 - 1301.0
Methylene chloride 20.36 20 0 102 70 - 1272.0
Naphthalene 16.79 20 0 83.9 70 - 1301.0
o-Xylene 18.76 20 0 93.8 75 - 1191.0
Tert-butyl alcohol 328.8 400 0 82.2 70 - 13010
Toluene 17.07 20 0 85.4 77 - 1181.0
Xylenes, Total 54.3 60 0 90.5 75 - 1223.0
44.23 50 0 88.5 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.18 50 0 94.4 77 - 1131.0Surr: 4-Bromofluorobenzene
49 50 0 98.0 73 - 1261.0Surr: Dibromofluoromethane
48.11 50 0 96.2 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Page 20 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071061-01MS Units:ug/L Analysis Date:21-Jul-2023 22:54
Run ID:VOA11_442011 SeqNo:7443885 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:PMW-R-S
1,2,4-Trimethylbenzene 17.31 20 0 86.5 70 - 1251.0
1,2-Dibromoethane 15.93 20 0 79.6 70 - 1241.0
1,2-Dichloroethane 17.11 20 0 85.6 70 - 1271.0
2-Methylnaphthalene 12.34 20 0 61.7 55 - 1401.0
4-Isopropyltoluene 16.95 20 0 84.8 70 - 1301.0
Benzene 17.76 20 0 88.8 70 - 1271.0
Chloroform 18.4 20 0 92.0 70 - 1251.0
Ethylbenzene 18.45 20 0 92.3 70 - 1241.0
m,p-Xylene 36.02 40 0 90.1 70 - 1302.0
Methyl tert-butyl ether 14.76 20 0 73.8 70 - 1301.0
Methylene chloride 18.72 20 0 93.6 70 - 1282.0
Naphthalene 14.87 20 0 74.4 70 - 1301.0
o-Xylene 17.72 20 0 88.6 70 - 1241.0
Tert-butyl alcohol 258.7 400 0 64.7 70 - 130 S10
Toluene 17.38 20 0 86.9 70 - 1231.0
Xylenes, Total 53.74 60 0 89.6 70 - 1303.0
44.87 50 0 89.7 70 - 1261.0Surr: 1,2-Dichloroethane-d4
49.63 50 0 99.3 77 - 1131.0Surr: 4-Bromofluorobenzene
48.34 50 0 96.7 77 - 1231.0Surr: Dibromofluoromethane
49.07 50 0 98.1 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Page 21 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071061-01MSD Units:ug/L Analysis Date:21-Jul-2023 23:15
Run ID:VOA11_442011 SeqNo:7443886 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:PMW-R-S
1,2,4-Trimethylbenzene 18.16 20 0 90.8 70 - 125 17.31 4.8 201.0
1,2-Dibromoethane 16.71 20 0 83.6 70 - 124 15.93 4.81 201.0
1,2-Dichloroethane 16.2 20 0 81.0 70 - 127 17.11 5.48 201.0
2-Methylnaphthalene 14.51 20 0 72.5 55 - 140 12.34 16.1 201.0
4-Isopropyltoluene 17.91 20 0 89.5 70 - 130 16.95 5.49 201.0
Benzene 17.26 20 0 86.3 70 - 127 17.76 2.87 201.0
Chloroform 17.7 20 0 88.5 70 - 125 18.4 3.9 201.0
Ethylbenzene 17.33 20 0 86.6 70 - 124 18.45 6.28 201.0
m,p-Xylene 36.56 40 0 91.4 70 - 130 36.02 1.49 202.0
Methyl tert-butyl ether 15.16 20 0 75.8 70 - 130 14.76 2.64 201.0
Methylene chloride 19.36 20 0 96.8 70 - 128 18.72 3.35 202.0
Naphthalene 15.95 20 0 79.7 70 - 130 14.87 6.98 201.0
o-Xylene 17.94 20 0 89.7 70 - 124 17.72 1.21 201.0
Tert-butyl alcohol 286.1 400 0 71.5 70 - 130 258.7 10.1 2010
Toluene 17.46 20 0 87.3 70 - 123 17.38 0.424 201.0
Xylenes, Total 54.5 60 0 90.8 70 - 130 53.74 1.4 203.0
45.11 50 0 90.2 70 - 126 44.87 0.532 201.0Surr: 1,2-Dichloroethane-d4
49.78 50 0 99.6 77 - 113 49.63 0.29 201.0Surr: 4-Bromofluorobenzene
49.51 50 0 99.0 77 - 123 48.34 2.39 201.0Surr: Dibromofluoromethane
50.63 50 0 101 82 - 127 49.07 3.13 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071061-01 HS23071061-02 HS23071061-03 HS23071061-04
HS23071061-05 HS23071061-06 HS23071061-07 HS23071061-08
HS23071061-09
ALS Houston, US Date: 04-Aug-23
Page 22 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:R441924 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442034 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442033 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.263 0.25 0 105 80 - 1200.0500
Sample ID:HS23071069-04MS Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442036 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.504 0.25 0.279 90.0 75 - 1250.0500
Sample ID:HS23071069-04MSD Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442035 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.505 0.25 0.279 90.4 75 - 125 0.504 0.198 200.0500
The following samples were analyzed in this batch:HS23071061-06
ALS Houston, US Date: 04-Aug-23
Page 23 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:R442963 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:01-Aug-2023 08:11
Run ID:ICS-Integrion_442963 SeqNo:7466487 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:01-Aug-2023 08:17
Run ID:ICS-Integrion_442963 SeqNo:7466488 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.49 20 0 97.5 90 - 1100.500
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:01-Aug-2023 09:50
Run ID:ICS-Integrion_442963 SeqNo:7466500 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 11.56 10 1.444 101 80 - 1200.500
Sample ID:HS23071029-06MS Units:mg/L Analysis Date:01-Aug-2023 08:34
Run ID:ICS-Integrion_442963 SeqNo:7466490 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 15.91 10 5.729 102 80 - 1200.500
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:01-Aug-2023 09:56
Run ID:ICS-Integrion_442963 SeqNo:7466501 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 11.99 10 1.444 105 80 - 120 11.56 3.66 200.500
Sample ID:HS23071029-06MSD Units:mg/L Analysis Date:01-Aug-2023 08:40
Run ID:ICS-Integrion_442963 SeqNo:7466491 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 15.86 10 5.729 101 80 - 120 15.91 0.28 200.500
The following samples were analyzed in this batch:HS23071061-06
ALS Houston, US Date: 04-Aug-23
Page 24 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:R443058 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:WBLKW1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:03
Run ID:ManTech01_443058 SeqNo:7469107 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:11
Run ID:ManTech01_443058 SeqNo:7469108 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)975.7 1000 0 97.6 85 - 1155.00
Alkalinity, Total (As CaCO3)994.5 1000 0 99.5 85 - 1155.00
Sample ID:LCSD1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:21
Run ID:ManTech01_443058 SeqNo:7469109 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)1006 1000 0 101 85 - 115 975.7 3.04 205.00
Alkalinity, Total (As CaCO3)1027 1000 0 103 85 - 115 994.5 3.2 205.00
Sample ID:HS23071063-02DUP Units:mg/L Analysis Date:02-Aug-2023 16:45
Run ID:ManTech01_443058 SeqNo:7469113 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)450.7 449.7 0.22 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)450.7 449.7 0.22 205.00
The following samples were analyzed in this batch:HS23071061-06
ALS Houston, US Date: 04-Aug-23
Page 25 of 31
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071061
QC BATCH REPORT
Batch ID:R443157 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:03-Aug-2023 22:27
Run ID:ICS-Integrion_443157 SeqNo:7471623 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:03-Aug-2023 22:39
Run ID:ICS-Integrion_443157 SeqNo:7471624 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.459 8 0 106 90 - 1100.200
Sample ID:HS23080130-01MS Units:mg/L Analysis Date:04-Aug-2023 00:17
Run ID:ICS-Integrion_443157 SeqNo:7471636 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)38.38 40 0 95.9 80 - 1202.00
Sample ID:HS23071390-01MS Units:mg/L Analysis Date:03-Aug-2023 23:14
Run ID:ICS-Integrion_443157 SeqNo:7471629 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)40.47 40 3.072 93.5 80 - 1202.00
Sample ID:HS23080130-01MSD Units:mg/L Analysis Date:04-Aug-2023 00:23
Run ID:ICS-Integrion_443157 SeqNo:7471637 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)39.27 40 0 98.2 80 - 120 38.38 2.31 202.00
Sample ID:HS23071390-01MSD Units:mg/L Analysis Date:03-Aug-2023 23:19
Run ID:ICS-Integrion_443157 SeqNo:7471630 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)40.72 40 3.072 94.1 80 - 120 40.47 0.621 202.00
The following samples were analyzed in this batch:HS23071061-06
ALS Houston, US Date: 04-Aug-23
Page 26 of 31
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071061
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 04-Aug-23
Page 27 of 31
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
04-Aug-23Date: ALS Houston, US
Page 28 of 31
Ragen Giga
20-Jul-2023 09:40Date/Time Received:HS23071061
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.8uc/3.7c IR31
Blue
07/20/2023
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Sample ID - COC = AMW-10 , Label = AMW-10S.
1 X Trip Blank Vial received broken
Completed By:/S/ Ragen Giga
Date/TimeeSignatureDate/TimeeSignature
21-Jul-2023 08:0920-Jul-2023 18:59
FedEx Priority OvernightWCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241119
ALS Houston, US 04-Aug-23Date:
Page 29 of 31
Page 30 of 31
Page 31 of 31
August 03, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 8 sample(s) on Jul 20, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071063
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 40
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071063
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071063-01 19-Jul-2023 13:25 20-Jul-2023 09:40MW-B-I Groundwater
HS23071063-02 19-Jul-2023 14:02 20-Jul-2023 09:40MW-B-D Groundwater
HS23071063-03 19-Jul-2023 13:50 20-Jul-2023 09:40MW-B-B Groundwater
HS23071063-04 19-Jul-2023 12:15 20-Jul-2023 09:40Z2-X20 Groundwater
HS23071063-05 19-Jul-2023 15:25 20-Jul-2023 09:40Z2-X35 Groundwater
HS23071063-06 19-Jul-2023 15:30 20-Jul-2023 09:40AMW-16S Groundwater
HS23071063-07 19-Jul-2023 14:55 20-Jul-2023 09:40AMW-18S Groundwater
HS23071063-08 19-Jul-2023 00:00 20-Jul-2023 09:40Trip Blank Water
ALS Houston, US 03-Aug-23Date:
Page 2 of 40
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071063
Work Order Comments
Login notes:
1 vial for sample MW-B-I received broken.
AMW-18S ferrous Fe pH>2(7) preserved w/HCL on 7-20-23 @11:25 by Sima. After preservation (1) LOT# 3100605321
•
ECD Organics by Method SW8011
Batch ID: 197847
Sample ID: MBLK-197847
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R442732
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R442040
Sample ID: HS23071175-03MS
MS and MSD are for an unrelated sample•
Batch ID: R442011
Sample ID: HS23071061-01MS
MS and MSD are for an unrelated sample•
Batch ID: R442056
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Metals by Method SW6020A
Batch ID: 198376
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R443058
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442963
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 3 of 40
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071063
WetChemistry by Method E300
Batch ID: R442706
Sample ID: AMW-16S (HS23071063-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: AMW-18S (HS23071063-07)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-B-B (HS23071063-03)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-B-D (HS23071063-02)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-B-I (HS23071063-01)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Z2-X20 (HS23071063-04)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441924
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 4 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-B-I
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-01
19-Jul-2023 13:25 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 01:420.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 01:420.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 01:420.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 01:421.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 01:420.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 01:420.20Benzene 1.0U
1ug/L 22-Jul-2023 01:420.20Chloroform 1.0U
1ug/L 22-Jul-2023 01:420.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 01:420.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 01:420.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 01:421.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 01:420.30Naphthalene 1.0U
1ug/L 22-Jul-2023 01:420.30o-Xylene 1.0U
1ug/L 22-Jul-2023 01:4210Tert-butyl alcohol 10400
1ug/L 22-Jul-2023 01:420.20Toluene 1.0U
1ug/L 22-Jul-2023 01:420.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 01:4210170-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 01:4294.4 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 01:4210577-123
Surr: Toluene-d8 1%REC 22-Jul-2023 01:4299.4 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 28-Jul-2023 13:470.107Methane 0.50033.4
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 18:400.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 01-Aug-2023
1mg/L 01-Aug-2023 21:210.0120Iron 0.2005.91
20mg/L 02-Aug-2023 13:510.0140Manganese 0.1001.90
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 11:110.200Sulfate 0.5001.46
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 04:300.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 16:325.00Alkalinity, Bicarbonate (As
CaCO3)5.00285
1mg/L 02-Aug-2023 16:325.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:325.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:32a5.00Alkalinity, Total (As CaCO3)5.00285
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.05000.509
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-B-D
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-02
19-Jul-2023 14:02 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 02:030.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 02:030.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 02:030.201,2-Dichloroethane 1.04.0
1ug/L 22-Jul-2023 02:031.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 02:030.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 02:030.20Benzene 1.0U
1ug/L 22-Jul-2023 02:030.20Chloroform 1.0U
1ug/L 22-Jul-2023 02:030.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 02:030.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 02:030.20Methyl tert-butyl ether 1.0180
1ug/L 22-Jul-2023 02:031.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 02:030.30Naphthalene 1.0U
1ug/L 22-Jul-2023 02:030.30o-Xylene 1.0U
100ug/L 22-Jul-2023 18:401000Tert-butyl alcohol 100030,000
1ug/L 22-Jul-2023 02:030.20Toluene 1.0U
1ug/L 22-Jul-2023 02:030.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 02:0397.6 70-126
Surr: 1,2-Dichloroethane-d4 100%REC 22-Jul-2023 18:4010370-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 02:0398.2 77-113
Surr: 4-Bromofluorobenzene 100%REC 22-Jul-2023 18:4089.9 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 02:0310277-123
Surr: Dibromofluoromethane 100%REC 22-Jul-2023 18:4010877-123
Surr: Toluene-d8 1%REC 22-Jul-2023 02:0398.8 82-127
Surr: Toluene-d8 100%REC 22-Jul-2023 18:4010182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
5ug/L 28-Jul-2023 16:480.535Methane 2.50101
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 19:030.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 01-Aug-2023
1mg/L 01-Aug-2023 21:230.0120Iron 0.2000.716
50mg/L 02-Aug-2023 13:530.0350Manganese 0.2505.37
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 11:170.200Sulfate 0.5000.778
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 04:480.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-B-D
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-02
19-Jul-2023 14:02 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 16:395.00Alkalinity, Bicarbonate (As
CaCO3)5.00450
1mg/L 02-Aug-2023 16:395.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:395.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:39a5.00Alkalinity, Total (As CaCO3)5.00450
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.05001.12
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-B-B
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-03
19-Jul-2023 13:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 02:24J0.301,2,4-Trimethylbenzene 1.00.81
1ug/L 22-Jul-2023 02:240.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 02:240.201,2-Dichloroethane 1.01.8
1ug/L 22-Jul-2023 02:241.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 02:240.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 02:240.20Benzene 1.0U
1ug/L 22-Jul-2023 02:240.20Chloroform 1.0U
1ug/L 22-Jul-2023 02:24J0.30Ethylbenzene 1.00.39
1ug/L 22-Jul-2023 02:24J0.50m,p-Xylene 2.01.1
1ug/L 22-Jul-2023 02:240.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 02:241.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 02:240.30Naphthalene 1.0U
1ug/L 22-Jul-2023 02:24J0.30o-Xylene 1.00.55
500ug/L 22-Jul-2023 19:015000Tert-butyl alcohol 5000100,000
1ug/L 22-Jul-2023 02:240.20Toluene 1.0U
1ug/L 22-Jul-2023 02:24J0.30Xylenes, Total 3.01.7
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 02:2492.0 70-126
Surr: 1,2-Dichloroethane-d4 500%REC 22-Jul-2023 19:0199.7 70-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 02:2491.9 77-113
Surr: 4-Bromofluorobenzene 500%REC 22-Jul-2023 19:0189.0 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 02:2498.3 77-123
Surr: Dibromofluoromethane 500%REC 22-Jul-2023 19:0110677-123
Surr: Toluene-d8 1%REC 22-Jul-2023 02:2410082-127
Surr: Toluene-d8 500%REC 22-Jul-2023 19:0197.5 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 28-Jul-2023 15:520.107Methane 0.5002.25
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 19:270.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 01-Aug-2023
1mg/L 01-Aug-2023 21:25J0.0120Iron 0.2000.0215
1mg/L 01-Aug-2023 21:250.000700Manganese 0.005000.00743
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 11:230.200Sulfate 0.5003.53
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 04:530.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-B-B
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-03
19-Jul-2023 13:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 16:535.00Alkalinity, Bicarbonate (As
CaCO3)5.0036.2
1mg/L 02-Aug-2023 16:535.00Alkalinity, Carbonate (As CaCO3)5.0034.7
1mg/L 02-Aug-2023 16:535.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:53a5.00Alkalinity, Total (As CaCO3)5.0071.0
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.05000.0510
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-X20
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-04
19-Jul-2023 12:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 02:450.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 02:450.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 02:450.201,2-Dichloroethane 1.01.2
1ug/L 22-Jul-2023 02:451.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 02:450.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 02:45J0.20Benzene 1.00.57
1ug/L 22-Jul-2023 02:450.20Chloroform 1.0U
1ug/L 22-Jul-2023 02:450.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 02:450.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 02:450.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 02:451.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 02:450.30Naphthalene 1.0U
1ug/L 22-Jul-2023 02:450.30o-Xylene 1.0U
1ug/L 22-Jul-2023 02:4510Tert-butyl alcohol 10630
1ug/L 22-Jul-2023 02:450.20Toluene 1.0U
1ug/L 22-Jul-2023 02:450.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 02:4510570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 02:4593.8 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 02:4510277-123
Surr: Toluene-d8 1%REC 22-Jul-2023 02:4510282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
20ug/L 28-Jul-2023 17:042.14Methane 10.0450
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 19:510.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 01-Aug-2023
1mg/L 01-Aug-2023 21:270.0120Iron 0.2009.28
50mg/L 02-Aug-2023 13:550.0350Manganese 0.2504.84
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 11:290.200Sulfate 0.5006.73
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 04:590.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 16:595.00Alkalinity, Bicarbonate (As
CaCO3)5.00219
1mg/L 02-Aug-2023 16:595.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:595.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 16:59a5.00Alkalinity, Total (As CaCO3)5.00219
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
10mg/L 21-Jul-2023 10:400.200Ferrous Iron 0.50011.8
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-X35
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-05
19-Jul-2023 15:25 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 03:060.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 03:060.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 03:060.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 03:061.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 03:060.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 03:060.20Benzene 1.0U
1ug/L 22-Jul-2023 03:060.20Chloroform 1.0U
1ug/L 22-Jul-2023 03:060.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 03:060.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 03:060.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 03:061.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 03:060.30Naphthalene 1.0U
1ug/L 22-Jul-2023 03:060.30o-Xylene 1.0U
1ug/L 22-Jul-2023 03:0610Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 03:060.20Toluene 1.0U
1ug/L 22-Jul-2023 03:060.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 03:0610170-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 03:0693.3 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 03:0610477-123
Surr: Toluene-d8 1%REC 22-Jul-2023 03:0610282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 20:140.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-16S
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-06
19-Jul-2023 15:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 03:280.301,2,4-Trimethylbenzene 1.011
1ug/L 22-Jul-2023 03:280.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 03:280.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 03:281.02-Methylnaphthalene 1.04.4
1ug/L 22-Jul-2023 03:280.304-Isopropyltoluene 1.0U
10ug/L 22-Jul-2023 23:562.0Benzene 10250
1ug/L 22-Jul-2023 03:280.20Chloroform 1.0U
1ug/L 22-Jul-2023 03:280.30Ethylbenzene 1.06.7
1ug/L 22-Jul-2023 03:280.50m,p-Xylene 2.07.6
1ug/L 22-Jul-2023 03:280.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 03:281.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 03:280.30Naphthalene 1.022
1ug/L 22-Jul-2023 03:280.30o-Xylene 1.01.8
1ug/L 22-Jul-2023 03:2810Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 03:280.20Toluene 1.04.7
1ug/L 22-Jul-2023 03:280.30Xylenes, Total 3.09.4
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 03:2889.2 70-126
Surr: 1,2-Dichloroethane-d4 10%REC 22-Jul-2023 23:5610570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 03:2895.5 77-113
Surr: 4-Bromofluorobenzene 10%REC 22-Jul-2023 23:5689.1 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 03:2895.2 77-123
Surr: Dibromofluoromethane 10%REC 22-Jul-2023 23:5610277-123
Surr: Toluene-d8 1%REC 22-Jul-2023 03:2899.6 82-127
Surr: Toluene-d8 10%REC 22-Jul-2023 23:5699.0 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
20ug/L 28-Jul-2023 17:142.14Methane 10.0472
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 20:380.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 01-Aug-2023
1mg/L 01-Aug-2023 21:290.0120Iron 0.2001.92
1mg/L 01-Aug-2023 21:290.000700Manganese 0.005000.729
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 11:340.200Sulfate 0.5001.79
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 05:050.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-16S
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-06
19-Jul-2023 15:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 17:235.00Alkalinity, Bicarbonate (As
CaCO3)5.00234
1mg/L 02-Aug-2023 17:235.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:235.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:23a5.00Alkalinity, Total (As CaCO3)5.00234
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
5mg/L 21-Jul-2023 10:400.100Ferrous Iron 0.2502.56
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-18S
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-07
19-Jul-2023 14:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 03:490.301,2,4-Trimethylbenzene 1.04.3
1ug/L 22-Jul-2023 03:490.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 03:490.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 03:491.02-Methylnaphthalene 1.09.2
1ug/L 22-Jul-2023 03:490.304-Isopropyltoluene 1.0U
10ug/L 23-Jul-2023 00:172.0Benzene 10870
1ug/L 22-Jul-2023 03:490.20Chloroform 1.0U
1ug/L 22-Jul-2023 03:490.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 03:490.50m,p-Xylene 2.045
1ug/L 22-Jul-2023 03:490.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 03:491.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 03:490.30Naphthalene 1.056
1ug/L 22-Jul-2023 03:490.30o-Xylene 1.012
1ug/L 22-Jul-2023 03:4910Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 03:490.20Toluene 1.02.4
1ug/L 22-Jul-2023 03:490.30Xylenes, Total 3.057
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 03:4987.8 70-126
Surr: 1,2-Dichloroethane-d4 10%REC 23-Jul-2023 00:1710570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 03:4994.0 77-113
Surr: 4-Bromofluorobenzene 10%REC 23-Jul-2023 00:1790.6 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 03:4991.5 77-123
Surr: Dibromofluoromethane 10%REC 23-Jul-2023 00:1710177-123
Surr: Toluene-d8 1%REC 22-Jul-2023 03:4999.2 82-127
Surr: Toluene-d8 10%REC 23-Jul-2023 00:1710182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
100ug/L 28-Jul-2023 17:2610.7Methane 50.02,870
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 21:010.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 01-Aug-2023
1mg/L 01-Aug-2023 21:310.0120Iron 0.2005.96
20mg/L 02-Aug-2023 13:570.0140Manganese 0.1002.06
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 11:400.200Sulfate 0.5000.892
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 05:110.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-18S
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-07
19-Jul-2023 14:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 17:295.00Alkalinity, Bicarbonate (As
CaCO3)5.00337
1mg/L 02-Aug-2023 17:295.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:295.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:29a5.00Alkalinity, Total (As CaCO3)5.00337
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
10mg/L 21-Jul-2023 10:400.200Ferrous Iron 0.5007.00
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071063
HS23071063-08
19-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 21:510.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 21:510.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 21:510.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 21:511.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 21:510.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 21:510.20Benzene 1.0U
1ug/L 21-Jul-2023 21:510.20Chloroform 1.0U
1ug/L 21-Jul-2023 21:510.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 21:510.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 21:510.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 21:511.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 21:510.30Naphthalene 1.0U
1ug/L 21-Jul-2023 21:510.30o-Xylene 1.0U
1ug/L 21-Jul-2023 21:5110Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 21:510.20Toluene 1.0U
1ug/L 21-Jul-2023 21:510.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 21:5199.8 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 21:5192.1 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 21:5110377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 21:5110082-127
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 16 of 40
Weight / Prep Log
HS23071063
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197847
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:56 End Date: 21 Jul 2023 09:56
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071063-01 35 (mL)40 mL VOA w/ HCL36.35 (mL)1.039
HS23071063-02 35 (mL)40 mL VOA w/ HCL36.6 (mL)1.046
HS23071063-03 35 (mL)40 mL VOA w/ HCL36.85 (mL)1.053
HS23071063-04 35 (mL)40 mL VOA w/ HCL37.07 (mL)1.059
HS23071063-05 35 (mL)40 mL VOA w/ HCL36.6 (mL)1.046
HS23071063-06 35 (mL)40 mL VOA w/ HCL36.33 (mL)1.038
HS23071063-07 35 (mL)40 mL VOA w/ HCL36.89 (mL)1.054
Batch ID:198376
Method:WATER - SW3010A 3010APrep Code:
Start Date: 01 Aug 2023 12:00 End Date: 01 Aug 2023 12:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071063-01 10 (mL)120 plastic HNO310 (mL)1
HS23071063-02 10 (mL)120 plastic HNO310 (mL)1
HS23071063-03 10 (mL)120 plastic HNO310 (mL)1
HS23071063-04 10 (mL)120 plastic HNO310 (mL)1
HS23071063-06 10 (mL)120 plastic HNO310 (mL)1
HS23071063-07 10 (mL)120 plastic HNO310 (mL)1
03-Aug-23Date: ALS Houston, US
Page 17 of 40
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071063
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197847 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:56 25 Jul 2023 18:40HS23071063-01 19 Jul 2023 13:25 1MW-B-I
21 Jul 2023 09:56 25 Jul 2023 19:03HS23071063-02 19 Jul 2023 14:02 1MW-B-D
21 Jul 2023 09:56 25 Jul 2023 19:27HS23071063-03 19 Jul 2023 13:50 1MW-B-B
21 Jul 2023 09:56 25 Jul 2023 19:51HS23071063-04 19 Jul 2023 12:15 1Z2-X20
21 Jul 2023 09:56 25 Jul 2023 20:14HS23071063-05 19 Jul 2023 15:25 1Z2-X35
21 Jul 2023 09:56 25 Jul 2023 20:38HS23071063-06 19 Jul 2023 15:30 1AMW-16S
21 Jul 2023 09:56 25 Jul 2023 21:01HS23071063-07 19 Jul 2023 14:55 1AMW-18S
Batch ID:198376 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
01 Aug 2023 12:00 02 Aug 2023 13:51HS23071063-01 19 Jul 2023 13:25 20MW-B-I
01 Aug 2023 12:00 01 Aug 2023 21:21HS23071063-01 19 Jul 2023 13:25 1MW-B-I
01 Aug 2023 12:00 02 Aug 2023 13:53HS23071063-02 19 Jul 2023 14:02 50MW-B-D
01 Aug 2023 12:00 01 Aug 2023 21:23HS23071063-02 19 Jul 2023 14:02 1MW-B-D
01 Aug 2023 12:00 01 Aug 2023 21:25HS23071063-03 19 Jul 2023 13:50 1MW-B-B
01 Aug 2023 12:00 02 Aug 2023 13:55HS23071063-04 19 Jul 2023 12:15 50Z2-X20
01 Aug 2023 12:00 01 Aug 2023 21:27HS23071063-04 19 Jul 2023 12:15 1Z2-X20
01 Aug 2023 12:00 01 Aug 2023 21:29HS23071063-06 19 Jul 2023 15:30 1AMW-16S
01 Aug 2023 12:00 02 Aug 2023 13:57HS23071063-07 19 Jul 2023 14:55 20AMW-18S
01 Aug 2023 12:00 01 Aug 2023 21:31HS23071063-07 19 Jul 2023 14:55 1AMW-18S
Batch ID:R441924 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
21 Jul 2023 10:40HS23071063-01 19 Jul 2023 13:25 1MW-B-I
21 Jul 2023 10:40HS23071063-02 19 Jul 2023 14:02 1MW-B-D
21 Jul 2023 10:40HS23071063-03 19 Jul 2023 13:50 1MW-B-B
21 Jul 2023 10:40HS23071063-04 19 Jul 2023 12:15 10Z2-X20
21 Jul 2023 10:40HS23071063-06 19 Jul 2023 15:30 5AMW-16S
21 Jul 2023 10:40HS23071063-07 19 Jul 2023 14:55 10AMW-18S
Batch ID:R442011 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
21 Jul 2023 21:51HS23071063-08 19 Jul 2023 00:00 1Trip Blank
Batch ID:R442011 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
22 Jul 2023 01:42HS23071063-01 19 Jul 2023 13:25 1MW-B-I
22 Jul 2023 02:03HS23071063-02 19 Jul 2023 14:02 1MW-B-D
22 Jul 2023 02:24HS23071063-03 19 Jul 2023 13:50 1MW-B-B
22 Jul 2023 02:45HS23071063-04 19 Jul 2023 12:15 1Z2-X20
22 Jul 2023 03:06HS23071063-05 19 Jul 2023 15:25 1Z2-X35
22 Jul 2023 03:28HS23071063-06 19 Jul 2023 15:30 1AMW-16S
22 Jul 2023 03:49HS23071063-07 19 Jul 2023 14:55 1AMW-18S
03-Aug-23Date: ALS Houston, US
Page 18 of 40
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071063
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442040 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
22 Jul 2023 18:40HS23071063-02 19 Jul 2023 14:02 100MW-B-D
22 Jul 2023 19:01HS23071063-03 19 Jul 2023 13:50 500MW-B-B
Batch ID:R442056 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
22 Jul 2023 23:56HS23071063-06 19 Jul 2023 15:30 10AMW-16S
23 Jul 2023 00:17HS23071063-07 19 Jul 2023 14:55 10AMW-18S
Batch ID:R442706 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
29 Jul 2023 04:30HS23071063-01 19 Jul 2023 13:25 10MW-B-I
29 Jul 2023 04:48HS23071063-02 19 Jul 2023 14:02 10MW-B-D
29 Jul 2023 04:53HS23071063-03 19 Jul 2023 13:50 10MW-B-B
29 Jul 2023 04:59HS23071063-04 19 Jul 2023 12:15 10Z2-X20
29 Jul 2023 05:05HS23071063-06 19 Jul 2023 15:30 10AMW-16S
29 Jul 2023 05:11HS23071063-07 19 Jul 2023 14:55 10AMW-18S
Batch ID:R442732 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
28 Jul 2023 13:47HS23071063-01 19 Jul 2023 13:25 1MW-B-I
28 Jul 2023 16:48HS23071063-02 19 Jul 2023 14:02 5MW-B-D
28 Jul 2023 15:52HS23071063-03 19 Jul 2023 13:50 1MW-B-B
28 Jul 2023 17:04HS23071063-04 19 Jul 2023 12:15 20Z2-X20
28 Jul 2023 17:14HS23071063-06 19 Jul 2023 15:30 20AMW-16S
28 Jul 2023 17:26HS23071063-07 19 Jul 2023 14:55 100AMW-18S
Batch ID:R442963 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
01 Aug 2023 11:11HS23071063-01 19 Jul 2023 13:25 1MW-B-I
01 Aug 2023 11:17HS23071063-02 19 Jul 2023 14:02 1MW-B-D
01 Aug 2023 11:23HS23071063-03 19 Jul 2023 13:50 1MW-B-B
01 Aug 2023 11:29HS23071063-04 19 Jul 2023 12:15 1Z2-X20
01 Aug 2023 11:34HS23071063-06 19 Jul 2023 15:30 1AMW-16S
01 Aug 2023 11:40HS23071063-07 19 Jul 2023 14:55 1AMW-18S
Batch ID:R443058 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
02 Aug 2023 16:32HS23071063-01 19 Jul 2023 13:25 1MW-B-I
02 Aug 2023 16:39HS23071063-02 19 Jul 2023 14:02 1MW-B-D
02 Aug 2023 16:53HS23071063-03 19 Jul 2023 13:50 1MW-B-B
02 Aug 2023 16:59HS23071063-04 19 Jul 2023 12:15 1Z2-X20
02 Aug 2023 17:23HS23071063-06 19 Jul 2023 15:30 1AMW-16S
02 Aug 2023 17:29HS23071063-07 19 Jul 2023 14:55 1AMW-18S
03-Aug-23Date: ALS Houston, US
Page 19 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:197847 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197847 Units:ug/L Analysis Date:25-Jul-2023 00:42
Run ID:ECD_13_442418 SeqNo:7453266 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197847 Units:ug/L Analysis Date:25-Jul-2023 01:06
Run ID:ECD_13_442418 SeqNo:7453267 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1954 0.25 0 78.2 60 - 1400.020
Sample ID:LCSD-197847 Units:ug/L Analysis Date:25-Jul-2023 01:29
Run ID:ECD_13_442418 SeqNo:7453268 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1962 0.25 0 78.5 60 - 140 0.1954 0.406 200.020
The following samples were analyzed in this batch:HS23071063-01 HS23071063-02 HS23071063-03 HS23071063-04
HS23071063-05 HS23071063-06 HS23071063-07
ALS Houston, US Date: 03-Aug-23
Page 20 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442732 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230728 Units:ug/L Analysis Date:28-Jul-2023 08:00
Run ID:FID-4_442732 SeqNo:7460972 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230728 Units:ug/L Analysis Date:28-Jul-2023 08:09
Run ID:FID-4_442732 SeqNo:7460973 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.953 9.647 0 82.4 75 - 1250.500
Sample ID:LCSD-230728 Units:ug/L Analysis Date:28-Jul-2023 08:18
Run ID:FID-4_442732 SeqNo:7460974 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 8.01 9.647 0 83.0 75 - 125 7.953 0.72 300.500
The following samples were analyzed in this batch:HS23071063-01 HS23071063-02 HS23071063-03 HS23071063-04
HS23071063-06 HS23071063-07
ALS Houston, US Date: 03-Aug-23
Page 21 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:198376 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198376 Units:mg/L Analysis Date:01-Aug-2023 20:53
Run ID:ICPMS05_442868 SeqNo:7465463 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:LCS-198376 Units:mg/L Analysis Date:01-Aug-2023 20:55
Run ID:ICPMS05_442868 SeqNo:7465464 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.799 5 0 96.0 80 - 1200.200
Manganese 0.04714 0.05 0 94.3 80 - 1200.00500
Sample ID:HS23071590-01MS Units:mg/L Analysis Date:01-Aug-2023 21:01
Run ID:ICPMS05_442868 SeqNo:7465467 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 4.853 5 0.09242 95.2 80 - 1200.200
Manganese 0.05012 0.05 0.006256 87.7 80 - 1200.00500
Sample ID:HS23071590-01MSD Units:mg/L Analysis Date:01-Aug-2023 21:03
Run ID:ICPMS05_442868 SeqNo:7465468 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 4.83 5 0.09242 94.8 80 - 120 4.853 0.457 200.200
Manganese 0.04956 0.05 0.006256 86.6 80 - 120 0.05012 1.14 200.00500
Sample ID:HS23071590-01PDS Units:mg/L Analysis Date:01-Aug-2023 21:05
Run ID:ICPMS05_442868 SeqNo:7465469 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 9.302 10 0.09242 92.1 75 - 1250.200
Manganese 0.0962 0.1 0.006256 89.9 75 - 1250.00500
ALS Houston, US Date: 03-Aug-23
Page 22 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:198376 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23071590-01SD Units:mg/L Analysis Date:01-Aug-2023 20:59
Run ID:ICPMS05_442868 SeqNo:7465466 PrepDate:01-Aug-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron 0.1269 0.09242 0 10 J 1.00
Manganese 0.006381 0.006256 0 10 J 0.0250
The following samples were analyzed in this batch:HS23071063-01 HS23071063-02 HS23071063-03 HS23071063-04
HS23071063-06 HS23071063-07
ALS Houston, US Date: 03-Aug-23
Page 23 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 21:30
Run ID:VOA11_442011 SeqNo:7443881 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
47.84 50 0 95.7 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.54 50 0 93.1 77 - 1131.0Surr: 4-Bromofluorobenzene
50.49 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
49.22 50 0 98.4 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 24 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 20:48
Run ID:VOA11_442011 SeqNo:7443880 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.12 20 0 90.6 73 - 1211.0
1,2-Dibromoethane 16.74 20 0 83.7 76 - 1231.0
1,2-Dichloroethane 16.44 20 0 82.2 70 - 1241.0
2-Methylnaphthalene 17.3 20 0 86.5 55 - 1401.0
4-Isopropyltoluene 17.68 20 0 88.4 74 - 1261.0
Benzene 17.13 20 0 85.7 74 - 1201.0
Chloroform 17.62 20 0 88.1 71 - 1211.0
Ethylbenzene 18.39 20 0 92.0 77 - 1171.0
m,p-Xylene 35.54 40 0 88.8 77 - 1222.0
Methyl tert-butyl ether 15.44 20 0 77.2 70 - 1301.0
Methylene chloride 20.36 20 0 102 70 - 1272.0
Naphthalene 16.79 20 0 83.9 70 - 1301.0
o-Xylene 18.76 20 0 93.8 75 - 1191.0
Tert-butyl alcohol 328.8 400 0 82.2 70 - 13010
Toluene 17.07 20 0 85.4 77 - 1181.0
Xylenes, Total 54.3 60 0 90.5 75 - 1223.0
44.23 50 0 88.5 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.18 50 0 94.4 77 - 1131.0Surr: 4-Bromofluorobenzene
49 50 0 98.0 73 - 1261.0Surr: Dibromofluoromethane
48.11 50 0 96.2 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 25 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071061-01MS Units:ug/L Analysis Date:21-Jul-2023 22:54
Run ID:VOA11_442011 SeqNo:7443885 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 17.31 20 0 86.5 70 - 1251.0
1,2-Dibromoethane 15.93 20 0 79.6 70 - 1241.0
1,2-Dichloroethane 17.11 20 0 85.6 70 - 1271.0
2-Methylnaphthalene 12.34 20 0 61.7 55 - 1401.0
4-Isopropyltoluene 16.95 20 0 84.8 70 - 1301.0
Benzene 17.76 20 0 88.8 70 - 1271.0
Chloroform 18.4 20 0 92.0 70 - 1251.0
Ethylbenzene 18.45 20 0 92.3 70 - 1241.0
m,p-Xylene 36.02 40 0 90.1 70 - 1302.0
Methyl tert-butyl ether 14.76 20 0 73.8 70 - 1301.0
Methylene chloride 18.72 20 0 93.6 70 - 1282.0
Naphthalene 14.87 20 0 74.4 70 - 1301.0
o-Xylene 17.72 20 0 88.6 70 - 1241.0
Tert-butyl alcohol 258.7 400 0 64.7 70 - 130 S10
Toluene 17.38 20 0 86.9 70 - 1231.0
Xylenes, Total 53.74 60 0 89.6 70 - 1303.0
44.87 50 0 89.7 70 - 1261.0Surr: 1,2-Dichloroethane-d4
49.63 50 0 99.3 77 - 1131.0Surr: 4-Bromofluorobenzene
48.34 50 0 96.7 77 - 1231.0Surr: Dibromofluoromethane
49.07 50 0 98.1 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 26 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071061-01MSD Units:ug/L Analysis Date:21-Jul-2023 23:15
Run ID:VOA11_442011 SeqNo:7443886 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 18.16 20 0 90.8 70 - 125 17.31 4.8 201.0
1,2-Dibromoethane 16.71 20 0 83.6 70 - 124 15.93 4.81 201.0
1,2-Dichloroethane 16.2 20 0 81.0 70 - 127 17.11 5.48 201.0
2-Methylnaphthalene 14.51 20 0 72.5 55 - 140 12.34 16.1 201.0
4-Isopropyltoluene 17.91 20 0 89.5 70 - 130 16.95 5.49 201.0
Benzene 17.26 20 0 86.3 70 - 127 17.76 2.87 201.0
Chloroform 17.7 20 0 88.5 70 - 125 18.4 3.9 201.0
Ethylbenzene 17.33 20 0 86.6 70 - 124 18.45 6.28 201.0
m,p-Xylene 36.56 40 0 91.4 70 - 130 36.02 1.49 202.0
Methyl tert-butyl ether 15.16 20 0 75.8 70 - 130 14.76 2.64 201.0
Methylene chloride 19.36 20 0 96.8 70 - 128 18.72 3.35 202.0
Naphthalene 15.95 20 0 79.7 70 - 130 14.87 6.98 201.0
o-Xylene 17.94 20 0 89.7 70 - 124 17.72 1.21 201.0
Tert-butyl alcohol 286.1 400 0 71.5 70 - 130 258.7 10.1 2010
Toluene 17.46 20 0 87.3 70 - 123 17.38 0.424 201.0
Xylenes, Total 54.5 60 0 90.8 70 - 130 53.74 1.4 203.0
45.11 50 0 90.2 70 - 126 44.87 0.532 201.0Surr: 1,2-Dichloroethane-d4
49.78 50 0 99.6 77 - 113 49.63 0.29 201.0Surr: 4-Bromofluorobenzene
49.51 50 0 99.0 77 - 123 48.34 2.39 201.0Surr: Dibromofluoromethane
50.63 50 0 101 82 - 127 49.07 3.13 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071063-01 HS23071063-02 HS23071063-03 HS23071063-04
HS23071063-05 HS23071063-06 HS23071063-07 HS23071063-08
ALS Houston, US Date: 03-Aug-23
Page 27 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442040 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230722 Units:ug/L Analysis Date:22-Jul-2023 11:39
Run ID:VOA11_442040 SeqNo:7444536 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Tert-butyl alcohol U 10
46.58 50 0 93.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.41 50 0 92.8 77 - 1131.0Surr: 4-Bromofluorobenzene
47.45 50 0 94.9 73 - 1261.0Surr: Dibromofluoromethane
50.36 50 0 101 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230722 Units:ug/L Analysis Date:22-Jul-2023 10:57
Run ID:VOA11_442040 SeqNo:7444763 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Tert-butyl alcohol 400.3 400 0 100 70 - 13010
46.39 50 0 92.8 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.83 50 0 97.7 77 - 1131.0Surr: 4-Bromofluorobenzene
48.33 50 0 96.7 73 - 1261.0Surr: Dibromofluoromethane
50.25 50 0 101 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23071175-03MS Units:ug/L Analysis Date:22-Jul-2023 12:21
Run ID:VOA11_442040 SeqNo:7444764 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Tert-butyl alcohol 276.2 400 0 69.0 70 - 130 S10
45.89 50 0 91.8 70 - 1261.0Surr: 1,2-Dichloroethane-d4
48.92 50 0 97.8 77 - 1131.0Surr: 4-Bromofluorobenzene
49.35 50 0 98.7 77 - 1231.0Surr: Dibromofluoromethane
49.21 50 0 98.4 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 28 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442040 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071175-03MSD Units:ug/L Analysis Date:22-Jul-2023 12:43
Run ID:VOA11_442040 SeqNo:7444765 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Tert-butyl alcohol 285.2 400 0 71.3 70 - 130 276.2 3.21 2010
44.54 50 0 89.1 70 - 126 45.89 2.99 201.0Surr: 1,2-Dichloroethane-d4
48.95 50 0 97.9 77 - 113 48.92 0.0486 201.0Surr: 4-Bromofluorobenzene
48.9 50 0 97.8 77 - 123 49.35 0.913 201.0Surr: Dibromofluoromethane
50.66 50 0 101 82 - 127 49.21 2.92 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071063-02 HS23071063-03
ALS Houston, US Date: 03-Aug-23
Page 29 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230722 Units:ug/L Analysis Date:22-Jul-2023 22:32
Run ID:VOA10_442056 SeqNo:7445003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Benzene U 1.0
51.96 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.12 50 0 90.2 77 - 1131.0Surr: 4-Bromofluorobenzene
50.63 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
49.14 50 0 98.3 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230722 Units:ug/L Analysis Date:22-Jul-2023 21:50
Run ID:VOA10_442056 SeqNo:7445002 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Benzene 17.28 20 0 86.4 74 - 1201.0
52.12 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.52 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
52.47 50 0 105 73 - 1261.0Surr: Dibromofluoromethane
50.46 50 0 101 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23071175-10MS Units:ug/L Analysis Date:22-Jul-2023 23:14
Run ID:VOA10_442056 SeqNo:7445005 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Benzene 17.53 20 0 87.7 70 - 1271.0
52.12 50 0 104 70 - 1261.0Surr: 1,2-Dichloroethane-d4
45.4 50 0 90.8 77 - 1131.0Surr: 4-Bromofluorobenzene
51.12 50 0 102 77 - 1231.0Surr: Dibromofluoromethane
52.07 50 0 104 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 30 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071175-10MSD Units:ug/L Analysis Date:22-Jul-2023 23:35
Run ID:VOA10_442056 SeqNo:7445006 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Benzene 16.86 20 0 84.3 70 - 127 17.53 3.93 201.0
52.45 50 0 105 70 - 126 52.12 0.623 201.0Surr: 1,2-Dichloroethane-d4
47.48 50 0 95.0 77 - 113 45.4 4.49 201.0Surr: 4-Bromofluorobenzene
51.2 50 0 102 77 - 123 51.12 0.159 201.0Surr: Dibromofluoromethane
51.09 50 0 102 82 - 127 52.07 1.91 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071063-06 HS23071063-07
ALS Houston, US Date: 03-Aug-23
Page 31 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R441924 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442034 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442033 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.263 0.25 0 105 80 - 1200.0500
Sample ID:HS23071069-04MS Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442036 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.504 0.25 0.279 90.0 75 - 1250.0500
Sample ID:HS23071069-04MSD Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442035 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.505 0.25 0.279 90.4 75 - 125 0.504 0.198 200.0500
The following samples were analyzed in this batch:HS23071063-01 HS23071063-02 HS23071063-03 HS23071063-04
HS23071063-06 HS23071063-07
ALS Houston, US Date: 03-Aug-23
Page 32 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442706 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 04:19
Run ID:ICS-Integrion_442706 SeqNo:7460175 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 04:24
Run ID:ICS-Integrion_442706 SeqNo:7460176 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)7.902 8 0 98.8 90 - 1100.200
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:29-Jul-2023 05:51
Run ID:ICS-Integrion_442706 SeqNo:7460188 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.68 40 0 94.2 80 - 1202.00
Sample ID:HS23071063-01MS Units:mg/L Analysis Date:29-Jul-2023 04:36
Run ID:ICS-Integrion_442706 SeqNo:7460178 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:MW-B-I
Nitrate/Nitrite (as N)37.84 40 0 94.6 80 - 1202.00
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:29-Jul-2023 05:57
Run ID:ICS-Integrion_442706 SeqNo:7460189 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.69 40 0 96.7 80 - 120 37.68 2.64 202.00
Sample ID:HS23071063-01MSD Units:mg/L Analysis Date:29-Jul-2023 04:42
Run ID:ICS-Integrion_442706 SeqNo:7460179 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:MW-B-I
Nitrate/Nitrite (as N)38.8 40 0 97.0 80 - 120 37.84 2.51 202.00
The following samples were analyzed in this batch:HS23071063-01 HS23071063-02 HS23071063-03 HS23071063-04
HS23071063-06 HS23071063-07
ALS Houston, US Date: 03-Aug-23
Page 33 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R442963 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:01-Aug-2023 08:11
Run ID:ICS-Integrion_442963 SeqNo:7466487 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:01-Aug-2023 08:17
Run ID:ICS-Integrion_442963 SeqNo:7466488 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.49 20 0 97.5 90 - 1100.500
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:01-Aug-2023 09:50
Run ID:ICS-Integrion_442963 SeqNo:7466500 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 11.56 10 1.444 101 80 - 1200.500
Sample ID:HS23071029-06MS Units:mg/L Analysis Date:01-Aug-2023 08:34
Run ID:ICS-Integrion_442963 SeqNo:7466490 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 15.91 10 5.729 102 80 - 1200.500
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:01-Aug-2023 09:56
Run ID:ICS-Integrion_442963 SeqNo:7466501 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 11.99 10 1.444 105 80 - 120 11.56 3.66 200.500
Sample ID:HS23071029-06MSD Units:mg/L Analysis Date:01-Aug-2023 08:40
Run ID:ICS-Integrion_442963 SeqNo:7466491 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 15.86 10 5.729 101 80 - 120 15.91 0.28 200.500
The following samples were analyzed in this batch:HS23071063-01 HS23071063-02 HS23071063-03 HS23071063-04
HS23071063-06 HS23071063-07
ALS Houston, US Date: 03-Aug-23
Page 34 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071063
QC BATCH REPORT
Batch ID:R443058 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:WBLKW1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:03
Run ID:ManTech01_443058 SeqNo:7469107 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:11
Run ID:ManTech01_443058 SeqNo:7469108 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)975.7 1000 0 97.6 85 - 1155.00
Alkalinity, Total (As CaCO3)994.5 1000 0 99.5 85 - 1155.00
Sample ID:LCSD1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:21
Run ID:ManTech01_443058 SeqNo:7469109 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)1006 1000 0 101 85 - 115 975.7 3.04 205.00
Alkalinity, Total (As CaCO3)1027 1000 0 103 85 - 115 994.5 3.2 205.00
Sample ID:HS23071063-02DUP Units:mg/L Analysis Date:02-Aug-2023 16:45
Run ID:ManTech01_443058 SeqNo:7469113 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:MW-B-D
Alkalinity, Bicarbonate (As CaCO3)450.7 449.7 0.22 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)450.7 449.7 0.22 205.00
The following samples were analyzed in this batch:HS23071063-01 HS23071063-02 HS23071063-03 HS23071063-04
HS23071063-06 HS23071063-07
ALS Houston, US Date: 03-Aug-23
Page 35 of 40
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071063
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 03-Aug-23
Page 36 of 40
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
03-Aug-23Date: ALS Houston, US
Page 37 of 40
Ragen Giga
20-Jul-2023 09:40Date/Time Received:HS23071063
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
2.8/2.7 uc/c IR 31
Blue
7-20-23 11:10
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
1 vial for sample MW-B-I received broken. AMW-18S ferrous Fe pH>2(7) preserved w/HCL on 7-20-23 @11:25 by Sima. After
preservation (1) LOT# 3100605321
Completed By:/S/ Bernadette A. Fini
Date/TimeeSignatureDate/TimeeSignature
20-Jul-2023 17:4620-Jul-2023 17:29
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241121
ALS Houston, US 03-Aug-23Date:
Page 38 of 40
Page 39 of 40
Page 40 of 40
August 03, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 13 sample(s) on Jul 20, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071066
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 45
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071066
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071066-01 19-Jul-2023 08:20 20-Jul-2023 09:40Z4-PZ9 Groundwater
HS23071066-02 19-Jul-2023 08:40 20-Jul-2023 09:40Z4-PZ7 Groundwater
HS23071066-03 19-Jul-2023 08:55 20-Jul-2023 09:40Z4-PZ4 Groundwater
HS23071066-04 19-Jul-2023 09:15 20-Jul-2023 09:40Z2-PZ-10 Groundwater
HS23071066-05 19-Jul-2023 09:30 20-Jul-2023 09:40Z2-PZ-9 Groundwater
HS23071066-06 19-Jul-2023 09:55 20-Jul-2023 09:40Z2-PZ-8 Groundwater
HS23071066-07 19-Jul-2023 10:15 20-Jul-2023 09:40Z2-PZ-6 Groundwater
HS23071066-08 19-Jul-2023 10:55 20-Jul-2023 09:40Z4-X63 Groundwater
HS23071066-09 19-Jul-2023 11:00 20-Jul-2023 09:40DUP #3 Groundwater
HS23071066-10 19-Jul-2023 12:50 20-Jul-2023 09:40Z4-X68 Groundwater
HS23071066-11 19-Jul-2023 11:40 20-Jul-2023 09:40Z4-X30 Groundwater
HS23071066-12 19-Jul-2023 14:35 20-Jul-2023 09:40Field Blank (FB) #3 Water
HS23071066-13 19-Jul-2023 00:00 20-Jul-2023 09:40Trip Blank Water
ALS Houston, US 03-Aug-23Date:
Page 2 of 45
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071066
ECD Organics by Method SW8011
Batch ID: 197848
Sample ID: MBLK-197848
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
Batch ID: 197847
Sample ID: MBLK-197847
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R442732
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R442011
Sample ID: HS23071061-01MS
MS and MSD are for an unrelated sample•
Batch ID: R442018,R442040
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Metals by Method SW6020A
Batch ID: 198376
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R443058
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442963
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R442706
Sample ID: Field Blank (FB) #3 (HS23071066-12)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441924
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 3 of 45
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071066
WetChemistry by Method SM3500FED
ALS Houston, US 03-Aug-23Date:
Page 4 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-PZ9
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-01
19-Jul-2023 08:20 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 04:100.301,2,4-Trimethylbenzene 1.025
1ug/L 22-Jul-2023 04:100.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 04:100.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 04:101.02-Methylnaphthalene 1.051
1ug/L 22-Jul-2023 04:100.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 04:100.20Benzene 1.0180
1ug/L 22-Jul-2023 04:100.20Chloroform 1.0U
10ug/L 22-Jul-2023 19:223.0Ethylbenzene 10290
1ug/L 22-Jul-2023 04:100.50m,p-Xylene 2.049
1ug/L 22-Jul-2023 04:100.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 04:101.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 04:100.30Naphthalene 1.096
1ug/L 22-Jul-2023 04:100.30o-Xylene 1.060
1ug/L 22-Jul-2023 04:1010Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 04:100.20Toluene 1.013
1ug/L 22-Jul-2023 04:100.30Xylenes, Total 3.0110
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 04:1085.2 70-126
Surr: 1,2-Dichloroethane-d4 10%REC 22-Jul-2023 19:2292.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 04:1010077-113
Surr: 4-Bromofluorobenzene 10%REC 22-Jul-2023 19:2293.5 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 04:1089.3 77-123
Surr: Dibromofluoromethane 10%REC 22-Jul-2023 19:2298.5 77-123
Surr: Toluene-d8 1%REC 22-Jul-2023 04:1098.3 82-127
Surr: Toluene-d8 10%REC 22-Jul-2023 19:2210082-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 21:250.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-PZ7
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-02
19-Jul-2023 08:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 04:310.301,2,4-Trimethylbenzene 1.05.8
1ug/L 22-Jul-2023 04:310.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 04:310.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 04:311.02-Methylnaphthalene 1.09.8
1ug/L 22-Jul-2023 04:310.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 04:310.20Benzene 1.018
1ug/L 22-Jul-2023 04:310.20Chloroform 1.0U
1ug/L 22-Jul-2023 04:310.30Ethylbenzene 1.047
1ug/L 22-Jul-2023 04:310.50m,p-Xylene 2.05.4
1ug/L 22-Jul-2023 04:310.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 04:311.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 04:310.30Naphthalene 1.027
1ug/L 22-Jul-2023 04:310.30o-Xylene 1.03.0
1ug/L 22-Jul-2023 04:3110Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 04:310.20Toluene 1.01.1
1ug/L 22-Jul-2023 04:310.30Xylenes, Total 3.08.5
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 04:3190.8 70-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 04:3196.4 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 04:3193.8 77-123
Surr: Toluene-d8 1%REC 22-Jul-2023 04:3197.7 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 25-Jul-2023 21:480.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-PZ4
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-03
19-Jul-2023 08:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 04:520.301,2,4-Trimethylbenzene 1.02.8
1ug/L 22-Jul-2023 04:520.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 04:520.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 04:521.02-Methylnaphthalene 1.068
1ug/L 22-Jul-2023 04:520.304-Isopropyltoluene 1.05.4
1ug/L 22-Jul-2023 04:520.20Benzene 1.03.2
1ug/L 22-Jul-2023 04:520.20Chloroform 1.0U
1ug/L 22-Jul-2023 04:520.30Ethylbenzene 1.09.2
1ug/L 22-Jul-2023 04:520.50m,p-Xylene 2.02.1
1ug/L 22-Jul-2023 04:520.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 04:521.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 04:520.30Naphthalene 1.032
1ug/L 22-Jul-2023 04:520.30o-Xylene 1.04.4
1ug/L 22-Jul-2023 04:5210Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 04:52J0.20Toluene 1.00.39
1ug/L 22-Jul-2023 04:520.30Xylenes, Total 3.06.5
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 04:5287.6 70-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 04:5297.8 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 04:5293.0 77-123
Surr: Toluene-d8 1%REC 22-Jul-2023 04:5210082-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 00:320.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-PZ-10
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-04
19-Jul-2023 09:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 17:230.301,2,4-Trimethylbenzene 1.01.7
1ug/L 21-Jul-2023 17:230.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 17:230.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 17:231.02-Methylnaphthalene 1.06.8
1ug/L 21-Jul-2023 17:230.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 17:23J0.20Benzene 1.00.58
1ug/L 21-Jul-2023 17:230.20Chloroform 1.0U
1ug/L 21-Jul-2023 17:230.30Ethylbenzene 1.03.1
1ug/L 21-Jul-2023 17:23J0.50m,p-Xylene 2.01.2
1ug/L 21-Jul-2023 17:230.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 17:231.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 17:230.30Naphthalene 1.06.3
1ug/L 21-Jul-2023 17:23J0.30o-Xylene 1.00.84
1ug/L 21-Jul-2023 17:2310Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 17:230.20Toluene 1.0U
1ug/L 21-Jul-2023 17:23J0.30Xylenes, Total 3.02.0
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 17:2310370-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 17:2392.1 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 17:2310377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 17:2310282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 00:550.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-PZ-9
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-05
19-Jul-2023 09:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 18:260.301,2,4-Trimethylbenzene 1.01.4
1ug/L 21-Jul-2023 18:260.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 18:260.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 18:261.02-Methylnaphthalene 1.07.4
1ug/L 21-Jul-2023 18:260.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 18:260.20Benzene 1.0U
1ug/L 21-Jul-2023 18:260.20Chloroform 1.0U
1ug/L 21-Jul-2023 18:260.30Ethylbenzene 1.04.8
1ug/L 21-Jul-2023 18:26J0.50m,p-Xylene 2.01.0
1ug/L 21-Jul-2023 18:260.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 18:261.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 18:260.30Naphthalene 1.08.5
1ug/L 21-Jul-2023 18:26J0.30o-Xylene 1.00.49
1ug/L 21-Jul-2023 18:2610Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 18:260.20Toluene 1.0U
1ug/L 21-Jul-2023 18:26J0.30Xylenes, Total 3.01.5
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 18:2610670-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 18:2693.9 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 18:2610177-123
Surr: Toluene-d8 1%REC 21-Jul-2023 18:2610082-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 01:190.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-PZ-8
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-06
19-Jul-2023 09:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 18:470.301,2,4-Trimethylbenzene 1.05.5
1ug/L 21-Jul-2023 18:470.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 18:470.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 18:471.02-Methylnaphthalene 1.087
1ug/L 21-Jul-2023 18:470.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 18:470.20Benzene 1.0U
1ug/L 21-Jul-2023 18:470.20Chloroform 1.0U
1ug/L 21-Jul-2023 18:470.30Ethylbenzene 1.054
1ug/L 21-Jul-2023 18:47J0.50m,p-Xylene 2.00.77
1ug/L 21-Jul-2023 18:470.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 18:471.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 18:470.30Naphthalene 1.0110
1ug/L 21-Jul-2023 18:47J0.30o-Xylene 1.00.49
1ug/L 21-Jul-2023 18:4710Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 18:470.20Toluene 1.0U
1ug/L 21-Jul-2023 18:47J0.30Xylenes, Total 3.01.3
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 18:4799.7 70-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 18:4795.4 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 18:4710377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 18:4710482-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 01:420.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-PZ-6
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-07
19-Jul-2023 10:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 19:080.301,2,4-Trimethylbenzene 1.05.3
1ug/L 21-Jul-2023 19:080.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 19:080.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 19:081.02-Methylnaphthalene 1.019
1ug/L 21-Jul-2023 19:080.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 19:080.20Benzene 1.011
1ug/L 21-Jul-2023 19:080.20Chloroform 1.0U
1ug/L 21-Jul-2023 19:080.30Ethylbenzene 1.022
1ug/L 21-Jul-2023 19:080.50m,p-Xylene 2.04.0
1ug/L 21-Jul-2023 19:080.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 19:081.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 19:080.30Naphthalene 1.019
1ug/L 21-Jul-2023 19:080.30o-Xylene 1.02.7
1ug/L 21-Jul-2023 19:0810Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 19:08J0.20Toluene 1.00.62
1ug/L 21-Jul-2023 19:080.30Xylenes, Total 3.06.7
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 19:0810370-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 19:0893.3 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 19:0810377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 19:0810082-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 02:060.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-X63
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-08
19-Jul-2023 10:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 19:290.301,2,4-Trimethylbenzene 1.023
1ug/L 21-Jul-2023 19:290.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 19:290.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 19:291.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 19:290.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 19:290.20Benzene 1.01.1
1ug/L 21-Jul-2023 19:290.20Chloroform 1.0U
1ug/L 21-Jul-2023 19:290.30Ethylbenzene 1.02.4
1ug/L 21-Jul-2023 19:290.50m,p-Xylene 2.02.1
1ug/L 21-Jul-2023 19:290.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 19:291.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 19:290.30Naphthalene 1.04.1
1ug/L 21-Jul-2023 19:29J0.30o-Xylene 1.00.37
1ug/L 21-Jul-2023 19:2910Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 19:290.20Toluene 1.0U
1ug/L 21-Jul-2023 19:29J0.30Xylenes, Total 3.02.4
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 19:2910270-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 19:2993.7 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 19:2910177-123
Surr: Toluene-d8 1%REC 21-Jul-2023 19:2910282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 02:290.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DUP #3
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-09
19-Jul-2023 11:00 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 19:500.301,2,4-Trimethylbenzene 1.022
1ug/L 21-Jul-2023 19:500.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 19:500.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 19:501.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 19:500.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 19:500.20Benzene 1.01.2
1ug/L 21-Jul-2023 19:500.20Chloroform 1.0U
1ug/L 21-Jul-2023 19:500.30Ethylbenzene 1.03.0
1ug/L 21-Jul-2023 19:500.50m,p-Xylene 2.02.1
1ug/L 21-Jul-2023 19:500.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 19:501.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 19:500.30Naphthalene 1.0U
1ug/L 21-Jul-2023 19:50J0.30o-Xylene 1.00.38
1ug/L 21-Jul-2023 19:5010Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 19:500.20Toluene 1.0U
1ug/L 21-Jul-2023 19:50J0.30Xylenes, Total 3.02.5
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 19:5010070-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 19:5094.0 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 19:5099.0 77-123
Surr: Toluene-d8 1%REC 21-Jul-2023 19:5010282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 04:020.00321,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-X68
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-10
19-Jul-2023 12:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 20:110.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 20:110.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 20:110.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 20:111.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 20:110.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 20:110.20Benzene 1.0U
1ug/L 21-Jul-2023 20:110.20Chloroform 1.0U
1ug/L 21-Jul-2023 20:110.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 20:110.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 20:110.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 20:111.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 20:110.30Naphthalene 1.0U
1ug/L 21-Jul-2023 20:110.30o-Xylene 1.0U
1ug/L 21-Jul-2023 20:1110Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 20:110.20Toluene 1.0U
1ug/L 21-Jul-2023 20:110.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 20:1110570-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 20:1195.9 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 20:1110377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 20:1110182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 04:260.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z4-X30
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-11
19-Jul-2023 11:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 20:320.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 20:320.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 20:320.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 20:321.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 20:320.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 20:320.20Benzene 1.0U
1ug/L 21-Jul-2023 20:320.20Chloroform 1.0U
1ug/L 21-Jul-2023 20:320.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 20:320.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 20:320.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 20:321.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 20:320.30Naphthalene 1.0U
1ug/L 21-Jul-2023 20:320.30o-Xylene 1.0U
1ug/L 21-Jul-2023 20:3210Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 20:320.20Toluene 1.0U
1ug/L 21-Jul-2023 20:320.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 20:3210470-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 20:3291.5 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 20:3210377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 20:3210182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 04:490.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Field Blank (FB) #3
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-12
19-Jul-2023 14:35 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 16:410.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 16:410.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 16:410.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 16:411.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 16:410.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 16:410.20Benzene 1.0U
1ug/L 21-Jul-2023 16:410.20Chloroform 1.0U
1ug/L 21-Jul-2023 16:410.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 16:410.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 16:410.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 16:411.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 16:410.30Naphthalene 1.0U
1ug/L 21-Jul-2023 16:410.30o-Xylene 1.0U
1ug/L 21-Jul-2023 16:4110Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 16:410.20Toluene 1.0U
1ug/L 21-Jul-2023 16:410.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 16:4110470-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 16:4193.9 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 16:4110277-123
Surr: Toluene-d8 1%REC 21-Jul-2023 16:4110382-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 28-Jul-2023 18:070.107Methane 0.5000.526
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 05:120.00311,2-Dibromoethane 0.020U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: MSCPrep:SW3010A / 01-Aug-2023
1mg/L 01-Aug-2023 21:370.0120Iron 0.200U
1mg/L 01-Aug-2023 21:370.000700Manganese 0.00500U
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 09:030.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 03:440.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 17:345.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:345.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:345.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:34a5.00Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.0500U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 16 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071066
HS23071066-13
19-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 17:020.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 17:020.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 17:020.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 17:021.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 17:020.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 17:020.20Benzene 1.0U
1ug/L 21-Jul-2023 17:020.20Chloroform 1.0U
1ug/L 21-Jul-2023 17:020.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 17:020.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 17:020.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 17:021.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 17:020.30Naphthalene 1.0U
1ug/L 21-Jul-2023 17:020.30o-Xylene 1.0U
1ug/L 21-Jul-2023 17:0210Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 17:020.20Toluene 1.0U
1ug/L 21-Jul-2023 17:020.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 17:0210670-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 17:0292.4 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 17:0210477-123
Surr: Toluene-d8 1%REC 21-Jul-2023 17:0210182-127
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 17 of 45
Weight / Prep Log
HS23071066
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197847
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 09:56 End Date: 21 Jul 2023 09:56
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071066-01 35 (mL)40 mL VOA w/ HCL36.08 (mL)1.031
HS23071066-02 35 (mL)40 mL VOA w/ HCL36.49 (mL)1.043
Batch ID:197848
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 10:02 End Date: 21 Jul 2023 10:02
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071066-03 35 (mL)40 mL VOA w/ HCL36.44 (mL)1.041
HS23071066-04 35 (mL)40 mL VOA w/ HCL36.62 (mL)1.046
HS23071066-05 35 (mL)40 mL VOA w/ HCL36.33 (mL)1.038
HS23071066-06 35 (mL)40 mL VOA w/ HCL36.45 (mL)1.041
HS23071066-07 35 (mL)40 mL VOA w/ HCL36.33 (mL)1.038
HS23071066-08 35 (mL)40 mL VOA w/ HCL36.08 (mL)1.031
HS23071066-09 35 (mL)40 mL VOA w/ HCL36.85 (mL)1.053
HS23071066-10 35 (mL)40 mL VOA w/ HCL35.96 (mL)1.027
HS23071066-11 35 (mL)40 mL VOA w/ HCL36.32 (mL)1.038
HS23071066-12 35 (mL)40 mL VOA w/ HCL35.87 (mL)1.025
Batch ID:198376
Method:WATER - SW3010A 3010APrep Code:
Start Date: 01 Aug 2023 12:00 End Date: 01 Aug 2023 12:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071066-12 10 (mL)120 plastic HNO310 (mL)1
03-Aug-23Date: ALS Houston, US
Page 18 of 45
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071066
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197847 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 09:56 25 Jul 2023 21:25HS23071066-01 19 Jul 2023 08:20 1Z4-PZ9
21 Jul 2023 09:56 25 Jul 2023 21:48HS23071066-02 19 Jul 2023 08:40 1Z4-PZ7
Batch ID:197848 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Water
21 Jul 2023 10:02 26 Jul 2023 05:12HS23071066-12 19 Jul 2023 14:35 1Field Blank (FB) #3
Batch ID:197848 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 10:02 26 Jul 2023 00:32HS23071066-03 19 Jul 2023 08:55 1Z4-PZ4
21 Jul 2023 10:02 26 Jul 2023 00:55HS23071066-04 19 Jul 2023 09:15 1Z2-PZ-10
21 Jul 2023 10:02 26 Jul 2023 01:19HS23071066-05 19 Jul 2023 09:30 1Z2-PZ-9
21 Jul 2023 10:02 26 Jul 2023 01:42HS23071066-06 19 Jul 2023 09:55 1Z2-PZ-8
21 Jul 2023 10:02 26 Jul 2023 02:06HS23071066-07 19 Jul 2023 10:15 1Z2-PZ-6
21 Jul 2023 10:02 26 Jul 2023 02:29HS23071066-08 19 Jul 2023 10:55 1Z4-X63
21 Jul 2023 10:02 26 Jul 2023 04:02HS23071066-09 19 Jul 2023 11:00 1DUP #3
21 Jul 2023 10:02 26 Jul 2023 04:26HS23071066-10 19 Jul 2023 12:50 1Z4-X68
21 Jul 2023 10:02 26 Jul 2023 04:49HS23071066-11 19 Jul 2023 11:40 1Z4-X30
Batch ID:198376 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Water
01 Aug 2023 12:00 01 Aug 2023 21:37HS23071066-12 19 Jul 2023 14:35 1Field Blank (FB) #3
Batch ID:R441924 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Water
21 Jul 2023 10:40HS23071066-12 19 Jul 2023 14:35 1Field Blank (FB) #3
Batch ID:R442011 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
22 Jul 2023 04:10HS23071066-01 19 Jul 2023 08:20 1Z4-PZ9
22 Jul 2023 04:31HS23071066-02 19 Jul 2023 08:40 1Z4-PZ7
22 Jul 2023 04:52HS23071066-03 19 Jul 2023 08:55 1Z4-PZ4
Batch ID:R442018 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
21 Jul 2023 16:41HS23071066-12 19 Jul 2023 14:35 1Field Blank (FB) #3
21 Jul 2023 17:02HS23071066-13 19 Jul 2023 00:00 1Trip Blank
Batch ID:R442018 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 17:23HS23071066-04 19 Jul 2023 09:15 1Z2-PZ-10
21 Jul 2023 18:26HS23071066-05 19 Jul 2023 09:30 1Z2-PZ-9
21 Jul 2023 18:47HS23071066-06 19 Jul 2023 09:55 1Z2-PZ-8
21 Jul 2023 19:08HS23071066-07 19 Jul 2023 10:15 1Z2-PZ-6
21 Jul 2023 19:29HS23071066-08 19 Jul 2023 10:55 1Z4-X63
21 Jul 2023 19:50HS23071066-09 19 Jul 2023 11:00 1DUP #3
21 Jul 2023 20:11HS23071066-10 19 Jul 2023 12:50 1Z4-X68
21 Jul 2023 20:32HS23071066-11 19 Jul 2023 11:40 1Z4-X30
Batch ID:R442040 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
22 Jul 2023 19:22HS23071066-01 19 Jul 2023 08:20 10Z4-PZ9
03-Aug-23Date: ALS Houston, US
Page 19 of 45
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071066
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442706 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Water
29 Jul 2023 03:44HS23071066-12 19 Jul 2023 14:35 10Field Blank (FB) #3
Batch ID:R442732 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Water
28 Jul 2023 18:07HS23071066-12 19 Jul 2023 14:35 1Field Blank (FB) #3
Batch ID:R442963 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Water
01 Aug 2023 09:03HS23071066-12 19 Jul 2023 14:35 1Field Blank (FB) #3
Batch ID:R443058 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Water
02 Aug 2023 17:34HS23071066-12 19 Jul 2023 14:35 1Field Blank (FB) #3
03-Aug-23Date: ALS Houston, US
Page 20 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:197847 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197847 Units:ug/L Analysis Date:25-Jul-2023 00:42
Run ID:ECD_13_442418 SeqNo:7453266 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197847 Units:ug/L Analysis Date:25-Jul-2023 01:06
Run ID:ECD_13_442418 SeqNo:7453267 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1954 0.25 0 78.2 60 - 1400.020
Sample ID:LCSD-197847 Units:ug/L Analysis Date:25-Jul-2023 01:29
Run ID:ECD_13_442418 SeqNo:7453268 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1962 0.25 0 78.5 60 - 140 0.1954 0.406 200.020
The following samples were analyzed in this batch:HS23071066-01 HS23071066-02
ALS Houston, US Date: 03-Aug-23
Page 21 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:197848 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197848 Units:ug/L Analysis Date:25-Jul-2023 23:22
Run ID:ECD_13_442420 SeqNo:7453289 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197848 Units:ug/L Analysis Date:25-Jul-2023 23:45
Run ID:ECD_13_442420 SeqNo:7453290 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1651 0.25 0 66.0 60 - 1400.020
Sample ID:LCSD-197848 Units:ug/L Analysis Date:26-Jul-2023 00:09
Run ID:ECD_13_442420 SeqNo:7453291 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1873 0.25 0 74.9 60 - 140 0.1651 12.6 200.020
The following samples were analyzed in this batch:HS23071066-03 HS23071066-04 HS23071066-05 HS23071066-06
HS23071066-07 HS23071066-08 HS23071066-09 HS23071066-10
HS23071066-11 HS23071066-12
ALS Houston, US Date: 03-Aug-23
Page 22 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442732 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230728 Units:ug/L Analysis Date:28-Jul-2023 08:00
Run ID:FID-4_442732 SeqNo:7460972 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230728 Units:ug/L Analysis Date:28-Jul-2023 08:09
Run ID:FID-4_442732 SeqNo:7460973 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.953 9.647 0 82.4 75 - 1250.500
Sample ID:LCSD-230728 Units:ug/L Analysis Date:28-Jul-2023 08:18
Run ID:FID-4_442732 SeqNo:7460974 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 8.01 9.647 0 83.0 75 - 125 7.953 0.72 300.500
The following samples were analyzed in this batch:HS23071066-12
ALS Houston, US Date: 03-Aug-23
Page 23 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:198376 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198376 Units:mg/L Analysis Date:01-Aug-2023 20:53
Run ID:ICPMS05_442868 SeqNo:7465463 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:LCS-198376 Units:mg/L Analysis Date:01-Aug-2023 20:55
Run ID:ICPMS05_442868 SeqNo:7465464 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.799 5 0 96.0 80 - 1200.200
Manganese 0.04714 0.05 0 94.3 80 - 1200.00500
Sample ID:HS23071590-01MS Units:mg/L Analysis Date:01-Aug-2023 21:01
Run ID:ICPMS05_442868 SeqNo:7465467 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 4.853 5 0.09242 95.2 80 - 1200.200
Manganese 0.05012 0.05 0.006256 87.7 80 - 1200.00500
Sample ID:HS23071590-01MSD Units:mg/L Analysis Date:01-Aug-2023 21:03
Run ID:ICPMS05_442868 SeqNo:7465468 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 4.83 5 0.09242 94.8 80 - 120 4.853 0.457 200.200
Manganese 0.04956 0.05 0.006256 86.6 80 - 120 0.05012 1.14 200.00500
Sample ID:HS23071590-01PDS Units:mg/L Analysis Date:01-Aug-2023 21:05
Run ID:ICPMS05_442868 SeqNo:7465469 PrepDate:01-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 9.302 10 0.09242 92.1 75 - 1250.200
Manganese 0.0962 0.1 0.006256 89.9 75 - 1250.00500
ALS Houston, US Date: 03-Aug-23
Page 24 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:198376 ( 0 )Instrument:ICPMS05 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23071590-01SD Units:mg/L Analysis Date:01-Aug-2023 20:59
Run ID:ICPMS05_442868 SeqNo:7465466 PrepDate:01-Aug-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron 0.1269 0.09242 0 10 J 1.00
Manganese 0.006381 0.006256 0 10 J 0.0250
The following samples were analyzed in this batch:HS23071066-12
ALS Houston, US Date: 03-Aug-23
Page 25 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 21:30
Run ID:VOA11_442011 SeqNo:7443881 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
47.84 50 0 95.7 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.54 50 0 93.1 77 - 1131.0Surr: 4-Bromofluorobenzene
50.49 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
49.22 50 0 98.4 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 26 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 20:48
Run ID:VOA11_442011 SeqNo:7443880 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.12 20 0 90.6 73 - 1211.0
1,2-Dibromoethane 16.74 20 0 83.7 76 - 1231.0
1,2-Dichloroethane 16.44 20 0 82.2 70 - 1241.0
2-Methylnaphthalene 17.3 20 0 86.5 55 - 1401.0
4-Isopropyltoluene 17.68 20 0 88.4 74 - 1261.0
Benzene 17.13 20 0 85.7 74 - 1201.0
Chloroform 17.62 20 0 88.1 71 - 1211.0
Ethylbenzene 18.39 20 0 92.0 77 - 1171.0
m,p-Xylene 35.54 40 0 88.8 77 - 1222.0
Methyl tert-butyl ether 15.44 20 0 77.2 70 - 1301.0
Methylene chloride 20.36 20 0 102 70 - 1272.0
Naphthalene 16.79 20 0 83.9 70 - 1301.0
o-Xylene 18.76 20 0 93.8 75 - 1191.0
Tert-butyl alcohol 328.8 400 0 82.2 70 - 13010
Toluene 17.07 20 0 85.4 77 - 1181.0
Xylenes, Total 54.3 60 0 90.5 75 - 1223.0
44.23 50 0 88.5 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.18 50 0 94.4 77 - 1131.0Surr: 4-Bromofluorobenzene
49 50 0 98.0 73 - 1261.0Surr: Dibromofluoromethane
48.11 50 0 96.2 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 27 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071061-01MS Units:ug/L Analysis Date:21-Jul-2023 22:54
Run ID:VOA11_442011 SeqNo:7443885 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 17.31 20 0 86.5 70 - 1251.0
1,2-Dibromoethane 15.93 20 0 79.6 70 - 1241.0
1,2-Dichloroethane 17.11 20 0 85.6 70 - 1271.0
2-Methylnaphthalene 12.34 20 0 61.7 55 - 1401.0
4-Isopropyltoluene 16.95 20 0 84.8 70 - 1301.0
Benzene 17.76 20 0 88.8 70 - 1271.0
Chloroform 18.4 20 0 92.0 70 - 1251.0
Ethylbenzene 18.45 20 0 92.3 70 - 1241.0
m,p-Xylene 36.02 40 0 90.1 70 - 1302.0
Methyl tert-butyl ether 14.76 20 0 73.8 70 - 1301.0
Methylene chloride 18.72 20 0 93.6 70 - 1282.0
Naphthalene 14.87 20 0 74.4 70 - 1301.0
o-Xylene 17.72 20 0 88.6 70 - 1241.0
Tert-butyl alcohol 258.7 400 0 64.7 70 - 130 S10
Toluene 17.38 20 0 86.9 70 - 1231.0
Xylenes, Total 53.74 60 0 89.6 70 - 1303.0
44.87 50 0 89.7 70 - 1261.0Surr: 1,2-Dichloroethane-d4
49.63 50 0 99.3 77 - 1131.0Surr: 4-Bromofluorobenzene
48.34 50 0 96.7 77 - 1231.0Surr: Dibromofluoromethane
49.07 50 0 98.1 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 28 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442011 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071061-01MSD Units:ug/L Analysis Date:21-Jul-2023 23:15
Run ID:VOA11_442011 SeqNo:7443886 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 18.16 20 0 90.8 70 - 125 17.31 4.8 201.0
1,2-Dibromoethane 16.71 20 0 83.6 70 - 124 15.93 4.81 201.0
1,2-Dichloroethane 16.2 20 0 81.0 70 - 127 17.11 5.48 201.0
2-Methylnaphthalene 14.51 20 0 72.5 55 - 140 12.34 16.1 201.0
4-Isopropyltoluene 17.91 20 0 89.5 70 - 130 16.95 5.49 201.0
Benzene 17.26 20 0 86.3 70 - 127 17.76 2.87 201.0
Chloroform 17.7 20 0 88.5 70 - 125 18.4 3.9 201.0
Ethylbenzene 17.33 20 0 86.6 70 - 124 18.45 6.28 201.0
m,p-Xylene 36.56 40 0 91.4 70 - 130 36.02 1.49 202.0
Methyl tert-butyl ether 15.16 20 0 75.8 70 - 130 14.76 2.64 201.0
Methylene chloride 19.36 20 0 96.8 70 - 128 18.72 3.35 202.0
Naphthalene 15.95 20 0 79.7 70 - 130 14.87 6.98 201.0
o-Xylene 17.94 20 0 89.7 70 - 124 17.72 1.21 201.0
Tert-butyl alcohol 286.1 400 0 71.5 70 - 130 258.7 10.1 2010
Toluene 17.46 20 0 87.3 70 - 123 17.38 0.424 201.0
Xylenes, Total 54.5 60 0 90.8 70 - 130 53.74 1.4 203.0
45.11 50 0 90.2 70 - 126 44.87 0.532 201.0Surr: 1,2-Dichloroethane-d4
49.78 50 0 99.6 77 - 113 49.63 0.29 201.0Surr: 4-Bromofluorobenzene
49.51 50 0 99.0 77 - 123 48.34 2.39 201.0Surr: Dibromofluoromethane
50.63 50 0 101 82 - 127 49.07 3.13 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071066-01 HS23071066-02 HS23071066-03
ALS Houston, US Date: 03-Aug-23
Page 29 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442018 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 15:38
Run ID:VOA10_442018 SeqNo:7444081 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
51.71 50 0 103 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.59 50 0 91.2 77 - 1131.0Surr: 4-Bromofluorobenzene
50.85 50 0 102 73 - 1261.0Surr: Dibromofluoromethane
50.43 50 0 101 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 30 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442018 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 14:56
Run ID:VOA10_442018 SeqNo:7444080 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 21.73 20 0 109 73 - 1211.0
1,2-Dibromoethane 20.72 20 0 104 76 - 1231.0
1,2-Dichloroethane 21.04 20 0 105 70 - 1241.0
2-Methylnaphthalene 22.37 20 0 112 55 - 1401.0
4-Isopropyltoluene 24.06 20 0 120 74 - 1261.0
Benzene 18.95 20 0 94.7 74 - 1201.0
Chloroform 21.39 20 0 107 71 - 1211.0
Ethylbenzene 20.23 20 0 101 77 - 1171.0
m,p-Xylene 39.3 40 0 98.2 77 - 1222.0
Methyl tert-butyl ether 20.45 20 0 102 70 - 1301.0
Methylene chloride 21.6 20 0 108 70 - 1272.0
Naphthalene 22.76 20 0 114 70 - 1301.0
o-Xylene 19.08 20 0 95.4 75 - 1191.0
Tert-butyl alcohol 442.3 400 0 111 70 - 13010
Toluene 20.48 20 0 102 77 - 1181.0
Xylenes, Total 58.38 60 0 97.3 75 - 1223.0
51.48 50 0 103 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.49 50 0 95.0 77 - 1131.0Surr: 4-Bromofluorobenzene
52.84 50 0 106 73 - 1261.0Surr: Dibromofluoromethane
52.09 50 0 104 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 31 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442018 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071066-04MS Units:ug/L Analysis Date:21-Jul-2023 17:44
Run ID:VOA10_442018 SeqNo:7444086 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:Z2-PZ-10
1,2,4-Trimethylbenzene 21.06 20 1.694 96.8 70 - 1251.0
1,2-Dibromoethane 17.58 20 0 87.9 70 - 1241.0
1,2-Dichloroethane 18.25 20 0 91.3 70 - 1271.0
2-Methylnaphthalene 18.35 20 6.819 57.6 55 - 1401.0
4-Isopropyltoluene 22.25 20 0 111 70 - 1301.0
Benzene 18.54 20 0.5825 89.8 70 - 1271.0
Chloroform 19.38 20 0 96.9 70 - 1251.0
Ethylbenzene 22.04 20 3.096 94.7 70 - 1241.0
m,p-Xylene 37.39 40 1.203 90.5 70 - 1302.0
Methyl tert-butyl ether 17.58 20 0 87.9 70 - 1301.0
Methylene chloride 18.37 20 0 91.8 70 - 1282.0
Naphthalene 24.11 20 6.33 88.9 70 - 1301.0
o-Xylene 17.43 20 0.84 82.9 70 - 1241.0
Tert-butyl alcohol 326.9 400 0 81.7 70 - 13010
Toluene 18.74 20 0 93.7 70 - 1231.0
Xylenes, Total 54.82 60 2.043 88.0 70 - 1303.0
50.39 50 0 101 70 - 1261.0Surr: 1,2-Dichloroethane-d4
46.23 50 0 92.5 77 - 1131.0Surr: 4-Bromofluorobenzene
51.96 50 0 104 77 - 1231.0Surr: Dibromofluoromethane
50.2 50 0 100 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 32 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442018 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071066-04MSD Units:ug/L Analysis Date:21-Jul-2023 18:05
Run ID:VOA10_442018 SeqNo:7444087 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:Z2-PZ-10
1,2,4-Trimethylbenzene 21.37 20 1.694 98.4 70 - 125 21.06 1.5 201.0
1,2-Dibromoethane 17.72 20 0 88.6 70 - 124 17.58 0.742 201.0
1,2-Dichloroethane 18.01 20 0 90.1 70 - 127 18.25 1.33 201.0
2-Methylnaphthalene 19.37 20 6.819 62.7 55 - 140 18.35 5.42 201.0
4-Isopropyltoluene 22.68 20 0 113 70 - 130 22.25 1.92 201.0
Benzene 17.46 20 0.5825 84.4 70 - 127 18.54 5.96 201.0
Chloroform 18.56 20 0 92.8 70 - 125 19.38 4.34 201.0
Ethylbenzene 21.66 20 3.096 92.8 70 - 124 22.04 1.72 201.0
m,p-Xylene 35.21 40 1.203 85.0 70 - 130 37.39 6.03 202.0
Methyl tert-butyl ether 17.54 20 0 87.7 70 - 130 17.58 0.251 201.0
Methylene chloride 17.3 20 0 86.5 70 - 128 18.37 5.97 202.0
Naphthalene 25.02 20 6.33 93.4 70 - 130 24.11 3.69 201.0
o-Xylene 17.29 20 0.84 82.2 70 - 124 17.43 0.781 201.0
Tert-butyl alcohol 329.3 400 0 82.3 70 - 130 326.9 0.734 2010
Toluene 18.33 20 0 91.7 70 - 123 18.74 2.2 201.0
Xylenes, Total 52.5 60 2.043 84.1 70 - 130 54.82 4.33 203.0
51.04 50 0 102 70 - 126 50.39 1.28 201.0Surr: 1,2-Dichloroethane-d4
45.21 50 0 90.4 77 - 113 46.23 2.24 201.0Surr: 4-Bromofluorobenzene
50.25 50 0 101 77 - 123 51.96 3.35 201.0Surr: Dibromofluoromethane
51.69 50 0 103 82 - 127 50.2 2.94 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071066-04 HS23071066-05 HS23071066-06 HS23071066-07
HS23071066-08 HS23071066-09 HS23071066-10 HS23071066-11
HS23071066-12 HS23071066-13
ALS Houston, US Date: 03-Aug-23
Page 33 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442040 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-230722 Units:ug/L Analysis Date:22-Jul-2023 11:39
Run ID:VOA11_442040 SeqNo:7444536 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ethylbenzene U 1.0
46.58 50 0 93.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.41 50 0 92.8 77 - 1131.0Surr: 4-Bromofluorobenzene
47.45 50 0 94.9 73 - 1261.0Surr: Dibromofluoromethane
50.36 50 0 101 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230722 Units:ug/L Analysis Date:22-Jul-2023 10:57
Run ID:VOA11_442040 SeqNo:7444763 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ethylbenzene 19.09 20 0 95.5 77 - 1171.0
46.39 50 0 92.8 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.83 50 0 97.7 77 - 1131.0Surr: 4-Bromofluorobenzene
48.33 50 0 96.7 73 - 1261.0Surr: Dibromofluoromethane
50.25 50 0 101 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23071175-03MS Units:ug/L Analysis Date:22-Jul-2023 12:21
Run ID:VOA11_442040 SeqNo:7444764 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ethylbenzene 18.13 20 0 90.6 70 - 1241.0
45.89 50 0 91.8 70 - 1261.0Surr: 1,2-Dichloroethane-d4
48.92 50 0 97.8 77 - 1131.0Surr: 4-Bromofluorobenzene
49.35 50 0 98.7 77 - 1231.0Surr: Dibromofluoromethane
49.21 50 0 98.4 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 34 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442040 ( 0 )Instrument:VOA11 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071175-03MSD Units:ug/L Analysis Date:22-Jul-2023 12:43
Run ID:VOA11_442040 SeqNo:7444765 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ethylbenzene 17.34 20 0 86.7 70 - 124 18.13 4.42 201.0
44.54 50 0 89.1 70 - 126 45.89 2.99 201.0Surr: 1,2-Dichloroethane-d4
48.95 50 0 97.9 77 - 113 48.92 0.0486 201.0Surr: 4-Bromofluorobenzene
48.9 50 0 97.8 77 - 123 49.35 0.913 201.0Surr: Dibromofluoromethane
50.66 50 0 101 82 - 127 49.21 2.92 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071066-01
ALS Houston, US Date: 03-Aug-23
Page 35 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R441924 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442034 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442033 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.263 0.25 0 105 80 - 1200.0500
Sample ID:HS23071069-04MS Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442036 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.504 0.25 0.279 90.0 75 - 1250.0500
Sample ID:HS23071069-04MSD Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442035 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.505 0.25 0.279 90.4 75 - 125 0.504 0.198 200.0500
The following samples were analyzed in this batch:HS23071066-12
ALS Houston, US Date: 03-Aug-23
Page 36 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442706 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 04:19
Run ID:ICS-Integrion_442706 SeqNo:7460175 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 04:24
Run ID:ICS-Integrion_442706 SeqNo:7460176 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)7.902 8 0 98.8 90 - 1100.200
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:29-Jul-2023 05:51
Run ID:ICS-Integrion_442706 SeqNo:7460188 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.68 40 0 94.2 80 - 1202.00
Sample ID:HS23071063-01MS Units:mg/L Analysis Date:29-Jul-2023 04:36
Run ID:ICS-Integrion_442706 SeqNo:7460178 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.84 40 0 94.6 80 - 1202.00
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:29-Jul-2023 05:57
Run ID:ICS-Integrion_442706 SeqNo:7460189 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.69 40 0 96.7 80 - 120 37.68 2.64 202.00
Sample ID:HS23071063-01MSD Units:mg/L Analysis Date:29-Jul-2023 04:42
Run ID:ICS-Integrion_442706 SeqNo:7460179 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.8 40 0 97.0 80 - 120 37.84 2.51 202.00
The following samples were analyzed in this batch:HS23071066-12
ALS Houston, US Date: 03-Aug-23
Page 37 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R442963 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:01-Aug-2023 08:11
Run ID:ICS-Integrion_442963 SeqNo:7466487 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:01-Aug-2023 08:17
Run ID:ICS-Integrion_442963 SeqNo:7466488 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.49 20 0 97.5 90 - 1100.500
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:01-Aug-2023 09:50
Run ID:ICS-Integrion_442963 SeqNo:7466500 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 11.56 10 1.444 101 80 - 1200.500
Sample ID:HS23071029-06MS Units:mg/L Analysis Date:01-Aug-2023 08:34
Run ID:ICS-Integrion_442963 SeqNo:7466490 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 15.91 10 5.729 102 80 - 1200.500
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:01-Aug-2023 09:56
Run ID:ICS-Integrion_442963 SeqNo:7466501 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 11.99 10 1.444 105 80 - 120 11.56 3.66 200.500
Sample ID:HS23071029-06MSD Units:mg/L Analysis Date:01-Aug-2023 08:40
Run ID:ICS-Integrion_442963 SeqNo:7466491 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 15.86 10 5.729 101 80 - 120 15.91 0.28 200.500
The following samples were analyzed in this batch:HS23071066-12
ALS Houston, US Date: 03-Aug-23
Page 38 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071066
QC BATCH REPORT
Batch ID:R443058 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:WBLKW1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:03
Run ID:ManTech01_443058 SeqNo:7469107 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:11
Run ID:ManTech01_443058 SeqNo:7469108 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)975.7 1000 0 97.6 85 - 1155.00
Alkalinity, Total (As CaCO3)994.5 1000 0 99.5 85 - 1155.00
Sample ID:LCSD1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:21
Run ID:ManTech01_443058 SeqNo:7469109 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)1006 1000 0 101 85 - 115 975.7 3.04 205.00
Alkalinity, Total (As CaCO3)1027 1000 0 103 85 - 115 994.5 3.2 205.00
Sample ID:HS23071063-02DUP Units:mg/L Analysis Date:02-Aug-2023 16:45
Run ID:ManTech01_443058 SeqNo:7469113 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)450.7 449.7 0.22 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)450.7 449.7 0.22 205.00
The following samples were analyzed in this batch:HS23071066-12
ALS Houston, US Date: 03-Aug-23
Page 39 of 45
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071066
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 03-Aug-23
Page 40 of 45
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
03-Aug-23Date: ALS Houston, US
Page 41 of 45
Ragen Giga
20-Jul-2023 09:40Date/Time Received:HS23071066
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.2C/3.1C UC/C IR 31
Blue
07/20/2023 13:30
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Nilesh D. Ranchod
Date/TimeeSignatureDate/TimeeSignature
20-Jul-2023 17:1620-Jul-2023 11:50
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
2 Page(s)
COC IDs:241078/241120
ALS Houston, US 03-Aug-23Date:
Page 42 of 45
Page 43 of 45
Page 44 of 45
Page 45 of 45
August 03, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 10 sample(s) on Jul 20, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071068
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 40
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071068
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071068-01 19-Jul-2023 10:40 20-Jul-2023 09:40PMW-P-D Groundwater
HS23071068-02 19-Jul-2023 11:00 20-Jul-2023 09:40PMW-P-B Groundwater
HS23071068-03 19-Jul-2023 11:15 20-Jul-2023 09:40PMW-Q-S Groundwater
HS23071068-04 19-Jul-2023 08:45 20-Jul-2023 09:40PMW-Q-I Groundwater
HS23071068-05 19-Jul-2023 09:15 20-Jul-2023 09:40PMW-Q-D Groundwater
HS23071068-06 19-Jul-2023 09:40 20-Jul-2023 09:40PMW-Q-B Groundwater
HS23071068-07 19-Jul-2023 11:40 20-Jul-2023 09:40PMW-P-I Groundwater
HS23071068-08 19-Jul-2023 11:00 20-Jul-2023 09:40PMW-P-S Groundwater
HS23071068-09 19-Jul-2023 12:15 20-Jul-2023 09:40FMW-21 Water
HS23071068-10 19-Jul-2023 00:00 20-Jul-2023 09:40Trip Blank Water
ALS Houston, US 03-Aug-23Date:
Page 2 of 40
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071068
ECD Organics by Method SW8011
Batch ID: 198051
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GC Semivolatiles by Method RSK-175
Batch ID: R442732
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R442019
Sample ID: FMW-21 (HS23071068-09MSD)
The recovery of the Matrix Spike Duplicate (MSD) associated to this analyte was outside of the established control limits. However,
the LCS was within control limits. The failed recovery of the MSD may be due to sample matrix interference. Tert-butyl alcohol
•
Batch ID: R442018,R442056
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Metals by Method SW6020A
Batch ID: 198394
Sample ID: HS23070985-01MS
MS and MSD are for an unrelated sample•
Sample ID: HS23070985-01PDS
PDS is for an unrelated sample•
WetChemistry by Method SM2320B
Batch ID: R443058
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442963
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R442706
Sample ID: FMW-21 (HS23071068-09)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441924
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 3 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-P-D
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-01
19-Jul-2023 10:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 20:530.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 20:530.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 20:530.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 20:531.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 20:530.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 20:530.20Benzene 1.0U
1ug/L 21-Jul-2023 20:530.20Chloroform 1.0U
1ug/L 21-Jul-2023 20:530.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 20:530.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 20:530.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 20:531.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 20:530.30Naphthalene 1.0U
1ug/L 21-Jul-2023 20:530.30o-Xylene 1.0U
1ug/L 21-Jul-2023 20:5310Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 20:530.20Toluene 1.0U
1ug/L 21-Jul-2023 20:530.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 20:5310570-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 20:5390.3 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 20:5310377-123
Surr: Toluene-d8 1%REC 21-Jul-2023 20:5310382-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 13:010.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-P-B
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-02
19-Jul-2023 11:00 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 21:140.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 21:140.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 21:140.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 21:141.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 21:140.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 21:140.20Benzene 1.0U
1ug/L 21-Jul-2023 21:140.20Chloroform 1.0U
1ug/L 21-Jul-2023 21:140.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 21:140.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 21:140.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 21:141.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 21:140.30Naphthalene 1.0U
1ug/L 21-Jul-2023 21:140.30o-Xylene 1.0U
1ug/L 21-Jul-2023 21:1410Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 21:140.20Toluene 1.0U
1ug/L 21-Jul-2023 21:140.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 21:1410570-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 21:1490.5 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 21:1410477-123
Surr: Toluene-d8 1%REC 21-Jul-2023 21:1499.8 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 13:250.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-Q-S
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-03
19-Jul-2023 11:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 03:110.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 03:110.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 03:110.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 03:111.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 03:110.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 03:110.20Benzene 1.0U
1ug/L 22-Jul-2023 03:110.20Chloroform 1.0U
1ug/L 22-Jul-2023 03:110.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 03:110.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 03:110.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 03:111.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 03:110.30Naphthalene 1.0U
1ug/L 22-Jul-2023 03:110.30o-Xylene 1.0U
1ug/L 22-Jul-2023 03:1110Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 03:110.20Toluene 1.0U
1ug/L 22-Jul-2023 03:110.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 03:1110370-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 03:1191.9 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 03:1110177-123
Surr: Toluene-d8 1%REC 22-Jul-2023 03:1110082-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 13:490.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-Q-I
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-04
19-Jul-2023 08:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 03:320.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 03:320.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 03:320.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 03:321.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 03:320.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 03:320.20Benzene 1.0U
1ug/L 22-Jul-2023 03:320.20Chloroform 1.0U
1ug/L 22-Jul-2023 03:320.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 03:320.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 03:320.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 03:321.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 03:320.30Naphthalene 1.0U
1ug/L 22-Jul-2023 03:320.30o-Xylene 1.0U
1ug/L 22-Jul-2023 03:3210Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 03:320.20Toluene 1.0U
1ug/L 22-Jul-2023 03:320.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 03:3210470-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 03:3293.5 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 03:3210277-123
Surr: Toluene-d8 1%REC 22-Jul-2023 03:3210182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 14:120.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-Q-D
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-05
19-Jul-2023 09:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 03:530.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 03:530.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 03:530.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 03:531.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 03:530.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 03:530.20Benzene 1.0U
1ug/L 22-Jul-2023 03:530.20Chloroform 1.0U
1ug/L 22-Jul-2023 03:530.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 03:530.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 03:530.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 03:531.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 03:530.30Naphthalene 1.0U
1ug/L 22-Jul-2023 03:530.30o-Xylene 1.0U
1ug/L 22-Jul-2023 03:5310Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 03:530.20Toluene 1.0U
1ug/L 22-Jul-2023 03:530.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 03:5310570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 03:5389.7 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 03:5310177-123
Surr: Toluene-d8 1%REC 22-Jul-2023 03:5310482-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 16:340.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-Q-B
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-06
19-Jul-2023 09:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 04:140.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 04:140.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 04:140.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 04:141.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 04:140.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 04:140.20Benzene 1.0U
1ug/L 22-Jul-2023 04:140.20Chloroform 1.0U
1ug/L 22-Jul-2023 04:140.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 04:140.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 04:140.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 04:141.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 04:140.30Naphthalene 1.0U
1ug/L 22-Jul-2023 04:140.30o-Xylene 1.0U
1ug/L 22-Jul-2023 04:1410Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 04:140.20Toluene 1.0U
1ug/L 22-Jul-2023 04:140.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 04:1410670-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 04:1492.4 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 04:1499.3 77-123
Surr: Toluene-d8 1%REC 22-Jul-2023 04:1410082-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 16:580.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-P-I
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-07
19-Jul-2023 11:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 04:350.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 04:350.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 04:350.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 04:351.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 04:350.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 04:350.20Benzene 1.0U
1ug/L 22-Jul-2023 04:350.20Chloroform 1.0U
1ug/L 22-Jul-2023 04:350.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 04:350.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 04:350.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 04:351.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 04:350.30Naphthalene 1.0U
1ug/L 22-Jul-2023 04:350.30o-Xylene 1.0U
1ug/L 22-Jul-2023 04:3510Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 04:350.20Toluene 1.0U
1ug/L 22-Jul-2023 04:350.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 04:3510570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 04:3592.0 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 04:3510477-123
Surr: Toluene-d8 1%REC 22-Jul-2023 04:3510182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 18:430.00311,2-Dibromoethane 0.020U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-P-S
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-08
19-Jul-2023 11:00 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 04:560.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 04:560.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 04:560.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 04:561.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 04:560.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 04:560.20Benzene 1.0U
1ug/L 22-Jul-2023 04:560.20Chloroform 1.0U
1ug/L 22-Jul-2023 04:560.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 04:560.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 04:560.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 04:561.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 04:560.30Naphthalene 1.0U
1ug/L 22-Jul-2023 04:560.30o-Xylene 1.0U
1ug/L 22-Jul-2023 04:5610Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 04:560.20Toluene 1.0U
1ug/L 22-Jul-2023 04:560.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 04:5610670-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 04:5690.2 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 04:5610477-123
Surr: Toluene-d8 1%REC 22-Jul-2023 04:5699.1 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 19:070.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-21
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-09
19-Jul-2023 12:15 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 02:080.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 02:080.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 02:080.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 02:081.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 02:080.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 02:080.20Benzene 1.0U
1ug/L 22-Jul-2023 02:080.20Chloroform 1.0U
1ug/L 22-Jul-2023 02:080.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 02:080.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 02:080.20Methyl tert-butyl ether 1.095
1ug/L 22-Jul-2023 02:081.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 02:080.30Naphthalene 1.0U
1ug/L 22-Jul-2023 02:080.30o-Xylene 1.0U
20ug/L 23-Jul-2023 00:38200Tert-butyl alcohol 2007,200
1ug/L 22-Jul-2023 02:080.20Toluene 1.0U
1ug/L 22-Jul-2023 02:080.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 02:0810370-126
Surr: 1,2-Dichloroethane-d4 20%REC 23-Jul-2023 00:3810570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 02:0895.1 77-113
Surr: 4-Bromofluorobenzene 20%REC 23-Jul-2023 00:3894.3 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 02:0899.7 77-123
Surr: Dibromofluoromethane 20%REC 23-Jul-2023 00:3810577-123
Surr: Toluene-d8 1%REC 22-Jul-2023 02:0810182-127
Surr: Toluene-d8 20%REC 23-Jul-2023 00:3899.9 82-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
10ug/L 28-Jul-2023 17:481.07Methane 5.00348
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 19:300.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 02-Aug-2023
1mg/L 02-Aug-2023 21:010.0120Iron 0.2002.71
20mg/L 03-Aug-2023 12:210.0140Manganese 0.1002.78
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 09:090.200Sulfate 0.5000.770
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 03:500.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-21
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-09
19-Jul-2023 12:15 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 17:405.00Alkalinity, Bicarbonate (As
CaCO3)5.00308
1mg/L 02-Aug-2023 17:405.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:405.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:40a5.00Alkalinity, Total (As CaCO3)5.00308
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
5mg/L 21-Jul-2023 10:400.100Ferrous Iron 0.2503.70
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 40
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071068
HS23071068-10
19-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 21-Jul-2023 16:200.301,2,4-Trimethylbenzene 1.0U
1ug/L 21-Jul-2023 16:200.201,2-Dibromoethane 1.0U
1ug/L 21-Jul-2023 16:200.201,2-Dichloroethane 1.0U
1ug/L 21-Jul-2023 16:201.02-Methylnaphthalene 1.0U
1ug/L 21-Jul-2023 16:200.304-Isopropyltoluene 1.0U
1ug/L 21-Jul-2023 16:200.20Benzene 1.0U
1ug/L 21-Jul-2023 16:200.20Chloroform 1.0U
1ug/L 21-Jul-2023 16:200.30Ethylbenzene 1.0U
1ug/L 21-Jul-2023 16:200.50m,p-Xylene 2.0U
1ug/L 21-Jul-2023 16:200.20Methyl tert-butyl ether 1.0U
1ug/L 21-Jul-2023 16:201.0Methylene chloride 2.0U
1ug/L 21-Jul-2023 16:200.30Naphthalene 1.0U
1ug/L 21-Jul-2023 16:200.30o-Xylene 1.0U
1ug/L 21-Jul-2023 16:2010Tert-butyl alcohol 10U
1ug/L 21-Jul-2023 16:200.20Toluene 1.0U
1ug/L 21-Jul-2023 16:200.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 21-Jul-2023 16:2010470-126
Surr: 4-Bromofluorobenzene 1%REC 21-Jul-2023 16:2090.6 77-113
Surr: Dibromofluoromethane 1%REC 21-Jul-2023 16:2010277-123
Surr: Toluene-d8 1%REC 21-Jul-2023 16:2010182-127
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 40
Weight / Prep Log
HS23071068
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:198051
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 26 Jul 2023 07:02 End Date: 26 Jul 2023 07:02
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071068-01 35 (mL)40 mL VOA w/ HCL36.31 (mL)1.037
HS23071068-02 35 (mL)40 mL VOA w/ HCL36.73 (mL)1.049
HS23071068-03 35 (mL)40 mL VOA w/ HCL36.38 (mL)1.039
HS23071068-04 35 (mL)40 mL VOA w/ HCL36.6 (mL)1.046
HS23071068-05 35 (mL)40 mL VOA w/ HCL36.66 (mL)1.047
HS23071068-06 35 (mL)40 mL VOA w/ HCL36.62 (mL)1.046
HS23071068-07 35 (mL)40 mL VOA w/ HCL35.79 (mL)1.023
HS23071068-08 35 (mL)40 mL VOA w/ HCL36.62 (mL)1.046
HS23071068-09 35 (mL)40 mL VOA w/ HCL36.34 (mL)1.038
Batch ID:198394
Method:WATER - SW3010A 3010APrep Code:
Start Date: 02 Aug 2023 08:00 End Date: 02 Aug 2023 08:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071068-09 10 (mL)120 plastic HNO310 (mL)1
03-Aug-23Date: ALS Houston, US
Page 15 of 40
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071068
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:198051 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Water
26 Jul 2023 07:02 26 Jul 2023 19:30HS23071068-09 19 Jul 2023 12:15 1FMW-21
Batch ID:198051 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
26 Jul 2023 07:02 26 Jul 2023 13:01HS23071068-01 19 Jul 2023 10:40 1PMW-P-D
26 Jul 2023 07:02 26 Jul 2023 13:25HS23071068-02 19 Jul 2023 11:00 1PMW-P-B
26 Jul 2023 07:02 26 Jul 2023 13:49HS23071068-03 19 Jul 2023 11:15 1PMW-Q-S
26 Jul 2023 07:02 26 Jul 2023 14:12HS23071068-04 19 Jul 2023 08:45 1PMW-Q-I
26 Jul 2023 07:02 26 Jul 2023 16:34HS23071068-05 19 Jul 2023 09:15 1PMW-Q-D
26 Jul 2023 07:02 26 Jul 2023 16:58HS23071068-06 19 Jul 2023 09:40 1PMW-Q-B
26 Jul 2023 07:02 26 Jul 2023 18:43HS23071068-07 19 Jul 2023 11:40 1PMW-P-I
26 Jul 2023 07:02 26 Jul 2023 19:07HS23071068-08 19 Jul 2023 11:00 1PMW-P-S
Batch ID:198394 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Water
02 Aug 2023 08:00 03 Aug 2023 12:21HS23071068-09 19 Jul 2023 12:15 20FMW-21
02 Aug 2023 08:00 02 Aug 2023 21:01HS23071068-09 19 Jul 2023 12:15 1FMW-21
Batch ID:R441924 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Water
21 Jul 2023 10:40HS23071068-09 19 Jul 2023 12:15 5FMW-21
Batch ID:R442018 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
21 Jul 2023 16:20HS23071068-10 19 Jul 2023 00:00 1Trip Blank
Batch ID:R442018 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
21 Jul 2023 20:53HS23071068-01 19 Jul 2023 10:40 1PMW-P-D
21 Jul 2023 21:14HS23071068-02 19 Jul 2023 11:00 1PMW-P-B
Batch ID:R442019 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
22 Jul 2023 02:08HS23071068-09 19 Jul 2023 12:15 1FMW-21
Batch ID:R442019 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
22 Jul 2023 03:11HS23071068-03 19 Jul 2023 11:15 1PMW-Q-S
22 Jul 2023 03:32HS23071068-04 19 Jul 2023 08:45 1PMW-Q-I
22 Jul 2023 03:53HS23071068-05 19 Jul 2023 09:15 1PMW-Q-D
22 Jul 2023 04:14HS23071068-06 19 Jul 2023 09:40 1PMW-Q-B
22 Jul 2023 04:35HS23071068-07 19 Jul 2023 11:40 1PMW-P-I
22 Jul 2023 04:56HS23071068-08 19 Jul 2023 11:00 1PMW-P-S
Batch ID:R442056 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
23 Jul 2023 00:38HS23071068-09 19 Jul 2023 12:15 20FMW-21
Batch ID:R442706 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Water
29 Jul 2023 03:50HS23071068-09 19 Jul 2023 12:15 10FMW-21
Batch ID:R442732 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Water
28 Jul 2023 17:48HS23071068-09 19 Jul 2023 12:15 10FMW-21
03-Aug-23Date: ALS Houston, US
Page 16 of 40
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071068
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442963 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Water
01 Aug 2023 09:09HS23071068-09 19 Jul 2023 12:15 1FMW-21
Batch ID:R443058 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Water
02 Aug 2023 17:40HS23071068-09 19 Jul 2023 12:15 1FMW-21
03-Aug-23Date: ALS Houston, US
Page 17 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:198051 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-198051 Units:ug/L Analysis Date:26-Jul-2023 11:51
Run ID:ECD_13_442465 SeqNo:7454594 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-198051 Units:ug/L Analysis Date:26-Jul-2023 12:14
Run ID:ECD_13_442465 SeqNo:7454595 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1692 0.25 0 67.7 60 - 1400.020
Sample ID:LCSD-198051 Units:ug/L Analysis Date:26-Jul-2023 12:38
Run ID:ECD_13_442465 SeqNo:7454596 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1705 0.25 0 68.2 60 - 140 0.1692 0.781 200.020
The following samples were analyzed in this batch:HS23071068-01 HS23071068-02 HS23071068-03 HS23071068-04
HS23071068-05 HS23071068-06 HS23071068-07 HS23071068-08
HS23071068-09
ALS Houston, US Date: 03-Aug-23
Page 18 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442732 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230728 Units:ug/L Analysis Date:28-Jul-2023 08:00
Run ID:FID-4_442732 SeqNo:7460972 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230728 Units:ug/L Analysis Date:28-Jul-2023 08:09
Run ID:FID-4_442732 SeqNo:7460973 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.953 9.647 0 82.4 75 - 1250.500
Sample ID:LCSD-230728 Units:ug/L Analysis Date:28-Jul-2023 08:18
Run ID:FID-4_442732 SeqNo:7460974 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 8.01 9.647 0 83.0 75 - 125 7.953 0.72 300.500
The following samples were analyzed in this batch:HS23071068-09
ALS Houston, US Date: 03-Aug-23
Page 19 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:198394 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198394 Units:mg/L Analysis Date:02-Aug-2023 21:33
Run ID:ICPMS06_442976 SeqNo:7468068 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:LCS-198394 Units:mg/L Analysis Date:02-Aug-2023 20:03
Run ID:ICPMS06_442976 SeqNo:7467996 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.968 5 0 99.4 80 - 1200.200
Manganese 0.04937 0.05 0 98.7 80 - 1200.00500
Sample ID:HS23070985-01MS Units:mg/L Analysis Date:02-Aug-2023 20:11
Run ID:ICPMS06_442976 SeqNo:7468000 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 4.979 5 0.1028 97.5 80 - 1200.200
Manganese 0.6415 0.05 0.6311 20.8 80 - 120 SO 0.00500
Sample ID:HS23070985-01MSD Units:mg/L Analysis Date:02-Aug-2023 20:15
Run ID:ICPMS06_442976 SeqNo:7468002 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.122 5 0.1028 100 80 - 120 4.979 2.84 200.200
Manganese 0.6606 0.05 0.6311 59.1 80 - 120 0.6415 2.94 20 SO 0.00500
Sample ID:HS23070985-01PDS Units:mg/L Analysis Date:02-Aug-2023 20:19
Run ID:ICPMS06_442976 SeqNo:7468004 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 10.81 10 0.1028 107 75 - 1250.200
Manganese 0.6958 0.1 0.6311 64.7 75 - 125 SO 0.00500
ALS Houston, US Date: 03-Aug-23
Page 20 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:198394 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23070985-01SD Units:mg/L Analysis Date:02-Aug-2023 20:07
Run ID:ICPMS06_442976 SeqNo:7467998 PrepDate:02-Aug-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron 0.1093 0.1028 0 10 J 1.00
Manganese 0.6661 0.6311 5.54 100.0250
The following samples were analyzed in this batch:HS23071068-09
ALS Houston, US Date: 03-Aug-23
Page 21 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442018 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230721 Units:ug/L Analysis Date:21-Jul-2023 15:38
Run ID:VOA10_442018 SeqNo:7444081 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
51.71 50 0 103 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.59 50 0 91.2 77 - 1131.0Surr: 4-Bromofluorobenzene
50.85 50 0 102 73 - 1261.0Surr: Dibromofluoromethane
50.43 50 0 101 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 22 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442018 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 14:56
Run ID:VOA10_442018 SeqNo:7444080 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 21.73 20 0 109 73 - 1211.0
1,2-Dibromoethane 20.72 20 0 104 76 - 1231.0
1,2-Dichloroethane 21.04 20 0 105 70 - 1241.0
2-Methylnaphthalene 22.37 20 0 112 55 - 1401.0
4-Isopropyltoluene 24.06 20 0 120 74 - 1261.0
Benzene 18.95 20 0 94.7 74 - 1201.0
Chloroform 21.39 20 0 107 71 - 1211.0
Ethylbenzene 20.23 20 0 101 77 - 1171.0
m,p-Xylene 39.3 40 0 98.2 77 - 1222.0
Methyl tert-butyl ether 20.45 20 0 102 70 - 1301.0
Methylene chloride 21.6 20 0 108 70 - 1272.0
Naphthalene 22.76 20 0 114 70 - 1301.0
o-Xylene 19.08 20 0 95.4 75 - 1191.0
Tert-butyl alcohol 442.3 400 0 111 70 - 13010
Toluene 20.48 20 0 102 77 - 1181.0
Xylenes, Total 58.38 60 0 97.3 75 - 1223.0
51.48 50 0 103 70 - 1231.0Surr: 1,2-Dichloroethane-d4
47.49 50 0 95.0 77 - 1131.0Surr: 4-Bromofluorobenzene
52.84 50 0 106 73 - 1261.0Surr: Dibromofluoromethane
52.09 50 0 104 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 23 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442018 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071066-04MS Units:ug/L Analysis Date:21-Jul-2023 17:44
Run ID:VOA10_442018 SeqNo:7444086 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 21.06 20 1.694 96.8 70 - 1251.0
1,2-Dibromoethane 17.58 20 0 87.9 70 - 1241.0
1,2-Dichloroethane 18.25 20 0 91.3 70 - 1271.0
2-Methylnaphthalene 18.35 20 6.819 57.6 55 - 1401.0
4-Isopropyltoluene 22.25 20 0 111 70 - 1301.0
Benzene 18.54 20 0.5825 89.8 70 - 1271.0
Chloroform 19.38 20 0 96.9 70 - 1251.0
Ethylbenzene 22.04 20 3.096 94.7 70 - 1241.0
m,p-Xylene 37.39 40 1.203 90.5 70 - 1302.0
Methyl tert-butyl ether 17.58 20 0 87.9 70 - 1301.0
Methylene chloride 18.37 20 0 91.8 70 - 1282.0
Naphthalene 24.11 20 6.33 88.9 70 - 1301.0
o-Xylene 17.43 20 0.84 82.9 70 - 1241.0
Tert-butyl alcohol 326.9 400 0 81.7 70 - 13010
Toluene 18.74 20 0 93.7 70 - 1231.0
Xylenes, Total 54.82 60 2.043 88.0 70 - 1303.0
50.39 50 0 101 70 - 1261.0Surr: 1,2-Dichloroethane-d4
46.23 50 0 92.5 77 - 1131.0Surr: 4-Bromofluorobenzene
51.96 50 0 104 77 - 1231.0Surr: Dibromofluoromethane
50.2 50 0 100 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 24 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442018 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071066-04MSD Units:ug/L Analysis Date:21-Jul-2023 18:05
Run ID:VOA10_442018 SeqNo:7444087 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 21.37 20 1.694 98.4 70 - 125 21.06 1.5 201.0
1,2-Dibromoethane 17.72 20 0 88.6 70 - 124 17.58 0.742 201.0
1,2-Dichloroethane 18.01 20 0 90.1 70 - 127 18.25 1.33 201.0
2-Methylnaphthalene 19.37 20 6.819 62.7 55 - 140 18.35 5.42 201.0
4-Isopropyltoluene 22.68 20 0 113 70 - 130 22.25 1.92 201.0
Benzene 17.46 20 0.5825 84.4 70 - 127 18.54 5.96 201.0
Chloroform 18.56 20 0 92.8 70 - 125 19.38 4.34 201.0
Ethylbenzene 21.66 20 3.096 92.8 70 - 124 22.04 1.72 201.0
m,p-Xylene 35.21 40 1.203 85.0 70 - 130 37.39 6.03 202.0
Methyl tert-butyl ether 17.54 20 0 87.7 70 - 130 17.58 0.251 201.0
Methylene chloride 17.3 20 0 86.5 70 - 128 18.37 5.97 202.0
Naphthalene 25.02 20 6.33 93.4 70 - 130 24.11 3.69 201.0
o-Xylene 17.29 20 0.84 82.2 70 - 124 17.43 0.781 201.0
Tert-butyl alcohol 329.3 400 0 82.3 70 - 130 326.9 0.734 2010
Toluene 18.33 20 0 91.7 70 - 123 18.74 2.2 201.0
Xylenes, Total 52.5 60 2.043 84.1 70 - 130 54.82 4.33 203.0
51.04 50 0 102 70 - 126 50.39 1.28 201.0Surr: 1,2-Dichloroethane-d4
45.21 50 0 90.4 77 - 113 46.23 2.24 201.0Surr: 4-Bromofluorobenzene
50.25 50 0 101 77 - 123 51.96 3.35 201.0Surr: Dibromofluoromethane
51.69 50 0 103 82 - 127 50.2 2.94 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071068-01 HS23071068-02 HS23071068-10
ALS Houston, US Date: 03-Aug-23
Page 25 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230721 Units:ug/L Analysis Date:22-Jul-2023 00:23
Run ID:VOA10_442019 SeqNo:7444113 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
52.96 50 0 106 70 - 1231.0Surr: 1,2-Dichloroethane-d4
44.29 50 0 88.6 77 - 1131.0Surr: 4-Bromofluorobenzene
51.71 50 0 103 73 - 1261.0Surr: Dibromofluoromethane
50.64 50 0 101 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 26 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 23:41
Run ID:VOA10_442019 SeqNo:7444112 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 21.08 20 0 105 73 - 1211.0
1,2-Dibromoethane 20.46 20 0 102 76 - 1231.0
1,2-Dichloroethane 19.8 20 0 99.0 70 - 1241.0
2-Methylnaphthalene 21.56 20 0 108 55 - 1401.0
4-Isopropyltoluene 22.86 20 0 114 74 - 1261.0
Benzene 18.27 20 0 91.4 74 - 1201.0
Chloroform 20.48 20 0 102 71 - 1211.0
Ethylbenzene 18.6 20 0 93.0 77 - 1171.0
m,p-Xylene 37.62 40 0 94.1 77 - 1222.0
Methyl tert-butyl ether 19.47 20 0 97.4 70 - 1301.0
Methylene chloride 20.75 20 0 104 70 - 1272.0
Naphthalene 22.76 20 0 114 70 - 1301.0
o-Xylene 17.96 20 0 89.8 75 - 1191.0
Tert-butyl alcohol 423.1 400 0 106 70 - 13010
Toluene 19.87 20 0 99.3 77 - 1181.0
Xylenes, Total 55.58 60 0 92.6 75 - 1223.0
52.88 50 0 106 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.49 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
50.36 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
50.91 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 27 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071068-09MS Units:ug/L Analysis Date:22-Jul-2023 02:29
Run ID:VOA10_442019 SeqNo:7444119 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:FMW-21
1,2,4-Trimethylbenzene 18.84 20 0 94.2 70 - 1251.0
1,2-Dibromoethane 18.49 20 0 92.5 70 - 1241.0
1,2-Dichloroethane 19.22 20 0 96.1 70 - 1271.0
2-Methylnaphthalene 18.08 20 0 90.4 55 - 1401.0
4-Isopropyltoluene 19.94 20 0 99.7 70 - 1301.0
Benzene 18.11 20 0 90.6 70 - 1271.0
Chloroform 18.26 20 0 91.3 70 - 1251.0
Ethylbenzene 18.07 20 0 90.4 70 - 1241.0
m,p-Xylene 35.76 40 0 89.4 70 - 1302.0
Methyl tert-butyl ether 112.1 20 94.54 87.6 70 - 130 O1.0
Methylene chloride 18.47 20 0 92.4 70 - 1282.0
Naphthalene 20.89 20 0 104 70 - 1301.0
o-Xylene 16.72 20 0 83.6 70 - 1241.0
Tert-butyl alcohol 9952 400 9652 75.0 70 - 130 EO10
Toluene 19.09 20 0 95.4 70 - 1231.0
Xylenes, Total 52.47 60 0 87.5 70 - 1303.0
50.92 50 0 102 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.37 50 0 94.7 77 - 1131.0Surr: 4-Bromofluorobenzene
49.4 50 0 98.8 77 - 1231.0Surr: Dibromofluoromethane
50.65 50 0 101 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 28 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071068-09MSD Units:ug/L Analysis Date:22-Jul-2023 02:50
Run ID:VOA10_442019 SeqNo:7444120 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:FMW-21
1,2,4-Trimethylbenzene 18.91 20 0 94.5 70 - 125 18.84 0.372 201.0
1,2-Dibromoethane 18.84 20 0 94.2 70 - 124 18.49 1.89 201.0
1,2-Dichloroethane 18.59 20 0 92.9 70 - 127 19.22 3.35 201.0
2-Methylnaphthalene 19.43 20 0 97.2 55 - 140 18.08 7.23 201.0
4-Isopropyltoluene 20.05 20 0 100 70 - 130 19.94 0.512 201.0
Benzene 17.12 20 0 85.6 70 - 127 18.11 5.61 201.0
Chloroform 18.54 20 0 92.7 70 - 125 18.26 1.53 201.0
Ethylbenzene 17.48 20 0 87.4 70 - 124 18.07 3.29 201.0
m,p-Xylene 33.9 40 0 84.8 70 - 130 35.76 5.31 202.0
Methyl tert-butyl ether 112.1 20 94.54 87.9 70 - 130 112.1 0.0531 20 O1.0
Methylene chloride 18.08 20 0 90.4 70 - 128 18.47 2.18 202.0
Naphthalene 21.53 20 0 108 70 - 130 20.89 3.02 201.0
o-Xylene 17.01 20 0 85.0 70 - 124 16.72 1.71 201.0
Tert-butyl alcohol 10190 400 9652 135 70 - 130 9952 2.39 20 SEO10
Toluene 18.33 20 0 91.6 70 - 123 19.09 4.06 201.0
Xylenes, Total 50.91 60 0 84.8 70 - 130 52.47 3.02 203.0
49.63 50 0 99.3 70 - 126 50.92 2.56 201.0Surr: 1,2-Dichloroethane-d4
46.4 50 0 92.8 77 - 113 47.37 2.07 201.0Surr: 4-Bromofluorobenzene
49.37 50 0 98.7 77 - 123 49.4 0.0786 201.0Surr: Dibromofluoromethane
50.37 50 0 101 82 - 127 50.65 0.552 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071068-03 HS23071068-04 HS23071068-05 HS23071068-06
HS23071068-07 HS23071068-08 HS23071068-09
ALS Houston, US Date: 03-Aug-23
Page 29 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230722 Units:ug/L Analysis Date:22-Jul-2023 22:32
Run ID:VOA10_442056 SeqNo:7445003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Tert-butyl alcohol U 10
51.96 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.12 50 0 90.2 77 - 1131.0Surr: 4-Bromofluorobenzene
50.63 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
49.14 50 0 98.3 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230722 Units:ug/L Analysis Date:22-Jul-2023 21:50
Run ID:VOA10_442056 SeqNo:7445002 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Tert-butyl alcohol 356.9 400 0 89.2 70 - 13010
52.12 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.52 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
52.47 50 0 105 73 - 1261.0Surr: Dibromofluoromethane
50.46 50 0 101 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23071175-10MS Units:ug/L Analysis Date:22-Jul-2023 23:14
Run ID:VOA10_442056 SeqNo:7445005 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Tert-butyl alcohol 297.9 400 0 74.5 70 - 13010
52.12 50 0 104 70 - 1261.0Surr: 1,2-Dichloroethane-d4
45.4 50 0 90.8 77 - 1131.0Surr: 4-Bromofluorobenzene
51.12 50 0 102 77 - 1231.0Surr: Dibromofluoromethane
52.07 50 0 104 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 30 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071175-10MSD Units:ug/L Analysis Date:22-Jul-2023 23:35
Run ID:VOA10_442056 SeqNo:7445006 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Tert-butyl alcohol 291.6 400 0 72.9 70 - 130 297.9 2.11 2010
52.45 50 0 105 70 - 126 52.12 0.623 201.0Surr: 1,2-Dichloroethane-d4
47.48 50 0 95.0 77 - 113 45.4 4.49 201.0Surr: 4-Bromofluorobenzene
51.2 50 0 102 77 - 123 51.12 0.159 201.0Surr: Dibromofluoromethane
51.09 50 0 102 82 - 127 52.07 1.91 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071068-09
ALS Houston, US Date: 03-Aug-23
Page 31 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R441924 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442034 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442033 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.263 0.25 0 105 80 - 1200.0500
Sample ID:HS23071069-04MS Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442036 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.504 0.25 0.279 90.0 75 - 1250.0500
Sample ID:HS23071069-04MSD Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442035 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.505 0.25 0.279 90.4 75 - 125 0.504 0.198 200.0500
The following samples were analyzed in this batch:HS23071068-09
ALS Houston, US Date: 03-Aug-23
Page 32 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442706 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 04:19
Run ID:ICS-Integrion_442706 SeqNo:7460175 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 04:24
Run ID:ICS-Integrion_442706 SeqNo:7460176 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)7.902 8 0 98.8 90 - 1100.200
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:29-Jul-2023 05:51
Run ID:ICS-Integrion_442706 SeqNo:7460188 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.68 40 0 94.2 80 - 1202.00
Sample ID:HS23071063-01MS Units:mg/L Analysis Date:29-Jul-2023 04:36
Run ID:ICS-Integrion_442706 SeqNo:7460178 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.84 40 0 94.6 80 - 1202.00
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:29-Jul-2023 05:57
Run ID:ICS-Integrion_442706 SeqNo:7460189 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.69 40 0 96.7 80 - 120 37.68 2.64 202.00
Sample ID:HS23071063-01MSD Units:mg/L Analysis Date:29-Jul-2023 04:42
Run ID:ICS-Integrion_442706 SeqNo:7460179 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.8 40 0 97.0 80 - 120 37.84 2.51 202.00
The following samples were analyzed in this batch:HS23071068-09
ALS Houston, US Date: 03-Aug-23
Page 33 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R442963 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:01-Aug-2023 08:11
Run ID:ICS-Integrion_442963 SeqNo:7466487 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:01-Aug-2023 08:17
Run ID:ICS-Integrion_442963 SeqNo:7466488 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.49 20 0 97.5 90 - 1100.500
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:01-Aug-2023 09:50
Run ID:ICS-Integrion_442963 SeqNo:7466500 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 11.56 10 1.444 101 80 - 1200.500
Sample ID:HS23071029-06MS Units:mg/L Analysis Date:01-Aug-2023 08:34
Run ID:ICS-Integrion_442963 SeqNo:7466490 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 15.91 10 5.729 102 80 - 1200.500
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:01-Aug-2023 09:56
Run ID:ICS-Integrion_442963 SeqNo:7466501 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 11.99 10 1.444 105 80 - 120 11.56 3.66 200.500
Sample ID:HS23071029-06MSD Units:mg/L Analysis Date:01-Aug-2023 08:40
Run ID:ICS-Integrion_442963 SeqNo:7466491 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 15.86 10 5.729 101 80 - 120 15.91 0.28 200.500
The following samples were analyzed in this batch:HS23071068-09
ALS Houston, US Date: 03-Aug-23
Page 34 of 40
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071068
QC BATCH REPORT
Batch ID:R443058 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:WBLKW1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:03
Run ID:ManTech01_443058 SeqNo:7469107 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:11
Run ID:ManTech01_443058 SeqNo:7469108 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)975.7 1000 0 97.6 85 - 1155.00
Alkalinity, Total (As CaCO3)994.5 1000 0 99.5 85 - 1155.00
Sample ID:LCSD1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:21
Run ID:ManTech01_443058 SeqNo:7469109 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)1006 1000 0 101 85 - 115 975.7 3.04 205.00
Alkalinity, Total (As CaCO3)1027 1000 0 103 85 - 115 994.5 3.2 205.00
Sample ID:HS23071063-02DUP Units:mg/L Analysis Date:02-Aug-2023 16:45
Run ID:ManTech01_443058 SeqNo:7469113 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)450.7 449.7 0.22 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)450.7 449.7 0.22 205.00
The following samples were analyzed in this batch:HS23071068-09
ALS Houston, US Date: 03-Aug-23
Page 35 of 40
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071068
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 03-Aug-23
Page 36 of 40
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
03-Aug-23Date: ALS Houston, US
Page 37 of 40
Ragen Giga
20-Jul-2023 09:40Date/Time Received:HS23071068
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.5C/3.4C UC/C IR 31
49889
07/20/2023 13:30
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Nilesh D. Ranchod
Date/TimeeSignatureDate/TimeeSignature
21-Jul-2023 08:0620-Jul-2023 11:50
FedEx Priority OvernightWaterCarrier name:Matrices:
Reviewed by:/S/ Nieka.Carson
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241118
ALS Houston, US 03-Aug-23Date:
Page 38 of 40
Page 39 of 40
Page 40 of 40
August 03, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 6 sample(s) on Jul 20, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071069
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 35
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071069
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071069-01 19-Jul-2023 16:35 20-Jul-2023 09:40FPZ-10I Water
HS23071069-02 19-Jul-2023 15:55 20-Jul-2023 09:40DEM-MW6I Water
HS23071069-03 19-Jul-2023 15:00 20-Jul-2023 09:40DEM-MW6R Water
HS23071069-04 19-Jul-2023 15:25 20-Jul-2023 09:40DEM-MW6D Water
HS23071069-05 19-Jul-2023 15:35 20-Jul-2023 09:40Equipment Blank #3 Water
HS23071069-06 19-Jul-2023 00:00 20-Jul-2023 09:40Trip Blank Water
ALS Houston, US 03-Aug-23Date:
Page 2 of 35
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071069
ECD Organics by Method SW8011
Batch ID: 197848
Sample ID: MBLK-197848
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R442303
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R442056
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R442019
Sample ID: HS23071068-09MS
MS and MSD are for an unrelated sample•
Metals by Method SW6020A
Batch ID: 198394
Sample ID: HS23070985-01MS
MS and MSD are for an unrelated sample•
Sample ID: HS23070985-01PDS
PDS is for an unrelated sample•
WetChemistry by Method SM2320B
Batch ID: R443058
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442963
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 3 of 35
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071069
WetChemistry by Method E300
Batch ID: R442706
Sample ID: DEM-MW6D (HS23071069-04)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: DEM-MW6I (HS23071069-02)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: DEM-MW6R (HS23071069-03)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Equipment Blank #3 (HS23071069-05)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: FPZ-10I (HS23071069-01)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441924
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 4 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FPZ-10I
WorkOrder:
Lab ID:
Collection Date:
HS23071069
HS23071069-01
19-Jul-2023 16:35 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 05:170.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 05:170.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 05:170.201,2-Dichloroethane 1.04.2
1ug/L 22-Jul-2023 05:171.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 05:170.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 05:170.20Benzene 1.0U
1ug/L 22-Jul-2023 05:170.20Chloroform 1.0U
1ug/L 22-Jul-2023 05:170.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 05:170.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 05:170.20Methyl tert-butyl ether 1.01.8
1ug/L 22-Jul-2023 05:171.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 05:170.30Naphthalene 1.0U
1ug/L 22-Jul-2023 05:170.30o-Xylene 1.0U
1ug/L 22-Jul-2023 05:1710Tert-butyl alcohol 10190
1ug/L 22-Jul-2023 05:170.20Toluene 1.0U
1ug/L 22-Jul-2023 05:170.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 05:1710370-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 05:1792.3 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 05:1710177-123
Surr: Toluene-d8 1%REC 22-Jul-2023 05:1710282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 15:510.107Methane 0.5000.829
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 05:360.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 02-Aug-2023
1mg/L 02-Aug-2023 21:04J0.0120Iron 0.2000.0190
1mg/L 02-Aug-2023 21:04J0.000700Manganese 0.005000.00493
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 09:440.200Sulfate 0.5001.44
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 05:450.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 17:475.00Alkalinity, Bicarbonate (As
CaCO3)5.00367
1mg/L 02-Aug-2023 17:475.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:475.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:47a5.00Alkalinity, Total (As CaCO3)5.00367
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:40J0.0200Ferrous Iron 0.05000.0350
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DEM-MW6I
WorkOrder:
Lab ID:
Collection Date:
HS23071069
HS23071069-02
19-Jul-2023 15:55 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 05:380.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 05:380.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 05:380.201,2-Dichloroethane 1.0140
1ug/L 22-Jul-2023 05:381.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 05:380.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 05:380.20Benzene 1.0U
1ug/L 22-Jul-2023 05:380.20Chloroform 1.0U
1ug/L 22-Jul-2023 05:380.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 05:380.50m,p-Xylene 2.0U
25ug/L 23-Jul-2023 00:595.0Methyl tert-butyl ether 25260
1ug/L 22-Jul-2023 05:381.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 05:380.30Naphthalene 1.0U
1ug/L 22-Jul-2023 05:380.30o-Xylene 1.0U
25ug/L 23-Jul-2023 00:59250Tert-butyl alcohol 25027,000
1ug/L 22-Jul-2023 05:380.20Toluene 1.0U
1ug/L 22-Jul-2023 05:380.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 05:3810270-126
Surr: 1,2-Dichloroethane-d4 25%REC 23-Jul-2023 00:5910570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 05:3892.1 77-113
Surr: 4-Bromofluorobenzene 25%REC 23-Jul-2023 00:5988.5 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 05:3810077-123
Surr: Dibromofluoromethane 25%REC 23-Jul-2023 00:5998.9 77-123
Surr: Toluene-d8 1%REC 22-Jul-2023 05:3810382-127
Surr: Toluene-d8 25%REC 23-Jul-2023 00:5910182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
5ug/L 21-Jul-2023 17:070.535Methane 2.50142
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 05:590.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 02-Aug-2023
1mg/L 02-Aug-2023 21:06J0.0120Iron 0.2000.0786
1mg/L 02-Aug-2023 21:060.000700Manganese 0.005000.00783
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 10:010.200Sulfate 0.5001.30
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 06:030.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DEM-MW6I
WorkOrder:
Lab ID:
Collection Date:
HS23071069
HS23071069-02
19-Jul-2023 15:55 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 17:535.00Alkalinity, Bicarbonate (As
CaCO3)5.00298
1mg/L 02-Aug-2023 17:535.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:535.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 17:53a5.00Alkalinity, Total (As CaCO3)5.00298
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.05000.0550
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DEM-MW6R
WorkOrder:
Lab ID:
Collection Date:
HS23071069
HS23071069-03
19-Jul-2023 15:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 05:59J0.301,2,4-Trimethylbenzene 1.00.97
1ug/L 22-Jul-2023 05:590.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 05:590.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 05:591.02-Methylnaphthalene 1.017
1ug/L 22-Jul-2023 05:590.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 05:590.20Benzene 1.014
1ug/L 22-Jul-2023 05:590.20Chloroform 1.0U
1ug/L 22-Jul-2023 05:59J0.30Ethylbenzene 1.00.63
1ug/L 22-Jul-2023 05:59J0.50m,p-Xylene 2.00.81
1ug/L 22-Jul-2023 05:590.20Methyl tert-butyl ether 1.031
1ug/L 22-Jul-2023 05:591.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 05:590.30Naphthalene 1.019
1ug/L 22-Jul-2023 05:59J0.30o-Xylene 1.00.59
10ug/L 23-Jul-2023 01:20100Tert-butyl alcohol 1005,800
1ug/L 22-Jul-2023 05:590.20Toluene 1.0U
1ug/L 22-Jul-2023 05:59J0.30Xylenes, Total 3.01.4
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 05:5998.1 70-126
Surr: 1,2-Dichloroethane-d4 10%REC 23-Jul-2023 01:2010670-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 05:5992.9 77-113
Surr: 4-Bromofluorobenzene 10%REC 23-Jul-2023 01:2092.3 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 05:5997.6 77-123
Surr: Dibromofluoromethane 10%REC 23-Jul-2023 01:2010377-123
Surr: Toluene-d8 1%REC 22-Jul-2023 05:5910582-127
Surr: Toluene-d8 10%REC 23-Jul-2023 01:2010282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
50ug/L 21-Jul-2023 17:165.35Methane 25.01,610
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 06:220.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 02-Aug-2023
1mg/L 02-Aug-2023 21:080.0120Iron 0.2005.99
50mg/L 03-Aug-2023 12:280.0350Manganese 0.2503.76
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 10:070.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 06:090.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DEM-MW6R
WorkOrder:
Lab ID:
Collection Date:
HS23071069
HS23071069-03
19-Jul-2023 15:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 18:005.00Alkalinity, Bicarbonate (As
CaCO3)5.00532
1mg/L 02-Aug-2023 18:005.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:005.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:00a5.00Alkalinity, Total (As CaCO3)5.00532
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
10mg/L 21-Jul-2023 10:400.200Ferrous Iron 0.50010.4
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DEM-MW6D
WorkOrder:
Lab ID:
Collection Date:
HS23071069
HS23071069-04
19-Jul-2023 15:25 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 06:200.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 06:200.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 06:200.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 06:201.02-Methylnaphthalene 1.05.2
1ug/L 22-Jul-2023 06:200.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 06:200.20Benzene 1.0U
1ug/L 22-Jul-2023 06:200.20Chloroform 1.0U
1ug/L 22-Jul-2023 06:200.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 06:200.50m,p-Xylene 2.0U
20ug/L 23-Jul-2023 01:414.0Methyl tert-butyl ether 20400
1ug/L 22-Jul-2023 06:201.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 06:200.30Naphthalene 1.03.1
1ug/L 22-Jul-2023 06:200.30o-Xylene 1.0U
20ug/L 23-Jul-2023 01:41200Tert-butyl alcohol 20015,000
1ug/L 22-Jul-2023 06:200.20Toluene 1.0U
1ug/L 22-Jul-2023 06:200.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 06:2010070-126
Surr: 1,2-Dichloroethane-d4 20%REC 23-Jul-2023 01:4110570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 06:2091.2 77-113
Surr: 4-Bromofluorobenzene 20%REC 23-Jul-2023 01:4192.4 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 06:2097.1 77-123
Surr: Dibromofluoromethane 20%REC 23-Jul-2023 01:4110177-123
Surr: Toluene-d8 1%REC 22-Jul-2023 06:2099.8 82-127
Surr: Toluene-d8 20%REC 23-Jul-2023 01:4110182-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 16:460.107Methane 0.50015.6
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 06:460.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 02-Aug-2023
1mg/L 02-Aug-2023 21:100.0120Iron 0.2000.211
1mg/L 02-Aug-2023 21:100.000700Manganese 0.005000.222
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 10:130.200Sulfate 0.5000.555
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 06:140.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DEM-MW6D
WorkOrder:
Lab ID:
Collection Date:
HS23071069
HS23071069-04
19-Jul-2023 15:25 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 18:075.00Alkalinity, Bicarbonate (As
CaCO3)5.00329
1mg/L 02-Aug-2023 18:075.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:075.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:07a5.00Alkalinity, Total (As CaCO3)5.00329
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.05000.279
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Equipment Blank #3
WorkOrder:
Lab ID:
Collection Date:
HS23071069
HS23071069-05
19-Jul-2023 15:35 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 01:050.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 01:050.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 01:050.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 01:051.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 01:050.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 01:050.20Benzene 1.0U
1ug/L 22-Jul-2023 01:050.20Chloroform 1.0U
1ug/L 22-Jul-2023 01:050.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 01:050.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 01:050.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 01:051.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 01:050.30Naphthalene 1.0U
1ug/L 22-Jul-2023 01:050.30o-Xylene 1.0U
1ug/L 22-Jul-2023 01:0510Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 01:050.20Toluene 1.0U
1ug/L 22-Jul-2023 01:050.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 01:0510670-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 01:0592.8 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 01:0510377-123
Surr: Toluene-d8 1%REC 22-Jul-2023 01:0510282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 21-Jul-2023 16:590.107Methane 0.500U
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 07:090.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 02-Aug-2023
1mg/L 02-Aug-2023 21:120.0120Iron 0.200U
1mg/L 02-Aug-2023 21:120.000700Manganese 0.00500U
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 10:190.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 06:200.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 18:125.00Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:125.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:125.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:12a5.00Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.0500U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 35
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071069
HS23071069-06
19-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 01:260.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 01:260.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 01:260.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 01:261.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 01:260.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 01:260.20Benzene 1.0U
1ug/L 22-Jul-2023 01:260.20Chloroform 1.0U
1ug/L 22-Jul-2023 01:260.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 01:260.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 01:260.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 01:261.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 01:260.30Naphthalene 1.0U
1ug/L 22-Jul-2023 01:260.30o-Xylene 1.0U
1ug/L 22-Jul-2023 01:2610Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 01:260.20Toluene 1.0U
1ug/L 22-Jul-2023 01:260.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 01:2610770-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 01:2691.2 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 01:2610477-123
Surr: Toluene-d8 1%REC 22-Jul-2023 01:2610182-127
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 35
Weight / Prep Log
HS23071069
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197848
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 10:02 End Date: 21 Jul 2023 10:02
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071069-01 35 (mL)40 mL VOA w/ HCL36.76 (mL)1.05
HS23071069-02 35 (mL)40 mL VOA w/ HCL36.82 (mL)1.052
HS23071069-03 35 (mL)40 mL VOA w/ HCL37.19 (mL)1.063
HS23071069-04 35 (mL)40 mL VOA w/ HCL36.75 (mL)1.05
HS23071069-05 35 (mL)40 mL VOA w/ HCL36.03 (mL)1.029
Batch ID:198394
Method:WATER - SW3010A 3010APrep Code:
Start Date: 02 Aug 2023 08:00 End Date: 02 Aug 2023 08:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071069-01 10 (mL)120 plastic HNO310 (mL)1
HS23071069-02 10 (mL)120 plastic HNO310 (mL)1
HS23071069-03 10 (mL)120 plastic HNO310 (mL)1
HS23071069-04 10 (mL)120 plastic HNO310 (mL)1
HS23071069-05 10 (mL)120 plastic HNO310 (mL)1
03-Aug-23Date: ALS Houston, US
Page 14 of 35
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071069
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197848 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Water
21 Jul 2023 10:02 26 Jul 2023 05:36HS23071069-01 19 Jul 2023 16:35 1FPZ-10I
21 Jul 2023 10:02 26 Jul 2023 05:59HS23071069-02 19 Jul 2023 15:55 1DEM-MW6I
21 Jul 2023 10:02 26 Jul 2023 06:22HS23071069-03 19 Jul 2023 15:00 1DEM-MW6R
21 Jul 2023 10:02 26 Jul 2023 06:46HS23071069-04 19 Jul 2023 15:25 1DEM-MW6D
21 Jul 2023 10:02 26 Jul 2023 07:09HS23071069-05 19 Jul 2023 15:35 1Equipment Blank #3
Batch ID:198394 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Water
02 Aug 2023 08:00 02 Aug 2023 21:04HS23071069-01 19 Jul 2023 16:35 1FPZ-10I
02 Aug 2023 08:00 02 Aug 2023 21:06HS23071069-02 19 Jul 2023 15:55 1DEM-MW6I
02 Aug 2023 08:00 03 Aug 2023 12:28HS23071069-03 19 Jul 2023 15:00 50DEM-MW6R
02 Aug 2023 08:00 02 Aug 2023 21:08HS23071069-03 19 Jul 2023 15:00 1DEM-MW6R
02 Aug 2023 08:00 02 Aug 2023 21:10HS23071069-04 19 Jul 2023 15:25 1DEM-MW6D
02 Aug 2023 08:00 02 Aug 2023 21:12HS23071069-05 19 Jul 2023 15:35 1Equipment Blank #3
Batch ID:R441924 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Water
21 Jul 2023 10:40HS23071069-01 19 Jul 2023 16:35 1FPZ-10I
21 Jul 2023 10:40HS23071069-02 19 Jul 2023 15:55 1DEM-MW6I
21 Jul 2023 10:40HS23071069-03 19 Jul 2023 15:00 10DEM-MW6R
21 Jul 2023 10:40HS23071069-04 19 Jul 2023 15:25 1DEM-MW6D
21 Jul 2023 10:40HS23071069-05 19 Jul 2023 15:35 1Equipment Blank #3
Batch ID:R442019 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
22 Jul 2023 05:17HS23071069-01 19 Jul 2023 16:35 1FPZ-10I
22 Jul 2023 05:38HS23071069-02 19 Jul 2023 15:55 1DEM-MW6I
22 Jul 2023 05:59HS23071069-03 19 Jul 2023 15:00 1DEM-MW6R
22 Jul 2023 06:20HS23071069-04 19 Jul 2023 15:25 1DEM-MW6D
22 Jul 2023 01:05HS23071069-05 19 Jul 2023 15:35 1Equipment Blank #3
22 Jul 2023 01:26HS23071069-06 19 Jul 2023 00:00 1Trip Blank
Batch ID:R442056 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
23 Jul 2023 00:59HS23071069-02 19 Jul 2023 15:55 25DEM-MW6I
23 Jul 2023 01:20HS23071069-03 19 Jul 2023 15:00 10DEM-MW6R
23 Jul 2023 01:41HS23071069-04 19 Jul 2023 15:25 20DEM-MW6D
Batch ID:R442303 ( 1 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Water
21 Jul 2023 15:51HS23071069-01 19 Jul 2023 16:35 1FPZ-10I
21 Jul 2023 17:07HS23071069-02 19 Jul 2023 15:55 5DEM-MW6I
21 Jul 2023 17:16HS23071069-03 19 Jul 2023 15:00 50DEM-MW6R
21 Jul 2023 16:46HS23071069-04 19 Jul 2023 15:25 1DEM-MW6D
21 Jul 2023 16:59HS23071069-05 19 Jul 2023 15:35 1Equipment Blank #3
03-Aug-23Date: ALS Houston, US
Page 15 of 35
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071069
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442706 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Water
29 Jul 2023 05:45HS23071069-01 19 Jul 2023 16:35 10FPZ-10I
29 Jul 2023 06:03HS23071069-02 19 Jul 2023 15:55 10DEM-MW6I
29 Jul 2023 06:09HS23071069-03 19 Jul 2023 15:00 10DEM-MW6R
29 Jul 2023 06:14HS23071069-04 19 Jul 2023 15:25 10DEM-MW6D
29 Jul 2023 06:20HS23071069-05 19 Jul 2023 15:35 10Equipment Blank #3
Batch ID:R442963 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Water
01 Aug 2023 09:44HS23071069-01 19 Jul 2023 16:35 1FPZ-10I
01 Aug 2023 10:01HS23071069-02 19 Jul 2023 15:55 1DEM-MW6I
01 Aug 2023 10:07HS23071069-03 19 Jul 2023 15:00 1DEM-MW6R
01 Aug 2023 10:13HS23071069-04 19 Jul 2023 15:25 1DEM-MW6D
01 Aug 2023 10:19HS23071069-05 19 Jul 2023 15:35 1Equipment Blank #3
Batch ID:R443058 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Water
02 Aug 2023 17:47HS23071069-01 19 Jul 2023 16:35 1FPZ-10I
02 Aug 2023 17:53HS23071069-02 19 Jul 2023 15:55 1DEM-MW6I
02 Aug 2023 18:00HS23071069-03 19 Jul 2023 15:00 1DEM-MW6R
02 Aug 2023 18:07HS23071069-04 19 Jul 2023 15:25 1DEM-MW6D
02 Aug 2023 18:12HS23071069-05 19 Jul 2023 15:35 1Equipment Blank #3
03-Aug-23Date: ALS Houston, US
Page 16 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:197848 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197848 Units:ug/L Analysis Date:25-Jul-2023 23:22
Run ID:ECD_13_442420 SeqNo:7453289 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197848 Units:ug/L Analysis Date:25-Jul-2023 23:45
Run ID:ECD_13_442420 SeqNo:7453290 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1651 0.25 0 66.0 60 - 1400.020
Sample ID:LCSD-197848 Units:ug/L Analysis Date:26-Jul-2023 00:09
Run ID:ECD_13_442420 SeqNo:7453291 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1873 0.25 0 74.9 60 - 140 0.1651 12.6 200.020
The following samples were analyzed in this batch:HS23071069-01 HS23071069-02 HS23071069-03 HS23071069-04
HS23071069-05
ALS Houston, US Date: 03-Aug-23
Page 17 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R442303 ( 1 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230721 Units:ug/L Analysis Date:21-Jul-2023 14:22
Run ID:FID-4_442303 SeqNo:7450742 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230721 Units:ug/L Analysis Date:21-Jul-2023 14:32
Run ID:FID-4_442303 SeqNo:7450743 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.86 9.647 0 81.5 75 - 1250.500
Sample ID:LCSD-230721 Units:ug/L Analysis Date:21-Jul-2023 14:47
Run ID:FID-4_442303 SeqNo:7450744 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 8.056 9.647 0 83.5 75 - 125 7.86 2.47 300.500
Sample ID:HS23071069-04DUP Units:ug/L Analysis Date:21-Jul-2023 19:32
Run ID:FID-4_442303 SeqNo:7450769 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:DEM-MW6D
Methane 15.63 15.58 0.335 300.500
The following samples were analyzed in this batch:HS23071069-01 HS23071069-02 HS23071069-03 HS23071069-04
HS23071069-05
ALS Houston, US Date: 03-Aug-23
Page 18 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:198394 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198394 Units:mg/L Analysis Date:02-Aug-2023 21:33
Run ID:ICPMS06_442976 SeqNo:7468068 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:LCS-198394 Units:mg/L Analysis Date:02-Aug-2023 20:03
Run ID:ICPMS06_442976 SeqNo:7467996 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.968 5 0 99.4 80 - 1200.200
Manganese 0.04937 0.05 0 98.7 80 - 1200.00500
Sample ID:HS23070985-01MS Units:mg/L Analysis Date:02-Aug-2023 20:11
Run ID:ICPMS06_442976 SeqNo:7468000 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 4.979 5 0.1028 97.5 80 - 1200.200
Manganese 0.6415 0.05 0.6311 20.8 80 - 120 SO 0.00500
Sample ID:HS23070985-01MSD Units:mg/L Analysis Date:02-Aug-2023 20:15
Run ID:ICPMS06_442976 SeqNo:7468002 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.122 5 0.1028 100 80 - 120 4.979 2.84 200.200
Manganese 0.6606 0.05 0.6311 59.1 80 - 120 0.6415 2.94 20 SO 0.00500
Sample ID:HS23070985-01PDS Units:mg/L Analysis Date:02-Aug-2023 20:19
Run ID:ICPMS06_442976 SeqNo:7468004 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 10.81 10 0.1028 107 75 - 1250.200
Manganese 0.6958 0.1 0.6311 64.7 75 - 125 SO 0.00500
ALS Houston, US Date: 03-Aug-23
Page 19 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:198394 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23070985-01SD Units:mg/L Analysis Date:02-Aug-2023 20:07
Run ID:ICPMS06_442976 SeqNo:7467998 PrepDate:02-Aug-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron 0.1093 0.1028 0 10 J 1.00
Manganese 0.6661 0.6311 5.54 100.0250
The following samples were analyzed in this batch:HS23071069-01 HS23071069-02 HS23071069-03 HS23071069-04
HS23071069-05
ALS Houston, US Date: 03-Aug-23
Page 20 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230721 Units:ug/L Analysis Date:22-Jul-2023 00:23
Run ID:VOA10_442019 SeqNo:7444113 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
52.96 50 0 106 70 - 1231.0Surr: 1,2-Dichloroethane-d4
44.29 50 0 88.6 77 - 1131.0Surr: 4-Bromofluorobenzene
51.71 50 0 103 73 - 1261.0Surr: Dibromofluoromethane
50.64 50 0 101 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 21 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 23:41
Run ID:VOA10_442019 SeqNo:7444112 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 21.08 20 0 105 73 - 1211.0
1,2-Dibromoethane 20.46 20 0 102 76 - 1231.0
1,2-Dichloroethane 19.8 20 0 99.0 70 - 1241.0
2-Methylnaphthalene 21.56 20 0 108 55 - 1401.0
4-Isopropyltoluene 22.86 20 0 114 74 - 1261.0
Benzene 18.27 20 0 91.4 74 - 1201.0
Chloroform 20.48 20 0 102 71 - 1211.0
Ethylbenzene 18.6 20 0 93.0 77 - 1171.0
m,p-Xylene 37.62 40 0 94.1 77 - 1222.0
Methyl tert-butyl ether 19.47 20 0 97.4 70 - 1301.0
Methylene chloride 20.75 20 0 104 70 - 1272.0
Naphthalene 22.76 20 0 114 70 - 1301.0
o-Xylene 17.96 20 0 89.8 75 - 1191.0
Tert-butyl alcohol 423.1 400 0 106 70 - 13010
Toluene 19.87 20 0 99.3 77 - 1181.0
Xylenes, Total 55.58 60 0 92.6 75 - 1223.0
52.88 50 0 106 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.49 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
50.36 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
50.91 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 22 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071068-09MS Units:ug/L Analysis Date:22-Jul-2023 02:29
Run ID:VOA10_442019 SeqNo:7444119 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 18.84 20 0 94.2 70 - 1251.0
1,2-Dibromoethane 18.49 20 0 92.5 70 - 1241.0
1,2-Dichloroethane 19.22 20 0 96.1 70 - 1271.0
2-Methylnaphthalene 18.08 20 0 90.4 55 - 1401.0
4-Isopropyltoluene 19.94 20 0 99.7 70 - 1301.0
Benzene 18.11 20 0 90.6 70 - 1271.0
Chloroform 18.26 20 0 91.3 70 - 1251.0
Ethylbenzene 18.07 20 0 90.4 70 - 1241.0
m,p-Xylene 35.76 40 0 89.4 70 - 1302.0
Methyl tert-butyl ether 112.1 20 94.54 87.6 70 - 130 O1.0
Methylene chloride 18.47 20 0 92.4 70 - 1282.0
Naphthalene 20.89 20 0 104 70 - 1301.0
o-Xylene 16.72 20 0 83.6 70 - 1241.0
Tert-butyl alcohol 9952 400 9652 75.0 70 - 130 EO10
Toluene 19.09 20 0 95.4 70 - 1231.0
Xylenes, Total 52.47 60 0 87.5 70 - 1303.0
50.92 50 0 102 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.37 50 0 94.7 77 - 1131.0Surr: 4-Bromofluorobenzene
49.4 50 0 98.8 77 - 1231.0Surr: Dibromofluoromethane
50.65 50 0 101 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 23 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071068-09MSD Units:ug/L Analysis Date:22-Jul-2023 02:50
Run ID:VOA10_442019 SeqNo:7444120 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 18.91 20 0 94.5 70 - 125 18.84 0.372 201.0
1,2-Dibromoethane 18.84 20 0 94.2 70 - 124 18.49 1.89 201.0
1,2-Dichloroethane 18.59 20 0 92.9 70 - 127 19.22 3.35 201.0
2-Methylnaphthalene 19.43 20 0 97.2 55 - 140 18.08 7.23 201.0
4-Isopropyltoluene 20.05 20 0 100 70 - 130 19.94 0.512 201.0
Benzene 17.12 20 0 85.6 70 - 127 18.11 5.61 201.0
Chloroform 18.54 20 0 92.7 70 - 125 18.26 1.53 201.0
Ethylbenzene 17.48 20 0 87.4 70 - 124 18.07 3.29 201.0
m,p-Xylene 33.9 40 0 84.8 70 - 130 35.76 5.31 202.0
Methyl tert-butyl ether 112.1 20 94.54 87.9 70 - 130 112.1 0.0531 20 O1.0
Methylene chloride 18.08 20 0 90.4 70 - 128 18.47 2.18 202.0
Naphthalene 21.53 20 0 108 70 - 130 20.89 3.02 201.0
o-Xylene 17.01 20 0 85.0 70 - 124 16.72 1.71 201.0
Tert-butyl alcohol 10190 400 9652 135 70 - 130 9952 2.39 20 SEO10
Toluene 18.33 20 0 91.6 70 - 123 19.09 4.06 201.0
Xylenes, Total 50.91 60 0 84.8 70 - 130 52.47 3.02 203.0
49.63 50 0 99.3 70 - 126 50.92 2.56 201.0Surr: 1,2-Dichloroethane-d4
46.4 50 0 92.8 77 - 113 47.37 2.07 201.0Surr: 4-Bromofluorobenzene
49.37 50 0 98.7 77 - 123 49.4 0.0786 201.0Surr: Dibromofluoromethane
50.37 50 0 101 82 - 127 50.65 0.552 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071069-01 HS23071069-02 HS23071069-03 HS23071069-04
HS23071069-05 HS23071069-06
ALS Houston, US Date: 03-Aug-23
Page 24 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230722 Units:ug/L Analysis Date:22-Jul-2023 22:32
Run ID:VOA10_442056 SeqNo:7445003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methyl tert-butyl ether U 1.0
Tert-butyl alcohol U 10
51.96 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.12 50 0 90.2 77 - 1131.0Surr: 4-Bromofluorobenzene
50.63 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
49.14 50 0 98.3 81 - 1201.0Surr: Toluene-d8
Sample ID:VLCSW-230722 Units:ug/L Analysis Date:22-Jul-2023 21:50
Run ID:VOA10_442056 SeqNo:7445002 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methyl tert-butyl ether 17.6 20 0 88.0 70 - 1301.0
Tert-butyl alcohol 356.9 400 0 89.2 70 - 13010
52.12 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.52 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
52.47 50 0 105 73 - 1261.0Surr: Dibromofluoromethane
50.46 50 0 101 81 - 1201.0Surr: Toluene-d8
Sample ID:HS23071175-10MS Units:ug/L Analysis Date:22-Jul-2023 23:14
Run ID:VOA10_442056 SeqNo:7445005 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Methyl tert-butyl ether 17.58 20 0 87.9 70 - 1301.0
Tert-butyl alcohol 297.9 400 0 74.5 70 - 13010
52.12 50 0 104 70 - 1261.0Surr: 1,2-Dichloroethane-d4
45.4 50 0 90.8 77 - 1131.0Surr: 4-Bromofluorobenzene
51.12 50 0 102 77 - 1231.0Surr: Dibromofluoromethane
52.07 50 0 104 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 25 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071175-10MSD Units:ug/L Analysis Date:22-Jul-2023 23:35
Run ID:VOA10_442056 SeqNo:7445006 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Methyl tert-butyl ether 16.61 20 0 83.0 70 - 130 17.58 5.67 201.0
Tert-butyl alcohol 291.6 400 0 72.9 70 - 130 297.9 2.11 2010
52.45 50 0 105 70 - 126 52.12 0.623 201.0Surr: 1,2-Dichloroethane-d4
47.48 50 0 95.0 77 - 113 45.4 4.49 201.0Surr: 4-Bromofluorobenzene
51.2 50 0 102 77 - 123 51.12 0.159 201.0Surr: Dibromofluoromethane
51.09 50 0 102 82 - 127 52.07 1.91 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071069-02 HS23071069-03 HS23071069-04
ALS Houston, US Date: 03-Aug-23
Page 26 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R441924 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442034 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442033 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.263 0.25 0 105 80 - 1200.0500
Sample ID:HS23071069-04MS Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442036 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:DEM-MW6D
Ferrous Iron 0.504 0.25 0.279 90.0 75 - 1250.0500
Sample ID:HS23071069-04MSD Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442035 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:DEM-MW6D
Ferrous Iron 0.505 0.25 0.279 90.4 75 - 125 0.504 0.198 200.0500
The following samples were analyzed in this batch:HS23071069-01 HS23071069-02 HS23071069-03 HS23071069-04
HS23071069-05
ALS Houston, US Date: 03-Aug-23
Page 27 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R442706 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 04:19
Run ID:ICS-Integrion_442706 SeqNo:7460175 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 04:24
Run ID:ICS-Integrion_442706 SeqNo:7460176 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)7.902 8 0 98.8 90 - 1100.200
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:29-Jul-2023 05:51
Run ID:ICS-Integrion_442706 SeqNo:7460188 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:FPZ-10I
Nitrate/Nitrite (as N)37.68 40 0 94.2 80 - 1202.00
Sample ID:HS23071063-01MS Units:mg/L Analysis Date:29-Jul-2023 04:36
Run ID:ICS-Integrion_442706 SeqNo:7460178 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.84 40 0 94.6 80 - 1202.00
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:29-Jul-2023 05:57
Run ID:ICS-Integrion_442706 SeqNo:7460189 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:FPZ-10I
Nitrate/Nitrite (as N)38.69 40 0 96.7 80 - 120 37.68 2.64 202.00
Sample ID:HS23071063-01MSD Units:mg/L Analysis Date:29-Jul-2023 04:42
Run ID:ICS-Integrion_442706 SeqNo:7460179 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.8 40 0 97.0 80 - 120 37.84 2.51 202.00
The following samples were analyzed in this batch:HS23071069-01 HS23071069-02 HS23071069-03 HS23071069-04
HS23071069-05
ALS Houston, US Date: 03-Aug-23
Page 28 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R442963 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:01-Aug-2023 08:11
Run ID:ICS-Integrion_442963 SeqNo:7466487 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:01-Aug-2023 08:17
Run ID:ICS-Integrion_442963 SeqNo:7466488 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.49 20 0 97.5 90 - 1100.500
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:01-Aug-2023 09:50
Run ID:ICS-Integrion_442963 SeqNo:7466500 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:FPZ-10I
Sulfate 11.56 10 1.444 101 80 - 1200.500
Sample ID:HS23071029-06MS Units:mg/L Analysis Date:01-Aug-2023 08:34
Run ID:ICS-Integrion_442963 SeqNo:7466490 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 15.91 10 5.729 102 80 - 1200.500
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:01-Aug-2023 09:56
Run ID:ICS-Integrion_442963 SeqNo:7466501 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:FPZ-10I
Sulfate 11.99 10 1.444 105 80 - 120 11.56 3.66 200.500
Sample ID:HS23071029-06MSD Units:mg/L Analysis Date:01-Aug-2023 08:40
Run ID:ICS-Integrion_442963 SeqNo:7466491 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 15.86 10 5.729 101 80 - 120 15.91 0.28 200.500
The following samples were analyzed in this batch:HS23071069-01 HS23071069-02 HS23071069-03 HS23071069-04
HS23071069-05
ALS Houston, US Date: 03-Aug-23
Page 29 of 35
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071069
QC BATCH REPORT
Batch ID:R443058 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:WBLKW1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:03
Run ID:ManTech01_443058 SeqNo:7469107 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:11
Run ID:ManTech01_443058 SeqNo:7469108 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)975.7 1000 0 97.6 85 - 1155.00
Alkalinity, Total (As CaCO3)994.5 1000 0 99.5 85 - 1155.00
Sample ID:LCSD1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:21
Run ID:ManTech01_443058 SeqNo:7469109 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)1006 1000 0 101 85 - 115 975.7 3.04 205.00
Alkalinity, Total (As CaCO3)1027 1000 0 103 85 - 115 994.5 3.2 205.00
Sample ID:HS23071063-02DUP Units:mg/L Analysis Date:02-Aug-2023 16:45
Run ID:ManTech01_443058 SeqNo:7469113 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)450.7 449.7 0.22 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)450.7 449.7 0.22 205.00
The following samples were analyzed in this batch:HS23071069-01 HS23071069-02 HS23071069-03 HS23071069-04
HS23071069-05
ALS Houston, US Date: 03-Aug-23
Page 30 of 35
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071069
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 03-Aug-23
Page 31 of 35
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
03-Aug-23Date: ALS Houston, US
Page 32 of 35
Ragen Giga
20-Jul-2023 09:40Date/Time Received:HS23071069
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.6UC/3.5C IR31
Blue
07/120/2023
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Ragen Giga
Date/TimeeSignatureDate/TimeeSignature
21-Jul-2023 08:0520-Jul-2023 18:34
FedEx Priority OvernightWCarrier name:Matrices:
Reviewed by:/S/ Nieka.Carson
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241122
ALS Houston, US 03-Aug-23Date:
Page 33 of 35
Page 34 of 35
Page 35 of 35
August 03, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 10 sample(s) on Jul 20, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071072
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 45
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071072
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071072-01 19-Jul-2023 09:05 20-Jul-2023 09:40PMW-O-I Groundwater
HS23071072-02 19-Jul-2023 09:30 20-Jul-2023 09:40PMW-O-D Groundwater
HS23071072-03 19-Jul-2023 10:00 20-Jul-2023 09:40PMW-O-B Groundwater
HS23071072-04 19-Jul-2023 10:30 20-Jul-2023 09:40AMW-11S Groundwater
HS23071072-05 19-Jul-2023 11:15 20-Jul-2023 09:40AMW-13I Groundwater
HS23071072-06 19-Jul-2023 11:45 20-Jul-2023 09:40AMW-13D Groundwater
HS23071072-07 19-Jul-2023 12:20 20-Jul-2023 09:40AMW-13S Groundwater
HS23071072-08 19-Jul-2023 12:45 20-Jul-2023 09:40AMW-13B Groundwater
HS23071072-09 19-Jul-2023 14:05 20-Jul-2023 09:40FMW-23R Groundwater
HS23071072-10 19-Jul-2023 00:00 20-Jul-2023 09:40Trip Blank Water
ALS Houston, US 03-Aug-23Date:
Page 2 of 45
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071072
ECD Organics by Method SW8011
Batch ID: 198051
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: 197848
Sample ID: MBLK-197848
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method RSK-175
Batch ID: R442316
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R442082
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R442053
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R442019
Sample ID: HS23071068-09MS
MS and MSD are for an unrelated sample•
Metals by Method SW6020A
Batch ID: 198394
Sample ID: HS23070985-01MS
MS and MSD are for an unrelated sample•
Sample ID: HS23070985-01PDS
PDS is for an unrelated sample•
WetChemistry by Method SM2320B
Batch ID: R443058
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R442966
Sample ID: HS23071215-03MS
MS and MSD are for an unrelated sample (Sulfate)•
ALS Houston, US 03-Aug-23Date:
Page 3 of 45
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071072
WetChemistry by Method E300
Batch ID: R442963
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R442706
Sample ID: AMW-13B (HS23071072-08)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: AMW-13S (HS23071072-07)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: FMW-23R (HS23071072-09)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
WetChemistry by Method SM3500FED
Batch ID: R441924
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 03-Aug-23Date:
Page 4 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-O-I
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-01
19-Jul-2023 09:05 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 24-Jul-2023 16:220.301,2,4-Trimethylbenzene 1.0U
1ug/L 24-Jul-2023 16:220.201,2-Dibromoethane 1.0U
1ug/L 24-Jul-2023 16:220.201,2-Dichloroethane 1.0U
1ug/L 24-Jul-2023 16:221.02-Methylnaphthalene 1.06.7
1ug/L 24-Jul-2023 16:220.304-Isopropyltoluene 1.0U
1ug/L 24-Jul-2023 16:220.20Benzene 1.0U
1ug/L 24-Jul-2023 16:220.20Chloroform 1.0U
1ug/L 24-Jul-2023 16:220.30Ethylbenzene 1.0U
1ug/L 24-Jul-2023 16:220.50m,p-Xylene 2.0U
1ug/L 24-Jul-2023 16:220.20Methyl tert-butyl ether 1.0U
1ug/L 24-Jul-2023 16:221.0Methylene chloride 2.0U
1ug/L 24-Jul-2023 16:220.30Naphthalene 1.03.6
1ug/L 24-Jul-2023 16:220.30o-Xylene 1.0U
1ug/L 24-Jul-2023 16:2210Tert-butyl alcohol 10220
1ug/L 24-Jul-2023 16:220.20Toluene 1.0U
1ug/L 24-Jul-2023 16:220.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 24-Jul-2023 16:2210970-126
Surr: 4-Bromofluorobenzene 1%REC 24-Jul-2023 16:2291.3 77-113
Surr: Dibromofluoromethane 1%REC 24-Jul-2023 16:2210377-123
Surr: Toluene-d8 1%REC 24-Jul-2023 16:2210382-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 08:420.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-O-D
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-02
19-Jul-2023 09:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 07:020.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 07:020.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 07:020.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 07:021.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 07:020.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 07:020.20Benzene 1.0U
1ug/L 22-Jul-2023 07:020.20Chloroform 1.0U
1ug/L 22-Jul-2023 07:020.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 07:020.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 07:020.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 07:021.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 07:020.30Naphthalene 1.0U
1ug/L 22-Jul-2023 07:020.30o-Xylene 1.0U
1ug/L 22-Jul-2023 07:0210Tert-butyl alcohol 10560
1ug/L 22-Jul-2023 07:020.20Toluene 1.0U
1ug/L 22-Jul-2023 07:020.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 07:0210170-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 07:0290.9 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 07:0210077-123
Surr: Toluene-d8 1%REC 22-Jul-2023 07:0298.3 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 09:060.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-O-B
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-03
19-Jul-2023 10:00 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 07:230.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 07:230.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 07:230.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 07:231.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 07:230.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 07:230.20Benzene 1.0U
1ug/L 22-Jul-2023 07:230.20Chloroform 1.0U
1ug/L 22-Jul-2023 07:230.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 07:230.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 07:230.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 07:231.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 07:230.30Naphthalene 1.0U
1ug/L 22-Jul-2023 07:230.30o-Xylene 1.0U
1ug/L 22-Jul-2023 07:2310Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 07:230.20Toluene 1.0U
1ug/L 22-Jul-2023 07:230.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 07:2310570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 07:2388.9 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 07:2310277-123
Surr: Toluene-d8 1%REC 22-Jul-2023 07:2310582-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 09:290.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-11S
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-04
19-Jul-2023 10:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 07:440.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 07:440.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 07:440.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 07:441.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 07:440.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 07:440.20Benzene 1.02.6
1ug/L 22-Jul-2023 07:440.20Chloroform 1.0U
1ug/L 22-Jul-2023 07:440.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 07:440.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 07:440.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 07:441.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 07:440.30Naphthalene 1.0U
1ug/L 22-Jul-2023 07:440.30o-Xylene 1.0U
1ug/L 22-Jul-2023 07:4410Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 07:440.20Toluene 1.0U
1ug/L 22-Jul-2023 07:440.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 07:4410470-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 07:4492.3 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 07:4410477-123
Surr: Toluene-d8 1%REC 22-Jul-2023 07:4410382-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 09:530.00321,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-13I
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-05
19-Jul-2023 11:15 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 08:050.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 08:050.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 08:050.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 08:051.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 08:050.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 08:050.20Benzene 1.0U
1ug/L 22-Jul-2023 08:050.20Chloroform 1.0U
1ug/L 22-Jul-2023 08:050.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 08:050.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 08:050.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 08:051.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 08:050.30Naphthalene 1.0U
1ug/L 22-Jul-2023 08:050.30o-Xylene 1.0U
1ug/L 22-Jul-2023 08:0510Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 08:050.20Toluene 1.0U
1ug/L 22-Jul-2023 08:050.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 08:0510370-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 08:0590.3 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 08:0510177-123
Surr: Toluene-d8 1%REC 22-Jul-2023 08:0510282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 21-Jul-2023
1ug/L 26-Jul-2023 10:160.00321,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-13D
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-06
19-Jul-2023 11:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 16:350.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 16:350.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 16:350.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 16:351.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 16:350.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 16:350.20Benzene 1.0U
1ug/L 22-Jul-2023 16:350.20Chloroform 1.0U
1ug/L 22-Jul-2023 16:350.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 16:350.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 16:350.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 16:351.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 16:350.30Naphthalene 1.0U
1ug/L 22-Jul-2023 16:350.30o-Xylene 1.0U
1ug/L 22-Jul-2023 16:3510Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 16:350.20Toluene 1.0U
1ug/L 22-Jul-2023 16:350.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 16:3510470-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 16:3587.7 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 16:3510377-123
Surr: Toluene-d8 1%REC 22-Jul-2023 16:3510582-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 19:540.00311,2-Dibromoethane 0.021U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-13S
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-07
19-Jul-2023 12:20 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 16:56J0.301,2,4-Trimethylbenzene 1.00.90
1ug/L 22-Jul-2023 16:560.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 16:560.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 16:561.02-Methylnaphthalene 1.08.3
1ug/L 22-Jul-2023 16:560.304-Isopropyltoluene 1.0U
10ug/L 24-Jul-2023 14:372.0Benzene 10260
1ug/L 22-Jul-2023 16:560.20Chloroform 1.0U
1ug/L 22-Jul-2023 16:560.30Ethylbenzene 1.04.5
1ug/L 22-Jul-2023 16:560.50m,p-Xylene 2.04.3
1ug/L 22-Jul-2023 16:560.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 16:561.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 16:560.30Naphthalene 1.013
1ug/L 22-Jul-2023 16:560.30o-Xylene 1.01.1
1ug/L 22-Jul-2023 16:5610Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 16:560.20Toluene 1.03.6
1ug/L 22-Jul-2023 16:560.30Xylenes, Total 3.05.4
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 16:5610070-126
Surr: 1,2-Dichloroethane-d4 10%REC 24-Jul-2023 14:3710470-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 16:5696.9 77-113
Surr: 4-Bromofluorobenzene 10%REC 24-Jul-2023 14:3793.1 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 16:5695.9 77-123
Surr: Dibromofluoromethane 10%REC 24-Jul-2023 14:3710177-123
Surr: Toluene-d8 1%REC 22-Jul-2023 16:5610582-127
Surr: Toluene-d8 10%REC 24-Jul-2023 14:3710282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
50ug/L 22-Jul-2023 13:515.35Methane 25.01,730
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 20:180.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 02-Aug-2023
1mg/L 02-Aug-2023 21:180.0120Iron 0.2004.79
1mg/L 02-Aug-2023 21:180.000700Manganese 0.005001.52
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 10:250.200Sulfate 0.5000.629
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 06:260.300Nitrate/Nitrite (as N)2.00U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-13S
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-07
19-Jul-2023 12:20 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 18:355.00Alkalinity, Bicarbonate (As
CaCO3)5.00421
1mg/L 02-Aug-2023 18:355.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:355.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:35a5.00Alkalinity, Total (As CaCO3)5.00421
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.05000.659
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-13B
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-08
19-Jul-2023 12:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 17:170.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 17:170.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 17:170.201,2-Dichloroethane 1.022
1ug/L 22-Jul-2023 17:171.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 17:170.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 17:170.20Benzene 1.0U
1ug/L 22-Jul-2023 17:170.20Chloroform 1.0U
1ug/L 22-Jul-2023 17:170.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 17:170.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 17:170.20Methyl tert-butyl ether 1.017
1ug/L 22-Jul-2023 17:171.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 17:170.30Naphthalene 1.02.5
1ug/L 22-Jul-2023 17:170.30o-Xylene 1.0U
1ug/L 22-Jul-2023 17:1710Tert-butyl alcohol 101,900
1ug/L 22-Jul-2023 17:170.20Toluene 1.0U
1ug/L 22-Jul-2023 17:170.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 17:1710570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 17:1792.3 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 17:1798.4 77-123
Surr: Toluene-d8 1%REC 22-Jul-2023 17:1710282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 22-Jul-2023 13:290.107Methane 0.50025.2
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 20:410.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 02-Aug-2023
1mg/L 02-Aug-2023 21:200.0120Iron 0.200U
1mg/L 02-Aug-2023 21:200.000700Manganese 0.005000.0757
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 10:310.200Sulfate 0.5001.89
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 06:320.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 18:415.00Alkalinity, Bicarbonate (As
CaCO3)5.00242
1mg/L 02-Aug-2023 18:415.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:415.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:41a5.00Alkalinity, Total (As CaCO3)5.00242
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.0500U
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-23R
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-09
19-Jul-2023 14:05 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 17:380.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 17:380.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 17:380.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 17:381.02-Methylnaphthalene 1.04.4
1ug/L 22-Jul-2023 17:380.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 17:380.20Benzene 1.04.9
1ug/L 22-Jul-2023 17:380.20Chloroform 1.0U
1ug/L 22-Jul-2023 17:380.30Ethylbenzene 1.09.8
1ug/L 22-Jul-2023 17:38J0.50m,p-Xylene 2.01.5
1ug/L 22-Jul-2023 17:380.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 17:381.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 17:380.30Naphthalene 1.06.1
1ug/L 22-Jul-2023 17:38J0.30o-Xylene 1.00.63
1ug/L 22-Jul-2023 17:3810Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 17:380.20Toluene 1.0U
1ug/L 22-Jul-2023 17:38J0.30Xylenes, Total 3.02.1
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 17:3810270-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 17:3892.7 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 17:3810077-123
Surr: Toluene-d8 1%REC 22-Jul-2023 17:3810282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
20ug/L 22-Jul-2023 14:002.14Methane 10.0381
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 21:050.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 02-Aug-2023
1mg/L 02-Aug-2023 21:220.0120Iron 0.2002.01
1mg/L 02-Aug-2023 21:220.000700Manganese 0.005000.939
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 01-Aug-2023 14:020.200Sulfate 0.5001.23
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 29-Jul-2023 06:380.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 18:485.00Alkalinity, Bicarbonate (As
CaCO3)5.00181
1mg/L 02-Aug-2023 18:485.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:485.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 18:48a5.00Alkalinity, Total (As CaCO3)5.00181
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:400.0200Ferrous Iron 0.05000.530
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 45
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071072
HS23071072-10
19-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 01:470.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 01:470.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 01:470.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 01:471.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 01:470.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 01:470.20Benzene 1.0U
1ug/L 22-Jul-2023 01:470.20Chloroform 1.0U
1ug/L 22-Jul-2023 01:470.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 01:470.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 01:470.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 01:471.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 01:470.30Naphthalene 1.0U
1ug/L 22-Jul-2023 01:470.30o-Xylene 1.0U
1ug/L 22-Jul-2023 01:4710Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 01:470.20Toluene 1.0U
1ug/L 22-Jul-2023 01:470.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 01:4710570-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 01:4789.7 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 01:4710477-123
Surr: Toluene-d8 1%REC 22-Jul-2023 01:4710482-127
03-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of 45
Weight / Prep Log
HS23071072
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:197848
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 21 Jul 2023 10:02 End Date: 21 Jul 2023 10:02
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071072-01 35 (mL)40 mL VOA vial, HCl to pH <236.44 (mL)1.041
HS23071072-02 35 (mL)40 mL VOA vial, HCl to pH <236.74 (mL)1.05
HS23071072-03 35 (mL)40 mL VOA vial, HCl to pH <236.19 (mL)1.034
HS23071072-04 35 (mL)40 mL VOA vial, HCl to pH <236.75 (mL)1.05
HS23071072-05 35 (mL)40 mL VOA vial, HCl to pH <236.92 (mL)1.055
Batch ID:198051
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 26 Jul 2023 07:02 End Date: 26 Jul 2023 07:02
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071072-06 35 (mL)40 mL VOA vial, HCl to pH <236.16 (mL)1.033
HS23071072-07 35 (mL)40 mL VOA vial, HCl to pH <236.35 (mL)1.039
HS23071072-08 35 (mL)40 mL VOA vial, HCl to pH <237.04 (mL)1.058
HS23071072-09 35 (mL)40 mL VOA vial, HCl to pH <236.81 (mL)1.052
Batch ID:198394
Method:WATER - SW3010A 3010APrep Code:
Start Date: 02 Aug 2023 08:00 End Date: 02 Aug 2023 08:00
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071072-07 10 (mL)120 plastic HNO310 (mL)1
HS23071072-08 10 (mL)120 plastic HNO310 (mL)1
HS23071072-09 10 (mL)120 plastic HNO310 (mL)1
03-Aug-23Date: ALS Houston, US
Page 16 of 45
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071072
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:197848 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
21 Jul 2023 10:02 26 Jul 2023 08:42HS23071072-01 19 Jul 2023 09:05 1PMW-O-I
21 Jul 2023 10:02 26 Jul 2023 09:06HS23071072-02 19 Jul 2023 09:30 1PMW-O-D
21 Jul 2023 10:02 26 Jul 2023 09:29HS23071072-03 19 Jul 2023 10:00 1PMW-O-B
21 Jul 2023 10:02 26 Jul 2023 09:53HS23071072-04 19 Jul 2023 10:30 1AMW-11S
21 Jul 2023 10:02 26 Jul 2023 10:16HS23071072-05 19 Jul 2023 11:15 1AMW-13I
Batch ID:198051 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
26 Jul 2023 07:02 26 Jul 2023 19:54HS23071072-06 19 Jul 2023 11:45 1AMW-13D
26 Jul 2023 07:02 26 Jul 2023 20:18HS23071072-07 19 Jul 2023 12:20 1AMW-13S
26 Jul 2023 07:02 26 Jul 2023 20:41HS23071072-08 19 Jul 2023 12:45 1AMW-13B
26 Jul 2023 07:02 26 Jul 2023 21:05HS23071072-09 19 Jul 2023 14:05 1FMW-23R
Batch ID:198394 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
02 Aug 2023 08:00 02 Aug 2023 21:18HS23071072-07 19 Jul 2023 12:20 1AMW-13S
02 Aug 2023 08:00 02 Aug 2023 21:20HS23071072-08 19 Jul 2023 12:45 1AMW-13B
02 Aug 2023 08:00 02 Aug 2023 21:22HS23071072-09 19 Jul 2023 14:05 1FMW-23R
Batch ID:R441924 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
21 Jul 2023 10:40HS23071072-07 19 Jul 2023 12:20 1AMW-13S
21 Jul 2023 10:40HS23071072-08 19 Jul 2023 12:45 1AMW-13B
21 Jul 2023 10:40HS23071072-09 19 Jul 2023 14:05 1FMW-23R
Batch ID:R442019 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
22 Jul 2023 01:47HS23071072-10 19 Jul 2023 00:00 1Trip Blank
Batch ID:R442019 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
22 Jul 2023 07:02HS23071072-02 19 Jul 2023 09:30 1PMW-O-D
22 Jul 2023 07:23HS23071072-03 19 Jul 2023 10:00 1PMW-O-B
22 Jul 2023 07:44HS23071072-04 19 Jul 2023 10:30 1AMW-11S
22 Jul 2023 08:05HS23071072-05 19 Jul 2023 11:15 1AMW-13I
Batch ID:R442053 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
22 Jul 2023 16:35HS23071072-06 19 Jul 2023 11:45 1AMW-13D
22 Jul 2023 16:56HS23071072-07 19 Jul 2023 12:20 1AMW-13S
22 Jul 2023 17:17HS23071072-08 19 Jul 2023 12:45 1AMW-13B
22 Jul 2023 17:38HS23071072-09 19 Jul 2023 14:05 1FMW-23R
Batch ID:R442082 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
24 Jul 2023 16:22HS23071072-01 19 Jul 2023 09:05 1PMW-O-I
24 Jul 2023 14:37HS23071072-07 19 Jul 2023 12:20 10AMW-13S
03-Aug-23Date: ALS Houston, US
Page 17 of 45
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071072
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R442316 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
22 Jul 2023 13:51HS23071072-07 19 Jul 2023 12:20 50AMW-13S
22 Jul 2023 13:29HS23071072-08 19 Jul 2023 12:45 1AMW-13B
22 Jul 2023 14:00HS23071072-09 19 Jul 2023 14:05 20FMW-23R
Batch ID:R442706 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
29 Jul 2023 06:26HS23071072-07 19 Jul 2023 12:20 10AMW-13S
29 Jul 2023 06:32HS23071072-08 19 Jul 2023 12:45 10AMW-13B
29 Jul 2023 06:38HS23071072-09 19 Jul 2023 14:05 10FMW-23R
Batch ID:R442963 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
01 Aug 2023 10:25HS23071072-07 19 Jul 2023 12:20 1AMW-13S
01 Aug 2023 10:31HS23071072-08 19 Jul 2023 12:45 1AMW-13B
Batch ID:R442966 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
01 Aug 2023 14:02HS23071072-09 19 Jul 2023 14:05 1FMW-23R
Batch ID:R443058 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
02 Aug 2023 18:35HS23071072-07 19 Jul 2023 12:20 1AMW-13S
02 Aug 2023 18:41HS23071072-08 19 Jul 2023 12:45 1AMW-13B
02 Aug 2023 18:48HS23071072-09 19 Jul 2023 14:05 1FMW-23R
03-Aug-23Date: ALS Houston, US
Page 18 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:197848 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-197848 Units:ug/L Analysis Date:25-Jul-2023 23:22
Run ID:ECD_13_442420 SeqNo:7453289 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-197848 Units:ug/L Analysis Date:25-Jul-2023 23:45
Run ID:ECD_13_442420 SeqNo:7453290 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1651 0.25 0 66.0 60 - 1400.020
Sample ID:LCSD-197848 Units:ug/L Analysis Date:26-Jul-2023 00:09
Run ID:ECD_13_442420 SeqNo:7453291 PrepDate:21-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1873 0.25 0 74.9 60 - 140 0.1651 12.6 200.020
The following samples were analyzed in this batch:HS23071072-01 HS23071072-02 HS23071072-03 HS23071072-04
HS23071072-05
ALS Houston, US Date: 03-Aug-23
Page 19 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:198051 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-198051 Units:ug/L Analysis Date:26-Jul-2023 11:51
Run ID:ECD_13_442465 SeqNo:7454594 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-198051 Units:ug/L Analysis Date:26-Jul-2023 12:14
Run ID:ECD_13_442465 SeqNo:7454595 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1692 0.25 0 67.7 60 - 1400.020
Sample ID:LCSD-198051 Units:ug/L Analysis Date:26-Jul-2023 12:38
Run ID:ECD_13_442465 SeqNo:7454596 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1705 0.25 0 68.2 60 - 140 0.1692 0.781 200.020
The following samples were analyzed in this batch:HS23071072-06 HS23071072-07 HS23071072-08 HS23071072-09
ALS Houston, US Date: 03-Aug-23
Page 20 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442316 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230722 Units:ug/L Analysis Date:22-Jul-2023 08:11
Run ID:FID-4_442316 SeqNo:7450987 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230722 Units:ug/L Analysis Date:22-Jul-2023 08:21
Run ID:FID-4_442316 SeqNo:7450988 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 8.179 9.647 0 84.8 75 - 1250.500
Sample ID:LCSD-230722 Units:ug/L Analysis Date:22-Jul-2023 08:33
Run ID:FID-4_442316 SeqNo:7450989 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 7.869 9.647 0 81.6 75 - 125 8.179 3.86 300.500
Sample ID:HS23070922-11DUP Units:ug/L Analysis Date:22-Jul-2023 10:23
Run ID:FID-4_442316 SeqNo:7450998 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Methane 14.19 12.65 11.4 300.500
The following samples were analyzed in this batch:HS23071072-07 HS23071072-08 HS23071072-09
ALS Houston, US Date: 03-Aug-23
Page 21 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:198394 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198394 Units:mg/L Analysis Date:02-Aug-2023 21:33
Run ID:ICPMS06_442976 SeqNo:7468068 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:LCS-198394 Units:mg/L Analysis Date:02-Aug-2023 20:03
Run ID:ICPMS06_442976 SeqNo:7467996 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.968 5 0 99.4 80 - 1200.200
Manganese 0.04937 0.05 0 98.7 80 - 1200.00500
Sample ID:HS23070985-01MS Units:mg/L Analysis Date:02-Aug-2023 20:11
Run ID:ICPMS06_442976 SeqNo:7468000 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 4.979 5 0.1028 97.5 80 - 1200.200
Manganese 0.6415 0.05 0.6311 20.8 80 - 120 SO 0.00500
Sample ID:HS23070985-01MSD Units:mg/L Analysis Date:02-Aug-2023 20:15
Run ID:ICPMS06_442976 SeqNo:7468002 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.122 5 0.1028 100 80 - 120 4.979 2.84 200.200
Manganese 0.6606 0.05 0.6311 59.1 80 - 120 0.6415 2.94 20 SO 0.00500
Sample ID:HS23070985-01PDS Units:mg/L Analysis Date:02-Aug-2023 20:19
Run ID:ICPMS06_442976 SeqNo:7468004 PrepDate:02-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 10.81 10 0.1028 107 75 - 1250.200
Manganese 0.6958 0.1 0.6311 64.7 75 - 125 SO 0.00500
ALS Houston, US Date: 03-Aug-23
Page 22 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:198394 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23070985-01SD Units:mg/L Analysis Date:02-Aug-2023 20:07
Run ID:ICPMS06_442976 SeqNo:7467998 PrepDate:02-Aug-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron 0.1093 0.1028 0 10 J 1.00
Manganese 0.6661 0.6311 5.54 100.0250
The following samples were analyzed in this batch:HS23071072-07 HS23071072-08 HS23071072-09
ALS Houston, US Date: 03-Aug-23
Page 23 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230721 Units:ug/L Analysis Date:22-Jul-2023 00:23
Run ID:VOA10_442019 SeqNo:7444113 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
52.96 50 0 106 70 - 1231.0Surr: 1,2-Dichloroethane-d4
44.29 50 0 88.6 77 - 1131.0Surr: 4-Bromofluorobenzene
51.71 50 0 103 73 - 1261.0Surr: Dibromofluoromethane
50.64 50 0 101 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 24 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230721 Units:ug/L Analysis Date:21-Jul-2023 23:41
Run ID:VOA10_442019 SeqNo:7444112 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 21.08 20 0 105 73 - 1211.0
1,2-Dibromoethane 20.46 20 0 102 76 - 1231.0
1,2-Dichloroethane 19.8 20 0 99.0 70 - 1241.0
2-Methylnaphthalene 21.56 20 0 108 55 - 1401.0
4-Isopropyltoluene 22.86 20 0 114 74 - 1261.0
Benzene 18.27 20 0 91.4 74 - 1201.0
Chloroform 20.48 20 0 102 71 - 1211.0
Ethylbenzene 18.6 20 0 93.0 77 - 1171.0
m,p-Xylene 37.62 40 0 94.1 77 - 1222.0
Methyl tert-butyl ether 19.47 20 0 97.4 70 - 1301.0
Methylene chloride 20.75 20 0 104 70 - 1272.0
Naphthalene 22.76 20 0 114 70 - 1301.0
o-Xylene 17.96 20 0 89.8 75 - 1191.0
Tert-butyl alcohol 423.1 400 0 106 70 - 13010
Toluene 19.87 20 0 99.3 77 - 1181.0
Xylenes, Total 55.58 60 0 92.6 75 - 1223.0
52.88 50 0 106 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.49 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
50.36 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
50.91 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 25 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071068-09MS Units:ug/L Analysis Date:22-Jul-2023 02:29
Run ID:VOA10_442019 SeqNo:7444119 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 18.84 20 0 94.2 70 - 1251.0
1,2-Dibromoethane 18.49 20 0 92.5 70 - 1241.0
1,2-Dichloroethane 19.22 20 0 96.1 70 - 1271.0
2-Methylnaphthalene 18.08 20 0 90.4 55 - 1401.0
4-Isopropyltoluene 19.94 20 0 99.7 70 - 1301.0
Benzene 18.11 20 0 90.6 70 - 1271.0
Chloroform 18.26 20 0 91.3 70 - 1251.0
Ethylbenzene 18.07 20 0 90.4 70 - 1241.0
m,p-Xylene 35.76 40 0 89.4 70 - 1302.0
Methyl tert-butyl ether 112.1 20 94.54 87.6 70 - 130 O1.0
Methylene chloride 18.47 20 0 92.4 70 - 1282.0
Naphthalene 20.89 20 0 104 70 - 1301.0
o-Xylene 16.72 20 0 83.6 70 - 1241.0
Tert-butyl alcohol 9952 400 9652 75.0 70 - 130 EO10
Toluene 19.09 20 0 95.4 70 - 1231.0
Xylenes, Total 52.47 60 0 87.5 70 - 1303.0
50.92 50 0 102 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.37 50 0 94.7 77 - 1131.0Surr: 4-Bromofluorobenzene
49.4 50 0 98.8 77 - 1231.0Surr: Dibromofluoromethane
50.65 50 0 101 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 26 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442019 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071068-09MSD Units:ug/L Analysis Date:22-Jul-2023 02:50
Run ID:VOA10_442019 SeqNo:7444120 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 18.91 20 0 94.5 70 - 125 18.84 0.372 201.0
1,2-Dibromoethane 18.84 20 0 94.2 70 - 124 18.49 1.89 201.0
1,2-Dichloroethane 18.59 20 0 92.9 70 - 127 19.22 3.35 201.0
2-Methylnaphthalene 19.43 20 0 97.2 55 - 140 18.08 7.23 201.0
4-Isopropyltoluene 20.05 20 0 100 70 - 130 19.94 0.512 201.0
Benzene 17.12 20 0 85.6 70 - 127 18.11 5.61 201.0
Chloroform 18.54 20 0 92.7 70 - 125 18.26 1.53 201.0
Ethylbenzene 17.48 20 0 87.4 70 - 124 18.07 3.29 201.0
m,p-Xylene 33.9 40 0 84.8 70 - 130 35.76 5.31 202.0
Methyl tert-butyl ether 112.1 20 94.54 87.9 70 - 130 112.1 0.0531 20 O1.0
Methylene chloride 18.08 20 0 90.4 70 - 128 18.47 2.18 202.0
Naphthalene 21.53 20 0 108 70 - 130 20.89 3.02 201.0
o-Xylene 17.01 20 0 85.0 70 - 124 16.72 1.71 201.0
Tert-butyl alcohol 10190 400 9652 135 70 - 130 9952 2.39 20 SEO10
Toluene 18.33 20 0 91.6 70 - 123 19.09 4.06 201.0
Xylenes, Total 50.91 60 0 84.8 70 - 130 52.47 3.02 203.0
49.63 50 0 99.3 70 - 126 50.92 2.56 201.0Surr: 1,2-Dichloroethane-d4
46.4 50 0 92.8 77 - 113 47.37 2.07 201.0Surr: 4-Bromofluorobenzene
49.37 50 0 98.7 77 - 123 49.4 0.0786 201.0Surr: Dibromofluoromethane
50.37 50 0 101 82 - 127 50.65 0.552 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071072-02 HS23071072-03 HS23071072-04 HS23071072-05
HS23071072-10
ALS Houston, US Date: 03-Aug-23
Page 27 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442053 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230722 Units:ug/L Analysis Date:22-Jul-2023 11:41
Run ID:VOA10_442053 SeqNo:7444839 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
51.39 50 0 103 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.48 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
52.66 50 0 105 73 - 1261.0Surr: Dibromofluoromethane
50.2 50 0 100 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 28 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442053 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230722 Units:ug/L Analysis Date:22-Jul-2023 10:59
Run ID:VOA10_442053 SeqNo:7444838 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 20.71 20 0 104 73 - 1211.0
1,2-Dibromoethane 19.69 20 0 98.5 76 - 1231.0
1,2-Dichloroethane 18.75 20 0 93.7 70 - 1241.0
2-Methylnaphthalene 20.29 20 0 101 55 - 1401.0
4-Isopropyltoluene 23.39 20 0 117 74 - 1261.0
Benzene 17.3 20 0 86.5 74 - 1201.0
Chloroform 18.37 20 0 91.9 71 - 1211.0
Ethylbenzene 17.99 20 0 89.9 77 - 1171.0
m,p-Xylene 36.93 40 0 92.3 77 - 1222.0
Methyl tert-butyl ether 17.87 20 0 89.3 70 - 1301.0
Methylene chloride 18.65 20 0 93.2 70 - 1272.0
Naphthalene 21.43 20 0 107 70 - 1301.0
o-Xylene 17.73 20 0 88.7 75 - 1191.0
Tert-butyl alcohol 353.5 400 0 88.4 70 - 13010
Toluene 19.64 20 0 98.2 77 - 1181.0
Xylenes, Total 54.66 60 0 91.1 75 - 1223.0
51.93 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.22 50 0 92.4 77 - 1131.0Surr: 4-Bromofluorobenzene
49.35 50 0 98.7 73 - 1261.0Surr: Dibromofluoromethane
52.53 50 0 105 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 29 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442053 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071230-10MS Units:ug/L Analysis Date:22-Jul-2023 12:23
Run ID:VOA10_442053 SeqNo:7444841 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 21.62 20 0 108 70 - 1251.0
1,2-Dibromoethane 18.92 20 0 94.6 70 - 1241.0
1,2-Dichloroethane 20.13 20 0 101 70 - 1271.0
2-Methylnaphthalene 16.4 20 0 82.0 55 - 1401.0
4-Isopropyltoluene 23.56 20 0 118 70 - 1301.0
Benzene 18.99 20 0 95.0 70 - 1271.0
Chloroform 19.95 20 0 99.7 70 - 1251.0
Ethylbenzene 19.54 20 0 97.7 70 - 1241.0
m,p-Xylene 39.43 40 0 98.6 70 - 1302.0
Methyl tert-butyl ether 18.07 20 0 90.3 70 - 1301.0
Methylene chloride 19.85 20 0 99.2 70 - 1282.0
Naphthalene 19.77 20 0 98.9 70 - 1301.0
o-Xylene 18.41 20 0 92.0 70 - 1241.0
Tert-butyl alcohol 308 400 0 77.0 70 - 13010
Toluene 20.8 20 0 104 70 - 1231.0
Xylenes, Total 57.84 60 0 96.4 70 - 1303.0
50.63 50 0 101 70 - 1261.0Surr: 1,2-Dichloroethane-d4
46.84 50 0 93.7 77 - 1131.0Surr: 4-Bromofluorobenzene
48.48 50 0 97.0 77 - 1231.0Surr: Dibromofluoromethane
51.25 50 0 103 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 30 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442053 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071230-10MSD Units:ug/L Analysis Date:22-Jul-2023 12:44
Run ID:VOA10_442053 SeqNo:7444842 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 21.19 20 0 106 70 - 125 21.62 2 201.0
1,2-Dibromoethane 19.53 20 0 97.6 70 - 124 18.92 3.19 201.0
1,2-Dichloroethane 20.15 20 0 101 70 - 127 20.13 0.105 201.0
2-Methylnaphthalene 18.64 20 0 93.2 55 - 140 16.4 12.8 201.0
4-Isopropyltoluene 23.98 20 0 120 70 - 130 23.56 1.76 201.0
Benzene 19.27 20 0 96.3 70 - 127 18.99 1.43 201.0
Chloroform 20.08 20 0 100 70 - 125 19.95 0.652 201.0
Ethylbenzene 18.89 20 0 94.5 70 - 124 19.54 3.35 201.0
m,p-Xylene 38.32 40 0 95.8 70 - 130 39.43 2.85 202.0
Methyl tert-butyl ether 18.37 20 0 91.9 70 - 130 18.07 1.69 201.0
Methylene chloride 18.03 20 0 90.1 70 - 128 19.85 9.6 202.0
Naphthalene 21.25 20 0 106 70 - 130 19.77 7.22 201.0
o-Xylene 17.43 20 0 87.1 70 - 124 18.41 5.48 201.0
Tert-butyl alcohol 334.8 400 0 83.7 70 - 130 308 8.35 2010
Toluene 19.95 20 0 99.7 70 - 123 20.8 4.18 201.0
Xylenes, Total 55.75 60 0 92.9 70 - 130 57.84 3.68 203.0
53.76 50 0 108 70 - 126 50.63 6 201.0Surr: 1,2-Dichloroethane-d4
46.83 50 0 93.7 77 - 113 46.84 0.0244 201.0Surr: 4-Bromofluorobenzene
49.62 50 0 99.2 77 - 123 48.48 2.31 201.0Surr: Dibromofluoromethane
50.77 50 0 102 82 - 127 51.25 0.943 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071072-06 HS23071072-07 HS23071072-08 HS23071072-09
ALS Houston, US Date: 03-Aug-23
Page 31 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442082 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230724 Units:ug/L Analysis Date:24-Jul-2023 10:25
Run ID:VOA10_442082 SeqNo:7445533 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
52.47 50 0 105 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.78 50 0 93.6 77 - 1131.0Surr: 4-Bromofluorobenzene
51.48 50 0 103 73 - 1261.0Surr: Dibromofluoromethane
50.01 50 0 100 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 32 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442082 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230724 Units:ug/L Analysis Date:24-Jul-2023 09:43
Run ID:VOA10_442082 SeqNo:7445532 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 20.87 20 0 104 73 - 1211.0
1,2-Dibromoethane 20.58 20 0 103 76 - 1231.0
1,2-Dichloroethane 20.74 20 0 104 70 - 1241.0
2-Methylnaphthalene 21.11 20 0 106 55 - 1401.0
4-Isopropyltoluene 22.31 20 0 112 74 - 1261.0
Benzene 18.96 20 0 94.8 74 - 1201.0
Chloroform 20.3 20 0 102 71 - 1211.0
Ethylbenzene 18.93 20 0 94.6 77 - 1171.0
m,p-Xylene 38.38 40 0 96.0 77 - 1222.0
Methyl tert-butyl ether 19.23 20 0 96.2 70 - 1301.0
Methylene chloride 19.74 20 0 98.7 70 - 1272.0
Naphthalene 21.26 20 0 106 70 - 1301.0
o-Xylene 18.53 20 0 92.6 75 - 1191.0
Tert-butyl alcohol 433.9 400 0 108 70 - 13010
Toluene 20.11 20 0 101 77 - 1181.0
Xylenes, Total 56.91 60 0 94.9 75 - 1223.0
52.42 50 0 105 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.32 50 0 96.6 77 - 1131.0Surr: 4-Bromofluorobenzene
51.2 50 0 102 73 - 1261.0Surr: Dibromofluoromethane
51.03 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 33 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442082 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071230-06MS Units:ug/L Analysis Date:24-Jul-2023 11:07
Run ID:VOA10_442082 SeqNo:7445535 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 20.87 20 0 104 70 - 1251.0
1,2-Dibromoethane 19.11 20 0 95.5 70 - 1241.0
1,2-Dichloroethane 20.49 20 0 102 70 - 1271.0
2-Methylnaphthalene 15.9 20 0 79.5 55 - 1401.0
4-Isopropyltoluene 23.29 20 0 116 70 - 1301.0
Benzene 18.89 20 0 94.5 70 - 1271.0
Chloroform 19.48 20 0 97.4 70 - 1251.0
Ethylbenzene 18.63 20 0 93.1 70 - 1241.0
m,p-Xylene 38.63 40 0 96.6 70 - 1302.0
Methyl tert-butyl ether 17.81 20 0 89.1 70 - 1301.0
Methylene chloride 19.36 20 0 96.8 70 - 1282.0
Naphthalene 19.33 20 0 96.7 70 - 1301.0
o-Xylene 17.36 20 0 86.8 70 - 1241.0
Tert-butyl alcohol 322.2 400 0 80.6 70 - 13010
Toluene 20.25 20 0 101 70 - 1231.0
Xylenes, Total 55.98 60 0 93.3 70 - 1303.0
53.52 50 0 107 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.39 50 0 94.8 77 - 1131.0Surr: 4-Bromofluorobenzene
50.15 50 0 100 77 - 1231.0Surr: Dibromofluoromethane
51.1 50 0 102 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 03-Aug-23
Page 34 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442082 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071230-06MSD Units:ug/L Analysis Date:24-Jul-2023 11:28
Run ID:VOA10_442082 SeqNo:7445536 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 20.44 20 0 102 70 - 125 20.87 2.09 201.0
1,2-Dibromoethane 18.18 20 0 90.9 70 - 124 19.11 4.99 201.0
1,2-Dichloroethane 19.69 20 0 98.5 70 - 127 20.49 3.94 201.0
2-Methylnaphthalene 17.23 20 0 86.1 55 - 140 15.9 8.04 201.0
4-Isopropyltoluene 23.22 20 0 116 70 - 130 23.29 0.288 201.0
Benzene 18.6 20 0 93.0 70 - 127 18.89 1.56 201.0
Chloroform 20.7 20 0 104 70 - 125 19.48 6.09 201.0
Ethylbenzene 18.34 20 0 91.7 70 - 124 18.63 1.59 201.0
m,p-Xylene 37.24 40 0 93.1 70 - 130 38.63 3.67 202.0
Methyl tert-butyl ether 18.53 20 0 92.6 70 - 130 17.81 3.93 201.0
Methylene chloride 18.97 20 0 94.9 70 - 128 19.36 2.03 202.0
Naphthalene 20.65 20 0 103 70 - 130 19.33 6.62 201.0
o-Xylene 17.77 20 0 88.8 70 - 124 17.36 2.36 201.0
Tert-butyl alcohol 337.5 400 0 84.4 70 - 130 322.2 4.64 2010
Toluene 19.54 20 0 97.7 70 - 123 20.25 3.56 201.0
Xylenes, Total 55 60 0 91.7 70 - 130 55.98 1.76 203.0
51.66 50 0 103 70 - 126 53.52 3.54 201.0Surr: 1,2-Dichloroethane-d4
47.25 50 0 94.5 77 - 113 47.39 0.286 201.0Surr: 4-Bromofluorobenzene
51.06 50 0 102 77 - 123 50.15 1.79 201.0Surr: Dibromofluoromethane
51.52 50 0 103 82 - 127 51.1 0.821 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071072-01 HS23071072-07
ALS Houston, US Date: 03-Aug-23
Page 35 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R441924 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442034 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442033 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.263 0.25 0 105 80 - 1200.0500
Sample ID:HS23071069-04MS Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442036 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.504 0.25 0.279 90.0 75 - 1250.0500
Sample ID:HS23071069-04MSD Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442035 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.505 0.25 0.279 90.4 75 - 125 0.504 0.198 200.0500
The following samples were analyzed in this batch:HS23071072-07 HS23071072-08 HS23071072-09
ALS Houston, US Date: 03-Aug-23
Page 36 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442706 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:29-Jul-2023 04:19
Run ID:ICS-Integrion_442706 SeqNo:7460175 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:29-Jul-2023 04:24
Run ID:ICS-Integrion_442706 SeqNo:7460176 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)7.902 8 0 98.8 90 - 1100.200
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:29-Jul-2023 05:51
Run ID:ICS-Integrion_442706 SeqNo:7460188 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.68 40 0 94.2 80 - 1202.00
Sample ID:HS23071063-01MS Units:mg/L Analysis Date:29-Jul-2023 04:36
Run ID:ICS-Integrion_442706 SeqNo:7460178 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)37.84 40 0 94.6 80 - 1202.00
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:29-Jul-2023 05:57
Run ID:ICS-Integrion_442706 SeqNo:7460189 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.69 40 0 96.7 80 - 120 37.68 2.64 202.00
Sample ID:HS23071063-01MSD Units:mg/L Analysis Date:29-Jul-2023 04:42
Run ID:ICS-Integrion_442706 SeqNo:7460179 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)38.8 40 0 97.0 80 - 120 37.84 2.51 202.00
The following samples were analyzed in this batch:HS23071072-07 HS23071072-08 HS23071072-09
ALS Houston, US Date: 03-Aug-23
Page 37 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442963 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:01-Aug-2023 08:11
Run ID:ICS-Integrion_442963 SeqNo:7466487 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:01-Aug-2023 08:17
Run ID:ICS-Integrion_442963 SeqNo:7466488 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 19.49 20 0 97.5 90 - 1100.500
Sample ID:HS23071069-01MS Units:mg/L Analysis Date:01-Aug-2023 09:50
Run ID:ICS-Integrion_442963 SeqNo:7466500 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 11.56 10 1.444 101 80 - 1200.500
Sample ID:HS23071029-06MS Units:mg/L Analysis Date:01-Aug-2023 08:34
Run ID:ICS-Integrion_442963 SeqNo:7466490 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 15.91 10 5.729 102 80 - 1200.500
Sample ID:HS23071069-01MSD Units:mg/L Analysis Date:01-Aug-2023 09:56
Run ID:ICS-Integrion_442963 SeqNo:7466501 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 11.99 10 1.444 105 80 - 120 11.56 3.66 200.500
Sample ID:HS23071029-06MSD Units:mg/L Analysis Date:01-Aug-2023 08:40
Run ID:ICS-Integrion_442963 SeqNo:7466491 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 15.86 10 5.729 101 80 - 120 15.91 0.28 200.500
The following samples were analyzed in this batch:HS23071072-07 HS23071072-08
ALS Houston, US Date: 03-Aug-23
Page 38 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R442966 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:01-Aug-2023 12:09
Run ID:ICS-Integrion_442966 SeqNo:7466554 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:01-Aug-2023 12:15
Run ID:ICS-Integrion_442966 SeqNo:7466555 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 20.66 20 0 103 90 - 1100.500
Sample ID:HS23080018-03MS Units:mg/L Analysis Date:01-Aug-2023 12:52
Run ID:ICS-Integrion_442966 SeqNo:7466557 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 22.72 10 12.17 106 80 - 1200.500
Sample ID:HS23071215-03MS Units:mg/L Analysis Date:01-Aug-2023 15:29
Run ID:ICS-Integrion_442966 SeqNo:7466579 PrepDate:DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 239.1 50 212.7 52.8 80 - 120 SO 2.50
Sample ID:HS23080018-03MSD Units:mg/L Analysis Date:01-Aug-2023 12:58
Run ID:ICS-Integrion_442966 SeqNo:7466558 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 23.4 10 12.17 112 80 - 120 22.72 2.91 200.500
Sample ID:HS23071215-03MSD Units:mg/L Analysis Date:01-Aug-2023 15:35
Run ID:ICS-Integrion_442966 SeqNo:7466580 PrepDate:DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 238 50 212.7 50.6 80 - 120 239.1 0.457 20 SO 2.50
The following samples were analyzed in this batch:HS23071072-09
ALS Houston, US Date: 03-Aug-23
Page 39 of 45
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071072
QC BATCH REPORT
Batch ID:R443058 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:WBLKW1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:03
Run ID:ManTech01_443058 SeqNo:7469107 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:11
Run ID:ManTech01_443058 SeqNo:7469108 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)975.7 1000 0 97.6 85 - 1155.00
Alkalinity, Total (As CaCO3)994.5 1000 0 99.5 85 - 1155.00
Sample ID:LCSD1-080223 Units:mg/L Analysis Date:02-Aug-2023 16:21
Run ID:ManTech01_443058 SeqNo:7469109 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)1006 1000 0 101 85 - 115 975.7 3.04 205.00
Alkalinity, Total (As CaCO3)1027 1000 0 103 85 - 115 994.5 3.2 205.00
Sample ID:HS23071063-02DUP Units:mg/L Analysis Date:02-Aug-2023 16:45
Run ID:ManTech01_443058 SeqNo:7469113 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)450.7 449.7 0.22 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)450.7 449.7 0.22 205.00
The following samples were analyzed in this batch:HS23071072-07 HS23071072-08 HS23071072-09
ALS Houston, US Date: 03-Aug-23
Page 40 of 45
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071072
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 03-Aug-23
Page 41 of 45
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
03-Aug-23Date: ALS Houston, US
Page 42 of 45
Ragen Giga
20-Jul-2023 09:40Date/Time Received:HS23071072
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.7uc/3.6c IR31
45286
07/20/23
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Ragen Giga
Date/TimeeSignatureDate/TimeeSignature
21-Jul-2023 08:0820-Jul-2023 18:30
FedEx Priority OvernightwCarrier name:Matrices:
Reviewed by:/S/ Nieka.Carson
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241086
ALS Houston, US 03-Aug-23Date:
Page 43 of 45
Page 44 of 45
Page 45 of 45
August 04, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 9 sample(s) on Jul 21, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071150
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071150
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071150-01 19-Jul-2023 08:55 21-Jul-2023 09:30AMW-9S Groundwater
HS23071150-02 19-Jul-2023 09:50 21-Jul-2023 09:30AMW-8S Groundwater
HS23071150-03 19-Jul-2023 11:45 21-Jul-2023 09:30PMW-J-I Groundwater
HS23071150-04 19-Jul-2023 10:50 21-Jul-2023 09:30PMW-J-D Groundwater
HS23071150-05 19-Jul-2023 12:40 21-Jul-2023 09:30PMW-J-B Groundwater
HS23071150-06 19-Jul-2023 13:40 21-Jul-2023 09:30FMW-24D Groundwater
HS23071150-07 19-Jul-2023 14:30 21-Jul-2023 09:30FMW-24 Groundwater
HS23071150-08 19-Jul-2023 15:30 21-Jul-2023 09:30FMW-24I Groundwater
HS23071150-09 19-Jul-2023 00:00cg-090622-
neat-184
21-Jul-2023 09:30Trip Blank Water
ALS Houston, US 04-Aug-23Date:
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071150
Work Order Comments
Login notes:
1 Trip Blank vial received broken, 1 remains for analysis
•
ECD Organics by Method SW8011
Batch ID: 198053
Sample ID: LCSD-198053
LCS/LCSD RPD exceeded the laboratory acceptance limit. Recovery met acceptance criteria. 1,2,3-Trichloropropane•
Batch ID: 198051
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GC Semivolatiles by Method RSK-175
Batch ID: R442732
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R442082
Sample ID: VLCSW-230724
LCS failed outside control limits high for 1,2-Dichlorobenzene and 1,4-Dichlorobenzene. Associated samples are ND.•
Batch ID: R442056
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R442053
Sample ID: VLCSW-230722
LCS failed outside control limits high for 1,2-Dichlorobenzene, 1,4-Dichlorobenzene and Bromobenzene. Associated samples are ND. •
Metals by Method SW6020A
Batch ID: 198516
Sample ID: FMW-24D (HS23071150-06MS)
The MS and/or MSD recovery was outside of the control; however, the result in the parent sample is greater than 4x the spike amount.
alcium.
•
Thallium failed on the MS but passed on the MSD and PDS.•
ALS Houston, US 04-Aug-23Date:
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071150
WetChemistry by Method E300
Batch ID: R443157
Sample ID: FMW-24 (HS23071150-07)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: FMW-24D (HS23071150-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Batch ID: R443081
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R443060
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM3500FED
Batch ID: R441924
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 04-Aug-23Date:
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-9S
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-01
19-Jul-2023 08:55 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 17:590.301,2,4-Trimethylbenzene 1.01.4
1ug/L 22-Jul-2023 17:590.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 17:590.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 17:591.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 17:590.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 17:590.20Benzene 1.012
1ug/L 22-Jul-2023 17:590.20Chloroform 1.0U
1ug/L 22-Jul-2023 17:590.30Ethylbenzene 1.04.5
1ug/L 22-Jul-2023 17:590.50m,p-Xylene 2.02.7
1ug/L 22-Jul-2023 17:590.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 17:591.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 17:590.30Naphthalene 1.02.4
1ug/L 22-Jul-2023 17:59J0.30o-Xylene 1.00.74
1ug/L 22-Jul-2023 17:5910Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 17:59J0.20Toluene 1.00.44
1ug/L 22-Jul-2023 17:590.30Xylenes, Total 3.03.5
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 17:5910370-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 17:5992.3 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 17:5910177-123
Surr: Toluene-d8 1%REC 22-Jul-2023 17:5910382-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 23:030.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-8S
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-02
19-Jul-2023 09:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 18:200.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 18:200.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 18:200.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 18:201.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 18:200.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 18:200.20Benzene 1.0U
1ug/L 22-Jul-2023 18:200.20Chloroform 1.0U
1ug/L 22-Jul-2023 18:200.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 18:200.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 18:200.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 18:201.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 18:200.30Naphthalene 1.0U
1ug/L 22-Jul-2023 18:200.30o-Xylene 1.0U
1ug/L 22-Jul-2023 18:2010Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 18:200.20Toluene 1.0U
1ug/L 22-Jul-2023 18:200.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 18:2010670-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 18:2092.2 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 18:2010077-123
Surr: Toluene-d8 1%REC 22-Jul-2023 18:2010082-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 23:270.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-J-I
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-03
19-Jul-2023 11:45 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 18:410.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 18:410.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 18:410.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 18:411.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 18:410.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 18:410.20Benzene 1.0U
1ug/L 22-Jul-2023 18:410.20Chloroform 1.0U
1ug/L 22-Jul-2023 18:410.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 18:410.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 18:410.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 18:411.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 18:410.30Naphthalene 1.0U
1ug/L 22-Jul-2023 18:410.30o-Xylene 1.0U
1ug/L 22-Jul-2023 18:4110Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 18:410.20Toluene 1.0U
1ug/L 22-Jul-2023 18:410.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 18:4110470-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 18:4190.1 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 18:4110477-123
Surr: Toluene-d8 1%REC 22-Jul-2023 18:4110182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 26-Jul-2023 23:500.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-J-D
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-04
19-Jul-2023 10:50 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 19:020.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 19:020.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 19:020.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 19:021.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 19:020.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 19:020.20Benzene 1.0U
1ug/L 22-Jul-2023 19:020.20Chloroform 1.0U
1ug/L 22-Jul-2023 19:020.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 19:020.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 19:020.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 19:021.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 19:020.30Naphthalene 1.0U
1ug/L 22-Jul-2023 19:020.30o-Xylene 1.0U
1ug/L 22-Jul-2023 19:0210Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 19:020.20Toluene 1.0U
1ug/L 22-Jul-2023 19:020.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 19:0210770-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 19:0288.9 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 19:0210577-123
Surr: Toluene-d8 1%REC 22-Jul-2023 19:0210282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 00:140.00321,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-J-B
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-05
19-Jul-2023 12:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 22-Jul-2023 19:230.301,2,4-Trimethylbenzene 1.0U
1ug/L 22-Jul-2023 19:230.201,2-Dibromoethane 1.0U
1ug/L 22-Jul-2023 19:230.201,2-Dichloroethane 1.0U
1ug/L 22-Jul-2023 19:231.02-Methylnaphthalene 1.0U
1ug/L 22-Jul-2023 19:230.304-Isopropyltoluene 1.0U
1ug/L 22-Jul-2023 19:230.20Benzene 1.0U
1ug/L 22-Jul-2023 19:230.20Chloroform 1.0U
1ug/L 22-Jul-2023 19:230.30Ethylbenzene 1.0U
1ug/L 22-Jul-2023 19:230.50m,p-Xylene 2.0U
1ug/L 22-Jul-2023 19:230.20Methyl tert-butyl ether 1.0U
1ug/L 22-Jul-2023 19:231.0Methylene chloride 2.0U
1ug/L 22-Jul-2023 19:230.30Naphthalene 1.0U
1ug/L 22-Jul-2023 19:230.30o-Xylene 1.0U
1ug/L 22-Jul-2023 19:2310Tert-butyl alcohol 10U
1ug/L 22-Jul-2023 19:230.20Toluene 1.0U
1ug/L 22-Jul-2023 19:230.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2023 19:2310470-126
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2023 19:2392.4 77-113
Surr: Dibromofluoromethane 1%REC 22-Jul-2023 19:2310277-123
Surr: Toluene-d8 1%REC 22-Jul-2023 19:2310282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 00:370.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-24D
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-06
19-Jul-2023 13:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 23-Jul-2023 04:500.301,2,4-Trimethylbenzene 1.0U
1ug/L 23-Jul-2023 04:500.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 04:500.201,2-Dichloroethane 1.0U
1ug/L 23-Jul-2023 04:501.02-Methylnaphthalene 1.0U
1ug/L 23-Jul-2023 04:500.304-Isopropyltoluene 1.0U
1ug/L 23-Jul-2023 04:500.20Benzene 1.0U
1ug/L 23-Jul-2023 04:500.20Chloroform 1.0U
1ug/L 23-Jul-2023 04:500.30Ethylbenzene 1.0U
1ug/L 23-Jul-2023 04:500.50m,p-Xylene 2.0U
1ug/L 23-Jul-2023 04:500.20Methyl tert-butyl ether 1.0U
1ug/L 23-Jul-2023 04:501.0Methylene chloride 2.0U
1ug/L 23-Jul-2023 04:500.30Naphthalene 1.0U
1ug/L 23-Jul-2023 04:500.30o-Xylene 1.0U
1ug/L 23-Jul-2023 04:5010Tert-butyl alcohol 10U
1ug/L 23-Jul-2023 04:500.20Toluene 1.0U
1ug/L 23-Jul-2023 04:500.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 04:5010770-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 04:5089.0 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 04:5098.9 77-123
Surr: Toluene-d8 1%REC 23-Jul-2023 04:5010382-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
1ug/L 28-Jul-2023 12:100.107Methane 0.5000.696
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 01:010.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: ALRPrep:SW3010A / 03-Aug-2023
1mg/L 04-Aug-2023 00:13J0.0120Iron 0.2000.0477
1mg/L 04-Aug-2023 00:130.000700Manganese 0.005000.0864
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 03-Aug-2023 02:190.200Sulfate 0.5002.13
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 03-Aug-2023 22:560.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 19:545.00Alkalinity, Bicarbonate (As
CaCO3)5.00389
1mg/L 02-Aug-2023 19:545.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 19:545.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 19:54a5.00Alkalinity, Total (As CaCO3)5.00389
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
1mg/L 21-Jul-2023 10:40J0.0200Ferrous Iron 0.05000.0340
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-24
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-07
19-Jul-2023 14:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
50ug/L 24-Jul-2023 14:16151,2,4-Trimethylbenzene 502,700
1ug/L 23-Jul-2023 05:110.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 05:110.201,2-Dichloroethane 1.0U
50ug/L 24-Jul-2023 14:16502-Methylnaphthalene 50560
1ug/L 23-Jul-2023 05:110.304-Isopropyltoluene 1.033
50ug/L 24-Jul-2023 14:1610Benzene507,100
1ug/L 23-Jul-2023 05:110.20Chloroform 1.0U
50ug/L 24-Jul-2023 14:1615Ethylbenzene501,200
50ug/L 24-Jul-2023 14:1625m,p-Xylene 1004,000
1ug/L 23-Jul-2023 05:110.20Methyl tert-butyl ether 1.03.3
1ug/L 23-Jul-2023 05:111.0Methylene chloride 2.0U
50ug/L 24-Jul-2023 14:1615Naphthalene50800
50ug/L 24-Jul-2023 14:1615o-Xylene 501,200
1ug/L 23-Jul-2023 05:1110Tert-butyl alcohol 10U
50ug/L 24-Jul-2023 14:1610Toluene50250
50ug/L 24-Jul-2023 14:1615Xylenes, Total 1505,100
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 05:1197.1 70-126
Surr: 1,2-Dichloroethane-d4 50%REC 24-Jul-2023 14:1610470-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 05:1110577-113
Surr: 4-Bromofluorobenzene 50%REC 24-Jul-2023 14:1691.2 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 05:1186.5 77-123
Surr: Dibromofluoromethane 50%REC 24-Jul-2023 14:1699.5 77-123
Surr: Toluene-d8 1%REC 23-Jul-2023 05:1110282-127
Surr: Toluene-d8 50%REC 24-Jul-2023 14:1610282-127
DISSOLVED GASES BY RSK-175 Method:RSK-175 Analyst: SAM
50ug/L 28-Jul-2023 13:305.35Methane 25.01,610
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 01:240.00301,2-Dibromoethane 0.020U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: ALRPrep:SW3010A / 03-Aug-2023
1mg/L 04-Aug-2023 00:280.0120Iron 0.20024.1
100mg/L 04-Aug-2023 13:100.0700Manganese 0.5009.96
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 03-Aug-2023 02:360.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
10mg/L 03-Aug-2023 23:02J0.300Nitrate/Nitrite (as N)2.000.899
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-24
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-07
19-Jul-2023 14:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
ALKALINITY BY SM 2320B-2011 Method:SM2320B Analyst: JAC
1mg/L 02-Aug-2023 20:005.00Alkalinity, Bicarbonate (As
CaCO3)5.00444
1mg/L 02-Aug-2023 20:005.00Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 02-Aug-2023 20:005.00Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 02-Aug-2023 20:00a5.00Alkalinity, Total (As CaCO3)5.00444
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: MZD
10mg/L 21-Jul-2023 10:400.200Ferrous Iron 0.50020.0
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-24I
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-08
19-Jul-2023 15:30 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 24-Jul-2023 16:010.301,2,4-Trimethylbenzene 1.0120
1ug/L 24-Jul-2023 16:010.201,2-Dibromoethane 1.0U
1ug/L 24-Jul-2023 16:010.201,2-Dichloroethane 1.0U
1ug/L 24-Jul-2023 16:011.02-Methylnaphthalene 1.037
1ug/L 24-Jul-2023 16:010.304-Isopropyltoluene 1.0U
1ug/L 24-Jul-2023 16:010.20Benzene 1.05.6
1ug/L 24-Jul-2023 16:010.20Chloroform 1.0U
1ug/L 24-Jul-2023 16:010.30Ethylbenzene 1.012
1ug/L 24-Jul-2023 16:010.50m,p-Xylene 2.034
1ug/L 24-Jul-2023 16:010.20Methyl tert-butyl ether 1.0U
1ug/L 24-Jul-2023 16:011.0Methylene chloride 2.0U
1ug/L 24-Jul-2023 16:010.30Naphthalene 1.053
1ug/L 24-Jul-2023 16:010.30o-Xylene 1.09.4
1ug/L 24-Jul-2023 16:0110Tert-butyl alcohol 10U
1ug/L 24-Jul-2023 16:01J0.20Toluene 1.00.54
1ug/L 24-Jul-2023 16:010.30Xylenes, Total 3.043
Surr: 1,2-Dichloroethane-d4 1%REC 24-Jul-2023 16:0110770-126
Surr: 4-Bromofluorobenzene 1%REC 24-Jul-2023 16:0192.9 77-113
Surr: Dibromofluoromethane 1%REC 24-Jul-2023 16:0110577-123
Surr: Toluene-d8 1%REC 24-Jul-2023 16:0110182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 01:480.00311,2-Dibromoethane 0.021U
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071150
HS23071150-09
19-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 24-Jul-2023 15:400.301,2,4-Trimethylbenzene 1.0U
1ug/L 24-Jul-2023 15:400.201,2-Dibromoethane 1.0U
1ug/L 24-Jul-2023 15:400.201,2-Dichloroethane 1.0U
1ug/L 24-Jul-2023 15:401.02-Methylnaphthalene 1.0U
1ug/L 24-Jul-2023 15:400.304-Isopropyltoluene 1.0U
1ug/L 24-Jul-2023 15:400.20Benzene 1.0U
1ug/L 24-Jul-2023 15:400.20Chloroform 1.0U
1ug/L 24-Jul-2023 15:400.30Ethylbenzene 1.0U
1ug/L 24-Jul-2023 15:400.50m,p-Xylene 2.0U
1ug/L 24-Jul-2023 15:400.20Methyl tert-butyl ether 1.0U
1ug/L 24-Jul-2023 15:401.0Methylene chloride 2.0U
1ug/L 24-Jul-2023 15:400.30Naphthalene 1.0U
1ug/L 24-Jul-2023 15:400.30o-Xylene 1.0U
1ug/L 24-Jul-2023 15:4010Tert-butyl alcohol 10U
1ug/L 24-Jul-2023 15:400.20Toluene 1.0U
1ug/L 24-Jul-2023 15:400.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 24-Jul-2023 15:4010670-126
Surr: 4-Bromofluorobenzene 1%REC 24-Jul-2023 15:4091.7 77-113
Surr: Dibromofluoromethane 1%REC 24-Jul-2023 15:4010477-123
Surr: Toluene-d8 1%REC 24-Jul-2023 15:4010282-127
04-Aug-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Weight / Prep Log
HS23071150
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:198051
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 26 Jul 2023 07:02 End Date: 26 Jul 2023 07:02
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071150-01 35 (mL)40 mL VOA vial, HCl to pH <236.52 (mL)1.043
HS23071150-02 35 (mL)40 mL VOA vial, HCl to pH <236.46 (mL)1.042
HS23071150-03 35 (mL)40 mL VOA vial, HCl to pH <236.63 (mL)1.047
HS23071150-04 35 (mL)40 mL VOA vial, HCl to pH <236.97 (mL)1.056
HS23071150-05 35 (mL)40 mL VOA vial, HCl to pH <236.46 (mL)1.042
HS23071150-06 35 (mL)40 mL VOA vial, HCl to pH <236.41 (mL)1.04
HS23071150-07 35 (mL)40 mL VOA vial, HCl to pH <235 (mL)1
Batch ID:198053
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 26 Jul 2023 07:05 End Date: 26 Jul 2023 07:05
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071150-08 35 (mL)40 mL VOA vial, HCl to pH <236.32 (mL)1.038
Batch ID:198516
Method:WATER - SW3010A 3010APrep Code:
Start Date: 03 Aug 2023 13:30 End Date: 03 Aug 2023 13:30
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071150-06 10 (mL)120 plastic HNO310 (mL)1
HS23071150-07 10 (mL)120 plastic HNO310 (mL)1
04-Aug-23Date: ALS Houston, US
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071150
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:198051 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
26 Jul 2023 07:02 26 Jul 2023 23:03HS23071150-01 19 Jul 2023 08:55 1AMW-9S
26 Jul 2023 07:02 26 Jul 2023 23:27HS23071150-02 19 Jul 2023 09:50 1AMW-8S
26 Jul 2023 07:02 26 Jul 2023 23:50HS23071150-03 19 Jul 2023 11:45 1PMW-J-I
26 Jul 2023 07:02 27 Jul 2023 00:14HS23071150-04 19 Jul 2023 10:50 1PMW-J-D
26 Jul 2023 07:02 27 Jul 2023 00:37HS23071150-05 19 Jul 2023 12:40 1PMW-J-B
26 Jul 2023 07:02 27 Jul 2023 01:01HS23071150-06 19 Jul 2023 13:40 1FMW-24D
26 Jul 2023 07:02 27 Jul 2023 01:24HS23071150-07 19 Jul 2023 14:30 1FMW-24
Batch ID:198053 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
26 Jul 2023 07:05 27 Jul 2023 01:48HS23071150-08 19 Jul 2023 15:30 1FMW-24I
Batch ID:198516 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Groundwater
03 Aug 2023 13:30 04 Aug 2023 00:13HS23071150-06 19 Jul 2023 13:40 1FMW-24D
03 Aug 2023 13:30 04 Aug 2023 13:10HS23071150-07 19 Jul 2023 14:30 100FMW-24
03 Aug 2023 13:30 04 Aug 2023 00:28HS23071150-07 19 Jul 2023 14:30 1FMW-24
Batch ID:R441924 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Groundwater
21 Jul 2023 10:40HS23071150-06 19 Jul 2023 13:40 1FMW-24D
21 Jul 2023 10:40HS23071150-07 19 Jul 2023 14:30 10FMW-24
Batch ID:R442053 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
22 Jul 2023 17:59HS23071150-01 19 Jul 2023 08:55 1AMW-9S
22 Jul 2023 18:20HS23071150-02 19 Jul 2023 09:50 1AMW-8S
22 Jul 2023 18:41HS23071150-03 19 Jul 2023 11:45 1PMW-J-I
22 Jul 2023 19:02HS23071150-04 19 Jul 2023 10:50 1PMW-J-D
22 Jul 2023 19:23HS23071150-05 19 Jul 2023 12:40 1PMW-J-B
Batch ID:R442056 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
23 Jul 2023 04:50HS23071150-06 19 Jul 2023 13:40 1FMW-24D
23 Jul 2023 05:11HS23071150-07 19 Jul 2023 14:30 1FMW-24
Batch ID:R442082 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
24 Jul 2023 15:40HS23071150-09 19 Jul 2023 00:00 1Trip Blank
Batch ID:R442082 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
24 Jul 2023 14:16HS23071150-07 19 Jul 2023 14:30 50FMW-24
24 Jul 2023 16:01HS23071150-08 19 Jul 2023 15:30 1FMW-24I
Batch ID:R442732 ( 0 ) Test Name :DISSOLVED GASES BY RSK-175 Matrix:Groundwater
28 Jul 2023 12:10HS23071150-06 19 Jul 2023 13:40 1FMW-24D
28 Jul 2023 13:30HS23071150-07 19 Jul 2023 14:30 50FMW-24
Batch ID:R443060 ( 0 ) Test Name :ALKALINITY BY SM 2320B-2011 Matrix:Groundwater
02 Aug 2023 19:54HS23071150-06 19 Jul 2023 13:40 1FMW-24D
02 Aug 2023 20:00HS23071150-07 19 Jul 2023 14:30 1FMW-24
04-Aug-23Date: ALS Houston, US
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071150
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R443081 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Groundwater
03 Aug 2023 02:19HS23071150-06 19 Jul 2023 13:40 1FMW-24D
03 Aug 2023 02:36HS23071150-07 19 Jul 2023 14:30 1FMW-24
Batch ID:R443157 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Groundwater
03 Aug 2023 22:56HS23071150-06 19 Jul 2023 13:40 10FMW-24D
03 Aug 2023 23:02HS23071150-07 19 Jul 2023 14:30 10FMW-24
04-Aug-23Date: ALS Houston, US
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:198051 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-198051 Units:ug/L Analysis Date:26-Jul-2023 11:51
Run ID:ECD_13_442465 SeqNo:7454594 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-198051 Units:ug/L Analysis Date:26-Jul-2023 12:14
Run ID:ECD_13_442465 SeqNo:7454595 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1692 0.25 0 67.7 60 - 1400.020
Sample ID:LCSD-198051 Units:ug/L Analysis Date:26-Jul-2023 12:38
Run ID:ECD_13_442465 SeqNo:7454596 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1705 0.25 0 68.2 60 - 140 0.1692 0.781 200.020
The following samples were analyzed in this batch:HS23071150-01 HS23071150-02 HS23071150-03 HS23071150-04
HS23071150-05 HS23071150-06 HS23071150-07
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:198053 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-198053 Units:ug/L Analysis Date:26-Jul-2023 14:36
Run ID:ECD_13_442466 SeqNo:7454617 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-198053 Units:ug/L Analysis Date:26-Jul-2023 15:00
Run ID:ECD_13_442466 SeqNo:7454618 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1669 0.25 0 66.8 60 - 1400.020
Sample ID:LCSD-198053 Units:ug/L Analysis Date:26-Jul-2023 15:23
Run ID:ECD_13_442466 SeqNo:7454619 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1805 0.25 0 72.2 60 - 140 0.1669 7.84 200.020
The following samples were analyzed in this batch:HS23071150-08
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442732 ( 0 )Instrument:FID-4 Method:DISSOLVED GASES BY RSK-175
Sample ID:MBLK-230728 Units:ug/L Analysis Date:28-Jul-2023 08:00
Run ID:FID-4_442732 SeqNo:7460972 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Methane U 0.500
Sample ID:LCS-230728 Units:ug/L Analysis Date:28-Jul-2023 08:09
Run ID:FID-4_442732 SeqNo:7460973 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Methane 7.953 9.647 0 82.4 75 - 1250.500
Sample ID:LCSD-230728 Units:ug/L Analysis Date:28-Jul-2023 08:18
Run ID:FID-4_442732 SeqNo:7460974 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Methane 8.01 9.647 0 83.0 75 - 125 7.953 0.72 300.500
The following samples were analyzed in this batch:HS23071150-06 HS23071150-07
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:198516 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-198516 Units:mg/L Analysis Date:04-Aug-2023 00:09
Run ID:ICPMS06_443146 SeqNo:7471560 PrepDate:03-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:LCS-198516 Units:mg/L Analysis Date:04-Aug-2023 00:11
Run ID:ICPMS06_443146 SeqNo:7471561 PrepDate:03-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.963 5 0 99.3 80 - 1200.200
Manganese 0.04918 0.05 0 98.4 80 - 1200.00500
Sample ID:HS23071150-06MS Units:mg/L Analysis Date:04-Aug-2023 00:18
Run ID:ICPMS06_443146 SeqNo:7471564 PrepDate:03-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:FMW-24D
Iron 4.61 5 0.04766 91.2 80 - 1200.200
Manganese 0.1328 0.05 0.08645 92.7 80 - 1200.00500
Sample ID:HS23071150-06MSD Units:mg/L Analysis Date:04-Aug-2023 00:20
Run ID:ICPMS06_443146 SeqNo:7471565 PrepDate:03-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:FMW-24D
Iron 4.612 5 0.04766 91.3 80 - 120 4.61 0.0556 200.200
Manganese 0.1314 0.05 0.08645 89.9 80 - 120 0.1328 1.06 200.00500
Sample ID:HS23071150-06PDS Units:mg/L Analysis Date:04-Aug-2023 00:22
Run ID:ICPMS06_443146 SeqNo:7471566 PrepDate:03-Aug-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:FMW-24D
Iron 9.582 10 0.04766 95.3 75 - 1250.200
Manganese 0.1835 0.1 0.08645 97.0 75 - 1250.00500
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:198516 ( 0 )Instrument:ICPMS06 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23071150-06SD Units:mg/L Analysis Date:04-Aug-2023 00:16
Run ID:ICPMS06_443146 SeqNo:7471563 PrepDate:03-Aug-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:FMW-24D
Iron U 0.04766 0 101.00
Manganese 0.08962 0.08645 3.67 100.0250
The following samples were analyzed in this batch:HS23071150-06 HS23071150-07
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442053 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230722 Units:ug/L Analysis Date:22-Jul-2023 11:41
Run ID:VOA10_442053 SeqNo:7444839 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
51.39 50 0 103 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.48 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
52.66 50 0 105 73 - 1261.0Surr: Dibromofluoromethane
50.2 50 0 100 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442053 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230722 Units:ug/L Analysis Date:22-Jul-2023 10:59
Run ID:VOA10_442053 SeqNo:7444838 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 20.71 20 0 104 73 - 1211.0
1,2-Dibromoethane 19.69 20 0 98.5 76 - 1231.0
1,2-Dichloroethane 18.75 20 0 93.7 70 - 1241.0
2-Methylnaphthalene 20.29 20 0 101 55 - 1401.0
4-Isopropyltoluene 23.39 20 0 117 74 - 1261.0
Benzene 17.3 20 0 86.5 74 - 1201.0
Chloroform 18.37 20 0 91.9 71 - 1211.0
Ethylbenzene 17.99 20 0 89.9 77 - 1171.0
m,p-Xylene 36.93 40 0 92.3 77 - 1222.0
Methyl tert-butyl ether 17.87 20 0 89.3 70 - 1301.0
Methylene chloride 18.65 20 0 93.2 70 - 1272.0
Naphthalene 21.43 20 0 107 70 - 1301.0
o-Xylene 17.73 20 0 88.7 75 - 1191.0
Tert-butyl alcohol 353.5 400 0 88.4 70 - 13010
Toluene 19.64 20 0 98.2 77 - 1181.0
Xylenes, Total 54.66 60 0 91.1 75 - 1223.0
51.93 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.22 50 0 92.4 77 - 1131.0Surr: 4-Bromofluorobenzene
49.35 50 0 98.7 73 - 1261.0Surr: Dibromofluoromethane
52.53 50 0 105 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442053 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071230-10MS Units:ug/L Analysis Date:22-Jul-2023 12:23
Run ID:VOA10_442053 SeqNo:7444841 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 21.62 20 0 108 70 - 1251.0
1,2-Dibromoethane 18.92 20 0 94.6 70 - 1241.0
1,2-Dichloroethane 20.13 20 0 101 70 - 1271.0
2-Methylnaphthalene 16.4 20 0 82.0 55 - 1401.0
4-Isopropyltoluene 23.56 20 0 118 70 - 1301.0
Benzene 18.99 20 0 95.0 70 - 1271.0
Chloroform 19.95 20 0 99.7 70 - 1251.0
Ethylbenzene 19.54 20 0 97.7 70 - 1241.0
m,p-Xylene 39.43 40 0 98.6 70 - 1302.0
Methyl tert-butyl ether 18.07 20 0 90.3 70 - 1301.0
Methylene chloride 19.85 20 0 99.2 70 - 1282.0
Naphthalene 19.77 20 0 98.9 70 - 1301.0
o-Xylene 18.41 20 0 92.0 70 - 1241.0
Tert-butyl alcohol 308 400 0 77.0 70 - 13010
Toluene 20.8 20 0 104 70 - 1231.0
Xylenes, Total 57.84 60 0 96.4 70 - 1303.0
50.63 50 0 101 70 - 1261.0Surr: 1,2-Dichloroethane-d4
46.84 50 0 93.7 77 - 1131.0Surr: 4-Bromofluorobenzene
48.48 50 0 97.0 77 - 1231.0Surr: Dibromofluoromethane
51.25 50 0 103 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442053 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071230-10MSD Units:ug/L Analysis Date:22-Jul-2023 12:44
Run ID:VOA10_442053 SeqNo:7444842 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 21.19 20 0 106 70 - 125 21.62 2 201.0
1,2-Dibromoethane 19.53 20 0 97.6 70 - 124 18.92 3.19 201.0
1,2-Dichloroethane 20.15 20 0 101 70 - 127 20.13 0.105 201.0
2-Methylnaphthalene 18.64 20 0 93.2 55 - 140 16.4 12.8 201.0
4-Isopropyltoluene 23.98 20 0 120 70 - 130 23.56 1.76 201.0
Benzene 19.27 20 0 96.3 70 - 127 18.99 1.43 201.0
Chloroform 20.08 20 0 100 70 - 125 19.95 0.652 201.0
Ethylbenzene 18.89 20 0 94.5 70 - 124 19.54 3.35 201.0
m,p-Xylene 38.32 40 0 95.8 70 - 130 39.43 2.85 202.0
Methyl tert-butyl ether 18.37 20 0 91.9 70 - 130 18.07 1.69 201.0
Methylene chloride 18.03 20 0 90.1 70 - 128 19.85 9.6 202.0
Naphthalene 21.25 20 0 106 70 - 130 19.77 7.22 201.0
o-Xylene 17.43 20 0 87.1 70 - 124 18.41 5.48 201.0
Tert-butyl alcohol 334.8 400 0 83.7 70 - 130 308 8.35 2010
Toluene 19.95 20 0 99.7 70 - 123 20.8 4.18 201.0
Xylenes, Total 55.75 60 0 92.9 70 - 130 57.84 3.68 203.0
53.76 50 0 108 70 - 126 50.63 6 201.0Surr: 1,2-Dichloroethane-d4
46.83 50 0 93.7 77 - 113 46.84 0.0244 201.0Surr: 4-Bromofluorobenzene
49.62 50 0 99.2 77 - 123 48.48 2.31 201.0Surr: Dibromofluoromethane
50.77 50 0 102 82 - 127 51.25 0.943 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071150-01 HS23071150-02 HS23071150-03 HS23071150-04
HS23071150-05
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230722 Units:ug/L Analysis Date:22-Jul-2023 22:32
Run ID:VOA10_442056 SeqNo:7445003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
51.96 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.12 50 0 90.2 77 - 1131.0Surr: 4-Bromofluorobenzene
50.63 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
49.14 50 0 98.3 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230722 Units:ug/L Analysis Date:22-Jul-2023 21:50
Run ID:VOA10_442056 SeqNo:7445002 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.9 20 0 94.5 73 - 1211.0
1,2-Dibromoethane 17.73 20 0 88.7 76 - 1231.0
1,2-Dichloroethane 18.09 20 0 90.5 70 - 1241.0
2-Methylnaphthalene 18.56 20 0 92.8 55 - 1401.0
4-Isopropyltoluene 21.17 20 0 106 74 - 1261.0
Benzene 17.28 20 0 86.4 74 - 1201.0
Chloroform 18.34 20 0 91.7 71 - 1211.0
Ethylbenzene 17.29 20 0 86.4 77 - 1171.0
m,p-Xylene 33.79 40 0 84.5 77 - 1222.0
Methyl tert-butyl ether 17.6 20 0 88.0 70 - 1301.0
Methylene chloride 18.42 20 0 92.1 70 - 1272.0
Naphthalene 19.51 20 0 97.6 70 - 1301.0
o-Xylene 16.4 20 0 82.0 75 - 1191.0
Tert-butyl alcohol 356.9 400 0 89.2 70 - 13010
Toluene 18.3 20 0 91.5 77 - 1181.0
Xylenes, Total 50.19 60 0 83.6 75 - 1223.0
52.12 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.52 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
52.47 50 0 105 73 - 1261.0Surr: Dibromofluoromethane
50.46 50 0 101 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071175-10MS Units:ug/L Analysis Date:22-Jul-2023 23:14
Run ID:VOA10_442056 SeqNo:7445005 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 21.16 20 0 106 70 - 1251.0
1,2-Dibromoethane 19.21 20 0 96.0 70 - 1241.0
1,2-Dichloroethane 18.93 20 0 94.7 70 - 1271.0
2-Methylnaphthalene 16 20 0 80.0 55 - 1401.0
4-Isopropyltoluene 23.15 20 0 116 70 - 1301.0
Benzene 17.53 20 0 87.7 70 - 1271.0
Chloroform 19.34 20 0 96.7 70 - 1251.0
Ethylbenzene 18.64 20 0 93.2 70 - 1241.0
m,p-Xylene 37.69 40 0 94.2 70 - 1302.0
Methyl tert-butyl ether 17.58 20 0 87.9 70 - 1301.0
Methylene chloride 15.45 20 0 77.2 70 - 1282.0
Naphthalene 20.23 20 0 101 70 - 1301.0
o-Xylene 18.13 20 0 90.7 70 - 1241.0
Tert-butyl alcohol 297.9 400 0 74.5 70 - 13010
Toluene 19.9 20 0 99.5 70 - 1231.0
Xylenes, Total 55.83 60 0 93.0 70 - 1303.0
52.12 50 0 104 70 - 1261.0Surr: 1,2-Dichloroethane-d4
45.4 50 0 90.8 77 - 1131.0Surr: 4-Bromofluorobenzene
51.12 50 0 102 77 - 1231.0Surr: Dibromofluoromethane
52.07 50 0 104 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071175-10MSD Units:ug/L Analysis Date:22-Jul-2023 23:35
Run ID:VOA10_442056 SeqNo:7445006 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 19.11 20 0 95.5 70 - 125 21.16 10.2 201.0
1,2-Dibromoethane 16.87 20 0 84.3 70 - 124 19.21 13 201.0
1,2-Dichloroethane 17.97 20 0 89.9 70 - 127 18.93 5.19 201.0
2-Methylnaphthalene 16.56 20 0 82.8 55 - 140 16 3.38 201.0
4-Isopropyltoluene 20.88 20 0 104 70 - 130 23.15 10.3 201.0
Benzene 16.86 20 0 84.3 70 - 127 17.53 3.93 201.0
Chloroform 18.61 20 0 93.1 70 - 125 19.34 3.85 201.0
Ethylbenzene 17.07 20 0 85.4 70 - 124 18.64 8.76 201.0
m,p-Xylene 35.12 40 0 87.8 70 - 130 37.69 7.07 202.0
Methyl tert-butyl ether 16.61 20 0 83.0 70 - 130 17.58 5.67 201.0
Methylene chloride 17.61 20 0 88.0 70 - 128 15.45 13.1 202.0
Naphthalene 18.65 20 0 93.3 70 - 130 20.23 8.12 201.0
o-Xylene 15.72 20 0 78.6 70 - 124 18.13 14.3 201.0
Tert-butyl alcohol 291.6 400 0 72.9 70 - 130 297.9 2.11 2010
Toluene 17.68 20 0 88.4 70 - 123 19.9 11.8 201.0
Xylenes, Total 50.84 60 0 84.7 70 - 130 55.83 9.35 203.0
52.45 50 0 105 70 - 126 52.12 0.623 201.0Surr: 1,2-Dichloroethane-d4
47.48 50 0 95.0 77 - 113 45.4 4.49 201.0Surr: 4-Bromofluorobenzene
51.2 50 0 102 77 - 123 51.12 0.159 201.0Surr: Dibromofluoromethane
51.09 50 0 102 82 - 127 52.07 1.91 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071150-06 HS23071150-07
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442082 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230724 Units:ug/L Analysis Date:24-Jul-2023 10:25
Run ID:VOA10_442082 SeqNo:7445533 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
52.47 50 0 105 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.78 50 0 93.6 77 - 1131.0Surr: 4-Bromofluorobenzene
51.48 50 0 103 73 - 1261.0Surr: Dibromofluoromethane
50.01 50 0 100 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442082 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230724 Units:ug/L Analysis Date:24-Jul-2023 09:43
Run ID:VOA10_442082 SeqNo:7445532 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 20.87 20 0 104 73 - 1211.0
1,2-Dibromoethane 20.58 20 0 103 76 - 1231.0
1,2-Dichloroethane 20.74 20 0 104 70 - 1241.0
2-Methylnaphthalene 21.11 20 0 106 55 - 1401.0
4-Isopropyltoluene 22.31 20 0 112 74 - 1261.0
Benzene 18.96 20 0 94.8 74 - 1201.0
Chloroform 20.3 20 0 102 71 - 1211.0
Ethylbenzene 18.93 20 0 94.6 77 - 1171.0
m,p-Xylene 38.38 40 0 96.0 77 - 1222.0
Methyl tert-butyl ether 19.23 20 0 96.2 70 - 1301.0
Methylene chloride 19.74 20 0 98.7 70 - 1272.0
Naphthalene 21.26 20 0 106 70 - 1301.0
o-Xylene 18.53 20 0 92.6 75 - 1191.0
Tert-butyl alcohol 433.9 400 0 108 70 - 13010
Toluene 20.11 20 0 101 77 - 1181.0
Xylenes, Total 56.91 60 0 94.9 75 - 1223.0
52.42 50 0 105 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.32 50 0 96.6 77 - 1131.0Surr: 4-Bromofluorobenzene
51.2 50 0 102 73 - 1261.0Surr: Dibromofluoromethane
51.03 50 0 102 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442082 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071230-06MS Units:ug/L Analysis Date:24-Jul-2023 11:07
Run ID:VOA10_442082 SeqNo:7445535 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 20.87 20 0 104 70 - 1251.0
1,2-Dibromoethane 19.11 20 0 95.5 70 - 1241.0
1,2-Dichloroethane 20.49 20 0 102 70 - 1271.0
2-Methylnaphthalene 15.9 20 0 79.5 55 - 1401.0
4-Isopropyltoluene 23.29 20 0 116 70 - 1301.0
Benzene 18.89 20 0 94.5 70 - 1271.0
Chloroform 19.48 20 0 97.4 70 - 1251.0
Ethylbenzene 18.63 20 0 93.1 70 - 1241.0
m,p-Xylene 38.63 40 0 96.6 70 - 1302.0
Methyl tert-butyl ether 17.81 20 0 89.1 70 - 1301.0
Methylene chloride 19.36 20 0 96.8 70 - 1282.0
Naphthalene 19.33 20 0 96.7 70 - 1301.0
o-Xylene 17.36 20 0 86.8 70 - 1241.0
Tert-butyl alcohol 322.2 400 0 80.6 70 - 13010
Toluene 20.25 20 0 101 70 - 1231.0
Xylenes, Total 55.98 60 0 93.3 70 - 1303.0
53.52 50 0 107 70 - 1261.0Surr: 1,2-Dichloroethane-d4
47.39 50 0 94.8 77 - 1131.0Surr: 4-Bromofluorobenzene
50.15 50 0 100 77 - 1231.0Surr: Dibromofluoromethane
51.1 50 0 102 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R442082 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071230-06MSD Units:ug/L Analysis Date:24-Jul-2023 11:28
Run ID:VOA10_442082 SeqNo:7445536 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 20.44 20 0 102 70 - 125 20.87 2.09 201.0
1,2-Dibromoethane 18.18 20 0 90.9 70 - 124 19.11 4.99 201.0
1,2-Dichloroethane 19.69 20 0 98.5 70 - 127 20.49 3.94 201.0
2-Methylnaphthalene 17.23 20 0 86.1 55 - 140 15.9 8.04 201.0
4-Isopropyltoluene 23.22 20 0 116 70 - 130 23.29 0.288 201.0
Benzene 18.6 20 0 93.0 70 - 127 18.89 1.56 201.0
Chloroform 20.7 20 0 104 70 - 125 19.48 6.09 201.0
Ethylbenzene 18.34 20 0 91.7 70 - 124 18.63 1.59 201.0
m,p-Xylene 37.24 40 0 93.1 70 - 130 38.63 3.67 202.0
Methyl tert-butyl ether 18.53 20 0 92.6 70 - 130 17.81 3.93 201.0
Methylene chloride 18.97 20 0 94.9 70 - 128 19.36 2.03 202.0
Naphthalene 20.65 20 0 103 70 - 130 19.33 6.62 201.0
o-Xylene 17.77 20 0 88.8 70 - 124 17.36 2.36 201.0
Tert-butyl alcohol 337.5 400 0 84.4 70 - 130 322.2 4.64 2010
Toluene 19.54 20 0 97.7 70 - 123 20.25 3.56 201.0
Xylenes, Total 55 60 0 91.7 70 - 130 55.98 1.76 203.0
51.66 50 0 103 70 - 126 53.52 3.54 201.0Surr: 1,2-Dichloroethane-d4
47.25 50 0 94.5 77 - 113 47.39 0.286 201.0Surr: 4-Bromofluorobenzene
51.06 50 0 102 77 - 123 50.15 1.79 201.0Surr: Dibromofluoromethane
51.52 50 0 103 82 - 127 51.1 0.821 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071150-07 HS23071150-08 HS23071150-09
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R441924 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442034 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R441924 Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442033 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.263 0.25 0 105 80 - 1200.0500
Sample ID:HS23071069-04MS Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442036 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ferrous Iron 0.504 0.25 0.279 90.0 75 - 1250.0500
Sample ID:HS23071069-04MSD Units:mg/L Analysis Date:21-Jul-2023 10:40
Run ID:UV-2450_441924 SeqNo:7442035 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ferrous Iron 0.505 0.25 0.279 90.4 75 - 125 0.504 0.198 200.0500
The following samples were analyzed in this batch:HS23071150-06 HS23071150-07
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R443060 ( 0 )Instrument:ManTech01 Method:ALKALINITY BY SM 2320B-2011
Sample ID:WBLKW2-080223 Units:mg/L Analysis Date:02-Aug-2023 19:40
Run ID:ManTech01_443060 SeqNo:7469149 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS2-080223 Units:mg/L Analysis Date:02-Aug-2023 19:11
Run ID:ManTech01_443060 SeqNo:7469145 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)988.4 1000 0 98.8 85 - 1155.00
Alkalinity, Total (As CaCO3)1028 1000 0 103 85 - 1155.00
Sample ID:LCSD2-080223 Units:mg/L Analysis Date:02-Aug-2023 19:20
Run ID:ManTech01_443060 SeqNo:7469146 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)997.6 1000 0 99.8 85 - 115 988.4 0.935 205.00
Alkalinity, Total (As CaCO3)1006 1000 0 101 85 - 115 1028 2.16 205.00
Sample ID:HS23071112-04DUP Units:mg/L Analysis Date:02-Aug-2023 19:47
Run ID:ManTech01_443060 SeqNo:7469151 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 0 0 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)U 0 0 205.00
The following samples were analyzed in this batch:HS23071150-06 HS23071150-07
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R443081 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:03-Aug-2023 00:40
Run ID:ICS-Integrion_443081 SeqNo:7469574 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:03-Aug-2023 00:46
Run ID:ICS-Integrion_443081 SeqNo:7469575 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 21.2 20 0 106 90 - 1100.500
Sample ID:HS23071261-08MS Units:mg/L Analysis Date:03-Aug-2023 01:27
Run ID:ICS-Integrion_443081 SeqNo:7469581 PrepDate:DF:100
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 2812 1000 1913 90.0 80 - 12050.0
Sample ID:HS23071150-06MS Units:mg/L Analysis Date:03-Aug-2023 02:25
Run ID:ICS-Integrion_443081 SeqNo:7469588 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:FMW-24D
Sulfate 12.76 10 2.128 106 80 - 1200.500
Sample ID:HS23071261-08MSD Units:mg/L Analysis Date:03-Aug-2023 01:32
Run ID:ICS-Integrion_443081 SeqNo:7469582 PrepDate:DF:100
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 2830 1000 1913 91.7 80 - 120 2812 0.614 2050.0
Sample ID:HS23071150-06MSD Units:mg/L Analysis Date:03-Aug-2023 02:30
Run ID:ICS-Integrion_443081 SeqNo:7469589 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:FMW-24D
Sulfate 12.99 10 2.128 109 80 - 120 12.76 1.79 200.500
The following samples were analyzed in this batch:HS23071150-06 HS23071150-07
ALS Houston, US Date: 04-Aug-23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071150
QC BATCH REPORT
Batch ID:R443157 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:03-Aug-2023 22:27
Run ID:ICS-Integrion_443157 SeqNo:7471623 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:03-Aug-2023 22:39
Run ID:ICS-Integrion_443157 SeqNo:7471624 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.459 8 0 106 90 - 1100.200
Sample ID:HS23080130-01MS Units:mg/L Analysis Date:04-Aug-2023 00:17
Run ID:ICS-Integrion_443157 SeqNo:7471636 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)38.38 40 0 95.9 80 - 1202.00
Sample ID:HS23071390-01MS Units:mg/L Analysis Date:03-Aug-2023 23:14
Run ID:ICS-Integrion_443157 SeqNo:7471629 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Nitrate/Nitrite (as N)40.47 40 3.072 93.5 80 - 1202.00
Sample ID:HS23080130-01MSD Units:mg/L Analysis Date:04-Aug-2023 00:23
Run ID:ICS-Integrion_443157 SeqNo:7471637 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)39.27 40 0 98.2 80 - 120 38.38 2.31 202.00
Sample ID:HS23071390-01MSD Units:mg/L Analysis Date:03-Aug-2023 23:19
Run ID:ICS-Integrion_443157 SeqNo:7471630 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Nitrate/Nitrite (as N)40.72 40 3.072 94.1 80 - 120 40.47 0.621 202.00
The following samples were analyzed in this batch:HS23071150-06 HS23071150-07
ALS Houston, US Date: 04-Aug-23
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071150
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 04-Aug-23
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
04-Aug-23Date: ALS Houston, US
Corey Grandits
21-Jul-2023 09:30Date/Time Received:HS23071150
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.1UC/3.0C IR31
50575
7/21/23
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
1 Trip Blank vial received broken
Completed By:/S/ Corey Grandits
Date/TimeeSignatureDate/TimeeSignature
21-Jul-2023 14:5221-Jul-2023 11:44
FedExWCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241079
ALS Houston, US 04-Aug-23Date:
July 28, 2023
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 8 sample(s) on Jul 21, 2023 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23071263
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 23
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23071263
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23071263-01 20-Jul-2023 09:36 21-Jul-2023 09:30FMW-15 Groundwater
HS23071263-02 20-Jul-2023 10:40 21-Jul-2023 09:30FPZ-10 Groundwater
HS23071263-03 20-Jul-2023 10:35 21-Jul-2023 09:30AMW-15S Groundwater
HS23071263-04 20-Jul-2023 00:00 21-Jul-2023 09:30DUP#4 Groundwater
HS23071263-05 20-Jul-2023 00:00 21-Jul-2023 09:30DUP#5 Groundwater
HS23071263-06 20-Jul-2023 11:10 21-Jul-2023 09:30Equipment Blank #4 Water
HS23071263-07 20-Jul-2023 11:15 21-Jul-2023 09:30Field Blank #4 Water
HS23071263-08 20-Jul-2023 00:00 21-Jul-2023 09:30Trip Blank Water
ALS Houston, US 28-Jul-23Date:
Page 2 of 23
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23071263
ECD Organics by Method SW8011
Batch ID: 198053
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R442056
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 28-Jul-23Date:
Page 3 of 23
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-15
WorkOrder:
Lab ID:
Collection Date:
HS23071263
HS23071263-01
20-Jul-2023 09:36 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 23-Jul-2023 03:050.301,2,4-Trimethylbenzene 1.0U
1ug/L 23-Jul-2023 03:050.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 03:050.201,2-Dichloroethane 1.0U
1ug/L 23-Jul-2023 03:051.02-Methylnaphthalene 1.0U
1ug/L 23-Jul-2023 03:050.304-Isopropyltoluene 1.0U
1ug/L 23-Jul-2023 03:050.20Benzene 1.0U
1ug/L 23-Jul-2023 03:050.20Chloroform 1.0U
1ug/L 23-Jul-2023 03:050.30Ethylbenzene 1.0U
1ug/L 23-Jul-2023 03:050.50m,p-Xylene 2.0U
1ug/L 23-Jul-2023 03:050.20Methyl tert-butyl ether 1.0U
1ug/L 23-Jul-2023 03:051.0Methylene chloride 2.0U
1ug/L 23-Jul-2023 03:050.30Naphthalene 1.0U
1ug/L 23-Jul-2023 03:050.30o-Xylene 1.0U
1ug/L 23-Jul-2023 03:0510Tert-butyl alcohol 10U
1ug/L 23-Jul-2023 03:050.20Toluene 1.0U
1ug/L 23-Jul-2023 03:050.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 03:0510570-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 03:0590.6 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 03:0510277-123
Surr: Toluene-d8 1%REC 23-Jul-2023 03:0599.8 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 03:220.00311,2-Dibromoethane 0.021U
28-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of 23
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FPZ-10
WorkOrder:
Lab ID:
Collection Date:
HS23071263
HS23071263-02
20-Jul-2023 10:40 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 23-Jul-2023 03:260.301,2,4-Trimethylbenzene 1.020
1ug/L 23-Jul-2023 03:260.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 03:260.201,2-Dichloroethane 1.0U
1ug/L 23-Jul-2023 03:261.02-Methylnaphthalene 1.06.4
1ug/L 23-Jul-2023 03:260.304-Isopropyltoluene 1.0U
1ug/L 23-Jul-2023 03:260.20Benzene 1.04.1
1ug/L 23-Jul-2023 03:260.20Chloroform 1.0U
1ug/L 23-Jul-2023 03:260.30Ethylbenzene 1.01.5
1ug/L 23-Jul-2023 03:260.50m,p-Xylene 2.04.1
1ug/L 23-Jul-2023 03:260.20Methyl tert-butyl ether 1.0U
1ug/L 23-Jul-2023 03:261.0Methylene chloride 2.0U
1ug/L 23-Jul-2023 03:260.30Naphthalene 1.08.1
1ug/L 23-Jul-2023 03:260.30o-Xylene 1.0U
1ug/L 23-Jul-2023 03:2610Tert-butyl alcohol 10U
1ug/L 23-Jul-2023 03:260.20Toluene 1.0U
1ug/L 23-Jul-2023 03:260.30Xylenes, Total 3.04.1
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 03:2697.8 70-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 03:2692.3 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 03:2696.3 77-123
Surr: Toluene-d8 1%REC 23-Jul-2023 03:2610182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 03:450.00311,2-Dibromoethane 0.021U
28-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 23
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-15S
WorkOrder:
Lab ID:
Collection Date:
HS23071263
HS23071263-03
20-Jul-2023 10:35 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 23-Jul-2023 03:470.301,2,4-Trimethylbenzene 1.0U
1ug/L 23-Jul-2023 03:470.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 03:470.201,2-Dichloroethane 1.0U
1ug/L 23-Jul-2023 03:471.02-Methylnaphthalene 1.0U
1ug/L 23-Jul-2023 03:470.304-Isopropyltoluene 1.0U
1ug/L 23-Jul-2023 03:470.20Benzene 1.0U
1ug/L 23-Jul-2023 03:470.20Chloroform 1.0U
1ug/L 23-Jul-2023 03:470.30Ethylbenzene 1.0U
1ug/L 23-Jul-2023 03:470.50m,p-Xylene 2.0U
1ug/L 23-Jul-2023 03:470.20Methyl tert-butyl ether 1.0U
1ug/L 23-Jul-2023 03:471.0Methylene chloride 2.0U
1ug/L 23-Jul-2023 03:470.30Naphthalene 1.0U
1ug/L 23-Jul-2023 03:470.30o-Xylene 1.0U
1ug/L 23-Jul-2023 03:4710Tert-butyl alcohol 10U
1ug/L 23-Jul-2023 03:470.20Toluene 1.0U
1ug/L 23-Jul-2023 03:470.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 03:4710670-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 03:4791.2 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 03:4710277-123
Surr: Toluene-d8 1%REC 23-Jul-2023 03:4710082-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 04:090.00311,2-Dibromoethane 0.021U
28-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 23
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DUP#4
WorkOrder:
Lab ID:
Collection Date:
HS23071263
HS23071263-04
20-Jul-2023 00:00 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 23-Jul-2023 04:080.301,2,4-Trimethylbenzene 1.0U
1ug/L 23-Jul-2023 04:080.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 04:080.201,2-Dichloroethane 1.0U
1ug/L 23-Jul-2023 04:081.02-Methylnaphthalene 1.0U
1ug/L 23-Jul-2023 04:080.304-Isopropyltoluene 1.0U
1ug/L 23-Jul-2023 04:080.20Benzene 1.0U
1ug/L 23-Jul-2023 04:080.20Chloroform 1.0U
1ug/L 23-Jul-2023 04:080.30Ethylbenzene 1.0U
1ug/L 23-Jul-2023 04:080.50m,p-Xylene 2.0U
1ug/L 23-Jul-2023 04:080.20Methyl tert-butyl ether 1.0U
1ug/L 23-Jul-2023 04:081.0Methylene chloride 2.0U
1ug/L 23-Jul-2023 04:080.30Naphthalene 1.0U
1ug/L 23-Jul-2023 04:080.30o-Xylene 1.0U
1ug/L 23-Jul-2023 04:0810Tert-butyl alcohol 10U
1ug/L 23-Jul-2023 04:080.20Toluene 1.0U
1ug/L 23-Jul-2023 04:080.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 04:0810370-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 04:0892.4 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 04:0810077-123
Surr: Toluene-d8 1%REC 23-Jul-2023 04:0899.7 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 04:320.00311,2-Dibromoethane 0.021U
28-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 23
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
DUP#5
WorkOrder:
Lab ID:
Collection Date:
HS23071263
HS23071263-05
20-Jul-2023 00:00 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 23-Jul-2023 04:290.301,2,4-Trimethylbenzene 1.08.2
1ug/L 23-Jul-2023 04:290.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 04:290.201,2-Dichloroethane 1.0U
1ug/L 23-Jul-2023 04:291.02-Methylnaphthalene 1.0U
1ug/L 23-Jul-2023 04:290.304-Isopropyltoluene 1.0U
1ug/L 23-Jul-2023 04:290.20Benzene 1.03.4
1ug/L 23-Jul-2023 04:290.20Chloroform 1.0U
1ug/L 23-Jul-2023 04:29J0.30Ethylbenzene 1.00.96
1ug/L 23-Jul-2023 04:290.50m,p-Xylene 2.02.3
1ug/L 23-Jul-2023 04:290.20Methyl tert-butyl ether 1.0U
1ug/L 23-Jul-2023 04:291.0Methylene chloride 2.0U
1ug/L 23-Jul-2023 04:290.30Naphthalene 1.04.2
1ug/L 23-Jul-2023 04:290.30o-Xylene 1.0U
1ug/L 23-Jul-2023 04:2910Tert-butyl alcohol 10U
1ug/L 23-Jul-2023 04:290.20Toluene 1.0U
1ug/L 23-Jul-2023 04:29J0.30Xylenes, Total 3.02.3
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 04:2910570-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 04:2991.3 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 04:2910177-123
Surr: Toluene-d8 1%REC 23-Jul-2023 04:2910282-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 04:560.00321,2-Dibromoethane 0.021U
28-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 23
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Equipment Blank #4
WorkOrder:
Lab ID:
Collection Date:
HS23071263
HS23071263-06
20-Jul-2023 11:10 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 23-Jul-2023 02:020.301,2,4-Trimethylbenzene 1.0U
1ug/L 23-Jul-2023 02:020.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 02:020.201,2-Dichloroethane 1.0U
1ug/L 23-Jul-2023 02:021.02-Methylnaphthalene 1.0U
1ug/L 23-Jul-2023 02:020.304-Isopropyltoluene 1.0U
1ug/L 23-Jul-2023 02:020.20Benzene 1.0U
1ug/L 23-Jul-2023 02:020.20Chloroform 1.0U
1ug/L 23-Jul-2023 02:020.30Ethylbenzene 1.0U
1ug/L 23-Jul-2023 02:020.50m,p-Xylene 2.0U
1ug/L 23-Jul-2023 02:020.20Methyl tert-butyl ether 1.0U
1ug/L 23-Jul-2023 02:021.0Methylene chloride 2.0U
1ug/L 23-Jul-2023 02:020.30Naphthalene 1.0U
1ug/L 23-Jul-2023 02:020.30o-Xylene 1.0U
1ug/L 23-Jul-2023 02:0210Tert-butyl alcohol 10U
1ug/L 23-Jul-2023 02:020.20Toluene 1.0U
1ug/L 23-Jul-2023 02:020.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 02:0210670-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 02:0290.6 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 02:0210377-123
Surr: Toluene-d8 1%REC 23-Jul-2023 02:0210382-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 05:200.00311,2-Dibromoethane 0.021U
28-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 23
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Field Blank #4
WorkOrder:
Lab ID:
Collection Date:
HS23071263
HS23071263-07
20-Jul-2023 11:15 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 23-Jul-2023 02:230.301,2,4-Trimethylbenzene 1.0U
1ug/L 23-Jul-2023 02:230.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 02:230.201,2-Dichloroethane 1.0U
1ug/L 23-Jul-2023 02:231.02-Methylnaphthalene 1.0U
1ug/L 23-Jul-2023 02:230.304-Isopropyltoluene 1.0U
1ug/L 23-Jul-2023 02:230.20Benzene 1.0U
1ug/L 23-Jul-2023 02:230.20Chloroform 1.0U
1ug/L 23-Jul-2023 02:230.30Ethylbenzene 1.0U
1ug/L 23-Jul-2023 02:230.50m,p-Xylene 2.0U
1ug/L 23-Jul-2023 02:230.20Methyl tert-butyl ether 1.0U
1ug/L 23-Jul-2023 02:231.0Methylene chloride 2.0U
1ug/L 23-Jul-2023 02:230.30Naphthalene 1.0U
1ug/L 23-Jul-2023 02:230.30o-Xylene 1.0U
1ug/L 23-Jul-2023 02:2310Tert-butyl alcohol 10U
1ug/L 23-Jul-2023 02:230.20Toluene 1.0U
1ug/L 23-Jul-2023 02:230.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 02:2310570-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 02:2391.7 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 02:2310277-123
Surr: Toluene-d8 1%REC 23-Jul-2023 02:2310182-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: JBAPrep:SW8011 / 26-Jul-2023
1ug/L 27-Jul-2023 05:430.00321,2-Dibromoethane 0.021U
28-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 23
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS23071263
HS23071263-08
20-Jul-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: FT
1ug/L 23-Jul-2023 02:440.301,2,4-Trimethylbenzene 1.0U
1ug/L 23-Jul-2023 02:440.201,2-Dibromoethane 1.0U
1ug/L 23-Jul-2023 02:440.201,2-Dichloroethane 1.0U
1ug/L 23-Jul-2023 02:441.02-Methylnaphthalene 1.0U
1ug/L 23-Jul-2023 02:440.304-Isopropyltoluene 1.0U
1ug/L 23-Jul-2023 02:440.20Benzene 1.0U
1ug/L 23-Jul-2023 02:440.20Chloroform 1.0U
1ug/L 23-Jul-2023 02:440.30Ethylbenzene 1.0U
1ug/L 23-Jul-2023 02:440.50m,p-Xylene 2.0U
1ug/L 23-Jul-2023 02:440.20Methyl tert-butyl ether 1.0U
1ug/L 23-Jul-2023 02:441.0Methylene chloride 2.0U
1ug/L 23-Jul-2023 02:440.30Naphthalene 1.0U
1ug/L 23-Jul-2023 02:440.30o-Xylene 1.0U
1ug/L 23-Jul-2023 02:4410Tert-butyl alcohol 10U
1ug/L 23-Jul-2023 02:440.20Toluene 1.0U
1ug/L 23-Jul-2023 02:440.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 23-Jul-2023 02:4410570-126
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2023 02:4490.4 77-113
Surr: Dibromofluoromethane 1%REC 23-Jul-2023 02:4410477-123
Surr: Toluene-d8 1%REC 23-Jul-2023 02:4410582-127
28-Jul-23Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 23
Weight / Prep Log
HS23071263
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:198053
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 26 Jul 2023 07:05 End Date: 26 Jul 2023 07:05
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23071263-01 35 (mL)40 mL VOA vial, HCl to pH <236.73 (mL)1.049
HS23071263-02 35 (mL)40 mL VOA vial, HCl to pH <236.61 (mL)1.046
HS23071263-03 35 (mL)40 mL VOA vial, HCl to pH <236.55 (mL)1.044
HS23071263-04 35 (mL)40 mL VOA vial, HCl to pH <236.15 (mL)1.033
HS23071263-05 35 (mL)40 mL VOA vial, HCl to pH <236.99 (mL)1.057
HS23071263-06 35 (mL)40 mL VOA vial, HCl to pH <236.56 (mL)1.045
HS23071263-07 35 (mL)40 mL VOA vial, HCl to pH <236.79 (mL)1.051
28-Jul-23Date: ALS Houston, US
Page 12 of 23
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23071263
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:198053 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Water
26 Jul 2023 07:05 27 Jul 2023 05:20HS23071263-06 20 Jul 2023 11:10 1Equipment Blank #4
26 Jul 2023 07:05 27 Jul 2023 05:43HS23071263-07 20 Jul 2023 11:15 1Field Blank #4
Batch ID:198053 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
26 Jul 2023 07:05 27 Jul 2023 03:22HS23071263-01 20 Jul 2023 09:36 1FMW-15
26 Jul 2023 07:05 27 Jul 2023 03:45HS23071263-02 20 Jul 2023 10:40 1FPZ-10
26 Jul 2023 07:05 27 Jul 2023 04:09HS23071263-03 20 Jul 2023 10:35 1AMW-15S
26 Jul 2023 07:05 27 Jul 2023 04:32HS23071263-04 20 Jul 2023 00:00 1DUP#4
26 Jul 2023 07:05 27 Jul 2023 04:56HS23071263-05 20 Jul 2023 00:00 1DUP#5
Batch ID:R442056 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
23 Jul 2023 02:02HS23071263-06 20 Jul 2023 11:10 1Equipment Blank #4
23 Jul 2023 02:23HS23071263-07 20 Jul 2023 11:15 1Field Blank #4
23 Jul 2023 02:44HS23071263-08 20 Jul 2023 00:00 1Trip Blank
Batch ID:R442056 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
23 Jul 2023 03:05HS23071263-01 20 Jul 2023 09:36 1FMW-15
23 Jul 2023 03:26HS23071263-02 20 Jul 2023 10:40 1FPZ-10
23 Jul 2023 03:47HS23071263-03 20 Jul 2023 10:35 1AMW-15S
23 Jul 2023 04:08HS23071263-04 20 Jul 2023 00:00 1DUP#4
23 Jul 2023 04:29HS23071263-05 20 Jul 2023 00:00 1DUP#5
28-Jul-23Date: ALS Houston, US
Page 13 of 23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071263
QC BATCH REPORT
Batch ID:198053 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-198053 Units:ug/L Analysis Date:26-Jul-2023 14:36
Run ID:ECD_13_442466 SeqNo:7454617 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-198053 Units:ug/L Analysis Date:26-Jul-2023 15:00
Run ID:ECD_13_442466 SeqNo:7454618 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.1669 0.25 0 66.8 60 - 1400.020
Sample ID:LCSD-198053 Units:ug/L Analysis Date:26-Jul-2023 15:23
Run ID:ECD_13_442466 SeqNo:7454619 PrepDate:26-Jul-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.1805 0.25 0 72.2 60 - 140 0.1669 7.84 200.020
The following samples were analyzed in this batch:HS23071263-01 HS23071263-02 HS23071263-03 HS23071263-04
HS23071263-05 HS23071263-06 HS23071263-07
ALS Houston, US Date: 28-Jul-23
Page 14 of 23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071263
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:MBLKW-230722 Units:ug/L Analysis Date:22-Jul-2023 22:32
Run ID:VOA10_442056 SeqNo:7445003 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
51.96 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.12 50 0 90.2 77 - 1131.0Surr: 4-Bromofluorobenzene
50.63 50 0 101 73 - 1261.0Surr: Dibromofluoromethane
49.14 50 0 98.3 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 28-Jul-23
Page 15 of 23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071263
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-230722 Units:ug/L Analysis Date:22-Jul-2023 21:50
Run ID:VOA10_442056 SeqNo:7445002 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.9 20 0 94.5 73 - 1211.0
1,2-Dibromoethane 17.73 20 0 88.7 76 - 1231.0
1,2-Dichloroethane 18.09 20 0 90.5 70 - 1241.0
2-Methylnaphthalene 18.56 20 0 92.8 55 - 1401.0
4-Isopropyltoluene 21.17 20 0 106 74 - 1261.0
Benzene 17.28 20 0 86.4 74 - 1201.0
Chloroform 18.34 20 0 91.7 71 - 1211.0
Ethylbenzene 17.29 20 0 86.4 77 - 1171.0
m,p-Xylene 33.79 40 0 84.5 77 - 1222.0
Methyl tert-butyl ether 17.6 20 0 88.0 70 - 1301.0
Methylene chloride 18.42 20 0 92.1 70 - 1272.0
Naphthalene 19.51 20 0 97.6 70 - 1301.0
o-Xylene 16.4 20 0 82.0 75 - 1191.0
Tert-butyl alcohol 356.9 400 0 89.2 70 - 13010
Toluene 18.3 20 0 91.5 77 - 1181.0
Xylenes, Total 50.19 60 0 83.6 75 - 1223.0
52.12 50 0 104 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.52 50 0 93.0 77 - 1131.0Surr: 4-Bromofluorobenzene
52.47 50 0 105 73 - 1261.0Surr: Dibromofluoromethane
50.46 50 0 101 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 28-Jul-23
Page 16 of 23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071263
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071175-10MS Units:ug/L Analysis Date:22-Jul-2023 23:14
Run ID:VOA10_442056 SeqNo:7445005 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 21.16 20 0 106 70 - 1251.0
1,2-Dibromoethane 19.21 20 0 96.0 70 - 1241.0
1,2-Dichloroethane 18.93 20 0 94.7 70 - 1271.0
2-Methylnaphthalene 16 20 0 80.0 55 - 1401.0
4-Isopropyltoluene 23.15 20 0 116 70 - 1301.0
Benzene 17.53 20 0 87.7 70 - 1271.0
Chloroform 19.34 20 0 96.7 70 - 1251.0
Ethylbenzene 18.64 20 0 93.2 70 - 1241.0
m,p-Xylene 37.69 40 0 94.2 70 - 1302.0
Methyl tert-butyl ether 17.58 20 0 87.9 70 - 1301.0
Methylene chloride 15.45 20 0 77.2 70 - 1282.0
Naphthalene 20.23 20 0 101 70 - 1301.0
o-Xylene 18.13 20 0 90.7 70 - 1241.0
Tert-butyl alcohol 297.9 400 0 74.5 70 - 13010
Toluene 19.9 20 0 99.5 70 - 1231.0
Xylenes, Total 55.83 60 0 93.0 70 - 1303.0
52.12 50 0 104 70 - 1261.0Surr: 1,2-Dichloroethane-d4
45.4 50 0 90.8 77 - 1131.0Surr: 4-Bromofluorobenzene
51.12 50 0 102 77 - 1231.0Surr: Dibromofluoromethane
52.07 50 0 104 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 28-Jul-23
Page 17 of 23
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23071263
QC BATCH REPORT
Batch ID:R442056 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23071175-10MSD Units:ug/L Analysis Date:22-Jul-2023 23:35
Run ID:VOA10_442056 SeqNo:7445006 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 19.11 20 0 95.5 70 - 125 21.16 10.2 201.0
1,2-Dibromoethane 16.87 20 0 84.3 70 - 124 19.21 13 201.0
1,2-Dichloroethane 17.97 20 0 89.9 70 - 127 18.93 5.19 201.0
2-Methylnaphthalene 16.56 20 0 82.8 55 - 140 16 3.38 201.0
4-Isopropyltoluene 20.88 20 0 104 70 - 130 23.15 10.3 201.0
Benzene 16.86 20 0 84.3 70 - 127 17.53 3.93 201.0
Chloroform 18.61 20 0 93.1 70 - 125 19.34 3.85 201.0
Ethylbenzene 17.07 20 0 85.4 70 - 124 18.64 8.76 201.0
m,p-Xylene 35.12 40 0 87.8 70 - 130 37.69 7.07 202.0
Methyl tert-butyl ether 16.61 20 0 83.0 70 - 130 17.58 5.67 201.0
Methylene chloride 17.61 20 0 88.0 70 - 128 15.45 13.1 202.0
Naphthalene 18.65 20 0 93.3 70 - 130 20.23 8.12 201.0
o-Xylene 15.72 20 0 78.6 70 - 124 18.13 14.3 201.0
Tert-butyl alcohol 291.6 400 0 72.9 70 - 130 297.9 2.11 2010
Toluene 17.68 20 0 88.4 70 - 123 19.9 11.8 201.0
Xylenes, Total 50.84 60 0 84.7 70 - 130 55.83 9.35 203.0
52.45 50 0 105 70 - 126 52.12 0.623 201.0Surr: 1,2-Dichloroethane-d4
47.48 50 0 95.0 77 - 113 45.4 4.49 201.0Surr: 4-Bromofluorobenzene
51.2 50 0 102 77 - 123 51.12 0.159 201.0Surr: Dibromofluoromethane
51.09 50 0 102 82 - 127 52.07 1.91 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23071263-01 HS23071263-02 HS23071263-03 HS23071263-04
HS23071263-05 HS23071263-06 HS23071263-07 HS23071263-08
ALS Houston, US Date: 28-Jul-23
Page 18 of 23
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23071263
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
ALS Houston, US Date: 28-Jul-23
Page 19 of 23
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352; 2022-2023 31-Jul-2023
Louisiana 03087-2023 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624-2023 31-Dec-2023
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2022-141 31-Aug-2023
Texas T104704231-23-31 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
28-Jul-23Date: ALS Houston, US
Page 20 of 23
Corey Grandits
21-Jul-2023 09:30Date/Time Received:HS23071263
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.4UC/3.3C IR31
Blue
7/21/23 18:00
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Nilesh D. Ranchod
Date/TimeeSignatureDate/TimeeSignature
24-Jul-2023 09:5422-Jul-2023 08:43
FedExWCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:241073
ALS Houston, US 28-Jul-23Date:
Page 21 of 23
Page 22 of 23
Page 23 of 23
Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendix F – Laboratory Analytical Reports –
Groundwater (December 2023/February 2024)

January 02, 2024
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
This is a REVISED REPORT. Please see the Case Narrative for discussion concerning this
revision.
Regards,
ALS Environmental received 12 sample(s) on Dec 07, 2023 for the analysis presented in
the following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS23120371
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 56
Client:Groundwater & Environmental Service, Inc.
Work Order:HS23120371
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS23120371-01 06-Dec-2023 15:00 07-Dec-2023 09:35AMW-11S Water
HS23120371-02 06-Dec-2023 12:40 07-Dec-2023 09:35AMW-13B Water
HS23120371-03 06-Dec-2023 10:36 07-Dec-2023 09:35AMW-14S Water
HS23120371-04 06-Dec-2023 14:40 07-Dec-2023 09:35FMW-21 Water
HS23120371-05 06-Dec-2023 12:15 07-Dec-2023 09:35FMW-24 Water
HS23120371-06 06-Dec-2023 13:40 07-Dec-2023 09:35MW-B-B Water
HS23120371-07 06-Dec-2023 00:00 07-Dec-2023 09:35Trip blank Water
HS23120371-08 06-Dec-2023 11:10 07-Dec-2023 09:35PMW-M-D Water
HS23120371-09 06-Dec-2023 13:42 07-Dec-2023 09:35Field Duplicate Water
HS23120371-10 06-Dec-2023 14:20 07-Dec-2023 09:35Equipment Blank Water
HS23120371-11 06-Dec-2023 14:10 07-Dec-2023 09:35Field Blank Water
HS23120371-12 06-Dec-2023 00:00 07-Dec-2023 09:35Trip blank Water
ALS Houston, US 02-Jan-24Date:
Revision: 1
Page 2 of 56
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23120371
Work Order Comments
This report was revised 01-02-2024 to remove RSK-175 as they were not requested on the chain of custody. •
ECD Organics by Method SW8011
Batch ID: 204538
Sample ID: MBLK-204538
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GCMS Volatiles by Method SW8260
Batch ID: R453614
Sample ID: Field Duplicate (HS23120371-09)
Lowest possible dilution due to high concentrations of target analytes.•
Sample ID: MW-B-B (HS23120371-06)
Lowest possible dilution due to high concentrations of target analytes.•
Sample ID: HS23120255-02MSD
MSD was performed on unrelated sample•
Batch ID: R453567
Sample ID: AMW-13B (HS23120371-02)
Surrogate failed QC limit for Dibromofluoromethane . Confirmed by reanalysis. Samples are ND•
Sample ID: HS23111909-02MSD
MSD was performed on unrelated sample•
Batch ID: R453608
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: R453785
Sample ID: HS23120412-01MSD
MSD was performed on unrelated sample•
Sample ID: VLCSW-231211
LCS failed outside control limits high for 1,2-Dichloroethane. Associated samples are ND.•
Metals by Method SW6020A
Batch ID: 204842
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 02-Jan-24Date:
Page 3 of 56
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS23120371
WetChemistry by Method SM2320B
Batch ID: R454606,R454677
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM3500FED
Batch ID: R454022
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method E300
Batch ID: R454413
Sample ID: AMW-13B (HS23120371-02)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Equipment Blank (HS23120371-10)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Field Blank (HS23120371-11)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: Field Duplicate (HS23120371-09)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: FMW-21 (HS23120371-04)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: FMW-24 (HS23120371-05)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Sample ID: MW-B-B (HS23120371-06)
The reporting limit is elevated due to dilution for high concentrations of non-target analytes. (Nitrate/Nitrite (as N))•
Batch ID: R454518
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Houston, US 02-Jan-24Date:
Page 4 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
SAMPLE DETECTION SUMMARY
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS MethodQUALMDL
AMW-11SHS23120371-01Lab ID:Client Sample ID:
1ug/L SW826010Tert-butyl alcohol 1036
AMW-13BHS23120371-02Lab ID:Client Sample ID:
1mg/L SW6020AJ0.0120Iron 0.2000.0340
1mg/L SW6020A0.000700Manganese 0.005000.0749
1mg/L E3000.200Sulfate 0.5001.80
1mg/L SM2320B3.50Alkalinity, Bicarbonate (As CaCO3)5.00210
1mg/L SM2320Ba3.50Alkalinity, Total (As CaCO3)5.00210
1mg/L SM3500FED0.0200Ferrous Iron 0.05000.0520
AMW-14SHS23120371-03Lab ID:Client Sample ID:
1ug/L SW82600.301,2,4-Trimethylbenzene 1.07.0
1ug/L SW82600.201,2-Dichloroethane 1.06.1
1ug/L SW82601.02-Methylnaphthalene 1.015
1ug/L SW8260J0.50m,p-Xylene 2.00.62
1ug/L SW82600.20Methyl tert-butyl ether 1.07.9
1ug/L SW82600.30Naphthalene 1.05.9
1ug/L SW8260J0.30o-Xylene 1.00.31
1ug/L SW8260J0.30Xylenes, Total 3.00.93
FMW-21HS23120371-04Lab ID:Client Sample ID:
1mg/L SW6020A0.0120Iron 0.2001.39
1mg/L SW6020A0.000700Manganese 0.005000.677
10ug/L SW82603.01,2,4-Trimethylbenzene 10270
1ug/L SW82600.201,2-Dichloroethane 1.09.8
1ug/L SW82601.02-Methylnaphthalene 1.0110
1ug/L SW82600.20Benzene 1.014
1ug/L SW82600.30Ethylbenzene 1.0100
1ug/L SW82600.50m,p-Xylene 2.0260
1ug/L SW82600.20Methyl tert-butyl ether 1.029
1ug/L SW82600.30Naphthalene 1.073
1ug/L SW82600.30o-Xylene 1.0100
1ug/L SW826010Tert-butyl alcohol 101,100
1ug/L SW82600.20Toluene 1.03.8
1ug/L SW82600.30Xylenes, Total 3.0370
1mg/L E3000.200Sulfate 0.5000.980
1mg/L SM2320B3.50Alkalinity, Bicarbonate (As CaCO3)5.00268
1mg/L SM2320Ba3.50Alkalinity, Total (As CaCO3)5.00268
10mg/L SM3500FED0.200Ferrous Iron 0.5001.42
02-Jan-24Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
1Revision:
Page 5 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
SAMPLE DETECTION SUMMARY
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS MethodQUALMDL
FMW-24HS23120371-05Lab ID:Client Sample ID:
1mg/L SW6020A0.0120Iron 0.20075.1
200mg/L SW6020A0.140Manganese 1.0033.9
20ug/L SW82606.01,2,4-Trimethylbenzene 202,200
20ug/L SW8260202-Methylnaphthalene 20370
200ug/L SW826040Benzene2006,600
20ug/L SW82606.0Ethylbenzene 201,400
20ug/L SW826010m,p-Xylene 403,900
20ug/L SW82606.0Naphthalene 20680
20ug/L SW82606.0o-Xylene 201,400
20ug/L SW82604.0Toluene 20230
20ug/L SW82606.0Xylenes, Total 605,400
1mg/L E3000.200Sulfate 0.50013.1
1mg/L SM2320B3.50Alkalinity, Bicarbonate (As CaCO3)5.00404
1mg/L SM2320Ba3.50Alkalinity, Total (As CaCO3)5.00404
100mg/L SM3500FED2.00Ferrous Iron 5.0033.4
MW-B-BHS23120371-06Lab ID:Client Sample ID:
1mg/L SW6020AJ0.0120Iron 0.2000.0160
1mg/L SW6020AJ0.000700Manganese 0.005000.00463
50ug/L SW8260500Tert-butyl alcohol 500150,000
1mg/L E3000.200Sulfate 0.5003.08
1mg/L SM2320B3.50Alkalinity, Bicarbonate (As CaCO3)5.0040.8
1mg/L SM2320B3.50Alkalinity, Carbonate (As CaCO3)5.0023.2
1mg/L SM2320Ba3.50Alkalinity, Total (As CaCO3)5.0064.0
1mg/L SM3500FEDJ0.0200Ferrous Iron 0.05000.0210
PMW-M-DHS23120371-08Lab ID:Client Sample ID:
1ug/L SW82600.201,2-Dichloroethane 1.090
1ug/L SW82600.20Benzene 1.03.5
1ug/L SW82600.20Methyl tert-butyl ether 1.047
5ug/L SW826050Tert-butyl alcohol 506,900
1ug/L SW8260J0.20Toluene 1.00.45
Field DuplicateHS23120371-09Lab ID:Client Sample ID:
1mg/L SW6020AJ0.0120Iron 0.2000.0127
1mg/L SW6020AJ0.000700Manganese 0.005000.00381
50ug/L SW8260500Tert-butyl alcohol 500140,000
1mg/L E3000.200Sulfate 0.5003.06
1mg/L SM2320B3.50Alkalinity, Bicarbonate (As CaCO3)5.0041.3
1mg/L SM2320B3.50Alkalinity, Carbonate (As CaCO3)5.0024.4
1mg/L SM2320Ba3.50Alkalinity, Total (As CaCO3)5.0065.7
02-Jan-24Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
1Revision:
Page 6 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
SAMPLE DETECTION SUMMARY
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS MethodQUALMDL
Equipment BlankHS23120371-10Lab ID:Client Sample ID:
1mg/L SW6020AJ0.000700Manganese 0.005000.00130
02-Jan-24Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
1Revision:
Page 7 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-11S
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-01
06-Dec-2023 15:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
1ug/L 11-Dec-2023 18:370.301,2,4-Trimethylbenzene 1.0U
1ug/L 11-Dec-2023 18:370.201,2-Dibromoethane 1.0U
1ug/L 11-Dec-2023 18:370.201,2-Dichloroethane 1.0U
1ug/L 11-Dec-2023 18:371.02-Methylnaphthalene 1.0U
1ug/L 11-Dec-2023 18:370.304-Isopropyltoluene 1.0U
1ug/L 11-Dec-2023 18:370.20Benzene 1.0U
1ug/L 11-Dec-2023 18:370.20Chloroform 1.0U
1ug/L 11-Dec-2023 18:370.30Ethylbenzene 1.0U
1ug/L 11-Dec-2023 18:370.50m,p-Xylene 2.0U
1ug/L 11-Dec-2023 18:370.20Methyl tert-butyl ether 1.0U
1ug/L 11-Dec-2023 18:371.0Methylene chloride 2.0U
1ug/L 11-Dec-2023 18:370.30Naphthalene 1.0U
1ug/L 11-Dec-2023 18:370.30o-Xylene 1.0U
1ug/L 11-Dec-2023 18:3710Tert-butyl alcohol 1036
1ug/L 11-Dec-2023 18:370.20Toluene 1.0U
1ug/L 11-Dec-2023 18:370.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 11-Dec-2023 18:3711270-126
Surr: 4-Bromofluorobenzene 1%REC 11-Dec-2023 18:3798.0 77-113
Surr: Dibromofluoromethane 1%REC 11-Dec-2023 18:3710477-123
Surr: Toluene-d8 1%REC 11-Dec-2023 18:3710782-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 15:570.00321,2-Dibromoethane 0.021U
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-13B
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-02
06-Dec-2023 12:40 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
1ug/L 07-Dec-2023 20:150.301,2,4-Trimethylbenzene 1.0U
1ug/L 07-Dec-2023 20:150.201,2-Dibromoethane 1.0U
1ug/L 07-Dec-2023 20:150.201,2-Dichloroethane 1.0U
1ug/L 08-Dec-2023 14:111.02-Methylnaphthalene 1.0U
1ug/L 07-Dec-2023 20:150.304-Isopropyltoluene 1.0U
1ug/L 07-Dec-2023 20:150.20Benzene 1.0U
1ug/L 07-Dec-2023 20:150.20Chloroform 1.0U
1ug/L 07-Dec-2023 20:150.30Ethylbenzene 1.0U
1ug/L 07-Dec-2023 20:150.50m,p-Xylene 2.0U
1ug/L 07-Dec-2023 20:150.20Methyl tert-butyl ether 1.0U
1ug/L 07-Dec-2023 20:151.0Methylene chloride 2.0U
1ug/L 07-Dec-2023 20:150.30Naphthalene 1.0U
1ug/L 07-Dec-2023 20:150.30o-Xylene 1.0U
1ug/L 07-Dec-2023 20:1510Tert-butyl alcohol 10U
1ug/L 07-Dec-2023 20:150.20Toluene 1.0U
1ug/L 07-Dec-2023 20:150.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 07-Dec-2023 20:1510870-126
Surr: 1,2-Dichloroethane-d4 1%REC 08-Dec-2023 14:1111670-126
Surr: 4-Bromofluorobenzene 1%REC 07-Dec-2023 20:1599.7 77-113
Surr: 4-Bromofluorobenzene 1%REC 08-Dec-2023 14:1110577-113
Surr: Dibromofluoromethane 1%REC 07-Dec-2023 20:1510777-123
Surr: Dibromofluoromethane 1%REC 08-Dec-2023 14:11S12377-123
Surr: Toluene-d8 1%REC 07-Dec-2023 20:1510382-127
Surr: Toluene-d8 1%REC 08-Dec-2023 14:1193.1 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 16:200.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 14-Dec-2023
1mg/L 18-Dec-2023 16:22J0.0120Iron 0.2000.0340
1mg/L 18-Dec-2023 16:220.000700Manganese 0.005000.0749
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 18-Dec-2023 10:430.200Sulfate 0.5001.80
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 17-Dec-2023 22:300.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY -2011 Method:SM2320B Analyst: DW
1mg/L 19-Dec-2023 14:393.50Alkalinity, Bicarbonate (As
CaCO3)5.00210
1mg/L 19-Dec-2023 14:393.50Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 19-Dec-2023 14:393.50Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 19-Dec-2023 14:39a3.50Alkalinity, Total (As CaCO3)5.00210
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-13B
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-02
06-Dec-2023 12:40 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: JAC
1mg/L 08-Dec-2023 10:290.0200Ferrous Iron 0.05000.0520
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
AMW-14S
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-03
06-Dec-2023 10:36 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
1ug/L 08-Dec-2023 02:320.301,2,4-Trimethylbenzene 1.07.0
1ug/L 08-Dec-2023 02:320.201,2-Dibromoethane 1.0U
1ug/L 08-Dec-2023 02:320.201,2-Dichloroethane 1.06.1
1ug/L 08-Dec-2023 02:321.02-Methylnaphthalene 1.015
1ug/L 08-Dec-2023 02:320.304-Isopropyltoluene 1.0U
1ug/L 08-Dec-2023 02:320.20Benzene 1.0U
1ug/L 08-Dec-2023 02:320.20Chloroform 1.0U
1ug/L 08-Dec-2023 02:320.30Ethylbenzene 1.0U
1ug/L 08-Dec-2023 02:32J0.50m,p-Xylene 2.00.62
1ug/L 08-Dec-2023 02:320.20Methyl tert-butyl ether 1.07.9
1ug/L 08-Dec-2023 02:321.0Methylene chloride 2.0U
1ug/L 08-Dec-2023 02:320.30Naphthalene 1.05.9
1ug/L 08-Dec-2023 02:32J0.30o-Xylene 1.00.31
1ug/L 08-Dec-2023 02:3210Tert-butyl alcohol 10U
1ug/L 08-Dec-2023 02:320.20Toluene 1.0U
1ug/L 08-Dec-2023 02:32J0.30Xylenes, Total 3.00.93
Surr: 1,2-Dichloroethane-d4 1%REC 08-Dec-2023 02:3210970-126
Surr: 4-Bromofluorobenzene 1%REC 08-Dec-2023 02:3297.6 77-113
Surr: Dibromofluoromethane 1%REC 08-Dec-2023 02:3210577-123
Surr: Toluene-d8 1%REC 08-Dec-2023 02:32100.0 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 16:430.00321,2-Dibromoethane 0.021U
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-21
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-04
06-Dec-2023 14:40 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
10ug/L 08-Dec-2023 16:373.01,2,4-Trimethylbenzene 10270
1ug/L 08-Dec-2023 02:530.201,2-Dibromoethane 1.0U
1ug/L 08-Dec-2023 02:530.201,2-Dichloroethane 1.09.8
1ug/L 08-Dec-2023 02:531.02-Methylnaphthalene 1.0110
1ug/L 08-Dec-2023 02:530.304-Isopropyltoluene 1.0U
1ug/L 08-Dec-2023 02:530.20Benzene 1.014
1ug/L 08-Dec-2023 02:530.20Chloroform 1.0U
1ug/L 08-Dec-2023 02:530.30Ethylbenzene 1.0100
1ug/L 08-Dec-2023 02:530.50m,p-Xylene 2.0260
1ug/L 08-Dec-2023 02:530.20Methyl tert-butyl ether 1.029
1ug/L 08-Dec-2023 02:531.0Methylene chloride 2.0U
1ug/L 08-Dec-2023 02:530.30Naphthalene 1.073
1ug/L 08-Dec-2023 02:530.30o-Xylene 1.0100
1ug/L 08-Dec-2023 02:5310Tert-butyl alcohol 101,100
1ug/L 08-Dec-2023 02:530.20Toluene 1.03.8
1ug/L 08-Dec-2023 02:530.30Xylenes, Total 3.0370
Surr: 1,2-Dichloroethane-d4 1%REC 08-Dec-2023 02:5310570-126
Surr: 1,2-Dichloroethane-d4 10%REC 08-Dec-2023 16:3711070-126
Surr: 4-Bromofluorobenzene 1%REC 08-Dec-2023 02:5310077-113
Surr: 4-Bromofluorobenzene 10%REC 08-Dec-2023 16:3710477-113
Surr: Dibromofluoromethane 1%REC 08-Dec-2023 02:5398.3 77-123
Surr: Dibromofluoromethane 10%REC 08-Dec-2023 16:3710877-123
Surr: Toluene-d8 1%REC 08-Dec-2023 02:5310082-127
Surr: Toluene-d8 10%REC 08-Dec-2023 16:3796.0 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 17:060.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 14-Dec-2023
1mg/L 18-Dec-2023 16:240.0120Iron 0.2001.39
1mg/L 18-Dec-2023 16:240.000700Manganese 0.005000.677
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 18-Dec-2023 11:000.200Sulfate 0.5000.980
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 17-Dec-2023 22:470.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY -2011 Method:SM2320B Analyst: DW
1mg/L 19-Dec-2023 14:453.50Alkalinity, Bicarbonate (As
CaCO3)5.00268
1mg/L 19-Dec-2023 14:453.50Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 19-Dec-2023 14:453.50Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 19-Dec-2023 14:45a3.50Alkalinity, Total (As CaCO3)5.00268
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-21
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-04
06-Dec-2023 14:40 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: JAC
10mg/L 08-Dec-2023 10:290.200Ferrous Iron 0.5001.42
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-24
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-05
06-Dec-2023 12:15 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
20ug/L 08-Dec-2023 06:236.01,2,4-Trimethylbenzene 202,200
20ug/L 08-Dec-2023 06:234.01,2-Dibromoethane 20U
20ug/L 08-Dec-2023 06:234.01,2-Dichloroethane 20U
20ug/L 08-Dec-2023 06:23202-Methylnaphthalene 20370
20ug/L 08-Dec-2023 06:236.04-Isopropyltoluene 20U
200ug/L 08-Dec-2023 15:5540Benzene2006,600
20ug/L 08-Dec-2023 06:234.0Chloroform 20U
20ug/L 08-Dec-2023 06:236.0Ethylbenzene 201,400
20ug/L 08-Dec-2023 06:2310m,p-Xylene 403,900
20ug/L 08-Dec-2023 06:234.0Methyl tert-butyl ether 20U
20ug/L 08-Dec-2023 06:2320Methylene chloride 40U
20ug/L 08-Dec-2023 06:236.0Naphthalene 20680
20ug/L 08-Dec-2023 06:236.0o-Xylene 201,400
20ug/L 08-Dec-2023 06:23200Tert-butyl alcohol 200U
20ug/L 08-Dec-2023 06:234.0Toluene 20230
20ug/L 08-Dec-2023 06:236.0Xylenes, Total 605,400
Surr: 1,2-Dichloroethane-d4 20%REC 08-Dec-2023 06:2310270-126
Surr: 1,2-Dichloroethane-d4 200%REC 08-Dec-2023 15:5510770-126
Surr: 4-Bromofluorobenzene 20%REC 08-Dec-2023 06:2397.5 77-113
Surr: 4-Bromofluorobenzene 200%REC 08-Dec-2023 15:5510377-113
Surr: Dibromofluoromethane 20%REC 08-Dec-2023 06:2399.5 77-123
Surr: Dibromofluoromethane 200%REC 08-Dec-2023 15:5510977-123
Surr: Toluene-d8 20%REC 08-Dec-2023 06:2310182-127
Surr: Toluene-d8 200%REC 08-Dec-2023 15:5596.6 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 17:290.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 14-Dec-2023
1mg/L 18-Dec-2023 16:260.0120Iron 0.20075.1
200mg/L 19-Dec-2023 12:130.140Manganese 1.0033.9
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 18-Dec-2023 11:060.200Sulfate 0.50013.1
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 17-Dec-2023 22:530.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY -2011 Method:SM2320B Analyst: DW
1mg/L 19-Dec-2023 14:513.50Alkalinity, Bicarbonate (As
CaCO3)5.00404
1mg/L 19-Dec-2023 14:513.50Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 19-Dec-2023 14:513.50Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 19-Dec-2023 14:51a3.50Alkalinity, Total (As CaCO3)5.00404
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
FMW-24
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-05
06-Dec-2023 12:15 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: JAC
100mg/L 08-Dec-2023 10:292.00Ferrous Iron 5.0033.4
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
MW-B-B
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-06
06-Dec-2023 13:40 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
50ug/L 08-Dec-2023 15:14151,2,4-Trimethylbenzene 50U
50ug/L 08-Dec-2023 15:14101,2-Dibromoethane 50U
50ug/L 08-Dec-2023 15:14101,2-Dichloroethane 50U
50ug/L 08-Dec-2023 15:14502-Methylnaphthalene 50U
50ug/L 08-Dec-2023 15:14154-Isopropyltoluene 50U
50ug/L 08-Dec-2023 15:1410Benzene50U
50ug/L 08-Dec-2023 15:1410Chloroform50U
50ug/L 08-Dec-2023 15:1415Ethylbenzene50U
50ug/L 08-Dec-2023 15:1425m,p-Xylene 100U
50ug/L 08-Dec-2023 15:1410Methyl tert-butyl ether 50U
50ug/L 08-Dec-2023 15:1450Methylene chloride 100U
50ug/L 08-Dec-2023 15:1415Naphthalene50U
50ug/L 08-Dec-2023 15:1415o-Xylene 50U
50ug/L 08-Dec-2023 15:14500Tert-butyl alcohol 500150,000
50ug/L 08-Dec-2023 15:1410Toluene50U
50ug/L 08-Dec-2023 15:1415Xylenes, Total 150U
Surr: 1,2-Dichloroethane-d4 50%REC 08-Dec-2023 15:1410670-126
Surr: 4-Bromofluorobenzene 50%REC 08-Dec-2023 15:1410377-113
Surr: Dibromofluoromethane 50%REC 08-Dec-2023 15:1411077-123
Surr: Toluene-d8 50%REC 08-Dec-2023 15:1494.6 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 17:520.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 14-Dec-2023
1mg/L 18-Dec-2023 16:29J0.0120Iron 0.2000.0160
1mg/L 18-Dec-2023 16:29J0.000700Manganese 0.005000.00463
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 18-Dec-2023 11:120.200Sulfate 0.5003.08
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 17-Dec-2023 22:590.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY -2011 Method:SM2320B Analyst: DW
1mg/L 19-Dec-2023 15:253.50Alkalinity, Bicarbonate (As
CaCO3)5.0040.8
1mg/L 19-Dec-2023 15:253.50Alkalinity, Carbonate (As CaCO3)5.0023.2
1mg/L 19-Dec-2023 15:253.50Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 19-Dec-2023 15:25a3.50Alkalinity, Total (As CaCO3)5.0064.0
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: JAC
1mg/L 08-Dec-2023 10:29J0.0200Ferrous Iron 0.05000.0210
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 16 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip blank
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-07
06-Dec-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
1ug/L 07-Dec-2023 23:440.301,2,4-Trimethylbenzene 1.0U
1ug/L 07-Dec-2023 23:440.201,2-Dibromoethane 1.0U
1ug/L 07-Dec-2023 23:440.201,2-Dichloroethane 1.0U
1ug/L 07-Dec-2023 23:441.02-Methylnaphthalene 1.0U
1ug/L 07-Dec-2023 23:440.304-Isopropyltoluene 1.0U
1ug/L 07-Dec-2023 23:440.20Benzene 1.0U
1ug/L 07-Dec-2023 23:440.20Chloroform 1.0U
1ug/L 07-Dec-2023 23:440.30Ethylbenzene 1.0U
1ug/L 07-Dec-2023 23:440.50m,p-Xylene 2.0U
1ug/L 07-Dec-2023 23:440.20Methyl tert-butyl ether 1.0U
1ug/L 07-Dec-2023 23:441.0Methylene chloride 2.0U
1ug/L 07-Dec-2023 23:440.30Naphthalene 1.0U
1ug/L 07-Dec-2023 23:440.30o-Xylene 1.0U
1ug/L 07-Dec-2023 23:4410Tert-butyl alcohol 10U
1ug/L 07-Dec-2023 23:440.20Toluene 1.0U
1ug/L 07-Dec-2023 23:440.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 07-Dec-2023 23:4410770-126
Surr: 4-Bromofluorobenzene 1%REC 07-Dec-2023 23:4498.2 77-113
Surr: Dibromofluoromethane 1%REC 07-Dec-2023 23:4410577-123
Surr: Toluene-d8 1%REC 07-Dec-2023 23:4497.9 82-127
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 17 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
PMW-M-D
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-08
06-Dec-2023 11:10 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
1ug/L 08-Dec-2023 14:320.301,2,4-Trimethylbenzene 1.0U
1ug/L 08-Dec-2023 14:320.201,2-Dibromoethane 1.0U
1ug/L 08-Dec-2023 14:320.201,2-Dichloroethane 1.090
1ug/L 08-Dec-2023 14:321.02-Methylnaphthalene 1.0U
1ug/L 08-Dec-2023 14:320.304-Isopropyltoluene 1.0U
1ug/L 08-Dec-2023 14:320.20Benzene 1.03.5
1ug/L 08-Dec-2023 14:320.20Chloroform 1.0U
1ug/L 08-Dec-2023 14:320.30Ethylbenzene 1.0U
1ug/L 08-Dec-2023 14:320.50m,p-Xylene 2.0U
1ug/L 08-Dec-2023 14:320.20Methyl tert-butyl ether 1.047
1ug/L 08-Dec-2023 14:321.0Methylene chloride 2.0U
1ug/L 08-Dec-2023 14:320.30Naphthalene 1.0U
1ug/L 08-Dec-2023 14:320.30o-Xylene 1.0U
5ug/L 08-Dec-2023 07:0550Tert-butyl alcohol 506,900
1ug/L 08-Dec-2023 14:32J0.20Toluene 1.00.45
1ug/L 08-Dec-2023 14:320.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 5%REC 08-Dec-2023 07:0511170-126
Surr: 1,2-Dichloroethane-d4 1%REC 08-Dec-2023 14:3210970-126
Surr: 4-Bromofluorobenzene 5%REC 08-Dec-2023 07:0597.7 77-113
Surr: 4-Bromofluorobenzene 1%REC 08-Dec-2023 14:3210277-113
Surr: Dibromofluoromethane 5%REC 08-Dec-2023 07:0510477-123
Surr: Dibromofluoromethane 1%REC 08-Dec-2023 14:3211377-123
Surr: Toluene-d8 5%REC 08-Dec-2023 07:0598.8 82-127
Surr: Toluene-d8 1%REC 08-Dec-2023 14:3292.7 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 18:150.00321,2-Dibromoethane 0.021U
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 18 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Field Duplicate
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-09
06-Dec-2023 13:42 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
50ug/L 08-Dec-2023 15:34151,2,4-Trimethylbenzene 50U
50ug/L 08-Dec-2023 15:34101,2-Dibromoethane 50U
50ug/L 08-Dec-2023 15:34101,2-Dichloroethane 50U
50ug/L 08-Dec-2023 15:34502-Methylnaphthalene 50U
50ug/L 08-Dec-2023 15:34154-Isopropyltoluene 50U
50ug/L 08-Dec-2023 15:3410Benzene50U
50ug/L 08-Dec-2023 15:3410Chloroform50U
50ug/L 08-Dec-2023 15:3415Ethylbenzene50U
50ug/L 08-Dec-2023 15:3425m,p-Xylene 100U
50ug/L 08-Dec-2023 15:3410Methyl tert-butyl ether 50U
50ug/L 08-Dec-2023 15:3450Methylene chloride 100U
50ug/L 08-Dec-2023 15:3415Naphthalene50U
50ug/L 08-Dec-2023 15:3415o-Xylene 50U
50ug/L 08-Dec-2023 15:34500Tert-butyl alcohol 500140,000
50ug/L 08-Dec-2023 15:3410Toluene50U
50ug/L 08-Dec-2023 15:3415Xylenes, Total 150U
Surr: 1,2-Dichloroethane-d4 50%REC 08-Dec-2023 15:3411170-126
Surr: 4-Bromofluorobenzene 50%REC 08-Dec-2023 15:3410377-113
Surr: Dibromofluoromethane 50%REC 08-Dec-2023 15:3411177-123
Surr: Toluene-d8 50%REC 08-Dec-2023 15:3495.0 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 18:380.00321,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 14-Dec-2023
1mg/L 18-Dec-2023 16:31J0.0120Iron 0.2000.0127
1mg/L 18-Dec-2023 16:31J0.000700Manganese 0.005000.00381
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 18-Dec-2023 11:180.200Sulfate 0.5003.06
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 17-Dec-2023 23:050.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY -2011 Method:SM2320B Analyst: DW
1mg/L 19-Dec-2023 15:373.50Alkalinity, Bicarbonate (As
CaCO3)5.0041.3
1mg/L 19-Dec-2023 15:373.50Alkalinity, Carbonate (As CaCO3)5.0024.4
1mg/L 19-Dec-2023 15:373.50Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 19-Dec-2023 15:37a3.50Alkalinity, Total (As CaCO3)5.0065.7
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: JAC
1mg/L 08-Dec-2023 10:290.0200Ferrous Iron 0.0500U
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 19 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Equipment Blank
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-10
06-Dec-2023 14:20 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
1ug/L 08-Dec-2023 00:050.301,2,4-Trimethylbenzene 1.0U
1ug/L 08-Dec-2023 00:050.201,2-Dibromoethane 1.0U
1ug/L 08-Dec-2023 00:050.201,2-Dichloroethane 1.0U
1ug/L 08-Dec-2023 00:051.02-Methylnaphthalene 1.0U
1ug/L 08-Dec-2023 00:050.304-Isopropyltoluene 1.0U
1ug/L 08-Dec-2023 00:050.20Benzene 1.0U
1ug/L 08-Dec-2023 00:050.20Chloroform 1.0U
1ug/L 08-Dec-2023 00:050.30Ethylbenzene 1.0U
1ug/L 08-Dec-2023 00:050.50m,p-Xylene 2.0U
1ug/L 08-Dec-2023 00:050.20Methyl tert-butyl ether 1.0U
1ug/L 08-Dec-2023 00:051.0Methylene chloride 2.0U
1ug/L 08-Dec-2023 00:050.30Naphthalene 1.0U
1ug/L 08-Dec-2023 00:050.30o-Xylene 1.0U
1ug/L 08-Dec-2023 00:0510Tert-butyl alcohol 10U
1ug/L 08-Dec-2023 00:050.20Toluene 1.0U
1ug/L 08-Dec-2023 00:050.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 08-Dec-2023 00:0510870-126
Surr: 4-Bromofluorobenzene 1%REC 08-Dec-2023 00:0599.5 77-113
Surr: Dibromofluoromethane 1%REC 08-Dec-2023 00:0510577-123
Surr: Toluene-d8 1%REC 08-Dec-2023 00:0599.4 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 19:020.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 14-Dec-2023
1mg/L 18-Dec-2023 16:330.0120Iron 0.200U
1mg/L 18-Dec-2023 16:33J0.000700Manganese 0.005000.00130
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 18-Dec-2023 11:240.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 17-Dec-2023 23:110.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY -2011 Method:SM2320B Analyst: DW
1mg/L 19-Dec-2023 15:413.50Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 19-Dec-2023 15:413.50Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 19-Dec-2023 15:413.50Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 19-Dec-2023 15:41a3.50Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: JAC
1mg/L 08-Dec-2023 10:290.0200Ferrous Iron 0.0500U
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 20 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Field Blank
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-11
06-Dec-2023 14:10 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
1ug/L 08-Dec-2023 00:260.301,2,4-Trimethylbenzene 1.0U
1ug/L 08-Dec-2023 00:260.201,2-Dibromoethane 1.0U
1ug/L 08-Dec-2023 00:260.201,2-Dichloroethane 1.0U
1ug/L 08-Dec-2023 00:261.02-Methylnaphthalene 1.0U
1ug/L 08-Dec-2023 00:260.304-Isopropyltoluene 1.0U
1ug/L 08-Dec-2023 00:260.20Benzene 1.0U
1ug/L 08-Dec-2023 00:260.20Chloroform 1.0U
1ug/L 08-Dec-2023 00:260.30Ethylbenzene 1.0U
1ug/L 08-Dec-2023 00:260.50m,p-Xylene 2.0U
1ug/L 08-Dec-2023 00:260.20Methyl tert-butyl ether 1.0U
1ug/L 08-Dec-2023 00:261.0Methylene chloride 2.0U
1ug/L 08-Dec-2023 00:260.30Naphthalene 1.0U
1ug/L 08-Dec-2023 00:260.30o-Xylene 1.0U
1ug/L 08-Dec-2023 00:2610Tert-butyl alcohol 10U
1ug/L 08-Dec-2023 00:260.20Toluene 1.0U
1ug/L 08-Dec-2023 00:260.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 08-Dec-2023 00:2610570-126
Surr: 4-Bromofluorobenzene 1%REC 08-Dec-2023 00:2610077-113
Surr: Dibromofluoromethane 1%REC 08-Dec-2023 00:2610577-123
Surr: Toluene-d8 1%REC 08-Dec-2023 00:2699.5 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 08-Dec-2023
1ug/L 08-Dec-2023 19:250.00311,2-Dibromoethane 0.021U
ICP-MS METALS BY SW6020A Method:SW6020A Analyst: JCPrep:SW3010A / 14-Dec-2023
1mg/L 18-Dec-2023 16:360.0120Iron 0.200U
1mg/L 18-Dec-2023 16:360.000700Manganese 0.00500U
ANIONS BY E300.0, REV 2.1, 1993 Method:E300 Analyst: TH
1mg/L 18-Dec-2023 11:590.200Sulfate 0.500U
NITRATE/NITRITE BY E300.0, REV 2.1,
1993 Method:E300 Analyst: TH
10mg/L 17-Dec-2023 23:520.300Nitrate/Nitrite (as N)2.00U
ALKALINITY BY -2011 Method:SM2320B Analyst: DW
1mg/L 19-Dec-2023 15:453.50Alkalinity, Bicarbonate (As CaCO3)5.00U
1mg/L 19-Dec-2023 15:453.50Alkalinity, Carbonate (As CaCO3)5.00U
1mg/L 19-Dec-2023 15:453.50Alkalinity, Hydroxide (As CaCO3)5.00U
1mg/L 19-Dec-2023 15:45a3.50Alkalinity, Total (As CaCO3)5.00U
FERROUS IRON BY SM3500 FE B Method:SM3500FED Analyst: JAC
1mg/L 08-Dec-2023 10:290.0200Ferrous Iron 0.0500U
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 21 of 56
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip blank
WorkOrder:
Lab ID:
Collection Date:
HS23120371
HS23120371-12
06-Dec-2023 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: TS
1ug/L 08-Dec-2023 00:470.301,2,4-Trimethylbenzene 1.0U
1ug/L 08-Dec-2023 00:470.201,2-Dibromoethane 1.0U
1ug/L 08-Dec-2023 00:470.201,2-Dichloroethane 1.0U
1ug/L 08-Dec-2023 00:471.02-Methylnaphthalene 1.0U
1ug/L 08-Dec-2023 00:470.304-Isopropyltoluene 1.0U
1ug/L 08-Dec-2023 00:470.20Benzene 1.0U
1ug/L 08-Dec-2023 00:470.20Chloroform 1.0U
1ug/L 08-Dec-2023 00:470.30Ethylbenzene 1.0U
1ug/L 08-Dec-2023 00:470.50m,p-Xylene 2.0U
1ug/L 08-Dec-2023 00:470.20Methyl tert-butyl ether 1.0U
1ug/L 08-Dec-2023 00:471.0Methylene chloride 2.0U
1ug/L 08-Dec-2023 00:470.30Naphthalene 1.0U
1ug/L 08-Dec-2023 00:470.30o-Xylene 1.0U
1ug/L 08-Dec-2023 00:4710Tert-butyl alcohol 10U
1ug/L 08-Dec-2023 00:470.20Toluene 1.0U
1ug/L 08-Dec-2023 00:470.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 08-Dec-2023 00:4710970-126
Surr: 4-Bromofluorobenzene 1%REC 08-Dec-2023 00:4798.9 77-113
Surr: Dibromofluoromethane 1%REC 08-Dec-2023 00:4710877-123
Surr: Toluene-d8 1%REC 08-Dec-2023 00:4799.5 82-127
02-Jan-24Date: ALS Houston, US
1Revision: Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 22 of 56
Weight / Prep Log
HS23120371
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:204538
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 08 Dec 2023 10:54 End Date: 08 Dec 2023 10:54
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23120371-01 35 (mL)40 mL VOA w/ HCL37.12 (mL)1.061
HS23120371-02 35 (mL)40 mL VOA w/ HCL37.14 (mL)1.061
HS23120371-03 35 (mL)40 mL VOA w/ HCL37.07 (mL)1.059
HS23120371-04 35 (mL)40 mL VOA w/ HCL36.51 (mL)1.043
HS23120371-05 35 (mL)40 mL VOA w/ HCL36.97 (mL)1.056
HS23120371-06 35 (mL)40 mL VOA w/ HCL37.08 (mL)1.059
HS23120371-08 35 (mL)40 mL VOA w/ HCL36.75 (mL)1.05
HS23120371-09 35 (mL)40 mL VOA w/ HCL37.13 (mL)1.061
HS23120371-10 35 (mL)40 mL VOA w/ HCL36.29 (mL)1.037
HS23120371-11 35 (mL)40 mL VOA w/ HCL36.53 (mL)1.044
Batch ID:204842
Method:WATER - SW3010A 3010APrep Code:
Start Date: 14 Dec 2023 10:30 End Date: 14 Dec 2023 10:30
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS23120371-02 10 (mL)120 plastic HNO310 (mL)1
HS23120371-04 10 (mL)120 plastic HNO310 (mL)1
HS23120371-05 10 (mL)120 plastic HNO310 (mL)1
HS23120371-06 10 (mL)120 plastic HNO310 (mL)1
HS23120371-09 10 (mL)120 plastic HNO310 (mL)1
HS23120371-10 10 (mL)120 plastic HNO310 (mL)1
HS23120371-11 10 (mL)120 plastic HNO310 (mL)1
02-Jan-24Date: ALS Houston, US
1Revision:
Page 23 of 56
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23120371
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:204538 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Water
08 Dec 2023 10:54 08 Dec 2023 15:57HS23120371-01 06 Dec 2023 15:00 1AMW-11S
08 Dec 2023 10:54 08 Dec 2023 16:20HS23120371-02 06 Dec 2023 12:40 1AMW-13B
08 Dec 2023 10:54 08 Dec 2023 16:43HS23120371-03 06 Dec 2023 10:36 1AMW-14S
08 Dec 2023 10:54 08 Dec 2023 17:06HS23120371-04 06 Dec 2023 14:40 1FMW-21
08 Dec 2023 10:54 08 Dec 2023 17:29HS23120371-05 06 Dec 2023 12:15 1FMW-24
08 Dec 2023 10:54 08 Dec 2023 17:52HS23120371-06 06 Dec 2023 13:40 1MW-B-B
08 Dec 2023 10:54 08 Dec 2023 18:15HS23120371-08 06 Dec 2023 11:10 1PMW-M-D
08 Dec 2023 10:54 08 Dec 2023 18:38HS23120371-09 06 Dec 2023 13:42 1Field Duplicate
08 Dec 2023 10:54 08 Dec 2023 19:02HS23120371-10 06 Dec 2023 14:20 1Equipment Blank
08 Dec 2023 10:54 08 Dec 2023 19:25HS23120371-11 06 Dec 2023 14:10 1Field Blank
Batch ID:204842 ( 0 ) Test Name :ICP-MS METALS BY SW6020A Matrix:Water
14 Dec 2023 10:30 18 Dec 2023 16:22HS23120371-02 06 Dec 2023 12:40 1AMW-13B
14 Dec 2023 10:30 18 Dec 2023 16:24HS23120371-04 06 Dec 2023 14:40 1FMW-21
14 Dec 2023 10:30 19 Dec 2023 12:13HS23120371-05 06 Dec 2023 12:15 200FMW-24
14 Dec 2023 10:30 18 Dec 2023 16:26HS23120371-05 06 Dec 2023 12:15 1FMW-24
14 Dec 2023 10:30 18 Dec 2023 16:29HS23120371-06 06 Dec 2023 13:40 1MW-B-B
14 Dec 2023 10:30 18 Dec 2023 16:31HS23120371-09 06 Dec 2023 13:42 1Field Duplicate
14 Dec 2023 10:30 18 Dec 2023 16:33HS23120371-10 06 Dec 2023 14:20 1Equipment Blank
14 Dec 2023 10:30 18 Dec 2023 16:36HS23120371-11 06 Dec 2023 14:10 1Field Blank
Batch ID:R453567 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
07 Dec 2023 20:15HS23120371-02 06 Dec 2023 12:40 1AMW-13B
Batch ID:R453608 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
08 Dec 2023 02:32HS23120371-03 06 Dec 2023 10:36 1AMW-14S
08 Dec 2023 02:53HS23120371-04 06 Dec 2023 14:40 1FMW-21
08 Dec 2023 06:23HS23120371-05 06 Dec 2023 12:15 20FMW-24
07 Dec 2023 23:44HS23120371-07 06 Dec 2023 00:00 1Trip blank
08 Dec 2023 07:05HS23120371-08 06 Dec 2023 11:10 5PMW-M-D
08 Dec 2023 00:05HS23120371-10 06 Dec 2023 14:20 1Equipment Blank
08 Dec 2023 00:26HS23120371-11 06 Dec 2023 14:10 1Field Blank
08 Dec 2023 00:47HS23120371-12 06 Dec 2023 00:00 1Trip blank
Batch ID:R453614 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
08 Dec 2023 14:11HS23120371-02 06 Dec 2023 12:40 1AMW-13B
08 Dec 2023 16:37HS23120371-04 06 Dec 2023 14:40 10FMW-21
08 Dec 2023 15:55HS23120371-05 06 Dec 2023 12:15 200FMW-24
08 Dec 2023 15:14HS23120371-06 06 Dec 2023 13:40 50MW-B-B
08 Dec 2023 14:32HS23120371-08 06 Dec 2023 11:10 1PMW-M-D
08 Dec 2023 15:34HS23120371-09 06 Dec 2023 13:42 50Field Duplicate
02-Jan-24Date: ALS Houston, US
Revision: 1
Page 24 of 56
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS23120371
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:R453785 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
11 Dec 2023 18:37HS23120371-01 06 Dec 2023 15:00 1AMW-11S
Batch ID:R454022 ( 0 ) Test Name :FERROUS IRON BY SM3500 FE B Matrix:Water
08 Dec 2023 10:29HS23120371-02 06 Dec 2023 12:40 1AMW-13B
08 Dec 2023 10:29HS23120371-04 06 Dec 2023 14:40 10FMW-21
08 Dec 2023 10:29HS23120371-05 06 Dec 2023 12:15 100FMW-24
08 Dec 2023 10:29HS23120371-06 06 Dec 2023 13:40 1MW-B-B
08 Dec 2023 10:29HS23120371-09 06 Dec 2023 13:42 1Field Duplicate
08 Dec 2023 10:29HS23120371-10 06 Dec 2023 14:20 1Equipment Blank
08 Dec 2023 10:29HS23120371-11 06 Dec 2023 14:10 1Field Blank
Batch ID:R454413 ( 0 ) Test Name :NITRATE/NITRITE BY E300.0, REV 2.1, 1993 Matrix:Water
17 Dec 2023 22:30HS23120371-02 06 Dec 2023 12:40 10AMW-13B
17 Dec 2023 22:47HS23120371-04 06 Dec 2023 14:40 10FMW-21
17 Dec 2023 22:53HS23120371-05 06 Dec 2023 12:15 10FMW-24
17 Dec 2023 22:59HS23120371-06 06 Dec 2023 13:40 10MW-B-B
17 Dec 2023 23:05HS23120371-09 06 Dec 2023 13:42 10Field Duplicate
17 Dec 2023 23:11HS23120371-10 06 Dec 2023 14:20 10Equipment Blank
17 Dec 2023 23:52HS23120371-11 06 Dec 2023 14:10 10Field Blank
Batch ID:R454518 ( 0 ) Test Name :ANIONS BY E300.0, REV 2.1, 1993 Matrix:Water
18 Dec 2023 10:43HS23120371-02 06 Dec 2023 12:40 1AMW-13B
18 Dec 2023 11:00HS23120371-04 06 Dec 2023 14:40 1FMW-21
18 Dec 2023 11:06HS23120371-05 06 Dec 2023 12:15 1FMW-24
18 Dec 2023 11:12HS23120371-06 06 Dec 2023 13:40 1MW-B-B
18 Dec 2023 11:18HS23120371-09 06 Dec 2023 13:42 1Field Duplicate
18 Dec 2023 11:24HS23120371-10 06 Dec 2023 14:20 1Equipment Blank
18 Dec 2023 11:59HS23120371-11 06 Dec 2023 14:10 1Field Blank
Batch ID:R454606 ( 0 ) Test Name :ALKALINITY BY -2011 Matrix:Water
19 Dec 2023 14:39HS23120371-02 06 Dec 2023 12:40 1AMW-13B
19 Dec 2023 14:45HS23120371-04 06 Dec 2023 14:40 1FMW-21
19 Dec 2023 14:51HS23120371-05 06 Dec 2023 12:15 1FMW-24
Batch ID:R454677 ( 0 ) Test Name :ALKALINITY BY -2011 Matrix:Water
19 Dec 2023 15:25HS23120371-06 06 Dec 2023 13:40 1MW-B-B
19 Dec 2023 15:37HS23120371-09 06 Dec 2023 13:42 1Field Duplicate
19 Dec 2023 15:41HS23120371-10 06 Dec 2023 14:20 1Equipment Blank
19 Dec 2023 15:45HS23120371-11 06 Dec 2023 14:10 1Field Blank
02-Jan-24Date: ALS Houston, US
Revision: 1
Page 25 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:204538 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-204538 Units:ug/L Analysis Date:08-Dec-2023 14:25
Run ID:ECD_13_453727 SeqNo:7718107 PrepDate:08-Dec-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-204538 Units:ug/L Analysis Date:08-Dec-2023 12:53
Run ID:ECD_13_453727 SeqNo:7718105 PrepDate:08-Dec-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.2505 0.25 0 100 60 - 1400.020
Sample ID:LCSD-204538 Units:ug/L Analysis Date:08-Dec-2023 13:16
Run ID:ECD_13_453727 SeqNo:7718106 PrepDate:08-Dec-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.2537 0.25 0 101 60 - 140 0.2505 1.29 200.020
The following samples were analyzed in this batch:HS23120371-01 HS23120371-02 HS23120371-03 HS23120371-04
HS23120371-05 HS23120371-06 HS23120371-08 HS23120371-09
HS23120371-10 HS23120371-11
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 26 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:204842 ( 0 )Instrument:ICPMS07 Method:ICP-MS METALS BY SW6020A
Sample ID:MBLK-204842 Units:mg/L Analysis Date:18-Dec-2023 15:51
Run ID:ICPMS07_454441 SeqNo:7735321 PrepDate:14-Dec-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Iron U 0.200
Manganese U 0.00500
Sample ID:LCS-204842 Units:mg/L Analysis Date:18-Dec-2023 15:53
Run ID:ICPMS07_454441 SeqNo:7735322 PrepDate:14-Dec-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Iron 4.918 5 0 98.4 80 - 1200.200
Manganese 0.04955 0.05 0 99.1 80 - 1200.00500
Sample ID:HS23120488-01MS Units:mg/L Analysis Date:18-Dec-2023 16:00
Run ID:ICPMS07_454441 SeqNo:7735325 PrepDate:14-Dec-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Iron 5.241 5 0.297 98.9 80 - 1200.200
Manganese 0.08382 0.05 0.03264 102 80 - 1200.00500
Sample ID:HS23120488-01MSD Units:mg/L Analysis Date:18-Dec-2023 16:03
Run ID:ICPMS07_454441 SeqNo:7735326 PrepDate:14-Dec-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Iron 5.251 5 0.297 99.1 80 - 120 5.241 0.184 200.200
Manganese 0.08469 0.05 0.03264 104 80 - 120 0.08382 1.03 200.00500
Sample ID:HS23120488-01PDS Units:mg/L Analysis Date:18-Dec-2023 16:05
Run ID:ICPMS07_454441 SeqNo:7735327 PrepDate:14-Dec-2023 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
PDS
Client ID:
Iron 9.774 10 0.297 94.8 75 - 1250.200
Manganese 0.1272 0.1 0.03264 94.5 75 - 1250.00500
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 27 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:204842 ( 0 )Instrument:ICPMS07 Method:ICP-MS METALS BY SW6020A
Sample ID:HS23120488-01SD Units:mg/L Analysis Date:18-Dec-2023 15:58
Run ID:ICPMS07_454441 SeqNo:7735324 PrepDate:14-Dec-2023 DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %D
%D
Limit Qual
SD
Client ID:
Iron 0.2844 0.297 0 10 J 1.00
Manganese 0.03256 0.03264 0.221 100.0250
The following samples were analyzed in this batch:HS23120371-02 HS23120371-04 HS23120371-05 HS23120371-06
HS23120371-09 HS23120371-10 HS23120371-11
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 28 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453567 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-231207 Units:ug/L Analysis Date:07-Dec-2023 11:51
Run ID:VOA10_453567 SeqNo:7714884 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
55.23 50 0 110 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.33 50 0 96.7 77 - 1131.0Surr: 4-Bromofluorobenzene
52.94 50 0 106 73 - 1261.0Surr: Dibromofluoromethane
49.87 50 0 99.7 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 29 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453567 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-231207 Units:ug/L Analysis Date:07-Dec-2023 11:09
Run ID:VOA10_453567 SeqNo:7714883 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 21.5 20 0 108 73 - 1211.0
1,2-Dibromoethane 21.75 20 0 109 76 - 1231.0
1,2-Dichloroethane 23.18 20 0 116 70 - 1241.0
4-Isopropyltoluene 21.82 20 0 109 74 - 1261.0
Benzene 20.48 20 0 102 74 - 1201.0
Chloroform 21.31 20 0 107 71 - 1211.0
Ethylbenzene 19.35 20 0 96.7 77 - 1171.0
m,p-Xylene 41.4 40 0 103 77 - 1222.0
Methyl tert-butyl ether 20.15 20 0 101 70 - 1301.0
Methylene chloride 18.73 20 0 93.7 70 - 1272.0
Naphthalene 21.09 20 0 105 70 - 1301.0
o-Xylene 20.74 20 0 104 75 - 1191.0
Tert-butyl alcohol 457.7 400 0 114 70 - 13010
Toluene 20.46 20 0 102 77 - 1181.0
Xylenes, Total 62.14 60 0 104 75 - 1223.0
53.99 50 0 108 70 - 1231.0Surr: 1,2-Dichloroethane-d4
50.45 50 0 101 77 - 1131.0Surr: 4-Bromofluorobenzene
52.27 50 0 105 73 - 1261.0Surr: Dibromofluoromethane
49.55 50 0 99.1 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 30 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453567 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23111909-02MS Units:ug/L Analysis Date:07-Dec-2023 13:36
Run ID:VOA10_453567 SeqNo:7714886 PrepDate:DF:20
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 369.7 400 0 92.4 70 - 12520
1,2-Dibromoethane 358.6 400 0 89.7 70 - 12420
1,2-Dichloroethane 409.7 400 0 102 70 - 12720
4-Isopropyltoluene 370.6 400 0 92.6 70 - 13020
Benzene 369.3 400 0 92.3 70 - 12720
Chloroform 376.7 400 0 94.2 70 - 12520
Ethylbenzene 361.8 400 0 90.5 70 - 12420
m,p-Xylene 754.5 800 0 94.3 70 - 13040
Methyl tert-butyl ether 358.7 400 0 89.7 70 - 13020
Methylene chloride 355.3 400 0 88.8 70 - 12840
Naphthalene 317 400 0 79.3 70 - 13020
o-Xylene 361.4 400 0 90.4 70 - 12420
Tert-butyl alcohol 6490 8000 0 81.1 70 - 130200
Toluene 379 400 0 94.8 70 - 12320
Xylenes, Total 1116 1200 0 93.0 70 - 13060
1077 1000 0 108 70 - 12620Surr: 1,2-Dichloroethane-d4
995.2 1000 0 99.5 77 - 11320Surr: 4-Bromofluorobenzene
1007 1000 0 101 77 - 12320Surr: Dibromofluoromethane
1018 1000 0 102 82 - 12720Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 31 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453567 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23111909-02MSD Units:ug/L Analysis Date:07-Dec-2023 13:57
Run ID:VOA10_453567 SeqNo:7714887 PrepDate:DF:20
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 344.6 400 0 86.1 70 - 125 369.7 7.03 2020
1,2-Dibromoethane 331.7 400 0 82.9 70 - 124 358.6 7.79 2020
1,2-Dichloroethane 350.5 400 0 87.6 70 - 127 409.7 15.6 2020
4-Isopropyltoluene 336.2 400 0 84.0 70 - 130 370.6 9.74 2020
Benzene 334 400 0 83.5 70 - 127 369.3 10.1 2020
Chloroform 336 400 0 84.0 70 - 125 376.7 11.4 2020
Ethylbenzene 335.9 400 0 84.0 70 - 124 361.8 7.44 2020
m,p-Xylene 675.8 800 0 84.5 70 - 130 754.5 11 2040
Methyl tert-butyl ether 332.3 400 0 83.1 70 - 130 358.7 7.62 2020
Methylene chloride 308.5 400 0 77.1 70 - 128 355.3 14.1 2040
Naphthalene 320.6 400 0 80.1 70 - 130 317 1.11 2020
o-Xylene 324.2 400 0 81.0 70 - 124 361.4 10.9 2020
Tert-butyl alcohol 5495 8000 0 68.7 70 - 130 6490 16.6 20 S200
Toluene 349.9 400 0 87.5 70 - 123 379 8 2020
Xylenes, Total 1000 1200 0 83.3 70 - 130 1116 11 2060
1095 1000 0 110 70 - 126 1077 1.65 2020Surr: 1,2-Dichloroethane-d4
996.4 1000 0 99.6 77 - 113 995.2 0.122 2020Surr: 4-Bromofluorobenzene
1010 1000 0 101 77 - 123 1007 0.365 2020Surr: Dibromofluoromethane
1015 1000 0 101 82 - 127 1018 0.335 2020Surr: Toluene-d8
The following samples were analyzed in this batch:HS23120371-02
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 32 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453608 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-231207 Units:ug/L Analysis Date:07-Dec-2023 23:23
Run ID:VOA10_453608 SeqNo:7715547 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
54.21 50 0 108 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.34 50 0 96.7 77 - 1131.0Surr: 4-Bromofluorobenzene
52.44 50 0 105 73 - 1261.0Surr: Dibromofluoromethane
49.93 50 0 99.9 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 33 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453608 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-231207 Units:ug/L Analysis Date:07-Dec-2023 22:41
Run ID:VOA10_453608 SeqNo:7715546 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 20.97 20 0 105 73 - 1211.0
1,2-Dibromoethane 20.8 20 0 104 76 - 1231.0
1,2-Dichloroethane 22.17 20 0 111 70 - 1241.0
2-Methylnaphthalene 27.9 20 0 140 55 - 1401.0
4-Isopropyltoluene 21.68 20 0 108 74 - 1261.0
Benzene 20.05 20 0 100 74 - 1201.0
Chloroform 20.63 20 0 103 71 - 1211.0
Ethylbenzene 20.04 20 0 100 77 - 1171.0
m,p-Xylene 39.98 40 0 99.9 77 - 1222.0
Methyl tert-butyl ether 21.62 20 0 108 70 - 1301.0
Methylene chloride 17.1 20 0 85.5 70 - 1272.0
Naphthalene 23.26 20 0 116 70 - 1301.0
o-Xylene 20.34 20 0 102 75 - 1191.0
Tert-butyl alcohol 502.7 400 0 126 70 - 13010
Toluene 20.33 20 0 102 77 - 1181.0
Xylenes, Total 60.32 60 0 101 75 - 1223.0
55.12 50 0 110 70 - 1231.0Surr: 1,2-Dichloroethane-d4
50.42 50 0 101 77 - 1131.0Surr: 4-Bromofluorobenzene
50.97 50 0 102 73 - 1261.0Surr: Dibromofluoromethane
50.06 50 0 100 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 34 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453608 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23120374-07MS Units:ug/L Analysis Date:08-Dec-2023 01:50
Run ID:VOA10_453608 SeqNo:7715554 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 17.55 20 0 87.7 70 - 1251.0
1,2-Dibromoethane 17.51 20 0 87.5 70 - 1241.0
1,2-Dichloroethane 19.82 20 0 99.1 70 - 1271.0
2-Methylnaphthalene 15.2 20 0 76.0 55 - 1401.0
4-Isopropyltoluene 17 20 0 85.0 70 - 1301.0
Benzene 18.1 20 0 90.5 70 - 1271.0
Chloroform 18.45 20 0 92.3 70 - 1251.0
Ethylbenzene 17.87 20 0 89.4 70 - 1241.0
m,p-Xylene 35.15 40 0 87.9 70 - 1302.0
Methyl tert-butyl ether 19.1 20 0 95.5 70 - 1301.0
Methylene chloride 15.87 20 0 79.4 70 - 1282.0
Naphthalene 16.75 20 0 83.7 70 - 1301.0
o-Xylene 17.07 20 0 85.3 70 - 1241.0
Tert-butyl alcohol 307.5 400 0 76.9 70 - 13010
Toluene 17.82 20 0 89.1 70 - 1231.0
Xylenes, Total 52.21 60 0 87.0 70 - 1303.0
55.63 50 0 111 70 - 1261.0Surr: 1,2-Dichloroethane-d4
50.03 50 0 100 77 - 1131.0Surr: 4-Bromofluorobenzene
52.31 50 0 105 77 - 1231.0Surr: Dibromofluoromethane
49.68 50 0 99.4 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 35 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453608 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23120374-07MSD Units:ug/L Analysis Date:08-Dec-2023 02:11
Run ID:VOA10_453608 SeqNo:7715555 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 15.8 20 0 79.0 70 - 125 17.55 10.5 201.0
1,2-Dibromoethane 16.08 20 0 80.4 70 - 124 17.51 8.49 201.0
1,2-Dichloroethane 17.33 20 0 86.6 70 - 127 19.82 13.4 201.0
2-Methylnaphthalene 15.24 20 0 76.2 55 - 140 15.2 0.287 201.0
4-Isopropyltoluene 15.41 20 0 77.0 70 - 130 17 9.8 201.0
Benzene 16.38 20 0 81.9 70 - 127 18.1 9.96 201.0
Chloroform 16.41 20 0 82.0 70 - 125 18.45 11.7 201.0
Ethylbenzene 16.28 20 0 81.4 70 - 124 17.87 9.35 201.0
m,p-Xylene 33.54 40 0 83.8 70 - 130 35.15 4.7 202.0
Methyl tert-butyl ether 17.71 20 0 88.6 70 - 130 19.1 7.53 201.0
Methylene chloride 15.15 20 0 75.7 70 - 128 15.87 4.69 202.0
Naphthalene 15.51 20 0 77.6 70 - 130 16.75 7.64 201.0
o-Xylene 15.79 20 0 78.9 70 - 124 17.07 7.78 201.0
Tert-butyl alcohol 308.2 400 0 77.1 70 - 130 307.5 0.224 2010
Toluene 16.79 20 0 83.9 70 - 123 17.82 5.98 201.0
Xylenes, Total 49.32 60 0 82.2 70 - 130 52.21 5.69 203.0
54.62 50 0 109 70 - 126 55.63 1.84 201.0Surr: 1,2-Dichloroethane-d4
49.25 50 0 98.5 77 - 113 50.03 1.56 201.0Surr: 4-Bromofluorobenzene
52.03 50 0 104 77 - 123 52.31 0.528 201.0Surr: Dibromofluoromethane
50.33 50 0 101 82 - 127 49.68 1.3 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23120371-03 HS23120371-04 HS23120371-05 HS23120371-07
HS23120371-08 HS23120371-10 HS23120371-11 HS23120371-12
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 36 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453614 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-231208 Units:ug/L Analysis Date:08-Dec-2023 11:15
Run ID:VOA10_453614 SeqNo:7715656 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
54.52 50 0 109 70 - 1231.0Surr: 1,2-Dichloroethane-d4
49.17 50 0 98.3 77 - 1131.0Surr: 4-Bromofluorobenzene
51.89 50 0 104 73 - 1261.0Surr: Dibromofluoromethane
49.39 50 0 98.8 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 37 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453614 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-231208 Units:ug/L Analysis Date:08-Dec-2023 10:33
Run ID:VOA10_453614 SeqNo:7715655 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 21.74 20 0 109 73 - 1211.0
1,2-Dibromoethane 21.02 20 0 105 76 - 1231.0
1,2-Dichloroethane 23.95 20 0 120 70 - 1241.0
2-Methylnaphthalene 24.73 20 0 124 55 - 1401.0
4-Isopropyltoluene 22.12 20 0 111 74 - 1261.0
Benzene 20.62 20 0 103 74 - 1201.0
Chloroform 20.96 20 0 105 71 - 1211.0
Ethylbenzene 20.5 20 0 102 77 - 1171.0
m,p-Xylene 41.13 40 0 103 77 - 1222.0
Methyl tert-butyl ether 22.15 20 0 111 70 - 1301.0
Methylene chloride 20.7 20 0 103 70 - 1272.0
Naphthalene 21.5 20 0 108 70 - 1301.0
o-Xylene 20.06 20 0 100 75 - 1191.0
Tert-butyl alcohol 446.6 400 0 112 70 - 13010
Toluene 20.19 20 0 101 77 - 1181.0
Xylenes, Total 61.19 60 0 102 75 - 1223.0
55.24 50 0 110 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.79 50 0 97.6 77 - 1131.0Surr: 4-Bromofluorobenzene
51.93 50 0 104 73 - 1261.0Surr: Dibromofluoromethane
49.84 50 0 99.7 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 38 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453614 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23120255-02MS Units:ug/L Analysis Date:08-Dec-2023 12:26
Run ID:VOA10_453614 SeqNo:7715659 PrepDate:DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 85.39 100 0 85.4 70 - 1255.0
1,2-Dibromoethane 83.69 100 0 83.7 70 - 1245.0
1,2-Dichloroethane 98.22 100 0 98.2 70 - 1275.0
2-Methylnaphthalene 68.18 100 0 68.2 55 - 1405.0
4-Isopropyltoluene 85.09 100 0 85.1 70 - 1305.0
Benzene 83.99 100 0 84.0 70 - 1275.0
Chloroform 85.08 100 0 85.1 70 - 1255.0
Ethylbenzene 84.32 100 0 84.3 70 - 1245.0
m,p-Xylene 170.4 200 0 85.2 70 - 13010
Methyl tert-butyl ether 370.7 100 284.6 86.1 70 - 1305.0
Methylene chloride 77.89 100 0 77.9 70 - 12810
Naphthalene 73.94 100 0 73.9 70 - 1305.0
o-Xylene 83.06 100 0 83.1 70 - 1245.0
Tert-butyl alcohol 1896 2000 0 94.8 70 - 13050
Toluene 85.04 100 0 85.0 70 - 1235.0
Xylenes, Total 253.4 300 0 84.5 70 - 13015
284.8 250 0 114 70 - 1265.0Surr: 1,2-Dichloroethane-d4
243.4 250 0 97.4 77 - 1135.0Surr: 4-Bromofluorobenzene
248.2 250 0 99.3 77 - 1235.0Surr: Dibromofluoromethane
251.7 250 0 101 82 - 1275.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 39 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453614 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23120255-02MSD Units:ug/L Analysis Date:08-Dec-2023 12:47
Run ID:VOA10_453614 SeqNo:7715660 PrepDate:DF:5
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 76.6 100 0 76.6 70 - 125 85.39 10.9 205.0
1,2-Dibromoethane 70.18 100 0 70.2 70 - 124 83.69 17.6 205.0
1,2-Dichloroethane 85.65 100 0 85.6 70 - 127 98.22 13.7 205.0
2-Methylnaphthalene 60.57 100 0 60.6 55 - 140 68.18 11.8 205.0
4-Isopropyltoluene 74.4 100 0 74.4 70 - 130 85.09 13.4 205.0
Benzene 78.31 100 0 78.3 70 - 127 83.99 7 205.0
Chloroform 78.18 100 0 78.2 70 - 125 85.08 8.45 205.0
Ethylbenzene 72.91 100 0 72.9 70 - 124 84.32 14.5 205.0
m,p-Xylene 145 200 0 72.5 70 - 130 170.4 16.1 2010
Methyl tert-butyl ether 370.9 100 284.6 86.4 70 - 130 370.7 0.0638 205.0
Methylene chloride 71.07 100 0 71.1 70 - 128 77.89 9.17 2010
Naphthalene 68.62 100 0 68.6 70 - 130 73.94 7.46 20 S5.0
o-Xylene 69.94 100 0 69.9 70 - 124 83.06 17.1 20 S5.0
Tert-butyl alcohol 1744 2000 0 87.2 70 - 130 1896 8.32 2050
Toluene 75.53 100 0 75.5 70 - 123 85.04 11.8 205.0
Xylenes, Total 214.9 300 0 71.6 70 - 130 253.4 16.4 2015
281.9 250 0 113 70 - 126 284.8 0.996 205.0Surr: 1,2-Dichloroethane-d4
245.9 250 0 98.4 77 - 113 243.4 1.03 205.0Surr: 4-Bromofluorobenzene
254.2 250 0 102 77 - 123 248.2 2.36 205.0Surr: Dibromofluoromethane
247.8 250 0 99.1 82 - 127 251.7 1.58 205.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS23120371-02 HS23120371-04 HS23120371-05 HS23120371-06
HS23120371-08 HS23120371-09
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 40 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453785 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-231211 Units:ug/L Analysis Date:11-Dec-2023 10:39
Run ID:VOA10_453785 SeqNo:7719128 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
53.02 50 0 106 70 - 1231.0Surr: 1,2-Dichloroethane-d4
46.46 50 0 92.9 77 - 1131.0Surr: 4-Bromofluorobenzene
50.09 50 0 100 73 - 1261.0Surr: Dibromofluoromethane
53.55 50 0 107 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 41 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453785 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-231211 Units:ug/L Analysis Date:11-Dec-2023 09:57
Run ID:VOA10_453785 SeqNo:7719177 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 20.9 20 0 105 73 - 1211.0
1,2-Dibromoethane 21.76 20 0 109 76 - 1231.0
1,2-Dichloroethane 22.71 20 0 114 70 - 1241.0
2-Methylnaphthalene 30 20 0 150 55 - 140 S1.0
4-Isopropyltoluene 21.2 20 0 106 74 - 1261.0
Benzene 19.31 20 0 96.6 74 - 1201.0
Chloroform 20.67 20 0 103 71 - 1211.0
Ethylbenzene 20.14 20 0 101 77 - 1171.0
m,p-Xylene 40.55 40 0 101 77 - 1222.0
Methyl tert-butyl ether 22.39 20 0 112 70 - 1301.0
Methylene chloride 16.62 20 0 83.1 70 - 1272.0
Naphthalene 24.51 20 0 123 70 - 1301.0
o-Xylene 19.04 20 0 95.2 75 - 1191.0
Tert-butyl alcohol 506.4 400 0 127 70 - 13010
Toluene 21.73 20 0 109 77 - 1181.0
Xylenes, Total 59.59 60 0 99.3 75 - 1223.0
53.24 50 0 106 70 - 1231.0Surr: 1,2-Dichloroethane-d4
45.98 50 0 92.0 77 - 1131.0Surr: 4-Bromofluorobenzene
49.6 50 0 99.2 73 - 1261.0Surr: Dibromofluoromethane
55.39 50 0 111 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 42 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453785 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23120412-01MS Units:ug/L Analysis Date:11-Dec-2023 13:06
Run ID:VOA10_453785 SeqNo:7719158 PrepDate:DF:20
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 325.8 400 0 81.5 70 - 12520
1,2-Dibromoethane 340.6 400 0 85.2 70 - 12420
1,2-Dichloroethane 357.6 400 0 89.4 70 - 12720
2-Methylnaphthalene 466.9 400 0 117 55 - 14020
4-Isopropyltoluene 321.2 400 0 80.3 70 - 13020
Benzene 315.6 400 0 78.9 70 - 12720
Chloroform 321.5 400 0 80.4 70 - 12520
Ethylbenzene 311.7 400 0 77.9 70 - 12420
m,p-Xylene 639.1 800 0 79.9 70 - 13040
Methyl tert-butyl ether 344 400 0 86.0 70 - 13020
Methylene chloride 306.7 400 0 76.7 70 - 12840
Naphthalene 343.2 400 0 85.8 70 - 13020
o-Xylene 293.1 400 0 73.3 70 - 12420
Tert-butyl alcohol 6672 8000 0 83.4 70 - 130200
Toluene 345.8 400 0 86.4 70 - 12320
Xylenes, Total 932.2 1200 0 77.7 70 - 13060
1162 1000 0 116 70 - 12620Surr: 1,2-Dichloroethane-d4
959 1000 0 95.9 77 - 11320Surr: 4-Bromofluorobenzene
1043 1000 0 104 77 - 12320Surr: Dibromofluoromethane
1076 1000 0 108 82 - 12720Surr: Toluene-d8
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 43 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R453785 ( 0 )Instrument:VOA10 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS23120412-01MSD Units:ug/L Analysis Date:11-Dec-2023 13:27
Run ID:VOA10_453785 SeqNo:7719159 PrepDate:DF:20
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 429.4 400 0 107 70 - 125 325.8 27.4 20 R20
1,2-Dibromoethane 437.4 400 0 109 70 - 124 340.6 24.9 20 R20
1,2-Dichloroethane 457.9 400 0 114 70 - 127 357.6 24.6 20 R20
2-Methylnaphthalene 573.3 400 0 143 55 - 140 466.9 20.5 20 SR20
4-Isopropyltoluene 435.2 400 0 109 70 - 130 321.2 30.1 20 R20
Benzene 413.5 400 0 103 70 - 127 315.6 26.9 20 R20
Chloroform 427 400 0 107 70 - 125 321.5 28.2 20 R20
Ethylbenzene 423.6 400 0 106 70 - 124 311.7 30.4 20 R20
m,p-Xylene 827.4 800 0 103 70 - 130 639.1 25.7 20 R40
Methyl tert-butyl ether 444.8 400 0 111 70 - 130 344 25.6 20 R20
Methylene chloride 356.6 400 0 89.1 70 - 128 306.7 15 2040
Naphthalene 474.7 400 0 119 70 - 130 343.2 32.1 20 R20
o-Xylene 410.8 400 0 103 70 - 124 293.1 33.4 20 R20
Tert-butyl alcohol 8801 8000 0 110 70 - 130 6672 27.5 20 R200
Toluene 455.5 400 0 114 70 - 123 345.8 27.4 20 R20
Xylenes, Total 1238 1200 0 103 70 - 130 932.2 28.2 20 R60
1109 1000 0 111 70 - 126 1162 4.69 2020Surr: 1,2-Dichloroethane-d4
958.6 1000 0 95.9 77 - 113 959 0.0371 2020Surr: 4-Bromofluorobenzene
987.5 1000 0 98.8 77 - 123 1043 5.5 2020Surr: Dibromofluoromethane
1092 1000 0 109 82 - 127 1076 1.54 2020Surr: Toluene-d8
The following samples were analyzed in this batch:HS23120371-01
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 44 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R454022 ( 0 )Instrument:UV-2450 Method:FERROUS IRON BY SM3500 FE B
Sample ID:MBLK-R454022 Units:mg/L Analysis Date:08-Dec-2023 10:29
Run ID:UV-2450_454022 SeqNo:7724287 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ferrous Iron U 80 - 1200.0500
Sample ID:LCS-R454022 Units:mg/L Analysis Date:08-Dec-2023 10:29
Run ID:UV-2450_454022 SeqNo:7724286 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ferrous Iron 0.246 0.25 0 98.4 80 - 1200.0500
Sample ID:HS23120371-02MS Units:mg/L Analysis Date:08-Dec-2023 10:29
Run ID:UV-2450_454022 SeqNo:7724289 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:AMW-13B
Ferrous Iron 0.3 0.25 0.052 99.2 75 - 1250.0500
Sample ID:HS23120371-02MSD Units:mg/L Analysis Date:08-Dec-2023 10:29
Run ID:UV-2450_454022 SeqNo:7724288 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:AMW-13B
Ferrous Iron 0.29 0.25 0.052 95.2 75 - 125 0.3 3.39 200.0500
The following samples were analyzed in this batch:HS23120371-02 HS23120371-04 HS23120371-05 HS23120371-06
HS23120371-09 HS23120371-10 HS23120371-11
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 45 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R454413 ( 0 )Instrument:ICS-Integrion Method:NITRATE/NITRITE BY E300.0, REV 2.1,
1993
Sample ID:MBLK Units:mg/L Analysis Date:17-Dec-2023 22:18
Run ID:ICS-Integrion_454413 SeqNo:7733025 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Nitrate/Nitrite (as N)U 0.200
Sample ID:LCS Units:mg/L Analysis Date:17-Dec-2023 22:24
Run ID:ICS-Integrion_454413 SeqNo:7733026 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Nitrate/Nitrite (as N)8.331 8 0 104 90 - 1100.200
Sample ID:HS23120371-02MS Units:mg/L Analysis Date:17-Dec-2023 22:36
Run ID:ICS-Integrion_454413 SeqNo:7733028 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:AMW-13B
Nitrate/Nitrite (as N)36.46 40 0 91.1 80 - 1202.00
Sample ID:HS23120371-02MSD Units:mg/L Analysis Date:17-Dec-2023 22:42
Run ID:ICS-Integrion_454413 SeqNo:7733029 PrepDate:DF:10
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:AMW-13B
Nitrate/Nitrite (as N)38.41 40 0 96.0 80 - 120 36.46 5.21 202.00
The following samples were analyzed in this batch:HS23120371-02 HS23120371-04 HS23120371-05 HS23120371-06
HS23120371-09 HS23120371-10 HS23120371-11
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 46 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R454518 ( 0 )Instrument:ICS-Integrion Method:ANIONS BY E300.0, REV 2.1, 1993
Sample ID:MBLK Units:mg/L Analysis Date:18-Dec-2023 10:31
Run ID:ICS-Integrion_454518 SeqNo:7735702 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Sulfate U 0.500
Sample ID:LCS Units:mg/L Analysis Date:18-Dec-2023 10:37
Run ID:ICS-Integrion_454518 SeqNo:7735703 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Sulfate 21.83 20 0 109 90 - 1100.500
Sample ID:HS23120844-03MS Units:mg/L Analysis Date:18-Dec-2023 12:28
Run ID:ICS-Integrion_454518 SeqNo:7735719 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Sulfate 29.49 10 19.78 97.1 80 - 1200.500
Sample ID:HS23120371-02MS Units:mg/L Analysis Date:18-Dec-2023 10:49
Run ID:ICS-Integrion_454518 SeqNo:7735705 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:AMW-13B
Sulfate 13.19 10 1.801 114 80 - 1200.500
Sample ID:HS23120844-03MSD Units:mg/L Analysis Date:18-Dec-2023 12:34
Run ID:ICS-Integrion_454518 SeqNo:7735720 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Sulfate 29.71 10 19.78 99.3 80 - 120 29.49 0.747 200.500
Sample ID:HS23120371-02MSD Units:mg/L Analysis Date:18-Dec-2023 10:54
Run ID:ICS-Integrion_454518 SeqNo:7735706 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:AMW-13B
Sulfate 13.28 10 1.801 115 80 - 120 13.19 0.65 200.500
The following samples were analyzed in this batch:HS23120371-02 HS23120371-04 HS23120371-05 HS23120371-06
HS23120371-09 HS23120371-10 HS23120371-11
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 47 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R454606 ( 0 )Instrument:Skalar 03 Method:ALKALINITY BY -2011
Sample ID:MBLK-12.19.2023 Units:mg/L Analysis Date:19-Dec-2023 12:15
Run ID:Skalar 03_454606 SeqNo:7737713 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-12.19.2023 Units:mg/L Analysis Date:19-Dec-2023 12:21
Run ID:Skalar 03_454606 SeqNo:7737714 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)917.2 1000 0 91.7 85 - 1155.00
Alkalinity, Total (As CaCO3)935.5 1000 0 93.6 85 - 1155.00
Sample ID:LCSD-12.19.2023 Units:mg/L Analysis Date:19-Dec-2023 12:28
Run ID:Skalar 03_454606 SeqNo:7737715 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)915 1000 0 91.5 85 - 115 917.2 0.24 205.00
Alkalinity, Total (As CaCO3)933.6 1000 0 93.4 85 - 115 935.5 0.203 205.00
Sample ID:HS23120692-01DUP Units:mg/L Analysis Date:19-Dec-2023 12:39
Run ID:Skalar 03_454606 SeqNo:7737717 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3)277.8 282.3 1.61 205.00
Alkalinity, Carbonate (As CaCO3)U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)277.8 282.3 1.61 205.00
The following samples were analyzed in this batch:HS23120371-02 HS23120371-04 HS23120371-05
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 48 of 56
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS23120371
QC BATCH REPORT
Batch ID:R454677 ( 0 )Instrument:Skalar 03 Method:ALKALINITY BY -2011
Sample ID:MBLK-12.19.2023 Units:mg/L Analysis Date:19-Dec-2023 15:06
Run ID:Skalar 03_454677 SeqNo:7739381 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3)U 5.00
Alkalinity, Carbonate (As CaCO3)U 5.00
Alkalinity, Hydroxide (As CaCO3)U 5.00
Alkalinity, Total (As CaCO3)U 5.00
Sample ID:LCS-12.19.2023 Units:mg/L Analysis Date:19-Dec-2023 15:12
Run ID:Skalar 03_454677 SeqNo:7739382 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3)894.6 1000 0 89.5 85 - 1155.00
Alkalinity, Total (As CaCO3)933.2 1000 0 93.3 85 - 1155.00
Sample ID:LCSD-12.19.2023 Units:mg/L Analysis Date:19-Dec-2023 15:19
Run ID:Skalar 03_454677 SeqNo:7739383 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3)891.8 1000 0 89.2 85 - 115 894.6 0.313 205.00
Alkalinity, Total (As CaCO3)931.7 1000 0 93.2 85 - 115 933.2 0.161 205.00
Sample ID:HS23120371-06DUP Units:mg/L Analysis Date:19-Dec-2023 15:31
Run ID:Skalar 03_454677 SeqNo:7739385 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:MW-B-B
Alkalinity, Bicarbonate (As CaCO3)40.9 40.8 0.245 205.00
Alkalinity, Carbonate (As CaCO3)24.4 23.2 5.04 205.00
Alkalinity, Hydroxide (As CaCO3)U 0 0 205.00
Alkalinity, Total (As CaCO3)65.3 64 2.01 205.00
The following samples were analyzed in this batch:HS23120371-06 HS23120371-09 HS23120371-10 HS23120371-11
ALS Houston, US Date: 02-Jan-24
1Revision:
Page 49 of 56
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS23120371
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
mg/L Milligrams per Liter
ALS Houston, US Date: 02-Jan-24
Page 50 of 56
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087 2023-2024 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2023-140 31-Aug-2024
Texas T104704231-23-32 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
02-Jan-24Date: ALS Houston, US
Page 51 of 56
Corey Grandits
07-Dec-2023 09:35Date/Time Received:HS23120371
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.5uc/3.4c,3.0uc/2.9c ir31
11234,51496
12/7/23 1205
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ Belinda Gomez
Date/TimeeSignatureDate/TimeeSignature
08-Dec-2023 09:5307-Dec-2023 12:05
FedExwCarrier name:Matrices:
Reviewed by:/S/ Bernadette A. Fini
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
2 Page(s)
COC IDs:306079,306081
ALS Houston, US 02-Jan-24Date:
Page 52 of 56
Page 53 of 56
Page 54 of 56
Page 55 of 56
Page 56 of 56
February 15, 2024
Daniel Breckenridge
Groundwater & Environmental Service, Inc.
571 Southlake Boulevard
Richmond, VA 23236
The analytical data provided relates directly to the samples received by ALS Environmental
and for only the analyses requested. Results are expressed as "as received" unless
otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the
Case Narrative or as noted with qualifiers in the QC batch information. Should this
laboratory report need to be reproduced, it should be reproduced in full unless written
approval has been obtained by ALS Environmental. Samples will be disposed in 30 days
unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 2 sample(s) on Feb 03, 2024 for the analysis presented in the
following report.
Laboratory Results for:Former Greensboro Terminal
Dear Daniel Breckenridge,
Work Order:HS24020476
Project Manager
Generated By: JUMOKE.LAWAL
Bernadette A. Fini
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
alsglobal.com
Page 1 of 18
Client:Groundwater & Environmental Service, Inc.
Work Order:HS24020476
Project:Former Greensboro Terminal SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrixTagNo Date Received Hold
HS24020476-01 02-Feb-2024 12:49 03-Feb-2024 09:10Z2-PZ-09 Groundwater
HS24020476-02 02-Feb-2024 00:00 03-Feb-2024 09:10Trip Blank Water
ALS Houston, US 15-Feb-24Date:
Page 2 of 18
Client:CASE NARRATIVE
Work Order:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
Project:
HS24020476
ECD Organics by Method SW8011
Batch ID: 207245
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
GCMS Volatiles by Method SW8260
Batch ID: R458535
Sample ID: Z2-PZ-09 (HS24020476-01)
Lowest practical dilution due to sample matrix and/or high concentration of non-target analyte(s).•
ALS Houston, US 15-Feb-24Date:
Page 3 of 18
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Z2-PZ-09
WorkOrder:
Lab ID:
Collection Date:
HS24020476
HS24020476-01
02-Feb-2024 12:49 Matrix:Groundwater
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP
5ug/L 09-Feb-2024 19:041.51,2,4-Trimethylbenzene 5.0U
5ug/L 09-Feb-2024 19:041.01,2-Dibromoethane 5.0U
5ug/L 09-Feb-2024 19:041.01,2-Dichloroethane 5.0U
5ug/L 09-Feb-2024 19:045.02-Methylnaphthalene 5.075
5ug/L 09-Feb-2024 19:041.54-Isopropyltoluene 5.0U
5ug/L 09-Feb-2024 19:041.0Benzene 5.0490
5ug/L 09-Feb-2024 19:041.0Chloroform 5.0U
5ug/L 09-Feb-2024 19:041.5Ethylbenzene 5.0U
5ug/L 09-Feb-2024 19:042.5m,p-Xylene 10260
5ug/L 09-Feb-2024 19:041.0Methyl tert-butyl ether 5.0U
5ug/L 09-Feb-2024 19:045.0Methylene chloride 10U
5ug/L 09-Feb-2024 19:041.5Naphthalene 5.0130
5ug/L 09-Feb-2024 19:041.5o-Xylene 5.025
5ug/L 09-Feb-2024 19:0450Tert-butyl alcohol 50U
5ug/L 09-Feb-2024 19:04J1.0Toluene 5.01.9
5ug/L 09-Feb-2024 19:041.5Xylenes, Total 15280
Surr: 1,2-Dichloroethane-d4 5%REC 09-Feb-2024 19:0485.7 70-126
Surr: 4-Bromofluorobenzene 5%REC 09-Feb-2024 19:0410377-113
Surr: Dibromofluoromethane 5%REC 09-Feb-2024 19:0485.3 77-123
Surr: Toluene-d8 5%REC 09-Feb-2024 19:0491.0 82-127
EDB-123TCP BY SW8011 Method:SW8011 Analyst: ASPrep:SW8011 / 13-Feb-2024
1ug/L 13-Feb-2024 19:010.00321,2-Dibromoethane 0.021U
15-Feb-24Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of 18
Client:
Project:
Sample ID:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
Trip Blank
WorkOrder:
Lab ID:
Collection Date:
HS24020476
HS24020476-02
02-Feb-2024 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP
1ug/L 09-Feb-2024 16:200.301,2,4-Trimethylbenzene 1.0U
1ug/L 09-Feb-2024 16:200.201,2-Dibromoethane 1.0U
1ug/L 09-Feb-2024 16:200.201,2-Dichloroethane 1.0U
1ug/L 09-Feb-2024 16:201.02-Methylnaphthalene 1.0U
1ug/L 09-Feb-2024 16:200.304-Isopropyltoluene 1.0U
1ug/L 09-Feb-2024 16:200.20Benzene 1.0U
1ug/L 09-Feb-2024 16:200.20Chloroform 1.0U
1ug/L 09-Feb-2024 16:200.30Ethylbenzene 1.0U
1ug/L 09-Feb-2024 16:200.50m,p-Xylene 2.0U
1ug/L 09-Feb-2024 16:200.20Methyl tert-butyl ether 1.0U
1ug/L 09-Feb-2024 16:201.0Methylene chloride 2.0U
1ug/L 09-Feb-2024 16:200.30Naphthalene 1.0U
1ug/L 09-Feb-2024 16:200.30o-Xylene 1.0U
1ug/L 09-Feb-2024 16:2010Tert-butyl alcohol 10U
1ug/L 09-Feb-2024 16:200.20Toluene 1.0U
1ug/L 09-Feb-2024 16:200.30Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 09-Feb-2024 16:2088.4 70-126
Surr: 4-Bromofluorobenzene 1%REC 09-Feb-2024 16:2094.8 77-113
Surr: Dibromofluoromethane 1%REC 09-Feb-2024 16:2092.8 77-123
Surr: Toluene-d8 1%REC 09-Feb-2024 16:2091.3 82-127
15-Feb-24Date: ALS Houston, US
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 18
Weight / Prep Log
HS24020476
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
Client:
Batch ID:207245
Method:AQPREP: 8011 EDB 8011_WPRPrep Code:
Start Date: 13 Feb 2024 10:41 End Date: 13 Feb 2024 10:41
ContainerSample ID
Sample
Wt/Vol
Final
Volume
Prep
Factor
HS24020476-01 35 (mL)40 mL VOA w/ HCL36.91 (mL)1.055
15-Feb-24Date: ALS Houston, US
Page 6 of 18
Client:
Former Greensboro Terminal
Groundwater & Environmental Service, Inc.
WorkOrder:
Project:
HS24020476
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID Leachate Date DF
Batch ID:207245 ( 0 ) Test Name :EDB-123TCP BY SW8011 Matrix:Groundwater
13 Feb 2024 10:41 13 Feb 2024 19:01HS24020476-01 02 Feb 2024 12:49 1Z2-PZ-09
Batch ID:R458535 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Water
09 Feb 2024 16:20HS24020476-02 02 Feb 2024 00:00 1Trip Blank
Batch ID:R458535 ( 0 ) Test Name :LOW LEVEL VOLATILES BY SW8260C Matrix:Groundwater
09 Feb 2024 19:04HS24020476-01 02 Feb 2024 12:49 5Z2-PZ-09
15-Feb-24Date: ALS Houston, US
Page 7 of 18
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS24020476
QC BATCH REPORT
Batch ID:207245 ( 0 )Instrument:ECD_13 Method:EDB-123TCP BY SW8011
Sample ID:MBLK-207245 Units:ug/L Analysis Date:13-Feb-2024 18:38
Run ID:ECD_13_458730 SeqNo:7829617 PrepDate:13-Feb-2024 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2-Dibromoethane U 0.020
Sample ID:LCS-207245 Units:ug/L Analysis Date:13-Feb-2024 17:50
Run ID:ECD_13_458730 SeqNo:7829615 PrepDate:13-Feb-2024 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2-Dibromoethane 0.2301 0.25 0 92.0 60 - 1400.020
Sample ID:LCSD-207245 Units:ug/L Analysis Date:13-Feb-2024 18:14
Run ID:ECD_13_458730 SeqNo:7829616 PrepDate:13-Feb-2024 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2-Dibromoethane 0.2304 0.25 0 92.2 60 - 140 0.2301 0.152 200.020
Sample ID:HS24020529-03MS Units:ug/L Analysis Date:13-Feb-2024 17:03
Run ID:ECD_13_458730 SeqNo:7829613 PrepDate:13-Feb-2024 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2-Dibromoethane 0.2173 0.25 0 86.9 60 - 1400.021
Sample ID:HS24020529-03MSD Units:ug/L Analysis Date:13-Feb-2024 17:27
Run ID:ECD_13_458730 SeqNo:7829614 PrepDate:13-Feb-2024 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2-Dibromoethane 0.19 0.25 0 76.0 60 - 140 0.2173 13.4 200.021
The following samples were analyzed in this batch:HS24020476-01
ALS Houston, US Date: 15-Feb-24
Page 8 of 18
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS24020476
QC BATCH REPORT
Batch ID:R458535 ( 0 )Instrument:VOA4 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VBLKW-240209 Units:ug/L Analysis Date:09-Feb-2024 11:24
Run ID:VOA4_458535 SeqNo:7825567 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,2,4-Trimethylbenzene U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichloroethane U 1.0
2-Methylnaphthalene U 1.0
4-Isopropyltoluene U 1.0
Benzene U 1.0
Chloroform U 1.0
Ethylbenzene U 1.0
m,p-Xylene U 2.0
Methyl tert-butyl ether U 1.0
Methylene chloride U 2.0
Naphthalene U 1.0
o-Xylene U 1.0
Tert-butyl alcohol U 10
Toluene U 1.0
Xylenes, Total U 3.0
41.09 50 0 82.2 70 - 1231.0Surr: 1,2-Dichloroethane-d4
48.7 50 0 97.4 77 - 1131.0Surr: 4-Bromofluorobenzene
43.11 50 0 86.2 73 - 1261.0Surr: Dibromofluoromethane
45.49 50 0 91.0 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 15-Feb-24
Page 9 of 18
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS24020476
QC BATCH REPORT
Batch ID:R458535 ( 0 )Instrument:VOA4 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSW-240209 Units:ug/L Analysis Date:09-Feb-2024 10:15
Run ID:VOA4_458535 SeqNo:7825565 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,2,4-Trimethylbenzene 18.77 20 0 93.9 73 - 1211.0
1,2-Dibromoethane 19.63 20 0 98.1 76 - 1231.0
1,2-Dichloroethane 20.36 20 0 102 70 - 1241.0
2-Methylnaphthalene 17.45 20 0 87.2 55 - 1401.0
4-Isopropyltoluene 19.29 20 0 96.5 74 - 1261.0
Benzene 17.63 20 0 88.1 74 - 1201.0
Chloroform 16.78 20 0 83.9 71 - 1211.0
Ethylbenzene 18.57 20 0 92.9 77 - 1171.0
m,p-Xylene 38.71 40 0 96.8 77 - 1222.0
Methyl tert-butyl ether 16.9 20 0 84.5 70 - 1301.0
Methylene chloride 17.13 20 0 85.6 70 - 1272.0
Naphthalene 19.51 20 0 97.5 70 - 1301.0
o-Xylene 19.56 20 0 97.8 75 - 1191.0
Tert-butyl alcohol 348.4 400 0 87.1 70 - 13010
Toluene 18.09 20 0 90.4 77 - 1181.0
Xylenes, Total 58.28 60 0 97.1 75 - 1223.0
40.34 50 0 80.7 70 - 1231.0Surr: 1,2-Dichloroethane-d4
50.39 50 0 101 77 - 1131.0Surr: 4-Bromofluorobenzene
41.83 50 0 83.7 73 - 1261.0Surr: Dibromofluoromethane
45.83 50 0 91.7 81 - 1201.0Surr: Toluene-d8
ALS Houston, US Date: 15-Feb-24
Page 10 of 18
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS24020476
QC BATCH REPORT
Batch ID:R458535 ( 0 )Instrument:VOA4 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:VLCSDW-240209 Units:ug/L Analysis Date:09-Feb-2024 10:38
Run ID:VOA4_458535 SeqNo:7825566 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,2,4-Trimethylbenzene 18.24 20 0 91.2 73 - 121 18.77 2.89 201.0
1,2-Dibromoethane 18.87 20 0 94.3 76 - 123 19.63 3.95 201.0
1,2-Dichloroethane 20.21 20 0 101 70 - 124 20.36 0.776 201.0
2-Methylnaphthalene 16.5 20 0 82.5 55 - 140 17.45 5.55 201.0
4-Isopropyltoluene 17.86 20 0 89.3 74 - 126 19.29 7.72 201.0
Benzene 16.73 20 0 83.7 74 - 120 17.63 5.2 201.0
Chloroform 16.35 20 0 81.8 71 - 121 16.78 2.6 201.0
Ethylbenzene 17.11 20 0 85.5 77 - 117 18.57 8.21 201.0
m,p-Xylene 35.99 40 0 90.0 77 - 122 38.71 7.3 202.0
Methyl tert-butyl ether 16.77 20 0 83.8 70 - 130 16.9 0.796 201.0
Methylene chloride 16.01 20 0 80.0 70 - 127 17.13 6.75 202.0
Naphthalene 19.12 20 0 95.6 70 - 130 19.51 2.01 201.0
o-Xylene 18.79 20 0 94.0 75 - 119 19.56 4.02 201.0
Tert-butyl alcohol 349.5 400 0 87.4 70 - 130 348.4 0.314 2010
Toluene 16.91 20 0 84.5 77 - 118 18.09 6.75 201.0
Xylenes, Total 54.78 60 0 91.3 75 - 122 58.28 6.19 203.0
39.2 50 0 78.4 70 - 123 40.34 2.87 201.0Surr: 1,2-Dichloroethane-d4
49.95 50 0 99.9 77 - 113 50.39 0.875 201.0Surr: 4-Bromofluorobenzene
40.8 50 0 81.6 73 - 126 41.83 2.48 201.0Surr: Dibromofluoromethane
46.64 50 0 93.3 81 - 120 45.83 1.75 201.0Surr: Toluene-d8
ALS Houston, US Date: 15-Feb-24
Page 11 of 18
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS24020476
QC BATCH REPORT
Batch ID:R458535 ( 0 )Instrument:VOA4 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS24020310-29MS Units:ug/L Analysis Date:09-Feb-2024 19:27
Run ID:VOA4_458535 SeqNo:7825590 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,2,4-Trimethylbenzene 18.98 20 0 94.9 70 - 1251.0
1,2-Dibromoethane 19.01 20 0 95.1 70 - 1241.0
1,2-Dichloroethane 20.74 20 0 104 70 - 1271.0
2-Methylnaphthalene 15.47 20 0 77.4 55 - 1401.0
4-Isopropyltoluene 19.18 20 0 95.9 70 - 1301.0
Benzene 18.2 20 0 91.0 70 - 1271.0
Chloroform 16.75 20 0 83.8 70 - 1251.0
Ethylbenzene 19.62 20 0 98.1 70 - 1241.0
m,p-Xylene 40.14 40 0 100 70 - 1302.0
Methyl tert-butyl ether 15.96 20 0 79.8 70 - 1301.0
Methylene chloride 16.66 20 0 83.3 70 - 1282.0
Naphthalene 17.55 20 0 87.8 70 - 1301.0
o-Xylene 19.49 20 0 97.5 70 - 1241.0
Tert-butyl alcohol 323.1 400 0 80.8 70 - 13010
Toluene 18.71 20 0 93.5 70 - 1231.0
Xylenes, Total 59.63 60 0 99.4 70 - 1303.0
40.25 50 0 80.5 70 - 1261.0Surr: 1,2-Dichloroethane-d4
51.05 50 0 102 77 - 1131.0Surr: 4-Bromofluorobenzene
41.18 50 0 82.4 77 - 1231.0Surr: Dibromofluoromethane
47.27 50 0 94.5 82 - 1271.0Surr: Toluene-d8
ALS Houston, US Date: 15-Feb-24
Page 12 of 18
Client:
Project:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
WorkOrder:HS24020476
QC BATCH REPORT
Batch ID:R458535 ( 0 )Instrument:VOA4 Method:LOW LEVEL VOLATILES BY SW8260C
Sample ID:HS24020310-29MSD Units:ug/L Analysis Date:09-Feb-2024 19:50
Run ID:VOA4_458535 SeqNo:7825591 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,2,4-Trimethylbenzene 18.59 20 0 93.0 70 - 125 18.98 2.06 201.0
1,2-Dibromoethane 18.91 20 0 94.5 70 - 124 19.01 0.564 201.0
1,2-Dichloroethane 19.75 20 0 98.7 70 - 127 20.74 4.93 201.0
2-Methylnaphthalene 15.38 20 0 76.9 55 - 140 15.47 0.614 201.0
4-Isopropyltoluene 18.39 20 0 91.9 70 - 130 19.18 4.24 201.0
Benzene 17.43 20 0 87.1 70 - 127 18.2 4.32 201.0
Chloroform 16.12 20 0 80.6 70 - 125 16.75 3.84 201.0
Ethylbenzene 18.4 20 0 92.0 70 - 124 19.62 6.43 201.0
m,p-Xylene 39.11 40 0 97.8 70 - 130 40.14 2.59 202.0
Methyl tert-butyl ether 15.77 20 0 78.9 70 - 130 15.96 1.15 201.0
Methylene chloride 15.13 20 0 75.7 70 - 128 16.66 9.61 202.0
Naphthalene 17.72 20 0 88.6 70 - 130 17.55 0.949 201.0
o-Xylene 18.8 20 0 94.0 70 - 124 19.49 3.63 201.0
Tert-butyl alcohol 322.9 400 0 80.7 70 - 130 323.1 0.0783 2010
Toluene 18.08 20 0 90.4 70 - 123 18.71 3.39 201.0
Xylenes, Total 57.91 60 0 96.5 70 - 130 59.63 2.93 203.0
40.1 50 0 80.2 70 - 126 40.25 0.368 201.0Surr: 1,2-Dichloroethane-d4
51.62 50 0 103 77 - 113 51.05 1.11 201.0Surr: 4-Bromofluorobenzene
42.51 50 0 85.0 77 - 123 41.18 3.17 201.0Surr: Dibromofluoromethane
46.66 50 0 93.3 82 - 127 47.27 1.29 201.0Surr: Toluene-d8
The following samples were analyzed in this batch:HS24020476-01 HS24020476-02
ALS Houston, US Date: 15-Feb-24
Page 13 of 18
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Groundwater & Environmental Service, Inc.
Former Greensboro Terminal
HS24020476
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
ALS Houston, US Date: 15-Feb-24
Page 14 of 18
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 88-00356 27-Mar-2024
California 2919; 2024 30-Apr-2024
Dept of Defense L23-358 31-May-2025
Florida E87611-38 30-Jun-2024
Illinois 2000322023-11 30-Jun-2024
Kansas E-10352 2023-2024 31-Jul-2024
Louisiana 03087 2023-2024 30-Jun-2024
Maryland 343; 2023-2024 30-Jun-2024
North Carolina 624 - 2024 31-Dec-2024
North Dakota R-193 2023-2024 30-Apr-2024
Oklahoma 2023-140 31-Aug-2024
Texas T104704231-23-32 30-Apr-2024
Utah TX026932023-14 31-Jul-2024
15-Feb-24Date: ALS Houston, US
Page 15 of 18
Jacob Coronado
03-Feb-2024 09:10Date/Time Received:HS24020476
GES Virginia
Work Order ID:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
3.7/3.6 31
Small blue
02/09/2024 12:30
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Completed By:/S/ RJ Modashia
Date/TimeeSignatureDate/TimeeSignature
09-Feb-2024 16:4809-Feb-2024 12:10
FedExWaterCarrier name:Matrices:
Reviewed by:/S/ luis.aguilar
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
VOA/TX1005/TX1006 Solids in hermetically sealed vials?
Samplers name present on COC?
1 Page(s)
COC IDs:273337
ALS Houston, US 15-Feb-24Date:
Page 16 of 18
Page 17 of 18
Page 18 of 18
Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendix G – Waste Documentation

Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendix H – Updated Well Permit List and May 7,
2024 Guilford County Email Correspondence

Comprehensive List of Monitoring and Recovery Wells
Included Under Permit
#143-96-MW115-RW23
RETIA USA
(Former TOTAL Site #1760)
Greensboro, North Carolina
AMW-8S FPZ-15 Z4-X68 PWM-J-B
AMW-9S OW-1 Z4-X70 PMW-K-I
AMW-10S OW-2 Z4-X72 PMW-K-D
AMW-11S OW-3
AMW-12S OW-4 Z4-PZ4
AMW-13S OW-6 Z4-PZ7
AMW-13I OW-7 Z4-PZ9
AMW-13D OW-8
AMW-16S SBMW-2I MW-B-D
AMW-17S SBMW-2R MW-B-B
AMW-18S Z1-X1 MW-C-I
DEM-MW-6R Z1-X25 MW-C-D PMW-O-D
DEM-MW-6I Z1-X27 MW-C-B PMW-O-B
FMW-22 Z2-X20 MW-E-D PMW-Q-S
FMW-23R Z2-X29 MW-E-B PMW-Q-I
FMW-24 Z2-X31 MW-F-I PMW-Q-D
FMW-24I Z2-X35 MW-F-D PMW-Q-B
FMW-24D Z2-PZ-6 MW-F-B PMWR-S
FPZ-6 Z2-PZ-9 MW-G-D PMW-R-D
FPZ-8 MW-H-I
FPZ-10 Z3-X82 MW-H-D
FPZ-10I Z4-X21 MW-H-B
FPZ-11 MW-I-I
FPZ-12
FPZ-12I Z4-X47 MW-I-B
Existing Wells
GES - May 2024 Page 1 of 1 RETIA USA (TOTAL #1760)
1
Daniel Breckenridge
From:Daniel Breckenridge
Sent:Wednesday, May 15, 2024 2:23 PM
To:Daniel Breckenridge
Subject:FW: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

From: Gene Mao <[e-mail]>
Sent: Tuesday, May 7, 2024 8:25 AM
To: Daniel Breckenridge <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

Stop – Look – Think – Decide: This e-mail came from outside of GES. Adhere to the guidelines of our ongoing GES
cybersecurity awareness and training presentations. Be Aware – Be Smart

Danny,

Forward the information for permit update.

Thanks.

Gene Mao

Hydrogeologist
Public Health

Guilford County Government
400 West Market Street, Greensboro, NC 27401
336-641-3589 | m: 336-451-7638 | f: 336-641-4812

[e-mail] | www.guilfordcountync.gov

From: Daniel Breckenridge <[e-mail]>
Sent: Tuesday, May 7, 2024 8:14 AM
To: Gene Mao <[e-mail]>
Cc: Vincent SWADIS <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

*WARNING* This email originated outside Guilford County's email system.
*WARNING*
Do not click unrecognized links or attachments. When in doubt, use the Phish Alert
Report button.
Gene, I just noticed the recipient information is incorrect. Can you please update to:

2
Vincent Swadis
Portfolio Manager
RETIA USA, Legacy Site Services LLC
TotalEnergies Petrochemical & Refining USA, Inc.

Office: [phone]
Cell: [phone]
[e-mail]

Thank you,
Danny

Daniel Breckenridge
Principal Project Manager

Office: 866-222-7786 ext. 4094
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
571 Southlake Boulevard
Richmond, VA 23236

Follow Us: Website | LinkedIn | Twitter

Safety: Plan, Prevent, Protect

From: Daniel Breckenridge
Sent: Tuesday, May 7, 2024 8:09 AM
To: 'Gene Mao' <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

Thank you very much Gene.

Danny

Daniel Breckenridge
Principal Project Manager

3
Office: 866-222-7786 ext. 4094
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
571 Southlake Boulevard
Richmond, VA 23236

Follow Us: Website | LinkedIn | Twitter

Safety: Plan, Prevent, Protect

From: Gene Mao <[e-mail]>
Sent: Monday, May 6, 2024 9:57 PM
To: Daniel Breckenridge <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

Stop – Look – Think – Decide: This e-mail came from outside of GES. Adhere to the guidelines of our ongoing GES
cybersecurity awareness and training presentations. Be Aware – Be Smart
Dan,

See the attached amended permit.

If you have questions, please let me know.

Thank you.

Gene Mao

Hydrogeologist
Public Health

Guilford County Government
400 West Market Street, Greensboro, NC 27401
336-641-3589 | m: 336-451-7638 | f: 336-641-4812

[e-mail] | www.guilfordcountync.gov

From: Daniel Breckenridge <[e-mail]>
Sent: Monday, May 6, 2024 3:56 PM
To: Gene Mao <[e-mail]>
Cc: Vincent SWADIS <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

4
*WARNING* This email originated outside Guilford County's email system.
*WARNING*
Do not click unrecognized links or attachments. When in doubt, use the Phish Alert
Report button.
Thanks again very much Gene. Have a great afternoon.

Danny

Daniel Breckenridge
Principal Project Manager

Office: 866-222-7786 ext. 4094
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
571 Southlake Boulevard
Richmond, VA 23236

Follow Us: Website | LinkedIn | Twitter

Safety: Plan, Prevent, Protect

From: Gene Mao <[e-mail]>
Sent: Monday, May 6, 2024 3:55 PM
To: Daniel Breckenridge <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

Stop – Look – Think – Decide: This e-mail came from outside of GES. Adhere to the guidelines of our ongoing GES
cybersecurity awareness and training presentations. Be Aware – Be Smart
Thanks.

I will send the records to the MW manager for amendment. I will follow up to make sure and
let you know.

Thank you.

Gene Mao

Hydrogeologist
Public Health

5

Guilford County Government
400 West Market Street, Greensboro, NC 27401
336-641-3589 | m: 336-451-7638 | f: 336-641-4812

[e-mail] | www.guilfordcountync.gov

From: Daniel Breckenridge <[e-mail]>
Sent: Monday, May 6, 2024 3:52 PM
To: Gene Mao <[e-mail]>
Cc: Vincent SWADIS <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

*WARNING* This email originated outside Guilford County's email system.
*WARNING*
Do not click unrecognized links or attachments. When in doubt, use the Phish Alert
Report button.
Gene, please see attached.

Thanks,
Danny

Daniel Breckenridge
Principal Project Manager

Office: 866-222-7786 ext. 4094
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
571 Southlake Boulevard
Richmond, VA 23236

Follow Us: Website | LinkedIn | Twitter

Safety: Plan, Prevent, Protect

From: Gene Mao <[e-mail]>
Sent: Monday, May 6, 2024 3:48 PM
To: Daniel Breckenridge <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

Stop – Look – Think – Decide: This e-mail came from outside of GES. Adhere to the guidelines of our ongoing GES
cybersecurity awareness and training presentations. Be Aware – Be Smart
6
Danny,

Can you email me the well abandonment records again?

Thank you.

Gene Mao

Hydrogeologist
Public Health

Guilford County Government
400 West Market Street, Greensboro, NC 27401
336-641-3589 | m: 336-451-7638 | f: 336-641-4812

[e-mail] | www.guilfordcountync.gov

From: Daniel Breckenridge <[e-mail]>
Sent: Monday, May 6, 2024 3:43 PM
To: Gene Mao <[e-mail]>
Cc: Vincent SWADIS <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

*WARNING* This email originated outside Guilford County's email system.
*WARNING*
Do not click unrecognized links or attachments. When in doubt, use the Phish Alert
Report button.
Thanks Gene. It should be:

 115 monitoring wells
 21 recovery wells (amended from 23 with recent abandonment of RW-1 and RW-2)

Thank you,
Danny

Daniel Breckenridge
Principal Project Manager

7
Office: 866-222-7786 ext. 4094
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
571 Southlake Boulevard
Richmond, VA 23236

Follow Us: Website | LinkedIn | Twitter

Safety: Plan, Prevent, Protect

From: Gene Mao <[e-mail]>
Sent: Monday, May 6, 2024 3:29 PM
To: Daniel Breckenridge <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

Stop – Look – Think – Decide: This e-mail came from outside of GES. Adhere to the guidelines of our ongoing GES
cybersecurity awareness and training presentations. Be Aware – Be Smart
Danny,

I just check the current well numbers in the permit. You have 115 monitoring wells and
23recovery wells.

Can you check if these numbers are correct?

Thank you.

Gene Mao

Hydrogeologist
Public Health

Guilford County Government
400 West Market Street, Greensboro, NC 27401
336-641-3589 | m: 336-451-7638 | f: 336-641-4812

[e-mail] | www.guilfordcountync.gov

From: Daniel Breckenridge <[e-mail]>
Sent: Monday, May 6, 2024 3:14 PM
To: Gene Mao <[e-mail]>
Cc: Vincent SWADIS <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

8
*WARNING* This email originated outside Guilford County's email system.
*WARNING*
Do not click unrecognized links or attachments. When in doubt, use the Phish Alert
Report button.
Good afternoon Gene, following-up on the below. Has the Monitoring Well Construction Permit been amended to
reduce the number of permitted wells?

If you need anything, please advise.

Thank you,
Danny

Daniel Breckenridge
Principal Project Manager

Office: 866-222-7786 ext. 4094
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
571 Southlake Boulevard
Richmond, VA 23236

Follow Us: Website | LinkedIn | Twitter

Safety: Plan, Prevent, Protect

From: Gene Mao <[e-mail]>
Sent: Friday, March 1, 2024 8:00 AM
To: Daniel Breckenridge <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

Stop – Look – Think – Decide: This e-mail came from outside of GES. Adhere to the guidelines of our ongoing GES
cybersecurity awareness and training presentations. Be Aware – Be Smart
Thanks, Danny.

I will let the MW manager to subtract these 2 wells from the permit.

Gene Mao

Hydrogeologist
Public Health

9

Guilford County Government
400 West Market Street, Greensboro, NC 27401
336-641-3589 | m: 336-451-7638 | f: 336-641-4812

[e-mail] | www.guilfordcountync.gov

From: Daniel Breckenridge <[e-mail]>
Sent: Wednesday, February 28, 2024 2:18 PM
To: Gene Mao <[e-mail]>
Cc: Vincent SWADIS <[e-mail]>; Daniel Breckenridge <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

*WARNING* This email originated outside Guilford County's email system.
*WARNING*
Do not click unrecognized links or attachments. When in doubt, use the Phish Alert
Report button.
Good afternoon Gene –

Per the below, two former recovery wells (RW-1 and RW-2) were abandoned earlier this month at the Former
Greensboro Terminal #1760 (Incident #5067).

Attached are the Well Abandonment Records.

If you need anything else at this time, please advise.

Thanks,
Danny

Daniel Breckenridge
Senior Project Manager

Office: 866-222-7786 ext. 4094
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
571 Southlake Boulevard
Richmond, VA 23236

Follow Us: Website | LinkedIn | Twitter

Safety: Plan, Prevent, Protect

10
From: Gene Mao <[e-mail]>
Sent: Monday, November 27, 2023 11:37 AM
To: Daniel Breckenridge <[e-mail]>
Subject: RE: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

Stop – Look – Think – Decide: This e-mail came from outside of GES. Adhere to the guidelines of our ongoing GES
cybersecurity awareness and training presentations. Be Aware – Be Smart
Danny,

Based on the information you provide, your request for abandoning RW-1 and RW-2 is
approved. Please submit a well abandonment report for us to amend the permit..

Thank you,

Gene Mao

Hydrogeologist
Public Health

Guilford County Government
400 West Market Street, Greensboro, NC 27401
336-641-3589 | m: 336-451-7638 | f: 336-641-4812

[e-mail] | www.guilfordcountync.gov

From: Daniel Breckenridge <[e-mail]>
Sent: Monday, November 27, 2023 11:25 AM
To: Gene Mao <[e-mail]>
Cc: Vincent SWADIS <[e-mail]>; Daniel Breckenridge <[e-mail]>
Subject: Former Greensboro Terminal Incident #5067 - Proposed Well Abandonment

*WARNING* This email originated outside Guilford County's email system.
*WARNING*
Do not click unrecognized links or attachments. When in doubt, use the Phish Alert
Report button.
Good morning Gene –

Thanks very much for your response to my voicemail about the Former Greensboro Terminal #5067. Attached is a Site
Map showing the two wells we proposed to abandon (highlighted yellow). I’ve also included a snippet from the Site
Map showing those locations (see below).

These two former recovery wells (RW-1 and RW-2) have been monitored since July 1997, since the installation of the
barrier wall. Historically in RW-1, no product has been detected. In RW-2, product was only detected between
November 1997 and January 2004. Additionally, these two wells have been sampled since October 2015 and all
contaminants of concern have been non-detect.

These former recovery wells no longer provide value to the long-term goals of the project.
11

Upon approval, we will abandon these two former recovery wells and provide notification once complete.

If you need anything else at this time, please let me know.

Thanks,
Danny

Daniel Breckenridge
Senior Project Manager

12
Office: 866-222-7786 ext. 4094
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
571 Southlake Boulevard
Richmond, VA 23236

Follow Us: Website | LinkedIn | Twitter

Safety: Plan, Prevent, Protect

Confidentiality Notice: This transmission (including any attachments) may contain confidential information belonging to
Groundwater & Environmental Services, Inc. and is intended only for the use of the party or entity to which it is
addressed. If you are not the intended recipient, you are hereby notified that any disclosure, copying, distribution,
retention or the taking of action in reliance on the contents of this transmission is strictly prohibited; provided, however,
the prohibition against disclosure shall not apply if the transmission is required by law to be disclosed by a governmental
intended party as a public record. If you have received this transmission in error, please immediately notify the sender
and erase all information and attachments. Thank You.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email before responding,
and use caution when clicking on links or opening attachments. If it appears suspicious, please report it or delete it
immediately.

Confidentiality Notice: This transmission (including any attachments) may contain confidential information
belonging to Groundwater & Environmental Services, Inc. and is intended only for the use of the party or
entity to which it is addressed. If you are not the intended recipient, you are hereby notified that any
disclosure, copying, distribution, retention or the taking of action in reliance on the contents of this
transmission is strictly prohibited; provided, however, the prohibition against disclosure shall not apply if the
transmission is required by law to be disclosed by a governmental intended party as a public record. If you
have received this transmission in error, please immediately notify the sender and erase all information and
attachments. Thank You.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email before responding,
and use caution when clicking on links or opening attachments. If it appears suspicious, please report it or delete it
immediately.

Confidentiality Notice: This transmission (including any attachments) may contain confidential information
belonging to Groundwater & Environmental Services, Inc. and is intended only for the use of the party or
entity to which it is addressed. If you are not the intended recipient, you are hereby notified that any
disclosure, copying, distribution, retention or the taking of action in reliance on the contents of this
transmission is strictly prohibited; provided, however, the prohibition against disclosure shall not apply if the
transmission is required by law to be disclosed by a governmental intended party as a public record. If you
have received this transmission in error, please immediately notify the sender and erase all information and
attachments. Thank You.
13

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email before responding,
and use caution when clicking on links or opening attachments. If it appears suspicious, please report it or delete it
immediately.

Confidentiality Notice: This transmission (including any attachments) may contain confidential information
belonging to Groundwater & Environmental Services, Inc. and is intended only for the use of the party or
entity to which it is addressed. If you are not the intended recipient, you are hereby notified that any
disclosure, copying, distribution, retention or the taking of action in reliance on the contents of this
transmission is strictly prohibited; provided, however, the prohibition against disclosure shall not apply if the
transmission is required by law to be disclosed by a governmental intended party as a public record. If you
have received this transmission in error, please immediately notify the sender and erase all information and
attachments. Thank You.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email before responding,
and use caution when clicking on links or opening attachments. If it appears suspicious, please report it or delete it
immediately.

Confidentiality Notice: This transmission (including any attachments) may contain confidential information
belonging to Groundwater & Environmental Services, Inc. and is intended only for the use of the party or
entity to which it is addressed. If you are not the intended recipient, you are hereby notified that any
disclosure, copying, distribution, retention or the taking of action in reliance on the contents of this
transmission is strictly prohibited; provided, however, the prohibition against disclosure shall not apply if the
transmission is required by law to be disclosed by a governmental intended party as a public record. If you
have received this transmission in error, please immediately notify the sender and erase all information and
attachments. Thank You.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email before responding,
and use caution when clicking on links or opening attachments. If it appears suspicious, please report it or delete it
immediately.

Confidentiality Notice: This transmission (including any attachments) may contain confidential information
belonging to Groundwater & Environmental Services, Inc. and is intended only for the use of the party or
entity to which it is addressed. If you are not the intended recipient, you are hereby notified that any
disclosure, copying, distribution, retention or the taking of action in reliance on the contents of this
transmission is strictly prohibited; provided, however, the prohibition against disclosure shall not apply if the
transmission is required by law to be disclosed by a governmental intended party as a public record. If you
have received this transmission in error, please immediately notify the sender and erase all information and
attachments. Thank You.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email before responding,
and use caution when clicking on links or opening attachments. If it appears suspicious, please report it or delete it
immediately.

Confidentiality Notice: This transmission (including any attachments) may contain confidential information
belonging to Groundwater & Environmental Services, Inc. and is intended only for the use of the party or
14
entity to which it is addressed. If you are not the intended recipient, you are hereby notified that any
disclosure, copying, distribution, retention or the taking of action in reliance on the contents of this
transmission is strictly prohibited; provided, however, the prohibition against disclosure shall not apply if the
transmission is required by law to be disclosed by a governmental intended party as a public record. If you
have received this transmission in error, please immediately notify the sender and erase all information and
attachments. Thank You.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email before responding,
and use caution when clicking on links or opening attachments. If it appears suspicious, please report it or delete it
immediately.

Confidentiality Notice: This transmission (including any attachments) may contain confidential information
belonging to Groundwater & Environmental Services, Inc. and is intended only for the use of the party or
entity to which it is addressed. If you are not the intended recipient, you are hereby notified that any
disclosure, copying, distribution, retention or the taking of action in reliance on the contents of this
transmission is strictly prohibited; provided, however, the prohibition against disclosure shall not apply if the
transmission is required by law to be disclosed by a governmental intended party as a public record. If you
have received this transmission in error, please immediately notify the sender and erase all information and
attachments. Thank You.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email before responding,
and use caution when clicking on links or opening attachments. If it appears suspicious, please report it or delete it
immediately.
Annual Monitoring Report
Former Greensboro Terminal #1760
7115 West Market Street
Greensboro, North Carolina 27409

Appendix I – Barrier Wall Well Gauging Data Graphs

Monthly Precipitation Time Trend
TotalEnergies Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
0
2
4
6
8
10
12
14
-1
9
8
8
-1
9
8
9
-1
9
9
0
-1
9
9
1
-1
9
9
2
-1
9
9
3
-1
9
9
4
-1
9
9
5
-1
9
9
6
-1
9
9
7
-1
9
9
8
-1
9
9
9
-2
0
0
0
-2
0
0
1
-2
0
0
2
-2
0
0
3
-2
0
0
4
-2
0
0
5
-2
0
0
6
-2
0
0
7
-2
0
0
8
-2
0
0
9
-2
0
1
0
-2
0
1
1
-2
0
1
2
-2
0
1
3
-2
0
1
4
-2
0
1
5
-2
0
1
6
-2
0
1
7
-2
0
1
8
-2
0
1
9
-2
0
2
0
-2
0
2
1
-2
0
2
2
-2
0
2
3
-2
0
2
4
Mo
n
t
h
l
y

P
r
e
c
i
p
i
t
a
t
i
o
n

(
i
n
c
h
e
s
)
Date
Groundwater Elevation and Monthly Precipitation Time Trend
TotalEnergies Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
0.0
2.0
4.0
6.0
8.0
10.0
12.0
862
867
872
877
882
887
Ma
r
c
h
-
1
4
Ju
n
e
-
1
4
Ma
y
-
1
5
Ap
r
i
l
-
1
6
Au
g
u
s
t
-
1
6
Ma
r
c
h
-
1
7
Ju
l
y
-
1
7
Ma
y
-
1
8
Ap
r
i
l
-
1
9
Au
g
u
s
t
-
1
9
Ma
r
c
h
-
2
0
Ju
l
y
-
2
0
Ju
n
e
-
2
1
Ap
r
i
l
-
2
2
Au
g
u
s
t
-
2
2
Ma
r
c
h
-
2
3
Ju
l
y
-
2
3
Ju
n
e
-
2
4
Mo
n
t
h
l
y

P
r
e
c
i
p
i
t
a
t
i
o
n

(
i
n
)
Gr
o
u
n
d
w
a
t
e
r

E
l
e
v
a
t
i
o
n

(
f
t
)
Date
Groundwater Elevation and LNAPL Elevation Time Trend for FPZ-10
TotalEnergies Petrochemicals Refining USA, Inc.
Facility #1760
Greensboro, North Carolina
866.00
868.00
870.00
872.00
874.00
876.00
878.00
May-97 November-02 May-08 October-13 April-19 October-24
Gr
o
u
n
d
w
a
t
e
r

E
l
e
v
a
t
i
o
n

(
f
t
)
LNAPL Elevation Groundwater Elevation