DC410064_20240708_Prioritization Assessment Report

AECOM
5438 Wade Park Boulevard, Suite 200
Raleigh, NC 27607

T: 919.461.1100
aecom.com

July 8, 2024

North Carolina Department of Environmental Quality
Division of Waste Management – DSCA Program
1646 Mail Service Center
Raleigh, NC 27699-1646

Attn: Ms. Ariana Rivera
DSCA Project Manager

Re: Prioritization Assessment Report
Frye & Webster Cleaners, DSCA Site ID DC410064
608 Elwell Avenue
Greensboro, Guilford County, North Carolina

Dear Ms. Rivera:

AECOM Technical Services of North Carolina, Inc. (AECOM) is pleased to provide the attached Prioritization
Assessment Report for Frye & Webster Cleaners (site) located at 608 Elwell Avenue in Greensboro, Guilford
County, North Carolina.

Frye & Webster Cleaners is an active dry-cleaner that operated using petroleum solvents from approximately 1955
through 1995, using chlorinated solvents from 1995 through 2015, and currently uses a water-based dry-cleaning
technique. The building is split into the active dry-cleaner on the northern half and a vacant southern half which
has been used for storage by the dry-cleaner at times. A general site location map is included as Figure 1, and a
site map with facility layout is included as Figure 2. The immediate surrounding land use is designated as
commercial mixed use as shown on Figure 3. Land use to the north is residential and recreational, and east, south,
and west along Elwell Avenue land use is largely commercial.

1.0 Site History

Based on data obtained from the DSCA Program, Guilford County GIS, and the Limited Soil & Groundwater
Assessment report prepared by Pyramid Environmental & Engineering, P.C. (Pyramid) dated November 1, 2021
(Pyramid, 2021), the site building (located at 608 and 606 Elwell Avenue) was constructed in 1940 and has
operated as a dry-cleaner since at least 1955. The site operated as a petroleum solvent dry-cleaner from at least
1955 through 1995, using an unknown petroleum-based dry-cleaning fluid. In 1995, the petroleum solvent machine
was replaced with a tetrachloroethylene (PCE) dry-cleaning machine which was located near the back of the
building. The approximate locations of the dry-cleaning machines present in 608 Elwell Avenue over time are
shown in Figure 2. In 2015, a new water-based MIELE® Machine was installed. According to a DSCA Compliance
Inspection Memo dated August 24, 2018, use of the PCE machine was discontinued at the site in January 2017,
and the inspector verified that the PCE dry-cleaning machine was disconnected from a power source, no solvent
was left inside the solvent tanks, that no solvent or solvent waste was stored on site, and the last waste pickup
occurred on March 30, 2018, at which time Safety Kleen picked up 500 pounds of liquid waste. The actual date
that the PCE machine was removed from the building was not documented. While the section of the building listed
as 606 Elwell Avenue has never been used as an operational part of the dry-cleaner, it has been utilized for storage
by the dry cleaner, and an unmarked 55-gallon drum, presumed to contain PCE solvent, was present in the 606
Elwell Avenue tenant space until removal by the dry-cleaning business owner in May 2024.

Based on the investigation completed in 2021 by Pyramid, samples from soil boring (SB-2) near the location of the
former PCE machine indicated concentrations of PCE in exceedance of the North Carolina Protection of

Frye & Webster Cleaners
DSCA Site ID DC410064
Page 2 of 7

Groundwater Preliminary Soil Remediation Goal (PSRG), and groundwater samples collected from two temporary
monitoring wells (TW-1 and TW-2) indicated exceedances of PCE above the North Carolina Department of
Environmental Quality (NCDEQ) 15A NCAC 2L Standard (2L Standard) for groundwater (Pyramid, 2021).
Concentrations of trichloroethylene (TCE), cis-1,2-dichloroethylene (cis-1,2-DCE), and vinyl chloride above the 2L
Standard were also detected in groundwater samples collected from TW-2. The locations of the historic soil borings
are shown on Figure 4 and locations of temporary monitoring wells are shown on Figure 5.

2.0 Surrounding Land Use

AECOM reviewed available zoning and land use information for the site and surrounding area from the City of
Greensboro’s GIS website:
https://greensboro.maps.arcgis.com/apps/webappviewer/index.html?id=3abbd307081d4cbdb7b1c4c56437c404.

The site/subject property is currently zoned for commercial medium use (C-M) and designated for commercial land
use by the City of Greensboro. Most of the immediately surrounding properties (adjacent to the site) to the east
and south are also C-M properties designated for commercial use. North and west of the site are generally zoned
for residential single-family or multi-family use. Further east from the site is primarily public and institutional land.
The land use designations for the site and surrounding properties are presented on Figure 3.

3.0 Soil Quality Assessment Activities

In January 2024, AECOM initiated soil assessment activities to determine the extent of soil contamination above
PSRG onsite. AECOM collected soil samples from nine soil borings (SB-3 through SB-11) located in areas where
dry-cleaning impacts were likely to be present based on the location of general dry-cleaning operations as shown
on Figure 4.

- Soil borings SB-3 and SB-4 were located adjacent to the historical locations of dry-cleaning machines.
- Soil borings SB-5 and SB-6 were located behind the building near the PCE machine vent pipe.
- Soil borings SB-7 and SB-8 were located in the alleyway between 608 Elwell Avenue and the neighboring
building located at 610 Elwell Avenue.
- Soil borings SB-9 and SB-11 were located west of the building outside the front, and SB-10 was located
near the bay doors at the adjacent 606 Elwell Avenue tenant space where drums of solvent may have
been loaded/unloaded.

Each shallow soil boring was completed using a hand auger advanced to a depth of at least five feet below ground
surface (ft bgs) and screened in one-foot intervals for head space readings for volatile organic compounds (VOCs)
using a photoionization detector (PID). Per the attached Standard Operating Procedure (SOP), included as
Appendix A, two soil samples were collected at each borehole: one surficial soil sample from ground surface to
one foot depth, and one sample from the one- to five-foot intervals which exhibited the highest PID reading (not
including the sample collected from ground surface to one foot depth). Soil samples were submitted to Pace
Analytical Laboratories, Inc. (Pace) for analysis of volatile organic compounds (VOC) by United States
Environmental Protection Agency (EPA) Method SW-846 8260D. Analytical results indicated that one or both
samples from soil borings SB-3, SB-5, SB-6, SB-7, and SB-10 exhibited PCE concentrations that exceeded the
PSRG of 0.0063 milligrams per kilogram (mg/kg). The surficial sample at SB-3 also contained TCE concentrations
that exceeded the PSRG of 0.021 mg/kg.

Soil impacts appear to be delineated on the western portion of the site, as illustrated on Figure 4. Additional soil
assessment will be necessary to the north, east and south to delineate impacts to the protection of groundwater
PSRG.

Analytical results are tabulated in Table 2. Soil boring logs are included in Appendix B and laboratory analytical
reports are included in Appendix C.

Frye & Webster Cleaners
DSCA Site ID DC410064
Page 3 of 7

4.0 Groundwater Quality Assessment Activities

Monitoring Well Installation

To further evaluate groundwater quality at the site, AECOM oversaw the installation of four monitoring wells (MW-
1 through MW-4) by Geologic Exploration, Inc. in January 2024.

- Monitoring well MW-1 was installed on the northwestern corner of the property.
- Monitoring well MW-2 was installed on the southwest corner of the shared parking lot for the area
businesses.
- Monitoring well MW-3 was installed on the southeast corner of the shared parking lot.
- Monitoring well MW-4 was installed on the northeast corner of the property.

The locations of the monitoring wells are indicated on Figure 5. The monitoring wells were surveyed for top of
casing elevation and coordinates during the February 2024 groundwater sampling event using a hand-held GPS
unit (VRS). Monitoring well construction data are summarized on Table 6, and monitoring well construction logs
are included in Appendix D.

Groundwater Sampling and Results

On February 9, 2024, AECOM gauged the depth to water in monitoring wells MW-1 through MW-4 and conducted
a comprehensive groundwater sampling event. As shown on Figure 6, groundwater flow is generally toward the
north. Groundwater gauging elevation data is tabulated on Table 7.

Groundwater samples were collected using low-flow groundwater sampling methods as described in the Low-Flow
Minimal Drawdown Sampling SOP provided in Appendix A. Groundwater samples collected from the newly
installed monitoring wells were submitted to Pace for analysis for VOCs by USEPA Method SW-846 8260D.
Groundwater sampling forms are included in Appendix E.

Analytical results indicated PCE concentrations of 1.60 micrograms per liter (µg/l) in monitoring well MW-1 and
63.3 µg/l in monitoring well MW-4, both of which exceed the 2L Standard of 0.7 µg/l. TCE was also detected above
the 2L Standard in monitoring wells MW-2 and MW-4. Benzene concentrations above the 2L Standard were
detected in samples collected from each site monitoring well (MW-1 through MW-4). Several other VOCs were
found above their respective 2L Standards in MW-1, MW-2, and MW-4, including cis-1,2-DCE, vinyl chloride, 1,2-
dichloroethane, methyl tert-butyl ether (MTBE), naphthalene, 1,1,2-trichloroethane, 1,2-dichloropropane, and di-
isopropyl ether. As indicated on Figure 5, the adjacent property to the south, 3201 E Bessemer Ave, is an active
underground storage tank (UST) facility (Higgin’s Curb Market; Facility ID: 00-0-0000009969) with multiple Notice
of Violation letters from the Division of Waste Management (DWM) since 2019. Based on the proximity of the UST
site, the direction of groundwater flow, and the configuration and magnitude of petroleum impacts, it is likely that
detections of petroleum-related compounds such as benzene, MTBE, and naphthalene in groundwater samples
collected from site wells originated from offsite. Groundwater sampling results from the February 2024 event are
summarized on Figure 5. The extent of groundwater impacts has not been fully delineated.

Groundwater sampling data are summarized in Table 8 and field parameter data are summarized on Table 12.
Laboratory analytical reports are included in Appendix C.

Frye & Webster Cleaners
DSCA Site ID DC410064
Page 4 of 7

DSCA groundwater to indoor air vapor intrusion risk calculators are included in Appendix F and summarized
below:

Sample ID Sample Date
Cumulative Risk:
Resident Non-Residential Worker
CR HI CR HI
MW-1 2/9/2024 3.6E-04 4.3E+00 8.2E-05 1.0E+00
MW-2 2/9/2024 3.7E-03 4.4E+01 8.5E-04 1.1E+01
MW-3 2/9/2024 1.4E-06 1.7E-02 3.3E-07 4.0E-03
MW-4 2/9/2024 6.7E-05 1.3E+01 1.1E-05 3.1E+00
CR = Calculated cumulative carcinogenic risk; acceptable calculated risk values are less than 1E-04; unacceptable calculated risk values
are greater than 1E-04.
HI = Calculated non-carcinogenic hazard quotient; acceptable hazard index values are less than 1.0; unacceptable hazard index values are
greater than 1.0.
5.0 Sub-Slab Vapor and Soil Gas Quality Assessment Activities

In January and February 2024, AECOM collected soil gas samples from eleven temporary soil gas monitoring
points (SG-1 through SG-11) to evaluate potential vapor intrusion risk around the building and near areas with a
higher likelihood of contamination from the former dry-cleaning operations. The locations of soil gas samples SG-
1 through SG-6 and SG-9 through SG-11 are indicated on Figure 6. The soil gas sample implants were installed
at approximately five ft bgs using a decontaminated hand auger in accordance with the attached SOP (Appendix
A). The vapor samples were submitted to Enthalpy Analytical (Enthalpy) for analysis by EPA Method TO-15 of a
site-specific list of compounds including PCE, TCE, cis-1,2-DCE, trans-1,2-DCE, and vinyl chloride, as well as
compounds detected in soil samples at concentrations greater than the PSRG, and/or in groundwater at
concentrations which represent a hazard quotient ≥ 0.1 or carcinogenic risk ≥ 1E-06 when entered in the DSCA
Groundwater to Indoor Air Risk Calculator, in accordance with DSCA Contractor Bulletin # 32 - Determination of
COCs for VI Investigations, dated June 25, 2018. Laboratory analytical results are summarized on Figure 7. Soil
gas sampling forms are included with the SOP in Appendix A. Soil gas sample SG-8 was not collected due to
shallow saturated soil conditions, likely caused by poor drainage from a building rain gutter present near the
sampling area. Soil gas sample SG-7 was collected and held by the laboratory for analysis after review of soil
analytical results but could not be analyzed due to laboratory error.

As indicated on Figure 7, soil gas samples SG-1 and SG-11 exceeded acceptable calculated vapor intrusion risk
for both residential and non-residential worker exposure. Soil gas samples SG-2, SG-3, SG-4, SG-5, and SG-10
exceeded acceptable calculated vapor intrusion risk for residential exposure but did not exceed acceptable
calculated risk for non-residential worker exposure. Soil gas samples SG-6 and SG-9 contained concentrations of
PCE and other VOCs above the laboratory reporting limit but below calculated risk levels for residential and non-
residential worker exposure. DSCA Risk Calculators are included in Appendix F and summarized below:

Frye & Webster Cleaners
DSCA Site ID DC410064
Page 5 of 7

Sample ID Sample Date
Cumulative Risk:
Resident Non-Residential Worker
CR HI CR HI
SG-1 1/31/2024 1.1E-02 2.4E+03 7.3E-04 1.9E+02
SG-2 1/31/2024 4.6E-06 1.4E+00 3.4E-07 1.1E-01
SG-3 1/31/2024 4.1E-05 1.0E+01 3.0E-06 8.3E-01
SG-4 2/1/2024 6.4E-06 8.2E+00 4.8E-07 6.5E-01
SG-5 1/29/2024 2.0E-05 5.5E+00 1.3E-06 4.4E-01
SG-6 2/1/2024 5.7E-07 9.7E-02 4.4E-08 7.7E-03
SG-9 1/31/2024 5.4E-06 2.4E-01 4.1E-07 1.9E-02
SG-10 1/31/2024 5.2E-06 1.3E+00 3.9E-07 1.1E-01
SG-11 1/31/2024 2.5E-02 4.8E+03 1.6E-03 3.8E+02
CR = Calculated cumulative carcinogenic risk; acceptable calculated risk values are less than 1E-04; unacceptable calculated risk values are
greater than 1E-04.
HI = Calculated non-carcinogenic hazard quotient; acceptable hazard index values are less than 1.0; unacceptable hazard index values are
greater than 1.0.

Laboratory analytical reports are included in Appendix C. Soil gas analytical data collected to date are summarized
in Table 4 and presented on Figure 7. As indicated on Figure 7, areas of soil gas contaminant concentrations
exceeding acceptable calculated risk for residential exposure have been delineated at the northwest corner of the
site, and areas of soil gas contaminant concentrations that exceed acceptable risk for non-residential exposure
have been sufficiently delineated to the north, east, and west of the site building.

6.0 Indoor Air Quality Assessment Activities

On March 15, 2024, AECOM collected one indoor air sample to assess the air quality inside the dry-cleaning facility
located in the 608 Elwell Avenue side of the building. An indoor air sample was not collected from the 606 Elwell
Avenue side of the building as that side is unoccupied and not in condition typical of occupancy. The location of
indoor air sample IA-1 is indicated on Figure 7. A stainless-steel summa canister with an eight-hour flow regulator
was placed inside the facility, in accordance with the attached SOP (Appendix A). The indoor air sample was
submitted to Enthalpy Analytical (Enthalpy) for analysis by EPA Method TO-15 of a site-specific list of VOC
compounds including PCE, TCE, cis-1,2-DCE, trans-1,2-DCE, and vinyl chloride, as well as compounds detected
in soil samples at concentrations greater than the PSRG, and/or in groundwater at concentrations which represent
a hazard quotient ≥ 0.1 or carcinogenic risk ≥ 1E-06 when entered in the DSCA Groundwater to Indoor Air Risk
Calculator, in accordance with DSCA Contractor Bulletin # 32 - Determination of COCs for VI Investigations, dated
June 25, 2018. Laboratory analytical results are summarized on Figure 7. The indoor air building survey form is
included with the SOP in Appendix A.

As indicated on Figure 7, indoor air sample IA-1 contained concentrations of several analytes above the laboratory
reporting limit (PCE, benzene, ethylbenzene, xylenes, chloroform, and 1,2,4-trimethylbenzene) but did not exceed
acceptable calculated vapor intrusion risk for either residential or non-residential worker exposure. DSCA Risk
Calculators are included in Appendix F and summarized below:

Frye & Webster Cleaners
DSCA Site ID DC410064
Page 6 of 7

Sample ID Sample Date
Cumulative Risk:
Resident Non-Residential Worker
CR HI CR HI
IA-1 3/15/2024 7.0E-06 1.1E-01 1.6E-06 2.7E-02
CR = Calculated cumulative carcinogenic risk; acceptable calculated risk values are less than 1E-04.
HI = Calculated non-carcinogenic hazard quotient; acceptable hazard index values are less than 1.0.

Laboratory analytical reports are included in Appendix C. March 2024 indoor air analytical data are summarized
in Table 5 and presented on Figure 7. As indicated on Figure 7, no indoor air contamination has been found
above acceptable limits.

7.0 Site Geology and Hydrogeology

According to the 1985 North Carolina Geological Map, the site is underlain by late Proterozoic to late Cambrian
metamorphosed granitic rock. Soil types encountered during the subsurface investigations completed at the site
include red-yellow to brown silty CLAY (CL), described on the United States Department of Agriculture (USDA)
Web Soil Survey website (https://websoilsurvey.nrcs.usda.gov/app/WebSoilSurvey.aspx) as Vance-Urban land
complex soil.

The uppermost aquifer, in which the site monitoring wells are screened, is classified as an unconfined surficial
aquifer, and depth to groundwater ranges from 10.99 (MW-1) to 14.35 (MW-4) feet below top of casing (ft btoc) as
measured in monitoring wells MW-1 through MW-4 in February 2024. Groundwater flow at the site is generally to
the north. Groundwater potentiometric data are summarized on Figure 6.

8.0 Receptor Information

In accordance with DSCA Guidance pursuant to receptor surveys, AECOM conducted a windshield survey and
reviewed available online resources to document water supply wells and other sensitive receptors located within
a 0.5-mile radius of the site. There are two riverine habitats approximately 0.22 miles from the site, one to the
northeast and one to the northwest, and one approximately 0.36 miles away to the southwest; however, no ponds,
lakes, or wetlands were observed or recorded within 0.5 miles of the site. No evidence of private water supply
wells was observed during the February 2024 windshield survey. In addition, AECOM prepared and sent 53 public
outreach letters to surrounding property owners located within a 500-foot radius of the dry-cleaning facility, as
documented in a Completion Documentation of the Public Outreach Mailings report, dated April 30, 2024. Of the
18 returned water supply well information request forms, one property owner indicated the presence of a water
supply well on their property. AECOM attempted to contact the property owner to ask for additional information
about the supply well but has not received a response as of June 2024.

Four churches were identified within 0.5 miles of the site, the nearest of which is located adjacent to the site (606
Elwell Avenue). The Otis L. Hairston Middle School is located approximately 0.28 miles southeast of the site, and
several parks and recreational fields exist in conjunction with the school. Additionally, Bessemer Elementary
School is located approximately 0.32 miles northeast of the site. A figure summarizing sensitive receptors within a
500-foot and 0.5-mile radius of the site is included as Figure 8. Site photographs for reference are included as
Appendix G.

9.0 Investigative Derived Waste (IDW)

Investigative derived waste (IDW) generated during assessment activities included soil cuttings from drilling, boring
advancement, soil sampling, and soil gas point installation; development water post well construction; and purge
water generated during groundwater sampling. During each event, IDW was placed in closed, properly labeled,
55-gallon drums that were stored onsite until transported to a licensed hazardous waste facility by a waste disposal
contractor. The waste manifest documenting IDW generated to date is included as Appendix H.

Frye & Webster Cleaners
DSCA Site ID DC410064
Page 7 of 7

10.0 Review of Laboratory Analytical Reports

In respect to the usability and reliance of analytical results provided by Pace - AECOM received Pace’s laboratory
reports dated February 19 and February 26, 2024. Pace is a North Carolina certified laboratory (North Carolina
Environmental Certificate # 375. As documented in the laboratory analytical report (Appendix C), “results reported
herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable,
unless otherwise noted in the body of the report”. Data are deemed usable for the purposes of the assessment
activities and conclusions documented in this submittal.

In respect to the usability and reliance of analytical results provided by Enthalpy - AECOM received Enthalpy’s
laboratory reports dated February 15 and March 7, 2024. As documented in the laboratory analytical report
(Appendix C), “The results presented in this report are representative of the samples as provided to the
laboratory.” Data are deemed usable for the purposes of the assessment activities and conclusions documented
in this submittal.

If you have any questions or require additional information, please do not hesitate to call either Rob MacWilliams
at 704-499-4839 or Stephanie Hempel at 919-548-4330.

Sincerely,

AECOM TECHNICAL SERVICES OF NORTH CAROLINA, INC.

Stephanie Hempel, PG Robert H. MacWilliams, PG
Project Manager Program Manager

Enclosures

Table of Contents
DSCA ID No.: DC410064
Form 1
Form 2
Form 3
Form 4
Form 5
Form 6
Table 1
Table 2
Table 4
Table 5
Table 6
Table 7
Table 8
Table 10
Table 12
Figure 1
Figure 2
Figure 3
Figure 4 Soil Quality Summary Map
Figure 5 Groundwater Quality Summary Map - February 2024
Figure 6
Figure 7 Vapor Quality Summary Map
Figure 8 Sensitive Receptor Map
App. A
App. B
App. C Analytical Laboratory Reports
App. D
App. E
App. F
App. G
App. H
Analytical Data Tables (ADTs)
Assessment Report Forms
Facility Information
Site History
Land Use and Receptor Survey
Groundwater Use, Surface Water Use, and Ecological Survey
Site Stratigraphy and Hydrogeology
Non-Aqueous Phase Liquid (NAPL) Information
Site Chronology
Analytical Data for Soil
Analytical Data for Soil Gas
Analytical Data for Indoor and Outdoor Air
Monitoring Well Construction Data
Groundwater Elevation Data
Analytical Data for Groundwater
Water Well(s) Survey Data
Surrounding Land Use Map
Groundwater Contour Map - February 2024
DSCA Vapor Intrusion Risk Calculators
Standard Operating Procedures
Monitoring Well Construction Data
Groundwater Sampling Forms
Soil Boring Logs
Photographic Log
Waste Manifest
Appendices
Figures
Site Location Map
Site Layout Map
Analytical Data for Natural Attenuation Parameters
DSCA ID No.:
Submittal Date:
Assessment Report Forms
for
North Carolina Dry-Cleaning Solvent Cleanup Act Program
Prepared By:
Facility Name:Frye & Webster Cleaners
608 Elwell Avenue, Greensboro, Guilford County North Carolina
5438 Wade Park Bvd, Suite 200, Raleigh, North Carolina
AECOM Technical Services of North Carolina, Inc.
July 2024
DC410064
Facility Information
DSCA ID No.: DC410064
Currently operating facility since
Previously operating facility since
Temporarily out of service from to
Permanently out of service since
Facility name:
Facility telephone number (if applicable):
Facility Owner's Name:
Owner's Mailing Address:
Owner's Telephone number:
Contractor Date
Printed Name Company Name
AR Form 1
I certify that the prioritization assessment as stated in this report was prepared under my
supervision.
AECOM
7/8/2024Carolina, Inc.
Stephanie Hempel
336-379-1732
336-379-1732
At least 1955
Provide the earliest known date of the facility use for dry-cleaning business and the name of the
dry-cleaning buisness (if applicable).
Report Prepared By
608 Elwell Avenue
Greensboro, Guilford County, North Carolinacentre and the county where facility is
located):
608 Elwell Avenue
Greensboro, North Carolina 27405
James Woo
The site operated as a varsol/petroleum-based dry cleaners from approximately 1955 through
1995, as a tetrachloroethylene (PCE) dry cleaners from 1995 to 2015, and currently operates as a
MIELE water-based dry-cleaner. The varsol machine and PCE machines have been removed
from site.
1955, Frye and Webster Cleaners
Provide information on businesses that occupied the facility that may use or have used solvents
and other chemicals. Identify solvents and chemicals used at the facility (if applicable).
Frye & Webster Cleaners
dry-cleaning business owner. If no current business at the facility, provide the name and address
of the last dry-cleaner doing business at the site.
Site History
DSCA ID No.: DC410064
Number of dry-cleaning machines used at current or former facility:
Type of dry-cleaning solvents used by each type of machine.
Unknown petroleum-based solvent, PCE solvent, water (respectively)
According to a DSCA Compliance Inspection Memo dated August 24, 2018, use of the PCE machine
was discontinued at the site in January 2017, and the inspector verified that the PCE dry-cleaning
machine was disconnected from a power source, no solvent was left inside the solvent tanks, that no
solvent or solvent waste was stored on site, and the last waste pickup occurred on March 30, 2018, at
which time Safety Kleen picked up 500 pounds of liquid waste. An unmarked 55-gallon drum,
presumed to contain PCE solvent, was present in the 606 Elwell Avenue tenant space until removal by
the dry-cleaning business owner in May 2024.
What methods of disposal are used or have been used for separator water?
If yes, provide information about the substance stored, year taken out of service, virgin solvent or
waste solvent, etc.
While the 606 Elwell Avenue portion of the building has never been used as an operational part of the
dry-cleaner, it was utilized for storage by the dry cleaner, and an unmarked 55-gallon drum, presumed
to contain PCE solvent, was present in the 606 Elwell Avenue tenant space until removal by the dry-
cleaning business owner in May 2024. No USTs, ASTs, or evidence of former tanks were found onsite
and the owner did not indicate the existence of any.
Separator is not currently in use. Historical practices are unknown; however, an apparent separator
mister pipe surrounded by severely corroded cinderblocks is visible on the rear wall of the dry-cleaner
building.
Where are/were the dry-cleaning solvents stored at the facility site? (Machine base tanks, UST(s),
AST(s), etc.)
Machine base tanks
AR Form 2
Are chlorinated dry cleaning solvents delivered to the facility by means of a closed, direct-coupled
delivery system?
No
Are virgin (new)solvents stored in containers other than the dry-
cleaning machine?
Are or were any USTs or ASTs used to store any petroleum or
hazardous substances other than dry-cleaning solvents at the facility
1955-1995, one petroleum-based dry-cleaning machine; 1995-2017, one PCE dry-cleaning machine;
2015-present, one water-based dry-cleaning machine.
1 current
Type of dry-cleaning machines used at current or former facility (e.g., transfer, dry-to-dry with vented
exhaust, etc.).
Provide information about the current/historical waste management practices, including types of wastes
that are/were generated and how the waste are/were stored and managed.
Yes No
Yes No
Unpaved
Paved % area paved:
Any visible cracks in pavement?
Have the utilities been screened for vapor levels?
If YES, attach documentation of vapor monitoring results.
Depth
[feet]
Type of
Material
Flow
Direction
Impacted
by Release
Potentially
Impacted
by Release
Sanitary sewer Unknown Unknown Unknown Unknown Unknown
Septic drainfields
Covered storm sewer Unknown Unknown Unknown Unknown Unknown
Open ditch
Water line Unknown Unknown Unknown Unknown Unknown
Gas line Unknown Unknown Unknown Unknown
Electric line Unknown Unknown Unknown Unknown
Telephone line Overhead
Other
Has the release been abated?
Is native soil impacted?
Is groundwater impacted?
Is surface water impacted?
UST(s)/AST(s) removal Known spill incident
Inventory control Citizen complaint
Facility remodeling/Construction activity Assessment on adjacent property
Environmental assessment Unknown
Other (specify)
Indicate which of the following utilities currently act as conduits, or are likely to become conduits,
under the columns entitled "Impacted by Release," and "Potentially Impacted by Release," respectively.
In the space provided for additional notes, please indicate the location and distance from soil and/or
groundwater contamination to the nearest subsurface utility line and access point (e.g., manhole).
Ground Surface Conditions
Subsurface Utilities
Surface water samples not collected
20
Release Characterization
found contamination of both soil and groundwater including PCE and related constituents.
No longer using PCE/petroleum onsite
Release Discovery
Soil and groundwater assessment involved with property transaction
found contamination of both soil and groundwater including PCE and related constituents.
Soil and groundwater assessment involved with property transaction
Date the release was discovered
Date the release was reported
Type of release (explain)
1-Sep-21
1-Nov-21
The time and location of the release are unknown.
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No

Spills/Overfills Tanks
Piping Unknown
Other (specify)

1,1,1-Trichloroethane cis-1,2-Dichloroethylene
1,1,2,2-Tetrachloroethane Ethylbenzene
1,1,2-Trichloroethanae Methyl tert-butyl ether (MTBE)
1,1-Dichloroethane Naphthalene
1,1-Dichloroethylene Tetrachloroethylene
1,2-Dichloroethane (EDC) Toluene
Benzene trans-1,2-Dichloroethylene
Benzo(a)pyrene Trichloroethylene
Carbon tetrachloride Vinyl chloride
Chloroform Xylenes (total)
Others
Historical dry-cleaning operations
Chemicals of Concern
Source(s) of Release
Chemicals of concern listed above are those analytes that have been detected in groundwater at
concentrations above the NCAC 2L Groundwater Standards (2L Standards) or in soil samples above
the Protection of Groundwater Preliminary Soil Remediation Goal (PSRG).
Soil: PCE contamination above the PSRG is present beneath the northeastern portion of 608 Elwell
Ave (northern) half of the building, along the firewall in 608 Elwell Ave, and is inferred to extend to
the outside the southern wall in the vicinity of bay doors in the 606 Elwell Ave half of the building.
Soil Gas: Results of samples SG-1 and SG-11, collected between the area of the former PCE machine
in 608 Elwell Ave, and between the fire door and the bay doors on southern wall of building in 606
Elwell Ave, respectively, exceed acceptable calculated risk for non-residential worker use when
entered into the DSCA Soil Gas to Indoor Air Risk Calculators.
Groundwater: Exceedances of PCE 2L Standards in MW-1 (northwest corner of property), MW-2
(southwest corner), and MW-4 (northeast corner). Exceedances of benzene 2L Standards in all four
monitoring wells; notably highest in MW-2 adjacent to gas station.
Additional Notes
1,2-Dichloropropane
Di-isopropyl Ether
Land Use and Receptor Survey
DSCA ID No.: DC410064
On-site Land Use Current Future
Residential
Commercial/Industrial
Other
Justify the choice for future land use:
North:
Northeast:
Northwest:
South:
Southeast:
Southwest:
West:
East:
Nearest residential site:
Nearest commercial/industrial site:
If site is vacant, nearest inhabited building:
Nearest school, hospital, day care, nursing home etc.:
Nearest public supply well:
Nearest private supply well:
Nearest surface water body:
AR Form 3
Land Use
Distance [feet] Direction
Recreational/residential - a church and then several single-family residences
Commercial - auto repair
Elwell Avenue, then residences
Commercial - auto repairs, Higgins Curb Market gas station
Commercial - auto repair
The site is currently a water-based dry-cleaning operation in a well-developed area, surrounded by other
commercial and residential properties. It is unlikely that future use will change from commercial.
Immediate Off-site Land Use (within 500 feet -at a minimum,state whether,residential,
commercial/industrial, agricultural, or ecologically sensitive area). Indicate distances to
residential/commercial/industrial buildings having basements which are occupied.
Receptor Survey
Nearest ecologically sensitive area (agricultural areas,
parks/recreational areas, widlife sanctuaries, wetlands):
Nearest point of exposure (current or potential) for
groundwater ingestion:
100
Elwell Avenue, then neighborhood grocery store
Residential
North
Auto repair and then residential
List the distance and the direction (downgradient, upgradient, or crossgradient) to these facilites within
0.5 mile radius of the site (If necessary provide details in additional notes).
20
NA
1,200
East
NA
Northeast
185 NA
1,200
Site
Northeast
Property boundary
Additional Notes
Nearest point of exposure (potential) is assumed to be the downgradient property boundary. The nearest
ecologically sensitive receptor is an unnamed tributary to Muddy Creek, located approximately 1,200 feet
northeast of the subject property, which appears to be downgradient. There are several churches and a
mosque within the search radius, the nearest of which being directly adjacent to the north. A private well
is reportedly located at 3217 East Bessemer Avenue, approximately 185 feet upgradient from the subject
property.
5 North (church)
None within 1 mi NA
Groundwater Use, Surface Water Use, and Ecological Survey
DSCA ID No.: DC410064
Is the groundwater used on-site?
If yes, specify the use:
Potable domestic supply
Non-potable domestic supply
Public/Municipal supply
Industrial supply
Agriculture
Other (explain in space provided below)
Is a surface water body present in 1,000 feet radius of the site?
If yes, specify the following:
Type of water body
North Carolina classification of water body
Does the water discharges into lake or reservoir?
Surface water use:
Potable domestic supply
Non-potable domestic supply
Public/Municipal supply
Industrial supply
Agriculture
Other (explain in space provided below)
2. Are there private water supply wells within 1500 feet radius from the site?
A tributary to Muddy Creek is located approximately 1,200 feet northeast of the subject property.
Additional Notes
One private well is reportedly located at 3217 East Bessemer Avenue, approximately 185 feet southeast (upgradient) of
the site, as documented in a Completion Documentation of the Public Outreach Mailings report, dated April 30, 2024.
1. Are there public/municipal water supply wells within 0.5 mile radius from
the
AR Form 4
Water Well(s) Information
Surface Water Use
Ecological Receptors and Habitats
1. Are there any ecological receptors or habitats present within 500 feet radius
from the site?
2. Are there visible indications of stressed receptors or habitats on or near the
site that may be a result of chemical release?
Groundwater Use
Yes No
River Wet weather creek Drain ditch Regular creek
Yes No
Yes No
Yes No
Yes No
Other:
Yes No
Yes No
Site Stratigraphy and Hydrogeology
DSCA ID No.: DC410064
Depth [feet]
0-20
Predominent Soil Type:
Depth [feet]
Unknown
Type of Aquifer?
Underlying predominent aquifer name:
Aquifer classification (if applicable):
Range of groundwater level fluctuations [feet bgs]:
Average depth to water table/static water level:
Flow direction:
Hydraulic gradient (i) [--]:
Hydraulic conductivity (K) [cm/year]:
Darcy velocity (K x i) [cm/year-calculated]:
Groundwater velocity (K x i/Porosity) [cm/year]:
Annual precipitation (average for last 30 years) [inches/year]:
Description of Soil
Additional Notes
Range of groundwater fluctuations and average depth to water is taken from measurements of
monitoring wells MW-1 though MW-4 on February 9, 2024. A hydraulic gradient of 0.0102 ft/ft was
calculated between MW-1 and MW-2 using February 2024 gauging data. An estimated hydraulic
conductivity based on published values for clay was used (Domenico and Schwartz, 1990).
Average annual precipitation obtained from U.S. Climate Data website
(https://www.usclimatedata.com/climate/greensboro/north-carolina/united-states/usnc0280).
~10-14 feet
Hydrogeology of the Saturated Impacted Zone
1.51
12.42
AR Form 5
Stratigraphy of Site
north
0.01
surficial aquifer
NA
7.56
Red-yellow to red-brown silty clay
Metamorphosed Granitic Rock (Geologic Map of NC; NCGS, 1985)
148.22
39.25
Type of Bedrock and Geological Formation
Confined Unconfined Perched
Values/Range Method
Dry bulk density [g/cm3]1.45 Estimated Measured
Total porosity [cm3/cm3]:0.5 Estimated Measured
Effective porosity [cm3/cm3]:0.2 Estimated Measured
Water content [cm3/cm3]:47.00% Estimated Measured
Fractional organic carbon content [g-C/g-soil]: Estimated Measured
Values/Range Method
Dry bulk density [g/cm3]1.45 Estimated Measured
Total porosity [cm3/cm3]:0.5 Estimated Measured
Effective porosity [cm3/cm3]0.2 Estimated Measured
Water content [cm3/cm3]:47 Estimated Measured
Fractional organic carbon content [g-C/g-soil]: Estimated Measured
Additional Notes
Vadose Zone Characteristics
Saturated Zone Characteristics
Values based on literature [Dry bulk density based on median soil value (ASTM, 1995), and total
porosity, effective porosity, and water content estimated based on observations of similar soils at other
locations (Yu et al, 1993; Hillel, 2003; Peck et al, 1974; and Domenico et al, 1990)].
Non-Aqueous Phase Liquid (NAPL) Information
DSCA ID No.: DC410064
Was NAPL discovered at the site:
If Yes, type of NAPL discovered: LNAPL DNAPL
Date LNAPL was discovered?
Type of LNAPL discovered (if known):
Number of monitoring wells/points currently at site:
Has LNAPL removal started?
If No, cite reason:
If Yes, specify method of removal (bailer, pump, etc.):
Removal points (MW #, Boring #, etc.):
Total number of recovery events to date:
Total amount of purge-water recovered:
Total amount of LNAPL recovered:
Date of latest LNAPL removal report submitted:
Date DNAPL was discovered?
Type of DNAPL discovered (if known):
Number of monitoring wells/points currently at site:
Has DNAPL removal started?
If No, cite reason:
If Yes, specify method of removal (bailer, pump, etc.):
Removal points (MW #, Boring #, etc.):
Total number of recovery events to date:
Total amount of purge-water recovered:
Total amount of DNAPL recovered:
Date of latest DNAPL removal report submitted:
Number of monitoring wells/points containing DNAPL (Note if any, list the monitoring wells/points
Number of monitoring wells/points containing LNAPL (Note if any, list the monitoring wells/points
containing NAPL):
Summary of DNAPL
AR Form 6
Summary of LNAPL
Additonal Notes
Yes No
DSCA ID No.:
Submittal Date:
Analytical Data Tables
for
North Carolina Dry-Cleaning Solvent Cleanup Act Program
Prepared By:
Facility Name:Frye & Webster Cleaners
608 Elwell Avenue, Greensboro, Guilford County, North Carolina
5438 Wade Park Boulevard, Suite 200, Raleigh, North Carolina
AECOM Technical Services of North Carolina, Inc.
July 2024
DC410064
Table 1: Site Chronology
DSCA ID No.: DC410064
Chronology of Events
1/29/2024-2/1/2024
AECOM conducted a site investigation including the collection of eighteen soil samples (two each from boring locations
SB-3 through SB-11); eleven soil gas samples (SG-1 through SG-11); installation and subsequent sampling of four
groundwater monitoring wells (MW-1 through MW-4); a half-mile windshield receptor survey, and site GPS surveying.
3/15/2024 AECOM conducted an additional indoor air sample (IA-1) to assess air quality inside the dry cleaning facility.
Instructions: Brief description of all significant events that have occurred since a problem was
suspected at the facility. Commence with the first date a problem was suspected and continue
through the most recent activity described in the current report.
Date
Page 1 of 1
Table 2: Analytical Data for Soil
DSCA ID No.: DC410064
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SB-1 5.5-6.5 9/16/21 ND ND ND ND ND ND 0.013 ND ND ND 0.012 ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
SB-2 6-7 9/17/21 ND ND ND ND ND 0.021 ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
SB-3 0-1 0-1 1/31/24 <0.00176 0.0391 <0.00440 <0.00176 <0.0220 8.66 <0.00880 <0.00880 0.127 <0.00440 <0.0114 0.00606 0.0173 J <0.00880 <0.00880 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.0449 <0.449 <0.449 <0.449 <0.0449
SB-3 1-2 1-2 1/31/24 <0.00159 0.00407 <0.00399 <0.00159 <0.0199 0.394 <0.00797 <0.00797 0.00432 <0.00399 <0.0104 0.00327 J 0.0172 J <0.00797 <0.00797 <0.0428 <0.0428 <0.0428 <0.0428 <0.0428 <0.0428 <0.0428 <0.0428 <0.0428 <0.0428 <0.0428 <0.0428 <0.0428 <0.428 <0.428 <0.428 <0.0428
SB-4 0-1 0-1 1/31/24 <0.00170 <0.00425 <0.00425 <0.00170 <0.0212 <0.00425 <0.00849 <0.00849 <0.00170 <0.00425 <0.0110 0.00328 J 0.0187 J <0.00849 <0.00849 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.0446 <0.446 <0.446 <0.446 <0.0446
SB-4 2-3 2-3 1/31/24 <0.00171 <0.00427 <0.00427 <0.00171 <0.0213 <0.00427 <0.00854 <0.00854 <0.00171 <0.00427 <0.0111 0.00318 J 0.0151 J <0.00854 <0.00854 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.0447 <0.447 <0.447 <0.447 <0.0447
SB-5 0-1 0-1 1/29/24 <0.00116 <0.00290 <0.00290 <0.00116 0.00687 J 0.380 0.00561 J <0.00581 <0.00116 <0.00290 0.011 0.00247 J 0.0107 J 0.00434 J <0.00581 <0.0358 0.00731 J 0.0284 J 0.0358 J 0.0110 J 0.0278 J 0.0306 J 0.0271 J <0.0358 0.0451 0.0195 J 0.0139 J 0.0388 0.0442 J <0.358 0.0150 J 0.0533
SB-5 4-5 4-5 1/29/24 <0.00163 <0.00407 <0.00407 <0.00163 <0.0203 0.0207 <0.00813 <0.00813 <0.00163 <0.00407 <0.0106 0.00351 J 0.0185 J <0.00813 <0.00813 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.0434 <0.434 <0.434 <0.434 <0.0434
SB-6 0-1 0-1 1/30/24 <0.00134 <0.00334 <0.00334 <0.00134 <0.0167 0.00907 0.00175 J <0.00668 <0.00134 <0.00334 0.00130 J 0.0020 J 0.00989 J <0.00668 <0.00668 <0.0382 <0.0382 <0.0382 <0.0382 <0.0382 <0.0382 <0.0382 <0.0382 <0.0382 <0.0382 <0.0382 <0.0382 <0.0382 <0.382 <0.382 <0.382 <0.0382
SB-6 1-2 1-2 1/30/24 <0.00160 <0.00400 <0.00400 <0.00160 <0.0200 0.00448 <0.00801 <0.00801 <0.00160 <0.00400 <0.0104 0.00298 J 0.0125 J <0.00801 <0.00801 <0.0422 <0.0422 <0.0422 <0.0422 <0.0422 <0.0422 <0.0422 <0.0422 <0.0422 <0.0422 <0.0422 0.0261 J <0.422 <0.422 <0.422 <0.0422 <0.0422
SB-7 0-1 0-1 1/29/24 <0.00151 <0.00377 <0.00377 <0.00151 <0.0188 0.141 <0.00754 <0.00754 <0.00151 <0.00377 <0.00980 0.00356 J 0.0133 J <0.00754 <0.00754 <0.0409 <0.0409 <0.0409 <0.0409 <0.0409 <0.0409 <0.0409 <0.0409 <0.0409 <0.0409 <0.0409 <0.0409 <0.0409 <0.409 <0.409 <0.409 <0.0409
SB-7 3-4 3-4 1/29/24 <0.00184 <0.00461 <0.00461 <0.00184 <0.0230 <0.00461 <0.00921 <0.00921 <0.00184 <0.00461 <0.0120 0.00507 0.0194 J <0.00921 <0.00921 <0.0469 <0.0469 <0.0469 <0.0469 <0.0469 <0.0469 <0.0469 <0.0469 <0.0469 <0.0469 <0.0469 <0.0469 <0.0469 <0.469 <0.469 <0.469 <0.0469
SB-8 0-1 0-1 1/29/24 <0.00159 <0.00399 <0.00399 <0.00159 <0.0199 <0.00399 <0.00797 <0.00797 <0.00159 <0.00399 <0.0104 0.00255 J 0.0110 J <0.00797 <0.00797 <0.0419 <0.0419 <0.0419 <0.0419 <0.0419 <0.0419 <0.0419 <0.0419 <0.0419 <0.0419 <0.0419 <0.0419 <0.0419 <0.419 <0.419 <0.419 <0.0419
SB-8 1-2 1-2 1/29/24 <0.00148 <0.00370 <0.00370 <0.00148 <0.0185 0.00210 J <0.00739 <0.00739 <0.00148 <0.00370 <0.00961 0.00243 J 0.00982 J <0.00739 <0.00739 <0.0402 <0.0402 <0.0402 <0.0402 <0.0402 <0.0402 <0.0402 <0.0402 <0.0402 <0.0402 <0.0402 <0.0402 <0.0402 <0.402 <0.402 <0.402 <0.0402
SB-9 0-1 0-1 1/29/24 <0.00133 <0.00333 <0.00333 <0.00133 <0.0166 <0.00333 <0.00665 <0.00665 <0.00133 <0.00333 0.00306 J 0.00278 J 0.0128 J 0.00475 J <0.000665 0.0126 J <0.0383 0.0330 J 0.0757 0.0215 J 0.0433 0.0461 0.0404 0.0107 J 0.0943 0.045 <0.0383 0.0362 J <0.383 0.268 J <0.383 0.0756
SB-9 1-2 1-2 1/29/24 <0.00179 <0.00447 <0.00447 <0.00179 <0.0223 <0.00447 <0.00893 <0.00893 <0.00179 <0.00447 <0.0116 0.00355 J 0.0146 J <0.00893 <0.00893 <0.0448 <0.0448 <0.0448 <0.0448 <0.0448 <0.0448 <0.0448 <0.0448 <0.0448 <0.0448 <0.0448 <0.0448 <0.0448 <0.448 <0.448 <0.448 <0.0448
SB-10 0-1 0-1 1/29/24 <0.00139 <0.00348 <0.00348 <0.00139 <0.0174 0.115 <0.00695 <0.00695 <0.00139 <0.00348 <0.00904 0.00317 J 0.0163 J <0.00695 <0.00695 <0.0395 <0.0395 <0.0395 <0.0395 <0.0395 <0.0395 <0.0395 <0.0395 <0.0395 <0.0395 <0.0395 <0.0395 <0.0395 <0.395 <0.395 <0.395 <0.0395
SB-10 3-4 3-4 1/29/24 <0.00153 <0.00383 <0.00383 <0.00153 <0.0191 <0.00383 <0.00765 <0.00765 <0.00153 <0.00383 <0.00995 0.00320 J 0.0152 J <0.00765 <0.00765 <0.0417 <0.0417 <0.0417 <0.0417 <0.0417 <0.0417 <0.0417 <0.0417 <0.0417 <0.0417 <0.0417 <0.0417 <0.0417 <0.417 <0.417 <0.417 <0.0417
SB-11 0-1 0-1 1/29/24 <0.00138 <0.00344 <0.00344 <0.00138 <0.0172 <0.00344 <0.00688 <0.00688 <0.00138 <0.00344 <0.00894 0.00195 J 0.0133 J <0.00688 <0.00688 <0.0390 <0.0390 0.00698 J 0.0124 J <0.0390 0.00952 J 0.00866 J 0.00788 J <0.0390 0.0163 J <0.0390 <0.0390 <0.0390 <0.390 <0.390 <0.390 0.0156 J
SB-11 1-2 1-2 1/29/24 <0.00188 <0.00469 <0.00469 <0.00188 <0.0235 <0.00469 <0.00939 <0.00939 <0.00188 <0.00469 <0.0122 0.00406 J 0.0166 J <0.00939 <0.00939 <0.0470 <0.0470 <0.0470 <0.0470 <0.0470 <0.0470 <0.0470 <0.0470 <0.0470 <0.0470 <0.0470 <0.0470 <0.0470 <0.470 <0.470 <0.470 <0.0470
Bold - compound detected
Sa
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g
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]
[mg/kg][mg/kg]
Page 1 of 1
Table 4: Analytical Data for Soil Gas
DSCA ID No.: DC410064
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Tr
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c
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Xy
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s

(
t
o
t
a
l
)
Pro
p
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Ch
l
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f
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1,
1
,
2
,
2
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T
e
t
r
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c
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l
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t
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Di
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Ch
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B
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t
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Tr
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Eth
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Ac
r
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Ac
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t
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Ca
r
b
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D
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f
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Is
o
p
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p
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Me
t
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C
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He
x
a
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Me
t
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y
l

E
t
h
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l

K
e
t
o
n
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(
2
-
Bu
t
a
n
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)
Eth
y
l

A
c
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t
a
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Te
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r
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f
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a
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2,
2
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4
-
T
r
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t
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p
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Me
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M
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c
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Me
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I
s
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b
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K
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t
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(M
I
B
K
)
2-
H
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x
a
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Sty
r
e
n
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4-
E
t
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t
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1,
3
,
5
-
T
r
i
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t
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n
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1,
2
,
4
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T
r
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t
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y
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n
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1-
O
c
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n-
O
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Is
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p
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(C
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)
n-
P
r
o
p
y
l
b
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n
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1,
1
-
D
i
c
h
l
o
r
o
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t
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Ac
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t
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t
r
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l
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1,
1
,
1
-
T
r
i
c
h
l
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r
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t
h
a
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e
2-
C
h
l
o
r
o
t
o
l
u
e
n
e

(
o
-
Ch
l
o
r
o
t
o
l
u
e
n
e
)
SG-1 5 10 m 1/31/24 <484 23276 <649 <558 <795 2043185 <578 <609 64278 <385 <1318 262 1165 1336 <729 <308 <324 <893 <281 <340 <358 <468 <369 <536 <539 <459 <542 <449 686 <727 <625 <646 <641 <631 <629 <753 <751 <741 <682 <725 <752 <759 <601 <252 <830 <787
SG-2 5 17 m 1/31/24 1.50 <0.432 5.84 <0.399 1.76 871 15.5 <0.436 5.14 <0.275 31.63 21.6 1.84 <0.748 2.33 0.862 1.39 1.24 9.81 0.426 22.9 1.18 2.66 1.86 1.79 1.11 1.45 0.436 0.937 0.56 1.12 1.35 4.6 2.46 0.503 2.27 3.49 15.4 3.99 7.13 <0.538 1.11 <0.430 <0.180 <0.594 <0.563
SG-3 5 6 m 1/31/24 0.751 16.0 1.16 <0.367 <0.522 12277 7.29 1.25 109 <0.253 6.08 5.02 0.999 <0.686 2.37 <0.202 <0.213 1.10 1.50 <0.223 23.8 3.00 0.558 0.838 1.65 6.03 <0.356 1.46 1.71 <0.478 1.43 <0.424 5.67 16.0 <0.413 0.859 1.06 4.12 1.31 1.46 0.434 0.912 0.769 0.178 15.6 <0.517
SG-4 5 6 m 2/1/24 0.389 6.04 0.726 <0.389 <0.553 1236 3.40 <0.424 9.03 <0.268 4.94 31.3 0.570 1.72 2.25 0.201 0.610 1.11 1.33 4.5 8.88 9.66 0.510 0.490 3.23 1.12 <0.377 0.475 5.67 1.45 1.39 4.15 35.7 14.5 <0.438 0.478 0.966 2.71 9.32 2.93 0.904 <0.529 <0.418 <0.175 <0.578 <0.548
SG-5 5 14 m 1/29/24 1.21 14.4 4.50 <0.343 0.850 3117 15.7 2.01 131 <0.236 24.83 7.22 5.25 0.775 2.44 0.77 0.718 1.32 6.59 0.803 84.9 1.55 4.77 0.665 2.5 18.7 4.13 7.17 1.46 3.28 1.78 0.387 30.7 98.7 0.444 3.67 3.91 15.1 1.74 3.28 1.23 2.59 <0.369 <0.155 <0.510 0.56
SG-6 5 7 m 2/1/24 <0.321 <0.400 <0.431 <0.371 <0.528 133 1.96 <0.404 <0.543 <0.255 <0.875 1.57 0.822 <0.694 2.32 0.405 <0.215 1.38 1.63 <0.226 17.5 1.18 1.04 0.363 0.833 0.687 <0.360 0.617 0.326 <0.483 <0.415 <0.429 0.398 0.396 <0.417 <0.500 <0.498 <0.492 <0.453 <0.481 <0.499 <0.504 <0.399 <0.167 <0.551 <0.522
SG-9 5 5 m 1/31/24 7.02 0.44 1.89 <0.332 <0.472 47.6 14.7 <0.362 0.525 <0.229 7 99.9 0.929 <0.621 2.24 0.27 11.7 1.17 4.28 <0.202 20.5 55.6 2.35 2 14.4 3.79 1.02 0.243 J 6.32 3.77 8.31 <0.384 0.917 0.577 0.577 0.417 J 0.657 1.82 5.49 4.96 0.587 0.483 <0.357 0.302 <0.493 <0.467
SG-10 5 8 m 1/31/24 4.08 1.20 13.6 0.806 1.13 236 14.6 <0.848 2.63 <0.535 90.5 64.5 1.99 1.70 2.31 0.727 5.28 1.29 4.54 0.682 31.0 46.3 2.14 0.849 4.32 2.04 1.28 <0.626 2.20 1.02 2.36 <0.899 14.5 8.29 1.56 3.55 5.39 21.7 28.1 94.6 1.39 2.16 <0.836 <0.351 <1.16 <1.10
SG-11 5 18 m 1/31/24 138 157117 2178 <60.9 <86.7 1729266 <63.0 439 233007 1072 317 223 650 6154 <79.5 <33.6 <35.4 <97.4 37.5 <37.1 4878 70.1 <40.3 119 15840 <50.1 <59.1 <49.0 18395 994 8701 35691 1231 19398 <68.6 3154 2001 9101 10460 7821 2672 5719 1939 <27.5 <90.5 <85.8
Bold - compound detected
1 Indicate "G" for grab sample or for longer samples indicate the number of hours followed by "h".
Sa
m
p
l
e

I
D
Sa
m
p
l
i
n
g

D
a
t
e

(
m
m
/
d
d
/
y
y
)
De
p
t
h
[fe
e
t

b
g
s
]
[µg/m3][µg/m3]Sa
m
p
l
e

D
u
r
a
t
i
o
n
1
ADT 4(1)
Page 1 of 1
Table 5: Analytical Data for Indoor and Outdoor Air
DSCA ID No.: DC410064
Be
n
z
e
n
e
ci
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e
Et
h
y
l
b
e
n
z
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n
e
Me
t
h
y
l

t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
Te
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e
To
l
u
e
n
e
tr
a
n
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e
Vi
n
y
l

c
h
l
o
r
i
d
e
Xy
l
e
n
e
s

(
t
o
t
a
l
)
Ch
l
o
r
o
f
o
r
m
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
IA-1 03/15/24 F SU 8h 1.19 <0.190 0.394 <0.176 <0.250 1.84 NA <0.192 <0.257 <0.121 1.821 0.385 0.500
Notes:
1 Indicate "F" for former or current dry-cleaning facility, "AD" for adjacent space, "R" for residence, "C" for commercial not adjacent space. If sample was taken outdoors, leave blank.
2 Indicate "SU" for summa canister, "FC" for flux chambers, "T" for tedlar bags, "P" for passive samplers, "O" for other.
3 Indicate "8h" for 8-hour, "24h" for 24-hour, "G" for grab sample, for other hours indicate the number of hours followed by "h" or "d" for days.
Sa
m
p
l
e

I
D
Sa
m
p
l
i
n
g

D
a
t
e

(
m
m
/
d
d
/
y
y
)
[µg/m3]Sa
m
p
l
e

L
o
c
a
t
i
o
n

1
Sa
m
p
l
i
n
g

D
u
r
a
t
i
o
n
3
Sa
m
p
l
i
n
g

M
e
t
h
o
d

2
ADT 5
Page 1 of 1
Table 5(2): Additional Data for Indoor and Outdoor Air
DSCA ID No.: DC410064
Attachment:
Sampling location map that indicates where all indoor air samples were collected. The map should clearly indicate the names/types of businesses and residence names sampled and in the vicinity of the
subject site that may be of concern.
Is dry-cleaning facility at the site: Operating Pick-up Only Abandoned
If facility is operating, solvents used are: Perc Petroleum Green Earth Other
For the active or former dry-cleaning space, describe the type and location of the air handling/HVAC unit (for example - a shared unit supplying two adjacent spaces; unit located on the roof):
Fan in back of facility and two roof vent fans; HVAC does not appear to be in use at site
For any other indoor spaces tested, describe the type and location of the air handling/HVAC unit (for example - a shared unit supplying two adjacent spaces; unit located on the roof):
NA
For any indoor air spaces tested, describe the current use of the space (for example - an ABC liquor store adjacent to the dry-cleaner, a residence approximately 200 feet from the dry-cleaner, etc.):
Current dry cleaning facility using water-based methods, as well as general laundry (washing machines/dryers, etc.).
Water-based Mielle
Page 1 of 1
Table 5(3): Additional Data for Indoor and Outdoor Air
DSCA ID No.: DC410064
Sample ID Name and Address for Sampling Location Property Owner Name, Address, and Phone Number Tenant Name, Address, and Phones Number
IA-1 Frye & Webster Cleaners, 608 Elwell Ave Fanuel Adnew, 608 Elwell Ave, 336-327-9030 James Woo, 608 Elwell Ave, 336-379-1732
Page 1 of 1
Table 6: Monitoring Well Construction Data
DSCA ID No.: DC410064
Well ID Date Installed
(mm/dd/yy)Number of Samples Well Depth
[feet]
Well Diameter
[inch]
Screen Interval
[feet]
Status
(Active/Inactive)
MW-1 1/30/24 1 20 2 5-20 Active
MW-2 1/30/24 1 20 2 5-20 Active
MW-3 1/30/24 1 20 2 5-20 Active
MW-4 1/30/24 1 20 2 5-20 Active
Page 1 of 1
Table 7: Groundwater Elevation Data
DSCA ID No.: DC410064
Groundwater
Sampling Point
Sampling Date
(mm/dd/yy)
TOC Elevation
[feet]
Depth to Water
[feet bgs]
Groundwater
Elevation
[feet]
Depth to NAPL
[feet bgs]
NAPL Thickness
[feet]
Corrected*
Groundwater
Elevation [feet]
MW-1 2/9/2024 816.48 10.99 805.49 NA NA NA
MW-2 2/9/2024 817.606 11.20 806.41 NA NA NA
MW-3 2/9/2024 820.119 13.42 806.70 NA NA NA
MW-4 2/9/2024 820.036 14.35 805.69 NA NA NA
ADT 7
Page 1 of 1
Analytical Data for Groundwater
DSCA ID No.: DC410064
Be
n
z
e
n
e
ci
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Me
t
h
y
l

t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
Te
t
r
a
c
h
l
o
r
o
e
t
h
y
l
e
n
e
To
l
u
e
n
e
tr
a
n
s
-
1
,
2
-
D
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e
Tr
i
c
h
l
o
r
o
e
t
h
y
l
e
n
e
Vi
n
y
l

c
h
l
o
r
i
d
e
Xy
l
e
n
e
s

(
t
o
t
a
l
)
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
te
r
t
-
B
u
t
y
l
b
e
n
z
e
n
e
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
Di
i
s
o
p
r
o
p
y
l

E
t
h
e
r
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e

(C
u
m
e
n
e
)
p-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Ac
e
t
o
n
e
MW-1 2/9/24 0.561 <0.000126 <0.000137 0.0114 0.0147 0.0016 0.000382 J <0.000149 0.000214 J <0.000234 <0.000174 0.000867 J 0.000464 J 0.00322 0.0104 0.00921 0.000248 J 0.000720 J <0.0113
MW-2 2/9/24 5.700 0.00361 J 0.170 4.620 0.0266 <0.00150 0.0551 <0.000745 0.00435 J <0.00117 0.129 0.00276 J 0.000665 J 0.0735 0.301 0.0268 0.00341 J 0.0368 0.0679 J
MW-3 2/9/24 0.00230 <0.000126 <0.000137 <0.000101 <0.0010 <0.00030 <0.000278 <0.000149 <0.000190 <0.000234 <0.000174 <0.000125 <0.000127 <0.0000819 <0.000105 <0.000105 <0.000120 <0.000993 0.0333 J
MW-4 2/9/24 0.0171 0.351 0.000929 J 0.00137 <0.0010 0.0633 0.000413 J 0.0156 0.0526 0.00115 0.000963 J 0.000410 J 0.000219 J <0.0000819 0.000244 J 0.000431 J 0.000316 J 0.000362 J 0.0170 J
Bold - compound detected
Table 8:
Gr
o
u
n
d
w
a
t
e
r

S
a
m
p
l
i
n
g

P
o
i
n
t
Sa
m
p
l
i
n
g

D
a
t
e

(
m
m
/
d
d
/
y
y
)
[mg/L]
Page 1 of 3
DSCA ID No.: DC410064
MW-1 2/9/24
MW-2 2/9/24
MW-3 2/9/24
MW-4 2/9/24
Bold - compound detected
Table 8:
Gr
o
u
n
d
w
a
t
e
r

S
a
m
p
l
i
n
g

P
o
i
n
t
Sa
m
p
l
i
n
g

D
a
t
e

(
m
m
/
d
d
/
y
y
)
Analytical Data for Groundwater
n-
B
u
t
y
l
b
e
n
z
e
n
e
Ch
l
o
r
o
b
e
n
z
e
n
e
Ch
l
o
r
o
f
o
r
m
1,
4
-
D
i
c
h
l
o
r
o
b
e
n
z
e
n
e
1,
2
-
D
i
c
h
l
o
r
o
p
r
o
p
a
n
e
2-
B
u
t
a
n
o
n
e

(
M
E
K
)
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
St
y
r
e
n
e
1,
1
,
2
-
T
r
i
c
h
l
o
r
o
e
t
h
a
n
e
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
2
,
3
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
1
-
D
i
c
h
l
o
r
o
e
t
h
e
n
e
Ac
e
n
a
p
h
t
h
e
n
e
Be
n
z
i
d
i
n
e
Fl
u
o
r
e
n
e
Ph
e
n
a
n
t
h
r
e
n
e
Di
e
t
h
y
l

P
h
t
h
a
l
a
t
e
<0.000157 <0.000116 <0.000111 <0.000120 <0.000149 <0.00119 <0.000430 <0.000118 <0.000158 <0.000322 <0.000104 <0.000104 <0.000188 <0.0000939 0.00396 J 0.000136 J 0.000268 J 0.000435 J
0.00340 J 0.0106 0.0195 J 0.00149 J 0.00492 J 0.00870 J 0.00232 J 0.00387 J 0.00144 J 0.0983 0.00596 0.0212 <0.000940 0.000937 J <0.00374 0.000177 J 0.000155 J 0.000313 J
<0.000157 <0.000116 <0.000111 <0.000120 <0.000149 <0.00119 <0.000430 <0.000118 <0.000158 <0.000322 <0.000104 <0.000104 <0.000188 <0.0000886 <0.00374 <0.000844 <0.000112 <0.000287
<0.000157 <0.000116 <0.000111 <0.000120 <0.000149 0.00268 J <0.000430 <0.000118 <0.000158 0.00292 0.00121 0.000812 J 000270 J 0.0000940 J <0.00393 0.000146 J <0.000118 <0.000301
[mg/L]
Page 2 of 3
DSCA ID No.: DC410064
MW-1 2/9/24
MW-2 2/9/24
MW-3 2/9/24
MW-4 2/9/24
Bold - compound detected
Table 8:
Gr
o
u
n
d
w
a
t
e
r

S
a
m
p
l
i
n
g

P
o
i
n
t
Sa
m
p
l
i
n
g

D
a
t
e

(
m
m
/
d
d
/
y
y
)
Analytical Data for Groundwater
Be
n
z
o
(
a
)
a
n
t
h
r
a
c
e
n
e
Be
n
z
o
(
b
)
f
l
u
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0.000214 J 0.000191 J 0.000265 J 0.000254 J 0.000120 J 0.000217 J 0.000303 J 0.000105 J 0.00109 J 0.0117
<0.000199 <0.000130 <0.000120 <0.000121 <0.0000381 <0.000130 <0.0000644 <0.000102 <0.000636 <0.00433
<0.000209 <0.000136 <0.000126 <0.000127 0.0000471 J <0.000136 0.0000819 J <0.000107 <0.0000668 <0.00455
[mg/L]
Page 3 of 3
Table 10: Water Well(s) Survey Data
DSCA ID No.: DC410064
Ref. No./
Well ID
Sampling Location
Name and Address
Property Owner
Name, Address, and
Phone Number
Tenant Name, Address,
and Phone Number
Distance
from
Source
[feet]
Well
Depth
[feet]
Screen
Interval
[feet]
Use of Well Source of Well
Identification
Direction
(downgradient,
upgradient, etc.,
to source area)
Status
(Active/
Inactive)
42 3217 E Bessemer Ave,
Greensboro, NC 27405
T & T AUTOMOTIVE
LLC 3114 PENINSULA
DR, Jamestown, NC,
27282
T & T Automotive Repair
3217 E Bessemer Ave,
Greensboro, NC 27405
[phone]
185 Unknown Unknown Irrigation Jan 2024 Public
Outreach Mailing Upgradient Unknown
ADT 10
Page 1 of 1
Table 12: Analytical Data for Natural Attenuation Parameters
DSCA ID No.: DC410064
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Units mg/L mg/L mg/L mg/L mg/L mg/L mV mg/L mg/L μs/cm2 std unit ° C mg/L mg/L mg/L
MW-1 2/9/2024 0.64 NA NA NA NA NA 81.8 NA NA 216 6.16 18.7 NA NA NA
MW-2 2/9/2024 3.7 NA NA NA NA NA 124.9 NA NA 113 5.05 19.3 NA NA NA
MW-3 2/9/2024 3.19 NA NA NA NA NA 127 NA NA 64 5.12 17.2 NA NA NA
MW-4 2/9/2024 6.84 NA NA NA NA NA 133.3 NA NA 145 5.37 17.2 NA NA NA
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ADT 12
Page 1 of 1
Figures
Site
Copyright:© 2013 National Geographic Society, i-cubed
0 ³
SHEET:
DRAWN BY:
CHECKED BY:
PROJECT NO:
LB - 06/29/2023
SDH - 06/29/2023
60722767
Figure 1
Site Location MapFrye & Webster608 Elwell AvenueGreensboro, NCDSCA Site DC410064
AECOM TECHNICAL SERVICES OF NORTH CAROLINA, INC.6000 FAIRVIEW ROAD, SUITE 200CHARLOTTE, NC 28210TEL: [phone]
APPROX. SCALE, ft.
0 30
SHEET:
Frye & Webster Cleaners LEGEND
Approximate Location of PCE Dry-Cleaning
Machine (1995-2015)
Approximate Location of Varsol / Petroleum
Machine (1955-1995)
Property Line (Guilford Co. GIS)
Site Property Boundary
Site Building (606 & 608 Elwell Ave)
Figure 2
Source: Esri, Maxar, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA,USGS, AeroGRID, IGN, and the GIS User Community
0 ³
SHEET:
DRAWN BY:
CHECKED BY:
PROJECT NO:
EMM - 04/24/2024
SDH - 04/30/2024
60722767
Figure 3
Surrounding Land Use MapFrye & Webster608 Elwell AvenueGreensboro, NCDSCA Site DC410064
AECOM TECHNICAL SERVICES OF NORTH CAROLINA, INC.6000 FAIRVIEW ROAD, SUITE 200CHARLOTTE, NC 28210TEL: [phone]
Site BoundaryZONINGC-M-COMMERCIAL MEDIUMC-M-COMMERCIAL MEDIUM,RM-18-Residential, Multi-Family, 18 units per acreCD-LI-LIGHT INDUSTRIALLI-Light IndustrialPI-Public and InstitutionalR-5-RESIDENTIAL SINGLE FAMILY 5RM-18-Residential, Multi-Family, 18 units per acre
APPROX. SCALE, ft.
0 30
SHEET:
Frye & Webster Cleaners
Figure 4
LEGEND
milligrams per kilogrammg/kg
PCE - Tetrachloroethylene
TCE - Trichloroethylene
DCE - Dichloroethylene
TMB - Trimethylbenzene
Soil and Groundwater Sample Location - Pyramid
Environmental & Engineering P.C. (Pyramid), September
16 & 17, 2021
micrograms per literµg/L
Approximate Location of PCE Dry-Cleaning
Machine (1995-2015)
Approximate Location of Varsol / Petroleum
Machine (1955-1995)
Soil Sample Location
Property Line (Guilford Co. GIS)
Site Property Boundary
Site Building (606 & 608 Elwell Ave)
Blank contamination was reported by the laboratory for
chloroform and methylene chloride
Estimated ValueJ
BJ
Inferred Area of PCE Impacts in Soil > NCDEQ
Preliminary Soil Remediation Goals (PSRG)
SB-8 (0-1’) (01/29/2024)
Chloroform - 0.00255 BJ mg/kg
Methylene Chloride - 0.0110 BJ mg/kg
SB-8 (1-2’) (01/29/2024)
PCE - 0.00210 J mg/kg
Chloroform - 0.00243 BJ mg/kg
Methylene Chloride - 0.00982 J mg/kg
SB-7 (0-1’) (01/29/2024)
PCE - 0.141 mg/kg
Chloroform - 0.00356 BJ mg/kg
Methylene Chloride - 0.0133 BJ mg/kg
SB-7 (3-4’) (01/29/2024)
Chloroform - 0.00507 mg/kg
Methylene Chloride - 0.0194 BJ mg/kg
SB-9 (0-1’) (01/29/2024)
Chloroform - 0.00278 BJ mg/kg
Methylene Chloride - 0.0128 BJ mg/kg
1,2,4-TMB 0.00475 J mg/kg
Xylenes - 0.00306 J mg/kg
SB-9 (1-2’) (01/29/2024)
Chloroform - 0.00355 BJ mg/kg
Methylene Chloride - 0.0146 BJ mg/kg
SB-11 (0-1’) (01/30/2024)
Chloroform - 0.00195 BJ mg/kg
Methylene Chloride - 0.0133 BJ mg/kg
SB-11 (1-2’) (01/30/2024)
Chloroform - 0.00406 BJ mg/kg
Methylene Chloride - 0.0166 BJ mg/kg SB-6 (0-1’) (01/30/2024)
PCE - 0.00907 mg/kg
Chloroform - 0.00200 BJ mg/kg
Methylene Chloride - 0.00989 BJ mg/kg
Toluene - 0.00175 J mg/kg
Xylenes - 0.00130 mg/kg
SB-6 (1-2’) (01/30/2024)
PCE - 0.00448 mg/kg
Chloroform - 0.00298 mg/kg
Methylene Chloride - 0.0125 BJ mg/kg
SB-4 (0-1’) (01/31/2024)
Chloroform - 0.00328 BJ mg/kg
Methylene Chloride - 0.0187 BJ mg/kg
SB-4 (2-3’) (01/31/2024)
Chloroform - 0.00318 BJ mg/kg
Methylene Chloride - 0.0151 BJ mg/kg
SB-3 (0-1’) (01/31/2024)
PCE - 8.66 mg/kg
TCE - 0.127 mg/kg
cis-1,2-DCE - 0.0391 mg/kg
Chloroform - 0.00606 mg/kg
Methylene Chloride - 0.0173 BJ mg/kg
SB-3 (1-2’) (01/31/2024)
PCE - 0.394 mg/kg
TCE - 0.00432 mg/kg
cis-1,2-DCE - 0.00407 mg/kg
Chloroform - 0.00327 BJ mg/kg
Methylene Chloride - 0.0172 BJ mg/kg
SB-5 (0-1’) (01/29/2024)
PCE - 0.380 mg/kg
Chloroform - 0.00247 BJ mg/kg
Methylene Chloride - 0.0107 BJ mg/kg
Naphthalene - 0.00687 J mg/kg
Toluene - 0.00561 J mg/kg
1,2,4-TMB - 0.00434 J mg/kg
1,2,3-TMB - 0.00290 J mg/kg
Xylenes - 0.0110 mg/kg
SB-5 (4-5’) (01/29/2024)
PCE - 0.0207 mg/kg
Chloroform - 0.00351 BJ mg/kg
Methylene Chloride - 0.0185 BJ mg/kg
SB-10 (0-1’) (01/29/2024)
PCE - 0.115 mg/kg
Chloroform - 0.00317 BJ mg/kg
Methylene Chloride - 0.0163 BJ mg/kg
SB-10 (3-4’) (01/29/2024)
Chloroform - 0.00320 BJ mg/kg
Methylene Chloride - 0.0152 BJ mg/kg
APPROX. SCALE, ft.
0 30
SHEET:
Frye & Webster Cleaners
806.0 ft
806.5 ft
805.5 ft
Figure 5
LEGEND
milligrams per kilogrammg/kg
PCE - Tetrachloroethylene
TCE - Trichloroethylene
DCE - Dichloroethylene
MTBE - Methyl tert-butyl ether
TMB - Trimethylbenzene
Soil and Groundwater Sample Location - Pyramid
Environmental & Engineering P.C. (Pyramid), September
16 & 17, 2021
micrograms per literµg/L
Approximate Location of former PCE Dry-Clean-
ing Machine (1995-2015)
Approximate Location of former Varsol / Petro-
leum Machine (1955-1995)
Analytical results do not exceed calculated vapor intrusion
risk for residential or non-residential exposure – DSCA
Groundwater to Indoor Air Risk Calculator.
Analytical results exceed calculated vapor intrusion risk for
residential and non-residential exposure – DSCA
Groundwater to Indoor Air Risk Calculator.
Monitoring Well Location
Property Line (Guilford Co. GIS)
Site Property Boundary
Site Building (606 & 608 Elwell Ave)
Area of PCE 2L Standard Exceedance
Red highlighted text indicates concentrations above 2L
Standards.
Potentiometric Surface Contour (ft)
Inferred Groundwater Flow Direction
MW-1 (5-20’) (02/09/2024)
PCE - 1.60 µg/l
TCE - 0.214 J µg/l
1,2-Dichloroethane - 3.22 µg/l
Benzene - 561 µg/l
Toluene - 0.382 J µg/l
MTBE - 11.4 µg/l
Naphthalene - 14.7 µg/l
sec-Butylbenzene - 0.867 J µg/l
tert-Butylbenzene - 0.464 J µg/l
Di-isopropyl ether - 10.4 µg/l
Isopropylbenzene - 9.21 µg/l
p-Isopropyltoluene - 0.248 J µg/l
n-Propylbenzene - 0.720 J µg/l
MW-3 (5-20’) (02/09/2024)
Benzene - 2.30 µg/l
Acetone - 33.3 J µg/l
MW-2 (5-20’) (02/09/2024)
TCE - 4.35 J µg/l
cis-1,2-DCE - 3.61 J µg/l
1,2-Dichloroethane - 73.5 µg/l
1,1,2-Trichloroethane - 1.44 J µg/l
Benzene - 5,700 µg/l
Toluene - 55.1 µg/l
Ethylbenzene - 170 µg/l
Xylenes - 129 µg/l
MTBE - 4,620 µg/l
Naphthalene - 26.6 µg/l
Acetone - 67.9 J µg/l
n-Butylbenzene - 3.40 J µg/l
sec-Butylbenzene - 2.76 J µg/l
tert-Butylbenzene - 0.665 J µg/l
Chlorobenzene - 10.6 µg/l
Chloroform - 19.5 J µg/l
1,4-Dichlorobenzene - 1.49 J µg/l
1,2-Dichloropropane - 4.92 J µg/l
Di-isopropyl ether - 301 µg/l
Isopropylbenzene - 26.8 µg/l
p-Isopropyltoluene - 3.41 J µg/l
2-Butanone - 8.70 J µg/l
Methylene Chloride - 2.32 J µg/l
n-Propylbenzene - 36.8 µg/l
Styrene - 3.87 J µg/l
1,2,4-TMB - 98.3 µg/l
1,2,3-TMB - 5.96 µg/l
1,3,5-TMB - 21.2 µg/l
MW-4 (5-20’) (02/09/2024)
PCE - 63.3 µg/l
TCE - 52.6 µg/l
cis-1,2-DCE - 351 µg/l
trans-1,2-DCE - 15.6 µg/l
Vinyl chloride - 1.15 µg/l
1,1-DCE - 0.270 J µg/l
Benzene - 17.1 µg/l
Toluene - 0.413 J µg/l
Ethylbenzene - 0.929 J µg/l
Xylenes - 0.963 J µg/l
MTBE - 1.37 µg/l
Acetone - 17.0 J µg/l
sec-Butylbenzene - 0.410 J µg/l
tert-Butylbenzene - 0.219 J µg/l
Di-isopropyl ether - 0.244 J µg/l
Isopropylbenzene - 0.431 J µg/l
p-Isopropyltoluene - 0.316 J µg/l
2-Butanone - 2.68 J µg/l
n-Propylbenzene - 0.362 µg/l
1,2,4-TMB - 2.92 µg/l
1,2,3-TMB - 1.21 µg/l
1,3,5-TMB - 0.812 J µg/l
610 Elwell Ave
606 Elwell Ave
608 Elwell Ave
Higgin’s Curb Market
Active UST Facility ID:
00-0-0000009969
APPROX. SCALE, ft.
0 30
SHEET:
Frye & Webster Cleaners
805.49
806.41
806.70
805.69
806.0 ft
806.5 ft
805.5 ft
LEGEND
Monitoring Well Location, Identification
and Relative Groundwater Elevation (ft)
Potentiometric Surface Contour (ft/msl)
MW-187.47
Deep Monitoring Well Location, Identification
and Relative Groundwater Elevation (ft)
- not used in contouringDMW-1(85.20)
Inferred Groundwater Flow Direction
Figure 6
Approximate Location of former PCE Dry-Clean-
ing Machine (1995-2015)
Approximate Location of former Varsol / Petro-
leum Machine (1955-1995)
MW-1
MW-2 MW-3
MW-4
MW-5
APPROX. SCALE, ft.
0 30
SHEET:
Frye & Webster Cleaners
606 Elwell Ave
(Vacant)
610 Elwell Ave
LEGEND
milligrams per kilogrammg/kg
Note: Compounds summarized on this map were selected based
on those detected in soil samples at concentrations greater than
the NCDEQ Preliminary Soil Remediation Goals, and in
groundwater at concentrations which represent a hazard quotient
≥ 0.1 or carcinogenic risk ≥ 1E-06 when entered in the DSCA
Groundwater to Indoor Air Risk Calculator, in accordance with
DSCA Contractor Bulletin # 32 - Determination of COCs for VI
Investigations, dated June 25, 2018. Comprehensive results are
included in DSCA Analytical Data Table 4 and in the DSCA Soil
Gas to Indoor Air Risk Calculators.
Property Line (Guilford Co. GIS)
micrograms per literµg/L
Approximate Location of PCE Dry-Cleaning
Machine (1995-2015)
Approximate Location of Varsol / Petroleum
Machine (1955-1995)
Analytical results do not exceed calculated vapor intrusion
risk for residential or non-residential exposure – DSCA
Indoor Air/Soil Gas to Indoor Air Risk Calculator.
Analytical results exceed calculated vapor intrusion risk for
residential and non-residential exposure – DSCA Soil Gas
to Indoor Air Risk Calculator.
Analytical results do not exceed calculated vapor intrusion risk for
non-residential exposure but do exceed for residential exposure –
DSCA Soil Gas to Indoor Air Risk Calculator.
Soil Gas Sample Location
Indoor Air Sample Location
Site Property Boundary
Site Building (606 & 608 Elwell Ave)
PCE - Tetrachloroethylene
TCE - Trichloroethylene
DCE - Dichloroethylene
TMB - Trimethylbenzene
MTBE - Methyl tert-butyl ether
Figure 7
SG-5 (01/29/2024)
PCE - 3,117 µg/mk
TCE - 131 µg/mk
cis-1,2-DCE - 14.4 µg/mk
trans-1,2-DCE - 2.01 µg/mk
Chloroform - 5.25 µg/mk
1,1,2-Trichloroethane - 0.553 µg/mk
Benzene - 1.21 µg/mk
Toluene - 15.7 µg/mk
Ethylbenzene - 4.50 µg/mk
m-/p-Xylenes - 18.1 µg/mk
o-Xylene - 6.73 µg/mk
Naphthalene - 0.850 µg/mk
1,2,4-TMB - 15.1 µg/mk
1,3,5-TMB - 3.91 µg/mk
SG-3 (01/29/2024)
PCE - 12,277 µg/mk
TCE - 109 µg/mk
cis-1,2-DCE - 16.0 µg/mk
trans-1,2-DCE - 2.01 µg/mk
Chloroform - 0.999 µg/mk
Benzene - 0.751 µg/mk
Toluene - 7.29 µg/mk
Ethylbenzene - 1.16 µg/mk
m-/p-Xylenes - 4.40 µg/mk
o-Xylene - 1.68 µg/mk
Naphthalene - 0.850 µg/mk
1,2,4-TMB - 4.12 µg/mk
1,3,5-TMB - 1.06 µg/mk
SG-2 (01/31/2024)
PCE - 871 µg/mk
TCE - 5.14 µg/mk
Chloroform - 1.84 µg/mk
Benzene - 1.50 µg/mk
Toluene - 15.5 µg/mk
Ethylbenzene - 5.84 µg/mk
m-/p-Xylenes - 24.0 µg/mk
o-Xylene - 7.63 µg/mk
Naphthalene - 1.76 µg/mk
1,2,4-TMB - 15.4 µg/mk
1,3,5-TMB - 3.49 µg/mk
SG-1 (01/31/2024)
PCE - 2,043,185 µg/mk
TCE - 64,278 µg/mk
cis-1,2-DCE - 23,276 µg/mk
Chloroform - 1,165 µg/mk
1,1,2,2-Tetrachloroethane - 1,336 µg/mk
SG-10 (01/31/2024)
PCE - 236 µg/mk
TCE - 2.63 µg/mk
cis-1,2-DCE - 1.20 µg/mk
Chloroform - 1.99 µg/mk
Benzene - 4.08 µg/mk
Toluene - 14.6 µg/mk
Ethylbenzene - 13.6 µg/mk
m-/p-Xylenes - 53.6 µg/mk
o-Xylene - 53.6 µg/mk
MTBE - 0.806 µg/mk
Naphthalene - 1.13 µg/mk
1,2,4-TMB - 21.7 µg/mk
1,3,5-TMB - 5.39 µg/mk
SG-11 (01/31/2024)
PCE - 1,729,266 µg/mk
TCE - 233,007 µg/mk
cis-1,2-DCE - 157,117 µg/mk
trans-1,2-DCE - 439 µg/mk
Vinyl chloride - 1,072 µg/mk
Benzene - 138 µg/mk
Ethylbenzene - 2,178 µg/mk
m-/p-Xylenes - 317 µg/mk
Chloroform - 650 µg/mk
1,1,2,2-Tetrachloroethane - 6,154 µg/mk
1,2-Dichloropropane - 1,476 µg/mk
1,1-Dichloroethene - 1,939 µg/mk
1,2,4-TMB - 9,101 µg/mk
1,3,5-TMB - 2,001 µg/mk
SG-6 (02/01/2024)
PCE - 133 µg/mk
Chloroform - 0.822 µg/mk
Toluene - 1.96 µg/mk
1,1,2,2-Tetrachloroethane - 6,154 µg/mk
1,2-Dichloropropane - 1,476 µg/mk
1,1-Dichloroethene - 1,939 µg/mk
SG-4 (02/01/2024)
PCE - 1,236 µg/mk
TCE - 9.03 µg/mk
cis-1,2-DCE - 6.04 µg/mk
trans-1,2-DCE - 2.01 µg/mk
1,2-Dichloroethane - 0.445 µg/mk
1,1,2-Trichloroethane - 4.99 µg/mk
Chloroform - 0.570 µg/mk
Benzene - 0.389 µg/mk
Toluene - 3.40 µg/mk
Ethylbenzene - 0.726 µg/mk
m-/p-Xylenes - 3.45 µg/mk
o-Xylene - 1.49 µg/mk
1,2,4-TMB - 2.71 µg/mk
1,3,5-TMB - 0.966 µg/mk
SG-9 (01/31/2024)
PCE - 47.6 µg/mk
TCE - 0.525 µg/mk
cis-1,2-DCE - 0.440 µg/mk
Benzene - 7.02 µg/mk
Ethylbenzene - 1.89 µg/mk
m-/p-Xylenes - 5.10 µg/mk
Chloroform - 0.929 µg/mk
IA-1 (03/15/2024)
PCE - 1.84 µg/mk
Benzene - 1.19 µg/mk
Ethylbenzene - 0.394 µg/mk
m-/p-Xylenes - 1.19 µg/mk
o-Xylenes - 0.631 µg/mk
Chloroform - 0.385 µg/mk
1,2,4-TMB - 0.500 µg/mk
0.5 mile
500 feet
APPROX. SCALE, ft.
0
SHEET:
100
Figure 8
LEGEND
Buffer Radius
Site Boundary
Wetlands Area
Allred & Allred Day Care
WD Mohammed Islamic Center
Otis L. Hairston Middle School
Kidzplay Childcare Inc.
Bessemer Elementary School
Word of Truth Fellowship
Churches
Schools and Daycares
Water Supply Wells - reported
Appendix A
AECOM Standard Operating Procedures

Soil Sampling Using Direct Push Technology ()
Revision 1 June 7, 2017
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 1/2

AECOM – North Carolina Standard Operating Procedures
Soil Sampling Using a Hand Auger

1. Purpose and Scope
Standard operating procedure for the collection of soil samples using a stainless steel hand auger.
2. Procedure
2.1 Required Equipment
 Stainless Steel Hand Auger with extensions
 Gloves (Leather, Latex and/or Nitrile)
 Sample Containers
 Field Logbook
 Sample Labels
 Chain-of-Custody
 Cooler with Ice
 GPS Unit
 Tape Measure
 Bentonite Chips/Portland Cement
 Organic Vapor Analyzer
2.2 Procedure
1. Verify sample collection location, sample identification, and required analyses.
2. Record GPS coordinates as applicable.
3. Assemble clean hand auger and inspect for damage.
4. Don new, uncontaminated gloves.
5. Advance the hand auger into the soil by turning the auger clockwise until the auger bucket is full.
6. Remove the soil from the auger bucket. Use a tape measure to periodically gauge depth of soil boring.
7. Retrieve a sample at interval specified in the scope of work, for screening with an organic vapor analysis
(OVA) meter, such as a photo ionization detector (PID).
8. Samples collected from each boring will be submitted to laboratory for analysis based on the parameters
and goals specific to each work plan.
9. Repeat steps 4 to 7 until the boring termination conditions are met.
10. Backfill soil borings terminated above the water table with native cuttings or bentonite chips. Backfill soil
borings that breach the water table using bentonite.
11. Complete all required documentation, including field logbook entries, soil description, sample container
label, and chain-of-custody form.
12. GPS, flag, stake, or otherwise mark the sample collection locations as necessary.

AECOM
Soil Sampling Using Direct Push Technology ()
Revision 1 June 7, 2017
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 2/2

3. Records
a. Field Notes
b. Equipment Calibration

Groundwater Sampling Using Low-Flow, Minimal-Drawdown Methods (V2)Revision July 2, 2024
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET.1/2
AECOM – North Carolina Standard Operating Procedures
Groundwater Sampling Using Low-Flow, Minimal-
1.Purpose and Scope
Standard operating procedures to collect groundwater samples using low-flow, minimal drawdown techniques.
2.Procedure
2.1 Required Equipment
HASP
Field Note Book and sampling logs.
Dedicated Teflon® tubing, scissors (instrument to cut tubing)
Peristaltic or Submersible Pump
Flexible tubing for peristaltic pump (as necessary)
Electronic water level indicator or oil-water interface probe
Collection container (5-gallon buck or similar container)
PPE
Sample bottles
Calculator
Water Quality Meter with flow through cell
Decontamination
2.2 Procedure
1.Review HASP. The field technician will don nitrile (or other HASP-approved gloves based on
contaminants) gloves for all associated field work and sampling.
2.Open all wells to be sampled and allow equilibration time. Well caps should be placed
adjacent to the monitoring wells on a clean area such as a small piece of plastic or towel.
3.Measure static water levels using the electronic water level indicator, or other similar
device, and utilizing decontamination procedures to decontaminate the water level
indicator before measuring water levels in the first well, between each well, and after
completion of all water level measurements.
4.Sampling should occur in a progression from least to most contaminated monitoring wells.
The tubing or pump should be carefully lowered to the middle of the screened interval or
slightly above the middle (e.g., 2-3 ft below the top of a 5 ft screen) to minimize disturbance
in the well. Only new, dedicated tubing should be used for each sample. If using a
submersible pump, the pump must be properly decontaminated before installation into each
monitoring well.
5.Begin pumping slowly, at approximately 100mL per minute to minimize the risk of over-
pumping the monitoring well and causing drawdown greater than 0.33 ft. The pumping rate
can be gradually increased if drawdown remains below 0.33 ft. Should drawdown greater
than 0.33 ft be observed, the pumping rate should be decreased until drawdown falls below
0.33 ft. If total drawdown exceeds 0.33 ft, the low-flow, minimal drawdown sampling method
of groundwater sampling should be reconsidered and other more appropriate sampling
techniques evaluated.

AECOM
Groundwater Sampling Using Low-Flow, Minimal-Drawdown Methods (V2)Revision July 2, 2024
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET.2/2
6.In-line water quality indicator parameters should be monitored at three to five minute
intervals during purging, dependent on pumping rate. The timing between the interval
readings should not be less than the turnover rate of the groundwater in the flow through
cell. For example, a three-minute interval would be acceptable when using a flow through
cell with a 500mL capacity at a pumping rate of 250mL/min rate. A three-minute reading
interval would not be acceptable when using flow through cell with a 500mL capacity and
pumping of 100mL/min rate.
7.Indicator parameters monitored will include pH, oxidation / redox potential (ORP),
conductivity, dissolved oxygen (DO) and turbidity. Stabilization is achieved after all
parameters have stabilized for three successive readings. Stabilization for the parameters is
considered to be: ± 0.1 for pH, ± 3% for conductivity, ± 10 mv for redox potential, and ± 10%
for turbidity and DO. Depth to groundwater should be collected at each interval to monitor
drawdown.
8.Following stabilization, sampling should be initiated. If using a submersible pump, such as a
bladder pump, the flow through cell should be disconnected or bypassed during sample
collection to avoid cross-contamination. The pumping rate should be decreased as
necessary to minimize loss of volatiles as a result of aeration during the filling of sample
bottles. If a peristaltic pump is used, the monitoring well should be sampled using one of the
below methods:
a.Remove the drop tubing from the inlet side of the pump. Submerge the drop tubing
into the water column while preventing the water in the tubing from flowing back into
the well. Carefully remove the drop tubing from the well and allow the groundwater
to drain into the sample containers. Repeat this process until all sample containers
are filled.
b.Fill the down-well tubing with the peristaltic pump. Once filled, remove the tubing
from the pump while preventing the water in the tubing from flowing back into the
well. Pull the tubing from the well, and then carefully allow the groundwater to drain
into the sample vials. Repeat this process until all sample containers are filled.
c.Use the pump to fill the drop tubing and then withdraw the tubing from the well.
Reverse the flow on the peristaltic pumps to deliver the sample into the sample
containers at a slow, steady rate while taking care not to sample groundwater that
has come into contact with the flexible tubing at the peristaltic pump. Repeat this
process until all sample containers are filled.
Care should be taken during each of these sampling methods to avoid aerating the sample.
9.Volatile and gas sensitive (e.g., Fe2+, CH4, H2 S/HS-, alkalinity) parameters should be
sampled first.
10.Label sample bottles – date, time, project identifier, sample location, depth (if required),
required analysis, preservative (if used), and sampler’s initials. Place samples in cooler with
ice. Complete chain-of-custody form (supplied by the laboratory) and record site activities
in field log book. Pack cooler for shipping or deliver samples to laboratory. Retain a copy of
chain-of-custody and submit other copies with samples. Remove all equipment from the
monitoring well. Close and secure the monitoring well.
3.Records
List of the official records that are generated and support this procedure
a.Field Notes
b.Equipment Calibration Sheets
c.Decontamination Records

Soil Gas Sampling (Rev2)Revision November 2023
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET.1/4
AECOM – North Carolina Standard Operating Procedures
Soil Gas Sampling
1.Purpose and Scope
Standard operating procedure for the collection of soil gas samples using laboratory provided Summa canisters.
2.Procedure
2.1 Required Equipment:
Project Health and Safety Plan (HASP)
Work Plan
Summa Canister with a Flow Regulator from a certified laboratory (pre-calibrated for a 200 ml/min flow rate,
Image-2, A1)
Field forms – Summa Canister Field Sampling Data Sheet
¼” Stainless steel nuts and ferrules
Stainless-steel hand auger
Stainless-steel SGV 6 IN. Screened Implant with Stepped Fitting (AMS Vapor Implants Sampling Method,
Image-1 and Image-2, B1)1/4" OD x 1/8" ID Teflon tubingHammer drill (If soil gas installation is being conducted in a location were concrete/asphalt is present)
Hammer drill bit, diameter size based on size of stainless-steel hand auger
Extension cord
Portable generator (If power is not available and hammer drill is required for installation)
#2 driller sand
Hydraulic cement and/or bentonite
Water
Decontamination equipment
Ziplock bags
Helium detector
Helium
Helium chamber
50mL Syringe with Luer-Lock tip Tedlar bags (Image-2, C1)
Safety Cones
Laminated Sign to notify Air Sampling in progress
Chain of Custody (COC)
FedEx forms Standard wrench setDigital camera3-Way Stopcock Valve (Image-2, D1)Two 1/4 in. O.D. Polypropylene Push-to-Connect Valve (Image-2, E1 & E2)
1/4 in. Push-To-Connect Polypropylene Tee Fitting (Image-2, F1)Shut-in Leak Check Assembly: Image-2, In-line vacuum pressure gauge (G1) and Brass two-way valve (G2).
2.2 Vapor Implant Sampling Method
1.Prior to mobilizing to the field, ensure summa canisters had adequate vacuum for sampling. Additionally, ensure
all summa canister components have been provided by the lab that are necessary to complete the sampling. If
there is any issues with a summa canister, contact the lab immediately for replacement.
2.Prior to intrusive activities, locate any underground utilities to ensure the safety of subsurface work conditions.

AECOM
Soil Gas Sampling (Rev2)Revision November 2023
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET.2/4
3.Use a clean, stainless steel hand auger to auger down to a minimum of 6 feet beneath the ground surface (ft
Bgs). If a minimum depth of 6 ft Bgs cannot be reached, notify the AECOM project manager for the site before
collecting a sample.
Note: Vapor implant should not be placed in saturated soils. Additionally, Soil gas sampling should not occur
during a significant rain event (e.g., 1/2 inch or greater of rainfall during a 24-hour period). A minimum of 5 days
after a significant rain event or 5 days after watering has stopped in areas that are irrigated to complete soil gas
sampling. This does not apply to areas where infiltration has not occurred, such as under buildings or high-
integrity pavement.
4.Attach Teflon tubing to the barbed tang of a 6” AMS Vapor Implant (AMS Item #21010). Make sure that the
connection between the barbed end of the implant and the Teflon tubing is secure.
*Stainless Steel SGV 6 IN. Screened Implant with Stepped Fitting (Image-1)
5.Lower the AMS Vapor Implant and attached tubing into the borehole until the Implant reaches the desired depth.
The top of the vapor implant should be a minimum of five feet below ground surface.
6.Cut the tubing to the desired length so that you have approximately 2’ of extra tubing to attach to the summa
canister.
7.Using #2A filter sand, add enough sand to cover the 6” Implant and 2-3” above the Implant. Check the depth of
sand using a measuring tape. The top of the sand should be a minimum of five feet below ground surface.
8.Add hydraulic cement or bentonite above the top of the sand to the surface to create a seal. If using cement,
place a thin layer of 1-2 inches of dry bentonite above the sand pack to prevent the cement from intruding into
the sand pack before it hardens. If using bentonite, hydrate the bentonite to ensure a proper seal. Wait 2 hours
or until the hydraulic cement has fully hardened, whichever is longer.
9.Use a syringe to purge the subsurface air through the Teflon tubing. Purge a maximum of three pore volume of
the borehole. The pore volume should be a minimum of the volume of the tubing and sand filter pack.
Calculate pore volume using formula: v = π ra2La + π rt2Lt where:
v =Volume
La =Length of sand-filled annular space, and
ra =Radius of annular space
Lt =Length of tubing, and
rt =Radius of tubing
10.Thread the tubing through the helium leak test device (helium chamber).
11.Connect the Teflon tubing from the soil gas point to a 2-way valve (Image-2, E1) and use Teflon tubing to
connect the 2-way valve (Image-2, E1) to the tee fitting (Image-2, F1).
12.Connect Teflon tubing to the stainless-steel summa canister (Image-2, A1) using air-tight stainless-steel fittings
and then connect the Teflon tubing to tee fitting (Image-2, F1).

AECOM
Soil Gas Sampling (Rev2)Revision November 2023
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET.3/4
13.Connect Teflon tubing to the last open connection on the tee fitting (Image-2, F1) then connect the Teflon tubing
to a 2-way valve (Image-2, E2).
14.Connect the 2-way valve (Image-2, E2) to the in line Shut-in Leak Check Assembly (Image-2: G1 and G2).
15.Connect the in line Shut-in Leak Check Assembly (Image-2: G1 and G2) to the 3-way stopcock valve (Image-2,
D1). One connection will be used to apply a vacuum using a syringe (Image-2, C1) and one connection will be
connected to a Tedlar bag.
16.Conduct the leak test and shut-in test as outlined in Section 3.
17.After the completion of the leak test and shut-in test, utilize the laboratory supplied flow controller to pull the
sample over the desired time interval. The extraction rate of the summa canister should not exceed 200 ml/min.
18.To remove the stainless-steel Implant, break up the hydraulic seal. Tug gently on the Teflon tubing until the
Implant is freed.
19.Remove the Teflon tubing from the barb and dispose of the tubing and the disposable stainless-steel Implant.
20.Backfill borehole with hydraulic cement.
3.Leak Test and Shut-In Test Procedure
1.Close the 2-way valve closest to the soil gas point (Image-2, E1).
2.Use a syringe (Image-2, C1) to extract a negative pressure of approximately 10-inches of mercury (inHg) to the
sample train.
* Shut-In Test Procedure (Image-2)

AECOM
Soil Gas Sampling (Rev2)Revision November 2023
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3.Close the 2-way brass valve (Image-2, G2) between the vacuum pressure gauge (Image-2, G1) and the vacuum
pump or syringe (Image-2, C1).
4.Record the initial negative pressure displayed on the vacuum pressure gauge (Image-2, G1).
5.Monitor the vacuum pressure gauge (Image-2, G1) for 5 minutes. Ensure that the negative pressure does not
decrease by more than 1-inHg.
6.Record the negative pressure reading on the summa cannister field data sheet. If the reading has dropped less
than 1-inHg, proceed to the next step. If the negative pressure reading has dropped more than 1-inHg,
reconstruct the sample train as necessary and repeat the test.
7.Close the 2-way valve (Image-2, E2) between the vacuum pressure gauge (Image-2, G1) and the tee fitting
(Image-2, F1).
8.Open the 2-way valve (Image-2, E1) between the tee fitting (Image-2, F1) and the soil gas point.
9.Monitor the vacuum presusure gauge for 5 minutes. Ensure that the negative pressure does not decrease by
more than 1-inHg.
10.Record the negative pressure reading. If the reading has dropped by less than 1-inHg, proceed to the next step.
If the negative pressure reading has dropped by more than 1-inHg, reconstruct the sample train as necessary
and repeat the test.
11.Open all 2-way valves (Image-2, E2 and G2) between the syringe (Image-2, C1) and the tee fitting (Image-2,
G1).
12.Attach the helium detector to the helium chamber. Attach the helium container to the helium chamber using
teflon tubing and fill the helium chamber with helium until the helium detector reads >50%.
13.Use the syringe to fill a 1 Liter Tedlar bag with air from the sample port. This can be done by filling the syringe
with the 3-way stopcock valve (Image-2, D1) to the Tedlar bag closed and the connection to the soil gas point
open and emptying the syringe with the 3-way stopcock valve (Image-2, D1) to the Tedlar bag open and the
connection to the soil gas point closed.
14.Close the Tedlar bag and detach it from the pump.
15.Turn off the flow of helium into the helium leak test device.
16.Remove the helium detector from the leak test device and allow the helium detector reading to reach 0 ppm.
17.Insert the helium detector into the silicon tubing attached to the Tedlar bag and open valve on the bag.
18.Record the reading. If the reading is below 10% of the value measured within the test device, proceed to the
next step. If the reading is above 10%, repeat the leak test and reconstruct the sample point as necessary.
19.Be sure that the valve to the Tedlar bag is open and that nothing is blocking the flow to the helium detector. The
detector may produce false readings if the detector pump is strained or if methane is present in the soil gas.
4.Records
a.Summa Canister Field Data Sheet
b.Equipment Calibration Sheets
5.Attachments
a.Summa Canister Field Data Sheet

Indoor Air Sampling SOP ()Revision June 4, 2017
PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET.1/3
AECOM – North Carolina Standard Operating Procedures
Indoor Air Sampling SOP
1.Purpose and Scope
Standard operating procedures for the collection of an indoor air sample using a laboratory provided
Summa canister.
2.Procedure
2.1 Required Equipment
Project Health and Safety Plan (HASP)
Work Plan
6 Liter Summa Canister with a Flow Regulator from a
certified laboratory (precalibrated for an 8 hour interval)Field forms –Building Survey form (Attachment 1),
Summa Canister Field Sampling Data Sheet
(Attachment 2)
¼” Stainless steel nuts and ferrules
1/4" OD x 1/8" ID Teflon tubing
Safety Cones
Laminated Sign to notify Air Sampling in progress
Chain of Custody (COC)
Shipping forms, if needed
Standard wrench set
Digital camera
2.2 Sampling Protocol
1.Select an indoor sampling location in the area of
highest subsurface contamination and/or the
location with the most traffic, if known.
2.If this information is not available, select a sampling
location near the center of the building.
3.The inlet of the sample should be at breathing height (between 3 feet and 5 feet above the floor).
4.If a stand or table is available, place the canister on the stand or table for sample collection.

AECOM
Indoor Air Sampling SOP ()Revision June 4, 2017
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5.If necessary, attach a short length of stainless-steel or Teflon tubing to the summa canister using
stainless steel air tight fittings and anchor the inlet of the tubing so that it is located at breathing
height (e.g., with a zip-tie).
6.Select an ambient air sampling location that is representative of
the heating, ventilation, and air conditioning (HVAC) system
inlet air for the building if an HVAC system is operating.
7.If the HVAC inlet is on the side of the building, locate the
summa canister inlet near the HVAC inlet.
8.If the HVAC inlet is on the roof of the building, locate the
summa canister inlet on the roof using the safest method
available.
9.If there is no HVAC inlet, select a monitoring location
immediately upwind of the building. Avoid sampling near walls,
under trees, or other areas with obstructed air flow.
10.Connect the Teflon tubing (if applicable) to the summa canister
using air tight stainless steel fittings.
11.Document the sampling locations using a tape measure.
12.Note the characteristics of the building, including cracks in the
floor, a list of chemicals (including the brand name of the
chemical, the quantity and the location) present in the building
that may affect results, and other pertinent information.
13.Complete the field forms and include as much detail as possible. A blank building survey form is
included in Attachment 1.
14.Check the canister vacuum with a dedicated gauge (i.e., check all canisters with the same
gauge. The vacuum should be about -28 to -29” Hg. If any canister differs from the others by 3”
Hg or more, do not use that canister.
15.Attach the summa canisters and flow controllers to the Teflon tubing (if applicable) using the
stainless steel fittings provided by the laboratory.
16.Set up both the ambient air and indoor air canisters prior to opening the canister valves.
17.Place safety cones and “Air Sample in Progress” signs around the sampling locations as
necessary.
18.Open the ambient air or indoor air canister valve and record the time and vacuum gauge reading
(if there is a built-in vacuum gauge). Complete the Summa Canister Field Data sheet
(Attachment 2).
19.Repeat this process on the other canister as soon as possible.
Figure 2: Summa Canister

AECOM
Indoor Air Sampling SOP ()Revision June 4, 2017
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20.The vacuum should decrease as determined by the flow controller requested from the
laboratory. Typically an 8 hour flow controller is requested. Record the final times and vacuums
prior to closing the valves.
21.Close the valves at approximately the same time.
22.Label the canisters and fill out the chain of custody.
23.The laboratory will analyze the sample using Method TO-15 SIM (Selected Ion Method).
Typically, a list of analytes will be chosen that is specific to the program.
24.Ship the canister to the laboratory.
25.Clean up and remove all sampling materials from the site.
3.Records
a.Building Survey Form
b.Summa Canister Field Data Sheet
4.Attachments
a.Building Survey Form
b.Summa Canister Field Data sheet
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Appendix B
Soil Boring Logs
Concrete and fill
Red-brown silty CLAY, low plasticity, mild odor
10
9
8
7
6
5
4
3
2
1
0
CL
Boring Terminated 5 feet below ground surface
608 Elwell Avenue
EM/TB
NA
Hand Auger
HA
60722767
SB-3
NA NA
5
1/31/2024 1/31/20244EM
NA
NA
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description
DEPTH TO WATER:
Wa
t
e
r

L
e
v
e
l
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767SB-3
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
App. B
Soil Boring LogNOTES:
Concrete and fill
Red-brown silty CLAY with gravel, low plasticity, no odor
10
9
8
7
6
5
4
3
2
1
0
CL
Boring Terminated 5 feet below ground surface
608 Elwell Avenue
EM/TB
NA
Hand Auger
HA
60722767
SB-4
NA NA
5
1/31/2024 1/31/20244EM
NA
NA
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description
DEPTH TO WATER:
Wa
t
e
r

L
e
v
e
l
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767SB-4
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
App. B
Soil Boring LogNOTES:
Gravel and organic soil
Brown silty CLAY, moist, no odor
10
9
8
7
6
5
4
3
2
1
0
CL
Boring Terminated 5 feet below ground surface
608 Elwell Avenue
EM/TB
NA
Hand Auger
HA
60722767
SB-5
NA NA
5
1/29/2024 1/29/20244TB
NA
NA
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description
DEPTH TO WATER:
Wa
t
e
r

L
e
v
e
l
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767SB-5
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
App. B
Soil Boring LogNOTES:
Organic soil
Red-brown silty CLAY
10
9
8
7
6
5
4
3
2
1
0
CL
Boring Terminated 5 feet below ground surface
608 Elwell Avenue
EM/TB
NA
Hand Auger
HA
60722767
SB-6
NA NA
5
1/30/2024 1/30/20244TB
NA
NA
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description
DEPTH TO WATER:
Wa
t
e
r

L
e
v
e
l
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767SB-6
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
App. B
Soil Boring LogNOTES:
Organic soil, gravel, glass
Red-brown silty CLAY with sand, no odor
10
9
8
7
6
5
4
3
2
1
0
CL
Boring Terminated 5 feet below ground surface
608 Elwell Avenue
EM/TB
NA
Hand Auger
HA
60722767
SB-7
NA NA
5
1/29/2024 1/29/20244TB
NA
NA
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description
DEPTH TO WATER:
Wa
t
e
r

L
e
v
e
l
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767SB-7
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
App. B
Soil Boring LogNOTES:
Red-brown silty CLAY, no odor
10
9
8
7
6
5
4
3
2
1
0
CL
Boring Terminated 5 feet below ground surface
608 Elwell Avenue
EM/TB
NA
Hand Auger
HA
60722767
SB-8
NA NA
5
1/29/2024 1/29/20244EM
NA
NA
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description
DEPTH TO WATER:
Wa
t
e
r

L
e
v
e
l
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767SB-8
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
App. B
Soil Boring LogNOTES:
Gravel and organic soil
Brown silty CLAY, moist, no odor
10
9
8
7
6
5
4
3
2
1
0
CL
Boring Terminated 5 feet below ground surface
608 Elwell Avenue
EM/TB
NA
Hand Auger
HA
60722767
SB-9
NA NA
5
1/29/2024 1/29/20244TB
NA
NA
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description
DEPTH TO WATER:
Wa
t
e
r

L
e
v
e
l
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767SB-9
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
App. B
Soil Boring LogNOTES:
Gravel
Brown silty CLAY, moist to wet, no odor
10
9
8
7
6
5
4
3
2
1
0
CL
Boring Terminated 5 feet below ground surface
608 Elwell Avenue
EM/TB
NA
Hand Auger
HA
60722767
SB-10
NA NA
5
1/30/2024 1/30/20244TB
NA
NA
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description
DEPTH TO WATER:
Wa
t
e
r

L
e
v
e
l
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767SB-10
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
App. B
Soil Boring LogNOTES:
Gravel
Red-brown silty CLAY with sand, no odor
10
9
8
7
6
5
4
3
2
1
0
CL
Boring Terminated 5 feet below ground surface
608 Elwell Avenue
EM/TB
NA
Hand Auger
HA
60722767
SB-11
NA NA
5
1/30/2024 1/30/20244TB
NA
NA
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description
DEPTH TO WATER:
Wa
t
e
r

L
e
v
e
l
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767SB-11
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
App. B
Soil Boring LogNOTES:
Appendix C
Laboratory Analytical Reports
ANALYTICAL REPORT
February 16, 2024
AECOM - Raleigh, NC
Sample Delivery Group:L1701794
Samples Received:02/02/2024
Project Number:60722767
Description:Frye and Webster DC410064
Site:DC410064
Report To:Stephanie Hempel
5438 Wade Park Blvd.
Suite 200
Raleigh, NC 27607
Entire Report Reviewed By:
February 16, 2024
[Preliminary Report]
Chris McCord
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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February 19, 2024
Chris McCord
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 6
Sr: Sample Results 7
SB-8 0-1 L1701794-01 7
SB-8 1-2 L1701794-02 10
SB-7 (0-1) L1701794-03 13
SB-7 (3-4) L1701794-04 16
SB-9 (0-1) L1701794-05 19
SB-9 (1-2) L1701794-06 22
SB-11 0-1 L1701794-07 25
SB-11 1-2 L1701794-08 28
SB-6 0-1 L1701794-09 31
SB-6 1-2 L1701794-10 34
SB-4 0-1 L1701794-11 37
SB-4 2-3 L1701794-12 40
SB-3 0-1 L1701794-13 43
SB-3 1-2 L1701794-14 46
SB-5 0-1 L1701794-15 49
SB-5 4-5 L1701794-16 52
SB-10 0-1 L1701794-17 55
SB-10 3-4 L1701794-18 58
Qc: Quality Control Summary 61
Total Solids by Method 2540 G-2011 61
Volatile Organic Compounds (GC/MS) by Method 8260D 64
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 69
Gl: Glossary of Terms 85
Al: Accreditations & Locations 87
Sc: Sample Chain of Custody 88
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-8 0-1 L1701794-01 Solid EM/TB 01/29/24 13:50 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219975 1 02/06/24 15:41 02/06/24 15:57 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 13:50 02/05/24 20:59 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220589 1 02/06/24 17:05 02/07/24 08:17 JCH Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-8 1-2 L1701794-02 Solid EM/TB 01/29/24 14:00 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 14:00 02/05/24 21:31 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2221334 1 02/07/24 08:21 02/09/24 04:28 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-7 (0-1) L1701794-03 Solid EM/TB 01/29/24 14:35 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 14:35 02/05/24 21:50 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 19:42 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-7 (3-4) L1701794-04 Solid EM/TB 01/29/24 14:35 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 14:35 02/05/24 22:08 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 18:20 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-9 (0-1) L1701794-05 Solid EM/TB 01/29/24 15:15 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 15:15 02/05/24 22:27 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/09/24 00:29 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-9 (1-2) L1701794-06 Solid EM/TB 01/29/24 15:20 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 15:20 02/05/24 22:46 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 18:41 AMS Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-11 0-1 L1701794-07 Solid EM/TB 01/30/24 09:05 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/30/24 09:05 02/05/24 23:06 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 19:22 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-11 1-2 L1701794-08 Solid EM/TB 01/30/24 09:15 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/30/24 09:15 02/05/24 23:25 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 19:01 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-6 0-1 L1701794-09 Solid EM/TB 01/30/24 14:45 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/30/24 14:45 02/05/24 23:44 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/09/24 00:09 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-6 1-2 L1701794-10 Solid EM/TB 01/30/24 14:55 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/30/24 14:55 02/06/24 00:03 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 20:03 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-4 0-1 L1701794-11 Solid EM/TB 01/31/24 10:45 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2219977 1 02/06/24 10:56 02/06/24 11:02 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/31/24 10:45 02/06/24 00:23 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/15/24 06:11 JRM Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-4 2-3 L1701794-12 Solid EM/TB 01/31/24 10:50 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2220127 1 02/06/24 15:18 02/06/24 15:26 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/31/24 10:50 02/06/24 00:42 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 20:23 AMS Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-3 0-1 L1701794-13 Solid EM/TB 01/31/24 10:55 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2220127 1 02/06/24 15:18 02/06/24 15:26 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/31/24 10:55 02/06/24 01:01 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2224617 20 01/31/24 10:55 02/13/24 12:22 ACG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 21:04 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-3 1-2 L1701794-14 Solid EM/TB 01/31/24 11:00 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2220127 1 02/06/24 15:18 02/06/24 15:26 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/31/24 11:00 02/06/24 01:20 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 20:44 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-5 0-1 L1701794-15 Solid EM/TB 01/29/24 16:30 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2220127 1 02/06/24 15:18 02/06/24 15:26 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 16:30 02/06/24 01:39 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/09/24 19:56 DSH Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-5 4-5 L1701794-16 Solid EM/TB 01/29/24 16:35 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2220127 1 02/06/24 15:18 02/06/24 15:26 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 16:35 02/06/24 01:58 GLN Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2224617 1 01/29/24 16:35 02/13/24 12:00 ACG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 21:45 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-10 0-1 L1701794-17 Solid EM/TB 01/29/24 16:45 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2220127 1 02/06/24 15:18 02/06/24 15:26 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 16:45 02/06/24 02:17 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 22:06 AMS Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-10 3-4 L1701794-18 Solid EM/TB 01/29/24 16:50 02/02/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2220127 1 02/06/24 15:18 02/06/24 15:26 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2220500 1 01/29/24 16:50 02/06/24 02:40 DWR Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2220590 1 02/07/24 08:09 02/08/24 21:25 AMS Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris McCord
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Chris McCord
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1701794
SB-8 0-1
Collected date/time: 01/29/24 13:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.5 1 02/06/2024 15:57 WG2219975
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0582 0.0797 1 02/05/2024 20:59 WG2220500
Acrylonitrile U 0.00575 0.0199 1 02/05/2024 20:59 WG2220500
Benzene U 0.000744 0.00159 1 02/05/2024 20:59 WG2220500
Bromobenzene U 0.00143 0.0199 1 02/05/2024 20:59 WG2220500
Bromodichloromethane U 0.00116 0.00399 1 02/05/2024 20:59 WG2220500
Bromoform U 0.00187 0.0399 1 02/05/2024 20:59 WG2220500
Bromomethane U 0.00314 0.0199 1 02/05/2024 20:59 WG2220500
n-Butylbenzene U 0.00837 0.0199 1 02/05/2024 20:59 WG2220500
sec-Butylbenzene U 0.00459 0.0199 1 02/05/2024 20:59 WG2220500
tert-Butylbenzene U 0.00311 0.00797 1 02/05/2024 20:59 WG2220500
Carbon tetrachloride U 0.00143 0.00797 1 02/05/2024 20:59 WG2220500
Chlorobenzene U 0.000335 0.00399 1 02/05/2024 20:59 WG2220500
Chlorodibromomethane U 0.000976 0.00399 1 02/05/2024 20:59 WG2220500
Chloroethane U 0.00271 0.00797 1 02/05/2024 20:59 WG2220500
Chloroform 0.00255 B J 0.00164 0.00399 1 02/05/2024 20:59 WG2220500
Chloromethane U 0.00693 0.0199 1 02/05/2024 20:59 WG2220500
2-Chlorotoluene U 0.00138 0.00399 1 02/05/2024 20:59 WG2220500
4-Chlorotoluene U 0.000717 0.00797 1 02/05/2024 20:59 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00622 0.0399 1 02/05/2024 20:59 WG2220500
1,2-Dibromoethane U 0.00103 0.00399 1 02/05/2024 20:59 WG2220500
Dibromomethane U 0.00120 0.00797 1 02/05/2024 20:59 WG2220500
1,2-Dichlorobenzene U 0.000678 0.00797 1 02/05/2024 20:59 WG2220500
1,3-Dichlorobenzene U 0.000956 0.00797 1 02/05/2024 20:59 WG2220500
1,4-Dichlorobenzene U 0.00112 0.00797 1 02/05/2024 20:59 WG2220500
Dichlorodifluoromethane U 0.00257 0.00797 1 02/05/2024 20:59 WG2220500
1,1-Dichloroethane U 0.000783 0.00399 1 02/05/2024 20:59 WG2220500
1,2-Dichloroethane U 0.00103 0.00399 1 02/05/2024 20:59 WG2220500
1,1-Dichloroethene U 0.000966 0.00399 1 02/05/2024 20:59 WG2220500
cis-1,2-Dichloroethene U 0.00117 0.00399 1 02/05/2024 20:59 WG2220500
trans-1,2-Dichloroethene U 0.00166 0.00797 1 02/05/2024 20:59 WG2220500
1,2-Dichloropropane U 0.00226 0.00797 1 02/05/2024 20:59 WG2220500
1,1-Dichloropropene U 0.00129 0.00399 1 02/05/2024 20:59 WG2220500
1,3-Dichloropropane U 0.000799 0.00797 1 02/05/2024 20:59 WG2220500
cis-1,3-Dichloropropene U 0.00121 0.00399 1 02/05/2024 20:59 WG2220500
trans-1,3-Dichloropropene U 0.00182 0.00797 1 02/05/2024 20:59 WG2220500
2,2-Dichloropropane U 0.00220 0.00399 1 02/05/2024 20:59 WG2220500
Di-isopropyl ether U 0.000654 0.00159 1 02/05/2024 20:59 WG2220500
Ethylbenzene U 0.00117 0.00399 1 02/05/2024 20:59 WG2220500
Hexachloro-1,3-butadiene U 0.00956 0.0399 1 02/05/2024 20:59 WG2220500
Isopropylbenzene U 0.000678 0.00399 1 02/05/2024 20:59 WG2220500
p-Isopropyltoluene U 0.00407 0.00797 1 02/05/2024 20:59 WG2220500
2-Butanone (MEK)U 0.101 0.159 1 02/05/2024 20:59 WG2220500
Methylene Chloride 0.0110 B J 0.0106 0.0399 1 02/05/2024 20:59 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00363 0.0399 1 02/05/2024 20:59 WG2220500
Methyl tert-butyl ether U 0.000558 0.00159 1 02/05/2024 20:59 WG2220500
Naphthalene U C3 0.00778 0.0199 1 02/05/2024 20:59 WG2220500
n-Propylbenzene U 0.00151 0.00797 1 02/05/2024 20:59 WG2220500
Styrene U 0.000365 0.0199 1 02/05/2024 20:59 WG2220500
1,1,1,2-Tetrachloroethane U 0.00151 0.00399 1 02/05/2024 20:59 WG2220500
1,1,2,2-Tetrachloroethane U 0.00111 0.00399 1 02/05/2024 20:59 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 7 of 89
SAMPLE RESULTS - 01
L1701794
SB-8 0-1
Collected date/time: 01/29/24 13:50
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00120 0.00399 1 02/05/2024 20:59 WG2220500
Tetrachloroethene U 0.00143 0.00399 1 02/05/2024 20:59 WG2220500
Toluene U 0.00207 0.00797 1 02/05/2024 20:59 WG2220500
1,2,3-Trichlorobenzene U 0.0117 0.0199 1 02/05/2024 20:59 WG2220500
1,2,4-Trichlorobenzene U 0.00701 0.0199 1 02/05/2024 20:59 WG2220500
1,1,1-Trichloroethane U 0.00147 0.00399 1 02/05/2024 20:59 WG2220500
1,1,2-Trichloroethane U 0.000952 0.00399 1 02/05/2024 20:59 WG2220500
Trichloroethene U J4 0.000931 0.00159 1 02/05/2024 20:59 WG2220500
Trichlorofluoromethane U 0.00132 0.00399 1 02/05/2024 20:59 WG2220500
1,2,3-Trichloropropane U 0.00258 0.0199 1 02/05/2024 20:59 WG2220500
1,2,4-Trimethylbenzene U 0.00252 0.00797 1 02/05/2024 20:59 WG2220500
1,2,3-Trimethylbenzene U 0.00252 0.00797 1 02/05/2024 20:59 WG2220500
1,3,5-Trimethylbenzene U 0.00319 0.00797 1 02/05/2024 20:59 WG2220500
Vinyl chloride U 0.00185 0.00399 1 02/05/2024 20:59 WG2220500
Xylenes, Total U 0.00140 0.0104 1 02/05/2024 20:59 WG2220500
(S) Toluene-d8 104 75.0-131 02/05/2024 20:59 WG2220500
(S) 4-Bromofluorobenzene 98.1 67.0-138 02/05/2024 20:59 WG2220500
(S) 1,2-Dichloroethane-d4 114 70.0-130 02/05/2024 20:59 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00678 0.0419 1 02/07/2024 08:17 WG2220589
Acenaphthylene U 0.00590 0.0419 1 02/07/2024 08:17 WG2220589
Anthracene U 0.00746 0.0419 1 02/07/2024 08:17 WG2220589
Benzidine U 0.0788 2.10 1 02/07/2024 08:17 WG2220589
Benzo(a)anthracene U 0.00739 0.0419 1 02/07/2024 08:17 WG2220589
Benzo(b)fluoranthene U 0.00781 0.0419 1 02/07/2024 08:17 WG2220589
Benzo(k)fluoranthene U 0.00745 0.0419 1 02/07/2024 08:17 WG2220589
Benzo(g,h,i)perylene U 0.00766 0.0419 1 02/07/2024 08:17 WG2220589
Benzo(a)pyrene U 0.00779 0.0419 1 02/07/2024 08:17 WG2220589
Bis(2-chlorethoxy)methane U 0.0126 0.419 1 02/07/2024 08:17 WG2220589
Bis(2-chloroethyl)ether U 0.0138 0.419 1 02/07/2024 08:17 WG2220589
2,2-Oxybis(1-Chloropropane)U 0.0181 0.419 1 02/07/2024 08:17 WG2220589
4-Bromophenyl-phenylether U 0.0147 0.419 1 02/07/2024 08:17 WG2220589
2-Chloronaphthalene U 0.00736 0.0419 1 02/07/2024 08:17 WG2220589
4-Chlorophenyl-phenylether U 0.0146 0.419 1 02/07/2024 08:17 WG2220589
Chrysene U 0.00833 0.0419 1 02/07/2024 08:17 WG2220589
Dibenz(a,h)anthracene U 0.0116 0.0419 1 02/07/2024 08:17 WG2220589
1,2-Dichlorobenzene U 0.0124 0.419 1 02/07/2024 08:17 WG2220589
1,3-Dichlorobenzene U 0.0127 0.419 1 02/07/2024 08:17 WG2220589
1,4-Dichlorobenzene U 0.0125 0.419 1 02/07/2024 08:17 WG2220589
3,3-Dichlorobenzidine U 0.0155 0.419 1 02/07/2024 08:17 WG2220589
2,4-Dinitrotoluene U 0.0120 0.419 1 02/07/2024 08:17 WG2220589
2,6-Dinitrotoluene U 0.0137 0.419 1 02/07/2024 08:17 WG2220589
Fluoranthene U 0.00756 0.0419 1 02/07/2024 08:17 WG2220589
Fluorene U 0.00682 0.0419 1 02/07/2024 08:17 WG2220589
Hexachlorobenzene U 0.0148 0.419 1 02/07/2024 08:17 WG2220589
Hexachloro-1,3-butadiene U 0.0141 0.419 1 02/07/2024 08:17 WG2220589
Hexachlorocyclopentadiene U 0.0220 0.419 1 02/07/2024 08:17 WG2220589
Hexachloroethane U 0.0165 0.419 1 02/07/2024 08:17 WG2220589
Indeno(1,2,3-cd)pyrene U 0.0118 0.0419 1 02/07/2024 08:17 WG2220589
Isophorone U 0.0128 0.419 1 02/07/2024 08:17 WG2220589
Naphthalene U 0.0105 0.0419 1 02/07/2024 08:17 WG2220589
Nitrobenzene U 0.0146 0.419 1 02/07/2024 08:17 WG2220589
n-Nitrosodimethylamine U 0.0622 0.419 1 02/07/2024 08:17 WG2220589
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 8 of 89
SAMPLE RESULTS - 01
L1701794
SB-8 0-1
Collected date/time: 01/29/24 13:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0317 0.419 1 02/07/2024 08:17 WG2220589
n-Nitrosodi-n-propylamine U 0.0140 0.419 1 02/07/2024 08:17 WG2220589
Phenanthrene U 0.00832 0.0419 1 02/07/2024 08:17 WG2220589
Benzylbutyl phthalate U 0.0131 0.419 1 02/07/2024 08:17 WG2220589
Bis(2-ethylhexyl)phthalate U 0.0531 0.419 1 02/07/2024 08:17 WG2220589
Di-n-butyl phthalate U 0.0143 0.419 1 02/07/2024 08:17 WG2220589
Diethyl phthalate U 0.0138 0.419 1 02/07/2024 08:17 WG2220589
Dimethyl phthalate U 0.0888 0.419 1 02/07/2024 08:17 WG2220589
Di-n-octyl phthalate U 0.0283 0.419 1 02/07/2024 08:17 WG2220589
Pyrene U 0.00815 0.0419 1 02/07/2024 08:17 WG2220589
1,2,4-Trichlorobenzene U 0.0131 0.419 1 02/07/2024 08:17 WG2220589
4-Chloro-3-methylphenol U 0.0136 0.419 1 02/07/2024 08:17 WG2220589
2-Chlorophenol U 0.0138 0.419 1 02/07/2024 08:17 WG2220589
2,4-Dichlorophenol U 0.0122 0.419 1 02/07/2024 08:17 WG2220589
2,4-Dimethylphenol U 0.0109 0.419 1 02/07/2024 08:17 WG2220589
4,6-Dinitro-2-methylphenol U 0.0950 0.419 1 02/07/2024 08:17 WG2220589
2,4-Dinitrophenol U 0.0980 0.419 1 02/07/2024 08:17 WG2220589
2-Nitrophenol U 0.0150 0.419 1 02/07/2024 08:17 WG2220589
4-Nitrophenol U 0.0131 0.419 1 02/07/2024 08:17 WG2220589
Pentachlorophenol U 0.0113 0.419 1 02/07/2024 08:17 WG2220589
Phenol U 0.0169 0.419 1 02/07/2024 08:17 WG2220589
2,4,6-Trichlorophenol U 0.0135 0.419 1 02/07/2024 08:17 WG2220589
(S) 2-Fluorophenol 64.3 12.0-120 02/07/2024 08:17 WG2220589
(S) Phenol-d5 58.7 10.0-120 02/07/2024 08:17 WG2220589
(S) Nitrobenzene-d5 62.2 10.0-122 02/07/2024 08:17 WG2220589
(S) 2-Fluorobiphenyl 58.9 15.0-120 02/07/2024 08:17 WG2220589
(S) 2,4,6-Tribromophenol 65.8 10.0-127 02/07/2024 08:17 WG2220589
(S) p-Terphenyl-d14 65.2 10.0-120 02/07/2024 08:17 WG2220589
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/16/24 11:51 9 of 89
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 9 of 89
SAMPLE RESULTS - 02
L1701794
SB-8 1-2
Collected date/time: 01/29/24 14:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.8 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0540 0.0739 1 02/05/2024 21:31 WG2220500
Acrylonitrile U 0.00534 0.0185 1 02/05/2024 21:31 WG2220500
Benzene U 0.000691 0.00148 1 02/05/2024 21:31 WG2220500
Bromobenzene U 0.00133 0.0185 1 02/05/2024 21:31 WG2220500
Bromodichloromethane U 0.00107 0.00370 1 02/05/2024 21:31 WG2220500
Bromoform U 0.00173 0.0370 1 02/05/2024 21:31 WG2220500
Bromomethane U 0.00291 0.0185 1 02/05/2024 21:31 WG2220500
n-Butylbenzene U 0.00776 0.0185 1 02/05/2024 21:31 WG2220500
sec-Butylbenzene U 0.00426 0.0185 1 02/05/2024 21:31 WG2220500
tert-Butylbenzene U 0.00288 0.00739 1 02/05/2024 21:31 WG2220500
Carbon tetrachloride U 0.00133 0.00739 1 02/05/2024 21:31 WG2220500
Chlorobenzene U 0.000311 0.00370 1 02/05/2024 21:31 WG2220500
Chlorodibromomethane U 0.000905 0.00370 1 02/05/2024 21:31 WG2220500
Chloroethane U 0.00251 0.00739 1 02/05/2024 21:31 WG2220500
Chloroform 0.00243 B J 0.00152 0.00370 1 02/05/2024 21:31 WG2220500
Chloromethane U 0.00643 0.0185 1 02/05/2024 21:31 WG2220500
2-Chlorotoluene U 0.00128 0.00370 1 02/05/2024 21:31 WG2220500
4-Chlorotoluene U 0.000666 0.00739 1 02/05/2024 21:31 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00577 0.0370 1 02/05/2024 21:31 WG2220500
1,2-Dibromoethane U 0.000958 0.00370 1 02/05/2024 21:31 WG2220500
Dibromomethane U 0.00111 0.00739 1 02/05/2024 21:31 WG2220500
1,2-Dichlorobenzene U 0.000629 0.00739 1 02/05/2024 21:31 WG2220500
1,3-Dichlorobenzene U 0.000887 0.00739 1 02/05/2024 21:31 WG2220500
1,4-Dichlorobenzene U 0.00104 0.00739 1 02/05/2024 21:31 WG2220500
Dichlorodifluoromethane U 0.00238 0.00739 1 02/05/2024 21:31 WG2220500
1,1-Dichloroethane U 0.000726 0.00370 1 02/05/2024 21:31 WG2220500
1,2-Dichloroethane U 0.000960 0.00370 1 02/05/2024 21:31 WG2220500
1,1-Dichloroethene U 0.000896 0.00370 1 02/05/2024 21:31 WG2220500
cis-1,2-Dichloroethene U 0.00109 0.00370 1 02/05/2024 21:31 WG2220500
trans-1,2-Dichloroethene U 0.00154 0.00739 1 02/05/2024 21:31 WG2220500
1,2-Dichloropropane U 0.00210 0.00739 1 02/05/2024 21:31 WG2220500
1,1-Dichloropropene U 0.00120 0.00370 1 02/05/2024 21:31 WG2220500
1,3-Dichloropropane U 0.000741 0.00739 1 02/05/2024 21:31 WG2220500
cis-1,3-Dichloropropene U 0.00112 0.00370 1 02/05/2024 21:31 WG2220500
trans-1,3-Dichloropropene U 0.00169 0.00739 1 02/05/2024 21:31 WG2220500
2,2-Dichloropropane U 0.00204 0.00370 1 02/05/2024 21:31 WG2220500
Di-isopropyl ether U 0.000606 0.00148 1 02/05/2024 21:31 WG2220500
Ethylbenzene U 0.00109 0.00370 1 02/05/2024 21:31 WG2220500
Hexachloro-1,3-butadiene U 0.00887 0.0370 1 02/05/2024 21:31 WG2220500
Isopropylbenzene U 0.000629 0.00370 1 02/05/2024 21:31 WG2220500
p-Isopropyltoluene U 0.00377 0.00739 1 02/05/2024 21:31 WG2220500
2-Butanone (MEK)U 0.0939 0.148 1 02/05/2024 21:31 WG2220500
Methylene Chloride 0.00982 J 0.00982 0.0370 1 02/05/2024 21:31 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00337 0.0370 1 02/05/2024 21:31 WG2220500
Methyl tert-butyl ether U 0.000518 0.00148 1 02/05/2024 21:31 WG2220500
Naphthalene U C3 0.00722 0.0185 1 02/05/2024 21:31 WG2220500
n-Propylbenzene U 0.00140 0.00739 1 02/05/2024 21:31 WG2220500
Styrene U 0.000339 0.0185 1 02/05/2024 21:31 WG2220500
1,1,1,2-Tetrachloroethane U 0.00140 0.00370 1 02/05/2024 21:31 WG2220500
1,1,2,2-Tetrachloroethane U 0.00103 0.00370 1 02/05/2024 21:31 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/16/24 11:51 10 of 89
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 10 of 89
SAMPLE RESULTS - 02
L1701794
SB-8 1-2
Collected date/time: 01/29/24 14:00
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00112 0.00370 1 02/05/2024 21:31 WG2220500
Tetrachloroethene 0.00210 J 0.00133 0.00370 1 02/05/2024 21:31 WG2220500
Toluene U 0.00192 0.00739 1 02/05/2024 21:31 WG2220500
1,2,3-Trichlorobenzene U 0.0108 0.0185 1 02/05/2024 21:31 WG2220500
1,2,4-Trichlorobenzene U 0.00651 0.0185 1 02/05/2024 21:31 WG2220500
1,1,1-Trichloroethane U 0.00137 0.00370 1 02/05/2024 21:31 WG2220500
1,1,2-Trichloroethane U 0.000883 0.00370 1 02/05/2024 21:31 WG2220500
Trichloroethene U J4 0.000864 0.00148 1 02/05/2024 21:31 WG2220500
Trichlorofluoromethane U 0.00122 0.00370 1 02/05/2024 21:31 WG2220500
1,2,3-Trichloropropane U 0.00240 0.0185 1 02/05/2024 21:31 WG2220500
1,2,4-Trimethylbenzene U 0.00234 0.00739 1 02/05/2024 21:31 WG2220500
1,2,3-Trimethylbenzene U 0.00234 0.00739 1 02/05/2024 21:31 WG2220500
1,3,5-Trimethylbenzene U 0.00296 0.00739 1 02/05/2024 21:31 WG2220500
Vinyl chloride U 0.00172 0.00370 1 02/05/2024 21:31 WG2220500
Xylenes, Total U 0.00130 0.00961 1 02/05/2024 21:31 WG2220500
(S) Toluene-d8 103 75.0-131 02/05/2024 21:31 WG2220500
(S) 4-Bromofluorobenzene 97.8 67.0-138 02/05/2024 21:31 WG2220500
(S) 1,2-Dichloroethane-d4 113 70.0-130 02/05/2024 21:31 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00651 0.0402 1 02/09/2024 04:28 WG2221334
Acenaphthylene U 0.00567 0.0402 1 02/09/2024 04:28 WG2221334
Anthracene U 0.00717 0.0402 1 02/09/2024 04:28 WG2221334
Benzidine U 0.0756 2.02 1 02/09/2024 04:28 WG2221334
Benzo(a)anthracene U 0.00709 0.0402 1 02/09/2024 04:28 WG2221334
Benzo(b)fluoranthene U 0.00750 0.0402 1 02/09/2024 04:28 WG2221334
Benzo(k)fluoranthene U 0.00715 0.0402 1 02/09/2024 04:28 WG2221334
Benzo(g,h,i)perylene U 0.00736 0.0402 1 02/09/2024 04:28 WG2221334
Benzo(a)pyrene U 0.00748 0.0402 1 02/09/2024 04:28 WG2221334
Bis(2-chlorethoxy)methane U 0.0121 0.402 1 02/09/2024 04:28 WG2221334
Bis(2-chloroethyl)ether U 0.0133 0.402 1 02/09/2024 04:28 WG2221334
2,2-Oxybis(1-Chloropropane)U 0.0174 0.402 1 02/09/2024 04:28 WG2221334
4-Bromophenyl-phenylether U 0.0141 0.402 1 02/09/2024 04:28 WG2221334
2-Chloronaphthalene U 0.00707 0.0402 1 02/09/2024 04:28 WG2221334
4-Chlorophenyl-phenylether U 0.0140 0.402 1 02/09/2024 04:28 WG2221334
Chrysene U 0.00800 0.0402 1 02/09/2024 04:28 WG2221334
Dibenz(a,h)anthracene U 0.0112 0.0402 1 02/09/2024 04:28 WG2221334
1,2-Dichlorobenzene U 0.0119 0.402 1 02/09/2024 04:28 WG2221334
1,3-Dichlorobenzene U 0.0122 0.402 1 02/09/2024 04:28 WG2221334
1,4-Dichlorobenzene U 0.0120 0.402 1 02/09/2024 04:28 WG2221334
3,3-Dichlorobenzidine U 0.0149 0.402 1 02/09/2024 04:28 WG2221334
2,4-Dinitrotoluene U 0.0115 0.402 1 02/09/2024 04:28 WG2221334
2,6-Dinitrotoluene U 0.0132 0.402 1 02/09/2024 04:28 WG2221334
Fluoranthene U 0.00726 0.0402 1 02/09/2024 04:28 WG2221334
Fluorene U 0.00655 0.0402 1 02/09/2024 04:28 WG2221334
Hexachlorobenzene U 0.0143 0.402 1 02/09/2024 04:28 WG2221334
Hexachloro-1,3-butadiene U 0.0135 0.402 1 02/09/2024 04:28 WG2221334
Hexachlorocyclopentadiene U 0.0211 0.402 1 02/09/2024 04:28 WG2221334
Hexachloroethane U 0.0158 0.402 1 02/09/2024 04:28 WG2221334
Indeno(1,2,3-cd)pyrene U 0.0114 0.0402 1 02/09/2024 04:28 WG2221334
Isophorone U 0.0123 0.402 1 02/09/2024 04:28 WG2221334
Naphthalene U 0.0101 0.0402 1 02/09/2024 04:28 WG2221334
Nitrobenzene U 0.0140 0.402 1 02/09/2024 04:28 WG2221334
n-Nitrosodimethylamine U 0.0597 0.402 1 02/09/2024 04:28 WG2221334
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/16/24 11:51 11 of 89
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 11 of 89
SAMPLE RESULTS - 02
L1701794
SB-8 1-2
Collected date/time: 01/29/24 14:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0305 0.402 1 02/09/2024 04:28 WG2221334
n-Nitrosodi-n-propylamine U 0.0134 0.402 1 02/09/2024 04:28 WG2221334
Phenanthrene U 0.00799 0.0402 1 02/09/2024 04:28 WG2221334
Benzylbutyl phthalate U 0.0126 0.402 1 02/09/2024 04:28 WG2221334
Bis(2-ethylhexyl)phthalate U 0.0510 0.402 1 02/09/2024 04:28 WG2221334
Di-n-butyl phthalate U 0.0138 0.402 1 02/09/2024 04:28 WG2221334
Diethyl phthalate U 0.0133 0.402 1 02/09/2024 04:28 WG2221334
Dimethyl phthalate U 0.0853 0.402 1 02/09/2024 04:28 WG2221334
Di-n-octyl phthalate U 0.0272 0.402 1 02/09/2024 04:28 WG2221334
Pyrene U 0.00783 0.0402 1 02/09/2024 04:28 WG2221334
1,2,4-Trichlorobenzene U 0.0126 0.402 1 02/09/2024 04:28 WG2221334
4-Chloro-3-methylphenol U 0.0131 0.402 1 02/09/2024 04:28 WG2221334
2-Chlorophenol U 0.0133 0.402 1 02/09/2024 04:28 WG2221334
2,4-Dichlorophenol U 0.0117 0.402 1 02/09/2024 04:28 WG2221334
2,4-Dimethylphenol U 0.0105 0.402 1 02/09/2024 04:28 WG2221334
4,6-Dinitro-2-methylphenol U 0.0912 0.402 1 02/09/2024 04:28 WG2221334
2,4-Dinitrophenol U 0.0941 0.402 1 02/09/2024 04:28 WG2221334
2-Nitrophenol U 0.0144 0.402 1 02/09/2024 04:28 WG2221334
4-Nitrophenol U 0.0126 0.402 1 02/09/2024 04:28 WG2221334
Pentachlorophenol U 0.0108 0.402 1 02/09/2024 04:28 WG2221334
Phenol U 0.0162 0.402 1 02/09/2024 04:28 WG2221334
2,4,6-Trichlorophenol U 0.0129 0.402 1 02/09/2024 04:28 WG2221334
(S) 2-Fluorophenol 67.8 12.0-120 02/09/2024 04:28 WG2221334
(S) Phenol-d5 62.1 10.0-120 02/09/2024 04:28 WG2221334
(S) Nitrobenzene-d5 66.2 10.0-122 02/09/2024 04:28 WG2221334
(S) 2-Fluorobiphenyl 64.4 15.0-120 02/09/2024 04:28 WG2221334
(S) 2,4,6-Tribromophenol 75.7 10.0-127 02/09/2024 04:28 WG2221334
(S) p-Terphenyl-d14 73.1 10.0-120 02/09/2024 04:28 WG2221334
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 12 of 89
SAMPLE RESULTS - 03
L1701794
SB-7 (0-1)
Collected date/time: 01/29/24 14:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.4 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0550 0.0754 1 02/05/2024 21:50 WG2220500
Acrylonitrile U 0.00544 0.0188 1 02/05/2024 21:50 WG2220500
Benzene U 0.000704 0.00151 1 02/05/2024 21:50 WG2220500
Bromobenzene U 0.00136 0.0188 1 02/05/2024 21:50 WG2220500
Bromodichloromethane U 0.00109 0.00377 1 02/05/2024 21:50 WG2220500
Bromoform U 0.00176 0.0377 1 02/05/2024 21:50 WG2220500
Bromomethane U 0.00297 0.0188 1 02/05/2024 21:50 WG2220500
n-Butylbenzene U 0.00791 0.0188 1 02/05/2024 21:50 WG2220500
sec-Butylbenzene U 0.00434 0.0188 1 02/05/2024 21:50 WG2220500
tert-Butylbenzene U 0.00294 0.00754 1 02/05/2024 21:50 WG2220500
Carbon tetrachloride U 0.00135 0.00754 1 02/05/2024 21:50 WG2220500
Chlorobenzene U 0.000317 0.00377 1 02/05/2024 21:50 WG2220500
Chlorodibromomethane U 0.000922 0.00377 1 02/05/2024 21:50 WG2220500
Chloroethane U 0.00256 0.00754 1 02/05/2024 21:50 WG2220500
Chloroform 0.00356 B J 0.00155 0.00377 1 02/05/2024 21:50 WG2220500
Chloromethane U 0.00656 0.0188 1 02/05/2024 21:50 WG2220500
2-Chlorotoluene U 0.00130 0.00377 1 02/05/2024 21:50 WG2220500
4-Chlorotoluene U 0.000678 0.00754 1 02/05/2024 21:50 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00588 0.0377 1 02/05/2024 21:50 WG2220500
1,2-Dibromoethane U 0.000977 0.00377 1 02/05/2024 21:50 WG2220500
Dibromomethane U 0.00113 0.00754 1 02/05/2024 21:50 WG2220500
1,2-Dichlorobenzene U 0.000641 0.00754 1 02/05/2024 21:50 WG2220500
1,3-Dichlorobenzene U 0.000904 0.00754 1 02/05/2024 21:50 WG2220500
1,4-Dichlorobenzene U 0.00106 0.00754 1 02/05/2024 21:50 WG2220500
Dichlorodifluoromethane U 0.00243 0.00754 1 02/05/2024 21:50 WG2220500
1,1-Dichloroethane U 0.000740 0.00377 1 02/05/2024 21:50 WG2220500
1,2-Dichloroethane U 0.000978 0.00377 1 02/05/2024 21:50 WG2220500
1,1-Dichloroethene U 0.000913 0.00377 1 02/05/2024 21:50 WG2220500
cis-1,2-Dichloroethene U 0.00111 0.00377 1 02/05/2024 21:50 WG2220500
trans-1,2-Dichloroethene U 0.00157 0.00754 1 02/05/2024 21:50 WG2220500
1,2-Dichloropropane U 0.00214 0.00754 1 02/05/2024 21:50 WG2220500
1,1-Dichloropropene U 0.00122 0.00377 1 02/05/2024 21:50 WG2220500
1,3-Dichloropropane U 0.000755 0.00754 1 02/05/2024 21:50 WG2220500
cis-1,3-Dichloropropene U 0.00114 0.00377 1 02/05/2024 21:50 WG2220500
trans-1,3-Dichloropropene U 0.00172 0.00754 1 02/05/2024 21:50 WG2220500
2,2-Dichloropropane U 0.00208 0.00377 1 02/05/2024 21:50 WG2220500
Di-isopropyl ether U 0.000618 0.00151 1 02/05/2024 21:50 WG2220500
Ethylbenzene U 0.00111 0.00377 1 02/05/2024 21:50 WG2220500
Hexachloro-1,3-butadiene U 0.00904 0.0377 1 02/05/2024 21:50 WG2220500
Isopropylbenzene U 0.000641 0.00377 1 02/05/2024 21:50 WG2220500
p-Isopropyltoluene U 0.00384 0.00754 1 02/05/2024 21:50 WG2220500
2-Butanone (MEK)U 0.0957 0.151 1 02/05/2024 21:50 WG2220500
Methylene Chloride 0.0133 B J 0.0100 0.0377 1 02/05/2024 21:50 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00344 0.0377 1 02/05/2024 21:50 WG2220500
Methyl tert-butyl ether U 0.000528 0.00151 1 02/05/2024 21:50 WG2220500
Naphthalene U C3 0.00736 0.0188 1 02/05/2024 21:50 WG2220500
n-Propylbenzene U 0.00143 0.00754 1 02/05/2024 21:50 WG2220500
Styrene U 0.000345 0.0188 1 02/05/2024 21:50 WG2220500
1,1,1,2-Tetrachloroethane U 0.00143 0.00377 1 02/05/2024 21:50 WG2220500
1,1,2,2-Tetrachloroethane U 0.00105 0.00377 1 02/05/2024 21:50 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 13 of 89
SAMPLE RESULTS - 03
L1701794
SB-7 (0-1)
Collected date/time: 01/29/24 14:35
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00114 0.00377 1 02/05/2024 21:50 WG2220500
Tetrachloroethene 0.141 0.00135 0.00377 1 02/05/2024 21:50 WG2220500
Toluene U 0.00196 0.00754 1 02/05/2024 21:50 WG2220500
1,2,3-Trichlorobenzene U 0.0110 0.0188 1 02/05/2024 21:50 WG2220500
1,2,4-Trichlorobenzene U 0.00663 0.0188 1 02/05/2024 21:50 WG2220500
1,1,1-Trichloroethane U 0.00139 0.00377 1 02/05/2024 21:50 WG2220500
1,1,2-Trichloroethane U 0.000900 0.00377 1 02/05/2024 21:50 WG2220500
Trichloroethene U J4 0.000880 0.00151 1 02/05/2024 21:50 WG2220500
Trichlorofluoromethane U 0.00125 0.00377 1 02/05/2024 21:50 WG2220500
1,2,3-Trichloropropane U 0.00244 0.0188 1 02/05/2024 21:50 WG2220500
1,2,4-Trimethylbenzene U 0.00238 0.00754 1 02/05/2024 21:50 WG2220500
1,2,3-Trimethylbenzene U 0.00238 0.00754 1 02/05/2024 21:50 WG2220500
1,3,5-Trimethylbenzene U 0.00301 0.00754 1 02/05/2024 21:50 WG2220500
Vinyl chloride U 0.00175 0.00377 1 02/05/2024 21:50 WG2220500
Xylenes, Total U 0.00133 0.00980 1 02/05/2024 21:50 WG2220500
(S) Toluene-d8 105 75.0-131 02/05/2024 21:50 WG2220500
(S) 4-Bromofluorobenzene 97.5 67.0-138 02/05/2024 21:50 WG2220500
(S) 1,2-Dichloroethane-d4 118 70.0-130 02/05/2024 21:50 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00663 0.0409 1 02/08/2024 19:42 WG2220590
Acenaphthylene U 0.00576 0.0409 1 02/08/2024 19:42 WG2220590
Anthracene U 0.00729 0.0409 1 02/08/2024 19:42 WG2220590
Benzidine U 0.0769 2.05 1 02/08/2024 19:42 WG2220590
Benzo(a)anthracene U 0.00722 0.0409 1 02/08/2024 19:42 WG2220590
Benzo(b)fluoranthene U 0.00763 0.0409 1 02/08/2024 19:42 WG2220590
Benzo(k)fluoranthene U 0.00728 0.0409 1 02/08/2024 19:42 WG2220590
Benzo(g,h,i)perylene U 0.00749 0.0409 1 02/08/2024 19:42 WG2220590
Benzo(a)pyrene U 0.00761 0.0409 1 02/08/2024 19:42 WG2220590
Bis(2-chlorethoxy)methane U 0.0123 0.409 1 02/08/2024 19:42 WG2220590
Bis(2-chloroethyl)ether U 0.0135 0.409 1 02/08/2024 19:42 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0177 0.409 1 02/08/2024 19:42 WG2220590
4-Bromophenyl-phenylether U 0.0144 0.409 1 02/08/2024 19:42 WG2220590
2-Chloronaphthalene U 0.00719 0.0409 1 02/08/2024 19:42 WG2220590
4-Chlorophenyl-phenylether U 0.0143 0.409 1 02/08/2024 19:42 WG2220590
Chrysene U 0.00814 0.0409 1 02/08/2024 19:42 WG2220590
Dibenz(a,h)anthracene U 0.0113 0.0409 1 02/08/2024 19:42 WG2220590
1,2-Dichlorobenzene U 0.0121 0.409 1 02/08/2024 19:42 WG2220590
1,3-Dichlorobenzene U 0.0124 0.409 1 02/08/2024 19:42 WG2220590
1,4-Dichlorobenzene U 0.0122 0.409 1 02/08/2024 19:42 WG2220590
3,3-Dichlorobenzidine U 0.0151 0.409 1 02/08/2024 19:42 WG2220590
2,4-Dinitrotoluene U 0.0117 0.409 1 02/08/2024 19:42 WG2220590
2,6-Dinitrotoluene U 0.0134 0.409 1 02/08/2024 19:42 WG2220590
Fluoranthene U 0.00739 0.0409 1 02/08/2024 19:42 WG2220590
Fluorene U 0.00666 0.0409 1 02/08/2024 19:42 WG2220590
Hexachlorobenzene U 0.0145 0.409 1 02/08/2024 19:42 WG2220590
Hexachloro-1,3-butadiene U 0.0138 0.409 1 02/08/2024 19:42 WG2220590
Hexachlorocyclopentadiene U 0.0215 0.409 1 02/08/2024 19:42 WG2220590
Hexachloroethane U 0.0161 0.409 1 02/08/2024 19:42 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0116 0.0409 1 02/08/2024 19:42 WG2220590
Isophorone U 0.0125 0.409 1 02/08/2024 19:42 WG2220590
Naphthalene U 0.0103 0.0409 1 02/08/2024 19:42 WG2220590
Nitrobenzene U 0.0143 0.409 1 02/08/2024 19:42 WG2220590
n-Nitrosodimethylamine U 0.0607 0.409 1 02/08/2024 19:42 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 14 of 89
SAMPLE RESULTS - 03
L1701794
SB-7 (0-1)
Collected date/time: 01/29/24 14:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0310 0.409 1 02/08/2024 19:42 WG2220590
n-Nitrosodi-n-propylamine U 0.0136 0.409 1 02/08/2024 19:42 WG2220590
Phenanthrene U 0.00812 0.0409 1 02/08/2024 19:42 WG2220590
Benzylbutyl phthalate U 0.0128 0.409 1 02/08/2024 19:42 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0519 0.409 1 02/08/2024 19:42 WG2220590
Di-n-butyl phthalate U 0.0140 0.409 1 02/08/2024 19:42 WG2220590
Diethyl phthalate U 0.0135 0.409 1 02/08/2024 19:42 WG2220590
Dimethyl phthalate U 0.0868 0.409 1 02/08/2024 19:42 WG2220590
Di-n-octyl phthalate U 0.0277 0.409 1 02/08/2024 19:42 WG2220590
Pyrene U 0.00797 0.0409 1 02/08/2024 19:42 WG2220590
1,2,4-Trichlorobenzene U 0.0128 0.409 1 02/08/2024 19:42 WG2220590
4-Chloro-3-methylphenol U 0.0133 0.409 1 02/08/2024 19:42 WG2220590
2-Chlorophenol U 0.0135 0.409 1 02/08/2024 19:42 WG2220590
2,4-Dichlorophenol U 0.0119 0.409 1 02/08/2024 19:42 WG2220590
2,4-Dimethylphenol U 0.0107 0.409 1 02/08/2024 19:42 WG2220590
4,6-Dinitro-2-methylphenol U 0.0928 0.409 1 02/08/2024 19:42 WG2220590
2,4-Dinitrophenol U 0.0958 0.409 1 02/08/2024 19:42 WG2220590
2-Nitrophenol U 0.0146 0.409 1 02/08/2024 19:42 WG2220590
4-Nitrophenol U 0.0128 0.409 1 02/08/2024 19:42 WG2220590
Pentachlorophenol U 0.0110 0.409 1 02/08/2024 19:42 WG2220590
Phenol U 0.0165 0.409 1 02/08/2024 19:42 WG2220590
2,4,6-Trichlorophenol U 0.0132 0.409 1 02/08/2024 19:42 WG2220590
(S) 2-Fluorophenol 70.0 12.0-120 02/08/2024 19:42 WG2220590
(S) Phenol-d5 72.2 10.0-120 02/08/2024 19:42 WG2220590
(S) Nitrobenzene-d5 64.1 10.0-122 02/08/2024 19:42 WG2220590
(S) 2-Fluorobiphenyl 69.8 15.0-120 02/08/2024 19:42 WG2220590
(S) 2,4,6-Tribromophenol 67.6 10.0-127 02/08/2024 19:42 WG2220590
(S) p-Terphenyl-d14 75.9 10.0-120 02/08/2024 19:42 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 15 of 89
SAMPLE RESULTS - 04
L1701794
SB-7 (3-4)
Collected date/time: 01/29/24 14:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 71.0 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0673 0.0921 1 02/05/2024 22:08 WG2220500
Acrylonitrile U 0.00665 0.0230 1 02/05/2024 22:08 WG2220500
Benzene U 0.000861 0.00184 1 02/05/2024 22:08 WG2220500
Bromobenzene U 0.00166 0.0230 1 02/05/2024 22:08 WG2220500
Bromodichloromethane U 0.00134 0.00461 1 02/05/2024 22:08 WG2220500
Bromoform U 0.00216 0.0461 1 02/05/2024 22:08 WG2220500
Bromomethane U 0.00363 0.0230 1 02/05/2024 22:08 WG2220500
n-Butylbenzene U 0.00968 0.0230 1 02/05/2024 22:08 WG2220500
sec-Butylbenzene U 0.00531 0.0230 1 02/05/2024 22:08 WG2220500
tert-Butylbenzene U 0.00359 0.00921 1 02/05/2024 22:08 WG2220500
Carbon tetrachloride U 0.00165 0.00921 1 02/05/2024 22:08 WG2220500
Chlorobenzene U 0.000387 0.00461 1 02/05/2024 22:08 WG2220500
Chlorodibromomethane U 0.00113 0.00461 1 02/05/2024 22:08 WG2220500
Chloroethane U 0.00313 0.00921 1 02/05/2024 22:08 WG2220500
Chloroform 0.00507 B 0.00190 0.00461 1 02/05/2024 22:08 WG2220500
Chloromethane U 0.00802 0.0230 1 02/05/2024 22:08 WG2220500
2-Chlorotoluene U 0.00159 0.00461 1 02/05/2024 22:08 WG2220500
4-Chlorotoluene U 0.000829 0.00921 1 02/05/2024 22:08 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00719 0.0461 1 02/05/2024 22:08 WG2220500
1,2-Dibromoethane U 0.00119 0.00461 1 02/05/2024 22:08 WG2220500
Dibromomethane U 0.00138 0.00921 1 02/05/2024 22:08 WG2220500
1,2-Dichlorobenzene U 0.000783 0.00921 1 02/05/2024 22:08 WG2220500
1,3-Dichlorobenzene U 0.00111 0.00921 1 02/05/2024 22:08 WG2220500
1,4-Dichlorobenzene U 0.00129 0.00921 1 02/05/2024 22:08 WG2220500
Dichlorodifluoromethane U 0.00297 0.00921 1 02/05/2024 22:08 WG2220500
1,1-Dichloroethane U 0.000905 0.00461 1 02/05/2024 22:08 WG2220500
1,2-Dichloroethane U 0.00120 0.00461 1 02/05/2024 22:08 WG2220500
1,1-Dichloroethene U 0.00112 0.00461 1 02/05/2024 22:08 WG2220500
cis-1,2-Dichloroethene U 0.00135 0.00461 1 02/05/2024 22:08 WG2220500
trans-1,2-Dichloroethene U 0.00192 0.00921 1 02/05/2024 22:08 WG2220500
1,2-Dichloropropane U 0.00262 0.00921 1 02/05/2024 22:08 WG2220500
1,1-Dichloropropene U 0.00149 0.00461 1 02/05/2024 22:08 WG2220500
1,3-Dichloropropane U 0.000923 0.00921 1 02/05/2024 22:08 WG2220500
cis-1,3-Dichloropropene U 0.00140 0.00461 1 02/05/2024 22:08 WG2220500
trans-1,3-Dichloropropene U 0.00210 0.00921 1 02/05/2024 22:08 WG2220500
2,2-Dichloropropane U 0.00254 0.00461 1 02/05/2024 22:08 WG2220500
Di-isopropyl ether U 0.000756 0.00184 1 02/05/2024 22:08 WG2220500
Ethylbenzene U 0.00136 0.00461 1 02/05/2024 22:08 WG2220500
Hexachloro-1,3-butadiene U 0.0111 0.0461 1 02/05/2024 22:08 WG2220500
Isopropylbenzene U 0.000783 0.00461 1 02/05/2024 22:08 WG2220500
p-Isopropyltoluene U 0.00470 0.00921 1 02/05/2024 22:08 WG2220500
2-Butanone (MEK)U 0.117 0.184 1 02/05/2024 22:08 WG2220500
Methylene Chloride 0.0194 B J 0.0122 0.0461 1 02/05/2024 22:08 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00420 0.0461 1 02/05/2024 22:08 WG2220500
Methyl tert-butyl ether U 0.000645 0.00184 1 02/05/2024 22:08 WG2220500
Naphthalene U C3 0.00899 0.0230 1 02/05/2024 22:08 WG2220500
n-Propylbenzene U 0.00175 0.00921 1 02/05/2024 22:08 WG2220500
Styrene U 0.000422 0.0230 1 02/05/2024 22:08 WG2220500
1,1,1,2-Tetrachloroethane U 0.00175 0.00461 1 02/05/2024 22:08 WG2220500
1,1,2,2-Tetrachloroethane U 0.00128 0.00461 1 02/05/2024 22:08 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 16 of 89
SAMPLE RESULTS - 04
L1701794
SB-7 (3-4)
Collected date/time: 01/29/24 14:35
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00139 0.00461 1 02/05/2024 22:08 WG2220500
Tetrachloroethene U 0.00165 0.00461 1 02/05/2024 22:08 WG2220500
Toluene U 0.00240 0.00921 1 02/05/2024 22:08 WG2220500
1,2,3-Trichlorobenzene U 0.0135 0.0230 1 02/05/2024 22:08 WG2220500
1,2,4-Trichlorobenzene U 0.00811 0.0230 1 02/05/2024 22:08 WG2220500
1,1,1-Trichloroethane U 0.00170 0.00461 1 02/05/2024 22:08 WG2220500
1,1,2-Trichloroethane U 0.00110 0.00461 1 02/05/2024 22:08 WG2220500
Trichloroethene U J4 0.00108 0.00184 1 02/05/2024 22:08 WG2220500
Trichlorofluoromethane U 0.00152 0.00461 1 02/05/2024 22:08 WG2220500
1,2,3-Trichloropropane U 0.00299 0.0230 1 02/05/2024 22:08 WG2220500
1,2,4-Trimethylbenzene U 0.00291 0.00921 1 02/05/2024 22:08 WG2220500
1,2,3-Trimethylbenzene U 0.00291 0.00921 1 02/05/2024 22:08 WG2220500
1,3,5-Trimethylbenzene U 0.00369 0.00921 1 02/05/2024 22:08 WG2220500
Vinyl chloride U 0.00214 0.00461 1 02/05/2024 22:08 WG2220500
Xylenes, Total U 0.00162 0.0120 1 02/05/2024 22:08 WG2220500
(S) Toluene-d8 105 75.0-131 02/05/2024 22:08 WG2220500
(S) 4-Bromofluorobenzene 97.6 67.0-138 02/05/2024 22:08 WG2220500
(S) 1,2-Dichloroethane-d4 116 70.0-130 02/05/2024 22:08 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00759 0.0469 1 02/08/2024 18:20 WG2220590
Acenaphthylene U 0.00660 0.0469 1 02/08/2024 18:20 WG2220590
Anthracene U 0.00835 0.0469 1 02/08/2024 18:20 WG2220590
Benzidine U 0.0881 2.35 1 02/08/2024 18:20 WG2220590
Benzo(a)anthracene U 0.00826 0.0469 1 02/08/2024 18:20 WG2220590
Benzo(b)fluoranthene U 0.00874 0.0469 1 02/08/2024 18:20 WG2220590
Benzo(k)fluoranthene U 0.00833 0.0469 1 02/08/2024 18:20 WG2220590
Benzo(g,h,i)perylene U 0.00857 0.0469 1 02/08/2024 18:20 WG2220590
Benzo(a)pyrene U 0.00871 0.0469 1 02/08/2024 18:20 WG2220590
Bis(2-chlorethoxy)methane U 0.0141 0.469 1 02/08/2024 18:20 WG2220590
Bis(2-chloroethyl)ether U 0.0155 0.469 1 02/08/2024 18:20 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0203 0.469 1 02/08/2024 18:20 WG2220590
4-Bromophenyl-phenylether U 0.0165 0.469 1 02/08/2024 18:20 WG2220590
2-Chloronaphthalene U 0.00824 0.0469 1 02/08/2024 18:20 WG2220590
4-Chlorophenyl-phenylether U 0.0163 0.469 1 02/08/2024 18:20 WG2220590
Chrysene U 0.00932 0.0469 1 02/08/2024 18:20 WG2220590
Dibenz(a,h)anthracene U 0.0130 0.0469 1 02/08/2024 18:20 WG2220590
1,2-Dichlorobenzene U 0.0139 0.469 1 02/08/2024 18:20 WG2220590
1,3-Dichlorobenzene U 0.0142 0.469 1 02/08/2024 18:20 WG2220590
1,4-Dichlorobenzene U 0.0140 0.469 1 02/08/2024 18:20 WG2220590
3,3-Dichlorobenzidine U 0.0173 0.469 1 02/08/2024 18:20 WG2220590
2,4-Dinitrotoluene U 0.0134 0.469 1 02/08/2024 18:20 WG2220590
2,6-Dinitrotoluene U 0.0153 0.469 1 02/08/2024 18:20 WG2220590
Fluoranthene U 0.00846 0.0469 1 02/08/2024 18:20 WG2220590
Fluorene U 0.00763 0.0469 1 02/08/2024 18:20 WG2220590
Hexachlorobenzene U 0.0166 0.469 1 02/08/2024 18:20 WG2220590
Hexachloro-1,3-butadiene U 0.0158 0.469 1 02/08/2024 18:20 WG2220590
Hexachlorocyclopentadiene U 0.0246 0.469 1 02/08/2024 18:20 WG2220590
Hexachloroethane U 0.0184 0.469 1 02/08/2024 18:20 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0132 0.0469 1 02/08/2024 18:20 WG2220590
Isophorone U 0.0144 0.469 1 02/08/2024 18:20 WG2220590
Naphthalene U 0.0118 0.0469 1 02/08/2024 18:20 WG2220590
Nitrobenzene U 0.0163 0.469 1 02/08/2024 18:20 WG2220590
n-Nitrosodimethylamine U 0.0695 0.469 1 02/08/2024 18:20 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1701794
SB-7 (3-4)
Collected date/time: 01/29/24 14:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0355 0.469 1 02/08/2024 18:20 WG2220590
n-Nitrosodi-n-propylamine U 0.0156 0.469 1 02/08/2024 18:20 WG2220590
Phenanthrene U 0.00931 0.0469 1 02/08/2024 18:20 WG2220590
Benzylbutyl phthalate U 0.0146 0.469 1 02/08/2024 18:20 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0594 0.469 1 02/08/2024 18:20 WG2220590
Di-n-butyl phthalate U 0.0160 0.469 1 02/08/2024 18:20 WG2220590
Diethyl phthalate U 0.0155 0.469 1 02/08/2024 18:20 WG2220590
Dimethyl phthalate U 0.0994 0.469 1 02/08/2024 18:20 WG2220590
Di-n-octyl phthalate U 0.0317 0.469 1 02/08/2024 18:20 WG2220590
Pyrene U 0.00912 0.0469 1 02/08/2024 18:20 WG2220590
1,2,4-Trichlorobenzene U 0.0146 0.469 1 02/08/2024 18:20 WG2220590
4-Chloro-3-methylphenol U 0.0152 0.469 1 02/08/2024 18:20 WG2220590
2-Chlorophenol U 0.0155 0.469 1 02/08/2024 18:20 WG2220590
2,4-Dichlorophenol U 0.0137 0.469 1 02/08/2024 18:20 WG2220590
2,4-Dimethylphenol U 0.0122 0.469 1 02/08/2024 18:20 WG2220590
4,6-Dinitro-2-methylphenol U 0.106 0.469 1 02/08/2024 18:20 WG2220590
2,4-Dinitrophenol U 0.110 0.469 1 02/08/2024 18:20 WG2220590
2-Nitrophenol U 0.0168 0.469 1 02/08/2024 18:20 WG2220590
4-Nitrophenol U 0.0146 0.469 1 02/08/2024 18:20 WG2220590
Pentachlorophenol U 0.0126 0.469 1 02/08/2024 18:20 WG2220590
Phenol U 0.0189 0.469 1 02/08/2024 18:20 WG2220590
2,4,6-Trichlorophenol U 0.0151 0.469 1 02/08/2024 18:20 WG2220590
(S) 2-Fluorophenol 72.3 12.0-120 02/08/2024 18:20 WG2220590
(S) Phenol-d5 70.2 10.0-120 02/08/2024 18:20 WG2220590
(S) Nitrobenzene-d5 68.7 10.0-122 02/08/2024 18:20 WG2220590
(S) 2-Fluorobiphenyl 71.1 15.0-120 02/08/2024 18:20 WG2220590
(S) 2,4,6-Tribromophenol 74.5 10.0-127 02/08/2024 18:20 WG2220590
(S) p-Terphenyl-d14 79.2 10.0-120 02/08/2024 18:20 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 18 of 89
SAMPLE RESULTS - 05
L1701794
SB-9 (0-1)
Collected date/time: 01/29/24 15:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 87.0 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0486 0.0665 1 02/05/2024 22:27 WG2220500
Acrylonitrile U 0.00480 0.0166 1 02/05/2024 22:27 WG2220500
Benzene U 0.000621 0.00133 1 02/05/2024 22:27 WG2220500
Bromobenzene U 0.00120 0.0166 1 02/05/2024 22:27 WG2220500
Bromodichloromethane U 0.000965 0.00333 1 02/05/2024 22:27 WG2220500
Bromoform U 0.00156 0.0333 1 02/05/2024 22:27 WG2220500
Bromomethane U 0.00262 0.0166 1 02/05/2024 22:27 WG2220500
n-Butylbenzene U 0.00699 0.0166 1 02/05/2024 22:27 WG2220500
sec-Butylbenzene U 0.00383 0.0166 1 02/05/2024 22:27 WG2220500
tert-Butylbenzene U 0.00260 0.00665 1 02/05/2024 22:27 WG2220500
Carbon tetrachloride U 0.00120 0.00665 1 02/05/2024 22:27 WG2220500
Chlorobenzene U 0.000279 0.00333 1 02/05/2024 22:27 WG2220500
Chlorodibromomethane U 0.000814 0.00333 1 02/05/2024 22:27 WG2220500
Chloroethane U 0.00226 0.00665 1 02/05/2024 22:27 WG2220500
Chloroform 0.00278 B J 0.00137 0.00333 1 02/05/2024 22:27 WG2220500
Chloromethane U 0.00579 0.0166 1 02/05/2024 22:27 WG2220500
2-Chlorotoluene U 0.00115 0.00333 1 02/05/2024 22:27 WG2220500
4-Chlorotoluene U 0.000599 0.00665 1 02/05/2024 22:27 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00519 0.0333 1 02/05/2024 22:27 WG2220500
1,2-Dibromoethane U 0.000862 0.00333 1 02/05/2024 22:27 WG2220500
Dibromomethane U 0.000998 0.00665 1 02/05/2024 22:27 WG2220500
1,2-Dichlorobenzene U 0.000566 0.00665 1 02/05/2024 22:27 WG2220500
1,3-Dichlorobenzene U 0.000798 0.00665 1 02/05/2024 22:27 WG2220500
1,4-Dichlorobenzene U 0.000932 0.00665 1 02/05/2024 22:27 WG2220500
Dichlorodifluoromethane U 0.00214 0.00665 1 02/05/2024 22:27 WG2220500
1,1-Dichloroethane U 0.000653 0.00333 1 02/05/2024 22:27 WG2220500
1,2-Dichloroethane U 0.000864 0.00333 1 02/05/2024 22:27 WG2220500
1,1-Dichloroethene U 0.000806 0.00333 1 02/05/2024 22:27 WG2220500
cis-1,2-Dichloroethene U 0.000977 0.00333 1 02/05/2024 22:27 WG2220500
trans-1,2-Dichloroethene U 0.00138 0.00665 1 02/05/2024 22:27 WG2220500
1,2-Dichloropropane U 0.00189 0.00665 1 02/05/2024 22:27 WG2220500
1,1-Dichloropropene U 0.00108 0.00333 1 02/05/2024 22:27 WG2220500
1,3-Dichloropropane U 0.000667 0.00665 1 02/05/2024 22:27 WG2220500
cis-1,3-Dichloropropene U 0.00101 0.00333 1 02/05/2024 22:27 WG2220500
trans-1,3-Dichloropropene U 0.00152 0.00665 1 02/05/2024 22:27 WG2220500
2,2-Dichloropropane U 0.00184 0.00333 1 02/05/2024 22:27 WG2220500
Di-isopropyl ether U 0.000546 0.00133 1 02/05/2024 22:27 WG2220500
Ethylbenzene U 0.000981 0.00333 1 02/05/2024 22:27 WG2220500
Hexachloro-1,3-butadiene U 0.00798 0.0333 1 02/05/2024 22:27 WG2220500
Isopropylbenzene U 0.000566 0.00333 1 02/05/2024 22:27 WG2220500
p-Isopropyltoluene U 0.00339 0.00665 1 02/05/2024 22:27 WG2220500
2-Butanone (MEK)U 0.0845 0.133 1 02/05/2024 22:27 WG2220500
Methylene Chloride 0.0128 B J 0.00884 0.0333 1 02/05/2024 22:27 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00303 0.0333 1 02/05/2024 22:27 WG2220500
Methyl tert-butyl ether U 0.000466 0.00133 1 02/05/2024 22:27 WG2220500
Naphthalene U C3 0.00649 0.0166 1 02/05/2024 22:27 WG2220500
n-Propylbenzene U 0.00126 0.00665 1 02/05/2024 22:27 WG2220500
Styrene U 0.000305 0.0166 1 02/05/2024 22:27 WG2220500
1,1,1,2-Tetrachloroethane U 0.00126 0.00333 1 02/05/2024 22:27 WG2220500
1,1,2,2-Tetrachloroethane U 0.000925 0.00333 1 02/05/2024 22:27 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 19 of 89
SAMPLE RESULTS - 05
L1701794
SB-9 (0-1)
Collected date/time: 01/29/24 15:15
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00100 0.00333 1 02/05/2024 22:27 WG2220500
Tetrachloroethene U 0.00119 0.00333 1 02/05/2024 22:27 WG2220500
Toluene U 0.00173 0.00665 1 02/05/2024 22:27 WG2220500
1,2,3-Trichlorobenzene U 0.00975 0.0166 1 02/05/2024 22:27 WG2220500
1,2,4-Trichlorobenzene U 0.00586 0.0166 1 02/05/2024 22:27 WG2220500
1,1,1-Trichloroethane U 0.00123 0.00333 1 02/05/2024 22:27 WG2220500
1,1,2-Trichloroethane U 0.000794 0.00333 1 02/05/2024 22:27 WG2220500
Trichloroethene U J4 0.000777 0.00133 1 02/05/2024 22:27 WG2220500
Trichlorofluoromethane U 0.00110 0.00333 1 02/05/2024 22:27 WG2220500
1,2,3-Trichloropropane U 0.00216 0.0166 1 02/05/2024 22:27 WG2220500
1,2,4-Trimethylbenzene 0.00475 J 0.00210 0.00665 1 02/05/2024 22:27 WG2220500
1,2,3-Trimethylbenzene U 0.00210 0.00665 1 02/05/2024 22:27 WG2220500
1,3,5-Trimethylbenzene U 0.00266 0.00665 1 02/05/2024 22:27 WG2220500
Vinyl chloride U 0.00154 0.00333 1 02/05/2024 22:27 WG2220500
Xylenes, Total 0.00306 J 0.00117 0.00865 1 02/05/2024 22:27 WG2220500
(S) Toluene-d8 104 75.0-131 02/05/2024 22:27 WG2220500
(S) 4-Bromofluorobenzene 97.4 67.0-138 02/05/2024 22:27 WG2220500
(S) 1,2-Dichloroethane-d4 114 70.0-130 02/05/2024 22:27 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00619 0.0383 1 02/09/2024 00:29 WG2220590
Acenaphthylene 0.0126 J 0.00539 0.0383 1 02/09/2024 00:29 WG2220590
Anthracene U 0.00681 0.0383 1 02/09/2024 00:29 WG2220590
Benzidine U 0.0719 1.92 1 02/09/2024 00:29 WG2220590
Benzo(a)anthracene 0.0330 J 0.00675 0.0383 1 02/09/2024 00:29 WG2220590
Benzo(b)fluoranthene 0.0757 0.00714 0.0383 1 02/09/2024 00:29 WG2220590
Benzo(k)fluoranthene 0.0215 J 0.00680 0.0383 1 02/09/2024 00:29 WG2220590
Benzo(g,h,i)perylene 0.0433 0.00700 0.0383 1 02/09/2024 00:29 WG2220590
Benzo(a)pyrene 0.0461 0.00711 0.0383 1 02/09/2024 00:29 WG2220590
Bis(2-chlorethoxy)methane U 0.0115 0.383 1 02/09/2024 00:29 WG2220590
Bis(2-chloroethyl)ether U 0.0126 0.383 1 02/09/2024 00:29 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0165 0.383 1 02/09/2024 00:29 WG2220590
4-Bromophenyl-phenylether U 0.0134 0.383 1 02/09/2024 00:29 WG2220590
2-Chloronaphthalene U 0.00672 0.0383 1 02/09/2024 00:29 WG2220590
4-Chlorophenyl-phenylether U 0.0133 0.383 1 02/09/2024 00:29 WG2220590
Chrysene 0.0404 0.00761 0.0383 1 02/09/2024 00:29 WG2220590
Dibenz(a,h)anthracene 0.0107 J 0.0106 0.0383 1 02/09/2024 00:29 WG2220590
1,2-Dichlorobenzene U 0.0113 0.383 1 02/09/2024 00:29 WG2220590
1,3-Dichlorobenzene U 0.0116 0.383 1 02/09/2024 00:29 WG2220590
1,4-Dichlorobenzene U 0.0114 0.383 1 02/09/2024 00:29 WG2220590
3,3-Dichlorobenzidine U 0.0141 0.383 1 02/09/2024 00:29 WG2220590
2,4-Dinitrotoluene U 0.0110 0.383 1 02/09/2024 00:29 WG2220590
2,6-Dinitrotoluene U 0.0125 0.383 1 02/09/2024 00:29 WG2220590
Fluoranthene 0.0943 0.00691 0.0383 1 02/09/2024 00:29 WG2220590
Fluorene U 0.00623 0.0383 1 02/09/2024 00:29 WG2220590
Hexachlorobenzene U 0.0136 0.383 1 02/09/2024 00:29 WG2220590
Hexachloro-1,3-butadiene U 0.0129 0.383 1 02/09/2024 00:29 WG2220590
Hexachlorocyclopentadiene U 0.0201 0.383 1 02/09/2024 00:29 WG2220590
Hexachloroethane U 0.0151 0.383 1 02/09/2024 00:29 WG2220590
Indeno(1,2,3-cd)pyrene 0.0450 0.0108 0.0383 1 02/09/2024 00:29 WG2220590
Isophorone U 0.0117 0.383 1 02/09/2024 00:29 WG2220590
Naphthalene U 0.00961 0.0383 1 02/09/2024 00:29 WG2220590
Nitrobenzene U 0.0133 0.383 1 02/09/2024 00:29 WG2220590
n-Nitrosodimethylamine U 0.0568 0.383 1 02/09/2024 00:29 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1701794
SB-9 (0-1)
Collected date/time: 01/29/24 15:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0290 0.383 1 02/09/2024 00:29 WG2220590
n-Nitrosodi-n-propylamine U 0.0128 0.383 1 02/09/2024 00:29 WG2220590
Phenanthrene 0.0362 J 0.00760 0.0383 1 02/09/2024 00:29 WG2220590
Benzylbutyl phthalate U 0.0120 0.383 1 02/09/2024 00:29 WG2220590
Bis(2-ethylhexyl)phthalate 0.268 J 0.0485 0.383 1 02/09/2024 00:29 WG2220590
Di-n-butyl phthalate U 0.0131 0.383 1 02/09/2024 00:29 WG2220590
Diethyl phthalate U 0.0126 0.383 1 02/09/2024 00:29 WG2220590
Dimethyl phthalate U 0.0811 0.383 1 02/09/2024 00:29 WG2220590
Di-n-octyl phthalate U 0.0259 0.383 1 02/09/2024 00:29 WG2220590
Pyrene 0.0756 0.00745 0.0383 1 02/09/2024 00:29 WG2220590
1,2,4-Trichlorobenzene U 0.0120 0.383 1 02/09/2024 00:29 WG2220590
4-Chloro-3-methylphenol U 0.0124 0.383 1 02/09/2024 00:29 WG2220590
2-Chlorophenol U 0.0126 0.383 1 02/09/2024 00:29 WG2220590
2,4-Dichlorophenol U 0.0111 0.383 1 02/09/2024 00:29 WG2220590
2,4-Dimethylphenol U 0.0100 0.383 1 02/09/2024 00:29 WG2220590
4,6-Dinitro-2-methylphenol U 0.0868 0.383 1 02/09/2024 00:29 WG2220590
2,4-Dinitrophenol U 0.0895 0.383 1 02/09/2024 00:29 WG2220590
2-Nitrophenol U 0.0137 0.383 1 02/09/2024 00:29 WG2220590
4-Nitrophenol U 0.0120 0.383 1 02/09/2024 00:29 WG2220590
Pentachlorophenol U 0.0103 0.383 1 02/09/2024 00:29 WG2220590
Phenol U 0.0154 0.383 1 02/09/2024 00:29 WG2220590
2,4,6-Trichlorophenol U 0.0123 0.383 1 02/09/2024 00:29 WG2220590
(S) 2-Fluorophenol 71.3 12.0-120 02/09/2024 00:29 WG2220590
(S) Phenol-d5 72.0 10.0-120 02/09/2024 00:29 WG2220590
(S) Nitrobenzene-d5 70.5 10.0-122 02/09/2024 00:29 WG2220590
(S) 2-Fluorobiphenyl 69.3 15.0-120 02/09/2024 00:29 WG2220590
(S) 2,4,6-Tribromophenol 73.1 10.0-127 02/09/2024 00:29 WG2220590
(S) p-Terphenyl-d14 76.4 10.0-120 02/09/2024 00:29 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 21 of 89
SAMPLE RESULTS - 06
L1701794
SB-9 (1-2)
Collected date/time: 01/29/24 15:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.4 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0652 0.0893 1 02/05/2024 22:46 WG2220500
Acrylonitrile U 0.00645 0.0223 1 02/05/2024 22:46 WG2220500
Benzene U 0.000834 0.00179 1 02/05/2024 22:46 WG2220500
Bromobenzene U 0.00161 0.0223 1 02/05/2024 22:46 WG2220500
Bromodichloromethane U 0.00130 0.00447 1 02/05/2024 22:46 WG2220500
Bromoform U 0.00209 0.0447 1 02/05/2024 22:46 WG2220500
Bromomethane U 0.00352 0.0223 1 02/05/2024 22:46 WG2220500
n-Butylbenzene U 0.00938 0.0223 1 02/05/2024 22:46 WG2220500
sec-Butylbenzene U 0.00514 0.0223 1 02/05/2024 22:46 WG2220500
tert-Butylbenzene U 0.00348 0.00893 1 02/05/2024 22:46 WG2220500
Carbon tetrachloride U 0.00160 0.00893 1 02/05/2024 22:46 WG2220500
Chlorobenzene U 0.000375 0.00447 1 02/05/2024 22:46 WG2220500
Chlorodibromomethane U 0.00109 0.00447 1 02/05/2024 22:46 WG2220500
Chloroethane U 0.00304 0.00893 1 02/05/2024 22:46 WG2220500
Chloroform 0.00355 B J 0.00184 0.00447 1 02/05/2024 22:46 WG2220500
Chloromethane U 0.00777 0.0223 1 02/05/2024 22:46 WG2220500
2-Chlorotoluene U 0.00155 0.00447 1 02/05/2024 22:46 WG2220500
4-Chlorotoluene U 0.000804 0.00893 1 02/05/2024 22:46 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00697 0.0447 1 02/05/2024 22:46 WG2220500
1,2-Dibromoethane U 0.00116 0.00447 1 02/05/2024 22:46 WG2220500
Dibromomethane U 0.00134 0.00893 1 02/05/2024 22:46 WG2220500
1,2-Dichlorobenzene U 0.000759 0.00893 1 02/05/2024 22:46 WG2220500
1,3-Dichlorobenzene U 0.00107 0.00893 1 02/05/2024 22:46 WG2220500
1,4-Dichlorobenzene U 0.00125 0.00893 1 02/05/2024 22:46 WG2220500
Dichlorodifluoromethane U 0.00288 0.00893 1 02/05/2024 22:46 WG2220500
1,1-Dichloroethane U 0.000877 0.00447 1 02/05/2024 22:46 WG2220500
1,2-Dichloroethane U 0.00116 0.00447 1 02/05/2024 22:46 WG2220500
1,1-Dichloroethene U 0.00108 0.00447 1 02/05/2024 22:46 WG2220500
cis-1,2-Dichloroethene U 0.00131 0.00447 1 02/05/2024 22:46 WG2220500
trans-1,2-Dichloroethene U 0.00186 0.00893 1 02/05/2024 22:46 WG2220500
1,2-Dichloropropane U 0.00254 0.00893 1 02/05/2024 22:46 WG2220500
1,1-Dichloropropene U 0.00145 0.00447 1 02/05/2024 22:46 WG2220500
1,3-Dichloropropane U 0.000895 0.00893 1 02/05/2024 22:46 WG2220500
cis-1,3-Dichloropropene U 0.00135 0.00447 1 02/05/2024 22:46 WG2220500
trans-1,3-Dichloropropene U 0.00204 0.00893 1 02/05/2024 22:46 WG2220500
2,2-Dichloropropane U 0.00246 0.00447 1 02/05/2024 22:46 WG2220500
Di-isopropyl ether U 0.000732 0.00179 1 02/05/2024 22:46 WG2220500
Ethylbenzene U 0.00132 0.00447 1 02/05/2024 22:46 WG2220500
Hexachloro-1,3-butadiene U 0.0107 0.0447 1 02/05/2024 22:46 WG2220500
Isopropylbenzene U 0.000759 0.00447 1 02/05/2024 22:46 WG2220500
p-Isopropyltoluene U 0.00455 0.00893 1 02/05/2024 22:46 WG2220500
2-Butanone (MEK)U 0.113 0.179 1 02/05/2024 22:46 WG2220500
Methylene Chloride 0.0146 B J 0.0119 0.0447 1 02/05/2024 22:46 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00407 0.0447 1 02/05/2024 22:46 WG2220500
Methyl tert-butyl ether U 0.000625 0.00179 1 02/05/2024 22:46 WG2220500
Naphthalene U C3 0.00872 0.0223 1 02/05/2024 22:46 WG2220500
n-Propylbenzene U 0.00170 0.00893 1 02/05/2024 22:46 WG2220500
Styrene U 0.000409 0.0223 1 02/05/2024 22:46 WG2220500
1,1,1,2-Tetrachloroethane U 0.00169 0.00447 1 02/05/2024 22:46 WG2220500
1,1,2,2-Tetrachloroethane U 0.00124 0.00447 1 02/05/2024 22:46 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 22 of 89
SAMPLE RESULTS - 06
L1701794
SB-9 (1-2)
Collected date/time: 01/29/24 15:20
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00135 0.00447 1 02/05/2024 22:46 WG2220500
Tetrachloroethene U 0.00160 0.00447 1 02/05/2024 22:46 WG2220500
Toluene U 0.00232 0.00893 1 02/05/2024 22:46 WG2220500
1,2,3-Trichlorobenzene U 0.0131 0.0223 1 02/05/2024 22:46 WG2220500
1,2,4-Trichlorobenzene U 0.00786 0.0223 1 02/05/2024 22:46 WG2220500
1,1,1-Trichloroethane U 0.00165 0.00447 1 02/05/2024 22:46 WG2220500
1,1,2-Trichloroethane U 0.00107 0.00447 1 02/05/2024 22:46 WG2220500
Trichloroethene U J4 0.00104 0.00179 1 02/05/2024 22:46 WG2220500
Trichlorofluoromethane U 0.00148 0.00447 1 02/05/2024 22:46 WG2220500
1,2,3-Trichloropropane U 0.00289 0.0223 1 02/05/2024 22:46 WG2220500
1,2,4-Trimethylbenzene U 0.00282 0.00893 1 02/05/2024 22:46 WG2220500
1,2,3-Trimethylbenzene U 0.00282 0.00893 1 02/05/2024 22:46 WG2220500
1,3,5-Trimethylbenzene U 0.00357 0.00893 1 02/05/2024 22:46 WG2220500
Vinyl chloride U 0.00207 0.00447 1 02/05/2024 22:46 WG2220500
Xylenes, Total U 0.00157 0.0116 1 02/05/2024 22:46 WG2220500
(S) Toluene-d8 105 75.0-131 02/05/2024 22:46 WG2220500
(S) 4-Bromofluorobenzene 98.4 67.0-138 02/05/2024 22:46 WG2220500
(S) 1,2-Dichloroethane-d4 115 70.0-130 02/05/2024 22:46 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00725 0.0448 1 02/08/2024 18:41 WG2220590
Acenaphthylene U 0.00631 0.0448 1 02/08/2024 18:41 WG2220590
Anthracene U 0.00798 0.0448 1 02/08/2024 18:41 WG2220590
Benzidine U 0.0842 2.25 1 02/08/2024 18:41 WG2220590
Benzo(a)anthracene U 0.00790 0.0448 1 02/08/2024 18:41 WG2220590
Benzo(b)fluoranthene U 0.00835 0.0448 1 02/08/2024 18:41 WG2220590
Benzo(k)fluoranthene U 0.00796 0.0448 1 02/08/2024 18:41 WG2220590
Benzo(g,h,i)perylene U 0.00819 0.0448 1 02/08/2024 18:41 WG2220590
Benzo(a)pyrene U 0.00833 0.0448 1 02/08/2024 18:41 WG2220590
Bis(2-chlorethoxy)methane U 0.0134 0.448 1 02/08/2024 18:41 WG2220590
Bis(2-chloroethyl)ether U 0.0148 0.448 1 02/08/2024 18:41 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0194 0.448 1 02/08/2024 18:41 WG2220590
4-Bromophenyl-phenylether U 0.0157 0.448 1 02/08/2024 18:41 WG2220590
2-Chloronaphthalene U 0.00787 0.0448 1 02/08/2024 18:41 WG2220590
4-Chlorophenyl-phenylether U 0.0156 0.448 1 02/08/2024 18:41 WG2220590
Chrysene U 0.00890 0.0448 1 02/08/2024 18:41 WG2220590
Dibenz(a,h)anthracene U 0.0124 0.0448 1 02/08/2024 18:41 WG2220590
1,2-Dichlorobenzene U 0.0133 0.448 1 02/08/2024 18:41 WG2220590
1,3-Dichlorobenzene U 0.0136 0.448 1 02/08/2024 18:41 WG2220590
1,4-Dichlorobenzene U 0.0133 0.448 1 02/08/2024 18:41 WG2220590
3,3-Dichlorobenzidine U 0.0165 0.448 1 02/08/2024 18:41 WG2220590
2,4-Dinitrotoluene U 0.0128 0.448 1 02/08/2024 18:41 WG2220590
2,6-Dinitrotoluene U 0.0147 0.448 1 02/08/2024 18:41 WG2220590
Fluoranthene U 0.00808 0.0448 1 02/08/2024 18:41 WG2220590
Fluorene U 0.00729 0.0448 1 02/08/2024 18:41 WG2220590
Hexachlorobenzene U 0.0159 0.448 1 02/08/2024 18:41 WG2220590
Hexachloro-1,3-butadiene U 0.0151 0.448 1 02/08/2024 18:41 WG2220590
Hexachlorocyclopentadiene U 0.0235 0.448 1 02/08/2024 18:41 WG2220590
Hexachloroethane U 0.0176 0.448 1 02/08/2024 18:41 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0127 0.0448 1 02/08/2024 18:41 WG2220590
Isophorone U 0.0137 0.448 1 02/08/2024 18:41 WG2220590
Naphthalene U 0.0112 0.0448 1 02/08/2024 18:41 WG2220590
Nitrobenzene U 0.0156 0.448 1 02/08/2024 18:41 WG2220590
n-Nitrosodimethylamine U 0.0664 0.448 1 02/08/2024 18:41 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 06
L1701794
SB-9 (1-2)
Collected date/time: 01/29/24 15:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0339 0.448 1 02/08/2024 18:41 WG2220590
n-Nitrosodi-n-propylamine U 0.0149 0.448 1 02/08/2024 18:41 WG2220590
Phenanthrene U 0.00889 0.0448 1 02/08/2024 18:41 WG2220590
Benzylbutyl phthalate U 0.0140 0.448 1 02/08/2024 18:41 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0568 0.448 1 02/08/2024 18:41 WG2220590
Di-n-butyl phthalate U 0.0153 0.448 1 02/08/2024 18:41 WG2220590
Diethyl phthalate U 0.0148 0.448 1 02/08/2024 18:41 WG2220590
Dimethyl phthalate U 0.0950 0.448 1 02/08/2024 18:41 WG2220590
Di-n-octyl phthalate U 0.0303 0.448 1 02/08/2024 18:41 WG2220590
Pyrene U 0.00872 0.0448 1 02/08/2024 18:41 WG2220590
1,2,4-Trichlorobenzene U 0.0140 0.448 1 02/08/2024 18:41 WG2220590
4-Chloro-3-methylphenol U 0.0145 0.448 1 02/08/2024 18:41 WG2220590
2-Chlorophenol U 0.0148 0.448 1 02/08/2024 18:41 WG2220590
2,4-Dichlorophenol U 0.0130 0.448 1 02/08/2024 18:41 WG2220590
2,4-Dimethylphenol U 0.0117 0.448 1 02/08/2024 18:41 WG2220590
4,6-Dinitro-2-methylphenol U 0.102 0.448 1 02/08/2024 18:41 WG2220590
2,4-Dinitrophenol U 0.105 0.448 1 02/08/2024 18:41 WG2220590
2-Nitrophenol U 0.0160 0.448 1 02/08/2024 18:41 WG2220590
4-Nitrophenol U 0.0140 0.448 1 02/08/2024 18:41 WG2220590
Pentachlorophenol U 0.0121 0.448 1 02/08/2024 18:41 WG2220590
Phenol U 0.0180 0.448 1 02/08/2024 18:41 WG2220590
2,4,6-Trichlorophenol U 0.0144 0.448 1 02/08/2024 18:41 WG2220590
(S) 2-Fluorophenol 71.7 12.0-120 02/08/2024 18:41 WG2220590
(S) Phenol-d5 71.6 10.0-120 02/08/2024 18:41 WG2220590
(S) Nitrobenzene-d5 67.6 10.0-122 02/08/2024 18:41 WG2220590
(S) 2-Fluorobiphenyl 70.5 15.0-120 02/08/2024 18:41 WG2220590
(S) 2,4,6-Tribromophenol 68.4 10.0-127 02/08/2024 18:41 WG2220590
(S) p-Terphenyl-d14 72.7 10.0-120 02/08/2024 18:41 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 24 of 89
SAMPLE RESULTS - 07
L1701794
SB-11 0-1
Collected date/time: 01/30/24 09:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.3 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0502 0.0688 1 02/05/2024 23:06 WG2220500
Acrylonitrile U 0.00497 0.0172 1 02/05/2024 23:06 WG2220500
Benzene U 0.000643 0.00138 1 02/05/2024 23:06 WG2220500
Bromobenzene U 0.00124 0.0172 1 02/05/2024 23:06 WG2220500
Bromodichloromethane U 0.000998 0.00344 1 02/05/2024 23:06 WG2220500
Bromoform U 0.00161 0.0344 1 02/05/2024 23:06 WG2220500
Bromomethane U 0.00271 0.0172 1 02/05/2024 23:06 WG2220500
n-Butylbenzene U 0.00722 0.0172 1 02/05/2024 23:06 WG2220500
sec-Butylbenzene U 0.00396 0.0172 1 02/05/2024 23:06 WG2220500
tert-Butylbenzene U 0.00268 0.00688 1 02/05/2024 23:06 WG2220500
Carbon tetrachloride U 0.00124 0.00688 1 02/05/2024 23:06 WG2220500
Chlorobenzene U 0.000289 0.00344 1 02/05/2024 23:06 WG2220500
Chlorodibromomethane U 0.000842 0.00344 1 02/05/2024 23:06 WG2220500
Chloroethane U 0.00234 0.00688 1 02/05/2024 23:06 WG2220500
Chloroform 0.00195 B J 0.00142 0.00344 1 02/05/2024 23:06 WG2220500
Chloromethane U 0.00599 0.0172 1 02/05/2024 23:06 WG2220500
2-Chlorotoluene U 0.00119 0.00344 1 02/05/2024 23:06 WG2220500
4-Chlorotoluene U 0.000619 0.00688 1 02/05/2024 23:06 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00537 0.0344 1 02/05/2024 23:06 WG2220500
1,2-Dibromoethane U 0.000892 0.00344 1 02/05/2024 23:06 WG2220500
Dibromomethane U 0.00103 0.00688 1 02/05/2024 23:06 WG2220500
1,2-Dichlorobenzene U 0.000585 0.00688 1 02/05/2024 23:06 WG2220500
1,3-Dichlorobenzene U 0.000826 0.00688 1 02/05/2024 23:06 WG2220500
1,4-Dichlorobenzene U 0.000963 0.00688 1 02/05/2024 23:06 WG2220500
Dichlorodifluoromethane U 0.00222 0.00688 1 02/05/2024 23:06 WG2220500
1,1-Dichloroethane U 0.000676 0.00344 1 02/05/2024 23:06 WG2220500
1,2-Dichloroethane U 0.000893 0.00344 1 02/05/2024 23:06 WG2220500
1,1-Dichloroethene U 0.000834 0.00344 1 02/05/2024 23:06 WG2220500
cis-1,2-Dichloroethene U 0.00101 0.00344 1 02/05/2024 23:06 WG2220500
trans-1,2-Dichloroethene U 0.00143 0.00688 1 02/05/2024 23:06 WG2220500
1,2-Dichloropropane U 0.00195 0.00688 1 02/05/2024 23:06 WG2220500
1,1-Dichloropropene U 0.00111 0.00344 1 02/05/2024 23:06 WG2220500
1,3-Dichloropropane U 0.000689 0.00688 1 02/05/2024 23:06 WG2220500
cis-1,3-Dichloropropene U 0.00104 0.00344 1 02/05/2024 23:06 WG2220500
trans-1,3-Dichloropropene U 0.00157 0.00688 1 02/05/2024 23:06 WG2220500
2,2-Dichloropropane U 0.00190 0.00344 1 02/05/2024 23:06 WG2220500
Di-isopropyl ether U 0.000564 0.00138 1 02/05/2024 23:06 WG2220500
Ethylbenzene U 0.00101 0.00344 1 02/05/2024 23:06 WG2220500
Hexachloro-1,3-butadiene U 0.00826 0.0344 1 02/05/2024 23:06 WG2220500
Isopropylbenzene U 0.000585 0.00344 1 02/05/2024 23:06 WG2220500
p-Isopropyltoluene U 0.00351 0.00688 1 02/05/2024 23:06 WG2220500
2-Butanone (MEK)U 0.0874 0.138 1 02/05/2024 23:06 WG2220500
Methylene Chloride 0.0133 B J 0.00914 0.0344 1 02/05/2024 23:06 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00314 0.0344 1 02/05/2024 23:06 WG2220500
Methyl tert-butyl ether U 0.000482 0.00138 1 02/05/2024 23:06 WG2220500
Naphthalene U C3 0.00671 0.0172 1 02/05/2024 23:06 WG2220500
n-Propylbenzene U 0.00131 0.00688 1 02/05/2024 23:06 WG2220500
Styrene U 0.000315 0.0172 1 02/05/2024 23:06 WG2220500
1,1,1,2-Tetrachloroethane U 0.00130 0.00344 1 02/05/2024 23:06 WG2220500
1,1,2,2-Tetrachloroethane U 0.000956 0.00344 1 02/05/2024 23:06 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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AECOM - Raleigh, NC 60722767 L1701794 02/19/24 20:18 25 of 89
SAMPLE RESULTS - 07
L1701794
SB-11 0-1
Collected date/time: 01/30/24 09:05
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00104 0.00344 1 02/05/2024 23:06 WG2220500
Tetrachloroethene U 0.00123 0.00344 1 02/05/2024 23:06 WG2220500
Toluene U 0.00179 0.00688 1 02/05/2024 23:06 WG2220500
1,2,3-Trichlorobenzene U 0.0101 0.0172 1 02/05/2024 23:06 WG2220500
1,2,4-Trichlorobenzene U 0.00605 0.0172 1 02/05/2024 23:06 WG2220500
1,1,1-Trichloroethane U 0.00127 0.00344 1 02/05/2024 23:06 WG2220500
1,1,2-Trichloroethane U 0.000821 0.00344 1 02/05/2024 23:06 WG2220500
Trichloroethene U J4 0.000804 0.00138 1 02/05/2024 23:06 WG2220500
Trichlorofluoromethane U 0.00114 0.00344 1 02/05/2024 23:06 WG2220500
1,2,3-Trichloropropane U 0.00223 0.0172 1 02/05/2024 23:06 WG2220500
1,2,4-Trimethylbenzene U 0.00217 0.00688 1 02/05/2024 23:06 WG2220500
1,2,3-Trimethylbenzene U 0.00217 0.00688 1 02/05/2024 23:06 WG2220500
1,3,5-Trimethylbenzene U 0.00275 0.00688 1 02/05/2024 23:06 WG2220500
Vinyl chloride U 0.00160 0.00344 1 02/05/2024 23:06 WG2220500
Xylenes, Total U 0.00121 0.00894 1 02/05/2024 23:06 WG2220500
(S) Toluene-d8 103 75.0-131 02/05/2024 23:06 WG2220500
(S) 4-Bromofluorobenzene 97.9 67.0-138 02/05/2024 23:06 WG2220500
(S) 1,2-Dichloroethane-d4 115 70.0-130 02/05/2024 23:06 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00632 0.0390 1 02/08/2024 19:22 WG2220590
Acenaphthylene U 0.00550 0.0390 1 02/08/2024 19:22 WG2220590
Anthracene U 0.00695 0.0390 1 02/08/2024 19:22 WG2220590
Benzidine U 0.0734 1.96 1 02/08/2024 19:22 WG2220590
Benzo(a)anthracene 0.00698 J 0.00688 0.0390 1 02/08/2024 19:22 WG2220590
Benzo(b)fluoranthene 0.0124 J 0.00728 0.0390 1 02/08/2024 19:22 WG2220590
Benzo(k)fluoranthene U 0.00694 0.0390 1 02/08/2024 19:22 WG2220590
Benzo(g,h,i)perylene 0.00952 J 0.00714 0.0390 1 02/08/2024 19:22 WG2220590
Benzo(a)pyrene 0.00866 J 0.00726 0.0390 1 02/08/2024 19:22 WG2220590
Bis(2-chlorethoxy)methane U 0.0117 0.390 1 02/08/2024 19:22 WG2220590
Bis(2-chloroethyl)ether U 0.0129 0.390 1 02/08/2024 19:22 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0169 0.390 1 02/08/2024 19:22 WG2220590
4-Bromophenyl-phenylether U 0.0137 0.390 1 02/08/2024 19:22 WG2220590
2-Chloronaphthalene U 0.00686 0.0390 1 02/08/2024 19:22 WG2220590
4-Chlorophenyl-phenylether U 0.0136 0.390 1 02/08/2024 19:22 WG2220590
Chrysene 0.00788 J 0.00776 0.0390 1 02/08/2024 19:22 WG2220590
Dibenz(a,h)anthracene U 0.0108 0.0390 1 02/08/2024 19:22 WG2220590
1,2-Dichlorobenzene U 0.0116 0.390 1 02/08/2024 19:22 WG2220590
1,3-Dichlorobenzene U 0.0118 0.390 1 02/08/2024 19:22 WG2220590
1,4-Dichlorobenzene U 0.0116 0.390 1 02/08/2024 19:22 WG2220590
3,3-Dichlorobenzidine U 0.0144 0.390 1 02/08/2024 19:22 WG2220590
2,4-Dinitrotoluene U 0.0112 0.390 1 02/08/2024 19:22 WG2220590
2,6-Dinitrotoluene U 0.0128 0.390 1 02/08/2024 19:22 WG2220590
Fluoranthene 0.0163 J 0.00705 0.0390 1 02/08/2024 19:22 WG2220590
Fluorene U 0.00635 0.0390 1 02/08/2024 19:22 WG2220590
Hexachlorobenzene U 0.0138 0.390 1 02/08/2024 19:22 WG2220590
Hexachloro-1,3-butadiene U 0.0131 0.390 1 02/08/2024 19:22 WG2220590
Hexachlorocyclopentadiene U 0.0205 0.390 1 02/08/2024 19:22 WG2220590
Hexachloroethane U 0.0154 0.390 1 02/08/2024 19:22 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0110 0.0390 1 02/08/2024 19:22 WG2220590
Isophorone U 0.0120 0.390 1 02/08/2024 19:22 WG2220590
Naphthalene U 0.00980 0.0390 1 02/08/2024 19:22 WG2220590
Nitrobenzene U 0.0136 0.390 1 02/08/2024 19:22 WG2220590
n-Nitrosodimethylamine U 0.0579 0.390 1 02/08/2024 19:22 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 07
L1701794
SB-11 0-1
Collected date/time: 01/30/24 09:05
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0295 0.390 1 02/08/2024 19:22 WG2220590
n-Nitrosodi-n-propylamine U 0.0130 0.390 1 02/08/2024 19:22 WG2220590
Phenanthrene U 0.00775 0.0390 1 02/08/2024 19:22 WG2220590
Benzylbutyl phthalate U 0.0122 0.390 1 02/08/2024 19:22 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0495 0.390 1 02/08/2024 19:22 WG2220590
Di-n-butyl phthalate U 0.0134 0.390 1 02/08/2024 19:22 WG2220590
Diethyl phthalate U 0.0129 0.390 1 02/08/2024 19:22 WG2220590
Dimethyl phthalate U 0.0828 0.390 1 02/08/2024 19:22 WG2220590
Di-n-octyl phthalate U 0.0264 0.390 1 02/08/2024 19:22 WG2220590
Pyrene 0.0156 J 0.00760 0.0390 1 02/08/2024 19:22 WG2220590
1,2,4-Trichlorobenzene U 0.0122 0.390 1 02/08/2024 19:22 WG2220590
4-Chloro-3-methylphenol U 0.0127 0.390 1 02/08/2024 19:22 WG2220590
2-Chlorophenol U 0.0129 0.390 1 02/08/2024 19:22 WG2220590
2,4-Dichlorophenol U 0.0114 0.390 1 02/08/2024 19:22 WG2220590
2,4-Dimethylphenol U 0.0102 0.390 1 02/08/2024 19:22 WG2220590
4,6-Dinitro-2-methylphenol U 0.0885 0.390 1 02/08/2024 19:22 WG2220590
2,4-Dinitrophenol U 0.0913 0.390 1 02/08/2024 19:22 WG2220590
2-Nitrophenol U 0.0140 0.390 1 02/08/2024 19:22 WG2220590
4-Nitrophenol U 0.0122 0.390 1 02/08/2024 19:22 WG2220590
Pentachlorophenol U 0.0105 0.390 1 02/08/2024 19:22 WG2220590
Phenol U 0.0157 0.390 1 02/08/2024 19:22 WG2220590
2,4,6-Trichlorophenol U 0.0125 0.390 1 02/08/2024 19:22 WG2220590
(S) 2-Fluorophenol 68.2 12.0-120 02/08/2024 19:22 WG2220590
(S) Phenol-d5 66.3 10.0-120 02/08/2024 19:22 WG2220590
(S) Nitrobenzene-d5 67.7 10.0-122 02/08/2024 19:22 WG2220590
(S) 2-Fluorobiphenyl 68.1 15.0-120 02/08/2024 19:22 WG2220590
(S) 2,4,6-Tribromophenol 70.4 10.0-127 02/08/2024 19:22 WG2220590
(S) p-Terphenyl-d14 73.5 10.0-120 02/08/2024 19:22 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 08
L1701794
SB-11 1-2
Collected date/time: 01/30/24 09:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 70.9 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0685 0.0939 1 02/05/2024 23:25 WG2220500
Acrylonitrile U 0.00678 0.0235 1 02/05/2024 23:25 WG2220500
Benzene U 0.000877 0.00188 1 02/05/2024 23:25 WG2220500
Bromobenzene U 0.00169 0.0235 1 02/05/2024 23:25 WG2220500
Bromodichloromethane U 0.00136 0.00469 1 02/05/2024 23:25 WG2220500
Bromoform U 0.00220 0.0469 1 02/05/2024 23:25 WG2220500
Bromomethane U 0.00370 0.0235 1 02/05/2024 23:25 WG2220500
n-Butylbenzene U 0.00986 0.0235 1 02/05/2024 23:25 WG2220500
sec-Butylbenzene U 0.00541 0.0235 1 02/05/2024 23:25 WG2220500
tert-Butylbenzene U 0.00366 0.00939 1 02/05/2024 23:25 WG2220500
Carbon tetrachloride U 0.00169 0.00939 1 02/05/2024 23:25 WG2220500
Chlorobenzene U 0.000394 0.00469 1 02/05/2024 23:25 WG2220500
Chlorodibromomethane U 0.00115 0.00469 1 02/05/2024 23:25 WG2220500
Chloroethane U 0.00319 0.00939 1 02/05/2024 23:25 WG2220500
Chloroform 0.00406 B J 0.00193 0.00469 1 02/05/2024 23:25 WG2220500
Chloromethane U 0.00817 0.0235 1 02/05/2024 23:25 WG2220500
2-Chlorotoluene U 0.00162 0.00469 1 02/05/2024 23:25 WG2220500
4-Chlorotoluene U 0.000845 0.00939 1 02/05/2024 23:25 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00732 0.0469 1 02/05/2024 23:25 WG2220500
1,2-Dibromoethane U 0.00122 0.00469 1 02/05/2024 23:25 WG2220500
Dibromomethane U 0.00141 0.00939 1 02/05/2024 23:25 WG2220500
1,2-Dichlorobenzene U 0.000798 0.00939 1 02/05/2024 23:25 WG2220500
1,3-Dichlorobenzene U 0.00113 0.00939 1 02/05/2024 23:25 WG2220500
1,4-Dichlorobenzene U 0.00131 0.00939 1 02/05/2024 23:25 WG2220500
Dichlorodifluoromethane U 0.00302 0.00939 1 02/05/2024 23:25 WG2220500
1,1-Dichloroethane U 0.000922 0.00469 1 02/05/2024 23:25 WG2220500
1,2-Dichloroethane U 0.00122 0.00469 1 02/05/2024 23:25 WG2220500
1,1-Dichloroethene U 0.00114 0.00469 1 02/05/2024 23:25 WG2220500
cis-1,2-Dichloroethene U 0.00138 0.00469 1 02/05/2024 23:25 WG2220500
trans-1,2-Dichloroethene U 0.00195 0.00939 1 02/05/2024 23:25 WG2220500
1,2-Dichloropropane U 0.00267 0.00939 1 02/05/2024 23:25 WG2220500
1,1-Dichloropropene U 0.00152 0.00469 1 02/05/2024 23:25 WG2220500
1,3-Dichloropropane U 0.000941 0.00939 1 02/05/2024 23:25 WG2220500
cis-1,3-Dichloropropene U 0.00142 0.00469 1 02/05/2024 23:25 WG2220500
trans-1,3-Dichloropropene U 0.00214 0.00939 1 02/05/2024 23:25 WG2220500
2,2-Dichloropropane U 0.00259 0.00469 1 02/05/2024 23:25 WG2220500
Di-isopropyl ether U 0.000770 0.00188 1 02/05/2024 23:25 WG2220500
Ethylbenzene U 0.00138 0.00469 1 02/05/2024 23:25 WG2220500
Hexachloro-1,3-butadiene U 0.0113 0.0469 1 02/05/2024 23:25 WG2220500
Isopropylbenzene U 0.000798 0.00469 1 02/05/2024 23:25 WG2220500
p-Isopropyltoluene U 0.00479 0.00939 1 02/05/2024 23:25 WG2220500
2-Butanone (MEK)U 0.119 0.188 1 02/05/2024 23:25 WG2220500
Methylene Chloride 0.0166 B J 0.0125 0.0469 1 02/05/2024 23:25 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00428 0.0469 1 02/05/2024 23:25 WG2220500
Methyl tert-butyl ether U 0.000657 0.00188 1 02/05/2024 23:25 WG2220500
Naphthalene U C3 0.00916 0.0235 1 02/05/2024 23:25 WG2220500
n-Propylbenzene U 0.00178 0.00939 1 02/05/2024 23:25 WG2220500
Styrene U 0.000430 0.0235 1 02/05/2024 23:25 WG2220500
1,1,1,2-Tetrachloroethane U 0.00178 0.00469 1 02/05/2024 23:25 WG2220500
1,1,2,2-Tetrachloroethane U 0.00131 0.00469 1 02/05/2024 23:25 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 08
L1701794
SB-11 1-2
Collected date/time: 01/30/24 09:15
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00142 0.00469 1 02/05/2024 23:25 WG2220500
Tetrachloroethene U 0.00168 0.00469 1 02/05/2024 23:25 WG2220500
Toluene U 0.00244 0.00939 1 02/05/2024 23:25 WG2220500
1,2,3-Trichlorobenzene U 0.0138 0.0235 1 02/05/2024 23:25 WG2220500
1,2,4-Trichlorobenzene U 0.00826 0.0235 1 02/05/2024 23:25 WG2220500
1,1,1-Trichloroethane U 0.00173 0.00469 1 02/05/2024 23:25 WG2220500
1,1,2-Trichloroethane U 0.00112 0.00469 1 02/05/2024 23:25 WG2220500
Trichloroethene U J4 0.00110 0.00188 1 02/05/2024 23:25 WG2220500
Trichlorofluoromethane U 0.00155 0.00469 1 02/05/2024 23:25 WG2220500
1,2,3-Trichloropropane U 0.00304 0.0235 1 02/05/2024 23:25 WG2220500
1,2,4-Trimethylbenzene U 0.00297 0.00939 1 02/05/2024 23:25 WG2220500
1,2,3-Trimethylbenzene U 0.00297 0.00939 1 02/05/2024 23:25 WG2220500
1,3,5-Trimethylbenzene U 0.00376 0.00939 1 02/05/2024 23:25 WG2220500
Vinyl chloride U 0.00218 0.00469 1 02/05/2024 23:25 WG2220500
Xylenes, Total U 0.00165 0.0122 1 02/05/2024 23:25 WG2220500
(S) Toluene-d8 106 75.0-131 02/05/2024 23:25 WG2220500
(S) 4-Bromofluorobenzene 98.8 67.0-138 02/05/2024 23:25 WG2220500
(S) 1,2-Dichloroethane-d4 117 70.0-130 02/05/2024 23:25 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00760 0.0470 1 02/08/2024 19:01 WG2220590
Acenaphthylene U 0.00662 0.0470 1 02/08/2024 19:01 WG2220590
Anthracene U 0.00837 0.0470 1 02/08/2024 19:01 WG2220590
Benzidine U 0.0883 2.36 1 02/08/2024 19:01 WG2220590
Benzo(a)anthracene U 0.00828 0.0470 1 02/08/2024 19:01 WG2220590
Benzo(b)fluoranthene U 0.00876 0.0470 1 02/08/2024 19:01 WG2220590
Benzo(k)fluoranthene U 0.00835 0.0470 1 02/08/2024 19:01 WG2220590
Benzo(g,h,i)perylene U 0.00859 0.0470 1 02/08/2024 19:01 WG2220590
Benzo(a)pyrene U 0.00873 0.0470 1 02/08/2024 19:01 WG2220590
Bis(2-chlorethoxy)methane U 0.0141 0.470 1 02/08/2024 19:01 WG2220590
Bis(2-chloroethyl)ether U 0.0155 0.470 1 02/08/2024 19:01 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0203 0.470 1 02/08/2024 19:01 WG2220590
4-Bromophenyl-phenylether U 0.0165 0.470 1 02/08/2024 19:01 WG2220590
2-Chloronaphthalene U 0.00825 0.0470 1 02/08/2024 19:01 WG2220590
4-Chlorophenyl-phenylether U 0.0164 0.470 1 02/08/2024 19:01 WG2220590
Chrysene U 0.00934 0.0470 1 02/08/2024 19:01 WG2220590
Dibenz(a,h)anthracene U 0.0130 0.0470 1 02/08/2024 19:01 WG2220590
1,2-Dichlorobenzene U 0.0139 0.470 1 02/08/2024 19:01 WG2220590
1,3-Dichlorobenzene U 0.0142 0.470 1 02/08/2024 19:01 WG2220590
1,4-Dichlorobenzene U 0.0140 0.470 1 02/08/2024 19:01 WG2220590
3,3-Dichlorobenzidine U 0.0174 0.470 1 02/08/2024 19:01 WG2220590
2,4-Dinitrotoluene U 0.0135 0.470 1 02/08/2024 19:01 WG2220590
2,6-Dinitrotoluene U 0.0154 0.470 1 02/08/2024 19:01 WG2220590
Fluoranthene U 0.00848 0.0470 1 02/08/2024 19:01 WG2220590
Fluorene U 0.00765 0.0470 1 02/08/2024 19:01 WG2220590
Hexachlorobenzene U 0.0166 0.470 1 02/08/2024 19:01 WG2220590
Hexachloro-1,3-butadiene U 0.0158 0.470 1 02/08/2024 19:01 WG2220590
Hexachlorocyclopentadiene U 0.0247 0.470 1 02/08/2024 19:01 WG2220590
Hexachloroethane U 0.0185 0.470 1 02/08/2024 19:01 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0133 0.0470 1 02/08/2024 19:01 WG2220590
Isophorone U 0.0144 0.470 1 02/08/2024 19:01 WG2220590
Naphthalene U 0.0118 0.0470 1 02/08/2024 19:01 WG2220590
Nitrobenzene U 0.0164 0.470 1 02/08/2024 19:01 WG2220590
n-Nitrosodimethylamine U 0.0697 0.470 1 02/08/2024 19:01 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 08
L1701794
SB-11 1-2
Collected date/time: 01/30/24 09:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0356 0.470 1 02/08/2024 19:01 WG2220590
n-Nitrosodi-n-propylamine U 0.0157 0.470 1 02/08/2024 19:01 WG2220590
Phenanthrene U 0.00933 0.0470 1 02/08/2024 19:01 WG2220590
Benzylbutyl phthalate U 0.0147 0.470 1 02/08/2024 19:01 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0595 0.470 1 02/08/2024 19:01 WG2220590
Di-n-butyl phthalate U 0.0161 0.470 1 02/08/2024 19:01 WG2220590
Diethyl phthalate U 0.0155 0.470 1 02/08/2024 19:01 WG2220590
Dimethyl phthalate U 0.0996 0.470 1 02/08/2024 19:01 WG2220590
Di-n-octyl phthalate U 0.0317 0.470 1 02/08/2024 19:01 WG2220590
Pyrene U 0.00914 0.0470 1 02/08/2024 19:01 WG2220590
1,2,4-Trichlorobenzene U 0.0147 0.470 1 02/08/2024 19:01 WG2220590
4-Chloro-3-methylphenol U 0.0152 0.470 1 02/08/2024 19:01 WG2220590
2-Chlorophenol U 0.0155 0.470 1 02/08/2024 19:01 WG2220590
2,4-Dichlorophenol U 0.0137 0.470 1 02/08/2024 19:01 WG2220590
2,4-Dimethylphenol U 0.0123 0.470 1 02/08/2024 19:01 WG2220590
4,6-Dinitro-2-methylphenol U 0.107 0.470 1 02/08/2024 19:01 WG2220590
2,4-Dinitrophenol U 0.110 0.470 1 02/08/2024 19:01 WG2220590
2-Nitrophenol U 0.0168 0.470 1 02/08/2024 19:01 WG2220590
4-Nitrophenol U 0.0147 0.470 1 02/08/2024 19:01 WG2220590
Pentachlorophenol U 0.0126 0.470 1 02/08/2024 19:01 WG2220590
Phenol U 0.0189 0.470 1 02/08/2024 19:01 WG2220590
2,4,6-Trichlorophenol U 0.0151 0.470 1 02/08/2024 19:01 WG2220590
(S) 2-Fluorophenol 71.6 12.0-120 02/08/2024 19:01 WG2220590
(S) Phenol-d5 72.2 10.0-120 02/08/2024 19:01 WG2220590
(S) Nitrobenzene-d5 67.2 10.0-122 02/08/2024 19:01 WG2220590
(S) 2-Fluorobiphenyl 68.4 15.0-120 02/08/2024 19:01 WG2220590
(S) 2,4,6-Tribromophenol 76.9 10.0-127 02/08/2024 19:01 WG2220590
(S) p-Terphenyl-d14 75.6 10.0-120 02/08/2024 19:01 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 09
L1701794
SB-6 0-1
Collected date/time: 01/30/24 14:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 87.2 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0487 0.0668 1 02/05/2024 23:44 WG2220500
Acrylonitrile U 0.00482 0.0167 1 02/05/2024 23:44 WG2220500
Benzene U 0.000624 0.00134 1 02/05/2024 23:44 WG2220500
Bromobenzene U 0.00120 0.0167 1 02/05/2024 23:44 WG2220500
Bromodichloromethane U 0.000968 0.00334 1 02/05/2024 23:44 WG2220500
Bromoform U 0.00156 0.0334 1 02/05/2024 23:44 WG2220500
Bromomethane U 0.00263 0.0167 1 02/05/2024 23:44 WG2220500
n-Butylbenzene U 0.00701 0.0167 1 02/05/2024 23:44 WG2220500
sec-Butylbenzene U 0.00385 0.0167 1 02/05/2024 23:44 WG2220500
tert-Butylbenzene U 0.00260 0.00668 1 02/05/2024 23:44 WG2220500
Carbon tetrachloride U 0.00120 0.00668 1 02/05/2024 23:44 WG2220500
Chlorobenzene U 0.000280 0.00334 1 02/05/2024 23:44 WG2220500
Chlorodibromomethane U 0.000817 0.00334 1 02/05/2024 23:44 WG2220500
Chloroethane U 0.00227 0.00668 1 02/05/2024 23:44 WG2220500
Chloroform 0.00200 B J 0.00138 0.00334 1 02/05/2024 23:44 WG2220500
Chloromethane U 0.00581 0.0167 1 02/05/2024 23:44 WG2220500
2-Chlorotoluene U 0.00115 0.00334 1 02/05/2024 23:44 WG2220500
4-Chlorotoluene U 0.000601 0.00668 1 02/05/2024 23:44 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00521 0.0334 1 02/05/2024 23:44 WG2220500
1,2-Dibromoethane U 0.000865 0.00334 1 02/05/2024 23:44 WG2220500
Dibromomethane U 0.00100 0.00668 1 02/05/2024 23:44 WG2220500
1,2-Dichlorobenzene U 0.000567 0.00668 1 02/05/2024 23:44 WG2220500
1,3-Dichlorobenzene U 0.000801 0.00668 1 02/05/2024 23:44 WG2220500
1,4-Dichlorobenzene U 0.000935 0.00668 1 02/05/2024 23:44 WG2220500
Dichlorodifluoromethane U 0.00215 0.00668 1 02/05/2024 23:44 WG2220500
1,1-Dichloroethane U 0.000656 0.00334 1 02/05/2024 23:44 WG2220500
1,2-Dichloroethane U 0.000867 0.00334 1 02/05/2024 23:44 WG2220500
1,1-Dichloroethene U 0.000809 0.00334 1 02/05/2024 23:44 WG2220500
cis-1,2-Dichloroethene U 0.000980 0.00334 1 02/05/2024 23:44 WG2220500
trans-1,2-Dichloroethene U 0.00139 0.00668 1 02/05/2024 23:44 WG2220500
1,2-Dichloropropane U 0.00190 0.00668 1 02/05/2024 23:44 WG2220500
1,1-Dichloropropene U 0.00108 0.00334 1 02/05/2024 23:44 WG2220500
1,3-Dichloropropane U 0.000669 0.00668 1 02/05/2024 23:44 WG2220500
cis-1,3-Dichloropropene U 0.00101 0.00334 1 02/05/2024 23:44 WG2220500
trans-1,3-Dichloropropene U 0.00152 0.00668 1 02/05/2024 23:44 WG2220500
2,2-Dichloropropane U 0.00184 0.00334 1 02/05/2024 23:44 WG2220500
Di-isopropyl ether U 0.000547 0.00134 1 02/05/2024 23:44 WG2220500
Ethylbenzene U 0.000984 0.00334 1 02/05/2024 23:44 WG2220500
Hexachloro-1,3-butadiene U 0.00801 0.0334 1 02/05/2024 23:44 WG2220500
Isopropylbenzene U 0.000567 0.00334 1 02/05/2024 23:44 WG2220500
p-Isopropyltoluene U 0.00340 0.00668 1 02/05/2024 23:44 WG2220500
2-Butanone (MEK)U 0.0848 0.134 1 02/05/2024 23:44 WG2220500
Methylene Chloride 0.00989 B J 0.00887 0.0334 1 02/05/2024 23:44 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00304 0.0334 1 02/05/2024 23:44 WG2220500
Methyl tert-butyl ether U 0.000467 0.00134 1 02/05/2024 23:44 WG2220500
Naphthalene U C3 0.00652 0.0167 1 02/05/2024 23:44 WG2220500
n-Propylbenzene U 0.00127 0.00668 1 02/05/2024 23:44 WG2220500
Styrene U 0.000306 0.0167 1 02/05/2024 23:44 WG2220500
1,1,1,2-Tetrachloroethane U 0.00127 0.00334 1 02/05/2024 23:44 WG2220500
1,1,2,2-Tetrachloroethane U 0.000928 0.00334 1 02/05/2024 23:44 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 09
L1701794
SB-6 0-1
Collected date/time: 01/30/24 14:45
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00101 0.00334 1 02/05/2024 23:44 WG2220500
Tetrachloroethene 0.00907 0.00120 0.00334 1 02/05/2024 23:44 WG2220500
Toluene 0.00175 J 0.00174 0.00668 1 02/05/2024 23:44 WG2220500
1,2,3-Trichlorobenzene U 0.00979 0.0167 1 02/05/2024 23:44 WG2220500
1,2,4-Trichlorobenzene U 0.00587 0.0167 1 02/05/2024 23:44 WG2220500
1,1,1-Trichloroethane U 0.00123 0.00334 1 02/05/2024 23:44 WG2220500
1,1,2-Trichloroethane U 0.000797 0.00334 1 02/05/2024 23:44 WG2220500
Trichloroethene U J4 0.000780 0.00134 1 02/05/2024 23:44 WG2220500
Trichlorofluoromethane U 0.00110 0.00334 1 02/05/2024 23:44 WG2220500
1,2,3-Trichloropropane U 0.00216 0.0167 1 02/05/2024 23:44 WG2220500
1,2,4-Trimethylbenzene U 0.00211 0.00668 1 02/05/2024 23:44 WG2220500
1,2,3-Trimethylbenzene U 0.00211 0.00668 1 02/05/2024 23:44 WG2220500
1,3,5-Trimethylbenzene U 0.00267 0.00668 1 02/05/2024 23:44 WG2220500
Vinyl chloride U 0.00155 0.00334 1 02/05/2024 23:44 WG2220500
Xylenes, Total 0.00130 J 0.00117 0.00868 1 02/05/2024 23:44 WG2220500
(S) Toluene-d8 105 75.0-131 02/05/2024 23:44 WG2220500
(S) 4-Bromofluorobenzene 99.8 67.0-138 02/05/2024 23:44 WG2220500
(S) 1,2-Dichloroethane-d4 114 70.0-130 02/05/2024 23:44 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00618 0.0382 1 02/09/2024 00:09 WG2220590
Acenaphthylene U 0.00538 0.0382 1 02/09/2024 00:09 WG2220590
Anthracene U 0.00680 0.0382 1 02/09/2024 00:09 WG2220590
Benzidine U 0.0718 1.92 1 02/09/2024 00:09 WG2220590
Benzo(a)anthracene U 0.00673 0.0382 1 02/09/2024 00:09 WG2220590
Benzo(b)fluoranthene U 0.00712 0.0382 1 02/09/2024 00:09 WG2220590
Benzo(k)fluoranthene U 0.00679 0.0382 1 02/09/2024 00:09 WG2220590
Benzo(g,h,i)perylene U 0.00699 0.0382 1 02/09/2024 00:09 WG2220590
Benzo(a)pyrene U 0.00710 0.0382 1 02/09/2024 00:09 WG2220590
Bis(2-chlorethoxy)methane U 0.0115 0.382 1 02/09/2024 00:09 WG2220590
Bis(2-chloroethyl)ether U 0.0126 0.382 1 02/09/2024 00:09 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0165 0.382 1 02/09/2024 00:09 WG2220590
4-Bromophenyl-phenylether U 0.0134 0.382 1 02/09/2024 00:09 WG2220590
2-Chloronaphthalene U 0.00671 0.0382 1 02/09/2024 00:09 WG2220590
4-Chlorophenyl-phenylether U 0.0133 0.382 1 02/09/2024 00:09 WG2220590
Chrysene U 0.00759 0.0382 1 02/09/2024 00:09 WG2220590
Dibenz(a,h)anthracene U 0.0106 0.0382 1 02/09/2024 00:09 WG2220590
1,2-Dichlorobenzene U 0.0113 0.382 1 02/09/2024 00:09 WG2220590
1,3-Dichlorobenzene U 0.0116 0.382 1 02/09/2024 00:09 WG2220590
1,4-Dichlorobenzene U 0.0114 0.382 1 02/09/2024 00:09 WG2220590
3,3-Dichlorobenzidine U 0.0141 0.382 1 02/09/2024 00:09 WG2220590
2,4-Dinitrotoluene U 0.0110 0.382 1 02/09/2024 00:09 WG2220590
2,6-Dinitrotoluene U 0.0125 0.382 1 02/09/2024 00:09 WG2220590
Fluoranthene U 0.00690 0.0382 1 02/09/2024 00:09 WG2220590
Fluorene U 0.00622 0.0382 1 02/09/2024 00:09 WG2220590
Hexachlorobenzene U 0.0135 0.382 1 02/09/2024 00:09 WG2220590
Hexachloro-1,3-butadiene U 0.0128 0.382 1 02/09/2024 00:09 WG2220590
Hexachlorocyclopentadiene U 0.0201 0.382 1 02/09/2024 00:09 WG2220590
Hexachloroethane U 0.0150 0.382 1 02/09/2024 00:09 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0108 0.0382 1 02/09/2024 00:09 WG2220590
Isophorone U 0.0117 0.382 1 02/09/2024 00:09 WG2220590
Naphthalene U 0.00959 0.0382 1 02/09/2024 00:09 WG2220590
Nitrobenzene U 0.0133 0.382 1 02/09/2024 00:09 WG2220590
n-Nitrosodimethylamine U 0.0567 0.382 1 02/09/2024 00:09 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 09
L1701794
SB-6 0-1
Collected date/time: 01/30/24 14:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0289 0.382 1 02/09/2024 00:09 WG2220590
n-Nitrosodi-n-propylamine U 0.0127 0.382 1 02/09/2024 00:09 WG2220590
Phenanthrene U 0.00758 0.0382 1 02/09/2024 00:09 WG2220590
Benzylbutyl phthalate U 0.0119 0.382 1 02/09/2024 00:09 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0484 0.382 1 02/09/2024 00:09 WG2220590
Di-n-butyl phthalate U 0.0131 0.382 1 02/09/2024 00:09 WG2220590
Diethyl phthalate U 0.0126 0.382 1 02/09/2024 00:09 WG2220590
Dimethyl phthalate U 0.0810 0.382 1 02/09/2024 00:09 WG2220590
Di-n-octyl phthalate U 0.0258 0.382 1 02/09/2024 00:09 WG2220590
Pyrene U 0.00743 0.0382 1 02/09/2024 00:09 WG2220590
1,2,4-Trichlorobenzene U 0.0119 0.382 1 02/09/2024 00:09 WG2220590
4-Chloro-3-methylphenol U 0.0124 0.382 1 02/09/2024 00:09 WG2220590
2-Chlorophenol U 0.0126 0.382 1 02/09/2024 00:09 WG2220590
2,4-Dichlorophenol U 0.0111 0.382 1 02/09/2024 00:09 WG2220590
2,4-Dimethylphenol U 0.00998 0.382 1 02/09/2024 00:09 WG2220590
4,6-Dinitro-2-methylphenol U 0.0866 0.382 1 02/09/2024 00:09 WG2220590
2,4-Dinitrophenol U 0.0894 0.382 1 02/09/2024 00:09 WG2220590
2-Nitrophenol U 0.0137 0.382 1 02/09/2024 00:09 WG2220590
4-Nitrophenol U 0.0119 0.382 1 02/09/2024 00:09 WG2220590
Pentachlorophenol U 0.0103 0.382 1 02/09/2024 00:09 WG2220590
Phenol U 0.0154 0.382 1 02/09/2024 00:09 WG2220590
2,4,6-Trichlorophenol U 0.0123 0.382 1 02/09/2024 00:09 WG2220590
(S) 2-Fluorophenol 75.0 12.0-120 02/09/2024 00:09 WG2220590
(S) Phenol-d5 74.1 10.0-120 02/09/2024 00:09 WG2220590
(S) Nitrobenzene-d5 69.8 10.0-122 02/09/2024 00:09 WG2220590
(S) 2-Fluorobiphenyl 70.7 15.0-120 02/09/2024 00:09 WG2220590
(S) 2,4,6-Tribromophenol 80.6 10.0-127 02/09/2024 00:09 WG2220590
(S) p-Terphenyl-d14 78.7 10.0-120 02/09/2024 00:09 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 10
L1701794
SB-6 1-2
Collected date/time: 01/30/24 14:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.0 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0585 0.0801 1 02/06/2024 00:03 WG2220500
Acrylonitrile U 0.00578 0.0200 1 02/06/2024 00:03 WG2220500
Benzene U 0.000748 0.00160 1 02/06/2024 00:03 WG2220500
Bromobenzene U 0.00144 0.0200 1 02/06/2024 00:03 WG2220500
Bromodichloromethane U 0.00116 0.00400 1 02/06/2024 00:03 WG2220500
Bromoform U 0.00187 0.0400 1 02/06/2024 00:03 WG2220500
Bromomethane U 0.00315 0.0200 1 02/06/2024 00:03 WG2220500
n-Butylbenzene U 0.00841 0.0200 1 02/06/2024 00:03 WG2220500
sec-Butylbenzene U 0.00461 0.0200 1 02/06/2024 00:03 WG2220500
tert-Butylbenzene U 0.00312 0.00801 1 02/06/2024 00:03 WG2220500
Carbon tetrachloride U 0.00144 0.00801 1 02/06/2024 00:03 WG2220500
Chlorobenzene U 0.000336 0.00400 1 02/06/2024 00:03 WG2220500
Chlorodibromomethane U 0.000980 0.00400 1 02/06/2024 00:03 WG2220500
Chloroethane U 0.00272 0.00801 1 02/06/2024 00:03 WG2220500
Chloroform 0.00298 B J 0.00165 0.00400 1 02/06/2024 00:03 WG2220500
Chloromethane U 0.00697 0.0200 1 02/06/2024 00:03 WG2220500
2-Chlorotoluene U 0.00139 0.00400 1 02/06/2024 00:03 WG2220500
4-Chlorotoluene U 0.000721 0.00801 1 02/06/2024 00:03 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00625 0.0400 1 02/06/2024 00:03 WG2220500
1,2-Dibromoethane U 0.00104 0.00400 1 02/06/2024 00:03 WG2220500
Dibromomethane U 0.00120 0.00801 1 02/06/2024 00:03 WG2220500
1,2-Dichlorobenzene U 0.000681 0.00801 1 02/06/2024 00:03 WG2220500
1,3-Dichlorobenzene U 0.000961 0.00801 1 02/06/2024 00:03 WG2220500
1,4-Dichlorobenzene U 0.00112 0.00801 1 02/06/2024 00:03 WG2220500
Dichlorodifluoromethane U 0.00258 0.00801 1 02/06/2024 00:03 WG2220500
1,1-Dichloroethane U 0.000786 0.00400 1 02/06/2024 00:03 WG2220500
1,2-Dichloroethane U 0.00104 0.00400 1 02/06/2024 00:03 WG2220500
1,1-Dichloroethene U 0.000970 0.00400 1 02/06/2024 00:03 WG2220500
cis-1,2-Dichloroethene U 0.00118 0.00400 1 02/06/2024 00:03 WG2220500
trans-1,2-Dichloroethene U 0.00167 0.00801 1 02/06/2024 00:03 WG2220500
1,2-Dichloropropane U 0.00227 0.00801 1 02/06/2024 00:03 WG2220500
1,1-Dichloropropene U 0.00130 0.00400 1 02/06/2024 00:03 WG2220500
1,3-Dichloropropane U 0.000802 0.00801 1 02/06/2024 00:03 WG2220500
cis-1,3-Dichloropropene U 0.00121 0.00400 1 02/06/2024 00:03 WG2220500
trans-1,3-Dichloropropene U 0.00183 0.00801 1 02/06/2024 00:03 WG2220500
2,2-Dichloropropane U 0.00221 0.00400 1 02/06/2024 00:03 WG2220500
Di-isopropyl ether U 0.000657 0.00160 1 02/06/2024 00:03 WG2220500
Ethylbenzene U 0.00118 0.00400 1 02/06/2024 00:03 WG2220500
Hexachloro-1,3-butadiene U 0.00961 0.0400 1 02/06/2024 00:03 WG2220500
Isopropylbenzene U 0.000681 0.00400 1 02/06/2024 00:03 WG2220500
p-Isopropyltoluene U 0.00408 0.00801 1 02/06/2024 00:03 WG2220500
2-Butanone (MEK)U 0.102 0.160 1 02/06/2024 00:03 WG2220500
Methylene Chloride 0.0125 B J 0.0106 0.0400 1 02/06/2024 00:03 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00365 0.0400 1 02/06/2024 00:03 WG2220500
Methyl tert-butyl ether U 0.000561 0.00160 1 02/06/2024 00:03 WG2220500
Naphthalene U C3 0.00782 0.0200 1 02/06/2024 00:03 WG2220500
n-Propylbenzene U 0.00152 0.00801 1 02/06/2024 00:03 WG2220500
Styrene U 0.000367 0.0200 1 02/06/2024 00:03 WG2220500
1,1,1,2-Tetrachloroethane U 0.00152 0.00400 1 02/06/2024 00:03 WG2220500
1,1,2,2-Tetrachloroethane U 0.00111 0.00400 1 02/06/2024 00:03 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 10
L1701794
SB-6 1-2
Collected date/time: 01/30/24 14:55
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00121 0.00400 1 02/06/2024 00:03 WG2220500
Tetrachloroethene 0.00448 0.00143 0.00400 1 02/06/2024 00:03 WG2220500
Toluene U 0.00208 0.00801 1 02/06/2024 00:03 WG2220500
1,2,3-Trichlorobenzene U 0.0117 0.0200 1 02/06/2024 00:03 WG2220500
1,2,4-Trichlorobenzene U 0.00705 0.0200 1 02/06/2024 00:03 WG2220500
1,1,1-Trichloroethane U 0.00148 0.00400 1 02/06/2024 00:03 WG2220500
1,1,2-Trichloroethane U 0.000956 0.00400 1 02/06/2024 00:03 WG2220500
Trichloroethene U J4 0.000935 0.00160 1 02/06/2024 00:03 WG2220500
Trichlorofluoromethane U 0.00132 0.00400 1 02/06/2024 00:03 WG2220500
1,2,3-Trichloropropane U 0.00259 0.0200 1 02/06/2024 00:03 WG2220500
1,2,4-Trimethylbenzene U 0.00253 0.00801 1 02/06/2024 00:03 WG2220500
1,2,3-Trimethylbenzene U 0.00253 0.00801 1 02/06/2024 00:03 WG2220500
1,3,5-Trimethylbenzene U 0.00320 0.00801 1 02/06/2024 00:03 WG2220500
Vinyl chloride U 0.00186 0.00400 1 02/06/2024 00:03 WG2220500
Xylenes, Total U 0.00141 0.0104 1 02/06/2024 00:03 WG2220500
(S) Toluene-d8 105 75.0-131 02/06/2024 00:03 WG2220500
(S) 4-Bromofluorobenzene 97.4 67.0-138 02/06/2024 00:03 WG2220500
(S) 1,2-Dichloroethane-d4 116 70.0-130 02/06/2024 00:03 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00682 0.0422 1 02/08/2024 20:03 WG2220590
Acenaphthylene U 0.00594 0.0422 1 02/08/2024 20:03 WG2220590
Anthracene U 0.00751 0.0422 1 02/08/2024 20:03 WG2220590
Benzidine U 0.0792 2.11 1 02/08/2024 20:03 WG2220590
Benzo(a)anthracene U 0.00743 0.0422 1 02/08/2024 20:03 WG2220590
Benzo(b)fluoranthene U 0.00786 0.0422 1 02/08/2024 20:03 WG2220590
Benzo(k)fluoranthene U 0.00749 0.0422 1 02/08/2024 20:03 WG2220590
Benzo(g,h,i)perylene U 0.00771 0.0422 1 02/08/2024 20:03 WG2220590
Benzo(a)pyrene U 0.00784 0.0422 1 02/08/2024 20:03 WG2220590
Bis(2-chlorethoxy)methane U 0.0127 0.422 1 02/08/2024 20:03 WG2220590
Bis(2-chloroethyl)ether U 0.0139 0.422 1 02/08/2024 20:03 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0182 0.422 1 02/08/2024 20:03 WG2220590
4-Bromophenyl-phenylether U 0.0148 0.422 1 02/08/2024 20:03 WG2220590
2-Chloronaphthalene U 0.00740 0.0422 1 02/08/2024 20:03 WG2220590
4-Chlorophenyl-phenylether U 0.0147 0.422 1 02/08/2024 20:03 WG2220590
Chrysene U 0.00838 0.0422 1 02/08/2024 20:03 WG2220590
Dibenz(a,h)anthracene U 0.0117 0.0422 1 02/08/2024 20:03 WG2220590
1,2-Dichlorobenzene U 0.0125 0.422 1 02/08/2024 20:03 WG2220590
1,3-Dichlorobenzene U 0.0128 0.422 1 02/08/2024 20:03 WG2220590
1,4-Dichlorobenzene U 0.0125 0.422 1 02/08/2024 20:03 WG2220590
3,3-Dichlorobenzidine U 0.0156 0.422 1 02/08/2024 20:03 WG2220590
2,4-Dinitrotoluene U 0.0121 0.422 1 02/08/2024 20:03 WG2220590
2,6-Dinitrotoluene U 0.0138 0.422 1 02/08/2024 20:03 WG2220590
Fluoranthene U 0.00761 0.0422 1 02/08/2024 20:03 WG2220590
Fluorene U 0.00686 0.0422 1 02/08/2024 20:03 WG2220590
Hexachlorobenzene U 0.0149 0.422 1 02/08/2024 20:03 WG2220590
Hexachloro-1,3-butadiene U 0.0142 0.422 1 02/08/2024 20:03 WG2220590
Hexachlorocyclopentadiene U 0.0222 0.422 1 02/08/2024 20:03 WG2220590
Hexachloroethane U 0.0166 0.422 1 02/08/2024 20:03 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0119 0.0422 1 02/08/2024 20:03 WG2220590
Isophorone U 0.0129 0.422 1 02/08/2024 20:03 WG2220590
Naphthalene 0.0261 J 0.0106 0.0422 1 02/08/2024 20:03 WG2220590
Nitrobenzene U 0.0147 0.422 1 02/08/2024 20:03 WG2220590
n-Nitrosodimethylamine U 0.0625 0.422 1 02/08/2024 20:03 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 10
L1701794
SB-6 1-2
Collected date/time: 01/30/24 14:55
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0319 0.422 1 02/08/2024 20:03 WG2220590
n-Nitrosodi-n-propylamine U 0.0141 0.422 1 02/08/2024 20:03 WG2220590
Phenanthrene U 0.00837 0.0422 1 02/08/2024 20:03 WG2220590
Benzylbutyl phthalate U 0.0132 0.422 1 02/08/2024 20:03 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0534 0.422 1 02/08/2024 20:03 WG2220590
Di-n-butyl phthalate U 0.0144 0.422 1 02/08/2024 20:03 WG2220590
Diethyl phthalate U 0.0139 0.422 1 02/08/2024 20:03 WG2220590
Dimethyl phthalate U 0.0894 0.422 1 02/08/2024 20:03 WG2220590
Di-n-octyl phthalate U 0.0285 0.422 1 02/08/2024 20:03 WG2220590
Pyrene U 0.00820 0.0422 1 02/08/2024 20:03 WG2220590
1,2,4-Trichlorobenzene U 0.0132 0.422 1 02/08/2024 20:03 WG2220590
4-Chloro-3-methylphenol U 0.0137 0.422 1 02/08/2024 20:03 WG2220590
2-Chlorophenol U 0.0139 0.422 1 02/08/2024 20:03 WG2220590
2,4-Dichlorophenol U 0.0123 0.422 1 02/08/2024 20:03 WG2220590
2,4-Dimethylphenol U 0.0110 0.422 1 02/08/2024 20:03 WG2220590
4,6-Dinitro-2-methylphenol U 0.0956 0.422 1 02/08/2024 20:03 WG2220590
2,4-Dinitrophenol U 0.0986 0.422 1 02/08/2024 20:03 WG2220590
2-Nitrophenol U 0.0151 0.422 1 02/08/2024 20:03 WG2220590
4-Nitrophenol U 0.0132 0.422 1 02/08/2024 20:03 WG2220590
Pentachlorophenol U 0.0113 0.422 1 02/08/2024 20:03 WG2220590
Phenol U 0.0170 0.422 1 02/08/2024 20:03 WG2220590
2,4,6-Trichlorophenol U 0.0135 0.422 1 02/08/2024 20:03 WG2220590
(S) 2-Fluorophenol 72.8 12.0-120 02/08/2024 20:03 WG2220590
(S) Phenol-d5 69.3 10.0-120 02/08/2024 20:03 WG2220590
(S) Nitrobenzene-d5 63.1 10.0-122 02/08/2024 20:03 WG2220590
(S) 2-Fluorobiphenyl 66.2 15.0-120 02/08/2024 20:03 WG2220590
(S) 2,4,6-Tribromophenol 70.8 10.0-127 02/08/2024 20:03 WG2220590
(S) p-Terphenyl-d14 77.0 10.0-120 02/08/2024 20:03 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 11
L1701794
SB-4 0-1
Collected date/time: 01/31/24 10:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.7 1 02/06/2024 11:02 WG2219977
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0620 0.0849 1 02/06/2024 00:23 WG2220500
Acrylonitrile U 0.00613 0.0212 1 02/06/2024 00:23 WG2220500
Benzene U 0.000793 0.00170 1 02/06/2024 00:23 WG2220500
Bromobenzene U 0.00153 0.0212 1 02/06/2024 00:23 WG2220500
Bromodichloromethane U 0.00123 0.00425 1 02/06/2024 00:23 WG2220500
Bromoform U 0.00199 0.0425 1 02/06/2024 00:23 WG2220500
Bromomethane U 0.00335 0.0212 1 02/06/2024 00:23 WG2220500
n-Butylbenzene U 0.00892 0.0212 1 02/06/2024 00:23 WG2220500
sec-Butylbenzene U 0.00489 0.0212 1 02/06/2024 00:23 WG2220500
tert-Butylbenzene U 0.00331 0.00849 1 02/06/2024 00:23 WG2220500
Carbon tetrachloride U 0.00152 0.00849 1 02/06/2024 00:23 WG2220500
Chlorobenzene U 0.000357 0.00425 1 02/06/2024 00:23 WG2220500
Chlorodibromomethane U 0.00104 0.00425 1 02/06/2024 00:23 WG2220500
Chloroethane U 0.00289 0.00849 1 02/06/2024 00:23 WG2220500
Chloroform 0.00328 B J 0.00175 0.00425 1 02/06/2024 00:23 WG2220500
Chloromethane U 0.00739 0.0212 1 02/06/2024 00:23 WG2220500
2-Chlorotoluene U 0.00147 0.00425 1 02/06/2024 00:23 WG2220500
4-Chlorotoluene U 0.000764 0.00849 1 02/06/2024 00:23 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00662 0.0425 1 02/06/2024 00:23 WG2220500
1,2-Dibromoethane U 0.00110 0.00425 1 02/06/2024 00:23 WG2220500
Dibromomethane U 0.00127 0.00849 1 02/06/2024 00:23 WG2220500
1,2-Dichlorobenzene U 0.000722 0.00849 1 02/06/2024 00:23 WG2220500
1,3-Dichlorobenzene U 0.00102 0.00849 1 02/06/2024 00:23 WG2220500
1,4-Dichlorobenzene U 0.00119 0.00849 1 02/06/2024 00:23 WG2220500
Dichlorodifluoromethane U 0.00273 0.00849 1 02/06/2024 00:23 WG2220500
1,1-Dichloroethane U 0.000834 0.00425 1 02/06/2024 00:23 WG2220500
1,2-Dichloroethane U 0.00110 0.00425 1 02/06/2024 00:23 WG2220500
1,1-Dichloroethene U 0.00103 0.00425 1 02/06/2024 00:23 WG2220500
cis-1,2-Dichloroethene U 0.00125 0.00425 1 02/06/2024 00:23 WG2220500
trans-1,2-Dichloroethene U 0.00177 0.00849 1 02/06/2024 00:23 WG2220500
1,2-Dichloropropane U 0.00241 0.00849 1 02/06/2024 00:23 WG2220500
1,1-Dichloropropene U 0.00137 0.00425 1 02/06/2024 00:23 WG2220500
1,3-Dichloropropane U 0.000851 0.00849 1 02/06/2024 00:23 WG2220500
cis-1,3-Dichloropropene U 0.00129 0.00425 1 02/06/2024 00:23 WG2220500
trans-1,3-Dichloropropene U 0.00194 0.00849 1 02/06/2024 00:23 WG2220500
2,2-Dichloropropane U 0.00234 0.00425 1 02/06/2024 00:23 WG2220500
Di-isopropyl ether U 0.000696 0.00170 1 02/06/2024 00:23 WG2220500
Ethylbenzene U 0.00125 0.00425 1 02/06/2024 00:23 WG2220500
Hexachloro-1,3-butadiene U 0.0102 0.0425 1 02/06/2024 00:23 WG2220500
Isopropylbenzene U 0.000722 0.00425 1 02/06/2024 00:23 WG2220500
p-Isopropyltoluene U 0.00433 0.00849 1 02/06/2024 00:23 WG2220500
2-Butanone (MEK)U 0.108 0.170 1 02/06/2024 00:23 WG2220500
Methylene Chloride 0.0187 B J 0.0113 0.0425 1 02/06/2024 00:23 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00387 0.0425 1 02/06/2024 00:23 WG2220500
Methyl tert-butyl ether U 0.000594 0.00170 1 02/06/2024 00:23 WG2220500
Naphthalene U C3 0.00829 0.0212 1 02/06/2024 00:23 WG2220500
n-Propylbenzene U 0.00161 0.00849 1 02/06/2024 00:23 WG2220500
Styrene U 0.000389 0.0212 1 02/06/2024 00:23 WG2220500
1,1,1,2-Tetrachloroethane U 0.00161 0.00425 1 02/06/2024 00:23 WG2220500
1,1,2,2-Tetrachloroethane U 0.00118 0.00425 1 02/06/2024 00:23 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 11
L1701794
SB-4 0-1
Collected date/time: 01/31/24 10:45
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00128 0.00425 1 02/06/2024 00:23 WG2220500
Tetrachloroethene U 0.00152 0.00425 1 02/06/2024 00:23 WG2220500
Toluene U 0.00221 0.00849 1 02/06/2024 00:23 WG2220500
1,2,3-Trichlorobenzene U 0.0124 0.0212 1 02/06/2024 00:23 WG2220500
1,2,4-Trichlorobenzene U 0.00747 0.0212 1 02/06/2024 00:23 WG2220500
1,1,1-Trichloroethane U 0.00157 0.00425 1 02/06/2024 00:23 WG2220500
1,1,2-Trichloroethane U 0.00101 0.00425 1 02/06/2024 00:23 WG2220500
Trichloroethene U J4 0.000992 0.00170 1 02/06/2024 00:23 WG2220500
Trichlorofluoromethane U 0.00140 0.00425 1 02/06/2024 00:23 WG2220500
1,2,3-Trichloropropane U 0.00275 0.0212 1 02/06/2024 00:23 WG2220500
1,2,4-Trimethylbenzene U 0.00268 0.00849 1 02/06/2024 00:23 WG2220500
1,2,3-Trimethylbenzene U 0.00268 0.00849 1 02/06/2024 00:23 WG2220500
1,3,5-Trimethylbenzene U 0.00340 0.00849 1 02/06/2024 00:23 WG2220500
Vinyl chloride U 0.00197 0.00425 1 02/06/2024 00:23 WG2220500
Xylenes, Total U 0.00149 0.0110 1 02/06/2024 00:23 WG2220500
(S) Toluene-d8 104 75.0-131 02/06/2024 00:23 WG2220500
(S) 4-Bromofluorobenzene 97.2 67.0-138 02/06/2024 00:23 WG2220500
(S) 1,2-Dichloroethane-d4 116 70.0-130 02/06/2024 00:23 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00722 0.0446 1 02/15/2024 06:11 WG2220590
Acenaphthylene U 0.00628 0.0446 1 02/15/2024 06:11 WG2220590
Anthracene U 0.00794 0.0446 1 02/15/2024 06:11 WG2220590
Benzidine U 0.0838 2.24 1 02/15/2024 06:11 WG2220590
Benzo(a)anthracene U 0.00786 0.0446 1 02/15/2024 06:11 WG2220590
Benzo(b)fluoranthene U 0.00832 0.0446 1 02/15/2024 06:11 WG2220590
Benzo(k)fluoranthene U 0.00793 0.0446 1 02/15/2024 06:11 WG2220590
Benzo(g,h,i)perylene U 0.00815 0.0446 1 02/15/2024 06:11 WG2220590
Benzo(a)pyrene U 0.00829 0.0446 1 02/15/2024 06:11 WG2220590
Bis(2-chlorethoxy)methane U 0.0134 0.446 1 02/15/2024 06:11 WG2220590
Bis(2-chloroethyl)ether U 0.0147 0.446 1 02/15/2024 06:11 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0193 0.446 1 02/15/2024 06:11 WG2220590
4-Bromophenyl-phenylether U 0.0157 0.446 1 02/15/2024 06:11 WG2220590
2-Chloronaphthalene U 0.00783 0.0446 1 02/15/2024 06:11 WG2220590
4-Chlorophenyl-phenylether U 0.0155 0.446 1 02/15/2024 06:11 WG2220590
Chrysene U 0.00886 0.0446 1 02/15/2024 06:11 WG2220590
Dibenz(a,h)anthracene U 0.0124 0.0446 1 02/15/2024 06:11 WG2220590
1,2-Dichlorobenzene U 0.0132 0.446 1 02/15/2024 06:11 WG2220590
1,3-Dichlorobenzene U 0.0135 0.446 1 02/15/2024 06:11 WG2220590
1,4-Dichlorobenzene U 0.0133 0.446 1 02/15/2024 06:11 WG2220590
3,3-Dichlorobenzidine U 0.0165 0.446 1 02/15/2024 06:11 WG2220590
2,4-Dinitrotoluene U 0.0128 0.446 1 02/15/2024 06:11 WG2220590
2,6-Dinitrotoluene U 0.0146 0.446 1 02/15/2024 06:11 WG2220590
Fluoranthene U 0.00805 0.0446 1 02/15/2024 06:11 WG2220590
Fluorene U 0.00726 0.0446 1 02/15/2024 06:11 WG2220590
Hexachlorobenzene U 0.0158 0.446 1 02/15/2024 06:11 WG2220590
Hexachloro-1,3-butadiene U 0.0150 0.446 1 02/15/2024 06:11 WG2220590
Hexachlorocyclopentadiene U 0.0234 0.446 1 02/15/2024 06:11 WG2220590
Hexachloroethane U 0.0175 0.446 1 02/15/2024 06:11 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0126 0.0446 1 02/15/2024 06:11 WG2220590
Isophorone U 0.0137 0.446 1 02/15/2024 06:11 WG2220590
Naphthalene U 0.0112 0.0446 1 02/15/2024 06:11 WG2220590
Nitrobenzene U 0.0155 0.446 1 02/15/2024 06:11 WG2220590
n-Nitrosodimethylamine U 0.0662 0.446 1 02/15/2024 06:11 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 11
L1701794
SB-4 0-1
Collected date/time: 01/31/24 10:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0337 0.446 1 02/15/2024 06:11 WG2220590
n-Nitrosodi-n-propylamine U 0.0149 0.446 1 02/15/2024 06:11 WG2220590
Phenanthrene U 0.00885 0.0446 1 02/15/2024 06:11 WG2220590
Benzylbutyl phthalate U 0.0139 0.446 1 02/15/2024 06:11 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0565 0.446 1 02/15/2024 06:11 WG2220590
Di-n-butyl phthalate U 0.0153 0.446 1 02/15/2024 06:11 WG2220590
Diethyl phthalate U 0.0147 0.446 1 02/15/2024 06:11 WG2220590
Dimethyl phthalate U 0.0945 0.446 1 02/15/2024 06:11 WG2220590
Di-n-octyl phthalate U 0.0301 0.446 1 02/15/2024 06:11 WG2220590
Pyrene U 0.00868 0.0446 1 02/15/2024 06:11 WG2220590
1,2,4-Trichlorobenzene U 0.0139 0.446 1 02/15/2024 06:11 WG2220590
4-Chloro-3-methylphenol U 0.0145 0.446 1 02/15/2024 06:11 WG2220590
2-Chlorophenol U 0.0147 0.446 1 02/15/2024 06:11 WG2220590
2,4-Dichlorophenol U 0.0130 0.446 1 02/15/2024 06:11 WG2220590
2,4-Dimethylphenol U 0.0116 0.446 1 02/15/2024 06:11 WG2220590
4,6-Dinitro-2-methylphenol U 0.101 0.446 1 02/15/2024 06:11 WG2220590
2,4-Dinitrophenol U 0.104 0.446 1 02/15/2024 06:11 WG2220590
2-Nitrophenol U 0.0159 0.446 1 02/15/2024 06:11 WG2220590
4-Nitrophenol U 0.0139 0.446 1 02/15/2024 06:11 WG2220590
Pentachlorophenol U 0.0120 0.446 1 02/15/2024 06:11 WG2220590
Phenol U 0.0179 0.446 1 02/15/2024 06:11 WG2220590
2,4,6-Trichlorophenol U 0.0143 0.446 1 02/15/2024 06:11 WG2220590
(S) 2-Fluorophenol 67.8 12.0-120 02/15/2024 06:11 WG2220590
(S) Phenol-d5 60.9 10.0-120 02/15/2024 06:11 WG2220590
(S) Nitrobenzene-d5 54.4 10.0-122 02/15/2024 06:11 WG2220590
(S) 2-Fluorobiphenyl 64.1 15.0-120 02/15/2024 06:11 WG2220590
(S) 2,4,6-Tribromophenol 84.8 10.0-127 02/15/2024 06:11 WG2220590
(S) p-Terphenyl-d14 71.2 10.0-120 02/15/2024 06:11 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 12
L1701794
SB-4 2-3
Collected date/time: 01/31/24 10:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.5 1 02/06/2024 15:26 WG2220127
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0623 0.0854 1 02/06/2024 00:42 WG2220500
Acrylonitrile U 0.00616 0.0213 1 02/06/2024 00:42 WG2220500
Benzene U 0.000797 0.00171 1 02/06/2024 00:42 WG2220500
Bromobenzene U 0.00154 0.0213 1 02/06/2024 00:42 WG2220500
Bromodichloromethane U 0.00124 0.00427 1 02/06/2024 00:42 WG2220500
Bromoform U 0.00200 0.0427 1 02/06/2024 00:42 WG2220500
Bromomethane U 0.00336 0.0213 1 02/06/2024 00:42 WG2220500
n-Butylbenzene U 0.00896 0.0213 1 02/06/2024 00:42 WG2220500
sec-Butylbenzene U 0.00492 0.0213 1 02/06/2024 00:42 WG2220500
tert-Butylbenzene U 0.00333 0.00854 1 02/06/2024 00:42 WG2220500
Carbon tetrachloride U 0.00153 0.00854 1 02/06/2024 00:42 WG2220500
Chlorobenzene U 0.000358 0.00427 1 02/06/2024 00:42 WG2220500
Chlorodibromomethane U 0.00104 0.00427 1 02/06/2024 00:42 WG2220500
Chloroethane U 0.00290 0.00854 1 02/06/2024 00:42 WG2220500
Chloroform 0.00318 B J 0.00176 0.00427 1 02/06/2024 00:42 WG2220500
Chloromethane U 0.00743 0.0213 1 02/06/2024 00:42 WG2220500
2-Chlorotoluene U 0.00148 0.00427 1 02/06/2024 00:42 WG2220500
4-Chlorotoluene U 0.000768 0.00854 1 02/06/2024 00:42 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00666 0.0427 1 02/06/2024 00:42 WG2220500
1,2-Dibromoethane U 0.00111 0.00427 1 02/06/2024 00:42 WG2220500
Dibromomethane U 0.00128 0.00854 1 02/06/2024 00:42 WG2220500
1,2-Dichlorobenzene U 0.000726 0.00854 1 02/06/2024 00:42 WG2220500
1,3-Dichlorobenzene U 0.00102 0.00854 1 02/06/2024 00:42 WG2220500
1,4-Dichlorobenzene U 0.00119 0.00854 1 02/06/2024 00:42 WG2220500
Dichlorodifluoromethane U 0.00275 0.00854 1 02/06/2024 00:42 WG2220500
1,1-Dichloroethane U 0.000838 0.00427 1 02/06/2024 00:42 WG2220500
1,2-Dichloroethane U 0.00111 0.00427 1 02/06/2024 00:42 WG2220500
1,1-Dichloroethene U 0.00103 0.00427 1 02/06/2024 00:42 WG2220500
cis-1,2-Dichloroethene U 0.00125 0.00427 1 02/06/2024 00:42 WG2220500
trans-1,2-Dichloroethene U 0.00178 0.00854 1 02/06/2024 00:42 WG2220500
1,2-Dichloropropane U 0.00242 0.00854 1 02/06/2024 00:42 WG2220500
1,1-Dichloropropene U 0.00138 0.00427 1 02/06/2024 00:42 WG2220500
1,3-Dichloropropane U 0.000855 0.00854 1 02/06/2024 00:42 WG2220500
cis-1,3-Dichloropropene U 0.00129 0.00427 1 02/06/2024 00:42 WG2220500
trans-1,3-Dichloropropene U 0.00195 0.00854 1 02/06/2024 00:42 WG2220500
2,2-Dichloropropane U 0.00236 0.00427 1 02/06/2024 00:42 WG2220500
Di-isopropyl ether U 0.000700 0.00171 1 02/06/2024 00:42 WG2220500
Ethylbenzene U 0.00126 0.00427 1 02/06/2024 00:42 WG2220500
Hexachloro-1,3-butadiene U 0.0102 0.0427 1 02/06/2024 00:42 WG2220500
Isopropylbenzene U 0.000726 0.00427 1 02/06/2024 00:42 WG2220500
p-Isopropyltoluene U 0.00435 0.00854 1 02/06/2024 00:42 WG2220500
2-Butanone (MEK)U 0.108 0.171 1 02/06/2024 00:42 WG2220500
Methylene Chloride 0.0151 B J 0.0113 0.0427 1 02/06/2024 00:42 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00389 0.0427 1 02/06/2024 00:42 WG2220500
Methyl tert-butyl ether U 0.000597 0.00171 1 02/06/2024 00:42 WG2220500
Naphthalene U C3 0.00833 0.0213 1 02/06/2024 00:42 WG2220500
n-Propylbenzene U 0.00162 0.00854 1 02/06/2024 00:42 WG2220500
Styrene U 0.000391 0.0213 1 02/06/2024 00:42 WG2220500
1,1,1,2-Tetrachloroethane U 0.00162 0.00427 1 02/06/2024 00:42 WG2220500
1,1,2,2-Tetrachloroethane U 0.00119 0.00427 1 02/06/2024 00:42 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 12
L1701794
SB-4 2-3
Collected date/time: 01/31/24 10:50
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00129 0.00427 1 02/06/2024 00:42 WG2220500
Tetrachloroethene U 0.00153 0.00427 1 02/06/2024 00:42 WG2220500
Toluene U 0.00222 0.00854 1 02/06/2024 00:42 WG2220500
1,2,3-Trichlorobenzene U 0.0125 0.0213 1 02/06/2024 00:42 WG2220500
1,2,4-Trichlorobenzene U 0.00751 0.0213 1 02/06/2024 00:42 WG2220500
1,1,1-Trichloroethane U 0.00158 0.00427 1 02/06/2024 00:42 WG2220500
1,1,2-Trichloroethane U 0.00102 0.00427 1 02/06/2024 00:42 WG2220500
Trichloroethene U J4 0.000997 0.00171 1 02/06/2024 00:42 WG2220500
Trichlorofluoromethane U 0.00141 0.00427 1 02/06/2024 00:42 WG2220500
1,2,3-Trichloropropane U 0.00277 0.0213 1 02/06/2024 00:42 WG2220500
1,2,4-Trimethylbenzene U 0.00270 0.00854 1 02/06/2024 00:42 WG2220500
1,2,3-Trimethylbenzene U 0.00270 0.00854 1 02/06/2024 00:42 WG2220500
1,3,5-Trimethylbenzene U 0.00341 0.00854 1 02/06/2024 00:42 WG2220500
Vinyl chloride U 0.00198 0.00427 1 02/06/2024 00:42 WG2220500
Xylenes, Total U 0.00150 0.0111 1 02/06/2024 00:42 WG2220500
(S) Toluene-d8 102 75.0-131 02/06/2024 00:42 WG2220500
(S) 4-Bromofluorobenzene 95.6 67.0-138 02/06/2024 00:42 WG2220500
(S) 1,2-Dichloroethane-d4 118 70.0-130 02/06/2024 00:42 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00724 0.0447 1 02/08/2024 20:23 WG2220590
Acenaphthylene U 0.00630 0.0447 1 02/08/2024 20:23 WG2220590
Anthracene U 0.00796 0.0447 1 02/08/2024 20:23 WG2220590
Benzidine U 0.0841 2.24 1 02/08/2024 20:23 WG2220590
Benzo(a)anthracene U 0.00788 0.0447 1 02/08/2024 20:23 WG2220590
Benzo(b)fluoranthene U 0.00834 0.0447 1 02/08/2024 20:23 WG2220590
Benzo(k)fluoranthene U 0.00795 0.0447 1 02/08/2024 20:23 WG2220590
Benzo(g,h,i)perylene U 0.00818 0.0447 1 02/08/2024 20:23 WG2220590
Benzo(a)pyrene U 0.00831 0.0447 1 02/08/2024 20:23 WG2220590
Bis(2-chlorethoxy)methane U 0.0134 0.447 1 02/08/2024 20:23 WG2220590
Bis(2-chloroethyl)ether U 0.0148 0.447 1 02/08/2024 20:23 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0193 0.447 1 02/08/2024 20:23 WG2220590
4-Bromophenyl-phenylether U 0.0157 0.447 1 02/08/2024 20:23 WG2220590
2-Chloronaphthalene U 0.00786 0.0447 1 02/08/2024 20:23 WG2220590
4-Chlorophenyl-phenylether U 0.0156 0.447 1 02/08/2024 20:23 WG2220590
Chrysene U 0.00889 0.0447 1 02/08/2024 20:23 WG2220590
Dibenz(a,h)anthracene U 0.0124 0.0447 1 02/08/2024 20:23 WG2220590
1,2-Dichlorobenzene U 0.0133 0.447 1 02/08/2024 20:23 WG2220590
1,3-Dichlorobenzene U 0.0136 0.447 1 02/08/2024 20:23 WG2220590
1,4-Dichlorobenzene U 0.0133 0.447 1 02/08/2024 20:23 WG2220590
3,3-Dichlorobenzidine U 0.0165 0.447 1 02/08/2024 20:23 WG2220590
2,4-Dinitrotoluene U 0.0128 0.447 1 02/08/2024 20:23 WG2220590
2,6-Dinitrotoluene U 0.0146 0.447 1 02/08/2024 20:23 WG2220590
Fluoranthene U 0.00807 0.0447 1 02/08/2024 20:23 WG2220590
Fluorene U 0.00728 0.0447 1 02/08/2024 20:23 WG2220590
Hexachlorobenzene U 0.0158 0.447 1 02/08/2024 20:23 WG2220590
Hexachloro-1,3-butadiene U 0.0150 0.447 1 02/08/2024 20:23 WG2220590
Hexachlorocyclopentadiene U 0.0235 0.447 1 02/08/2024 20:23 WG2220590
Hexachloroethane U 0.0176 0.447 1 02/08/2024 20:23 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0126 0.0447 1 02/08/2024 20:23 WG2220590
Isophorone U 0.0137 0.447 1 02/08/2024 20:23 WG2220590
Naphthalene U 0.0112 0.0447 1 02/08/2024 20:23 WG2220590
Nitrobenzene U 0.0156 0.447 1 02/08/2024 20:23 WG2220590
n-Nitrosodimethylamine U 0.0663 0.447 1 02/08/2024 20:23 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 12
L1701794
SB-4 2-3
Collected date/time: 01/31/24 10:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0338 0.447 1 02/08/2024 20:23 WG2220590
n-Nitrosodi-n-propylamine U 0.0149 0.447 1 02/08/2024 20:23 WG2220590
Phenanthrene U 0.00888 0.0447 1 02/08/2024 20:23 WG2220590
Benzylbutyl phthalate U 0.0140 0.447 1 02/08/2024 20:23 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0567 0.447 1 02/08/2024 20:23 WG2220590
Di-n-butyl phthalate U 0.0153 0.447 1 02/08/2024 20:23 WG2220590
Diethyl phthalate U 0.0148 0.447 1 02/08/2024 20:23 WG2220590
Dimethyl phthalate U 0.0948 0.447 1 02/08/2024 20:23 WG2220590
Di-n-octyl phthalate U 0.0302 0.447 1 02/08/2024 20:23 WG2220590
Pyrene U 0.00870 0.0447 1 02/08/2024 20:23 WG2220590
1,2,4-Trichlorobenzene U 0.0140 0.447 1 02/08/2024 20:23 WG2220590
4-Chloro-3-methylphenol U 0.0145 0.447 1 02/08/2024 20:23 WG2220590
2-Chlorophenol U 0.0148 0.447 1 02/08/2024 20:23 WG2220590
2,4-Dichlorophenol U 0.0130 0.447 1 02/08/2024 20:23 WG2220590
2,4-Dimethylphenol U 0.0117 0.447 1 02/08/2024 20:23 WG2220590
4,6-Dinitro-2-methylphenol U 0.101 0.447 1 02/08/2024 20:23 WG2220590
2,4-Dinitrophenol U 0.105 0.447 1 02/08/2024 20:23 WG2220590
2-Nitrophenol U 0.0160 0.447 1 02/08/2024 20:23 WG2220590
4-Nitrophenol U 0.0140 0.447 1 02/08/2024 20:23 WG2220590
Pentachlorophenol U 0.0120 0.447 1 02/08/2024 20:23 WG2220590
Phenol U 0.0180 0.447 1 02/08/2024 20:23 WG2220590
2,4,6-Trichlorophenol U 0.0144 0.447 1 02/08/2024 20:23 WG2220590
(S) 2-Fluorophenol 71.4 12.0-120 02/08/2024 20:23 WG2220590
(S) Phenol-d5 69.7 10.0-120 02/08/2024 20:23 WG2220590
(S) Nitrobenzene-d5 67.3 10.0-122 02/08/2024 20:23 WG2220590
(S) 2-Fluorobiphenyl 70.5 15.0-120 02/08/2024 20:23 WG2220590
(S) 2,4,6-Tribromophenol 73.2 10.0-127 02/08/2024 20:23 WG2220590
(S) p-Terphenyl-d14 77.8 10.0-120 02/08/2024 20:23 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 13
L1701794
SB-3 0-1
Collected date/time: 01/31/24 10:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 74.2 1 02/06/2024 15:26 WG2220127
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0643 0.0880 1 02/06/2024 01:01 WG2220500
Acrylonitrile U 0.00635 0.0220 1 02/06/2024 01:01 WG2220500
Benzene U 0.000822 0.00176 1 02/06/2024 01:01 WG2220500
Bromobenzene U 0.00158 0.0220 1 02/06/2024 01:01 WG2220500
Bromodichloromethane U 0.00128 0.00440 1 02/06/2024 01:01 WG2220500
Bromoform U 0.00206 0.0440 1 02/06/2024 01:01 WG2220500
Bromomethane U 0.00347 0.0220 1 02/06/2024 01:01 WG2220500
n-Butylbenzene U 0.00924 0.0220 1 02/06/2024 01:01 WG2220500
sec-Butylbenzene U 0.00507 0.0220 1 02/06/2024 01:01 WG2220500
tert-Butylbenzene U 0.00343 0.00880 1 02/06/2024 01:01 WG2220500
Carbon tetrachloride U 0.00158 0.00880 1 02/06/2024 01:01 WG2220500
Chlorobenzene U 0.000370 0.00440 1 02/06/2024 01:01 WG2220500
Chlorodibromomethane U 0.00108 0.00440 1 02/06/2024 01:01 WG2220500
Chloroethane U 0.00299 0.00880 1 02/06/2024 01:01 WG2220500
Chloroform 0.00606 B 0.00181 0.00440 1 02/06/2024 01:01 WG2220500
Chloromethane U 0.00766 0.0220 1 02/06/2024 01:01 WG2220500
2-Chlorotoluene U 0.00152 0.00440 1 02/06/2024 01:01 WG2220500
4-Chlorotoluene U 0.000792 0.00880 1 02/06/2024 01:01 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00687 0.0440 1 02/06/2024 01:01 WG2220500
1,2-Dibromoethane U 0.00114 0.00440 1 02/06/2024 01:01 WG2220500
Dibromomethane U 0.00132 0.00880 1 02/06/2024 01:01 WG2220500
1,2-Dichlorobenzene U 0.000748 0.00880 1 02/06/2024 01:01 WG2220500
1,3-Dichlorobenzene U 0.00106 0.00880 1 02/06/2024 01:01 WG2220500
1,4-Dichlorobenzene U 0.00123 0.00880 1 02/06/2024 01:01 WG2220500
Dichlorodifluoromethane U 0.00283 0.00880 1 02/06/2024 01:01 WG2220500
1,1-Dichloroethane U 0.000864 0.00440 1 02/06/2024 01:01 WG2220500
1,2-Dichloroethane U 0.00114 0.00440 1 02/06/2024 01:01 WG2220500
1,1-Dichloroethene U 0.00107 0.00440 1 02/06/2024 01:01 WG2220500
cis-1,2-Dichloroethene 0.0391 0.00129 0.00440 1 02/06/2024 01:01 WG2220500
trans-1,2-Dichloroethene U 0.00183 0.00880 1 02/06/2024 01:01 WG2220500
1,2-Dichloropropane U 0.00250 0.00880 1 02/06/2024 01:01 WG2220500
1,1-Dichloropropene U 0.00142 0.00440 1 02/06/2024 01:01 WG2220500
1,3-Dichloropropane U 0.000882 0.00880 1 02/06/2024 01:01 WG2220500
cis-1,3-Dichloropropene U 0.00133 0.00440 1 02/06/2024 01:01 WG2220500
trans-1,3-Dichloropropene U 0.00201 0.00880 1 02/06/2024 01:01 WG2220500
2,2-Dichloropropane U 0.00243 0.00440 1 02/06/2024 01:01 WG2220500
Di-isopropyl ether U 0.000722 0.00176 1 02/06/2024 01:01 WG2220500
Ethylbenzene U 0.00130 0.00440 1 02/06/2024 01:01 WG2220500
Hexachloro-1,3-butadiene U 0.0106 0.0440 1 02/06/2024 01:01 WG2220500
Isopropylbenzene U 0.000748 0.00440 1 02/06/2024 01:01 WG2220500
p-Isopropyltoluene U 0.00449 0.00880 1 02/06/2024 01:01 WG2220500
2-Butanone (MEK)U 0.112 0.176 1 02/06/2024 01:01 WG2220500
Methylene Chloride 0.0173 B J 0.0117 0.0440 1 02/06/2024 01:01 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00401 0.0440 1 02/06/2024 01:01 WG2220500
Methyl tert-butyl ether U 0.000616 0.00176 1 02/06/2024 01:01 WG2220500
Naphthalene U C3 0.00859 0.0220 1 02/06/2024 01:01 WG2220500
n-Propylbenzene U 0.00167 0.00880 1 02/06/2024 01:01 WG2220500
Styrene U 0.000403 0.0220 1 02/06/2024 01:01 WG2220500
1,1,1,2-Tetrachloroethane U 0.00167 0.00440 1 02/06/2024 01:01 WG2220500
1,1,2,2-Tetrachloroethane U 0.00122 0.00440 1 02/06/2024 01:01 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 13
L1701794
SB-3 0-1
Collected date/time: 01/31/24 10:55
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00133 0.00440 1 02/06/2024 01:01 WG2220500
Tetrachloroethene 8.66 0.0315 0.0880 20 02/13/2024 12:22 WG2224617
Toluene U 0.00229 0.00880 1 02/06/2024 01:01 WG2220500
1,2,3-Trichlorobenzene U 0.0129 0.0220 1 02/06/2024 01:01 WG2220500
1,2,4-Trichlorobenzene U 0.00775 0.0220 1 02/06/2024 01:01 WG2220500
1,1,1-Trichloroethane U 0.00162 0.00440 1 02/06/2024 01:01 WG2220500
1,1,2-Trichloroethane U 0.00105 0.00440 1 02/06/2024 01:01 WG2220500
Trichloroethene 0.127 C5 J4 0.00103 0.00176 1 02/06/2024 01:01 WG2220500
Trichlorofluoromethane U 0.00146 0.00440 1 02/06/2024 01:01 WG2220500
1,2,3-Trichloropropane U 0.00285 0.0220 1 02/06/2024 01:01 WG2220500
1,2,4-Trimethylbenzene U 0.00278 0.00880 1 02/06/2024 01:01 WG2220500
1,2,3-Trimethylbenzene U 0.00278 0.00880 1 02/06/2024 01:01 WG2220500
1,3,5-Trimethylbenzene U 0.00352 0.00880 1 02/06/2024 01:01 WG2220500
Vinyl chloride U 0.00204 0.00440 1 02/06/2024 01:01 WG2220500
Xylenes, Total U 0.00155 0.0114 1 02/06/2024 01:01 WG2220500
(S) Toluene-d8 104 75.0-131 02/06/2024 01:01 WG2220500
(S) Toluene-d8 102 75.0-131 02/13/2024 12:22 WG2224617
(S) 4-Bromofluorobenzene 96.8 67.0-138 02/06/2024 01:01 WG2220500
(S) 4-Bromofluorobenzene 97.8 67.0-138 02/13/2024 12:22 WG2224617
(S) 1,2-Dichloroethane-d4 119 70.0-130 02/06/2024 01:01 WG2220500
(S) 1,2-Dichloroethane-d4 83.5 70.0-130 02/13/2024 12:22 WG2224617
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00726 0.0449 1 02/08/2024 21:04 WG2220590
Acenaphthylene U 0.00632 0.0449 1 02/08/2024 21:04 WG2220590
Anthracene U 0.00799 0.0449 1 02/08/2024 21:04 WG2220590
Benzidine U 0.0843 2.25 1 02/08/2024 21:04 WG2220590
Benzo(a)anthracene U 0.00791 0.0449 1 02/08/2024 21:04 WG2220590
Benzo(b)fluoranthene U 0.00836 0.0449 1 02/08/2024 21:04 WG2220590
Benzo(k)fluoranthene U 0.00797 0.0449 1 02/08/2024 21:04 WG2220590
Benzo(g,h,i)perylene U 0.00820 0.0449 1 02/08/2024 21:04 WG2220590
Benzo(a)pyrene U 0.00834 0.0449 1 02/08/2024 21:04 WG2220590
Bis(2-chlorethoxy)methane U 0.0135 0.449 1 02/08/2024 21:04 WG2220590
Bis(2-chloroethyl)ether U 0.0148 0.449 1 02/08/2024 21:04 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0194 0.449 1 02/08/2024 21:04 WG2220590
4-Bromophenyl-phenylether U 0.0158 0.449 1 02/08/2024 21:04 WG2220590
2-Chloronaphthalene U 0.00788 0.0449 1 02/08/2024 21:04 WG2220590
4-Chlorophenyl-phenylether U 0.0156 0.449 1 02/08/2024 21:04 WG2220590
Chrysene U 0.00892 0.0449 1 02/08/2024 21:04 WG2220590
Dibenz(a,h)anthracene U 0.0124 0.0449 1 02/08/2024 21:04 WG2220590
1,2-Dichlorobenzene U 0.0133 0.449 1 02/08/2024 21:04 WG2220590
1,3-Dichlorobenzene U 0.0136 0.449 1 02/08/2024 21:04 WG2220590
1,4-Dichlorobenzene U 0.0133 0.449 1 02/08/2024 21:04 WG2220590
3,3-Dichlorobenzidine U 0.0166 0.449 1 02/08/2024 21:04 WG2220590
2,4-Dinitrotoluene U 0.0129 0.449 1 02/08/2024 21:04 WG2220590
2,6-Dinitrotoluene U 0.0147 0.449 1 02/08/2024 21:04 WG2220590
Fluoranthene U 0.00810 0.0449 1 02/08/2024 21:04 WG2220590
Fluorene U 0.00730 0.0449 1 02/08/2024 21:04 WG2220590
Hexachlorobenzene U 0.0159 0.449 1 02/08/2024 21:04 WG2220590
Hexachloro-1,3-butadiene U 0.0151 0.449 1 02/08/2024 21:04 WG2220590
Hexachlorocyclopentadiene U 0.0236 0.449 1 02/08/2024 21:04 WG2220590
Hexachloroethane U 0.0176 0.449 1 02/08/2024 21:04 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0127 0.0449 1 02/08/2024 21:04 WG2220590
Isophorone U 0.0137 0.449 1 02/08/2024 21:04 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 13
L1701794
SB-3 0-1
Collected date/time: 01/31/24 10:55
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Naphthalene U 0.0113 0.0449 1 02/08/2024 21:04 WG2220590
Nitrobenzene U 0.0156 0.449 1 02/08/2024 21:04 WG2220590
n-Nitrosodimethylamine U 0.0665 0.449 1 02/08/2024 21:04 WG2220590
n-Nitrosodiphenylamine U 0.0339 0.449 1 02/08/2024 21:04 WG2220590
n-Nitrosodi-n-propylamine U 0.0150 0.449 1 02/08/2024 21:04 WG2220590
Phenanthrene U 0.00890 0.0449 1 02/08/2024 21:04 WG2220590
Benzylbutyl phthalate U 0.0140 0.449 1 02/08/2024 21:04 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0568 0.449 1 02/08/2024 21:04 WG2220590
Di-n-butyl phthalate U 0.0154 0.449 1 02/08/2024 21:04 WG2220590
Diethyl phthalate U 0.0148 0.449 1 02/08/2024 21:04 WG2220590
Dimethyl phthalate U 0.0951 0.449 1 02/08/2024 21:04 WG2220590
Di-n-octyl phthalate U 0.0303 0.449 1 02/08/2024 21:04 WG2220590
Pyrene U 0.00873 0.0449 1 02/08/2024 21:04 WG2220590
1,2,4-Trichlorobenzene U 0.0140 0.449 1 02/08/2024 21:04 WG2220590
4-Chloro-3-methylphenol U 0.0145 0.449 1 02/08/2024 21:04 WG2220590
2-Chlorophenol U 0.0148 0.449 1 02/08/2024 21:04 WG2220590
2,4-Dichlorophenol U 0.0131 0.449 1 02/08/2024 21:04 WG2220590
2,4-Dimethylphenol U 0.0117 0.449 1 02/08/2024 21:04 WG2220590
4,6-Dinitro-2-methylphenol U 0.102 0.449 1 02/08/2024 21:04 WG2220590
2,4-Dinitrophenol U 0.105 0.449 1 02/08/2024 21:04 WG2220590
2-Nitrophenol U 0.0160 0.449 1 02/08/2024 21:04 WG2220590
4-Nitrophenol U 0.0140 0.449 1 02/08/2024 21:04 WG2220590
Pentachlorophenol U 0.0121 0.449 1 02/08/2024 21:04 WG2220590
Phenol U 0.0181 0.449 1 02/08/2024 21:04 WG2220590
2,4,6-Trichlorophenol U 0.0144 0.449 1 02/08/2024 21:04 WG2220590
(S) 2-Fluorophenol 69.7 12.0-120 02/08/2024 21:04 WG2220590
(S) Phenol-d5 70.6 10.0-120 02/08/2024 21:04 WG2220590
(S) Nitrobenzene-d5 67.8 10.0-122 02/08/2024 21:04 WG2220590
(S) 2-Fluorobiphenyl 67.8 15.0-120 02/08/2024 21:04 WG2220590
(S) 2,4,6-Tribromophenol 69.0 10.0-127 02/08/2024 21:04 WG2220590
(S) p-Terphenyl-d14 77.4 10.0-120 02/08/2024 21:04 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 14
L1701794
SB-3 1-2
Collected date/time: 01/31/24 11:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.9 1 02/06/2024 15:26 WG2220127
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0582 0.0797 1 02/06/2024 01:20 WG2220500
Acrylonitrile U 0.00576 0.0199 1 02/06/2024 01:20 WG2220500
Benzene U 0.000745 0.00159 1 02/06/2024 01:20 WG2220500
Bromobenzene U 0.00143 0.0199 1 02/06/2024 01:20 WG2220500
Bromodichloromethane U 0.00116 0.00399 1 02/06/2024 01:20 WG2220500
Bromoform U 0.00187 0.0399 1 02/06/2024 01:20 WG2220500
Bromomethane U 0.00314 0.0199 1 02/06/2024 01:20 WG2220500
n-Butylbenzene U 0.00837 0.0199 1 02/06/2024 01:20 WG2220500
sec-Butylbenzene U 0.00459 0.0199 1 02/06/2024 01:20 WG2220500
tert-Butylbenzene U 0.00311 0.00797 1 02/06/2024 01:20 WG2220500
Carbon tetrachloride U 0.00143 0.00797 1 02/06/2024 01:20 WG2220500
Chlorobenzene U 0.000335 0.00399 1 02/06/2024 01:20 WG2220500
Chlorodibromomethane U 0.000976 0.00399 1 02/06/2024 01:20 WG2220500
Chloroethane U 0.00271 0.00797 1 02/06/2024 01:20 WG2220500
Chloroform 0.00327 B J 0.00164 0.00399 1 02/06/2024 01:20 WG2220500
Chloromethane U 0.00694 0.0199 1 02/06/2024 01:20 WG2220500
2-Chlorotoluene U 0.00138 0.00399 1 02/06/2024 01:20 WG2220500
4-Chlorotoluene U 0.000717 0.00797 1 02/06/2024 01:20 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00622 0.0399 1 02/06/2024 01:20 WG2220500
1,2-Dibromoethane U 0.00103 0.00399 1 02/06/2024 01:20 WG2220500
Dibromomethane U 0.00120 0.00797 1 02/06/2024 01:20 WG2220500
1,2-Dichlorobenzene U 0.000678 0.00797 1 02/06/2024 01:20 WG2220500
1,3-Dichlorobenzene U 0.000957 0.00797 1 02/06/2024 01:20 WG2220500
1,4-Dichlorobenzene U 0.00112 0.00797 1 02/06/2024 01:20 WG2220500
Dichlorodifluoromethane U 0.00257 0.00797 1 02/06/2024 01:20 WG2220500
1,1-Dichloroethane U 0.000783 0.00399 1 02/06/2024 01:20 WG2220500
1,2-Dichloroethane U 0.00103 0.00399 1 02/06/2024 01:20 WG2220500
1,1-Dichloroethene U 0.000966 0.00399 1 02/06/2024 01:20 WG2220500
cis-1,2-Dichloroethene 0.00407 0.00117 0.00399 1 02/06/2024 01:20 WG2220500
trans-1,2-Dichloroethene U 0.00166 0.00797 1 02/06/2024 01:20 WG2220500
1,2-Dichloropropane U 0.00226 0.00797 1 02/06/2024 01:20 WG2220500
1,1-Dichloropropene U 0.00129 0.00399 1 02/06/2024 01:20 WG2220500
1,3-Dichloropropane U 0.000799 0.00797 1 02/06/2024 01:20 WG2220500
cis-1,3-Dichloropropene U 0.00121 0.00399 1 02/06/2024 01:20 WG2220500
trans-1,3-Dichloropropene U 0.00182 0.00797 1 02/06/2024 01:20 WG2220500
2,2-Dichloropropane U 0.00220 0.00399 1 02/06/2024 01:20 WG2220500
Di-isopropyl ether U 0.000654 0.00159 1 02/06/2024 01:20 WG2220500
Ethylbenzene U 0.00118 0.00399 1 02/06/2024 01:20 WG2220500
Hexachloro-1,3-butadiene U 0.00957 0.0399 1 02/06/2024 01:20 WG2220500
Isopropylbenzene U 0.000678 0.00399 1 02/06/2024 01:20 WG2220500
p-Isopropyltoluene U 0.00407 0.00797 1 02/06/2024 01:20 WG2220500
2-Butanone (MEK)U 0.101 0.159 1 02/06/2024 01:20 WG2220500
Methylene Chloride 0.0172 B J 0.0106 0.0399 1 02/06/2024 01:20 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00364 0.0399 1 02/06/2024 01:20 WG2220500
Methyl tert-butyl ether U 0.000558 0.00159 1 02/06/2024 01:20 WG2220500
Naphthalene U C3 0.00778 0.0199 1 02/06/2024 01:20 WG2220500
n-Propylbenzene U 0.00151 0.00797 1 02/06/2024 01:20 WG2220500
Styrene U 0.000365 0.0199 1 02/06/2024 01:20 WG2220500
1,1,1,2-Tetrachloroethane U 0.00151 0.00399 1 02/06/2024 01:20 WG2220500
1,1,2,2-Tetrachloroethane U 0.00111 0.00399 1 02/06/2024 01:20 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 14
L1701794
SB-3 1-2
Collected date/time: 01/31/24 11:00
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00120 0.00399 1 02/06/2024 01:20 WG2220500
Tetrachloroethene 0.394 0.00143 0.00399 1 02/06/2024 01:20 WG2220500
Toluene U 0.00207 0.00797 1 02/06/2024 01:20 WG2220500
1,2,3-Trichlorobenzene U 0.0117 0.0199 1 02/06/2024 01:20 WG2220500
1,2,4-Trichlorobenzene U 0.00702 0.0199 1 02/06/2024 01:20 WG2220500
1,1,1-Trichloroethane U 0.00147 0.00399 1 02/06/2024 01:20 WG2220500
1,1,2-Trichloroethane U 0.000952 0.00399 1 02/06/2024 01:20 WG2220500
Trichloroethene 0.00432 C5 J4 0.000931 0.00159 1 02/06/2024 01:20 WG2220500
Trichlorofluoromethane U 0.00132 0.00399 1 02/06/2024 01:20 WG2220500
1,2,3-Trichloropropane U 0.00258 0.0199 1 02/06/2024 01:20 WG2220500
1,2,4-Trimethylbenzene U 0.00252 0.00797 1 02/06/2024 01:20 WG2220500
1,2,3-Trimethylbenzene U 0.00252 0.00797 1 02/06/2024 01:20 WG2220500
1,3,5-Trimethylbenzene U 0.00319 0.00797 1 02/06/2024 01:20 WG2220500
Vinyl chloride U 0.00185 0.00399 1 02/06/2024 01:20 WG2220500
Xylenes, Total U 0.00140 0.0104 1 02/06/2024 01:20 WG2220500
(S) Toluene-d8 105 75.0-131 02/06/2024 01:20 WG2220500
(S) 4-Bromofluorobenzene 97.9 67.0-138 02/06/2024 01:20 WG2220500
(S) 1,2-Dichloroethane-d4 115 70.0-130 02/06/2024 01:20 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00692 0.0428 1 02/08/2024 20:44 WG2220590
Acenaphthylene U 0.00602 0.0428 1 02/08/2024 20:44 WG2220590
Anthracene U 0.00761 0.0428 1 02/08/2024 20:44 WG2220590
Benzidine U 0.0804 2.14 1 02/08/2024 20:44 WG2220590
Benzo(a)anthracene U 0.00754 0.0428 1 02/08/2024 20:44 WG2220590
Benzo(b)fluoranthene U 0.00797 0.0428 1 02/08/2024 20:44 WG2220590
Benzo(k)fluoranthene U 0.00760 0.0428 1 02/08/2024 20:44 WG2220590
Benzo(g,h,i)perylene U 0.00782 0.0428 1 02/08/2024 20:44 WG2220590
Benzo(a)pyrene U 0.00795 0.0428 1 02/08/2024 20:44 WG2220590
Bis(2-chlorethoxy)methane U 0.0128 0.428 1 02/08/2024 20:44 WG2220590
Bis(2-chloroethyl)ether U 0.0141 0.428 1 02/08/2024 20:44 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0185 0.428 1 02/08/2024 20:44 WG2220590
4-Bromophenyl-phenylether U 0.0150 0.428 1 02/08/2024 20:44 WG2220590
2-Chloronaphthalene U 0.00751 0.0428 1 02/08/2024 20:44 WG2220590
4-Chlorophenyl-phenylether U 0.0149 0.428 1 02/08/2024 20:44 WG2220590
Chrysene U 0.00850 0.0428 1 02/08/2024 20:44 WG2220590
Dibenz(a,h)anthracene U 0.0118 0.0428 1 02/08/2024 20:44 WG2220590
1,2-Dichlorobenzene U 0.0127 0.428 1 02/08/2024 20:44 WG2220590
1,3-Dichlorobenzene U 0.0130 0.428 1 02/08/2024 20:44 WG2220590
1,4-Dichlorobenzene U 0.0127 0.428 1 02/08/2024 20:44 WG2220590
3,3-Dichlorobenzidine U 0.0158 0.428 1 02/08/2024 20:44 WG2220590
2,4-Dinitrotoluene U 0.0123 0.428 1 02/08/2024 20:44 WG2220590
2,6-Dinitrotoluene U 0.0140 0.428 1 02/08/2024 20:44 WG2220590
Fluoranthene U 0.00772 0.0428 1 02/08/2024 20:44 WG2220590
Fluorene U 0.00696 0.0428 1 02/08/2024 20:44 WG2220590
Hexachlorobenzene U 0.0151 0.428 1 02/08/2024 20:44 WG2220590
Hexachloro-1,3-butadiene U 0.0144 0.428 1 02/08/2024 20:44 WG2220590
Hexachlorocyclopentadiene U 0.0225 0.428 1 02/08/2024 20:44 WG2220590
Hexachloroethane U 0.0168 0.428 1 02/08/2024 20:44 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0121 0.0428 1 02/08/2024 20:44 WG2220590
Isophorone U 0.0131 0.428 1 02/08/2024 20:44 WG2220590
Naphthalene U 0.0107 0.0428 1 02/08/2024 20:44 WG2220590
Nitrobenzene U 0.0149 0.428 1 02/08/2024 20:44 WG2220590
n-Nitrosodimethylamine U 0.0634 0.428 1 02/08/2024 20:44 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 14
L1701794
SB-3 1-2
Collected date/time: 01/31/24 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0324 0.428 1 02/08/2024 20:44 WG2220590
n-Nitrosodi-n-propylamine U 0.0143 0.428 1 02/08/2024 20:44 WG2220590
Phenanthrene U 0.00849 0.0428 1 02/08/2024 20:44 WG2220590
Benzylbutyl phthalate U 0.0134 0.428 1 02/08/2024 20:44 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0542 0.428 1 02/08/2024 20:44 WG2220590
Di-n-butyl phthalate U 0.0146 0.428 1 02/08/2024 20:44 WG2220590
Diethyl phthalate U 0.0141 0.428 1 02/08/2024 20:44 WG2220590
Dimethyl phthalate U 0.0906 0.428 1 02/08/2024 20:44 WG2220590
Di-n-octyl phthalate U 0.0289 0.428 1 02/08/2024 20:44 WG2220590
Pyrene U 0.00832 0.0428 1 02/08/2024 20:44 WG2220590
1,2,4-Trichlorobenzene U 0.0134 0.428 1 02/08/2024 20:44 WG2220590
4-Chloro-3-methylphenol U 0.0139 0.428 1 02/08/2024 20:44 WG2220590
2-Chlorophenol U 0.0141 0.428 1 02/08/2024 20:44 WG2220590
2,4-Dichlorophenol U 0.0125 0.428 1 02/08/2024 20:44 WG2220590
2,4-Dimethylphenol U 0.0112 0.428 1 02/08/2024 20:44 WG2220590
4,6-Dinitro-2-methylphenol U 0.0969 0.428 1 02/08/2024 20:44 WG2220590
2,4-Dinitrophenol U 0.100 0.428 1 02/08/2024 20:44 WG2220590
2-Nitrophenol U 0.0153 0.428 1 02/08/2024 20:44 WG2220590
4-Nitrophenol U 0.0134 0.428 1 02/08/2024 20:44 WG2220590
Pentachlorophenol U 0.0115 0.428 1 02/08/2024 20:44 WG2220590
Phenol U 0.0172 0.428 1 02/08/2024 20:44 WG2220590
2,4,6-Trichlorophenol U 0.0137 0.428 1 02/08/2024 20:44 WG2220590
(S) 2-Fluorophenol 74.2 12.0-120 02/08/2024 20:44 WG2220590
(S) Phenol-d5 72.9 10.0-120 02/08/2024 20:44 WG2220590
(S) Nitrobenzene-d5 67.2 10.0-122 02/08/2024 20:44 WG2220590
(S) 2-Fluorobiphenyl 69.0 15.0-120 02/08/2024 20:44 WG2220590
(S) 2,4,6-Tribromophenol 68.8 10.0-127 02/08/2024 20:44 WG2220590
(S) p-Terphenyl-d14 74.2 10.0-120 02/08/2024 20:44 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 15
L1701794
SB-5 0-1
Collected date/time: 01/29/24 16:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 93.0 1 02/06/2024 15:26 WG2220127
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0424 0.0581 1 02/06/2024 01:39 WG2220500
Acrylonitrile U 0.00419 0.0145 1 02/06/2024 01:39 WG2220500
Benzene U 0.000542 0.00116 1 02/06/2024 01:39 WG2220500
Bromobenzene U 0.00104 0.0145 1 02/06/2024 01:39 WG2220500
Bromodichloromethane U 0.000842 0.00290 1 02/06/2024 01:39 WG2220500
Bromoform U 0.00136 0.0290 1 02/06/2024 01:39 WG2220500
Bromomethane U 0.00229 0.0145 1 02/06/2024 01:39 WG2220500
n-Butylbenzene U 0.00610 0.0145 1 02/06/2024 01:39 WG2220500
sec-Butylbenzene U 0.00334 0.0145 1 02/06/2024 01:39 WG2220500
tert-Butylbenzene U 0.00226 0.00581 1 02/06/2024 01:39 WG2220500
Carbon tetrachloride U 0.00104 0.00581 1 02/06/2024 01:39 WG2220500
Chlorobenzene U 0.000244 0.00290 1 02/06/2024 01:39 WG2220500
Chlorodibromomethane U 0.000711 0.00290 1 02/06/2024 01:39 WG2220500
Chloroethane U 0.00197 0.00581 1 02/06/2024 01:39 WG2220500
Chloroform 0.00247 B J 0.00120 0.00290 1 02/06/2024 01:39 WG2220500
Chloromethane U 0.00505 0.0145 1 02/06/2024 01:39 WG2220500
2-Chlorotoluene U 0.00100 0.00290 1 02/06/2024 01:39 WG2220500
4-Chlorotoluene U 0.000522 0.00581 1 02/06/2024 01:39 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00453 0.0290 1 02/06/2024 01:39 WG2220500
1,2-Dibromoethane U 0.000752 0.00290 1 02/06/2024 01:39 WG2220500
Dibromomethane U 0.000871 0.00581 1 02/06/2024 01:39 WG2220500
1,2-Dichlorobenzene U 0.000493 0.00581 1 02/06/2024 01:39 WG2220500
1,3-Dichlorobenzene U 0.000697 0.00581 1 02/06/2024 01:39 WG2220500
1,4-Dichlorobenzene U 0.000813 0.00581 1 02/06/2024 01:39 WG2220500
Dichlorodifluoromethane U 0.00187 0.00581 1 02/06/2024 01:39 WG2220500
1,1-Dichloroethane U 0.000570 0.00290 1 02/06/2024 01:39 WG2220500
1,2-Dichloroethane U 0.000754 0.00290 1 02/06/2024 01:39 WG2220500
1,1-Dichloroethene U 0.000704 0.00290 1 02/06/2024 01:39 WG2220500
cis-1,2-Dichloroethene U 0.000852 0.00290 1 02/06/2024 01:39 WG2220500
trans-1,2-Dichloroethene U 0.00121 0.00581 1 02/06/2024 01:39 WG2220500
1,2-Dichloropropane U 0.00165 0.00581 1 02/06/2024 01:39 WG2220500
1,1-Dichloropropene U 0.000939 0.00290 1 02/06/2024 01:39 WG2220500
1,3-Dichloropropane U 0.000582 0.00581 1 02/06/2024 01:39 WG2220500
cis-1,3-Dichloropropene U 0.000879 0.00290 1 02/06/2024 01:39 WG2220500
trans-1,3-Dichloropropene U 0.00132 0.00581 1 02/06/2024 01:39 WG2220500
2,2-Dichloropropane U 0.00160 0.00290 1 02/06/2024 01:39 WG2220500
Di-isopropyl ether U 0.000476 0.00116 1 02/06/2024 01:39 WG2220500
Ethylbenzene U 0.000856 0.00290 1 02/06/2024 01:39 WG2220500
Hexachloro-1,3-butadiene U 0.00697 0.0290 1 02/06/2024 01:39 WG2220500
Isopropylbenzene U 0.000493 0.00290 1 02/06/2024 01:39 WG2220500
p-Isopropyltoluene U 0.00296 0.00581 1 02/06/2024 01:39 WG2220500
2-Butanone (MEK)U 0.0737 0.116 1 02/06/2024 01:39 WG2220500
Methylene Chloride 0.0107 B J 0.00771 0.0290 1 02/06/2024 01:39 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00265 0.0290 1 02/06/2024 01:39 WG2220500
Methyl tert-butyl ether U 0.000406 0.00116 1 02/06/2024 01:39 WG2220500
Naphthalene 0.00687 C3 J 0.00567 0.0145 1 02/06/2024 01:39 WG2220500
n-Propylbenzene U 0.00110 0.00581 1 02/06/2024 01:39 WG2220500
Styrene U 0.000266 0.0145 1 02/06/2024 01:39 WG2220500
1,1,1,2-Tetrachloroethane U 0.00110 0.00290 1 02/06/2024 01:39 WG2220500
1,1,2,2-Tetrachloroethane U 0.000807 0.00290 1 02/06/2024 01:39 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 15
L1701794
SB-5 0-1
Collected date/time: 01/29/24 16:30
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.000875 0.00290 1 02/06/2024 01:39 WG2220500
Tetrachloroethene 0.380 0.00104 0.00290 1 02/06/2024 01:39 WG2220500
Toluene 0.00561 J 0.00151 0.00581 1 02/06/2024 01:39 WG2220500
1,2,3-Trichlorobenzene U 0.00851 0.0145 1 02/06/2024 01:39 WG2220500
1,2,4-Trichlorobenzene U 0.00511 0.0145 1 02/06/2024 01:39 WG2220500
1,1,1-Trichloroethane U 0.00107 0.00290 1 02/06/2024 01:39 WG2220500
1,1,2-Trichloroethane U 0.000693 0.00290 1 02/06/2024 01:39 WG2220500
Trichloroethene U J4 0.000678 0.00116 1 02/06/2024 01:39 WG2220500
Trichlorofluoromethane U 0.000960 0.00290 1 02/06/2024 01:39 WG2220500
1,2,3-Trichloropropane U 0.00188 0.0145 1 02/06/2024 01:39 WG2220500
1,2,4-Trimethylbenzene 0.00434 J 0.00183 0.00581 1 02/06/2024 01:39 WG2220500
1,2,3-Trimethylbenzene 0.00290 J 0.00183 0.00581 1 02/06/2024 01:39 WG2220500
1,3,5-Trimethylbenzene U 0.00232 0.00581 1 02/06/2024 01:39 WG2220500
Vinyl chloride U 0.00135 0.00290 1 02/06/2024 01:39 WG2220500
Xylenes, Total 0.0110 0.00102 0.00755 1 02/06/2024 01:39 WG2220500
(S) Toluene-d8 104 75.0-131 02/06/2024 01:39 WG2220500
(S) 4-Bromofluorobenzene 97.9 67.0-138 02/06/2024 01:39 WG2220500
(S) 1,2-Dichloroethane-d4 114 70.0-130 02/06/2024 01:39 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00579 0.0358 1 02/09/2024 19:56 WG2220590
Acenaphthylene U 0.00504 0.0358 1 02/09/2024 19:56 WG2220590
Anthracene 0.00731 J 0.00637 0.0358 1 02/09/2024 19:56 WG2220590
Benzidine U 0.0673 1.79 1 02/09/2024 19:56 WG2220590
Benzo(a)anthracene 0.0284 J 0.00631 0.0358 1 02/09/2024 19:56 WG2220590
Benzo(b)fluoranthene 0.0358 J 0.00667 0.0358 1 02/09/2024 19:56 WG2220590
Benzo(k)fluoranthene 0.0110 J 0.00636 0.0358 1 02/09/2024 19:56 WG2220590
Benzo(g,h,i)perylene 0.0278 J 0.00655 0.0358 1 02/09/2024 19:56 WG2220590
Benzo(a)pyrene 0.0306 J 0.00665 0.0358 1 02/09/2024 19:56 WG2220590
Bis(2-chlorethoxy)methane U 0.0107 0.358 1 02/09/2024 19:56 WG2220590
Bis(2-chloroethyl)ether U 0.0118 0.358 1 02/09/2024 19:56 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0155 0.358 1 02/09/2024 19:56 WG2220590
4-Bromophenyl-phenylether U 0.0126 0.358 1 02/09/2024 19:56 WG2220590
2-Chloronaphthalene U 0.00629 0.0358 1 02/09/2024 19:56 WG2220590
4-Chlorophenyl-phenylether U 0.0125 0.358 1 02/09/2024 19:56 WG2220590
Chrysene 0.0271 J 0.00711 0.0358 1 02/09/2024 19:56 WG2220590
Dibenz(a,h)anthracene U 0.00992 0.0358 1 02/09/2024 19:56 WG2220590
1,2-Dichlorobenzene U 0.0106 0.358 1 02/09/2024 19:56 WG2220590
1,3-Dichlorobenzene U 0.0109 0.358 1 02/09/2024 19:56 WG2220590
1,4-Dichlorobenzene U 0.0107 0.358 1 02/09/2024 19:56 WG2220590
3,3-Dichlorobenzidine U 0.0132 0.358 1 02/09/2024 19:56 WG2220590
2,4-Dinitrotoluene U 0.0103 0.358 1 02/09/2024 19:56 WG2220590
2,6-Dinitrotoluene U 0.0117 0.358 1 02/09/2024 19:56 WG2220590
Fluoranthene 0.0451 0.00646 0.0358 1 02/09/2024 19:56 WG2220590
Fluorene U 0.00583 0.0358 1 02/09/2024 19:56 WG2220590
Hexachlorobenzene U 0.0127 0.358 1 02/09/2024 19:56 WG2220590
Hexachloro-1,3-butadiene U 0.0120 0.358 1 02/09/2024 19:56 WG2220590
Hexachlorocyclopentadiene U 0.0188 0.358 1 02/09/2024 19:56 WG2220590
Hexachloroethane U 0.0141 0.358 1 02/09/2024 19:56 WG2220590
Indeno(1,2,3-cd)pyrene 0.0195 J 0.0101 0.0358 1 02/09/2024 19:56 WG2220590
Isophorone U 0.0110 0.358 1 02/09/2024 19:56 WG2220590
Naphthalene 0.0139 J 0.00898 0.0358 1 02/09/2024 19:56 WG2220590
Nitrobenzene U 0.0125 0.358 1 02/09/2024 19:56 WG2220590
n-Nitrosodimethylamine U 0.0531 0.358 1 02/09/2024 19:56 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 15
L1701794
SB-5 0-1
Collected date/time: 01/29/24 16:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0271 0.358 1 02/09/2024 19:56 WG2220590
n-Nitrosodi-n-propylamine U 0.0119 0.358 1 02/09/2024 19:56 WG2220590
Phenanthrene 0.0388 0.00710 0.0358 1 02/09/2024 19:56 WG2220590
Benzylbutyl phthalate 0.0442 J 0.0112 0.358 1 02/09/2024 19:56 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0454 0.358 1 02/09/2024 19:56 WG2220590
Di-n-butyl phthalate 0.0150 J 0.0123 0.358 1 02/09/2024 19:56 WG2220590
Diethyl phthalate U 0.0118 0.358 1 02/09/2024 19:56 WG2220590
Dimethyl phthalate U 0.0759 0.358 1 02/09/2024 19:56 WG2220590
Di-n-octyl phthalate U 0.0242 0.358 1 02/09/2024 19:56 WG2220590
Pyrene 0.0533 0.00696 0.0358 1 02/09/2024 19:56 WG2220590
1,2,4-Trichlorobenzene U 0.0112 0.358 1 02/09/2024 19:56 WG2220590
4-Chloro-3-methylphenol U 0.0116 0.358 1 02/09/2024 19:56 WG2220590
2-Chlorophenol U 0.0118 0.358 1 02/09/2024 19:56 WG2220590
2,4-Dichlorophenol U 0.0104 0.358 1 02/09/2024 19:56 WG2220590
2,4-Dimethylphenol U 0.00935 0.358 1 02/09/2024 19:56 WG2220590
4,6-Dinitro-2-methylphenol U 0.0811 0.358 1 02/09/2024 19:56 WG2220590
2,4-Dinitrophenol U 0.0837 0.358 1 02/09/2024 19:56 WG2220590
2-Nitrophenol U 0.0128 0.358 1 02/09/2024 19:56 WG2220590
4-Nitrophenol U 0.0112 0.358 1 02/09/2024 19:56 WG2220590
Pentachlorophenol U 0.00963 0.358 1 02/09/2024 19:56 WG2220590
Phenol U 0.0144 0.358 1 02/09/2024 19:56 WG2220590
2,4,6-Trichlorophenol U 0.0115 0.358 1 02/09/2024 19:56 WG2220590
(S) 2-Fluorophenol 70.6 12.0-120 02/09/2024 19:56 WG2220590
(S) Phenol-d5 70.6 10.0-120 02/09/2024 19:56 WG2220590
(S) Nitrobenzene-d5 68.4 10.0-122 02/09/2024 19:56 WG2220590
(S) 2-Fluorobiphenyl 67.2 15.0-120 02/09/2024 19:56 WG2220590
(S) 2,4,6-Tribromophenol 66.9 10.0-127 02/09/2024 19:56 WG2220590
(S) p-Terphenyl-d14 76.4 10.0-120 02/09/2024 19:56 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 16
L1701794
SB-5 4-5
Collected date/time: 01/29/24 16:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.8 1 02/06/2024 15:26 WG2220127
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0594 0.0813 1 02/06/2024 01:58 WG2220500
Acrylonitrile U 0.00587 0.0203 1 02/06/2024 01:58 WG2220500
Benzene U 0.000760 0.00163 1 02/06/2024 01:58 WG2220500
Bromobenzene U 0.00146 0.0203 1 02/06/2024 01:58 WG2220500
Bromodichloromethane U 0.00118 0.00407 1 02/06/2024 01:58 WG2220500
Bromoform U 0.00190 0.0407 1 02/06/2024 01:58 WG2220500
Bromomethane U 0.00320 0.0203 1 02/06/2024 01:58 WG2220500
n-Butylbenzene U 0.00854 0.0203 1 02/06/2024 01:58 WG2220500
sec-Butylbenzene U 0.00469 0.0203 1 02/06/2024 01:58 WG2220500
tert-Butylbenzene U 0.00317 0.00813 1 02/06/2024 01:58 WG2220500
Carbon tetrachloride U 0.00146 0.00813 1 02/06/2024 01:58 WG2220500
Chlorobenzene U 0.000342 0.00407 1 02/06/2024 01:58 WG2220500
Chlorodibromomethane U 0.000996 0.00407 1 02/06/2024 01:58 WG2220500
Chloroethane U 0.00277 0.00813 1 02/06/2024 01:58 WG2220500
Chloroform 0.00351 B J 0.00168 0.00407 1 02/06/2024 01:58 WG2220500
Chloromethane U 0.00708 0.0203 1 02/06/2024 01:58 WG2220500
2-Chlorotoluene U 0.00141 0.00407 1 02/06/2024 01:58 WG2220500
4-Chlorotoluene U 0.000732 0.00813 1 02/06/2024 01:58 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00634 0.0407 1 02/06/2024 01:58 WG2220500
1,2-Dibromoethane U 0.00105 0.00407 1 02/06/2024 01:58 WG2220500
Dibromomethane U 0.00122 0.00813 1 02/06/2024 01:58 WG2220500
1,2-Dichlorobenzene U 0.000691 0.00813 1 02/06/2024 01:58 WG2220500
1,3-Dichlorobenzene U 0.000976 0.00813 1 02/06/2024 01:58 WG2220500
1,4-Dichlorobenzene U 0.00114 0.00813 1 02/06/2024 01:58 WG2220500
Dichlorodifluoromethane U 0.00262 0.00813 1 02/06/2024 01:58 WG2220500
1,1-Dichloroethane U 0.000799 0.00407 1 02/06/2024 01:58 WG2220500
1,2-Dichloroethane U 0.00106 0.00407 1 02/06/2024 01:58 WG2220500
1,1-Dichloroethene U 0.000986 0.00407 1 02/06/2024 01:58 WG2220500
cis-1,2-Dichloroethene U 0.00119 0.00407 1 02/06/2024 01:58 WG2220500
trans-1,2-Dichloroethene U 0.00169 0.00813 1 02/06/2024 01:58 WG2220500
1,2-Dichloropropane U 0.00231 0.00813 1 02/06/2024 01:58 WG2220500
1,1-Dichloropropene U 0.00132 0.00407 1 02/06/2024 01:58 WG2220500
1,3-Dichloropropane U 0.000815 0.00813 1 02/06/2024 01:58 WG2220500
cis-1,3-Dichloropropene U 0.00123 0.00407 1 02/06/2024 01:58 WG2220500
trans-1,3-Dichloropropene U 0.00185 0.00813 1 02/06/2024 01:58 WG2220500
2,2-Dichloropropane U 0.00224 0.00407 1 02/06/2024 01:58 WG2220500
Di-isopropyl ether U 0.000667 0.00163 1 02/06/2024 01:58 WG2220500
Ethylbenzene U 0.00120 0.00407 1 02/06/2024 01:58 WG2220500
Hexachloro-1,3-butadiene U 0.00976 0.0407 1 02/06/2024 01:58 WG2220500
Isopropylbenzene U 0.000691 0.00407 1 02/06/2024 01:58 WG2220500
p-Isopropyltoluene U 0.00415 0.00813 1 02/06/2024 01:58 WG2220500
2-Butanone (MEK)U 0.103 0.163 1 02/06/2024 01:58 WG2220500
Methylene Chloride 0.0185 B J 0.0108 0.0407 1 02/06/2024 01:58 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00371 0.0407 1 02/06/2024 01:58 WG2220500
Methyl tert-butyl ether U 0.000569 0.00163 1 02/06/2024 01:58 WG2220500
Naphthalene U C3 0.00794 0.0203 1 02/06/2024 01:58 WG2220500
n-Propylbenzene U 0.00155 0.00813 1 02/06/2024 01:58 WG2220500
Styrene U 0.000373 0.0203 1 02/06/2024 01:58 WG2220500
1,1,1,2-Tetrachloroethane U 0.00154 0.00407 1 02/06/2024 01:58 WG2220500
1,1,2,2-Tetrachloroethane U 0.00113 0.00407 1 02/06/2024 01:58 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 16
L1701794
SB-5 4-5
Collected date/time: 01/29/24 16:35
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00123 0.00407 1 02/06/2024 01:58 WG2220500
Tetrachloroethene 0.0207 0.00146 0.00407 1 02/06/2024 01:58 WG2220500
Tetrachloroethene 0.0141 Q 0.00146 0.00407 1 02/13/2024 12:00 WG2224617
Toluene U 0.00211 0.00813 1 02/06/2024 01:58 WG2220500
1,2,3-Trichlorobenzene U 0.0119 0.0203 1 02/06/2024 01:58 WG2220500
1,2,4-Trichlorobenzene U 0.00716 0.0203 1 02/06/2024 01:58 WG2220500
1,1,1-Trichloroethane U 0.00150 0.00407 1 02/06/2024 01:58 WG2220500
1,1,2-Trichloroethane U 0.000971 0.00407 1 02/06/2024 01:58 WG2220500
Trichloroethene U J4 0.000950 0.00163 1 02/06/2024 01:58 WG2220500
Trichlorofluoromethane U 0.00135 0.00407 1 02/06/2024 01:58 WG2220500
1,2,3-Trichloropropane U 0.00264 0.0203 1 02/06/2024 01:58 WG2220500
1,2,4-Trimethylbenzene U 0.00257 0.00813 1 02/06/2024 01:58 WG2220500
1,2,3-Trimethylbenzene U 0.00257 0.00813 1 02/06/2024 01:58 WG2220500
1,3,5-Trimethylbenzene U 0.00325 0.00813 1 02/06/2024 01:58 WG2220500
Vinyl chloride U 0.00189 0.00407 1 02/06/2024 01:58 WG2220500
Xylenes, Total U 0.00143 0.0106 1 02/06/2024 01:58 WG2220500
(S) Toluene-d8 105 75.0-131 02/06/2024 01:58 WG2220500
(S) Toluene-d8 101 75.0-131 02/13/2024 12:00 WG2224617
(S) 4-Bromofluorobenzene 97.1 67.0-138 02/06/2024 01:58 WG2220500
(S) 4-Bromofluorobenzene 91.2 67.0-138 02/13/2024 12:00 WG2224617
(S) 1,2-Dichloroethane-d4 115 70.0-130 02/06/2024 01:58 WG2220500
(S) 1,2-Dichloroethane-d4 77.6 70.0-130 02/13/2024 12:00 WG2224617
Sample Narrative:
L1701794-16 WG2220500: PCE result possible biased high due to carryover from -15.
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00702 0.0434 1 02/08/2024 21:45 WG2220590
Acenaphthylene U 0.00611 0.0434 1 02/08/2024 21:45 WG2220590
Anthracene U 0.00772 0.0434 1 02/08/2024 21:45 WG2220590
Benzidine U 0.0815 2.17 1 02/08/2024 21:45 WG2220590
Benzo(a)anthracene U 0.00764 0.0434 1 02/08/2024 21:45 WG2220590
Benzo(b)fluoranthene U 0.00808 0.0434 1 02/08/2024 21:45 WG2220590
Benzo(k)fluoranthene U 0.00771 0.0434 1 02/08/2024 21:45 WG2220590
Benzo(g,h,i)perylene U 0.00793 0.0434 1 02/08/2024 21:45 WG2220590
Benzo(a)pyrene U 0.00806 0.0434 1 02/08/2024 21:45 WG2220590
Bis(2-chlorethoxy)methane U 0.0130 0.434 1 02/08/2024 21:45 WG2220590
Bis(2-chloroethyl)ether U 0.0143 0.434 1 02/08/2024 21:45 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0187 0.434 1 02/08/2024 21:45 WG2220590
4-Bromophenyl-phenylether U 0.0152 0.434 1 02/08/2024 21:45 WG2220590
2-Chloronaphthalene U 0.00762 0.0434 1 02/08/2024 21:45 WG2220590
4-Chlorophenyl-phenylether U 0.0151 0.434 1 02/08/2024 21:45 WG2220590
Chrysene U 0.00862 0.0434 1 02/08/2024 21:45 WG2220590
Dibenz(a,h)anthracene U 0.0120 0.0434 1 02/08/2024 21:45 WG2220590
1,2-Dichlorobenzene U 0.0128 0.434 1 02/08/2024 21:45 WG2220590
1,3-Dichlorobenzene U 0.0131 0.434 1 02/08/2024 21:45 WG2220590
1,4-Dichlorobenzene U 0.0129 0.434 1 02/08/2024 21:45 WG2220590
3,3-Dichlorobenzidine U 0.0160 0.434 1 02/08/2024 21:45 WG2220590
2,4-Dinitrotoluene U 0.0124 0.434 1 02/08/2024 21:45 WG2220590
2,6-Dinitrotoluene U 0.0142 0.434 1 02/08/2024 21:45 WG2220590
Fluoranthene U 0.00782 0.0434 1 02/08/2024 21:45 WG2220590
Fluorene U 0.00706 0.0434 1 02/08/2024 21:45 WG2220590
Hexachlorobenzene U 0.0154 0.434 1 02/08/2024 21:45 WG2220590
Hexachloro-1,3-butadiene U 0.0146 0.434 1 02/08/2024 21:45 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 16
L1701794
SB-5 4-5
Collected date/time: 01/29/24 16:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexachlorocyclopentadiene U 0.0228 0.434 1 02/08/2024 21:45 WG2220590
Hexachloroethane U 0.0171 0.434 1 02/08/2024 21:45 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0123 0.0434 1 02/08/2024 21:45 WG2220590
Isophorone U 0.0133 0.434 1 02/08/2024 21:45 WG2220590
Naphthalene U 0.0109 0.0434 1 02/08/2024 21:45 WG2220590
Nitrobenzene U 0.0151 0.434 1 02/08/2024 21:45 WG2220590
n-Nitrosodimethylamine U 0.0643 0.434 1 02/08/2024 21:45 WG2220590
n-Nitrosodiphenylamine U 0.0328 0.434 1 02/08/2024 21:45 WG2220590
n-Nitrosodi-n-propylamine U 0.0145 0.434 1 02/08/2024 21:45 WG2220590
Phenanthrene U 0.00861 0.0434 1 02/08/2024 21:45 WG2220590
Benzylbutyl phthalate U 0.0135 0.434 1 02/08/2024 21:45 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0549 0.434 1 02/08/2024 21:45 WG2220590
Di-n-butyl phthalate U 0.0148 0.434 1 02/08/2024 21:45 WG2220590
Diethyl phthalate U 0.0143 0.434 1 02/08/2024 21:45 WG2220590
Dimethyl phthalate U 0.0919 0.434 1 02/08/2024 21:45 WG2220590
Di-n-octyl phthalate U 0.0293 0.434 1 02/08/2024 21:45 WG2220590
Pyrene U 0.00844 0.0434 1 02/08/2024 21:45 WG2220590
1,2,4-Trichlorobenzene U 0.0135 0.434 1 02/08/2024 21:45 WG2220590
4-Chloro-3-methylphenol U 0.0141 0.434 1 02/08/2024 21:45 WG2220590
2-Chlorophenol U 0.0143 0.434 1 02/08/2024 21:45 WG2220590
2,4-Dichlorophenol U 0.0126 0.434 1 02/08/2024 21:45 WG2220590
2,4-Dimethylphenol U 0.0113 0.434 1 02/08/2024 21:45 WG2220590
4,6-Dinitro-2-methylphenol U 0.0983 0.434 1 02/08/2024 21:45 WG2220590
2,4-Dinitrophenol U 0.101 0.434 1 02/08/2024 21:45 WG2220590
2-Nitrophenol U 0.0155 0.434 1 02/08/2024 21:45 WG2220590
4-Nitrophenol U 0.0135 0.434 1 02/08/2024 21:45 WG2220590
Pentachlorophenol U 0.0117 0.434 1 02/08/2024 21:45 WG2220590
Phenol U 0.0174 0.434 1 02/08/2024 21:45 WG2220590
2,4,6-Trichlorophenol U 0.0139 0.434 1 02/08/2024 21:45 WG2220590
(S) 2-Fluorophenol 70.5 12.0-120 02/08/2024 21:45 WG2220590
(S) Phenol-d5 70.9 10.0-120 02/08/2024 21:45 WG2220590
(S) Nitrobenzene-d5 66.1 10.0-122 02/08/2024 21:45 WG2220590
(S) 2-Fluorobiphenyl 65.7 15.0-120 02/08/2024 21:45 WG2220590
(S) 2,4,6-Tribromophenol 67.4 10.0-127 02/08/2024 21:45 WG2220590
(S) p-Terphenyl-d14 74.3 10.0-120 02/08/2024 21:45 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 17
L1701794
SB-10 0-1
Collected date/time: 01/29/24 16:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 84.3 1 02/06/2024 15:26 WG2220127
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0508 0.0695 1 02/06/2024 02:17 WG2220500
Acrylonitrile U 0.00502 0.0174 1 02/06/2024 02:17 WG2220500
Benzene U 0.000649 0.00139 1 02/06/2024 02:17 WG2220500
Bromobenzene U 0.00125 0.0174 1 02/06/2024 02:17 WG2220500
Bromodichloromethane U 0.00101 0.00348 1 02/06/2024 02:17 WG2220500
Bromoform U 0.00163 0.0348 1 02/06/2024 02:17 WG2220500
Bromomethane U 0.00274 0.0174 1 02/06/2024 02:17 WG2220500
n-Butylbenzene U 0.00730 0.0174 1 02/06/2024 02:17 WG2220500
sec-Butylbenzene U 0.00401 0.0174 1 02/06/2024 02:17 WG2220500
tert-Butylbenzene U 0.00271 0.00695 1 02/06/2024 02:17 WG2220500
Carbon tetrachloride U 0.00125 0.00695 1 02/06/2024 02:17 WG2220500
Chlorobenzene U 0.000292 0.00348 1 02/06/2024 02:17 WG2220500
Chlorodibromomethane U 0.000851 0.00348 1 02/06/2024 02:17 WG2220500
Chloroethane U 0.00236 0.00695 1 02/06/2024 02:17 WG2220500
Chloroform 0.00317 B J 0.00143 0.00348 1 02/06/2024 02:17 WG2220500
Chloromethane U 0.00605 0.0174 1 02/06/2024 02:17 WG2220500
2-Chlorotoluene U 0.00120 0.00348 1 02/06/2024 02:17 WG2220500
4-Chlorotoluene U 0.000626 0.00695 1 02/06/2024 02:17 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00542 0.0348 1 02/06/2024 02:17 WG2220500
1,2-Dibromoethane U 0.000901 0.00348 1 02/06/2024 02:17 WG2220500
Dibromomethane U 0.00104 0.00695 1 02/06/2024 02:17 WG2220500
1,2-Dichlorobenzene U 0.000591 0.00695 1 02/06/2024 02:17 WG2220500
1,3-Dichlorobenzene U 0.000834 0.00695 1 02/06/2024 02:17 WG2220500
1,4-Dichlorobenzene U 0.000974 0.00695 1 02/06/2024 02:17 WG2220500
Dichlorodifluoromethane U 0.00224 0.00695 1 02/06/2024 02:17 WG2220500
1,1-Dichloroethane U 0.000683 0.00348 1 02/06/2024 02:17 WG2220500
1,2-Dichloroethane U 0.000903 0.00348 1 02/06/2024 02:17 WG2220500
1,1-Dichloroethene U 0.000843 0.00348 1 02/06/2024 02:17 WG2220500
cis-1,2-Dichloroethene U 0.00102 0.00348 1 02/06/2024 02:17 WG2220500
trans-1,2-Dichloroethene U 0.00145 0.00695 1 02/06/2024 02:17 WG2220500
1,2-Dichloropropane U 0.00197 0.00695 1 02/06/2024 02:17 WG2220500
1,1-Dichloropropene U 0.00113 0.00348 1 02/06/2024 02:17 WG2220500
1,3-Dichloropropane U 0.000697 0.00695 1 02/06/2024 02:17 WG2220500
cis-1,3-Dichloropropene U 0.00105 0.00348 1 02/06/2024 02:17 WG2220500
trans-1,3-Dichloropropene U 0.00159 0.00695 1 02/06/2024 02:17 WG2220500
2,2-Dichloropropane U 0.00192 0.00348 1 02/06/2024 02:17 WG2220500
Di-isopropyl ether U 0.000570 0.00139 1 02/06/2024 02:17 WG2220500
Ethylbenzene U 0.00102 0.00348 1 02/06/2024 02:17 WG2220500
Hexachloro-1,3-butadiene U 0.00834 0.0348 1 02/06/2024 02:17 WG2220500
Isopropylbenzene U 0.000591 0.00348 1 02/06/2024 02:17 WG2220500
p-Isopropyltoluene U 0.00355 0.00695 1 02/06/2024 02:17 WG2220500
2-Butanone (MEK)U 0.0883 0.139 1 02/06/2024 02:17 WG2220500
Methylene Chloride 0.0163 B J 0.00923 0.0348 1 02/06/2024 02:17 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00317 0.0348 1 02/06/2024 02:17 WG2220500
Methyl tert-butyl ether U 0.000487 0.00139 1 02/06/2024 02:17 WG2220500
Naphthalene U C3 0.00679 0.0174 1 02/06/2024 02:17 WG2220500
n-Propylbenzene U 0.00132 0.00695 1 02/06/2024 02:17 WG2220500
Styrene U 0.000318 0.0174 1 02/06/2024 02:17 WG2220500
1,1,1,2-Tetrachloroethane U 0.00132 0.00348 1 02/06/2024 02:17 WG2220500
1,1,2,2-Tetrachloroethane U 0.000967 0.00348 1 02/06/2024 02:17 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 17
L1701794
SB-10 0-1
Collected date/time: 01/29/24 16:45
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00105 0.00348 1 02/06/2024 02:17 WG2220500
Tetrachloroethene 0.115 0.00125 0.00348 1 02/06/2024 02:17 WG2220500
Toluene U 0.00181 0.00695 1 02/06/2024 02:17 WG2220500
1,2,3-Trichlorobenzene U 0.0102 0.0174 1 02/06/2024 02:17 WG2220500
1,2,4-Trichlorobenzene U 0.00612 0.0174 1 02/06/2024 02:17 WG2220500
1,1,1-Trichloroethane U 0.00128 0.00348 1 02/06/2024 02:17 WG2220500
1,1,2-Trichloroethane U 0.000830 0.00348 1 02/06/2024 02:17 WG2220500
Trichloroethene U J4 0.000812 0.00139 1 02/06/2024 02:17 WG2220500
Trichlorofluoromethane U 0.00115 0.00348 1 02/06/2024 02:17 WG2220500
1,2,3-Trichloropropane U 0.00225 0.0174 1 02/06/2024 02:17 WG2220500
1,2,4-Trimethylbenzene U 0.00220 0.00695 1 02/06/2024 02:17 WG2220500
1,2,3-Trimethylbenzene U 0.00220 0.00695 1 02/06/2024 02:17 WG2220500
1,3,5-Trimethylbenzene U 0.00278 0.00695 1 02/06/2024 02:17 WG2220500
Vinyl chloride U 0.00161 0.00348 1 02/06/2024 02:17 WG2220500
Xylenes, Total U 0.00122 0.00904 1 02/06/2024 02:17 WG2220500
(S) Toluene-d8 104 75.0-131 02/06/2024 02:17 WG2220500
(S) 4-Bromofluorobenzene 94.7 67.0-138 02/06/2024 02:17 WG2220500
(S) 1,2-Dichloroethane-d4 116 70.0-130 02/06/2024 02:17 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00639 0.0395 1 02/08/2024 22:06 WG2220590
Acenaphthylene U 0.00556 0.0395 1 02/08/2024 22:06 WG2220590
Anthracene U 0.00703 0.0395 1 02/08/2024 22:06 WG2220590
Benzidine U 0.0742 1.98 1 02/08/2024 22:06 WG2220590
Benzo(a)anthracene U 0.00696 0.0395 1 02/08/2024 22:06 WG2220590
Benzo(b)fluoranthene U 0.00736 0.0395 1 02/08/2024 22:06 WG2220590
Benzo(k)fluoranthene U 0.00702 0.0395 1 02/08/2024 22:06 WG2220590
Benzo(g,h,i)perylene U 0.00722 0.0395 1 02/08/2024 22:06 WG2220590
Benzo(a)pyrene U 0.00734 0.0395 1 02/08/2024 22:06 WG2220590
Bis(2-chlorethoxy)methane U 0.0119 0.395 1 02/08/2024 22:06 WG2220590
Bis(2-chloroethyl)ether U 0.0130 0.395 1 02/08/2024 22:06 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0171 0.395 1 02/08/2024 22:06 WG2220590
4-Bromophenyl-phenylether U 0.0139 0.395 1 02/08/2024 22:06 WG2220590
2-Chloronaphthalene U 0.00694 0.0395 1 02/08/2024 22:06 WG2220590
4-Chlorophenyl-phenylether U 0.0138 0.395 1 02/08/2024 22:06 WG2220590
Chrysene U 0.00785 0.0395 1 02/08/2024 22:06 WG2220590
Dibenz(a,h)anthracene U 0.0109 0.0395 1 02/08/2024 22:06 WG2220590
1,2-Dichlorobenzene U 0.0117 0.395 1 02/08/2024 22:06 WG2220590
1,3-Dichlorobenzene U 0.0120 0.395 1 02/08/2024 22:06 WG2220590
1,4-Dichlorobenzene U 0.0118 0.395 1 02/08/2024 22:06 WG2220590
3,3-Dichlorobenzidine U 0.0146 0.395 1 02/08/2024 22:06 WG2220590
2,4-Dinitrotoluene U 0.0113 0.395 1 02/08/2024 22:06 WG2220590
2,6-Dinitrotoluene U 0.0129 0.395 1 02/08/2024 22:06 WG2220590
Fluoranthene U 0.00713 0.0395 1 02/08/2024 22:06 WG2220590
Fluorene U 0.00643 0.0395 1 02/08/2024 22:06 WG2220590
Hexachlorobenzene U 0.0140 0.395 1 02/08/2024 22:06 WG2220590
Hexachloro-1,3-butadiene U 0.0133 0.395 1 02/08/2024 22:06 WG2220590
Hexachlorocyclopentadiene U 0.0208 0.395 1 02/08/2024 22:06 WG2220590
Hexachloroethane U 0.0155 0.395 1 02/08/2024 22:06 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0112 0.0395 1 02/08/2024 22:06 WG2220590
Isophorone U 0.0121 0.395 1 02/08/2024 22:06 WG2220590
Naphthalene U 0.00991 0.0395 1 02/08/2024 22:06 WG2220590
Nitrobenzene U 0.0138 0.395 1 02/08/2024 22:06 WG2220590
n-Nitrosodimethylamine U 0.0586 0.395 1 02/08/2024 22:06 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 17
L1701794
SB-10 0-1
Collected date/time: 01/29/24 16:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0299 0.395 1 02/08/2024 22:06 WG2220590
n-Nitrosodi-n-propylamine U 0.0132 0.395 1 02/08/2024 22:06 WG2220590
Phenanthrene U 0.00784 0.0395 1 02/08/2024 22:06 WG2220590
Benzylbutyl phthalate U 0.0123 0.395 1 02/08/2024 22:06 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0500 0.395 1 02/08/2024 22:06 WG2220590
Di-n-butyl phthalate U 0.0135 0.395 1 02/08/2024 22:06 WG2220590
Diethyl phthalate U 0.0130 0.395 1 02/08/2024 22:06 WG2220590
Dimethyl phthalate U 0.0837 0.395 1 02/08/2024 22:06 WG2220590
Di-n-octyl phthalate U 0.0267 0.395 1 02/08/2024 22:06 WG2220590
Pyrene U 0.00769 0.0395 1 02/08/2024 22:06 WG2220590
1,2,4-Trichlorobenzene U 0.0123 0.395 1 02/08/2024 22:06 WG2220590
4-Chloro-3-methylphenol U 0.0128 0.395 1 02/08/2024 22:06 WG2220590
2-Chlorophenol U 0.0130 0.395 1 02/08/2024 22:06 WG2220590
2,4-Dichlorophenol U 0.0115 0.395 1 02/08/2024 22:06 WG2220590
2,4-Dimethylphenol U 0.0103 0.395 1 02/08/2024 22:06 WG2220590
4,6-Dinitro-2-methylphenol U 0.0895 0.395 1 02/08/2024 22:06 WG2220590
2,4-Dinitrophenol U 0.0924 0.395 1 02/08/2024 22:06 WG2220590
2-Nitrophenol U 0.0141 0.395 1 02/08/2024 22:06 WG2220590
4-Nitrophenol U 0.0123 0.395 1 02/08/2024 22:06 WG2220590
Pentachlorophenol U 0.0106 0.395 1 02/08/2024 22:06 WG2220590
Phenol U 0.0159 0.395 1 02/08/2024 22:06 WG2220590
2,4,6-Trichlorophenol U 0.0127 0.395 1 02/08/2024 22:06 WG2220590
(S) 2-Fluorophenol 66.9 12.0-120 02/08/2024 22:06 WG2220590
(S) Phenol-d5 68.0 10.0-120 02/08/2024 22:06 WG2220590
(S) Nitrobenzene-d5 60.8 10.0-122 02/08/2024 22:06 WG2220590
(S) 2-Fluorobiphenyl 62.7 15.0-120 02/08/2024 22:06 WG2220590
(S) 2,4,6-Tribromophenol 66.7 10.0-127 02/08/2024 22:06 WG2220590
(S) p-Terphenyl-d14 75.8 10.0-120 02/08/2024 22:06 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 18
L1701794
SB-10 3-4
Collected date/time: 01/29/24 16:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.9 1 02/06/2024 15:26 WG2220127
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0559 0.0765 1 02/06/2024 02:40 WG2220500
Acrylonitrile U 0.00552 0.0191 1 02/06/2024 02:40 WG2220500
Benzene U 0.000715 0.00153 1 02/06/2024 02:40 WG2220500
Bromobenzene U 0.00138 0.0191 1 02/06/2024 02:40 WG2220500
Bromodichloromethane U 0.00111 0.00383 1 02/06/2024 02:40 WG2220500
Bromoform U 0.00179 0.0383 1 02/06/2024 02:40 WG2220500
Bromomethane U 0.00301 0.0191 1 02/06/2024 02:40 WG2220500
n-Butylbenzene U 0.00803 0.0191 1 02/06/2024 02:40 WG2220500
sec-Butylbenzene U 0.00441 0.0191 1 02/06/2024 02:40 WG2220500
tert-Butylbenzene U 0.00298 0.00765 1 02/06/2024 02:40 WG2220500
Carbon tetrachloride U 0.00137 0.00765 1 02/06/2024 02:40 WG2220500
Chlorobenzene U 0.000321 0.00383 1 02/06/2024 02:40 WG2220500
Chlorodibromomethane U 0.000937 0.00383 1 02/06/2024 02:40 WG2220500
Chloroethane U 0.00260 0.00765 1 02/06/2024 02:40 WG2220500
Chloroform 0.00320 B J 0.00158 0.00383 1 02/06/2024 02:40 WG2220500
Chloromethane U 0.00666 0.0191 1 02/06/2024 02:40 WG2220500
2-Chlorotoluene U 0.00132 0.00383 1 02/06/2024 02:40 WG2220500
4-Chlorotoluene U 0.000689 0.00765 1 02/06/2024 02:40 WG2220500
1,2-Dibromo-3-Chloropropane U 0.00597 0.0383 1 02/06/2024 02:40 WG2220500
1,2-Dibromoethane U 0.000992 0.00383 1 02/06/2024 02:40 WG2220500
Dibromomethane U 0.00115 0.00765 1 02/06/2024 02:40 WG2220500
1,2-Dichlorobenzene U 0.000650 0.00765 1 02/06/2024 02:40 WG2220500
1,3-Dichlorobenzene U 0.000918 0.00765 1 02/06/2024 02:40 WG2220500
1,4-Dichlorobenzene U 0.00107 0.00765 1 02/06/2024 02:40 WG2220500
Dichlorodifluoromethane U 0.00246 0.00765 1 02/06/2024 02:40 WG2220500
1,1-Dichloroethane U 0.000751 0.00383 1 02/06/2024 02:40 WG2220500
1,2-Dichloroethane U 0.000993 0.00383 1 02/06/2024 02:40 WG2220500
1,1-Dichloroethene U 0.000927 0.00383 1 02/06/2024 02:40 WG2220500
cis-1,2-Dichloroethene U 0.00112 0.00383 1 02/06/2024 02:40 WG2220500
trans-1,2-Dichloroethene U 0.00159 0.00765 1 02/06/2024 02:40 WG2220500
1,2-Dichloropropane U 0.00217 0.00765 1 02/06/2024 02:40 WG2220500
1,1-Dichloropropene U 0.00124 0.00383 1 02/06/2024 02:40 WG2220500
1,3-Dichloropropane U 0.000767 0.00765 1 02/06/2024 02:40 WG2220500
cis-1,3-Dichloropropene U 0.00116 0.00383 1 02/06/2024 02:40 WG2220500
trans-1,3-Dichloropropene U 0.00174 0.00765 1 02/06/2024 02:40 WG2220500
2,2-Dichloropropane U 0.00211 0.00383 1 02/06/2024 02:40 WG2220500
Di-isopropyl ether U 0.000627 0.00153 1 02/06/2024 02:40 WG2220500
Ethylbenzene U 0.00113 0.00383 1 02/06/2024 02:40 WG2220500
Hexachloro-1,3-butadiene U 0.00918 0.0383 1 02/06/2024 02:40 WG2220500
Isopropylbenzene U 0.000650 0.00383 1 02/06/2024 02:40 WG2220500
p-Isopropyltoluene U 0.00390 0.00765 1 02/06/2024 02:40 WG2220500
2-Butanone (MEK)U 0.0972 0.153 1 02/06/2024 02:40 WG2220500
Methylene Chloride 0.0152 B J 0.0102 0.0383 1 02/06/2024 02:40 WG2220500
4-Methyl-2-pentanone (MIBK)U 0.00349 0.0383 1 02/06/2024 02:40 WG2220500
Methyl tert-butyl ether U 0.000536 0.00153 1 02/06/2024 02:40 WG2220500
Naphthalene U C3 0.00747 0.0191 1 02/06/2024 02:40 WG2220500
n-Propylbenzene U 0.00145 0.00765 1 02/06/2024 02:40 WG2220500
Styrene U 0.000350 0.0191 1 02/06/2024 02:40 WG2220500
1,1,1,2-Tetrachloroethane U 0.00145 0.00383 1 02/06/2024 02:40 WG2220500
1,1,2,2-Tetrachloroethane U 0.00106 0.00383 1 02/06/2024 02:40 WG2220500
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 18
L1701794
SB-10 3-4
Collected date/time: 01/29/24 16:50
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane U 0.00115 0.00383 1 02/06/2024 02:40 WG2220500
Tetrachloroethene U 0.00137 0.00383 1 02/06/2024 02:40 WG2220500
Toluene U 0.00199 0.00765 1 02/06/2024 02:40 WG2220500
1,2,3-Trichlorobenzene U 0.0112 0.0191 1 02/06/2024 02:40 WG2220500
1,2,4-Trichlorobenzene U 0.00673 0.0191 1 02/06/2024 02:40 WG2220500
1,1,1-Trichloroethane U 0.00141 0.00383 1 02/06/2024 02:40 WG2220500
1,1,2-Trichloroethane U 0.000914 0.00383 1 02/06/2024 02:40 WG2220500
Trichloroethene U J4 0.000894 0.00153 1 02/06/2024 02:40 WG2220500
Trichlorofluoromethane U 0.00127 0.00383 1 02/06/2024 02:40 WG2220500
1,2,3-Trichloropropane U 0.00248 0.0191 1 02/06/2024 02:40 WG2220500
1,2,4-Trimethylbenzene U 0.00242 0.00765 1 02/06/2024 02:40 WG2220500
1,2,3-Trimethylbenzene U 0.00242 0.00765 1 02/06/2024 02:40 WG2220500
1,3,5-Trimethylbenzene U 0.00306 0.00765 1 02/06/2024 02:40 WG2220500
Vinyl chloride U 0.00178 0.00383 1 02/06/2024 02:40 WG2220500
Xylenes, Total U 0.00135 0.00995 1 02/06/2024 02:40 WG2220500
(S) Toluene-d8 107 75.0-131 02/06/2024 02:40 WG2220500
(S) 4-Bromofluorobenzene 97.9 67.0-138 02/06/2024 02:40 WG2220500
(S) 1,2-Dichloroethane-d4 116 70.0-130 02/06/2024 02:40 WG2220500
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00675 0.0417 1 02/08/2024 21:25 WG2220590
Acenaphthylene U 0.00587 0.0417 1 02/08/2024 21:25 WG2220590
Anthracene U 0.00743 0.0417 1 02/08/2024 21:25 WG2220590
Benzidine U 0.0784 2.09 1 02/08/2024 21:25 WG2220590
Benzo(a)anthracene U 0.00735 0.0417 1 02/08/2024 21:25 WG2220590
Benzo(b)fluoranthene U 0.00778 0.0417 1 02/08/2024 21:25 WG2220590
Benzo(k)fluoranthene U 0.00741 0.0417 1 02/08/2024 21:25 WG2220590
Benzo(g,h,i)perylene U 0.00763 0.0417 1 02/08/2024 21:25 WG2220590
Benzo(a)pyrene U 0.00775 0.0417 1 02/08/2024 21:25 WG2220590
Bis(2-chlorethoxy)methane U 0.0125 0.417 1 02/08/2024 21:25 WG2220590
Bis(2-chloroethyl)ether U 0.0138 0.417 1 02/08/2024 21:25 WG2220590
2,2-Oxybis(1-Chloropropane)U 0.0180 0.417 1 02/08/2024 21:25 WG2220590
4-Bromophenyl-phenylether U 0.0147 0.417 1 02/08/2024 21:25 WG2220590
2-Chloronaphthalene U 0.00733 0.0417 1 02/08/2024 21:25 WG2220590
4-Chlorophenyl-phenylether U 0.0145 0.417 1 02/08/2024 21:25 WG2220590
Chrysene U 0.00829 0.0417 1 02/08/2024 21:25 WG2220590
Dibenz(a,h)anthracene U 0.0116 0.0417 1 02/08/2024 21:25 WG2220590
1,2-Dichlorobenzene U 0.0124 0.417 1 02/08/2024 21:25 WG2220590
1,3-Dichlorobenzene U 0.0126 0.417 1 02/08/2024 21:25 WG2220590
1,4-Dichlorobenzene U 0.0124 0.417 1 02/08/2024 21:25 WG2220590
3,3-Dichlorobenzidine U 0.0154 0.417 1 02/08/2024 21:25 WG2220590
2,4-Dinitrotoluene U 0.0120 0.417 1 02/08/2024 21:25 WG2220590
2,6-Dinitrotoluene U 0.0136 0.417 1 02/08/2024 21:25 WG2220590
Fluoranthene U 0.00753 0.0417 1 02/08/2024 21:25 WG2220590
Fluorene U 0.00679 0.0417 1 02/08/2024 21:25 WG2220590
Hexachlorobenzene U 0.0148 0.417 1 02/08/2024 21:25 WG2220590
Hexachloro-1,3-butadiene U 0.0140 0.417 1 02/08/2024 21:25 WG2220590
Hexachlorocyclopentadiene U 0.0219 0.417 1 02/08/2024 21:25 WG2220590
Hexachloroethane U 0.0164 0.417 1 02/08/2024 21:25 WG2220590
Indeno(1,2,3-cd)pyrene U 0.0118 0.0417 1 02/08/2024 21:25 WG2220590
Isophorone U 0.0128 0.417 1 02/08/2024 21:25 WG2220590
Naphthalene U 0.0105 0.0417 1 02/08/2024 21:25 WG2220590
Nitrobenzene U 0.0145 0.417 1 02/08/2024 21:25 WG2220590
n-Nitrosodimethylamine U 0.0619 0.417 1 02/08/2024 21:25 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 18
L1701794
SB-10 3-4
Collected date/time: 01/29/24 16:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
n-Nitrosodiphenylamine U 0.0316 0.417 1 02/08/2024 21:25 WG2220590
n-Nitrosodi-n-propylamine U 0.0139 0.417 1 02/08/2024 21:25 WG2220590
Phenanthrene U 0.00828 0.0417 1 02/08/2024 21:25 WG2220590
Benzylbutyl phthalate U 0.0130 0.417 1 02/08/2024 21:25 WG2220590
Bis(2-ethylhexyl)phthalate U 0.0528 0.417 1 02/08/2024 21:25 WG2220590
Di-n-butyl phthalate U 0.0143 0.417 1 02/08/2024 21:25 WG2220590
Diethyl phthalate U 0.0138 0.417 1 02/08/2024 21:25 WG2220590
Dimethyl phthalate U 0.0884 0.417 1 02/08/2024 21:25 WG2220590
Di-n-octyl phthalate U 0.0282 0.417 1 02/08/2024 21:25 WG2220590
Pyrene U 0.00811 0.0417 1 02/08/2024 21:25 WG2220590
1,2,4-Trichlorobenzene U 0.0130 0.417 1 02/08/2024 21:25 WG2220590
4-Chloro-3-methylphenol U 0.0135 0.417 1 02/08/2024 21:25 WG2220590
2-Chlorophenol U 0.0138 0.417 1 02/08/2024 21:25 WG2220590
2,4-Dichlorophenol U 0.0121 0.417 1 02/08/2024 21:25 WG2220590
2,4-Dimethylphenol U 0.0109 0.417 1 02/08/2024 21:25 WG2220590
4,6-Dinitro-2-methylphenol U 0.0945 0.417 1 02/08/2024 21:25 WG2220590
2,4-Dinitrophenol U 0.0975 0.417 1 02/08/2024 21:25 WG2220590
2-Nitrophenol U 0.0149 0.417 1 02/08/2024 21:25 WG2220590
4-Nitrophenol U 0.0130 0.417 1 02/08/2024 21:25 WG2220590
Pentachlorophenol U 0.0112 0.417 1 02/08/2024 21:25 WG2220590
Phenol U 0.0168 0.417 1 02/08/2024 21:25 WG2220590
2,4,6-Trichlorophenol U 0.0134 0.417 1 02/08/2024 21:25 WG2220590
(S) 2-Fluorophenol 63.4 12.0-120 02/08/2024 21:25 WG2220590
(S) Phenol-d5 63.4 10.0-120 02/08/2024 21:25 WG2220590
(S) Nitrobenzene-d5 63.7 10.0-122 02/08/2024 21:25 WG2220590
(S) 2-Fluorobiphenyl 61.2 15.0-120 02/08/2024 21:25 WG2220590
(S) 2,4,6-Tribromophenol 63.5 10.0-127 02/08/2024 21:25 WG2220590
(S) p-Terphenyl-d14 69.6 10.0-120 02/08/2024 21:25 WG2220590
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2219975
Total Solids by Method 2540 G-2011 L1701794-01
Method Blank (MB)
(MB) R4030682-1 02/06/24 15:57
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1701791-08 Original Sample (OS) • Duplicate (DUP)
(OS) L1701791-08 02/06/24 15:57 • (DUP) R4030682-3 02/06/24 15:57
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 83.0 83.4 1 0.428 10
Laboratory Control Sample (LCS)
(LCS) R4030682-2 02/06/24 15:57
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 90.0-110
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2219977
Total Solids by Method 2540 G-2011 L1701794-02,03,04,05,06,07,08,09,10,11
Method Blank (MB)
(MB) R4030705-1 02/06/24 11:02
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00200
L1701794-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1701794-04 02/06/24 11:02 • (DUP) R4030705-3 02/06/24 11:02
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 71.0 71.8 1 1.10 10
Laboratory Control Sample (LCS)
(LCS) R4030705-2 02/06/24 11:02
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 90.0-110
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220127
Total Solids by Method 2540 G-2011 L1701794-12,13,14,15,16,17,18
Method Blank (MB)
(MB) R4030675-1 02/06/24 15:26
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00300
L1701794-18 Original Sample (OS) • Duplicate (DUP)
(OS) L1701794-18 02/06/24 15:26 • (DUP) R4030675-3 02/06/24 15:26
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 79.9 78.0 1 2.36 10
Laboratory Control Sample (LCS)
(LCS) R4030675-2 02/06/24 15:26
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 90.0-110
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220500
Volatile Organic Compounds (GC/MS) by Method 8260D L1701794-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R4032507-2 02/05/24 19:15
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform 0.00115 J 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00500
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220500
Volatile Organic Compounds (GC/MS) by Method 8260D L1701794-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R4032507-2 02/05/24 19:15
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride 0.0125 J 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 103 75.0-131
(S) 4-Bromofluorobenzene 98.6 67.0-138
(S) 1,2-Dichloroethane-d4 116 70.0-130
Laboratory Control Sample (LCS)
(LCS) R4032507-1 02/05/24 17:56
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.699 112 10.0-160
Acrylonitrile 0.625 0.607 97.1 45.0-153
Benzene 0.125 0.137 110 70.0-123
Bromobenzene 0.125 0.138 110 73.0-121
Bromodichloromethane 0.125 0.135 108 73.0-121
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220500
Volatile Organic Compounds (GC/MS) by Method 8260D L1701794-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Laboratory Control Sample (LCS)
(LCS) R4032507-1 02/05/24 17:56
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromoform 0.125 0.128 102 64.0-132
Bromomethane 0.125 0.141 113 56.0-147
n-Butylbenzene 0.125 0.112 89.6 68.0-135
sec-Butylbenzene 0.125 0.114 91.2 74.0-130
tert-Butylbenzene 0.125 0.121 96.8 75.0-127
Carbon tetrachloride 0.125 0.156 125 66.0-128
Chlorobenzene 0.125 0.137 110 76.0-128
Chlorodibromomethane 0.125 0.142 114 74.0-127
Chloroethane 0.125 0.140 112 61.0-134
Chloroform 0.125 0.138 110 72.0-123
Chloromethane 0.125 0.132 106 51.0-138
2-Chlorotoluene 0.125 0.121 96.8 75.0-124
4-Chlorotoluene 0.125 0.129 103 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.117 93.6 59.0-130
1,2-Dibromoethane 0.125 0.140 112 74.0-128
Dibromomethane 0.125 0.143 114 75.0-122
1,2-Dichlorobenzene 0.125 0.131 105 76.0-124
1,3-Dichlorobenzene 0.125 0.130 104 76.0-125
1,4-Dichlorobenzene 0.125 0.105 84.0 77.0-121
Dichlorodifluoromethane 0.125 0.178 142 43.0-156
1,1-Dichloroethane 0.125 0.133 106 70.0-127
1,2-Dichloroethane 0.125 0.158 126 65.0-131
1,1-Dichloroethene 0.125 0.136 109 65.0-131
cis-1,2-Dichloroethene 0.125 0.136 109 73.0-125
trans-1,2-Dichloroethene 0.125 0.136 109 71.0-125
1,2-Dichloropropane 0.125 0.128 102 74.0-125
1,1-Dichloropropene 0.125 0.155 124 73.0-125
1,3-Dichloropropane 0.125 0.142 114 80.0-125
cis-1,3-Dichloropropene 0.125 0.130 104 76.0-127
trans-1,3-Dichloropropene 0.125 0.143 114 73.0-127
2,2-Dichloropropane 0.125 0.153 122 59.0-135
Di-isopropyl ether 0.125 0.113 90.4 60.0-136
Ethylbenzene 0.125 0.133 106 74.0-126
Hexachloro-1,3-butadiene 0.125 0.125 100 57.0-150
Isopropylbenzene 0.125 0.124 99.2 72.0-127
p-Isopropyltoluene 0.125 0.114 91.2 72.0-133
2-Butanone (MEK)0.625 0.702 112 30.0-160
Methylene Chloride 0.125 0.127 102 68.0-123
4-Methyl-2-pentanone (MIBK)0.625 0.665 106 56.0-143
Methyl tert-butyl ether 0.125 0.133 106 66.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220500
Volatile Organic Compounds (GC/MS) by Method 8260D L1701794-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Laboratory Control Sample (LCS)
(LCS) R4032507-1 02/05/24 17:56
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Naphthalene 0.125 0.0960 76.8 59.0-130
n-Propylbenzene 0.125 0.125 100 74.0-126
Styrene 0.125 0.121 96.8 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.142 114 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.110 88.0 68.0-128
1,1,2-Trichlorotrifluoroethane 0.125 0.152 122 61.0-139
Tetrachloroethene 0.125 0.145 116 70.0-136
Toluene 0.125 0.133 106 75.0-121
1,2,3-Trichlorobenzene 0.125 0.107 85.6 59.0-139
1,2,4-Trichlorobenzene 0.125 0.108 86.4 62.0-137
1,1,1-Trichloroethane 0.125 0.150 120 69.0-126
1,1,2-Trichloroethane 0.125 0.112 89.6 78.0-123
Trichloroethene 0.125 0.162 130 76.0-126 J4
Trichlorofluoromethane 0.125 0.149 119 61.0-142
1,2,3-Trichloropropane 0.125 0.145 116 67.0-129
1,2,4-Trimethylbenzene 0.125 0.109 87.2 70.0-126
1,2,3-Trimethylbenzene 0.125 0.118 94.4 74.0-124
1,3,5-Trimethylbenzene 0.125 0.115 92.0 73.0-127
Vinyl chloride 0.125 0.136 109 63.0-134
Xylenes, Total 0.375 0.389 104 72.0-127
(S) Toluene-d8 103 75.0-131
(S) 4-Bromofluorobenzene 102 67.0-138
(S) 1,2-Dichloroethane-d4 117 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2224617
Volatile Organic Compounds (GC/MS) by Method 8260D L1701794-13,16
Method Blank (MB)
(MB) R4033240-3 02/13/24 11:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Tetrachloroethene U 0.000896 0.00250
(S) Toluene-d8 97.9 75.0-131
(S) 4-Bromofluorobenzene 94.0 67.0-138
(S) 1,2-Dichloroethane-d4 77.3 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4033240-1 02/13/24 09:17 • (LCSD) R4033240-2 02/13/24 09:39
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Tetrachloroethene 0.125 0.121 0.112 96.8 89.6 70.0-136 7.73 20
(S) Toluene-d8 100 95.6 75.0-131
(S) 4-Bromofluorobenzene 96.5 97.2 67.0-138
(S) 1,2-Dichloroethane-d4 83.4 86.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220589
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-01
Method Blank (MB)
(MB) R4031345-2 02/07/24 00:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane)U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
1,2-Dichlorobenzene U 0.00987 0.333
1,3-Dichlorobenzene U 0.0101 0.333
1,4-Dichlorobenzene U 0.00991 0.333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220589
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-01
Method Blank (MB)
(MB) R4031345-2 02/07/24 00:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) 2-Fluorophenol 70.9 12.0-120
(S) Phenol-d5 64.6 10.0-120
(S) Nitrobenzene-d5 66.1 10.0-122
(S) 2-Fluorobiphenyl 63.7 15.0-120
(S) 2,4,6-Tribromophenol 64.4 10.0-127
(S) p-Terphenyl-d14 72.7 10.0-120
Laboratory Control Sample (LCS)
(LCS) R4031345-1 02/07/24 00:26
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.430 64.6 38.0-120
Acenaphthylene 0.666 0.478 71.8 40.0-120
Anthracene 0.666 0.461 69.2 42.0-120
Benzidine 1.33 0.677 50.9 10.0-120
Benzo(a)anthracene 0.666 0.492 73.9 44.0-120
Benzo(b)fluoranthene 0.666 0.463 69.5 43.0-120
Benzo(k)fluoranthene 0.666 0.461 69.2 44.0-120
Benzo(g,h,i)perylene 0.666 0.475 71.3 43.0-120
Benzo(a)pyrene 0.666 0.485 72.8 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.341 51.2 20.0-120
Bis(2-chloroethyl)ether 0.666 0.418 62.8 16.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220589
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-01
Laboratory Control Sample (LCS)
(LCS) R4031345-1 02/07/24 00:26
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2,2-Oxybis(1-Chloropropane)0.666 0.413 62.0 23.0-120
4-Bromophenyl-phenylether 0.666 0.454 68.2 40.0-120
2-Chloronaphthalene 0.666 0.427 64.1 35.0-120
4-Chlorophenyl-phenylether 0.666 0.466 70.0 40.0-120
Chrysene 0.666 0.458 68.8 43.0-120
Dibenz(a,h)anthracene 0.666 0.499 74.9 44.0-120
1,2-Dichlorobenzene 0.666 0.396 59.5 32.0-120
1,3-Dichlorobenzene 0.666 0.389 58.4 30.0-120
1,4-Dichlorobenzene 0.666 0.412 61.9 31.0-120
3,3-Dichlorobenzidine 1.33 0.938 70.5 28.0-120
2,4-Dinitrotoluene 0.666 0.482 72.4 45.0-120
2,6-Dinitrotoluene 0.666 0.483 72.5 42.0-120
Fluoranthene 0.666 0.462 69.4 44.0-120
Fluorene 0.666 0.457 68.6 41.0-120
Hexachlorobenzene 0.666 0.445 66.8 39.0-120
Hexachloro-1,3-butadiene 0.666 0.331 49.7 15.0-120
Hexachlorocyclopentadiene 0.666 0.312 46.8 15.0-120
Hexachloroethane 0.666 0.396 59.5 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.518 77.8 45.0-120
Isophorone 0.666 0.381 57.2 23.0-120
Naphthalene 0.666 0.343 51.5 18.0-120
Nitrobenzene 0.666 0.352 52.9 17.0-120
n-Nitrosodimethylamine 0.666 0.396 59.5 10.0-125
n-Nitrosodiphenylamine 0.666 0.438 65.8 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.494 74.2 26.0-120
Phenanthrene 0.666 0.435 65.3 42.0-120
Benzylbutyl phthalate 0.666 0.557 83.6 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.535 80.3 41.0-120
Di-n-butyl phthalate 0.666 0.451 67.7 43.0-120
Diethyl phthalate 0.666 0.501 75.2 43.0-120
Dimethyl phthalate 0.666 0.501 75.2 43.0-120
Di-n-octyl phthalate 0.666 0.540 81.1 40.0-120
Pyrene 0.666 0.468 70.3 41.0-120
1,2,4-Trichlorobenzene 0.666 0.344 51.7 17.0-120
4-Chloro-3-methylphenol 0.666 0.371 55.7 28.0-120
2-Chlorophenol 0.666 0.416 62.5 28.0-120
2,4-Dichlorophenol 0.666 0.340 51.1 25.0-120
2,4-Dimethylphenol 0.666 0.327 49.1 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.419 62.9 16.0-120
2,4-Dinitrophenol 0.666 0.286 42.9 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220589
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-01
Laboratory Control Sample (LCS)
(LCS) R4031345-1 02/07/24 00:26
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2-Nitrophenol 0.666 0.360 54.1 20.0-120
4-Nitrophenol 0.666 0.496 74.5 27.0-120
Pentachlorophenol 0.666 0.350 52.6 29.0-120
Phenol 0.666 0.416 62.5 28.0-120
2,4,6-Trichlorophenol 0.666 0.420 63.1 37.0-120
(S) 2-Fluorophenol 72.2 12.0-120
(S) Phenol-d5 66.1 10.0-120
(S) Nitrobenzene-d5 57.7 10.0-122
(S) 2-Fluorobiphenyl 67.3 15.0-120
(S) 2,4,6-Tribromophenol 74.9 10.0-127
(S) p-Terphenyl-d14 73.9 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220590
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R4031977-2 02/08/24 14:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane)U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
1,2-Dichlorobenzene U 0.00987 0.333
1,3-Dichlorobenzene U 0.0101 0.333
1,4-Dichlorobenzene U 0.00991 0.333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220590
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R4031977-2 02/08/24 14:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) 2-Fluorophenol 70.4 12.0-120
(S) Phenol-d5 66.4 10.0-120
(S) Nitrobenzene-d5 67.9 10.0-122
(S) 2-Fluorobiphenyl 67.9 15.0-120
(S) 2,4,6-Tribromophenol 64.4 10.0-127
(S) p-Terphenyl-d14 79.0 10.0-120
Laboratory Control Sample (LCS)
(LCS) R4031977-1 02/08/24 14:14
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.544 81.7 38.0-120
Acenaphthylene 0.666 0.551 82.7 40.0-120
Anthracene 0.666 0.548 82.3 42.0-120
Benzidine 1.33 0.796 59.8 10.0-120
Benzo(a)anthracene 0.666 0.600 90.1 44.0-120
Benzo(b)fluoranthene 0.666 0.596 89.5 43.0-120
Benzo(k)fluoranthene 0.666 0.562 84.4 44.0-120
Benzo(g,h,i)perylene 0.666 0.644 96.7 43.0-120
Benzo(a)pyrene 0.666 0.613 92.0 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.454 68.2 20.0-120
Bis(2-chloroethyl)ether 0.666 0.624 93.7 16.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220590
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Laboratory Control Sample (LCS)
(LCS) R4031977-1 02/08/24 14:14
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2,2-Oxybis(1-Chloropropane)0.666 0.469 70.4 23.0-120
4-Bromophenyl-phenylether 0.666 0.512 76.9 40.0-120
2-Chloronaphthalene 0.666 0.507 76.1 35.0-120
4-Chlorophenyl-phenylether 0.666 0.636 95.5 40.0-120
Chrysene 0.666 0.566 85.0 43.0-120
Dibenz(a,h)anthracene 0.666 0.631 94.7 44.0-120
1,2-Dichlorobenzene 0.666 0.505 75.8 32.0-120
1,3-Dichlorobenzene 0.666 0.485 72.8 30.0-120
1,4-Dichlorobenzene 0.666 0.495 74.3 31.0-120
3,3-Dichlorobenzidine 1.33 1.17 88.0 28.0-120
2,4-Dinitrotoluene 0.666 0.641 96.2 45.0-120
2,6-Dinitrotoluene 0.666 0.629 94.4 42.0-120
Fluoranthene 0.666 0.567 85.1 44.0-120
Fluorene 0.666 0.548 82.3 41.0-120
Hexachlorobenzene 0.666 0.524 78.7 39.0-120
Hexachloro-1,3-butadiene 0.666 0.519 77.9 15.0-120
Hexachlorocyclopentadiene 0.666 0.276 41.4 15.0-120
Hexachloroethane 0.666 0.539 80.9 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.637 95.6 45.0-120
Isophorone 0.666 0.437 65.6 23.0-120
Naphthalene 0.666 0.404 60.7 18.0-120
Nitrobenzene 0.666 0.442 66.4 17.0-120
n-Nitrosodimethylamine 0.666 0.558 83.8 10.0-125
n-Nitrosodiphenylamine 0.666 0.478 71.8 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.514 77.2 26.0-120
Phenanthrene 0.666 0.527 79.1 42.0-120
Benzylbutyl phthalate 0.666 0.692 104 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.671 101 41.0-120
Di-n-butyl phthalate 0.666 0.558 83.8 43.0-120
Diethyl phthalate 0.666 0.630 94.6 43.0-120
Dimethyl phthalate 0.666 0.600 90.1 43.0-120
Di-n-octyl phthalate 0.666 0.707 106 40.0-120
Pyrene 0.666 0.601 90.2 41.0-120
1,2,4-Trichlorobenzene 0.666 0.462 69.4 17.0-120
4-Chloro-3-methylphenol 0.666 0.478 71.8 28.0-120
2-Chlorophenol 0.666 0.531 79.7 28.0-120
2,4-Dichlorophenol 0.666 0.491 73.7 25.0-120
2,4-Dimethylphenol 0.666 0.628 94.3 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.512 76.9 16.0-120
2,4-Dinitrophenol 0.666 0.456 68.5 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220590
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Laboratory Control Sample (LCS)
(LCS) R4031977-1 02/08/24 14:14
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2-Nitrophenol 0.666 0.497 74.6 20.0-120
4-Nitrophenol 0.666 0.512 76.9 27.0-120
Pentachlorophenol 0.666 0.475 71.3 29.0-120
Phenol 0.666 0.522 78.4 28.0-120
2,4,6-Trichlorophenol 0.666 0.593 89.0 37.0-120
(S) 2-Fluorophenol 81.1 12.0-120
(S) Phenol-d5 81.1 10.0-120
(S) Nitrobenzene-d5 59.5 10.0-122
(S) 2-Fluorobiphenyl 78.1 15.0-120
(S) 2,4,6-Tribromophenol 80.3 10.0-127
(S) p-Terphenyl-d14 88.3 10.0-120
L1701809-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1701809-01 02/10/24 06:43 • (MS) R4032740-1 02/10/24 07:04 • (MSD) R4032740-2 02/10/24 07:24
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.782 U 0.625 0.567 79.8 72.9 2 18.0-120 9.70 32
Acenaphthylene 0.782 U 0.614 0.558 78.5 71.8 2 25.0-120 9.45 32
Anthracene 0.782 U 0.622 0.567 79.5 72.9 2 22.0-120 9.31 29
Benzidine 1.56 U 0.486 0.179 31.1 11.6 2 10.0-120 J3 92.2 40
Benzo(a)anthracene 0.782 0.0932 0.710 0.613 78.9 66.8 2 25.0-120 14.7 29
Benzo(b)fluoranthene 0.782 0.182 0.751 0.623 72.8 56.8 2 19.0-122 18.6 31
Benzo(k)fluoranthene 0.782 0.0611 0.633 0.548 73.1 62.6 2 23.0-120 14.5 30
Benzo(g,h,i)perylene 0.782 0.122 0.690 0.575 72.6 58.4 2 10.0-120 18.1 33
Benzo(a)pyrene 0.782 0.126 0.704 0.627 73.8 64.4 2 24.0-120 11.6 30
Bis(2-chlorethoxy)methane 0.782 U 0.546 0.503 69.8 64.7 2 10.0-120 8.26 34
Bis(2-chloroethyl)ether 0.782 U 0.673 0.782 86.0 101 2 10.0-120 15.1 40
2,2-Oxybis(1-Chloropropane)0.782 U 0.511 0.437 65.4 56.2 2 10.0-120 15.7 40
4-Bromophenyl-phenylether 0.782 U 0.609 0.539 77.8 69.3 2 27.0-120 12.2 30
2-Chloronaphthalene 0.782 U 0.574 0.509 73.4 65.5 2 20.0-120 12.0 32
4-Chlorophenyl-phenylether 0.782 U 0.711 0.628 90.9 80.8 2 24.0-120 12.4 29
Chrysene 0.782 0.114 0.694 0.597 74.2 62.1 2 21.0-120 15.1 29
Dibenz(a,h)anthracene 0.782 0.0277 0.657 0.572 80.5 70.0 2 10.0-120 13.9 32
1,2-Dichlorobenzene 0.782 U 0.520 0.497 66.5 63.9 2 10.0-120 4.50 38
1,3-Dichlorobenzene 0.782 U 0.507 0.472 64.8 60.7 2 10.0-120 7.13 40
1,4-Dichlorobenzene 0.782 U 0.501 0.469 64.0 60.4 2 10.0-120 6.45 39
3,3-Dichlorobenzidine 1.56 U 1.40 1.08 89.2 69.4 2 10.0-120 25.8 34
2,4-Dinitrotoluene 0.782 U 0.710 0.619 90.8 79.6 2 30.0-120 13.8 31
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220590
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
L1701809-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1701809-01 02/10/24 06:43 • (MS) R4032740-1 02/10/24 07:04 • (MSD) R4032740-2 02/10/24 07:24
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
2,6-Dinitrotoluene 0.782 U 0.703 0.615 89.8 79.1 2 25.0-120 13.3 31
Fluoranthene 0.782 0.267 0.764 0.627 63.5 46.3 2 18.0-126 19.7 32
Fluorene 0.782 U 0.617 0.549 78.9 70.6 2 25.0-120 11.8 30
Hexachlorobenzene 0.782 U 0.619 0.563 79.1 72.4 2 27.0-120 9.37 28
Hexachloro-1,3-butadiene 0.782 U 0.668 0.597 85.4 76.8 2 10.0-120 11.2 38
Hexachlorocyclopentadiene 0.782 U U U 0.000 0.000 2 10.0-120 J6 J6 0.000 40
Hexachloroethane 0.782 U 0.480 0.427 61.4 55.0 2 10.0-120 11.7 40
Indeno(1,2,3-cd)pyrene 0.782 0.108 0.698 0.601 75.4 63.3 2 10.0-120 15.0 32
Isophorone 0.782 U 0.510 0.498 65.2 64.1 2 13.0-120 2.39 34
Naphthalene 0.782 U 0.480 0.461 61.4 59.3 2 10.0-120 4.09 35
Nitrobenzene 0.782 U 0.538 0.513 68.8 65.9 2 10.0-120 4.81 36
n-Nitrosodimethylamine 0.782 U 0.663 0.560 84.8 72.0 2 10.0-127 16.9 40
n-Nitrosodiphenylamine 0.782 U 0.544 0.496 69.5 63.8 2 17.0-120 9.26 29
n-Nitrosodi-n-propylamine 0.782 U 0.570 0.508 72.9 65.3 2 10.0-120 11.6 37
Phenanthrene 0.782 0.114 0.641 0.572 67.4 58.8 2 17.0-120 11.5 31
Benzylbutyl phthalate 0.782 U 0.785 0.699 100 89.9 2 23.0-120 11.5 30
Bis(2-ethylhexyl)phthalate 0.782 U 0.844 0.720 108 92.6 2 17.0-126 15.9 30
Di-n-butyl phthalate 0.782 U 0.635 0.564 81.2 72.6 2 30.0-120 11.8 29
Diethyl phthalate 0.782 U 0.723 0.639 92.5 82.2 2 26.0-120 12.4 28
Dimethyl phthalate 0.782 U 0.661 0.611 84.5 78.6 2 25.0-120 7.76 29
Di-n-octyl phthalate 0.782 U 0.828 0.745 106 95.8 2 21.0-123 10.6 29
Pyrene 0.782 0.225 0.752 0.649 67.4 54.5 2 16.0-121 14.8 32
1,2,4-Trichlorobenzene 0.782 U 0.567 0.538 72.5 69.2 2 12.0-120 5.23 37
4-Chloro-3-methylphenol 0.782 U 0.602 0.579 76.9 74.5 2 15.0-120 3.87 30
2-Chlorophenol 0.782 U 0.567 0.520 72.5 66.9 2 15.0-120 8.64 37
2,4-Dichlorophenol 0.782 U 0.540 0.528 69.1 68.0 2 20.0-120 2.25 31
2,4-Dimethylphenol 0.782 U 0.781 0.717 99.8 92.3 2 10.0-120 8.51 33
4,6-Dinitro-2-methylphenol 0.782 U 0.265 0.205 33.8 26.3 2 10.0-120 25.6 39
2,4-Dinitrophenol 0.782 U 0.343 0.292 43.8 37.6 2 10.0-121 15.9 40
2-Nitrophenol 0.782 U 0.548 0.498 70.0 64.1 2 12.0-120 9.44 39
4-Nitrophenol 0.782 U 0.619 0.514 79.1 66.1 2 10.0-137 18.5 32
Pentachlorophenol 0.782 U 0.505 0.380 64.6 48.9 2 10.0-160 28.3 31
Phenol 0.782 U 0.575 0.510 73.5 65.6 2 12.0-120 12.0 38
2,4,6-Trichlorophenol 0.782 U 0.658 0.601 84.2 77.2 2 19.0-120 9.18 32
(S) 2-Fluorophenol 79.2 71.4 12.0-120
(S) Phenol-d5 76.3 71.1 10.0-120
(S) Nitrobenzene-d5 65.2 64.4 10.0-122
(S) 2-Fluorobiphenyl 76.0 69.7 15.0-120
(S) 2,4,6-Tribromophenol 83.4 77.6 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2220590
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
L1701809-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1701809-01 02/10/24 06:43 • (MS) R4032740-1 02/10/24 07:04 • (MSD) R4032740-2 02/10/24 07:24
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
(S) p-Terphenyl-d14 85.2 74.6 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2221334
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-02
Method Blank (MB)
(MB) R4031845-2 02/08/24 23:22
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane)U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
1,2-Dichlorobenzene U 0.00987 0.333
1,3-Dichlorobenzene U 0.0101 0.333
1,4-Dichlorobenzene U 0.00991 0.333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2221334
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-02
Method Blank (MB)
(MB) R4031845-2 02/08/24 23:22
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) 2-Fluorophenol 70.0 12.0-120
(S) Phenol-d5 64.6 10.0-120
(S) Nitrobenzene-d5 69.7 10.0-122
(S) 2-Fluorobiphenyl 67.3 15.0-120
(S) 2,4,6-Tribromophenol 66.1 10.0-127
(S) p-Terphenyl-d14 80.2 10.0-120
Laboratory Control Sample (LCS)
(LCS) R4031845-1 02/08/24 22:57
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.426 64.0 38.0-120
Acenaphthylene 0.666 0.473 71.0 40.0-120
Anthracene 0.666 0.457 68.6 42.0-120
Benzidine 1.33 0.725 54.5 10.0-120
Benzo(a)anthracene 0.666 0.502 75.4 44.0-120
Benzo(b)fluoranthene 0.666 0.479 71.9 43.0-120
Benzo(k)fluoranthene 0.666 0.469 70.4 44.0-120
Benzo(g,h,i)perylene 0.666 0.492 73.9 43.0-120
Benzo(a)pyrene 0.666 0.497 74.6 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.351 52.7 20.0-120
Bis(2-chloroethyl)ether 0.666 0.391 58.7 16.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2221334
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-02
Laboratory Control Sample (LCS)
(LCS) R4031845-1 02/08/24 22:57
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2,2-Oxybis(1-Chloropropane)0.666 0.420 63.1 23.0-120
4-Bromophenyl-phenylether 0.666 0.474 71.2 40.0-120
2-Chloronaphthalene 0.666 0.417 62.6 35.0-120
4-Chlorophenyl-phenylether 0.666 0.484 72.7 40.0-120
Chrysene 0.666 0.459 68.9 43.0-120
Dibenz(a,h)anthracene 0.666 0.513 77.0 44.0-120
1,2-Dichlorobenzene 0.666 0.393 59.0 32.0-120
1,3-Dichlorobenzene 0.666 0.384 57.7 30.0-120
1,4-Dichlorobenzene 0.666 0.403 60.5 31.0-120
3,3-Dichlorobenzidine 1.33 1.01 75.9 28.0-120
2,4-Dinitrotoluene 0.666 0.516 77.5 45.0-120
2,6-Dinitrotoluene 0.666 0.503 75.5 42.0-120
Fluoranthene 0.666 0.482 72.4 44.0-120
Fluorene 0.666 0.455 68.3 41.0-120
Hexachlorobenzene 0.666 0.481 72.2 39.0-120
Hexachloro-1,3-butadiene 0.666 0.338 50.8 15.0-120
Hexachlorocyclopentadiene 0.666 0.165 24.8 15.0-120
Hexachloroethane 0.666 0.382 57.4 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.540 81.1 45.0-120
Isophorone 0.666 0.390 58.6 23.0-120
Naphthalene 0.666 0.344 51.7 18.0-120
Nitrobenzene 0.666 0.357 53.6 17.0-120
n-Nitrosodimethylamine 0.666 0.363 54.5 10.0-125
n-Nitrosodiphenylamine 0.666 0.449 67.4 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.511 76.7 26.0-120
Phenanthrene 0.666 0.440 66.1 42.0-120
Benzylbutyl phthalate 0.666 0.558 83.8 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.540 81.1 41.0-120
Di-n-butyl phthalate 0.666 0.463 69.5 43.0-120
Diethyl phthalate 0.666 0.505 75.8 43.0-120
Dimethyl phthalate 0.666 0.506 76.0 43.0-120
Di-n-octyl phthalate 0.666 0.558 83.8 40.0-120
Pyrene 0.666 0.464 69.7 41.0-120
1,2,4-Trichlorobenzene 0.666 0.338 50.8 17.0-120
4-Chloro-3-methylphenol 0.666 0.383 57.5 28.0-120
2-Chlorophenol 0.666 0.427 64.1 28.0-120
2,4-Dichlorophenol 0.666 0.318 47.7 25.0-120
2,4-Dimethylphenol 0.666 0.309 46.4 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.446 67.0 16.0-120
2,4-Dinitrophenol 0.666 0.312 46.8 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2221334
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-02
Laboratory Control Sample (LCS)
(LCS) R4031845-1 02/08/24 22:57
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
2-Nitrophenol 0.666 0.370 55.6 20.0-120
4-Nitrophenol 0.666 0.491 73.7 27.0-120
Pentachlorophenol 0.666 0.372 55.9 29.0-120
Phenol 0.666 0.417 62.6 28.0-120
2,4,6-Trichlorophenol 0.666 0.401 60.2 37.0-120
(S) 2-Fluorophenol 73.0 12.0-120
(S) Phenol-d5 65.8 10.0-120
(S) Nitrobenzene-d5 58.3 10.0-122
(S) 2-Fluorobiphenyl 65.2 15.0-120
(S) 2,4,6-Tribromophenol 81.4 10.0-127
(S) p-Terphenyl-d14 74.8 10.0-120
L1701865-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1701865-06 02/09/24 04:52 • (MS) R4031845-3 02/09/24 05:17 • (MSD) R4031845-4 02/09/24 05:42
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Acenaphthene 0.798 U 0.343 0.445 42.9 55.8 1 18.0-120 26.1 32
Acenaphthylene 0.798 U 0.382 0.497 47.9 62.3 1 25.0-120 26.2 32
Anthracene 0.798 U 0.373 0.488 46.8 61.2 1 22.0-120 26.7 29
Benzidine 1.59 U 0.654 0.885 41.1 55.6 1 10.0-120 30.1 40
Benzo(a)anthracene 0.798 U 0.401 0.531 50.3 66.6 1 25.0-120 27.8 29
Benzo(b)fluoranthene 0.798 U 0.381 0.499 47.7 62.6 1 19.0-122 27.0 31
Benzo(k)fluoranthene 0.798 U 0.373 0.476 46.8 59.7 1 23.0-120 24.2 30
Benzo(g,h,i)perylene 0.798 U 0.400 0.515 50.2 64.6 1 10.0-120 25.1 33
Benzo(a)pyrene 0.798 U 0.398 0.515 49.8 64.6 1 24.0-120 25.7 30
Bis(2-chlorethoxy)methane 0.798 U 0.301 0.378 37.7 47.4 1 10.0-120 22.7 34
Bis(2-chloroethyl)ether 0.798 U 0.327 0.420 41.0 52.6 1 10.0-120 24.9 40
2,2-Oxybis(1-Chloropropane)0.798 U 0.332 0.421 41.6 52.8 1 10.0-120 23.7 40
4-Bromophenyl-phenylether 0.798 U 0.379 0.508 47.5 63.7 1 27.0-120 29.0 30
2-Chloronaphthalene 0.798 U 0.337 0.444 42.2 55.7 1 20.0-120 27.6 32
4-Chlorophenyl-phenylether 0.798 U 0.395 0.499 49.5 62.6 1 24.0-120 23.3 29
Chrysene 0.798 U 0.377 0.487 47.2 61.0 1 21.0-120 25.5 29
Dibenz(a,h)anthracene 0.798 U 0.421 0.535 52.8 67.0 1 10.0-120 23.8 32
1,2-Dichlorobenzene 0.798 U 0.317 0.401 39.7 50.3 1 10.0-120 23.5 38
1,3-Dichlorobenzene 0.798 U 0.301 0.389 37.7 48.8 1 10.0-120 25.5 40
1,4-Dichlorobenzene 0.798 U 0.322 0.410 40.3 51.4 1 10.0-120 24.1 39
3,3-Dichlorobenzidine 1.59 U 0.871 1.12 54.8 70.2 1 10.0-120 24.6 34
2,4-Dinitrotoluene 0.798 U 0.417 0.545 52.3 68.3 1 30.0-120 26.5 31
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2221334
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-02
L1701865-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1701865-06 02/09/24 04:52 • (MS) R4031845-3 02/09/24 05:17 • (MSD) R4031845-4 02/09/24 05:42
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
2,6-Dinitrotoluene 0.798 U 0.408 0.535 51.1 67.0 1 25.0-120 27.0 31
Fluoranthene 0.798 U 0.388 0.504 48.6 63.2 1 18.0-126 26.1 32
Fluorene 0.798 U 0.366 0.479 45.9 60.0 1 25.0-120 26.7 30
Hexachlorobenzene 0.798 U 0.368 0.496 46.2 62.1 1 27.0-120 J3 29.5 28
Hexachloro-1,3-butadiene 0.798 U 0.277 0.343 34.7 42.9 1 10.0-120 21.3 38
Hexachlorocyclopentadiene 0.798 U U U 0.000 0.000 1 10.0-120 J6 J6 0.000 40
Hexachloroethane 0.798 U 0.304 0.392 38.0 49.1 1 10.0-120 25.4 40
Indeno(1,2,3-cd)pyrene 0.798 U 0.439 0.568 55.1 71.2 1 10.0-120 25.5 32
Isophorone 0.798 U 0.340 0.415 42.6 52.0 1 13.0-120 19.8 34
Naphthalene 0.798 U 0.291 0.360 36.5 45.1 1 10.0-120 21.1 35
Nitrobenzene 0.798 U 0.304 0.371 38.0 46.5 1 10.0-120 20.0 36
n-Nitrosodimethylamine 0.798 U 0.306 0.375 38.3 46.9 1 10.0-127 20.1 40
n-Nitrosodiphenylamine 0.798 U 0.370 0.480 46.3 60.1 1 17.0-120 25.9 29
n-Nitrosodi-n-propylamine 0.798 U 0.426 0.536 53.4 67.2 1 10.0-120 22.9 37
Phenanthrene 0.798 U 0.359 0.461 44.9 57.8 1 17.0-120 25.1 31
Benzylbutyl phthalate 0.798 U 0.450 0.583 56.4 73.0 1 23.0-120 25.6 30
Bis(2-ethylhexyl)phthalate 0.798 U 0.432 0.562 54.1 70.4 1 17.0-126 26.1 30
Di-n-butyl phthalate 0.798 U 0.368 0.479 46.2 60.0 1 30.0-120 26.0 29
Diethyl phthalate 0.798 U 0.419 0.535 52.5 67.0 1 26.0-120 24.4 28
Dimethyl phthalate 0.798 U 0.416 0.541 52.1 67.8 1 25.0-120 26.1 29
Di-n-octyl phthalate 0.798 U 0.445 0.590 55.8 73.9 1 21.0-123 27.9 29
Pyrene 0.798 U 0.378 0.492 47.4 61.7 1 16.0-121 26.2 32
1,2,4-Trichlorobenzene 0.798 U 0.286 0.361 35.9 45.2 1 12.0-120 23.1 37
4-Chloro-3-methylphenol 0.798 U 0.333 0.410 41.7 51.4 1 15.0-120 20.8 30
2-Chlorophenol 0.798 U 0.357 0.438 44.8 54.9 1 15.0-120 20.3 37
2,4-Dichlorophenol 0.798 U 0.281 0.343 35.3 42.9 1 20.0-120 19.6 31
2,4-Dimethylphenol 0.798 U 0.272 0.334 34.0 41.9 1 10.0-120 20.6 33
4,6-Dinitro-2-methylphenol 0.798 U 0.434 0.523 54.4 65.5 1 10.0-120 18.4 39
2,4-Dinitrophenol 0.798 U 0.388 0.428 48.6 53.7 1 10.0-121 9.90 40
2-Nitrophenol 0.798 U 0.326 0.399 40.8 50.0 1 12.0-120 20.3 39
4-Nitrophenol 0.798 U 0.417 0.499 52.3 62.6 1 10.0-137 17.9 32
Pentachlorophenol 0.798 U 0.335 0.398 42.0 49.8 1 10.0-160 17.0 31
Phenol 0.798 U 0.356 0.437 44.6 54.8 1 12.0-120 20.4 38
2,4,6-Trichlorophenol 0.798 U 0.334 0.421 41.9 52.8 1 19.0-120 23.0 32
(S) 2-Fluorophenol 57.2 64.3 12.0-120
(S) Phenol-d5 52.5 58.4 10.0-120
(S) Nitrobenzene-d5 46.6 52.5 10.0-122
(S) 2-Fluorobiphenyl 50.0 58.9 15.0-120
(S) 2,4,6-Tribromophenol 63.7 74.4 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2221334
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1701794-02
L1701865-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1701865-06 02/09/24 04:52 • (MS) R4031845-3 02/09/24 05:17 • (MSD) R4031845-4 02/09/24 05:42
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
(S) p-Terphenyl-d14 58.9 67.8 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
C5 The reported concentration is an estimate. The continuing calibration standard associated with this data responded high.
Data is likely to show a high bias concerning the result.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Qualifier Description
Q Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be
considered minimum values.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ANALYTICAL REPORT
February 21, 2024
AECOM - Raleigh, NC
Sample Delivery Group:L1704882
Samples Received:02/13/2024
Project Number:60722767
Description:Frye and Webster DC410064
Site:DC410064
Report To:Stephanie Hempel
5438 Wade Park Blvd.
Suite 200
Raleigh, NC 27607
Entire Report Reviewed By:
February 21, 2024
[Preliminary Report]
Chris McCord
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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February 26, 2024
Chris McCord
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-1 L1704882-01 5
MW-3 L1704882-02 8
MW-2 L1704882-03 11
MW-4 L1704882-04 14
Qc: Quality Control Summary 17
Volatile Organic Compounds (GC/MS) by Method 8260D 17
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 22
Gl: Glossary of Terms 26
Al: Accreditations & Locations 27
Sc: Sample Chain of Custody 28
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L1704882-01 GW EM 02/09/24 10:20 02/13/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260D WG2226299 1 02/14/24 16:17 02/14/24 16:17 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2229263 25 02/20/24 01:16 02/20/24 01:16 DYW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2225388 1.06 02/13/24 16:51 02/15/24 19:09 ALM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1704882-02 GW EM 02/09/24 11:10 02/13/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260D WG2226299 1 02/14/24 16:36 02/14/24 16:36 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2229263 1 02/20/24 01:38 02/20/24 01:38 DYW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2225388 1 02/13/24 16:51 02/15/24 19:31 ALM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1704882-03 GW EM 02/09/24 11:55 02/13/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260D WG2226299 5 02/14/24 21:37 02/14/24 21:37 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2229263 250 02/20/24 01:59 02/20/24 01:59 DYW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2225388 1 02/13/24 16:51 02/15/24 19:53 ALM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4 L1704882-04 GW EM 02/09/24 12:45 02/13/24 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260D WG2226299 1 02/14/24 16:55 02/14/24 16:55 DYW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2229263 20 02/20/24 02:20 02/20/24 02:20 DYW Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2225388 1.05 02/13/24 16:51 02/15/24 20:37 ALM Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Chris McCord
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Chris McCord
Project Manager
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SAMPLE RESULTS - 01
L1704882
MW-1
Collected date/time: 02/09/24 10:20
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 11.3 50.0 1 02/14/2024 16:17 WG2226299
Acrolein U J4 2.54 50.0 1 02/14/2024 16:17 WG2226299
Acrylonitrile U C3 0.671 10.0 1 02/14/2024 16:17 WG2226299
Benzene 561 2.35 25.0 25 02/20/2024 01:16 WG2229263
Bromobenzene U 0.118 1.00 1 02/14/2024 16:17 WG2226299
Bromodichloromethane U 0.136 1.00 1 02/14/2024 16:17 WG2226299
Bromoform U 0.129 1.00 1 02/14/2024 16:17 WG2226299
Bromomethane U 0.605 5.00 1 02/14/2024 16:17 WG2226299
n-Butylbenzene U 0.157 1.00 1 02/14/2024 16:17 WG2226299
sec-Butylbenzene 0.867 J 0.125 1.00 1 02/14/2024 16:17 WG2226299
tert-Butylbenzene 0.464 J 0.127 1.00 1 02/14/2024 16:17 WG2226299
Carbon tetrachloride U 0.128 1.00 1 02/14/2024 16:17 WG2226299
Chlorobenzene U 0.116 1.00 1 02/14/2024 16:17 WG2226299
Chlorodibromomethane U 0.140 1.00 1 02/14/2024 16:17 WG2226299
Chloroethane U 0.192 5.00 1 02/14/2024 16:17 WG2226299
Chloroform U 0.111 5.00 1 02/14/2024 16:17 WG2226299
Chloromethane U C3 0.960 2.50 1 02/14/2024 16:17 WG2226299
2-Chlorotoluene U 0.106 1.00 1 02/14/2024 16:17 WG2226299
4-Chlorotoluene U 0.114 1.00 1 02/14/2024 16:17 WG2226299
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 02/14/2024 16:17 WG2226299
1,2-Dibromoethane U 0.126 1.00 1 02/14/2024 16:17 WG2226299
Dibromomethane U 0.122 1.00 1 02/14/2024 16:17 WG2226299
1,2-Dichlorobenzene U 0.107 1.00 1 02/14/2024 16:17 WG2226299
1,3-Dichlorobenzene U 0.110 1.00 1 02/14/2024 16:17 WG2226299
1,4-Dichlorobenzene U 0.120 1.00 1 02/14/2024 16:17 WG2226299
Dichlorodifluoromethane U 0.374 5.00 1 02/14/2024 16:17 WG2226299
1,1-Dichloroethane U 0.100 1.00 1 02/14/2024 16:17 WG2226299
1,2-Dichloroethane 3.22 0.0819 1.00 1 02/14/2024 16:17 WG2226299
1,1-Dichloroethene U 0.188 1.00 1 02/14/2024 16:17 WG2226299
cis-1,2-Dichloroethene U 0.126 1.00 1 02/14/2024 16:17 WG2226299
trans-1,2-Dichloroethene U 0.149 1.00 1 02/14/2024 16:17 WG2226299
1,2-Dichloropropane U C3 J4 0.149 1.00 1 02/14/2024 16:17 WG2226299
1,1-Dichloropropene U 0.142 1.00 1 02/14/2024 16:17 WG2226299
1,3-Dichloropropane U 0.110 1.00 1 02/14/2024 16:17 WG2226299
cis-1,3-Dichloropropene U 0.111 1.00 1 02/14/2024 16:17 WG2226299
trans-1,3-Dichloropropene U 0.118 1.00 1 02/14/2024 16:17 WG2226299
2,2-Dichloropropane U 0.161 1.00 1 02/14/2024 16:17 WG2226299
Di-isopropyl ether 10.4 C3 0.105 1.00 1 02/14/2024 16:17 WG2226299
Ethylbenzene U 0.137 1.00 1 02/14/2024 16:17 WG2226299
Hexachloro-1,3-butadiene U 0.337 1.00 1 02/14/2024 16:17 WG2226299
Isopropylbenzene 9.21 0.105 1.00 1 02/14/2024 16:17 WG2226299
p-Isopropyltoluene 0.248 J 0.120 1.00 1 02/14/2024 16:17 WG2226299
2-Butanone (MEK)U 1.19 10.0 1 02/14/2024 16:17 WG2226299
Methylene Chloride U 0.430 5.00 1 02/14/2024 16:17 WG2226299
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 02/14/2024 16:17 WG2226299
Methyl tert-butyl ether 11.4 0.101 1.00 1 02/14/2024 16:17 WG2226299
Naphthalene 14.7 1.00 5.00 1 02/14/2024 16:17 WG2226299
n-Propylbenzene 0.720 J 0.0993 1.00 1 02/14/2024 16:17 WG2226299
Styrene U 0.118 1.00 1 02/14/2024 16:17 WG2226299
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 02/14/2024 16:17 WG2226299
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 02/14/2024 16:17 WG2226299
1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 02/14/2024 16:17 WG2226299
Tetrachloroethene 1.60 0.300 1.00 1 02/14/2024 16:17 WG2226299
Toluene 0.382 J 0.278 1.00 1 02/14/2024 16:17 WG2226299
1,2,3-Trichlorobenzene U 0.230 1.00 1 02/14/2024 16:17 WG2226299
1,2,4-Trichlorobenzene U 0.481 1.00 1 02/14/2024 16:17 WG2226299
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1704882
MW-1
Collected date/time: 02/09/24 10:20
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1,1-Trichloroethane U 0.149 1.00 1 02/14/2024 16:17 WG2226299
1,1,2-Trichloroethane U 0.158 1.00 1 02/14/2024 16:17 WG2226299
Trichloroethene 0.214 J 0.190 1.00 1 02/14/2024 16:17 WG2226299
Trichlorofluoromethane U 0.160 5.00 1 02/14/2024 16:17 WG2226299
1,2,3-Trichloropropane U 0.237 2.50 1 02/14/2024 16:17 WG2226299
1,2,4-Trimethylbenzene U 0.322 1.00 1 02/14/2024 16:17 WG2226299
1,2,3-Trimethylbenzene U 0.104 1.00 1 02/14/2024 16:17 WG2226299
1,3,5-Trimethylbenzene U 0.104 1.00 1 02/14/2024 16:17 WG2226299
Vinyl chloride U 0.234 1.00 1 02/14/2024 16:17 WG2226299
Xylenes, Total U 0.174 3.00 1 02/14/2024 16:17 WG2226299
(S) Toluene-d8 102 80.0-120 02/14/2024 16:17 WG2226299
(S) Toluene-d8 93.0 80.0-120 02/20/2024 01:16 WG2229263
(S) 4-Bromofluorobenzene 95.9 77.0-126 02/14/2024 16:17 WG2226299
(S) 4-Bromofluorobenzene 107 77.0-126 02/20/2024 01:16 WG2229263
(S) 1,2-Dichloroethane-d4 100 70.0-130 02/14/2024 16:17 WG2226299
(S) 1,2-Dichloroethane-d4 92.6 70.0-130 02/20/2024 01:16 WG2229263
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0939 1.06 1.06 02/15/2024 19:09 WG2225388
Acenaphthylene U 0.0976 1.06 1.06 02/15/2024 19:09 WG2225388
Anthracene U 0.0852 1.06 1.06 02/15/2024 19:09 WG2225388
Benzidine 3.96 J J3 J4 3.96 10.6 1.06 02/15/2024 19:09 WG2225388
Benzo(a)anthracene U 0.211 1.06 1.06 02/15/2024 19:09 WG2225388
Benzo(b)fluoranthene U 0.138 1.06 1.06 02/15/2024 19:09 WG2225388
Benzo(k)fluoranthene U 0.127 1.06 1.06 02/15/2024 19:09 WG2225388
Benzo(g,h,i)perylene U 0.128 1.06 1.06 02/15/2024 19:09 WG2225388
Benzo(a)pyrene U 0.0404 1.06 1.06 02/15/2024 19:09 WG2225388
Bis(2-chlorethoxy)methane U 0.123 10.6 1.06 02/15/2024 19:09 WG2225388
Bis(2-chloroethyl)ether U 0.145 10.6 1.06 02/15/2024 19:09 WG2225388
2,2-Oxybis(1-Chloropropane)U 0.223 10.6 1.06 02/15/2024 19:09 WG2225388
4-Bromophenyl-phenylether U 0.0930 10.6 1.06 02/15/2024 19:09 WG2225388
2-Chloronaphthalene U 0.0687 1.06 1.06 02/15/2024 19:09 WG2225388
4-Chlorophenyl-phenylether U 0.0982 10.6 1.06 02/15/2024 19:09 WG2225388
Chrysene U 0.138 1.06 1.06 02/15/2024 19:09 WG2225388
Dibenz(a,h)anthracene U 0.0683 1.06 1.06 02/15/2024 19:09 WG2225388
1,2-Dichlorobenzene U 0.0756 10.6 1.06 02/15/2024 19:09 WG2225388
1,3-Dichlorobenzene U 0.140 10.6 1.06 02/15/2024 19:09 WG2225388
1,4-Dichlorobenzene U 0.0999 10.6 1.06 02/15/2024 19:09 WG2225388
3,3-Dichlorobenzidine U 0.225 10.6 1.06 02/15/2024 19:09 WG2225388
2,4-Dinitrotoluene U 0.104 10.6 1.06 02/15/2024 19:09 WG2225388
2,6-Dinitrotoluene U 0.265 10.6 1.06 02/15/2024 19:09 WG2225388
Fluoranthene U 0.108 1.06 1.06 02/15/2024 19:09 WG2225388
Fluorene 0.136 J 0.0895 1.06 1.06 02/15/2024 19:09 WG2225388
Hexachlorobenzene U 0.0800 1.06 1.06 02/15/2024 19:09 WG2225388
Hexachloro-1,3-butadiene U 0.103 10.6 1.06 02/15/2024 19:09 WG2225388
Hexachlorocyclopentadiene U 0.0634 10.6 1.06 02/15/2024 19:09 WG2225388
Hexachloroethane U 0.135 10.6 1.06 02/15/2024 19:09 WG2225388
Indeno(1,2,3-cd)pyrene U 0.296 1.06 1.06 02/15/2024 19:09 WG2225388
Isophorone U 0.152 10.6 1.06 02/15/2024 19:09 WG2225388
Naphthalene U 0.169 1.06 1.06 02/15/2024 19:09 WG2225388
Nitrobenzene U 0.315 10.6 1.06 02/15/2024 19:09 WG2225388
n-Nitrosodimethylamine U 1.06 10.6 1.06 02/15/2024 19:09 WG2225388
n-Nitrosodiphenylamine U 2.51 10.6 1.06 02/15/2024 19:09 WG2225388
n-Nitrosodi-n-propylamine U 0.277 10.6 1.06 02/15/2024 19:09 WG2225388
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1704882
MW-1
Collected date/time: 02/09/24 10:20
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Phenanthrene 0.268 J 0.119 1.06 1.06 02/15/2024 19:09 WG2225388
Benzylbutyl phthalate U 0.811 3.18 1.06 02/15/2024 19:09 WG2225388
Bis(2-ethylhexyl)phthalate U 0.949 3.18 1.06 02/15/2024 19:09 WG2225388
Di-n-butyl phthalate U 0.480 3.18 1.06 02/15/2024 19:09 WG2225388
Diethyl phthalate 0.435 J 0.304 3.18 1.06 02/15/2024 19:09 WG2225388
Dimethyl phthalate U 0.276 3.18 1.06 02/15/2024 19:09 WG2225388
Di-n-octyl phthalate U 0.988 3.18 1.06 02/15/2024 19:09 WG2225388
Pyrene U 0.113 1.06 1.06 02/15/2024 19:09 WG2225388
1,2,4-Trichlorobenzene U 0.0740 10.6 1.06 02/15/2024 19:09 WG2225388
4-Chloro-3-methylphenol U J4 0.139 10.6 1.06 02/15/2024 19:09 WG2225388
2-Chlorophenol U 0.141 10.6 1.06 02/15/2024 19:09 WG2225388
2,4-Dichlorophenol U 0.108 10.6 1.06 02/15/2024 19:09 WG2225388
2,4-Dimethylphenol U 0.0674 10.6 1.06 02/15/2024 19:09 WG2225388
4,6-Dinitro-2-methylphenol U 1.19 10.6 1.06 02/15/2024 19:09 WG2225388
2,4-Dinitrophenol U 6.29 10.6 1.06 02/15/2024 19:09 WG2225388
2-Nitrophenol U 0.124 10.6 1.06 02/15/2024 19:09 WG2225388
4-Nitrophenol U 0.152 10.6 1.06 02/15/2024 19:09 WG2225388
Pentachlorophenol U 0.332 10.6 1.06 02/15/2024 19:09 WG2225388
Phenol U 4.59 10.6 1.06 02/15/2024 19:09 WG2225388
2,4,6-Trichlorophenol U 0.106 10.6 1.06 02/15/2024 19:09 WG2225388
(S) 2-Fluorophenol 34.9 10.0-120 02/15/2024 19:09 WG2225388
(S) Phenol-d5 24.3 10.0-120 02/15/2024 19:09 WG2225388
(S) Nitrobenzene-d5 50.6 10.0-127 02/15/2024 19:09 WG2225388
(S) 2-Fluorobiphenyl 50.6 10.0-130 02/15/2024 19:09 WG2225388
(S) 2,4,6-Tribromophenol 56.8 10.0-155 02/15/2024 19:09 WG2225388
(S) p-Terphenyl-d14 59.1 10.0-128 02/15/2024 19:09 WG2225388
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 7 of 28
SAMPLE RESULTS - 02
L1704882
MW-3
Collected date/time: 02/09/24 11:10
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone 33.3 J 11.3 50.0 1 02/14/2024 16:36 WG2226299
Acrolein U J4 2.54 50.0 1 02/14/2024 16:36 WG2226299
Acrylonitrile U C3 0.671 10.0 1 02/14/2024 16:36 WG2226299
Benzene 2.30 0.0941 1.00 1 02/20/2024 01:38 WG2229263
Bromobenzene U 0.118 1.00 1 02/14/2024 16:36 WG2226299
Bromodichloromethane U 0.136 1.00 1 02/14/2024 16:36 WG2226299
Bromoform U 0.129 1.00 1 02/14/2024 16:36 WG2226299
Bromomethane U 0.605 5.00 1 02/14/2024 16:36 WG2226299
n-Butylbenzene U 0.157 1.00 1 02/14/2024 16:36 WG2226299
sec-Butylbenzene U 0.125 1.00 1 02/14/2024 16:36 WG2226299
tert-Butylbenzene U 0.127 1.00 1 02/14/2024 16:36 WG2226299
Carbon tetrachloride U 0.128 1.00 1 02/14/2024 16:36 WG2226299
Chlorobenzene U 0.116 1.00 1 02/14/2024 16:36 WG2226299
Chlorodibromomethane U 0.140 1.00 1 02/14/2024 16:36 WG2226299
Chloroethane U 0.192 5.00 1 02/14/2024 16:36 WG2226299
Chloroform U 0.111 5.00 1 02/14/2024 16:36 WG2226299
Chloromethane U C3 0.960 2.50 1 02/14/2024 16:36 WG2226299
2-Chlorotoluene U 0.106 1.00 1 02/14/2024 16:36 WG2226299
4-Chlorotoluene U 0.114 1.00 1 02/14/2024 16:36 WG2226299
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 02/14/2024 16:36 WG2226299
1,2-Dibromoethane U 0.126 1.00 1 02/14/2024 16:36 WG2226299
Dibromomethane U 0.122 1.00 1 02/14/2024 16:36 WG2226299
1,2-Dichlorobenzene U 0.107 1.00 1 02/14/2024 16:36 WG2226299
1,3-Dichlorobenzene U 0.110 1.00 1 02/14/2024 16:36 WG2226299
1,4-Dichlorobenzene U 0.120 1.00 1 02/14/2024 16:36 WG2226299
Dichlorodifluoromethane U 0.374 5.00 1 02/14/2024 16:36 WG2226299
1,1-Dichloroethane U 0.100 1.00 1 02/14/2024 16:36 WG2226299
1,2-Dichloroethane U 0.0819 1.00 1 02/14/2024 16:36 WG2226299
1,1-Dichloroethene U 0.188 1.00 1 02/14/2024 16:36 WG2226299
cis-1,2-Dichloroethene U 0.126 1.00 1 02/14/2024 16:36 WG2226299
trans-1,2-Dichloroethene U 0.149 1.00 1 02/14/2024 16:36 WG2226299
1,2-Dichloropropane U C3 J4 0.149 1.00 1 02/14/2024 16:36 WG2226299
1,1-Dichloropropene U 0.142 1.00 1 02/14/2024 16:36 WG2226299
1,3-Dichloropropane U 0.110 1.00 1 02/14/2024 16:36 WG2226299
cis-1,3-Dichloropropene U 0.111 1.00 1 02/14/2024 16:36 WG2226299
trans-1,3-Dichloropropene U 0.118 1.00 1 02/14/2024 16:36 WG2226299
2,2-Dichloropropane U 0.161 1.00 1 02/14/2024 16:36 WG2226299
Di-isopropyl ether U C3 0.105 1.00 1 02/14/2024 16:36 WG2226299
Ethylbenzene U 0.137 1.00 1 02/14/2024 16:36 WG2226299
Hexachloro-1,3-butadiene U 0.337 1.00 1 02/14/2024 16:36 WG2226299
Isopropylbenzene U 0.105 1.00 1 02/14/2024 16:36 WG2226299
p-Isopropyltoluene U 0.120 1.00 1 02/14/2024 16:36 WG2226299
2-Butanone (MEK)U 1.19 10.0 1 02/14/2024 16:36 WG2226299
Methylene Chloride U 0.430 5.00 1 02/14/2024 16:36 WG2226299
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 02/14/2024 16:36 WG2226299
Methyl tert-butyl ether U 0.101 1.00 1 02/14/2024 16:36 WG2226299
Naphthalene U 1.00 5.00 1 02/14/2024 16:36 WG2226299
n-Propylbenzene U 0.0993 1.00 1 02/14/2024 16:36 WG2226299
Styrene U 0.118 1.00 1 02/14/2024 16:36 WG2226299
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 02/14/2024 16:36 WG2226299
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 02/14/2024 16:36 WG2226299
1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 02/14/2024 16:36 WG2226299
Tetrachloroethene U 0.300 1.00 1 02/14/2024 16:36 WG2226299
Toluene U 0.278 1.00 1 02/14/2024 16:36 WG2226299
1,2,3-Trichlorobenzene U 0.230 1.00 1 02/14/2024 16:36 WG2226299
1,2,4-Trichlorobenzene U 0.481 1.00 1 02/14/2024 16:36 WG2226299
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 8 of 28
SAMPLE RESULTS - 02
L1704882
MW-3
Collected date/time: 02/09/24 11:10
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1,1-Trichloroethane U 0.149 1.00 1 02/14/2024 16:36 WG2226299
1,1,2-Trichloroethane U 0.158 1.00 1 02/14/2024 16:36 WG2226299
Trichloroethene U 0.190 1.00 1 02/14/2024 16:36 WG2226299
Trichlorofluoromethane U 0.160 5.00 1 02/14/2024 16:36 WG2226299
1,2,3-Trichloropropane U 0.237 2.50 1 02/14/2024 16:36 WG2226299
1,2,4-Trimethylbenzene U 0.322 1.00 1 02/14/2024 16:36 WG2226299
1,2,3-Trimethylbenzene U 0.104 1.00 1 02/14/2024 16:36 WG2226299
1,3,5-Trimethylbenzene U 0.104 1.00 1 02/14/2024 16:36 WG2226299
Vinyl chloride U 0.234 1.00 1 02/14/2024 16:36 WG2226299
Xylenes, Total U 0.174 3.00 1 02/14/2024 16:36 WG2226299
(S) Toluene-d8 104 80.0-120 02/14/2024 16:36 WG2226299
(S) Toluene-d8 95.5 80.0-120 02/20/2024 01:38 WG2229263
(S) 4-Bromofluorobenzene 95.9 77.0-126 02/14/2024 16:36 WG2226299
(S) 4-Bromofluorobenzene 105 77.0-126 02/20/2024 01:38 WG2229263
(S) 1,2-Dichloroethane-d4 97.1 70.0-130 02/14/2024 16:36 WG2226299
(S) 1,2-Dichloroethane-d4 95.2 70.0-130 02/20/2024 01:38 WG2229263
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.0886 1.00 1 02/15/2024 19:31 WG2225388
Acenaphthylene U 0.0921 1.00 1 02/15/2024 19:31 WG2225388
Anthracene U 0.0804 1.00 1 02/15/2024 19:31 WG2225388
Benzidine U J3 J4 3.74 10.0 1 02/15/2024 19:31 WG2225388
Benzo(a)anthracene U 0.199 1.00 1 02/15/2024 19:31 WG2225388
Benzo(b)fluoranthene U 0.130 1.00 1 02/15/2024 19:31 WG2225388
Benzo(k)fluoranthene U 0.120 1.00 1 02/15/2024 19:31 WG2225388
Benzo(g,h,i)perylene U 0.121 1.00 1 02/15/2024 19:31 WG2225388
Benzo(a)pyrene U 0.0381 1.00 1 02/15/2024 19:31 WG2225388
Bis(2-chlorethoxy)methane U 0.116 10.0 1 02/15/2024 19:31 WG2225388
Bis(2-chloroethyl)ether U 0.137 10.0 1 02/15/2024 19:31 WG2225388
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 02/15/2024 19:31 WG2225388
4-Bromophenyl-phenylether U 0.0877 10.0 1 02/15/2024 19:31 WG2225388
2-Chloronaphthalene U 0.0648 1.00 1 02/15/2024 19:31 WG2225388
4-Chlorophenyl-phenylether U 0.0926 10.0 1 02/15/2024 19:31 WG2225388
Chrysene U 0.130 1.00 1 02/15/2024 19:31 WG2225388
Dibenz(a,h)anthracene U 0.0644 1.00 1 02/15/2024 19:31 WG2225388
1,2-Dichlorobenzene U 0.0713 10.0 1 02/15/2024 19:31 WG2225388
1,3-Dichlorobenzene U 0.132 10.0 1 02/15/2024 19:31 WG2225388
1,4-Dichlorobenzene U 0.0942 10.0 1 02/15/2024 19:31 WG2225388
3,3-Dichlorobenzidine U 0.212 10.0 1 02/15/2024 19:31 WG2225388
2,4-Dinitrotoluene U 0.0983 10.0 1 02/15/2024 19:31 WG2225388
2,6-Dinitrotoluene U 0.250 10.0 1 02/15/2024 19:31 WG2225388
Fluoranthene U 0.102 1.00 1 02/15/2024 19:31 WG2225388
Fluorene U 0.0844 1.00 1 02/15/2024 19:31 WG2225388
Hexachlorobenzene U 0.0755 1.00 1 02/15/2024 19:31 WG2225388
Hexachloro-1,3-butadiene U 0.0968 10.0 1 02/15/2024 19:31 WG2225388
Hexachlorocyclopentadiene U 0.0598 10.0 1 02/15/2024 19:31 WG2225388
Hexachloroethane U 0.127 10.0 1 02/15/2024 19:31 WG2225388
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 02/15/2024 19:31 WG2225388
Isophorone U 0.143 10.0 1 02/15/2024 19:31 WG2225388
Naphthalene U 0.159 1.00 1 02/15/2024 19:31 WG2225388
Nitrobenzene U 0.297 10.0 1 02/15/2024 19:31 WG2225388
n-Nitrosodimethylamine U 0.998 10.0 1 02/15/2024 19:31 WG2225388
n-Nitrosodiphenylamine U 2.37 10.0 1 02/15/2024 19:31 WG2225388
n-Nitrosodi-n-propylamine U 0.261 10.0 1 02/15/2024 19:31 WG2225388
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/21/24 11:14 9 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 9 of 28
SAMPLE RESULTS - 02
L1704882
MW-3
Collected date/time: 02/09/24 11:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Phenanthrene U 0.112 1.00 1 02/15/2024 19:31 WG2225388
Benzylbutyl phthalate U 0.765 3.00 1 02/15/2024 19:31 WG2225388
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 02/15/2024 19:31 WG2225388
Di-n-butyl phthalate U 0.453 3.00 1 02/15/2024 19:31 WG2225388
Diethyl phthalate U 0.287 3.00 1 02/15/2024 19:31 WG2225388
Dimethyl phthalate U 0.260 3.00 1 02/15/2024 19:31 WG2225388
Di-n-octyl phthalate U 0.932 3.00 1 02/15/2024 19:31 WG2225388
Pyrene U 0.107 1.00 1 02/15/2024 19:31 WG2225388
1,2,4-Trichlorobenzene U 0.0698 10.0 1 02/15/2024 19:31 WG2225388
4-Chloro-3-methylphenol U J4 0.131 10.0 1 02/15/2024 19:31 WG2225388
2-Chlorophenol U 0.133 10.0 1 02/15/2024 19:31 WG2225388
2,4-Dichlorophenol U 0.102 10.0 1 02/15/2024 19:31 WG2225388
2,4-Dimethylphenol U 0.0636 10.0 1 02/15/2024 19:31 WG2225388
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 02/15/2024 19:31 WG2225388
2,4-Dinitrophenol U 5.93 10.0 1 02/15/2024 19:31 WG2225388
2-Nitrophenol U 0.117 10.0 1 02/15/2024 19:31 WG2225388
4-Nitrophenol U 0.143 10.0 1 02/15/2024 19:31 WG2225388
Pentachlorophenol U 0.313 10.0 1 02/15/2024 19:31 WG2225388
Phenol U 4.33 10.0 1 02/15/2024 19:31 WG2225388
2,4,6-Trichlorophenol U 0.100 10.0 1 02/15/2024 19:31 WG2225388
(S) 2-Fluorophenol 23.7 10.0-120 02/15/2024 19:31 WG2225388
(S) Phenol-d5 16.2 10.0-120 02/15/2024 19:31 WG2225388
(S) Nitrobenzene-d5 50.1 10.0-127 02/15/2024 19:31 WG2225388
(S) 2-Fluorobiphenyl 50.5 10.0-130 02/15/2024 19:31 WG2225388
(S) 2,4,6-Tribromophenol 37.1 10.0-155 02/15/2024 19:31 WG2225388
(S) p-Terphenyl-d14 42.7 10.0-128 02/15/2024 19:31 WG2225388
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/21/24 11:14 10 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 10 of 28
SAMPLE RESULTS - 03
L1704882
MW-2
Collected date/time: 02/09/24 11:55
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone 67.9 J 56.5 250 5 02/14/2024 21:37 WG2226299
Acrolein U J4 12.7 250 5 02/14/2024 21:37 WG2226299
Acrylonitrile U C3 3.36 50.0 5 02/14/2024 21:37 WG2226299
Benzene 5700 23.5 250 250 02/20/2024 01:59 WG2229263
Bromobenzene U 0.590 5.00 5 02/14/2024 21:37 WG2226299
Bromodichloromethane U 0.680 5.00 5 02/14/2024 21:37 WG2226299
Bromoform U 0.645 5.00 5 02/14/2024 21:37 WG2226299
Bromomethane U 3.03 25.0 5 02/14/2024 21:37 WG2226299
n-Butylbenzene 3.40 J 0.785 5.00 5 02/14/2024 21:37 WG2226299
sec-Butylbenzene 2.76 J 0.625 5.00 5 02/14/2024 21:37 WG2226299
tert-Butylbenzene 0.665 J 0.635 5.00 5 02/14/2024 21:37 WG2226299
Carbon tetrachloride U 0.640 5.00 5 02/14/2024 21:37 WG2226299
Chlorobenzene 10.6 0.580 5.00 5 02/14/2024 21:37 WG2226299
Chlorodibromomethane U 0.700 5.00 5 02/14/2024 21:37 WG2226299
Chloroethane U 0.960 25.0 5 02/14/2024 21:37 WG2226299
Chloroform 19.5 J 0.555 25.0 5 02/14/2024 21:37 WG2226299
Chloromethane U C3 4.80 12.5 5 02/14/2024 21:37 WG2226299
2-Chlorotoluene U 0.530 5.00 5 02/14/2024 21:37 WG2226299
4-Chlorotoluene U 0.570 5.00 5 02/14/2024 21:37 WG2226299
1,2-Dibromo-3-Chloropropane U 1.38 25.0 5 02/14/2024 21:37 WG2226299
1,2-Dibromoethane U 0.630 5.00 5 02/14/2024 21:37 WG2226299
Dibromomethane U 0.610 5.00 5 02/14/2024 21:37 WG2226299
1,2-Dichlorobenzene U 0.535 5.00 5 02/14/2024 21:37 WG2226299
1,3-Dichlorobenzene U 0.550 5.00 5 02/14/2024 21:37 WG2226299
1,4-Dichlorobenzene 1.49 J 0.600 5.00 5 02/14/2024 21:37 WG2226299
Dichlorodifluoromethane U 1.87 25.0 5 02/14/2024 21:37 WG2226299
1,1-Dichloroethane U 0.500 5.00 5 02/14/2024 21:37 WG2226299
1,2-Dichloroethane 73.5 0.409 5.00 5 02/14/2024 21:37 WG2226299
1,1-Dichloroethene U 0.940 5.00 5 02/14/2024 21:37 WG2226299
cis-1,2-Dichloroethene 3.61 J 0.630 5.00 5 02/14/2024 21:37 WG2226299
trans-1,2-Dichloroethene U 0.745 5.00 5 02/14/2024 21:37 WG2226299
1,2-Dichloropropane 4.92 C3 J J4 0.745 5.00 5 02/14/2024 21:37 WG2226299
1,1-Dichloropropene U 0.710 5.00 5 02/14/2024 21:37 WG2226299
1,3-Dichloropropane U 0.550 5.00 5 02/14/2024 21:37 WG2226299
cis-1,3-Dichloropropene U 0.555 5.00 5 02/14/2024 21:37 WG2226299
trans-1,3-Dichloropropene U 0.590 5.00 5 02/14/2024 21:37 WG2226299
2,2-Dichloropropane U 0.805 5.00 5 02/14/2024 21:37 WG2226299
Di-isopropyl ether 301 C3 0.525 5.00 5 02/14/2024 21:37 WG2226299
Ethylbenzene 170 0.685 5.00 5 02/14/2024 21:37 WG2226299
Hexachloro-1,3-butadiene U 1.69 5.00 5 02/14/2024 21:37 WG2226299
Isopropylbenzene 26.8 0.525 5.00 5 02/14/2024 21:37 WG2226299
p-Isopropyltoluene 3.41 J 0.600 5.00 5 02/14/2024 21:37 WG2226299
2-Butanone (MEK)8.70 J 5.95 50.0 5 02/14/2024 21:37 WG2226299
Methylene Chloride 2.32 J 2.15 25.0 5 02/14/2024 21:37 WG2226299
4-Methyl-2-pentanone (MIBK)U 2.39 50.0 5 02/14/2024 21:37 WG2226299
Methyl tert-butyl ether 4620 25.3 250 250 02/20/2024 01:59 WG2229263
Naphthalene 26.6 5.00 25.0 5 02/14/2024 21:37 WG2226299
n-Propylbenzene 36.8 0.497 5.00 5 02/14/2024 21:37 WG2226299
Styrene 3.87 J 0.590 5.00 5 02/14/2024 21:37 WG2226299
1,1,1,2-Tetrachloroethane U 0.735 5.00 5 02/14/2024 21:37 WG2226299
1,1,2,2-Tetrachloroethane U 0.665 5.00 5 02/14/2024 21:37 WG2226299
1,1,2-Trichlorotrifluoroethane U 0.900 5.00 5 02/14/2024 21:37 WG2226299
Tetrachloroethene U 1.50 5.00 5 02/14/2024 21:37 WG2226299
Toluene 55.1 1.39 5.00 5 02/14/2024 21:37 WG2226299
1,2,3-Trichlorobenzene U 1.15 5.00 5 02/14/2024 21:37 WG2226299
1,2,4-Trichlorobenzene U 2.41 5.00 5 02/14/2024 21:37 WG2226299
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/21/24 11:14 11 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 11 of 28
SAMPLE RESULTS - 03
L1704882
MW-2
Collected date/time: 02/09/24 11:55
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1,1-Trichloroethane U 0.745 5.00 5 02/14/2024 21:37 WG2226299
1,1,2-Trichloroethane 1.44 J 0.790 5.00 5 02/14/2024 21:37 WG2226299
Trichloroethene 4.35 J 0.950 5.00 5 02/14/2024 21:37 WG2226299
Trichlorofluoromethane U 0.800 25.0 5 02/14/2024 21:37 WG2226299
1,2,3-Trichloropropane U 1.19 12.5 5 02/14/2024 21:37 WG2226299
1,2,4-Trimethylbenzene 98.3 1.61 5.00 5 02/14/2024 21:37 WG2226299
1,2,3-Trimethylbenzene 5.96 0.520 5.00 5 02/14/2024 21:37 WG2226299
1,3,5-Trimethylbenzene 21.2 0.520 5.00 5 02/14/2024 21:37 WG2226299
Vinyl chloride U 1.17 5.00 5 02/14/2024 21:37 WG2226299
Xylenes, Total 129 0.870 15.0 5 02/14/2024 21:37 WG2226299
(S) Toluene-d8 100 80.0-120 02/14/2024 21:37 WG2226299
(S) Toluene-d8 93.3 80.0-120 02/20/2024 01:59 WG2229263
(S) 4-Bromofluorobenzene 97.4 77.0-126 02/14/2024 21:37 WG2226299
(S) 4-Bromofluorobenzene 103 77.0-126 02/20/2024 01:59 WG2229263
(S) 1,2-Dichloroethane-d4 106 70.0-130 02/14/2024 21:37 WG2226299
(S) 1,2-Dichloroethane-d4 94.3 70.0-130 02/20/2024 01:59 WG2229263
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene 0.0937 J 0.0886 1.00 1 02/15/2024 19:53 WG2225388
Acenaphthylene U 0.0921 1.00 1 02/15/2024 19:53 WG2225388
Anthracene U 0.0804 1.00 1 02/15/2024 19:53 WG2225388
Benzidine U J3 J4 3.74 10.0 1 02/15/2024 19:53 WG2225388
Benzo(a)anthracene 0.214 J 0.199 1.00 1 02/15/2024 19:53 WG2225388
Benzo(b)fluoranthene 0.191 J 0.130 1.00 1 02/15/2024 19:53 WG2225388
Benzo(k)fluoranthene 0.265 J 0.120 1.00 1 02/15/2024 19:53 WG2225388
Benzo(g,h,i)perylene 0.254 J 0.121 1.00 1 02/15/2024 19:53 WG2225388
Benzo(a)pyrene 0.120 J 0.0381 1.00 1 02/15/2024 19:53 WG2225388
Bis(2-chlorethoxy)methane U 0.116 10.0 1 02/15/2024 19:53 WG2225388
Bis(2-chloroethyl)ether U 0.137 10.0 1 02/15/2024 19:53 WG2225388
2,2-Oxybis(1-Chloropropane)U 0.210 10.0 1 02/15/2024 19:53 WG2225388
4-Bromophenyl-phenylether U 0.0877 10.0 1 02/15/2024 19:53 WG2225388
2-Chloronaphthalene U 0.0648 1.00 1 02/15/2024 19:53 WG2225388
4-Chlorophenyl-phenylether U 0.0926 10.0 1 02/15/2024 19:53 WG2225388
Chrysene 0.217 J 0.130 1.00 1 02/15/2024 19:53 WG2225388
Dibenz(a,h)anthracene 0.303 B J 0.0644 1.00 1 02/15/2024 19:53 WG2225388
1,2-Dichlorobenzene U 0.0713 10.0 1 02/15/2024 19:53 WG2225388
1,3-Dichlorobenzene U 0.132 10.0 1 02/15/2024 19:53 WG2225388
1,4-Dichlorobenzene 1.06 J 0.0942 10.0 1 02/15/2024 19:53 WG2225388
3,3-Dichlorobenzidine U 0.212 10.0 1 02/15/2024 19:53 WG2225388
2,4-Dinitrotoluene U 0.0983 10.0 1 02/15/2024 19:53 WG2225388
2,6-Dinitrotoluene U 0.250 10.0 1 02/15/2024 19:53 WG2225388
Fluoranthene 0.105 J 0.102 1.00 1 02/15/2024 19:53 WG2225388
Fluorene 0.177 J 0.0844 1.00 1 02/15/2024 19:53 WG2225388
Hexachlorobenzene U 0.0755 1.00 1 02/15/2024 19:53 WG2225388
Hexachloro-1,3-butadiene U 0.0968 10.0 1 02/15/2024 19:53 WG2225388
Hexachlorocyclopentadiene U 0.0598 10.0 1 02/15/2024 19:53 WG2225388
Hexachloroethane U 0.127 10.0 1 02/15/2024 19:53 WG2225388
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 02/15/2024 19:53 WG2225388
Isophorone U 0.143 10.0 1 02/15/2024 19:53 WG2225388
Naphthalene 5.15 0.159 1.00 1 02/15/2024 19:53 WG2225388
Nitrobenzene U 0.297 10.0 1 02/15/2024 19:53 WG2225388
n-Nitrosodimethylamine U 0.998 10.0 1 02/15/2024 19:53 WG2225388
n-Nitrosodiphenylamine U 2.37 10.0 1 02/15/2024 19:53 WG2225388
n-Nitrosodi-n-propylamine U 0.261 10.0 1 02/15/2024 19:53 WG2225388
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/21/24 11:14 12 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 12 of 28
SAMPLE RESULTS - 03
L1704882
MW-2
Collected date/time: 02/09/24 11:55
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Phenanthrene 0.155 J 0.112 1.00 1 02/15/2024 19:53 WG2225388
Benzylbutyl phthalate U 0.765 3.00 1 02/15/2024 19:53 WG2225388
Bis(2-ethylhexyl)phthalate U 0.895 3.00 1 02/15/2024 19:53 WG2225388
Di-n-butyl phthalate U 0.453 3.00 1 02/15/2024 19:53 WG2225388
Diethyl phthalate 0.313 J 0.287 3.00 1 02/15/2024 19:53 WG2225388
Dimethyl phthalate U 0.260 3.00 1 02/15/2024 19:53 WG2225388
Di-n-octyl phthalate U 0.932 3.00 1 02/15/2024 19:53 WG2225388
Pyrene U 0.107 1.00 1 02/15/2024 19:53 WG2225388
1,2,4-Trichlorobenzene U 0.0698 10.0 1 02/15/2024 19:53 WG2225388
4-Chloro-3-methylphenol U J4 0.131 10.0 1 02/15/2024 19:53 WG2225388
2-Chlorophenol U 0.133 10.0 1 02/15/2024 19:53 WG2225388
2,4-Dichlorophenol U 0.102 10.0 1 02/15/2024 19:53 WG2225388
2,4-Dimethylphenol 1.09 J 0.0636 10.0 1 02/15/2024 19:53 WG2225388
4,6-Dinitro-2-methylphenol U 1.12 10.0 1 02/15/2024 19:53 WG2225388
2,4-Dinitrophenol U 5.93 10.0 1 02/15/2024 19:53 WG2225388
2-Nitrophenol U 0.117 10.0 1 02/15/2024 19:53 WG2225388
4-Nitrophenol U 0.143 10.0 1 02/15/2024 19:53 WG2225388
Pentachlorophenol U 0.313 10.0 1 02/15/2024 19:53 WG2225388
Phenol 11.7 4.33 10.0 1 02/15/2024 19:53 WG2225388
2,4,6-Trichlorophenol U 0.100 10.0 1 02/15/2024 19:53 WG2225388
(S) 2-Fluorophenol 0.000 J2 10.0-120 02/15/2024 19:53 WG2225388
(S) Phenol-d5 0.000 J2 10.0-120 02/15/2024 19:53 WG2225388
(S) Nitrobenzene-d5 74.4 10.0-127 02/15/2024 19:53 WG2225388
(S) 2-Fluorobiphenyl 55.6 10.0-130 02/15/2024 19:53 WG2225388
(S) 2,4,6-Tribromophenol 42.4 10.0-155 02/15/2024 19:53 WG2225388
(S) p-Terphenyl-d14 45.9 10.0-128 02/15/2024 19:53 WG2225388
Sample Narrative:
L1704882-03 WG2225388: Surrogate failure due to matrix interference
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/21/24 11:14 13 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 13 of 28
SAMPLE RESULTS - 04
L1704882
MW-4
Collected date/time: 02/09/24 12:45
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone 17.0 J 11.3 50.0 1 02/14/2024 16:55 WG2226299
Acrolein U J4 2.54 50.0 1 02/14/2024 16:55 WG2226299
Acrylonitrile U C3 0.671 10.0 1 02/14/2024 16:55 WG2226299
Benzene 17.1 0.0941 1.00 1 02/14/2024 16:55 WG2226299
Bromobenzene U 0.118 1.00 1 02/14/2024 16:55 WG2226299
Bromodichloromethane U 0.136 1.00 1 02/14/2024 16:55 WG2226299
Bromoform U 0.129 1.00 1 02/14/2024 16:55 WG2226299
Bromomethane U 0.605 5.00 1 02/14/2024 16:55 WG2226299
n-Butylbenzene U 0.157 1.00 1 02/14/2024 16:55 WG2226299
sec-Butylbenzene 0.410 J 0.125 1.00 1 02/14/2024 16:55 WG2226299
tert-Butylbenzene 0.219 J 0.127 1.00 1 02/14/2024 16:55 WG2226299
Carbon tetrachloride U 0.128 1.00 1 02/14/2024 16:55 WG2226299
Chlorobenzene U 0.116 1.00 1 02/14/2024 16:55 WG2226299
Chlorodibromomethane U 0.140 1.00 1 02/14/2024 16:55 WG2226299
Chloroethane U 0.192 5.00 1 02/14/2024 16:55 WG2226299
Chloroform U 0.111 5.00 1 02/14/2024 16:55 WG2226299
Chloromethane U C3 0.960 2.50 1 02/14/2024 16:55 WG2226299
2-Chlorotoluene U 0.106 1.00 1 02/14/2024 16:55 WG2226299
4-Chlorotoluene U 0.114 1.00 1 02/14/2024 16:55 WG2226299
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 02/14/2024 16:55 WG2226299
1,2-Dibromoethane U 0.126 1.00 1 02/14/2024 16:55 WG2226299
Dibromomethane U 0.122 1.00 1 02/14/2024 16:55 WG2226299
1,2-Dichlorobenzene U 0.107 1.00 1 02/14/2024 16:55 WG2226299
1,3-Dichlorobenzene U 0.110 1.00 1 02/14/2024 16:55 WG2226299
1,4-Dichlorobenzene U 0.120 1.00 1 02/14/2024 16:55 WG2226299
Dichlorodifluoromethane U 0.374 5.00 1 02/14/2024 16:55 WG2226299
1,1-Dichloroethane U 0.100 1.00 1 02/14/2024 16:55 WG2226299
1,2-Dichloroethane U 0.0819 1.00 1 02/14/2024 16:55 WG2226299
1,1-Dichloroethene 0.270 J 0.188 1.00 1 02/14/2024 16:55 WG2226299
cis-1,2-Dichloroethene 351 2.52 20.0 20 02/20/2024 02:20 WG2229263
trans-1,2-Dichloroethene 15.6 0.149 1.00 1 02/14/2024 16:55 WG2226299
1,2-Dichloropropane U C3 J4 0.149 1.00 1 02/14/2024 16:55 WG2226299
1,1-Dichloropropene U 0.142 1.00 1 02/14/2024 16:55 WG2226299
1,3-Dichloropropane U 0.110 1.00 1 02/14/2024 16:55 WG2226299
cis-1,3-Dichloropropene U 0.111 1.00 1 02/14/2024 16:55 WG2226299
trans-1,3-Dichloropropene U 0.118 1.00 1 02/14/2024 16:55 WG2226299
2,2-Dichloropropane U 0.161 1.00 1 02/14/2024 16:55 WG2226299
Di-isopropyl ether 0.244 C3 J 0.105 1.00 1 02/14/2024 16:55 WG2226299
Ethylbenzene 0.929 J 0.137 1.00 1 02/14/2024 16:55 WG2226299
Hexachloro-1,3-butadiene U 0.337 1.00 1 02/14/2024 16:55 WG2226299
Isopropylbenzene 0.431 J 0.105 1.00 1 02/14/2024 16:55 WG2226299
p-Isopropyltoluene 0.316 J 0.120 1.00 1 02/14/2024 16:55 WG2226299
2-Butanone (MEK)2.68 J 1.19 10.0 1 02/14/2024 16:55 WG2226299
Methylene Chloride U 0.430 5.00 1 02/14/2024 16:55 WG2226299
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 02/14/2024 16:55 WG2226299
Methyl tert-butyl ether 1.37 0.101 1.00 1 02/14/2024 16:55 WG2226299
Naphthalene U 1.00 5.00 1 02/14/2024 16:55 WG2226299
n-Propylbenzene 0.362 J 0.0993 1.00 1 02/14/2024 16:55 WG2226299
Styrene U 0.118 1.00 1 02/14/2024 16:55 WG2226299
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 02/14/2024 16:55 WG2226299
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 02/14/2024 16:55 WG2226299
1,1,2-Trichlorotrifluoroethane U 0.180 1.00 1 02/14/2024 16:55 WG2226299
Tetrachloroethene 63.3 0.300 1.00 1 02/14/2024 16:55 WG2226299
Toluene 0.413 J 0.278 1.00 1 02/14/2024 16:55 WG2226299
1,2,3-Trichlorobenzene U 0.230 1.00 1 02/14/2024 16:55 WG2226299
1,2,4-Trichlorobenzene U 0.481 1.00 1 02/14/2024 16:55 WG2226299
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/21/24 11:14 14 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 14 of 28
SAMPLE RESULTS - 04
L1704882
MW-4
Collected date/time: 02/09/24 12:45
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1,1-Trichloroethane U 0.149 1.00 1 02/14/2024 16:55 WG2226299
1,1,2-Trichloroethane U 0.158 1.00 1 02/14/2024 16:55 WG2226299
Trichloroethene 52.6 0.190 1.00 1 02/14/2024 16:55 WG2226299
Trichlorofluoromethane U 0.160 5.00 1 02/14/2024 16:55 WG2226299
1,2,3-Trichloropropane U 0.237 2.50 1 02/14/2024 16:55 WG2226299
1,2,4-Trimethylbenzene 2.92 0.322 1.00 1 02/14/2024 16:55 WG2226299
1,2,3-Trimethylbenzene 1.21 0.104 1.00 1 02/14/2024 16:55 WG2226299
1,3,5-Trimethylbenzene 0.812 J 0.104 1.00 1 02/14/2024 16:55 WG2226299
Vinyl chloride 1.15 0.234 1.00 1 02/14/2024 16:55 WG2226299
Xylenes, Total 0.963 J 0.174 3.00 1 02/14/2024 16:55 WG2226299
(S) Toluene-d8 103 80.0-120 02/14/2024 16:55 WG2226299
(S) Toluene-d8 92.8 80.0-120 02/20/2024 02:20 WG2229263
(S) 4-Bromofluorobenzene 97.8 77.0-126 02/14/2024 16:55 WG2226299
(S) 4-Bromofluorobenzene 105 77.0-126 02/20/2024 02:20 WG2229263
(S) 1,2-Dichloroethane-d4 96.7 70.0-130 02/14/2024 16:55 WG2226299
(S) 1,2-Dichloroethane-d4 97.0 70.0-130 02/20/2024 02:20 WG2229263
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene 0.0940 J 0.0930 1.05 1.05 02/15/2024 20:37 WG2225388
Acenaphthylene U 0.0967 1.05 1.05 02/15/2024 20:37 WG2225388
Anthracene U 0.0844 1.05 1.05 02/15/2024 20:37 WG2225388
Benzidine U J3 J4 3.93 10.5 1.05 02/15/2024 20:37 WG2225388
Benzo(a)anthracene U 0.209 1.05 1.05 02/15/2024 20:37 WG2225388
Benzo(b)fluoranthene U 0.136 1.05 1.05 02/15/2024 20:37 WG2225388
Benzo(k)fluoranthene U 0.126 1.05 1.05 02/15/2024 20:37 WG2225388
Benzo(g,h,i)perylene U 0.127 1.05 1.05 02/15/2024 20:37 WG2225388
Benzo(a)pyrene 0.0471 J 0.0400 1.05 1.05 02/15/2024 20:37 WG2225388
Bis(2-chlorethoxy)methane U 0.122 10.5 1.05 02/15/2024 20:37 WG2225388
Bis(2-chloroethyl)ether U 0.144 10.5 1.05 02/15/2024 20:37 WG2225388
2,2-Oxybis(1-Chloropropane)U 0.221 10.5 1.05 02/15/2024 20:37 WG2225388
4-Bromophenyl-phenylether U 0.0921 10.5 1.05 02/15/2024 20:37 WG2225388
2-Chloronaphthalene U 0.0680 1.05 1.05 02/15/2024 20:37 WG2225388
4-Chlorophenyl-phenylether U 0.0972 10.5 1.05 02/15/2024 20:37 WG2225388
Chrysene U 0.136 1.05 1.05 02/15/2024 20:37 WG2225388
Dibenz(a,h)anthracene 0.0819 B J 0.0676 1.05 1.05 02/15/2024 20:37 WG2225388
1,2-Dichlorobenzene U 0.0749 10.5 1.05 02/15/2024 20:37 WG2225388
1,3-Dichlorobenzene U 0.139 10.5 1.05 02/15/2024 20:37 WG2225388
1,4-Dichlorobenzene U 0.0989 10.5 1.05 02/15/2024 20:37 WG2225388
3,3-Dichlorobenzidine U 0.223 10.5 1.05 02/15/2024 20:37 WG2225388
2,4-Dinitrotoluene U 0.103 10.5 1.05 02/15/2024 20:37 WG2225388
2,6-Dinitrotoluene U 0.263 10.5 1.05 02/15/2024 20:37 WG2225388
Fluoranthene U 0.107 1.05 1.05 02/15/2024 20:37 WG2225388
Fluorene 0.146 J 0.0886 1.05 1.05 02/15/2024 20:37 WG2225388
Hexachlorobenzene U 0.0793 1.05 1.05 02/15/2024 20:37 WG2225388
Hexachloro-1,3-butadiene U 0.102 10.5 1.05 02/15/2024 20:37 WG2225388
Hexachlorocyclopentadiene U 0.0628 10.5 1.05 02/15/2024 20:37 WG2225388
Hexachloroethane U 0.133 10.5 1.05 02/15/2024 20:37 WG2225388
Indeno(1,2,3-cd)pyrene U 0.293 1.05 1.05 02/15/2024 20:37 WG2225388
Isophorone U 0.150 10.5 1.05 02/15/2024 20:37 WG2225388
Naphthalene 0.306 J 0.167 1.05 1.05 02/15/2024 20:37 WG2225388
Nitrobenzene U 0.312 10.5 1.05 02/15/2024 20:37 WG2225388
n-Nitrosodimethylamine U 1.05 10.5 1.05 02/15/2024 20:37 WG2225388
n-Nitrosodiphenylamine U 2.49 10.5 1.05 02/15/2024 20:37 WG2225388
n-Nitrosodi-n-propylamine U 0.274 10.5 1.05 02/15/2024 20:37 WG2225388
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/21/24 11:14 15 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 15 of 28
SAMPLE RESULTS - 04
L1704882
MW-4
Collected date/time: 02/09/24 12:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Phenanthrene U 0.118 1.05 1.05 02/15/2024 20:37 WG2225388
Benzylbutyl phthalate U 0.803 3.15 1.05 02/15/2024 20:37 WG2225388
Bis(2-ethylhexyl)phthalate U 0.940 3.15 1.05 02/15/2024 20:37 WG2225388
Di-n-butyl phthalate U 0.476 3.15 1.05 02/15/2024 20:37 WG2225388
Diethyl phthalate U 0.301 3.15 1.05 02/15/2024 20:37 WG2225388
Dimethyl phthalate U 0.273 3.15 1.05 02/15/2024 20:37 WG2225388
Di-n-octyl phthalate U 0.979 3.15 1.05 02/15/2024 20:37 WG2225388
Pyrene U 0.112 1.05 1.05 02/15/2024 20:37 WG2225388
1,2,4-Trichlorobenzene U 0.0733 10.5 1.05 02/15/2024 20:37 WG2225388
4-Chloro-3-methylphenol U J4 0.138 10.5 1.05 02/15/2024 20:37 WG2225388
2-Chlorophenol U 0.140 10.5 1.05 02/15/2024 20:37 WG2225388
2,4-Dichlorophenol U 0.107 10.5 1.05 02/15/2024 20:37 WG2225388
2,4-Dimethylphenol U 0.0668 10.5 1.05 02/15/2024 20:37 WG2225388
4,6-Dinitro-2-methylphenol U 1.18 10.5 1.05 02/15/2024 20:37 WG2225388
2,4-Dinitrophenol U 6.23 10.5 1.05 02/15/2024 20:37 WG2225388
2-Nitrophenol U 0.123 10.5 1.05 02/15/2024 20:37 WG2225388
4-Nitrophenol U 0.150 10.5 1.05 02/15/2024 20:37 WG2225388
Pentachlorophenol U 0.329 10.5 1.05 02/15/2024 20:37 WG2225388
Phenol U 4.55 10.5 1.05 02/15/2024 20:37 WG2225388
2,4,6-Trichlorophenol U 0.105 10.5 1.05 02/15/2024 20:37 WG2225388
(S) 2-Fluorophenol 30.7 10.0-120 02/15/2024 20:37 WG2225388
(S) Phenol-d5 20.8 10.0-120 02/15/2024 20:37 WG2225388
(S) Nitrobenzene-d5 48.4 10.0-127 02/15/2024 20:37 WG2225388
(S) 2-Fluorobiphenyl 49.0 10.0-130 02/15/2024 20:37 WG2225388
(S) 2,4,6-Tribromophenol 57.1 10.0-155 02/15/2024 20:37 WG2225388
(S) p-Terphenyl-d14 56.3 10.0-128 02/15/2024 20:37 WG2225388
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2226299
Volatile Organic Compounds (GC/MS) by Method 8260D L1704882-01,02,03,04
Method Blank (MB)
(MB) R4035273-3 02/14/24 10:41
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2226299
Volatile Organic Compounds (GC/MS) by Method 8260D L1704882-01,02,03,04
Method Blank (MB)
(MB) R4035273-3 02/14/24 10:41
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
2-Butanone (MEK)U 1.19 10.0
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
1,1,2-Trichlorotrifluoroethane U 0.180 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,2,3-Trimethylbenzene U 0.104 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
Xylenes, Total U 0.174 3.00
(S) Toluene-d8 108 80.0-120
(S) 4-Bromofluorobenzene 94.9 77.0-126
(S) 1,2-Dichloroethane-d4 96.7 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4035273-1 02/14/24 09:45 • (LCSD) R4035273-2 02/14/24 10:04
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 27.9 23.4 112 93.6 19.0-160 17.5 27
Acrolein 25.0 402 420 1610 1680 10.0-160 J4 J4 4.38 26
Acrylonitrile 25.0 19.8 20.6 79.2 82.4 55.0-149 3.96 20
Benzene 5.00 4.76 4.62 95.2 92.4 70.0-123 2.99 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2226299
Volatile Organic Compounds (GC/MS) by Method 8260D L1704882-01,02,03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4035273-1 02/14/24 09:45 • (LCSD) R4035273-2 02/14/24 10:04
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromobenzene 5.00 4.50 4.47 90.0 89.4 73.0-121 0.669 20
Bromodichloromethane 5.00 4.85 4.73 97.0 94.6 75.0-120 2.51 20
Bromoform 5.00 4.91 4.62 98.2 92.4 68.0-132 6.09 20
Bromomethane 5.00 5.75 5.52 115 110 10.0-160 4.08 25
n-Butylbenzene 5.00 4.86 4.44 97.2 88.8 73.0-125 9.03 20
sec-Butylbenzene 5.00 4.65 4.57 93.0 91.4 75.0-125 1.74 20
tert-Butylbenzene 5.00 4.82 4.74 96.4 94.8 76.0-124 1.67 20
Carbon tetrachloride 5.00 5.12 4.85 102 97.0 68.0-126 5.42 20
Chlorobenzene 5.00 5.02 4.93 100 98.6 80.0-121 1.81 20
Chlorodibromomethane 5.00 5.02 5.06 100 101 77.0-125 0.794 20
Chloroethane 5.00 4.36 4.38 87.2 87.6 47.0-150 0.458 20
Chloroform 5.00 4.93 4.67 98.6 93.4 73.0-120 5.42 20
Chloromethane 5.00 3.66 3.29 73.2 65.8 41.0-142 10.6 20
2-Chlorotoluene 5.00 4.52 4.77 90.4 95.4 76.0-123 5.38 20
4-Chlorotoluene 5.00 4.67 4.65 93.4 93.0 75.0-122 0.429 20
1,2-Dibromo-3-Chloropropane 5.00 4.92 4.26 98.4 85.2 58.0-134 14.4 20
1,2-Dibromoethane 5.00 4.81 4.79 96.2 95.8 80.0-122 0.417 20
Dibromomethane 5.00 4.62 4.51 92.4 90.2 80.0-120 2.41 20
1,2-Dichlorobenzene 5.00 5.08 5.03 102 101 79.0-121 0.989 20
1,3-Dichlorobenzene 5.00 4.85 4.86 97.0 97.2 79.0-120 0.206 20
1,4-Dichlorobenzene 5.00 4.76 4.72 95.2 94.4 79.0-120 0.844 20
Dichlorodifluoromethane 5.00 4.60 4.42 92.0 88.4 51.0-149 3.99 20
1,1-Dichloroethane 5.00 4.44 4.20 88.8 84.0 70.0-126 5.56 20
1,2-Dichloroethane 5.00 4.49 4.48 89.8 89.6 70.0-128 0.223 20
1,1-Dichloroethene 5.00 4.91 4.70 98.2 94.0 71.0-124 4.37 20
cis-1,2-Dichloroethene 5.00 4.89 4.53 97.8 90.6 73.0-120 7.64 20
trans-1,2-Dichloroethene 5.00 4.95 4.55 99.0 91.0 73.0-120 8.42 20
1,2-Dichloropropane 5.00 3.96 3.66 79.2 73.2 77.0-125 J4 7.87 20
1,1-Dichloropropene 5.00 4.57 4.41 91.4 88.2 74.0-126 3.56 20
1,3-Dichloropropane 5.00 4.86 4.65 97.2 93.0 80.0-120 4.42 20
cis-1,3-Dichloropropene 5.00 4.72 4.50 94.4 90.0 80.0-123 4.77 20
trans-1,3-Dichloropropene 5.00 4.73 4.73 94.6 94.6 78.0-124 0.000 20
2,2-Dichloropropane 5.00 5.42 5.64 108 113 58.0-130 3.98 20
Di-isopropyl ether 5.00 3.82 3.78 76.4 75.6 58.0-138 1.05 20
Ethylbenzene 5.00 4.99 4.90 99.8 98.0 79.0-123 1.82 20
Hexachloro-1,3-butadiene 5.00 4.59 4.06 91.8 81.2 54.0-138 12.3 20
Isopropylbenzene 5.00 5.08 4.80 102 96.0 76.0-127 5.67 20
p-Isopropyltoluene 5.00 4.92 4.76 98.4 95.2 76.0-125 3.31 20
2-Butanone (MEK)25.0 21.2 20.2 84.8 80.8 44.0-160 4.83 20
Methylene Chloride 5.00 4.77 4.67 95.4 93.4 67.0-120 2.12 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2226299
Volatile Organic Compounds (GC/MS) by Method 8260D L1704882-01,02,03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4035273-1 02/14/24 09:45 • (LCSD) R4035273-2 02/14/24 10:04
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
4-Methyl-2-pentanone (MIBK)25.0 22.6 22.0 90.4 88.0 68.0-142 2.69 20
Methyl tert-butyl ether 5.00 4.75 4.57 95.0 91.4 68.0-125 3.86 20
Naphthalene 5.00 4.15 4.25 83.0 85.0 54.0-135 2.38 20
n-Propylbenzene 5.00 4.77 4.62 95.4 92.4 77.0-124 3.19 20
Styrene 5.00 4.41 4.34 88.2 86.8 73.0-130 1.60 20
1,1,1,2-Tetrachloroethane 5.00 5.10 4.97 102 99.4 75.0-125 2.58 20
1,1,2,2-Tetrachloroethane 5.00 4.93 5.19 98.6 104 65.0-130 5.14 20
1,1,2-Trichlorotrifluoroethane 5.00 4.99 4.94 99.8 98.8 69.0-132 1.01 20
Tetrachloroethene 5.00 5.07 4.80 101 96.0 72.0-132 5.47 20
Toluene 5.00 4.93 4.91 98.6 98.2 79.0-120 0.406 20
1,2,3-Trichlorobenzene 5.00 4.23 4.45 84.6 89.0 50.0-138 5.07 20
1,2,4-Trichlorobenzene 5.00 4.73 4.60 94.6 92.0 57.0-137 2.79 20
1,1,1-Trichloroethane 5.00 5.37 4.68 107 93.6 73.0-124 13.7 20
1,1,2-Trichloroethane 5.00 4.93 4.83 98.6 96.6 80.0-120 2.05 20
Trichloroethene 5.00 4.83 4.82 96.6 96.4 78.0-124 0.207 20
Trichlorofluoromethane 5.00 5.23 5.09 105 102 59.0-147 2.71 20
1,2,3-Trichloropropane 5.00 4.49 4.54 89.8 90.8 73.0-130 1.11 20
1,2,4-Trimethylbenzene 5.00 4.73 4.67 94.6 93.4 76.0-121 1.28 20
1,2,3-Trimethylbenzene 5.00 4.62 4.53 92.4 90.6 77.0-120 1.97 20
1,3,5-Trimethylbenzene 5.00 4.72 4.72 94.4 94.4 76.0-122 0.000 20
Vinyl chloride 5.00 4.19 4.19 83.8 83.8 67.0-131 0.000 20
Xylenes, Total 15.0 15.4 14.8 103 98.7 79.0-123 3.97 20
(S) Toluene-d8 105 107 80.0-120
(S) 4-Bromofluorobenzene 99.1 99.7 77.0-126
(S) 1,2-Dichloroethane-d4 95.2 95.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2229263
Volatile Organic Compounds (GC/MS) by Method 8260D L1704882-01,02,03,04
Method Blank (MB)
(MB) R4036326-3 02/19/24 18:50
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.0941 1.00
cis-1,2-Dichloroethene U 0.126 1.00
Methyl tert-butyl ether U 0.101 1.00
(S) Toluene-d8 94.1 80.0-120
(S) 4-Bromofluorobenzene 104 77.0-126
(S) 1,2-Dichloroethane-d4 95.9 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4036326-1 02/19/24 17:45 • (LCSD) R4036326-2 02/19/24 18:06
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 5.00 4.56 4.59 91.2 91.8 70.0-123 0.656 20
cis-1,2-Dichloroethene 5.00 4.34 4.52 86.8 90.4 73.0-120 4.06 20
Methyl tert-butyl ether 5.00 4.34 4.28 86.8 85.6 68.0-125 1.39 20
(S) Toluene-d8 91.8 90.9 80.0-120
(S) 4-Bromofluorobenzene 101 102 77.0-126
(S) 1,2-Dichloroethane-d4 97.3 99.1 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2225388
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1704882-01,02,03,04
Method Blank (MB)
(MB) R4035204-3 02/15/24 13:19
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.0886 1.00
Acenaphthylene U 0.0921 1.00
Anthracene U 0.0804 1.00
Benzidine U 3.74 10.0
Benzo(a)anthracene U 0.199 1.00
Benzo(b)fluoranthene U 0.130 1.00
Benzo(k)fluoranthene U 0.120 1.00
Benzo(g,h,i)perylene U 0.121 1.00
Benzo(a)pyrene U 0.0381 1.00
Bis(2-chlorethoxy)methane U 0.116 10.0
Bis(2-chloroethyl)ether U 0.137 10.0
2,2-Oxybis(1-Chloropropane)U 0.210 10.0
4-Bromophenyl-phenylether U 0.0877 10.0
2-Chloronaphthalene U 0.0648 1.00
4-Chlorophenyl-phenylether U 0.0926 10.0
Chrysene U 0.130 1.00
Dibenz(a,h)anthracene 0.0651 J 0.0644 1.00
1,2-Dichlorobenzene U 0.0713 10.0
1,3-Dichlorobenzene U 0.132 10.0
1,4-Dichlorobenzene U 0.0942 10.0
3,3-Dichlorobenzidine U 0.212 10.0
2,4-Dinitrotoluene U 0.0983 10.0
2,6-Dinitrotoluene U 0.250 10.0
Fluoranthene U 0.102 1.00
Fluorene U 0.0844 1.00
Hexachlorobenzene U 0.0755 1.00
Hexachloro-1,3-butadiene U 0.0968 10.0
Hexachlorocyclopentadiene U 0.0598 10.0
Hexachloroethane U 0.127 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.143 10.0
Naphthalene U 0.159 1.00
Nitrobenzene U 0.297 10.0
n-Nitrosodimethylamine U 0.998 10.0
n-Nitrosodiphenylamine U 2.37 10.0
n-Nitrosodi-n-propylamine U 0.261 10.0
Phenanthrene U 0.112 1.00
Benzylbutyl phthalate U 0.765 3.00
Bis(2-ethylhexyl)phthalate U 0.895 3.00
Di-n-butyl phthalate U 0.453 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2225388
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1704882-01,02,03,04
Method Blank (MB)
(MB) R4035204-3 02/15/24 13:19
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Diethyl phthalate U 0.287 3.00
Dimethyl phthalate U 0.260 3.00
Di-n-octyl phthalate U 0.932 3.00
Pyrene U 0.107 1.00
1,2,4-Trichlorobenzene U 0.0698 10.0
4-Chloro-3-methylphenol U 0.131 10.0
2-Chlorophenol U 0.133 10.0
2,4-Dichlorophenol U 0.102 10.0
2,4-Dimethylphenol U 0.0636 10.0
4,6-Dinitro-2-methylphenol U 1.12 10.0
2,4-Dinitrophenol U 5.93 10.0
2-Nitrophenol U 0.117 10.0
4-Nitrophenol U 0.143 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 4.33 10.0
2,4,6-Trichlorophenol U 0.100 10.0
(S) 2-Fluorophenol 30.1 10.0-120
(S) Phenol-d5 19.1 10.0-120
(S) Nitrobenzene-d5 51.8 10.0-127
(S) 2-Fluorobiphenyl 53.7 10.0-130
(S) 2,4,6-Tribromophenol 47.3 10.0-155
(S) p-Terphenyl-d14 52.9 10.0-128
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4035204-1 02/15/24 12:36 • (LCSD) R4035204-2 02/15/24 12:57
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 28.4 25.4 56.8 50.8 41.0-120 11.2 22
Acenaphthylene 50.0 30.6 27.1 61.2 54.2 43.0-120 12.1 22
Anthracene 50.0 30.0 27.4 60.0 54.8 45.0-120 9.06 20
Benzidine 100 3.82 17.0 3.82 17.0 10.0-120 J4 J3 127 36
Benzo(a)anthracene 50.0 29.1 27.8 58.2 55.6 47.0-120 4.57 20
Benzo(b)fluoranthene 50.0 29.1 28.2 58.2 56.4 46.0-120 3.14 20
Benzo(k)fluoranthene 50.0 28.7 27.5 57.4 55.0 46.0-120 4.27 21
Benzo(g,h,i)perylene 50.0 27.4 25.7 54.8 51.4 48.0-121 6.40 20
Benzo(a)pyrene 50.0 28.1 27.5 56.2 55.0 47.0-120 2.16 20
Bis(2-chlorethoxy)methane 50.0 26.7 24.2 53.4 48.4 33.0-120 9.82 24
Bis(2-chloroethyl)ether 50.0 30.6 28.2 61.2 56.4 23.0-120 8.16 33
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2225388
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1704882-01,02,03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4035204-1 02/15/24 12:36 • (LCSD) R4035204-2 02/15/24 12:57
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
2,2-Oxybis(1-Chloropropane)50.0 27.9 25.4 55.8 50.8 28.0-120 9.38 31
4-Bromophenyl-phenylether 50.0 29.5 26.3 59.0 52.6 45.0-120 11.5 20
2-Chloronaphthalene 50.0 27.9 24.6 55.8 49.2 37.0-120 12.6 25
4-Chlorophenyl-phenylether 50.0 29.1 26.1 58.2 52.2 44.0-120 10.9 20
Chrysene 50.0 27.8 26.7 55.6 53.4 48.0-120 4.04 20
Dibenz(a,h)anthracene 50.0 28.1 26.8 56.2 53.6 47.0-120 4.74 20
1,2-Dichlorobenzene 50.0 27.1 24.9 54.2 49.8 20.0-120 8.46 34
1,3-Dichlorobenzene 50.0 27.7 24.9 55.4 49.8 17.0-120 10.6 35
1,4-Dichlorobenzene 50.0 28.9 26.5 57.8 53.0 18.0-120 8.66 34
3,3-Dichlorobenzidine 100 63.5 62.2 63.5 62.2 44.0-120 2.07 20
2,4-Dinitrotoluene 50.0 35.9 32.8 71.8 65.6 49.0-124 9.02 20
2,6-Dinitrotoluene 50.0 32.7 29.3 65.4 58.6 46.0-120 11.0 21
Fluoranthene 50.0 32.4 29.8 64.8 59.6 51.0-120 8.36 20
Fluorene 50.0 29.9 26.5 59.8 53.0 47.0-120 12.1 20
Hexachlorobenzene 50.0 28.3 25.8 56.6 51.6 44.0-120 9.24 20
Hexachloro-1,3-butadiene 50.0 21.2 19.5 42.4 39.0 19.0-120 8.35 32
Hexachlorocyclopentadiene 50.0 10.6 9.72 21.2 19.4 15.0-120 8.66 31
Hexachloroethane 50.0 26.4 24.5 52.8 49.0 15.0-120 7.47 37
Indeno(1,2,3-cd)pyrene 50.0 29.1 27.6 58.2 55.2 49.0-122 5.29 20
Isophorone 50.0 26.3 24.1 52.6 48.2 36.0-120 8.73 23
Naphthalene 50.0 27.2 24.3 54.4 48.6 27.0-120 11.3 27
Nitrobenzene 50.0 26.0 23.2 52.0 46.4 27.0-120 11.4 29
n-Nitrosodimethylamine 50.0 18.0 16.7 36.0 33.4 10.0-120 7.49 40
n-Nitrosodiphenylamine 50.0 30.7 26.7 61.4 53.4 47.0-120 13.9 20
n-Nitrosodi-n-propylamine 50.0 28.6 26.0 57.2 52.0 31.0-120 9.52 28
Phenanthrene 50.0 29.4 26.2 58.8 52.4 46.0-120 11.5 20
Benzylbutyl phthalate 50.0 31.7 30.8 63.4 61.6 43.0-121 2.88 20
Bis(2-ethylhexyl)phthalate 50.0 31.8 31.8 63.6 63.6 43.0-122 0.000 20
Di-n-butyl phthalate 50.0 33.2 31.4 66.4 62.8 49.0-121 5.57 20
Diethyl phthalate 50.0 31.4 29.3 62.8 58.6 48.0-122 6.92 20
Dimethyl phthalate 50.0 31.4 29.1 62.8 58.2 48.0-120 7.60 20
Di-n-octyl phthalate 50.0 30.5 30.8 61.0 61.6 42.0-125 0.979 20
Pyrene 50.0 27.5 25.7 55.0 51.4 47.0-120 6.77 20
1,2,4-Trichlorobenzene 50.0 25.1 22.4 50.2 44.8 24.0-120 11.4 29
4-Chloro-3-methylphenol 50.0 19.3 20.2 38.6 40.4 40.0-120 J4 4.56 21
2-Chlorophenol 50.0 19.2 19.6 38.4 39.2 25.0-120 2.06 35
2,4-Dichlorophenol 50.0 20.9 21.9 41.8 43.8 36.0-120 4.67 26
2,4-Dimethylphenol 50.0 17.0 17.2 34.0 34.4 33.0-120 1.17 26
4,6-Dinitro-2-methylphenol 50.0 35.0 35.2 70.0 70.4 38.0-138 0.570 25
2,4-Dinitrophenol 50.0 29.5 30.2 59.0 60.4 10.0-120 2.35 39
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2225388
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1704882-01,02,03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R4035204-1 02/15/24 12:36 • (LCSD) R4035204-2 02/15/24 12:57
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
2-Nitrophenol 50.0 24.0 24.9 48.0 49.8 31.0-120 3.68 29
4-Nitrophenol 50.0 12.8 11.9 25.6 23.8 10.0-120 7.29 33
Pentachlorophenol 50.0 24.5 23.2 49.0 46.4 23.0-120 5.45 25
Phenol 50.0 10.7 10.1 21.4 20.2 10.0-120 5.77 36
2,4,6-Trichlorophenol 50.0 24.3 24.5 48.6 49.0 42.0-120 0.820 23
(S) 2-Fluorophenol 30.4 29.3 10.0-120
(S) Phenol-d5 21.3 19.7 10.0-120
(S) Nitrobenzene-d5 46.2 39.8 10.0-127
(S) 2-Fluorobiphenyl 58.0 49.5 10.0-130
(S) 2,4,6-Tribromophenol 53.0 52.0 10.0-155
(S) p-Terphenyl-d14 56.0 53.2 10.0-128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 26 of 28

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
AECOM - Raleigh, NC 60722767 L1704882 02/26/24 10:07 27 of 28
AECOM - Morrisville
1600 Perimeter Park Dr.
Morrisville, NC 27560

Frye & Webster – DC410064
Client Project# 60722767

Analytical Report
(0124-075)

EPA Method TO-15
TO-15 Target Compund List

Enthalpy Analytical, LLC
Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com
800-1 Capitola Drive Durham, NC 27713-4385

I certify that to the best of my knowledge all analytical data presented in this report:
 Have been checked for completeness
 Are accurate, error-free, and legible
 Have been conducted in accordance with approved protocol, and that all deviations and
analytical problems are summarized in the appropriate narrative(s)
This analytical report was prepared in Portable Document Format (.PDF). This report shall not be
reproduced except in full without approval of the laboratory. This will provide assurance that parts of a
report are not taken out of context.

Report Issued: 2/15/24
EA # 0124-075 Page 2 of 85

Results
EA # 0124-075 Page 3 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene 4.20 0.0894 0.0810 7.22 0.154 0.139 m
Freon 12 (CCl2F2)0.493 0.0906 0.0810 2.44 0.448 0.400
Freon 114 (C2Cl2F4)ND 0.0928 0.0810 ND 0.648 0.566
Chloromethane 0.373 0.0916 0.0810 0.770 0.189 0.167
Chloroethene (Vinyl chloride)ND 0.0925 0.0810 ND 0.236 0.207
1,3-Butadiene 0.325 0.0901 0.0810 0.718 0.199 0.179
Bromomethane ND 0.0908 0.0810 ND 0.352 0.314
Chloroethane ND 0.0941 0.0810 ND 0.248 0.214
Bromoethene (Vinyl bromide)ND 0.0905 0.0810 ND 0.396 0.354
Freon 11 (CCl3F)0.236 0.0977 0.0810 1.32 0.548 0.455
Ethanol 3.50 0.0917 0.0917 6.59 0.173 0.173
Acrolein 0.350 0.0912 0.0810 0.803 0.209 0.186 m
Freon 113 (C2Cl3F3)ND 0.0940 0.0810 ND 0.720 0.620
1,1-Dichloroethene ND 0.0931 0.0810 ND 0.369 0.321
Acetone 35.8 0.0928 0.0810 84.9 0.220 0.192
Carbon disulfide 0.500 0.0923 0.0810 1.55 0.287 0.252
Isopropyl alcohol 1.94 0.0923 0.0810 4.77 0.227 0.199
Allyl chloride (3-chloropropene)ND 0.1000 0.0810 ND 0.313 0.253
Acetonitrile ND 0.0923 0.0810 ND 0.155 0.136
Methylene chloride 0.192 0.0948 0.0810 0.665 0.329 0.281
trans-1,2-Dichloroethene 0.506 0.0944 0.0810 2.01 0.374 0.321
Methyl tert-butyl ether ND 0.0952 0.0810 ND 0.343 0.292
Acrylonitrile ND 0.0942 0.0810 ND 0.204 0.176
Hexane 0.710 0.0941 0.0810 2.50 0.331 0.285
1,1-Dichloroethane ND 0.0919 0.0810 ND 0.372 0.328
Vinyl acetate ND 0.0947 0.0810 ND 0.333 0.285
cis-1,2-Dichloroethene 3.64 0.0935 0.0810 14.4 0.371 0.321
Methyl ethyl ketone (2-Butanone)6.34 0.0957 0.0810 18.7 0.282 0.239 m
Ethyl acetate 1.15 0.0924 0.0810 4.13 0.333 0.292
Chloroform 1.08 0.0929 0.0810 5.25 0.453 0.395
Tetrahydrofuran 2.43 0.0937 0.0810 7.17 0.276 0.239
Air
KMB
Xavier
0124-075.SG-5.Can
X2400589.D
1.000
2.315
2024-02-01 16:22
TO15_SCNV6.M
0124-075; 500mL Load; Can #12165
2024-01-29 17:02
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-5
EA # 0124-075 Page 4 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
KMB
Xavier
0124-075.SG-5.Can
X2400589.D
1.000
2.315
2024-02-01 16:22
TO15_SCNV6.M
0124-075; 500mL Load; Can #12165
2024-01-29 17:02
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-5
1,1,1-Trichloroethane ND 0.0935 0.0810 ND 0.510 0.442
Cyclohexane 0.424 0.0949 0.0810 1.46 0.326 0.279
Carbon tetrachloride 0.0812 0.0932 0.0810 0.510 0.586 0.509 J
Benzene 0.379 0.0931 0.0810 1.21 0.297 0.259
2,2,4-trimethylpentane 0.703 0.0957 0.0810 3.28 0.447 0.378
1,2-Dichloroethane ND 0.0953 0.0810 ND 0.385 0.328
Heptane 0.435 0.0938 0.0810 1.78 0.384 0.332
Trichloroethene 24.4 0.0936 0.0810 131 0.503 0.435
1,2-Dichloropropane ND 0.0932 0.0810 ND 0.431 0.374
Methyl methacrylate 0.0946 0.0969 0.0810 0.387 0.397 0.332 J, m
1,4-Dioxane 0.370 0.0929 0.0810 1.33 0.334 0.292
Bromodichloromethane ND 0.0935 0.0810 ND 0.626 0.542
cis-1,3-Dichloropropene ND 0.0919 0.0810 ND 0.417 0.367
Methyl isobutyl ketone 7.51 0.0962 0.0810 30.7 0.394 0.332
Toluene 4.18 0.0942 0.0810 15.7 0.355 0.305
trans-1,3-Dichloropropene ND 0.0955 0.0810 ND 0.433 0.367
1,1,2-Trichloroethane 0.101 0.0942 0.0810 0.553 0.513 0.442
2-Hexanone (Methyl butyl ketone)24.1 0.0947 0.0810 98.7 0.388 0.332 m
Dibromochloromethane ND 0.0933 0.0810 ND 0.794 0.690
1,2-Dibromoethane ND 0.0947 0.0810 ND 0.727 0.622
Chlorobenzene ND 0.0954 0.0810 ND 0.439 0.373
Ethylbenzene 1.04 0.0919 0.0810 4.50 0.399 0.352
1,1,1,2-Tetrachloroethane ND 0.0933 0.0810 ND 0.640 0.556
m-/p-Xylenes 4.18 0.0939 0.0810 18.1 0.407 0.352
o-Xylene 1.55 0.0928 0.0810 6.73 0.403 0.352
Styrene 0.104 0.0907 0.0810 0.444 0.386 0.345
Bromoform ND 0.0929 0.0810 ND 0.959 0.837
1,1,2,2-Tetrachloroethane 0.113 0.0936 0.0810 0.775 0.642 0.556
4-Ethyltoluene 0.747 0.0942 0.0810 3.67 0.463 0.398 m
2-Chlorotoluene 0.108 0.0934 0.0810 0.560 0.483 0.419 m
1,3,5-Trimethylbenzene 0.796 0.0939 0.0810 3.91 0.461 0.398
EA # 0124-075 Page 5 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
KMB
Xavier
0124-075.SG-5.Can
X2400589.D
1.000
2.315
2024-02-01 16:22
TO15_SCNV6.M
0124-075; 500mL Load; Can #12165
2024-01-29 17:02
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-5
1,2,4-Trimethylbenzene 3.07 0.0927 0.0810 15.1 0.455 0.398 m
1,3-Dichlorobenzene ND 0.0941 0.0810 ND 0.565 0.487
1,4-Dichlorobenzene ND 0.0930 0.0810 ND 0.559 0.487
Benzyl chloride ND 0.0931 0.0810 ND 0.482 0.419
1,2-Dichlorobenzene ND 0.0938 0.0810 ND 0.564 0.487
1,2,4-Trichlorobenzene ND 0.0922 0.0810 ND 0.684 0.601
Hexachlorobutadiene ND 0.0915 0.0810 ND 0.975 0.863
Naphthalene 0.162 0.0932 0.0810 0.850 0.488 0.424 m
1-Bromopropane ND 0.0918 0.0810 ND 0.462 0.407
1-Octene 0.380 0.0914 0.0810 1.74 0.419 0.372
n-Octane 0.703 0.0954 0.0810 3.28 0.445 0.378
Isopropylbenzene 0.250 0.0941 0.0810 1.23 0.462 0.398
n-Propylbenzene 0.528 0.0950 0.0810 2.59 0.467 0.398
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)894,652 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,401,139 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,986,829 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 6 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Tetrachloroethene 460 4.74 4.05 3,117 32.1 27.5
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)789,096 11.02 5.21 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
Air
TDD
Xavier
0124-075.SG-5.Can
X2400666.D
50.000
2.315
2024-02-06 08:31
TO15_SCNV6.M
0124-075; *50=10mL Load; Can #12165
2024-01-29 17:02
2024-02-01 00:00
Sample
Xavier_X020524A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-5
EA # 0124-075 Page 7 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene 2.92 0.0956 0.0866 5.02 0.164 0.149
Freon 12 (CCl2F2)0.479 0.0969 0.0866 2.37 0.479 0.428 m
Freon 114 (C2Cl2F4)ND 0.0992 0.0866 ND 0.693 0.605
Chloromethane ND 0.0979 0.0866 ND 0.202 0.179
Chloroethene (Vinyl chloride)ND 0.0989 0.0866 ND 0.253 0.221
1,3-Butadiene ND 0.0963 0.0866 ND 0.213 0.191
Bromomethane ND 0.0971 0.0866 ND 0.377 0.336
Chloroethane ND 0.101 0.0866 ND 0.265 0.228
Bromoethene (Vinyl bromide)ND 0.0968 0.0866 ND 0.423 0.379
Freon 11 (CCl3F)0.195 0.104 0.0866 1.10 0.586 0.486
Ethanol 0.797 0.0981 0.0981 1.50 0.185 0.185 m
Acrolein ND 0.0975 0.0866 ND 0.223 0.198
Freon 113 (C2Cl3F3)ND 0.100 0.0866 ND 0.769 0.663
1,1-Dichloroethene 0.194 0.0996 0.0866 0.769 0.394 0.343
Acetone 10.0 0.0992 0.0866 23.8 0.235 0.206
Carbon disulfide 0.963 0.0987 0.0866 3.00 0.307 0.269
Isopropyl alcohol 0.227 0.0987 0.0866 0.558 0.242 0.213 m
Allyl chloride (3-chloropropene)ND 0.107 0.0866 ND 0.334 0.271
Acetonitrile 0.106 0.0987 0.0866 0.178 0.166 0.145
Methylene chloride 0.241 0.101 0.0866 0.838 0.352 0.301
trans-1,2-Dichloroethene 0.316 0.101 0.0866 1.25 0.400 0.343
Methyl tert-butyl ether ND 0.102 0.0866 ND 0.367 0.312
Acrylonitrile ND 0.101 0.0866 ND 0.219 0.188
Hexane 0.469 0.101 0.0866 1.65 0.354 0.305 m
1,1-Dichloroethane ND 0.0983 0.0866 ND 0.398 0.350
Vinyl acetate ND 0.101 0.0866 ND 0.356 0.305
cis-1,2-Dichloroethene 4.03 0.1000 0.0866 16.0 0.396 0.343
Methyl ethyl ketone (2-Butanone)2.05 0.102 0.0866 6.03 0.302 0.255
Ethyl acetate ND 0.0988 0.0866 ND 0.356 0.312
Chloroform 0.205 0.0993 0.0866 0.999 0.484 0.423
Tetrahydrofuran 0.497 0.100 0.0866 1.46 0.295 0.255
Air
KMB
Xavier
0124-075.SG-3.Can
X2400590.D
1.000
2.474
2024-02-01 17:17
TO15_SCNV6.M
0124-075; 500mL Load; Can #6041/C10125
2024-01-31 12:31
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-3
EA # 0124-075 Page 8 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
KMB
Xavier
0124-075.SG-3.Can
X2400590.D
1.000
2.474
2024-02-01 17:17
TO15_SCNV6.M
0124-075; 500mL Load; Can #6041/C10125
2024-01-31 12:31
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-3
1,1,1-Trichloroethane 2.87 0.1000 0.0866 15.6 0.545 0.472
Cyclohexane 0.498 0.101 0.0866 1.71 0.349 0.298
Carbon tetrachloride ND 0.0997 0.0866 ND 0.627 0.544
Benzene 0.235 0.0996 0.0866 0.751 0.318 0.276
2,2,4-trimethylpentane ND 0.102 0.0866 ND 0.478 0.404
1,2-Dichloroethane ND 0.102 0.0866 ND 0.412 0.350
Heptane 0.348 0.100 0.0866 1.43 0.411 0.355
Trichloroethene 20.3 0.100 0.0866 109 0.537 0.465
1,2-Dichloropropane ND 0.0997 0.0866 ND 0.460 0.400
Methyl methacrylate ND 0.104 0.0866 ND 0.424 0.354
1,4-Dioxane ND 0.0993 0.0866 ND 0.357 0.312
Bromodichloromethane ND 0.1000 0.0866 ND 0.669 0.580
cis-1,3-Dichloropropene ND 0.0983 0.0866 ND 0.446 0.393
Methyl isobutyl ketone 1.39 0.103 0.0866 5.67 0.421 0.355
Toluene 1.94 0.101 0.0866 7.29 0.379 0.326
trans-1,3-Dichloropropene ND 0.102 0.0866 ND 0.463 0.393
1,1,2-Trichloroethane ND 0.101 0.0866 ND 0.549 0.472
2-Hexanone (Methyl butyl ketone)3.92 0.101 0.0866 16.0 0.414 0.355 m
Dibromochloromethane ND 0.0998 0.0866 ND 0.849 0.737
1,2-Dibromoethane ND 0.101 0.0866 ND 0.777 0.665
Chlorobenzene ND 0.102 0.0866 ND 0.469 0.398
Ethylbenzene 0.267 0.0983 0.0866 1.16 0.426 0.376
1,1,1,2-Tetrachloroethane ND 0.0998 0.0866 ND 0.684 0.594
m-/p-Xylenes 1.01 0.100 0.0866 4.40 0.435 0.376
o-Xylene 0.387 0.0992 0.0866 1.68 0.430 0.376
Styrene ND 0.0970 0.0866 ND 0.413 0.369
Bromoform ND 0.0993 0.0866 ND 1.03 0.895
1,1,2,2-Tetrachloroethane ND 0.100 0.0866 ND 0.686 0.594
4-Ethyltoluene 0.175 0.101 0.0866 0.859 0.494 0.425 m
2-Chlorotoluene ND 0.0999 0.0866 ND 0.517 0.448
1,3,5-Trimethylbenzene 0.216 0.100 0.0866 1.06 0.493 0.425
EA # 0124-075 Page 9 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
KMB
Xavier
0124-075.SG-3.Can
X2400590.D
1.000
2.474
2024-02-01 17:17
TO15_SCNV6.M
0124-075; 500mL Load; Can #6041/C10125
2024-01-31 12:31
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-3
1,2,4-Trimethylbenzene 0.839 0.0991 0.0866 4.12 0.487 0.425
1,3-Dichlorobenzene ND 0.101 0.0866 ND 0.604 0.520
1,4-Dichlorobenzene ND 0.0995 0.0866 ND 0.598 0.520
Benzyl chloride ND 0.0996 0.0866 ND 0.515 0.448
1,2-Dichlorobenzene ND 0.100 0.0866 ND 0.602 0.520
1,2,4-Trichlorobenzene ND 0.0986 0.0866 ND 0.731 0.642
Hexachlorobutadiene ND 0.0978 0.0866 ND 1.04 0.923
Naphthalene ND 0.0997 0.0866 ND 0.522 0.454
1-Bromopropane ND 0.0982 0.0866 ND 0.494 0.435
1-Octene 0.286 0.0977 0.0866 1.31 0.448 0.397 m
n-Octane 0.314 0.102 0.0866 1.46 0.476 0.404
Isopropylbenzene 0.0884 0.101 0.0866 0.434 0.494 0.425 J
n-Propylbenzene 0.186 0.102 0.0866 0.912 0.499 0.425
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)931,462 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,553,555 12.44 5.16 pass
Chlorobenzene-d5 (IS)3,089,601 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 10 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Tetrachloroethene 1,811 5.06 4.33 12,277 34.3 29.3
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)816,524 11.02 5.21 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
Air
TDD
Xavier
0124-075.SG-3.Can
X2400682.D
50.000
2.474
2024-02-06 21:41
TO15_SCNV6.M
0124-075; *50=10mL Load; Can #6041/C10125
2024-01-31 12:31
2024-02-01 00:00
Sample
Xavier_X020624A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-3
EA # 0124-075 Page 11 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene 12.6 0.104 0.0944 21.6 0.179 0.162
Freon 12 (CCl2F2)0.472 0.106 0.0944 2.33 0.522 0.466 m
Freon 114 (C2Cl2F4)ND 0.108 0.0944 ND 0.755 0.659
Chloromethane 0.418 0.107 0.0944 0.862 0.220 0.195
Chloroethene (Vinyl chloride)ND 0.108 0.0944 ND 0.275 0.241
1,3-Butadiene 0.630 0.105 0.0944 1.39 0.232 0.209
Bromomethane ND 0.106 0.0944 ND 0.411 0.366
Chloroethane ND 0.110 0.0944 ND 0.289 0.249
Bromoethene (Vinyl bromide)ND 0.105 0.0944 ND 0.461 0.413
Freon 11 (CCl3F)0.221 0.114 0.0944 1.24 0.639 0.530
Ethanol 5.21 0.107 0.107 9.81 0.201 0.201
Acrolein 0.186 0.106 0.0944 0.426 0.243 0.216 m
Freon 113 (C2Cl3F3)ND 0.109 0.0944 ND 0.838 0.723
1,1-Dichloroethene ND 0.108 0.0944 ND 0.430 0.374
Acetone 9.63 0.108 0.0944 22.9 0.257 0.224
Carbon disulfide 0.381 0.108 0.0944 1.18 0.335 0.294
Isopropyl alcohol 1.08 0.108 0.0944 2.66 0.264 0.232
Allyl chloride (3-chloropropene)ND 0.116 0.0944 ND 0.364 0.295
Acetonitrile ND 0.108 0.0944 ND 0.180 0.158
Methylene chloride 0.536 0.110 0.0944 1.86 0.383 0.328
trans-1,2-Dichloroethene ND 0.110 0.0944 ND 0.436 0.374
Methyl tert-butyl ether ND 0.111 0.0944 ND 0.399 0.340
Acrylonitrile ND 0.110 0.0944 ND 0.238 0.205
Hexane 0.509 0.110 0.0944 1.79 0.386 0.332
1,1-Dichloroethane ND 0.107 0.0944 ND 0.433 0.382
Vinyl acetate ND 0.110 0.0944 ND 0.388 0.332
cis-1,2-Dichloroethene ND 0.109 0.0944 ND 0.432 0.374
Methyl ethyl ketone (2-Butanone)0.378 0.112 0.0944 1.11 0.329 0.278
Ethyl acetate 0.401 0.108 0.0944 1.45 0.388 0.340
Chloroform 0.378 0.108 0.0944 1.84 0.528 0.460
Tetrahydrofuran 0.148 0.109 0.0944 0.436 0.322 0.278 m
Air
KMB
Xavier
0124-075.SG-2.Can
X2400591.D
1.000
2.696
2024-02-01 18:11
TO15_SCNV6.M
0124-075; 500mL Load; Can #13542
2024-01-31 13:11
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-2
EA # 0124-075 Page 12 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
KMB
Xavier
0124-075.SG-2.Can
X2400591.D
1.000
2.696
2024-02-01 18:11
TO15_SCNV6.M
0124-075; 500mL Load; Can #13542
2024-01-31 13:11
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-2
1,1,1-Trichloroethane ND 0.109 0.0944 ND 0.594 0.515
Cyclohexane 0.272 0.111 0.0944 0.937 0.380 0.325
Carbon tetrachloride ND 0.109 0.0944 ND 0.683 0.593
Benzene 0.470 0.108 0.0944 1.50 0.346 0.301
2,2,4-trimethylpentane 0.120 0.112 0.0944 0.560 0.521 0.441
1,2-Dichloroethane ND 0.111 0.0944 ND 0.449 0.382
Heptane 0.272 0.109 0.0944 1.12 0.447 0.386
Trichloroethene 0.958 0.109 0.0944 5.14 0.586 0.507
1,2-Dichloropropane ND 0.109 0.0944 ND 0.502 0.436
Methyl methacrylate 0.329 0.113 0.0944 1.35 0.462 0.386
1,4-Dioxane ND 0.108 0.0944 ND 0.390 0.340
Bromodichloromethane ND 0.109 0.0944 ND 0.729 0.632
cis-1,3-Dichloropropene ND 0.107 0.0944 ND 0.486 0.428
Methyl isobutyl ketone 1.12 0.112 0.0944 4.60 0.459 0.386 m
Toluene 4.13 0.110 0.0944 15.5 0.413 0.355
trans-1,3-Dichloropropene ND 0.111 0.0944 ND 0.505 0.428
1,1,2-Trichloroethane ND 0.110 0.0944 ND 0.598 0.515
2-Hexanone (Methyl butyl ketone)0.600 0.110 0.0944 2.46 0.452 0.386 m
Dibromochloromethane ND 0.109 0.0944 ND 0.925 0.803
1,2-Dibromoethane ND 0.110 0.0944 ND 0.847 0.725
Chlorobenzene ND 0.111 0.0944 ND 0.511 0.434
Ethylbenzene 1.35 0.107 0.0944 5.84 0.465 0.410
1,1,1,2-Tetrachloroethane ND 0.109 0.0944 ND 0.746 0.647
m-/p-Xylenes 5.52 0.109 0.0944 24.0 0.475 0.410
o-Xylene 1.76 0.108 0.0944 7.63 0.469 0.410
Styrene 0.118 0.106 0.0944 0.503 0.450 0.402 m
Bromoform ND 0.108 0.0944 ND 1.12 0.975
1,1,2,2-Tetrachloroethane ND 0.109 0.0944 ND 0.748 0.647
4-Ethyltoluene 0.462 0.110 0.0944 2.27 0.539 0.464 m
2-Chlorotoluene ND 0.109 0.0944 ND 0.563 0.488
1,3,5-Trimethylbenzene 0.710 0.109 0.0944 3.49 0.537 0.464
EA # 0124-075 Page 13 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
KMB
Xavier
0124-075.SG-2.Can
X2400591.D
1.000
2.696
2024-02-01 18:11
TO15_SCNV6.M
0124-075; 500mL Load; Can #13542
2024-01-31 13:11
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-2
1,2,4-Trimethylbenzene 3.13 0.108 0.0944 15.4 0.530 0.464
1,3-Dichlorobenzene ND 0.110 0.0944 ND 0.658 0.567
1,4-Dichlorobenzene ND 0.108 0.0944 ND 0.651 0.567
Benzyl chloride ND 0.108 0.0944 ND 0.561 0.488
1,2-Dichlorobenzene ND 0.109 0.0944 ND 0.656 0.567
1,2,4-Trichlorobenzene ND 0.107 0.0944 ND 0.797 0.700
Hexachlorobutadiene ND 0.107 0.0944 ND 1.14 1.01
Naphthalene 0.335 0.109 0.0944 1.76 0.569 0.494
1-Bromopropane ND 0.107 0.0944 ND 0.538 0.474
1-Octene 0.870 0.106 0.0944 3.99 0.488 0.433
n-Octane 1.53 0.111 0.0944 7.13 0.519 0.441
Isopropylbenzene ND 0.110 0.0944 ND 0.538 0.464
n-Propylbenzene 0.226 0.111 0.0944 1.11 0.544 0.464
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)928,326 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,555,364 12.44 5.16 pass
Chlorobenzene-d5 (IS)3,101,825 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 14 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Tetrachloroethene 129 0.441 0.377 871 2.99 2.56
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)761,368 11.02 5.21 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
Air
TDD
Xavier
0124-075.SG-2.Can
X2400665.D
4.000
2.696
2024-02-06 07:44
TO15_SCNV6.M
0124-075; *4=125mL Load; Can #13542
2024-01-31 13:11
2024-02-01 00:00
Sample
Xavier_X020524A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-2
EA # 0124-075 Page 15 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene 153 146 132 262 250 227
Freon 12 (CCl2F2)ND 148 132 ND 729 652
Freon 114 (C2Cl2F4)ND 151 132 ND 1,055 921
Chloromethane ND 149 132 ND 308 272
Chloroethene (Vinyl chloride)ND 151 132 ND 385 337
1,3-Butadiene ND 147 132 ND 324 291
Bromomethane ND 148 132 ND 574 512
Chloroethane ND 153 132 ND 404 348
Bromoethene (Vinyl bromide)ND 147 132 ND 644 576
Freon 11 (CCl3F)ND 159 132 ND 893 740
Ethanol ND 149 149 ND 281 281
Acrolein ND 148 132 ND 340 302
Freon 113 (C2Cl3F3)ND 153 132 ND 1,171 1,010
1,1-Dichloroethene ND 152 132 ND 601 522
Acetone ND 151 132 ND 358 313
Carbon disulfide ND 150 132 ND 468 410
Isopropyl alcohol ND 150 132 ND 369 324
Allyl chloride (3-chloropropene)ND 163 132 ND 509 412
Acetonitrile ND 150 132 ND 252 221
Methylene chloride ND 154 132 ND 536 458
trans-1,2-Dichloroethene ND 154 132 ND 609 522
Methyl tert-butyl ether ND 155 132 ND 558 475
Acrylonitrile ND 153 132 ND 333 286
Hexane ND 153 132 ND 539 464
1,1-Dichloroethane ND 150 132 ND 605 533
Vinyl acetate ND 154 132 ND 542 464
cis-1,2-Dichloroethene 5,874 152 132 23,276 603 522
Methyl ethyl ketone (2-Butanone)ND 156 132 ND 459 389
Ethyl acetate ND 150 132 ND 542 475
Chloroform 239 151 132 1,165 737 643
Tetrahydrofuran ND 152 132 ND 449 389
Air
TDD
Xavier
0124-075.SG-1.CanP2
X2400715.D
1000.000
3.767
2024-02-08 06:35
TO15_SCNV6.M
0124-075; *1000=0.5mL load (2nd TP); Can #12423; MP2
2024-01-31 13:50
2024-02-01 00:00
Sample
Xavier_X020724A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-1
EA # 0124-075 Page 16 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0124-075.SG-1.CanP2
X2400715.D
1000.000
3.767
2024-02-08 06:35
TO15_SCNV6.M
0124-075; *1000=0.5mL load (2nd TP); Can #12423; MP2
2024-01-31 13:50
2024-02-01 00:00
Sample
Xavier_X020724A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-1
1,1,1-Trichloroethane ND 152 132 ND 830 719
Cyclohexane 199 154 132 686 531 454 m
Carbon tetrachloride ND 152 132 ND 954 829
Benzene ND 152 132 ND 484 421
2,2,4-trimethylpentane ND 156 132 ND 727 616
1,2-Dichloroethane ND 155 132 ND 627 533
Heptane ND 153 132 ND 625 540
Trichloroethene 11,969 152 132 64,278 818 708
1,2-Dichloropropane ND 152 132 ND 701 609
Methyl methacrylate ND 158 132 ND 646 540
1,4-Dioxane ND 151 132 ND 544 475
Bromodichloromethane ND 152 132 ND 1,019 883
cis-1,3-Dichloropropene ND 150 132 ND 679 598
Methyl isobutyl ketone ND 157 132 ND 641 540
Toluene ND 153 132 ND 578 497
trans-1,3-Dichloropropene ND 156 132 ND 705 598
1,1,2-Trichloroethane ND 153 132 ND 836 719
2-Hexanone (Methyl butyl ketone)ND 154 132 ND 631 540
Dibromochloromethane ND 152 132 ND 1,293 1,122
1,2-Dibromoethane ND 154 132 ND 1,184 1,012
Chlorobenzene ND 155 132 ND 714 607
Ethylbenzene ND 150 132 ND 649 572
1,1,1,2-Tetrachloroethane ND 152 132 ND 1,042 905
m-/p-Xylenes ND 153 132 ND 663 572
o-Xylene ND 151 132 ND 655 572
Styrene ND 148 132 ND 629 561
Bromoform ND 151 132 ND 1,561 1,362
1,1,2,2-Tetrachloroethane 195 152 132 1,336 1,045 905 m
4-Ethyltoluene ND 153 132 ND 753 648
2-Chlorotoluene ND 152 132 ND 787 682
1,3,5-Trimethylbenzene ND 153 132 ND 751 648
EA # 0124-075 Page 17 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0124-075.SG-1.CanP2
X2400715.D
1000.000
3.767
2024-02-08 06:35
TO15_SCNV6.M
0124-075; *1000=0.5mL load (2nd TP); Can #12423; MP2
2024-01-31 13:50
2024-02-01 00:00
Sample
Xavier_X020724A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-1
1,2,4-Trimethylbenzene ND 151 132 ND 741 648
1,3-Dichlorobenzene ND 153 132 ND 920 792
1,4-Dichlorobenzene ND 151 132 ND 910 792
Benzyl chloride ND 152 132 ND 784 682
1,2-Dichlorobenzene ND 153 132 ND 917 792
1,2,4-Trichlorobenzene ND 150 132 ND 1,113 978
Hexachlorobutadiene ND 149 132 ND 1,587 1,405
Naphthalene ND 152 132 ND 795 691
1-Bromopropane ND 149 132 ND 751 663
1-Octene ND 149 132 ND 682 605
n-Octane ND 155 132 ND 725 616
Isopropylbenzene ND 153 132 ND 752 648
n-Propylbenzene ND 155 132 ND 759 648
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)757,494 11.02 5.21 pass
1,4-Difluorobenzene (IS)2,942,726 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,579,309 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 18 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Tetrachloroethene 301,437 1,541 1,318 2,043,185 10,448 8,937
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)774,435 11.02 5.21 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
Air
TDD
Xavier
0124-075.SG-1.CanP2
X2400693.D
10000.000
3.767
2024-02-07 11:23
TO15_SCNV6.M
0124-075; *10,000=0.5mL Loop@10xSyrDil (2nd TP); Can #12423; MP2
2024-01-31 13:50
2024-02-01 00:00
Sample
Xavier_X020624A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-1
EA # 0124-075 Page 19 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene 37.5 0.203 0.184 64.5 0.349 0.316
Freon 12 (CCl2F2)0.467 0.205 0.184 2.31 1.01 0.907
Freon 114 (C2Cl2F4)ND 0.210 0.184 ND 1.47 1.28
Chloromethane 0.352 0.207 0.184 0.727 0.428 0.379
Chloroethene (Vinyl chloride)ND 0.210 0.184 ND 0.535 0.469
1,3-Butadiene 2.39 0.204 0.184 5.28 0.451 0.406
Bromomethane ND 0.206 0.184 ND 0.799 0.712
Chloroethane ND 0.213 0.184 ND 0.562 0.484
Bromoethene (Vinyl bromide)ND 0.205 0.184 ND 0.897 0.802
Freon 11 (CCl3F)0.230 0.221 0.184 1.29 1.24 1.03
Ethanol 2.41 0.208 0.208 4.54 0.391 0.391
Acrolein 0.298 0.207 0.184 0.682 0.473 0.421 m
Freon 113 (C2Cl3F3)ND 0.213 0.184 ND 1.63 1.41
1,1-Dichloroethene ND 0.211 0.184 ND 0.836 0.727
Acetone 13.1 0.210 0.184 31.0 0.499 0.436
Carbon disulfide 14.9 0.209 0.184 46.3 0.651 0.571
Isopropyl alcohol 0.872 0.209 0.184 2.14 0.514 0.451
Allyl chloride (3-chloropropene)ND 0.227 0.184 ND 0.709 0.574
Acetonitrile ND 0.209 0.184 ND 0.351 0.308
Methylene chloride 0.245 0.215 0.184 0.849 0.746 0.637
trans-1,2-Dichloroethene ND 0.214 0.184 ND 0.848 0.727
Methyl tert-butyl ether 0.224 0.216 0.184 0.806 0.777 0.661
Acrylonitrile ND 0.214 0.184 ND 0.463 0.398
Hexane 1.23 0.213 0.184 4.32 0.751 0.647
1,1-Dichloroethane ND 0.208 0.184 ND 0.843 0.742
Vinyl acetate ND 0.215 0.184 ND 0.755 0.646
cis-1,2-Dichloroethene 0.303 0.212 0.184 1.20 0.839 0.727
Methyl ethyl ketone (2-Butanone)0.691 0.217 0.184 2.04 0.639 0.541
Ethyl acetate 0.356 0.209 0.184 1.28 0.754 0.661
Chloroform 0.407 0.210 0.184 1.99 1.03 0.896
Tetrahydrofuran ND 0.212 0.184 ND 0.626 0.541
Air
TDD
Xavier
0124-075.SG-10.Can
X2400663.D
2.000
2.622
2024-02-06 03:51
TO15_SCNV6.M
0124-075; *2=250mL Load; Can #11251
2024-01-31 14:32
2024-02-01 00:00
Sample
Xavier_X020524A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-10
EA # 0124-075 Page 20 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
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Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0124-075.SG-10.Can
X2400663.D
2.000
2.622
2024-02-06 03:51
TO15_SCNV6.M
0124-075; *2=250mL Load; Can #11251
2024-01-31 14:32
2024-02-01 00:00
Sample
Xavier_X020524A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-10
1,1,1-Trichloroethane ND 0.212 0.184 ND 1.16 1.00
Cyclohexane 0.639 0.215 0.184 2.20 0.740 0.631
Carbon tetrachloride ND 0.211 0.184 ND 1.33 1.15
Benzene 1.28 0.211 0.184 4.08 0.674 0.586
2,2,4-trimethylpentane 0.218 0.217 0.184 1.02 1.01 0.857
1,2-Dichloroethane ND 0.216 0.184 ND 0.873 0.742
Heptane 0.575 0.212 0.184 2.36 0.870 0.752
Trichloroethene 0.489 0.212 0.184 2.63 1.14 0.986
1,2-Dichloropropane ND 0.211 0.184 ND 0.976 0.848
Methyl methacrylate ND 0.220 0.184 ND 0.899 0.751
1,4-Dioxane ND 0.210 0.184 ND 0.758 0.661
Bromodichloromethane ND 0.212 0.184 ND 1.42 1.23
cis-1,3-Dichloropropene ND 0.208 0.184 ND 0.945 0.833
Methyl isobutyl ketone 3.55 0.218 0.184 14.5 0.892 0.751
Toluene 3.88 0.214 0.184 14.6 0.804 0.691
trans-1,3-Dichloropropene ND 0.216 0.184 ND 0.982 0.833
1,1,2-Trichloroethane ND 0.213 0.184 ND 1.16 1.00
Tetrachloroethene 34.8 0.215 0.184 236 1.45 1.24
2-Hexanone (Methyl butyl ketone)2.03 0.215 0.184 8.29 0.879 0.751 m
Dibromochloromethane ND 0.211 0.184 ND 1.80 1.56
1,2-Dibromoethane ND 0.215 0.184 ND 1.65 1.41
Chlorobenzene ND 0.216 0.184 ND 0.994 0.844
Ethylbenzene 3.13 0.208 0.184 13.6 0.904 0.796
1,1,1,2-Tetrachloroethane ND 0.211 0.184 ND 1.45 1.26
m-/p-Xylenes 12.4 0.213 0.184 53.6 0.923 0.796
o-Xylene 8.51 0.210 0.184 36.9 0.912 0.796
Styrene 0.367 0.206 0.184 1.56 0.875 0.781 m
Bromoform ND 0.210 0.184 ND 2.17 1.90
1,1,2,2-Tetrachloroethane 0.248 0.212 0.184 1.70 1.45 1.26
4-Ethyltoluene 0.722 0.213 0.184 3.55 1.05 0.902 m
2-Chlorotoluene ND 0.212 0.184 ND 1.10 0.950
EA # 0124-075 Page 21 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0124-075.SG-10.Can
X2400663.D
2.000
2.622
2024-02-06 03:51
TO15_SCNV6.M
0124-075; *2=250mL Load; Can #11251
2024-01-31 14:32
2024-02-01 00:00
Sample
Xavier_X020524A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-10
1,3,5-Trimethylbenzene 1.10 0.213 0.184 5.39 1.04 0.902
1,2,4-Trimethylbenzene 4.43 0.210 0.184 21.7 1.03 0.902
1,3-Dichlorobenzene ND 0.213 0.184 ND 1.28 1.10
1,4-Dichlorobenzene ND 0.211 0.184 ND 1.27 1.10
Benzyl chloride ND 0.211 0.184 ND 1.09 0.950
1,2-Dichlorobenzene ND 0.212 0.184 ND 1.28 1.10
1,2,4-Trichlorobenzene ND 0.209 0.184 ND 1.55 1.36
Hexachlorobutadiene ND 0.207 0.184 ND 2.21 1.96
Naphthalene 0.216 0.211 0.184 1.13 1.11 0.962 m
1-Bromopropane ND 0.208 0.184 ND 1.05 0.923
1-Octene 6.13 0.207 0.184 28.1 0.950 0.842
n-Octane 20.3 0.216 0.184 94.6 1.01 0.857
Isopropylbenzene 0.282 0.213 0.184 1.39 1.05 0.902
n-Propylbenzene 0.439 0.215 0.184 2.16 1.06 0.902
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)781,565 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,028,498 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,608,714 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 22 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene 130 15.9 14.4 223 27.3 24.7
Freon 12 (CCl2F2)ND 16.1 14.4 ND 79.5 71.1
Freon 114 (C2Cl2F4)ND 16.5 14.4 ND 115 100
Chloromethane ND 16.3 14.4 ND 33.6 29.7
Chloroethene (Vinyl chloride)420 16.4 14.4 1,072 42.0 36.7 m
1,3-Butadiene ND 16.0 14.4 ND 35.4 31.8
Bromomethane ND 16.1 14.4 ND 62.6 55.8
Chloroethane ND 16.7 14.4 ND 44.0 37.9
Bromoethene (Vinyl bromide)ND 16.1 14.4 ND 70.3 62.9
Freon 11 (CCl3F)ND 17.3 14.4 ND 97.4 80.8
Ethanol 19.9 16.3 16.3 37.5 30.7 30.7
Acrolein ND 16.2 14.4 ND 37.1 33.0
Freon 113 (C2Cl3F3)ND 16.7 14.4 ND 128 110
1,1-Dichloroethene 489 16.5 14.4 1,939 65.5 57.0
Acetone 2,055 16.5 14.4 4,878 39.1 34.1
Carbon disulfide 22.5 16.4 14.4 70.1 51.0 44.8 m
Isopropyl alcohol ND 16.4 14.4 ND 40.3 35.3
Allyl chloride (3-chloropropene)ND 17.8 14.4 ND 55.5 45.0
Acetonitrile ND 16.4 14.4 ND 27.5 24.1
Methylene chloride 34.2 16.8 14.4 119 58.4 49.9 m
trans-1,2-Dichloroethene 111 16.8 14.4 439 66.4 57.0
Methyl tert-butyl ether ND 16.9 14.4 ND 60.9 51.8
Acrylonitrile 472 16.7 14.4 1,023 36.3 31.2
Hexane 4,497 16.7 14.4 15,840 58.8 50.7
1,1-Dichloroethane ND 16.3 14.4 ND 66.0 58.2
Vinyl acetate ND 16.8 14.4 ND 59.2 50.6
Methyl ethyl ketone (2-Butanone)ND 17.0 14.4 ND 50.1 42.4
Ethyl acetate ND 16.4 14.4 ND 59.1 51.8
Chloroform 133 16.5 14.4 650 80.5 70.2
Tetrahydrofuran ND 16.6 14.4 ND 49.0 42.4
1,1,1-Trichloroethane ND 16.6 14.4 ND 90.5 78.4
Air
TDD
Xavier
0124-075.SG-11.CanP2
X2400741.D
100.000
4.110
2024-02-09 07:25
TO15_SCNV6.M
0124-075; *100=5mL load (2nd TP); Can #13541; MP2
2024-01-31 14:52
2024-02-01 00:00
Sample
Xavier_X020924A_0124-075.v2
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-11
EA # 0124-075 Page 23 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0124-075.SG-11.CanP2
X2400741.D
100.000
4.110
2024-02-09 07:25
TO15_SCNV6.M
0124-075; *100=5mL load (2nd TP); Can #13541; MP2
2024-01-31 14:52
2024-02-01 00:00
Sample
Xavier_X020924A_0124-075.v2
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-11
Cyclohexane 5,347 16.8 14.4 18,395 58.0 49.5
Carbon tetrachloride ND 16.6 14.4 ND 104 90.4
Benzene 43.1 16.5 14.4 138 52.8 45.9
2,2,4-trimethylpentane 213 17.0 14.4 994 79.4 67.2 m
1,2-Dichloroethane ND 16.9 14.4 ND 68.4 58.2
Heptane 2,124 16.7 14.4 8,701 68.2 58.9
1,2-Dichloropropane 320 16.6 14.4 1,476 76.4 66.4 m
Methyl methacrylate 8,721 17.2 14.4 35,691 70.4 58.9
1,4-Dioxane ND 16.5 14.4 ND 59.4 51.8
Bromodichloromethane ND 16.6 14.4 ND 111 96.3
cis-1,3-Dichloropropene ND 16.3 14.4 ND 74.0 65.2
Methyl isobutyl ketone 301 17.1 14.4 1,231 69.9 58.9
Toluene ND 16.7 14.4 ND 63.0 54.2
trans-1,3-Dichloropropene ND 17.0 14.4 ND 76.9 65.2
1,1,2-Trichloroethane ND 16.7 14.4 ND 91.2 78.4
2-Hexanone (Methyl butyl ketone)4,738 16.8 14.4 19,398 68.8 58.9 m
Dibromochloromethane ND 16.6 14.4 ND 141 122
1,2-Dibromoethane ND 16.8 14.4 ND 129 110
Chlorobenzene 21.5 16.9 14.4 99.0 77.9 66.2
Ethylbenzene 502 16.3 14.4 2,178 70.8 62.4
1,1,1,2-Tetrachloroethane ND 16.6 14.4 ND 114 98.7
m-/p-Xylenes 73.1 16.7 14.4 317 72.3 62.4
o-Xylene ND 16.5 14.4 ND 71.5 62.4
Styrene ND 16.1 14.4 ND 68.6 61.2
Bromoform ND 16.5 14.4 ND 170 149
1,1,2,2-Tetrachloroethane 897 16.6 14.4 6,154 114 98.7 m
4-Ethyltoluene 642 16.7 14.4 3,154 82.1 70.7 m
2-Chlorotoluene ND 16.6 14.4 ND 85.8 74.4
1,3,5-Trimethylbenzene 407 16.7 14.4 2,001 81.9 70.7
1,2,4-Trimethylbenzene 1,853 16.5 14.4 9,101 80.8 70.7
1,3-Dichlorobenzene ND 16.7 14.4 ND 100 86.4
EA # 0124-075 Page 24 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0124-075.SG-11.CanP2
X2400741.D
100.000
4.110
2024-02-09 07:25
TO15_SCNV6.M
0124-075; *100=5mL load (2nd TP); Can #13541; MP2
2024-01-31 14:52
2024-02-01 00:00
Sample
Xavier_X020924A_0124-075.v2
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-11
1,4-Dichlorobenzene ND 16.5 14.4 ND 99.3 86.4
Benzyl chloride 284 16.5 14.4 1,467 85.6 74.4 m
1,2-Dichlorobenzene ND 16.7 14.4 ND 100 86.4
1,2,4-Trichlorobenzene ND 16.4 14.4 ND 121 107
Hexachlorobutadiene ND 16.2 14.4 ND 173 153
Naphthalene ND 16.6 14.4 ND 86.7 75.4
1-Bromopropane ND 16.3 14.4 ND 82.0 72.3
1-Octene 2,281 16.2 14.4 10,460 74.4 66.0
n-Octane 1,675 16.9 14.4 7,821 79.1 67.2
Isopropylbenzene 544 16.7 14.4 2,672 82.0 70.7 m
n-Propylbenzene 1,164 16.9 14.4 5,719 82.9 70.7
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)890,488 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,396,180 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,992,102 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 25 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
cis-1,2-Dichloroethene 39,653 1,660 1,438 157,117 6,578 5,699
Trichloroethene 43,387 1,662 1,438 233,007 8,925 7,724
Tetrachloroethene 255,124 1,682 1,438 1,729,266 11,398 9,749 m
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)774,578 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,019,070 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,635,794 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
Air
TDD
Xavier
0124-075.SG-11.CanP2
X2400692.D
10000.000
4.110
2024-02-07 10:23
TO15_SCNV6.M
0124-075; *10,000=0.5mL Loop@10xSyrDil (2nd TP); Can #13541; MP2
2024-01-31 14:52
2024-02-01 00:00
Sample
Xavier_X020624A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-11
EA # 0124-075 Page 26 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene 0.915 0.0967 0.0876 1.57 0.166 0.151
Freon 12 (CCl2F2)0.469 0.0980 0.0876 2.32 0.484 0.433
Freon 114 (C2Cl2F4)ND 0.100 0.0876 ND 0.700 0.612
Chloromethane 0.196 0.0990 0.0876 0.405 0.204 0.181
Chloroethene (Vinyl chloride)ND 0.1000 0.0876 ND 0.255 0.224
1,3-Butadiene ND 0.0974 0.0876 ND 0.215 0.194
Bromomethane ND 0.0982 0.0876 ND 0.381 0.340
Chloroethane ND 0.102 0.0876 ND 0.268 0.231
Bromoethene (Vinyl bromide)ND 0.0979 0.0876 ND 0.428 0.383
Freon 11 (CCl3F)0.245 0.106 0.0876 1.38 0.593 0.492
Ethanol 0.866 0.0992 0.0992 1.63 0.187 0.187
Acrolein ND 0.0986 0.0876 ND 0.226 0.201
Freon 113 (C2Cl3F3)ND 0.102 0.0876 ND 0.778 0.671
1,1-Dichloroethene ND 0.101 0.0876 ND 0.399 0.347
Acetone 7.37 0.100 0.0876 17.5 0.238 0.208
Carbon disulfide 0.378 0.0998 0.0876 1.18 0.310 0.272
Isopropyl alcohol 0.423 0.0998 0.0876 1.04 0.245 0.215 m
Allyl chloride (3-chloropropene)ND 0.108 0.0876 ND 0.338 0.274
Acetonitrile ND 0.0998 0.0876 ND 0.167 0.147
Methylene chloride 0.104 0.102 0.0876 0.363 0.356 0.304
trans-1,2-Dichloroethene ND 0.102 0.0876 ND 0.404 0.347
Methyl tert-butyl ether ND 0.103 0.0876 ND 0.371 0.315
Acrylonitrile ND 0.102 0.0876 ND 0.221 0.190
Hexane 0.237 0.102 0.0876 0.833 0.358 0.308
1,1-Dichloroethane ND 0.0994 0.0876 ND 0.402 0.354
Vinyl acetate ND 0.102 0.0876 ND 0.360 0.308
cis-1,2-Dichloroethene ND 0.101 0.0876 ND 0.400 0.347
Methyl ethyl ketone (2-Butanone)0.233 0.103 0.0876 0.687 0.305 0.258 m
Ethyl acetate ND 0.0999 0.0876 ND 0.360 0.315
Chloroform 0.168 0.100 0.0876 0.822 0.490 0.427
Tetrahydrofuran 0.209 0.101 0.0876 0.617 0.298 0.258
Air
TDD
Xavier
0124-075.SG-6.Can
X2400662.D
1.000
2.502
2024-02-06 03:00
TO15_SCNV6.M
0124-075; 500mL Load; Can #5731
2024-02-01 09:20
2024-02-01 00:00
Sample
Xavier_X020524A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-6
EA # 0124-075 Page 27 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0124-075.SG-6.Can
X2400662.D
1.000
2.502
2024-02-06 03:00
TO15_SCNV6.M
0124-075; 500mL Load; Can #5731
2024-02-01 09:20
2024-02-01 00:00
Sample
Xavier_X020524A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-6
1,1,1-Trichloroethane ND 0.101 0.0876 ND 0.551 0.477
Cyclohexane 0.0949 0.103 0.0876 0.326 0.353 0.301 J
Carbon tetrachloride ND 0.101 0.0876 ND 0.634 0.550
Benzene ND 0.101 0.0876 ND 0.321 0.280
2,2,4-trimethylpentane ND 0.103 0.0876 ND 0.483 0.409
1,2-Dichloroethane ND 0.103 0.0876 ND 0.416 0.354
Heptane ND 0.101 0.0876 ND 0.415 0.359
Trichloroethene ND 0.101 0.0876 ND 0.543 0.470
1,2-Dichloropropane ND 0.101 0.0876 ND 0.465 0.404
Methyl methacrylate ND 0.105 0.0876 ND 0.429 0.358
1,4-Dioxane ND 0.100 0.0876 ND 0.361 0.315
Bromodichloromethane ND 0.101 0.0876 ND 0.677 0.586
cis-1,3-Dichloropropene ND 0.0994 0.0876 ND 0.451 0.397
Methyl isobutyl ketone 0.0973 0.104 0.0876 0.398 0.426 0.358 J
Toluene 0.521 0.102 0.0876 1.96 0.384 0.330
trans-1,3-Dichloropropene ND 0.103 0.0876 ND 0.468 0.397
1,1,2-Trichloroethane ND 0.102 0.0876 ND 0.555 0.477
Tetrachloroethene 19.6 0.102 0.0876 133 0.694 0.593
2-Hexanone (Methyl butyl ketone)0.0967 0.102 0.0876 0.396 0.419 0.358 J
Dibromochloromethane ND 0.101 0.0876 ND 0.859 0.745
1,2-Dibromoethane ND 0.102 0.0876 ND 0.786 0.672
Chlorobenzene ND 0.103 0.0876 ND 0.474 0.403
Ethylbenzene ND 0.0994 0.0876 ND 0.431 0.380
1,1,1,2-Tetrachloroethane ND 0.101 0.0876 ND 0.692 0.601
m-/p-Xylenes ND 0.101 0.0876 ND 0.440 0.380
o-Xylene ND 0.100 0.0876 ND 0.435 0.380
Styrene ND 0.0981 0.0876 ND 0.417 0.373
Bromoform ND 0.100 0.0876 ND 1.04 0.904
1,1,2,2-Tetrachloroethane ND 0.101 0.0876 ND 0.694 0.601
4-Ethyltoluene ND 0.102 0.0876 ND 0.500 0.430
2-Chlorotoluene ND 0.101 0.0876 ND 0.522 0.453
EA # 0124-075 Page 28 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0124-075.SG-6.Can
X2400662.D
1.000
2.502
2024-02-06 03:00
TO15_SCNV6.M
0124-075; 500mL Load; Can #5731
2024-02-01 09:20
2024-02-01 00:00
Sample
Xavier_X020524A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-6
1,3,5-Trimethylbenzene ND 0.101 0.0876 ND 0.498 0.430
1,2,4-Trimethylbenzene ND 0.100 0.0876 ND 0.492 0.430
1,3-Dichlorobenzene ND 0.102 0.0876 ND 0.611 0.526
1,4-Dichlorobenzene ND 0.101 0.0876 ND 0.604 0.526
Benzyl chloride ND 0.101 0.0876 ND 0.521 0.453
1,2-Dichlorobenzene ND 0.101 0.0876 ND 0.609 0.526
1,2,4-Trichlorobenzene ND 0.0997 0.0876 ND 0.739 0.649
Hexachlorobutadiene ND 0.0989 0.0876 ND 1.05 0.933
Naphthalene ND 0.101 0.0876 ND 0.528 0.459
1-Bromopropane ND 0.0993 0.0876 ND 0.499 0.440
1-Octene ND 0.0988 0.0876 ND 0.453 0.402
n-Octane ND 0.103 0.0876 ND 0.481 0.409
Isopropylbenzene ND 0.102 0.0876 ND 0.499 0.430
n-Propylbenzene ND 0.103 0.0876 ND 0.504 0.430
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)786,425 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,020,836 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,606,419 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 29 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene 18.2 0.101 0.0918 31.3 0.174 0.158
Freon 12 (CCl2F2)0.456 0.103 0.0918 2.25 0.508 0.454 m
Freon 114 (C2Cl2F4)ND 0.105 0.0918 ND 0.734 0.641
Chloromethane 0.0976 0.104 0.0918 0.201 0.214 0.189 J
Chloroethene (Vinyl chloride)ND 0.105 0.0918 ND 0.268 0.235
1,3-Butadiene 0.276 0.102 0.0918 0.610 0.226 0.203
Bromomethane ND 0.103 0.0918 ND 0.399 0.356
Chloroethane 0.0942 0.107 0.0918 0.248 0.281 0.242 J, m
Bromoethene (Vinyl bromide)ND 0.103 0.0918 ND 0.449 0.401
Freon 11 (CCl3F)0.197 0.111 0.0918 1.11 0.621 0.515
Ethanol 0.709 0.104 0.104 1.33 0.196 0.196 m
Acrolein 1.96 0.103 0.0918 4.50 0.237 0.210 m
Freon 113 (C2Cl3F3)ND 0.106 0.0918 ND 0.816 0.703
1,1-Dichloroethene ND 0.106 0.0918 ND 0.418 0.364
Acetone 3.74 0.105 0.0918 8.88 0.250 0.218
Carbon disulfide 3.10 0.105 0.0918 9.66 0.326 0.286
Isopropyl alcohol 0.208 0.105 0.0918 0.510 0.257 0.225
Allyl chloride (3-chloropropene)ND 0.113 0.0918 ND 0.354 0.287
Acetonitrile ND 0.105 0.0918 ND 0.175 0.154
Methylene chloride 0.141 0.107 0.0918 0.490 0.373 0.319 m
trans-1,2-Dichloroethene ND 0.107 0.0918 ND 0.424 0.364
Methyl tert-butyl ether ND 0.108 0.0918 ND 0.389 0.331
Acrylonitrile ND 0.107 0.0918 ND 0.232 0.199
Hexane 0.916 0.107 0.0918 3.23 0.375 0.323
1,1-Dichloroethane ND 0.104 0.0918 ND 0.421 0.371
Vinyl acetate ND 0.107 0.0918 ND 0.378 0.323
cis-1,2-Dichloroethene 1.52 0.106 0.0918 6.04 0.420 0.364
Methyl ethyl ketone (2-Butanone)0.380 0.108 0.0918 1.12 0.320 0.271
Ethyl acetate ND 0.105 0.0918 ND 0.377 0.331
Chloroform 0.117 0.105 0.0918 0.570 0.513 0.448
Tetrahydrofuran 0.161 0.106 0.0918 0.475 0.313 0.271
Air
KMB
Xavier
0124-075.SG-4.Can
X2400596.D
1.000
2.623
2024-02-01 22:42
TO15_SCNV6.M
0124-075; 500mL Load; Can #5703/C10119
2024-02-01 10:19
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-4
EA # 0124-075 Page 30 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
KMB
Xavier
0124-075.SG-4.Can
X2400596.D
1.000
2.623
2024-02-01 22:42
TO15_SCNV6.M
0124-075; 500mL Load; Can #5703/C10119
2024-02-01 10:19
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-4
1,1,1-Trichloroethane ND 0.106 0.0918 ND 0.578 0.501
Cyclohexane 1.65 0.108 0.0918 5.67 0.370 0.316
Carbon tetrachloride ND 0.106 0.0918 ND 0.664 0.577
Benzene 0.122 0.106 0.0918 0.389 0.337 0.293
2,2,4-trimethylpentane 0.311 0.108 0.0918 1.45 0.506 0.429
1,2-Dichloroethane 0.110 0.108 0.0918 0.445 0.437 0.371
Heptane 0.340 0.106 0.0918 1.39 0.435 0.376
Trichloroethene 1.68 0.106 0.0918 9.03 0.570 0.493
1,2-Dichloropropane ND 0.106 0.0918 ND 0.488 0.424
Methyl methacrylate 1.01 0.110 0.0918 4.15 0.449 0.376
1,4-Dioxane ND 0.105 0.0918 ND 0.379 0.331
Bromodichloromethane ND 0.106 0.0918 ND 0.710 0.615
cis-1,3-Dichloropropene ND 0.104 0.0918 ND 0.473 0.416
Methyl isobutyl ketone 8.73 0.109 0.0918 35.7 0.446 0.376
Toluene 0.903 0.107 0.0918 3.40 0.402 0.346
trans-1,3-Dichloropropene ND 0.108 0.0918 ND 0.491 0.416
1,1,2-Trichloroethane 0.916 0.107 0.0918 4.99 0.582 0.501
2-Hexanone (Methyl butyl ketone)3.53 0.107 0.0918 14.5 0.439 0.376
Dibromochloromethane ND 0.106 0.0918 ND 0.900 0.781
1,2-Dibromoethane ND 0.107 0.0918 ND 0.824 0.705
Chlorobenzene ND 0.108 0.0918 ND 0.497 0.422
Ethylbenzene 0.167 0.104 0.0918 0.726 0.452 0.398
1,1,1,2-Tetrachloroethane ND 0.106 0.0918 ND 0.726 0.630
m-/p-Xylenes 0.796 0.106 0.0918 3.45 0.462 0.398
o-Xylene 0.344 0.105 0.0918 1.49 0.456 0.398
Styrene ND 0.103 0.0918 ND 0.438 0.391
Bromoform ND 0.105 0.0918 ND 1.09 0.948
1,1,2,2-Tetrachloroethane 0.250 0.106 0.0918 1.72 0.728 0.630 m
4-Ethyltoluene 0.0972 0.107 0.0918 0.478 0.524 0.451 J, m
2-Chlorotoluene ND 0.106 0.0918 ND 0.548 0.475
1,3,5-Trimethylbenzene 0.197 0.106 0.0918 0.966 0.523 0.451 m
EA # 0124-075 Page 31 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
KMB
Xavier
0124-075.SG-4.Can
X2400596.D
1.000
2.623
2024-02-01 22:42
TO15_SCNV6.M
0124-075; 500mL Load; Can #5703/C10119
2024-02-01 10:19
2024-02-01 00:00
Sample
Xavier_X020124A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-4
1,2,4-Trimethylbenzene 0.552 0.105 0.0918 2.71 0.516 0.451
1,3-Dichlorobenzene ND 0.107 0.0918 ND 0.640 0.552
1,4-Dichlorobenzene ND 0.105 0.0918 ND 0.633 0.552
Benzyl chloride ND 0.106 0.0918 ND 0.546 0.475
1,2-Dichlorobenzene ND 0.106 0.0918 ND 0.639 0.552
1,2,4-Trichlorobenzene ND 0.104 0.0918 ND 0.775 0.681
Hexachlorobutadiene ND 0.104 0.0918 ND 1.10 0.978
Naphthalene ND 0.106 0.0918 ND 0.553 0.481
1-Bromopropane ND 0.104 0.0918 ND 0.523 0.461
1-Octene 2.03 0.104 0.0918 9.32 0.475 0.421
n-Octane 0.628 0.108 0.0918 2.93 0.505 0.429
Isopropylbenzene 0.184 0.107 0.0918 0.904 0.524 0.451
n-Propylbenzene ND 0.108 0.0918 ND 0.529 0.451
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)714,424 11.02 5.21 pass
1,4-Difluorobenzene (IS)2,710,198 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,332,221 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 32 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Tetrachloroethene 182 0.537 0.459 1,236 3.64 3.11
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)812,295 11.02 5.21 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
Air
TDD
Xavier
0124-075.SG-4.Can
X2400664.D
5.000
2.623
2024-02-06 06:55
TO15_SCNV6.M
0124-075; *5=100mL Load; Can #5703/C10119
2024-02-01 10:19
2024-02-01 00:00
Sample
Xavier_X020524A_0124-075.v1
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-4
EA # 0124-075 Page 33 of 85
Job No.
Company
Site
Can Number 12165 6041 13542 11251 5731 5703
Job 0124-075 0124-075 0124-075 0124-075 0124-075 0124-075
Sample ID SG-5 SG-3 SG-2 SG-10 SG-6 SG-4
CleanDate 01/25/2024 01/10/2024 01/18/2024 01/09/2024 01/18/2024 01/09/2024
LeakCheckDate 01/26/2024 01/16/2024 01/23/2024 01/11/2024 01/23/2024 01/11/2024
LeakCheckAnalyst pamooney pamooney pamooney pamooney pamooney pamooney
BlankCheckRef Y2400259 Y2400151 Y2400231 Y2400143 Y2400229 Y2400145
Weather Station ID 88 88 88 88 88 88
Weather Station Exp.02/02/2024 02/02/2024 02/02/2024 02/02/2024 02/02/2024 02/02/2024
Transducer ID 3 3 3 3 3 3
Transducer Exp.11/17/2024 11/17/2024 11/17/2024 11/17/2024 11/17/2024 11/17/2024
Can Size (L)1.4 1.4 1.4 1.4 1.4 1.4
Evac Temp (F)65.9 65.9 65.9 65.9 65.9 65.9
Evac Pbar (mmHg)761.0 761.0 761.0 761.0 761.0 761.0
Evac Gauge (mmHg)-761.0 -761.0 -761.0 -761.0 -761.0 -761.0
Evac Analyst pamooney pamooney pamooney pamooney pamooney pamooney
Evac Time 01/26/24 08:40 01/25/24 10:35 01/25/24 10:47 01/25/24 10:26 01/25/24 10:21 01/25/24 10:15
Evac Vol (L)0.000 0.000 0.000 0.000 0.000 0.000
Recd. Temp (F)66.7 66.7 66.7 66.7 66.7 66.7
Recd. Pbar (mmHg)757.7 757.7 757.7 757.7 757.7 757.7
Recd. Gauge (mmHg)-143.0 -175.0 -220.0 -209.0 -183.0 -208.0
Recd Vol (L)1.135 1.076 0.993 1.013 1.061 1.015
P1 Temp (F)66.7 66.7 66.7 66.7 66.7 66.7
P1 Pbar (mmHg)757.7 757.7 757.7 757.7 757.7 757.7
P1 Gauge (mmHg)665.0 684.0 692.0 681.0 680.0 684.0
P1 Analyst pamooney pamooney pamooney pamooney pamooney pamooney
P1 Time 02/01/24 13:09 02/01/24 13:15 02/01/24 13:19 02/01/24 13:30 02/01/24 13:47 02/01/24 13:51
P1 Fill Gas Nitrogen Nitrogen Nitrogen Nitrogen Nitrogen Nitrogen
P1 Vol (L)2.627 2.662 2.677 2.657 2.655 2.662
P1 DF Override false false false false false false
P1 Dilution Factor 2.315 2.474 2.696 2.622 2.502 2.623
Enthalpy Analytical -- Canister Pressurization
0124-075
AECOM - Morrisville
Frye & Webster DC410064
Canister Pressurization Report 20230531 Report Printed 2/12/2024 12:41:56 PM
EA # 0124-075 Page 34 of 85
Job No.
Company
Site
Can Number 12423 13541
Job 0124-075 0124-075
Sample ID SG-1 SG-11
CleanDate 01/17/2024 01/17/2024
LeakCheckDate 01/19/2024 01/19/2024
LeakCheckAnalyst pamooney pamooney
BlankCheckRef X2400323 Y2400322
Weather Station ID 88 88
Weather Station Exp.02/02/2024 02/02/2024
Transducer ID 3 3
Transducer Exp.11/17/2024 11/17/2024
Can Size (L)1.4 1.4
Evac Temp (F)65.9 65.9
Evac Pbar (mmHg)761.0 761.0
Evac Gauge (mmHg)-761.0 -761.0
Evac Analyst pamooney pamooney
Evac Time 01/25/24 11:03 01/25/24 10:54
Evac Vol (L)0.000 0.000
Recd. Temp (F)66.7 66.7
Recd. Pbar (mmHg)757.7 757.7
Recd. Gauge (mmHg)-195.0 -258.0
Recd Vol (L)1.039 0.923
P1 Temp (F)66.7 66.7
P1 Pbar (mmHg)757.7 757.7
P1 Gauge (mmHg)745.0 686.0
P1 Analyst pamooney pamooney
P1 Time 02/01/24 13:27 02/01/24 13:34
P1 Fill Gas Nitrogen Nitrogen
P1 Vol (L)2.775 2.666
P1 DF Override false false
P1 Dilution Factor 2.671 2.889
Mid 1-2 Temp (F)67.0 67.0
Mid 1-2 Pbar (mmHg)763.3 756.3
Mid 1-2 Gauge (mmHg)397.2 354.0
Mid 1-2 Vol (L)2.142 2.049
P2 Temp (F)67.0 67.0
P2 Pbar (mmHg)763.3 756.3
P2 Gauge (mmHg)873.7 823.0
P2 Analyst pamooney pamooney
P2 Time 02/07/24 08:54 02/07/24 08:46
P2 FillGas Nitrogen Nitrogen
P2 Vol (L)3.021 2.915
P2 Dilution Factor 3.767 4.110
Enthalpy Analytical -- Canister Pressurization
0124-075
AECOM - Morrisville
Frye & Webster DC410064
Canister Pressurization Report 20230531 Report Printed 2/12/2024 12:41:56 PM
EA # 0124-075 Page 35 of 85

Lab QC
EA # 0124-075 Page 36 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Parent Conc
(ppbv)
Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
Dup
Diff (%)
Flags
Propylene 130 124 15.9 14.4 214 27.3 4.5 pass
Freon 12 (CCl2F2)ND ND 16.1 14.4 ND 79.5
Freon 114 (C2Cl2F4)ND ND 16.5 14.4 ND 115
Chloromethane ND ND 16.3 14.4 ND 33.6
Chloroethene (Vinyl chloride)420 401 16.4 14.4 1,024 42.0 4.6 pass, m
1,3-Butadiene ND ND 16.0 14.4 ND 35.4
Bromomethane ND ND 16.1 14.4 ND 62.6
Chloroethane ND ND 16.7 14.4 ND 44.0
Bromoethene (Vinyl bromide)ND ND 16.1 14.4 ND 70.3
Freon 11 (CCl3F)ND ND 17.3 14.4 ND 97.4
Ethanol 19.9 ND 16.3 16.3 ND 30.7
Acrolein ND ND 16.2 14.4 ND 37.1
Freon 113 (C2Cl3F3)ND ND 16.7 14.4 ND 128
1,1-Dichloroethene 489 480 16.5 14.4 1,902 65.5 1.9 pass
Acetone 2,055 1,857 16.5 14.4 4,409 39.1 10.1 pass
Carbon disulfide 22.5 22.1 16.4 14.4 68.9 51.0 1.8 pass, m
Isopropyl alcohol ND ND 16.4 14.4 ND 40.3
Allyl chloride (3-chloropropene)ND ND 17.8 14.4 ND 55.5
Acetonitrile ND ND 16.4 14.4 ND 27.5
Methylene chloride 34.2 28.7 16.8 14.4 99.6 58.4 17.6 pass, m
trans-1,2-Dichloroethene 111 100 16.8 14.4 397 66.4 9.8 pass
Methyl tert-butyl ether ND ND 16.9 14.4 ND 60.9
Acrylonitrile 472 477 16.7 14.4 1,035 36.3 1.2 pass
Hexane 4,497 4,236 16.7 14.4 14,922 58.8 6.0 pass
1,1-Dichloroethane ND ND 16.3 14.4 ND 66.0
Vinyl acetate ND ND 16.8 14.4 ND 59.2
Methyl ethyl ketone (2-Butanone)ND ND 17.0 14.4 ND 50.1
Ethyl acetate ND ND 16.4 14.4 ND 59.1
Chloroform 133 127 16.5 14.4 618 80.5 5.0 pass
Tetrahydrofuran ND ND 16.6 14.4 ND 49.0
1,1,1-Trichloroethane ND ND 16.6 14.4 ND 90.5
Cyclohexane 5,347 5,023 16.8 14.4 17,280 58.0 6.2 pass
Carbon tetrachloride ND ND 16.6 14.4 ND 104
Benzene 43.1 42.2 16.5 14.4 135 52.8 2.3 pass
2,2,4-trimethylpentane 213 208 17.0 14.4 970 79.4 2.4 pass, m
1,2-Dichloroethane ND ND 16.9 14.4 ND 68.4
Heptane 2,124 2,010 16.7 14.4 8,233 68.2 5.5 pass
1,2-Dichloropropane 320 324 16.6 14.4 1,499 76.4 1.5 pass, m
Methyl methacrylate 8,721 8,730 17.2 14.4 35,725 70.4 0.1 pass
1,4-Dioxane ND ND 16.5 14.4 ND 59.4
Bromodichloromethane ND ND 16.6 14.4 ND 111
cis-1,3-Dichloropropene ND ND 16.3 14.4 ND 74.0
96.3
65.2
58.2
58.9
66.4
58.9
51.8
78.4
49.5
90.4
45.9
67.2
50.6
42.4
51.8
70.2
42.4
57.0
51.8
31.2
50.7
58.2
44.8
35.3
45.0
24.1
49.9
30.7
33.0
110
57.0
34.1
31.8
55.8
37.9
62.9
80.8
24.7
71.1
100
29.7
36.7
Air
0124-075.SG-11.CanP2
0124-075.SG-11.LDP2
MDL
(ug/m³)
X2400742.D
100.000
4.110
2024-02-09 08:15
TO15_SCNV6.M
0124-075; *100=5mL load (2nd TP); Can #13541; MP2
2024-01-31 14:52
2024-02-01 00:00
LabDup
Xavier_X020924A_0124-075.v2
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
0124-075.SG-11.LDP2
EA # 0124-075 Page 37 of 85
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Parent Conc
(ppbv)
Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
Dup
Diff (%)
Flags
Air
0124-075.SG-11.CanP2
0124-075.SG-11.LDP2
MDL
(ug/m³)
X2400742.D
100.000
4.110
2024-02-09 08:15
TO15_SCNV6.M
0124-075; *100=5mL load (2nd TP); Can #13541; MP2
2024-01-31 14:52
2024-02-01 00:00
LabDup
Xavier_X020924A_0124-075.v2
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
0124-075.SG-11.LDP2
Methyl isobutyl ketone 301 215 17.1 14.4 879 69.9 33.4 fail, m
Toluene ND ND 16.7 14.4 ND 63.0
trans-1,3-Dichloropropene ND ND 17.0 14.4 ND 76.9
1,1,2-Trichloroethane ND ND 16.7 14.4 ND 91.2
2-Hexanone (Methyl butyl ketone)4,738 4,730 16.8 14.4 19,366 68.8 0.2 pass, m
Dibromochloromethane ND ND 16.6 14.4 ND 141
1,2-Dibromoethane ND ND 16.8 14.4 ND 129
Chlorobenzene 21.5 19.1 16.9 14.4 87.9 77.9 11.8 pass
Ethylbenzene 502 498 16.3 14.4 2,159 70.8 0.9 pass
1,1,1,2-Tetrachloroethane ND ND 16.6 14.4 ND 114
m-/p-Xylenes 73.1 71.7 16.7 14.4 311 72.3 1.9 pass, m
o-Xylene ND ND 16.5 14.4 ND 71.5
Styrene ND ND 16.1 14.4 ND 68.6
Bromoform ND ND 16.5 14.4 ND 170
1,1,2,2-Tetrachloroethane 897 840 16.6 14.4 5,763 114 6.6 pass, m
4-Ethyltoluene 642 625 16.7 14.4 3,072 82.1 2.6 pass, m
2-Chlorotoluene ND ND 16.6 14.4 ND 85.8
1,3,5-Trimethylbenzene 407 390 16.7 14.4 1,916 81.9 4.3 pass
1,2,4-Trimethylbenzene 1,853 1,748 16.5 14.4 8,587 80.8 5.8 pass
1,3-Dichlorobenzene ND ND 16.7 14.4 ND 100
1,4-Dichlorobenzene ND ND 16.5 14.4 ND 99.3
Benzyl chloride 284 278 16.5 14.4 1,439 85.6 1.9 pass, m
1,2-Dichlorobenzene ND ND 16.7 14.4 ND 100
1,2,4-Trichlorobenzene ND ND 16.4 14.4 ND 121
Hexachlorobutadiene ND ND 16.2 14.4 ND 173
Naphthalene ND ND 16.6 14.4 ND 86.7
1-Bromopropane ND ND 16.3 14.4 ND 82.0
1-Octene 2,281 2,491 16.2 14.4 11,425 74.4 8.8 pass
n-Octane 1,675 1,725 16.9 14.4 8,054 79.1 2.9 pass
Isopropylbenzene 544 548 16.7 14.4 2,691 82.0 0.7 pass
n-Propylbenzene 1,164 1,145 16.9 14.4 5,624 82.9 1.7 pass
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)874,856 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,273,784 12.44 5.16 pass
Chlorobenzene-d5 (IS)3,030,112 16.58 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
67.2
70.7
70.7
107
153
75.4
72.3
66.0
70.7
86.4
86.4
74.4
86.4
149
98.7
70.7
74.4
70.7
62.4
98.7
62.4
62.4
61.2
78.4
58.9
122
110
66.2
58.9
54.2
65.2
EA # 0124-075 Page 38 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene ND 0.0386 0.0350 ND 0.0665 0.0602 pass
Freon 12 (CCl2F2)ND 0.0392 0.0350 ND 0.194 0.173 pass
Freon 114 (C2Cl2F4)ND 0.0401 0.0350 ND 0.280 0.245 pass
Chloromethane ND 0.0396 0.0350 ND 0.0816 0.0722 pass
Chloroethene (Vinyl chloride)ND 0.0400 0.0350 ND 0.102 0.0894 pass
1,3-Butadiene ND 0.0389 0.0350 ND 0.0860 0.0774 pass
Bromomethane ND 0.0392 0.0350 ND 0.152 0.136 pass
Chloroethane ND 0.0406 0.0350 ND 0.107 0.0923 pass
Bromoethene (Vinyl bromide)ND 0.0391 0.0350 ND 0.171 0.153 pass
Freon 11 (CCl3F)ND 0.0422 0.0350 ND 0.237 0.197 pass
Ethanol 0.0585 0.0396 0.0396 0.110 0.0746 0.0746 pass
Acrolein ND 0.0394 0.0350 ND 0.0903 0.0802 pass
Freon 113 (C2Cl3F3)ND 0.0406 0.0350 ND 0.311 0.268 pass
1,1-Dichloroethene ND 0.0402 0.0350 ND 0.159 0.139 pass
Acetone ND 0.0401 0.0350 ND 0.0951 0.0831 pass
Carbon disulfide ND 0.0399 0.0350 ND 0.124 0.109 pass
Isopropyl alcohol ND 0.0399 0.0350 ND 0.0980 0.0860 pass
Allyl chloride (3-chloropropene)ND 0.0432 0.0350 ND 0.135 0.109 pass
Acetonitrile ND 0.0399 0.0350 ND 0.0669 0.0587 pass
Methylene chloride ND 0.0410 0.0350 ND 0.142 0.122 pass
trans-1,2-Dichloroethene ND 0.0408 0.0350 ND 0.162 0.139 pass
Methyl tert-butyl ether ND 0.0411 0.0350 ND 0.148 0.126 pass
Acrylonitrile ND 0.0407 0.0350 ND 0.0883 0.0759 pass
Hexane ND 0.0406 0.0350 ND 0.143 0.123 pass
1,1-Dichloroethane ND 0.0397 0.0350 ND 0.161 0.142 pass
Vinyl acetate ND 0.0409 0.0350 ND 0.144 0.123 pass
cis-1,2-Dichloroethene ND 0.0404 0.0350 ND 0.160 0.139 pass
Methyl ethyl ketone (2-Butanone)ND 0.0414 0.0350 ND 0.122 0.103 pass
Ethyl acetate ND 0.0399 0.0350 ND 0.144 0.126 pass
Chloroform ND 0.0401 0.0350 ND 0.196 0.171 pass
Tetrahydrofuran ND 0.0405 0.0350 ND 0.119 0.103 pass
1,1,1-Trichloroethane ND 0.0404 0.0350 ND 0.220 0.191 pass
Cyclohexane ND 0.0410 0.0350 ND 0.141 0.120 pass
Xavier
X020124A_Humid Blank #0702
1.000
2024-02-01 15:28
TO15_SCNV6.M
Air
KMB
500mL load
Blank
Xavier_X020124A_0124-075.v1
X2400588.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020124A_Humid Blank #0702
EA # 0124-075 Page 39 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X020124A_Humid Blank #0702
1.000
2024-02-01 15:28
TO15_SCNV6.M
Air
KMB
500mL load
Blank
Xavier_X020124A_0124-075.v1
X2400588.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020124A_Humid Blank #0702
Carbon tetrachloride ND 0.0403 0.0350 ND 0.253 0.220 pass
Benzene ND 0.0402 0.0350 ND 0.128 0.112 pass
2,2,4-trimethylpentane ND 0.0414 0.0350 ND 0.193 0.163 pass
1,2-Dichloroethane ND 0.0412 0.0350 ND 0.166 0.142 pass
Heptane ND 0.0405 0.0350 ND 0.166 0.143 pass
Trichloroethene ND 0.0404 0.0350 ND 0.217 0.188 pass
1,2-Dichloropropane ND 0.0403 0.0350 ND 0.186 0.162 pass
Methyl methacrylate ND 0.0419 0.0350 ND 0.171 0.143 pass
1,4-Dioxane ND 0.0401 0.0350 ND 0.144 0.126 pass
Bromodichloromethane ND 0.0404 0.0350 ND 0.271 0.234 pass
cis-1,3-Dichloropropene ND 0.0397 0.0350 ND 0.180 0.159 pass
Methyl isobutyl ketone ND 0.0416 0.0350 ND 0.170 0.143 pass
Toluene ND 0.0407 0.0350 ND 0.153 0.132 pass
trans-1,3-Dichloropropene ND 0.0413 0.0350 ND 0.187 0.159 pass
1,1,2-Trichloroethane ND 0.0407 0.0350 ND 0.222 0.191 pass
Tetrachloroethene ND 0.0409 0.0350 ND 0.277 0.237 pass
2-Hexanone (Methyl butyl ketone)ND 0.0409 0.0350 ND 0.168 0.143 pass
Dibromochloromethane ND 0.0403 0.0350 ND 0.343 0.298 pass
1,2-Dibromoethane ND 0.0409 0.0350 ND 0.314 0.269 pass
Chlorobenzene ND 0.0412 0.0350 ND 0.190 0.161 pass
Ethylbenzene ND 0.0397 0.0350 ND 0.172 0.152 pass
1,1,1,2-Tetrachloroethane ND 0.0403 0.0350 ND 0.277 0.240 pass
m-/p-Xylenes ND 0.0406 0.0350 ND 0.176 0.152 pass
o-Xylene ND 0.0401 0.0350 ND 0.174 0.152 pass
Styrene ND 0.0392 0.0350 ND 0.167 0.149 pass
Bromoform ND 0.0401 0.0350 ND 0.414 0.362 pass
1,1,2,2-Tetrachloroethane ND 0.0404 0.0350 ND 0.277 0.240 pass
4-Ethyltoluene ND 0.0407 0.0350 ND 0.200 0.172 pass
2-Chlorotoluene ND 0.0404 0.0350 ND 0.209 0.181 pass
1,3,5-Trimethylbenzene ND 0.0406 0.0350 ND 0.199 0.172 pass
1,2,4-Trimethylbenzene ND 0.0400 0.0350 ND 0.197 0.172 pass
1,3-Dichlorobenzene ND 0.0406 0.0350 ND 0.244 0.210 pass
1,4-Dichlorobenzene ND 0.0402 0.0350 ND 0.242 0.210 pass
EA # 0124-075 Page 40 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X020124A_Humid Blank #0702
1.000
2024-02-01 15:28
TO15_SCNV6.M
Air
KMB
500mL load
Blank
Xavier_X020124A_0124-075.v1
X2400588.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020124A_Humid Blank #0702
Benzyl chloride ND 0.0402 0.0350 ND 0.208 0.181 pass
1,2-Dichlorobenzene ND 0.0405 0.0350 ND 0.243 0.210 pass
1,2,4-Trichlorobenzene ND 0.0398 0.0350 ND 0.295 0.260 pass
Hexachlorobutadiene ND 0.0395 0.0350 ND 0.421 0.373 pass
Naphthalene ND 0.0403 0.0350 ND 0.211 0.183 pass
1-Bromopropane ND 0.0397 0.0350 ND 0.199 0.176 pass
1-Octene ND 0.0395 0.0350 ND 0.181 0.161 pass
n-Octane ND 0.0412 0.0350 ND 0.192 0.163 pass
Isopropylbenzene ND 0.0406 0.0350 ND 0.200 0.172 pass
n-Propylbenzene ND 0.0410 0.0350 ND 0.202 0.172 pass
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)865,573 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,356,893 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,937,742 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 41 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene ND 0.0386 0.0350 ND 0.0665 0.0602 pass
Freon 12 (CCl2F2)ND 0.0392 0.0350 ND 0.194 0.173 pass
Freon 114 (C2Cl2F4)ND 0.0401 0.0350 ND 0.280 0.245 pass
Chloromethane ND 0.0396 0.0350 ND 0.0816 0.0722 pass
Chloroethene (Vinyl chloride)ND 0.0400 0.0350 ND 0.102 0.0894 pass
1,3-Butadiene ND 0.0389 0.0350 ND 0.0860 0.0774 pass
Bromomethane ND 0.0392 0.0350 ND 0.152 0.136 pass
Chloroethane ND 0.0406 0.0350 ND 0.107 0.0923 pass
Bromoethene (Vinyl bromide)ND 0.0391 0.0350 ND 0.171 0.153 pass
Freon 11 (CCl3F)ND 0.0422 0.0350 ND 0.237 0.197 pass
Ethanol 0.0526 0.0396 0.0396 0.0991 0.0746 0.0746 pass
Acrolein ND 0.0394 0.0350 ND 0.0903 0.0802 pass
Freon 113 (C2Cl3F3)ND 0.0406 0.0350 ND 0.311 0.268 pass
1,1-Dichloroethene ND 0.0402 0.0350 ND 0.159 0.139 pass
Acetone ND 0.0401 0.0350 ND 0.0951 0.0831 pass
Carbon disulfide ND 0.0399 0.0350 ND 0.124 0.109 pass
Isopropyl alcohol ND 0.0399 0.0350 ND 0.0980 0.0860 pass
Allyl chloride (3-chloropropene)ND 0.0432 0.0350 ND 0.135 0.109 pass
Acetonitrile ND 0.0399 0.0350 ND 0.0669 0.0587 pass
Methylene chloride ND 0.0410 0.0350 ND 0.142 0.122 pass
trans-1,2-Dichloroethene ND 0.0408 0.0350 ND 0.162 0.139 pass
Methyl tert-butyl ether ND 0.0411 0.0350 ND 0.148 0.126 pass
Acrylonitrile ND 0.0407 0.0350 ND 0.0883 0.0759 pass
Hexane ND 0.0406 0.0350 ND 0.143 0.123 pass
1,1-Dichloroethane ND 0.0397 0.0350 ND 0.161 0.142 pass
Vinyl acetate ND 0.0409 0.0350 ND 0.144 0.123 pass
cis-1,2-Dichloroethene ND 0.0404 0.0350 ND 0.160 0.139 pass
Methyl ethyl ketone (2-Butanone)ND 0.0414 0.0350 ND 0.122 0.103 pass
Ethyl acetate ND 0.0399 0.0350 ND 0.144 0.126 pass
Chloroform ND 0.0401 0.0350 ND 0.196 0.171 pass
Tetrahydrofuran ND 0.0405 0.0350 ND 0.119 0.103 pass
1,1,1-Trichloroethane ND 0.0404 0.0350 ND 0.220 0.191 pass
Cyclohexane ND 0.0410 0.0350 ND 0.141 0.120 pass
Xavier
X020524A_Humid Blank #0702
1.000
2024-02-05 19:04
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020524A_0124-075.v1
X2400653.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020524A_Humid Blank #0702
EA # 0124-075 Page 42 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X020524A_Humid Blank #0702
1.000
2024-02-05 19:04
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020524A_0124-075.v1
X2400653.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020524A_Humid Blank #0702
Carbon tetrachloride ND 0.0403 0.0350 ND 0.253 0.220 pass
Benzene ND 0.0402 0.0350 ND 0.128 0.112 pass
2,2,4-trimethylpentane ND 0.0414 0.0350 ND 0.193 0.163 pass
1,2-Dichloroethane ND 0.0412 0.0350 ND 0.166 0.142 pass
Heptane ND 0.0405 0.0350 ND 0.166 0.143 pass
Trichloroethene ND 0.0404 0.0350 ND 0.217 0.188 pass
1,2-Dichloropropane ND 0.0403 0.0350 ND 0.186 0.162 pass
Methyl methacrylate ND 0.0419 0.0350 ND 0.171 0.143 pass
1,4-Dioxane ND 0.0401 0.0350 ND 0.144 0.126 pass
Bromodichloromethane ND 0.0404 0.0350 ND 0.271 0.234 pass
cis-1,3-Dichloropropene ND 0.0397 0.0350 ND 0.180 0.159 pass
Methyl isobutyl ketone ND 0.0416 0.0350 ND 0.170 0.143 pass
Toluene ND 0.0407 0.0350 ND 0.153 0.132 pass
trans-1,3-Dichloropropene ND 0.0413 0.0350 ND 0.187 0.159 pass
1,1,2-Trichloroethane ND 0.0407 0.0350 ND 0.222 0.191 pass
Tetrachloroethene ND 0.0409 0.0350 ND 0.277 0.237 pass
2-Hexanone (Methyl butyl ketone)ND 0.0409 0.0350 ND 0.168 0.143 pass
Dibromochloromethane ND 0.0403 0.0350 ND 0.343 0.298 pass
1,2-Dibromoethane ND 0.0409 0.0350 ND 0.314 0.269 pass
Chlorobenzene ND 0.0412 0.0350 ND 0.190 0.161 pass
Ethylbenzene ND 0.0397 0.0350 ND 0.172 0.152 pass
1,1,1,2-Tetrachloroethane ND 0.0403 0.0350 ND 0.277 0.240 pass
m-/p-Xylenes ND 0.0406 0.0350 ND 0.176 0.152 pass
o-Xylene ND 0.0401 0.0350 ND 0.174 0.152 pass
Styrene ND 0.0392 0.0350 ND 0.167 0.149 pass
Bromoform ND 0.0401 0.0350 ND 0.414 0.362 pass
1,1,2,2-Tetrachloroethane ND 0.0404 0.0350 ND 0.277 0.240 pass
4-Ethyltoluene ND 0.0407 0.0350 ND 0.200 0.172 pass
2-Chlorotoluene ND 0.0404 0.0350 ND 0.209 0.181 pass
1,3,5-Trimethylbenzene ND 0.0406 0.0350 ND 0.199 0.172 pass
1,2,4-Trimethylbenzene ND 0.0400 0.0350 ND 0.197 0.172 pass
1,3-Dichlorobenzene ND 0.0406 0.0350 ND 0.244 0.210 pass
1,4-Dichlorobenzene ND 0.0402 0.0350 ND 0.242 0.210 pass
EA # 0124-075 Page 43 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X020524A_Humid Blank #0702
1.000
2024-02-05 19:04
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020524A_0124-075.v1
X2400653.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020524A_Humid Blank #0702
Benzyl chloride ND 0.0402 0.0350 ND 0.208 0.181 pass
1,2-Dichlorobenzene ND 0.0405 0.0350 ND 0.243 0.210 pass
1,2,4-Trichlorobenzene ND 0.0398 0.0350 ND 0.295 0.260 pass
Hexachlorobutadiene ND 0.0395 0.0350 ND 0.421 0.373 pass
Naphthalene ND 0.0403 0.0350 ND 0.211 0.183 pass
1-Bromopropane ND 0.0397 0.0350 ND 0.199 0.176 pass
1-Octene ND 0.0395 0.0350 ND 0.181 0.161 pass
n-Octane ND 0.0412 0.0350 ND 0.192 0.163 pass
Isopropylbenzene ND 0.0406 0.0350 ND 0.200 0.172 pass
n-Propylbenzene ND 0.0410 0.0350 ND 0.202 0.172 pass
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)855,401 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,291,931 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,893,110 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 44 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
cis-1,2-Dichloroethene ND 0.0404 0.0350 ND 0.160 0.139 pass
Trichloroethene ND 0.0404 0.0350 ND 0.217 0.188 pass
Tetrachloroethene ND 0.0409 0.0350 ND 0.277 0.237 pass
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)851,211 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,308,570 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,889,606 16.57 4.92 pass
Xavier
X020624A_Humid Blank #0702
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
1.000
2024-02-06 16:11
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020624A_0124-075.v1
X2400675.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020624A_Humid Blank #0702
EA # 0124-075 Page 45 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene ND 0.0386 0.0350 ND 0.0665 0.0602 pass
Freon 12 (CCl2F2)ND 0.0392 0.0350 ND 0.194 0.173 pass
Freon 114 (C2Cl2F4)ND 0.0401 0.0350 ND 0.280 0.245 pass
Chloromethane ND 0.0396 0.0350 ND 0.0816 0.0722 pass
Chloroethene (Vinyl chloride)ND 0.0400 0.0350 ND 0.102 0.0894 pass
1,3-Butadiene ND 0.0389 0.0350 ND 0.0860 0.0774 pass
Bromomethane ND 0.0392 0.0350 ND 0.152 0.136 pass
Chloroethane ND 0.0406 0.0350 ND 0.107 0.0923 pass
Bromoethene (Vinyl bromide)ND 0.0391 0.0350 ND 0.171 0.153 pass
Freon 11 (CCl3F)ND 0.0422 0.0350 ND 0.237 0.197 pass
Ethanol 0.0469 0.0396 0.0396 0.0883 0.0746 0.0746 pass
Acrolein ND 0.0394 0.0350 ND 0.0903 0.0802 pass
Freon 113 (C2Cl3F3)ND 0.0406 0.0350 ND 0.311 0.268 pass
1,1-Dichloroethene ND 0.0402 0.0350 ND 0.159 0.139 pass
Acetone 0.0364 0.0401 0.0350 0.0864 0.0951 0.0831 pass, J
Carbon disulfide ND 0.0399 0.0350 ND 0.124 0.109 pass
Isopropyl alcohol ND 0.0399 0.0350 ND 0.0980 0.0860 pass
Allyl chloride (3-chloropropene)ND 0.0432 0.0350 ND 0.135 0.109 pass
Acetonitrile ND 0.0399 0.0350 ND 0.0669 0.0587 pass
Methylene chloride ND 0.0410 0.0350 ND 0.142 0.122 pass
trans-1,2-Dichloroethene ND 0.0408 0.0350 ND 0.162 0.139 pass
Methyl tert-butyl ether ND 0.0411 0.0350 ND 0.148 0.126 pass
Acrylonitrile ND 0.0407 0.0350 ND 0.0883 0.0759 pass
Hexane ND 0.0406 0.0350 ND 0.143 0.123 pass
1,1-Dichloroethane ND 0.0397 0.0350 ND 0.161 0.142 pass
Vinyl acetate ND 0.0409 0.0350 ND 0.144 0.123 pass
cis-1,2-Dichloroethene ND 0.0404 0.0350 ND 0.160 0.139 pass
Methyl ethyl ketone (2-Butanone)ND 0.0414 0.0350 ND 0.122 0.103 pass
Ethyl acetate ND 0.0399 0.0350 ND 0.144 0.126 pass
Chloroform ND 0.0401 0.0350 ND 0.196 0.171 pass
Tetrahydrofuran ND 0.0405 0.0350 ND 0.119 0.103 pass
1,1,1-Trichloroethane ND 0.0404 0.0350 ND 0.220 0.191 pass
Cyclohexane ND 0.0410 0.0350 ND 0.141 0.120 pass
Xavier
X020724A_Humid Blank #0702
1.000
2024-02-07 16:27
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020724A_0124-075.v1
X2400699.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020724A_Humid Blank #0702
EA # 0124-075 Page 46 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X020724A_Humid Blank #0702
1.000
2024-02-07 16:27
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020724A_0124-075.v1
X2400699.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020724A_Humid Blank #0702
Carbon tetrachloride ND 0.0403 0.0350 ND 0.253 0.220 pass
Benzene ND 0.0402 0.0350 ND 0.128 0.112 pass
2,2,4-trimethylpentane ND 0.0414 0.0350 ND 0.193 0.163 pass
1,2-Dichloroethane ND 0.0412 0.0350 ND 0.166 0.142 pass
Heptane ND 0.0405 0.0350 ND 0.166 0.143 pass
Trichloroethene ND 0.0404 0.0350 ND 0.217 0.188 pass
1,2-Dichloropropane ND 0.0403 0.0350 ND 0.186 0.162 pass
Methyl methacrylate ND 0.0419 0.0350 ND 0.171 0.143 pass
1,4-Dioxane ND 0.0401 0.0350 ND 0.144 0.126 pass
Bromodichloromethane ND 0.0404 0.0350 ND 0.271 0.234 pass
cis-1,3-Dichloropropene ND 0.0397 0.0350 ND 0.180 0.159 pass
Methyl isobutyl ketone ND 0.0416 0.0350 ND 0.170 0.143 pass
Toluene ND 0.0407 0.0350 ND 0.153 0.132 pass
trans-1,3-Dichloropropene ND 0.0413 0.0350 ND 0.187 0.159 pass
1,1,2-Trichloroethane ND 0.0407 0.0350 ND 0.222 0.191 pass
Tetrachloroethene ND 0.0409 0.0350 ND 0.277 0.237 pass
2-Hexanone (Methyl butyl ketone)ND 0.0409 0.0350 ND 0.168 0.143 pass
Dibromochloromethane ND 0.0403 0.0350 ND 0.343 0.298 pass
1,2-Dibromoethane ND 0.0409 0.0350 ND 0.314 0.269 pass
Chlorobenzene ND 0.0412 0.0350 ND 0.190 0.161 pass
Ethylbenzene ND 0.0397 0.0350 ND 0.172 0.152 pass
1,1,1,2-Tetrachloroethane ND 0.0403 0.0350 ND 0.277 0.240 pass
m-/p-Xylenes ND 0.0406 0.0350 ND 0.176 0.152 pass
o-Xylene ND 0.0401 0.0350 ND 0.174 0.152 pass
Styrene ND 0.0392 0.0350 ND 0.167 0.149 pass
Bromoform ND 0.0401 0.0350 ND 0.414 0.362 pass
1,1,2,2-Tetrachloroethane ND 0.0404 0.0350 ND 0.277 0.240 pass
4-Ethyltoluene ND 0.0407 0.0350 ND 0.200 0.172 pass
2-Chlorotoluene ND 0.0404 0.0350 ND 0.209 0.181 pass
1,3,5-Trimethylbenzene ND 0.0406 0.0350 ND 0.199 0.172 pass
1,2,4-Trimethylbenzene ND 0.0400 0.0350 ND 0.197 0.172 pass
1,3-Dichlorobenzene ND 0.0406 0.0350 ND 0.244 0.210 pass
1,4-Dichlorobenzene ND 0.0402 0.0350 ND 0.242 0.210 pass
EA # 0124-075 Page 47 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X020724A_Humid Blank #0702
1.000
2024-02-07 16:27
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020724A_0124-075.v1
X2400699.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020724A_Humid Blank #0702
Benzyl chloride ND 0.0402 0.0350 ND 0.208 0.181 pass
1,2-Dichlorobenzene ND 0.0405 0.0350 ND 0.243 0.210 pass
1,2,4-Trichlorobenzene ND 0.0398 0.0350 ND 0.295 0.260 pass
Hexachlorobutadiene ND 0.0395 0.0350 ND 0.421 0.373 pass
Naphthalene ND 0.0403 0.0350 ND 0.211 0.183 pass
1-Bromopropane ND 0.0397 0.0350 ND 0.199 0.176 pass
1-Octene ND 0.0395 0.0350 ND 0.181 0.161 pass
n-Octane ND 0.0412 0.0350 ND 0.192 0.163 pass
Isopropylbenzene ND 0.0406 0.0350 ND 0.200 0.172 pass
n-Propylbenzene ND 0.0410 0.0350 ND 0.202 0.172 pass
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)808,821 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,082,312 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,712,547 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 48 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene ND 0.0386 0.0350 ND 0.0665 0.0602 pass
Freon 12 (CCl2F2)ND 0.0392 0.0350 ND 0.194 0.173 pass
Freon 114 (C2Cl2F4)ND 0.0401 0.0350 ND 0.280 0.245 pass
Chloromethane ND 0.0396 0.0350 ND 0.0816 0.0722 pass
Chloroethene (Vinyl chloride)ND 0.0400 0.0350 ND 0.102 0.0894 pass
1,3-Butadiene ND 0.0389 0.0350 ND 0.0860 0.0774 pass
Bromomethane ND 0.0392 0.0350 ND 0.152 0.136 pass
Chloroethane ND 0.0406 0.0350 ND 0.107 0.0923 pass
Bromoethene (Vinyl bromide)ND 0.0391 0.0350 ND 0.171 0.153 pass
Freon 11 (CCl3F)ND 0.0422 0.0350 ND 0.237 0.197 pass
Ethanol 0.0650 0.0396 0.0396 0.122 0.0746 0.0746 pass
Acrolein ND 0.0394 0.0350 ND 0.0903 0.0802 pass
Freon 113 (C2Cl3F3)ND 0.0406 0.0350 ND 0.311 0.268 pass
1,1-Dichloroethene ND 0.0402 0.0350 ND 0.159 0.139 pass
Acetone 0.0407 0.0401 0.0350 0.0965 0.0951 0.0831 pass
Carbon disulfide ND 0.0399 0.0350 ND 0.124 0.109 pass
Isopropyl alcohol ND 0.0399 0.0350 ND 0.0980 0.0860 pass
Allyl chloride (3-chloropropene)ND 0.0432 0.0350 ND 0.135 0.109 pass
Acetonitrile ND 0.0399 0.0350 ND 0.0669 0.0587 pass
Methylene chloride ND 0.0410 0.0350 ND 0.142 0.122 pass
trans-1,2-Dichloroethene ND 0.0408 0.0350 ND 0.162 0.139 pass
Methyl tert-butyl ether ND 0.0411 0.0350 ND 0.148 0.126 pass
Acrylonitrile ND 0.0407 0.0350 ND 0.0883 0.0759 pass
Hexane ND 0.0406 0.0350 ND 0.143 0.123 pass
1,1-Dichloroethane ND 0.0397 0.0350 ND 0.161 0.142 pass
Vinyl acetate ND 0.0409 0.0350 ND 0.144 0.123 pass
Methyl ethyl ketone (2-Butanone)ND 0.0414 0.0350 ND 0.122 0.103 pass
Ethyl acetate ND 0.0399 0.0350 ND 0.144 0.126 pass
Chloroform ND 0.0401 0.0350 ND 0.196 0.171 pass
Tetrahydrofuran ND 0.0405 0.0350 ND 0.119 0.103 pass
1,1,1-Trichloroethane ND 0.0404 0.0350 ND 0.220 0.191 pass
Cyclohexane ND 0.0410 0.0350 ND 0.141 0.120 pass
Carbon tetrachloride ND 0.0403 0.0350 ND 0.253 0.220 pass
Xavier
X020924A_Humid Blank #0702
1.000
2024-02-09 06:06
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020924A_0124-075.v2
X2400740.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020924A_Humid Blank #0702
EA # 0124-075 Page 49 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X020924A_Humid Blank #0702
1.000
2024-02-09 06:06
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020924A_0124-075.v2
X2400740.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020924A_Humid Blank #0702
Benzene ND 0.0402 0.0350 ND 0.128 0.112 pass
2,2,4-trimethylpentane ND 0.0414 0.0350 ND 0.193 0.163 pass
1,2-Dichloroethane ND 0.0412 0.0350 ND 0.166 0.142 pass
Heptane ND 0.0405 0.0350 ND 0.166 0.143 pass
1,2-Dichloropropane ND 0.0403 0.0350 ND 0.186 0.162 pass
Methyl methacrylate ND 0.0419 0.0350 ND 0.171 0.143 pass
1,4-Dioxane ND 0.0401 0.0350 ND 0.144 0.126 pass
Bromodichloromethane ND 0.0404 0.0350 ND 0.271 0.234 pass
cis-1,3-Dichloropropene ND 0.0397 0.0350 ND 0.180 0.159 pass
Methyl isobutyl ketone ND 0.0416 0.0350 ND 0.170 0.143 pass
Toluene ND 0.0407 0.0350 ND 0.153 0.132 pass
trans-1,3-Dichloropropene ND 0.0413 0.0350 ND 0.187 0.159 pass
1,1,2-Trichloroethane ND 0.0407 0.0350 ND 0.222 0.191 pass
2-Hexanone (Methyl butyl ketone)ND 0.0409 0.0350 ND 0.168 0.143 pass
Dibromochloromethane ND 0.0403 0.0350 ND 0.343 0.298 pass
1,2-Dibromoethane ND 0.0409 0.0350 ND 0.314 0.269 pass
Chlorobenzene ND 0.0412 0.0350 ND 0.190 0.161 pass
Ethylbenzene ND 0.0397 0.0350 ND 0.172 0.152 pass
1,1,1,2-Tetrachloroethane ND 0.0403 0.0350 ND 0.277 0.240 pass
m-/p-Xylenes ND 0.0406 0.0350 ND 0.176 0.152 pass
o-Xylene ND 0.0401 0.0350 ND 0.174 0.152 pass
Styrene ND 0.0392 0.0350 ND 0.167 0.149 pass
Bromoform ND 0.0401 0.0350 ND 0.414 0.362 pass
1,1,2,2-Tetrachloroethane ND 0.0404 0.0350 ND 0.277 0.240 pass
4-Ethyltoluene ND 0.0407 0.0350 ND 0.200 0.172 pass
2-Chlorotoluene ND 0.0404 0.0350 ND 0.209 0.181 pass
1,3,5-Trimethylbenzene ND 0.0406 0.0350 ND 0.199 0.172 pass
1,2,4-Trimethylbenzene ND 0.0400 0.0350 ND 0.197 0.172 pass
1,3-Dichlorobenzene ND 0.0406 0.0350 ND 0.244 0.210 pass
1,4-Dichlorobenzene ND 0.0402 0.0350 ND 0.242 0.210 pass
Benzyl chloride ND 0.0402 0.0350 ND 0.208 0.181 pass
1,2-Dichlorobenzene ND 0.0405 0.0350 ND 0.243 0.210 pass
1,2,4-Trichlorobenzene ND 0.0398 0.0350 ND 0.295 0.260 pass
EA # 0124-075 Page 50 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X020924A_Humid Blank #0702
1.000
2024-02-09 06:06
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X020924A_0124-075.v2
X2400740.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020924A_Humid Blank #0702
Hexachlorobutadiene ND 0.0395 0.0350 ND 0.421 0.373 pass
Naphthalene ND 0.0403 0.0350 ND 0.211 0.183 pass
1-Bromopropane ND 0.0397 0.0350 ND 0.199 0.176 pass
1-Octene ND 0.0395 0.0350 ND 0.181 0.161 pass
n-Octane ND 0.0412 0.0350 ND 0.192 0.163 pass
Isopropylbenzene ND 0.0406 0.0350 ND 0.200 0.172 pass
n-Propylbenzene ND 0.0410 0.0350 ND 0.202 0.172 pass
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)870,801 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,343,686 12.44 5.16 pass
Chlorobenzene-d5 (IS)3,019,018 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 51 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 694,977 4.58 4.83 94.9 pass
Freon 12 (CCl2F2)2,087,221 4.76 4.90 97.3 pass
Freon 114 (C2Cl2F4)2,136,646 4.72 5.01 94.2 pass
Chloromethane 707,215 4.48 4.94 90.7 pass
Chloroethene (Vinyl chloride)384,129 4.13 5.00 82.6 pass, m
1,3-Butadiene 697,388 4.45 4.86 91.4 pass
Bromomethane 420,171 4.17 4.90 85.1 pass, m
Chloroethane 353,987 4.74 5.08 93.2 pass
Bromoethene (Vinyl bromide)767,047 4.27 4.89 87.2 pass
Freon 11 (CCl3F)2,332,880 5.35 5.28 101 pass
Ethanol 328,968 3.74 4.96 75.5 pass
Acrolein 267,625 4.32 4.92 87.7 pass
Freon 113 (C2Cl3F3)1,505,762 4.78 5.08 94.2 pass
1,1-Dichloroethene 1,319,131 4.69 5.03 93.2 pass
Acetone 1,490,025 4.60 5.01 91.9 pass
Carbon disulfide 2,127,577 4.81 4.98 96.5 pass
Isopropyl alcohol 1,557,062 4.69 4.98 94.2 pass
Allyl chloride (3-chloropropene)324,917 5.13 5.04 102 pass
Acetonitrile 704,274 4.73 4.98 94.8 pass, m
Methylene chloride 1,091,627 4.54 5.12 88.7 pass
trans-1,2-Dichloroethene 1,168,140 5.09 5.10 99.8 pass
Methyl tert-butyl ether 2,076,538 5.36 5.14 104 pass
Acrylonitrile 562,472 4.61 5.09 90.6 pass, m
Hexane 1,206,305 5.19 5.08 102 pass
1,1-Dichloroethane 1,434,100 5.14 4.96 104 pass
Vinyl acetate 2,257,807 4.97 5.12 97.2 pass
cis-1,2-Dichloroethene 1,364,299 5.39 5.05 107 pass
Methyl ethyl ketone (2-Butanone)364,686 5.24 5.17 101 pass
Ethyl acetate 330,109 4.89 4.99 98.1 pass
Chloroform 1,776,048 5.38 5.02 107 pass
Tetrahydrofuran 338,388 5.22 5.06 103 pass
1,1,1-Trichloroethane 1,826,137 5.35 5.05 106 pass
Cyclohexane 1,278,084 5.41 5.12 106 pass
Carbon tetrachloride 2,039,744 5.33 5.04 106 pass
1.000
2024-02-01 12:52
TO15_SCNV6.M
Air
X020124A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020124A_0124-075.v1
X2400585.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020124A_5ppbv TO15 LCS
EA # 0124-075 Page 52 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 694,977 4.58 4.83 94.9 pass
1.000
2024-02-01 12:52
TO15_SCNV6.M
Air
X020124A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020124A_0124-075.v1
X2400585.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020124A_5ppbv TO15 LCS
Benzene 2,220,802 4.91 5.03 97.7 pass
2,2,4-trimethylpentane 4,097,316 5.16 5.17 99.7 pass
1,2-Dichloroethane 1,196,800 4.94 5.14 96.0 pass
Heptane 783,352 4.94 5.06 97.5 pass
Trichloroethene 1,202,025 4.50 5.06 89.1 pass
1,2-Dichloropropane 942,353 5.01 5.04 99.5 pass
Methyl methacrylate 844,713 5.34 5.24 102 pass
1,4-Dioxane 525,643 5.04 5.02 101 pass
Bromodichloromethane 1,898,491 5.19 5.05 103 pass
cis-1,3-Dichloropropene 1,294,676 4.73 4.96 95.3 pass
Methyl isobutyl ketone 2,613,386 5.20 5.20 100 pass, m
Toluene 2,953,926 4.67 5.09 91.8 pass
trans-1,3-Dichloropropene 1,328,309 4.62 5.16 89.6 pass
1,1,2-Trichloroethane 1,038,320 4.67 5.08 91.9 pass
Tetrachloroethene 1,798,909 4.90 5.12 95.8 pass
2-Hexanone (Methyl butyl ketone)2,496,079 5.12 5.12 100 pass, m
Dibromochloromethane 2,308,788 4.95 5.04 98.2 pass
1,2-Dibromoethane 1,898,392 4.85 5.12 94.8 pass
Chlorobenzene 2,560,922 4.62 5.15 89.7 pass
Ethylbenzene 3,823,273 4.64 4.96 93.4 pass
1,1,1,2-Tetrachloroethane 1,516,292 4.64 5.04 92.0 pass
m-/p-Xylenes 3,099,477 4.97 5.07 98.1 pass
o-Xylene 3,091,400 4.76 5.01 95.0 pass
Styrene 2,361,297 4.63 4.90 94.4 pass
Bromoform 2,638,057 5.41 5.02 108 pass
1,1,2,2-Tetrachloroethane 2,439,286 4.92 5.06 97.4 pass
4-Ethyltoluene 4,408,271 4.72 5.08 92.9 pass
2-Chlorotoluene 3,763,797 4.88 5.04 96.7 pass
1,3,5-Trimethylbenzene 3,809,952 4.91 5.07 96.9 pass
1,2,4-Trimethylbenzene 3,751,086 4.74 5.00 94.8 pass
1,3-Dichlorobenzene 2,949,202 4.60 5.08 90.5 pass
1,4-Dichlorobenzene 2,948,685 4.51 5.02 89.8 pass
Benzyl chloride 3,472,233 5.05 5.03 100 pass
EA # 0124-075 Page 53 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 694,977 4.58 4.83 94.9 pass
1.000
2024-02-01 12:52
TO15_SCNV6.M
Air
X020124A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020124A_0124-075.v1
X2400585.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020124A_5ppbv TO15 LCS
1,2-Dichlorobenzene 2,915,013 4.72 5.06 93.1 pass
1,2,4-Trichlorobenzene 2,274,674 4.26 4.98 85.5 pass
Hexachlorobutadiene 2,382,995 5.12 4.94 104 pass
Naphthalene 4,802,740 3.93 5.04 78.0 pass
1-Bromopropane 1,762,373 5.17 4.96 104 pass
1-Octene 651,655 5.04 4.94 102 pass
n-Octane 861,397 5.02 5.02 100 pass
Isopropylbenzene 4,475,078 4.74 5.08 93.4 pass
n-Propylbenzene 5,305,793 5.01 5.13 97.6 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)951,424 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,611,252 12.44 5.16 pass
Chlorobenzene-d5 (IS)3,168,512 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 54 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 684,084 4.98 4.83 103 pass
Freon 12 (CCl2F2)1,898,609 4.78 4.90 97.7 pass
Freon 114 (C2Cl2F4)2,000,067 4.87 5.01 97.2 pass
Chloromethane 683,985 4.78 4.94 96.7 pass
Chloroethene (Vinyl chloride)355,824 4.22 5.00 84.4 pass
1,3-Butadiene 627,461 4.41 4.86 90.7 pass
Bromomethane 409,771 4.49 4.90 91.5 pass, m
Chloroethane 339,118 5.00 5.08 98.5 pass
Bromoethene (Vinyl bromide)745,201 4.57 4.89 93.5 pass
Freon 11 (CCl3F)2,089,155 5.28 5.28 100 pass
Ethanol 317,094 3.98 4.96 80.2 pass
Acrolein 260,041 4.63 4.92 94.0 pass
Freon 113 (C2Cl3F3)1,447,016 5.06 5.08 99.8 pass
1,1-Dichloroethene 1,205,932 4.73 5.03 94.0 pass
Acetone 1,366,336 4.65 5.01 92.9 pass
Carbon disulfide 1,988,250 4.96 4.98 99.4 pass
Isopropyl alcohol 1,460,788 4.86 4.98 97.4 pass
Allyl chloride (3-chloropropene)292,997 5.10 5.04 101 pass
Acetonitrile 681,491 5.04 4.98 101 pass, m
Methylene chloride 1,005,655 4.61 5.12 90.1 pass
trans-1,2-Dichloroethene 1,069,696 5.14 5.10 101 pass
Methyl tert-butyl ether 1,900,051 5.41 5.14 105 pass
Acrylonitrile 547,162 4.94 5.09 97.1 pass, m
Hexane 1,136,586 5.39 5.08 106 pass
1,1-Dichloroethane 1,311,912 5.19 4.96 104 pass
Vinyl acetate 2,123,439 5.16 5.12 101 pass
cis-1,2-Dichloroethene 1,245,611 5.42 5.05 107 pass
Methyl ethyl ketone (2-Butanone)335,596 5.32 5.17 103 pass
Ethyl acetate 311,042 5.09 4.99 102 pass
Chloroform 1,610,352 5.38 5.02 107 pass
Tetrahydrofuran 318,875 5.43 5.06 107 pass
1,1,1-Trichloroethane 1,628,391 5.26 5.05 104 pass
Cyclohexane 1,206,711 5.63 5.12 110 pass
Carbon tetrachloride 1,785,384 5.14 5.04 102 pass
1.000
2024-02-05 16:25
TO15_SCNV6.M
Air
X020524A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020524A_0124-075.v1
X2400650.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020524A_5ppbv TO15 LCS
EA # 0124-075 Page 55 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 684,084 4.98 4.83 103 pass
1.000
2024-02-05 16:25
TO15_SCNV6.M
Air
X020524A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020524A_0124-075.v1
X2400650.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020524A_5ppbv TO15 LCS
Benzene 2,092,799 5.00 5.03 99.4 pass
2,2,4-trimethylpentane 3,832,027 5.21 5.17 101 pass
1,2-Dichloroethane 1,057,150 4.71 5.14 91.6 pass
Heptane 728,201 4.96 5.06 97.9 pass
Trichloroethene 1,141,346 4.62 5.06 91.3 pass
1,2-Dichloropropane 883,455 5.07 5.04 101 pass
Methyl methacrylate 783,286 5.35 5.24 102 pass
1,4-Dioxane 497,355 5.15 5.02 103 pass
Bromodichloromethane 1,701,186 5.03 5.05 99.5 pass
cis-1,3-Dichloropropene 1,197,382 4.73 4.96 95.2 pass
Methyl isobutyl ketone 2,391,791 5.14 5.20 99.0 pass
Toluene 2,758,049 4.59 5.09 90.1 pass
trans-1,3-Dichloropropene 1,193,576 4.37 5.16 84.7 pass
1,1,2-Trichloroethane 978,770 4.63 5.08 91.1 pass
Tetrachloroethene 1,718,215 4.93 5.12 96.3 pass
2-Hexanone (Methyl butyl ketone)2,295,117 4.95 5.12 96.7 pass
Dibromochloromethane 2,086,809 4.71 5.04 93.4 pass
1,2-Dibromoethane 1,765,447 4.75 5.12 92.8 pass
Chlorobenzene 2,400,891 4.56 5.15 88.5 pass
Ethylbenzene 3,549,991 4.53 4.96 91.2 pass
1,1,1,2-Tetrachloroethane 1,402,793 4.51 5.04 89.6 pass
m-/p-Xylenes 2,878,746 4.86 5.07 95.8 pass
o-Xylene 2,868,311 4.64 5.01 92.7 pass
Styrene 2,257,442 4.65 4.90 94.9 pass
Bromoform 2,409,851 5.20 5.02 104 pass
1,1,2,2-Tetrachloroethane 2,265,977 4.81 5.06 95.2 pass
4-Ethyltoluene 4,118,922 4.64 5.08 91.3 pass
2-Chlorotoluene 3,474,286 4.74 5.04 93.9 pass
1,3,5-Trimethylbenzene 3,516,318 4.77 5.07 94.1 pass
1,2,4-Trimethylbenzene 3,460,063 4.60 5.00 92.0 pass
1,3-Dichlorobenzene 2,783,023 4.56 5.08 89.8 pass
1,4-Dichlorobenzene 2,783,308 4.48 5.02 89.1 pass
Benzyl chloride 3,166,503 4.84 5.03 96.3 pass
EA # 0124-075 Page 56 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 684,084 4.98 4.83 103 pass
1.000
2024-02-05 16:25
TO15_SCNV6.M
Air
X020524A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020524A_0124-075.v1
X2400650.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020524A_5ppbv TO15 LCS
1,2-Dichlorobenzene 2,710,294 4.61 5.06 91.1 pass
1,2,4-Trichlorobenzene 2,219,382 4.37 4.98 87.8 pass
Hexachlorobutadiene 2,273,667 5.14 4.94 104 pass
Naphthalene 4,558,572 3.92 5.04 77.9 pass
1-Bromopropane 1,631,192 5.27 4.96 106 pass
1-Octene 600,694 4.88 4.94 98.9 pass
n-Octane 805,427 4.93 5.02 98.4 pass
Isopropylbenzene 4,167,528 4.65 5.08 91.5 pass
n-Propylbenzene 4,924,926 4.89 5.13 95.3 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)862,700 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,343,476 12.44 5.16 pass
Chlorobenzene-d5 (IS)3,011,767 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 57 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
cis-1,2-Dichloroethene 1,193,124 5.23 5.05 104 pass
Trichloroethene 1,117,720 4.62 5.06 91.4 pass
Tetrachloroethene 1,700,382 5.16 5.12 101 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)857,544 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,272,282 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,847,370 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
1.000
2024-02-06 13:32
TO15_SCNV6.M
Air
X020624A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020624A_0124-075.v1
X2400672.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020624A_5ppbv TO15 LCS
EA # 0124-075 Page 58 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 668,997 5.27 4.83 109 pass
Freon 12 (CCl2F2)1,690,315 4.61 4.90 94.2 pass
Freon 114 (C2Cl2F4)1,830,471 4.83 5.01 96.4 pass
Chloromethane 618,022 4.68 4.94 94.7 pass
Chloroethene (Vinyl chloride)319,973 4.11 5.00 82.2 pass, m
1,3-Butadiene 565,312 4.31 4.86 88.5 pass
Bromomethane 369,171 4.38 4.90 89.4 pass, m
Chloroethane 302,659 4.84 5.08 95.3 pass
Bromoethene (Vinyl bromide)673,489 4.48 4.89 91.5 pass
Freon 11 (CCl3F)1,825,203 5.00 5.28 94.8 pass
Ethanol 284,325 3.86 4.96 78.0 pass, m
Acrolein 228,252 4.40 4.92 89.4 pass
Freon 113 (C2Cl3F3)1,315,781 4.99 5.08 98.3 pass
1,1-Dichloroethene 1,035,626 4.40 5.03 87.4 pass
Acetone 1,186,332 4.38 5.01 87.4 pass
Carbon disulfide 1,762,789 4.76 4.98 95.5 pass
Isopropyl alcohol 1,306,825 4.71 4.98 94.4 pass
Allyl chloride (3-chloropropene)268,963 5.07 5.04 101 pass
Acetonitrile 634,673 5.09 4.98 102 pass
Methylene chloride 893,608 4.44 5.12 86.7 pass
trans-1,2-Dichloroethene 924,171 4.81 5.10 94.3 pass
Methyl tert-butyl ether 1,653,120 5.10 5.14 99.2 pass
Acrylonitrile 470,735 4.61 5.09 90.6 pass, m
Hexane 1,000,176 5.14 5.08 101 pass
1,1-Dichloroethane 1,143,513 4.90 4.96 98.6 pass
Vinyl acetate 1,900,936 5.00 5.12 97.8 pass, m
cis-1,2-Dichloroethene 1,074,571 5.07 5.05 100 pass
Methyl ethyl ketone (2-Butanone)285,462 4.90 5.17 94.8 pass
Ethyl acetate 275,042 4.87 4.99 97.7 pass
Chloroform 1,397,088 5.05 5.02 101 pass
Tetrahydrofuran 282,375 5.21 5.06 103 pass
1,1,1-Trichloroethane 1,431,449 5.01 5.05 99.2 pass
Cyclohexane 1,050,756 5.31 5.12 104 pass
Carbon tetrachloride 1,567,093 4.89 5.04 97.1 pass
1.000
2024-02-07 13:49
TO15_SCNV6.M
Air
X020724A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020724A_0124-075.v1
X2400696.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020724A_5ppbv TO15 LCS
EA # 0124-075 Page 59 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 668,997 5.27 4.83 109 pass
1.000
2024-02-07 13:49
TO15_SCNV6.M
Air
X020724A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020724A_0124-075.v1
X2400696.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020724A_5ppbv TO15 LCS
Benzene 1,846,366 4.84 5.03 96.2 pass
2,2,4-trimethylpentane 3,384,905 5.05 5.17 97.6 pass
1,2-Dichloroethane 911,251 4.46 5.14 86.6 pass
Heptane 638,583 4.77 5.06 94.2 pass
Trichloroethene 1,025,007 4.55 5.06 90.0 pass
1,2-Dichloropropane 765,531 4.82 5.04 95.7 pass
Methyl methacrylate 679,896 5.10 5.24 97.3 pass
1,4-Dioxane 432,846 4.92 5.02 98.1 pass
Bromodichloromethane 1,477,167 4.79 5.05 94.8 pass
cis-1,3-Dichloropropene 1,056,902 4.58 4.96 92.2 pass
Methyl isobutyl ketone 2,141,137 5.05 5.20 97.2 pass
Toluene 2,409,822 4.51 5.09 88.5 pass
trans-1,3-Dichloropropene 1,032,562 4.25 5.16 82.3 pass
1,1,2-Trichloroethane 870,888 4.63 5.08 91.1 pass
Tetrachloroethene 1,564,590 5.04 5.12 98.6 pass
2-Hexanone (Methyl butyl ketone)2,020,197 4.89 5.12 95.7 pass
Dibromochloromethane 1,874,529 4.75 5.04 94.2 pass
1,2-Dibromoethane 1,585,409 4.79 5.12 93.6 pass
Chlorobenzene 2,158,094 4.60 5.15 89.4 pass
Ethylbenzene 3,108,605 4.46 4.96 89.8 pass
1,1,1,2-Tetrachloroethane 1,268,970 4.59 5.04 91.0 pass
m-/p-Xylenes 2,542,599 4.82 5.07 95.1 pass
o-Xylene 2,534,541 4.61 5.01 92.1 pass
Styrene 2,002,582 4.64 4.90 94.6 pass
Bromoform 2,198,203 5.33 5.02 106 pass
1,1,2,2-Tetrachloroethane 2,016,057 4.81 5.06 95.2 pass
4-Ethyltoluene 3,662,683 4.64 5.08 91.2 pass
2-Chlorotoluene 3,054,369 4.68 5.04 92.8 pass
1,3,5-Trimethylbenzene 3,143,320 4.79 5.07 94.5 pass
1,2,4-Trimethylbenzene 3,086,793 4.61 5.00 92.2 pass
1,3-Dichlorobenzene 2,541,984 4.68 5.08 92.2 pass
1,4-Dichlorobenzene 2,558,622 4.63 5.02 92.1 pass
Benzyl chloride 2,784,131 4.79 5.03 95.1 pass
EA # 0124-075 Page 60 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 668,997 5.27 4.83 109 pass
1.000
2024-02-07 13:49
TO15_SCNV6.M
Air
X020724A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020724A_0124-075.v1
X2400696.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020724A_5ppbv TO15 LCS
1,2-Dichlorobenzene 2,495,454 4.77 5.06 94.2 pass
1,2,4-Trichlorobenzene 2,114,085 4.68 4.98 93.9 pass
Hexachlorobutadiene 2,171,415 5.52 4.94 112 pass
Naphthalene 4,347,307 4.20 5.04 83.5 pass
1-Bromopropane 1,483,344 5.20 4.96 105 pass
1-Octene 526,998 4.81 4.94 97.6 pass
n-Octane 703,032 4.84 5.02 96.5 pass
Isopropylbenzene 3,718,879 4.66 5.08 91.7 pass
n-Propylbenzene 4,355,540 4.86 5.13 94.7 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)796,254 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,048,665 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,680,041 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 61 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 742,804 5.42 4.83 112 pass
Freon 12 (CCl2F2)1,860,217 4.70 4.90 96.0 pass
Freon 114 (C2Cl2F4)2,001,619 4.89 5.01 97.6 pass
Chloromethane 691,112 4.85 4.94 98.1 pass
Chloroethene (Vinyl chloride)387,432 4.61 5.00 92.3 pass
1,3-Butadiene 705,323 4.98 4.86 102 pass
Bromomethane 404,914 4.45 4.90 90.8 pass
Chloroethane 338,694 5.02 5.08 98.8 pass
Bromoethene (Vinyl bromide)741,202 4.56 4.89 93.3 pass
Freon 11 (CCl3F)2,033,138 5.16 5.28 97.8 pass
Ethanol 327,235 4.12 4.96 83.1 pass
Acrolein 257,598 4.60 4.92 93.5 pass
Freon 113 (C2Cl3F3)1,437,745 5.05 5.08 99.5 pass
1,1-Dichloroethene 1,165,562 4.58 5.03 91.2 pass
Acetone 1,348,999 4.61 5.01 92.1 pass
Carbon disulfide 2,006,130 5.02 4.98 101 pass
Isopropyl alcohol 1,469,129 4.90 4.98 98.4 pass
Allyl chloride (3-chloropropene)302,664 5.29 5.04 105 pass
Acetonitrile 723,942 5.38 4.98 108 pass
Methylene chloride 1,008,573 4.64 5.12 90.7 pass
trans-1,2-Dichloroethene 1,042,764 5.03 5.10 98.6 pass
Methyl tert-butyl ether 1,851,716 5.29 5.14 103 pass
Acrylonitrile 549,629 4.99 5.09 97.9 pass, m
Hexane 1,128,878 5.37 5.08 106 pass
1,1-Dichloroethane 1,294,734 5.14 4.96 103 pass
Vinyl acetate 2,059,777 5.02 5.12 98.2 pass, m
Methyl ethyl ketone (2-Butanone)332,981 5.29 5.17 102 pass
Ethyl acetate 316,650 5.20 4.99 104 pass
Chloroform 1,576,953 5.29 5.02 105 pass
Tetrahydrofuran 310,602 5.31 5.06 105 pass, m
1,1,1-Trichloroethane 1,576,022 5.11 5.05 101 pass
Cyclohexane 1,200,519 5.62 5.12 110 pass
Carbon tetrachloride 1,762,191 5.09 5.04 101 pass
Benzene 2,071,550 4.98 5.03 98.9 pass
1.000
2024-02-09 03:27
TO15_SCNV6.M
Air
X020924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020924A_0124-075.v2
X2400737.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020924A_5ppbv TO15 LCS
EA # 0124-075 Page 62 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 742,804 5.42 4.83 112 pass
1.000
2024-02-09 03:27
TO15_SCNV6.M
Air
X020924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020924A_0124-075.v2
X2400737.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020924A_5ppbv TO15 LCS
2,2,4-trimethylpentane 3,832,254 5.24 5.17 101 pass
1,2-Dichloroethane 1,006,795 4.51 5.14 87.7 pass
Heptane 734,679 5.03 5.06 99.3 pass
1,2-Dichloropropane 874,258 5.05 5.04 100 pass
Methyl methacrylate 767,002 5.27 5.24 101 pass
1,4-Dioxane 497,393 5.18 5.02 103 pass
Bromodichloromethane 1,656,701 4.92 5.05 97.5 pass
cis-1,3-Dichloropropene 1,161,513 4.61 4.96 92.8 pass
Methyl isobutyl ketone 2,432,153 5.26 5.20 101 pass
Toluene 2,731,880 4.73 5.09 93.0 pass
trans-1,3-Dichloropropene 1,148,693 4.38 5.16 84.9 pass
1,1,2-Trichloroethane 987,571 4.87 5.08 95.7 pass
2-Hexanone (Methyl butyl ketone)2,312,903 5.19 5.12 101 pass
Dibromochloromethane 2,071,023 4.86 5.04 96.5 pass
1,2-Dibromoethane 1,757,762 4.92 5.12 96.2 pass
Chlorobenzene 2,394,629 4.73 5.15 91.9 pass
Ethylbenzene 3,462,632 4.60 4.96 92.6 pass
1,1,1,2-Tetrachloroethane 1,387,445 4.65 5.04 92.2 pass
m-/p-Xylenes 2,834,133 4.98 5.07 98.2 pass
o-Xylene 2,827,942 4.77 5.01 95.2 pass
Styrene 2,228,815 4.78 4.90 97.6 pass
Bromoform 2,414,440 5.42 5.02 108 pass
1,1,2,2-Tetrachloroethane 2,266,423 5.01 5.06 99.1 pass
4-Ethyltoluene 4,030,938 4.73 5.08 93.0 pass
2-Chlorotoluene 3,401,650 4.83 5.04 95.7 pass
1,3,5-Trimethylbenzene 3,474,075 4.91 5.07 96.8 pass
1,2,4-Trimethylbenzene 3,416,585 4.73 5.00 94.5 pass
1,3-Dichlorobenzene 2,791,800 4.77 5.08 93.8 pass
1,4-Dichlorobenzene 2,811,223 4.71 5.02 93.7 pass
Benzyl chloride 3,138,848 5.00 5.03 99.4 pass
1,2-Dichlorobenzene 2,727,762 4.83 5.06 95.4 pass
1,2,4-Trichlorobenzene 2,303,970 4.72 4.98 94.8 pass
Hexachlorobutadiene 2,357,408 5.55 4.94 112 pass
EA # 0124-075 Page 63 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Flags
Propylene 742,804 5.42 4.83 112 pass
1.000
2024-02-09 03:27
TO15_SCNV6.M
Air
X020924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QC
Xavier_X020924A_0124-075.v2
X2400737.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020924A_5ppbv TO15 LCS
Naphthalene 4,815,130 4.31 5.04 85.6 pass
1-Bromopropane 1,678,551 5.45 4.96 110 pass
1-Octene 597,792 5.06 4.94 103 pass
n-Octane 790,644 5.04 5.02 101 pass
Isopropylbenzene 4,130,196 4.79 5.08 94.4 pass
n-Propylbenzene 4,890,611 5.05 5.13 98.5 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)859,553 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,325,670 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,892,857 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 64 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
Propylene 698,735 4.71 4.83 4.58 97.6 2.8 pass
Freon 12 (CCl2F2)2,098,876 4.90 4.90 4.76 100 2.8 pass
Freon 114 (C2Cl2F4)2,150,558 4.86 5.01 4.72 97.0 2.9 pass
Chloromethane 709,642 4.60 4.94 4.48 93.1 2.6 pass
Chloroethene (Vinyl chloride)386,655 4.25 5.00 4.13 85.1 2.9 pass, m
1,3-Butadiene 717,788 4.68 4.86 4.45 96.2 5.2 pass
Bromomethane 426,898 4.34 4.90 4.17 88.5 3.9 pass
Chloroethane 349,631 4.79 5.08 4.74 94.2 1.0 pass
Bromoethene (Vinyl bromide)789,471 4.49 4.89 4.27 91.9 5.2 pass
Freon 11 (CCl3F)2,355,720 5.52 5.28 5.35 105 3.2 pass
Ethanol 332,941 3.87 4.96 3.74 78.1 3.5 pass
Acrolein 272,885 4.51 4.92 4.32 91.5 4.2 pass
Freon 113 (C2Cl3F3)1,523,118 4.95 5.08 4.78 97.4 3.4 pass
1,1-Dichloroethene 1,336,585 4.86 5.03 4.69 96.6 3.6 pass
Acetone 1,512,554 4.78 5.01 4.60 95.4 3.8 pass
Carbon disulfide 2,110,193 4.88 4.98 4.81 97.9 1.5 pass
Isopropyl alcohol 1,588,963 4.90 4.98 4.69 98.3 4.3 pass
Allyl chloride (3-chloropropene)319,805 5.17 5.04 5.13 102 0.7 pass
Acetonitrile 741,604 5.09 4.98 4.73 102 7.4 pass, m
Methylene chloride 1,093,526 4.65 5.12 4.54 90.9 2.4 pass
trans-1,2-Dichloroethene 1,169,169 5.21 5.10 5.09 102 2.4 pass
Methyl tert-butyl ether 2,101,958 5.55 5.14 5.36 108 3.5 pass
Acrylonitrile 581,170 4.87 5.09 4.61 95.7 5.5 pass, m
Hexane 1,211,314 5.33 5.08 5.19 105 2.7 pass
1,1-Dichloroethane 1,431,330 5.25 4.96 5.14 106 2.1 pass
Vinyl acetate 2,260,407 5.09 5.12 4.97 99.6 2.4 pass
cis-1,2-Dichloroethene 1,386,806 5.60 5.05 5.39 111 3.9 pass
Methyl ethyl ketone (2-Butanone)361,348 5.31 5.17 5.24 103 1.4 pass
Ethyl acetate 336,125 5.10 4.99 4.89 102 4.1 pass
Chloroform 1,767,449 5.47 5.02 5.38 109 1.8 pass
Tetrahydrofuran 345,954 5.46 5.06 5.22 108 4.5 pass, m
1,1,1-Trichloroethane 1,809,018 5.42 5.05 5.35 107 1.3 pass
Cyclohexane 1,284,385 5.56 5.12 5.41 109 2.8 pass
X020124A_5ppbv TO15 LCS LD
1.000
2024-02-01 13:40
TO15_SCNV6.M
Air
X020124A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020124A_0124-075.v1
X2400586.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020124A_5ppbv TO15 LCS LD
EA # 0124-075 Page 65 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X020124A_5ppbv TO15 LCS LD
1.000
2024-02-01 13:40
TO15_SCNV6.M
Air
X020124A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020124A_0124-075.v1
X2400586.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020124A_5ppbv TO15 LCS LD
Carbon tetrachloride 2,051,128 5.48 5.04 5.33 109 2.8 pass
Benzene 2,215,393 5.01 5.03 4.91 99.7 2.0 pass
2,2,4-trimethylpentane 4,103,276 5.28 5.17 5.16 102 2.4 pass
1,2-Dichloroethane 1,194,704 5.04 5.14 4.94 98.0 2.1 pass
Heptane 773,496 4.99 5.06 4.94 98.5 1.0 pass
Trichloroethene 1,216,769 4.66 5.06 4.50 92.2 3.5 pass
1,2-Dichloropropane 941,904 5.12 5.04 5.01 102 2.2 pass
Methyl methacrylate 849,858 5.50 5.24 5.34 105 2.9 pass
1,4-Dioxane 533,113 5.23 5.02 5.04 104 3.7 pass
Bromodichloromethane 1,914,215 5.36 5.05 5.19 106 3.1 pass
cis-1,3-Dichloropropene 1,293,742 4.84 4.96 4.73 97.4 2.2 pass
Methyl isobutyl ketone 2,621,170 5.34 5.20 5.20 103 2.6 pass
Toluene 2,953,552 4.80 5.09 4.67 94.3 2.7 pass
trans-1,3-Dichloropropene 1,323,999 4.74 5.16 4.62 91.8 2.4 pass
1,1,2-Trichloroethane 1,053,363 4.87 5.08 4.67 95.8 4.2 pass
Tetrachloroethene 1,812,874 5.08 5.12 4.90 99.3 3.5 pass
2-Hexanone (Methyl butyl ketone)2,503,977 5.28 5.12 5.12 103 3.1 pass
Dibromochloromethane 2,330,020 5.13 5.04 4.95 102 3.7 pass
1,2-Dibromoethane 1,904,416 5.00 5.12 4.85 97.8 3.1 pass
Chlorobenzene 2,585,662 4.80 5.15 4.62 93.1 3.7 pass
Ethylbenzene 3,843,824 4.79 4.96 4.64 96.5 3.3 pass
1,1,1,2-Tetrachloroethane 1,548,862 4.87 5.04 4.64 96.6 4.9 pass
m-/p-Xylenes 3,103,815 5.12 5.07 4.97 101 2.9 pass
o-Xylene 3,113,681 4.93 5.01 4.76 98.3 3.5 pass
Styrene 2,387,802 4.81 4.90 4.63 98.1 3.9 pass
Bromoform 2,671,774 5.63 5.02 5.41 112 4.0 pass
1,1,2,2-Tetrachloroethane 2,454,563 5.09 5.06 4.92 101 3.4 pass
4-Ethyltoluene 4,468,194 4.92 5.08 4.72 96.8 4.1 pass
2-Chlorotoluene 3,795,877 5.06 5.04 4.88 100 3.6 pass
1,3,5-Trimethylbenzene 3,793,727 5.03 5.07 4.91 99.2 2.3 pass
1,2,4-Trimethylbenzene 3,781,402 4.92 5.00 4.74 98.2 3.6 pass
1,3-Dichlorobenzene 2,994,577 4.80 5.08 4.60 94.4 4.3 pass
1,4-Dichlorobenzene 3,026,149 4.76 5.02 4.51 94.7 5.4 pass
EA # 0124-075 Page 66 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X020124A_5ppbv TO15 LCS LD
1.000
2024-02-01 13:40
TO15_SCNV6.M
Air
X020124A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020124A_0124-075.v1
X2400586.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020124A_5ppbv TO15 LCS LD
Benzyl chloride 3,522,736 5.26 5.03 5.05 105 4.2 pass
1,2-Dichlorobenzene 2,930,299 4.87 5.06 4.72 96.2 3.3 pass
1,2,4-Trichlorobenzene 2,423,239 4.66 4.98 4.26 93.6 9.1 pass
Hexachlorobutadiene 2,497,078 5.52 4.94 5.12 112 7.4 pass
Naphthalene 5,036,384 4.23 5.04 3.93 84.1 7.5 pass
1-Bromopropane 1,769,583 5.31 4.96 5.17 107 2.7 pass
1-Octene 652,406 5.18 4.94 5.04 105 2.9 pass
n-Octane 858,469 5.14 5.02 5.02 102 2.4 pass
Isopropylbenzene 4,456,440 4.85 5.08 4.74 95.6 2.3 pass
n-Propylbenzene 5,344,053 5.18 5.13 5.01 101 3.5 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)930,038 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,530,378 12.44 5.16 pass
Chlorobenzene-d5 (IS)3,082,249 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 67 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
Propylene 673,910 4.88 4.83 4.98 101 1.9 pass
Freon 12 (CCl2F2)1,866,102 4.68 4.90 4.78 95.6 2.2 pass
Freon 114 (C2Cl2F4)1,976,669 4.79 5.01 4.87 95.6 1.6 pass
Chloromethane 669,445 4.66 4.94 4.78 94.3 2.6 pass
Chloroethene (Vinyl chloride)337,372 3.98 5.00 4.22 79.7 5.8 pass, m
1,3-Butadiene 597,995 4.19 4.86 4.41 86.1 5.3 pass
Bromomethane 401,964 4.39 4.90 4.49 89.4 2.4 pass, m
Chloroethane 333,151 4.89 5.08 5.00 96.4 2.2 pass
Bromoethene (Vinyl bromide)723,904 4.42 4.89 4.57 90.4 3.3 pass
Freon 11 (CCl3F)2,036,531 5.13 5.28 5.28 97.2 3.0 pass
Ethanol 314,398 3.92 4.96 3.98 79.2 1.3 pass
Acrolein 260,406 4.62 4.92 4.63 93.7 0.3 pass
Freon 113 (C2Cl3F3)1,430,709 4.99 5.08 5.06 98.2 1.6 pass
1,1-Dichloroethene 1,170,522 4.57 5.03 4.73 90.8 3.4 pass
Acetone 1,328,313 4.51 5.01 4.65 89.9 3.3 pass
Carbon disulfide 1,954,467 4.85 4.98 4.96 97.3 2.2 pass
Isopropyl alcohol 1,431,256 4.74 4.98 4.86 95.0 2.5 pass
Allyl chloride (3-chloropropene)298,400 5.17 5.04 5.10 103 1.4 pass
Acetonitrile 676,976 4.99 4.98 5.04 100 1.1 pass
Methylene chloride 995,688 4.55 5.12 4.61 88.8 1.4 pass
trans-1,2-Dichloroethene 1,046,391 5.00 5.10 5.14 98.1 2.6 pass
Methyl tert-butyl ether 1,868,489 5.29 5.14 5.41 103 2.1 pass
Acrylonitrile 546,956 4.92 5.09 4.94 96.7 0.5 pass, m
Hexane 1,114,820 5.26 5.08 5.39 104 2.4 pass
1,1-Dichloroethane 1,280,699 5.04 4.96 5.19 102 2.8 pass
Vinyl acetate 2,077,676 5.02 5.12 5.16 98.2 2.6 pass, m
cis-1,2-Dichloroethene 1,222,409 5.30 5.05 5.42 105 2.3 pass
Methyl ethyl ketone (2-Butanone)330,760 5.22 5.17 5.32 101 1.9 pass
Ethyl acetate 304,595 4.96 4.99 5.09 99.4 2.5 pass
Chloroform 1,578,277 5.25 5.02 5.38 105 2.5 pass
Tetrahydrofuran 313,088 5.31 5.06 5.43 105 2.3 pass
1,1,1-Trichloroethane 1,595,299 5.13 5.05 5.26 102 2.5 pass
Cyclohexane 1,169,329 5.43 5.12 5.63 106 3.6 pass
X020524A_5ppbv TO15 LCS LD
1.000
2024-02-05 17:14
TO15_SCNV6.M
Air
X020524A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020524A_0124-075.v1
X2400651.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020524A_5ppbv TO15 LCS LD
EA # 0124-075 Page 68 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X020524A_5ppbv TO15 LCS LD
1.000
2024-02-05 17:14
TO15_SCNV6.M
Air
X020524A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020524A_0124-075.v1
X2400651.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020524A_5ppbv TO15 LCS LD
Carbon tetrachloride 1,772,129 5.08 5.04 5.14 101 1.2 pass
Benzene 2,064,389 5.06 5.03 5.00 101 1.2 pass
2,2,4-trimethylpentane 3,751,181 5.23 5.17 5.21 101 0.5 pass
1,2-Dichloroethane 1,037,309 4.75 5.14 4.71 92.2 0.7 pass
Heptane 721,937 5.05 5.06 4.96 99.6 1.7 pass
Trichloroethene 1,105,609 4.59 5.06 4.62 90.8 0.6 pass
1,2-Dichloropropane 860,074 5.07 5.04 5.07 101 0.1 pass
Methyl methacrylate 772,394 5.42 5.24 5.35 103 1.2 pass
1,4-Dioxane 489,510 5.20 5.02 5.15 104 1.0 pass
Bromodichloromethane 1,661,349 5.04 5.05 5.03 99.8 0.2 pass
cis-1,3-Dichloropropene 1,170,571 4.74 4.96 4.73 95.5 0.3 pass
Methyl isobutyl ketone 2,358,149 5.20 5.20 5.14 100 1.2 pass
Toluene 2,702,313 4.54 5.09 4.59 89.2 1.0 pass
trans-1,3-Dichloropropene 1,170,756 4.33 5.16 4.37 84.0 0.9 pass
1,1,2-Trichloroethane 967,253 4.63 5.08 4.63 91.0 0.1 pass
Tetrachloroethene 1,683,510 4.88 5.12 4.93 95.4 1.0 pass
2-Hexanone (Methyl butyl ketone)2,242,910 4.89 5.12 4.95 95.5 1.3 pass
Dibromochloromethane 2,046,957 4.66 5.04 4.71 92.5 0.9 pass
1,2-Dibromoethane 1,735,924 4.71 5.12 4.75 92.2 0.6 pass
Chlorobenzene 2,376,680 4.56 5.15 4.56 88.5 0.0 pass
Ethylbenzene 3,482,428 4.49 4.96 4.53 90.4 0.9 pass
1,1,1,2-Tetrachloroethane 1,378,560 4.48 5.04 4.51 88.9 0.7 pass
m-/p-Xylenes 2,809,621 4.79 5.07 4.86 94.5 1.4 pass
o-Xylene 2,811,752 4.60 5.01 4.64 91.8 1.0 pass
Styrene 2,204,319 4.59 4.90 4.65 93.7 1.3 pass
Bromoform 2,366,449 5.16 5.02 5.20 103 0.8 pass
1,1,2,2-Tetrachloroethane 2,215,599 4.75 5.06 4.81 94.0 1.2 pass
4-Ethyltoluene 4,037,905 4.60 5.08 4.64 90.4 0.9 pass
2-Chlorotoluene 3,408,023 4.70 5.04 4.74 93.1 0.9 pass
1,3,5-Trimethylbenzene 3,491,409 4.79 5.07 4.77 94.4 0.3 pass
1,2,4-Trimethylbenzene 3,426,069 4.60 5.00 4.60 92.0 0.0 pass
1,3-Dichlorobenzene 2,758,067 4.57 5.08 4.56 89.9 0.1 pass
1,4-Dichlorobenzene 2,777,382 4.52 5.02 4.48 89.9 0.8 pass
EA # 0124-075 Page 69 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X020524A_5ppbv TO15 LCS LD
1.000
2024-02-05 17:14
TO15_SCNV6.M
Air
X020524A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020524A_0124-075.v1
X2400651.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020524A_5ppbv TO15 LCS LD
Benzyl chloride 3,121,358 4.82 5.03 4.84 95.9 0.4 pass
1,2-Dichlorobenzene 2,686,714 4.62 5.06 4.61 91.2 0.2 pass
1,2,4-Trichlorobenzene 2,280,657 4.54 4.98 4.37 91.1 3.8 pass
Hexachlorobutadiene 2,356,942 5.39 4.94 5.14 109 4.6 pass
Naphthalene 4,674,334 4.06 5.04 3.92 80.7 3.5 pass
1-Bromopropane 1,599,013 5.15 4.96 5.27 104 2.4 pass
1-Octene 601,035 4.94 4.94 4.88 100 1.1 pass
n-Octane 791,905 4.90 5.02 4.93 97.8 0.7 pass
Isopropylbenzene 4,123,424 4.65 5.08 4.65 91.4 0.0 pass
n-Propylbenzene 4,860,497 4.87 5.13 4.89 95.0 0.3 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)866,523 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,258,055 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,980,697 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 70 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
cis-1,2-Dichloroethene 1,191,790 5.27 5.05 5.23 104 0.8 pass
Trichloroethene 1,122,333 4.60 5.06 4.62 91.0 0.4 pass
Tetrachloroethene 1,708,005 5.22 5.12 5.16 102 1.2 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)849,589 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,299,608 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,827,373 16.57 4.92 pass
X020624A_5ppbv TO15 LCS LD
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
1.000
2024-02-06 14:21
TO15_SCNV6.M
Air
X020624A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020624A_0124-075.v1
X2400673.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020624A_5ppbv TO15 LCS LD
EA # 0124-075 Page 71 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
Propylene 664,826 5.29 4.83 5.27 110 0.3 pass
Freon 12 (CCl2F2)1,692,655 4.66 4.90 4.61 95.2 1.1 pass
Freon 114 (C2Cl2F4)1,821,662 4.85 5.01 4.83 96.8 0.5 pass
Chloromethane 620,548 4.75 4.94 4.68 96.0 1.4 pass
Chloroethene (Vinyl chloride)317,454 4.11 5.00 4.11 82.4 0.2 pass
1,3-Butadiene 577,436 4.44 4.86 4.31 91.3 3.1 pass
Bromomethane 372,571 4.47 4.90 4.38 91.0 1.9 pass, m
Chloroethane 301,704 4.87 5.08 4.84 95.9 0.6 pass
Bromoethene (Vinyl bromide)676,054 4.54 4.89 4.48 92.8 1.3 pass
Freon 11 (CCl3F)1,834,734 5.07 5.28 5.00 96.2 1.5 pass
Ethanol 292,211 4.01 4.96 3.86 80.9 3.7 pass
Acrolein 231,684 4.51 4.92 4.40 91.6 2.4 pass
Freon 113 (C2Cl3F3)1,322,652 5.06 5.08 4.99 99.8 1.5 pass
1,1-Dichloroethene 1,040,157 4.46 5.03 4.40 88.6 1.4 pass
Acetone 1,186,736 4.42 5.01 4.38 88.3 1.0 pass
Carbon disulfide 1,764,187 4.81 4.98 4.76 96.5 1.0 pass
Isopropyl alcohol 1,307,132 4.75 4.98 4.71 95.4 1.0 pass
Allyl chloride (3-chloropropene)258,999 4.93 5.04 5.07 97.9 2.8 pass
Acetonitrile 639,036 5.17 4.98 5.09 104 1.6 pass
Methylene chloride 888,102 4.45 5.12 4.44 87.0 0.3 pass
trans-1,2-Dichloroethene 929,546 4.88 5.10 4.81 95.8 1.5 pass
Methyl tert-butyl ether 1,638,517 5.10 5.14 5.10 99.2 0.1 pass
Acrylonitrile 489,788 4.84 5.09 4.61 95.1 4.9 pass, m
Hexane 993,191 5.15 5.08 5.14 101 0.2 pass
1,1-Dichloroethane 1,146,383 4.96 4.96 4.90 99.8 1.2 pass
Vinyl acetate 1,895,851 5.04 5.12 5.00 98.5 0.7 pass
cis-1,2-Dichloroethene 1,083,484 5.16 5.05 5.07 102 1.8 pass
Methyl ethyl ketone (2-Butanone)290,491 5.03 5.17 4.90 97.3 2.7 pass
Ethyl acetate 274,662 4.91 4.99 4.87 98.4 0.8 pass
Chloroform 1,413,892 5.16 5.02 5.05 103 2.1 pass
Tetrahydrofuran 281,602 5.24 5.06 5.21 104 0.7 pass
1,1,1-Trichloroethane 1,417,656 5.01 5.05 5.01 99.2 0.0 pass
Cyclohexane 1,050,427 5.36 5.12 5.31 105 0.9 pass
X020724A_5ppbv TO15 LCS LD
1.000
2024-02-07 14:37
TO15_SCNV6.M
Air
X020724A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020724A_0124-075.v1
X2400697.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020724A_5ppbv TO15 LCS LD
EA # 0124-075 Page 72 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X020724A_5ppbv TO15 LCS LD
1.000
2024-02-07 14:37
TO15_SCNV6.M
Air
X020724A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020724A_0124-075.v1
X2400697.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020724A_5ppbv TO15 LCS LD
Carbon tetrachloride 1,571,497 4.95 5.04 4.89 98.3 1.2 pass
Benzene 1,836,268 4.83 5.03 4.84 96.1 0.2 pass
2,2,4-trimethylpentane 3,345,694 5.01 5.17 5.05 96.8 0.8 pass
1,2-Dichloroethane 912,341 4.48 5.14 4.46 87.0 0.5 pass
Heptane 642,972 4.82 5.06 4.77 95.2 1.1 pass
Trichloroethene 1,021,411 4.55 5.06 4.55 90.0 0.0 pass
1,2-Dichloropropane 760,685 4.81 5.04 4.82 95.5 0.2 pass
Methyl methacrylate 688,140 5.18 5.24 5.10 98.9 1.6 pass, m
1,4-Dioxane 446,107 5.09 5.02 4.92 101 3.4 pass
Bromodichloromethane 1,490,453 4.85 5.05 4.79 96.0 1.3 pass
cis-1,3-Dichloropropene 1,049,629 4.56 4.96 4.58 91.9 0.3 pass
Methyl isobutyl ketone 2,149,892 5.09 5.20 5.05 97.9 0.8 pass
Toluene 2,434,953 4.56 5.09 4.51 89.5 1.2 pass
trans-1,3-Dichloropropene 1,055,304 4.35 5.16 4.25 84.3 2.3 pass
1,1,2-Trichloroethane 871,793 4.64 5.08 4.63 91.3 0.2 pass
Tetrachloroethene 1,550,828 5.00 5.12 5.04 97.8 0.8 pass
2-Hexanone (Methyl butyl ketone)2,030,402 4.93 5.12 4.89 96.3 0.6 pass
Dibromochloromethane 1,868,123 4.74 5.04 4.75 94.0 0.2 pass
1,2-Dibromoethane 1,588,847 4.81 5.12 4.79 93.9 0.3 pass
Chlorobenzene 2,182,400 4.66 5.15 4.60 90.5 1.2 pass
Ethylbenzene 3,111,498 4.47 4.96 4.46 90.0 0.2 pass
1,1,1,2-Tetrachloroethane 1,273,720 4.61 5.04 4.59 91.5 0.5 pass
m-/p-Xylenes 2,535,808 4.82 5.07 4.82 95.0 0.1 pass
o-Xylene 2,541,059 4.63 5.01 4.61 92.4 0.4 pass
Styrene 2,018,159 4.68 4.90 4.64 95.5 0.9 pass
Bromoform 2,214,432 5.38 5.02 5.33 107 0.9 pass
1,1,2,2-Tetrachloroethane 2,015,544 4.82 5.06 4.81 95.3 0.1 pass
4-Ethyltoluene 3,670,449 4.65 5.08 4.64 91.5 0.3 pass
2-Chlorotoluene 3,069,161 4.71 5.04 4.68 93.3 0.6 pass
1,3,5-Trimethylbenzene 3,156,418 4.82 5.07 4.79 95.0 0.5 pass
1,2,4-Trimethylbenzene 3,107,671 4.65 5.00 4.61 92.9 0.8 pass
1,3-Dichlorobenzene 2,573,579 4.75 5.08 4.68 93.5 1.4 pass
1,4-Dichlorobenzene 2,594,084 4.70 5.02 4.63 93.5 1.5 pass
EA # 0124-075 Page 73 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X020724A_5ppbv TO15 LCS LD
1.000
2024-02-07 14:37
TO15_SCNV6.M
Air
X020724A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020724A_0124-075.v1
X2400697.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020724A_5ppbv TO15 LCS LD
Benzyl chloride 2,826,901 4.87 5.03 4.79 96.7 1.7 pass
1,2-Dichlorobenzene 2,528,573 4.84 5.06 4.77 95.6 1.4 pass
1,2,4-Trichlorobenzene 2,234,190 4.95 4.98 4.68 99.4 5.7 pass
Hexachlorobutadiene 2,265,170 5.77 4.94 5.52 117 4.4 pass
Naphthalene 4,569,083 4.42 5.04 4.20 87.8 5.1 pass
1-Bromopropane 1,472,874 5.21 4.96 5.20 105 0.2 pass
1-Octene 524,716 4.80 4.94 4.81 97.3 0.3 pass
n-Octane 710,067 4.90 5.02 4.84 97.6 1.1 pass
Isopropylbenzene 3,717,958 4.66 5.08 4.66 91.8 0.1 pass
n-Propylbenzene 4,391,284 4.90 5.13 4.86 95.6 0.9 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)788,768 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,036,867 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,676,651 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 74 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
Propylene 746,594 5.44 4.83 5.42 113 0.3 pass
Freon 12 (CCl2F2)1,865,810 4.71 4.90 4.70 96.2 0.1 pass
Freon 114 (C2Cl2F4)2,009,777 4.90 5.01 4.89 97.9 0.2 pass
Chloromethane 693,256 4.86 4.94 4.85 98.2 0.1 pass
Chloroethene (Vinyl chloride)398,676 4.73 5.00 4.61 94.8 2.7 pass, m
1,3-Butadiene 705,751 4.97 4.86 4.98 102 0.1 pass
Bromomethane 404,572 4.44 4.90 4.45 90.6 0.3 pass
Chloroethane 335,639 4.96 5.08 5.02 97.7 1.1 pass
Bromoethene (Vinyl bromide)750,219 4.61 4.89 4.56 94.3 1.0 pass
Freon 11 (CCl3F)2,049,551 5.19 5.28 5.16 98.4 0.6 pass
Ethanol 333,249 4.19 4.96 4.12 84.5 1.6 pass
Acrolein 260,078 4.64 4.92 4.60 94.2 0.8 pass
Freon 113 (C2Cl3F3)1,447,253 5.08 5.08 5.05 100 0.5 pass
1,1-Dichloroethene 1,178,498 4.63 5.03 4.58 92.0 0.9 pass
Acetone 1,355,389 4.63 5.01 4.61 92.3 0.3 pass
Carbon disulfide 2,001,446 5.00 4.98 5.02 100 0.4 pass
Isopropyl alcohol 1,495,127 4.98 4.98 4.90 99.9 1.6 pass
Allyl chloride (3-chloropropene)299,518 5.23 5.04 5.29 104 1.2 pass
Acetonitrile 715,944 5.31 4.98 5.38 107 1.3 pass, m
Methylene chloride 1,003,220 4.61 5.12 4.64 90.0 0.7 pass
trans-1,2-Dichloroethene 1,046,813 5.04 5.10 5.03 98.8 0.2 pass
Methyl tert-butyl ether 1,846,015 5.26 5.14 5.29 102 0.5 pass
Acrylonitrile 552,099 5.00 5.09 4.99 98.2 0.3 pass, m
Hexane 1,136,906 5.40 5.08 5.37 106 0.5 pass
1,1-Dichloroethane 1,287,253 5.10 4.96 5.14 103 0.8 pass
Vinyl acetate 2,095,273 5.10 5.12 5.02 99.7 1.5 pass, m
Methyl ethyl ketone (2-Butanone)335,069 5.32 5.17 5.29 103 0.5 pass
Ethyl acetate 316,097 5.18 4.99 5.20 104 0.3 pass
Chloroform 1,580,690 5.29 5.02 5.29 105 0.1 pass
Tetrahydrofuran 312,318 5.33 5.06 5.31 105 0.4 pass
1,1,1-Trichloroethane 1,593,323 5.16 5.05 5.11 102 0.9 pass
Cyclohexane 1,209,128 5.65 5.12 5.62 110 0.5 pass
Carbon tetrachloride 1,766,312 5.10 5.04 5.09 101 0.1 pass
X020924A_5ppbv TO15 LCS LD
1.000
2024-02-09 04:15
TO15_SCNV6.M
Air
X020924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020924A_0124-075.v2
X2400738.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020924A_5ppbv TO15 LCS LD
EA # 0124-075 Page 75 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X020924A_5ppbv TO15 LCS LD
1.000
2024-02-09 04:15
TO15_SCNV6.M
Air
X020924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020924A_0124-075.v2
X2400738.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020924A_5ppbv TO15 LCS LD
Benzene 2,096,036 5.01 5.03 4.98 99.6 0.7 pass
2,2,4-trimethylpentane 3,875,336 5.27 5.17 5.24 102 0.6 pass
1,2-Dichloroethane 1,007,746 4.49 5.14 4.51 87.4 0.4 pass
Heptane 741,395 5.05 5.06 5.03 99.7 0.4 pass
1,2-Dichloropropane 872,753 5.01 5.04 5.05 99.6 0.7 pass
Methyl methacrylate 771,376 5.27 5.24 5.27 101 0.1 pass
1,4-Dioxane 491,640 5.10 5.02 5.18 102 1.7 pass
Bromodichloromethane 1,682,954 4.98 5.05 4.92 98.5 1.1 pass
cis-1,3-Dichloropropene 1,173,486 4.63 4.96 4.61 93.3 0.5 pass
Methyl isobutyl ketone 2,447,292 5.26 5.20 5.26 101 0.1 pass
Toluene 2,713,113 4.59 5.09 4.73 90.2 3.0 pass
trans-1,3-Dichloropropene 1,163,973 4.33 5.16 4.38 84.0 1.0 pass
1,1,2-Trichloroethane 983,141 4.73 5.08 4.87 93.1 2.8 pass
2-Hexanone (Methyl butyl ketone)2,318,576 5.08 5.12 5.19 99.4 2.1 pass
Dibromochloromethane 2,053,078 4.71 5.04 4.86 93.4 3.2 pass
1,2-Dibromoethane 1,737,268 4.75 5.12 4.92 92.8 3.5 pass
Chlorobenzene 2,480,640 4.79 5.15 4.73 93.0 1.2 pass
Ethylbenzene 3,511,886 4.56 4.96 4.60 91.8 0.9 pass
1,1,1,2-Tetrachloroethane 1,413,874 4.63 5.04 4.65 91.8 0.5 pass
m-/p-Xylenes 2,908,122 4.99 5.07 4.98 98.4 0.2 pass
o-Xylene 2,858,708 4.71 5.01 4.77 94.0 1.3 pass
Styrene 2,235,848 4.69 4.90 4.78 95.6 2.0 pass
Bromoform 2,462,207 5.40 5.02 5.42 108 0.4 pass
1,1,2,2-Tetrachloroethane 2,340,129 5.05 5.06 5.01 100.0 0.9 pass
4-Ethyltoluene 3,954,735 4.53 5.08 4.73 89.1 4.3 pass
2-Chlorotoluene 3,314,306 4.60 5.04 4.83 91.1 4.9 pass
1,3,5-Trimethylbenzene 3,439,579 4.75 5.07 4.91 93.6 3.3 pass
1,2,4-Trimethylbenzene 3,456,002 4.68 5.00 4.73 93.4 1.2 pass
1,3-Dichlorobenzene 2,843,381 4.74 5.08 4.77 93.3 0.5 pass
1,4-Dichlorobenzene 2,868,410 4.69 5.02 4.71 93.4 0.3 pass
Benzyl chloride 3,158,527 4.91 5.03 5.00 97.7 1.7 pass
1,2-Dichlorobenzene 2,792,212 4.83 5.06 4.83 95.4 0.0 pass
1,2,4-Trichlorobenzene 2,417,839 4.84 4.98 4.72 97.2 2.5 pass
EA # 0124-075 Page 76 of 85
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X020924A_5ppbv TO15 LCS LD
1.000
2024-02-09 04:15
TO15_SCNV6.M
Air
X020924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X020924A_0124-075.v2
X2400738.D
1.000
Enthalpy Analytical
Job No.: 0124-075-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X020924A_5ppbv TO15 LCS LD
Hexachlorobutadiene 2,497,937 5.75 4.94 5.55 116 3.4 pass
Naphthalene 5,039,400 4.41 5.04 4.31 87.5 2.2 pass
1-Bromopropane 1,696,076 5.49 4.96 5.45 111 0.9 pass
1-Octene 606,256 5.01 4.94 5.06 102 0.9 pass
n-Octane 784,896 4.89 5.02 5.04 97.5 3.1 pass
Isopropylbenzene 4,141,608 4.70 5.08 4.79 92.4 2.1 pass
n-Propylbenzene 4,961,183 5.01 5.13 5.05 97.6 0.9 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)861,025 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,341,981 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,961,563 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0124-075 Page 77 of 85

Narrative Summary

EA # 0124-075 Page 78 of 85

Enthalpy Analytical Narrative Summary

Company AECOM - Morrisville Client # Frye & Webster – DC410064
Client Project# 60722767
Analyst TDD/KMB Job # 0124-075
Parameters EPA Method TO-15 # Samples 8 (1.4L) Canisters

Custody David Myers received the samples on 2/1/2024 after being relinquished
by AECOM - Morrisville. The samples were then logged in by Alyssa
Miller the same day. The samples were received at ambient temperature
and in good condition.
Prior to, during, and after analysis, the samples were kept under lock with
access only to authorized personnel by Enthalpy Analytical, LLC.
Analysis The samples were analyzed for the TO-15 target compound list using the
analytical procedures in EPA Method TO-15, Determination of Volatile
Organic Compounds (VOCs) In Air Collected In Specially-Prepared
Canister And Analyzed by Gas Chromatography/Mass Spectrometry
(GC/MS).
Upon receipt, the canister pressures were measured and recorded. The
canisters were then pressurized with UHP nitrogen and a dilution ratio
was calculated for each canister. See the Canister Pressurization Data
sheet located in the Results section of this report.
The samples were analyzed at various dilutions to bring
Tetrachloroethene into the instrument’s calibration range and to achieve
the client’s MDL as best as possible. Due to sample matrix interfering
with the quantitative analysis of the samples, the lowest dilutions reported
for SG-1 and SG-11 are 1,000-fold and 100-fold, respectively. Dilution
factors are included in the sample header information.
The Agilent Technologies Model 6890N, Gas Chromatograph "Xavier"
(S/N US10721018) equipped with a 5975C VL Mass Selective Detector
(S/N US71215962) was used for this analysis. The samples and standards
were introduced directly to the analyzer using an Entech 7200
Preconcentrator.

Calibration The BFB tune analyses associated with the initial and continuing
calibrations met all method acceptance criteria.
The initial calibration (X100722A-TO15) met the 30% RSD criteria. The
initial calibration verification (ICV) met the 70-130% recovery criteria.
The continuing calibration (CCV) met the 30% difference criteria. Full
calibration data is available upon request.
EA # 0124-075 Page 79 of 85

Enthalpy Analytical Narrative Summary
(continued)

Chromatographic
Conditions
The acquisition method (TO15_SCNV6.M) may be made available upon
request.
QC Notes All internal standard area (IS) responses and retention time criteria were
met for this analysis.
The laboratory duplicate (LD) analyzed with this sample set met the 25%
difference criteria for all detected compounds with the exception of
Methyl isobutyl ketone at approximately 33%. The LCSs were also
analyzed in duplicate and meet the 25% difference criteria for all reported
compounds.
The laboratory humid blanks associated with this analysis did not contain
any of the target analytes at a concentration greater than 3x their MDL.
The Laboratory Control Samples (LCS) met the 70-130% recovery
criteria for all reported compounds.
The samples were analyzed within the 30-day holding time required by
the method.
Reporting Notes The analysis met the requirements of the TNI Standard. Any deviations
from the requirements of the reference method or TNI Standard have been
stated above.
The results presented in this report are representative of the samples as
provided to the laboratory.

EA # 0124-075 Page 80 of 85

General Reporting Notes

The following are general reporting notes that are applicable to all Enthalpy Analytical, LLC data
reports, unless specifically noted otherwise.

 Any analysis which refers to the method as “Type” represents a planned deviation from the
reference method. For instance a Hydrogen Sulfide assay from a Tedlar bag would be labeled
as “EPA Method 16-Type” because Tedlar bags are not mentioned as one of the collection
options in EPA Method 16.
 The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory
cannot determine the presence of the analyte of interest reliably.
 The acronym LOQ represents the Limit of Quantification. Below this value the laboratory
cannot quantitate the analyte of interest within the criteria of the method.
 The acronym ND following a value indicates a non-detect or analytical result below the MDL.
 The letter J in the Qualifier or Flag column in the results indicates that the value is between
the MDL and the LOQ. The laboratory can positively identify the analyte of interest as
present, but the value should be considered an estimate.
 The letter E in the Qualifier or Flag column indicates an analytical result exceeding 100% of
the highest calibration point. The associated value should be considered as an estimate.
 Sample results are presented ‘as measured’ for single injection methodologies, or an average
value if multiple injections are made. If all injections are below the MDL, the sample is
considered non-detect and the ND value is presented. If one, but not all, are below the MDL,
the MDL value is used for any injections that are below the MDL. For example, if the MDL is
0.500 and LOQ is 1.00, and the instrument measures 0.355, 0.620, and 0.442 - the result
reported is the average of 0.500, 0.620, and 0.500 - - - i.e. 0.540 with a J flag.
 When a spike recovery (Bag Spike, Collocated Spike Train, or liquid matrix spike) is being
calculated, the native (unspiked) sample result is used in the calculations, as long as the value
is above the MDL. If a sample is ND, then 0 is used as the native amount (not the MDL
value).
 The acronym DF represents Dilution Factor. This number represents dilution of the sample
during the preparation and/or analysis process. The analytical result taken from a laboratory
instrument is multiplied by the DF to determine the final undiluted sample results.
 The addition of MS to the Sample ID represents a Matrix Spike. An aliquot of an actual
sample is spiked with a known amount of analyte so that a percent recovery value can be
determined. The MS analysis indicates what effect the sample matrix may have on the target
analyte, i.e. whether or not anything in the sample matrix interferes with the analysis of the
analyte(s).
EA # 0124-075 Page 81 of 85

General Reporting Notes
(continued)
 The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the
same manner as a MS, the use of duplicate matrix spikes allows further confirmation of
laboratory quality by showing the consistency of results gained by performing the same steps
multiple times.
 The addition of LD to the Sample ID represents a Laboratory Duplicate. The analyst prepares
an additional aliquot of sample for testing and the results of the duplicate analysis are
compared to the initial result. The result should have a difference value of within 10% of the
initial result (if the results of the original analysis are greater than the LOQ).
 The addition of AD to the Sample ID represents an Alternate Dilution. The analyst prepares an
additional aliquot at a different dilution factor (usually double the initial factor). This analysis
helps confirm that no additional compound is present and coeluting or sharing absorbance with
the analyte of interest, as they would have a different response/absorbance than the analyte of
interest.
 The Sample ID LCS represents a Laboratory Control Sample. Clean matrix, similar to the
client sample matrix, prepared and analyzed by the laboratory using the same reagents, spiking
standards and procedures used for the client samples. The LCS is used to assess the control of
the laboratory’s analytical system. Whenever spikes are prepared for our client projects, two
spikes are retained as LCSs. The LCSs are labeled with the associated project number and kept
in-house at the appropriate temperature conditions. When the project samples are received for
analysis, the LCSs are analyzed to confirm that the analyte could be recovered from the media,
separate from the samples which were used on the project and which may have been affected
by source matrix, sample collection, and/or sample transport.
 Significant Figures: Where the reported value is much greater than unity (1.00) in the units
expressed, the number is rounded to a whole number of units, rather than to 3 significant
figures. For example, a value of 10,456.45 ug catch is rounded to 10,456 ug. There are five
significant digits displayed, but no confidence should be placed on more than two significant
digits. In the case of small numbers, generally 3 significant figures are presented, but still only
2 should be used with confidence. Many neat materials are only certified to 3 digits, and as the
mathematically correct final result is always 1 digit less than all its pre-cursors - 2 significant
figures are what are most defensible.
 Manual Integration: The data systems used for processing will flag manually integrated
peaks with an “M”. There are several reasons a peak may be manually integrated. These
reasons will be identified by the following two letter designations on sample chromatograms,
if provided in the report. The peak was not integrated by the software “NI”, the peak was
integrated incorrectly by the software “II” or the wrong peak was integrated by the software
“WP”. These codes will accompany the analyst’s manual integration stamp placed next to the
compound name on the chromatogram.
EA # 0124-075 Page 82 of 85

Sample Custody
EA # 0124-075 Page 83 of 85
EA # 0124-075 Page 84 of 85

This Is The Last Page
Of This Report.

EA # 0124-075 Page 85 of 85
AECOM - Morrisville
1600 Perimeter Park Dr.
Morrisville, NC 27560

Frye & Webster – DC410064
Client Project# 60722767

Analytical Report
(0224-196)

EPA Method TO-15
TO-15 Target Compund List

Enthalpy Analytical, LLC
Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com
800-1 Capitola Drive Durham, NC 27713-4385

I certify that to the best of my knowledge all analytical data presented in this report:
 Have been checked for completeness
 Are accurate, error-free, and legible
 Have been conducted in accordance with approved protocol, and that all deviations and
analytical problems are summarized in the appropriate narrative(s)
This analytical report was prepared in Portable Document Format (.PDF). This report shall not be
reproduced except in full without approval of the laboratory. This will provide assurance that parts of a
report are not taken out of context.

Report Issued: 3/7/24
EA # 0224-196 Page 2 of 25

Results
EA # 0224-196 Page 3 of 25
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene 58.1 0.0865 0.0783 99.9 0.149 0.135
Freon 12 (CCl2F2)0.453 0.0877 0.0783 2.24 0.433 0.387
Freon 114 (C2Cl2F4)ND 0.0897 0.0783 ND 0.627 0.547
Chloromethane 0.131 0.0886 0.0783 0.270 0.183 0.162
Chloroethene (Vinyl chloride)ND 0.0895 0.0783 ND 0.229 0.200
1,3-Butadiene 5.27 0.0871 0.0783 11.7 0.193 0.173
Bromomethane ND 0.0878 0.0783 ND 0.341 0.304
Chloroethane ND 0.0910 0.0783 ND 0.240 0.207
Bromoethene (Vinyl bromide)ND 0.0876 0.0783 ND 0.383 0.342
Freon 11 (CCl3F)0.209 0.0945 0.0783 1.17 0.530 0.440
Ethanol 2.27 0.0887 0.0887 4.28 0.167 0.167
Acrolein ND 0.0882 0.0783 ND 0.202 0.180
Freon 113 (C2Cl3F3)ND 0.0909 0.0783 ND 0.696 0.600
1,1-Dichloroethene ND 0.0901 0.0783 ND 0.357 0.310
Acetone 8.63 0.0897 0.0783 20.5 0.213 0.186
Carbon disulfide 17.9 0.0893 0.0783 55.6 0.278 0.244
Isopropyl alcohol 0.955 0.0893 0.0783 2.35 0.219 0.192
Allyl chloride (3-chloropropene)ND 0.0967 0.0783 ND 0.302 0.245
Acetonitrile 0.180 0.0893 0.0783 0.302 0.150 0.131
Methylene chloride 0.576 0.0917 0.0783 2.00 0.318 0.272
trans-1,2-Dichloroethene ND 0.0913 0.0783 ND 0.362 0.310
Methyl tert-butyl ether ND 0.0920 0.0783 ND 0.332 0.282
Acrylonitrile 0.346 0.0912 0.0783 0.751 0.198 0.170 m
Hexane 4.08 0.0910 0.0783 14.4 0.320 0.276
1,1-Dichloroethane ND 0.0889 0.0783 ND 0.360 0.317
Vinyl acetate ND 0.0916 0.0783 ND 0.322 0.276
cis-1,2-Dichloroethene 0.111 0.0904 0.0783 0.440 0.358 0.310
Methyl ethyl ketone (2-Butanone)1.29 0.0926 0.0783 3.79 0.273 0.231
Ethyl acetate 0.284 0.0894 0.0783 1.02 0.322 0.282
Chloroform 0.190 0.0898 0.0783 0.929 0.438 0.382 m
Tetrahydrofuran 0.0826 0.0906 0.0783 0.243 0.267 0.231 J, m
Air
TDD
Xavier
0224-196.SG-9.Can
X2401100.D
1.000
2.239
2024-03-01 09:35
TO15_SCNV6.M
0224-196; 500mL Load; Can#6052/C10126
2024-01-31 11:45
2024-02-29 00:00
Sample
Xavier_X022924A_0224-196.v1
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-9
EA # 0224-196 Page 4 of 25
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0224-196.SG-9.Can
X2401100.D
1.000
2.239
2024-03-01 09:35
TO15_SCNV6.M
0224-196; 500mL Load; Can#6052/C10126
2024-01-31 11:45
2024-02-29 00:00
Sample
Xavier_X022924A_0224-196.v1
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-9
1,1,1-Trichloroethane ND 0.0904 0.0783 ND 0.493 0.427
Cyclohexane 1.84 0.0918 0.0783 6.32 0.316 0.270
Carbon tetrachloride ND 0.0902 0.0783 ND 0.567 0.493
Benzene 2.20 0.0901 0.0783 7.02 0.288 0.250
2,2,4-trimethylpentane 0.808 0.0926 0.0783 3.77 0.432 0.366
1,2-Dichloroethane ND 0.0921 0.0783 ND 0.373 0.317
Heptane 2.03 0.0907 0.0783 8.31 0.371 0.321
Trichloroethene 0.0978 0.0905 0.0783 0.525 0.486 0.421
1,2-Dichloropropane ND 0.0902 0.0783 ND 0.416 0.362
Methyl methacrylate ND 0.0937 0.0783 ND 0.384 0.321
1,4-Dioxane ND 0.0898 0.0783 ND 0.323 0.282
Bromodichloromethane ND 0.0904 0.0783 ND 0.606 0.525
cis-1,3-Dichloropropene ND 0.0889 0.0783 ND 0.403 0.355
Methyl isobutyl ketone 0.224 0.0930 0.0783 0.917 0.381 0.321
Toluene 3.90 0.0912 0.0783 14.7 0.343 0.295
trans-1,3-Dichloropropene ND 0.0924 0.0783 ND 0.419 0.355
1,1,2-Trichloroethane ND 0.0911 0.0783 ND 0.497 0.427
Tetrachloroethene 7.03 0.0916 0.0783 47.6 0.621 0.531
2-Hexanone (Methyl butyl ketone)0.141 0.0916 0.0783 0.577 0.375 0.321
Dibromochloromethane ND 0.0903 0.0783 ND 0.768 0.667
1,2-Dibromoethane ND 0.0916 0.0783 ND 0.703 0.602
Chlorobenzene ND 0.0922 0.0783 ND 0.424 0.360
Ethylbenzene 0.435 0.0889 0.0783 1.89 0.386 0.340 m
1,1,1,2-Tetrachloroethane ND 0.0903 0.0783 ND 0.619 0.538
m-/p-Xylenes 1.17 0.0908 0.0783 5.10 0.394 0.340
o-Xylene 0.437 0.0897 0.0783 1.90 0.389 0.340
Styrene 0.136 0.0878 0.0783 0.577 0.374 0.334
Bromoform ND 0.0898 0.0783 ND 0.928 0.809
1,1,2,2-Tetrachloroethane ND 0.0905 0.0783 ND 0.621 0.538
4-Ethyltoluene 0.0848 0.0911 0.0783 0.417 0.447 0.385 J, m
2-Chlorotoluene ND 0.0903 0.0783 ND 0.467 0.405
EA # 0224-196 Page 5 of 25
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Air
TDD
Xavier
0224-196.SG-9.Can
X2401100.D
1.000
2.239
2024-03-01 09:35
TO15_SCNV6.M
0224-196; 500mL Load; Can#6052/C10126
2024-01-31 11:45
2024-02-29 00:00
Sample
Xavier_X022924A_0224-196.v1
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
SG-9
1,3,5-Trimethylbenzene 0.134 0.0908 0.0783 0.657 0.446 0.385
1,2,4-Trimethylbenzene 0.370 0.0896 0.0783 1.82 0.440 0.385
1,3-Dichlorobenzene ND 0.0910 0.0783 ND 0.547 0.471
1,4-Dichlorobenzene ND 0.0900 0.0783 ND 0.541 0.471
Benzyl chloride ND 0.0901 0.0783 ND 0.466 0.405
1,2-Dichlorobenzene ND 0.0907 0.0783 ND 0.545 0.471
1,2,4-Trichlorobenzene ND 0.0892 0.0783 ND 0.661 0.581
Hexachlorobutadiene ND 0.0885 0.0783 ND 0.943 0.835
Naphthalene ND 0.0902 0.0783 ND 0.472 0.410
1-Bromopropane 0.0845 0.0888 0.0783 0.425 0.447 0.394 J
1-Octene 1.20 0.0884 0.0783 5.49 0.405 0.359 m
n-Octane 1.06 0.0922 0.0783 4.96 0.431 0.366
Isopropylbenzene 0.119 0.0910 0.0783 0.587 0.447 0.385
n-Propylbenzene 0.0983 0.0919 0.0783 0.483 0.451 0.385
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)845,157 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,409,280 12.44 5.16 pass
Chlorobenzene-d5 (IS)2,883,541 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0224-196 Page 6 of 25
Job No.
Company
Site
Can Number 6052
Job 0124-075
Sample ID SG-9
CleanDate 01/18/2024
LeakCheckDate 01/23/2024
LeakCheckAnalyst pamooney
BlankCheckRef Y2400230
Weather Station ID 88
Weather Station Exp.02/02/2024
Transducer ID 3
Transducer Exp.11/17/2024
Can Size (L)1.4
Evac Temp (F)65.9
Evac Pbar (mmHg)761.0
Evac Gauge (mmHg)-761.0
Evac Analyst pamooney
Evac Time 01/25/24 10:23
Evac Vol (L)0.000
Recd. Temp (F)66.7
Recd. Pbar (mmHg)757.7
Recd. Gauge (mmHg)-115.0
Recd Vol (L)1.187
P1 Temp (F)66.7
P1 Pbar (mmHg)757.7
P1 Gauge (mmHg)681.0
P1 Analyst pamooney
P1 Time 02/01/24 13:12
P1 Fill Gas Nitrogen
P1 Vol (L)2.657
P1 DF Override false
P1 Dilution Factor 2.239
Enthalpy Analytical -- Canister Pressurization
0224-196
AECOM - Morrisville
Frye & Webster DC410064
Canister Pressurization Report 20230531 Report Printed 2/12/2024 12:41:56 PM
EA # 0224-196 Page 7 of 25

Lab QC
EA # 0224-196 Page 8 of 25
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Propylene ND 0.0386 0.0350 ND 0.0665 0.0602 pass
Freon 12 (CCl2F2)ND 0.0392 0.0350 ND 0.194 0.173 pass
Freon 114 (C2Cl2F4)ND 0.0401 0.0350 ND 0.280 0.245 pass
Chloromethane ND 0.0396 0.0350 ND 0.0816 0.0722 pass
Chloroethene (Vinyl chloride)ND 0.0400 0.0350 ND 0.102 0.0894 pass
1,3-Butadiene ND 0.0389 0.0350 ND 0.0860 0.0774 pass
Bromomethane ND 0.0392 0.0350 ND 0.152 0.136 pass
Chloroethane ND 0.0406 0.0350 ND 0.107 0.0923 pass
Bromoethene (Vinyl bromide)ND 0.0391 0.0350 ND 0.171 0.153 pass
Freon 11 (CCl3F)ND 0.0422 0.0350 ND 0.237 0.197 pass
Ethanol 0.0843 0.0396 0.0396 0.159 0.0746 0.0746 pass
Acrolein ND 0.0394 0.0350 ND 0.0903 0.0802 pass
Freon 113 (C2Cl3F3)ND 0.0406 0.0350 ND 0.311 0.268 pass
1,1-Dichloroethene ND 0.0402 0.0350 ND 0.159 0.139 pass
Acetone 0.0821 0.0401 0.0350 0.195 0.0951 0.0831 pass, m
Carbon disulfide ND 0.0399 0.0350 ND 0.124 0.109 pass
Isopropyl alcohol ND 0.0399 0.0350 ND 0.0980 0.0860 pass
Allyl chloride (3-chloropropene)ND 0.0432 0.0350 ND 0.135 0.109 pass
Acetonitrile ND 0.0399 0.0350 ND 0.0669 0.0587 pass
Methylene chloride ND 0.0410 0.0350 ND 0.142 0.122 pass
trans-1,2-Dichloroethene ND 0.0408 0.0350 ND 0.162 0.139 pass
Methyl tert-butyl ether ND 0.0411 0.0350 ND 0.148 0.126 pass
Acrylonitrile ND 0.0407 0.0350 ND 0.0883 0.0759 pass
Hexane ND 0.0406 0.0350 ND 0.143 0.123 pass
1,1-Dichloroethane ND 0.0397 0.0350 ND 0.161 0.142 pass
Vinyl acetate ND 0.0409 0.0350 ND 0.144 0.123 pass
cis-1,2-Dichloroethene ND 0.0404 0.0350 ND 0.160 0.139 pass
Methyl ethyl ketone (2-Butanone)ND 0.0414 0.0350 ND 0.122 0.103 pass
Ethyl acetate ND 0.0399 0.0350 ND 0.144 0.126 pass
Chloroform ND 0.0401 0.0350 ND 0.196 0.171 pass
Tetrahydrofuran ND 0.0405 0.0350 ND 0.119 0.103 pass
1,1,1-Trichloroethane ND 0.0404 0.0350 ND 0.220 0.191 pass
Cyclohexane ND 0.0410 0.0350 ND 0.141 0.120 pass
Xavier
X022924A_Humid Blank #1882
1.000
2024-02-29 21:08
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X022924A_0224-196.v1
X2401086.D
1.000
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X022924A_Humid Blank #1882
EA # 0224-196 Page 9 of 25
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X022924A_Humid Blank #1882
1.000
2024-02-29 21:08
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X022924A_0224-196.v1
X2401086.D
1.000
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X022924A_Humid Blank #1882
Carbon tetrachloride ND 0.0403 0.0350 ND 0.253 0.220 pass
Benzene ND 0.0402 0.0350 ND 0.128 0.112 pass
2,2,4-trimethylpentane ND 0.0414 0.0350 ND 0.193 0.163 pass
1,2-Dichloroethane ND 0.0412 0.0350 ND 0.166 0.142 pass
Heptane ND 0.0405 0.0350 ND 0.166 0.143 pass
Trichloroethene ND 0.0404 0.0350 ND 0.217 0.188 pass
1,2-Dichloropropane ND 0.0403 0.0350 ND 0.186 0.162 pass
Methyl methacrylate ND 0.0419 0.0350 ND 0.171 0.143 pass
1,4-Dioxane ND 0.0401 0.0350 ND 0.144 0.126 pass
Bromodichloromethane ND 0.0404 0.0350 ND 0.271 0.234 pass
cis-1,3-Dichloropropene ND 0.0397 0.0350 ND 0.180 0.159 pass
Methyl isobutyl ketone ND 0.0416 0.0350 ND 0.170 0.143 pass
Toluene ND 0.0407 0.0350 ND 0.153 0.132 pass
trans-1,3-Dichloropropene ND 0.0413 0.0350 ND 0.187 0.159 pass
1,1,2-Trichloroethane ND 0.0407 0.0350 ND 0.222 0.191 pass
Tetrachloroethene ND 0.0409 0.0350 ND 0.277 0.237 pass
2-Hexanone (Methyl butyl ketone)ND 0.0409 0.0350 ND 0.168 0.143 pass
Dibromochloromethane ND 0.0403 0.0350 ND 0.343 0.298 pass
1,2-Dibromoethane ND 0.0409 0.0350 ND 0.314 0.269 pass
Chlorobenzene ND 0.0412 0.0350 ND 0.190 0.161 pass
Ethylbenzene ND 0.0397 0.0350 ND 0.172 0.152 pass
1,1,1,2-Tetrachloroethane ND 0.0403 0.0350 ND 0.277 0.240 pass
m-/p-Xylenes ND 0.0406 0.0350 ND 0.176 0.152 pass
o-Xylene ND 0.0401 0.0350 ND 0.174 0.152 pass
Styrene ND 0.0392 0.0350 ND 0.167 0.149 pass
Bromoform ND 0.0401 0.0350 ND 0.414 0.362 pass
1,1,2,2-Tetrachloroethane ND 0.0404 0.0350 ND 0.277 0.240 pass
4-Ethyltoluene ND 0.0407 0.0350 ND 0.200 0.172 pass
2-Chlorotoluene ND 0.0404 0.0350 ND 0.209 0.181 pass
1,3,5-Trimethylbenzene ND 0.0406 0.0350 ND 0.199 0.172 pass
1,2,4-Trimethylbenzene ND 0.0400 0.0350 ND 0.197 0.172 pass
1,3-Dichlorobenzene ND 0.0406 0.0350 ND 0.244 0.210 pass
1,4-Dichlorobenzene ND 0.0402 0.0350 ND 0.242 0.210 pass
EA # 0224-196 Page 10 of 25
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Xavier
X022924A_Humid Blank #1882
1.000
2024-02-29 21:08
TO15_SCNV6.M
Air
TDD
500mL load
Blank
Xavier_X022924A_0224-196.v1
X2401086.D
1.000
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X022924A_Humid Blank #1882
Benzyl chloride ND 0.0402 0.0350 ND 0.208 0.181 pass
1,2-Dichlorobenzene ND 0.0405 0.0350 ND 0.243 0.210 pass
1,2,4-Trichlorobenzene ND 0.0398 0.0350 ND 0.295 0.260 pass
Hexachlorobutadiene ND 0.0395 0.0350 ND 0.421 0.373 pass
Naphthalene ND 0.0403 0.0350 ND 0.211 0.183 pass
1-Bromopropane ND 0.0397 0.0350 ND 0.199 0.176 pass
1-Octene ND 0.0395 0.0350 ND 0.181 0.161 pass
n-Octane ND 0.0412 0.0350 ND 0.192 0.163 pass
Isopropylbenzene ND 0.0406 0.0350 ND 0.200 0.172 pass
n-Propylbenzene ND 0.0410 0.0350 ND 0.202 0.172 pass
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)887,328 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,534,551 12.44 5.16 pass
Chlorobenzene-d5 (IS)3,025,656 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0224-196 Page 11 of 25
Flags
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass, m
pass
pass
pass, m
pass
pass
pass
pass
pass, m
pass
pass
pass
pass
pass
pass
pass
pass, m
pass
passCyclohexane1,362,352 6.11 5.12 119
1,1,1-Trichloroethane 1,631,204 5.07 5.05 100
Tetrahydrofuran 338,339 5.54 5.06 109
Chloroform 1,585,900 5.09 5.02 101
Ethyl acetate 309,320 4.86 4.99 97.4
Methyl ethyl ketone (2-Butanone)354,838 5.40 5.17 104
cis-1,2-Dichloroethene 1,392,678 5.83 5.05 115
Vinyl acetate 2,125,113 4.96 5.12 97.0
1,1-Dichloroethane 1,414,679 5.38 4.96 108
Hexane 1,254,934 5.72 5.08 113
Acrylonitrile 607,569 5.28 5.09 104
Methyl tert-butyl ether 1,959,529 5.36 5.14 104
trans-1,2-Dichloroethene 1,163,993 5.37 5.10 105
Methylene chloride 1,089,910 4.80 5.12 93.8
Acetonitrile 678,687 4.83 4.98 96.9
Allyl chloride (3-chloropropene)316,633 5.30 5.04 105
Isopropyl alcohol 1,399,109 4.47 4.98 89.7
Carbon disulfide 2,142,765 5.13 4.98 103
Acetone 1,206,978 3.95 5.01 78.9
1,1-Dichloroethene 1,292,944 4.87 5.03 96.8
Freon 113 (C2Cl3F3)1,471,380 4.95 5.08 97.5
Acrolein 265,744 4.55 4.92 92.3
Ethanol 317,253 3.82 4.96 77.2
Freon 11 (CCl3F)2,067,979 5.02 5.28 95.3
Bromoethene (Vinyl bromide)765,327 4.51 4.89 92.3
Chloroethane 373,168 5.29 5.08 104
Bromomethane 421,436 4.44 4.90 90.5
1,3-Butadiene 594,141 4.02 4.86 82.5
Chloroethene (Vinyl chloride)424,348 4.83 5.00 96.8
Chloromethane 793,328 5.33 4.94 108
Freon 114 (C2Cl2F4)2,070,646 4.85 5.01 96.7
Freon 12 (CCl2F2)1,910,287 4.62 4.90 94.4
Propylene 686,040 4.80 4.83 99.3
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Matrix Air
Enthalpy ID X022924A_5ppbv TO15 LCS
Pressurization Factor 1.000
Acquisition Date 2024-02-29 12:13
Instrument Method TO15_SCNV6.M
Batch Xavier_X022924A_0224-196.v1
Data File X2401077.D
Dilution 1.000
Sample Name X022924A_5ppbv TO15 LCS
Sample Info.125mL load; Can #2037; GCMSPrepPg1321
Sample Type QC
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
EA # 0224-196 Page 12 of 25
FlagsTarget Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Matrix Air
Enthalpy ID X022924A_5ppbv TO15 LCS
Pressurization Factor 1.000
Acquisition Date 2024-02-29 12:13
Instrument Method TO15_SCNV6.M
Batch Xavier_X022924A_0224-196.v1
Data File X2401077.D
Dilution 1.000
Sample Name X022924A_5ppbv TO15 LCS
Sample Info.125mL load; Can #2037; GCMSPrepPg1321
Sample Type QC
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass1,4-Dichlorobenzene 2,890,197 4.55 5.02 90.6
1,3-Dichlorobenzene 2,923,626 4.69 5.08 92.4
1,2,4-Trimethylbenzene 3,697,576 4.82 5.00 96.2
1,3,5-Trimethylbenzene 3,706,757 4.92 5.07 97.1
2-Chlorotoluene 3,742,885 5.00 5.04 99.0
4-Ethyltoluene 4,461,375 4.92 5.08 96.8
1,1,2,2-Tetrachloroethane 2,389,414 4.97 5.06 98.3
Bromoform 2,454,247 5.18 5.02 103
Styrene 2,383,111 4.81 4.90 98.1
o-Xylene 3,100,540 4.92 5.01 98.1
m-/p-Xylenes 3,078,505 5.09 5.07 100
1,1,1,2-Tetrachloroethane 1,429,799 4.50 5.04 89.4
Ethylbenzene 3,834,323 4.79 4.96 96.5
Chlorobenzene 2,606,639 4.84 5.15 94.1
1,2-Dibromoethane 1,796,049 4.73 5.12 92.4
Dibromochloromethane 2,152,758 4.75 5.04 94.3
2-Hexanone (Methyl butyl ketone)2,188,878 4.62 5.12 90.3
Tetrachloroethene 1,688,291 4.74 5.12 92.7
1,1,2-Trichloroethane 1,027,353 4.76 5.08 93.6
trans-1,3-Dichloropropene 1,310,009 4.70 5.16 91.0
Toluene 2,997,900 4.88 5.09 95.9
Methyl isobutyl ketone 2,303,661 4.65 5.20 89.5
cis-1,3-Dichloropropene 1,318,436 4.89 4.96 98.4
Bromodichloromethane 1,733,887 4.81 5.05 95.3
1,4-Dioxane 512,946 4.99 5.02 99.5
Methyl methacrylate 841,336 5.40 5.24 103
1,2-Dichloropropane 988,086 5.33 5.04 106
Trichloroethene 1,188,301 4.51 5.06 89.3
Heptane 829,437 5.31 5.06 105
1,2-Dichloroethane 1,084,643 4.54 5.14 88.2
2,2,4-trimethylpentane 4,319,610 5.51 5.17 107
Benzene 2,239,631 5.03 5.03 99.9
Carbon tetrachloride 1,864,894 5.16 5.04 103
EA # 0224-196 Page 13 of 25
FlagsTarget Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Matrix Air
Enthalpy ID X022924A_5ppbv TO15 LCS
Pressurization Factor 1.000
Acquisition Date 2024-02-29 12:13
Instrument Method TO15_SCNV6.M
Batch Xavier_X022924A_0224-196.v1
Data File X2401077.D
Dilution 1.000
Sample Name X022924A_5ppbv TO15 LCS
Sample Info.125mL load; Can #2037; GCMSPrepPg1321
Sample Type QC
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
Chlorobenzene-d5 (IS)3,076,119 16.57 4.92 pass
1,4-Difluorobenzene (IS)3,560,492 12.44 5.16 pass
Bromochloromethane (IS)897,573 11.02 5.21 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
n-Propylbenzene 5,400,304 5.25 5.13 102
Isopropylbenzene 4,413,221 4.82 5.08 94.8
n-Octane 827,685 4.96 5.02 99.0
1-Octene 658,722 5.24 4.94 106
1-Bromopropane 1,592,185 4.95 4.96 99.8
Naphthalene 5,297,744 4.46 5.04 88.6
Hexachlorobutadiene 2,329,481 5.16 4.94 104
1,2,4-Trichlorobenzene 2,545,202 4.91 4.98 98.5
1,2-Dichlorobenzene 2,865,510 4.78 5.06 94.3
Benzyl chloride 3,481,870 5.21 5.03 104
EA # 0224-196 Page 14 of 25
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
Propylene 706,256 4.83 4.83 4.80 100.0 0.7 pass
Freon 12 (CCl2F2)1,942,184 4.60 4.90 4.62 93.9 0.6 pass
Freon 114 (C2Cl2F4)2,111,283 4.83 5.01 4.85 96.5 0.3 pass
Chloromethane 819,337 5.39 4.94 5.33 109 1.0 pass
Chloroethene (Vinyl chloride)434,803 4.84 5.00 4.83 97.0 0.2 pass
1,3-Butadiene 616,116 4.07 4.86 4.02 83.7 1.4 pass
Bromomethane 437,055 4.50 4.90 4.44 91.8 1.4 pass
Chloroethane 381,094 5.29 5.08 5.29 104 0.1 pass
Bromoethene (Vinyl bromide)781,096 4.50 4.89 4.51 92.1 0.2 pass
Freon 11 (CCl3F)2,110,876 5.02 5.28 5.02 95.1 0.2 pass
Ethanol 331,869 3.91 4.96 3.82 78.9 2.3 pass
Acrolein 279,027 4.67 4.92 4.55 94.8 2.7 pass
Freon 113 (C2Cl3F3)1,506,711 4.96 5.08 4.95 97.7 0.1 pass
1,1-Dichloroethene 1,335,265 4.92 5.03 4.87 97.8 1.0 pass
Acetone 1,265,212 4.05 5.01 3.95 80.9 2.5 pass, m
Carbon disulfide 2,199,484 5.15 4.98 5.13 103 0.4 pass
Isopropyl alcohol 1,461,677 4.57 4.98 4.47 91.6 2.2 pass
Allyl chloride (3-chloropropene)340,984 5.58 5.04 5.30 111 5.2 pass
Acetonitrile 666,696 4.64 4.98 4.83 93.1 4.0 pass
Methylene chloride 1,120,748 4.83 5.12 4.80 94.4 0.6 pass
trans-1,2-Dichloroethene 1,198,203 5.41 5.10 5.37 106 0.7 pass
Methyl tert-butyl ether 2,045,978 5.47 5.14 5.36 106 2.1 pass
Acrylonitrile 630,604 5.36 5.09 5.28 105 1.5 pass, m
Hexane 1,298,794 5.79 5.08 5.72 114 1.2 pass
1,1-Dichloroethane 1,448,950 5.38 4.96 5.38 108 0.2 pass
Vinyl acetate 2,143,977 4.89 5.12 4.96 95.7 1.3 pass
cis-1,2-Dichloroethene 1,411,710 5.78 5.05 5.83 114 0.9 pass
Methyl ethyl ketone (2-Butanone)363,360 5.41 5.17 5.40 105 0.1 pass
Ethyl acetate 309,857 4.76 4.99 4.86 95.5 2.1 pass
Chloroform 1,631,392 5.12 5.02 5.09 102 0.6 pass
Tetrahydrofuran 338,945 5.42 5.06 5.54 107 2.0 pass
1,1,1-Trichloroethane 1,649,408 5.01 5.05 5.07 99.2 1.1 pass
Cyclohexane 1,404,328 6.16 5.12 6.11 120 0.8 pass
X022924A_5ppbv TO15 LCS LD
1.000
2024-02-29 13:01
TO15_SCNV6.M
Air
X022924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X022924A_0224-196.v1
X2401078.D
1.000
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X022924A_5ppbv TO15 LCS LD
EA # 0224-196 Page 15 of 25
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X022924A_5ppbv TO15 LCS LD
1.000
2024-02-29 13:01
TO15_SCNV6.M
Air
X022924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X022924A_0224-196.v1
X2401078.D
1.000
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X022924A_5ppbv TO15 LCS LD
Carbon tetrachloride 1,875,923 5.08 5.04 5.16 101 1.6 pass
Benzene 2,306,979 5.11 5.03 5.03 102 1.7 pass
2,2,4-trimethylpentane 4,394,641 5.54 5.17 5.51 107 0.4 pass
1,2-Dichloroethane 1,084,878 4.48 5.14 4.54 87.2 1.3 pass
Heptane 839,922 5.30 5.06 5.31 105 0.0 pass
Trichloroethene 1,198,104 4.49 5.06 4.51 88.9 0.5 pass
1,2-Dichloropropane 999,776 5.32 5.04 5.33 106 0.1 pass
Methyl methacrylate 855,210 5.42 5.24 5.40 104 0.4 pass
1,4-Dioxane 516,422 4.96 5.02 4.99 98.9 0.6 pass
Bromodichloromethane 1,737,796 4.76 5.05 4.81 94.3 1.0 pass
cis-1,3-Dichloropropene 1,327,066 4.86 4.96 4.89 97.8 0.6 pass
Methyl isobutyl ketone 2,318,677 4.62 5.20 4.65 88.9 0.6 pass
Toluene 3,045,861 4.87 5.09 4.88 95.6 0.3 pass
trans-1,3-Dichloropropene 1,317,699 4.63 5.16 4.70 89.8 1.3 pass
1,1,2-Trichloroethane 1,038,043 4.72 5.08 4.76 92.8 0.9 pass
Tetrachloroethene 1,709,246 4.71 5.12 4.74 92.0 0.7 pass
2-Hexanone (Methyl butyl ketone)2,196,835 4.55 5.12 4.62 88.9 1.6 pass
Dibromochloromethane 2,182,743 4.73 5.04 4.75 93.8 0.5 pass
1,2-Dibromoethane 1,799,242 4.64 5.12 4.73 90.8 1.7 pass
Chlorobenzene 2,633,689 4.80 5.15 4.84 93.2 0.9 pass
Ethylbenzene 3,907,164 4.79 4.96 4.79 96.4 0.0 pass
1,1,1,2-Tetrachloroethane 1,446,236 4.47 5.04 4.50 88.7 0.8 pass
m-/p-Xylenes 3,117,875 5.05 5.07 5.09 99.7 0.7 pass
o-Xylene 3,143,412 4.89 5.01 4.92 97.6 0.6 pass
Styrene 2,414,739 4.78 4.90 4.81 97.5 0.6 pass
Bromoform 2,462,323 5.10 5.02 5.18 102 1.6 pass
1,1,2,2-Tetrachloroethane 2,390,112 4.87 5.06 4.97 96.4 1.9 pass
4-Ethyltoluene 4,500,482 4.87 5.08 4.92 95.8 1.1 pass
2-Chlorotoluene 3,769,669 4.94 5.04 5.00 97.8 1.2 pass
1,3,5-Trimethylbenzene 3,721,107 4.85 5.07 4.92 95.6 1.5 pass
1,2,4-Trimethylbenzene 3,725,607 4.76 5.00 4.82 95.1 1.2 pass
1,3-Dichlorobenzene 2,966,527 4.67 5.08 4.69 92.0 0.5 pass
1,4-Dichlorobenzene 2,968,493 4.59 5.02 4.55 91.3 0.7 pass
EA # 0224-196 Page 16 of 25
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
X022924A_5ppbv TO15 LCS LD
1.000
2024-02-29 13:01
TO15_SCNV6.M
Air
X022924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X022924A_0224-196.v1
X2401078.D
1.000
Enthalpy Analytical
Job No.: 0224-196-1 EPA Method TO-15 Analysis -- Run
AECOM - Morrisville 60722767 Frye & Webster DC410064
X022924A_5ppbv TO15 LCS LD
Benzyl chloride 3,516,230 5.17 5.03 5.21 103 0.9 pass
1,2-Dichlorobenzene 2,879,125 4.71 5.06 4.78 92.9 1.5 pass
1,2,4-Trichlorobenzene 2,591,437 4.90 4.98 4.91 98.4 0.1 pass
Hexachlorobutadiene 2,373,292 5.16 4.94 5.16 104 0.1 pass
Naphthalene 5,381,360 4.45 5.04 4.46 88.3 0.4 pass
1-Bromopropane 1,628,789 4.95 4.96 4.95 99.8 0.0 pass
1-Octene 665,857 5.20 4.94 5.24 105 0.8 pass
n-Octane 854,491 5.03 5.02 4.96 100 1.3 pass
Isopropylbenzene 4,487,551 4.80 5.08 4.82 94.6 0.3 pass
n-Propylbenzene 5,400,913 5.15 5.13 5.25 100 1.9 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS)917,757 11.02 5.21 pass
1,4-Difluorobenzene (IS)3,606,174 12.44 5.16 pass
Chlorobenzene-d5 (IS)3,135,942 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
EA # 0224-196 Page 17 of 25

Narrative Summary

EA # 0224-196 Page 18 of 25

Enthalpy Analytical Narrative Summary

Company AECOM - Morrisville Client #Frye & Webster – DC410064
Client Project# 60722767
Analyst TDD Job #0224-196
Parameters EPA Method TO-15 # Samples 1 (1.4L) Canister

Custody David Myers received the sample on 2/1/2024 after being relinquished by
AECOM - Morrisville. The sample was then logged in by Alyssa Miller
the same day. The sample was received at ambient temperature and in
good condition. After pressurization, the sample was archived until
analysis was requested by AECOM – Morrisville on 2/29/24.
Prior to, during, and after analysis, the sample was kept under lock with
access only to authorized personnel by Enthalpy Analytical, LLC.
Analysis The sample was analyzed for the TO-15 target compound list using the
analytical procedures in EPA Method TO-15, Determination of Volatile
Organic Compounds (VOCs) In Air Collected In Specially-Prepared
Canister And Analyzed by Gas Chromatography/Mass Spectrometry
(GC/MS).
Upon receipt, the canister pressure were measured and recorded. The
canister was then pressurized with UHP nitrogen and a dilution ratio was
calculated. See the Canister Pressurization Data sheet located in the
Results section of this report.
The sample was analyzed undiluted.
The Agilent Technologies Model 6890N, Gas Chromatograph "Xavier"
(S/N US10721018) equipped with a 5975C VL Mass Selective Detector
(S/N US71215962) was used for this analysis. The sample and standards
were introduced directly to the analyzer using an Entech 7200
Preconcentrator.

Calibration The BFB tune analyses associated with the initial and continuing
calibrations met all method acceptance criteria.
The initial calibration (X100722A-TO15) met the 30% RSD criteria. The
initial calibration verification (ICV) met the 70-130% recovery criteria.
The continuing calibration (CCV) met the 30% difference criteria. Full
calibration data is available upon request.
Chromatographic
Conditions
The acquisition method (TO15_SCNV6.M) may be made available upon
request.
EA # 0224-196 Page 19 of 25

Enthalpy Analytical Narrative Summary
(continued)

QC Notes All internal standard area (IS) responses and retention time criteria were
met for this analysis.
The LCSs was analyzed as the Laboratory Duplicate (LD) and meet the
25% difference criteria for all reported compounds.
The laboratory humid blank associated with this analysis did not contain
any of the target analytes at a concentration greater than 3x their MDL.
The Laboratory Control Sample (LCS) met the 70-130% recovery criteria
for all reported compounds.
The sample was analyzed within the 30-day holding time required by the
method.
Reporting Notes The analysis met the requirements of the TNI Standard. Any deviations
from the requirements of the reference method or TNI Standard have been
stated above.
The results presented in this report are representative of the samples as
provided to the laboratory.

EA # 0224-196 Page 20 of 25

General Reporting Notes

The following are general reporting notes that are applicable to all Enthalpy Analytical, LLC data
reports, unless specifically noted otherwise.

 Any analysis which refers to the method as “Type” represents a planned deviation from the
reference method. For instance a Hydrogen Sulfide assay from a Tedlar bag would be labeled
as “EPA Method 16-Type” because Tedlar bags are not mentioned as one of the collection
options in EPA Method 16.
 The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory
cannot determine the presence of the analyte of interest reliably.
 The acronym LOQ represents the Limit of Quantification. Below this value the laboratory
cannot quantitate the analyte of interest within the criteria of the method.
 The acronym ND following a value indicates a non-detect or analytical result below the MDL.
 The letter J in the Qualifier or Flag column in the results indicates that the value is between
the MDL and the LOQ. The laboratory can positively identify the analyte of interest as
present, but the value should be considered an estimate.
 The letter E in the Qualifier or Flag column indicates an analytical result exceeding 100% of
the highest calibration point. The associated value should be considered as an estimate.
 Sample results are presented ‘as measured’ for single injection methodologies, or an average
value if multiple injections are made. If all injections are below the MDL, the sample is
considered non-detect and the ND value is presented. If one, but not all, are below the MDL,
the MDL value is used for any injections that are below the MDL. For example, if the MDL is
0.500 and LOQ is 1.00, and the instrument measures 0.355, 0.620, and 0.442 - the result
reported is the average of 0.500, 0.620, and 0.500 - - - i.e. 0.540 with a J flag.
 When a spike recovery (Bag Spike, Collocated Spike Train, or liquid matrix spike) is being
calculated, the native (unspiked) sample result is used in the calculations, as long as the value
is above the MDL. If a sample is ND, then 0 is used as the native amount (not the MDL
value).
 The acronym DF represents Dilution Factor. This number represents dilution of the sample
during the preparation and/or analysis process. The analytical result taken from a laboratory
instrument is multiplied by the DF to determine the final undiluted sample results.
 The addition of MS to the Sample ID represents a Matrix Spike. An aliquot of an actual
sample is spiked with a known amount of analyte so that a percent recovery value can be
determined. The MS analysis indicates what effect the sample matrix may have on the target
analyte, i.e. whether or not anything in the sample matrix interferes with the analysis of the
analyte(s).
EA # 0224-196 Page 21 of 25

General Reporting Notes
(continued)
 The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the
same manner as a MS, the use of duplicate matrix spikes allows further confirmation of
laboratory quality by showing the consistency of results gained by performing the same steps
multiple times.
 The addition of LD to the Sample ID represents a Laboratory Duplicate. The analyst prepares
an additional aliquot of sample for testing and the results of the duplicate analysis are
compared to the initial result. The result should have a difference value of within 10% of the
initial result (if the results of the original analysis are greater than the LOQ).
 The addition of AD to the Sample ID represents an Alternate Dilution. The analyst prepares an
additional aliquot at a different dilution factor (usually double the initial factor). This analysis
helps confirm that no additional compound is present and coeluting or sharing absorbance with
the analyte of interest, as they would have a different response/absorbance than the analyte of
interest.
 The Sample ID LCS represents a Laboratory Control Sample. Clean matrix, similar to the
client sample matrix, prepared and analyzed by the laboratory using the same reagents, spiking
standards and procedures used for the client samples. The LCS is used to assess the control of
the laboratory’s analytical system. Whenever spikes are prepared for our client projects, two
spikes are retained as LCSs. The LCSs are labeled with the associated project number and kept
in-house at the appropriate temperature conditions. When the project samples are received for
analysis, the LCSs are analyzed to confirm that the analyte could be recovered from the media,
separate from the samples which were used on the project and which may have been affected
by source matrix, sample collection, and/or sample transport.
 Significant Figures: Where the reported value is much greater than unity (1.00) in the units
expressed, the number is rounded to a whole number of units, rather than to 3 significant
figures. For example, a value of 10,456.45 ug catch is rounded to 10,456 ug. There are five
significant digits displayed, but no confidence should be placed on more than two significant
digits. In the case of small numbers, generally 3 significant figures are presented, but still only
2 should be used with confidence. Many neat materials are only certified to 3 digits, and as the
mathematically correct final result is always 1 digit less than all its pre-cursors - 2 significant
figures are what are most defensible.
 Manual Integration: The data systems used for processing will flag manually integrated
peaks with an “M”. There are several reasons a peak may be manually integrated. These
reasons will be identified by the following two letter designations on sample chromatograms,
if provided in the report. The peak was not integrated by the software “NI”, the peak was
integrated incorrectly by the software “II” or the wrong peak was integrated by the software
“WP”. These codes will accompany the analyst’s manual integration stamp placed next to the
compound name on the chromatogram.
EA # 0224-196 Page 22 of 25

Sample Custody
EA # 0224-196 Page 23 of 25
EA # 0224-196 Page 24 of 25

This Is The Last Page
Of This Report.

EA # 0224-196 Page 25 of 25
AECOM - Morrisville
1600 Perimeter Park Drive, Suite 400
Morrisville, NC 27560

Frye & Webster
Client Project# 60722767

Analytical Report
(0324-073)

EPA Method TO-15
TO15 Client Specified Compound List

Enthalpy Analytical, LLC
Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com
800-1 Capitola Drive Durham, NC 27713-4385

I certify that to the best of my knowledge all analytical data presented in this report:
 Have been checked for completeness
 Are accurate, error-free, and legible
 Have been conducted in accordance with approved protocol, and that all deviations and
analytical problems are summarized in the appropriate narrative(s)
This analytical report was prepared in Portable Document Format (.PDF). This report shall not be
reproduced except in full without approval of the laboratory. This will provide assurance that parts of a
report are not taken out of context.

Report Issued: 4/3/24
EA # 0324-073 Page 2 of 17

Results
EA # 0324-073 Page 3 of 17
Sample Name
Sample Info.
Sampling Date
Received Date
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Chloroethene (Vinyl chloride) ND 0.0474 0.0415 ND 0.121 0.106
1,1-Dichloroethene ND 0.0477 0.0415 ND 0.189 0.164
trans-1,2-Dichloroethene ND 0.0484 0.0415 ND 0.192 0.164
Methyl tert-butyl ether ND 0.0487 0.0415 ND 0.176 0.149
cis-1,2-Dichloroethene ND 0.0479 0.0415 ND 0.190 0.164
Chloroform 0.0789 0.0476 0.0415 0.385 0.232 0.202
Benzene 0.372 0.0477 0.0415 1.19 0.152 0.132
1,2-Dichloroethane ND 0.0488 0.0415 ND 0.197 0.168
Trichloroethene ND 0.0479 0.0415 ND 0.257 0.223
1,2-Dichloropropane ND 0.0477 0.0415 ND 0.220 0.192
1,1,2-Trichloroethane ND 0.0482 0.0415 ND 0.263 0.226
Tetrachloroethene 0.272 0.0485 0.0415 1.84 0.329 0.281
Ethylbenzene 0.0908 0.0471 0.0415 0.394 0.204 0.180
m-/p-Xylenes 0.275 0.0481 0.0415 1.19 0.209 0.180
o-Xylene 0.145 0.0475 0.0415 0.631 0.206 0.180
1,1,2,2-Tetrachloroethane ND 0.0479 0.0415 ND 0.329 0.285
1,3,5-Trimethylbenzene ND 0.0481 0.0415 ND 0.236 0.204
1,2,4-Trimethylbenzene 0.102 0.0475 0.0415 0.500 0.233 0.204
Naphthalene ND 0.0477 0.0415 ND 0.250 0.217
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS) 876,745 11.02 5.21 pass
1,4-Difluorobenzene (IS) 3,463,104 12.44 5.16 pass
Chlorobenzene-d5 (IS) 2,917,747 16.57 4.92 pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
Air
KMB
Xavier
0324-073.IA-1.Can
X2401347.D
0.667
1.777
2024-03-20 02:23
TO15_SCNV6.M
0324-073; *0.667=750mL load; Can #C78149
2024-03-15 08:40
2024-03-19 00:00
Sample
Xavier_X031924A_AECOM.v1
Enthalpy Analytical
Job No.: 0324-073-1 EPA Method TO-15 Analysis -- Runs
AECOM - Morrisville 60722767 Frye & Webster
IA-1
EA # 0324-073 Page 4 of 17
Job No.
Company
Site
Can Number C78149
Job 0324-073
Sample ID IA-1
CleanDate 12/07/2023
LeakCheckDate 12/07/2023
LeakCheckAnalyst pamooney
BlankCheckRef T2302284
Weather Station ID 97
Weather Station Exp.08/24/2025
Transducer ID 3
Transducer Exp.11/17/2024
Can Size (L)6
Evac Temp (F)69.3
Evac Pbar (mmHg)757.9
Evac Gauge (mmHg)-757.9
Evac Analyst pamooney
Evac Time 03/14/24 09:37
Evac Vol (L)0.000
Recd. Temp (F)69.8
Recd. Pbar (mmHg)753.6
Recd. Gauge (mmHg)-204.0
Recd Vol (L)4.324
P1 Temp (F)69.8
P1 Pbar (mmHg)753.6
P1 Gauge (mmHg)223.0
P1 Analyst erwright
P1 Time 03/19/24 15:57
P1 Fill Gas Nitrogen
P1 Vol (L)7.684
P1 DF Override false
P1 Dilution Factor 1.777
Enthalpy Analytical -- Canister Pressurization
0324-073
AECOM - Morrisville
Frye & Webster
Canister Pressurization Report ver. 20240301 Report Printed 3/20/2024 8:52:02 AM
EA # 0324-073 Page 5 of 17

Lab QC
EA # 0324-073 Page 6 of 17
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Analyst
Instrument
Enthalpy ID
Target Compound Concentration
(ppbv)
RL
(ppbv)
MDL
(ppbv)
Concentration
(ug/m³)
RL
(ug/m³)
MDL
(ug/m³)
Flags
Chloroethene (Vinyl chloride) ND 0.0400 0.0350 ND 0.102 0.0894 pass
1,1-Dichloroethene ND 0.0402 0.0350 ND 0.159 0.139 pass
trans-1,2-Dichloroethene ND 0.0408 0.0350 ND 0.162 0.139 pass
Methyl tert-butyl ether ND 0.0411 0.0350 ND 0.148 0.126 pass
cis-1,2-Dichloroethene ND 0.0404 0.0350 ND 0.160 0.139 pass
Chloroform ND 0.0401 0.0350 ND 0.196 0.171 pass
Benzene ND 0.0402 0.0350 ND 0.128 0.112 pass
1,2-Dichloroethane ND 0.0412 0.0350 ND 0.166 0.142 pass
Trichloroethene ND 0.0404 0.0350 ND 0.217 0.188 pass
1,2-Dichloropropane ND 0.0403 0.0350 ND 0.186 0.162 pass
1,1,2-Trichloroethane ND 0.0407 0.0350 ND 0.222 0.191 pass
Tetrachloroethene ND 0.0409 0.0350 ND 0.277 0.237 pass
Ethylbenzene ND 0.0397 0.0350 ND 0.172 0.152 pass
m-/p-Xylenes ND 0.0406 0.0350 ND 0.176 0.152 pass
o-Xylene ND 0.0401 0.0350 ND 0.174 0.152 pass
1,1,2,2-Tetrachloroethane ND 0.0404 0.0350 ND 0.277 0.240 pass
1,3,5-Trimethylbenzene ND 0.0406 0.0350 ND 0.199 0.172 pass
1,2,4-Trimethylbenzene ND 0.0400 0.0350 ND 0.197 0.172 pass
Naphthalene ND 0.0403 0.0350 ND 0.211 0.183 pass
Compound Response Retention
Time (min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS) 826,484 11.02 5.21 pass
1,4-Difluorobenzene (IS) 3,238,912 12.44 5.16 pass
Chlorobenzene-d5 (IS) 2,804,920 16.57 4.92 pass
Xavier
X031924A_Humid Blank #1861
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
1.000
2024-03-19 12:34
TO15_SCNV6.M
Air
KMB
500mL load
Blank
Xavier_X031924A_AECOM.v1
X2401332.D
1.000
Enthalpy Analytical
Job No.: 0324-073-1 EPA Method TO-15 Analysis -- Runs
AECOM - Morrisville 60722767 Frye & Webster
X031924A_Humid Blank #1861
EA # 0324-073 Page 7 of 17
Flags
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
pass
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
Chlorobenzene-d5 (IS) 2,774,911 16.57 4.92 pass
1,4-Difluorobenzene (IS) 3,260,766 12.44 5.16 pass
Bromochloromethane (IS) 842,104 11.02 5.21 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Naphthalene 4,826,511 4.51 5.04 89.5
1,2,4-Trimethylbenzene 3,551,389 5.13 5.00 102
1,3,5-Trimethylbenzene 3,559,730 5.24 5.07 103
1,1,2,2-Tetrachloroethane 2,125,256 4.90 5.06 96.9
o-Xylene 2,909,526 5.11 5.01 102
m-/p-Xylenes 2,946,780 5.40 5.07 106
Ethylbenzene 3,532,592 4.89 4.96 98.5
Tetrachloroethene 1,586,414 4.94 5.12 96.5
1,1,2-Trichloroethane 957,467 4.92 5.08 96.7
1,2-Dichloropropane 837,552 4.93 5.04 97.9
Trichloroethene 1,122,159 4.65 5.06 92.1
1,2-Dichloroethane 1,236,038 5.65 5.14 110
Benzene 2,090,743 5.12 5.03 102
Chloroform 1,669,568 5.71 5.02 114
cis-1,2-Dichloroethene 1,289,464 5.75 5.05 114
Methyl tert-butyl ether 2,013,100 5.87 5.14 114
trans-1,2-Dichloroethene 1,111,332 5.47 5.10 107
1,1-Dichloroethene 1,294,179 5.20 5.03 103
Chloroethene (Vinyl chloride) 365,888 4.44 5.00 88.9
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Recovery
(%)
Matrix Air
Enthalpy ID X031924A_5ppbv TO15 LCS
Pressurization Factor 1.000
Acquisition Date 2024-03-19 09:57
Instrument Method TO15_SCNV6.M
Batch Xavier_X031924A_AECOM.v1
Data File X2401329.D
Dilution 1.000
Sample Name X031924A_5ppbv TO15 LCS
Sample Info. 125mL load; Can #2037; GCMSPrepPg1321
Sample Type QC
Enthalpy Analytical
Job No.: 0324-073-1 EPA Method TO-15 Analysis -- Runs
AECOM - Morrisville 60722767 Frye & Webster
EA # 0324-073 Page 8 of 17
Sample Name
Sample Info.
Sample Type
Batch
Data File
Dilution
Pressurization Factor
Acquisition Date
Instrument Method
Matrix
Parent
Enthalpy ID
Target Compound Response Concentration
(ppbv)
Expected
Conc (ppbv)
Parent
Conc (ppbv)
Recovery
(%)
Diff
(%)
Flags
Chloroethene (Vinyl chloride) 369,275 4.51 5.00 4.44 90.2 1.5 pass
1,1-Dichloroethene 1,291,529 5.21 5.03 5.20 104 0.3 pass
trans-1,2-Dichloroethene 1,109,983 5.49 5.10 5.47 108 0.4 pass
Methyl tert-butyl ether 2,012,277 5.90 5.14 5.87 115 0.5 pass
cis-1,2-Dichloroethene 1,288,876 5.78 5.05 5.75 115 0.5 pass
Chloroform 1,660,800 5.71 5.02 5.71 114 0.0 pass
Benzene 2,094,182 5.07 5.03 5.12 101 1.0 pass
1,2-Dichloroethane 1,249,852 5.65 5.14 5.65 110 0.1 pass
Trichloroethene 1,119,365 4.59 5.06 4.65 90.8 1.4 pass
1,2-Dichloropropane 843,273 4.91 5.04 4.93 97.4 0.5 pass
1,1,2-Trichloroethane 941,582 4.77 5.08 4.92 93.8 3.1 pass
Tetrachloroethene 1,598,579 4.90 5.12 4.94 95.9 0.7 pass
Ethylbenzene 3,513,258 4.80 4.96 4.89 96.6 2.0 pass
m-/p-Xylenes 2,941,521 5.31 5.07 5.40 105 1.6 pass
o-Xylene 2,915,319 5.05 5.01 5.11 101 1.2 pass
1,1,2,2-Tetrachloroethane 2,149,007 4.88 5.06 4.90 96.6 0.3 pass
1,3,5-Trimethylbenzene 3,551,548 5.16 5.07 5.24 102 1.7 pass
1,2,4-Trimethylbenzene 3,563,201 5.07 5.00 5.13 101 1.1 pass
Naphthalene 4,959,138 4.56 5.04 4.51 90.6 1.3 pass
Compound Response Retention Time
(min)
Concentration
(ppbv)
Flag
Bromochloromethane (IS) 837,455 11.02 5.21 pass
1,4-Difluorobenzene (IS) 3,299,519 12.44 5.16 pass
Chlorobenzene-d5 (IS) 2,815,055 16.57 4.92 pass
X031924A_5ppbv TO15 LCS LD
(ND) = Not Detected
(J) = Below Calibration Range, (E) = Above Calibration Range, (m) = Manual Integration
IS Acceptance Criteria: RT +/- 20 sec, Response +/- 40%
1.000
2024-03-19 10:45
TO15_SCNV6.M
Air
X031924A_5ppbv TO15 LCS
125mL load; Can #2037; GCMSPrepPg1321
QcDup
Xavier_X031924A_AECOM.v1
X2401330.D
1.000
Enthalpy Analytical
Job No.: 0324-073-1 EPA Method TO-15 Analysis -- Runs
AECOM - Morrisville 60722767 Frye & Webster
X031924A_5ppbv TO15 LCS LD
EA # 0324-073 Page 9 of 17

Narrative Summary

EA # 0324-073 Page 10 of 17

Enthalpy Analytical Narrative Summary

Company AECOM - Morrisville Client #Frye & Webster –
Client Project# 60722767
Analyst KMB Job #0324-073
Parameters EPA Method TO-15 # Sample 1 (6L) Canister

Custody Barry Johnson received the sample on 3/19/24 after being relinquished
by AECOM - Morrisville. The sample was then transported to Enthalpy’s
Durham location where it was logged in by Alyssa Miller. The sample
was received at ambient temperature and in good condition.
Prior to, during, and after analysis, the sample was kept under lock with
access only to authorized personnel by Enthalpy Analytical, LLC.
Analysis The sample was analyzed for a client specified target compound list using
the analytical procedures in EPA Method TO-15, Determination of
Volatile Organic Compounds (VOCs) In Air Collected In Specially-
Prepared Canister And Analyzed by Gas Chromatography/Mass
Spectrometry (GC/MS).
Upon receipt, the canister pressure was measured and recorded. The
canister was then pressurized with UHP nitrogen and a dilution ratio was
calculated for each canister. See the Canister Pressurization Data sheet
located in the Results section of this report.
The sample was analyzed undiluted.
The Agilent Technologies Model 6890N, Gas Chromatograph "Xavier"
(S/N US10721018) equipped with a 5975C VL Mass Selective Detector
(S/N US71215962) was used for this analysis. The sample and standards
were introduced directly to the analyzer using an Entech 7200
Preconcentrator.
Calibration The BFB tune analyses associated with the initial and continuing
calibrations met all method acceptance criteria.
The initial calibration (X100722A-TO15) met the 30% RSD criteria. The
initial calibration verification (ICV) met the 70-130% recovery criteria.
The continuing calibration (CCV) met the 30% difference criteria. Full
calibration data is available upon request.
Chromatographic
Conditions
The acquisition method (TO15_SCNV6.M) may be made available upon
request.
EA # 0324-073 Page 11 of 17

Enthalpy Analytical Narrative Summary
(continued)

QC Notes All internal standard area (IS) responses and retention time criteria were
met for this analysis.
The LCS was analyzed as the laboratory duplicate (LD) and met the 25%
difference criteria for all reported compounds.
The laboratory humid blank associated with this analysis did not contain
any of the target analytes at a concentration greater than 3x their MDL.
The Laboratory Control Sample (LCS) met the 70-130% recovery criteria
for all reported compounds.
The sample was analyzed within the 30-day holding time required by the
method.
Reporting Notes The analysis met the requirements of the TNI Standard. Any deviations
from the requirements of the reference method or TNI Standard have been
stated above.
The results presented in this report are representative of the sample as
provided to the laboratory.

EA # 0324-073 Page 12 of 17

General Reporting Notes

The following are general reporting notes that are applicable to all Enthalpy Analytical, LLC data
reports, unless specifically noted otherwise.

 Any analysis which refers to the method as “Type” represents a planned deviation from the
reference method. For instance a Hydrogen Sulfide assay from a Tedlar bag would be labeled
as “EPA Method 16-Type” because Tedlar bags are not mentioned as one of the collection
options in EPA Method 16.
 The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory
cannot determine the presence of the analyte of interest reliably.
 The acronym LOQ represents the Limit of Quantification. Below this value the laboratory
cannot quantitate the analyte of interest within the criteria of the method.
 The acronym ND following a value indicates a non-detect or analytical result below the MDL.
 The letter J in the Qualifier or Flag column in the results indicates that the value is between
the MDL and the LOQ. The laboratory can positively identify the analyte of interest as
present, but the value should be considered an estimate.
 The letter E in the Qualifier or Flag column indicates an analytical result exceeding 100% of
the highest calibration point. The associated value should be considered as an estimate.
 Sample results are presented ‘as measured’ for single injection methodologies, or an average
value if multiple injections are made. If all injections are below the MDL, the sample is
considered non-detect and the ND value is presented. If one, but not all, are below the MDL,
the MDL value is used for any injections that are below the MDL. For example, if the MDL is
0.500 and LOQ is 1.00, and the instrument measures 0.355, 0.620, and 0.442 - the result
reported is the average of 0.500, 0.620, and 0.500 - - - i.e. 0.540 with a J flag.
 When a spike recovery (Bag Spike, Collocated Spike Train, or liquid matrix spike) is being
calculated, the native (unspiked) sample result is used in the calculations, as long as the value
is above the MDL. If a sample is ND, then 0 is used as the native amount (not the MDL
value).
 The acronym DF represents Dilution Factor. This number represents dilution of the sample
during the preparation and/or analysis process. The analytical result taken from a laboratory
instrument is multiplied by the DF to determine the final undiluted sample results.
 The addition of MS to the Sample ID represents a Matrix Spike. An aliquot of an actual
sample is spiked with a known amount of analyte so that a percent recovery value can be
determined. The MS analysis indicates what effect the sample matrix may have on the target
analyte, i.e. whether or not anything in the sample matrix interferes with the analysis of the
analyte(s).
EA # 0324-073 Page 13 of 17

General Reporting Notes
(continued)
 The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the
same manner as a MS, the use of duplicate matrix spikes allows further confirmation of
laboratory quality by showing the consistency of results gained by performing the same steps
multiple times.
 The addition of LD to the Sample ID represents a Laboratory Duplicate. The analyst prepares
an additional aliquot of sample for testing and the results of the duplicate analysis are
compared to the initial result. The result should have a difference value of within 10% of the
initial result (if the results of the original analysis are greater than the LOQ).
 The addition of AD to the Sample ID represents an Alternate Dilution. The analyst prepares an
additional aliquot at a different dilution factor (usually double the initial factor). This analysis
helps confirm that no additional compound is present and coeluting or sharing absorbance with
the analyte of interest, as they would have a different response/absorbance than the analyte of
interest.
 The Sample ID LCS represents a Laboratory Control Sample. Clean matrix, similar to the
client sample matrix, prepared and analyzed by the laboratory using the same reagents, spiking
standards and procedures used for the client samples. The LCS is used to assess the control of
the laboratory’s analytical system. Whenever spikes are prepared for our client projects, two
spikes are retained as LCSs. The LCSs are labeled with the associated project number and kept
in-house at the appropriate temperature conditions. When the project samples are received for
analysis, the LCSs are analyzed to confirm that the analyte could be recovered from the media,
separate from the samples which were used on the project and which may have been affected
by source matrix, sample collection, and/or sample transport.
 Significant Figures: Where the reported value is much greater than unity (1.00) in the units
expressed, the number is rounded to a whole number of units, rather than to 3 significant
figures. For example, a value of 10,456.45 ug catch is rounded to 10,456 ug. There are five
significant digits displayed, but no confidence should be placed on more than two significant
digits. In the case of small numbers, generally 3 significant figures are presented, but still only
2 should be used with confidence. Many neat materials are only certified to 3 digits, and as the
mathematically correct final result is always 1 digit less than all its pre-cursors - 2 significant
figures are what are most defensible.
 Manual Integration: The data systems used for processing will flag manually integrated
peaks with an “M”. There are several reasons a peak may be manually integrated. These
reasons will be identified by the following two letter designations on sample chromatograms,
if provided in the report. The peak was not integrated by the software “NI”, the peak was
integrated incorrectly by the software “II” or the wrong peak was integrated by the software
“WP”. These codes will accompany the analyst’s manual integration stamp placed next to the
compound name on the chromatogram.
EA # 0324-073 Page 14 of 17

Sample Custody
EA # 0324-073 Page 15 of 17
EA # 0324-073 Page 16 of 17

This Is The Last Page
Of This Report.

EA # 0324-073 Page 17 of 17
Appendix D
Monitoring Well Construction Logs
asphalt/fill material
Red-orange stiff silty CLAY, some saprolite near 10 feet
Red-orange stiff silty CLAY, no saprolite, no odor
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
0
2" PVC Riser
Concrete Pad
Cap
Grout
Bentonite Seal
816
814
812
810
808
806
804
802
800
798
796
794
792
CL
0.010" Slotted
Screen
Filter Pack
608 Elwell Avenue
David Hall
Geologic Exploration, Inc.
GeoProbe
HSA
60722767
MW-1
850908.5 1780373
20
1/30/2024 1/31/20248E. Mayle
816.48
10.99
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description Well Construction
DEPTH TO WATER:
El
e
v
a
t
i
o
n

(
f
t

M
S
L
)
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767MW-1
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
ATT. A
Well Installation LogNOTES:
Gravel
Red-yellow very stiff silty CLAY, low-no plasticity, no odor,
with saprolite below 5 feet
Red-yellow very stiff silty CLAY with slight chlorine odor, moist
Red-yellow very stiff silty CLAY with slight chlorine odor, wet
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
0
2" PVC Riser
Concrete Pad
Cap
Grout
Bentonite Seal
818
816
814
812
810
808
806
804
802
800
798
796
794
CL
0.010" Slotted
Screen
Filter Pack
608 Elwell Avenue
David Hall
Geologic Exploration, Inc.
GeoProbe
HSA
60722767
MW-2
850795 1780394.3
20
1/30/2024 1/31/20248E. Mayle
817.606
11.2
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description Well Construction
DEPTH TO WATER:
El
e
v
a
t
i
o
n

(
f
t

M
S
L
)
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767MW-2
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
ATT. A
Well Installation LogNOTES:
Gravel
Red-yellow stiff silty CLAY, low plasticity, no odor
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
0
2" PVC Riser
Concrete Pad
Cap
Grout
Bentonite Seal
820
818
816
814
812
810
808
806
804
802
800
798
796
CL
0.010" Slotted
Screen
Filter Pack
608 Elwell Avenue
David Hall
Geologic Exploration, Inc.
GeoProbe
HSA
60722767
MW-3
850801.2 1780510.9
20
1/30/2024 1/31/20248E. Mayle
820.119
13.42
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description Well Construction
DEPTH TO WATER:
El
e
v
a
t
i
o
n

(
f
t

M
S
L
)
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767MW-3
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
ATT. A
Well Installation LogNOTES:
Black organic silt, no odor
Red-brown silty CLAY, no odor
Red-brown silty CLAY with black rocky material, slight odor
26
25
24
23
22
21
20
19
18
17
16
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
0
2" PVC Riser
Concrete Pad
Cap
Grout
Bentonite Seal
820
818
816
814
812
810
808
806
804
802
800
798
796
CL
0.010" Slotted
Screen
Filter Pack
608 Elwell Avenue
David Hall
Geologic Exploration, Inc.
GeoProbe
HSA
60722767
MW-4
850924.6 1780511
20
1/30/2024 1/31/20248E. Mayle
820.036
14.35
Frye & Webster Cleaners DC410064
PROJECT NAME:
LOCATION:
DRILLING CONTRACTOR:
DRILLING METHOD:
DRILLING EQUIPMENT:
PROJECT NO.:
NORTHING: EASTING:
DRILLER:
TOTAL DEPTH:
WELL/BORING ID:
TOC ELEVATION:
LOGGED BY:BORE HOLE DIAMETER:DATE STARTED:DATE COMPLETED:
De
p
t
h

(
f
e
e
t
)
Description Well Construction
DEPTH TO WATER:
El
e
v
a
t
i
o
n

(
f
t

M
S
L
)
Greensboro, NC
CITY, STATE:
ProfileUSCS
EMM
SDH
60722767MW-4
Frye & Webster Cleaners DC410064
608 Elwell Avenue
Greensboro, NC
PROJECT NO.:
DRAWN BY:
CHECKED BY:
SHEET ID:
ATT. A
Well Installation LogNOTES:
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 6-6-2018
1.Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2.Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3.Well Use (check well use):
Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation □Wells > 100,000 GPDNon-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient)
N W
6.Is(are) the well(s): □Permanent or □Temporary
7.Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wellsdrilled:
9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below top of casing: (ft.) If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
22.Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well construction info (add 'See Over' in Remarks Box). You may also attach additional pages if necessary.
24.SUBMITTAL INSTRUCTIONS
Submit this GW-1 within 30 days of well completion per the following:
24a. For All Wells: Original form to Division of Water Resources (DWR), Information Processing Unit, 1617 MSC, Raleigh, NC 27699-1617
24b. For Injection Wells: Copy to DWR, Underground Injection Control (IUC) Program, 1636 MSC, Raleigh, NC 27699-1636
24c. For Water Supply and Open-Loop Geothermal Return Wells: Copy to the county environmental health department of the county where installed
24d. For Water Wells producing over 100,000 GPD: Copy to DWR, CCPCUA Permit Program, 1611 MSC, Raleigh, NC 27699-1611
DAVID HALL
A - 4459
GEOLOGIC EXPLORATION

0.0 5.0 SCH 40
5.0 20.0 .010
l
0.0 PORTLAND BENTONITE
4.0 20-40
0.0 ASPHALT/GRAVEL/SILTY CLAY 01/29/24 MW-1
FRYE & WEBSTER CLEANERS
608 ELWELL AVENUE GREENSBORO 27405
GUILFORD BENTONITE SEAL ~ 3.0 - 4.0 FEET
36° 05' 08.26" 79° 44' 34.86"02/06/24
l
20.0
10.0
8.0
AUGER
PVC
SCH 40 PVC
2.0

2.0
3.0
20.0
20.0

FINE SILICA SAND
SLURRY
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 6-6-2018
1.Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2.Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3.Well Use (check well use):
Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation □Wells > 100,000 GPDNon-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient)
N W
6.Is(are) the well(s): □Permanent or □Temporary
7.Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wellsdrilled:
9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below top of casing: (ft.) If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
22.Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well construction info (add 'See Over' in Remarks Box). You may also attach additional pages if necessary.
24.SUBMITTAL INSTRUCTIONS
Submit this GW-1 within 30 days of well completion per the following:
24a. For All Wells: Original form to Division of Water Resources (DWR), Information Processing Unit, 1617 MSC, Raleigh, NC 27699-1617
24b. For Injection Wells: Copy to DWR, Underground Injection Control (IUC) Program, 1636 MSC, Raleigh, NC 27699-1636
24c. For Water Supply and Open-Loop Geothermal Return Wells: Copy to the county environmental health department of the county where installed
24d. For Water Wells producing over 100,000 GPD: Copy to DWR, CCPCUA Permit Program, 1611 MSC, Raleigh, NC 27699-1611
DAVID HALL
A - 4459
GEOLOGIC EXPLORATION

0.0 5.0 SCH 40
5.0 20.0 .010
l
0.0 PORTLAND BENTONITE
4.0 20-40
0.0 GRAVEL/SILTY CLAY 01/29/24 MW-2
FRYE & WEBSTER CLEANERS
608 ELWELL AVENUE GREENSBORO 27405
GUILFORD BENTONITE SEAL ~ 3.0 - 4.0 FEET
36° 05' 08.26" 79° 44' 34.86"02/06/24
l
20.0
10.0
8.0
AUGER
PVC
SCH 40 PVC
2.0

2.0
3.0
20.0
20.0

FINE SILICA SAND
SLURRY
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 6-6-2018
1.Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2.Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3.Well Use (check well use):
Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation □Wells > 100,000 GPDNon-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient)
N W
6.Is(are) the well(s): □Permanent or □Temporary
7.Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wellsdrilled:
9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below top of casing: (ft.) If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
22.Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well construction info (add 'See Over' in Remarks Box). You may also attach additional pages if necessary.
24.SUBMITTAL INSTRUCTIONS
Submit this GW-1 within 30 days of well completion per the following:
24a. For All Wells: Original form to Division of Water Resources (DWR), Information Processing Unit, 1617 MSC, Raleigh, NC 27699-1617
24b. For Injection Wells: Copy to DWR, Underground Injection Control (IUC) Program, 1636 MSC, Raleigh, NC 27699-1636
24c. For Water Supply and Open-Loop Geothermal Return Wells: Copy to the county environmental health department of the county where installed
24d. For Water Wells producing over 100,000 GPD: Copy to DWR, CCPCUA Permit Program, 1611 MSC, Raleigh, NC 27699-1611
DAVID HALL
A - 4459
GEOLOGIC EXPLORATION

0.0 5.0 SCH 40
5.0 20.0 .010
l
0.0 PORTLAND BENTONITE
4.0 20-40
0.0 GRAVEL/SILTY CLAY 01/29/24 MW-3
FRYE & WEBSTER CLEANERS
608 ELWELL AVENUE GREENSBORO 27405
GUILFORD BENTONITE SEAL ~ 3.0 - 4.0 FEET
36° 05' 08.26" 79° 44' 34.86"02/06/24
l
20.0
10.0
8.0
AUGER
PVC
SCH 40 PVC
2.0

2.0
3.0
20.0
20.0

FINE SILICA SAND
SLURRY
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 6-6-2018
1.Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2.Well Construction Permit #: List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3.Well Use (check well use):
Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared) □Irrigation □Wells > 100,000 GPDNon-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient)
N W
6.Is(are) the well(s): □Permanent or □Temporary
7.Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wellsdrilled:
9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below top of casing: (ft.) If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
22.Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well construction info (add 'See Over' in Remarks Box). You may also attach additional pages if necessary.
24.SUBMITTAL INSTRUCTIONS
Submit this GW-1 within 30 days of well completion per the following:
24a. For All Wells: Original form to Division of Water Resources (DWR), Information Processing Unit, 1617 MSC, Raleigh, NC 27699-1617
24b. For Injection Wells: Copy to DWR, Underground Injection Control (IUC) Program, 1636 MSC, Raleigh, NC 27699-1636
24c. For Water Supply and Open-Loop Geothermal Return Wells: Copy to the county environmental health department of the county where installed
24d. For Water Wells producing over 100,000 GPD: Copy to DWR, CCPCUA Permit Program, 1611 MSC, Raleigh, NC 27699-1611
DAVID HALL
A - 4459
GEOLOGIC EXPLORATION

0.0 5.0 SCH 40
5.0 20.0 .010
l
0.0 PORTLAND BENTONITE
4.0 20-40
0.0 GRAVEL/SILTY CLAY 01/29/24 MW-4
FRYE & WEBSTER CLEANERS
608 ELWELL AVENUE GREENSBORO 27405
GUILFORD BENTONITE SEAL ~ 3.0 - 4.0 FEET
36° 05' 08.26" 79° 44' 34.86"02/06/24
l
20.0
10.0
8.0
AUGER
PVC
SCH 40 PVC
2.0

2.0
3.0
20.0
20.0

FINE SILICA SAND
SLURRY
Appendix E
Groundwater Sampling Forms
Appendix F
DSCA Indoor Air Risk Calculators
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:3/15/2024
Sample ID:IA-1
All concentrations are in ug/m3
CAS # Chemical Name:
Indoor Air
Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens
@ TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard
Quotient
71-43-2 Benzene 1.19 3.6E-01 6.3E+00 3.3E-06 3.8E-02
67-66-3 Chloroform 0.385 1.2E-01 2.0E+01 3.2E-06 3.8E-03
100-41-4 Ethylbenzene 0.394 1.1E+00 2.1E+02 3.5E-07 3.8E-04
127-18-4 Tetrachloroethylene 1.84 1.1E+01 8.3E+00 1.7E-07 4.4E-02
95-63-6 Trimethylbenzene, 1,2,4-0.5 -1.3E+01 8.0E-03
108-38-3 Xylene, m-0.595 -2.1E+01 5.7E-03
95-47-6 Xylene, o-0.631 -2.1E+01 6.1E-03
106-42-3 Xylene, p-0.595 -2.1E+01 5.7E-03
Cumulative: 7.0E-06 1.1E-01
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations
are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion.
Frye & Webster Cleaners / 608 Elwell Avenue, Greensboro, Guilford Co., NC
Frye & Webster Cleaners / 608 Elwell Avenue, Greensboro, Guilford Co., NC
DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:3/15/2024
Sample ID:IA-1
All concentrations are in ug/m3
CAS # Chemical Name:
Indoor Air
Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens
@ TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard
Quotient
71-43-2 Benzene 1.19 1.6E+00 2.6E+01 7.6E-07 9.1E-03
67-66-3 Chloroform 0.385 5.3E-01 8.6E+01 7.2E-07 9.0E-04
100-41-4 Ethylbenzene 0.394 4.9E+00 8.8E+02 8.0E-08 9.0E-05
127-18-4 Tetrachloroethylene 1.84 4.7E+01 3.5E+01 3.9E-08 1.1E-02
95-63-6 Trimethylbenzene, 1,2,4-0.5 -5.3E+01 1.9E-03
108-38-3 Xylene, m-0.595 -8.8E+01 1.4E-03
95-47-6 Xylene, o-0.631 -8.8E+01 1.4E-03
106-42-3 Xylene, p-0.595 -8.8E+01 1.4E-03
Cumulative: 1.6E-06 2.7E-02
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations
are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion.
DSCA Indoor Air Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Frye & Webster Cleaners / 608 Elwell Avenue, Greensboro, Guilford Co., NC
Frye & Webster Cleaners / 608 Elwell Avenue, Greensboro, Guilford Co., NC
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-1
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-66-3 Chloroform 1165 34.95 1.2E-01 2.0E+01 2.9E-04 3.4E-01
110-82-7 Cyclohexane 686 20.58 -1.3E+03 3.3E-03
156-59-2 Dichloroethylene, cis-1,2-23276 698.28 -8.3E+00 1.7E+01
115-07-1 Propylene 262 7.86 -6.3E+02 2.5E-03
79-34-5 Tetrachloroethane, 1,1,2,2-1336 40.08 4.8E-02 -8.3E-04
127-18-4 Tetrachloroethylene 2043185 61295.55 1.1E+01 8.3E+00 5.7E-03 1.5E+03
79-01-6 Trichloroethylene 64278 1928.34 4.8E-01 4.2E-01 4.0E-03 9.2E+02
Cumulative: 1.1E-02 2.4E+03
DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-1
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-66-3 Chloroform 1165 11.65 5.3E-01 8.6E+01 2.2E-05 2.7E-02
110-82-7 Cyclohexane 686 6.86 -5.3E+03 2.6E-04
156-59-2 Dichloroethylene, cis-1,2-23276 232.76 -3.5E+01 1.3E+00
115-07-1 Propylene 262 2.62 -2.6E+03 2.0E-04
79-34-5 Tetrachloroethane, 1,1,2,2-1336 13.36 2.1E-01 -6.3E-05
127-18-4 Tetrachloroethylene 2043185 20431.85 4.7E+01 3.5E+01 4.3E-04 1.2E+02
79-01-6 Trichloroethylene 64278 642.78 3.0E+00 1.8E+00 2.1E-04 7.3E+01
Cumulative: 7.3E-04 1.9E+02
DSCA Soil Gas Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-2
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 22.9 0.687 --
107-02-8 Acrolein 0.426 0.01278 -4.2E-03 6.1E-01
71-43-2 Benzene 1.5 0.045 3.6E-01 6.3E+00 1.3E-07 1.4E-03
106-99-0 Butadiene, 1,3-1.39 0.0417 9.4E-02 4.2E-01 4.5E-07 2.0E-02
75-15-0 Carbon Disulfide 1.18 0.0354 -1.5E+02 4.8E-05
67-66-3 Chloroform 1.84 0.0552 1.2E-01 2.0E+01 4.5E-07 5.4E-04
74-87-3 Chloromethane 0.862 0.02586 -1.9E+01 2.8E-04
110-82-7 Cyclohexane 0.937 0.02811 -1.3E+03 4.5E-06
75-71-8 Dichlorodifluoromethane 2.33 0.0699 -2.1E+01 6.7E-04
111-77-3 Ethanol, 2-(2-methoxyethoxy)-9.81 0.2943 --
141-78-6 Ethyl Acetate 1.45 0.0435 -1.5E+01 6.0E-04
100-41-4 Ethylbenzene 5.84 0.1752 1.1E+00 2.1E+02 1.6E-07 1.7E-04
142-82-5 Heptane, N-1.12 0.0336 -8.3E+01 8.1E-05
E5241997 Hexane, Commercial 1.79 0.0537 1.4E+01 1.3E+02 3.8E-09 8.6E-05
591-78-6 Hexanone, 2-2.46 0.0738 -6.3E+00 2.4E-03
67-63-0 Isopropanol 2.66 0.0798 -4.2E+01 3.8E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)1.11 0.0333 -1.0E+03 6.4E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)4.6 0.138 - 6.3E+02 4.4E-05
80-62-6 Methyl Methacrylate 1.35 0.0405 -1.5E+02 5.5E-05
75-09-2 Methylene Chloride 1.86 0.0558 1.0E+02 1.3E+02 5.5E-10 8.9E-05
91-20-3 ~Naphthalene 1.76 0.0528 8.3E-02 6.3E-01 6.4E-07 1.7E-02
103-65-1 Propyl benzene 1.11 0.0333 -2.1E+02 3.2E-05
115-07-1 Propylene 21.6 0.648 -6.3E+02 2.1E-04
100-42-5 Styrene 0.503 0.01509 -2.1E+02 1.4E-05
127-18-4 Tetrachloroethylene 871 26.13 1.1E+01 8.3E+00 2.4E-06 6.3E-01
108-88-3 Toluene 15.5 0.465 -1.0E+03 8.9E-05
79-01-6 Trichloroethylene 5.14 0.1542 4.8E-01 4.2E-01 3.2E-07 7.4E-02
75-69-4 Trichlorofluoromethane 1.24 0.0372 --
95-63-6 Trimethylbenzene, 1,2,4-15.4 0.462 -1.3E+01 7.4E-03
108-67-8 Trimethylbenzene, 1,3,5-3.49 0.1047 -1.3E+01 1.7E-03
25167-70-8 Trimethylpentene, 2,4,4-0.56 0.0168 --
1330-20-7 Xylenes 31.63 0.9489 -2.1E+01 9.1E-03
Cumulative: 4.6E-06 1.4E+00
DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-2
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 22.9 0.229 --
107-02-8 Acrolein 0.426 0.00426 -1.8E-02 4.9E-02
71-43-2 Benzene 1.5 0.015 1.6E+00 2.6E+01 9.5E-09 1.1E-04
106-99-0 Butadiene, 1,3-1.39 0.0139 4.1E-01 1.8E+00 3.4E-08 1.6E-03
75-15-0 Carbon Disulfide 1.18 0.0118 -6.1E+02 3.8E-06
67-66-3 Chloroform 1.84 0.0184 5.3E-01 8.6E+01 3.5E-08 4.3E-05
74-87-3 Chloromethane 0.862 0.00862 -7.9E+01 2.2E-05
110-82-7 Cyclohexane 0.937 0.00937 -5.3E+03 3.6E-07
75-71-8 Dichlorodifluoromethane 2.33 0.0233 -8.8E+01 5.3E-05
111-77-3 Ethanol, 2-(2-methoxyethoxy)-9.81 0.0981 --
141-78-6 Ethyl Acetate 1.45 0.0145 -6.1E+01 4.7E-05
100-41-4 Ethylbenzene 5.84 0.0584 4.9E+00 8.8E+02 1.2E-08 1.3E-05
142-82-5 Heptane, N-1.12 0.0112 -3.5E+02 6.4E-06
E5241997 Hexane, Commercial 1.79 0.0179 6.1E+01 5.3E+02 2.9E-10 6.8E-06
591-78-6 Hexanone, 2-2.46 0.0246 -2.6E+01 1.9E-04
67-63-0 Isopropanol 2.66 0.0266 -1.8E+02 3.0E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)1.11 0.0111 -4.4E+03 5.1E-07
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)1.12 0.0112 - 2.6E+03 8.5E-07
80-62-6 Methyl Methacrylate 1.35 0.0135 -6.1E+02 4.4E-06
75-09-2 Methylene Chloride 1.86 0.0186 1.2E+03 5.3E+02 1.5E-11 7.1E-06
91-20-3 ~Naphthalene 1.76 0.0176 3.6E-01 2.6E+00 4.9E-08 1.3E-03
103-65-1 Propyl benzene 1.11 0.0111 -8.8E+02 2.5E-06
115-07-1 Propylene 21.6 0.216 -2.6E+03 1.6E-05
100-42-5 Styrene 0.503 0.00503 -8.8E+02 1.1E-06
127-18-4 Tetrachloroethylene 871 8.71 4.7E+01 3.5E+01 1.8E-07 5.0E-02
108-88-3 Toluene 4.13 0.0413 -4.4E+03 1.9E-06
79-01-6 Trichloroethylene 5.14 0.0514 3.0E+00 1.8E+00 1.7E-08 5.9E-03
75-69-4 Trichlorofluoromethane 1.24 0.0124 --
95-63-6 Trimethylbenzene, 1,2,4-15.4 0.154 -5.3E+01 5.9E-04
108-67-8 Trimethylbenzene, 1,3,5-3.49 0.0349 -5.3E+01 1.3E-04
25167-70-8 Trimethylpentene, 2,4,4-0.56 0.0056 --
1330-20-7 Xylenes 31.63 0.3163 -8.8E+01 7.2E-04
Cumulative: 3.4E-07 1.1E-01
DSCA Soil Gas Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-3
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 23.8 0.714 --
75-05-8 Acetonitrile 0.178 0.00534 -1.3E+01 8.5E-05
71-43-2 Benzene 0.751 0.02253 3.6E-01 6.3E+00 6.3E-08 7.2E-04
75-15-0 Carbon Disulfide 3 0.09 -1.5E+02 1.2E-04
67-66-3 Chloroform 0.999 0.02997 1.2E-01 2.0E+01 2.5E-07 2.9E-04
98-82-8 Cumene 0.434 0.01302 -8.3E+01 3.1E-05
110-82-7 Cyclohexane 1.71 0.0513 -1.3E+03 8.2E-06
75-35-4 Dichloroethylene, 1,1-0.769 0.02307 -4.2E+01 1.1E-04
156-59-2 Dichloroethylene, cis-1,2-16 0.48 -8.3E+00 1.2E-02
156-60-5 Dichloroethylene, trans-1,2-1.25 0.0375 -8.3E+00 9.0E-04
111-77-3 Ethanol, 2-(2-methoxyethoxy)-1.5 0.045 --
100-41-4 Ethylbenzene 1.16 0.0348 1.1E+00 2.1E+02 3.1E-08 3.3E-05
142-82-5 Heptane, N-1.43 0.0429 -8.3E+01 1.0E-04
E5241997 Hexane, Commercial 1.65 0.0495 1.4E+01 1.3E+02 3.5E-09 7.9E-05
591-78-6 Hexanone, 2-16 0.48 -6.3E+00 1.5E-02
67-63-0 Isopropanol 0.558 0.01674 -4.2E+01 8.0E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)6.03 0.1809 -1.0E+03 3.5E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)5.67 0.1701 - 6.3E+02 5.4E-05
75-09-2 Methylene Chloride 0.838 0.02514 1.0E+02 1.3E+02 2.5E-10 4.0E-05
103-65-1 Propyl benzene 0.912 0.02736 -2.1E+02 2.6E-05
115-07-1 Propylene 5.02 0.1506 -6.3E+02 4.8E-05
127-18-4 Tetrachloroethylene 12277 368.31 1.1E+01 8.3E+00 3.4E-05 8.8E+00
108-88-3 Toluene 7.29 0.2187 -1.0E+03 4.2E-05
71-55-6 Trichloroethane, 1,1,1-15.6 0.468 -1.0E+03 9.0E-05
79-01-6 Trichloroethylene 109 3.27 4.8E-01 4.2E-01 6.8E-06 1.6E+00
75-69-4 Trichlorofluoromethane 1.1 0.033 --
95-63-6 Trimethylbenzene, 1,2,4-4.12 0.1236 -1.3E+01 2.0E-03
108-67-8 Trimethylbenzene, 1,3,5-1.06 0.0318 -1.3E+01 5.1E-04
1330-20-7 Xylenes 6.08 0.1824 -2.1E+01 1.7E-03
Cumulative: 4.1E-05 1.0E+01
DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-3
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 23.8 0.238 --
75-05-8 Acetonitrile 0.178 0.00178 -5.3E+01 6.8E-06
71-43-2 Benzene 0.751 0.00751 1.6E+00 2.6E+01 4.8E-09 5.7E-05
75-15-0 Carbon Disulfide 3 0.03 -6.1E+02 9.8E-06
67-66-3 Chloroform 0.999 0.00999 5.3E-01 8.6E+01 1.9E-08 2.3E-05
98-82-8 Cumene 0.434 0.00434 -3.5E+02 2.5E-06
110-82-7 Cyclohexane 1.71 0.0171 -5.3E+03 6.5E-07
75-35-4 Dichloroethylene, 1,1-0.769 0.00769 -1.8E+02 8.8E-06
156-59-2 Dichloroethylene, cis-1,2-16 0.16 -3.5E+01 9.1E-04
156-60-5 Dichloroethylene, trans-1,2-1.25 0.0125 -3.5E+01 7.1E-05
111-77-3 Ethanol, 2-(2-methoxyethoxy)-1.5 0.015 --
100-41-4 Ethylbenzene 1.16 0.0116 4.9E+00 8.8E+02 2.4E-09 2.6E-06
142-82-5 Heptane, N-1.43 0.0143 -3.5E+02 8.2E-06
E5241997 Hexane, Commercial 1.65 0.0165 6.1E+01 5.3E+02 2.7E-10 6.3E-06
591-78-6 Hexanone, 2-16 0.16 -2.6E+01 1.2E-03
67-63-0 Isopropanol 0.558 0.00558 -1.8E+02 6.4E-06
78-93-3 Methyl Ethyl Ketone (2-Butanone)6.03 0.0603 -4.4E+03 2.8E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)5.67 0.0567 - 2.6E+03 4.3E-06
75-09-2 Methylene Chloride 0.838 0.00838 1.2E+03 5.3E+02 6.8E-12 3.2E-06
103-65-1 Propyl benzene 0.912 0.00912 -8.8E+02 2.1E-06
115-07-1 Propylene 5.02 0.0502 -2.6E+03 3.8E-06
127-18-4 Tetrachloroethylene 12277 122.77 4.7E+01 3.5E+01 2.6E-06 7.0E-01
108-88-3 Toluene 1.94 0.0194 -4.4E+03 8.9E-07
71-55-6 Trichloroethane, 1,1,1-15.6 0.156 -4.4E+03 7.1E-06
79-01-6 Trichloroethylene 109 1.09 3.0E+00 1.8E+00 3.6E-07 1.2E-01
75-69-4 Trichlorofluoromethane 1.1 0.011 --
95-63-6 Trimethylbenzene, 1,2,4-4.12 0.0412 -5.3E+01 1.6E-04
108-67-8 Trimethylbenzene, 1,3,5-1.06 0.0106 -5.3E+01 4.0E-05
1330-20-7 Xylenes 6.08 0.0608 -8.8E+01 1.4E-04
Cumulative: 3.0E-06 8.3E-01
DSCA Soil Gas Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:2/1/2024
Sample ID:SG-4
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 8.88 0.2664 --
107-02-8 Acrolein 4.5 0.135 -4.2E-03 6.5E+00
71-43-2 Benzene 0.389 0.01167 3.6E-01 6.3E+00 3.2E-08 3.7E-04
106-99-0 Butadiene, 1,3-0.61 0.0183 9.4E-02 4.2E-01 2.0E-07 8.8E-03
75-15-0 Carbon Disulfide 9.66 0.2898 -1.5E+02 4.0E-04
67-66-3 Chloroform 0.57 0.0171 1.2E-01 2.0E+01 1.4E-07 1.7E-04
74-87-3 Chloromethane 0.201 0.00603 -1.9E+01 6.4E-05
98-82-8 Cumene 0.904 0.02712 -8.3E+01 6.5E-05
110-82-7 Cyclohexane 5.67 0.1701 -1.3E+03 2.7E-05
75-71-8 Dichlorodifluoromethane 2.25 0.0675 -2.1E+01 6.5E-04
107-06-2 Dichloroethane, 1,2-0.445 0.01335 1.1E-01 1.5E+00 1.2E-07 1.8E-03
156-59-2 Dichloroethylene, cis-1,2-6.04 0.1812 -8.3E+00 4.3E-03
111-77-3 Ethanol, 2-(2-methoxyethoxy)-1.33 0.0399 --
75-00-3 Ethyl Chloride (Chloroethane)0.248 0.00744 -8.3E+02 1.8E-06
100-41-4 Ethylbenzene 0.726 0.02178 1.1E+00 2.1E+02 1.9E-08 2.1E-05
142-82-5 Heptane, N-1.39 0.0417 -8.3E+01 1.0E-04
E5241997 Hexane, Commercial 3.23 0.0969 1.4E+01 1.3E+02 6.9E-09 1.5E-04
591-78-6 Hexanone, 2-14.5 0.435 -6.3E+00 1.4E-02
67-63-0 Isopropanol 0.51 0.0153 -4.2E+01 7.3E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)1.12 0.0336 -1.0E+03 6.4E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)35.7 1.071 - 6.3E+02 3.4E-04
80-62-6 Methyl Methacrylate 4.15 0.1245 -1.5E+02 1.7E-04
75-09-2 Methylene Chloride 0.49 0.0147 1.0E+02 1.3E+02 1.4E-10 2.3E-05
115-07-1 Propylene 31.3 0.939 -6.3E+02 3.0E-04
79-34-5 Tetrachloroethane, 1,1,2,2-1.72 0.0516 4.8E-02 -1.1E-06
127-18-4 Tetrachloroethylene 1236 37.08 1.1E+01 8.3E+00 3.4E-06 8.9E-01
108-88-3 Toluene 3.4 0.102 -1.0E+03 2.0E-05
79-00-5 Trichloroethane, 1,1,2-4.99 0.1497 1.8E-01 4.2E-02 8.5E-07 7.2E-01
79-01-6 Trichloroethylene 9.03 0.2709 4.8E-01 4.2E-01 5.7E-07 1.3E-01
75-69-4 Trichlorofluoromethane 1.11 0.0333 --
95-63-6 Trimethylbenzene, 1,2,4-2.71 0.0813 -1.3E+01 1.3E-03
108-67-8 Trimethylbenzene, 1,3,5-0.966 0.02898 -1.3E+01 4.6E-04
25167-70-8 Trimethylpentene, 2,4,4-1.45 0.0435 --
1330-20-7 Xylenes 4.94 0.1482 -2.1E+01 1.4E-03
Cumulative: 6.4E-06 8.2E+00
DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:2/1/2024
Sample ID:SG-4
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 8.88 0.0888 --
107-02-8 Acrolein 4.5 0.045 -1.8E-02 5.1E-01
71-43-2 Benzene 0.389 0.00389 1.6E+00 2.6E+01 2.5E-09 3.0E-05
106-99-0 Butadiene, 1,3-0.61 0.0061 4.1E-01 1.8E+00 1.5E-08 7.0E-04
75-15-0 Carbon Disulfide 9.66 0.0966 -6.1E+02 3.2E-05
67-66-3 Chloroform 0.57 0.0057 5.3E-01 8.6E+01 1.1E-08 1.3E-05
74-87-3 Chloromethane 0.201 0.00201 -7.9E+01 5.1E-06
98-82-8 Cumene 0.904 0.00904 -3.5E+02 5.2E-06
110-82-7 Cyclohexane 5.67 0.0567 -5.3E+03 2.2E-06
75-71-8 Dichlorodifluoromethane 2.25 0.0225 -8.8E+01 5.1E-05
107-06-2 Dichloroethane, 1,2-0.445 0.00445 4.7E-01 6.1E+00 9.4E-09 1.5E-04
156-59-2 Dichloroethylene, cis-1,2-6.04 0.0604 -3.5E+01 3.4E-04
111-77-3 Ethanol, 2-(2-methoxyethoxy)-1.33 0.0133 --
75-00-3 Ethyl Chloride (Chloroethane)0.248 0.00248 -3.5E+03 1.4E-07
100-41-4 Ethylbenzene 0.726 0.00726 4.9E+00 8.8E+02 1.5E-09 1.7E-06
142-82-5 Heptane, N-1.39 0.0139 -3.5E+02 7.9E-06
E5241997 Hexane, Commercial 3.23 0.0323 6.1E+01 5.3E+02 5.3E-10 1.2E-05
591-78-6 Hexanone, 2-14.5 0.145 -2.6E+01 1.1E-03
67-63-0 Isopropanol 0.51 0.0051 -1.8E+02 5.8E-06
78-93-3 Methyl Ethyl Ketone (2-Butanone)1.12 0.0112 -4.4E+03 5.1E-07
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)35.7 0.357 - 2.6E+03 2.7E-05
80-62-6 Methyl Methacrylate 4.15 0.0415 -6.1E+02 1.4E-05
75-09-2 Methylene Chloride 0.49 0.0049 1.2E+03 5.3E+02 4.0E-12 1.9E-06
115-07-1 Propylene 31.3 0.313 -2.6E+03 2.4E-05
79-34-5 Tetrachloroethane, 1,1,2,2-1.72 0.0172 2.1E-01 -8.1E-08
127-18-4 Tetrachloroethylene 1236 12.36 4.7E+01 3.5E+01 2.6E-07 7.1E-02
108-88-3 Toluene 3.4 0.034 -4.4E+03 1.6E-06
79-00-5 Trichloroethane, 1,1,2-4.99 0.0499 7.7E-01 1.8E-01 6.5E-08 5.7E-02
79-01-6 Trichloroethylene 9.03 0.0903 3.0E+00 1.8E+00 3.0E-08 1.0E-02
75-69-4 Trichlorofluoromethane 1.11 0.0111 --
95-63-6 Trimethylbenzene, 1,2,4-2.71 0.0271 -5.3E+01 1.0E-04
108-67-8 Trimethylbenzene, 1,3,5-0.966 0.00966 -5.3E+01 3.7E-05
25167-70-8 Trimethylpentene, 2,4,4-1.4 0.014 --
1330-20-7 Xylenes 4.94 0.0494 -8.8E+01 1.1E-04
Cumulative: 4.8E-07 6.5E-01
DSCA Soil Gas Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/29/2024
Sample ID:SG-5
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 84.9 2.547 --
107-02-8 Acrolein 0.803 0.02409 -4.2E-03 1.2E+00
71-43-2 Benzene 1.21 0.0363 3.6E-01 6.3E+00 1.0E-07 1.2E-03
106-99-0 Butadiene, 1,3-0.718 0.02154 9.4E-02 4.2E-01 2.3E-07 1.0E-02
75-15-0 Carbon Disulfide 1.55 0.0465 -1.5E+02 6.4E-05
56-23-5 Carbon Tetrachloride 0.51 0.0153 4.7E-01 2.1E+01 3.3E-08 1.5E-04
67-66-3 Chloroform 5.25 0.1575 1.2E-01 2.0E+01 1.3E-06 1.5E-03
74-87-3 Chloromethane 0.77 0.0231 -1.9E+01 2.5E-04
95-49-8 Chlorotoluene, o-0.56 0.0168 --
98-82-8 Cumene 1.23 0.0369 -8.3E+01 8.8E-05
110-82-7 Cyclohexane 1.46 0.0438 -1.3E+03 7.0E-06
75-71-8 Dichlorodifluoromethane 2.44 0.0732 -2.1E+01 7.0E-04
156-59-2 Dichloroethylene, cis-1,2-14.4 0.432 -8.3E+00 1.0E-02
156-60-5 Dichloroethylene, trans-1,2-2.01 0.0603 -8.3E+00 1.4E-03
123-91-1 Dioxane, 1,4-1.33 0.0399 5.6E-01 6.3E+00 7.1E-08 1.3E-03
111-77-3 Ethanol, 2-(2-methoxyethoxy)-6.59 0.1977 --
141-78-6 Ethyl Acetate 4.13 0.1239 -1.5E+01 1.7E-03
100-41-4 Ethylbenzene 4.5 0.135 1.1E+00 2.1E+02 1.2E-07 1.3E-04
142-82-5 Heptane, N-1.78 0.0534 -8.3E+01 1.3E-04
E5241997 Hexane, Commercial 2.5 0.075 1.4E+01 1.3E+02 5.3E-09 1.2E-04
591-78-6 Hexanone, 2-98.7 2.961 -6.3E+00 9.5E-02
67-63-0 Isopropanol 4.77 0.1431 -4.2E+01 6.9E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)18.7 0.561 -1.0E+03 1.1E-04
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)30.7 0.921 - 6.3E+02 2.9E-04
80-62-6 Methyl Methacrylate 0.387 0.01161 -1.5E+02 1.6E-05
75-09-2 Methylene Chloride 0.665 0.01995 1.0E+02 1.3E+02 2.0E-10 3.2E-05
91-20-3 ~Naphthalene 0.85 0.0255 8.3E-02 6.3E-01 3.1E-07 8.2E-03
103-65-1 Propyl benzene 2.59 0.0777 -2.1E+02 7.5E-05
115-07-1 Propylene 7.22 0.2166 -6.3E+02 6.9E-05
100-42-5 Styrene 0.444 0.01332 -2.1E+02 1.3E-05
79-34-5 Tetrachloroethane, 1,1,2,2-0.775 0.02325 4.8E-02 -4.8E-07
127-18-4 Tetrachloroethylene 3117 93.51 1.1E+01 8.3E+00 8.7E-06 2.2E+00
108-88-3 Toluene 15.7 0.471 -1.0E+03 9.0E-05
79-00-5 Trichloroethane, 1,1,2-0.553 0.01659 1.8E-01 4.2E-02 9.5E-08 8.0E-02
79-01-6 Trichloroethylene 131 3.93 4.8E-01 4.2E-01 8.2E-06 1.9E+00
75-69-4 Trichlorofluoromethane 1.32 0.0396 --
95-63-6 Trimethylbenzene, 1,2,4-15.1 0.453 -1.3E+01 7.2E-03
108-67-8 Trimethylbenzene, 1,3,5-3.91 0.1173 -1.3E+01 1.9E-03
25167-70-8 Trimethylpentene, 2,4,4-3.28 0.0984 --
1330-20-7 Xylenes 24.83 0.7449 -2.1E+01 7.1E-03
Cumulative: 2.0E-05 5.5E+00
DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/29/2024
Sample ID:SG-5
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 84.9 0.849 --
107-02-8 Acrolein 0.803 0.00803 -1.8E-02 9.2E-02
71-43-2 Benzene 1.21 0.0121 1.6E+00 2.6E+01 7.7E-09 9.2E-05
106-99-0 Butadiene, 1,3-0.718 0.00718 4.1E-01 1.8E+00 1.8E-08 8.2E-04
75-15-0 Carbon Disulfide 1.55 0.0155 -6.1E+02 5.1E-06
56-23-5 Carbon Tetrachloride 0.51 0.0051 2.0E+00 8.8E+01 2.5E-09 1.2E-05
67-66-3 Chloroform 5.25 0.0525 5.3E-01 8.6E+01 9.8E-08 1.2E-04
74-87-3 Chloromethane 0.77 0.0077 -7.9E+01 2.0E-05
95-49-8 Chlorotoluene, o-0.56 0.0056 --
98-82-8 Cumene 1.23 0.0123 -3.5E+02 7.0E-06
110-82-7 Cyclohexane 1.46 0.0146 -5.3E+03 5.6E-07
75-71-8 Dichlorodifluoromethane 2.44 0.0244 -8.8E+01 5.6E-05
156-59-2 Dichloroethylene, cis-1,2-14.4 0.144 -3.5E+01 8.2E-04
156-60-5 Dichloroethylene, trans-1,2-2.01 0.0201 -3.5E+01 1.1E-04
123-91-1 Dioxane, 1,4-1.33 0.0133 2.5E+00 2.6E+01 5.4E-09 1.0E-04
111-77-3 Ethanol, 2-(2-methoxyethoxy)-6.59 0.0659 --
141-78-6 Ethyl Acetate 4.13 0.0413 -6.1E+01 1.3E-04
100-41-4 Ethylbenzene 4.5 0.045 4.9E+00 8.8E+02 9.2E-09 1.0E-05
142-82-5 Heptane, N-1.78 0.0178 -3.5E+02 1.0E-05
E5241997 Hexane, Commercial 2.5 0.025 6.1E+01 5.3E+02 4.1E-10 9.5E-06
591-78-6 Hexanone, 2-98.7 0.987 -2.6E+01 7.5E-03
67-63-0 Isopropanol 4.77 0.0477 -1.8E+02 5.4E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)18.7 0.187 -4.4E+03 8.5E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)30.7 0.307 - 2.6E+03 2.3E-05
80-62-6 Methyl Methacrylate 0.387 0.00387 -6.1E+02 1.3E-06
75-09-2 Methylene Chloride 0.665 0.00665 1.2E+03 5.3E+02 5.4E-12 2.5E-06
91-20-3 ~Naphthalene 0.85 0.0085 3.6E-01 2.6E+00 2.4E-08 6.5E-04
103-65-1 Propyl benzene 2.59 0.0259 -8.8E+02 5.9E-06
115-07-1 Propylene 7.22 0.0722 -2.6E+03 5.5E-06
100-42-5 Styrene 0.444 0.00444 -8.8E+02 1.0E-06
79-34-5 Tetrachloroethane, 1,1,2,2-0.775 0.00775 2.1E-01 -3.7E-08
127-18-4 Tetrachloroethylene 3117 31.17 4.7E+01 3.5E+01 6.6E-07 1.8E-01
108-88-3 Toluene 15.7 0.157 -4.4E+03 7.2E-06
79-00-5 Trichloroethane, 1,1,2-0.553 0.00553 7.7E-01 1.8E-01 7.2E-09 6.3E-03
79-01-6 Trichloroethylene 131 1.31 3.0E+00 1.8E+00 4.4E-07 1.5E-01
75-69-4 Trichlorofluoromethane 1.32 0.0132 --
95-63-6 Trimethylbenzene, 1,2,4-15.1 0.151 -5.3E+01 5.7E-04
108-67-8 Trimethylbenzene, 1,3,5-3.91 0.0391 -5.3E+01 1.5E-04
25167-70-8 Trimethylpentene, 2,4,4-3.28 0.0328 --
1330-20-7 Xylenes 24.83 0.2483 -8.8E+01 5.7E-04
Cumulative: 1.3E-06 4.4E-01
DSCA Soil Gas Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:2/1/2024
Sample ID:SG-6
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 17.5 0.525 --
75-15-0 Carbon Disulfide 1.18 0.0354 -1.5E+02 4.8E-05
67-66-3 Chloroform 0.822 0.02466 1.2E-01 2.0E+01 2.0E-07 2.4E-04
74-87-3 Chloromethane 0.405 0.01215 -1.9E+01 1.3E-04
110-82-7 Cyclohexane 0.326 0.00978 -1.3E+03 1.6E-06
75-71-8 Dichlorodifluoromethane 2.32 0.0696 -2.1E+01 6.7E-04
111-77-3 Ethanol, 2-(2-methoxyethoxy)-1.63 0.0489 --
E5241997 Hexane, Commercial 0.833 0.02499 1.4E+01 1.3E+02 1.8E-09 4.0E-05
591-78-6 Hexanone, 2-0.396 0.01188 -6.3E+00 3.8E-04
67-63-0 Isopropanol 1.04 0.0312 -4.2E+01 1.5E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)0.687 0.02061 -1.0E+03 4.0E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)0.398 0.01194 - 6.3E+02 3.8E-06
75-09-2 Methylene Chloride 0.363 0.01089 1.0E+02 1.3E+02 1.1E-10 1.7E-05
115-07-1 Propylene 1.57 0.0471 -6.3E+02 1.5E-05
127-18-4 Tetrachloroethylene 133 3.99 1.1E+01 8.3E+00 3.7E-07 9.6E-02
108-88-3 Toluene 1.96 0.0588 -1.0E+03 1.1E-05
75-69-4 Trichlorofluoromethane 1.38 0.0414 --
Cumulative: 5.7E-07 9.7E-02
DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:2/1/2024
Sample ID:SG-6
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 17.5 0.175 --
75-15-0 Carbon Disulfide 1.18 0.0118 -6.1E+02 3.8E-06
67-66-3 Chloroform 0.822 0.00822 5.3E-01 8.6E+01 1.5E-08 1.9E-05
74-87-3 Chloromethane 0.405 0.00405 -7.9E+01 1.0E-05
110-82-7 Cyclohexane 0.326 0.00326 -5.3E+03 1.2E-07
75-71-8 Dichlorodifluoromethane 2.32 0.0232 -8.8E+01 5.3E-05
111-77-3 Ethanol, 2-(2-methoxyethoxy)-1.63 0.0163 --
E5241997 Hexane, Commercial 0.833 0.00833 6.1E+01 5.3E+02 1.4E-10 3.2E-06
591-78-6 Hexanone, 2-0.396 0.00396 -2.6E+01 3.0E-05
67-63-0 Isopropanol 1.04 0.0104 -1.8E+02 1.2E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)0.687 0.00687 -4.4E+03 3.1E-07
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)0.398 0.00398 - 2.6E+03 3.0E-07
75-09-2 Methylene Chloride 0.363 0.00363 1.2E+03 5.3E+02 3.0E-12 1.4E-06
115-07-1 Propylene 1.57 0.0157 -2.6E+03 1.2E-06
127-18-4 Tetrachloroethylene 133 1.33 4.7E+01 3.5E+01 2.8E-08 7.6E-03
108-88-3 Toluene 1.96 0.0196 -4.4E+03 8.9E-07
75-69-4 Trichlorofluoromethane 1.38 0.0138 --
Cumulative: 4.4E-08 7.7E-03
DSCA Soil Gas Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-9
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 20.5 0.615 --
75-05-8 Acetonitrile 0.302 0.00906 -1.3E+01 1.4E-04
107-13-1 Acrylonitrile 0.751 0.02253 4.1E-02 4.2E-01 5.5E-07 1.1E-02
71-43-2 Benzene 7.02 0.2106 3.6E-01 6.3E+00 5.9E-07 6.7E-03
106-94-5 Bromopropane, 1-0.425 0.01275 -2.1E+01 1.2E-04
106-99-0 Butadiene, 1,3-11.7 0.351 9.4E-02 4.2E-01 3.8E-06 1.7E-01
75-15-0 Carbon Disulfide 55.6 1.668 -1.5E+02 2.3E-03
67-66-3 Chloroform 0.929 0.02787 1.2E-01 2.0E+01 2.3E-07 2.7E-04
74-87-3 Chloromethane 0.27 0.0081 -1.9E+01 8.6E-05
98-82-8 Cumene 0.587 0.01761 -8.3E+01 4.2E-05
110-82-7 Cyclohexane 6.32 0.1896 -1.3E+03 3.0E-05
75-71-8 Dichlorodifluoromethane 2.24 0.0672 -2.1E+01 6.4E-04
156-59-2 Dichloroethylene, cis-1,2-0.44 0.0132 -8.3E+00 3.2E-04
111-77-3 Ethanol, 2-(2-methoxyethoxy)-4.28 0.1284 --
141-78-6 Ethyl Acetate 1.02 0.0306 -1.5E+01 4.2E-04
100-41-4 Ethylbenzene 1.89 0.0567 1.1E+00 2.1E+02 5.0E-08 5.4E-05
142-82-5 Heptane, N-8.31 0.2493 -8.3E+01 6.0E-04
E5241997 Hexane, Commercial 14.4 0.432 1.4E+01 1.3E+02 3.1E-08 6.9E-04
591-78-6 Hexanone, 2-0.577 0.01731 -6.3E+00 5.5E-04
67-63-0 Isopropanol 2.35 0.0705 -4.2E+01 3.4E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)3.79 0.1137 -1.0E+03 2.2E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)0.917 0.02751 - 6.3E+02 8.8E-06
75-09-2 Methylene Chloride 2 0.06 1.0E+02 1.3E+02 5.9E-10 9.6E-05
103-65-1 Propyl benzene 0.483 0.01449 -2.1E+02 1.4E-05
115-07-1 Propylene 99.9 2.997 -6.3E+02 9.6E-04
100-42-5 Styrene 0.577 0.01731 -2.1E+02 1.7E-05
127-18-4 Tetrachloroethylene 47.6 1.428 1.1E+01 8.3E+00 1.3E-07 3.4E-02
108-88-3 Toluene 14.7 0.441 -1.0E+03 8.5E-05
79-01-6 Trichloroethylene 0.525 0.01575 4.8E-01 4.2E-01 3.3E-08 7.6E-03
75-69-4 Trichlorofluoromethane 1.17 0.0351 --
95-63-6 Trimethylbenzene, 1,2,4-1.82 0.0546 -1.3E+01 8.7E-04
108-67-8 Trimethylbenzene, 1,3,5-0.657 0.01971 -1.3E+01 3.2E-04
25167-70-8 Trimethylpentene, 2,4,4-3.77 0.1131 --
1330-20-7 Xylenes 7 0.21 -2.1E+01 2.0E-03
Cumulative: 5.4E-06 2.4E-01
DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:2/1/2024
Sample ID:SG-9
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 20.5 0.205 --
75-05-8 Acetonitrile 0.302 0.00302 -5.3E+01 1.1E-05
107-13-1 Acrylonitrile 0.751 0.00751 1.8E-01 1.8E+00 4.2E-08 8.6E-04
71-43-2 Benzene 7.02 0.0702 1.6E+00 2.6E+01 4.5E-08 5.3E-04
106-94-5 Bromopropane, 1-0.425 0.00425 -8.8E+01 9.7E-06
106-99-0 Butadiene, 1,3-11.7 0.117 4.1E-01 1.8E+00 2.9E-07 1.3E-02
75-15-0 Carbon Disulfide 55.6 0.556 -6.1E+02 1.8E-04
67-66-3 Chloroform 0.929 0.00929 5.3E-01 8.6E+01 1.7E-08 2.2E-05
74-87-3 Chloromethane 0.27 0.0027 -7.9E+01 6.8E-06
98-82-8 Cumene 0.587 0.00587 -3.5E+02 3.4E-06
110-82-7 Cyclohexane 6.32 0.0632 -5.3E+03 2.4E-06
75-71-8 Dichlorodifluoromethane 2.24 0.0224 -8.8E+01 5.1E-05
156-59-2 Dichloroethylene, cis-1,2-0.44 0.0044 -3.5E+01 2.5E-05
111-77-3 Ethanol, 2-(2-methoxyethoxy)-4.28 0.0428 --
141-78-6 Ethyl Acetate 1.02 0.0102 -6.1E+01 3.3E-05
100-41-4 Ethylbenzene 1.89 0.0189 4.9E+00 8.8E+02 3.9E-09 4.3E-06
142-82-5 Heptane, N-8.31 0.0831 -3.5E+02 4.7E-05
E5241997 Hexane, Commercial 14.4 0.144 6.1E+01 5.3E+02 2.3E-09 5.5E-05
591-78-6 Hexanone, 2-0.577 0.00577 -2.6E+01 4.4E-05
67-63-0 Isopropanol 2.35 0.0235 -1.8E+02 2.7E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)3.79 0.0379 -4.4E+03 1.7E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)0.917 0.00917 - 2.6E+03 7.0E-07
75-09-2 Methylene Chloride 2 0.02 1.2E+03 5.3E+02 1.6E-11 7.6E-06
103-65-1 Propyl benzene 0.483 0.00483 -8.8E+02 1.1E-06
115-07-1 Propylene 99.9 0.999 -2.6E+03 7.6E-05
100-42-5 Styrene 0.577 0.00577 -8.8E+02 1.3E-06
127-18-4 Tetrachloroethylene 47.6 0.476 4.7E+01 3.5E+01 1.0E-08 2.7E-03
108-88-3 Toluene 14.7 0.147 -4.4E+03 6.7E-06
79-01-6 Trichloroethylene 0.525 0.00525 3.0E+00 1.8E+00 1.8E-09 6.0E-04
75-69-4 Trichlorofluoromethane 1.17 0.0117 --
95-63-6 Trimethylbenzene, 1,2,4-1.82 0.0182 -5.3E+01 6.9E-05
108-67-8 Trimethylbenzene, 1,3,5-0.657 0.00657 -5.3E+01 2.5E-05
25167-70-8 Trimethylpentene, 2,4,4-3.77 0.0377 --
1330-20-7 Xylenes 7 0.07 -8.8E+01 1.6E-04
Cumulative: 4.1E-07 1.9E-02
DSCA Soil Gas Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-10
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 31 0.93 --
107-02-8 Acrolein 0.682 0.02046 -4.2E-03 9.8E-01
71-43-2 Benzene 4.08 0.1224 3.6E-01 6.3E+00 3.4E-07 3.9E-03
106-99-0 Butadiene, 1,3-5.28 0.1584 9.4E-02 4.2E-01 1.7E-06 7.6E-02
75-15-0 Carbon Disulfide 46.3 1.389 -1.5E+02 1.9E-03
67-66-3 Chloroform 1.99 0.0597 1.2E-01 2.0E+01 4.9E-07 5.8E-04
74-87-3 Chloromethane 0.727 0.02181 -1.9E+01 2.3E-04
98-82-8 Cumene 1.39 0.0417 -8.3E+01 1.0E-04
110-82-7 Cyclohexane 2.2 0.066 -1.3E+03 1.1E-05
75-71-8 Dichlorodifluoromethane 2.31 0.0693 -2.1E+01 6.6E-04
156-59-2 Dichloroethylene, cis-1,2-1.2 0.036 -8.3E+00 8.6E-04
111-77-3 Ethanol, 2-(2-methoxyethoxy)-4.54 0.1362 --
141-78-6 Ethyl Acetate 1.28 0.0384 -1.5E+01 5.3E-04
100-41-4 Ethylbenzene 13.6 0.408 1.1E+00 2.1E+02 3.6E-07 3.9E-04
142-82-5 Heptane, N-2.36 0.0708 -8.3E+01 1.7E-04
E5241997 Hexane, Commercial 4.32 0.1296 1.4E+01 1.3E+02 9.2E-09 2.1E-04
591-78-6 Hexanone, 2-8.29 0.2487 -6.3E+00 7.9E-03
67-63-0 Isopropanol 2.14 0.0642 -4.2E+01 3.1E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)2.04 0.0612 -1.0E+03 1.2E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)14.5 0.435 - 6.3E+02 1.4E-04
1634-04-4 Methyl tert-Butyl Ether (MTBE)0.806 0.02418 1.1E+01 6.3E+02 2.2E-09 7.7E-06
75-09-2 Methylene Chloride 0.849 0.02547 1.0E+02 1.3E+02 2.5E-10 4.1E-05
91-20-3 ~Naphthalene 1.13 0.0339 8.3E-02 6.3E-01 4.1E-07 1.1E-02
103-65-1 Propyl benzene 2.16 0.0648 -2.1E+02 6.2E-05
115-07-1 Propylene 64.5 1.935 -6.3E+02 6.2E-04
100-42-5 Styrene 1.56 0.0468 -2.1E+02 4.5E-05
79-34-5 Tetrachloroethane, 1,1,2,2-1.7 0.051 4.8E-02 -1.1E-06
127-18-4 Tetrachloroethylene 236 7.08 1.1E+01 8.3E+00 6.6E-07 1.7E-01
108-88-3 Toluene 14.6 0.438 -1.0E+03 8.4E-05
79-01-6 Trichloroethylene 2.63 0.0789 4.8E-01 4.2E-01 1.6E-07 3.8E-02
75-69-4 Trichlorofluoromethane 1.29 0.0387 --
95-63-6 Trimethylbenzene, 1,2,4-21.7 0.651 -1.3E+01 1.0E-02
108-67-8 Trimethylbenzene, 1,3,5-5.39 0.1617 -1.3E+01 2.6E-03
25167-70-8 Trimethylpentene, 2,4,4-1.02 0.0306 --
1330-20-7 Xylenes 90.5 2.715 -2.1E+01 2.6E-02
Cumulative: 5.2E-06 1.3E+00
DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-10
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 31 0.31 --
107-02-8 Acrolein 0.682 0.00682 -1.8E-02 7.8E-02
71-43-2 Benzene 4.08 0.0408 1.6E+00 2.6E+01 2.6E-08 3.1E-04
106-99-0 Butadiene, 1,3-5.28 0.0528 4.1E-01 1.8E+00 1.3E-07 6.0E-03
75-15-0 Carbon Disulfide 46.3 0.463 -6.1E+02 1.5E-04
67-66-3 Chloroform 1.99 0.0199 5.3E-01 8.6E+01 3.7E-08 4.6E-05
74-87-3 Chloromethane 0.727 0.00727 -7.9E+01 1.8E-05
98-82-8 Cumene 1.39 0.0139 -3.5E+02 7.9E-06
110-82-7 Cyclohexane 2.2 0.022 -5.3E+03 8.4E-07
75-71-8 Dichlorodifluoromethane 2.31 0.0231 -8.8E+01 5.3E-05
156-59-2 Dichloroethylene, cis-1,2-1.2 0.012 -3.5E+01 6.8E-05
111-77-3 Ethanol, 2-(2-methoxyethoxy)-4.54 0.0454 --
141-78-6 Ethyl Acetate 1.28 0.0128 -6.1E+01 4.2E-05
100-41-4 Ethylbenzene 13.6 0.136 4.9E+00 8.8E+02 2.8E-08 3.1E-05
142-82-5 Heptane, N-2.36 0.0236 -3.5E+02 1.3E-05
E5241997 Hexane, Commercial 4.32 0.0432 6.1E+01 5.3E+02 7.0E-10 1.6E-05
591-78-6 Hexanone, 2-8.29 0.0829 -2.6E+01 6.3E-04
67-63-0 Isopropanol 2.14 0.0214 -1.8E+02 2.4E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)2.04 0.0204 -4.4E+03 9.3E-07
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)14.5 0.145 - 2.6E+03 1.1E-05
1634-04-4 Methyl tert-Butyl Ether (MTBE)0.806 0.00806 4.7E+01 2.6E+03 1.7E-10 6.1E-07
75-09-2 Methylene Chloride 0.849 0.00849 1.2E+03 5.3E+02 6.9E-12 3.2E-06
91-20-3 ~Naphthalene 1.13 0.0113 3.6E-01 2.6E+00 3.1E-08 8.6E-04
103-65-1 Propyl benzene 2.16 0.0216 -8.8E+02 4.9E-06
115-07-1 Propylene 64.5 0.645 -2.6E+03 4.9E-05
100-42-5 Styrene 1.56 0.0156 -8.8E+02 3.6E-06
79-34-5 Tetrachloroethane, 1,1,2,2-1.7 0.017 2.1E-01 -8.0E-08
127-18-4 Tetrachloroethylene 236 2.36 4.7E+01 3.5E+01 5.0E-08 1.3E-02
108-88-3 Toluene 14.6 0.146 -4.4E+03 6.7E-06
79-01-6 Trichloroethylene 2.63 0.0263 3.0E+00 1.8E+00 8.8E-09 3.0E-03
75-69-4 Trichlorofluoromethane 1.29 0.0129 --
95-63-6 Trimethylbenzene, 1,2,4-21.7 0.217 -5.3E+01 8.3E-04
108-67-8 Trimethylbenzene, 1,3,5-5.39 0.0539 -5.3E+01 2.1E-04
25167-70-8 Trimethylpentene, 2,4,4-1.02 0.0102 --
1330-20-7 Xylenes 90.5 0.905 -8.8E+01 2.1E-03
Cumulative: 3.9E-07 1.1E-01
DSCA Soil Gas Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-11
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 4878 146.34 --
107-13-1 Acrylonitrile 1023 30.69 4.1E-02 4.2E-01 7.4E-04 1.5E+01
71-43-2 Benzene 138 4.14 3.6E-01 6.3E+00 1.2E-05 1.3E-01
100-44-7 Benzyl Chloride 1467 44.01 5.7E-02 2.1E-01 7.7E-04 4.2E+01
75-15-0 Carbon Disulfide 70.1 2.103 -1.5E+02 2.9E-03
108-90-7 Chlorobenzene 99 2.97 -1.0E+01 5.7E-02
67-66-3 Chloroform 650 19.5 1.2E-01 2.0E+01 1.6E-04 1.9E-01
98-82-8 Cumene 2672 80.16 -8.3E+01 1.9E-01
110-82-7 Cyclohexane 18395 551.85 -1.3E+03 8.8E-02
75-35-4 Dichloroethylene, 1,1-1939 58.17 -4.2E+01 2.8E-01
156-59-2 Dichloroethylene, cis-1,2-157117 4713.51 -8.3E+00 1.1E+02
156-60-5 Dichloroethylene, trans-1,2-439 13.17 -8.3E+00 3.2E-01
78-87-5 Dichloropropane, 1,2-1476 44.28 7.6E-01 8.3E-01 5.8E-05 1.1E+01
111-77-3 Ethanol, 2-(2-methoxyethoxy)-37.5 1.125 --
100-41-4 Ethylbenzene 2178 65.34 1.1E+00 2.1E+02 5.8E-05 6.3E-02
142-82-5 Heptane, N-8701 261.03 -8.3E+01 6.3E-01
E5241997 Hexane, Commercial 15840 475.2 1.4E+01 1.3E+02 3.4E-05 7.6E-01
591-78-6 Hexanone, 2-19398 581.94 -6.3E+00 1.9E+01
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)1231 36.93 - 6.3E+02 1.2E-02
80-62-6 Methyl Methacrylate 35691 1070.73 -1.5E+02 1.5E+00
75-09-2 Methylene Chloride 119 3.57 1.0E+02 1.3E+02 3.5E-08 5.7E-03
103-65-1 Propyl benzene 5719 171.57 -2.1E+02 1.6E-01
115-07-1 Propylene 223 6.69 -6.3E+02 2.1E-03
79-34-5 Tetrachloroethane, 1,1,2,2-6154 184.62 4.8E-02 -3.8E-03
127-18-4 Tetrachloroethylene 1729266 51877.98 1.1E+01 8.3E+00 4.8E-03 1.2E+03
79-01-6 Trichloroethylene 233007 6990.21 4.8E-01 4.2E-01 1.5E-02 3.4E+03
95-63-6 Trimethylbenzene, 1,2,4-9101 273.03 -1.3E+01 4.4E+00
108-67-8 Trimethylbenzene, 1,3,5-2001 60.03 -1.3E+01 9.6E-01
25167-70-8 Trimethylpentene, 2,4,4-994 29.82 --
75-01-4 Vinyl Chloride 1072 32.16 1.7E-01 1.7E+01 1.9E-04 3.9E-01
1330-20-7 Xylenes 317 9.51 -2.1E+01 9.1E-02
Cumulative: 2.5E-02 4.8E+03
DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Name/Address of Sampling Location:Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, NC
Sampling Date:1/31/2024
Sample ID:SG-11
All concentrations are in ug/m3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level
for Carcinogens @
TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 4878 48.78 --
107-13-1 Acrylonitrile 1023 10.23 1.8E-01 1.8E+00 5.7E-05 1.2E+00
71-43-2 Benzene 138 1.38 1.6E+00 2.6E+01 8.8E-07 1.1E-02
100-44-7 Benzyl Chloride 1467 14.67 2.5E-01 8.8E-01 5.9E-05 3.3E+00
75-15-0 Carbon Disulfide 70.1 0.701 -6.1E+02 2.3E-04
108-90-7 Chlorobenzene 99 0.99 -4.4E+01 4.5E-03
67-66-3 Chloroform 650 6.5 5.3E-01 8.6E+01 1.2E-05 1.5E-02
98-82-8 Cumene 2672 26.72 -3.5E+02 1.5E-02
110-82-7 Cyclohexane 18395 183.95 -5.3E+03 7.0E-03
75-35-4 Dichloroethylene, 1,1-1939 19.39 -1.8E+02 2.2E-02
156-59-2 Dichloroethylene, cis-1,2-157117 1571.17 -3.5E+01 9.0E+00
156-60-5 Dichloroethylene, trans-1,2-439 4.39 -3.5E+01 2.5E-02
78-87-5 Dichloropropane, 1,2-1476 14.76 3.3E+00 3.5E+00 4.5E-06 8.4E-01
111-77-3 Ethanol, 2-(2-methoxyethoxy)-37.5 0.375 --
100-41-4 Ethylbenzene 2178 21.78 4.9E+00 8.8E+02 4.4E-06 5.0E-03
142-82-5 Heptane, N-8701 87.01 -3.5E+02 5.0E-02
E5241997 Hexane, Commercial 15840 158.4 6.1E+01 5.3E+02 2.6E-06 6.0E-02
591-78-6 Hexanone, 2-19398 193.98 -2.6E+01 1.5E+00
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)1231 12.31 - 2.6E+03 9.4E-04
80-62-6 Methyl Methacrylate 35691 356.91 -6.1E+02 1.2E-01
75-09-2 Methylene Chloride 119 1.19 1.2E+03 5.3E+02 9.7E-10 4.5E-04
103-65-1 Propyl benzene 5719 57.19 -8.8E+02 1.3E-02
115-07-1 Propylene 223 2.23 -2.6E+03 1.7E-04
79-34-5 Tetrachloroethane, 1,1,2,2-6154 61.54 2.1E-01 -2.9E-04
127-18-4 Tetrachloroethylene 1729266 17292.66 4.7E+01 3.5E+01 3.7E-04 9.9E+01
79-01-6 Trichloroethylene 233007 2330.07 3.0E+00 1.8E+00 7.8E-04 2.7E+02
95-63-6 Trimethylbenzene, 1,2,4-9101 91.01 -5.3E+01 3.5E-01
108-67-8 Trimethylbenzene, 1,3,5-2001 20.01 -5.3E+01 7.6E-02
25167-70-8 Trimethylpentene, 2,4,4-994 9.94 --
75-01-4 Vinyl Chloride 1072 10.72 2.8E+00 7.0E+01 3.8E-06 3.1E-02
1330-20-7 Xylenes 317 3.17 -8.8E+01 7.2E-03
Cumulative: 1.6E-03 3.8E+02
DSCA Soil Gas Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk
values are calculated for these chemicals.
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:2/9/2024
Sample ID:MW-1
Average Groundwater Temperature (°C):25 (Use default of 25⁰C unless site-specific data is available confirming the groundwater temperature during worst-case summer conditions.)
CAS # Chemical Name:
Groundwater
Concentration
(ug/L)
Henry's Constant
at 25°C
(dimensionless)
Temperature Adjusted Henry's
Constant
(dimensionless)
Henry's Constant used for
calculations
(dimensionless)
Calculated
Indoor Air
Concentration
(ug/m3)
Indoor Air Screening Level
for Carcinogens
@ TCR = 1E-06
Indoor Air Screening Level
for Non-
Carcinogens @ THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
71-43-2 Benzene 561 0.226901063 0.226901063 0.226901063 1.3E+02 3.6E-01 6.3E+00 3.5E-04 4.1E+00
92-87-5 Benzidine 3.96 2.11365E-09 2.11365E-09 2.11365E-09 8.4E-09 1.5E-05 -
135-98-8 Butylbenzene, sec-0.867 0.71954211 0.71954211 0.71954211 6.2E-01 --
98-06-6 Butylbenzene, tert-0.464 0.539656582 0.539656582 0.539656582 2.5E-01 --
98-82-8 Cumene 9.21 0.470155356 0.470155356 0.470155356 4.3E+00 -8.3E+01 1.0E-02
107-06-2 Dichloroethane, 1,2-3.22 0.048242028 0.048242028 0.048242028 1.6E-01 1.1E-01 1.5E+00 1.4E-06 2.1E-02
108-20-3 Diisopropyl Ether 10.4 0.10466067 0.10466067 0.10466067 1.1E+00 -1.5E+02 1.5E-03
7782-41-4 Fluorine (Soluble Fluoride)0.136 -2.7E+001634-04-4 Methyl tert-Butyl Ether (MTBE)11.4 0.023998365 0.023998365 0.023998365 2.7E-01 1.1E+01 6.3E+02 2.5E-08 8.7E-05
91-20-3 ~Naphthalene 14.7 0.017988553 0.017988553 0.017988553 2.6E-01 8.3E-02 6.3E-01 3.2E-06 8.5E-02
103-65-1 Propyl benzene 0.72 0.429272281 0.429272281 0.429272281 3.1E-01 -2.1E+02 3.0E-04
127-18-4 Tetrachloroethylene 1.6 0.723630417 0.723630417 0.723630417 1.2E+00 1.1E+01 8.3E+00 1.1E-07 2.8E-02108-88-3 Toluene 0.382 0.271463614 0.271463614 0.271463614 1.0E-01 -1.0E+03 2.0E-05
79-01-6 Trichloroethylene 0.214 0.402698283 0.402698283 0.402698283 8.6E-02 4.8E-01 4.2E-01 1.8E-07 4.1E-02
Cumulative: 3.6E-04 4.3E+00
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:2/9/2024
Sample ID:MW-1
Average Groundwater Temperature (°C):25 (Use default of 25⁰C unless site-specific data is available confirming the groundwater temperature during worst-case summer conditions.)
CAS # Chemical Name:
Groundwater
Concentration
(ug/L)
Henry's Constant
at 25°
(dimensionless)
Temperature
Adjusted Henry's Constant
(dimensionless)
Henry's Constant
used for calculations
(dimensionless)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level for Carcinogens
@ TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
71-43-2 Benzene 561 0.226901063 0.226901063 0.226901063 1.3E+02 1.6E+00 2.6E+01 8.1E-05 9.7E-01
92-87-5 Benzidine 3.96 2.11365E-09 2.11365E-09 2.11365E-09 8.4E-09 1.8E-04 -
135-98-8 Butylbenzene, sec-0.867 0.71954211 0.71954211 0.71954211 6.2E-01 --
98-06-6 Butylbenzene, tert-0.464 0.539656582 0.539656582 0.539656582 2.5E-01 --
98-82-8 Cumene 9.21 0.470155356 0.470155356 0.470155356 4.3E+00 -3.5E+02 2.5E-03107-06-2 Dichloroethane, 1,2-3.22 0.048242028 0.048242028 0.048242028 1.6E-01 4.7E-01 6.1E+00 3.3E-07 5.1E-03
108-20-3 Diisopropyl Ether 10.4 0.10466067 0.10466067 0.10466067 1.1E+00 -6.1E+02 3.6E-04
7782-41-4 Fluorine (Soluble Fluoride)0.136 -1.1E+01
1634-04-4 Methyl tert-Butyl Ether (MTBE)11.4 0.023998365 0.023998365 0.023998365 2.7E-01 4.7E+01 2.6E+03 5.8E-09 2.1E-05
91-20-3 ~Naphthalene 14.7 0.017988553 0.017988553 0.017988553 2.6E-01 3.6E-01 2.6E+00 7.3E-07 2.0E-02
103-65-1 Propyl benzene 0.72 0.429272281 0.429272281 0.429272281 3.1E-01 -8.8E+02 7.1E-05
127-18-4 Tetrachloroethylene 1.6 0.723630417 0.723630417 0.723630417 1.2E+00 4.7E+01 3.5E+01 2.5E-08 6.6E-03
108-88-3 Toluene 0.382 0.271463614 0.271463614 0.271463614 1.0E-01 -4.4E+03 4.7E-06
79-01-6 Trichloroethylene 0.214 0.402698283 0.402698283 0.402698283 8.6E-02 3.0E+00 1.8E+00 2.9E-08 9.8E-03
Cumulative: 8.2E-05 1.0E+00
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
DSCA Indoor Air Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:2/9/2024
Sample ID:MW-2
Average Groundwater Temperature (°C):25 (Use default of 25⁰C unless site-specific data is available confirming the groundwater temperature during worst-case summer conditions.)
CAS # Chemical Name:
Groundwater
Concentration
(ug/L)
Henry's Constant
at 25°C
(dimensionless)
Temperature Adjusted Henry's
Constant
(dimensionless)
Henry's Constant used for
calculations
(dimensionless)
Calculated
Indoor Air
Concentration
(ug/m3)
Indoor Air Screening Level
for Carcinogens
@ TCR = 1E-06
Indoor Air Screening Level
for Non-
Carcinogens @ THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 67.9 0.001430908 0.001430908 0.001430908 9.7E-02 --
71-43-2 Benzene 5700 0.226901063 0.226901063 0.226901063 1.3E+03 3.6E-01 6.3E+00 3.6E-03 4.1E+01
104-51-8 Butylbenzene, n-3.4 0.650040883 0.650040883 0.650040883 2.2E+00 --
135-98-8 Butylbenzene, sec-2.76 0.71954211 0.71954211 0.71954211 2.0E+00 --
98-06-6 Butylbenzene, tert-0.665 0.539656582 0.539656582 0.539656582 3.6E-01 --
108-90-7 Chlorobenzene 10.6 0.127146361 0.127146361 0.127146361 1.3E+00 -1.0E+01 2.6E-02
67-66-3 Chloroform 19.5 0.150040883 0.150040883 0.150040883 2.9E+00 1.2E-01 2.0E+01 2.4E-05 2.9E-02
98-82-8 Cumene 26.8 0.470155356 0.470155356 0.470155356 1.3E+01 -8.3E+01 3.0E-02106-46-7 Dichlorobenzene, 1,4-1.49 0.098528209 0.098528209 0.098528209 1.5E-01 2.6E-01 1.7E+02 5.8E-07 1.8E-04
107-06-2 Dichloroethane, 1,2-73.5 0.048242028 0.048242028 0.048242028 3.5E+00 1.1E-01 1.5E+00 3.3E-05 4.9E-01
156-59-2 Dichloroethylene, cis-1,2-3.61 0.166802944 0.166802944 0.166802944 6.0E-01 -8.3E+00 1.4E-02
78-87-5 Dichloropropane, 1,2-4.92 0.11529027 0.11529027 0.11529027 5.7E-01 7.6E-01 8.3E-01 7.5E-07 1.4E-01108-20-3 Diisopropyl Ether 301 0.10466067 0.10466067 0.10466067 3.2E+01 -1.5E+02 4.3E-02
100-41-4 Ethylbenzene 170 0.322158626 0.322158626 0.322158626 5.5E+01 1.1E+00 2.1E+02 4.9E-05 5.3E-02
78-93-3 Methyl Ethyl Ketone (2-Butanone)8.7 0.002326247 0.002326247 0.002326247 2.0E-02 -1.0E+03 3.9E-06
1634-04-4 Methyl tert-Butyl Ether (MTBE)4620 0.023998365 0.023998365 0.023998365 1.1E+02 1.1E+01 6.3E+02 1.0E-05 3.5E-0275-09-2 Methylene Chloride 2.32 0.132869992 0.132869992 0.132869992 3.1E-01 1.0E+02 1.3E+02 3.0E-09 4.9E-04
108-95-2 Phenol 11.7 1.36141E-05 1.36141E-05 1.36141E-05 1.6E-04 -4.2E+01
83-32-9 ~Acenaphthene 0.0937 0.007522486 0.007522486 0.007522486 7.0E-04 --
56-55-3 ~Benz[a]anthracene 0.214 0.000490597 0.000490597 0.000490597 1.0E-04 1.7E-02 -6.2E-09
50-32-8 ~Benzo[a]pyrene 0.12 1.86836E-05 1.86836E-05 1.86836E-05 2.2E-06 1.7E-03 4.2E-04205-99-2 ~Benzo[b]fluoranthene 0.191 2.68602E-05 2.68602E-05 2.68602E-05 5.1E-06 1.7E-02 -
207-08-9 ~Benzo[k]fluoranthene 0.265 2.38757E-05 2.38757E-05 2.38757E-05 6.3E-06 1.7E-01 -
218-01-9 ~Chrysene 0.217 0.000213818 0.000213818 0.000213818 4.6E-05 1.7E+00 -
53-70-3 ~Dibenz[a,h]anthracene 0.303 5.76451E-06 5.76451E-06 5.76451E-06 1.7E-06 1.7E-03 -206-44-0 ~Fluoranthene 0.105 0.000362224 0.000362224 0.000362224 3.8E-05 --
86-73-7 ~Fluorene 0.177 0.003932952 0.003932952 0.003932952 7.0E-04 --
91-20-3 ~Naphthalene 26.6 0.017988553 0.017988553 0.017988553 4.8E-01 8.3E-02 6.3E-01 5.8E-06 1.5E-01
103-65-1 Propyl benzene 36.8 0.429272281 0.429272281 0.429272281 1.6E+01 -2.1E+02 1.5E-02100-42-5 Styrene 3.87 0.112428455 0.112428455 0.112428455 4.4E-01 -2.1E+02 4.2E-04
108-88-3 Toluene 55.1 0.271463614 0.271463614 0.271463614 1.5E+01 -1.0E+03 2.9E-03
79-00-5 Trichloroethane, 1,1,2-1.44 0.033687653 0.033687653 0.033687653 4.9E-02 1.8E-01 4.2E-02 2.8E-07 2.3E-01
79-01-6 Trichloroethylene 4.35 0.402698283 0.402698283 0.402698283 1.8E+00 4.8E-01 4.2E-01 3.7E-06 8.4E-01526-73-8 Trimethylbenzene, 1,2,3-5.96 0.178250204 0.178250204 0.178250204 1.1E+00 -1.3E+01 1.7E-02
95-63-6 Trimethylbenzene, 1,2,4-98.3 0.251839738 0.251839738 0.251839738 2.5E+01 -1.3E+01 4.0E-01
108-67-8 Trimethylbenzene, 1,3,5-21.2 0.358544563 0.358544563 0.358544563 7.6E+00 -1.3E+01 1.2E-01
1330-20-7 Xylenes 129 0.271054783 0.271054783 0.271054783 3.5E+01 -2.1E+01 3.4E-01
Cumulative: 3.7E-03 4.4E+01
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:2/9/2024
Sample ID:MW-2
Average Groundwater Temperature (°C):25 (Use default of 25⁰C unless site-specific data is available confirming the groundwater temperature during worst-case summer conditions.)
CAS # Chemical Name:
Groundwater
Concentration
(ug/L)
Henry's Constant
at 25°
(dimensionless)
Temperature
Adjusted Henry's Constant
(dimensionless)
Henry's Constant
used for calculations
(dimensionless)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level for Carcinogens
@ TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 67.9 0.001430908 0.001430908 0.001430908 9.7E-02 --
71-43-2 Benzene 5700 0.226901063 0.226901063 0.226901063 1.3E+03 1.6E+00 2.6E+01 8.2E-04 9.8E+00
104-51-8 Butylbenzene, n-3.4 0.650040883 0.650040883 0.650040883 2.2E+00 --
135-98-8 Butylbenzene, sec-2.76 0.71954211 0.71954211 0.71954211 2.0E+00 --
98-06-6 Butylbenzene, tert-0.665 0.539656582 0.539656582 0.539656582 3.6E-01 --108-90-7 Chlorobenzene 10.6 0.127146361 0.127146361 0.127146361 1.3E+00 -4.4E+01 6.2E-03
67-66-3 Chloroform 19.5 0.150040883 0.150040883 0.150040883 2.9E+00 5.3E-01 8.6E+01 5.5E-06 6.8E-03
98-82-8 Cumene 26.8 0.470155356 0.470155356 0.470155356 1.3E+01 -3.5E+02 7.2E-03
106-46-7 Dichlorobenzene, 1,4-1.49 0.098528209 0.098528209 0.098528209 1.5E-01 1.1E+00 7.0E+02 1.3E-07 4.2E-05
107-06-2 Dichloroethane, 1,2-73.5 0.048242028 0.048242028 0.048242028 3.5E+00 4.7E-01 6.1E+00 7.5E-06 1.2E-01
156-59-2 Dichloroethylene, cis-1,2-3.61 0.166802944 0.166802944 0.166802944 6.0E-01 -3.5E+01 3.4E-03
78-87-5 Dichloropropane, 1,2-4.92 0.11529027 0.11529027 0.11529027 5.7E-01 3.3E+00 3.5E+00 1.7E-07 3.2E-02
108-20-3 Diisopropyl Ether 301 0.10466067 0.10466067 0.10466067 3.2E+01 -6.1E+02 1.0E-02
100-41-4 Ethylbenzene 170 0.322158626 0.322158626 0.322158626 5.5E+01 4.9E+00 8.8E+02 1.1E-05 1.3E-02
78-93-3 Methyl Ethyl Ketone (2-Butanone)8.7 0.002326247 0.002326247 0.002326247 2.0E-02 -4.4E+03 9.2E-07
1634-04-4 Methyl tert-Butyl Ether (MTBE)4620 0.023998365 0.023998365 0.023998365 1.1E+02 4.7E+01 2.6E+03 2.4E-06 8.4E-03
75-09-2 Methylene Chloride 2.32 0.132869992 0.132869992 0.132869992 3.1E-01 1.2E+03 5.3E+02 2.5E-10 1.2E-04
108-95-2 Phenol 11.7 1.36141E-05 1.36141E-05 1.36141E-05 1.6E-04 -1.8E+0283-32-9 ~Acenaphthene 0.0937 0.007522486 0.007522486 0.007522486 7.0E-04 --
56-55-3 ~Benz[a]anthracene 0.214 0.000490597 0.000490597 0.000490597 1.0E-04 2.0E-01 -5.1E-10
50-32-8 ~Benzo[a]pyrene 0.12 1.86836E-05 1.86836E-05 1.86836E-05 2.2E-06 2.0E-02 1.8E-03
205-99-2 ~Benzo[b]fluoranthene 0.191 2.68602E-05 2.68602E-05 2.68602E-05 5.1E-06 2.0E-01 -
207-08-9 ~Benzo[k]fluoranthene 0.265 2.38757E-05 2.38757E-05 2.38757E-05 6.3E-06 2.0E+00 -
218-01-9 ~Chrysene 0.217 0.000213818 0.000213818 0.000213818 4.6E-05 2.0E+01 -
53-70-3 ~Dibenz[a,h]anthracene 0.303 5.76451E-06 5.76451E-06 5.76451E-06 1.7E-06 2.0E-02 -
206-44-0 ~Fluoranthene 0.105 0.000362224 0.000362224 0.000362224 3.8E-05 --
86-73-7 ~Fluorene 0.177 0.003932952 0.003932952 0.003932952 7.0E-04 --
91-20-3 ~Naphthalene 26.6 0.017988553 0.017988553 0.017988553 4.8E-01 3.6E-01 2.6E+00 1.3E-06 3.6E-02
103-65-1 Propyl benzene 36.8 0.429272281 0.429272281 0.429272281 1.6E+01 -8.8E+02 3.6E-03
100-42-5 Styrene 3.87 0.112428455 0.112428455 0.112428455 4.4E-01 -8.8E+02 9.9E-05
108-88-3 Toluene 55.1 0.271463614 0.271463614 0.271463614 1.5E+01 -4.4E+03 6.8E-0479-00-5 Trichloroethane, 1,1,2-1.44 0.033687653 0.033687653 0.033687653 4.9E-02 7.7E-01 1.8E-01 6.3E-08 5.5E-02
79-01-6 Trichloroethylene 4.35 0.402698283 0.402698283 0.402698283 1.8E+00 3.0E+00 1.8E+00 5.9E-07 2.0E-01
526-73-8 Trimethylbenzene, 1,2,3-5.96 0.178250204 0.178250204 0.178250204 1.1E+00 -5.3E+01 4.0E-03
95-63-6 Trimethylbenzene, 1,2,4-98.3 0.251839738 0.251839738 0.251839738 2.5E+01 -5.3E+01 9.4E-02108-67-8 Trimethylbenzene, 1,3,5-21.2 0.358544563 0.358544563 0.358544563 7.6E+00 -5.3E+01 2.9E-02
1330-20-7 Xylenes 129 0.271054783 0.271054783 0.271054783 3.5E+01 -8.8E+01 8.0E-02
Cumulative: 8.5E-04 1.1E+01
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
DSCA Indoor Air Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:2/9/2024
Sample ID:MW-3
Average Groundwater Temperature (°C):25 (Use default of 25⁰C unless site-specific data is available confirming the groundwater temperature during worst-case summer conditions.)
CAS # Chemical Name:
Groundwater
Concentration
(ug/L)
Henry's Constant
at 25°C
(dimensionless)
Temperature Adjusted Henry's
Constant
(dimensionless)
Henry's Constant used for
calculations
(dimensionless)
Calculated
Indoor Air
Concentration
(ug/m3)
Indoor Air Screening Level
for Carcinogens
@ TCR = 1E-06
Indoor Air Screening Level
for Non-
Carcinogens @ THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 33.3 0.001430908 0.001430908 0.001430908 4.8E-02 --
71-43-2 Benzene 2.3 0.226901063 0.226901063 0.226901063 5.2E-01 3.6E-01 6.3E+00 1.4E-06 1.7E-02
Cumulative: 1.4E-06 1.7E-02
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:2/9/2024
Sample ID:MW-3
Average Groundwater Temperature (°C):25 (Use default of 25⁰C unless site-specific data is available confirming the groundwater temperature during worst-case summer conditions.)
CAS # Chemical Name:
Groundwater
Concentration
(ug/L)
Henry's Constant
at 25°
(dimensionless)
Temperature
Adjusted Henry's Constant
(dimensionless)
Henry's Constant
used for calculations
(dimensionless)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level for Carcinogens
@ TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 33.3 0.001430908 0.001430908 0.001430908 4.8E-02 --
71-43-2 Benzene 2.3 0.226901063 0.226901063 0.226901063 5.2E-01 1.6E+00 2.6E+01 3.3E-07 4.0E-03
Cumulative: 3.3E-07 4.0E-03
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
DSCA Indoor Air Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:2/9/2024
Sample ID:MW-4
Average Groundwater Temperature (°C):25 (Use default of 25⁰C unless site-specific data is available confirming the groundwater temperature during worst-case summer conditions.)
CAS # Chemical Name:
Groundwater
Concentration
(ug/L)
Henry's Constant
at 25°C
(dimensionless)
Temperature Adjusted Henry's
Constant
(dimensionless)
Henry's Constant used for
calculations
(dimensionless)
Calculated
Indoor Air
Concentration
(ug/m3)
Indoor Air Screening Level
for Carcinogens
@ TCR = 1E-06
Indoor Air Screening Level
for Non-
Carcinogens @ THQ = 0.2
Calculated
Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 17 0.001430908 0.001430908 0.001430908 2.4E-02 --
71-43-2 Benzene 17.1 0.226901063 0.226901063 0.226901063 3.9E+00 3.6E-01 6.3E+00 1.1E-05 1.2E-01
135-98-8 Butylbenzene, sec-0.41 0.71954211 0.71954211 0.71954211 3.0E-01 --
98-06-6 Butylbenzene, tert-0.219 0.539656582 0.539656582 0.539656582 1.2E-01 --
98-82-8 Cumene 0.431 0.470155356 0.470155356 0.470155356 2.0E-01 -8.3E+01 4.9E-04
75-35-4 Dichloroethylene, 1,1-0.27 1.067048242 1.067048242 1.067048242 2.9E-01 -4.2E+01 1.4E-03
156-59-2 Dichloroethylene, cis-1,2-351 0.166802944 0.166802944 0.166802944 5.9E+01 -8.3E+00 1.4E+00
156-60-5 Dichloroethylene, trans-1,2-15.6 0.383483238 0.383483238 0.383483238 6.0E+00 -8.3E+00 1.4E-01108-20-3 Diisopropyl Ether 0.244 0.10466067 0.10466067 0.10466067 2.6E-02 -1.5E+02 3.5E-05
100-41-4 Ethylbenzene 0.929 0.322158626 0.322158626 0.322158626 3.0E-01 1.1E+00 2.1E+02 2.7E-07 2.9E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)2.68 0.002326247 0.002326247 0.002326247 6.2E-03 -1.0E+03 1.2E-06
1634-04-4 Methyl tert-Butyl Ether (MTBE)1.37 0.023998365 0.023998365 0.023998365 3.3E-02 1.1E+01 6.3E+02 3.0E-09 1.1E-05103-65-1 Propyl benzene 0.362 0.429272281 0.429272281 0.429272281 1.6E-01 -2.1E+02 1.5E-04
127-18-4 Tetrachloroethylene 63.3 0.723630417 0.723630417 0.723630417 4.6E+01 1.1E+01 8.3E+00 4.2E-06 1.1E+00
108-88-3 Toluene 0.413 0.271463614 0.271463614 0.271463614 1.1E-01 -1.0E+03 2.2E-05
79-01-6 Trichloroethylene 52.6 0.402698283 0.402698283 0.402698283 2.1E+01 4.8E-01 4.2E-01 4.4E-05 1.0E+01526-73-8 Trimethylbenzene, 1,2,3-1.21 0.178250204 0.178250204 0.178250204 2.2E-01 -1.3E+01 3.4E-03
95-63-6 Trimethylbenzene, 1,2,4-2.92 0.251839738 0.251839738 0.251839738 7.4E-01 -1.3E+01 1.2E-02
108-67-8 Trimethylbenzene, 1,3,5-0.812 0.358544563 0.358544563 0.358544563 2.9E-01 -1.3E+01 4.7E-03
75-01-4 Vinyl Chloride 1.15 1.136549469 1.136549469 1.136549469 1.3E+00 1.7E-01 1.7E+01 7.8E-06 1.6E-021330-20-7 Xylenes 0.963 0.271054783 0.271054783 0.271054783 2.6E-01 -2.1E+01 2.5E-03
Cumulative: 6.7E-05 1.3E+01
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident
Version 11, July 2023
DC410064
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
DSCA ID No:
Name/Address of DSCA Site:
Name/Address of Sampling Location:
Sampling Date:2/9/2024
Sample ID:MW-4
Average Groundwater Temperature (°C):25 (Use default of 25⁰C unless site-specific data is available confirming the groundwater temperature during worst-case summer conditions.)
CAS # Chemical Name:
Groundwater
Concentration
(ug/L)
Henry's Constant
at 25°
(dimensionless)
Temperature
Adjusted Henry's Constant
(dimensionless)
Henry's Constant
used for calculations
(dimensionless)
Calculated Indoor
Air Concentration
(ug/m3)
Indoor Air
Screening Level for Carcinogens
@ TCR = 1E-06
Indoor Air
Screening Level
for Non-
Carcinogens @
THQ = 0.2
Calculated Carcinogenic Risk
Calculated Non-
Carcinogenic
Hazard Quotient
67-64-1 Acetone 17 0.001430908 0.001430908 0.001430908 2.4E-02 --
71-43-2 Benzene 17.1 0.226901063 0.226901063 0.226901063 3.9E+00 1.6E+00 2.6E+01 2.5E-06 3.0E-02
135-98-8 Butylbenzene, sec-0.41 0.71954211 0.71954211 0.71954211 3.0E-01 --
98-06-6 Butylbenzene, tert-0.219 0.539656582 0.539656582 0.539656582 1.2E-01 --
98-82-8 Cumene 0.431 0.470155356 0.470155356 0.470155356 2.0E-01 -3.5E+02 1.2E-0475-35-4 Dichloroethylene, 1,1-0.27 1.067048242 1.067048242 1.067048242 2.9E-01 -1.8E+02 3.3E-04
156-59-2 Dichloroethylene, cis-1,2-351 0.166802944 0.166802944 0.166802944 5.9E+01 -3.5E+01 3.3E-01
156-60-5 Dichloroethylene, trans-1,2-15.6 0.383483238 0.383483238 0.383483238 6.0E+00 -3.5E+01 3.4E-02
108-20-3 Diisopropyl Ether 0.244 0.10466067 0.10466067 0.10466067 2.6E-02 -6.1E+02 8.3E-06
100-41-4 Ethylbenzene 0.929 0.322158626 0.322158626 0.322158626 3.0E-01 4.9E+00 8.8E+02 6.1E-08 6.8E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)2.68 0.002326247 0.002326247 0.002326247 6.2E-03 -4.4E+03 2.8E-07
1634-04-4 Methyl tert-Butyl Ether (MTBE)1.37 0.023998365 0.023998365 0.023998365 3.3E-02 4.7E+01 2.6E+03 7.0E-10 2.5E-06
103-65-1 Propyl benzene 0.362 0.429272281 0.429272281 0.429272281 1.6E-01 -8.8E+02 3.5E-05
127-18-4 Tetrachloroethylene 63.3 0.723630417 0.723630417 0.723630417 4.6E+01 4.7E+01 3.5E+01 9.7E-07 2.6E-01
108-88-3 Toluene 0.413 0.271463614 0.271463614 0.271463614 1.1E-01 -4.4E+03 5.1E-06
79-01-6 Trichloroethylene 52.6 0.402698283 0.402698283 0.402698283 2.1E+01 3.0E+00 1.8E+00 7.1E-06 2.4E+00
526-73-8 Trimethylbenzene, 1,2,3-1.21 0.178250204 0.178250204 0.178250204 2.2E-01 -5.3E+01 8.2E-04
95-63-6 Trimethylbenzene, 1,2,4-2.92 0.251839738 0.251839738 0.251839738 7.4E-01 -5.3E+01 2.8E-03108-67-8 Trimethylbenzene, 1,3,5-0.812 0.358544563 0.358544563 0.358544563 2.9E-01 -5.3E+01 1.1E-03
75-01-4 Vinyl Chloride 1.15 1.136549469 1.136549469 1.136549469 1.3E+00 2.8E+00 7.0E+01 4.7E-07 3.7E-03
1330-20-7 Xylenes 0.963 0.271054783 0.271054783 0.271054783 2.6E-01 -8.8E+01 6.0E-04
Cumulative: 1.1E-05 3.1E+00
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
DSCA Indoor Air Risk Calculator - Cumulative Risk for Non-Residential Worker
Version 11, July 2023
DC410064
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
Frye & Webster Cleaners/608 Elwell Avenue, Greensboro, North Carolina
Appendix G
Photographic Log
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
1/29/2024
Direction:
Southeast
Description:
Subject Property, 608 and 606
Elwell Avenue
Photolog, Photo No.1
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
1/30/2024
Direction:
South
Description:
Back of 608 Elwell Avenue dry-
cleaner facility
Photolog, Photo No.2
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
1/31/2024
Direction:
East
Description:
Area between 608 Elwell Ave
and adjacent 610 Elwell Ave
Photolog, Photo No.3
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
1/31/2024
Direction:
West
Description:
Inside of vacant 606 Elwell
Avenue building area; SG-10
sample location in foreground.
Photolog, Photo No.4
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
3/15/2024
Direction:
North
Description:
SG-11 location. Fire door
between 608 and 606 Elwell
Avenue form 606 side; unlabeled
drum removed by dry-cleaner
operator in May 2024.
Photolog, Photo No.5
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
3/15/2024
Direction:
East
Description:
Interior of dry-cleaning facility;
SB-4/SG-2 sample location in
foreground
Photolog, Photo No.6
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
3/15/2024
Direction:
South
Description:
Fire door between 608 and 606
Elwell Avenue from 608 side
(behind tool wall); SG-1/SB-3
sample location in foreground
Photolog, Photo No.7
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
1/30/2024
Direction:
South
Description:
MW-1 installation at northwest
corner of property
Photolog, Photo No.8
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
1/30/2024
Direction:
South
Description:
MW-2 installation on southwest
corner of property
Photolog, Photo No.9
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
1/30/2024
Direction:
South
Description:
MW-3 installation on southeast
corner of property
Photolog, Photo No.10
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
2/1/2024
Direction:
North
Description:
MW-4 and SG-4/SB-7 sample
location on northeast corner of
property
Photolog, Photo No.11
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
1/30/2024
Direction:
Northeast
Description:
Back wall of dry-cleaning
facility
Photolog, Photo No.12
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
3/15/2024
Direction:
West
Description:
Chemical storage area of dry-
cleaning facility
Photolog, Photo No.13
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
3/15/2024
Direction:
Northwest
Description:
Additional chemical storage
within dry-cleaning facility
Photolog, Photo No.14
DSCA Site DC410064
Frye & Webster
Cleaners
Date of Photograph:
3/15/2024
Direction:
South
Description:
Additional chemical storage
within dry-cleaning facility
Photolog, Photo No.15
Appendix H
Waste Manifest