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MO-7639_36272_CA_IAR_20070526_Inital Abatement Action Report
INTIAL ABATEMENT ACTION REPORT (Revision 2) FOR�ai� CROWELL PROPERTY 7901 North Tryon Street rz"� Charlotte, Mecklenburg County, North Carolina Facility I.D. Number: N/A {pr Incident Number: 36272 f .;,,� : ; , °X?'1cc Risk Classification: Unknown Latitude: 35° 17' 43.64" North Longitude: 80° 45' 18.74" West May 26, 2007 Prepared For: Mr. Ken Raznick C/o University Center, LLC 32255 Northwestern Highway Farmington Hills, Michigan 88334 (248)865-5063 UST OWNER/OPERATOR/PROPERTY OWNER Mr. Brevard B. Crowell (Property Owner) 6864 Baltusrol Lane Charlotte, North Carolina 28210 (704)553-6097 CONSULTANT EnviroAssessments, PLLC 9307 Monroe Rd., Suite K Charlotte, North Carolina 28270 (704)846-8853 EA Project No. 07-6797.1 RELEASE INFORMATION On June 28, 2006, a release was discovered at the site during a Phase II Environmental Site Assessment, during which soil samples were collected around one 550-gallon residential heating oil tank located at the Project. The release is the result of past discharges from holes observed in the tank bottom during the subsequent tank removal on November 27, 2006. The estimated quantity of the release is unknown. Jeremy Odom Senior Project Manager Gary K. Sawyer, P.G. Principal/Licensed Geologist Initial Abatement Action Report — Revision 2 Crowell Property 7901 North Tryon Street, Charlotte, North Carolina Incident Number: 36272 EA Project No. 07-6797.1 May 26, 2007 A. Site Information 1. Site Identification Date of Report: May 10, 2007 Facility ID#: N/A UST Incident#: 36272 Site Name: Crowell Property Site Street Address: 7901 North Tryon Street Nearest City/Town: Charlotte Zip Code: 28262 County: Mecklenburg Latitude: 35' 17' 43.64" North Longitude: 80° 45' 18.74" West 2. Contact Information UST Owner: Unknown UST Operator: Unknown Property Owner: Mr. Brevard B. Crowell Address: 6864 Baltusrol Lane Phone: 704-553-6097 Charlotte, North Carolina 28210 Property Occupant: Vacant Consultant/Contractor: EnviroAssessments, PLLC Address: 9307 Monroe Road, Suite K, Charlotte, North Carolina 28270 Analytical Laboratory: Test America Address: Queen City Drive, Carolina Business Center, Building 2838, Suite B Charlotte, North Carolina 28208 State Certification Number: 387 Phone: 877-855-0885 3. Release Information Date Discovered: June 28, 2006 Estimated Ouantity of Release: Unknown Cause of Release: Holes in bottom of UST Source of Release: Heating oil UST Size and Contents of UST System(s) from which the release occurred: 550-gallon heating oil UST 1 Initial Abatement Action Report — Revision 2 Crowell Property 7901 North Tryon Street, Charlotte, North Carolina Incident Number: 36272 EA Project No. 07-6797.1 May 26, 2007 I, GM K. Sawver, a Licensed Geologist for EnviroAssessments, PLLC, do certify that the information contained in this report is correct and accurate to the best of my knowledge. Gary K. Sawyer, P.G. Principal/Licensed Geologist EnviroAssessments, PLLC is licensed to practice Geology in North Carolina. The certification number of the company is C-385. Initial Abatement Action Report — Revision 2 Crowell Property 7901 North Tryon Street, Charlotte, North Carolina Incident Number: 36272 EA Project No. 07-6797.1 May 26, 2007 B. Site History and Characterization The UST system is as follows: US'pl#1 ?a.Vgduct Capacity Date Installed ; Date, Removed or _ Was. Release (gallons) Closed Assoc, with UST S stem 1 Heating Oil 550 Unknown November 27, Yes 2006 The UST Owner/Operator information is as follows: UST Name of Dates of Owner or Address Telephone ID# Owner/ Ownership/ Operator Number O erator Operation 1 Property Unknown- Property 6864 Baltusrol Lane 704-553- Owner - 2006 Owner Charlotte, NC 28210 6097 Brevard B. Crowell On June 28, 2006, representatives of S&ME collected three soil samples from areas surrounding a 550- gallon heating oil underground storage tank (UST) located at 7901 North Tryon Street, Charlotte, Mecklenburg County, North Carolina. A Site Location Map is attached as Figure 1. A hand auger was used to collect the samples from depths ranging from 5 to 7 feet below grade (BG). Laboratory analysis of the soil samples for Total Petroleum Hydrocarbons — Diesel Range Organics (TPH-DRO) confirmed that a release had occurred. Based on an interview with the property owner, the subject UST has not been in use since the mid- 1980s. The property is located in the northeastern part of Charlotte, North Carolina. The surrounding properties are primarily commercial in nature. North Tryon Street fronts the subject Property to the east. A water supply well was observed on the subject property; it is unknown whether this well was most recently used for irrigation or drinking water purposes. Municipal water and sewer are available in the site area. The subject property is expected to be re -developed as a shopping center. C. Site Check Report Section C is not applicable to this Initial Abatement Action Report. Initial Abatement Action Report — Revision 2 4 Crowell Property 7901 North Tryon Street, Charlotte, North Carolina Incident Number: 36272 EA Project No. 07-6797.1 May 26, 2007 D. UST Closure Report On November 27, 2006, EA and its subcontractors excavated and removed the heating oil underground storage tank (UST) that was located near the former on -site house. During the UST excavation activities, heating oil odors and stains were noted in soil in the bottom and sidewalls of the UST excavation. EA and its subcontractor, ICES -Carolinas, Inc. (ICES) removed the 550-gallon heating oil UST from the site. The UST was located adjacent to the west side of the residence. The soil above and around the UST was excavated using a mini excavator. The top of the UST was situated at approximately 3 feet BG. The UST was 3.8 feet in diameter and 6.2 feet in length. The UST was removed from the excavation and transported to Morris Scrap Metal in Kings Mountain, North Carolina for disposal. A disposal manifest for the tank is included as Appendix 1. The UST was of steel construction and several holes were observed in the bottom and lower half of the tank. The copper product and return lines servicing the tank were disconnected, purged and crimped. The Site Investigation Report for Permanent Closure or Change - In -Service of UST (UST-12 Form) is attached as Appendix 2. The soil around the UST consisted of red silty clay transitioning to tan clayey silt. Visible staining and petroleum odor were noted in the soil at the base of the UST and below; EA authorized ICES to continue to excavate soil exhibiting staining and petroleum odors from the former tank basin. On April 9, 2007, EA personnel collected one composited soil sample (identified as Stockpile) from the stockpiled soil that had been excavated from the UST pit. The sample was placed into a proper container, labeled and shipped to Test America in Charlotte, North Carolina (a North Carolina certified laboratory). The soil sample was submitted for laboratory analysis for Diesel Range Organics (DRO) for total petroleum hydrocarbons (TPH) by EPA Method 3550. DRO was detected in the Stockpile sample at a concentration of 9,800 mg/kg, which exceeds the regulatory reportable limit of 10 mg/kg set forth by the North Carolina Department of Environment and Natural Resources (NCDENR). A copy of the stockpile soil sample laboratory analytical report is attached as Appendix 3. On April 19, 2007, notice of the release was provided verbally and by written form (24-Hour Release Notice) to the NCDENR by EnviroAssessments, PLLC (EA). No groundwater was encountered in the excavation, and groundwater was not sampled during the excavation activities. As authorized by the Client, EA continued to excavate contaminated soil from the UST basin. Specifics related to the soil excavation activities are discussed in detail Section H of this report. E. Free Product Investigation and Recovery Report Section E is not applicable to this Initial Abatement Action Report. Initial Abatement Action Report — Revision 2 Crowell Property 7901 North Tryon Street, Charlotte, North Carolina Incident Number: 36272 EA Project No. 07-6797.1 May 26, 2007 F. Groundwater and Surface Water Investigation Section F is not applicable to this Initial Abatement Action Report. No groundwater was encountered in the excavation, and no groundwater or surface water was sampled during the investigation. G. Initial Response and Abatement Action On June 28, 2006, as part of a Phase II ESA, representatives of S&ME collected three soil samples from areas surrounding the 550-gallon heating oil UST. A hand auger was used to collect the samples from depths ranging from 5 to 7 feet below grade (BG). Laboratory analysis of the soil samples for Total Petroleum Hydrocarbons — Diesel Range Organics (TPH-DRO) confirmed that a release had occurred. The results of S&ME's initial investigation are summarized in S&ME's Phase II Environmental Site Assessment dated June 2006. On November 27, 2006, EA and its subcontractors excavated and removed the heating oil underground storage tank (UST) that was located near the former on -site house. During the UST excavation activities, heating oil odors and stains were noted in soil in the bottom and sidewalls of the UST excavation. EA and its subcontractors excavated and removed the 550-gallon heating oil UST and excavated and removed a total of approximately 884.48 tons of petroleum -contaminated soil. The UST and soil were properly disposed off -site, and the resultant excavation pit was backfilled and compacted. Confirmation soil samples were collected from the sidewalls and bottom of the excavation pit. Only one soil sample exhibited any detectable concentrations of the target analytes. Soil sample S-1 revealed an Acetone concentration of 12.3 mg/kg, which exceeds its respective Soil -to -Water Maximum Soil Contaminant Concentration (MSCC) of 3 mg/kg. The Acetone concentration is well below the Residential MSCC of 1564 mg/kg. Acetone is a naturally -occurring compound that is produced as a by-product of the degradation of naturally -occurring organic compounds. Acetone is also a common laboratory -introduced contaminant associated with the EPA 8260B Test Method. Its presence in sample S-I at the relatively low level and in the absence of other related compounds is not considered to be a significant environmental concern with regard to the Project incident. None of the target analytes were detected in any of the other confirmation soil samples. No groundwater was encountered in the excavation, and groundwater was not sampled during the excavation activities. H. Excavation of Contaminated Soil The source of contamination is a 550-gallon underground heating oil storage tank (UST) formerly located at 7901 North Tryon Street, Charlotte, Mecklenburg County, North Carolina. Laboratory analysis of soil samples collected by S&ME around the former UST in June 2006 confirmed that a release had occurred. Initial Abatement Action Report — Revision 2 Crowell Property 7901 North Tryon Street, Charlotte, North Carolina Incident Number: 36272 EA Project No. 07-6797.1 May 26, 2007 Gl On November 27, 2006, EA and its subcontractor, ICES -Carolinas, Inc. (ICES) removed the 550-gallon heating oil UST from the site. The UST was located adjacent to the west side of the residence. The soil above and around the UST was excavated using a mini excavator. The soil around the UST consisted of red silty clay transitioning to tan clayey silt. Visible staining and petroleum odor were noted in the soil at the base of the UST and below; EA authorized ICES to continue to excavate soil exhibiting staining and petroleum odors from the former tank basin. The excavation was extended laterally to the north and south approximately 11 feet and to the east (away from the house) approximately 10 feet. The lateral extent to the east was limited due to the close proximity to the house. The vertical depth of the excavation at that time was 12 feet BG. The excavation location is presented on the attached Figure 2. Due to the proximity of the house to the excavation area and in order to allow time for re-evaluation of the incident by the subject property seller and prospective purchaser, excavation activities were discontinued in December 2006 until April 2007. At the time, EA had removed approximately 85.37 tons of petroleum -contaminated soil. The impacted soil was transported to Environmental Soils, Inc. in Lattimore, North Carolina for treatment and disposal. Waste disposal manifests are included as Appendix 4. In March 2007, EA personnel razed the house structure and removed the resultant debris from the UST basin area for proper off -site disposal. In April 2007, EA and its subcontractor resumed soil excavation activities. Between April 9, 2007 and April 17, 2007, EA and its subcontractor continued to excavate soil exhibiting staining and petroleum odors from the tank basin, resulting in the removal of an additional 798.11 tons of petroleum - contaminated soil from the UST basin. The impacted soil was transported to Environmental Soils, Inc. in Lattimore, North Carolina for treatment and disposal. Waste disposal manifests are included as Appendix 4. The dimensions of the UST excavation pit measured approximately 40 feet long, 26 feet wide and 23 feet deep. No groundwater or bedrock was encountered in the excavation pit. EA personnel collected confirmation soil samples from the UST excavation basin on April 17, 2007. A total of five samples (S-1 through S-5) were collected from the four sidewalls and the bottom of the excavation. The soil samples were grab samples collected from the bucket of the excavator. Sidewall samples (S-1 through S-4) were collected from an approximate depth of 12 feet BG and the bottom sample (S-5) was collected from a depth of 23 feet BG. EA personnel screened each soil sample for volatile organic vapors using a photo ionization detector (PID). The PID revealed no detectable levels of organic vapors in any of the soil samples. The soil sample locations are depicted on the attached Figure 2. The soil samples were placed into proper containers, labeled and shipped to Test America in Charlotte, North Carolina on April 17, 2007. Test America received the samples on April 18, 2007. The soil samples were submitted for analysis for volatile organic compounds by EPA Method 8260 with IPE and MTBE, semi -volatile organic compounds by EPA Method 8270, MADEP volatile petroleum hydrocarbons (VPH) and MADEP extractable petroleum hydrocarbons (EPH). Initial Abatement Action Report — Revision 2 Crowell Property 7901 North Tryon Street, Charlotte, North Carolina Incident Number: 36272 EA Project No. 07-6797.1 May 26, 2007 7 A copy of the laboratory analytical report for the bottom and sidewall samples is included as Appendix 5. Table 1 presents a summary of the target analytes detected in the soil samples. The only soil sample that exhibited any detectable concentrations of the target analytes was soil sample S-1. The analysis of S-1 revealed an Acetone concentration of 12.3 mg/kg, which exceeds its respective Soil -to -Water Maximum Soil Contaminant Concentration (MSCC) of 3 mg/kg. The Acetone concentration is well below the Residential MSCC of 1564 mg/kg. Acetone is a naturally -occurring compound that is produced as a by- product of the degradation of naturally -occurring organic compounds. Acetone is also a common laboratory -introduced contaminant associated with the EPA 8260B Test Method. Its presence in sample S-1 at the relatively low level and in the absence of other related compounds is not considered to be a significant environmental concern with regard to the Project incident. None of the target analytes were detected in any of the other confirmation soil samples. No groundwater was encountered in the excavation, and groundwater was not sampled during the excavation activities. On April 25 and 26, 2007, ICES personnel backfilled the excavation. The bottom of the excavation was filled with No. 57 wash stone to a thickness of approximately 2 feet. The stone was overlain by a NCDOT-approved geo-textile fabric Mirifi 500X. The remainder of the excavation was backfilled with clean overburden soils and fill imported from a local quarry. The soil lifts were compacted with a mechanical tamper. Soil compaction was confirmed using field density tests compared to Standard Proctor Tests. Supporting documentation regarding the Proctor tests was not available to EA as of the submittal date of this report and will be forwarded to the Client upon EA's receipt. I. Conclusions Considering the findings of this investigation, on behalf of University Center, LLC, EA requests that the Department issue a notice of no further action under NCAC 2L .0115(h). Considering that acetone was reported in only one of the five confirmation samples and is a common laboratory contaminant, we believe that a Notice of Residual Petroleum should not be required. FIGURES .. AA. 6k TA 41 �V J!j We Al 4a� N. 4.n All + 0 Lli TABLES APPENDIX 1 APPENDIX 2 T=2 Site Investigation Report for Permanent Closure or Change -in -Service of UST Return completed form to: STATE USE ONLY: The DWM Regional Office located in the area where the facility is located. Send a copy to the Central Office in Raleigh so that I,D. # the status of the tank may be changed to "PERMANENTLY CLOSED" and your tank fee account can be closed out. SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES. Date Received INSTRUCTIONS READ THIS FIRST For more than five UST systems you may attach additional forms as needed. Permanent closure — For permanent closure, complete all sections of this form. Chanae-in-service — For change -in-service where UST systems will be converted from containing a regulated substance to storing a non -regulated substance, complete sections I, Il, III, IV, and VIII Effective February 1, 1995, all UST closure/change-in-service reports must be submitted in the format provided in the UST-12 form. UST closure and change -in -services must be completed in accordance with the latest version of the Guidelines for Tank Closure. A copy of the UST-12 form and the Guidelines for Tank Closure can be obtained at www.wastenotnc.org, You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you could be held responsible for the cleanup of any environmental damage that occurs. NOTE: If a release from the tank(s) has occurred, the site assessment portion of the tank closure must be conducted under the supervision of a P.E. or L.G., with all closure site assessment reports bearing the signature and seal of the P.E. or L.G. ' r» S IP Q : i : K if. LOCATION, F K$ ° . Owner Name (Corporation, Individual, Public Agency, or Other Entity) Facility Name or Company Brevard B. Crowell Street Address Facility ID # (If known) 6864 Baltusrol Lane City County Street Address Charlotte Mecklenburg 7901 N. Trvon Street State Zip Code City County Zip Code NC 28210 Charlotte Mecklenburg 28262 Phone Number Phone Number Ill. CONTACT PERSONNEL Contact for Facility: Job Title: Phone. No: Closure Contractor Name: Closure Contractor Company: Address: Phone. No: Tim Morgan ICES -Carolinas Inc. PO Box 66, Kings Mountain, NC 28086 704.734.0736 Primary Consultant Name: Primary Consultant Company: Address: Phone. No: Amanda Petoskey Enviroassssments, PLLC 9307 Monroe Rd. Ste K Charlotte,NC 704.846.8853 IV. UST INFORMATION FOR'REGISTERED UST SYSTEMS V. -EXCAVATION COND.rr101 Tank Size in Tank Last Last Use Permanent Change -in- water in Free Notable odor or visible ID No. Gallons Dimensions Contents Date Close Date Service excavator PrOoduct soil contamination Yes No Yes No Yes No Date ❑ ❑ ❑ ❑ ❑ 1 ❑ ❑ ❑ ❑ ❑ ❑ ❑ D ❑ ❑ ❑ ❑ ❑ ❑ ❑ V1. UST INFORMATION FOR UNREGISTERED UST SYSTEMS VII. EXCAVATION CONDITION Tank Size in Tank Last Last Use Permanent Tank Owner Water in Free Notable odor or visible ID No. Gallons Dimensions Contents Date Close Date Name * excavation product soil contamination Yes No Yes No Yes No 1 550 6.2 x 3.8 Heating Oil unk 11/27/06 ❑ ❑ ❑ ❑ ❑ ❑ * If the tank owner address is different from the one listed in Section I., then enter the street address, city, state, zip code and telephone no. below: Vlll. CERTIFICATION I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and complete. Print name and official title of owner or owner's authorized representative Signature Date Signed Amanda Petoskey (Staff Geologist) UST-2 Rev 11/2006 d p o o o - C �aic�rnY � 3 d Qi N r . U rnrn 3� 3 E Va. i� LL C M O sz�rn aim — M ui A OfamAle • �gQ€iz 3 c H C L ti M cn. W a y Durham W V NV �'C2 rc? C1 Ora w C r 0 00 (0 2 N M,� G w C AlamaIlCB V �i i�1 ego ti N a�CL Z� n' • a: po N 00 3 g R Z r Co 00 m • _ r O ~ CD N M �> IZ...Np ne+�i� c p R eLp O z y o�r� V�� T • Meld U s -C I OM g C = Sao p �rn c"c7�cfaLL Lnco 3 0*�Ill I r( 10 p0�00 0P'-r-1nM C \ = �4L dtUrnr; g d= OpN� h N�N E E 41� C Qj co s0 cm QNcndL ; s N f.1 O q*_ C Q. 'arm? eoi Me� r- CiN O �m m asi�o ri ii a LL 4v o N !E9 O aco am O 2,tL'rn aaNCW)C U-:� co ev y•y v0 Ow N !CO$O `'CG�aILL II co 0 APPENDIX 3 April 18, 2007 10:52:20AM Client: EnviroAssessments (2165) 9307 Monroe Road, Suite K Charlotte, NC 28270 Attn: Amanda Simpson -Petoskey SAMPLE IDENTIFICATION Stockpile 2960 Foster Creighton Road Nashville, TN 37204. 800-765- M80 • Fax 615-726-3404 Work Order: NQD1221 Project Name: EnviroAssessments (NC) Project Nbr: 07-6797.1/7901 N.Tyron Street P/O Nbr: Date Received: 04/11/07 LAB NUMBER COLLECTION DATE AND TIME NQD1221-01 04/09/07 09:15 An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at 1-800-765-0980. Any opinions, if expressed, are outside the scope of the Laboratory's accreditation. This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is privileged and confidential. If you are not the intended recipient, or the employee or agent responsible for delivering this material to the intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you have received this material in error, please notify us immediately at 615-726-0177. North Carolina Certification Number: 387 The Chain(s) of Custody, 2 pages, are included and are an integral part of this report. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Estimated uncertainity is available upon request. This report has been electronically signed. Report Approved By: Roxanne Connor Program Manager - Conventional Accounts Page 1 of 7 Client EnviroAssessments (2165) 9307 Monroe Road, Suite K Charlotte, NC 28270 Ann Amanda Simpson -Petoskey 2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980' Fax 615-726-3404 Work Order: NQD1221 Project Name: EnviroAssessments (NC) Project Number: 07-6797.1/7901 N.Tyron Street Received: 04/11/07 08:40 ANALYTICAL REPORT Dilution Analysis Analyte Result Flag Units ---------I------------------------------------------------------------------------------- MRL Factor ------------------------------ Date/Time Method ----------------------- Batch Sample ID: NQD1221-01(Stockpile - Soil) Sampled: 04/09/07 09:15 General Chemistry Parameters % Dry Solids 83.9 % 0,500 1 04/17/07 08:15 SW-846 7042545 Extractable Petroleum Hydrocarbons Diesel 9800 mg/kg dry 586 100 04/13/07 10:45 SW846 8015B 7042155 Surr. o-Terphenyl (32-132%) ' Z3 04/13/0710. 45 SW846 8015E 7042155 Page 2 of 7 Client EnviroAssessments (2165) 9307 Monroe Road, Suite K Charlotte, NC 28270 Attu Amanda Simpson -Petoskey 29W Foster Creighton Road Nashville, TN 37204 . WO-765.09W * Fax 615-726-3404 Work Order: NQD1221 Project Name: EnviroAssessments (NC) Project Number: 07-6797.1 /7901 N.Tyron Street Received: 04/11/07 08:40 SAMPLE EXTRACTION DATA WtNol Extraction Parameter -------------------------------------------------- Batch Lab Number --------------------------------------------------------------------------- Extracted Extracted Vol Date Analyst Method ------------------ Extractable Petroleum Hydrocarbons SW846 8015B 7042155 NQD1221-01 25.44 1.00 04/12/07 07:05 BJM EPA 3550B SW846 8015B 7042155 NQD1221-OIREI 25.44 1.00 04/12/07 07:05 BJM EPA 3550B SW846 8015B 7042155 NQ131221-01RE2 25.44 1.00 04/12/07 07:05 BJM EPA 3550B Page 3 of 7 Client EnviroAssessments (2165) 9307 Monroe Road, Suite K Charlotte, NC 28270 Attn Amanda Simpson -Petoskey 2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980' Fax 615-726-3404 Work Order: NQD1221 Project Name: EnviroAssessments (NC) Project Number: 07-6797.1/7901 N.Tyron Street Received: 04/11/07 08:40 PROJECT QUALITY CONTROL DATA Blank Analyte Blank Value Q Units Q.C. Batch Lab Number Analyzed Date/Time Extractable Petroleum Hydrocarbons 7042155-BLKI Diesel <2.00 mg/kgwet 7042155 7042155-BLKI 04/12/07 17:19 Surrogate: o-Terphenyt 116% 7042155 7042155-BLKI 04/12/07 17:19 Page 4 of 7 Client EnviroAssessments (2165) 9307 Monroe Road, Suite K Charlotte, NC 28270 Alm Amanda Simpson -Petoskey 29W Foster Creighton Road Nashville, TN 37204.800-765-0980 • Fax 615-726-3404 Work Order: NQD1221 Project Name: EnviroAssessments (NC) Project Number. 07-6797.117901 N.Tyron Street Received: 04/11/07 08:40 PROJECT QUALITY CONTROL DATA LCS Target Analyzed Analyte Known Val. Analyzed Val Q Units %Rec. Range Batch Date/Time -------- I-------------------------------------------------------------------------------------------------- ------------------_ ------- Extractable Petroleum Hydrocarbons 7042155-BSI Diesel 40.0 35.3 M3 mg/kg wet 88% 41 - 141 7042155 04/12/07 17:36 Surrogate: o-Terpheuyl 0.800 0.876 110% 32 - 132 7042155 04/12/07 17:36 Page 5 of 7 Client EnviroAssessments (2165) 9307 Monroe Road, Suite K Charlotte, NC 28270 Attn Amanda Simpson -Petoskey TestAmerica - Nashville, TN 2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980' Fax 615-726-3404 Work Order: NQD1221 Project Name: EnviroAssessments (NC) Project Number: 07-6797.1/7901 N.Tyron Street Received: 04/11/07 08:40 CERTIFICATION SUMMARY Method Matrix A1HA Nelac North Carolina ----------------------- —------- — -------------------- — - ---------------- ------------------------------------------------------------------- SW846 8015B Soil N/A X X SW-846 Soil Page 6 of 7 Client EnviroAssessments (2165) 9307 Monroe Road, Suite K Charlotte, NC 28270 Atm Amanda Simpson -Petoskey 2960 Foster Creighton Road Nashville, TN 37204 . NO-765-OM • Fax 615-7283404 Work Order: NQD1221 Project Name: EnviroAssessments (NC) Project Number: 07-6797.1/7901 N.Tyron Street Received: 04/11/07 08:40 DATA QUALIFIERS AND DEFINITIONS M3 Results exceeded the linear range in the MS/MSD and therefore are not available for reporting. The batch was accepted based on acceptable recovery in the Blank Spike (LCS). 73 The sample required a dilution due to the nature of the sample matrix. Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information. ND Not detected at the reporting limit (or method detection limit if shown) METHOD MODIFICATION NOTES Page 7 of 7 Ml J. V O I)it..'-Jk111.V1 1'l�tt,l l ANALYTICAL TESTING CORPORATION 1111111111 Nashville Division NOW 221 COOLER RECEIPT FORM BC# Cooler Received/Opened On:_ 4/11/2007 @ 8:40 Col l Indicate the Airbill Tracking Number (last 4 digits for Fedex only) and Name of Courier below:- Fed -Ex 2. Temperature of representative sample or temperature bland when opened: �� Degrees Celsius (indicate IR Gun ID#) 92171982 3. Were custody seals on outside of cooler? ............................................................ ..............» i YFS.}.NO....NA ( a. If yes, how many and where: ` 1 ��It1 4. Were the seats Intact, signed, and dated correctly?............................................................. O...NA S. Were custody papers inside cooler?............................................................................... ?.NO...NA T . ilia,. ihst T nnene.l the rnnler and answered ouestions 1-5 (Intilll 6. Were custody seals on containers: YES QO and Intact YllT.S NO were these signed, and dated correctly?--.-.— ......................................... YES ...NO .NA 7. What kind of packing material usedC:� bbl ap Peanuts Vermiculite Foam Insert Plash Paper ther None 8. Cooling process: Ice Ice -pack Ice (direct contact) Dry ice Other None 9. Did all containers arrive In good condition ( unbroken)?................... » » ».—.----. » • ••-•••• ..NO ... NA 10. Were all container labels complete (#, date, signed, pres., ete)?..... ....................................... NO ... NA 11. Did all container labels and tags agree with custody papers? ............................................... YE4 .NO...NA 12. a. Were VOA vials reccived?....................................................................................» T...NA b. Was there any observable head space present in any VOA vial?........ » ..».» - » »»»- • YE I certify that I unloaded the cooler and answered auesdous 6-12 fintiaD .......................... 13. a. On preserved bottles did the pH test strips suggest that preservation reached the correct pH level? YES.. O...NA b. Did the bottle labels indicate that the correct preservatives were used ...................... YES ... NO ... NA If preservation in-house was needed, record standard ID of preservative used 14. Was residual chlorine present?......................................................................»............ — YES ... NO ... NA I certify that I checked for chlorine and DH as oer SOP and answered questions 13-14 rintial) . 15. Were custody papers properly filled out (ink, signed, etc)? ................................................ YES ... NO ... NA 16. Did you sign the custody papers in the appropriate place? ................................................ YES .... NO ... NA 17. Were correct containers used for the analysis requested? ................................................... YES ... NO ... NA 18. Was sufficient amount of sample sent in each container?..................................................... YES ... NO ... NA I certify that I entered this aroiect into LIMS and answered questions 15-18 tintiall ........... I certify that I attached a label with the unique L1MS number to each container (iatlel)% ........ ..... 19. Were there Non -Conformance issues at login YES NO Was a PIPE generated YES NO # BIS = Broken in shipment Cooler Receipt Form LF-1 Revised 3/9/06 End of Form f a 3 ;� ��. 3� ��L � O g S' �� 3 g�� 3 F a APPENDIX 4 ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28089 704-434-0075 NON -HAZARDOUS PETROLEUM CONTAMINATED SOIL APPROVAL# __ MANIFEST# LOCATION OF SOIL: TRANSPORTER: TIME: DATE: DRIVER SIGNATURE TIME: DATE: 7- DRIVER SIGNATURE TIME. . 11 1 Is-", DATE: I DRIVER SIG6TURE TRUCK #_Ak LICENS&# . TRUCK# p u - LICENSE # TRUCK &QENSE# TIME: TRUCK DATE: 6,6 LICENSE DRIVER SlGkATURE/- INSPECTED & ACCEPTED BY SUPERVISOR'S SIGNATURE LS, INC. GROSS WT. tk� LBS. TARE WT. -zW( )b LBS. GROSS WT. LBS, TARE WT. LBS. GROSS WT. 1 LBS. TARE WT. - sz-LBS. GROSS WT. gS_9 6 8 LBS. TARE WT., LBS. ml 111 sm 1- Room 4 TOTAL NET WT. _!t 0., '7 qD TOTAL EQUIV-TONS Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075• Fax 704-434-9533 Non -Hazardous Waste Manifest # Date Load Number (numbered sequentially as trucks are dispatched) EAWRONMEArML CONSULTfINT L t rn t1 Contact: Phone: N 9q(0' C Fax: 'l(q- ?'qO 39'71 GENER4TOR: 32255 Llw, PA A i Address: qq&F I V County: t " Contact: a_ow 4- ` �,(rl_ �Q�$41Z Phone: 'j7ZZ- A WASTE ORIGRUTIONPOINT. Complete Address: TO IV Class &Type of Contaminate in soil _ J SOURCE OFCONTAMINJTION (ex. UST or other source) _ T nj'l GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmitting analytical data (methods 8240 and 8270) verf;ing that the waste in question does not contain organic constituents other than those which would nog znatly a. pear in analysis of virgin petraleum product residue, lam submitting this Certificate of Waste Constituents. I certify that I am familiarwith the source of contamination of the soil and further certify the source, to the best of my knowledgef"f4ins no carxiamir{antsj8ther than that listed above. Generators Contact: Phone: Date: 1 As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: �L_%� TYJ 7 VOLUME: TRUCK DRIVER SIGNATURE: DATE: DESTIM4TION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Signature: i"rCJ.t;L/(/�ep ,�-LJ`2...--.-�--;� Date: Company Name 4:5- S - Title: Date: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE N.C. 28086-0489 70Zi434.0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.. Tare Wgt: Net Wgt.: PUE]i�'�fr�rY �/A LICENSE PI F? L:7 S Tons: PAUL T.DA. ';(), 4 V) c --tOC7 �WWALao L NLg S- rqlio Weighed by: l(GCdl.', Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075- Fax 704-434-9533 Non -Hazardous Waste Manifest # C-3 Date Load Number tj (num red sequentially as trucks are dispatched) ENJ,7R0NMENTAL CONSULTANT - Contact: _Phone:�'�_�" GENER,4T0R: 'IP(I Address: I�i P U�r'1 n 1A ounty: Contact: Phone: -.2C.P WASTE ORIGINATIONPOINT. Complete Address: o i �Y Class &Type of Contaminate in soil _ SOURCE OF CONTAMINATION. (ex. UST or other source) � _ �1► GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. • In lieu ofsubmitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, n ns no her than that listed above. Generators Signature. I. Date: ! 1 AQ Q TRANSPORTER: r �✓���jlr n Contact: R G hua,rd- Ug M (,-3 •n f' Phone: D ' ' l0 5`.1 ;Z 2 13 As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Zv A."�_v ' Date: t / a- S- _ TRUCK #: !'� TAG #: LIT_ S 5 l 3 VOLUMI TRUCK DRIVER SIGNATURE: Lv I ,d�, DATE:IV f r DESTINATION.• Environmental Soils Inc. 91.0 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or dis osal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: ��- �`' �- Date: j t� Signature: u JZ\ _ Date: 1 Company Name --�- Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: Tare Wgt: Net Wgt.: 14UM 1 rl PUBLIC WEIGHIVIASTER Tons: LICENSE EXPIRES JUNE 30,2W �At ii -r r%A%,FiC31724 INVALID UNLESS MONO Weighed by: Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 t Non -Hazardous Waste Manifest # Date t 108. Q ENVIRONMENTAL CONSULTANT.-. Contact: GENERfITOP, Address: Contact: Load Number WASTE ORIGINATIONPOINT: Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION• (ex. UST or other source) sequentially as trucks are dispatched) W� M—N ay GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods 8240 and 8270) verq�ing that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virginpetroleumprodtictresidue, I am submitting this Certificate of Waste Constituents. I certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, ta: u no contain ants other than that listed above. Generators Signature: --^� L Date: TRANSPORTER: Contact: Phone: 9 UO - 9 3 �- As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable reg lations g ng transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: 0 �a / &t15 TRUCK#: V C2�_S TAG#: VOLUME: TRUCK DRIVER SIGNATURE: s DATE: 1 / - r3 . DESTINATION- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: TDate: l Signature: �� �--�� Date: Company Name _, s Title: _ White/Facility Canaiy/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENIAL SOILS, INC. P.O. BOX 295 LAT MORE, N.C. 28086-0489 7041434-0075 (704) 434-9533 FAX job Name: Truck# Gross Wgt.: S Tare Wgt: Net Wgt.: NORTH CAROLINA PUBLIC WE I G H tyll A S T E R Tons: LICENSE EXPIRES JUNE 30,20017 DAVIS�1 724 INVALID UNLESS StQNE-D Weighed by: Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075• Fax 704-434-9533 Non -Hazardous Waste Manifest # Date 2 Load Number r (number q sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTANT Contact: GENERATOR: I� C P Phone: F. ` Z' tJ(a � Class &Type of Contaminate in soil SOURCE OF CONTAMINATION.• (ex. UST or other source) - D GENERATORS CERTIFICATION OI, WASTE CONSTITUENTS. In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those wbicb would normally appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I cert fy that l am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, ins no rn in is other than that listed above. Generators Signature: Date: 11 /-Xku TRANSPORTER: Contact: �/ �i! y �/�t�G----- Phone: .01 As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date:_ 11—; F o ` _ TRUCK #: TRUCK DRIVER SIG DESTINATION.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or dis osal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Signature: __z Company Name .�.) i/ Date: � I o-!r' V-3 �--a Date: S _4 - Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C- 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# 9 y Gross Wgt.: Tare Wgt: Not Wgt.: PUBLIC WEIGHMASTER LICENSE EXPIRESUNE 30,2007 Tons: PAULT DAVIS , -Z2 31724 INVALID UNLESS SIGNED — Weighed by: ENVIRONMENTAL SOILS, INC. APPROVAL# LOCATION OF SOIL: TRANSPORTER: _- TIME: DATE: DRIVER P.O. BOX 295 LATTIMORE, N.C. 28089 704-434-0075 NON -HAZARDOUS PETROLEUM CONTAMINATED SOIL MANIFEST # TRUCK # M P/ __ TIME: TRUCK # DATE: - U 6 LICENSE DRIVER SIGNATURE TIME:. DATE: DRIVER SIGNATURE TIME: f 0 DATE: �— DRIVER SIGNATURE INSPECTED & ACCEPTED BY ENVI SUPERVISOR'S SIGNATURE TRUCK TRUCK # f:JW'q-3 INC GROSS WT. * 0 LBS. TARE WT. d ( 'o'W6 LBS. GROSS WT. LBS. TARE WT. gi LBS. ::.e...<...... 4:� :; GROSS WT. 3?4F E5 LBS. TARE WT. �-� LBS. GROSS WT. LBS. TARE WT. �� LBS. \*.' { y:! {� •.fin. r ', t+: .�� ti..:: '...vti,.:k: . tii .) Y.;:-1` : �$':i:''; :y,•..,•.::Mcq:•.:N.r .• .v->av ...:,i.;c: TOTAL NET WT. TOTAL EOUIV-TONS Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # Date �(I� r IN Load Number ENVIRONMENTAL CONSULTANT Contact: GENERATOR Address: Contact: WASTE ORIGINATIONPOINT Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION.• (ex. UST or other source) sequentially as trucks are dispatched). MY- ftL- 301 qc� rizz - zU2C GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally a. ppear in analysis of virginpetrokuynproduct residue, I am submitting this Certificate of Waste Constituents. I certify that I am fand iar with the source of contamination of the soil and furtlser certify the source, to the best ofmy knowledge, cynlain? nod hliNinafts other tban that listed above. Generators TMINSPORTER: Contact: Phone: Date:/,Y/o� As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK A T VOLUME: � n : fi TRUCK DRIVER SIGNATURE: DATE: DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Elo �' ls'' Signature: t Z=�� 4Z �-----mate: Company Name Title: Date: t/ C31 White/Facility Canarv/Invoice Pink/Carrier t ol(i en mr]/l rPn Prq tnr ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX ) Name: ck# — )ss Wgt.: lao Wgt: twgt.: NORTH CAROLINA is: PUBLIC MGHMASTER EXVIKES-JUNE 30 2007 PAUL T. DAV is p'o'. 31724 sighed by: INVALWWWA:94 8lQ95 Environmental. Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # Date Load Number (numbged sequentially as trucks are dispatched) EAWRONMENTIIL CONSUL7MNT Contact: GENERdTOR: Address: C y Class &Type of Contaminate in soil Phone: Fax: 35t11 1 I SOURCE OFCONTAMIVJTION.• (ex. UST or other source) UL he-atiYU � GENERATORS CERTIFICATION OFWISTE CONSTITUENTS: In lieu ofsubmittinganalytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleumproduct residue, Iam submitting this Certificate of Waste Constituents. I certify that IVn familiar with the source of contambwtion of the soil and further certify the source, to the best of my knowledge count ins no contamina other than that listed above. r Generators Signature Date: lzslou TRANSPORTER O-W 14 v As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: _` � 'k :hat�itt CJ�G Date: -A -10 .C? TRUCK#:Mv.H ZT G # - VOLUME: TRUCK DRIVER SIGNATURE: DATE: i f ',ag__L',l',� DESTINATION.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: n_ - 0( -),--L" Wai Date: t ' Signature: l ���? e.�l� /!L(�� Date: Company Name .5 ,� Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 7041434-0075 (704) 434-9533 FAX Job Name; Truck# tv Gross Wgt.: Tare Wgt: n-n 7 '0 Net Wgt.: 14914*11GARGUNA— PUBLIC VADGHMASTER LICENSE EXPIRES JUNIE 30.2007 Tons: -PAUL T.DAV12P P 3*24 0, INVALID UNLESS SIGNED__ Weighed by: Date Environmental. Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest # b� ENVIRONMENTAL CONSULTANT Contact: L GENERATOR Address: Contact: >� WASTE ORIGINATIONPOIN7: Class &Type of Contaminate in soil Load Number (numbered sequentially as trucks are dispatched) SOURCE OF CONTAMINA770N.• (ex. UST or other source) �0— WZ- j3e5; GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, phloins no eoi a"Qants other than that listed above. Generators Signature: ZA6�0(j.)gu-7 Date: /(-)-Q TRANSPORTER l%/u LilU55 Contact: ,��LN�/;� Phone: 1 As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for elivery to the facility designate. Carrier Signature: ' /�G-�.� ��-'�S''f Date: 6 TRUCK #: TAG #: VOLUME: �Q 3 ° TRUCK DRIVER SIGNATURE: DATE: DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal ' n a Fer that has been authorized by the Sate of North Carolina. Facility Signature: �C3 - � Date: 1_1D4ve,6 Signature:Date: Company Name Title: if White/Facility Canary/Invoice Pink/Carrier GA1r1Pnrnrl/rPnPrat-nr ENVIF(ONif.NTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truckft — /0 k Gross Wgt.: Tare Wgt: Not Wgt.: UNORTH CAROLINA BLIC VWIGH-OvIASTER Tons: LICENSE EXPIRFIR MUL T DAMS RVAt—a UM, 31724 j, J Weighed by: Environmental Soils Inc. PO Box 295 ° Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # Date Load Number ENffRONMENTIL CONSULTdNT.• (-- A Contact: Lu ; (L)FA5-S Phone: GENERATOR QAA "WOE -LC___ sequentially as trucks are dispatched) Fax: ' $uC.Q'. Address: S County: Contact: _L%Oa.' 3,n _MT Phone: WASTE ORIGINfITIONPOINTt Complete Address:19 Q I Ny . # u)n ,�'R Class &Type of Contaminate in soil SOURCE OF CONT?MINATION. (ex. UST or other source) GENER4TORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmitting analyticaldata (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I certify that ain familiar with the source of contamination of the soil and ficrther certify the source, to the best of my knowledge, co t no contam v is her than that listed above. Generators Signature: Date: -z g L6 c-P, TRANSPORTER: f Contact: Phone: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing an ortation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: L K I-VOLUM: TRUCK DRIVER SIGNATURE: D1 DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/ osal in a�-maannnerr that has been authorized by the Sate of North Carolina. Facility AL Signature: �-' Date: Signature: Date: �f Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenmd/Genemrnr ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0076 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: Tare Wgt: Net Wgt.: NORTH CAROLINA Trans:PUBLIC WEIGH?AAs-rFq 200-7 DA S �: . V'� 'U�D U PAUL T DAVIS 317Z4. Weighed by: 1W D UN Ss ohr'soiu-ce) .,. �, ;�IUS'7'tTUI N7'S Iri�euo y Y..p4 fJ�y✓�Y , Or�', ��s 1TotCoittCll i1 Or�rR}ZZC COnS�l ioeTrrrt resielrrc, an, subm ty' f� Source -Jfcow,?)r1inaflb- s other than that listed rzbt�fie. Ac F9'rrrcclyticIV IIcrta (metbo'cls imer than tbos��rt�hich 2t oarld catt 71Yt%ml, Certt& be source, 10 f r z x+ :fs `thc c<zi 1cl "CerI� g trials described abbe bean manifest are p th g atppec� undi✓�� ;a ��;k%}�-tl,,patkaged, labeled, secured and "are ' �fiterials in proper`ccli�c'tic�f�p�rt ''Commerce under the designate ble regu(la ions gouerning'transportation, and I hereby receive this niat i' #'fir deliver to ' facility designate. y .the Carrier Signature: Date TRUCI{ #: ` r . G# f f J - TRUCKDRIVER DES TINdTION' Environmental Soils Inc. 910 Crowder Ind, Shelby, NC 28150 Site Permit #SR0300038 Y Dedicated Land Application 'I certify that the carrier has delivered the materials described above to this faeili and I hereby for treatment and/or disposal in a manner that has been authorized by the Sate of No' th Carol accept this material l - na. Facility Signaturex q- ; r Date: Si gAatures t, Company Name ice-----'"_._�__- Date: ( _- Title: White/Facility j� Canary/Invoice Pink/Carrier Goldenrod/Generator Gross Wgt.: Environmental Soils Inc. r` PO Box 295 • Lattimore, NC 28089 Phone 704=�, - 007 "Fax 704-434-9533 Nori-I=Iaza # 21 � �6 rdriiis`Waste 1�Iatzifest ' Date Load.;NumbO' f (numbered sequentially as trucks `are dispatched) ENVIRONMENTfIL CONSULTWN7: i Contact: :> EIZfITOR: Phone: is Fax GEN ' 1,, ,l , ..� Address. y Contact ,1 County: TVf1STE ORIGINWTIONPOINT Complete Address: ; Phone Class &Type of Contaminate in soil — SOURCE OFCONTfIMIMMON.• (ex. UST or other source) a GENER,4TORS CERTIFICIITIONOFT�V4STE CONSTITUENTS. In.liezz ofsubinittin anal tical data ethods 8240 and 8270) ver fving that the waste in question does not contain organicconstituents oth g that those wl'ich11 would normally appear in analysis of viigitz petroleuinproduct residue, .I ant submitting this Certificate of Waste Coststttueitts. I cert fy that I ain fcrnziliar witli the source of contantincttion of the soil and fzzrther certify the source to the best of my knowledge, contains no contarhinants other tltaiz that listed above: fy ' Generators Signature:"" Date. ' ,'` ' ' fi i — TPUNSPORTER: Contact: _ Phone: - As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are -properly classified, par kaged, labeled, -secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for deliver to the facility designate. y Carrier Signature: Date::.: TRUCK # TAG #:-�----r r TRUCK DRIVER SIGNATURE: VOLUME ' . DATI✓ DESTIN.dTION.• Environmental Soils Inc. 910 Crowder. Rd, Shelby; NC 28150 Dedicated Land A Site Permit 4SR0300038 pphcation I.certify that the carrier has d livered the materials described above to this facility, and Lhereby aece p rthi " is material for treatment and/or Ali$ psal in a�manner that has_been authorized by the 5ate.of North CatrWina Facility Signature: ate: f Sign ature: Company r Date: Name 4 ' Title: White/Facility Canary/Invoce . Pink/Carrier Goldenrod/Generator Tare Tons Weic i-Invironmental Soils Inc. PO Box 295 • Lattimore, NC 28089 dFf Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # X .+.• $ ' .' t >' Load Number EAWRONMENTAL CONSULTANT Contact: GENERATOR: Address: Contact: (numbered sequentially as trucks are dispatched) Phone: WASTE ORIGINJTIONPOINT Complete Address: Class fir, Tvpe of Contaminate in soil SOURCE OF CONTAMINATION (ex. UST or other source) Fax: County: -Phone: GENERATORS CERTIFICATION OF WASTE CONSTITUENTS.. In lieu of sub�:itti�:g analytical data (methods 8240 and 8270) ver�ing that the waste in gluestion does not contain organic constituents other than those which iethowould norirrally appear in analysts of virgin fietrolez�rn product residue, I ans submitting this Certfcate of Waste Constituents. I cert6rY that I am fainiliar with the source of contamination of the soil and farther certify the sortree, to the best of 9ny knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER. Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non-ha7�lydous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: TRUCK DRIVER SIGNATURE: VOLUME: DATE: DESTINATION Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby -ac for treatment and/or disposal in a manner that has been authorized by the Sate of North Ca olinaCept this material Facility Signature: Signature: Company Name Date: Title: Date: White/l ability Canary/Invoice Pink/Carrier Goldenrod/Generator Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Nan -Hazardous Waste Manifest # 21409 Date Load Number ENYIRONMENT4L CONSULTfINT (numbered sequentially as trucks are dispatched) Contact: Phone: GENERdTOR: Fax: Address: _- Contact: County: W4STE ORIGIN4TIONPOINT Complete Address: Phone: Class &Type of Contaminate in soil SOURCE OFCONTiIMINWTION (cx. UST or other source) GENER.4TORS CERTIFICWTION OF WJSTE CONSTITUENTS: In lieu ofsubmitting analytical data (methods 8240 and 8270) ver6ing that the waste in question does not contain organic constituents other thast those which would normally appear in analysis of viy9inpetroleumproduct residue, lam submitting this Certificate of Waste Constituents. I cert f thatl art: familiar with the source of conian,%nat%on of the soil and further certify the source, to the best of Yny knowledge, contains no contaminants other than that listed above. Generators Signatu Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materiels manifest are properly classified, packaged, labeled, secured, and arc in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: .:.. . Date: TRUCK #: TAG VOLUME: TRUCK DRIVER SIGNATURE: DATE: DESTINWTION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Ap lication Site Permit #SR0300038 p I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Signature: Company Name White/Facility Date: Date: Title: Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORF—A-AC". 28086-0489 7041434-0075 (704) 434-9533 FAX Job Name:. Truck# Gross w6t: Tare Wqt: Net Wgt.: Tons: Weighed by: Environmental Soils Inc. PO Box 295 , Lattimore, NC 28089 i "Phone 704-434-_0075 Fax 704-434` 4533 Non -Hazardous Waste 'Man ifestk Load Number (number sequentially as trucks are dispatched) ENIjIRONMENTQL CONS.ULTl4NT. Contact 1��___ Phone ,`i " jy�y�/y +/�r y�{ y ..0 f� T�. A }aA ! 4 4 3t f tt Addresst >.'v r y s'ae s t •.,. xn ; County: rF. Contact t ' T"I' f `� IbOl1V7 _ .. Phone. f �iSTE ` " _`. oznpletc Address: 1 Class &Type of Cr"r tarnmate in soil SOURCT OFCOlUIfllillN.17`IO�V (ex. UST or other source) I GLNI.IZf1TOIZS CRTIF,IC14TlONOF WASTE GONSTITUla1VTS: In lieu ofsubinitting anal tical data nzet 8240 and 8270)e ` 3i $ that thods he waste in question sloes not contain organic constituents other than those wbich would normally appeal in,' ysis of virgin petroleum product resid7te, I a)n submitting this Certificate of Waste Constituents. I cert tljgtl am familiar with the source of contamination of tl?e Soil and farther certio the source to the best of niy knowledge, contains no contaminants other than-tb' t listed above. ' i�enei•ators Signature: - - Date. TPUNSPORTLR Contact; - Phonc: As the carrier, I certify that the materials, described above being shipped under this .non -hazard ous materials rr�anifestare pfoperly'classif ed, package, labeled, secured, and are in propercondition for transport in commerce under the applicable regulations go n t sportation, and I hereby receive this material for deliver to the facility, designate: y Carrier Signature: - _--- Date: 1 riC %l f TRUCK#: - TAG #: VOLUME 7`"� . TRUCK DRIVER SIGNN_ruRE: DATE. DESTINfITION.. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land A lioatior Site Permit #SR0300038 pp l x=r I certify that the carrier has delivered the materials described above to this -facility, f and or treatment -I hereb accept and/orrc jp.osal in a manner. that has been authorized' by the Sate of Northtarol nacept this material Facility Signatures �,/ r j Date: r41 Signature: R %` an Name a Date: Company P �. Title: White/Facility Canary/Invoice . Pink/Carrier Goldenrod/Generator S. ENVIRONMENTAL SOILS, INC. P 0. Rk� X�:2g5 LATTIMORE, `N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: _,_• , �a s. Truck# Grossgt� Tire YYgt1�e hh'x Net Wgt. Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # H 4 3' 1 Date Load Number ENYfRONMENT4L CONSULTANT -(numbered sequentially as trucks are dispatched) Contact: Phone: Fax: GENER-4TOR: Address: County: Contact: WASTE ORIGIMITIONPOINT Complete Address: Phone: Class &,Type of Contaminate in soil SOURCE OF C0NT4MIN4TI0N. (ex. UST or other source) GENER.4TORS CERTIFIC YTION OF WASTE CONSTITUENTS. In lieu of szrbnaitting analytical data (methods 82d0 and 8270j verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I certify that I ani familiar with the source of contasnination of the soil and further certio the source, to the best of my knowledge, contains no contan:inants other than that listed above. Generators Signature: Date: TRANSPORTER. - Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: TRUCK DRIVER SIGNATURE: VOLUME: DATE: DESTTMITION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated band Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator .ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C.- 28086-0489 704A34-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: L Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 2 12Y Date EAWRONMENTAL CONSULTANT Contact: GENERATOR: Address: Contact: Load Number (numbered sequentially as trucks are dispatched) Phone: Fax: WASTE ORIGINATIONPOINT.• Complete Address: Class & ype of Contaminate in soil SOURCE OF COAMAMINATION.• (ex. UST or other source) County: Phone: GENERATORS CERTIFICATION OF WASTE CONSTITUENTS.In lieu of submitting analytical data (methods 82,;'0 and 8270) ver6ing that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, lam submitting this Certificate of Waste Constituents. I certify that I am familiar with the sourre of contamination of the soil and further cert#ythe source, to the best of niy knowledge, contains no contaminants other than that listed above. Generators Sit;na TMINSPORTER. Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: Date: TRUCK #: TAG #: TRUCK DRIVER SIGNATURE: ......... . VOLUME:: DATE: DESTINATION Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: i Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC.' P.O. BOX 295 LATTIMORIE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.• Weighed by: ENVIRONNIEA74L CONSUMN7s 1 Contact. J, - Phone. hone: GE;NT'"-7'0R Class &Type SOURCE OF 8240 arrd $2 m) ve normally appear in Constituents. I cert the hest of my know i'1MIti�l7IO1V (e. UST or other source) �TIfiICIITION OF. I11WSTF, CONSTITU4NTS. In lieu ofsubnatt&r al ' .; ta (methods at the waste;in question does not contain organic constiitssents 6 iee i�b�tl.ose which would al su'of g-in petroleumprodyict residue, k4 subfn ttsn` is Cert fcate o l caste that,I ant familiar with the source of cohtdhib iltion of t%e loll a?2d further certify.the soicrce, to �e,:- contains no coutaini)tants,btljer than thatlisteel above: Generators Signature Date: 1 TR,4NSPO1?TtR: Contact: Phone: As the carrier, I certify that the materials, described above being shippedunder this non -hazardous materials manifest are properly dlassified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. - r F• Carrier Signature: = - Date - TRUCK rs TRUCK �` TAG #: _ VOLUME:a E r: TRUCK DRIVER SIGNAI'URE: _ 1�1 DATE:' DESTMTIDN.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit#SR0�00038 I certify hat the carrier dishas delivered the materials described above to this facility, and-1 hereby accept'this niaterial for treatxnept.and/or p9sal in a mannerthat has-been authorized by the Sate of North Carolina. Facility. Signatur . !`�.L� l+.i , '"r'i ►,�} t f ; ! / ; t Date '? ; J� f .-�• Signature Date: �t r Company Name f l= - Title: - White/Facility. Canary/invoice, Pink/Carrier Goldenrad/Generator Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 Nor-i-Hazardous Waste Manifest #21.438 Date Load Number (numbered sequentially as trucks are dispatched) EAWIRONMENTAL CONSULTANT - Contact: Phone: Fax: GENEjMTOR: Address: County: Contact: Phone: _ WASTE ORIGINATIONPOIAT. (�omplete Address: Class &.Type of Contaminate in soil SOURCE OF CONTAMINATION (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In tieu of ncbmitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petrolerrrst product ? esidue, Ian-, submitting this Certificate of Waste Constituents. I cert�q that I am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: W. TRUCK #: �: TAG #: VOLUME:1.- TRUCK DRIVER SIGNATURE: DATE: DESTINATION Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. . Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice , Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: _ Tare Wgt: Net Wgt.: Tons: Weighed by: Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 , Fax 704-434-9533 Non -Hazardous Waste Manifest # 2) 14 Date Load Number (numbered sequentially as trucks are dispatched) EAWIRONMENTAL CONSULTANT Contact: Phone: Fax: GENERATOR. Address: Contact: WASTE ORIGINATIONPOINT.• Complete Address: _ Class &Type of Contaminate in soil SOURCE OF CONTAII1INATION.• (ex. UST or other source) County: - Phone: GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmittinganalytical data (methods 8240 and 8270) ver ping that the waste in question does not contain organic constituents other than those which would norina#y appear in analysts of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I cert�q that I am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: _Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: TRUCK DRIVER SIGNATURE: DATE: DESTINATION.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: t Company Name _ Date: Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name• Truck# Gross Wgt.: _ Tare Wgt: Net Wgt.: Tons: Weighed by: Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest # 211, Date Load Number EAWRONMENTQL CONSUMNT.• Contact: GENERATOR: (numbered sequentially as trucks are dispatched) -Phone: Fax: Address: County: Contact: WdSTE ORIGIN,4TI0NPOINT.-Complete Address: Class & Type of Contaminate in soil SOURCE OF CONTAMINATION • (ex. UST or other source) Phone: GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of s:rbsnitting analytical data (methods 8240 and 8270) verD54ng that the waste in Juestion does not contain organic constituents other than those which would normally appear in analysis of virgin petr oleum product residue, I am submitting this Certyicate of Waste Constituents. I certify that I ant familiar with the source of contamination of the soil and further certify the source, to the best of :ny knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: f TRUCK #: ... .. , ,. , TAG #: VOLUME:-........_._;..r... Y ; ; TRUCK DRIVER SIGNATURE: DATE: DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator .ENVIRONMEN"TAL SOILS, INC.:�- P O. BOX 295 ,PVIRONMENTAL SOILS, INC., LATTIMORE, N.C. 28086 0489r P.O.-BOX 295 704/434-0075 LATTIMORE, N.C. 28086-0489 (704) 434-9533 FAX 7041434-0075 + (704)-434-9533 FAX Job Name. Job Name: �� 1,43 Truck#, Gross w9t.:` Truck# ` I< Y'fi✓Yw .Y l Tare Wgt: f C t'Y irk► ; �t{h lty �; r ri rT At Ps , VA `-fr;:, " Net Wgt. h; srs r �A¢r�ra t tit t ,. Net Tons { j ! i Torts: P Weighed by: 1 Weighed by: x Environmental Soils Inc. F PC)yB& 295 Lattimore, NC 280$9:. Phone b4Y434=0075 •;Fax 704 44 g533 t}?L Non -Hazardous Waste Manifest # 2 1 '4 3 0 Date _ _ F:1 ¢.{ `,'1�•, Load Number (nuinbcred sequentially as trucks are dispatched) EjV1/7R0jViIIENIf?L CONSUJXliVT i ontaet Phone:,fit:. �, f �; z ' ` �'1 Fax Y _ GEAERAT07 4S C z ". r pia e# 4 _ � Addrrs`'rr IE Count co Tt�f?S?'E Ol��t to ,� 7 riir plCtc Addre,, l i,4d t iA '+ 1Ts Class &'1 ype of UniSt4'r Izte in soil -- - t; S0UPC,E, OhCO�V' h1V�1`I�OV (e�. UST or other source)_ t ! 1 4 C,L1 rE?Z�17`GaR,S' C,Z;R`I II{IC ITlO��' Ol Tit?SI'E CON�STIfiIT' TS: sfr lien of strb'mittttsgdi glytieal rldfe r3st� M. 8240rttzd b'2iD) <<:er ing that the waste n yuestion noes not contain organic constituents ot�Ei "t%an those wl� ztf�lt� normally q -tr itt analysis of virgin pefrolezr3zi produet resirine, l azzz szibt timpigthisCerto rite o TPaste f Constiiuonts. I cert 0*�_ that I atsz. familiar wzt1) the source,of contannnatton of &soil and j6Aer certify the sour.'ce, to the bes' dX tst kno Ie a contaizzs no cotztarnanan s,other than that listed above. Geneox`S nature S >a .� _ Y Dater TR 4NSPORTER: ` )1 Contact: ._._ Phone: f As the carrier, I certify that 'the niaterials'described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are.in proper condition for transport in coznrnerce under the applicable' regulations governing transportation, and I hereby receive this material for deliver yto the facility designate. Carrier Signature: Date: TRUCK #:--�—_ ,-- r{n:�YT�S�a VOLUME , TRUCK DRIVER SIGNATURE: fr DATE: �r�, r�r -� DESTINATION- Environmental Soils Inc. 910 Crowder Rd, Shelby; NC 28150 Dedicated Land Application Site Permit#SR0300038 I certify that the carrier has delivered the 'mate rials described above to this facility, and I hereby accept this material for treatment and/or.disposal in a manner that has been authorized by the Sate of North Carolina. Eacili 5i nahlr . + ar_; ;` o` Date: r r / 0 Signature Date: j i r— Company Name Title: —� White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator .,q '.Environmental Soils Inc. PO Box 295 • Lattimore, NC 29089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 21,433 Date Load Number (numbered sequentially as trucks are dispatched) EIWIRONMENT4L CONSULTANT - Contact: Phone: Fax: GENERATOR: Address: County: Contact: Phone: WASTE ORIGINfITIONPOIN7: Complete Address: K, Class & Type of Contaminate in soil SOURCE OF CONTAMINATION. (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmitting analytical data (methods 8240 and 8270) verfting that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleumproduct residue, Iam submitting this Certificate of Waste Constituents. I certify that I am familiar with the source of contamination of thesoilandfurther certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: Contact: Phone: rd As the carrier, I certify that the materials described above being.shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and,are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: = ;' TRUCK # TAG #: VOLUME: TRUCK DRIVER SIGNATURE: _.....; Y, DATE: <: DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature. Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name:.. 'x Truck# Gross Wgt. Tare Wgt: Net Wgt.: Tons: Weighed by: ,Environmental Soils Mc. PO Box 295 • Lattimore, NC 28089 Phone 704=434-.0075 Fax 704-434-9533 Non -Hazardous Waste Manifest # `21.4 3 4 Date. +. J # Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENT-4L CONSULTfINT ' Contact: 3 Ylione %'� = Fax: GENERzITOR: ' County: Contact: L Phone fV,4STI ORrGI1NWTIONPOI,V7:• Complete Address: _ ` ;_ ; , , ; J . � v Class &,Type of Contaminate in soil SOURCE OF CONTMAIIINIITION: (ex. UST or other source) GF_NER,4TORS C ,RTIFICA77ONOI,'tV11ST, CONSTITUENTS: In lieu ofsubsnittinganalytical data (methods 8240 and S270 veri f yin,( that the waste in question doeSrrnot contain organic constituents other than those which �zvould izormally appear in analysis of viTin petroleum product residue, I anti submitting..this Certificate of Waste Constituents. I cert�61 that I am familiar with the source of contamination of the soil aid further certj the source, to the best of myknowledge; contains no contaminants; other than that listed above. 1 Generators Signature: Date: / , TRANSPORTER: Z tContact 1,l i : k, Phone: <7�4� As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are.properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations p$-, in -transportation, and I hereby receive this material for delivery to the facility designate Carrier Signature:` Date: TRUCK #: , i;' TAG # VOLUME. -� r TRUCK DRIVER SIGNATURE: DATE: S,> " i. I�EST1 ATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit#SR0300038 I certify that the carrier has delivered `the materials described above to this facility; and I' hereby accept this material for treatment and/or dispwal in a manner that -as been authorized by the Sate of North Carolina: r� � 1 Facility Signature: Signature: t i ,' .t_ , °_� { �F, 'F' ....._ Date: i Company Name Title: l� White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator N Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest # 2 - 4 3 ES Date Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTANT: Contact: Phone: Fax: GENERATOR Address: County: Contact. Phone: WASTE ORWINATIONPOINT.• Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION: (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods 8240 and 8270) ver wing that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleumproduct residue, I am submitting this Cert yicate of Waste Constituents. I cert6 thatl am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TR.INSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: TRUCK DRIVER SIGNATURE: DATE:: DESTINATION Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. :P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: f;s Environmental Soils Inc: > POD Box295 • Lattimore, NC 28089 075 �04-434- 9533 • Fa�c t Nait=Hazardous Waste Manifest # 21426VY is ; as �, Load Number �ruiibexed sequentially as trucks are dispatched) - COnt l(,t - -s I�11611e M& `i Fax: 1 i Address : 1 r, i , LL County _. --- Contact _ Phorie Jir4S> 1 � T 0A1110_INT.• Com lete Address; p 4 Cl ' 'ap s &e o t t al i ftAte in soil SOURCE OF t 1.TION: (ex. UST or othersource) CTNEI?,/ RS CEIZ7`1'FI fITION OF lV�ISTE CONSTITUENTS 'In liete of su t�! tt y cc�l data (methods 8240 and 8270) verifjing that thewaste in question does not contain organicconstit bt` Ihose'whi.ch zuoitlr . normally appear in analysis of virgin petroleum product residue, I am subinitting.�this Constituents. .I cert�& that am familiar with the source of contamination of the so tanc Ef�'t�i tE the source, to �. the st of i)iy k?iowledge, eontii)u-no conta�isi�ti�nts'other than hat listed above. Generators Sgnature#`t' `` ^t f� r D ate r TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials .manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrierature: Date. TRICK # s - TAG #: VOLUME: TRUCK DRIVER SIGNATURE: DATE: IIESTINITTION Eniironmental Soils'Inc 910 Crowder :Rd; Shell�y,:'NCIWO Dedicated Land Application Site Permit #SR030003$ L—A I certify that the carrier has delivered the materials described above to thm fiacility, and I hereby accept this material for treatment and/or. dispgsal it a manner that has biers authorized by the Site of North Carolina. Facility Signature: - 1. r. Date G� Signature i a�_�� `` Company Name Title: White/Facility „. Canary/Invoice Pink/Carrier Goldenrod/Generator xrvt,`.'ii...p��r.'m.m"r, Environmental Soils Inc. PO Box 295 • Lattimore, NC-28089 Phone 704-434-0075 • Fax 704-434-9533 Non�Hazardous Waste Manifest # 214 0 4 Dare Load Number (numbered sequentially as trucks are dispatched) ENIVIRONMENE4L CONSULT9NT. Contact: Phone: Fax: t GENERATOR: Address. County Contact: Phone: WASTE ORIGINATIONPO•INT Complete Address: `1 Class &Type of Gontarniriate in soil SOURCE OF CONTIMIN_4TION.• (ex. UST ovother source) GENER,4TORS CERTIFICATtO.NOFWASTE CONSTITUENTS: In lieu ofsubrnittinganalytical data (methods 8240 aszd 8270) ver isig that the:waste;in.question does not contain organic constituents other than those which would rcormallj� appear an anolysis`of virginpetroleuinproduct residue, Taft submitting this 'Certificate of Waste 01istituuesitts. I tent that I am fatriiliar with tl)e source of contanztnatio of tlie'soil and further certzi - e source, to the best of'my k"Wedge, con >tns:no;cfntanainanix other than tlsat lutedabove. Generators Signature: Date. TRANSPO9TE7Zr Contact: Phone: As the carrier,_I :certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: .r=-% ' Date: c�ri ._.ram--•--- ;..--' • a`` � �-. 1 TRUCK #: ' -' TAG#: VOLUME: = ' i ��.G �? TRUCK DRIVER SIGNATURE: ' ..,t'•-;'->;, . �x _ -:; DATE~ DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or. in a manner that has been authorized by the Sate of North Carolina. . z Facility Signature: j j-> ,f Date: Signature: ;'' `r t `' Date Company Name .' :.`..-----_.-- Title White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator . ;i7..;:.•yk e. 9' :S:+r,'c;ukpnp+wu,r-:�•'Frei,:•obl�.i:'%:TTii?':.z:���;'f7�'`Ln'sa�,',�a�..^ ENV'IF �NMENlA,L SOILS, INC. } P.O. BOX 295 -ATTIMORE, N.C. 28086-0489 704/434-0075 (7--04) 434-9533 FAX.: } Job Name :` jA:041 i ;r'r Truck# Gross Wgt:' Tare Wgt: Net Wgt.• " y. Ail rY Weighed by: `environmental Soils Inc. Address: County: Contact. Phone. r. i- WASTE ORIGIN-4TIONPOIIVT.• Complete Address: `{ Class &Type of Contaminate in soil SOURCE OF CONT 4MINJTION.• (ex. UST or other source) i i -7— GFNER,4TORS CERTIFICATIONOF 1F,4STE CONSTITUENTS: In lieu ofs u bm itting a n alytical data (methods _ 5240 and 8270) <ver�oing that the waste in question does i:ot contain organic constituents other than.those which" would normally appear in analysis of virgin petroleun1product 4•esidue, I ant submitting this Certificate of Waste -C titrsents: I cert that l ant familiar with the source o contamination of the soil and fisr her cent the source, to �tbest of my knowledge, contains no contanrtnants other) all. that listed above. a4� ; �P zlGenerators Signature.JJ t ,, r TRJNSAORTER: Contact: Phone: As the carrier, I certifyrthat the materials described above being shipped under this non -hazardous materials" manifest are properly classified, packaged; labeled, secured, and are in proper condition for traisport in commerce under the applicable regulatioris:governing .transportation, and I hereby :receive this material for delivery to _the facility designate. y Carrier $ignature:%`''j �Date: , TRUCK # fr? fiAG # VOLUME (G.( : /1. l . .TRUCK f.}l2:IVER SIGNATURES c -.,,., i DA`':F DESTIM076N.• riwirotirrienta�l<Soils Inc::910 Crowder d;:8helby; lVC 281�U` dedicated I�and.Applieation Site Permit #SR0300038 Lcertify thafthe carrier has delivered the materials desciibed.above o tli s.facility, and I hereby accept this material ' foi="treatment and/ordisposal oral m: manner that.has been.authorizedty the.'Sate of North Carolina. Facility Signature:'i f� ft t >� �� -�" Bate: f/:t Signature ,i A Date Company Name Title: ; White/Facility Canary/Invoice - Pink/Carrier Goldenrod/Generator i Gh'NE1Z�17'O1Z � } Address: } Contact: (numbered sequentially as trucks are dispatched)- �� i { r,_ County: Phone: ", •1 Class & ype of Contaminate'in soil r SO URCE OF CONI IMINW HON.- (ex. UST. or other source) G1siVT1?,JT6RS CERTIFIC,11TIONOFW4STE CONSTITUENTS. In lieu of submitting analyticaldata (methods 8240 and 8270) ver�&ing that the' waste in,question does not contain organic'constituents other than those which would normally afi - in analysis of virgin petroleumproduct resi :te, I am stt�irnitting this Certificate of ffaste Co stitueitts: I certify that ani familiar -with the source of coiitaminatio"ti of the soil and fuYther cert� tl7e,solirce, to the est of&my knowledge, contains tro contanainanits otIJL an that Izsted above enerarors Sigriafiire:=r.�.�` Date TWANSPORTEIY Contact: Phone:. As the carrier;1 certify that the materialSr described above being shipped under -this non -hazardous materials' manifest..are:properly classified, packaged;labeled, secured,arad are in proper condition for frarispoxt in commerce' under the applicable regulations .goyerr irig transportation, and I hereby tt eive this material for Ad1hreiy to the facility designate: Carnet Signature: Date TRUCK TAG.# VOILUIVIE: ' TRIkY, DRIVERSIGNATURE: IjESTIN�4TION.• Environffi6' l Soils Inc. 3T0 .Ctbwder. ka;-Shelby, NC 2$150 '1�edicated Lan Application &te%tnit #SR0300638 f "k IVASTE ORIG[MMONPOINT Complete Address: I certify that the carrier has delivered the materials described .above to this -,facility, and I hereby aceept1thi6_ft aterial for treatment acid/o,,diposa in a manner that has been authorized liy the Sate of North Carolina ? , Facility%Signature ; �, ; �• - �Y`t •.. Date: Signature L t Date: /. y an ComP Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator . ,r ..«. y.,nab.�r�i8ya:�e,Yx7,:�h•,�vgix•ry.� y.yoyyv,.ra.m,..,,:'uyY ,.: •.r :vr•.!s ENVIRONMENTAL SOILS, INC. `< P.O. BOX.295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# lolun fare ._ 4/17/2007 56940 lb 6 Gross Wgt.: Tare Wgt` i- Net Wgt . Tons: Weighed by: , Environmental. Soils`Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 214 4 3 6 Date Load Number ENHRONMENT4L CONSULT41VT Contact: GENERATOR: Address: (numbered sequentially as trucks are dispatched) Phone: Fax: County: Contact: Phone: WASTE ORIGINATIONPO.WT Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION.• (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lien of submitting analytical data methods 8240 and 8270l verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum piroditct residue, I ant submitting this Certif sate of Waste Constituents. I certtFy thatl ain familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that fistedabove. Generators Signature: . ..... Date: - TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK*: TRUCK DRIVER SIGNATURE: TAG #: VOLUME: DATE: DESTWATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: -. .. Date - Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 UtflMORE, N.C. 28086-0489 7041434-0075: -; - (704) 434-9533 FAX Job Name• Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: y Environmental Soils Inc. PO Box 295 Lattimore, NC 28089 Phone 704-434 ,0075 Fax 704-434-:9 8 Non. -Hazardous Waste Manifest # a 4 2 7 . Date { Load Number (numbered sequentially as trucks are dispatched) FNUROA 1IFN711L CUNSULTgNT. Contact: Phone. i� Fax: GENER ITOR address: — C©tlratiy; Iione: rr��, w"IsTiG' ORIdI�1�_ : .DINT &replete Address: ^_ Class & Type of Contarninate in soil SOURCI' OF COA"111NIIV,47YON.• (ex. UST or other source) GENER,11TORS CERHFICITI0N0.FW11S7T CONSI:ITUENZS: In lief: of suhrnitting analytical data (methods. 8240 and 8270) verifying that the waste in question does not contain organic constituents other t*l t those which would nor 1nrrlly appear in analysis of virgin petroleum product residue, lam submitting this Certi ff o, f l haste Constituents. I cert0i that I ain familiar with the source of contamination of the soil and fiirther certify the source; to the hest of myknowledge, contains no contaminants other than that listed above. Generators Signature: Date: ; TRJIVSPOA,TER: .�A, Contact: f 1�r Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations.governingaransportation, and I hereby receive this material for delivery to the facility designate. ; ? f, Air ` � ' / �. Carrier Signature: �. ? ,� r f✓x::; r Date: f TRUCK #: TAG #: VOLUME.� -. TRUCK DRIVER SIGNATURE: . ° DATE: 4/ i DESTINATION-., Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application' Site Permit#50300038 I cortify:thavthe carrier has delivered.the materials described above to this facility, and I hereby accept this material for; treatment and/or dispt-saldh a manner that has been authorized by the.Sate of North Carolina: i � rl..ai f..;.� t-' �jy Date-.. Y Facility Signature: .24 r �'" Signature: � �{ .� • f. .�_ , � , . `�,......... 4 :. t, , ,t r Date: Company Name .. ..Title: r' White/Facility . Canary/Invoice. - - Pirik/Carrier ' Geildenrod/Generator Gross Wgt.: F) r i Environmental Soils Ind. PO Box295 • Lattimore, NC 28089 Phone 704`-434-0075 • Fax 704=�t!�533 Noy -Hazardous Waste Manifest # 2 14 2 8 Date Load Number ; (numbered sequentially as. trucks are dispatched) ENVIRONNIENT111, COjVSULT1N`I Contact - Phone: Fax: - --- — GL'N �RjT'_r Address. County: Y C:ofitact t �_ Phone:. ii��S?'E ORI1fIT1�N1�OrN"..Complete Address: Class &Type of Contaminate in soil SOURCE OFCONT11JW1NJTJON.• (ex. UST or other source) GE�VL�ILITORS CLRT11"'CATIONOFW,4STE CONS71TUFNTSrinliert of3ttbmittitt uttalytugilddta (inethorlc .:.... . . 8240 and 8270) verifying that`the waste in question does not containorganic constitttntsotheYtin those 2uhich would nornl;41 i appear in analysis of viigin petroleum product residue, I ant submitting this Certieafe l'Yaste; Constituents. I certify that lant familiar with the source of contamination of the soil and furt-x#tify the source, to the best of tsty knowledge, contains no contatn.inants other than that listed ahove. 'Generators $�, mature: Date. TRfINSPOR?ER:'. Contact: r" f.t Phone: As the Carrier, I certify that ;the `materials described above. being shipped under this non -hazardous materials manifest are properly classified,:packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for': delivery to the facility designate. f' Carrier Signature: r' LI� Date .:, .0 -' - -4 TRUCK # _G 4 VOLUME -. ts- TRUCK DRIVER SIGNATURE.:' • ' C it ` DATE: t 0 7 I DESTINA 'ION Environmental Soils Inc. 910 Crowaer•Rd, Shelby, NC 28150 Dedicated -`Land Application Site Permit #SR0300038 I, certify;that the carrier has delivered .the materials described above to this facility,and I hereby accept this material for trea#merit and/or disposal iri a.ma'riner.that has been authorized by the Sate of North Carolina: j f Facty Signature _ 1` �; f --, ~ l r j •;. fir_ t / Date:'` r Signature: �% l � AI' .'•. »r• .� -, _= .. D �.ate: ..Gonmpany Name Title White/Facility Canary/Invoice . Pink/Carrier Goldenrod/Generator IM ENVIRONMENTAL SOILS, INC. PA. BOX 295 LATTIMORE, N.CC: 28086-0480 704/434-0075 (704) `434=9533 FAX Job Name: 4 Truck# 71=:,4 {'a141 4740 1#� 'r ,,GrossWgt,s ,Y.� < ;�,,; ' fiye t } , �f2 �+•�, �'.'%:. J.vl^••�'IL r'*�%3�>:�nN' Yf'ri!'1)w!",:a: tj .J %1 l i � ` f >>js�yy�vyy'isy�j�•+��YX h'd,+i r�t� "'�y�',vY,,jlif�'a"�r, '� L t r �l: F •;ti"r+. } '1 t i LSR e "'`j ?: 4-^ Net Wgt� tk, r NIP Xri + W Tons: ,1 > r Weighed by: Contact: s' - Phone F Fax: GENERJTOR 'Address, Count),: Conta 104- a Phone:^. IMSTV,O?`Complete Address: Class &Type A'Vk �€�fi��Me in soil YS Ig SOURCE OF L�111IV41'ION.• (ex. UST or other source) G1,'A R11TORS Cl RTIFICJTIONOFTVIISTE CONSTITUENTS. In lieu of submitting, analytical data (nuetljorls 8240 and 82 70),verifying that the.waste in question does not contain organic constituents other than those which would norfnahy appear in analysis oftr�tn petroleum product residue, I amsuhnAtting this Certificate of Waste Constituents. I cert�ft that l40�. ih» iliar with the source of contatnination of the soil and further certify the source, to the best.ofmy knowledge, contctt'iis no contantinants.other than that listed above. GeneratorsSignature: J Date TPUNSPORTER: f Contact: r 'y;' Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce. under the applicable regulations governing transportation, and I hereby reideiye this material for delivery to the facility designate. r Carrier Signature: - ;t , r Date: TRUCK #i l .. T VOLUME;'�1 TRUCK DRIVER SIGNATURE:4 t DATE: ,A�...; DESTINATION. Environmental Soils Inca}1 wdei Rd, Shelby; NC 28150 Dedicated Land Application Site Permit #SR0300038 1-certify that: the carrier has: delivered the .irtaterials described above to this facility, and I hereby accept this maYeiial for treatment and/or -.disposal in a manner that has .been authorized by the Sate of North Carolina. l Facility Signature: ` . i '> Date: Signature: i f L.: Date: .. r. Company Name t Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator E1bAironmental Soils Inc. PO Box 295 Lattimore; NC 28089 Phone 704-434-.0075 • Fax 704-434=9533 Novi-Hazazdous Waste Manifest # 2 1 4 1 4 Date{? Load Number (numbered sequentially as trucks are dispatched) ENMONMENTMI, CONS ULTWN`l. If s ,( V{ Contact: Phone: Otl " VI � Fax G NER11TOR: r i i'� Tyra �A _ Address —� ` �1r,tt�t; e�Erti{x,<:tJstf;#t C}�, £ County: Contact: ; , t �c Phone tt'YIS'II' ORICINJTIOIVPOIN:I' Complete; Address: y - C Class & Type of Contaminate in soil SOURCE OF CONLIIIIN<ITION.• (ex. UST or other source) GL'NFR,1ITORS CF-,RTIFICfITION OF WASTE CONSTITUENTS: In lieu of subfnitting analytical data (methods 8240 and S270) ver�ing that the waste ih question does not contain organic constituents other than hose which would normally appear zn arla6�sis of virgin petroleum product residue, I ant submitting this Certificate o�T,.as e z.. Constituents. I cert�'tl�atI am familiar with the source of contamination of the soil ald further cep ft y the source, to the best of nzy knogi ledge, contains no contaminants listed above. ' Generators Signattue:•Date;�IJA TRfINSPORTER: �' s Contact: 4, Phone: As the carrier, I certify that the materials described4bove being shipped under this;non-hazardous materials manifest are properly: classified, packaged, labeled, secured, and are in proper condition for transport:i'n commerce under the applic l��e:' lations governing transportation, and I hereby receive this:material for. delively tool facility design gte , Carrier Signature. ._._ram` i'g f } t�;'",� P; Date ' t`V � t TRUCf� # 'TAB # VC)I:,UIVI..,�.�3,{/ TRUCK DRIVER SIGNkniL E J'` :�k ,- ; ::.r ,� y� G' i DATE: ESINIITION Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land tApplication Site Permit #SR0300038 I certify that the carrier has delivered the materials described aboveto this `facility, and I Hereby accept this `material for :treatment and/or .disposal in a manner: -.that has been authorized by the :Sate of North Carolina. Facility Signature: Date = r f rr f Signature: /, t "'L lei.l `.� t:~r _ • �_�. Date: Company N P yame _ Title: _ White/Facility Canary/Invoice Pink/Carrier Goldenro-d/Generator 47400 lb Gross:Wgt..-- t r SY •i»�Yj r�r,,r r� Sl`, �v,r,��'.�r f�,`<X^�ra;F!r� i{ tf,.. j S +t Y MISS! _ �0�3 C ({({ t -1 f tlf {r; t 2 1 /a I W�ig�h�ct`b�i� I `Environmental Soils Inc. PO Box 295 - Lattirnore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 Non Hazardous Waste Manifest # 21415 Date Load Number (numbered sequentially as, trucks are dispatched) ENT17RONMENT11L CONSUET41vT. Phone: '�i 04-1- ISIS- Fax: Contact: GENEPUTOR: k' . . . . . . Address; County: 64, Contact: Phone: S t 01A POLVT Complete Address: I "V. WASTE OP1,01,117MYMN Class'&-'Fype of Contaminate in, soil. SO URGE OF CONT4MINATION.- (ex. UST or other source) GENE, RJTOR S CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmittin P, data (methods 8240 and Iii3g 46f the waste in question does not contain organic constituents other thaft t0tv!jichwould normally appear in analysis of irginpetroleum.product residue, I am submitting this Certificate of Waste Constituents. I cert� that Iamfamiliar with the source of contamination of the soil and further certifydje source, to the best of myknowledge, contains no contaminants other than that listed above. Generators Signature:-Y�2_, Date: LLL fl,;?- 61 TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are improper condition for transport in commerce ani s under the applicable reg`governing ernin tXansportation, and I hereby receive this material for delivery to the WPM facility designate. /�; Carrier S* ate: ignature:( D L TRUCK #: k" TAG #: VOLUME: 7 (i,' TRUCK DRIVER SIGNATURE: DATE: 41 A ;L DES.TINATION Envirohmdrfg -Soils Inc. 910 Crowdee'Ad, Shelby,: NC 28150 Dedicated LandApplication .:Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or-,d-isposal in a manner that has been authorized by the Sate of North Carolina. L Facility Signature: k/ Date: I I ? Signature: 1:: ' . Company Name Date: Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator 7z-. %.nr to vt"re'2Ynr 3Y yxrnex ENVIRONMENTAL SOILS, INC. - RO. BOX 295 LATTIMORE, N.C.28086-0489 704/434-0075 (704):434-9533 FAX a .t Job Name: Truck# 1. . 107 f rdssVf�i% } ht � 2 'LJ'1-s 'j�a Y`it%�� Environmental Soils Inc. PO Box 295 Lattimore, NC 28.0$9 Phone 704-434-0075 , Fax 704-434-9533 Non.=Hazardous Waste Manifest # 2144 8 Date ' `i ,' W Load Number (niimbeted sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTANT Contact. iris. # t r ; C ,,,� .: Phone f;� �'rf� �Y => Fax - - -- CENER11TOIZ Address: County ; Contact: M L:i a L ;, Phone o WASTE ORIGTIONPOIN? Complete Address _ r Ir} f[ 1 Class &'Iype of Contaminate in soil SO URGE OF CONLIMIAWT ION.- (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmitting analytical data (methods 8240 and 82 6) everEying that the waste in question does not contain organic constituents other than those whiehwould noi-nially appear in analysis of virgin petroleum product residue, I atrt submitting this Certificate of Waste Constituents. Icert�othatI am familiar with the source of contamination of the soil and farther certify the source, to the best of my hnoaoledge, contains no contaminants other than that listed above. Generators Signature; Date 01 t 1 6 TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and:are in proper condition for transport in commerce under the applicable regulations governing' transportation, and I hereby receive this material for `delivery to the facility designate ; Carrier Signature i'` .s ��,, E . Date: TRUCK #.� TAG # VOLUME ,— TRUCK DRIER SIGNATURE: " t. I DATE::. DESTINATION. • Envirrsrimerital Soils lne::910 Crovitder Rd� :Shelby, NC 28150 Dedicatedt d.Applieation Site �ertriit #SE0300038 I certify .that the carrier;has delivered the materials described above to this .facility; and I -hereby accept this rriaterial for treatment and/or -disposal in a.inanricr that has bo-6n authorized by the Sate of North Carolina. { � ' f Facility Signature J r -t �,j y� :+ f>' Date: t r f Signature. i .. 1 Date: Company Name Title: White/FacilityCanary/Invoice Pink/Carrier Goldenrod/Generator ENV II 'CJNMENUL SOILS, INC. P.O. BOX 29b LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# l 1'30 pt1 4/ 1./' 00? 56 40 rb F? Gross Wgt. iJ ` Tare Wgt:,��'� ±" a LV yy. Net Wgt. Tons: Weighed by: Environmental Soils Inch PO Box 295 Lattimore, NC 28089 i Phone 704-434-0075 . Fax 704-434-9533 Non -Hazardous Waste Manifest # 21413 Date Load Number, (numbered sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTIN7 i Contact _ ; , 4 Phone ? Fax: GENER4TOR Address: t i s i is County: Contact: i � r� , r s ;::: -,� -W— Y-s.r.a _. _ _ _ Phone ; r.. (, tar �r: TV14ST.E OR-10IN T tONPOIAT Complete Address: C i ! t Class .TOP,mate in soil SOURGI OI{'C,Y" y i 1 EITION. {ex. UST or other source) GENERATORS CER7"IIi IC11TlON OF W-ISTT CONS , ,2'�IEN'lS: In lieu of submitting analytical data (nnethods 8240 and 8270)vertfj iq that the waste in question does.1.notrc i`i�#'tatit os-ganky6nstitrsents other than those which would normally appear tn;t �szsvtrrttrole roductr¢�tbrm submtitt�t this Cerisate of Waste Constituents. Z certt�1 utrrt faa!•�tvit =the:souree o/� c�ritatrnt�t�n o]�1t�iei"l and 7/7t(Y'eY cert2J( the source to the best of my krronvltY � tEAFt3t3:no f$tf atht>rdnis other than that listed above. . Generators Signature: w _ `tSr _ Date ,,. TMNSPORTER: .Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, pacl aged labeled; secured, and are< h proper condition -for transport in commerce under. the applicable regulations governing transportation, and I hereby reeei�e this material for delivery to the facility designate. Carrier Signature: Date: T12UGK T111 VOLUME 1 " TRtJK DF�VER SIGNATU., r .r l7ATE s� t :1EST7N12"lON Erivir6nmerital Soils Inc. 910 Crowder Rd, Shelby, NC 1950 ]�edtcated Land Application Site erin t #9R0300038 I certify that the carrier has delivered the materials described above to this facility; and I hereby accept this material for treatment.and/or,dis a in -a manner that ha eni authorized by the Sate of North Carolinal Facility Signature: ! Date: oignacurm..,, i f , _� �2:- , F ; t 1- - t Company Name `� = Titlei i /f White/Facility. ... Canary/Invoice Pink/Carrier Goldenrod/Generator Weighed by: Contact: fi_ i fit }� �; .E PhoIle%�... cil1 c a I'3J{: GENER,4T OR i ,, , f ;;', ;y r , fi' Address: ' k j_i`t 1 i .4 4.� 'tl•�Y f t=1`rt T 1�4 ". 1 � s d�'� _i ' County: Contact: 4 1 Phone: <fg 0lj� — WASTE OR r6,fN17'XONPOINY' Complete Address: }�i:: r�I Class &'Iyhe of Contaminate in soil SOURCE OF GONTAAYIN ATION.• (ex. UST or other source) GENER,4TORS CERTIFICfITIONOF`MISTE CONSTITUENT In lieu ofsubmitting analytical data (methods Alz 8240 and 82i0) ver�0ing that the waste in question flocs not contain ozganic constituents other than'tljose <ivbichwoua: normally ap pear in analysis of tirgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I certio that Ianz familiar with the source of contamination of the soil and further cert�o the source, fo the best of yny knowledge, contains no contaminants other than that listed above. Generators Signature:,.' 1�-`� Date ,_43-,471 TMNSPORTER Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous rinaterials,; manifest are properly classified, packaged, labeled, secured, and are. in prop rtotidition for transport. n.:comrnerce under the applicable regulations governing i*46' ortation, and I hereby recew.6 this material far delivery --.6 the facility designate. Carrier Signature: Tate: TRUCK #: ► ter,} cs i TAG #: VOLUME: TRUCK DRIVER SIGNATURE: ';�f, , ,ry ? _;; ; . DATE. DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shglby, NC 28150 Dedicated Land Application Site Permit #SRO3 38 - I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or.dispgsal in a manner that has been authorized by the Sate of North Carolina. , Facility Signature: Date: Signature: E a �..... Date: Company Name Title: White/Facility Canary/Invoice . , Pink/Carrier Goldenrod/Generator ' X i Environmental Soils Inc' PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 -,Fax 704-434-9533 Non -Hazardous Waste Manifest lk 21417 Date �~ri r` r;<` Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTIINT Contact; ' ���/,l/f,¢1 ; C, S,)ti1�;,isR: Phone,,, GE NE, RA Address: Coug�S' Conta ,; 5 < ' x ` x ,� f».�}�� _ _ Phon"f k ` 1 ,, o > Vic, �. W11STL� bC` T Complete Address: :AIV. Class &Type of Contamid� SOURCE OF CON ( ''k (ex: UST or other source) GENE,RJTORS CERIIIIC.�ONOFTF,4STE CONSTITUENTS: In liens ofsifbnattCttt �t l�,vealdata (methods 8240 and 8270) ver ing tit t re zvnste in question does not Colrtaitz organic constituents ��1��t,�d>�r�"ose which would normally appear in i7i is of witgin petroleum product residue; I am suhmitti"ng this Certificate of `Waste Cotzstituetzts., I cent f thhtl attz familiar with the source of contamination of soil and further cent the source, to he hest of ntyknowledge, contains no contaminants other than that listed ahorve. Generators Signaturesf' Date h TR,4NSP0R7'ER.f Contact: Phone: As the carrier; I certify that the materials described above being shipped under this non -Hazardous materials manifest are;properly'classified, packaged, labe10,,secured, and are in proper condition for transport in commerce under the applicable �e"ulations goyernt . trans tortation; and l.hereby receive this material for delivery to'th-e facility designate. Carrier Signature: t:•- ;--�r Date: TRUCK#:r��G�� VOLUME [A� r TRUCK DRIVER SIGNATURE DATE: fi i DESTINATION. Environmental Soils Inc. 910 Crowder.Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the -carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disRosal in a manner that has. been authorized by the Sate of North Carolina. {j, n fig/ Facility Signature: ;4, 4 `='- Date: ! ! �' .} 6 �i�y�;, Signature: i;� ;�- " --- f --Date: Company Name'-- Title: White/Facility : Canary/Invoice Pink/Carrier Goldenrod/Generator f Environmental Soils Inc.` PO Boa 295 • Lattimore, NC 28089 Phone 704-43-0075 •Fax 704=434-9533 Non Hazardous Waste Manifest # 21419 Date 4j Load Number (numbered sequentially as trucks are dispatched) F,ATMONMENT4L CONSULMNT 3 Contact: _ i Phone: Y ( 1 i { -- hax: 1 GFIVE12,1TOR: Address�; - -: --- _ .county: Phone: } f IWSTT' ORIGIAtAl?ONPOINT CoPnplete .Address; Class &Type of Cotut"aminate in soil SOURCE OFCOI\J tV111 11TIO1V (ex. UST or other source) ; GENE Rf1TOR S CERT IFICATION OF JVASTE CONSTITUENTS: Iit lieu ofsitbin itting a72alyttca1 data (in etbods 8240 and 8270) ver�oing that the waste in question does,not contain organic constituents other than those which would nornnally appear in analysis_of virgin petroleum product residue, I am submitting this. CertOcate of Waste Constituents. I certify that l am fiimiliar with the, source of contamination of the soil aind further certify the source; to the best of myknowledge, contaits no contaminants other than that li ted abo e. Generators Signature:_ s Date: TR,4NSPORTER Contact: Phone: As the carrier, I'certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured; and are in proper condition for transport it! commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: _ TRUCK #: wrclt/ y f , VOLUME:I..: I TRUCK DRIVER SIGNATURE: -'�-`'. DATE: DESTIMTION.• Environmental Soils Inc 910 Czov der -Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR030003$ . I certify that -the carrier has delivered the materials described: above to this facility, and I hereby accept this material l in a manner that has been authorized by the Sate of-Nortl Carolina: for treatment and/or.:disposa Facility Signature 1 l 1`j V Signature: J .�` ;Ir,) - Date: (, . Company Name -> Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator 4vironmental Soils Inca PO Box 295 Lattimore, NC 28089 ' Phone,704A34:.0075 • Fax t4-434=9533 Non_Hazardous Waste Manifest # 2 i 2 Date "..1 Load Number (numbered sequentially astrucks are dispatched) ENHIRONMENE4L CONSULZflN Contact: 1 1 1 >) P11o1Ze 1 i �` F }C: 4 _ GENEI L4TOR: r Address 3k`tY L tllf1g'iallk,County Contact Phone:�:tt W4STE ORIGINIITIONPOINT.'lComplete Address: Class &Type of Contaminate in soil SOURCE OF CONE MINWTION.• (ex. UST or other source) r GENERATORS CERTIFICATION OF iVASTE CONSTITUENTS: In lieu ofstibmitting analy''tical data methods 8240 and 8270) ver'4ng that the waste in question does not contain organic'constituents other than those which would normally appear to analysis of virginpetroleumproduct residue, Iant submitting this Cert f sate of Waste Constituents: I certify that I am familiar wig the source,,of contamination of the soil and further "certify the source, to the best of my hnowledge, contaitts' :o contaminants tither than thtitlisted above. Generators Signature:- : J4.1 2 Date: TRANSPORTER: Contacts Phone: As the carrier, I certify that the materials.described.abtwe being shipped under this non -hazardous matcnals manifest are properly classified, package; labeled, seCtired, and arein proper condition for transport in commerce under the applicable regulations;goyerning transportation, and I hereby receive this material for delivery to the facility;:desigriate: Carver Signature: Date: TRUCK #, i - - VtOLi�ME• 1 TRUCK DRIVER SIGNATURE t` �. :� : DA�'E: DESTI�VX�70N.• Fnvironni tal'Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Applic2ition Site Permit #SR0300038 I certify .that the carrier has delivered the materials described above "to this facility, and 1 hereby accept this material ..._.. for treatment and/ar dis. osal in a manner that has been authorized by the Sate of North Carolina: DSignature: j `; ; ; Z// %r ..... g. - ' L ` ' ti' ate: Facility . f i Signature: t..-- Date: Company Name '�- _ Title: White/Facility C-anary/Invoice, Pink/Carrier Goldenrod/Generator ENVIRONMENAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Class &Type of Contarninate in soil SOURCE OFCOMMMINATION.• (ex. UST or other source) OENER.11TORS CERTIMCJTIONOF JMSTE CONSTITUENTS: In lieu of submitting analytical data (inethods 8M itt d U- 70) ver fling that the waste in question does not contain organic constituentsother than those which 2uould nortna11y arliear in analysis of viegin petroleutn productresidue, I ant submitting this Certificate of Waste Constituents. I certify that l,am fantiliar with the source of contamination of the soil and firth" e rtifyihe source; to the best of my knowledge, contain?s no contaminants other "tban that listed above. Generators Signature x- r , ' :'•.:, Date.(" TRANSPORTER: Contact: Phone: As the carrier; I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations:governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: �, TRUCK #: ;TAG:# VOLUME. TRUCK DRIVER SIGNATURE S � <� ' �.:'� DATE: DESTIMMON.• Environmental Soils Inca 910 Crowder Rd, Shelby, NC28150 Dedicated Land Application ' Site Permit#SR0300038 I certify:that the carrier has. delivered the materials described above to this facility, and thereby thkrhaterial for treatment and/or disTosg in a• manner that.has been authorized ''by the:Sate of North Carolina, Facility Signature:] .1. �'. �--~ Date r � , Signature: r` r-: ' �. ,. 1. c F Date: r' ; Company Name Title: White/Facility Canary/Invoice I I : Pink/Carrier Goldenrod/Generator Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 21. 4 . i Date ENVIRONMENTAL CONSULTANT Contact: GENERATOR: Address: Load Number (numbered sequentially as trucks are dispatched) Phone: Fax: County: Contact: Phone: WASTE ORIGINATIONPOINT Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION. (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods 8240 and 8270) ver�htg that the waste in question does not contain organic constituents other than those whirls would normally appear in analysis of virgin petroleunt product residue, I am submitting this Certacate of Waste Constituents. I certify that I ain familiar with the source of contamination of the soil and ficrtber certify the source, to the best of nay knowledge, contains no contaminants other than that listed above. Generators Signature: Date: ' TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: TRUCK DRIVER SIGNATURE: DATE: DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. p O. BOX 295 LATTIMORE, N:C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: Tare W gt: Net Wgt.: Tons: Weighed by: Environmental Soils Inca" PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # Date ' Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTANT Contact: Phone: Fax: GENERATOR: Address: County: Contact: Phone: WASTE ORIGINATIONPOINT Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION.• (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmitting analytical data (:netbods 8240 and 8270) vertrying that the waste in tguestion does not contain organic constituents other than those which would normally appear in analysis o f virgin petroleum product residue, lam submitting this Certificate of Waste Constituents. I certify that I ani familiar with the source of contamination of the soil and fitrther cert q the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TRUCK DRIVER SIGNATURE: TAG #: VOLUME: DATE: DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENWRONMENTAL SOILS, INC. P.O. BOX. 295 LATTIMORE, h*C. 28086-0489 7041434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 ° Fax 704-434-9533 Non -Hazardous Waste Manifest #21442 Date ENVIRONMENTAL CONSULTANT Load Number (numbered sequentially as trucks are dispatched) Contact: Phone: Fax: GENERATOR: Address: County: Contact: Phone: WASTE OR.IGINATIONPOIN7: Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION. (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitti ng analytical data (methods 8240 and 8270) very�ing that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I ant submitting this Certificate of Waste Constituents. I cert�5 that I ani familiar with the source of contamination of the soil and further certq� the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: TRUCK DRIVER SIGNATURE: DATE: DESTINATION Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Company Name Date: Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 2 .,�'� A 4 3 Date ENVIRONMENTAL CONSULTANT Contact: GENERATOR: Load Number ,�)3 . l6) 5,TC) (numbered sequentially as trucks are dispatched) Phone: Fax: Address: County: Contact: Phone: WASTE ORIGINATIONPOINT Complete Address: Class &.Type of Contaminate in soil SOURCE OF CONTAMINATION.• (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lien of submitting analytical data (wetbods 8240 and 82 70) verf�utg that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petr oleum pi-od:tct residue, I ant submitting this Certiftcate of Waste Constituents. I cettify that 1 am familiar with the source of contamination of the soil and furtber certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: r.: .: Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: - Date: TRUCK #: TAG #: VOLUME: — TRUCK DRIVER SIGNATURE: DATE: DESTINATION Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28686-0489 704/434-0075 (704) 434-9533. FAX Job Name:. Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: - Environmental Soils Inc. PO Box 295 • Lattimore, NC 28099 Phone 704-434-0075 • Fax 704-434-9533 r38 a Non -Hazardous Waste Manifest # 2 1. Date Load Number (numbered sequentially as trucks are dispatched) ENYIRONMENTAL CONSULTANT Phone: Fax: Contact: GENERATOR. Address: County: Contact: I,YASTE ORIGINATIONPOINT Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION. (ex. UST or other source) Phone: GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods 8240 and 8270) very�ing that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I am suhmitting this Certyicate of Waste Constituents. I certify thatl ant familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: . Date: TX INSPORTER. C Phone: ontact. As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature:: Date: TRUCK #: TAG #: VOLUME: .:.... TRUCK DRIVER SIGNATURE: DATE:; DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Company Name Date: Title- w hite/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATi`IMORE, N.C. 28086-0489 7041434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: Environmental Soils Inc. -- PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest # 21 l 47 Date ENVIRONMENTAL CONSULTANT: Contact: Load Number (numbered sequentially as trucks are dispatched) Phone: Fax: GENERATOR: Address: County: Contact: WASTE ORIGEVATIONPOINT Complete Address: Class &,Type of Contaminate in soil SOURCE OF CONTAMINATION.- (ex. UST or other source) Phone: GENF,RdTORS CERTIFICATION OF bYASTE CONSTITUENTS. In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in rluestion does not contain organic cotutituents other than those which would normally appear in analysis of tiirgin petroleum product residue, I anz submitting this Certificate of I'Vaste Cotastituetits. I certify that I am faynillar with the source of contamination of the soil and further certify the source, to the best of stay knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: C on tact• Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TRUCK DRIVER SIGNATURE: TAG #: VOLUME: DATE: DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Signature: Company Name White/Facility Date: Date: Title: Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 296 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: — Tare Wgt: Net Wgt.: Tons• Weighed by: Environmental Soils Inc. PO Box 295 Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 No i-Hazardous Waste Manifest # 214 4 9 Date ;'``iI Load Number i(numbered sequentially as trucks are dispatched) ENVIROMWENT1II CONSULTANT Contact: Phone t} `5 t/ r Fax. 1 GENERrITOP. Address:my.,+:wt4 County: A 1 Contact: ! L 1.. Phone: i `Sly '�'t WASTE ORIG MQV POINT Complete Address 210 i A, Class &Type of Contaminate in soil ff SOURCE OFCONE4MIN_4TION.- (ex. UST or other source) i, 7 GENERATORS CERTIFICfITION OF IVASTE CONSTITUENTS. In lien of submitting analytical data (»zethods 8240 and `8270) verifying that the waste in question sloes not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I ant submitting this Certificate of [ [Taste Constitrtettts:I cert1, tatl am an�.iliar with the source o contamination o soil the soand rther certj `zhf f f 6 the source, to the best of my knowle ., t) contains no contaminants other.tban that listed above. �. Generators'Signature� �� Date c1 `>",-J !'Rfi'1VSPORTER. contact: Phone: As the carrier; I certify that the m4ferii&Aescribed ab ove being shipped under this non -hazardous materials manifest are properly classified, pack�g+d labeled, secured, and are in proper condition for transport in commerce under the applicable regulations govt. ning transportation, and I hereby receive this material for delivery to the facility designate f ,t Carrier Signature < . Date: ref✓,�- TRUCK #: � TAG #• VOLVlVXME: E. TRUCK DRIVER SIdNAT'URE: ;r` f , DATE: DESTINJTION., Environmental Soils Inc: 910 Crowder Rd, Shelby;- NC 28150 Dedicated Enid A iOh atiion' Site Permit#SR0300038 I eertity tliat the; carrier has delivered the materials described above to this facility, arlrl"I h b' accept this material for.tre.at-ment aiid/or disposal in a manner thathas been authorized by the Sate of North' Carolina. , FacilitySignature: - ti} i i —' 1� �:-4_ fr �� �' Date: Signature: -0.;'`y Date: Company Name Title: I - ,: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-6075 (704) 434-9533 FAX # 0 Environmental Soil" ffc PO`Box 295�•�L.attimore, NC 28089 Phone `704-434-007�-- Fa- '704-434-953-3 Norm -Hazardous' Vastc:Manifes ' # Z 14 b v Date t r. Load Number' numbered sequentially as trtrcics are dispatched) M�,h ENVIRONNIL;NTAL CONSULTANT Contact: Phone. Z+LJL- Fax: GENE'KdTOR: C..",r1 l z_f Address: rv.' f �Lit�r f f: r�. County Phone. COIltaCt t' .� 1 y' . L:= ri ' r f . it ,a. WASTE 012I6 fITIONPOINT. Complete Address: t Class &:Type'of Contaminate"iri soil" . SOURCE OF CONTAMINATION.- (ex. UST or other source) GENERATORS C16RZT'IFICATI0N OF MSTE CONSTITUENTS: In lieu of submitting analytie#t�� to (methods 8240 and UM) ve1`E' tt %i![i;t, e waste in questiondoes not contain organic constituents oilier than tl3d i b-woisld ttorntall a ear in anal s '�d , ix in. etrolertsst rodiict residue I afst subntittin this Certificate o Wasfe Y p15 Y,' g p p gf Constituents. l cert thatl atrt familiar with the soatrce of contamination of the soil and further cerlfcyFtbe source, to the hest of zny knowledge, contains no contaminants otb&,thayt that listed above. Generators-Signature%i� ✓�.T -�.? �f Date �,'.-� ram-- �; TPMNSPORTER: .Contact: Phone: As the -carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce .under tl�e applicable regul4 ons overnin nsportation, and I her y� receive this material for delivery to the facility designate. {2� f Gamier Signature: Date: TRUCK #: AT. # /� Vf3 UME r 1 TRUCK DRIVER SIGNATURE:.. ! .`�� DATES `/ DE,STINrq :ION•:: Environmental Soils Inc. 910 Crowde-r Rd, : lielby, NC 28150 Dedicated Land Application r Site Permit #SR0300038 r I certify that the carrier has. delivered the materials described above.to this "facility, and I hereby kc-ept skis rriaterial. for treatment and/or disposal ina.rnanner that -has beers authorized by the Sate of North Careliha:, Facility Signaturg-``,r `; t °_ t%"'.f Date: Signature: i Date: ry'. .' `r Company. Name .. Title: White/Facility.. Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LdI` WORE, lq.C. 2g086 0489 704/434-0075 (704) 434-9533 FAX Joky N�m� 1 Truck# Pill Grass Wgt.: rr Tare Net Wgt.- T04 ; Weighed by: _:.u:LLi.�.++� Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 1_ 422 Date i Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTINT Contact: Phone: Fax: GENER,4TOR: Address: County: Contact: Phone: W 1STF. ORIGINflTIONPOINT Complete Address: Class &Type of Contaminate in soil SOURCE OF CONE1MDVATION.• (ex. UST or other source) GENERATORS CERTIFICATION OF WhiSTE CONSTITUENTS: In lieu of submitting analytical data (inethod r 8240 and 8270) ver f ing that the waste in question does not contain organic constituents other than those which would tzorrnally appear in analysis of virgin petroleum product residue, l anz submitting this Certificate of Waste Constituents. I certify that I anz familiar with the source of contamination of the soil and further certf� the source, to the best of nzy knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER - Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest sue properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the . facility designate. Carrier Signature: Date: TRUCK #: TRUCK DRIVER SIGNATURE: TAG #: VOLUME: DATE: DESTINWTION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Company Name Date: Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator EN . VIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 86-0489 704/434-0075 (704) 434-9533 FAX Job Name* Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: - Date Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest # 2.14 4 Load Number (numbered sequentially as trucks are dispatched) EAWIRONMENT4L CONSULTANT Contact: Phone: Fax: GENERATOR: Address: County: Contact: Phone: WASTE ORIGIN47YONPOINT? Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION.- (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data (methods 8240 and 8270) verifidng that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I an: submitting this Certificate of Waste Constituents. I certb� that antfamiliar with the source of contamination of the soil and further cert6 the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: TRUCI{ DRIVER SIGNATURE: DATE: DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: - Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL aO1LS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075- Fax 704-434-9533 Non -Hazardous Waste Manifest # 2 . 18, Date ENVIRONMENTAL CONSULTANT - Contact: GENERATOR: Address: Load Number (numbered sequentially as trucks are dispatched) Phone: Fax: County: Contact: Phone: WASTE ORIGINATIONPOINT Complete Address: Class &'Type of Contaminate in soil SOURCE OF CONTAMINATION. (ex. UST or other source) GENEX4TORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu ofsubmittinganalyticaldata (n:etbods 8240 and 8270) ver Being that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I ant submitting this Certificate of Waste Constituents. I certify that I ant familiar with the source of contantination of the soil and further cert6 the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier. Signature: Date: _ TRUCK #: TAG #: VOLUME: — TRUCK DRIVER SIGNATURE: DATE: DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS;-INC. P.O BOX 295 LATTIMORE, N.C. 28086-0489 704J434-4075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: Date ;. Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 2 �. 4 2y 1: Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTANT Contact: Phone: Fax: GENERATOR, - Address: County: Contact: WASTE ORIGINATIONPOINT Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION (ex. UST or other source) Phone: GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum: product residue, I asn submitting this Certificate of Waste Constituents. I cert j& that I ant familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: Contact. Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: _ TRUCK DRIVER SIGNATURE: DATE: DESTINATION: Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-9533 FAX Job Name: Truck# Gross Wgt.: _ Tare Wgt: Net Wgt.: Tons: Weighed by: Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 �� Non -Hazardous Waste Manifest # 2 1 Date ENVIRONMENTIiL CONSULTANT: Contact: Load Number (numbered sequentially as trucks are dispatched) Phone: Fax: GENERATOR: Address: County: Contact: Phone: WASTE ORIGINATIONPOINT.• Complete Address: Class &.Type of Contaminate in soil SOURCE: OFCONTAMINATION.• (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu ofsubmitting analytical data (methods 8240 and 8270) verq�ing that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste Constituents. I certio that I ani familiar with the source of rnntasnination of the soil andfurther cent the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signatu TRANSPORTER: Date: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Dare: Carrier Signature: TRUCK #: TRUCK DRIVER SIGNATURE: TAG #: VOLUME: DATE: DESTINATION.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Signature: Company Name White/Facility Canary/Invoice Date: Title: Pink/Carrier Date: Goldenrod/Generator cNVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-0075 (704) 434-0533 FAX Job Name: Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons• Weighed by: ITUFENTS: In lieu contain orffanzccqx hie, I aw subh" Intamination of the, it that listed above. YW,LVSP0RWffR.- Date: Contact- Phone: As the carrier, I certify that the materials described above bcing shipped under this non -hazardous materials manifest are properly classified, packaged; labeled, secured, and are in proper condition for transport in,commercd-, under the applicable r6giilations governing. -trans V(rtation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: --Z — TRUCK TAG # VOLUME: TRUCK DRIVER SIGNATURE: DATE: DESTINATION.• Environmental Soils Inc. 910 Crowder Rd Shelby, NC28150 Dedicated Land Ap'-plication Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this, facility, and I hereby accepts this material for treatment and/or�-4vosatin a manner that has been authorized by the Sate of North Carolina. ig C: ]Facility S' Date. qatqr ���, �, 1. / % c' . t_ Date.._``. Signature . Company Name Title: .White/Facility Canary/Invoice Pink/Carrier 'Qolde*od/Generator Environmental Soils Inc. POBox295 -:Lattimore, NC 28089 Phone 704-434-0075 • Fax 704=434-9533 Non=hlazardous Waste Manifest # 214 25 Date ' i '-i Load Number (numbei sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTANT i I Contact - `,� . �i�'�1 Phone _ td Fax: GENERATOR , t Address - J i 's'14�_,� s-:t ; ; i „ f r County Contact t, �r:l'�,. -- Phone 4iF- . i�F�ISlE ORI��'IOIVPOINT.• CoInplete Address: Class &T}ape of Contaminate in sod SOURCE OF CON�TION.• (ex: UST or other source) 1 i GEATER.lTORS CERTIFIC4TIONOF N7,4STE CONSTITUENTS: In lieu of submitting analytical data methods 8240 and 8270) ver��ftgaliat the waste in ,question does not contain organic constituents other than those which would ngrmally appear in analysis of virginpetroleuin'prodtict residue, I am submitting. this Certificate of Waste Constituents. I cert f�, that asn familiar with the source of contamination of the soil and further certthe source, to the best of my knowledge; contains no contaminants other than that listed above. Generators Signature < a i Date i TRJNSPORTER: Contact: Phone: As the carrier, I certify thax-tlje materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are iq proper condition for t" ansport in commerce 1 :under the,applicable regulations governing transportation, and I heteby receive this material for delivery to the facility designate. Carrier Signature: Dater :.: r / , ' ;' TRUCK # :� TAG #.... VOLUME: .5 `1l 7/ 40 TRUCK DRIVER SIGNATURE DATE. - DESTINATION.- Environmental: Soils Inc. 910 Crowder Rd,•Shelby, NC 28150 Dedicated Land Application _ Site Permit #SR0300038 I certify that the Carrier has delivered the materials described above to this facility; and I hereby accept this material for treatment and/at: isposal in' a;manner that has been authorized by the Sate of North Carolina../ Facility Signature.-, j- 1 ; { E ! lJ:_ Date % Signature,! Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldeiirod/Generator Environmental Soils Inc. PO Box 295 • Lattimore, NC 280,99 c, Phone 704-434475 Fax 704-434-9533 Non -Hazardous Waste Manifest # 23365 D"ate r , �; l - ;: ,:1 Load Number _ _ , �x`] [ r (( (numbered sequen-tytially as trucks are dispatched} %1 cA 7C..t) ���r - �J - -� Fax: /�%�r.. L`�/ rye.. 1 f ui VT�v�iJ �� i��� T j' Y- K'l{LM •v l., 11' } Y• iyu% G A ' a { i ! ( - 1. �� - '� �- County: � w.• r x,•�,y„�•.f ,t,>i•"vre 1 �. x ! � ¢'fit, +'g,j.''�, a �E >�'n$°a;. P� e 4� �c ,� 3 r:C i4'K�7,..: y.'C'.4 f ��t} )� °..�i., �;y :;'�rw.>.;'f Y X' '%7!'i • •x: ii' y, ! i �`1� .. ia>'y'Ks'�;,..;�az-•"+l3#r,•E:3.-;,iq,•s u rt _4 .ys: j' V'.^ �'bPl eL.!•d`: . ;.: y_ "��<�,`nsri`,�i alar)$?zur �wx,:a? ,t o�iF V:vS = • ,ass + •� - r r source) ("AEffi �, :?:»o;; tti;> Via# t. i ...',;?;*,$..•",:''!'!. .t 1�`,:. VS117VENT�S': In ien of submtttt tp ci�tat is al datu;j%ihe I o '.+` i g .�a. �:.�..•^�:,+, O "t . ��?!.:5; 5.. r �� , ,.e aEkftid tltal <l�0 s izot coittaztr orbctl3iC tOf�4ittrlcnts otl.�er than tbse 2vrJi.10 � '°3t`•y.;9ni 3` x ;•a, �, r y R_ F x dz'f vi%ti a /' j�y/ 9f°,'•istGtl 0%(��1" i2(jl�Ptfo�eittiresicl�te,Lasn'subt�I�ili thzq Gerd sate oJrL�Qy(to ^k ,flrt'Raintnilra, zv2tlsdtrt of contasrt�nYttto�t t13e toil nnf`urtller certthe source, to (' Yl f tTtti6 v eige, contatri3 p cottir t � S� tease that l'is`fed'rt owe. Gencramrs'Sgnature ' �' '�' Tate: IIL VS] ORTER CON Abtl+�.� Phone: � �s As Aii'carrier, I certify that the materials described above being shipped tinder this non -hazardous materials manifest are properly classified, packaged, labeled, secured; and are 'in proper condition for:transport in commerce under the applicable regulations governing transportation, and'I hereby receive this,material for delivery to the facility designate:. Carrier Signature: Date: TRUCK #: TAG #: VOLUME -,- TRUCK DRIVER SIGNATURE: DATE: DESTINATION..- Environmental Soils Inc. 910 Crowder Rd; Shelby, NC 28150 Dedicated Land Application: Site Permit #SR0300038 I certifv that the carrier has delivered the materials described aboveto this facility, and I hereby accept this material for treatment and/or dj sal in a rnanr er thathas been authorized'byahe Sate of North Carolitla. Facility Sig ature: l i yNJ —�" Date: / an, - Date: --,any Name �"". .> l Title: '-/Facility' Canary/Invoice Pink/Carrier Goldenrod/Generator Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 _, -P-Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 2J. 4 .;..1 Date Load Number (numbered sequentially as trucks are dispatched) EATHRONMENT4L CONSULTANT Contact: Phone: GENERATOR: [`nn to rt• WASTE ORIGINATIONPOINT Complete Address: Class &- Type of Contaminate in soil SOURCE OF CONTAMINATION. (ex. UST or other source) Fax: County: Phone: GENERATORS CERTIFICATION OF WASTE CONSTITUENTS- Its lieu ofs"bm:itting analytical data (methods 8240 and 8270) vertrying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin pets oleuns product residue, I am submitting this Certificate of Waste Constituents. I certify thatl ans fafniliar with the source of contamination of the soil and further cert� the source, to the best of may knowledge, contains no contaminants other than that listed above. Generators Signature- Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: — TRUCK DRIVER SIGNATURE: DATE: DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 704/434-00'i� (704) 434-9533 FAX Job Name. Truck# Gross Wgt.: Tare Wgt: Net Wgt.: Tons: Weighed by: APPENDIX 5 April 24, 2007 Client: ENVIROASSESSMENTS 9307 MONROE RD., SUITE K CHARLOTTE, NC 28270 Attn: AMANDA PETOSKEY SAMPLE IDENTIFICATION S-5 S-1 S-2 S-3 S-4 MADEP EPH, MADEP VPH analysis performed at Lab ID: 647 Samples were received into laboratory at a temperature of 3.00 °C. 4310 East Anderson Road Orlando, FL 32812' 800-851-2560 • Fax 407-856-0885 Work Order: OQD0273 Project Name: N. TRYON ST. PROPERTY Project Number: 07-6797.1 Date Received: 04/18/07 LAB NUMBER COLLECTION DATE AND TIME OQD0273-01 04/17/07 12:00 OQD0273-02 04/17/07 13:00 OQD0273-03 04/17/07 13:05 OQD0273-04 04/17/07 13:10 OQD0273-05 04/17/07 13:15 An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager. Any opinions, if expressed, are outside the scope of the Laboratory's accreditation. This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is privileged and confidential. If you are not the intended recipient, or the employee or agent responsible for delivering this material to the intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you have recieved this material in error, please notify us immediately. Results are reported on a wet weight basis unless otherwise noted The reported results were obtained in compliance with 2003 NELAC standards unless otherwise noted. These results relate only to the items tested Estimated uncertainty is available upon request. North Carolina Certification Number: DWQ ID # 327, NCPH ID #12708 This report has been electronically signed. Approved By: TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page] of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560 • Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-5 - Lab Number: OQD0273-01 - Matrix: Solid/Soil Dil CAS 4 Analyte Result Q ------------------------------ Units PQL Factor ---------- Dat�iimme ------------- By -------------------------- Method Batch .... I ------ ------------- ---------- --------------- General Chemistry Parameters -------------- NA %Solids 75.6 % 0.100 1 04/19/07 16:00 RRP EPA 160.3 7D19040 Volatile Organic Compounds by EPA Method 8260B 630-20-6 1,1,1,2-Tetrachloroetham ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 9260B 71)18028 71-55-6 l,l,t-Trichloroedme ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA9260D 71)18028 79-34-5 1,1,2,2-Tetrachloroethane ND ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 9260B 7DIS028 79-00-5 1,1,2-Trichloroedmne ND ug/kgdry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DIS028 75-34-3 I,l-Dichloroethane ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 75-35-4 l,l-Dichloroethene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 563-58-6 ],I-Dichloropropene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 87-61-6 1,2,3-Trichlorobenzene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI8028 %-184 1,2,3-Trichloropropane ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260E 7D18028 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 8260B 7DI8028 95-63-6 1,2,4-Trimethylbenzene ND ug/kg dry 7.25 1 04/1V07 13:39 JWT EPA 8260B 7D18028 %-12-8 1,2-Dibromo-3-chloropropane ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI8028 106-93-4 1,2-Dibromoethane (EDB) NO ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI9028 95-50-1 1,2-Dichlorobenzene ND ug/kgdry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DIS028 107-06-2 1,2-Dichloroethane ND tgAg dry 7.25 1 04/18/07 13:39 JWT EPA 8260E 71118028 78-87-5 1,2-Dichloropropane ND Ll ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18029 108-67-8 1,3,5-Trimethylbenzene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI8029 541-73-1 1,3-Dichlorobenzene ND ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 8260B 7D18028 142-28-9 1,3-Dichloropropane ND ug/kg dry 7.25 l 04/19/07 13:39 JWT EPA 8260B 7DI8028 106.46-7 1,4-Dichlorobenzene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI8028 594-20-7 2,2-Dichloropropane ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 78-93-3 2-Butanone ND ug/kgdry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 110-75-8 2-Chloroethylvinyl ether ND M2 ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 95-49-8 2-Chlorotoluene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DIS028 591-78-6 2-Hexanone ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 79-46-9 2-Nitropropane ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 106.43.4 4-Chlorotoluene ND ughg dry 7.25 1 04/18/07 13:39 JWT EPA 8260E 7D18028 108-10-1 4-Methyl-2-pentanone ND ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 8260E 7DIS028 67-64-1 Acetone ND ug/kg dry 7.25 l 04/18/07 13:39 JWT EPA 8260B 7D18028 7143-2 Benzene ND ug/kg dry 0.725 1 04/18/07 13:39 JWT EPA 8260B 7D18028 108-86-1 Bromobenzene ND ug/kgdry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI8028 74-97-5 Bromochloromethane ND LI ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DIS028 75-27-4 Bromodichloromethane ND ug/kg dry 7.25 l 04/18/07 13:39 JWT EPA 8260B 7DIS028 75-25-2 Bromoform ND ug/kgdry 7.25 1 04/19/07 13:39 JWT EPA 8260B 7DI8028 74-83-9 Bromomethane ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 75-15-0 Carbon disulfide ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 9260B 7DI8028 56-23-5 Carbon Tetrachloride ND LI ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 108-90-7 Chlorobenzene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 124-48-1 Chlorodibromomethane ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI8028 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 2 of 47 R'. 4310 East Anderson Road Orlando, FL 32812' SM-851-25W * Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-5 - Lab Number: OQD0273-01- Matrix: Solid/Soil Dil Analyzed CAS 9 ----------- Analyte - ---------- ------------------- Result Q ------------- — -------------------------------------------------------------------------------------- Units PQL Factor Date/Time By Method Batch Volatile Organic Compounds by EPA Method 8260B - Cont. 75-00-3 Chloroethane NO ugAg dry 7.25 1 04/18/07 13:39 JWT EPA 9260B 7DI9028 67-66-3 Chloroform ND ugAg dry 7.25 l 04/18/07 13:39 JWT EPA 8260B 7DIS028 74-87-3 Chloromethane ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 156-59-2 cis-1,2-Dichloroethene ND Ll ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D►8029 10061-01-5 cis-1,3-Dichloropropene ND LI ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 9260B 7DI8029 74-95-3 Dibromomethane ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI8028 75-71-8 Dichlorodifluoromethane ND ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 8260B 7DI8028 100414 Ethylbenzene ND ug/kg dry 0.725 1 04/18/07 13:39 JWT EPA 8260B 7D18028 87-68-3 Hexachlorobutadiene NO ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 9260B 7D18029 98-82-8 Isopropylbenzene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 9260B 7D18028 1634-044 Methyl tert-Butyl Ether ND ug/kg dry 0.725 l 04/18/07 13:39 JWT EPA 8260E 7DI8028 75-09-2 Methylene Chloride ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI8028 91-20-3 Naphthalene ND ug/kg dry 0.725 1 04/18/07 13:39 JWT EPA 8260B 7DI8028 104-51-8 n-Butylbenzene NO ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 103-65-1 n-Propylbenzene ND ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 8260B 7D18028 99-87-6 p-Isopropyltoluene NO ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 8260B 7DI8028 135-98-8 sec-Butylbenzene NO ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 10042-5 Styrene NO ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 98-06-6 tert-Butylbenzene NO ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 8260B 7D18028 127-184 Tetrachloroethene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 9260B 7DI8028 108-88-3 Toluene ND ug/kg dry 0.725 1 04/18/07 13:39 JWT EPA 8260B 7D18028 156-60-5 trans-1,2-Dichloroethene ND ug/kg dry 7.25 1 04/19/07 13:39 JWT EPA 8260E 7DI8028 10061-02-6 trans-1,3-Dichloropropene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DI8028 79-01-6 Trichloroethene ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7DIS028 75-69-4 Trichlorofluoromethane ND ug/kgdry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 75-014 Vinyl chloride ND ug/kg dry 7.25 1 04/18/07 13:39 JWT EPA 8260B 7D18028 1330-20-7 Xylenes, total ND ug/kg dry 0.725 1 04/19/07 13:39 JWT EPA 8260B 7D18028 Surrogate: 1,2-Dichloroethane-d4 (73-13701o) 116 % Surrogate: 4-BromoJluorobenzene (59-118%) 104 % Surrogate: Dibromojluoromethane (55-145%) 110 % Surrogate: Toluene-d8 (80-117%) 108 % Semivolatile Organic Compounds by EPA Method 8270C 86-30-6 N-Nitrosodiphenylamine ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 95-50-1 1,2-Dichlorobenzene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 541-73-1 1,3-Dichlorobenzene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 10646-7 1,4-Dichlorobenzene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 100-254 1,4-Dinitrobenzene ND ug/kg dry 440 1 04/19/07 22:43 REM EPA 8270c 7DIS013 90-12-0 I-Methylnaphthalene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 95-95-4 2,4,5-Trichlorophenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DIS013 88-06-2 2,4,6-Trichlorophenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 120-83-2 2,4-Dichlorophenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 71)18013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 3 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0888 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-5 - Lab Number: OQD0273-01 - Matrix: Solid/Soil Dil CAS # Analyte Result Q Units PQL Factor Date/Timc ----------------------- By Method Batch — -------- ------------------------------------------------------------------ Semivolatile Organic Compounds by EPA Method 8270C - Cont. ........... ---------------------- 105-67-9 2,4-Dimethylphenol ND ugAcg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 51-28-5 2,4-Dinitrophenol ND ug/kg dry 221 1 04/19/07 22.43 REM EPA 8270c 7D18013 121-14-2 2,4-Dinitrotoluene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 606-20-2 2,6-Dinitrotoluene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 91-59-7 2-Chloronaphthalene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI9013 95-57-8 2-Chlorophenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 91-57-6 2-Methylnaphthalene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 95-48-7 2-Methylphenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 88-74-4 2-Nitroaniline ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 88-75-5 2-Nitrophenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 91-94-1 3,3'-Dichlorobenzidine ND ug/kg dry 221 1 04/19/07 22.43 REM EPA 8270c 71318013 1319-77-3 3/4-Methylphenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI9013 99.09-2 3-Nitroaniline ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 534-52-1 4,6-Dinitro-2-methylphenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 101-55-3 4-Bromophenyl phenyl ether ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 59-50-7 4-Chloro-3-methylphenol ND ug/kS dry 221 1 04/19/07 22:43 REM EPA 8270c 7D19013 10647-8 4-Chloroaniline ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DIS013 7005-72-3 4-Chlorophenyl phenyl ether ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 100-01-6 4-Nitroaniline ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 100-02-7 4-Nitrophenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 83-32-9 Acenaphthene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 208-%-8 Acenaphthylene NO ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 62-53-3 Aniline ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 120-12-7 Anthracene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 528-29-0 1,2-Dinitrobenzene ND ug/kg dry 440 1 04/19/07 22:43 REM EPA 8270c 7D18013 92-87-5 Benzidine ND L2 ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 56-55-3 Benzo (a) anthracene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 99.65-0 1,3-Dinitrobenzene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 50-32-8 Benzo (a) pyrene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 205-99-2 Benzo (b) fluoranthene ND ugAg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 191-24-2 Benzo (g,h,i) perylene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 207-08-9 Benzo (k) fluoranthene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 100-51-6 Benzyl alcohol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 111-91-1 Bis(2-chloroethoxy)ynethane ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 111444 Bis(2-ehloroethyl)ether ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 3%38-32-9 Bis(2-chloroisopropyl)ether ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 117-81-7 Bis(2-ethylhexyl)phthalate ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 85-68-7 Butyl benzyl phthalate ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 86-74-8 Carbazole ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 218-01-9 Chrysene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 53-70-3 Dibenz (a,h) anthracene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 4 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/19/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-5 - Lab Number: OQD0273-01 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL Factor Date/Time By .......... Method ------------- Batch ------------------------------------------------------------------ Semivolatile Organic Compounds by EPA Method 8270C - Cont. -------------------------------------------- 132-64-9 Dibenzofuran NO ugA S dry 221 1 04/19/07 22:43 REM EPA 8270c 7DIS013 84-66-2 Diethyl phthalate NO ugAg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 131-11-3 Dimethyl phthalate NO ugAg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 84-74-2 Di-n-butyl phthalate ND ugAg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 117-94-0 Di-n-octyl phthalate ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 122-39-4 Diphenylamine ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 206-44-0 Fluoranthene NO ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 122-66-7 1,2-Diphenylhydrazine ND ug/kg dry 221 I 04/19/07 22:43 REM EPA 8270c 7D18013 86-73-7 Fluorene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 118-74-1 Hexachlorobenzene NO ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 87-68-3 Hexachlorobutadiene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 77-47-4 Hexachlorocyclopentadiene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 67-72-1 Hexachloroethane NO ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 193-39-5 Indeno (1,2,3-ed) pyrene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 78-59-1 Isophorone ND L2 ugAg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 91-20-3 Naphthalene NO ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 98-95-3 Nitrobenzene NO ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D►8013 62-75-9 N-Nitrosodimethylamine NO ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 621-64-7 N-Nitrosodi-n-propylamine ND ug/kg dry 221 1 04/I9/07 22:43 REM EPA 8270c 7D18013 87-86-5 Pentachlorophenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 85-01-8 Phenanthrene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 108-95-2 Phenol ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 129-00-0 Pyrene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 110-86-1 Pyridine ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7DI8013 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 221 1 04/19/07 22:43 REM EPA 8270c 7D18013 Surrogate: 2,4,6-Tribromophenol (11-135%) 38 % Surrogate: 2-Fluorobiphenyl (24-121%) 54 % Surrogate: 2-Fluorophenol (13-108•0) 42 % Surrogate: Nitrobenzene-d5 (19-111 %) 42 % Surrogate: Phenol-d5 (18-113%) 46 % Surrogate: Terphetry6d14 (44-171 %) 72 % MA-EPH 83-32-9 Acenaphthene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 208-96-8 Acenaphthylene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 120-12-7 Anthracene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 56-55-3 Benzo[a]anthracene NO mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 50-32-8 Benzo[a]pyrene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 205-99-2 Benzo[b]fluoranthene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 191-24-2 Benzo[g,h,i]perylene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 207-08-9 Benzo[k]fluoranthene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 218-01-9 Chrysene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 5 of 47 4310 East Anderson Road Orlando, Fl- 32812.800-851-25W * Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-5 - Lab Number: OQD0273-01 - Matrix: Solid/Soil Dd Analyzed CAS # Analyte Result Q Units PQL Factor Date/Time ----------- By ------------------------- Method Batch -------------- —------------------------------...--------------------------------------- MA-EPA - Cont. 53-70-3 Dibenz(a,h)anthracene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 206-44-0 Fluoranthene ND mg/Kg dry 0.44 1 04/19/07 05:51 TP MA-EPH 17612 86-73-7 Fluorene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 193-39-5 Indeno[t,2,3-cd]pyrene ND mg/Kg dry 0.44 1 04118/07 05:51 TP MA-EPH 17612 91-57-6 2-Methylnaphthalene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 91-20-3 Naphthalene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 85-01-8 Phenanthrene ND mg/Kg dry 0.44 1 04/18/07 05:51 TP MA-EPH 17612 129-00-0 Pyrene ND mg/Kg dry 0.44 1 04119/07 05:51 TP MA-EPH 17612 NA C 1 I-C22 Aromatics (unadjusted) ND mg/Kg dry 4.4 1 04/18/07 05:51 TP MA-EPH 17612 NA Cl 1-C22 Aromatics (Adjusted) ND mg/Kg dry 4.4 1 04/18/07 05:51 TP MA-EPH 17612 NA C19-06 Aliphatics ND mg/Kg dry 4.4 1 04/18/07 05:51 TP MA-EPH 17612 NA C9-C I8 Aliphatics ND mg/KS dry 4.4 I 04/18/07 05:51 TP MA-EPH 17612 NA Total EPH ND mg/Kg dry 4.4 1 04/18/07 05:51 TP MA-EPH 17612 Surrogate: 2-Bromonaphthalene (40-140'1) 90 % Surrogate: 2-Fluorobiphenyl (40-140%) 97 % Surrogate: o-Terphenyl (40-140%) 65 % Surrogate: I-Chloroociadecane (40-140'�) 53 % MAVPH 7143-2 Benzene ND mg/Kg dry 0.71 1 04/23/07 06:38 JLD MAVPH 17704 NA C9-C12 Aliphatics (adjusted) ND mg/Kg dry 7.1 1 04/23/07 06:38 JLD MAVPH 17704 NA C9-CI0 Aromatics ND mg/Kg dry 7.1 1 04/23/07 06:38 ILD MAVPH 17704 100414 Ethylbenzene ND mg/Kg dry 0.71 1 04/23/07 06:38 JLD MAVPH 17704 136777-61-2 m-Xylene & p-Xylene ND mg/Kg dry 1.4 1 04/23/07 06:38 JLD MAVPH 17704 NA Total VPH ND mg/Kg dry 7.1 1 04/23/07 06:38 JLD MAVPH 17704 Surrogate: 2,5-Dibromotoluene (fid) (70-130%) 103 % 1634-044 Methyl tert-butyl ether ND mg/Kg dry 0.14 1 04/23/07 06:38 JLD MAVPH 17704 Surrogate: 1,5-Dibromotoluene (pid) (70-130%) 102 % 91-20-3 Naphthalene ND mg/Kg dry 1.4 1 04/23/07 06:38 JLD MAVPH 17704 9547-6 o-Xylene ND mg/Kg dry 0.71 1 04/23/07 06:38 JLD MAVPH 17704 108-88-3 Toluene ND mg/Kg dry 0.71 1 04/23/07 06:38 JLD MAVPH 17704 NA C5-C8 Aliphatics (unadjusted) ND mg/Kg dry 7.1 1 04/23/07 06:38 JLD MAVPH 17704 NA C9-C12 Aliphatics (unadjusted) ND mg/Kg dry 7.1 1 04/23/07 06:38 JLD MAVPH 17704 NA C5-C8 Aliphatics (adjusted) ND mg/Kg dry 7.1 1 04/23/07 06:38 JLD MAVPH 17704 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 6 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560 • Fax 407-856-OSM Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-1- Lab Number: OQD0273-02 - Matrix: Solid/Soil Dil Analyzed CAS # ----------- Analyte I------------------------------------------- Result Q ---------------- Units ------------------------------------------------- PQL Factor Daterrime By Method Batch General Chemistry Parameters ---------------------- NA %Solids 74.2 %. 0.100 1 04/19/07 16:00 RRP EPA 160.3 7DI9040 Volatile Organic Compounds by EPA Method 8260B 630-20-6 1,1,1,2-Tetrachloroethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 71-55-6 1,1,1-Trichloroethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 79-34-5 1,1,2,2-Tetmchloroethane ND ugAg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 79-00-5 1,1,2-Trichloroethane ND ug/kg dry 7.28 1 04/l8/07 14:02 JWT EPA9260B 7D18028 75-34-3 1,1-Dichloroethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 75-354 I,l-Dichloroethene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 563-58-6 l,l-Dichloropropene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 87-61-6 1,2,3-Trichlorobenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 96-18-4 1,2,3-Trichloropropane ND usAg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 7.28 1 04/19/07 14:02 JWT EPA 8260B 7DI8029 95-63-6 1,2,4-Trimethylbenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 92608 7D18028 96-12-8 1,2-Dibromo-3-chloropropane ND ug/kg dry 7.29 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 106-93-4 1,2-Dibromoethane (EDB) ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 95-50-1 1,2-Dichlorobenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260E 71)18028 107-06-2 1,2-Dichloroethane ND ug/kgdry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 78-87-5 1,2-Dichloropropane ND LI ug/kg dry 7.29 1 04/18/07 14:02 JWT EPA 8260B 7DIS028 108-67-8 1,3,5-Trimethylbenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260E 7DI8028 541-73-1 1,3-Dichlorobeuzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 142-28-9 1,3-Dichlompropane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 10646-7 1,4-Dichlorobenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 594-20-7 212-Dichloropropane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 78.93-3 2-Butanone ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 110-75-8 2-Chloroethylvinyl ether ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 95.49-8 2-Chlorotoluene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 591-78-6 2-Hexanone ND ug/kg dry 7.28 I 04/18/07 14:02 JWT EPA 8260B 7D18028 7946-9 2-Nitropropane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA82608 7D18028 106434 4-Chlorotoluene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 108-10-1 4-Methyl-2-pentanone ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18029 67-64-1 Acetone 12.3 R3 ug/kgdry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 71-43-2 Benzene ND ug/kg dry 0.728 1 04/18/07 14:02 JWT EPA 8260B 7D18028 108-86-1 Bromobenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 74-97-5 Bromochloromethane ND L1 ug/kg dry 7.28 I 04/18/07 14:02 JWT EPA 8260B 7D18028 75-274 Bromodichloromethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 75-25-2 Bromoform ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 74-93-9 Bromomethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 75-15-0 Carbon disulfide ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260E 7D18028 56-23-5 Carbon Tetrachloride ND LI ug/kg dry 7.28 1 04/18/07 I4:02 JWT EPA 8260B 7DI8028 108-90-7 Chlorobenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 12448-1 Chlorodibromomethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 7 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560 • Fax 407-856-08M Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-1- Lab Number: OQD0273-02 - Matrix: Solid/Soil Dil Analyzed CAS # ------------------------------------------------------- Analyte Result Q ----------------------------------------- Units PQL Factor Date/time - — ---------------------------------- By Method Batch --------- Volatile Organic Compounds by EPA Method 8260B - Cont, 75-00-3 Chloroethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DIS028 67-66-3 Chloroform ND ug/kg dry 7.28 1 04/19/07 14:02 JWT EPA 8260E 7D18028 74-87-3 Chloromethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 9260B 7DI8028 156-59-2 cis-1,2-Dichloroethene ND Ll ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18029 10061-01-5 cis-1,3-Dichloropropene ND LI ug/kg dry 7.29 1 04/18/07 14:02 JWT EPA 8260B 7DIS029 74-95-3 Dibromomethane ND ug/kgdry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 75-71-8 Dichlorodifluoromethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 100414 Ethylbenzene ND ug/kg dry 0.728 1 04/18/07 14:02 JWT EPA 8260B 7D18028 87-68-3 Hexachlorobutadiene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260E 7DI8028 98-82-8 lsopropylbenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 1634-044 Methyl tert-Butyl Ether ND ug/kg dry 0.728 1 04/18/07 14:02 JWT EPA 8260B 7D18028 75-09-2 Methylene Chloride ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 91-20-3 Naphthalene ND ug/kg dry 0.728 1 04/19/07 14:02 JWT EPA 8260B 7DIS028 104-51-8 n-Butylbenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260E 7DI8028 103-65-1 n-Propylbemene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 99-97-6 p-Isopropyltoluene ND ug/kg dry 7.29 1 04/18/07 14:02 JWT EPA 8260B 7D18028 135-98-8 sec-Butylbenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 10042-5 Styrene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 98-06-6 tert-Butylbenzene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 127-19-4 Tetrachloroethene ND ug/kg dry 7.29 1 04/18/07 14:02 JWT EPA 9260B 7D18028 108-88-3 Toluene ND ug/kg dry 0.728 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 156-60-5 trans-1,2-Dichloroethene ND ug/kgdry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 10061-02-6 trans-1,3-Dichloropropene ND ug/kgdry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 79-01-6 Trichloroethene ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7D18028 75-69-4 Trichlorofluoromethane ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 75-01-4 Vinyl chloride ND ug/kg dry 7.28 1 04/18/07 14:02 JWT EPA 8260B 7DI8028 1330-20-7 Xylenes, total ND ug/kg dry 0.728 1 04/18/07 14:02 JWT EPA 8260B 7D18028 Surrogate: 1,2-Dichloroethane-d4 (73-/37%) 115 % Surrogate: 4-Bromq/luorobenzene (59-118%) 103 % Surrogate: DibromoJluoromethane (55-145%) 110 % Surrogate: Toluene-d8 (80-117%) 108 % Semivolatile Organic Compounds by EPA Method 8270C 86-30-6 N-Nitrosodiphenylamine ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DIS013 95-50-1 1,2-Dichlorobenzene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 541-73-1 1,3-Dichlorobenzene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 10646-7 1,4-Dichlorobenzene NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 71)18013 100-254 1,4-Dinitrobenzene ND ugAg dry 449 1 04/19/07 23:13 REM EPA 8270c 7DI8013 90.12-0 1-Methylnaphthalene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 95-954 2,4,5-Trichlorophenol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 88-06-2 2,4,6-Trichlorophenol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 120-83-2 2,4-Dichlorophenol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 8 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0888 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-1 - Lab Number: OQD0273-02 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL Factor Date/Time --------------- By ------------ Method Batch --------------------------------------------------------------------- Semivolatile Organic Compounds by EPA Method 8270C - Cont. ----------------------------- 105-67-9 2,4-Dimedrylphenol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI9013 51-28-5 2,4-Dinitrophenol ND ug/kgdry 225 1 04/19/07 23:13 REM EPA 8270c 7DIS013 121-14-2 2,4-Dinitrotoluene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 606-20-2 2,6-Dinitrotoluene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 91-58-7 2-Chloronaphthalene ND ug/kg dry 225 l 04/19/07 23:13 REM EPA 8270c 7D18013 95-57-8 2-Chlorophenol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI9013 91-57-6 2-Methylnaphthalene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 95.48-7 2-Methylphenol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 88-74-4 2-Nitroaniline NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 88-75-5 2-Nitrophenol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 91-94-1 3,3'-Dichlorobenzidine NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DIS013 1319-77-3 3/4-Methylphenol NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 99-09-2 3-Nitroaniline ND ul Acg dry 225 l 04/19/07 23:13 REM EPA 8270c 7D18013 534-52-1 4,6-Dinitro-2-methylphenol ND ug/kg dry 225 l 04/19/07 23:13 REM EPA 8270c 7D18013 101-55-3 4-Bromophenyl phenyl ether ND ug/kg dry 225 t 04/19/07 23:13 REM EPA 8270c 7D18013 59-50-7 4-Chloro-3-methylphenol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 106-47-8 4-Chloroaniline ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 7005-72-3 4-Chlorophenyl phenyl ether ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 100-01-6 4-Nitroaniline ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 100-02-7 4-Nitrophenol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DIS013 83-32-9 Acenaphthene ND ug/kg dry 225 I 04/19/07 23:13 REM EPA 8270c 7D18013 208-96-8 Acenaphthylene ND ug/kg dry 225 l 04/19/07 23:13 REM EPA 8270c 7D18013 62-53-3 Aniline ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI9013 120-12-7 Anthracene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 528-29-0 1,2-Dinitrobenzene ND ug/kg dry 449 1 04/19/07 23:13 REM EPA 8270c 7D18013 92-87-5 Benzidine ND L2 ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 56-55-3 Benzo (a) anthracene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 99-65-0 1,3-Dinitrobenzene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 50-32-8 Benzo (a) pyrene ND ug/kg dry 225 l 04/19/07 23:13 REM EPA 8270c 7D18013 205-99-2 Benzo (b) fluoranthene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 191-24-2 Benzo (g,h i) perylene NO ug/kg dry 225 1 04/) 9/07 23:13 REM EPA 8270c 7D 18013 207-08-9 Benzo (k) fluonmthene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI9013 100-51-6 Benzyl alcohol ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 111-91-1 Bis(2-chloroethoxy)methane ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 I11444 Bis(2-chloroethyl)ether ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 39638-32-9 Bis(2-chloroisopropyl)ether ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 117-81-7 Bis(2-ethylhexyl)phthalate ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 85-68-7 Butyl benzyl phthalate ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 86-74-8 Carbazole ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 218-01-9 Chrysene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 53-70-3 Dibenz (a,h) anthracene ND ug/kg dry 225 l 04/19/07 23:13 REM EPA 8270c 7DI8013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 9 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560 • Fax 407-858-0885 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-1- Lab Number: OQD0273-02 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL Factor Dateaime By Method Batch -------------------------------- ---------------------------------------------------------------- Semivolatile Organic Compounds by EPA Method 8270C - Cont. ------ --------------------`--------- 132-64-9 Dibenzofivan NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 84-66-2 Diethyl phthalate ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DIS013 131-I1-3 Dimethyl phthalate ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 84-74-2 Di-n-butyl phthalate NO uAg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 117-84-0 Di-n-octyl phthalate ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 122-394 Diphenylamine ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 20644-0 Fluoranthene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 71)18013 122-66-7 1,2-Diphenylhydrazine NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 W73-7 Fluorene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 118-74-1 Hexachlorobenzene NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 87-68-3 Hexachlorobutadiene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 77-47-4 Hexachlorocyclopentadiene NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 67-72-1 Hexachloroethane NO ughg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 193-39-5 Indeno (1,2,3-cd) pyrene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 78-59-1 Isophorone ND L2 ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 91-20-3 Naphthalene NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 98-95-3 Nitrobenzene ND ug/kgdry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 62-75-9 N-Nitrosodimethylamine ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 621-64-7 N-Nitrosodi-n-propylamine NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 87-86-5 Pentachlorophenol NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 85-01-8 Phenanthrene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D►8013 109-95-2 Phenol NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7D18013 129-00-0 Pyrene NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 I10-86-1 Pyridine NO ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 225 1 04/19/07 23:13 REM EPA 8270c 7DI8013 Surrogate: 2,4,6-Tribromophenol (11-135016) 50 % Surrogate: 2-Fluorobiphenyl (14-121 %) 60 % Surrogate: 2-Fluorophenol (13-108%) 49 % Surrogate: Nitrobenzene-d5 (19-111 %) 46 % Surrogate: Phenol -di (18-113%) 53 % Surrogate: Terphenyl-d14 (44-171 %) 73 % MA-EPH 83-32-9 Acenaphthene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 208-96-8 Acenaphthylene NO mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 120-12-7 Anthracene NO mg/Kgdry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 56-55-3 Benzo[alanthracene ND mg/KS dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 50-32-8 Benzo[alpyrene NO mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 205-99-2 Benzo[b]fluoranthene NO mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 191-24-2 Benzo[g,h,ilperylene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 207-08-9 Benzo[k]fluoranthene NO mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 218-01-9 Chrysene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 10 of 47 4310 East Anderson Road Orlando, FL 32812' 8OD-851-2660' Fax 407-856-08M Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-1 - Lab Number: OQD0273-02 - Matrix: Solid/Soil DAl Analyzed CAS # Analyte — Result Q Units ...... ------------- PQL — Factor -------------------------------------------------- DateTime By Method Batch ------------------------------------- ------------------------------- MA-EPH - Cont. 53-70-3 Dibenz(a,h)anthracene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 206-44-0 Fluoranthene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 86-73-7 Fluorene ND mgJKg dry 0.46 1 04/19/07 06:14 TP MA-EPH 17612 193-39-5 Indeno[1,2,3-cd]pyrene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 91-57-6 2-Methylnaphthalene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 91-20-3 Naphthalene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 85-01-8 Phenanthrene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 ' 129-00-0 Pyrene ND mg/Kg dry 0.46 1 04/18/07 06:14 TP MA-EPH 17612 NA Cl I-C22 Aromatics (unadjusted) ND mg/Kg dry 4.6 1 04/19/07 06:14 TP MA-EPH 17612 NA Cl 1-C22 Aromatics (Adjusted) ND mg/Kg dry 4.6 1 04/18/07 06:14 TP MA-EPH 17612 NA C19-06Aliphatics ND mg/Kgdry 4.6 1 04/19/07 06:14 TP MA-EPH 17612 NA C9-C I8 Aliphatics ND mg/Kg dry 4.6 1 04/18/07 06:14 TP MA-EPH 17612 NA Total EPH ND mg/Kg dry 4.6 1 04/19/07 06:14 TP MA-EPH 17612 Surrogate: 2-Bromonaphthalene (40-140%) 98 % Surrogate: 2-Fluorobiphenyl (40-140%) 105 % Surrogate: o-Terphenyl (40-140%) 71 % Surrogate: I-Chloroociadecane (40-140%) 52 % MAVPH 7143-2 Benzene ND mg/Kg dry 0.76 1 04/23/07 07:11 JLD MAVPH 17704 NA C9-C12 Aliphatics (adjusted) ND mg/Kg dry 7.6 1 0423/07 07:11 JLD MAVPH 17704 NA C9-CIO Aromatics ND mg/Kg dry 7.6 1 04/23/07 07:11 JLD MAVPH 17704 100414 Ethylbenzene ND mg/Kg dry 0.76 1 04/23/07 07:11 JLD MAVPH 17704 136777-61-2 m-Xylene & p-Xylene ND mg/Kg dry 1.5 1 04/23/07 07:11 JLD MAVPH 17704 NA Total VPH ND mg/Kg dry 7.6 1 04/23/07 07:11 JLD MAVPH 17704 Surrogate: 2,5-Dibromotoluene (fid) (7&130%) 103 % 1634-044 Methyl tent -butyl ether i ND mg/Kg dry 0.15 1 04/23/07 07:11 JLD MAVPH 17704 Surrogate: 1,5-Dibromotoluene (pid) (70-130%) 101 % 91-20-3 Naphthalene ND mg/Kg dry 1.5 1 04/23/07 07:11 JLD MAVPH 17704 9547-6 o-Xylene ND mg/Kg dry 0.76 1 04/23/07 07:11 JLD MAVPH 17704 108-99-3 Toluene ND mg/Kg dry 0.76 1 04/23/07 07:11 JLD MAVPH 17704 NA C5-C8 Aliphatics (unadjusted) ND mg/Kg dry 7.6 1 04/23/07 07:11 JLD MAVPH 17704 NA C9-C12 Aliphatics (unadjusted) ND mg/Kg dry 7.6 1 04/23/07 07:11 JLD MAVPH 17704 NA C5-C8 Aliphatics (adjusted) ND mg/Kg dry 7.6 1 04/23/07 07:11 JLD MAVPH 17704 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 11 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-858-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-2 - Lab Number: OQD0273-03 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL ------------------ Factor Date/Time ---------------------------------------- By Method Batch --------------------------I--------------------------------------------------------- General Chemistry Parameters NA %Solids 87.9 %. 0.100 1 04/19/07 16:00 RRP EPA 160.3 7D19040 Volatile Organic Compounds by EPA Method 8260B 630-20-6 1,1,1,2-Tetrachloroethane ND ug/kg dry 5.85 1 04/19/07 14:19 JWT EPA 8260B 7DIS028 71-55-6 l,l,l-Trichloroethane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 79-34-5 1,1,2,2-Tetrachloroethane ND ug/kg dry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7DI8028 79-00-5 1,1,2-Trichloroethane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 75-34-3 1,1-Dichloroethane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 75-35-4 1,1-Dichloroethene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 563-58-6 I,1-Dichloropropene ND ug/kg dry 5.85 1 04/19/07 14:19 JWT EPA 8260B 7D18028 87-61-6 1,2,3-Trichlorobenzene ND ug/kg dry 5.85 1 04/19/07 14:19 JWT EPA 8260B 7D18028 96-18-4 1,2,3-Trichloropropane ND ug/kgdry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8029 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 95-63-6 1,2,4-Trimethylbenzene ND usAg dry 5.85 1 04/19/07 14:18 JWT EPA 8260E 7DI8028 96-12-8 1,2-Dibromo-3-chloropropane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 106-93-4 1,2-Dibromoethane (EDB) ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18029 95-50-1 1,2-Dichlorobenzene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 107-06-2 1,2-Dichloroethane ND ug/kg dry 5.83 1 04/18/07 14:19 JWT EPA 8260B 7DI8028 78-87-5 1,2-Dichloropropane ND Ll ug/kg dry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7DI8028 I08.67-8 1,3,5-Trimethylbenzene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 541-73-1 1,3-Dichlorobemsne ND ug/kgdry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 142-28-9 1,3-Dichloropropane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 106.46-7 1,4-Dichlorobenzene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 594-20-7 2,2-Dichloropropane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260E 7DI8028 78-93-3 2-Butanone ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 I10-75-8 2-Chloroethylvinyl ether ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 95-49-8 2-Chlorotoluene ND ug/kgdry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7D18028 591-78-6 2-Hexanone ND ug/kg dry 3.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 7946-9 2-Nitropropane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260E 7DI8028 106-434 4-Chlorotoluene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 108-10-1 4-Methyl-2-pentanone ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 67-64-1 Acetone ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 71.43-2 Benzene ND ug/kg dry 0.585 1 04/18/07 14:18 JWT EPA 8260B 7D18028 108-86-1 Bromobenzene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 74-97-5 Bromochloromethane ND Ll ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 75-27-4 Bromodichloromethane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 75-25-2 Bromoform ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 74-83-9 Bromomethane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 75-15-0 Carbon disulfide ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 56-23-5 Carbon Tetrachloride ND LI ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 71)18028 108-90-7 Chlorobenzene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 12448-1 Chlorodibromomethane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 71)18028 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 12 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-858-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-2 - Lab Number: OQD0273-03 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL Factor Doe/Time ------------------------------- By Method Batch ----------------------------------------------------------------------- Volatile Organic Compounds by EPA Method 8260B - Cont. ---------------------------------------- 75-00-3 Chloroethane ND usAg dry 5.85 1 04/18/07 14:19 JWT EPA 8260E 7DI9029 67-66-3 Chloroform ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8029 74-87-3 Chloromethane ND ugAg dry 5.85 1 04/18/07 14:18 JWT EPA 8260E 7DI8028 156-59-2 cis-1,2-Dichloroethene ND Ll ug/kg dry 5.85 I 04/18/07 14:19 JWT EPA 9260B 7DIS028 10061-01-5 cis-1,3-Dichloropropene ND Ll ug/kg dry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7DI8028 74-95-3 Dibromomethane ND ug/kg dry 5.85 1 04/18/07 14:19 JWT EPA 8260B 7DI8028 75-71-8 Dichlorodifluoromethane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 10041-4 Ethylbenzene ND ug/kg dry 0.585 1 04/18/07 14:18 JWT EPA 8260E 7DI8028 87-68-3 Hexachlorobutadiene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 9260B 7D18028 98-82-8 Isopropylbenzene ND ug/kg dry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7D18028 1634-044 Methyl tert-Butyl Ether ND ug/kg dry 0.585 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 75-09-2 Methylene Chloride ND ughg dry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7DI8028 91-20-3 Naphthalene ND ug/kg dry 0.585 1 04/19/07 14:18 JWT EPA 9260B 7D18029 104-51-8 n-Butylbenzene ND ug/kg dry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7DI8028 103-65-1 n-Propylbenzene ND ug/kg dry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7D18028 99-87-6 p-Isopropyltoluene ND ug/kg dry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7DI9028 135-98-8 sec-Butylbenzene ND ug/kg dry 5.85 1 04/19/07 14:18 JWT EPA 8260B 7DI8028 100-42-5 Styrene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 98-06-6 tent-Butylbenzene ND W&g dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 127-18-4 Tetrachloroethene ND ug/kg dry 5.95 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 108-88-3 Toluene ND ug/kg dry 0.585 1 04/18/07 14:18 JWT EPA 8260E 7D18028 156-60-5 trans-1,2-Dichloroethene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7D18028 10061-02-6 trans-1,3-DicHoropropene ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260E 7D18028 79-01-6 Trichloroethene NO ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 75-694 Trichlorofluoromethane ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 75-01-4 Vinyl chloride ND ug/kg dry 5.85 1 04/18/07 14:18 JWT EPA 9260B 7DI8028 1330-20-7 Xylenes, total ND ug/kg dry 0.585 1 04/18/07 14:18 JWT EPA 8260B 7DI8028 Surrogate: 1,1-Dichloroethane-d4 (73-137%) 115 % Surrogate: a-Bromofluorobenzene (59-118%) 103 % Surrogate: Dibromo/luoromethane (55-145%) 1// % Surrogate: Toluene-& (80-117%) 108 % Semivolatile Organic Compounds by EPA Method 8270C 86-30-6 N-Nitrosodiphenylamine ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 95-50-1 1,2-Dichlorobenzene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 541-73-1 1,3-Dichlorobenzene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 10646-7 1,4-Dichlorobenzene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 100-254 1,4-Dinitrobenzene ND ug/kg dry 379 1 04/19/07 23:43 REM EPA 8270c 7DI8013 90-12-0 1-Methylnaphthalene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 95-95-4 2,4,5-Trichlorophenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 88-06-2 2,4,6-Trichlorophenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 120-83-2 2,4-Dichlorophenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 13 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-2 - Lab Number: OQD0273-03 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL Factor Date/Time By Method Batch -----------------------I----------I----------------------------------------------------------------------------------------------------------- Semivolatile Organic Compounds by EPA Method 8270C - Cont. 105-67-9 2,4-Dimedrylphenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 51-28-5 2,4-Dinitrophenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 121-14-2 2,4-Dinitrotoluene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 606-20-2 2,6-Dinitrotoluem ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 91-58-7 2-Chloronaphthalene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 95-57-8 2-Chlorophenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 91-57-6 2-Methylnaphthalene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DIS013 95-48-7 2-Methylphenol ND ug/kgdry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 88-74-4 2-Nitroaniline ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 88-75-5 2-Nitrophenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 91-94-1 3,3'-Dichlorobenzidine ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 1319-77-3 3/4-Methylphenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 99-09-2 3-Nitroaniline ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 534-52-1 4,6-Dinitro-2-methylphenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 I01-55-3 4-Bromophenyl phenyl ether ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 59-50-7 4-Chloro-3-methylphenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 106-47-8 4-Chloroaniline ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 7005-72-3 4-Chlorophenol phenyl ether ND ug/kg dry 190 I 04/19/07 23:43 REM EPA 8270c 7DI8013 100-01-6 4-Nitroaniline ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI9013 100-02-7 4-Nitrophenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DIS013 83-32-9 Acenaphthene ND ugAcg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 208-%-8 Acenaphthylene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 62-53-3 Aniline ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 120-12-7 Anthracene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 528-29-0 1,2-Dinitrobenzene ND ug/kg dry 379 1 04/19/07 23:43 REM EPA 8270c 7DI8013 92-87-5 Benzidine ND L2 ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 56-55-3 Benzo (a) anthracene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 99-65-0 1,3-Dinitrobenzene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 50-32-8 Benzo (a) pyrene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 205-99-2 Benzo (b) fluoranthene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 191-24-2 Benzo (g,h,i) perylene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 207-08-9 Benzo (k) fluoranthene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 100-51-6 Benzyl alcohol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 l l 1-91-1 Bis(2-chloroethoxy)mcthane ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 111444 Bis(2-chloroethyl)ether ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI9013 3%38-32-9 Bis(2-chloroisopropyl)ether ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 117-81-7 Bis(2-ethylhexyl)phthalate ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 85-68-7 Butyl benzyl phthalate ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 86-74-8 Carbazole ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 218-01-9 Chrysene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 53-70-3 Dibenz (a,h) anthracene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 14 of 47 4310 East Anderson Road Orlando, FL 32812 ' 800-851-2560' Fax 4074W-0888 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD,, SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-2 - Lab Number: OQD0273-03 - Matrix: Solid/Soil CAS # Analyte ----------------------------------------------- Result Q ----------- Units PQL Dil Factor Analyzed Date rime By Method Batch ---------- Semivolatile Organic Compounds by EPA Method 8270C - Cont. ------------ ----------- ----------- ----------- -------- -------------------- 132-64-9 Dibenzo1bran ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 84-66-2 Diethyl phthalate ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 131-11-3 Dimethyl phthalate ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 84-74-2 Di-n-butyl phthalate ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 117-84-0 Di-n-octyl phthalate ND ugAg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 122-394 Diphenylamine ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 20644-0 Fluoranthene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DIS013 122-66-7 1,2-Diphenylhydrazine ND ug/kg dry 190 ► 04/19/07 23:43 REM EPA 8270c 7DI8013 86-73-7 Fluorene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 118-74-1 Hexachlorobenzene ND ugAg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DIS013 87-68-3 Hexachlorobutadiene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 7747-4 Hexachlorocyclopentadiene ND uVkg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DIS013 67-72-1 Hexachloroethane ND ugAg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 193-39-5 Indeno (1,2,3-cd) pyrene ND ug&g dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 78-59-1 lsophorone ND L2 ugAg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 91-20-3 Naphthalene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DIS013 98-95-3 Nitrobenzene ND ugAg dry 190 I 04/19/07 23:43 REM EPA 8270c 7DI8013 62-75-9 N-Nitrosodimethylamine ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 621-64-7 N-Nitrosodi-n-propylamine ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 87-86-5 Pentachlorophenol ND ugAg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DIS013 85-01-8 Phenanthrene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 108-95-2 Phenol ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7DI8013 129-00-0 Pyrene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 I10-86-1 Pyridine ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 190 1 04/19/07 23:43 REM EPA 8270c 7D18013 Surrogate: 2,4,6-Trtbromophenol (11-135%) 49 % Surrogate: 2-Fluorobiphenyl (14-111%) 51 % Surrogate: 2-Fluorophenol (13-108%) 43 % Surrogate: Nitrobenzene-0 (19-111 %) 40 % Surrogate: Phenol-d5 (18-113%) 46 % Surrogate: Tenphenyl-dl4 (44-171 %) 78 % MA-EPH 83-32-9 Acenaphthene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 208-96-8 Acenaphthylene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 120-12-7 Anthracene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 56-55-3 Benzo[a]anthracene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 50-32-8 Benzo[a]pyrene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 205-99-2 Benzo[b]fluoranthene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 191-24-2 Benzo[g,h,i]perylene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 207-08-9 Benzo[k]fluoranthene ND mg/Kg dry 0.43 1 04/18/07 06:37 'TP MA-EPH 17612 218-01-9 Chrysene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 15 of 47 4310 East Anderson Road Orlando, FL 32812.800-851-2560 • Fax 407-856-OM Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-2 - Lab Number: OQD0273-03 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL Factor Date/Time By Method ------------- Batch ------------------------------------------------------ MA-EPH - Cont. --------------------------------------------------------------------------- 53-70-3 Dibenz(a,h)anthracene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 206-44-0 Fluoranthene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 86-73-7 Fluorene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 193-39-5 Indeno[1,2,3-cd]pyrene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 91-57-6 2-Methylnaphthalene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 91-20-3 Naphthalene ND mg/Kg dry 0.43 1 04/I8/07 06:37 TP MA-EPH 17612 85-01-8 Phenanthrene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 129-00-0 Pyrene ND mg/Kg dry 0.43 1 04/18/07 06:37 TP MA-EPH 17612 NA CI I-C22 Aromatics (unadjusted) ND mg/Kg dry 4.3 1 04/18/07 06:37 TP MA-EPH 17612 NA Cl 1-C22 Aromatics (Adjusted) ND mg/Kg dry 4.3 1 04/18/07 06:37 TP MA-EPH 17612 NA C19-C36 Aliphatics ND mg/Kg dry 4.3 1 04/18/07 06:37 TP MA-EPH 17612 NA C9-C 18 Aliphatics ND mg/Kg dry 4.3 1 04/19/07 06:37 TP MA-EPH 17612 NA Total EPH ND mg/Kg dry 4.3 1 04/18/07 06:37 TP MA-EPH 17612 Surrogate: 2-Bromonaphihalene (40-140%) 93 Surrogate: 2-Fluorobiphenyl (40-140•160) 99 % Surrogate: o-Ter he 1 40-140% 8 P rN ( ) 66 % Surrogate: I-Chloroocradecane (40-140%) 50 % MAVPH 7143-2 Benzene ND mgJKg dry 0.65 1 04/23/07 07:44 JLD MAVPH 17704 NA C9-C12 Aliphatics (adjusted) ND mg/Kg dry 6.5 1 04/23/07 07:44 JLD MAVPH 17704 NA C9-C10 Aromatics ND mg/Kg dry 6.5 1 04/23/07 07:44 JLD MAVPH 17704 100414 Ethylbenzene ND mg/Kg dry 0.65 1 04/23/07 07:44 JLD MAVPH 17704 136777-61-2 m-Xylene & p-Xylene ND mg/Kg dry 1.3 1 04/23/07 07:44 JLD MAVPH 17704 NA Total VPH ND mg/Kg dry 6.5 1 04/23/07 07:44 JLD MAVPH 17704 Surrogate: 2,5-Dibromotoluene 6rid) (70-130%) I01 % 1634-044 Methyl tert-butyl ether ND mg/Kg dry 0.13 1 04/23/07 07:44 JLD MAVPH 17704 Surrogate: 2,5-Dibromotoluene (pid) (70-130916) 98 % 91-20-3 Naphthalene ND mg/Kg dry 1.3 1 04/23/07 07:44 JLD MAVPH 17704 9547-6 o-Xylene ND mg/Kg dry 0.65 1 04/23/07 07:44 JLD MAVPH 17704 108-88-3 Toluene ND mg/Kg dry 0.65 1 04/23/07 07:44 JLD MAVPH 17704 NA C5-C8 Aliphatics (unadjusted) ND mg/Kg dry 6.5 1 04/23/07 07:44 JLD MAVPH 17704 NA C9-02 Ahphatics (unadjusted) ND mg/Kg dry 6.5 1 04/23/07 07:44 JLD MAVPH 17704 NA C5-C8 Aliphatics (adjusted) ND mg/Kg dry 6.5 1 04/23/07 07:44 JLD MAVPH 17704 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 16 of 47 4310 East Anderson Road Orlando, FL 32812.800-851-2560' Fax 407-awoe88 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-3 - Lab Number: OQD0273-04 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL Factor Daterrime -------------------------- By Method ------------ Batch --------------------------------------------------- General Chemistry Parameters ------------------------------------ ----------------- NA %Solids 86.4 %. 0.100 1 04/19/07 16:00 RRP EPA 160.3 7DI9040 Volatile Organic Compounds by EPA Method 8260B 630-20-6 1,1,1,2-Tetrachloroethane ND ug/kgdry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18029 71-55-6 1,1,1-Trichloroethane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260E 7D18028 79-34-5 1,1,2,2-Tetrachloroethane ND ug/kg dry 5.99 1 04/18/07 14:35 JWT EPA 8260E 7DI9028 79-00-5 1,1,2-Trichloroethane ND ug/kg dry 5.89 1 04/19/07 14:35 JWT EPA 8260B 7D18028 75-34-3 1,1-Dichloroethane ND ugAg dry 5.99 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 75-35-4 I,I-Dichloroethene ND ullft dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 563-58-6 I,l-Dichloropropene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 87-61-6 1,2,3-Trichlorobenzene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 %-18-4 1,2,3-Trichloropropane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 9260B 7D18028 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 95-63-6 1,2,4-Trimethylbenzem ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 9260B 7D18028 %-12-8 1,2-Dibromo-3-chloropropane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 106-934 1,2-Dibromoethane (EDB) ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 9260B 7D18028 95-50-1 1,2-Dichlorobenzene ND ugAg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 107-06-2 1,2-Dichloroedtane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 78-87-5 1,2-Dichloropropane ND Ll ug/kgdry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 108-67-8 1,3,5-Trimethy1benzene ND ug/kg city 5.89 1 04/19/07 14:35 JWT EPA 8260B 7D18028 541-73-1 1,3-Dichlorobenzene ND ug/kg dry 5.99 1 04/19/07 14:35 JWT EPA 8260B 7DI8028 142-28-9 1,3-Dichloropropane ND ug/kg dry 5.89 1 04/19/07 14:35 JWT EPA 8260B 7D18028 106-46-7 1,4-Dichlorobenzene ND ug/kgdry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 594-20-7 2,2-Dichloropropane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 78-93-3 2-Butanone ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 110-75-8 2-Chloroethylvinyl ether ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DIS028 9549-8 2-Chlorotoluene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 591-78-6 2-Hexanone ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 79-46-9 2-Nitropropane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260E 7D18028 106434 4-Chlorotoluene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 108-10-1 4-Methyl-2-pentanone ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI9028 67-64-1 Acetone ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 71-43-2 Benzene ND ug/kg dry 0.589 1 04/18/07 14:35 JWT EPA 8260B 7D18028 108-86-1 Bromobenzene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260E 7DI8028 74-97-5 Bromochloromethane ND Ll ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 75-274 Bromodichloromethane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 75-25-2 Bromofonn ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 74-83-9 Bromomethane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 75-15-0 Carbon disulfide ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 56-23-5 Carbon Tetrachloride ND Ll ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260E 7D18028 108-90-7 Chlorobenzene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 12448-1 Chlorodibromomethane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 17 of 47 4310 East Anderson Road Orlando, Fl- 32812' 800-851-2560' Fax 407-85"886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Ntunber: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-3 - Lab Number: OQD0273-04 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL Factor Date By Method Batch ----------------------------- Volatile Organic ------------------------- --------------------- Compounds by EPA Method 8260B - Cont. ---------------------------------------------------------------- 75-00-3 Chloroethane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 826013 7DI9029 67-66-3 Chloroform ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8029 74-87-3 Chloromethane ND ug/kg dry 5.89 1 04/19/07 14:35 JWT EPA 8260B 7DI8028 156-59-2 cis-1,2-Dichloroethene ND LI ug/kg dry 5.89 l 04/19/07 14:35 JWT EPA 8260B 7DIS029 10061-01-5 cis-1,3-Dichloropropene ND Ll ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 74-95-3 Dibromomethane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 9260B 7D18028 75-71-8 Dichlorodifluoromethane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 100-41-4 Ethylbenzene ND ug/kg dry 0.589 1 04/19/07 14:35 JWT EPA 8260B 7DI8028 87-68-3 Hexachlorobutadiene ND ug/kg dry 5.89 1 04/19/07 14:35 JWT EPA 8260B 7D18028 98-82-8 Isopropylbenzene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 1634-044 Methyl tert-Butyl Ether ND ug/kg dry 0.589 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 75-09-2 Methylene Chloride ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 91-20-3 Naphthalene ND ug/kg dry 0.589 1 04/19/07 14:35 JWT EPA 8260B 7DI8028 104-51-8 n-Butylbenzene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 71318028 103-65-1 n-Propylbenzene ND ug/kg dry 5.99 1 04/19/07 14:35 JWT EPA 8260B 7DI8028 99-87-6 p-Isopropyltoluene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 I35-98-8 sec-Butylbenzene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI9028 10042-5 Styrene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 98-06-6 tert-Butylbenzene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7D18028 127-184 Tetrachloroethene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 108-88-3 Toluene ND ug/kg dry 0.589 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 156-60-5 trans-1,2-Dichlomethene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 I0061-02.6 trans-1,3-Dichloropropene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 79-01-6 Trichloroethene ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 75-69-4 Trichlorofluoromethane ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 75-01-4 Vinyl chloride ND ug/kg dry 5.89 1 04/18/07 14:35 JWT EPA 8260B 7DI8028 I330-20-7 Xylenes, total ND ug/kg dry 0.589 1 04/18/07 14:35 JWT EPA 8260B 7D18028 Surrogate: 1,1-Dichloroeiham-t/4 (73-137%) 114 % Surrogate: 4-BromoJluorobenzene (59-118%) 101 % Surrogate: DibromoJluoromethane (55-145%) 110 % Surrogate: Toluene-d8 (80-117%) 107 % Semivolatile Organic Compounds by EPA Method 8270C 86-30-6 N-Nitrosodiphenylamine ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 95-50-1 1,2-Dichlorobenzene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 541-73-1 1,3-Dichlorobenzene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 10646-7 1,4-Dichlorobenzene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 100-254 1,4-Dinitrobenzene ND ug/kg dry 385 1 04/20/07 00:13 REM EPA 8270c 7DI8013 90-12-0 1-Methylnaphthalene ND ug/kgdry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 95-95-4 2,4,5-Trichlorophenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 88-06-2 2,4,6-Trichlorophenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DIS0I3 120-83-2 2,4-Dichlorophenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 18 of 47 4310 East Anderson Road Orlando, Ft. 32812.800-851-2560 • Fax 407-856-GM Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-3 - Lab Number: OQD0273-04 - Matrix: Solid/Soil Dil An CAS # Analyte Result Q Units PQL Factor Date/Time By Method ----------------- Batch -- ------------------------------------------------------ Semivolatile Organic Compounds by EPA Method 8270C - Cont. ---------------------------------------------- 105-67-9 2,4-Dimethylphenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 51-28-5 2,4-Dinitrophenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 121-14-2 2,4-Dinitrotoluene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 606-20-2 2,6-Dinitrotoluene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 91-58-7 2-Chloronaphthalene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 95-57-8 2-Chlorophenol ND ugAg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DIS013 91-57-6 2-Methylnaphthalene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 9548-7 2-Methylphenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 88-74-4 2-Nitroaniline ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 88-75-5 2-Nitrophenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 91-94-1 3,3'-Dichlorobenzidine ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 1319-77-3 3/4-Methylphenol ND ugAg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 99-09-2 3-Nitroaniline ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 534-52-1 4,6-Dinitro-2-methylphenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 101-55-3 4-Bromophenyt phenyl ether ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 59-50-7 4-Chloro-3-methylphenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 106-47-8 4-0lomaniline NO ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 7005-72-3 4-Chlorophenyl phenyl ether ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D1 S013 100-01-6 4-Nitroaniline ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 100-02-7 4-Nitrophenol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI9013 83-32-9 Acenaphthene ND ug/kg dry 193 I 04/20/07 00:13 REM EPA 8270c 7D18013 208-96-8 Acenaphthylene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 62-53-3 Aniline ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 120-12-7 Anthracene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 528-29-0 1,2-Dinitrobenzene ND ug/kg dry 385 1 04/20/07 00:13 REM EPA 8270c 7D18013 92-87-5 Benzidine ND L2 ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 56-55-3 Benzo (a) anthracene ND ug/kg dry 193 I 0420/07 00:13 REM EPA 8270c 7D18013 99-65-0 1,3-Dinitrobenzene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 50-32-8 Benzo (a) pyrene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 71)18013 205-99-2 Benzo (b) fluoranthene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 191-24-2 Benzo (g,h,i) perylene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 207-08-9 Benzo (k) fluoranthene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 100-51-6 Benzyl alcohol ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 .111-91-1 Bis(2-chloroethoxy)methane ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 111-44-4 Bis(2-chloroethyl)ether ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 39638-32-9 Bis(2-chloroisopropyl)ether ND ug/kg dry 193 I 04/20/07 00:13 REM EPA 8270c 7DI8013 117-81-7 Bis(2-ethylhexyl)phthalate ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 85-68-7 Butyl benzyl phthalate ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 86-74-8 Carbazole ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 218-01-9 Chrysene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D 18013 53-70-3 Dibenz (a,h) anthracene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 19 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-25W ` Fax 407.856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-3 - Lab Number: OQD0273-04 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q ------------------- Units -------------------- PQL Factor --------------------------------------------------- Date/Time By Method Batch --------------------------------------------------- Semivolatile Organic Compounds by EPA Method 8270C - Cont. 132.64-9 Dibenzofuran ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 84-66-2 Diethyl phthalate ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DIS013 131-I1-3 Dimethyl phthalate ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 84-74-2 Di-n-butyl phthalate ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 117-94-0 Di-n-octyl phthalate ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 122-394 Diphenylamine ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7D18013 206-44-0 Fluoranthene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 122-66-7 1,2-Diphenylhydrazine ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 86-73-7 Fluorene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 118-74-1 Hexachlorobenzene ND ug/kg dry 193 1 04/20/07 00:13 REM EPA 8270c 7DI8013 87-68-3 Hexachlorobutadiene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 7747-4 Hexachlorocyclopentadiene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 67-72-1 Hexachloroethane ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 193-39-5 Indeno (1,2,3-cd) pyrene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 78-59-1 Isophorone ND L2 ug/kgdry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 91-20-3 Naphthalene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 98-95-3 Nitrobenzene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DIS013 62-75-9 N-Nitrosodimethylamine ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 621.64-7 N-Nitrosodi-n-propylamine ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 87-96-5 Pentachlorophenol ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 85-01-8 Phenanthrene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 108-95-2 Phenol ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 129-00-0 Pyrene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7D18013 110-86-1 Pyridine ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 193 1 0420/07 00:13 REM EPA 8270c 7DI8013 Surrogate: 2,4,6-Tribromophenol (11-135116) 56 % Surrogate: 2-Fluorobiphenyl (14-121%) 67 % Surrogate: 1-Fluorophenol (13-108%) M % Surrogate: Nitrobetnene-d5 (19-11 /%) 51 % Surrogate: Phenol-d5 (18-113%) 58 % Surrogate: Terphenyl-d14 (44-171 %) 80 % MA-EPH 83-32-9 Acenaphthene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 208-96-8 Acenaphthylene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 120-12-7 Anthracene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 56-55-3 Benzo[a]anthracene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 50-32-8 Benzo[a]pyrene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 205-99-2 Benzo[b]fluoranthene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 191-24-2 Benzo[g,h,i]perylene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 207-08-9 Benzo[k]fluoranthene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 218-01-9 Chrysene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 20 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-858-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S-3 - Lab Number: OQD0273-04 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte -------------- Result Q Units PQL Factor Datelrime By ----------------------- Method Batch -------------------------------- MA-EPH - Cont. ------------------------------------------------------------------------- 53-70-3 DiberWa h)attthracene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 2064" Flumanthene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 86-73-7 Fluorene ND mg/Kg dry 0.37 1 04/19/07 07:00 TP MA-EPH 17612 193-39-5 Indeno[I,2,3-cd]pyrene ND mg/Kg (by 0.37 1 04/18/07 07:00 TP MA-EPH 17612 91-57-6 2-Methylnaphthalene ND mg/Kg dry 0.37 1 04/19/07 07:00 TP MA-EPH 17612 91-20-3 Naphthalene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 85-01-8 Phenandwene ND mg/Kg dry 0.37 1 04/19/07 07:00 TP MA-EPH 17612 129-00-0 Pyrene ND mg/Kg dry 0.37 1 04/18/07 07:00 TP MA-EPH 17612 NA C 11-C22 Aromatics (unadjusted) ND mg/K8 dry 3.7 1 04/18/07 07:00 TP MA-EPH 17612 NA C l 1-C22 Aromatics (Adjusted) ND mg/Kg dry 3.7 1 04/19/07 07:00 TP MA-EPH 17612 NA C 19-06 Aliphatics ND mg/Kg dry 3.7 1 04/18/07 07:00 TP MA-EPH 17612 NA C9-C18 Aliphatics ND mg/Kg dry 3.7 1 04/18/07 07:00 TP MA-EPH 17612 NA Total EPH ND mg/Kg dry 3.7 1 04/18/07 07:00 TP MA-EPH 17612 Surrogate: 2-Bromonaphthalene (40-140*16) 88 % Surrogate: 2-Fluorobiphenyl (40-140%) 95 % Surrogate: o-Terphenyl (40-140'0) 65 % Surrogate: I-Chlorooetadecane (40-140''A) 55 % MAVPH 7143-2 Benzene ND mg/Kg dry 0.64 1 04/23/07 08:17 JLD MAVPH 17704 NA C9-C12 Aliphatics (adjusted) ND mg/Kg dry 6.4 1 04/23/07 08:17 JLD MAVPH 17704 NA C9-C10 Aromatics ND mg/Kg dry 6.4 1 04/23/07 08:17 JLD MAVPH 17704 100414 Ethylbenzene ND mg/Kg dry 0.64 l 04/23/07 08:17 JLD MAVPH 17704 136777-61-2 m-Xylene & p-Xylene ND mg/Kg dry 1.3 1 04/23/07 08:17 JLD MAVPH 17704 NA Total VPH ND mg/Kg dry 6.4 1 04/23/07 08:17 JLD MAVPH 17704 Surrogate: 2,5-Dibromoioluene fd) (70-130%) 102 % 1634-04-4 Methyl tert-butyl ether ND mg/Kg dry 0.13 1 04/23/07 08:17 JLD MAVPH 17704 Surrogate: 2,5-Dibromoioluene (pid) (70-13(r%) 98 % 91-20-3 Naphthalene ND mg/Kg dry 1.3 1 04/23/07 08:17 JLD MAVPH 17704 9547-6 o-Xylene ND mg/Kg dry 0.64 1 04/23/07 08:17 JLD MAVPH 17704 108-88-3 Toluene ND mg/Kg dry 0.64 1 04/23/07 08:17 JLD MAVPH 17704 NA C5-C8 Aliphatics (unadjusted) ND mg/Kg dry 6.4 1 04/23/07 08:17 JLD MAVPH 17704 NA C9-C12 Aliphatics (unadjusted) ND mg/Kg dry 6.4 1 04/23/07 09:17 JLD MAVPH 17704 NA C5-C8 Aliphatics (adjusted) ND mg/Kg dry 6.4 1 04/23/07 08:17 JLD MAVPH 17704 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 21 of 47 4310 East Anderson Road Orlando, FL 32812. 800-851-2560 • Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S4 - Lab Number: OQD0273-05 - Matrix: Solid/Soil Dil CAS # ---------- Analyte -------------------- Result -------------------------------------- Q Units PQL --------------------------------------------- Factor Datemwe By Method ------- Batch - --- General Chemistry Parameters NA %Solids 91.1 °/a 0.100 1 04/19/07 16:00 RRP EPA 160.3 7DI9040 Volatile Organic Compounds by EPA Method 8260B 630-20-6 1,1,1,2-Tetrachloroethane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 71-55-6 1,1,l-Trichloroethane ND ug/kg dry 5.86 1 04/19/07 14:52 JWT EPA 8260B 7DI9028 79-34-5 1,1,2,2-Tetrachloroethane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 79-00-5 1,1,2-Trichloroethane ND ug/kgdry 5.86 1 04/18/07 14:52 JWT EPA9260B 7DIS028 75-34-3 1,1-Dichloroethane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 75-35-4 1,1-Dichloroethene ND ugAg dry 5.86 1 64/18/07 14:52 JWT EPA 8260B 7DI8028 563-58-6 I,I-Dichloropropene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260E 7D18028 87-61-6 1,2,3-Trichlorobenzene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 96-19-4 1,2,3-Trichloropropane ND ug/kg dry 5.86 1 04/19/07 14:52 JWT EPA 8260B 7DI8028 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260E 7DI9028 95-63-6 1,2,4-Trimethylbenzene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 96-12-8 1,2-Dibromo-3-chloropropane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 106-93-4 1,2-Dibromoethane (EDB) ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260E 7D18028 95-50-1 1,2-Dichlorobenzene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA9260B 7DIS028 107-06-2 1,2-Dichloroedme ND ug/kg dry 5.86 1 04/19/07 14:52 JWT EPA 8260B 7D18028 78-87-5 1,2-Dichloropropane ND LI ug/kgdry 5.96 1 04/18/07 14:52 JWT EPA 8260B 7D18028 108-67-8 1,3,5-Trimethylbenzene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 9260B 7DI8028 541-73-1 1,3-Dichlorobenzene ND ug/kg dry 5.86 1 04/19/07 14:52 JWT EPA 8260B 7DIS028 142-28-9 1,3-Dichloropropane ND ug/kg dry 5.96 1 04/18/07 14:52 JWT EPA 8260B 7D18028 106-46-7 1,4-Dichlorobenzme ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 594-20-7 2,2-Dichloropropane ND ug/kg dry 5.86 1 04/19/07 14:52 JWT EPA 8260B 7D18028 78.93-3 2-Butanone ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 110-75-8 2-Chloroethylvinyl ether ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 9549-8 2-Chlorotoluene ND ug/kg dry 5.86 I 04/19/07 14:52 JWT EPA 8260B 7DI8028 591-79-6 2-Hexanone ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 7946-9 2-Nitropropane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 10643-4 4-Chlorotoluene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260E 7DI8028 108-10-1 4-Methyl-2-pentanone ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 67-64-1 Acetone ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 7143-2 Benzene ND ug/kg dry 0.586 1 04/18/07 14:52 JWT EPA 8260E 7DIS028 108-86-1 Bromobenzene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 74-97-5 Bromochloromethane ND LI ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DIS028 75-274 Bromodichloromethane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 75.25-2 Bromoform ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 74-83-9 Bromomethane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 75-15-0 Carbon disulfide ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 56-23-5 Carbon Tetrachloride ND LI ug/kgdry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 108-90-7 Chlorobenzene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 71)18028 124-48-1 Chlorodibromomethane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 22 of 47 4310 East Anderson Road Orlando, FL 32812.800461-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S4 - Lab Number: OQD0273-05 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte Result Q Units PQL Factor Date/Time By Method --------------- Batch ----- -------------------------------------------------------------------------------------------------------------------------- Volatile Organic Compounds by EPA Method 8260B - Cont. 75-00-3 Chloroethane ND ug/kgdry 5.96 t 04/19/07 14:52 JWT EPA 8260B 7DIS028 67-W3 Chloroform ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260E 7DIS028 74-87-3 Chloromethane ND ug&S dry 5.96 1 04/19/07 14:52 JWT EPA 8260B 7DI9028 156-59-2 cis-1,2-Dichloroethene ND LI ug/kg dry 5.86 l 04/18/07 14:52 JWT EPA 8260B 7D18028 10061-01-5 cis-1,3-Dichloropropene ND Ll ug/kg dry 5.86 l 04/18/07 14:52 JWT EPA 8260B 7DI8028 74-95-3 Dibromomethane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 9260B 7D18029 75-71-8 Dichlorodifluoromethane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 9260B 7DI8028 100414 Ethylbenzene ND ug/kg dry 0.586 1 04/18/07 14:52 JWT EPA 8260B 7D18028 87-69-3 Hexachlorobutadiene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 98-82-8 lsopropylbenzene ND ug/kgdry 5.96 1 04/18/07 14:52 JWT EPA 8260B 7D18028 1634-044 Methyl tert-Butyl Ether ND ug/kg dry 0.596 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 75-09-2 Methylene Chloride ND ug/kg dry 5.86 1 04/19/07 14:52 JWT EPA 8260B 7D18028 91-20-3 Naphthalene ND ug/kg dry 0.586 1 04/18/07 14:52 JWT EPA 8260B 7D18028 104-51-8 n-Buylbenzene ND ug/kg dry 5.86 1 04/19/07 14:52 JWT EPA 8260B 7D18028 103-65-1 n-Propylbenzene ND ug/kgdry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 99-87-6 p-Isopropyltoluene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DIS028 135-98-8 sec-Buylbenzene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 10042-5 Styrene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 98-06-6 ten-Buylbenzene ND ug/kgdry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7D18028 127-19-4 Tetrachloroethene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 108-88-3 Toluene ND ug/kgdry 0.586 1 04/19/07 14:52 JWT EPA 8260B 7DIS028 156-60-5 trans-1,2-Dichloroethene ND ug/kgdry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 10061-02-6 trans-1,3-Dichloropropene ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 79-01-6 Trichloroethene ND ug/kgdry 5.86 1 04/19/07 14:52 JWT EPA 8260B 7D18028 75-69-4 Trichlorofluoromethane ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260B 7DI8028 75-014 Vinyl chloride ND ug/kg dry 5.86 1 04/18/07 14:52 JWT EPA 8260E 7DI8028 1330-20-7 Xylenes, total ND ug/kg dry 0.586 1 04/18/07 14:52 JWT EPA 8260B 7D18028 Surrogate: 1,1-Dichloroeihane-d4 (73-137%) 119 % Surrogate: a-Bromo/luorobenzene (59-118%) 101 % Surrogate: Dibromo/luoromethane (55-1 a5%) 110 % Surrogate: Toluene48 (80-117%) 107 % Semivolatile Organic Compounds by EPA Method 8270C 86-30-6 N-Nitrosodiphenylamine ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 95-50-1 1,2-Dichlorobenzene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 541-73-1 1,3-Dichlorobenzene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 10646-7 1,4-Dichlorobenzene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 100-254 1,4-Dinitrobenzene ND ug/kg dry 411 1 04/20/07 00:43 REM EPA 8270c 7DI8013 90-12-0 I-Methylnaphthalene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 95-95-4 2,4,5-Trichlorophenol ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI9013 88-06-2 2,4,6-Trichlorophenol ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 120-83-2 2,4-Dichlorophenol ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 23 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560 • Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S4 - Lab Number: OQD0273-05 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte —------------------------------------------------------------- Result Q Units PQL Factor ........... Date/rime ----------------------------------- By Method Batch --------------- Semivolatile Organic Compounds by EPA Method 8270C - Cont. 105-67-9 2,4-Dimethylphenol ND ugAg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 51-28-5 2,4-Dinitrophenol ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 121-14-2 2,4-Dinitrotoluene ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 606-20-2 2,6-Dinitrotoluene ND ug/kg dry 206 1 0420/07 00,43 REM EPA 8270c 7DI8013 91-58-7 2-Chloronaphthalene ND ugAg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 95-57-8 2-Chlorophenol ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 91-57-6 2-Methylnaphthalene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 9548-7 2-Methylphenol ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 88-74-4 2-Nitroaniline ND ug/kg dry 206 I 04/20/07 00:43 REM EPA 8270c 7D18013 88-75-5 2-Nitrophenol ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D 18013 91-94-1 3,3'-Dichlorobenzidine ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 1319-77-3 3/4-Methylphenol ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 99-09-2 3-Nitroaniline ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 534-52-1 4,6-Dinitro-2-methylphenol ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 101-55-3 4-Bromophenyl phenyl ether ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 59-50-7 4-Chloro-3-methylphenol ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 10647-8 4-Chloroaniline ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 7005-72-3 4-Chlorophenol phenyl ether ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 100-01.6 4-Nitroaniline ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DIS013 100-02-7 4-Nitrophenol ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 83-32-9 Acenaphthene ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 209-96-8 Acenaphthylene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 62-53-3 Aniline ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 120-12-7 Anthracene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 528-29-0 1,2-Dinitrobenzene ND ug/kg dry 411 1 0420/07 00:43 REM EPA 8270c 7D18013 92-87-5 Benzidine ND L2 ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 56-55-3 Benzo (a) anthracene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 99-65-0 1,3-Dinitrobenzene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 50-32-8 Benzo (a) pyrene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 205-99-2 Benzo (b) fluoranthene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 191-24-2 Benzo (g,h,i) perylene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 207-08-9 Benzo (k) fluoranthene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 100-51-6 Benzyl alcohol ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 111-91-1 Bis(2-chloroethoxy)methane ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 111444 Bis(2-chloroethyl)ether ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 39638-32-9 Bis(2-chloroisepropyl)ether ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 117-81-7 Bis(2-ethylhexyl)phthalate ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 85-68-7 Butyl benzyl phthalate ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 86-74-8 Carbazole ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 71) 18013 218-01-9 Chrysene ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 53-70-3 Dibenz (a,h) anthracene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 24 of 47 4310 East Anderson Road Orlando, FL 32812.OW-851-2560 • Fax 407-858-0888 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S4 - Lab Number: OQD0273-05 - Matrix: Solid/Soil Dil Analyzed CAS # Analyte ---------------- Result Q ------------ — ---------------------------------------------------------......---------------- Units PQL Factor Date/Time By Method Batch --------------------------------- Semivolatile Organic Compounds by EPA Method 8270C - Cont. 132-64-9 Dibenzof mm ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D I9013 94.66-2 Diethyl phthalate ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D I9013 131-11-3 Dimethyl phthalate ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 84-74-2 Di-n-butyl phthalate ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 117-94-0 Di-n-octyl phthalate ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 122-39-4 Diphenylamine ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 206-44-0 Fluoranthene ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 122-66-7 1,2-Dipherrylhydrazine ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 86-73-7 Fluorene ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI9013 118-74-1 Hexachlorobenzene ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 87-68-3 Hexachlorobutadiene ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 77-47-4 Hexachlorocyclopentadiene ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 67-72-1 Hexachloroethane ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7D18013 193-39-5 Indeno (1,2,3-ed) pyrene ND ug/kg dry 206 1 04/20/07 00:43 REM EPA 8270c 7DI8013 78-59-1 lsophorone ND L2 ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 91-20-3 Naphthalene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 98-95-3 Nitrobenzene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 62-75-9 N-Nitrosodimethylamine ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 62t-64-7 N-Nitrosodi-n-propylamine ND ugAg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 87-86-5 Pentachlorophenol ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 85-01-8 Phenandurne ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 108-95-2 Phenol ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 129-00-0 Pyrene ND ugAg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 110-86-1 Pyridine ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7DI8013 120-82-1 1,2,4-Trichlorobenzene ND ug/kg dry 206 1 0420/07 00:43 REM EPA 8270c 7D18013 Surrogate: 1,4,6-Tribromophenol (11-135%) 39 % Surrogate: 2-Fluorobiphenyl (24-121%) 53 % Surrogate: 2-Fluorophenol (13-108%) 42 % Surrogate: Nitrobenzene-0 (19-111 %) 40 % Surrogate: Phenol-d5 (18-113%) 44 % Surrogate: Terphenyl-d14 (44-171 %) 70 % MA-EPH 83-32-9 Acenaphthene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 208-96-8 Acenaphthylene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 120-12-7 Anthracene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 56-55-3 Benzo(a]anthracene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 50-32-8 Benzo[a]pyrene ND mg/Kg dry 0.36 1 04/19/07 07:23 TP MA-EPH 17612 205-99-2 Benzo[b]fluoranthene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 191-24-2 Benzo[g,h,i]perylene ND mg/Kgdry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 207-08-9 Benzo[k]fluoranthene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 218-01-9 Chrysene NO mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 25 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560 • Fax 407-856-08M Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY LABORATORY REPORT Sample ID: S4 - Lab Number: OQD0273-05 - Matrix: Solid/Soil IAl Analyzed CAS # Analyte Result Q Units PQL Factor ------------------------- Dat&Time By Method --------------------- Batch ----------- -- —------------------------------- MA-EPH - Cont. —---------------------------------------------- 53-70-3 Dibenz(a,h)anthracene ND mg/Kgdry 0.36 1 04/19/07 07:23 TP MA-EPH 17612 20644-0 Fluoranthene ND mg/Kg dry 0.36 1 04/19/07 07:23 TP MA-EPH 17612 W73-7 Fluorene ND mg/KS dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 193-39-5 Indeno[1,2,3-ed]pyrene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 91-57-6 2-Methylnaphthalene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 91-20-3 Naphthalene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 85-01-8 Phenanthrene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 129-00-0 Pyrene ND mg/Kg dry 0.36 1 04/18/07 07:23 TP MA-EPH 17612 NA Cl1-C22 Aromatics (unadjusted) ND mg/Kg dry 3.6 1 04/18/07 07:23 TP MA-EPH 17612 NA Cl 1-C22 Aromatics (Adjusted) ND mg/Kg dry 3.6 l 04/18/07 07:23 TP MA-EPH 17612 NA C19-06 Aliphatics ND mg/Kg dry 3.6 1 04/18/07 07:23 TP MA-EPH 17612 NA C9-C18 Aliphatics ND mg/KS dry 3.6 1 04/18/07 07:23 TP MA-EPH 17612 NA Total EPH ND mg/Kg dry 3.6 1 04/19/07 07:23 TP MA-EPH 17612 Surrogate: 1-Bromonaphihalene (40-14lW/.,) 97 % Surrogate: 2-Fluorobiphenyl (40-140%) 104 % Surrogate: o-Terphenyl (40-140%) 70 % Surrogate: I-Chloroociadecane (40-140%) 51 % MAVPH 7143-2 Benzene ND mg/Kg dry 0.55 1 04/23/07 08:50 JLD MAVPH 17704 NA C9-C12 Aliphatics (adjusted) ND mg/Kg dry 5.5 1 04/23/07 08:50 JLD MAVPH 17704 NA C9-C10 Aromatics ND mg/Kg dry 5.5 1 04/23/07 08:50 JLD MAVPH 17704 100.414 Ethylbenzene ND mg/Kg dry 0.55 1 04/23/07 08:50 JLD MAVPH 17704 136777-61-2 m-Xylene & p-Xylene ND mg/Kg dry 1.1 1 04/23/07 08:50 JLD MAVPH 17704 NA Total VPH ND mg/Kg dry 5.5 1 04/23/07 08:50 JLD MAVPH 17704 Surrogate: 2,5-Dibromotoluene (fid) (70-130%) 102 % 1634-044 Methyl tert-butyl ether ND mg/Kg dry 0.11 1 04/23/07 08:50 JLD MAVPH 17704 Surrogate: 1,5-Dibromotoluene (pid) (70-130%) 99 % 91-20-3 Naphthalene ND mg/Kg dry 1.1 1 04/23/07 08:50 JLD MAVPH 17704 9547-6 o-Xylene ND mg/Kg dry 0.55 1 04/23/07 08:50 JLD MAVPH 17704 108-88-3 Toluene ND mg/Kg dry 0.55 1 04/23/07 08:50 JLD MAVPH 17704 NA C5-C8 Aliphatics (unadjusted) ND mg/KS dry 5.5 1 04/23/07 08:50 JLD MAVPH 17704 NA C9-C12 Aliphatics (unadjusted) ND mg/Kg dry 5.5 1 04/23/07 08:50 JLD MAVPH 17704 NA C5-C8 Aliphatics (adjusted) ND mg/Kg dry 5.5 1 04/23/07 08:50 JLD MAVPH 17704 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 26 of 47 4310 East Anderson Road Orlando, Fl. 32812' 80D-851-2560' Fax 407-858-0888 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY SAMPLE EXTRACTION DATA Wt/Vol Parameter ---- Lab Number --------------------------------------- Extracted Extracted Vol ----.------------...............------------. Date Analyst Method ------. ------------------- ----------- ----- Semivolatile Organic Compounds by EPA Method 8270C -- OQD0273-01 30.0 g 1.0 mL 04/182007 AYN EPA 3545 MS Semivolatile Organic Compounds by EPA Method 8270C OQD0273-02 30.0 g LO mL 04/182007 AYN EPA 3545 MS Semivolatile Organic Compounds by EPA Method 8270C OQD0273-03 30.0 g 1.0 mL 04/19/2007 AYN EPA 3545 MS Semivolatile Organic Compounds by EPA Method 9270C OQD0273-04 30.0 g 1.0 mL 04/182007 AYN EPA 3545 MS Semivolatile Organic Compounds by EPA Method 8270C OQD0273-05 30.0 g 1.0 mL 04/182007 AYN EPA 3545 MS TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 27 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560 • Fax 407-856-0888 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Blank Analyte Blank Value Q Units Q.C. Batch Lab Number General Chemistry Parameters %Solids 100 %. 7D19040 7DI9040-BLKI Volatile Organic Compounds by EPA Method 8260B 1,1,1,2-Tebuhloroetltane ND ug/kg wet 7D18028 7DI8028-BLKI l,l,l-Trichloroethane ND ug/kgwet 7D18028 7DI8029-BLKI 1,1,2,2-Tetrachloroethane ND ug/kg wet 7DI9028 7DI8028-BLKI 1,1,2-Trichloroethane ND ug/kgwet 7DI8028 7DI9028-BLKI 1,1-Dichloroethane ND ug/kgwet 7D18028 7D18029-BLKI 1,1-Dichloroethene ND ug/kg wet 7DI8028 7DI8028-BLKI 1,1-Dichloropropene ND ug/kg wet 7D18028 7DI8029-BLKI 1,2,3-Trichlorobenzene ND ug/kg wet 7D18028 7DI8028-BLKI 1,2,3-Trichloropropane ND ug/kg wet 7DI8028 7DI8028-BLKI 1,2,4-Trichlorobenzene ND ug/kg wet 7D18028 7DI8028-BLKI 1,2,4-Trimethylbenzene ND ug/kg wet 7DI8028 7DI8028-BLKI 1,2-Dibromo-3-chloropropane ND ug/kg wet 7DI8028 7DI8028-BLKI 1,2-Dibromoethane(EDB) ND ug/kgwet 7D18028 7DI8028-BLKI 1,2-Dichlorobenzene ND ug/kg wet 7D18028 7DI8028-BLKI 1,2-Dichloroethane ND ug/kg wet 7DI8028 7DI8028-BLKI 1,2-Dichloropropane ND ugAgwet 7DI8028 7DI8028-BLKI 1,3,5-Trimethylbenzene ND ug/kg wet 7DI8028 7DIS028-BLKI 1,3-Dichlorobenzene ND ug/kg wet 7D18028 7DI8028-BLKI 1,3-Dichloropropane ND ug/kg wet 7DI8028 7DI8028-BLKI 1,4-Dichlorobenzene ND ug/kg wet 7DI8028 7DI8028-BLKI 2,2-Dichloropropane ND ug/kgwet 7D18029 7DI8028-BLKI 2-Butanone ND ug/kg wet 7D18028 7DI8028-BLKI 2-Chlomethylvinyl ether ND ug/kg wet 7DI8028 7DI8028-BLKI 2-Chlorotoluene ND ug/kgwet 7DI8028 7DI8028-BLKI 2-Hexanone ND ug/kg wet 7DIS028 7DI8028-BLKI 2-Nitropropane ND ug/kg wet 7D18028 7DI8028-BLKI 4-Chlorotoluene ND ug/kg wet 7DI8028 7DI8028-BLKI 4-Methyl-2-pentanone ND ug/kg wet 7D18028 7DI8028-BLKI Acetone ND ug/kg wet 7DI8028 7DI8028-BLKI Benzene ND ug/kg wet 7DI8028 7DI8028-BLKI Bromobenzene ND ug/kg wet 7DI8028 7DI9028-BLKI Bromochloromethane ND ug/kg wet 7DI8028 7DI8028-BLKI Bromodichloromethane ND ug/kg wet 7D18028 7DI8028-BLKI Bromoform ND ug/kg wet 7D18028 7DI8028-BLKI Bromomethane ND ug/kg wet 71)18028 7DI8028-BLKI Carbon disulfide ND ug/kgwet 7D18028 7DI8028-BLKI Carbon Tetrachloride ND ug/kg wet 7DI9028 7DI8028-BLKI Chlorobenzene ND ug/kg wet 7D18028 7DI8028-BLKI Chlorodibromomethane ND ug/kg wet 7D18028 7D18028-BLKI Chloroethane ND ug/kg wet 7D18028 7DI8028-BLKI Chloroform ND ug/kg wet 7D 18028 71) 18028-BLK I TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 28 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-OM Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Blank - Cont. Analyte Blank Value Q Units Q.C. Batch Lab Number Volatile Organic Compounds by EPA Method 8260B Chloromethane ND ug/kg wet 7D18028 7DI8028-BLKI cis-1,2-Dichloroethene ND ug/kg wet 7D18028 7D18029-BLKI cis-1,3-Dichloropropene ND ug/kgwet 7DI9028 7DIS028-BLKI Dibromomethane ND ug/kg wet 7DI8028 7D18028-BLKI Dichlorodifluoromethane ND ug/kg wet 7D18028 7DIS028-BLKI Ethylbenzene ND ug/kg wet 7DI8028 7DI8028-BLKI Hexachlorobutadiene ND ug/kg wet 7D18028 7DI9028-BLKI lsopropylbenzene ND ugAg wet 7D18028 7DIS029-BLKI Methyl tert-Butyl Ether ND ug/kg wet 7DI8028 7DI8028-BLKI Methylene Chloride 9.29 ug/kg wet 7D18028 7D18029-BLKI Naphthalene ND ug/kg wet 7DI8028 7D18028-BLKI n-Buylbenzene ND ug/kg wet 7D18028 7DI8029-BLKI n-Propylbenzene ND twkg wet 7D18028 7DI8028-BLKI p-Isopropyltoluene ND ug/kg wet 7DI8028 7D18028-BLKI sec-Buylbenzene ND ug/kg wet 7D18028 7DI8029-BLKI Styrene ND ug/kg wet 7D18028 71)18028-BLKI tent-Buylbenzene ND ug/kgwet 7D18028 7DI8028-BLKI Tetrachloroethene ND ug/kg wet 7D18029 7D18028-BLKI Toluene 0.580 ug/kg wet 7DIS028 7DI8028-BLKI trans-1,2-Dichloroethene ND ug/kgwet 7DIS028 7DI8028-BLKI trans-1,3-Dichloropropene ND ug/kg wet 7DI8028 7D18029-BLKI Trichloroethene ND ug/kg wet 7DI8028 7DI8028-BLKI Trichlorofluoromethane ND ug/kg wet 7D18028 7D18029-BLKI Vinyl chloride ND uSAS wet 7D18028 7DI8029-BLKI Xylenes, total ND ug/kg wet 7D18028 7D18029-BLKI Surrogate:l,2-Dichloroeihane-d4 51.2 ug/kg wet 7D18028 7D18029-BLKI Surrogate: 4-Bromq luorobenzene 50.0 ug/kg wet 7DI8028 7DI8028-BLKI Surrogate: Dibromo/luoromethane 52.6 ug/kg wet 7D18028 7DI8028-BLKI Surrogate: Toluene-d8 53.1 ug/kg wet 7DI8028 7DI8029-BLKI Semivolatile Organic Compounds by EPA Method 8270C N-Nitrosodiphenylamine ND ug/kg wet 7D18013 7DI8013-BLKI 1,2-Dichlorobenzene ND ug/kg wet 7D18013 7DI8013-BLKI 1,3-Dichiorobenzene ND ug/kg wet 7DI8013 7DI8013-BLKI 1,4-Dichlorobenzene ND ug/kg wet 7D18013 7DI8013-BLKI 1,4-Dinitrobenzene ND ug/kg wet 7D18013 7DI8013-BLKI I-Methylnaphthalene ND ug/kg wet 71318013 7DIS013-BLKI 2,4,5-Trichlorophenol ND ug/kg wet 7D18013 7DI8013-BLKI 2,4,6-Trichlorophenol ND ug/kg wet 7DI8013 7DI8013-BLKI 2,4-Dichlorophenol ND ug/kg wet 7DI8013 7DI8013-BLKI 2,4-Dimethylphenol ND ug/kg wet 7DI8013 7DI8013-BLKI 2,4-Dinitrophenol ND ug/kg wet 7DI8013 7DIS013-BLKI 2,4-Dinitrotoluene ND ug/kg wet 7DI8013 7DI8013-BLKI 2,6-Dinitrotoluene ND ug/kg wet 7DI8013 7DI8013-BLKI 2-Chloronaphthalene ND ug/kg wet 7DI8013 7DI8013-BLKI TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 29 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Blank - Cont. Analyte Blank Value Q Units Q.C. Batch Lab Number Semivolatile Organic Compounds by EPA Method 8270C 2-Chlorophenol ND ug/kg wet 7DI8013 7DI8013-BLKI 2-Methylnaphthalene ND ug/kg wet 7D18013 7DI8013-BLKI 2-Methylphenol ND ug/kg wet 7DI8013 7D18013-BLKI 2-Nibxmiline ND ug/kg wet 7D18013 7DI8013-BLKI 2-Nitrophenol ND ug/kg wet 7DI8013 7DI8013-BLKI 3,3'-Dichlorobermdine ND ug/kg wet 7DI8013 7DI8013-BLKI 3-Nitroaniline ND ug/kg wet 7D18013 7DI8013-BLKI 4,6-Dinitro-2-methylphenol ND ug/kg wet 7D18013 7DI8013-BLKI 4-Bromophenyl phenyl ether ND ug/kg wet 7DI8013 7DI8013-BLKI 4-Chloro-3-methylphenol ND usAg wet 7DI8013 7DI8013-BLKI 4-Chloroaniline ND ug/kg wet 7D18013 7DI8013-BLKI 4-Chlorophenyl phenyl ether ND ug/kg wet 7DI8013 7DI8013-BLKI 4-Nitroaniline ND ug/kgwet 7D18013 7DI8013-BLKI 4-Nitrophenol ND ug/kgwet 7DI8013 7DI8013-BLKI Acenaphthene ND ug/kgwet 7DI8013 7DI8013-BLKI Acenaphthylene ND ug/kg wet 7D18013 7DI8013-BLKI Aniline NO ug/kgwet 7DI8013 7D18013-BLKI Anthracene ND ug/kgwet 7DI8013 7DI8013-BLKI 1,2-Dinitrobenzene ND ug/kg wet 7DI8013 7DI8013-BLKI Benzidine ND ug/kg wet 7D18013 7DI8013-BLKI Benzo (a) anduacene ND ug/kg wet 7DI8013 7DI8013-BLKI 1,3-Dinitrobenzene ND ug/kg wet 7D18013 7DI8013-BLKI Benzo (a) pyrene ND ug/kg wet 7D18013 7DI8013-BLKI Benzo (b) fluoranthene ND ug/kgwet 7D18013 7DI8013-BLKI Benzo (g,h i) perylene ND ug/kg wet 7DI8013 7DI8013-BLKI Benzo (k) fluoranthene ND ug/kg wet 7D18013 7DI8013-BLK I Benzyl alcohol ND ug/kg wet 7D18013 7DI8013-BLKI Bis(2-chloroethoxy)methane ND ug/kg wet 7DI8013 7DI8013-BLKI Bis(2chloroethyl)ether ND ug/kg wet 7DI8013 7DI8013-BLKI Bis(2chloroisopropyl)ether ND ug/kg wet 7D18013 7DI8013-BLKI Bis(2-ethylhexyl)phthalate ND ug/kg wet 7D18013 7DI8013-BLKI Butyl benzyl phthalate ND ug/kg wet 7DI8013 7DI8013-BLKI Carbazole ND ug/kg wet 7DI8013 7DI8013-BLKI Chrysene ND ug/kg wet 7D18013 7DI8013-BLKI Dibenz (a,h) anthracene ND ug/kg wet 7D18013 7DI8013-BLKI Dibenzofivan NO ug/kg wet 7DI8013 7DI8013-BLKI Diethyl phthalate ND ug/kg wet 7DI8013 7DI8013-BLKI Dimethyl phthalate ND ug/kg wet 7DI8013 7DI8013-BLKI Di-n-butyl phthalate ND ug/kg wet 7D18013 7DI8013-BLKI Di-n-octyl phthalate ND ug/kg wet 7D18013 7DI8013-BLKI Diphenylamine ND ug/kg wet 71)18013 7DI8013-BLKI Fluoranthene ND ug/kg wet 7DI8013 7DI8013-BLKI 1,2-Diphenylhydrazine ND ug/kg wet 7D18013 7DI8013-BLKI Fluorene ND ug/kg wet 7D18013 7DI8013-BLKI TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 30 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Blank - Cont. Analyte Blank Value Q Units Q.C. Batch Lab Number Semivolatile Organic Compounds by EPA Method 8270C Hexachlorobenzene ND ug/kgwet 7D18013 7DI8013-BLKI Hexachlorobutadiene ND ug/kg wet 7D18013 7DI9013-BLKI Hexachlorocyclopentadiene ND ug/kg wet 7D18013 7DIS013-BLKI Hexachloroethane ND ug/kg wet 7DI8013 7DI9013-BLKI Indeno (1,2,3-ed)pyrene ND ug/kg wet 7D18013 7DIS013-BLKI Isophorone ND ug/kg wet 7D18013 7D18013-BLKI Naphthalene ND ug/kg wet 7W8013 7DI8013-BLKI Nitrobenzene NO ug/kg wet 7DIS013 7DIS013-BLKI N-Nitrosodimethylamine ND ug/kg wet 7D18013 7DI8013-BLKI N-Nitrosodi-n-propylamine ND ug/kg wet 7DIS013 7DIS013-BLKI Pentachlorophenol ND ug/kg wet 7D►8013 7DI8013-BLKI Phenanthrene ND ug/kg wet 7M8013 7DI8013-BLKI Phenol ND ug/kg wet 7D18013 7DI8013-BLKI Pyrene ND ug/kg wet 7D18013 7DI8013-BLKI Pyridine ND ug/kg wet 7DI8013 7DIS013-BLKI 1,2,4-Trichlorobenzene ND ug/kg wet 7D18013 7DI8013-BLKI Surrogate: 1,4,6-Tribromophenol 4700 ug/kg wet 7D18013 7DI8013-BLKI Surrogate:2-Fluorobipherryl 2310 ug/kg wet 7D18013 7DI8013-BLKI Surrogate: 2-Fluorophenol 3780 ug/kg wet 7DI8013 7DI8013-BLKI Surrogate: Nitrobenzene-0 1780 ug/kg wet 7DI8013 7DI8013-BLKI Surrogate: Phenol-0 4200 ug/kg wet 7DI9013 7DI9013-BLKI Surrogate: Terphenyl-d14 2930 ug/kg wet 7D18013 7DI8013-BLKI MA-EPH Acenaphthene ND mg/Kg dry 17612 360-17650-2 Acenaphthylene ND mg/Kg dry 17612 360-17650-2 Anthracene ND mg/Kg dry 17612 360-17650-2 Benzo[a]anthracene NO mg/Kg dry 17612 360-17650-2 Benzo[a]pyrene ND mg/Kg dry 17612 360-17650-2 Benzo[b]fluoranthene ND mg/Kg dry 17612 360-17650-2 Benzo[g,h,i]perylene ND mg/Kg dry 17612 360-17650-2 Benzo[k]fluoranthene ND mg/Kg dry 17612 360-17650-2 Chrysene NO mg/Kg dry 17612 360-17650-2 Dibenz(a,h)anthracene ND mg/Kg dry 17612 360-17650-2 Fluoranthene ND mg/Kg dry 17612 360-17650-2 Fluorene ND mg/Kg dry 17612 360-17650-2 Indeno[1,2,3-cd]pyrene ND mg/Kg dry 17612 360-17650-2 2-Methylnaphthalene ND mg/Kg dry 17612 360-17650-2 Naphthalene ND mg/Kg dry 17612 360-17650-2 Phenanthrene ND mg/Kg dry 17612 360-17650-2 Pyrene ND mg/Kg dry 17612 360-17650-2 CI I-C22 Aromatics (unadjusted) ND mg/Kg dry 17612 360-17650-2 C I I -C22 Aromatics (Adjusted) ND mg/Kgdry 17612 360-17650-2 C19-06 Aliphatics ND mg/Kg dry 17612 360-17650-2 C9-C 18 Aliphatics ND mg/Kg dry 17612 360-17650-2 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 31 of 47 4310 East Anderson Road Orlando, FL 32812. 800-851-2560 • Fax 407-856-OBW Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Blank - Cont. Analyte ------------------------------- Blank Value — --------- -- Q Units -- — --------...---------------- Q.C. Batch — Lab Number —------------------------------- ----------------- MA-EPH Total EPH ND mg/Kg dry 17612 360-17650-2 Surrogate: 2-Bromonaphthalene 3.3 mg/4 dry 17612 360-17650.2 Surrogate: 2-Fluorobiphe* 3.6 mg/Kg dry 17612 360-17650-2 Surrogate: o-Terphenyl 5.6 mg/Kg dry 17612 360-17650.2 Surrogate: I-Chloroociadecane 4.4 mg/Kg dry 17612 360-17650-2 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 32 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-OM Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Duplicate Sample Analyze -rig. Val. Duplicate Q Units R- - RPD Limit Q.C. Batch Duplicated General Chemistry Parameters %Solids 75.6 75.2 "/n. 0.5 20 7DI9040 OQD0273-01 Volatile Organic Compounds by EPA Method 8260B 1,1,1,2-Tetrachloroethane ND ND ug/kg dry 30 7D18028 OQD0273-02 1,1,1-Trichloroethane ND ND ug/kgdry 30 7DI8028 OQD0273-02 1,1,2,2-Tetrachloroethane ND ND ug/kg dry 30 7DI8028 OQD0273-02 1,1,2-Trichloroethane ND ND ug/kg dry 30 7DI8028 OQD0273-02 1,1-Dichloroethane ND ND ug/kg dry 30 7DI8028 OQD0273-02 1, 1 -Dichloroethene ND ND ug/kg dry 30 7DI8028 OQD0273-02 1,1-Dichloropropene ND ND ug/kg dry 30 7D18028 OQD0273-02 1,2,3-Trichlorobenzene ND ND ug/kg dry 30 7D18028 OQD0273-02 1,2,3-Trichloropropane ND ND ug/kg dry 30 7DI8029 0QD0273-02 1,2,4-Trichlorobenzene ND ND ug/kg dry 30 7D 18028 OQD0273-02 1,2,4-Trimethylbenzene ND ND ug/kg dry 30 7D18028 OQD0273-02 1,2-Dibromo-3-chloropropane ND ND ug/kg dry 30 7D18028 OQD0273-02 1,2-Dibromoethane (EDB) ND ND ug/kg dry 30 7D18028 OQD0273-02 1,2-Dichlorobenzene NO NO ug/kg dry 30 7DIS028 OQD0273-02 1,2-Dichloroethane ND ND ug/kg dry 30 7DI8028 OQD0273-02 1,2-Dichloropropane ND ND ug/kg dry 30 7DI8028 OQD0273-02 1,3,5-Trimethylbenzene ND ND ug/kg dry 30 7D18028 OQD0273-02 1,3-Dichlorobenzene ND ND ug/kg dry 30 7DI8028 OQD0273-02 1,3-Dichloropropane ND ND ug/kg dry 30 7D18028 OQD0273-02 1,4-Dichlorobenzene ND ND ug/kg dry 30 7DI8028 OQD0273-02 2,2-Dichloropropane ND ND ug/kg dry 30 7D18028 OQD0273-02 2-Butanone ND 3.66 ug/kgdry 30 7D18028 OQD0273-02 2-Chloroethylvinyl ether ND ND ug/kg dry 30 7DI8028 OQD0273-02 2-Chlorotoluene ND ND ug/kg dry 30 7DI8028 OQD0273-02 2-Hexanone ND ND ug/kg dry 30 7D18028 OQD0273-02 2-Nitropropane ND ND ug/kg dry 30 7DI8028 OQD0273-02 4-Chlorotoluene ND ND ug/kg dry 30 7DI8028 OQD0273-02 4-Methyl-2-pentanone ND ND ug/kg dry 30 7DI8028 OQD0273-02 Acetone 12.3 20.7 It3 uSAg dry 51 30 7D18028 OQD0273-02 Benzene ND ND ug/kg dry 30 7D18028 OQD0273-02 Bromobenzene ND ND ug/kg dry 30 7D18028 OQD0273-02 Bromochloromethane ND ND ug/kg dry 30 7DI8028 OQD0273-02 Bromodichloromethane ND ND ug/kg dry 30 7D18028 OQD0273-02 Bromofonn ND ND ug/kg dry 30 7D18028 OQD0273-02 Bromomethane ND ND ug/kg dry 30 7D18028 OQD0273-02 Carbon disulfide ND ND ug/kg dry 30 7D18028 OQD0273-02 Carbon Tetrachloride ND ND ug/kg dry 30 7D18028 OQD0273-02 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 33 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-25M * Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Duplicate - Cont. Sample Analyte Orig. Val. Duplicate Q — Units RPD RPD Limit Q.C. Batch Du heated Volatile Organic Compounds by EPA Method 8260B Chlorobenzene ND ND ug/kg dry 30 7DI8028 OQD0273-02 Chlorodibromomethane ND ND ug/kg dry 30 7DIS028 OQD0273-02 Chloroethane ND ND ug/kg dry 30 7DI8028 OQD0273-02 Chloroform ND ND ug/kg dry 30 7D18029 OQD0273-02 Chloromethane ND ND ug/kg dry 30 7D18029 OQD0273-02 cis-1,2-Dichloroethene ND ND ug/kg dry 30 7DI8028 OQD0273-02 cis-1,3-Dichloropropene ND ND ug/kg dry 30 7DI8028 OQD0273-02 Dibromomethane ND ND ug/kg dry 30 7D18028 OQD0273-02 Dichlorodifluoromethane ND ND ug/kg dry 30 7D18028 OQD0273-02 Ethylbenzene ND ND ug/kg dry 30 7D18028 OQD0273-02 Hexachlorobutadiene ND ND ug/kg dry 30 7D18028 OQD0273-02 Isopropylbenzene ND ND ug/kg dry 30 7DI8028 OQD0273-02 Methyl tert-Butyl Ether ND ND ug/kg dry 30 7DI8028 OQD0273-02 Methylene Chloride ND ND ug/kg dry 30 7DI8028 OQD0273-02 Naphthalene ND ND ug/kg dry 30 7D18028 OQD0273-02 n-Bhylbenzene ND ND ug/kg dry 30 7DI8028 OQD0273-02 n-Propylbenzene ND ND ug/kg dry 30 7DI8028 OQD0273-02 p-Isopropyltoluene ND ND ug/kgdry 30 7D18028 OQD0273-02 sec-Buylbenzene ND ND ug/kg dry 30 7D18028 OQD0273-02 Styrene ND ND ug/kg dry 30 7DI8028 OQD0273-02 tert-Buylbenzene ND ND ug/kg dry 30 7DI8028 OQD0273-02 Tetrachloroethene ND ND ug/kg dry 30 7D18028 OQD0273-02 Toluene ND ND ug/kgdry 30 7DI8028 OQD0273-02 trans-1,2-Dichloroethene ND ND ug/kg dry 30 7DI8028 OQD0273-02 trans-1,3-Dichloropropene ND ND ug/kg dry 30 7DI8028 OQD0273-02 Trichloroethene NO NO ug/kg dry 30 7D18028 OQD0273-02 Trichlorofluoromethane ND ND ug/kg dry 30 7DI8028 OQD0273-02 Vinyl chloride ND ND ug/kg dry 30 7D18028 OQD0273-02 Xylenes, total ND ND ug/kg dry 30 7D18028 OQD0273-02 Surrogate: 1,2-Dichloroethane-di 57.0 ug/kg dry 7D18028 OQD0273-02 Surrogate: 4-Bromofluorobenzene 50.0 ug/kg dry 7D18028 OQD0273-02 Surrogate: Dibromq luoromethane 54.6 ug/kg dry 7D18028 OQD0273-02 Surrogate: Toluene-dS 54.0 ug/kg dry 71318028 OQD0273-02 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 34 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0888 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA LCS Analyte ----------------------------------------------------------------------------------- Known Val. Analyzed Val Q Units - -------------------------------------------------------- % Rec. Target Range Q.C. Batch General Chemistry Parameters %Solids 1000 960 %. 96 90-110 7D19040 Volatile Organic Compounds by EPA Method 8260B 1,1,1,2-Tettachloroethane 50.0 54.2 ugAg wet 108 76 - 116 7D18028 1,1,1-Trichloroethane 50.0 60.0 ug/kg wet 120 67 - 126 7DI9028 1,1,2,2-Tetrachloroethane 50.0 46.7 ug/kg wet 93 67-125 7DI8028 1,1,2-Trichloroethane 50.0 59.2 ug/kg wet 118 79-121 7DI8028 I,I-Dichloroethane 50.0 59.4 ug/kg wet 119 76- 120 7D18029 1,1-Dichloroethene 50.0 60.8 ug/kg wet 122 62 - 129 7DIS028 1,1-Dichloropropene 50.0 60.7 ug/kg wet 121 69- 126 7DIS028 1,2,3-Trichlorobenzene 50.0 51.2 ug/kg wet 102 61 - 137 7D18028 1,2,3-Trichloropropane 50.0 47.4 ug/kg wet 95 78 - 111 7DI8028 1,2,4-Trichlorobenzene 50.0 50.8 ug/kg wet 102 48 - 149 7DIS028 1,2,4-Trimethylbenzene 50.0 51.8 ug/kg wet 104 65 - 126 7DI8028 1,2-Dibromo-3-chloropropane 50.0 44.5 ug/kg wet 89 66 - 129 7DI8028 1,2-Dibromoethane (EDB) 50.0 58.2 ug/kg wet 116 73 - 123 7D18028 1,2-Dichlombenzene 50.0 49.6 ug/kg wet 99 76 - 118 7D18028 1,2-Dichloroethane 50.0 59.3 ug/kg wet 119 70 - 130 7DIS028 1,2-Dichloropropane 50.0 61.4 L I ug/kg wet 123 86 - 122 7D18028 1,3,5-Trimethylbenzene 50.0 51.3 ug/kg wet 103 73 - 133 7DI8028 1,3-Dichlorobenzene 50.0 52.2 ug/kg wet 104 74 - 140 7DI8028 1,3-Dichloropropane 50.0 59.5 ug/kg wet 119 78 - 120 7DI8028 1,4-Dichlorobenzene 50.0 50.3 ugAg wet lot 74-130 71)18028 2,2-Dichloropropane 50.0 60.1 ug/kg wet 120 63 - 125 7DI8028 2-Butanone 50.0 43.9 ug/kg wet 88 11 - 140 7DI8028 2-Chloroethylvinyl ether 50.0 42.8 ug/kg wet 86 5 - 100 7D18028 2-Chlorotoluene 50.0 51.8 ug/kg wet 104 69 - 132 7DI8028 2-Hexanone 50.0 51.0 ug/kg wet 102 51 - 130 7D18028 2-Nitropropane 50.0 53.6 ug/kg wet 107 56 - 124 7D18028 4-Chlorotoluene 50.0 52.6 ug/kg wet 105 71 - 144 7DI8028 4-Methyl-2-pentanone 50.0 58.0 ug/kg wet 116 57 - 145 7DI9028 Acetone 50.0 39.9 ug/kg wet 80 15 - 145 7D18028 Benzene 50.0 59.9 ug/kg wet 120 76 - 117 7D18028 Bromobenzene 50.0 51.5 ug/kg wet 103 80 - 113 7DI8028 Bromochloromethane 50.0 60.6 L 1 ug/kg wet 121 80 - 117 7D18028 Bromodichloromethane 50.0 62.8 ug/kg wet 126 78 - 128 7D18028 Bromoform 50.0 48.8 ug/kg wet 98 76 - 111 7DI8028 Bromomethane 50.0 61.6 ug/kg wet 123 71 - 163 7DI8028 Carbon disulfide 50.0 53.1 ug/kg wet 106 62 - 120 7DI8028 Carbon Tetrachloride 50.0 60.9 L 1 ug/kg wet 122 72 - 120 7DIS028 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 35 of 47 4310 East Anderson Road Orlando, FL 32812.80D-851-2560 • Fax 407-856-08W Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA LCS - Cont. Analyte - ------------------------------------------------------------------------- Known Val. Analyzed Val Q Units ------------- %Rec. Target Range --- ----- Q.C. Batch Volatile Organic Compounds by EPA Method 8260B Chlorobenzene 50.0 53.0 ugAg wet 106 74 - 116 7DIS028 Chlorodibromomethane 50.0 59.4 ug/kg wet 119 79 - 119 7DI8028 Chloroethane 50.0 56.3 ug/kg wet 113 63 - 133 7DI8028 Chloroform 50.0 58.3 ug/kg wet 117 73 - 118 7D18028 Chloromethane 50.0 58.1 ug/kg wet 116 60 - 143 7DI8028 cis-1,2-Dichloroethene 50.0 61.7 Ll ug/kg wet 123 86- 118 7DI9029 cis-1,3-Dichloropropene 50.0 61.3 Ll ug/kg wet 123 79-120 7DIS028 Dibromomethane 50.0 58.4 ug/kg wet 117 75 - 123 7DI8028 Dichlorodifluoromethane 50.0 56.2 ug/kg wet 112 41 - 171 7DI8028 Ethylbenzene 50.0 52.4 ug/kg wet 105 71 - 129 7DIS028 Hexachlorobutadiene 50.0 50.3 ugAg wet 101 59 - 132 7DI9028 Isopropylbenzene 50.0 51.8 ug/kg wet 104 68 - 119 7DI9028 Methyl tert-Butyl Ether 50.0 55.2 ug/kg wet 110 58 - 119 7DI8028 Methylene Chloride 50.0 70.8 ug/kg wet 142 51 - 167 7DI8028 Naphthalene 50.0 50.1 ug/kg wet 100 72. 126 7DIS028 n-Butylbenzene 50.0 50.2 ug/kg wet 100 57 - 140 7DI8028 n-Propylbenzene 50.0 53.2 ug/kg wet 106 65 - 128 7DIS028 p-Isopropyltoluene 50.0 51.0 ug/kg wet 102 61 - 129 7D18028 sec-Butylbenzene 50.0 51.4 ug/kg wet 103 70-123 7DIS028 Styrene 50.0 52.6 ug/kg wet 105 73 - 119 7DIS028 tert-Butylbenzene 50.0 52.0 ug/kg wet 104 65 - 127 7DI8028 Tetrachloroethene 50.0 60.3 ug/kg wet 121 70 - 122 7DI8028 Toluene 50.0 60.1 usAg wet 120 65 - 128 7DI8028 trans-1,2-Dichloroethene 50.0 59.6 ug/kg wet 119 70 - 120 7DI8028 trans-1,3-Dichloropropene 50.0 57.4 ug/kg wet 115 74 - 116 7D18028 Trichloroethene 50.0 61.6 ug/kg wet 123 73 - 125 7DIS028 Trichlorofluoromethane 50.0 53.8 ug/kg wet 108 59 - 137 7DI9028 Vinyl chloride 50.0 51.4 ug/kg wet 103 61 - 132 7DI8028 Xylenes, total 150 159 ug/kg wet 106 68 - 120 7DI8028 Surrogate: /,2-Dichloroethane-d4 50.0 50.6 ug/kg wet 101 73. 137 7DI8028 Surrogate: 4-Bromonuorohenzene 50.0 51.8 ug/kg wet 104 59 - 118 7DI8028 Surrogate: Dibromq luoromethane 50.0 52.6 ug/kg wet 105 55. 145 7DI8028 Surrogate: Toluene-d8 50.0 53.5 ug/kg wet 107 80 - 117 7D18028 Semivolatile Organic Compounds by EPA Method 8270C N-Nitrosodiphenylamine 3330 2610 ug/kg wet 78 47 - 151 7DI8013 1,2-Dichlorobenzene 3330 2200 ug/kg wet 66 53 - 112 7DI8013 1,3-Dichlorobenzene 3330 2010 ug/kg wet 60 49 - 105 7D18013 1,4-Dichlorobenzene 3330 2010 ug/kg wet 60 52 - 104 7DI8013 1,4-Dinitrobenzene 3330 3280 ug/kg wet 98 68 - 118 7DI8013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 36 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0888 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA LCS - Cont. Analyte Known Val. Analyzed Val Q Units %Rec. Target Range Q.C. Batch Semivolatile Organic Compounds by EPA Method 8270C 1-Methy1naphdWene 3330 1680 ug/kg wet 50 18 - 115 7DIS013 2,4,5-Trichlorophenol 3330 3050 ug/kg wet 92 59-115 7DIS013 2,4,6-Trichlorophenol 3330 3010 ug/kg wet 90 44 - 126 7D18013 2,4-Dichlorophenol 3330 2030 ug/kg wet 61 25 - 113 7DIS013 2,4-Dimethylphenol 3330 1950 ug/kg wet 59 29-111 71DI8013 2,4-Dinitrophenot 3330 2590 ug/kg wet 78 38 - 165 7DI9013 2,4-Dinitmtoluene 3330 2500 ugAg wet 75 65 - 129 7DI9013 2,6-Dinitrotoluene 3330 2700 ug/kg wet 81 66 - 112 7DI8013 2-Chloronaphthalene 3330 2740 ug/kg wet 82 55 - 116 7DI8013 2-Chlorophenol 3330 2150 ug/kg wet 65 52 - 109 7DIS013 2-Methylnaphthalene 3330 1820 ug/kg wet 55 20 - 125 7DI8013 2-Methylphenol 3330 2300 ug/kg wet 69 55 - 113 7D18013 2-Nitroaniline 3330 2770 ug/kg wet 83 65 - 117 7DI8013 2-Nitrophenol 3330 1990 ug/kg wet 60 24 - 117 7DI8013 3,3'-Dichlorobenzidine 3330 3500 ug/kg wet 105 I0 - 163 7DIS013 3-Nitroaniline 3330 2440 ug/kg wet 73 48- 110 7DIS013 4,6-Dinitro-2-methylphenol 3330 4030 ug/kg wet 121 72 - 136 7D18013 4-Bromophenyl phenyl ether 3330 2580 ug/kg wet 77 64 - 100 7DIS013 4-Chloro-3-methylphenol 3330 1870 ug/kg wet 56 30 - 117 7DI8013 4-Chloroaniline 3330 1570 ug/kg wet 47 13 - 88 7DIS013 4-Chlorophenyl phenyl ether 3330 2280 ug/kg wet 68 53 - 122 7D18013 4-Nitroaniline 3330 2450 ug/kg wet 74 49 - 132 7D18013 4-Nitrophenol 3330 2500 ug/kg wet 75 38 - 146 7D18013 Acenaphthene 3330 2550 ug/kg wet 77 51 - 124 7DIS013 Acenaphthylene 3330 2570 ug/kg wet 77 58- 124 7DIS013 Aniline 3330 1460 ug/kg wet 44 10 - 167 7DIS013 Andracene 3330 2650 ug/kg wet 80 61 - 122 7DI8013 1,2-Dinitrobenzene 3330 2770 ug/kg wet 83 52 - 146 7DIS013 Benzidine 3330 ND L2 ug/kg wet 5 - 145 7DI9013 Benzo (a) anthmcene 3330 2580 ug/kg wet 77 51 - 139 7DI8013 1,3-Dinitrobenzene 3330 2890 ug/kg wet 87 69 - 120 7DI8013 Benzo (a) pyrene 3330 2840 ug/kg wet 85 65 - 109 7DI8013 Benzo (b) fluoranthene 3330 3050 ug/kg wet 92 57 - 129 7DIS013 Benzo (g,h,i) petylene 3330 1740 ug/kg wet 52 34 - 123 71)18013 Benzo (k) fluoranthene 3330 2960 ug/kg wet 89 53 - 127 7DI8013 Benzyl alcohol 3330 2230 ug/kg wet 67 58 - 113 7DIS013 Bis(2-chloroetboxy)tnethane 3330 1830 ug/kg wet 55 27 - 111 7D18013 Bis(2-chloroethyl)ether 3330 1830 ug/kg wet 55 44-109 7DIS013 Bis(2-chloroisopropyl)ether 3330 2020 ug/kg wet 61 54 - 110 7DI8013 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 37 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA LCS - Cont. Analyte -------------------- ------------------ Known Val. .---------------------------------------------------------------------------------------------------- Analyzed Val Q Units %Rec. Target Range Q.C. Batch Semivolatile Organic Compounds by EPA Method 8270C Bis(2 ethylhexyl)phdudate 3330 2410 ug/kg wet 72 45 - 153 7DI8013 Butyl benzyl phthalate 3330 2520 ug/kg wet 76 43 - 152 7D18013 Carbazole 3330 2550 ug/kg wet 77 57 -123 7D18013 Chrysene 3330 2560 ug/kg wet 77 55 - 130 7D18013 Dibenz (a,h) anthracene 3330 1940 ugAg wet 58 48 - 125 7D18013 Dibenzo[uran 3330 2490 ug/kg wet 75 60 - 128 7DI8013 Diethyl phthalate 3330 2330 ugAg wet 70 52 - 142 7DI8013 Dimethyl phthalate 3330 2680 ug/kg wet 80 62 - 117 7D18013 Di-n-butyl phthalate 3330 2340 ug/kg wet 70 56 - 125 7DI8013 Di-n-octyl phthalate 3330 2270 ug/kg wet 68 47 - 145 7DI8013 Diphenylamine 3330 2610 ug/kg wet 78 51-100 7D18013 Fluoranthene 3330 2520 ug/kg wet 76 58 - 129 7DIS013 1,2-Diphenylhydrazine 3330 2760 ug/kg wet 83 50 - 126 7DI9013 Fluorene 3330 2380 ug/kg wet 71 61 - 129 7D18013 Hexachlorobenzene 3330 2930 ug/kg wet 88 76 - 1 l3 7DI8013 Hexachlorobutadiene 3330 2020 ug/kg wet 61 29 - 120 7D18013 Hexachlorocyclopentadiene 3330 1520 ug/kg wet 46 21 - 115 7DI8013 Hexachloroethane 3330 1940 ugAg wet 58 50 - 104 7D18013 Indeno (1,2,3-cd) pyrene 3330 1940 ug/kg wet 58 44 - 126 7DI8013 Isophorone 3330 708 L2 ug/kg wet 21 24 - I00 7D18013 Naphthalene 3330 1810 ug/kg wet 54 23 - I I8 7DI9013 Nitrobenzene 3330 1770 ug/kg wet 53 26 - 105 7D18013 N-Nitrosodimethylamine 3330 1750 ug/kg wet 53 37 - 100 7D18013 N-Nitrosodi-n-propylamine 3330 2140 ug/kg wet 64 26 - 136 7DI8013 Pentachlorophenol 3330 3110 ug/kg wet 93 30 - 176 7DI8013 Phenanthrene 3330 2660 ug/kg wet 80 61 - 120 7D18013 Phenol 3330 2250 ug/kg wet 68 55 - 114 7DI8013 Pyrene 3330 2130 ug/kg wet 64 45 - 141 7DI8013 Pyridine 3330 1660 ug/kg wet 50 22 - 100 7D18013 1,2,4-Trichlorobenzene 3330 1810 ug/kg wet 54 24 - 108 7D18013 Surrogate: 2,4,6-Tribromophenol 6670 4960 ug/kg wet 74 11 - 135 7DI8013 Surrogate: 2-Fluorobiphenyl 3330 2580 ug/kg wet 77 24 - 121 7D 18013 Surrogate: 2-Fluorophenol 6670 3710 ug/kg wet 56 13 - 108 7D 18013 Surrogate: Nitrohenzene-d5 3330 1630 ug/kg wet 49 19 - l 11 7DI8013 Surrogate: Phenol-d5 6670 4130 ug/kg wet 62 18 - 113 7D 18013 Surrogate: Terphenyl-d]4 3330 2720 ug/kg wet 82 44 - 171 7D18013 MA-EPH Acenaphthene 6.67 4.97 mg/Kg dry 75 40 - 140 17612 Acenaphthylene 6.67 5.02 mg/Kg dry 75 40 - 140 17612 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 38 of47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560 • Fax 4074LW-0885 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA LCS - Cont. Analyte ._- ------------------------------- Known Val. - - --------------------------------- Analyzed Vat Q Units ---- %Rec. ---------- TargetRmW - - -------------------------- Q.C. Batch MA-EPH Anthracene 6.67 6.24 mg/Kg dry 94 40 - 140 17612 Benzo[a]anthracene 6.67 6.75 mg/Kg dry 101 40 -140 17612 Benzo[a]pyrene 6.67 7.23 mg/Kg dry 109 40 - 140 17612 Benzo[b]flumanthene 6.67 6.75 mg/Kg dry 101 40 - 140 17612 Benzo[g,h,i]petylene 6.67 7.29 mg/Kg dry 109 40 -140 17612 Benzo[k]fluotanthene 6.67 7.73 mg/Kg dry 116 40 - 140 17612 Chrysene 6.67 7.04 mg/Kg dry 106 40 - 140 17612 Ihbenz(a,h)anthracene 6.67 7.39 mg/Kg dry 111 40 - 140 17612 Fluoranthene 6.67 6.48 mg/Kg dry 97 40 - 140 17612 Fluorene 6.67 5.48 mg/Kg dry 82 40 - 140 17612 1ndeno[1,2,3-cd]pyrene 6.67 6.96 mg/Kg dry 104 40 -140 17612 2-Methylnaphthalene 6.67 4.60 mg/Kg dry 69 40 - 140 17612 Naphthalene 6.67 3.95 mg/Kg dry 59 40 - 140 17612 Phenanthrene 6.67 5.81 mg/Kg dry 87 40 - 140 17612 Pyrene 6.67 6.73 mg/Kg dry 101 40 - 140 17612 CI I-C22 Aromatics (unadjusted) 113 106 mg/Kg dry 94 40 - I40 17612 C19-C36 Aliphatics 53.3 37.5 mg/Kg dry 70 40 - 140 17612 C9-C18 Aliphatics 40.0 18.5 mg/Kg dry 46 40 - 140 17612 Surrogate: 1-Bromonaphthalene 3,33 3.2 mg/Kg dry 96 40 - 140 17612 Surrogate: 1-Fluorobiphenyl 3.33 3.4 mg/Kg dry 102 40 - 140 17612 Surrogate: o-Terphenyl 6.67 6.0 mg/Kg dry 91 40 - 140 17612 Surrogate: 1-Chlorooctadecone 6.67 4.0 mg/Kg dry 60 40 - 140 17612 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 39 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA LCS Dup RPD Sample Analyte -------------------------------------- Orig. Val. Duplicate Q ------------------------------------------------------------------- Units Spike Conc %Rec. RPD Limn ------------ Q.C. Batch Duplicated MA-EPH Acenaphthene 5.41 mg/Kg dry 6.67 81 8 25 17612 Known Acenaphthylene 5.45 mg/Kg dry 6.67 82 8 25 17612 Known Anthracene 6.88 mg/Kg dry 6.67 103 10 25 17612 Known Benzo[a]anthracene 7.65 mg/Kg dry 6.67 115 12 25 17612 Known Benzo[a]pyrene 8.12 mg/Kg dry 6.67 122 11 25 17612 Known Benzo[b]fluoranthene 7.24 mg/Kg dry 6.67 109 7 25 17612 Known Benzo[g,h,i]perylene 8.28 mg/KS dry 6.67 124 13 25 17612 Known Benzo[k]fluoranthene 8.14 mg/Kg dry 6.67 122 5 25 17612 Known Chrysene 7.90 mg/KS dry 6.67 118 11 25 17612 Known Dibenz(a,h)anthracene 8.11 mg/Kg dry 6.67 122 9 25 17612 Known Fluoranthene 7.17 mg/Kg dry 6.67 108 10 25 17612 Known Fluorene 5.98 mg/Kg dry 6.67 90 9 25 17612 Known Indeno[1,2,3-cd]pyrene 8.04 mg/Kg dry 6.67 121 14 25 17612 Known 2-Methylnaphthalene 5.00 mg/Kg dry 6.67 75 8 25 17612 Known Naphthalene 4.30 mg/Kg dry 6.67 65 9 25 17612 Known Phenanthrene 6.39 mg/Kg dry 6.67 % 9 25 17612 Known Pyrene 7.51 mg/Kg dry 6.67 113 11 25 17612 Known CI I-C22 Aromatics (unadjusted) 119 mg/KS dry 113 105 11 25 17612 Known C19-C36 Aliphatics 43.7 mg/Kg dry 53.3 82 15 25 17612 Known C9-C 18 Aliphatics 21.2 mg/Kg dry 40.0 53 13 25 17612 Known Surrogate: 2-Bromonaphihalene 3.3 mg/Kg dry 3.33 100 17612 Known Surrogate: 2-Fluorobiphenyl 3.5 mg/Kg dry 3.33 106 17612 Known Surrogate: o-TerpheW 6.4 mg/Kg dry 6.67 % 17612 Known Surrogate: l-Chlorooctadecane 4.3 mg/Kg dry 6.67 65 17612 Known TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 40 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-OM Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Matrix Spike Sample Analyte -------------------------------------------------------------------------------------------------------------------- Orig. Val. MS Val Q Units Spike Conc %Rec. Target Range --------------- Batch S �ed -P*..... Volatile Organic Compounds by EPA Method 8260B 1, 1, 1,2-Tetrachloroethane ND 58.9 ug/kg dry 68.5 86 12 - 122 7DIS028 OQD0273-01 1,1,1-Trichloroedme ND 72.1 ug/kg dry 68.5 105 23-128 7DI8028 OQD0273-01 1,1,2,2-Tetrachloroethane ND 61.6 ugAg dry 68.5 90 10-136 7DIS028 OQD0273-01 1,1,2-Trichloroethane ND 75.2 ug/kg dry 68.5 110 10- 145 7D18028 OQD0273-01 IJ-Dichioroethane ND 71.9 ug/kg dry 68.5 105 19- 135 7DIS028 OQD0273-01 I J-Dichloroethene ND 75.7 UsAg dry 68.5 111 10 - 140 7DI8028 OQD0273-01 1,1-Dichloropropene ND 75.2 ug/kg dry 68.5 110 19- 128 7D18028 OQD0273-01 1,2,3-Trichlorobenzene ND 58.2 ug/kg dry 68.5 85 10 - 106 7DI8028 OQD0273-01 1,2,3-Trichloropropane ND 62.5 ug/kg dry 68.5 91 10 - 134 7D18028 OQD0273-01 1,2,4-Trichlorobenzene ND 57.0 ug/kg dry 68.5 83 10 - 100 7D18028 OQD0273-01 1,2,4-Trimethylbenzene ND 56.9 ug/kg dry 68.5 83 10 - 135 7D18028 OQD0273-01 1,2-Dibromo-3-chloropropane ND 59.8 ug/kg dry 68.5 87 10 - 143 71318028 OQD0273-01 1,2-Dibromoethane (EDB) ND 74.9 ug/kg dry 68.5 109 10 - 134 7DI8028 OQD0273-01 1,2-Dichlorobenzene ND 56.7 ug/kg dry 68.5 83 10- 119 7D19028 OQD0273-01 1,2-Mhloroethane ND 73.1 ug/kg dry 68.5 107 10- 140 7DI8028 OQD0273-01 1,2-Dichloropropane ND 73.8 ug/kg dry 68.5 108 13 - 139 7DIS028 OQD0273-01 1,3,5-Trimethylbenzene ND 57.2 ug/kg dry 68.5 84 10 - 105 7DI8028 OQD0273-01 1,3-Dichlorobenzene ND 57.3 ug/kg dry 68.5 84 10 - 103 7DI8028 OQD0273-01 113-Dichloropropene ND 75.7 ug/kg dry 68.5 111 10 - 135 7DI8028 OQD0273-01 1,4-Dichlorobenzene ND 57.9 ug/kg dry 68.5 85 to - 119 7DI9028 OQD0273-01 212-Dichloropropane ND 73.2 ug/kg dry 68.5 107 10 - 155 7D18028 OQD0273-01 2-Butanone ND 56.9 ug/kg dry 68.5 83 11 - 140 7D18028 OQD0273-01 2-Chloroethylvinyl ether ND ND M2 ug/kg dry 68.5 5 - 100 7DIS028 OQD0273-01 2-Chlorotoluene ND 57.9 ug/kg dry 68.5 85 10 - 106 7DI8028 OQD0273-01 2-Hexanone ND 74.9 ug/kg dry 68.5 109 10 - 166 7DI8028 OQD0273-01 2-Nitropropane ND 75.2 ug/kg dry 68.5 110 23 - 132 71)18028 OQD0273-01 4-Chlorotoluene ND 59.8 ug/kg dry 68.5 87 10 - 117 71)18028 OQD0273-01 4-Methyl-2-pentanone ND 86.6 ug/kg dry 68.5 126 10 - 141 71) 18028 OQM273-01 Acetone ND 44.4 ug/kg dry 68.5 65 10 - 162 7D18028 OQD0273-01 Benzene ND 71.0 ug/kg dry 68.5 104 I8 - 126 7D18028 OQD0273-01 Bromobenzene ND 58.0 ug/kg dry 68.5 85 10 - 107 7DI8028 OQD0273-01 Bromochloromethane ND 70.1 ughgdry 68.5 102 10-135 7DIS028 OQD0273-01 Bromodichloromethane ND 74.7 ug/kg dry 68.5 109 10 - 137 71318028 OQD0273-01 Bromoform ND 59.0 ug/kg dry 68.5 86 10 - 118 7DI8029 OQD0273-01 Bromomethane ND 72.5 ug/kg dry 68.5 106 10 - 152 7DI8028 OQD0273-01 Carbon disulfide ND 66.0 ug/kg dry 68.5 % 10 - 111 7DIS028 OQD0273-01 Carbon Tetrachloride ND 71.3 ug/kg dry 68.5 104 22 - 121 7DI8028 OQD0273-01 Chlorobenzene ND 59.6 ug/kg dry 68.5 87 10 - 123 7D18028 OQD0273-01 Chlorodibromomethane ND 70.9 ug/kg dry 68.5 104 10 - 123 7DI8028 OQD0273-01 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 41 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Matrix Spike - Cont. Sample Analyte --------------------------------------.....-------------------------------------- Orig. Val. MS Val Q Units Spike Conc % Rec. -------------------------- Target Range Batch - S iked p Volatile Organic Compounds by EPA Method 8260B Chloroethane ND 37.6 ugAg dry 68.5 55 10 - 149 7DI8028 OQD0273-01 Chloroform ND 69.7 ug/kg dry 68.5 102 19- 132 7DIS028 OQD0273-01 Chloromedwe ND 72.1 ug/kg dry 68.5 105 20- 126 7DIS028 OQD0273-01 cis-1,2-Dichloroethene ND 72.8 ug/kgdry 68.5 106 10-136 7DI8028 OQD0273-01 cis-1,3-Dichloropropene ND 73.8 usAg dry 68.5 108 10-125 7DI8028 OQD0273-01 Dibromomethane ND 72.7 ug/kg dry 68.5 106 10 - 136 7D18028 OQD0273-01 Dichlorodifluoromethane ND 80.7 ugAg dry 68.5 118 41 - 171 7DIS028 OQD0273-01 Ethylbenzene ND 59.7 ug/kg dry 69.5 87 12 - 120 7D18028 OQD0273-01 Hexachlorobutadiene ND 48.3 ugAg dry 68.5 71 10 - 100 7DI9028 OQD0273-01 Isopropylbenzene ND 58.0 ug/kg dry 68.5 85 10 - 124 7D18028 OQD0273-01 Methyl tert-Butyl Ether ND 69.0 ug/kg dry 69.5 101 10 - 139 7D18028 OQD0273-01 Methylene Chloride ND 71.6 ug/kg dry 68.5 105 19 - 134 7D18028 OQD0273-01 Naphthalene ND 61.6 ug/kg dry 68.5 90 10 - 125 7D18029 OQD0273-01 n-Butylbenzene ND 56.4 ug/kg dry 68.5 82 10 - 138 7D18028 OQD0273-01 n-Propylbenzene ND 59.9 ug/kg dry 68.5 87 10 - 118 7DI8028 OQD0273-01 p-Isopropyltoluene ND 54.9 ug/kg dry 68.5 80 10 - 121 7D18028 OQD0273-01 sec-Burylbenzene ND 54.8 ug/kg dry 68.5 80 10 - 116 7DIS028 OQD0273-01 Styrene NO 56.5 ug/kg dry 68.5 82 10 - 115 7DI8028 OQD0273-01 tert-Butylbenzene ND 55.5 ug/kg dry 68.5 81 10 - 100 7DI8028 OQD0273-01 Tetrachloroethene ND 70.0 ugAg dry 68.5 102 10-144 7DIS028 OQD0273-01 Toluene ND 69.9 ug/kg dry 68.5 102 10 - 130 7D18028 OQD0273-01 trans-1,2-Dichloroethene ND 71.3 ug/kg dry 68.5 104 11 - 126 7DI9028 OQD0273-01 trans-1,3-Dichloropropene ND 69.6 ug/kg dry 68.5 102 12 - 110 7D18028 OQD0273-01 Trichloroethene ND 73.7 ug/kg dry 68.5 108 16 - 164 7DI8028 OQD0273-01 Trichlorofluoromethane ND 74.7 ugAg dry 68.5 109 31 - 145 7DIS028 OQD0273-01 Vinyl chloride ND 66.7 ug/kg dry 68.5 97 39 - 145 7D18028 OQD0273-01 Xylenes, total ND 178 ug/kg dry 205 87 10 - 126 7DI8028 OQD0273-01 Surrogate: 1,2-Dichloroethane-d4 56.4 ugAg dry 50.0 113 73 - 137 7D18028 OQD0273-01 Surrogate: 4-Bromo/luorobenzene 50.6 ug/kg dry 50.0 101 59 - 118 7DI8028 OQD0273-01 Surrogate: Dibromo/luoromethane 54.1 ugAg dry 50.0 108 55 - 145 7D18028 OQD0273-01 Surrogate: Toluene-d8 53.8 ug/kg dry 50.0 108 80 - 117 7D18028 OQD0273-01 Semivolatile Organic Compounds by EPA Method 8270C N-Nitrosodiphenylamine ND 2680 ug/kg dry 4410 61 10 - 151 7D18013 OQD0273-01 1,2-Dichlorobenzene ND 2690 ug/kg dry 4410 61 29 - 116 7DI8013 OQD0273-01 1,3-Dichlorobenzene ND 2470 ug/kg dry 4410 56 26-108 7DIS013 OQD0273-01 1,4-Dichlorobenzene ND 2460 ug/kg dry 4410 56 27-109 7DIS013 OQD0273-01 1,4-Dinitrobenzene ND 3970 ug/kg dry 4410 90 56 - 120 7DI8013 OQD0273-01 I-Methylnaphthalene ND 2170 ug/kg dry 4410 49 11 - 112 7DI8013 OQD0273-01 2,4,5-Trichlorophenol ND 3560 ug/kg dry 4410 81 48 - 113 7DI8013 OQD0273-01 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 42 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Matrix Spike - Cont. Sample Anal to y Orig. Val. g. MS Val Q Units Spike - - - - % Rec. Target Range Batch Spiked Semivolatile Organic Compounds by EPA Method 8270C 2,4,6-Trichlorophenol ND 3550 ug/kg dry 4410 80 35 - 130 7D18013 OQD0273-01 2,4-Dichlorophenol ND 2520 ug/kg dry 4410 57 16 - 110 7D18013 OQD0273-01 2,4-Dimethylphenol ND 1650 ug/kg dry 4410 37 20 - 109 7DIS013 OQD0273-01 2,4-Dinitrophenol ND 3090 ug/kg dry 4410 70 10 - 178 7D18013 OQD0273-01 2,4-Dinitrotoluene ND 3110 ug/kg dry 4410 71 49 - 134 7D18013 OQD0273-01 2,6-Dinitrotoluene ND 3270 ug/kg dry 4410 74 55 - 114 7DIS013 OQD0273-01 2-Chloronaphthalene ND 3370 ug/kg dry 4410 76 38- 121 7DIS013 OQD0273-01 2-Chlorophenol ND 2700 ug/kg dry 4410 61 28 - 116 7DI8013 OQD0273-01 2-Methy1naphthalene ND 2350 ug/kg dry 4410 53 11 - 122 7DIS013 OQD0273-01 2-Methylphenol ND 2760 ug/kg dry 4410 63 30 - 122 7DI8013 OQD0273-01 2-Nitroaniline ND 3400 ug/kg dry 4410 77 51 - 121 7D18013 OQD0273-01 2-Nitrophenol ND 2490 ug/kg dry 4410 56 12 - 115 7DIS013 OQD0273-01 3,3'-Dichlorobenzidine ND 1620 ug/kg dry 4410 37 10 - 163 7DI8013 OQD0273-01 3-Nitroaniline ND 2960 ug/kg dry 4410 67 38 - 116 7DI8013 OQD0273-01 4,6-Dinitro-2-methylphenol ND 4660 ug/kg dry 4410 106 28 - 156 7DI8013 OQD0273-01 4-Bromophenyl phenyl ether ND 3070 ug/kg dry 4410 70 30 - 130 7D18013 OQD0273-01 4-Chloro-3-methylphenol ND 2340 uSAg dry 4410 53 30 - 117 7D18013 OQD0273-01 4-Chloroaniline ND 1950 ug/kg dry 4410 44 10 - 88 7DI9013 OQD0273-01 4-Chlorophenyl phenyl ether ND 2840 ug/kg dry 4410 64 45 - 122 7DI8013 OQD0273-01 4-Nitroaniline ND 2760 ugAg dry 4410 63 34-137 7DIS013 OQD0273-01 4-Nitrophenol ND 3070 ug/kg dry 4410 70 10 - 168 7D18013 OQD0273-01 Acenaphthene ND 3170 ug/kg dry 4410 72 40 - 125 7D 18013 OQD0273-01 Acenaphthylene ND 3160 ug/kg dry 4410 72 44 - 125 7D18013 OQD0273-01 Aniline ND 1820 ug/kg dry 4410 41 10 - 167 7DI8013 OQD0273-01 Anthracene ND 3210 ugAg dry 4410 73 53 - 121 7DI8013 OQD0273-01 1,2-Dinitrobenzene NO 3380 ug/kg dry 4410 77 38 - 147 7DI8013 OQD0273-01 Benzidine NO ND L2 ug/kg dry 4410 5 - 145 7D18013 OQD0273-01 Benzo (a) anthracene ND 3060 ug/kg dry 4410 69 46 - 135 7D18013 OQD0273-01 1,3-Dinitrobenzene ND 3530 ug/kg dry 4410 80 52 - 122 7DI8013 OQD0273-01 Benzo (a) pyrene ND 3420 ug/kg dry 4410 78 51 - 115 7D18013 OQD0273-01 Benzo (b) fluoranthene ND 3580 ug/kg dry 4410 81 44 - 136 7D18013 OQD0273-01 Benzo (g h i) perylene ND 2080 ug/kg dry 4410 47 34 - 123 7DI8013 OQD0273-01 Benzo (k) fluoranthene ND 3690 ug/kg dry 4410 84 43 - 131 7DI8013 OQD0273-01 Benzyl alcohol ND 2830 ug/kg dry 4410 64 31 - 124 7D18013 OQD0273-01 Bis(2-chloroethoxy)methane ND 2340 ug/kg dry 4410 53 16 - 109 7DI8013 OQD0273-01 Bis(2-chloroethyl)ether ND 2310 ug/kg dry 4410 52 19 - 118 7DI8013 OQD0273-01 Bis(2-chloroisopropyl)ether ND 2570 ug/kg dry 4410 58 28 - 120 7DI8013 OQD0273-01 Bis(2-ethylhexyl)phthalate ND 2820 ug/kg dry 4410 64 34 - 165 7D18013 OQD0273-01 Butyl benzyl phthalate ND 3010 ug/kg dry 4410 68 39 - 154 7D 180 13 OQD0273-01 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 43 of 47 4310 East Anderson Road Orlando, FL 32812.800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Matrix Spike - Cont. Sample Anal to y Orig. Val. g. MS Val Q Units Spike Conc % Rec. Target Range Batch Spiked - . - Semivolatile Organic Compounds by EPA Method 8270C Carbazole ND 2760 ug/kg dry 4410 63 32 - 133 7DIS013 OQD0273-01 Chrysene NO 3070 ug/kg dry 4410 70 48 - 126 7DIS013 OQD0273-01 Dibenz (a h) anthracene NO 2280 ug/kg dry 4410 52 38 - 119 7DI8013 OQD0273-01 Dibenzofit an ND 3110 ug/kg dry 4410 71 46 - 130 7DIS013 OQD0273-01 Diethyl phthalate ND 2860 ug/kg dry 4410 65 48 - 138 7D18013 OQD0273-01 Dimethyl phthalate ND 3270 ug/kg dry 4410 74 53 - 118 7DI8013 OQD0273-01 Di-n-butyl phthalate ND 2810 ug/kg dry 4410 64 53 - 122 7DIS013 OQD0273-01 Di-n-octyl phthalate ND 2670 ug/kg dry 4410 61 38 - 141 7DI8013 OQD0273-01 Diphenylamine ND 2680 ug/kg dry 4410 61 10 - 159 7DIS013 OQD0273-01 Fluoranthene ND 2990 ug/kg dry 4410 68 33 - 138 7DI8013 OQD0273-01 12-Diphenylhydrazine ND 3220 ug/kg dry 4410 73 19 - 156 7D 18013 OQD0273-01 Fluorene ND 2%0 ugAg dry 4410 67 48 - 128 7D 18013 OQD0273-01 Hexachlorobenzene NO 3520 ug/kg dry 4410 80 59 - 122 7D18013 OQD0273-01 Hexachlorobutadiene ND 2520 ug/kg dry 4410 57 I5 - 117 7D18013 OQD0273-01 Hexachlorocyclopentadiene ND 1800 ug/kg dry 4410 41 10 - 125 7DI9013 OQD0273-01 Hexachloroethane ND 2370 ug/kg dry 4410 54 21 - 111 7D18013 OQD0273-01 Indeno (1,2,3-ed) pyrene NO 2290 ug/kg dry 4410 52 37 - 117 7DI8013 OQD0273-01 lsophorone ND 895 ug/kg dry 4410 20 17 - 100 7DI8013 OQD0273-01 Naphthalene ND 2320 ug/kg dry 4410 53 15 - 116 7DI8013 OQD0273-01 Nitrobenzene ND 2240 ug/kg dry 4410 51 I5 - 102 7D18013 OQD0273-01 N-Nitrosodimethylamine ND 2200 ug/kg dry 4410 50 22 - 100 7D18013 OQD0273-01 N-Nitrosodi-n-propylamine ND 2710 ug/kg dry 4410 61 12 - 140 7D18013 OQD0273-01 Pentachlorophenol ND 3570 ug/kg dry 4410 81 30 - 176 7DI8013 OQD0273-01 Phenanthrene ND 3210 ug/kg dry 4410 73 52- 123 7D18013 OQD0273-01 Phenol ND 2800 ug/kg dry 4410 63 32 - 121 7DI8013 OQD0273-01 Pyrene ND 2560 ug/kg dry 4410 58 31 - 155 7D18013 OQD0273-01 Pyridine ND 1250 ug/kg dry 4410 28 10 - 102 7DI8013 OQD0273-01 1,2,4-Trichlorobenzene ND 2270 ug/kg dry 4410 51 13 - 105 7DIS013 OQD0273-01 Surrogate: 2,4,6-Tribromophenol 5660 ug/kg dry 8820 64 11 - 135 7D18013 OQD0273-01 Surrogate: 2-Fluorohiphenyl 3100 ug/kg dry 4410 70 24 - 121 7DI8013 OQD0273-01 Surrogate: 2-Fluorophenol 4610 ug/kg dry 8820 52 13 - 108 7D18013 OQD0273-01 Surrogate: Nitrobenzene-d5 2100 ug/kg dry 4410 48 19-111 7DIS013 OQD0273-01 Surrogate: Phenol-d5 5210 ug/kg dry 8820 59 18 - 113 7DI8013 OQD0273-01 Surrogate: Terphenyl-dl4 3260 ug/kg dry 4410 74 44 - 171 7DIS013 OQD0273-01 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 44 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-0886 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Matrix Spike Dup RPD Sample Analyte --------------------------------------------------- Orig. Val. Duplicate Q --------- Units ----------------------------------- Spike Conc %Rec. RPD Limit Q.C. Batch DuP lica<ed Semivolatile Organic Compounds by EPA Method 8270C N-Nitrosodiphenylamine ND 2230 ug/kg dry 4410 51 18 80 7DIS013 OQD0273-01 1,2-Dichlombenzene ND 2110 ug/kg dry 4410 48 24 58 7D18013 OQD0273-01 1,3-Dichlorobenzene ND 1940 ug/kg dry 4410 44 24 57 7DI8013 OQD0273-01 1,4-Dichlorobenzene ND 1930 ug/kg dry 4410 44 24 57 7DI8013 OQD0273-01 1,4-Dinitrobenzene ND 3290 ug/kg dry 4410 75 19 50 7DI9013 OQD0273-01 1-Methylnaphthalene ND 1780 ug/kg dry 4410 40 20 60 7DI8013 OQD0273-01 2,4,5-Trichlorophenol ND 2860 ug/kg dry 4410 65 22 80 7DIS013 OQD0273-01 2,4,6-Trichlorophenol ND 2780 ug/kg dry 4410 63 24 60 7DI8013 OQD0273-01 2,4-Dichlorophenol ND 2060 ug/kg dry 4410 47 20 82 7DI8013 OQD0273-01 2,4-Dimethylphenol ND 1180 ug/kg dry 4410 27 33 38 7DIS013 OQD0273-01 2,4-Dinitrophenol ND 2530 ug/kg dry 4410 57 20 91 7DI8013 OQD0273-01 2,4-Dinitrotoluene ND 2610 ug/kg dry 4410 59 17 79 7D18013 OQD0273-01 2,6-Dinitrotoluene ND 2690 ug/kg dry 4410 61 19 47 7DI8013 OQD0273-01 2-Chloronaphthalene ND 2690 ug/kg dry 4410 61 22 70 7DIS013 OQD0273-01 2-Chlorophenol ND 2100 ug/kg dry 4410 48 25 97 7D18013 OQD0273-01 2-Methy1naphthalene ND 1930 ug/kg dry 4410 44 20 71 7DI8013 OQD0273-01 2-Methylphenol ND 2130 ug/kg dry 4410 48 26 50 7DI9013 OQD0273-01 2-Nitroaniline ND 2770 ug/kg dry 4410 63 20 48 7DI9013 OQD0273-01 2-Nitrophenol ND 2050 ug/kg dry 4410 46 19 71 7DIS013 OQD0273-01 3,3'-Dichloroben2idine ND 1130 tTAg dry 4410 26 36 54 7D18013 OQD0273-0t 3-Nitroaniline ND 2420 ug/kg dry 4410 55 20 79 7D18013 OQD0273-01 4,6-Dinitro-2-methylphenol ND 3%0 ugAg dry 4410 90 16 60 7DIS013 OQD0273-01 4-Bromophenyl phenyl ether ND 2550 ug/kg dry 4410 58 19 50 7DI8013 OQD0273-01 4-Chloro-3-methylphenol ND 1900 ug/kg dry 4410 43 21 56 7DI8013 OQD0273-01 4-Chloroaniline ND 1590 ug/kg dry 4410 36 20 % 7DIS013 OQD0273-01 4-Chlorophenyl phenyl ether ND 2300 ug/kg dry 4410 52 21 55 7DI9013 OQD0273-01 4-Nitroaniline ND 2240 ug/kg dry 4410 51 21 105 7D18013 OQD0273-01 4-Nitrophenol ND 2530 ug/kg dry 4410 57 19 50 7D18013 OQD0273-01 Acenaphthene ND 2540 ug/kg dry 4410 58 22 60 7DI8013 OQD0273-01 Acenaphthylene ND 2540 ug/kg dry 4410 58 22 51 7D18013 OQD0273-01 Aniline ND 1380 ug/kg dry 4410 31 28 50 7DI8013 OQD0273-01 Anthracene ND 2760 ug/kg dry 4410 63 15 60 7DI8013 OQD0273-01 1,2-Dinitrobenzene ND 2790 ug/kg dry 4410 63 19 50 7DI8013 OQD0273-01 Benzidine ND ND L2 ug/kg dry 4410 50 7DI8013 OQD0273-01 Benzo (a) anthracene ND 2660 ug/kg dry 4410 60 14 46 7DI8013 OQD0273-01 1,3-Dinitrobenzene ND 2930 ug/kg dry 4410 66 19 60 7D18013 OQD0273-01 Benzo (a) pyrene ND 2850 ug/kg dry 4410 65 18 48 7D18013 OQD0273-01 Benzo (b) fluoranthene ND 3110 ug/kg dry 4410 71 14 60 7D18013 OQD0273-01 Benzo (g,h,i) perylene ND 1750 ug/kg dry 4410 40 17 38 7D18013 OQD0273-01 Benzo (k) fluoranthene ND 3010 ug/kg dry 4410 68 20 60 7D18013 OQD0273-01 Benzyl alcohol ND 2210 ug/kg dry 4410 50 25 48 7DI8013 OQD0273-01 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 45 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-2560' Fax 407-856-08M Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY PROJECT QUALITY CONTROL DATA Matrix Spike Dup - Cont. RPD Sample Analyte -------------------- — ..---------------- Orig. Val. '-----------'-------------------------- Duplicate Q Units Spike Conc ------------------------- %Rec. RPD Lima Q.C. Batch licated Semivolatile Organic Compounds by EPA Method 8270C Bis(2-chloroethoxy)nethane ND 1920 ug/kg dry 4410 44 20 97 7D18013 OQD0273-01 Bis(2-cWoroethyl)ether ND 1800 ug/kg dry 4410 41 25 50 7DI8013 OQD0273-01 Bis(2-chloroisopropyl)ether ND 1980 ug/kg dry 4410 45 26 50 7DI8013 OQD0273-01 Bis(2-ethylhexyl)phthalate ND 2480 ug/kg dry 4410 56 13 49 7DIS013 OQD0273-01 Butyl benzyl phthalate ND 2640 ug/kg dry 4410 60 13 50 7DI8013 OQD0273-01 Carbazole ND 2420 ug/kg dry 4410 55 13 50 7DI8013 OQD0273-01 Chrysene ND 2670 ug/kg dry 4410 61 14 36 7D18013 OQD0273-01 Dibenz (a h) anthracene ND 1970 ug/kg dry 4410 45 15 60 7D I S013 OQD0273-01 Dibenzofuran ND 2500 ug/kg dry 4410 57 22 47 7D18013 OQD0273-01 Diethyl phthalate NO 2410 ug/kg dry 4410 55 17 45 7DI8013 OQD0273-01 Dimethyl phthalate NO 2690 ug/kg dry 4410 61 19 49 7DI8013 OQD0273-01 Di-n-butyl phthalate ND 2510 ug/kg dry 4410 57 11 48 7DI8013 OQD0273-01 Di-n-octyl phthalate ND 2310 ug/kg dry 4410 52 14 81 7DI8013 OQD0273-0I Diphenylamine ND 2230 ug/kg dry 4410 51 18 80 7DI8013 OQD0273-01 Fluotanthene ND 2710 ug/kg dry 4410 61 10 63 7D18013 OQD0273-01 1,2-Diphenylhydrazine ND 2660 ug/kg dry 4410 60 19 53 7D18013 OQD0273-01 Fluorene NO 2410 ug/kg dry 4410 55 20 49 7DI8013 OQD0273-01 Hexachlorobenzene ND 2950 ug/kg dry 4410 67 17 49 7DI8013 OQD0273-01 Hexachlorobutadiene ND 2050 ug/kgdry 4410 46 21 50 7D18013 OQD0273-01 Hexachlorocyclopentadiene ND 1380 ug/kg dry 4410 31 26 50 7D18013 OQD0273-01 Hexachloroethane ND 1820 ug/kg dry 4410 41 26 87 7DI8013 OQD0273-01 Indeno (1,2,3-cd) pyrene ND 1970 upAg dry 4410 45 15 60 7D18013 OQD0273-01 Isophonme ND 743 ug/kg dry 4410 17 19 75 7D18013 OQD0273-01 Naphthalene ND 1910 ug/kg dry 4410 43 19 81 7D18013 OQD0273-01 Nitrobenzene ND 1830 ug/kg dry 4410 41 20 too 7DI8013 OQD0273-01 N-Nitrosodimethylamine ND 1750 ug/kg dry 4410 40 23 93 7D18013 OQD0273-01 N-Nitrosodi-n-propylamine ND 2120 ug/kg dry 4410 48 24 44 7D18013 OQD0273-01 Pentachlorophenol ND 3040 ug/kg dry 4410 69 16 92 7DI8013 OQD0273-01 Phenanthrene ND 2750 ug/kg dry 4410 62 15 60 7DI8013 OQD0273-01 Phenol ND 2210 ug/kg dry 4410 50 24 73 7DI9013 OQD0273-01 Pyrene ND 2340 ug/kg dry 4410 53 9 90 7DI8013 OQD0273-01 Pyridine ND 1230 ug/kg dry 4410 28 2 97 7D18013 OQD0273-01 1,2,4-Trichlorobenzene ND 1880 ug/kg dry 4410 43 19 97 7DI9013 OQD0273-01 Surrogate:2,a,6-Trihromophenol 4640 ug/kg dry 8820 53 7DI8013 OQD0273-01 Surrogate: 2-Fluorobiphenyl 2510 ug/kg dry 4410 57 7DI8013 OQD0273-01 Surrogate: 2-Fluorophenol 3610 ug/kg dry 8820 41 7D18013 OQD0273-01 Surrogate: Nitrobenzene-0 1740 ug/kg dry 4410 39 7D18013 OQD0273-01 Surrogate: Phenol-d5 4090 ug/kg dry 8820 46 7D18013 OQD0273-01 Surrogate: Terphenyl-dla 2800 ug/kg dry 4410 63 7DI8013 OQD0273-01 TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 46 of 47 4310 East Anderson Road Orlando, FL 32812' 800-851-25W * Fax 4074858.0885 Client: ENVIROASSESSMENTS Work Order: OQD0273 Sampled: 04/17/07 9307 MONROE RD., SUITE K Project: N. TRYON ST. PROPERTY Received: 04/18/07 CHARLOTTE, NC 28270 Project Number: 07-6797.1 Attn: AMANDA PETOSKEY CERTIFICATION SUMMARY TestAmerica - Orlando, FL Method Matrix Nelac North Carolina -- -------- --------------------------------------------------------------------------------- EPA 160.3 -------------------------------------------------- Solid/Soil EPA 8260B Solid/Soil X X EPA 8270c Solid/Soil X X Subcontracted Laboratories STL - Westfield, MA North Carolina Cert #647 53 SOUTHAMPTON RD - WESTFIELD, MA 01085 Analysis Performed: MADEP-EPH Samples: OQD0273-01, OQD0273-02, OQD0273-03, OQD0273-04, OQD0273-05 Analysis Performed: MADEP-VPH Samples: OQD0273-01, OQD0273-02, OQD0273-03, OQD0273-04, OQD0273-05 STL Westfield Method Performed: MA-EPH Samples: OQD0273-01, OQD0273-02, OQD0273-03, OQD0273-04, OQD0273-05 Method Performed: MAVPH Samples: OQD0273-01, OQD0273-02, OQD0273-03, OQD0273-04, OQD0273-05 DATA QUALIFIERS AND DEFINITIONS Ll Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above acceptance limits. L2 Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was below acceptance limits. M2 The MS and/or MSD were below the acceptance limits due to sample matrix interference. See Blank Spike (LCS). R3 The RPD exceeded the acceptance limit due to sample matrix effects. ADDITIONAL COMMENTS When insufficient sample volume is received for Matrix Spike and Matrix Spike Duplicate, Laboratory Control Spike and Laboratory Control Spike Duplicate data is used for batch QC. Results are reported on a wet weight basis unless otherwise noted. TestAmerica - Orlando, FL Enid Ortiz For Holli Raffington Project Manager Page 47 of 47 • tes rnerica AwyriCAL Tesmo CORPORATION 4310 East Anderson Road • Orlando. FL 32812' 407-861-2WO • Fax 407468 OM * 800.881- Client: ENVIROASSESSMENTS Shipped By: Fed Ex Cooler Received On: 04/18/07 09:20 Received By: Stephanie Bull Project: 0 D0273 Tracking Number: 859399223221 nn And Opened On (Date/time): ($ �q Logged in by: Stephanie Bull Were custody seals on the outside of cooler? YES ,1 NO If Yes # Location Were custody seals intact? YES %i _ NO NIA (no seals present) Chain of Custody Complete? YES ,1 NO Discreoancv Comments: s-1 far ))as 6le LF 41310� d. ac) al\ Co ,Mrs rave 64e 6� 1r3,wk b a(x voq kvq- wvvb ae t l;Do , OM von- t� �arnQ v 00's hare. of 14: o u L j� Lr p� 1 t'3., l� Cooler Temparture When Opened: 3.00 Degrees Celsius Temparture Blank Included: YES NO J Packing Material: Bubblewrap NONE Other: Received on Ice: YES J_ NO Other: Total # Of Containers:' # Vials Any Bottles Broken? YES NO 31_ If Yes Which One(s)? Any Missing Samples? YES NO J If Yes Which One(s)? PH Levels: H2SO4 <=2? HNO3 <=2? HCL <=2? NaOH >>=10? , 2 # Of Containers Unpreserved between 6 and 8? SG��v m 1 8:5�•���� � �- me.0 Any Air Bubbles in VOA Vials? YES NO N/A�(_ (no VOA vials received) Was there enough sample shipped in each container? YES J NO Correct Preservatives Used? YES J NO If No, see comments: Project Manager. Holli Raffington Actions Taken q I G7 z MMME F&I 0 C U N — D ,C- L/4 tier ( Spocffy) ', ;o m IZ �L ID IH Ca SUBCONTRACT ORDER TestAmerica - Orlando, FL OQD0273 SENDING LABORATORY: RECEIVING LABORATORY: TestAmerica - Orlando, FL STL - Westfield, MA 4310 East Anderson Road 53 SOUTHAMPTON RD Orlando, FL 32812 WESTFIELD, MA 01085 Phone: 800-851-2560 Phone :(413) 572-4000 Fax: 407-856-0886 Fax: (413) 572-3707 Project Manager: Holli Raffington Project Location: North Carolina Client: ENVIROASSESSMENTS Receipt Temperature: °C Ice: Y / N Analysis Due Expires Interlab Surch Comments C�iew� Sample ID: 00D0273-01 Solid/Soil Sampled: 0411710712:00 RUSH MADEP-EPH 04/23/0716:00 05/01/0712:00 $107.00 25% MADEP-VPH 04/23/0716:00 05/01/0712:00 $52.00 25% Containers Supplied: 4kI IA� Sample ID: 00D0273-02 Solid/Soil Sampled: 0411710713:00 RUSH MADEP-EPH 04/23/0716:00 05/01/0713:00 $107.00 25% STL-Wakefield MADEP-VPH 04/23/0716:00 05/01/0713:00 $52.00 25% STL-Wakefield Containers Supplied: Sample ID: OQD0273-03 Solid/Soil Sampled: 0411710713:05 RUSH MADEP-EPH 04/23/0716:00 05/01/0713:05 $107.00 25% STL-Wakefield MADEP-VPH 04/23/0716:00 05/01/0713:05 $52.00 25% STL-Wakefield Containers Supplied: S-3 Sample ID: 00D0273-04 Solid/Soil Sarnpled: 04/17,0713.10 RUSH MADEP-EPH 04/23/0716:00 06101/0713:10 $107.00 25% STL-Wakefield MADEP-VPH 04/23/0716:00 05/01/0713:10 $52.00 25% STL-Wakefield Containers Supplied: Sample ID: 00D0273-05 Solid/Soil Sampled: 04117/07 13.15 RUSH S — 4 MADEP-EPH 04/2310716:00 05/01/0713:15 $107.00 25% STL-Wakefield MADEP-VPH 04/23/0716:00 05/0110713:15 $52.00 25% STL-Wakefield Containers Supplied: Released By Daterfime Received By Date/Time Released By Date/Time Received By Date/Time Page 1 of 1 ANALYTICAL REPORT Job Number: 360-9440-1 Job Description: OQD0273 For: TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Attention: Ms. Holli Raffington Z�6� a - naz;'�')- - Joe Chimi Report Production Representative jchimi@stl-inc.com 04/24/2007 Project Manager: Beata Fleury STL The test results in this report meet all NELAC requirements for accredited parameters. Any exceptions to NELAC requirements are noted in this report. Pursuant to NELAC, this report may not be reproduced except in full, and with written approval from the laboratory. STL Westfield Certifications and Approvals: MADEP MA014, RIDOH57, CTDPH 0494, VT DECWSD, NH DES 253903-A, NELAP FL E87912 TOX, NELAP NJ MA008 TOX, NELAP NY 10843, NY DOH 10843. Severn Trent Laboratories, Inc. �����.'-""'� STL Westfield Westfield Executive Park 53 Southampton Road, r Westfield, MA 01085 Tel (413) 572-4000 Fax (413) 572-3707 www.stl-inc.com page 1 of 25 METHOD SUMMARY Client: TestAmerica Analytical Testing Corp Job Number: 360-9440-1 Description Lab Location Method Preparation Method Matrix: Solid MADEP - Volatile Petroleum Hydrocarbons Closed System Purge & Trap/Field Preservation MADEP - Extractable Petroleum Hydrocarbons Microwave Extraction Percent Moisture LAB REFERENCES: STL WFD = STL Westfield METHOD REFERENCES: EPA - US Environmental Protection Agency STL WFD MA DEP MAVPH STL WFD SW846 5035 STL WFD MA DEP MA-EPH STL WFD SW846 3546 STL WFD EPA PercentMolsture MA DEP - Massachusetts Department Of Environmental Protection STL Westfield Page 2 of 25 METHOD / ANALYST SUMMARY Client: TestAmerica Analytical Testing Corp Job Number: 360-9440-1 Method Analyst Anal st ID MA DEP MAVPH Doane, Jessica L JLD MA DEP MA-EPH Pham, Tam TP EPA PercentMoisture Rachtan, Karolina KR STL Westfield Page 3 of 25 SAMPLE SUMMARY Client: TestAmerica Analytical Testing Corp Job Number: 360-9440-1 Lab Sample ID Client Sample ID Client Matrix Date/Time Sampled Date/Time Received 360-9440-1 00DO273-01 Solid 04/17/2007 1200 04/18/2007 0945 360-9440-2 00DO273-02 Solid 04/17/2007 1300 04/18/2007 0945 360-9440-3 OQD0273-03 Solid 04/17/2007 1305 04/18/2007 0945 360-9440-4 OQD0273-04 Solid 04/17/2007 1310 04/18/2007 0945 360-9440-5 00D0273-05 Solid 04/17/2007 1315 04/18/2007 0945 STL Westfield Page 4 of 25 STL Westfield IPLE RESULTS Page 5 of 25 Ms. Holli Raffington TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Client Sample ID: 00D0273-01 Lab Sample ID: 360-9440-1 Analyte Method: MAVPH Prep Method: 6036 ResultlQualifier Date Analyzed: Date Prepared: Job Number: 360-9440-1 Date Sampled: 04/17/2007 1200 Date Received: 04/18/2007 0945 Client Matrix: Solid Percent Solids: 74 Unit RL Dilution 04/23/2007 1838 04/18/2007 1300 Benzene ND mg/Kg 0.71 1.0 Ethylbenzene ND mg/Kg 0.71 1.0 m-Xylene & p-Xylene ND mg/Kg 1.4 1.0 Methyl tert-butyl ether ND mg/Kg 0.14 1.0 Naphthalene ND mg/Kg 1.4 1.0 o-Xylene ND mg/Kg 0.71 1.0 Toluene ND mg/Kg 0.71 1.0 C5-C8 Aliphatics (unadjusted) ND mg/Kg 7.1 1.0 C9-C12 Aliphatics (unadjusted) ND mg/Kg 7.1 1.0 C5-C8 Aliphatics (adjusted) ND mg/Kg 7.1 1.0 C9-C12 Aliphatics (adjusted) ND mg/Kg 7.1 1.0 C9-C10 Aromatics ND mg/Kg 7.1 1.0 Total VPH ND mg/Kg 7.1 1.0 Surrogate .... .. Acceptance Limits ................. 2,5-Dibromotoluene (fid)....... 103o 70 - 130 2,5-Dibromotoluene (pid) 102 % 70 - 130 Method: MA-EPH Date Analyzed: 04/18/2007 1751 Prep Method: 3546 Date Prepared: 04/18/2007 1252 Acenaphthene ND mg/Kg 0.44 1.0 Acenaphthylene ND mg/Kg 0.44 1.0 Anthracene ND mg/Kg 0.44 1.0 Benzo[a]anthracene ND mg/Kg 0.44 1.0 Benzo[a]pyrene ND mg/Kg 0.44 1.0 Benzo(b]fluoranthens ND mg/Kg 0.44 1.0 Benzo[g,h,i]perylene ND mg/Kg 0.44 1.0 Benzo(k]fluoranthene ND mg/Kg 0.44 1.0 Chrysene ND mg/Kg 0.44 1.0 Dibenz(a,h)anthracene ND mg/Kg 0.44 1.0 Fluoranthene ND mg/Kg 0.44 1.0 Fluorene ND mg/Kg 0.44 1.0 Indeno[1,2,3-cd]pyrene ND mg/Kg 0.44 1.0 2-Methyl naphthalene ND mg/Kg 0.44 1.0 Naphthalene ND mg/Kg 0.44 1.0 Phenanthrene ND mg/Kg 0.44 1.0 Pyrene ND mg/Kg 0.44 1.0 C11-C22 Aromatics (unadjusted) ND mg/Kg 4.4 1.0 C11-C22 Aromatics (Adjusted) ND mg/Kg 4.4 1.0 C19-C36 Aliphatics ND mg/Kg 4.4 1.0 Page 6 of 25 Ms. Holii Raffington TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, 1=L 32812 Job Number: 360-9440-1 Client Sample ID: OQD0273-01 Date Sampled: 04/17/2007 1200 Lab Sample ID: 360-9440-1 Date Received: 04/18/2007 0945 Client Matrix: Solid Percent Solids: 74 Analyte Result(Qualifier Unit RL Method: MA-EPH Date Analyzed: 04/18/2007 1751 Prep Method: 3646 Date Prepared: 04/18/2007 1252 C9-C18 Aliphatics ND mg/Kg 4.4 Total EPH ND mg/Kg 4.4 Surrogate. .................... Acceptance Limits..... . 2-Bromonsphthalene 90 0 40 -140 2-Fluorobiphenyl 97 % 40 - 140 o-Terphenyl 65 % 40 -140 1-Chlorooctadecane 53 % 40 -140 Method: PercentMolsture Date Analyzed: 04/18/2007 1646 Percent Moisture 26 % 1-0 Page 7 of 25 Dilution 1.0 1.0 1.0 Ms. Holli Raffington TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Client Sample ID: OQD0273-02 Lab Sample ID: 360-9440.2 Analyte Result/Qualifier Unit Job Number: 360-9440-1 Date Sampled: 04/17/2007 1300 Date Received: 04/18/2007 0945 Client Matrix: Solid Percent Solids: 70 RL Dilution Method: MAVPH Date Analyzed: 04/23/2007 1911 Prep Method: 5035 Date Prepared: 04/18/2007 1300 Benzene ND mg/Kg 0.76 1.0 Ethylbenzene ND mg/Kg 0.76 1.0 m-Xylene & p-Xylene ND mg/Kg 1.5 1.0 Methyl tert-butyl ether ND mg/Kg 0.15 1.0 Naphthalene ND mg/Kg 1.5 1.0 o-Xylene ND mg/Kg 0.76 1.0 Toluene ND mg/Kg 0.76 1.0 C5-C8 Aliphatics (unadjusted) ND mg/Kg 7.6 1.0 C9-C12 Aliphatics (unadjusted) ND mg/Kg 7.6 1.0 C5-C8 Aliphatics (adjusted) ND mg/Kg 7.6 1.0 C9-C12 Aliphatics (adjusted) ND mg/Kg 7.6 1.0 C9-C10 Aromatics ND mg/Kg 7.6 1.0 Total VPH ND mg/Kg 7.6 1.0 Surrogate,. Appgptanc*...Limits 2,5-Dibromotoluene (fid) 103 % 70 -130 2,5-Dibromotoluene (pid) 101 % 70 -130 Method: MA-EPH Date Analyzed: 04/18/2007 1814 Prep Method: 3646 Date Prepared: 04/18/2007 1252 Acenaphthene ND mg/Kg 0.46 1.0 Acenaphthylene ND mg/Kg 0.46 1.0 Anthracene ND mg/Kg 0.46 1.0 Benzo[a]anthracene ND mg/Kg 0.46 1.0 Benzo[a]pyrene ND mg/Kg 0.46 1.0 Benzo[b]fluoranthene ND mg/Kg 0.46 1.0 Benzo[g,h,i]perylene ND mg/Kg 0.46 1.0 Benzo[k]fluoranthene ND mg/Kg 0.46 1.0 Chrysene ND mg/Kg 0.46 1.0 Dibenz(a,h)anthracene ND mg/Kg 0.46 1.0 Fluoranthene ND mg/Kg 0.46 1.0 Fluorene ND mg/Kg 0.46 1.0 Indeno[1,2,3-cd]pyrene ND mg/Kg 0.46 1.0 2-Methyinaphthalene ND mg/Kg 0.46 1.0 Naphthalene ND mg/Kg 0.46 1.0 Phenanthrene ND mg/Kg 0.46 1.0 Pyrene ND mg/Kg 0.46 1.0 C11-C22 Aromatics (unadjusted) ND mg/Kg 4.6 1.0 C11-C22 Aromatics (Adjusted) ND mg/Kg 4.6 1.0 C19-C36 Aliphatics ND mg/Kg 4.6 1.0 Page 8 of 25 Ms. Holli Rafti'fngton Job Number: 360-9440-1 TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Client Sample ID: OQD0273-02 Date Sampled: 04/17/2007 1300 Lab Sample ID: 360-9440-2 Date Received: 04/18/2007 0945 Client Matrix: Solid Percent Solids: 70 Analyte Result/Qualifier Unit RL Dilution Method: MA-EPH Date Analyzed: 04/18/2007 1814 Prep Method: 3546 Date Prepared: 04/18/2007 1252 C9-C18 Aliphatics ND mg/Kg 4.6 1.0 Total EPH ND mg/Kg 4.6 1.0 Surrogate... .... Acceptance Limits . ......... 2-Bromonaphthalene 98 % 40 - 140 2-Fluorobiphenyl 105 % 40 - 140 o-Terphenyl 72 % 40 - 140 1-Chlorooctadecane 52 % 40 -140 Method: PercentMoisture Date Analyzed: 04/18/2007 1646 Percent Moisture 30 % 1.0 1.0 Page 9 of 25 Ms. Holli Raffington TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Client Sample ID: 00D0273-03 Lab Sample ID: 360-9440.3 Job Number: 360-9440-1 Date Sampled: 04/17/2007 1305 Date Received: 04/18/2007 0945 Client Matrix: Solid Percent Solids: 76 Analyte Result/Qualffier Unit RL Dilution Method: MAVPH Date Analyzed: 04/23/2007 1944 Prep Method: 6035 Date Prepared: 04/18/2007 1300 Benzene ND mg/Kg 0.65 1.0 Ethylbenzene ND mg/Kg 0.65 1.0 m-Xylene & p-Xylene ND mg/Kg 1.3 1.0 Methyl tert-butyl ether ND mg/Kg 0.13 1.0 Naphthalene ND mg/Kg 1.3 1.0 o-Xylene ND mg/Kg 0.65 1.0 Toluene ND mg/Kg 0.65 1.0 C5-C8 Aliphatics (unadjusted) ND mg/Kg 6.5 1.0 C9-C12 Aliphatics (unadjusted) ND mg/Kg 6.5 1.0 C5-C8 Aliphatics (adjusted) ND mg/Kg 6.5 1.0 C9-C12 Aliphatics (adjusted) ND mg/Kg 6.5 1.0 C9-C10 Aromatics ND mg/Kg 6.5 1.0 Total VPH ND mg/Kg 6.5 1.0 Surrogate .. Acceptance.. Limits 2,5-Dibromotoluene (fid) 101 % 70 -136 2,5-Dibromotoluene (pid) 98 % 70 -130 Method: MA-EPH Date Analyzed: 04/18/2007 1837 Prep Method: 3646 Date Prepared: 04/18/2007 1252 Acenaphthene ND mg/Kg 0.43 1.0 Acenaphthylene ND mg/Kg 0.43 1.0 Anthracene ND mg/Kg 0.43 1.0 Benzo[a]anthracene ND mg/Kg 0.43 1.0 Benzo[a]pyrene ND mg/Kg 0.43 1.0 Benzo(b]fluoranthene ND mg/Kg 0.43 1.0 Benzo(g,h,i]perylene ND mg/Kg 0.43 1.0 Benzo(k]fluoranthene ND mg/Kg 0.43 1.0 Chrysene ND mg/Kg 0.43 1.0 Dibenz(a,h)anthracene ND mg/Kg 0.43 1.0 Fluoranthene ND mg/Kg 0.43 1.0 Fluorene ND mg/Kg 0.43 1.0 Indeno[1,2,3-cd]pyrene ND mg/Kg 0.43 1.0 2-Methylnaphthalene ND mg/Kg 0.43 1.0 Naphthalene ND mg/Kg 0.43 1.0 Phenanthrene ND mg/Kg 0.43 1.0 Pyrene ND mg/Kg 0.43 1.0 C11-C22 Aromatics (unadjusted) ND mg/Kg 4.3 1.0 C11-C22 Aromatics (Adjusted) ND mg/Kg 4.3 1.0 C19-C36 Aliphatics ND mg/Kg 4.3 1.0 Page 10 of 25 Ms. Holli Raffington TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Client Sample ID: OQD0273-03 Lab Sample ID: 360-9440-3 Analyte Method: MA-EPH Prep Method: 3546 C9-C18 Aliphatics Total EPH Surrogate 2-Bromonsphthalene 2-Fluorobiphenyl o-Terphenyl 1-Chlorooctadecane Method: PercentMoisture Percent Moisture Job Number: 360-9440-1 Date Sampled: 04/17/2007 1305 Date Received: 04/18/2007 0945 Client Matrix: Solid Percent Solids: 76 Result/Qualifier Unit RL Dilution Date Analyzed: 04/18/2007 1837 Date Prepared: 04/18/2007 1252 ND mg/Kg 4.3 1.0 ND mg/Kg 4.3 1.0 ............ Acceptam* Limits........... 93 %... 40 -140 99 % 40 -140 fib % 40 -140 50 % 40 -140 Date Analyzed: 04/18/2007 1646 24 % 1.0 1.0 Page 11 of 25 Ms. Holli Raffington TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Client Sample ID: 00D0273-04 Lab Sample ID: 360-9440-4 Job Number. 360-9440-1 Date Sampled: 04/17/2007 1310 Date Received: 04/18/2007 0945 Client Matrix: Solid Percent Solids: 87 Analyte Result/Qualifier . Unit RL Dilution Method: MAVPH Date Analyzed: 04/23/2007 2017 Prep Method: 6036 Date Prepared: 04/18n007 1300 Benzene ND mg/Kg 0.64 1.0 Ethylbenzene ND mg/Kg 0.64 1.0 m-Xylene & p-Xylene ND mg/Kg 1.3 1.0 Methyl tert-butyl ether ND mg/Kg 0.13 1.0 Naphthalene ND mg/Kg 1.3 1.0 o-Xylene ND mg/Kg 0.64 1.0 Toluene ND mg/Kg 0.64 1.0 CS-C8 Aliphatics (unadjusted) ND mg/Kg 6.4 1.0 C9-C12 Aliphatics (unadjusted) ND mg/Kg 6.4 1.0 C5-C8 Aliphatics (adjusted) ND mg/Kg 6.4 1.0 C9-C12 Aliphatics (adjusted) ND mg/Kg 6.4 1.0 C9-C 10 Aromatics ND mg/Kg 6.4 1.0 Total VPH ND mg/Kg 6.4 1-0 $.u...rrogate... ........ Acceptance Limits 2,5-Dibromotoluene (fid) 102 70 -130 2,5-Dibromotoluene (pid) 98 % 70 -130 Method: MA-EPH Date Analyzed: 04/18/2007 1900 Prep Method: 3546 Date Prepared: 04/18/2007 1252 Acenaphthene ND mg/Kg 0-37 1.0 Acenaphthylene ND mg/Kg 0.37 1.0 Anthracene ND mg/Kg 0.37 1.0 Benzo[a]anthracene ND mg/Kg 0.37 1.0 Benzo[a]pyrene ND mg/Kg 0.37 1.0 Benzo[b]fluoranthene ND mg/Kg 0.37 1.0 Benzo[g,h,i]perylene ND mg/Kg 0.37 1.0 Benzo[k]fluoranthene ND. mg/Kg 0.37 1.0 Chrysene ND mg/Kg 0.37 1.0 Dibenz(a,h)anthracene ND mg/Kg 0.37 1.0 Fluoranthene ND mg/Kg 0.37 1.0 Fluorene ND mg/Kg 0.37 1.0 Indeno[1,2,3-cd]pyrene ND mg/Kg 0.37 1.0 2-Methyl naphthalene ND mg/Kg 0.37 1.0 Naphthalene ND mg/Kg 0.37 1.0 Phenanthrene ND mg/Kg 0.37 1.0 Pyrene ND mg/Kg 0.37 1.0 C11-C22 Aromatics (unadjusted) ND mg/Kg 3.7 1.0 C11-C22 Aromatics (Adjusted) ND mg/Kg 3.7 1.0 C19-C36 Aliphatics ND mg/Kg 3.7 1.0 Page 12 of 25 Ms. Holli Raffington TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Client Sample ID: OQD0273-04 Lab Sample ID: 360-9440-4 Analyte _ Method: MA-EPH Prep Method: 3546 C9-C18 Aliphatics Total EPH Surrogate...... 2-Bromonaphthalene 2-Fluorobiphenyl o-Terphenyl 1-Chlorooctadecane Method: PercentMolsture Percent Moisture Result/Qualifier Date Analyzed: Date Prepared: ND ND 88 95 65 55 Date Analyzed: 13 Job Number: 360-9440-1 Date Sampled: 04/17/2007 1310 Date Received: 04/18/2007 0946 Client Matrix: Solid Percent Solids: 87 Unit_ 04/18/2007 1900 04/18/2007 1252 mg/Kg mg/Kg o� o� 04/18/2007 1646 Page 13 of 25 RL Dilution 3.7 1.0 3.7 1.0 Acceptance Limits ............................ 40 -140 40 -140 40 -140 40 -140 1.0 1.0 Ms. Holli Raffington TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Client Sample ID: OQD0273-05 Lab Sample ID: 360-9440-5 Analyte _ Method: MAVPH Prep Method: 5036 ResultlQualitler Date Analyzed: Date Prepared: Job Number: 360-9440-1 Date Sampled: 04/17/2007 1315 Date Received: 04/18/2007 0945 Client Matrix: Solid Percent Solids: 91 Unit 04/23/2007 2050 04/18/2007 1300 RL Dilution Benzene ND mg/Kg 0.55 1.0 Ethylbenzene ND mg/Kg 0.55 1.0 m-Xylene & p-Xylene ND mg/Kg 1.1 1.0 Methyl tart -butyl ether ND mg/Kg 0.11 1.0 Naphthalene ND mg/Kg 1.1 1.0 o-Xylene ND mg/Kg 0.55 1.0 Toluene ND mg/Kg 0.55 1.0 C5-C8 Aliphatics (unadjusted) ND mg/Kg 5.5 1.0 C9-C12 Aliphatics (unadjusted) ND mg/Kg 5.5 1.0 C5-C8 Aliphatics (adjusted) ND mg/Kg 6.5 1.0 C9-C12 Aliphatics (adjusted) ND mg/Kg 5.5 1.0 C9-C10 Aromatics ND mg/Kg 5.5 1.0 Total VPH ND mg/Kg 5.5 1.0 Surrogate _.A...cceptance.. Limits ............. . 2,5-Dibromotoluene (fid) 102 % 70 -130 2,5-Dibromotoluene (pid) 99 % 70 -130 Method: MA-EPH Date Analyzed: 04/18/2007 1923 Prep Method: 3546 Date Prepared: 04/18/2007 1252 Acenaphthene ND mg/Kg 0.36 1.0 Acenaphthylene ND mg/Kg 0.36 1.0 Anthracene ND mg/Kg 0.36 1.0 Benzo[a]anthracene ND mg/Kg 0.36 1.0 Benzo[a]pyrene ND mg/Kg 0.36 1.0 Benzo[b]fluoranthene ND mg/Kg 0.36 1.0 Benzo[g,h,i]perylene ND mg/Kg 0.36 1.0 Benzo[k]fluoranthene ND mg/Kg 0.36 1.0 Chrysene ND mg/Kg 0.36 1.0 Dibenz(a,h)anthracene ND mg/Kg 0.36 1.0 Fluoranthene ND mg/Kg 0.36 1.0 Fluorene ND mg/Kg 0.36 1.0 Indeno[1,2,3-cd]pyrene ND mg/Kg 0.36 1.0 2-Methylnaphthalene ND mg/Kg 0.36 1.0 Naphthalene ND mg/Kg 0.36 1.0 Phenanthrene ND mg/Kg 0.36 1.0 Pyrene ND mg/Kg 0.36 1.0 C11-C22 Aromatics (unadjusted) ND mg/Kg 3.6 1.0 C11-C22 Aromatics (Adjusted) ND mg/Kg 3.6 1.0 C19-C36 Aliphatics ND mg/Kg 3.6 1.0 Page 14 of 25 Ms. Holli Raffington TestAmerica Analytical Testing Corp 4310 East Anderson Road Orlando, FL 32812 Client Sample ID: OQD0273-06 Lab Sample ID: 360-9440-5 Job Number: 360-9440-1 Date Sampled: 04/17/2007 1315 Date Received: 04/18/2007 0945 Client Matrix: Solid Percent Solids: 91 Analyte Result/Qualifier Unit RL Dilution Method: MA-EPH Date Analyzed: 04/18/2007 1923 Prep Method: 3646 Date Prepared: 04/18/2007 1252 C9-C18 Aliphatics ND mg/Kg 3.6 1.0 Total EPH ND mg/Kg 3.6 1.0 Surrogate........... .-.,,..._.................. Acpeptance Limits 2-Bromonaphthalene 97.. % 40 -140 2-Fluorobiphenyl 104 % 40 -140 o-Terphenyl 70 % 40 -140 1-Chlorooctadecane 51 % 40 -140 Method: PercentMolsture Date Analyzed: 04/18/2007 1646 Percent Moisture 9.3 % 1.0 1.0 Page 15 of 25 STL Westfield QUALITY CONTROL RESULTS Page 16 of 25 Client: TestAmerica Analytical Testing Corp QC Association Summary Quality Control Results Job Number: 360-9440-1 Report Lab Sample ID Client Sample ID Basis Client Matrix Method Prep Batch GC VOA _ ........................................ ....... .................. Prep Batch: 360-17704 360-9440-1 00D0273-01 T Solid 5035 360-9440-2 OQD0273-02 T Solid 5036 360-9440-3 0000273-03 T Solid 5035 360-9440-4 OQD0273-04 T Solid 5035 360-9440-5 OQD0273-05 T Solid 5036 Analysis Batch:360-17776 LCS 360-17776/1 Lab Control Spike T Solid MAVPH LCSD 360-17776/2 Lab Control Spike Duplicate T Solid MAVPH MB 360-17776/3 Method Blank T Solid MAVPH 360-9440-1 OQD0273-01 T Solid MAVPH 360-17704 360-9440-2 OQD0273-02 T Solid MAVPH 360-17704 360-9440-3 OQD0273-03 T Solid MAVPH 360-17704 360-9440-4 OQD0273-04 T Solid MAVPH 360-17704 360-9440-5 OQD0273-05 T Solid MAVPH 360-17704 Report Basis T - Total GC Semi VOA Prep Batch: 360.17612 LCS 360-17612/2-AA LCSD 360-1761213-AA MB 360-17612/1-AA 360-9440-1 360-9440-2 360-9440-3 360-9440-4 360-9440-5 Analysis Batch:360-17650 LCS 360-17612/2-AA LCSD 360-17612/3-AA MB 360-17612/1-AA 360-9440-1 360-9440-2 360-9440-3 350-9440-4 360-9440-5 Report Basis T - Total STL Westfield Lab Control Spike Lab Control Spike Duplicate Method Blank OQD0273-01 OQD0273-02 OQD0273-03 OQD0273-04 OQD0273-05 Lab Control Spike Lab Control Spike Duplicate Method Blank OQD0273-01 OQD0273-02 OQD0273-03 OQD0273-04 OQD0273-05 T Solid 3546 T Solid 3546 T Solid 3546 T Solid 3546 T Solid 3546 T Solid 3546 T Solid 3546 T Solid 3546 T Solid MA-EPH 360-17612 T Solid MA-EPH 360-17612 T Solid MA-EPH 360-17612 T Solid MA-EPH 360-17612 T Solid MA-EPH 360-17612 T Solid MA-EPH 360-17612 T Solid MA-EPH 360-17612 T Solid MA-EPH 360-17612 Page 17 of 25 Client: TestAmerica Analytical Testing Corp QC Association Summary Quality Control Results Job Number. 360-9440-1 Report Lab Sample ID Client Sample ID Basis Client Matrix Method Prep Batch General Chemistry .................... ........................... _ .. ...... Analysis Batch:360-17624 360-9440-1 OQD0273-01 T Solid PercentMoisture 360-9440-2 OQD0273-02 T Solid PercentMoisture 360-9440-3 00DO273-03 T Solid PercentMoisture 360-9440-4 OQD0273-04 T Solid PercentMoisture 360-9440-5 OQD0273-05 T Solid PercentMoisture Report Basis T - Total STL Westfield Page 18 of 25 Client: TestAmerica Analytical Testing Corp Method Blank - Batch: 360-17776 Lab Sample ID: MB 360-17776/3 Analysis Batch: 360-17776 Client Matrix: Solid Prep Batch: N/A Dilution: 1.0 Units: mg/Kg Date Analyzed: 04/23/2007 1805 Date Prepared: N/A Analyte Result Benzene ND Ethylbenzene ND m-Xylene & p-Xylene ND Methyl tart -butyl ether ND Naphthalene ND o-Xylene ND Toluene ND C5-C8 Aliphatics (unadjusted) ND C9-C12 Aliphatics (unadjusted) ND C5-C8 Aliphatics (adjusted) ND C9-C12 Aliphatics (adjusted) ND C9-CIO Aromatics ND Total VPH ND Surrogate ............. % Rec 2,5-Dibromotoluene (fid) 101 2,5-Dibromotoluene (pid) 100 Quality Control Results Job Number: 360-9440-1 Method: MAVPH Preparatlon: NIA Instrument ID: HP 589011 GC w/ PID/FID Lab File ID: L5908.D Initial WeighWolume: 0.10 mL Final WeighWolume: 5 mL Injection Volume: Column ID: PRIMARY Qual ................ Acceptance Limits 70 -130 70 -130 Calculations are performed before rounding to avoid round -off errors in calculated results. STL Westfield Page 19 of 25 RL 0.25 0.25 0.50 0.050 0.50 0.25 0.25 2.5 2.5 2.5 2.5 2.5 2.5 Client: TestAmerica Analytical Testing Corp Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 360-17776 LCS Lab Sample ID: LCS 360-17776/1 Analysis Batch: 360-17776 Client Matrix: Solid Prep Batch: N/A Dilution: 1.0 Units: mg/Kg Date Analyzed: 04/23/2007 1625 Date Prepared: N/A .......... .......................... LCSD Lab Sample ID: LCSD 360-17776/2 Analysis Batch: 360-17776 Client Matrix: Solid Prep Batch: N/A Dilution: 1.0 Units: mg/Kg Date Analyzed: 04/23/2007 1659 Date Prepared: N/A Analyte ............ ..._ __........... _................_._ ...._. Benzene Ethylbenzene m-Xylene & p-Xylene Methyl tert-butyl ether Naphthalene o-Xylene Toluene C5-C8 Aliphatics (unadjusted) C9-C12 Aliphatics (unadjusted) C9-C 10 Aromatics Surrogate 2,5-Dibromptoluene (fid) 2,5-Dibromotoluene (pid) Quallty Control Results Job Number: 360-9440-1 Method: MAVPH Preparation: NIA Instrument ID: HP 589011 GC w/ PID/FID Lab File ID: L5905.D Initial WeighWolume: 5 mL Final WeighWolume: 5 mL Injection Volume: Column ID: PRIMARY Instrument ID: HP 589011 GC w/ PID/FID Lab File ID: L5906.D Initial WeighWolume: 5 mL Final WeighWolume: 5 mL Injection Volume: Column ID: PRIMARY % Rec. LCS LCSD Limit RPD 98 98 70 -130 1 98 97 70 -130 1 97 96 70 - 130 1 106 107 70 - 130 1 109 110 70 - 130 0 90 91 70 - 130 0 89 88 70 - 130 1 104 105 70 -130 0 104 102 70 -130 2 110 107 70 - 130 3 LCS % Rec LCSD % Rec 107 106 107 106 Calculations are performed before rounding to avoid round -off errors in calculated results. STL Westfield Page 20 of 25 RPD, Limit LCS Qual LCSD Qual 25 25 25 25 25 25 25 25 25 25 Acceptance Limits 70 -130 70 -130 Client: TestAmerica Analytical Testing Corp Method Blank - Batch: 360-17612 Lab Sample ID: MB 360-17612/1-AA Analysis Batch: 360-17650 Client Matrix: Solid Prep Batch: 360-17612 Dilution: 1.0 Units: mg/Kg Date Analyzed: 04/18/2007 1946 Date Prepared: 04/18/2007 1252 Quality Control Results Job Number: 360-9440-1 Method: MA-EPH Preparation: 3546 Instrument ID: HP 6890 GC w/ dual FIDs Lab File ID: R04644A.D Initial WeighWolume: 30.00 g Final WeighWolume: 2.0 mL Injection Volume: Analyte Result Qual RL ........ .......... _.......................,.,.._ Acenaphthene _......... ...... _._._.......... ... _._... .. ND M - _........................ 0.33 Ac enaphthylene ND 0.33 Anthracene ND 0.33 Senzo[a)anthracene ND 0.33 Benzo[a]pyrene ND 0.33 Benzo[b]fluoranthene ND 0.33 Benzo[g,h,i]perylene ND 0.33 Benzo[k]fluoranthene ND 0.33 Chrysene ND 0.33 Dibenz(a,h)anthracene ND 0.33 Fluoranthene ND 0.33 Fluorene ND 0.33 Indeno[1,2,3-cd]pyrene ND 0.33 2-Methylnaphthatene ND 0.33 Naphthalene ND 0.33 Phenanthrene ND 0.33 Pyrene ND 0.33 C11-C22 Aromatics (unadjusted) ND 3.3 C11-C22 Aromatics (Adjusted) ND 3.3 C19-C36 Allphatics ND 3.3 C9-C18 Aliphatics ND 3.3 Total EPH ND 3.3 Surrogate 2-Bromonaphthalene 2-Fluorobiphenyl o-Terphenyl 1-Chlorooctedecane % Rec 100 107 84 65 Calculations are performed before rounding to avoid round -off errors in calculated results. STL Westfield Page 21 of 25 Acceptance Limits 40 - 140 40 - 140 40 - 140 40 - 140 Client: TestAmerica Analytical Testing Corp Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 360-17612 LCS Lab Sample ID: LCS 360-17612/2-AA Analysis Batch: 360-17650 Client Matrix: Solid Prep Batch: 360-17612 Dilution: 1.0 Units: mg/Kg Date Analyzed: 04/18/2007 1705 Date Prepared: 04/18/2007 1252 LCSD Lab Sample ID: LCSD 360-17612/3-AA Analysis Batch: 360-17650 Client Matrix: Solid Prep Batch: 360-17612 Dilution: 1.0 Units: mg/Kg Date Analyzed: 04/18/2007 1728 Date Prepared: 04/18/2007 1252 Quality Control Results Job Number: 360-9440-1 Method: MA-EPH Preparation: 3646 Instrument ID: HP 6890 GC w/ dual FIDs Lab File ID: R04646.D Initial Weight/Volume: 30.00 g Final Weight/Volume: 2.0 mL Injection Volume: Instrument ID: HP 6890 GC w/ dual FID, Lab File ID: R04648.D Initial Weight/Volume: 30.00 g Final WeighWolume: 2.0 mL Injection Volume: Rec, Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual _._ ___........ Acenaphthene 75 .......... . I I .... ....... 81 .. 40 - 140 _ ._......,.....,.. 8 25 _...... ..... ..-............ Acenaphthylene 75 82 40 - 140 8 25 Anthracene 94 103 40 -140 10 25 Benzo[a]anthracene 101 115 40 - 140 12 25 Benzo[a]pyrene 109 122 40 -140 11 25 Benzo[b]fluoranthene 101 109 40 -140 7 25 Benzo[g,h,i]perylene 109 124 40 - 140 13 25 Benzo[k]fluoranthene 116 122 40 - 140 5 25 Chrysene 106 118 40 - 140 11 25 Dibenz(a,h)anthracene 111 122 40 -140 9 25 Fluoranthene 97 108 40 - 140 10 25 Fluorene 82 90 40 -140 9 25 Indeno[1,2,3-cd]pyrene 104 121 40 -140 14 25 2-Methylnaphthalene 59 75 40 -140 8 25 Naphthalene 59 65 40 -140 9 25 Phenanthrene 87 96 40 - 140 9 25 Pyrene 101 113 40 -140 11 25 C11-C22 Aromatics (unadjusted) 94 105 40 - 140 11 25 C19-C36 Aliphatics 70 82 40 - 140 15 25 C9-C18 Aliphatics 46 53 40 - 140 13 25 Surrogate LCS % Rec LCSD % Rec Acceptance Limits 2-Bromonaphthalene 96 100 40 - 140 2-Fluorobiphenyl 102 106 40 - 140 o-Terphenyl 91 96 40 - 140 1-Chlorooctadecane 60 65 40 - 140 Calculations are performed before rounding to avoid round -off errors in calculated results. STL Westfield Page 22 of 25 LOGIN SAMPLE RECEIPT CHECK LIST Client: TestAmerica Analytical Testing Corp Job Number: 360-9440-1 Login Number: 9440 Question T/F/NA Comment Radioactivity either was not measured or, if measured, is at or below background NA The cooler's custody seal, if present, is intact. NA The cooler or samples do not appear to have been compromised or tampered with. True Samples were received on ice. True Cooler Temperature is acceptable. True 1.4 C Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True There are no discrepancies between the sample IDs on the containers and the True COC. Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True There is sufficient vol. for all requested analyses, Incl, any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. NA If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present. True Samples do not require splitting or compositing. True STL Westfield Page 23 of 25 SUBCONTRACT ORDER TestArnerica - Orlando, FL OQD0273 §JNDING LA130MMRY: RECEIVINO LABORATORY: TestAmerica - Orlando, FL STL - Westtield, MA 4310 East Anderson Road 53 SOUTHAMPTON RD Orlando, FL 32812 WESTFIELD, MA 01085 Phone: 800-851-2560 Phone :(413) 572-4000 . Fax: 407-866-0886 Fax: (413) 572-3707 Project Manager: Hoili Raffington Project Location: North Carolina Client: ENM0ASSESSME7M Receipt Temperance: °C Ice: Y / N Analysis Due Expires Interlab Surch Comments Clits.l Sample ID: OQD0273.01 Solid/Soil Samoled: 04M7/0712:00 RUSH A - MADEP-EPH 04/23/0716:00 05101/0712:00 �10 MADEP-VPH 04/23/0716:00 0101/0712:00 mom Containers Supplied: Sample 1D: OQD0273.02 Solid/Sofl RUSH MADEP-EPH 0412310716:00 .05101/0713:00 STL-Wakefleld MADEP-VPH 04123/0716:00 05/01/0713:00 STL-Wakefield Containers Supplied: Sample 1D: 00DO273-03 Solid/Sall RUSH Sampled-, _Mj7107 1a;os - Z MADEP-EPH 04/23/0716*00 05/01i0713:05 � 00 STL-Wakefield MADEP-VPH 04/23/0716:00 OBM110713:05 M-Wakefield Containers Supplied: 5--3 Sample ID; OQD0273-04 Solid/Soil m RUSH MADEP-EPH 04123/0716:00 05/M/0713:10 STL-Wakefield MADEP-VPH 04=0716:00 05/01/O713:10 8TL-Wakefield Containers Supplied., Sample ID: 0000273-05 Solid/Soil RUSH MADEP-EPH 04/23/0716:00 05101/0713:15 STL-Wakefield MADEP-VPH 04/2310716:00 05/01/0713:15 STL-Wakefield Containers Supplied: Released By Daterfime Received By Datefllme• S - Released By Dateffime Received By Dateffime Page 1 of 1 Page 24 of 25 O S �C�:IIII�OC��� • � �� � - r��r��cres�a�...■.■ �rns�i��eeeo� �Ere,iaEeeoo� �EEaluluc€E06I I.IGII Ip I �`'i Page 25 of 25 p -u -D. v - P 0 X VV I v 06