AS-3650_28785_CA_MRP_20240624

Groundwater Monitoring Report Eblen Short Stop #2 Asheville, North Carolina

ACTIVE REMEDIATION MONITORING
REPORT

For

BILTMORE OIL COMPANY
EBLEN SHORT STOP #2
217 Amboy Road Asheville, North Carolina 28806 Incident No. 28785

PREPARED FOR: Biltmore Oil Company
191 Amboy Road
Asheville, NC 28806

PREPARED BY: Singleton Environmental, Inc. PO Box 604 Fletcher, NC 28732

June 24, 2024

Singleton Environmental, Inc
Groundwater Monitoring Report Eblen Short Stop #2 Asheville, North Carolina
GROUNDWATER MONITORING REPORT
June 24, 2024 Site Name: Eblen Short Stop #2 217 Amboy Road
Asheville, NC 28806 Buncombe County Incident Number: 28785 Risk Classification: Intermediate Responsible Party (UST): Biltmore Oil Company Attn: Mr. Rick Perkins 191 Amboy Road
Asheville, NC 28806 Property Owner: SANISCO, LLC PO Box 2805 Asheville, NC 28802
Report Prepared By: Singleton Environmental, Inc PO Box 604 Fletcher, North Carolina, 28732 [phone] Release Location: 35.567029 / -82.573258
Signature and Seal of the Certifying Licensed Geologist: I, Christopher D. Singleton, a North Carolina Licensed Geologist, do certify that the information
contained in this report is correct and accurate to the best of my knowledge. ___________________________________ Christopher D. Singleton, P.G. #1928 NC License #2033

Singleton Environmental, Inc. is licensed to practice geology in North Carolina. The corporate license
number is C-443.

Groundwater Monitoring Report Eblen Short Stop #2 Asheville, North Carolina
Table of Contents
Introduction ................................................................................................................................1
Site History…......................…………......................................... .................................................1 Free Phase Product…......................…………......................................... ......................................3 Groundwater Monitoring…......................…………......................................... .............................4 Conclusions and Recommendations…..................…………......................................... ................5
Tables Table 1: Monitoring Well Construction Details Table 2: Groundwater Elevation Data Table 3: Groundwater Quality Data-Volatile Organic Compounds
Table 4: Groundwater Quality Data-Semi-volatile Organic Compounds Table 5: Groundwater Quality Data-MADEP VPH/EPH Figures
Figure 1: Site Vicinity Map Figure 2: Site Map Figure 3: Free Product/LNAPL Isoconcentration Contour Map
Figure 4: Groundwater Elevation Map Figure 5: Groundwater Quality Map Figure 6: BTEX Isoconcentration Contour Map Figure 7: Naphthalene Isoconcentration Contour Map
Appendices Appendix A: Field Notes Appendix B: Laboratory Analytical Report Appendix
Groundwater Monitoring Report Eblen Short Stop #2 Asheville, North Carolina
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Introduction
Singleton Environmental, Inc. is presenting a summary of groundwater monitoring activities related to a release from the underground storage tank (UST) system at the Eblen Short Stop #2
located at 217 Amboy Road in Asheville, NC. The monitoring event was conducted on June 17, 2024. Figure 1 is a portion of the 2017 Lidar Hillshade with topographic contours and depicts the site location and vicinity with relevant topographic features. Figure 2 is a site map showing the UST field and monitoring well locations on a 2019 aerial image basemap. The site is located
on the north side of Amboy Road in an area of commercial and residential development.
Site History
During a routine site inspection conducted in 2009, a release from the diesel dispenser was detected. Soil samples collected indicated total petroleum hydrocarbons as diesel and gasoline range organics (TPH-DRO/GRO) at a concentration of 669 milligrams per kilogram (mg/kg) and 374 mg/kg, respectively. The Site Check Report was submitted (by others) to The North Carolina
Department of Environmental Quality (NCDEQ) in December 2009. Impacted soil associated
with the diesel fuel dispenser was subsequently excavated in August 2011 and post excavation samples indicated no analytes in excess of the soil to water maximum contaminant concentrations (MSCCs). The Initial Abatement Action Report was submitted to NCDEQ in October 2011.
In September 2011 a leak was detected in the 8,000-gallon gasoline underground storage tank (UST). As part of the initial abatement activities, the UST was pumped out and repaired. Subsequent assessment activities included the installation of on-site monitoring wells and sampling. Monitoring wells MW-1, MW-3, and MW-5 historically contained free phase product
and four aggressive fluid vapor recovery events (AFVR) were conducted between December
2012 and May 2013 removing approximately 1,742-gallons of product. The following assessment reports have been submitted (by others) to NCDEQ in relation to the gasoline release at the Eblen Short Stop #2
• 20-Day Report – October 2011
• Initial Abatement Action Report (IAAR) – June 2014
• Limited Site Assessment Report (LSA) – August 2014
• Comprehensive Site Assessment Report (CSA) – October 2016
• Groundwater Monitoring Report – April 10, 2019
• Groundwater Monitoring Report – November 13, 2019
• Groundwater Monitoring Report – April 13, 2020
• Groundwater Monitoring Report – November 30, 2020
• Groundwater Monitoring Report – August 23, 2022
• Groundwater Monitoring Report – April 12, 2023
• Groundwater Monitoring Report with MMPE – January 30, 2024
Groundwater Monitoring Report Eblen Short Stop #2 Asheville, North Carolina
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On July 24, 2019, a Notice of Violation letter was issued by NCDEQ indicating that the diesel dispenser (9/10) did not have a proper spill containment bucket installed. Therefore, Biltmore Oil
Company contracted Mountain Environmental to perform site check activities. On August 6, 2019, Mountain Environmental personnel visited the subject site with Biltmore Oil personnel in order to perform site check soil sampling activities. According to Biltmore Oil
personnel, dispenser 9/10, which did not contain proper spill containment, was the stand-alone
diesel fuel dispenser. One soil sample (DISP-1) was collected immediately underneath the fuel dispenser utilizing a stainless-steel hand auger. The soil sample was collected at approximately 1.5-2 feet below ground surface (bgs) and submitted to Pace Analytical for analysis of total petroleum hydrocarbons – gasoline range organics (GRO) and diesel range organics (DRO). Laboratory results indicate that the sample contained TPH-DRO at a concentration of 741 mg/kg
and TPH-GRO at a concentration of 464 mg/kg. Both the TPH-DRO and TPH-GRO concentrations exceed the NCDEQ Cleanup Level of 100 mg/kg and 50 mg/kg, respectively indicating a reportable release has occurred.
On October 17, 2019, Mountain Environmental Services, Inc. performed additional site check
activities. Due to the elevated TPH-DRO/GRO levels, an additional soil sample was collected underneath the stand-alone diesel dispenser in the same location as the August 2019 sampling. The additional soil sample D-1 was submitted to Pace Analytical for analysis of Risk-Based Parameters. This included volatile organic compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method 8270, and MADEP Methods for
extractable and volatile petroleum hydrocarbons (MADEP-EPH/VPH). According to the laboratory analytical report total C9-C22 aromatics exceeded the soil-to-groundwater maximum contaminant concentrations (MSCCs). No analytes exceeded the
residential or industrial/commercial MSCCs. The Site Check Report was submitted to NCDEQ
on November 13, 2019. The following table summarizes information about USTs at this site:
Tank No. Volume (gallons)
Contents (i.e., gasoline, diesel, kerosene, heating oil, waste oil,
Use (resale, heating building, distribution, farm or residential, etc.)
Date last used
Indicate whether UST has been removed or closed in place
Date of permanent closure (if
applicable)
Was a release detected from this UST system? If yes, give
Groundwater Monitoring Report Eblen Short Stop #2 Asheville, North Carolina
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The following table summarizes information about ASTs at this site:
Tank No. Volume (gallons)
Contents (i.e., gasoline, diesel, kerosene, heating oil, waste oil,
Use (resale, heating building, distribution, farm or residential, etc.)
Date last used
Indicate whether UST has been removed or closed in place
Date of permanent closure (if applicable)
Was a release detected from this UST system? If yes, give
Free Phase Product

Monitoring wells MW-1, MW-3, and MW-5 have historically contained free phase product and four aggressive fluid vapor recovery events (AFVR) were conducted between December 2012 and October 2019 removing approximately 1,767-gallons of product.
During the August 2022 sampling event, free product was detected in monitoring wells MW-1 and MW-5 at a thickness of 0.10 feet and 0.11 feet, respectively. Approximately 2-gallons of product and liquid was bailed from each monitoring well (MW-1 and MW-5). Absorbent socks were subsequently placed in each well.

During the February 2023 sampling event, free product was detected in monitoring wells MW-1
and MW-5 at a thickness of 0.21 feet and 0.43 feet, respectively. Approximately 5-gallons of product and liquid were bailed from each monitoring well (MW-1 and MW-5) and absorbent socks were subsequently replaced in each well. During the August 2023 sampling event, free product was detected in monitoring wells MW-1 and MW-5 at a thickness of 0.80 feet and 0.30 feet, respectively. Approximately 5-gallons of product and liquid were bailed from each monitoring well (MW-1 and MW-5) and absorbent socks were subsequently replaced in each well.

A mobile multi-phase extraction event (MMPE) was conducted between December 18-22, 2023. Prior to the MMPE free product was detected in monitoring wells MW-1 and MW-5 at a thickness of 0.73 feet, 0.28 feet, respectively. During the event, SEI was able to evacuate approximately 3,600 gallons of contaminated groundwater. Based on total emission calculations,
the event removed approximately 264.698 pounds (or 42.35 gallons) of petroleum product and vapor from beneath the site. During the June 2024 monitoring event absorbent socks were removed from MW-3 and replaced in monitoring wells MW-1 and MW-5. The spent absorbents were transported to Biltmore Oil
Groundwater Monitoring Report Eblen Short Stop #2 Asheville, North Carolina
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Company and placed in a 55-gallon drum for storage pending bulk disposal by SES Environmental.
Figure 3 depicts the estimated free product/LNAPL isoconcentration contours. Groundwater Monitoring Monitoring wells MW-1, MW-2, MW-3, MW-4, MW-5, MW-6, and MW-7 were gauged as part of the monitoring event on June 17, 2024. Based on groundwater elevation data, groundwater
flow appears to be directed to the southwest toward Moore Branch. This is consistent with
historical observations. Monitoring well construction details are summarized on Table 1.
Groundwater elevation data is summarized in Table 2 and a groundwater elevation map indicating groundwater flow direction is included as Figure 4. Field notes are included as Appendix A.
Monitoring wells MW-2, MW-3, MW-4, MW-6, and MW-7 were sampled as part of the monitoring event on June 17, 2024. Monitoring wells MW-1 and MW-5 contained approximately 0.35 feet and 0.03 feet of free product, respectively. Groundwater samples were submitted to Pace Analytical in Asheville, NC for analysis of volatile organic compounds
(VOCs) by EPA Method 6200 and semi-volatile organic compounds (SVOCs) by EPA Method
625. Laboratory analytical results indicate the following VOCs in excess of the NCAC 2L
Standards:
• Benzene: MW-3 (7,920 ug/l).
• Toluene: MW-3 (16,900 ug/l).
• Ethylbenzene: MW-3 (2,890 ug/l).
• Total xylenes: MW-2 (981 ug/l) and MW-3 (14,330 ug/l).
• Naphthalene (6200): MW-2 (95.2 ug/l) and MW-3 (538 ug/l).
• N-Propylbenzene: MW-3 (279 ug/l).
• Isopropylbenzene: MW-3 (103 ug/l).
• 1,2,4-Trimethylbenzene: MW-2 (1,390 ug/l) and MW-3 (2,250 ug/l).

• 1,3,5-Trimethylbenzene: MW-2 (444 ug/l) and MW-3 (509 ug/l).
• 1,2,3-Trichloropropane: MW-2 (11.6 ug/l).

Groundwater Monitoring Report Eblen Short Stop #2 Asheville, North Carolina
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Additionally, benzene exceeded the GCL in MW-3.
Laboratory analytical results indicate the following SVOCs in excess of the NCAC 2L Standards:
• Naphthalene (625): MW-3 (555 ug/l). VOC groundwater quality data is included in Table 3. SVOC groundwater quality data is included as Table 4 and historical VPH/EPH groundwater quality data is included as Table 5. Groundwater quality data is included as Figure 5, a total BTEX isoconcentration contour map, is
included as Figure 6 and a naphthalene isoconcentration contour map is included as Figure 7.
The laboratory analytical report is included as Appendix B.
Conclusions and Recommendations
Based on the June 2024 monitoring event, laboratory results indicate that VOCs and SVOCs
exceed the NCAC 2L Standards in MW-2 and MW-3. The analyte benzene exceeded the corresponding GCL in MW-3. Free product was detected in MW-1 and MW-5 at a thickness of 0.35 feet and 0.03 feet, respectively. The results of the June 2024 monitoring event are consistent with the historical data collected at the site.
At this time, Singleton Environmental, Inc. recommends continuing pre-CAP monitoring activities with an MMPE for the next groundwater monitoring event to be conducted in December 2024. In addition, absorbent socks will continue to be replaced as necessary.

Tables
Well Well Type Date
Installed Elevation1 Well Diameter
(inches)Total Depth2
(ft)
MW-1 Type II 06/06/22 98.06 2"5.00 -15.00 15.00
MW-2 Type II 06/06/22 100.54 2"5.00 -15.00 15.00
MW-3 Type II 02/15/13 96.53 2"6.00 -16.00 16.00
MW-4 Type II 06/06/22 95.83 2"5.00 -15.00 15.00
MW-5 Type II 05/08/13 96.51 2"6.00 -16.00 16.00
MW-6 Type II 10/01/16 91.24 2"1.50 -4.00 4.00
MW-7 Type II 06/07/22 100.86 2"5.00 -15.00 15.00
NOTES:
1. TOC = Top Of Casing. Elevation is based on a relative datum, not elevation above sea level.
Screened
Interval (ft)
Well ID Date
TOC
Elevation1 NAPL2
Depth to
Water3
Product
Thickness4 Groundwater
Elevation5 (ft)
10/2/2016 11.38 11.57 0.19 86.64
3/25/2019 NM 10.88 NM 89.12
10/17/2019 NM 10.97 NM 89.03
4/2/2020 NM NM NM NM
11/4/2020 NM NM NM NM
2/8/2022 NM NM NM NM
8/10/2022 9.19 9.29 0.10 88.85
2/16/2023 9.01 9.22 0.21 89.01
8/7/2023 9.10 9.90 0.80 88.80
12/18/2023 9.18 9.91 0.73 88.73
1/8/2024 9.09 9.15 0.06 88.96
6/17/2024 8.90 9.25 0.35 89.09
10/2/2016 NM 11.74 NM 88.80
3/25/2019 NM 10.96 NM 89.58
10/17/2019 NM 11.25 NM 89.23
4/2/2020 NM 11.03 NM 89.45
11/4/2020 NM 11.01 NM 89.47
2/8/2022 NM 10.45 NM 90.03
8/10/2022 NM 11.50 NM 89.04
2/16/2023 NM 10.41 NM 90.13
8/7/2023 NM 11.55 NM 88.99
1/8/2024 NM 11.38 NM 89.16
6/17/2024 NM 11.10 NM 89.44
NOTES:
1. TOC = Top Of Casing. Elevation is based on a relative datum, not elevation above sea lev
2. NAPL = Non aqueous petroeum liquid (free product).
3. Depth to NAPL/water reported in feet below top of casing.
4. NM=Not Measured.
6. Monitoring wells MW-1, MW-2, MW-4, and MW-7 were replaced and re-surveyed.
on June 6-7, 2022.
MW-1 98.06
MW-2 100.54
Table 2
Groundwater Elevation Data
Eblen Short Stop #2
Asheville, North Carolina
Well ID Date
TOC
Elevation1 NAPL2
Depth to
Water3
Product
Thickness4 Groundwater
Elevation5 (ft)
10/2/2016 NM 8.15 NM 88.38
3/25/2019 NM 8.01 NM 88.52
10/17/2019 9.45 9.61 0.16 87.05
4/2/2020 NM 9.11 NM 87.42
11/4/2020 NM 9.05 NM 87.48
2/8/2022 NM 7.27 NM 89.26
8/10/2022 NM 8.45 NM 88.08
2/16/2023 NM 7.31 NM 89.22
8/7/2023 NM 8.50 NM 88.03
12/18/2023 NM 8.58 NM 87.95
1/8/2024 7.50 7.70 0.20 88.99
6/17/2024 NM 8.55 NM 87.98
10/2/2016 NM 7.84 NM 87.99
3/25/2019 NM NM NM NM
10/17/2019 NM NM NM NM
4/2/2020 NM NM NM NM
11/4/2020 NM NM NM NM
2/8/2022 NM NM NM NM
8/10/2022 NM 8.81 NM 87.02
2/16/2023 NM 9.92 NM 85.91
8/7/2023 NM 8.86 NM 86.97
1/8/2024 NM 8.45 NM 87.38
6/17/2024 NM 8.48 NM 87.35
NOTES:
1. TOC = Top Of Casing. Elevation is based on a relative datum, not elevation above sea lev
2. NAPL = Non aqueous petroeum liquid (free product).
3. Depth to NAPL/water reported in feet below top of casing.
4. NM=Not Measured.
6. Monitoring wells MW-1, MW-2, MW-4, and MW-7 were replaced and re-surveyed.
on June 6-7, 2022.
MW-4 95.83
MW-3 96.53
Table 2
Groundwater Elevation Data
Eblen Short Stop #2
Asheville, North Carolina
Well ID Date Elevation1 NAPL2 Water3 Thickness4 Elevation5 (ft)
10/2/2016 NM 8.18 NM 88.33
3/25/2019 NM 8.05 NM 88.46
10/17/2019 9.33 9.61 0.28 87.12
4/2/2020 9.22 9.23 0.01 87.29
11/4/2020 NM 9.95 NM 86.56
2/8/2022 7.05 7.15 0.10 89.44
8/10/2022 8.29 8.40 0.11 88.20
2/16/2023 8.01 8.44 0.43 88.41
8/7/2023 9.40 9.70 0.30 87.05
12/18/2023 9.38 9.66 0.28 87.07
1/8/2024 8.04 8.10 0.06 88.46
6/17/2024 7.95 7.98 0.03 88.55
10/2/2016 NM 3.03 NM 88.21
3/25/2019 NM 2.90 NM 88.34
10/17/2019 NM 2.81 NM 88.43
4/2/2020 NM 1.06 NM 90.18
11/4/2020 NM 1.00 NM 90.24
2/8/2022 NM 0.95 NM 89.29
8/10/2022 NM 0.88 NM 90.36
2/16/2023 NM 0.55 NM 90.69
8/7/2023 NM 0.78 NM 90.46
1/8/2024 NM 0.55 NM 90.69
6/17/2024 NM 0.61 NM 90.63
10/2/2016 NM 10.70 NM 90.16
3/25/2019 NM NM NM NM
10/17/2019 NM NM NM NM
4/2/2020 NM NM NM NM
11/4/2020 NM NM NM NM
2/8/2022 NM NM NM NM
8/10/2022 NM 11.99 NM 88.87
2/16/2023 NM 10.22 NM 90.64
8/7/2023 NM 12.10 NM 88.76
1/8/2024 NM 11.87 NM 88.99
6/17/2024 NM 11.50 NM 89.36
NOTES:
1. TOC = Top Of Casing. Elevation is based on a relative datum, not elevation above sea leve
2. NAPL = Non aqueous petroeum liquid (free product).
3. Depth to NAPL/water reported in feet below top of casing.
4. NM=Not Measured.
(TOC Elevation-DTW)+(0.80x(product thickness)
6. Monitoring wells MW-1, MW-2, MW-4, and MW-7 were replaced and re-surveyed.
on June 6-7, 2022.
100.86
Table 2
Groundwater Elevation Data
Eblen Short Stop #2
Asheville, North Carolina
MW-5 96.51
MW-6 91.24
MW-7
Table 4 Groundwater Quality Data Semi-Volatile Organic Compounds Eblen Short Stop #2 Asheville, North Carolina
Monitoring
Well Sample
Date µg/l µg/l µg/l µg/l µg/l µg/l
2L Standard 100 6 300 30 3 200
GCL 100,000 6,000 845 30,000 135 550
10/15/2011
1/18/2012 ------------
12/1/2012
5/1/2013
3/25/2014 ------------
10/2/2016
3/25/2019 15.3 426 427 428
10/17/2019 <10.0 216 <5.0 <5.0
4/2/2020
11/4/2020
2/8/2022
8/10/2022
2/16/2023
8/7/2023
1/8/2024
6/17/2024
12/1/2012
3/25/2014 ------------
10/2/2016 <25 ----------
3/25/2019 <100 217 218 --219
10/17/2019 <10.0 317 6.1 ----6.6
4/2/2020 <50.0 329 <25.0 <25.0 <25.0 <25.0
11/4/2020 <50.0 <25.0 <25.0 <25.0 <25.0 <25.0
2/8/2022 <9.1 49 <4.5 <4.5 <4.5 <4.5
8/10/2022 <45.5 24.2 <22.7 <22.7 <22.7 <22.7
2/16/2023 <10.0 25.4 <5.0 <5.0 <5.0 <5.0
8/7/2023 <8.3 26.0 <4.2 <4.2 <4.2 <4.2
1/8/2024 <10.0 7.0 <5.0 <5.0 <5.0 <5.0
6/17/2024 <167 <83.3 <83.3 <83.3 <83.3 <83.3
12/1/2012
5/1/2013
3/25/2014
10/2/2016
3/25/2019 <300 2,550 2,551 2,552
10/17/2019
4/2/2020 <50.0 215 <25.0 <25.0 <25.0 <25.0
11/4/2020 <50.0 392 <25.0 <25.0 <25.0 <25.0
2/8/2022 <9.1 296 4.9 <4.5 <4.5 <4.5
8/10/2022 <83.3 217 <41.7 <41.7 <41.7 <41.7
2/16/2023 54.5 193 <5.0 27.3 6.9 <5.0
8/7/2023 <100 1,300 62 <50.0 <50.0 <50.0
1/8/2024
6/17/2024 <167 555 <83.3 <83.3 <83.3 <83.3
NOTES:
1. μg/L - micrograms per liter
2. ND - Not Detected
bis(2-Ethyhexyl)phthalate
Could Not Locate
0.10' Free product-Bailed during sampling and absorbent socks placed in well
0.21' Free product-Bailed during sampling and absorbent socks placed in well
2,4-Dimethylphenol Naphthalene (EPA 625)Flourene Phenol Phenanthrene
2.5" Free product
3" Free product
2" Free product
Could Not Locate
Could Not Locate
Free product bailed during sampling
7" Free product
MW-1
MW-2
MW-3
0.06' Free product-Absorbent socks placed in well
0.20' Free product-Absorbent socks placed in well
0.80' Free product-Bailed during sampling and absorbent socks placed in well
8" Free product
0.5" Free product
Table 3 Groundwater Quality Data Volatile Organic Compounds Eblen Short Stop #2 Asheville, North Carolina
Monitoring
Well Sample
Date µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l
2L Standard 1 600 70 70 70 600 500 6 70 70 400 400 NE 20 70 NE
GCL 5,000 260,000 5,900 8,800 70,000 80,000 50,000 6,000 26,100 30,500 28,500 24,100 NE 20,000 70,000 NE
3/25/2014 <1 14 ------2 13 ------------<1 ----
10/2/2016 <1 <1 <1 ----<1 <2 ----<1 <1 <1 --<1 ----
3/25/2019
10/17/2019
4/2/2020
11/4/2020
2/8/2022
8/10/2022 <0.50 <0.50 <0.50 ----<0.50 <1.5 <2.0 <0.50 <0.50 6.3 2.3 <0.50 0.86 <0.50 <0.50
2/16/2023 <0.50 <0.50 <0.50 ----<0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 15.1 1.9
8/7/2023 <0.50 <0.50 <0.50 0.83 0.54 <0.50 <1.5 <2.0 <0.50 0 1.9 0.6 <0.50 <0.50 <0.50 <0.50
1/8/2024 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
6/17/2024 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <0.50 0.85 <0.50 <0.50 <0.50 <0.50 <0.50
5/1/2013
3/25/2014
10/2/2016
3/25/2019 7,620 6,530 143 ----2,250 9,730 587 --136 3,090 807 --<25 ----
10/17/2019
4/2/2020
11/4/2020 2,780 694 <20 ----1,700 --<20 ----
2/8/2022
8/10/2022
2/16/2023
8/7/2023
1/8/2024
6/17/2024
10/2/2016 20 1 ------1 5 ----1 6 1 --2 ----
3/25/2019 169 234 <2.5 ----299 2,161 275 --40.6 1,500 348 --52.1 ----
10/17/2019 <12.5 187 <12.5 ----530 6,390 272 <12.5 68.2 1,880 552 --<12.5 ----
4/2/2020 298 1.7 <1.2 ----1.3 6.8 <5.0 1.9 <1.2 1.4 <1.2 --47 ----
11/4/2020 8.2 45.7 <2.0 ----60.2 296.1 123 <2.0 6.7 228 56.7 --<2.0 ----
2/8/2022 <0.50 <0.50 <0.50 ----<0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 ----
8/10/2022 <0.50 <0.50 <0.50 ----<0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 76.3 4.8
2/16/2023 <0.50 <0.50 <0.50 ----<0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
8/7/2023 <0.50 <0.50 <0.50 ----<0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 6.1 <0.50
1/8/2024 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 3.1 <0.50
6/17/2024 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
10/2/2016 <1 <1 <1 ----<1 <2 --<1 <1 <1 --<1 ----
3/25/2019
10/17/2019
4/2/2020
11/4/2020
11/5/2020
8/10/2022 <0.50 <0.50 <0.50 ----<0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 3.4 <0.50
2/16/2023 <0.50 <0.50 0.87 ----<0.50 <1.5 <2.0 <0.50 <0.50 1.0 <0.50 <0.50 <0.50 2.8 <0.50
8/7/2023 <0.50 <0.50 <0.50 ----<0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 6.1 <0.50
1/8/2024 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 2.3 <0.50
6/17/2024 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 4.3 <0.51
Moore Branch 10/2/2016 <1 <1 <1 ----<1 <2 ----<1 <1 <1 --<1 ----
NOTES:
1. μg/L - micrograms per liter
2. ND - Not Detected
3. Monitoring wells MW-1, MW-2, MW-4, and MW-7 were replaced and re-surveyed on June 6-7, 2022
Diisopropyl ether
Could not locate
Could not locate
Could not locate
0.43' Free Product-Bailed during sampling and absorbent socks placed in well
0.30' Free Product-Bailed during sampling and absorbent socks placed in well
0.06' Free Product-Bailed during sampling and absorbent socks placed in well
Could not locate
0.03' Free Product-Bailed during sampling and absorbent socks placed in well
MW-4
Benzene Toluene n-butylbenzene
0.25' Free product
Free product bailed during sampling
1.0" Free Product
Could not locate
Could not locate
0.5' Free product
0.11' Free Product-Bailed during sampling and absorbent socks placed in well
MW-5
sec-butylbenzene
MW-6
MW-7
Chloroform Bromodichloromethanen-Propylbenzene
Could not locate
Could not locate
Ethylbenzene Xylenes Naphthalene (EPA 6200)Isopropylbenzene 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene 1,2,3-Trichloropropane MTBE
Could not locate
Table 4 Groundwater Quality Data Semi-Volatile Organic Compounds Eblen Short Stop #2 Asheville, North Carolina
Monitoring
Well Sample
Date µg/l µg/l µg/l µg/l µg/l µg/l
2L Standard 100 6 300 30 3 200
GCL 100,000 6,000 845 30,000 135 550
10/15/2011
1/18/2012 ------------
12/1/2012
5/1/2013
3/25/2014 ------------
10/2/2016
3/25/2019 15.3 426 427 428
10/17/2019 <10.0 216 <5.0 <5.0
4/2/2020
11/4/2020
2/8/2022
8/10/2022
2/16/2023
8/7/2023
1/8/2024
6/17/2024
12/1/2012
3/25/2014 ------------
10/2/2016 <25 ----------
3/25/2019 <100 217 218 --219
10/17/2019 <10.0 317 6.1 ----6.6
4/2/2020 <50.0 329 <25.0 <25.0 <25.0 <25.0
11/4/2020 <50.0 <25.0 <25.0 <25.0 <25.0 <25.0
2/8/2022 <9.1 49 <4.5 <4.5 <4.5 <4.5
8/10/2022 <45.5 24.2 <22.7 <22.7 <22.7 <22.7
2/16/2023 <10.0 25.4 <5.0 <5.0 <5.0 <5.0
8/7/2023 <8.3 26.0 <4.2 <4.2 <4.2 <4.2
1/8/2024 <10.0 7.0 <5.0 <5.0 <5.0 <5.0
6/17/2024 <167 <83.3 <83.3 <83.3 <83.3 <83.3
12/1/2012
5/1/2013
3/25/2014
10/2/2016
3/25/2019 <300 2,550 2,551 2,552
10/17/2019
4/2/2020 <50.0 215 <25.0 <25.0 <25.0 <25.0
11/4/2020 <50.0 392 <25.0 <25.0 <25.0 <25.0
2/8/2022 <9.1 296 4.9 <4.5 <4.5 <4.5
8/10/2022 <83.3 217 <41.7 <41.7 <41.7 <41.7
2/16/2023 54.5 193 <5.0 27.3 6.9 <5.0
8/7/2023 <100 1,300 62 <50.0 <50.0 <50.0
1/8/2024
6/17/2024 <167 555 <83.3 <83.3 <83.3 <83.3
NOTES:
1. μg/L - micrograms per liter
2. ND - Not Detected
Free product bailed during sampling
7" Free product
MW-1
MW-2
MW-3
0.06' Free product-Absorbent socks placed in well
0.20' Free product-Absorbent socks placed in well
0.80' Free product-Bailed during sampling and absorbent socks placed in well
8" Free product
0.5" Free product
bis(2-Ethyhexyl)phthalate
Could Not Locate
0.10' Free product-Bailed during sampling and absorbent socks placed in well
0.21' Free product-Bailed during sampling and absorbent socks placed in well
2,4-Dimethylphenol Naphthalene (EPA 625)Flourene Phenol Phenanthrene
2.5" Free product
3" Free product
2" Free product
Could Not Locate
Could Not Locate
Table 4 Groundwater Quality Data Semi-Volatile Organic Compounds Eblen Short Stop #2 Asheville, North Carolina
Monitoring
Well Sample
Date µg/l µg/l µg/l µg/l µg/l
2L Standard 100 6 300 30 200
GCL 100,000 6,000 990 30,000 410
3/25/2014 ----------
10/2/2016 ----------
3/25/2019
10/17/2019
4/2/2020
11/4/2020
2/8/2022
8/10/2022 <8.3 <4.2 <4.2 <4.2 <4.2
2/16/2023 <8.3 <4.2 <4.2 <4.2 <4.2
8/7/2023 <10 <5.0 <5.0 <5.0 <5.0
1/8/2024 <8.3 <4.2 <4.2 <4.2 <4.2
6/17/2024 <10 <5.0 <5.0 <5.0 <5.0
5/1/2013
3/25/2014
10/2/2016
3/25/2019 <100 508 509 510
10/17/2019
4/2/2020
11/4/2020 <50.0 820 <25.0 <25.0 <25.0
2/8/2022
8/10/2022
2/16/2023
8/7/2023
1/8/2024
6/17/2024
10/2/2016 ----------
3/25/2019 <100 208 209 --210
10/17/2019 <10.0 195 <5.0 --<5.0
4/2/2020 <10.0 <5.0 <5.0 8.4 <5.0
11/4/2020 <50.0 105 <25.0 <25.0 <25.0
2/8/2022 <9.1 <4.5 <4.5 <4.5 <4.5
8/10/2022 <10 <5.0 <5.0 <5.0 <5.0
2/16/2023 <8.3 <4.2 <4.2 <4.2 <4.2
8/7/2023 <10.0 <5.0 <5.0 <5.0 <5.0
1/8/2024 <8.3 <4.2 <4.2 <4.2 <4.2
6/17/2024 <8.3 <4.2 <4.2 <4.2 <4.2
10/2/2016 ----------
3/25/2019
10/17/2019
4/2/2020
11/4/2020
2/8/2022
8/10/2022 <9.1 <4.5 <4.5 <4.5 <4.5
2/16/2023 <8.3 <4.2 <4.2 <4.2 <4.2
8/7/2023 <8.3 <4.2 <4.2 <4.2 <4.2
1/8/2024 <10 <5.0 <5.0 <5.0 <5.0
6/17/2024 <8.3 <4.2 <4.2 <4.2 <4.2
Moore Branch 10/2/2016 ----------
NOTES:
1. μg/L - micrograms per liter
2. ND - Not Detected
3. Monitoring wells MW-1, MW-2, MW-4, and MW-7 were replaced and re-surveyed on June 6-7, 2022
MW-4
MW-5
MW-6
MW-7
0.5" Free product
0.25" Free product
Free product bailed during sampling
2.8" Free Product
Sheen
Could not locate
1.0" Free Product
0.11'Free product-Bailed during sampling and absorbent socks placed in well
Could not locate
Could not locate
Could not locate
0.30' Free product-Bailed during sampling and absorbent socks placed in well
Could not locate
0.06' Free product-Absorbent socks placed in well
0.43' Free product-Bailed during sampling and absorbent socks placed in well
2,4-Dimethylphenol Naphthalene (EPA 625)Flourene Phenol Phenanthrene
Could not locate
Could not locate
Could not locate
Could not locate
Could not locate
0.03' Free product-Absorbent socks placed in well
Table 5
Groundwater Quality Data MADEP VPH/EPH
Eblen Short Stop #2
Asheville, North Carolina
Monitoring
Well Sample
Date µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l
2L Standard 400 ----700 --10,000 --200
GCL ----------------
10/2/2016
3/25/2019 129,000 112,000 2,150 114,150 54,100 <392 271 271
10/17/2019 21,000 61,000 2,470 63,470 31,100 <240 1,310 32,410
4/2/2020
11/4/2020
2/8/2022
8/10/2022
10/2/2016 NS NS NS NS NS NS NS NS
3/25/2019 95,000 184,000 582 184,582 103,000 <98 218 103,218
10/17/2019 54,800 97,400 45,400 142,800 44,100 <4,900 12,100 56,200
4/2/2020 NS NS NS NS NS NS NS NS
11/4/2020 1,090 3,620 635 4,255 2,740 <100 116 2,856
2/8/2022 5,970 3,620 430 4,050 4,410 120 470 4,880
8/10/2022 7,630 2,340 855 3,195 4,560 <100 930 5,490
10/2/2016
3/25/2019 118,000 231,000 400,000 631,000 116,000 <49,000 35,100 151,100
10/17/2019
4/2/2020 NS NS NS NS NS NS NS NS
11/4/2020 36,600 21,300 55,600 76,900 10,200 <10,000 21,000 31,200
2/8/2022 101,000 29,700 3,900 33,600 12,700 110 1,800 14,500
8/10/2022 210,000 30,000 43,100 73,100 13,700 <2,500 6,090 19,790
NOTES:
1. μg/L - micrograms per liter
2. ND - Not Detected
3. Monitoring wells MW-1, MW-2, MW-4, and MW-7 were replaced and re-surveyed on
June 6-7, 2022
C11-C22 Aromatics TOTAL C9-C22 AromaticsC5-C8 Aliphatics
MW-1
MW-2
C9-C12 Aliphatics C9-C18 Aliphatics Total C9-C18 Aliphatics C9-C10 Aromatics C19-C36 Aliphatics
MW-3
2" Free product
Could not locate
Could not locate
0.10" Free product-Bailed during sampling and absorbent socks placed in well
Free product bailed during sampling
1.6" Free Product
Table 5 Groundwater Quality Data MADEP VPH/EPH Eblen Short Stop #2 Asheville, North Carolina
Monitoring
Well Sample
Date µg/l µg/l µg/l µg/l µg/l µg/l µg/l µg/l
2L Standard 400 ----700 --10,000 --200
GCL ----------------
10/2/2016 NS NS NS NS NS NS NS NS
3/25/2019
10/17/2019
4/2/2020
11/4/2020
2/8/2022
8/10/2022 193 <50 817 817 65.2 <200 <200 65.2
10/2/2016
3/25/2019 47,200 87,700 145,000 232,700 48,100 <19,600 19,400 67,500
10/17/2019
4/2/2020
11/4/2020 5,450 7,830 54,300 62,130 6,170 <10,000 13,800 19,970
2/8/2022
8/10/2022
10/2/2016 53 <50 NS <50 <50 NS NS <50
3/25/2019 1,600 12,500 4,210 16,710 7,740 <490 975 8,715
10/17/2019 15,600 48,400 9,470 57,870 23,000 <962 2,830 25,830
4/2/2020 NS NS NS NS NS NS NS NS
11/4/2020 <100 284 3,720 4,004 430 <400 856 1,286
2/8/2022 <50 <50 <96 <50 <50 <96 <96 <50
8/10/2022 <50 <50 <100 <150 <50 <100 <100 <150
10/2/2016 <50 <50 NS <50 <50 NS NS <50
3/25/2019
10/17/2019
4/2/2020
11/4/2020
2/8/2022
8/10/2022 <50 <50 288 288 <50 <200 <200 <200
Moore Branch 10/2/2016 NS NS NS NS NS NS NS NS
NOTES:
1. μg/L - micrograms per liter
2. ND - Not Detected
3. Monitoring wells MW-1, MW-2, MW-4, and MW-7 were replaced and re-surveyed on
June 6-7, 2022
C11-C22 Aromatics TOTAL C9-C22 Aromatics
Sheen
1.0" Free Product
0.11" Free product-Bailed during sampling and absorbent socks placed in well
Could not locate
Could not locate
Could not locate
Could not locate
2.8" Free Product
C9-C12
Aliphatics
C9-C18
Aliphatics
Total C9-C18
Aliphatics
C9-C10
Aromatics
C19-C36
Aliphatics
C5-C8
Aliphatics
MW-4
MW-5
MW-6
MW-7
Could not locate
Could not locate
Could not locate

Figures
Contour interval 40 feet.
Site
Figure 1
SITE LOCATION MAP
Biltmore Oil-Eblen Short Stop #2
217 Amboy Road Asheville, NC
General location
Figure 2
Site Map
Eblen Short Stop #2
217 Amboy Road
Asheville, NC
MW-5
MW-6
MW-3
MW-1
MW-2
MW-7
State

S
t
.
Joyner Ave.
Amboy Rd.
C-Store
UST
Basin
MW-4
Canopy
Approximate
St
a
t
e

S
t
.
Joyner Ave.
Amboy Rd.
C-Store
UST
Basin
Canopy
Figure 4
Free Product/LNAPL Isoconcentration Contour
Map Eblen Short Stop #2
217 Amboy Road
Asheville, NC
Notes1.Monitoring wells were gauged and sampled on
June 17, 2024.
2.--- - - Free Product/LNAPL Isoconcentration
Contour Line.
3
Figure 4
Groundwater Elevation Map
Eblen Short Stop #2
217 Amboy Road Asheville,
NC
Notes1.Monitoring wells were gauged and sampled on June 17, 2024.
2.Monitoring well MW-3 and MW-6 were not
used to calculate groundwater flow direction.
St
a
t
e

S
t
.
Joyner Ave.
Amboy Rd.
C-Store
UST
Basin
Canopy
MW-1
89.09
MW-2
89.44 MW-7
89.36
MW-3
87.98
MW-4
87.35
MW-5
88.55
MW-6
90.63
89.00
88.50
88.00
87.50
Figure 5
Groundwater Quality Map
Eblen Short Stop #2
217 Amboy Road Asheville, NC
Notes1.Monitoring wells were gauged and sampled on June 17, 2024.2.Analytes listed represent NCDEQ Exceedance.
St
a
t
e

S
t
.
Joyner Ave.
Amboy Rd.
C-Store
UST
Basin
Canopy
MW-10.35’ free product gauged. Absorbent
socks replaced in well.
MW-2Naphthalene (6200)-95.2 ug/l 1,2,3-Trichloropropane-11.6 ug/l 1,2,4-Trimethylbenzene-1,390 ug/l1,3,5-Trimethylbenzene-444 ug/l Total Xylenes-981 ug/l
MW-3Benzene-7,920 ug/lToluene-16,900 ug/l\Ethylbenzene-2,890 ug/lTotal Xylenes-14,330 ug/lNaphthalene (6200)-538 ug/lNaphthalene (625)-555 ug/ln-Propylbenzene-279 ug/lIsopropylbenzene-103 ug/l1,2,4-Trimethylbenzene-2,250 ug/l1,3,5-Trimethylbenzene-509 ug/l
MW-7
No Exceedances
MW-5
0.03’ Free product gauged. Absorbent
socks replaced in well.
MW-4 No Exceedance
MW-6No Exceedances
St
a
t
e

S
t
.
Joyner Ave.
Amboy Rd.
C-Store
UST
Basin
Canopy
Figure 6
BTEX Isoconcentration Contour Map
Eblen Short Stop #2
217 Amboy Road
Asheville, NC
Notes
Monitoring wells were gauged and sampled on June 17, 2024.
(42,040)-BTEX Concentration in ug/l (ppb).
--- - - - BTEX Isoconcentration Contour in ug/l (ppb).
10,000 ug/lLN
A
P
L

100 ug/l
MW-3BTEX-42,040 ug/l
1,000 ug/l
St
a
t
e

S
t
.
Joyner Ave.
Amboy Rd.
C-Store
UST
Basin
Canopy
Figure 7
Naphthalene Isoconcentration
Contour Map
Eblen Short Stop #2
217 Amboy Road
Asheville, NC
Notes
Monitoring wells were gauged and sampled on June 17, 2024.
(538)-Naphthalene Concentration in ug/l (ppb).
--- - - - Naphthalene Isoconcentration Contour in ug/l (ppb).
100 ug/lLN
A
P
L

10 ug/l
1 ug/l

Appendix A

Field Notes

Appendix B

Laboratory Analytical Report

#=CL#
June 21, 2024
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92736862
92736862
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
BOC- Amboy Road
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2024. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
704-977-0942
Enclosures
cc:Brian Bauer, Singleton Environmental
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 38
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 38
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92736862001 MW - 7 EPA 625.1 58 PASI-CICO
SM 6200B 63 PASI-CLMB
92736862002 MW - 2 EPA 625.1 58 PASI-CICO
SM 6200B 63 PASI-CLMB
92736862003 MW - 4 EPA 625.1 58 PASI-CICO
SM 6200B 63 PASI-CLMB
92736862004 MW - 6 EPA 625.1 58 PASI-CICO
SM 6200B 63 PASI-CLMB
92736862005 MW - 3 EPA 625.1 58 PASI-CICO
SM 6200B 63 PASI-CLMB
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 7 Lab ID:92736862001 Collected:06/17/24 09:00 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 06/20/24 03:00 83-32-906/18/24 18:224.2 1
Acenaphthylene ND ug/L 06/20/24 03:00 208-96-806/18/24 18:224.2 1
Anthracene ND ug/L 06/20/24 03:00 120-12-706/18/24 18:224.2 1
Benzo(a)anthracene ND ug/L 06/20/24 03:00 56-55-306/18/24 18:224.2 1
Benzo(a)pyrene ND ug/L 06/20/24 03:00 50-32-806/18/24 18:224.2 1
Benzo(b)fluoranthene ND ug/L 06/20/24 03:00 205-99-206/18/24 18:224.2 1
Benzo(g,h,i)perylene ND ug/L 06/20/24 03:00 191-24-206/18/24 18:224.2 1
Benzo(k)fluoranthene ND ug/L 06/20/24 03:00 207-08-906/18/24 18:224.2 1
4-Bromophenylphenyl ether ND ug/L 06/20/24 03:00 101-55-306/18/24 18:224.2 1
Butylbenzylphthalate ND ug/L 06/20/24 03:00 85-68-706/18/24 18:224.2 1
4-Chloro-3-methylphenol ND ug/L 06/20/24 03:00 59-50-706/18/24 18:224.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/20/24 03:00 111-91-106/18/24 18:228.3 1
bis(2-Chloroethyl) ether ND ug/L 06/20/24 03:00 111-44-406/18/24 18:224.2 1
2-Chloronaphthalene ND ug/L 06/20/24 03:00 91-58-706/18/24 18:224.2 1
2-Chlorophenol ND ug/L 06/20/24 03:00 95-57-806/18/24 18:224.2 1
4-Chlorophenylphenyl ether ND ug/L 06/20/24 03:00 7005-72-306/18/24 18:224.2 1
Chrysene ND ug/L 06/20/24 03:00 218-01-906/18/24 18:224.2 1
Dibenz(a,h)anthracene ND ug/L 06/20/24 03:00 53-70-306/18/24 18:224.2 1
3,3'-Dichlorobenzidine ND ug/L 06/20/24 03:00 91-94-106/18/24 18:228.3 1
2,4-Dichlorophenol ND ug/L 06/20/24 03:00 120-83-206/18/24 18:224.2 1
Diethylphthalate ND ug/L 06/20/24 03:00 84-66-206/18/24 18:224.2 1
2,4-Dimethylphenol ND ug/L 06/20/24 03:00 105-67-906/18/24 18:228.3 1
Dimethylphthalate ND ug/L 06/20/24 03:00 131-11-306/18/24 18:224.2 1
Di-n-butylphthalate ND ug/L 06/20/24 03:00 84-74-206/18/24 18:224.2 1
4,6-Dinitro-2-methylphenol ND ug/L 06/20/24 03:00 534-52-106/18/24 18:228.3 1
2,4-Dinitrophenol ND ug/L 06/20/24 03:00 51-28-506/18/24 18:2241.7 1
2,4-Dinitrotoluene ND ug/L 06/20/24 03:00 121-14-206/18/24 18:224.2 1
2,6-Dinitrotoluene ND ug/L 06/20/24 03:00 606-20-206/18/24 18:224.2 1
Di-n-octylphthalate ND ug/L 06/20/24 03:00 117-84-006/18/24 18:224.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/20/24 03:00 117-81-706/18/24 18:224.2 1
Fluoranthene ND ug/L 06/20/24 03:00 206-44-006/18/24 18:224.2 1
Fluorene ND ug/L 06/20/24 03:00 86-73-706/18/24 18:224.2 1
Hexachloro-1,3-butadiene ND ug/L 06/20/24 03:00 87-68-306/18/24 18:224.2 1
Hexachlorobenzene ND ug/L 06/20/24 03:00 118-74-106/18/24 18:224.2 1
Hexachlorocyclopentadiene ND ug/L 06/20/24 03:00 77-47-406/18/24 18:228.3 1
Hexachloroethane ND ug/L 06/20/24 03:00 67-72-106/18/24 18:224.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/20/24 03:00 193-39-506/18/24 18:224.2 1
Isophorone ND ug/L 06/20/24 03:00 78-59-106/18/24 18:228.3 1
Naphthalene ND ug/L 06/20/24 03:00 91-20-306/18/24 18:224.2 1
Nitrobenzene ND ug/L 06/20/24 03:00 98-95-306/18/24 18:224.2 1
2-Nitrophenol ND ug/L 06/20/24 03:00 88-75-506/18/24 18:224.2 1
4-Nitrophenol ND ug/L 06/20/24 03:00 100-02-706/18/24 18:228.3 1
N-Nitrosodimethylamine ND ug/L 06/20/24 03:00 62-75-906/18/24 18:224.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/20/24 03:00 621-64-706/18/24 18:224.2 1
N-Nitrosodiphenylamine ND ug/L 06/20/24 03:00 86-30-606/18/24 18:228.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/20/24 03:00 108-60-106/18/24 18:224.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 7 Lab ID:92736862001 Collected:06/17/24 09:00 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol ND ug/L 06/20/24 03:00 87-86-506/18/24 18:228.3 1
Phenanthrene ND ug/L 06/20/24 03:00 85-01-806/18/24 18:224.2 1
Phenol ND ug/L 06/20/24 03:00 108-95-206/18/24 18:224.2 1
Pyrene ND ug/L 06/20/24 03:00 129-00-006/18/24 18:224.2 1
1,2,4-Trichlorobenzene ND ug/L 06/20/24 03:00 120-82-106/18/24 18:224.2 1
2,4,6-Trichlorophenol ND ug/L 06/20/24 03:00 88-06-206/18/24 18:228.3 1
Surrogates
Nitrobenzene-d5 (S)104 %06/20/24 03:00 4165-60-006/18/24 18:2210-120 1
2-Fluorobiphenyl (S)81 %06/20/24 03:00 321-60-806/18/24 18:2215-120 1
Terphenyl-d14 (S)119 %06/20/24 03:00 1718-51-006/18/24 18:2211-131 1
Phenol-d6 (S)59 %06/20/24 03:00 13127-88-306/18/24 18:2210-120 1
2-Fluorophenol (S)72 %06/20/24 03:00 367-12-406/18/24 18:2210-120 1
2,4,6-Tribromophenol (S)118 %06/20/24 03:00 118-79-606/18/24 18:2210-137 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/18/24 16:36 71-43-20.50 1
Bromobenzene ND ug/L 06/18/24 16:36 108-86-10.50 1
Bromochloromethane ND ug/L 06/18/24 16:36 74-97-50.50 1
Bromodichloromethane ND ug/L 06/18/24 16:36 75-27-40.50 1
Bromoform ND ug/L 06/18/24 16:36 75-25-20.50 1
Bromomethane ND ug/L 06/18/24 16:36 74-83-95.0 1
n-Butylbenzene ND ug/L 06/18/24 16:36 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/18/24 16:36 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/18/24 16:36 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/18/24 16:36 56-23-50.50 1
Chlorobenzene ND ug/L 06/18/24 16:36 108-90-70.50 1
Chloroethane ND ug/L 06/18/24 16:36 75-00-31.0 1
Chloroform 4.3 ug/L 06/18/24 16:36 67-66-30.50 1
Chloromethane ND ug/L 06/18/24 16:36 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/18/24 16:36 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/18/24 16:36 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/18/24 16:36 96-12-81.0 1
Dibromochloromethane ND ug/L 06/18/24 16:36 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/18/24 16:36 106-93-40.50 1
Dibromomethane ND ug/L 06/18/24 16:36 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/18/24 16:36 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/18/24 16:36 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/18/24 16:36 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/18/24 16:36 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/18/24 16:36 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/18/24 16:36 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/18/24 16:36 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/18/24 16:36 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/18/24 16:36 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/18/24 16:36 78-87-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 7 Lab ID:92736862001 Collected:06/17/24 09:00 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3-Dichloropropane ND ug/L 06/18/24 16:36 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/18/24 16:36 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/18/24 16:36 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/18/24 16:36 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/18/24 16:36 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/18/24 16:36 108-20-30.50 1
Ethylbenzene ND ug/L 06/18/24 16:36 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/18/24 16:36 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/18/24 16:36 98-82-80.50 1
Methylene Chloride ND ug/L 06/18/24 16:36 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/18/24 16:36 1634-04-40.50 1
Naphthalene ND ug/L 06/18/24 16:36 91-20-32.0 1
n-Propylbenzene ND ug/L 06/18/24 16:36 103-65-10.50 1
Styrene ND ug/L 06/18/24 16:36 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/18/24 16:36 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/18/24 16:36 79-34-50.50 1
Tetrachloroethene ND ug/L 06/18/24 16:36 127-18-40.50 1
Toluene ND ug/L 06/18/24 16:36 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/18/24 16:36 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/18/24 16:36 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/18/24 16:36 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/18/24 16:36 79-00-50.50 1
Trichloroethene ND ug/L 06/18/24 16:36 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/18/24 16:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/18/24 16:36 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/18/24 16:36 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/18/24 16:36 108-67-80.50 1
Vinyl chloride ND ug/L 06/18/24 16:36 75-01-41.0 1
m&p-Xylene ND ug/L 06/18/24 16:36 179601-23-11.0 1
o-Xylene ND ug/L 06/18/24 16:36 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %06/18/24 16:36 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %06/18/24 16:36 460-00-470-130 1
Toluene-d8 (S)99 %06/18/24 16:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 2 Lab ID:92736862002 Collected:06/17/24 09:40 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 06/20/24 16:31 83-32-906/18/24 18:2283.3 20
Acenaphthylene ND ug/L 06/20/24 16:31 208-96-806/18/24 18:2283.3 20
Anthracene ND ug/L 06/20/24 16:31 120-12-706/18/24 18:2283.3 20
Benzo(a)anthracene ND ug/L 06/20/24 16:31 56-55-306/18/24 18:2283.3 20
Benzo(a)pyrene ND ug/L 06/20/24 16:31 50-32-806/18/24 18:2283.3 20
Benzo(b)fluoranthene ND ug/L 06/20/24 16:31 205-99-206/18/24 18:2283.3 20
Benzo(g,h,i)perylene ND ug/L 06/20/24 16:31 191-24-206/18/24 18:2283.3 20
Benzo(k)fluoranthene ND ug/L 06/20/24 16:31 207-08-906/18/24 18:2283.3 20
4-Bromophenylphenyl ether ND ug/L 06/20/24 16:31 101-55-306/18/24 18:2283.3 20
Butylbenzylphthalate ND ug/L 06/20/24 16:31 85-68-706/18/24 18:2283.3 20
4-Chloro-3-methylphenol ND ug/L 06/20/24 16:31 59-50-706/18/24 18:2283.3 20
bis(2-Chloroethoxy)methane ND ug/L 06/20/24 16:31 111-91-106/18/24 18:2216720
bis(2-Chloroethyl) ether ND ug/L 06/20/24 16:31 111-44-406/18/24 18:2283.3 20
2-Chloronaphthalene ND ug/L 06/20/24 16:31 91-58-706/18/24 18:2283.3 20
2-Chlorophenol ND ug/L 06/20/24 16:31 95-57-806/18/24 18:2283.3 20
4-Chlorophenylphenyl ether ND ug/L 06/20/24 16:31 7005-72-306/18/24 18:2283.3 20
Chrysene ND ug/L 06/20/24 16:31 218-01-906/18/24 18:2283.3 20
Dibenz(a,h)anthracene ND ug/L 06/20/24 16:31 53-70-306/18/24 18:2283.3 20
3,3'-Dichlorobenzidine ND ug/L 06/20/24 16:31 91-94-106/18/24 18:2216720
2,4-Dichlorophenol ND ug/L 06/20/24 16:31 120-83-206/18/24 18:2283.3 20
Diethylphthalate ND ug/L 06/20/24 16:31 84-66-206/18/24 18:2283.3 20
2,4-Dimethylphenol ND ug/L 06/20/24 16:31 105-67-906/18/24 18:2216720
Dimethylphthalate ND ug/L 06/20/24 16:31 131-11-306/18/24 18:2283.3 20
Di-n-butylphthalate ND ug/L 06/20/24 16:31 84-74-206/18/24 18:2283.3 20
4,6-Dinitro-2-methylphenol ND ug/L 06/20/24 16:31 534-52-106/18/24 18:2216720
2,4-Dinitrophenol ND ug/L 06/20/24 16:31 51-28-506/18/24 18:2283320
2,4-Dinitrotoluene ND ug/L 06/20/24 16:31 121-14-206/18/24 18:2283.3 20
2,6-Dinitrotoluene ND ug/L 06/20/24 16:31 606-20-206/18/24 18:2283.3 20
Di-n-octylphthalate ND ug/L 06/20/24 16:31 117-84-006/18/24 18:2283.3 20
bis(2-Ethylhexyl)phthalate ND ug/L 06/20/24 16:31 117-81-706/18/24 18:2283.3 20
Fluoranthene ND ug/L 06/20/24 16:31 206-44-006/18/24 18:2283.3 20
Fluorene ND ug/L 06/20/24 16:31 86-73-706/18/24 18:2283.3 20
Hexachloro-1,3-butadiene ND ug/L 06/20/24 16:31 87-68-306/18/24 18:2283.3 20
Hexachlorobenzene ND ug/L 06/20/24 16:31 118-74-106/18/24 18:2283.3 20
Hexachlorocyclopentadiene ND ug/L 06/20/24 16:31 77-47-406/18/24 18:2216720
Hexachloroethane ND ug/L 06/20/24 16:31 67-72-106/18/24 18:2283.3 20
Indeno(1,2,3-cd)pyrene ND ug/L 06/20/24 16:31 193-39-506/18/24 18:2283.3 20
Isophorone ND ug/L 06/20/24 16:31 78-59-106/18/24 18:2216720
Naphthalene ND ug/L 06/20/24 16:31 91-20-306/18/24 18:2283.3 20
Nitrobenzene ND ug/L 06/20/24 16:31 98-95-306/18/24 18:2283.3 20
2-Nitrophenol ND ug/L 06/20/24 16:31 88-75-506/18/24 18:2283.3 20
4-Nitrophenol ND ug/L 06/20/24 16:31 100-02-706/18/24 18:2216720
N-Nitrosodimethylamine ND ug/L 06/20/24 16:31 62-75-906/18/24 18:2283.3 20
N-Nitroso-di-n-propylamine ND ug/L 06/20/24 16:31 621-64-706/18/24 18:2283.3 20
N-Nitrosodiphenylamine ND ug/L 06/20/24 16:31 86-30-606/18/24 18:2216720
2,2'-Oxybis(1-chloropropane)ND ug/L 06/20/24 16:31 108-60-106/18/24 18:2283.3 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 2 Lab ID:92736862002 Collected:06/17/24 09:40 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol ND ug/L 06/20/24 16:31 87-86-506/18/24 18:2216720
Phenanthrene ND ug/L 06/20/24 16:31 85-01-806/18/24 18:2283.3 20
Phenol ND ug/L 06/20/24 16:31 108-95-206/18/24 18:2283.3 20
Pyrene ND ug/L 06/20/24 16:31 129-00-006/18/24 18:2283.3 20
1,2,4-Trichlorobenzene ND ug/L 06/20/24 16:31 120-82-106/18/24 18:2283.3 20
2,4,6-Trichlorophenol ND ug/L 06/20/24 16:31 88-06-206/18/24 18:2216720
Surrogates
Nitrobenzene-d5 (S)0 %06/20/24 16:31 4165-60-0 D3,S406/18/24 18:2210-120 20
2-Fluorobiphenyl (S)0 %06/20/24 16:31 321-60-8 S406/18/24 18:2215-120 20
Terphenyl-d14 (S)0 %06/20/24 16:31 1718-51-0 S406/18/24 18:2211-131 20
Phenol-d6 (S)0 %06/20/24 16:31 13127-88-3 S406/18/24 18:2210-120 20
2-Fluorophenol (S)0 %06/20/24 16:31 367-12-4 S406/18/24 18:2210-120 20
2,4,6-Tribromophenol (S)0 %06/20/24 16:31 118-79-6 S406/18/24 18:2210-137 20
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/18/24 19:56 71-43-25.0 10
Bromobenzene ND ug/L 06/18/24 19:56 108-86-15.0 10
Bromochloromethane ND ug/L 06/18/24 19:56 74-97-55.0 10
Bromodichloromethane ND ug/L 06/18/24 19:56 75-27-45.0 10
Bromoform ND ug/L 06/18/24 19:56 75-25-25.0 10
Bromomethane ND ug/L 06/18/24 19:56 74-83-950.0 10
n-Butylbenzene 38.7 ug/L 06/18/24 19:56 104-51-85.0 10
sec-Butylbenzene ND ug/L 06/18/24 19:56 135-98-85.0 10
tert-Butylbenzene ND ug/L 06/18/24 19:56 98-06-65.0 10
Carbon tetrachloride ND ug/L 06/18/24 19:56 56-23-55.0 10
Chlorobenzene ND ug/L 06/18/24 19:56 108-90-75.0 10
Chloroethane ND ug/L 06/18/24 19:56 75-00-310.0 10
Chloroform ND ug/L 06/18/24 19:56 67-66-35.0 10
Chloromethane ND ug/L 06/18/24 19:56 74-87-310.0 10
2-Chlorotoluene ND ug/L 06/18/24 19:56 95-49-85.0 10
4-Chlorotoluene ND ug/L 06/18/24 19:56 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 06/18/24 19:56 96-12-810.0 10
Dibromochloromethane ND ug/L 06/18/24 19:56 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 06/18/24 19:56 106-93-45.0 10
Dibromomethane ND ug/L 06/18/24 19:56 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 06/18/24 19:56 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 06/18/24 19:56 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 06/18/24 19:56 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 06/18/24 19:56 75-71-85.0 10
1,1-Dichloroethane ND ug/L 06/18/24 19:56 75-34-35.0 10
1,2-Dichloroethane ND ug/L 06/18/24 19:56 107-06-25.0 10
1,1-Dichloroethene ND ug/L 06/18/24 19:56 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 06/18/24 19:56 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 06/18/24 19:56 156-60-55.0 10
1,2-Dichloropropane ND ug/L 06/18/24 19:56 78-87-55.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 2 Lab ID:92736862002 Collected:06/17/24 09:40 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3-Dichloropropane ND ug/L 06/18/24 19:56 142-28-95.0 10
2,2-Dichloropropane ND ug/L 06/18/24 19:56 594-20-75.0 10
1,1-Dichloropropene ND ug/L 06/18/24 19:56 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 06/18/24 19:56 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 06/18/24 19:56 10061-02-65.0 10
Diisopropyl ether ND ug/L 06/18/24 19:56 108-20-35.0 10
Ethylbenzene 32.4 ug/L 06/18/24 19:56 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 06/18/24 19:56 87-68-320.0 10
Isopropylbenzene (Cumene)29.0 ug/L 06/18/24 19:56 98-82-85.0 10
Methylene Chloride ND ug/L 06/18/24 19:56 75-09-220.0 10
Methyl-tert-butyl ether ND ug/L 06/18/24 19:56 1634-04-45.0 10
Naphthalene 95.2 ug/L 06/18/24 19:56 91-20-320.0 10
n-Propylbenzene 51.6 ug/L 06/18/24 19:56 103-65-15.0 10
Styrene ND ug/L 06/18/24 19:56 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 06/18/24 19:56 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 06/18/24 19:56 79-34-55.0 10
Tetrachloroethene ND ug/L 06/18/24 19:56 127-18-45.0 10
Toluene ND ug/L 06/18/24 19:56 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 06/18/24 19:56 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 06/18/24 19:56 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 06/18/24 19:56 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 06/18/24 19:56 79-00-55.0 10
Trichloroethene ND ug/L 06/18/24 19:56 79-01-65.0 10
Trichlorofluoromethane ND ug/L 06/18/24 19:56 75-69-410.0 10
1,2,3-Trichloropropane 11.6 ug/L 06/18/24 19:56 96-18-45.0 10
1,2,4-Trimethylbenzene 1390 ug/L 06/18/24 19:56 95-63-65.0 10
1,3,5-Trimethylbenzene 444 ug/L 06/18/24 19:56 108-67-85.0 10
Vinyl chloride ND ug/L 06/18/24 19:56 75-01-410.0 10
m&p-Xylene 557 ug/L 06/18/24 19:56 179601-23-110.0 10
o-Xylene 424 ug/L 06/18/24 19:56 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)95 %06/18/24 19:56 17060-07-070-130 10
4-Bromofluorobenzene (S)99 %06/18/24 19:56 460-00-470-130 10
Toluene-d8 (S)99 %06/18/24 19:56 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 4 Lab ID:92736862003 Collected:06/17/24 10:15 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 06/20/24 03:50 83-32-906/18/24 18:225.0 1
Acenaphthylene ND ug/L 06/20/24 03:50 208-96-806/18/24 18:225.0 1
Anthracene ND ug/L 06/20/24 03:50 120-12-706/18/24 18:225.0 1
Benzo(a)anthracene ND ug/L 06/20/24 03:50 56-55-306/18/24 18:225.0 1
Benzo(a)pyrene ND ug/L 06/20/24 03:50 50-32-806/18/24 18:225.0 1
Benzo(b)fluoranthene ND ug/L 06/20/24 03:50 205-99-206/18/24 18:225.0 1
Benzo(g,h,i)perylene ND ug/L 06/20/24 03:50 191-24-206/18/24 18:225.0 1
Benzo(k)fluoranthene ND ug/L 06/20/24 03:50 207-08-906/18/24 18:225.0 1
4-Bromophenylphenyl ether ND ug/L 06/20/24 03:50 101-55-306/18/24 18:225.0 1
Butylbenzylphthalate ND ug/L 06/20/24 03:50 85-68-706/18/24 18:225.0 1
4-Chloro-3-methylphenol ND ug/L 06/20/24 03:50 59-50-706/18/24 18:225.0 1
bis(2-Chloroethoxy)methane ND ug/L 06/20/24 03:50 111-91-106/18/24 18:2210.0 1
bis(2-Chloroethyl) ether ND ug/L 06/20/24 03:50 111-44-406/18/24 18:225.0 1
2-Chloronaphthalene ND ug/L 06/20/24 03:50 91-58-706/18/24 18:225.0 1
2-Chlorophenol ND ug/L 06/20/24 03:50 95-57-806/18/24 18:225.0 1
4-Chlorophenylphenyl ether ND ug/L 06/20/24 03:50 7005-72-306/18/24 18:225.0 1
Chrysene ND ug/L 06/20/24 03:50 218-01-906/18/24 18:225.0 1
Dibenz(a,h)anthracene ND ug/L 06/20/24 03:50 53-70-306/18/24 18:225.0 1
3,3'-Dichlorobenzidine ND ug/L 06/20/24 03:50 91-94-106/18/24 18:2210.0 1
2,4-Dichlorophenol ND ug/L 06/20/24 03:50 120-83-206/18/24 18:225.0 1
Diethylphthalate ND ug/L 06/20/24 03:50 84-66-206/18/24 18:225.0 1
2,4-Dimethylphenol ND ug/L 06/20/24 03:50 105-67-906/18/24 18:2210.0 1
Dimethylphthalate ND ug/L 06/20/24 03:50 131-11-306/18/24 18:225.0 1
Di-n-butylphthalate ND ug/L 06/20/24 03:50 84-74-206/18/24 18:225.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/20/24 03:50 534-52-106/18/24 18:2210.0 1
2,4-Dinitrophenol ND ug/L 06/20/24 03:50 51-28-506/18/24 18:2250.0 1
2,4-Dinitrotoluene ND ug/L 06/20/24 03:50 121-14-206/18/24 18:225.0 1
2,6-Dinitrotoluene ND ug/L 06/20/24 03:50 606-20-206/18/24 18:225.0 1
Di-n-octylphthalate ND ug/L 06/20/24 03:50 117-84-006/18/24 18:225.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/20/24 03:50 117-81-706/18/24 18:225.0 1
Fluoranthene ND ug/L 06/20/24 03:50 206-44-006/18/24 18:225.0 1
Fluorene ND ug/L 06/20/24 03:50 86-73-706/18/24 18:225.0 1
Hexachloro-1,3-butadiene ND ug/L 06/20/24 03:50 87-68-306/18/24 18:225.0 1
Hexachlorobenzene ND ug/L 06/20/24 03:50 118-74-106/18/24 18:225.0 1
Hexachlorocyclopentadiene ND ug/L 06/20/24 03:50 77-47-406/18/24 18:2210.0 1
Hexachloroethane ND ug/L 06/20/24 03:50 67-72-106/18/24 18:225.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/20/24 03:50 193-39-506/18/24 18:225.0 1
Isophorone ND ug/L 06/20/24 03:50 78-59-106/18/24 18:2210.0 1
Naphthalene ND ug/L 06/20/24 03:50 91-20-306/18/24 18:225.0 1
Nitrobenzene ND ug/L 06/20/24 03:50 98-95-306/18/24 18:225.0 1
2-Nitrophenol ND ug/L 06/20/24 03:50 88-75-506/18/24 18:225.0 1
4-Nitrophenol ND ug/L 06/20/24 03:50 100-02-706/18/24 18:2210.0 1
N-Nitrosodimethylamine ND ug/L 06/20/24 03:50 62-75-906/18/24 18:225.0 1
N-Nitroso-di-n-propylamine ND ug/L 06/20/24 03:50 621-64-706/18/24 18:225.0 1
N-Nitrosodiphenylamine ND ug/L 06/20/24 03:50 86-30-606/18/24 18:2210.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/20/24 03:50 108-60-106/18/24 18:225.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 4 Lab ID:92736862003 Collected:06/17/24 10:15 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol ND ug/L 06/20/24 03:50 87-86-506/18/24 18:2210.0 1
Phenanthrene ND ug/L 06/20/24 03:50 85-01-806/18/24 18:225.0 1
Phenol ND ug/L 06/20/24 03:50 108-95-206/18/24 18:225.0 1
Pyrene ND ug/L 06/20/24 03:50 129-00-006/18/24 18:225.0 1
1,2,4-Trichlorobenzene ND ug/L 06/20/24 03:50 120-82-106/18/24 18:225.0 1
2,4,6-Trichlorophenol ND ug/L 06/20/24 03:50 88-06-206/18/24 18:2210.0 1
Surrogates
Nitrobenzene-d5 (S)92 %06/20/24 03:50 4165-60-006/18/24 18:2210-120 1
2-Fluorobiphenyl (S)78 %06/20/24 03:50 321-60-806/18/24 18:2215-120 1
Terphenyl-d14 (S)124 %06/20/24 03:50 1718-51-006/18/24 18:2211-131 1
Phenol-d6 (S)28 %06/20/24 03:50 13127-88-306/18/24 18:2210-120 1
2-Fluorophenol (S)7 %06/20/24 03:50 367-12-4 S006/18/24 18:2210-120 1
2,4,6-Tribromophenol (S)10 %06/20/24 03:50 118-79-606/18/24 18:2210-137 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/18/24 16:54 71-43-20.50 1
Bromobenzene ND ug/L 06/18/24 16:54 108-86-10.50 1
Bromochloromethane ND ug/L 06/18/24 16:54 74-97-50.50 1
Bromodichloromethane ND ug/L 06/18/24 16:54 75-27-40.50 1
Bromoform ND ug/L 06/18/24 16:54 75-25-20.50 1
Bromomethane ND ug/L 06/18/24 16:54 74-83-95.0 1
n-Butylbenzene ND ug/L 06/18/24 16:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/18/24 16:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/18/24 16:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/18/24 16:54 56-23-50.50 1
Chlorobenzene ND ug/L 06/18/24 16:54 108-90-70.50 1
Chloroethane ND ug/L 06/18/24 16:54 75-00-31.0 1
Chloroform ND ug/L 06/18/24 16:54 67-66-30.50 1
Chloromethane ND ug/L 06/18/24 16:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/18/24 16:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/18/24 16:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/18/24 16:54 96-12-81.0 1
Dibromochloromethane ND ug/L 06/18/24 16:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/18/24 16:54 106-93-40.50 1
Dibromomethane ND ug/L 06/18/24 16:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/18/24 16:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/18/24 16:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/18/24 16:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/18/24 16:54 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/18/24 16:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/18/24 16:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/18/24 16:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/18/24 16:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/18/24 16:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/18/24 16:54 78-87-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 4 Lab ID:92736862003 Collected:06/17/24 10:15 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3-Dichloropropane ND ug/L 06/18/24 16:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/18/24 16:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/18/24 16:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/18/24 16:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/18/24 16:54 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/18/24 16:54 108-20-30.50 1
Ethylbenzene ND ug/L 06/18/24 16:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/18/24 16:54 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/18/24 16:54 98-82-80.50 1
Methylene Chloride ND ug/L 06/18/24 16:54 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/18/24 16:54 1634-04-40.50 1
Naphthalene ND ug/L 06/18/24 16:54 91-20-32.0 1
n-Propylbenzene ND ug/L 06/18/24 16:54 103-65-10.50 1
Styrene ND ug/L 06/18/24 16:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/18/24 16:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/18/24 16:54 79-34-50.50 1
Tetrachloroethene ND ug/L 06/18/24 16:54 127-18-40.50 1
Toluene ND ug/L 06/18/24 16:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/18/24 16:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/18/24 16:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/18/24 16:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/18/24 16:54 79-00-50.50 1
Trichloroethene ND ug/L 06/18/24 16:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/18/24 16:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/18/24 16:54 96-18-40.50 1
1,2,4-Trimethylbenzene 0.85 ug/L 06/18/24 16:54 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/18/24 16:54 108-67-80.50 1
Vinyl chloride ND ug/L 06/18/24 16:54 75-01-41.0 1
m&p-Xylene ND ug/L 06/18/24 16:54 179601-23-11.0 1
o-Xylene ND ug/L 06/18/24 16:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %06/18/24 16:54 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/18/24 16:54 460-00-470-130 1
Toluene-d8 (S)99 %06/18/24 16:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 6 Lab ID:92736862004 Collected:06/17/24 10:45 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 06/20/24 04:15 83-32-906/18/24 18:224.2 1
Acenaphthylene ND ug/L 06/20/24 04:15 208-96-806/18/24 18:224.2 1
Anthracene ND ug/L 06/20/24 04:15 120-12-706/18/24 18:224.2 1
Benzo(a)anthracene ND ug/L 06/20/24 04:15 56-55-306/18/24 18:224.2 1
Benzo(a)pyrene ND ug/L 06/20/24 04:15 50-32-806/18/24 18:224.2 1
Benzo(b)fluoranthene ND ug/L 06/20/24 04:15 205-99-206/18/24 18:224.2 1
Benzo(g,h,i)perylene ND ug/L 06/20/24 04:15 191-24-206/18/24 18:224.2 1
Benzo(k)fluoranthene ND ug/L 06/20/24 04:15 207-08-906/18/24 18:224.2 1
4-Bromophenylphenyl ether ND ug/L 06/20/24 04:15 101-55-306/18/24 18:224.2 1
Butylbenzylphthalate ND ug/L 06/20/24 04:15 85-68-706/18/24 18:224.2 1
4-Chloro-3-methylphenol ND ug/L 06/20/24 04:15 59-50-706/18/24 18:224.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/20/24 04:15 111-91-106/18/24 18:228.3 1
bis(2-Chloroethyl) ether ND ug/L 06/20/24 04:15 111-44-406/18/24 18:224.2 1
2-Chloronaphthalene ND ug/L 06/20/24 04:15 91-58-706/18/24 18:224.2 1
2-Chlorophenol ND ug/L 06/20/24 04:15 95-57-806/18/24 18:224.2 1
4-Chlorophenylphenyl ether ND ug/L 06/20/24 04:15 7005-72-306/18/24 18:224.2 1
Chrysene ND ug/L 06/20/24 04:15 218-01-906/18/24 18:224.2 1
Dibenz(a,h)anthracene ND ug/L 06/20/24 04:15 53-70-306/18/24 18:224.2 1
3,3'-Dichlorobenzidine ND ug/L 06/20/24 04:15 91-94-106/18/24 18:228.3 1
2,4-Dichlorophenol ND ug/L 06/20/24 04:15 120-83-206/18/24 18:224.2 1
Diethylphthalate ND ug/L 06/20/24 04:15 84-66-206/18/24 18:224.2 1
2,4-Dimethylphenol ND ug/L 06/20/24 04:15 105-67-906/18/24 18:228.3 1
Dimethylphthalate ND ug/L 06/20/24 04:15 131-11-306/18/24 18:224.2 1
Di-n-butylphthalate ND ug/L 06/20/24 04:15 84-74-206/18/24 18:224.2 1
4,6-Dinitro-2-methylphenol ND ug/L 06/20/24 04:15 534-52-106/18/24 18:228.3 1
2,4-Dinitrophenol ND ug/L 06/20/24 04:15 51-28-506/18/24 18:2241.7 1
2,4-Dinitrotoluene ND ug/L 06/20/24 04:15 121-14-206/18/24 18:224.2 1
2,6-Dinitrotoluene ND ug/L 06/20/24 04:15 606-20-206/18/24 18:224.2 1
Di-n-octylphthalate ND ug/L 06/20/24 04:15 117-84-006/18/24 18:224.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/20/24 04:15 117-81-706/18/24 18:224.2 1
Fluoranthene ND ug/L 06/20/24 04:15 206-44-006/18/24 18:224.2 1
Fluorene ND ug/L 06/20/24 04:15 86-73-706/18/24 18:224.2 1
Hexachloro-1,3-butadiene ND ug/L 06/20/24 04:15 87-68-306/18/24 18:224.2 1
Hexachlorobenzene ND ug/L 06/20/24 04:15 118-74-106/18/24 18:224.2 1
Hexachlorocyclopentadiene ND ug/L 06/20/24 04:15 77-47-406/18/24 18:228.3 1
Hexachloroethane ND ug/L 06/20/24 04:15 67-72-106/18/24 18:224.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/20/24 04:15 193-39-506/18/24 18:224.2 1
Isophorone ND ug/L 06/20/24 04:15 78-59-106/18/24 18:228.3 1
Naphthalene ND ug/L 06/20/24 04:15 91-20-306/18/24 18:224.2 1
Nitrobenzene ND ug/L 06/20/24 04:15 98-95-306/18/24 18:224.2 1
2-Nitrophenol ND ug/L 06/20/24 04:15 88-75-506/18/24 18:224.2 1
4-Nitrophenol ND ug/L 06/20/24 04:15 100-02-706/18/24 18:228.3 1
N-Nitrosodimethylamine ND ug/L 06/20/24 04:15 62-75-906/18/24 18:224.2 1
N-Nitroso-di-n-propylamine ND ug/L 06/20/24 04:15 621-64-706/18/24 18:224.2 1
N-Nitrosodiphenylamine ND ug/L 06/20/24 04:15 86-30-606/18/24 18:228.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/20/24 04:15 108-60-106/18/24 18:224.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 6 Lab ID:92736862004 Collected:06/17/24 10:45 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol ND ug/L 06/20/24 04:15 87-86-506/18/24 18:228.3 1
Phenanthrene ND ug/L 06/20/24 04:15 85-01-806/18/24 18:224.2 1
Phenol ND ug/L 06/20/24 04:15 108-95-206/18/24 18:224.2 1
Pyrene ND ug/L 06/20/24 04:15 129-00-006/18/24 18:224.2 1
1,2,4-Trichlorobenzene ND ug/L 06/20/24 04:15 120-82-106/18/24 18:224.2 1
2,4,6-Trichlorophenol ND ug/L 06/20/24 04:15 88-06-206/18/24 18:228.3 1
Surrogates
Nitrobenzene-d5 (S)118 %06/20/24 04:15 4165-60-006/18/24 18:2210-120 1
2-Fluorobiphenyl (S)107 %06/20/24 04:15 321-60-806/18/24 18:2215-120 1
Terphenyl-d14 (S)120 %06/20/24 04:15 1718-51-006/18/24 18:2211-131 1
Phenol-d6 (S)56 %06/20/24 04:15 13127-88-306/18/24 18:2210-120 1
2-Fluorophenol (S)40 %06/20/24 04:15 367-12-406/18/24 18:2210-120 1
2,4,6-Tribromophenol (S)52 %06/20/24 04:15 118-79-606/18/24 18:2210-137 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/18/24 17:12 71-43-20.50 1
Bromobenzene ND ug/L 06/18/24 17:12 108-86-10.50 1
Bromochloromethane ND ug/L 06/18/24 17:12 74-97-50.50 1
Bromodichloromethane ND ug/L 06/18/24 17:12 75-27-40.50 1
Bromoform ND ug/L 06/18/24 17:12 75-25-20.50 1
Bromomethane ND ug/L 06/18/24 17:12 74-83-95.0 1
n-Butylbenzene ND ug/L 06/18/24 17:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/18/24 17:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/18/24 17:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/18/24 17:12 56-23-50.50 1
Chlorobenzene ND ug/L 06/18/24 17:12 108-90-70.50 1
Chloroethane ND ug/L 06/18/24 17:12 75-00-31.0 1
Chloroform ND ug/L 06/18/24 17:12 67-66-30.50 1
Chloromethane ND ug/L 06/18/24 17:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/18/24 17:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/18/24 17:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/18/24 17:12 96-12-81.0 1
Dibromochloromethane ND ug/L 06/18/24 17:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/18/24 17:12 106-93-40.50 1
Dibromomethane ND ug/L 06/18/24 17:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/18/24 17:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/18/24 17:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/18/24 17:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/18/24 17:12 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/18/24 17:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/18/24 17:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/18/24 17:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/18/24 17:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/18/24 17:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/18/24 17:12 78-87-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 6 Lab ID:92736862004 Collected:06/17/24 10:45 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3-Dichloropropane ND ug/L 06/18/24 17:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/18/24 17:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/18/24 17:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/18/24 17:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/18/24 17:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/18/24 17:12 108-20-30.50 1
Ethylbenzene ND ug/L 06/18/24 17:12 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/18/24 17:12 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/18/24 17:12 98-82-80.50 1
Methylene Chloride ND ug/L 06/18/24 17:12 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/18/24 17:12 1634-04-40.50 1
Naphthalene ND ug/L 06/18/24 17:12 91-20-32.0 1
n-Propylbenzene ND ug/L 06/18/24 17:12 103-65-10.50 1
Styrene ND ug/L 06/18/24 17:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/18/24 17:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/18/24 17:12 79-34-50.50 1
Tetrachloroethene ND ug/L 06/18/24 17:12 127-18-40.50 1
Toluene ND ug/L 06/18/24 17:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/18/24 17:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/18/24 17:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/18/24 17:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/18/24 17:12 79-00-50.50 1
Trichloroethene ND ug/L 06/18/24 17:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/18/24 17:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/18/24 17:12 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/18/24 17:12 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/18/24 17:12 108-67-80.50 1
Vinyl chloride ND ug/L 06/18/24 17:12 75-01-41.0 1
m&p-Xylene ND ug/L 06/18/24 17:12 179601-23-11.0 1
o-Xylene ND ug/L 06/18/24 17:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %06/18/24 17:12 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %06/18/24 17:12 460-00-470-130 1
Toluene-d8 (S)99 %06/18/24 17:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 3 Lab ID:92736862005 Collected:06/17/24 11:15 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 06/20/24 16:57 83-32-906/18/24 18:2283.3 20
Acenaphthylene ND ug/L 06/20/24 16:57 208-96-806/18/24 18:2283.3 20
Anthracene ND ug/L 06/20/24 16:57 120-12-706/18/24 18:2283.3 20
Benzo(a)anthracene ND ug/L 06/20/24 16:57 56-55-306/18/24 18:2283.3 20
Benzo(a)pyrene ND ug/L 06/20/24 16:57 50-32-806/18/24 18:2283.3 20
Benzo(b)fluoranthene ND ug/L 06/20/24 16:57 205-99-206/18/24 18:2283.3 20
Benzo(g,h,i)perylene ND ug/L 06/20/24 16:57 191-24-206/18/24 18:2283.3 20
Benzo(k)fluoranthene ND ug/L 06/20/24 16:57 207-08-906/18/24 18:2283.3 20
4-Bromophenylphenyl ether ND ug/L 06/20/24 16:57 101-55-306/18/24 18:2283.3 20
Butylbenzylphthalate ND ug/L 06/20/24 16:57 85-68-706/18/24 18:2283.3 20
4-Chloro-3-methylphenol ND ug/L 06/20/24 16:57 59-50-706/18/24 18:2283.3 20
bis(2-Chloroethoxy)methane ND ug/L 06/20/24 16:57 111-91-106/18/24 18:2216720
bis(2-Chloroethyl) ether ND ug/L 06/20/24 16:57 111-44-406/18/24 18:2283.3 20
2-Chloronaphthalene ND ug/L 06/20/24 16:57 91-58-706/18/24 18:2283.3 20
2-Chlorophenol ND ug/L 06/20/24 16:57 95-57-806/18/24 18:2283.3 20
4-Chlorophenylphenyl ether ND ug/L 06/20/24 16:57 7005-72-306/18/24 18:2283.3 20
Chrysene ND ug/L 06/20/24 16:57 218-01-906/18/24 18:2283.3 20
Dibenz(a,h)anthracene ND ug/L 06/20/24 16:57 53-70-306/18/24 18:2283.3 20
3,3'-Dichlorobenzidine ND ug/L 06/20/24 16:57 91-94-106/18/24 18:2216720
2,4-Dichlorophenol ND ug/L 06/20/24 16:57 120-83-206/18/24 18:2283.3 20
Diethylphthalate ND ug/L 06/20/24 16:57 84-66-206/18/24 18:2283.3 20
2,4-Dimethylphenol ND ug/L 06/20/24 16:57 105-67-906/18/24 18:2216720
Dimethylphthalate ND ug/L 06/20/24 16:57 131-11-306/18/24 18:2283.3 20
Di-n-butylphthalate ND ug/L 06/20/24 16:57 84-74-206/18/24 18:2283.3 20
4,6-Dinitro-2-methylphenol ND ug/L 06/20/24 16:57 534-52-106/18/24 18:2216720
2,4-Dinitrophenol ND ug/L 06/20/24 16:57 51-28-506/18/24 18:2283320
2,4-Dinitrotoluene ND ug/L 06/20/24 16:57 121-14-206/18/24 18:2283.3 20
2,6-Dinitrotoluene ND ug/L 06/20/24 16:57 606-20-206/18/24 18:2283.3 20
Di-n-octylphthalate ND ug/L 06/20/24 16:57 117-84-006/18/24 18:2283.3 20
bis(2-Ethylhexyl)phthalate ND ug/L 06/20/24 16:57 117-81-706/18/24 18:2283.3 20
Fluoranthene ND ug/L 06/20/24 16:57 206-44-006/18/24 18:2283.3 20
Fluorene ND ug/L 06/20/24 16:57 86-73-706/18/24 18:2283.3 20
Hexachloro-1,3-butadiene ND ug/L 06/20/24 16:57 87-68-306/18/24 18:2283.3 20
Hexachlorobenzene ND ug/L 06/20/24 16:57 118-74-106/18/24 18:2283.3 20
Hexachlorocyclopentadiene ND ug/L 06/20/24 16:57 77-47-406/18/24 18:2216720
Hexachloroethane ND ug/L 06/20/24 16:57 67-72-106/18/24 18:2283.3 20
Indeno(1,2,3-cd)pyrene ND ug/L 06/20/24 16:57 193-39-506/18/24 18:2283.3 20
Isophorone ND ug/L 06/20/24 16:57 78-59-106/18/24 18:2216720
Naphthalene 555 ug/L 06/20/24 16:57 91-20-306/18/24 18:2283.3 20
Nitrobenzene ND ug/L 06/20/24 16:57 98-95-306/18/24 18:2283.3 20
2-Nitrophenol ND ug/L 06/20/24 16:57 88-75-506/18/24 18:2283.3 20
4-Nitrophenol ND ug/L 06/20/24 16:57 100-02-706/18/24 18:2216720
N-Nitrosodimethylamine ND ug/L 06/20/24 16:57 62-75-906/18/24 18:2283.3 20
N-Nitroso-di-n-propylamine ND ug/L 06/20/24 16:57 621-64-706/18/24 18:2283.3 20
N-Nitrosodiphenylamine ND ug/L 06/20/24 16:57 86-30-606/18/24 18:2216720
2,2'-Oxybis(1-chloropropane)ND ug/L 06/20/24 16:57 108-60-106/18/24 18:2283.3 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 3 Lab ID:92736862005 Collected:06/17/24 11:15 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol ND ug/L 06/20/24 16:57 87-86-506/18/24 18:2216720
Phenanthrene ND ug/L 06/20/24 16:57 85-01-806/18/24 18:2283.3 20
Phenol ND ug/L 06/20/24 16:57 108-95-206/18/24 18:2283.3 20
Pyrene ND ug/L 06/20/24 16:57 129-00-006/18/24 18:2283.3 20
1,2,4-Trichlorobenzene ND ug/L 06/20/24 16:57 120-82-106/18/24 18:2283.3 20
2,4,6-Trichlorophenol ND ug/L 06/20/24 16:57 88-06-206/18/24 18:2216720
Surrogates
Nitrobenzene-d5 (S)0 %06/20/24 16:57 4165-60-0 D3,S406/18/24 18:2210-120 20
2-Fluorobiphenyl (S)0 %06/20/24 16:57 321-60-8 S406/18/24 18:2215-120 20
Terphenyl-d14 (S)0 %06/20/24 16:57 1718-51-0 S406/18/24 18:2211-131 20
Phenol-d6 (S)0 %06/20/24 16:57 13127-88-3 S406/18/24 18:2210-120 20
2-Fluorophenol (S)0 %06/20/24 16:57 367-12-4 S406/18/24 18:2210-120 20
2,4,6-Tribromophenol (S)0 %06/20/24 16:57 118-79-6 S406/18/24 18:2210-137 20
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 7920 ug/L 06/19/24 16:01 71-43-262.5 125
Bromobenzene ND ug/L 06/19/24 16:01 108-86-162.5 125
Bromochloromethane ND ug/L 06/19/24 16:01 74-97-562.5 125
Bromodichloromethane ND ug/L 06/19/24 16:01 75-27-462.5 125
Bromoform ND ug/L 06/19/24 16:01 75-25-262.5 125
Bromomethane ND ug/L 06/19/24 16:01 74-83-9625125
n-Butylbenzene ND ug/L 06/19/24 16:01 104-51-862.5 125
sec-Butylbenzene ND ug/L 06/19/24 16:01 135-98-862.5 125
tert-Butylbenzene ND ug/L 06/19/24 16:01 98-06-662.5 125
Carbon tetrachloride ND ug/L 06/19/24 16:01 56-23-562.5 125
Chlorobenzene ND ug/L 06/19/24 16:01 108-90-762.5 125
Chloroethane ND ug/L 06/19/24 16:01 75-00-3125125
Chloroform ND ug/L 06/19/24 16:01 67-66-362.5 125
Chloromethane ND ug/L 06/19/24 16:01 74-87-3125125
2-Chlorotoluene ND ug/L 06/19/24 16:01 95-49-862.5 125
4-Chlorotoluene ND ug/L 06/19/24 16:01 106-43-462.5 125
1,2-Dibromo-3-chloropropane ND ug/L 06/19/24 16:01 96-12-8125125
Dibromochloromethane ND ug/L 06/19/24 16:01 124-48-162.5 125
1,2-Dibromoethane (EDB)ND ug/L 06/19/24 16:01 106-93-462.5 125
Dibromomethane ND ug/L 06/19/24 16:01 74-95-362.5 125
1,2-Dichlorobenzene ND ug/L 06/19/24 16:01 95-50-162.5 125
1,3-Dichlorobenzene ND ug/L 06/19/24 16:01 541-73-162.5 125
1,4-Dichlorobenzene ND ug/L 06/19/24 16:01 106-46-762.5 125
Dichlorodifluoromethane ND ug/L 06/19/24 16:01 75-71-862.5 125
1,1-Dichloroethane ND ug/L 06/19/24 16:01 75-34-362.5 125
1,2-Dichloroethane ND ug/L 06/19/24 16:01 107-06-262.5 125
1,1-Dichloroethene ND ug/L 06/19/24 16:01 75-35-462.5 125
cis-1,2-Dichloroethene ND ug/L 06/19/24 16:01 156-59-262.5 125
trans-1,2-Dichloroethene ND ug/L 06/19/24 16:01 156-60-562.5 125
1,2-Dichloropropane ND ug/L 06/19/24 16:01 78-87-562.5 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Sample:MW - 3 Lab ID:92736862005 Collected:06/17/24 11:15 Received:06/17/24 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,3-Dichloropropane ND ug/L 06/19/24 16:01 142-28-962.5 125
2,2-Dichloropropane ND ug/L 06/19/24 16:01 594-20-762.5 125
1,1-Dichloropropene ND ug/L 06/19/24 16:01 563-58-662.5 125
cis-1,3-Dichloropropene ND ug/L 06/19/24 16:01 10061-01-562.5 125
trans-1,3-Dichloropropene ND ug/L 06/19/24 16:01 10061-02-662.5 125
Diisopropyl ether ND ug/L 06/19/24 16:01 108-20-362.5 125
Ethylbenzene 2890 ug/L 06/19/24 16:01 100-41-462.5 125
Hexachloro-1,3-butadiene ND ug/L 06/19/24 16:01 87-68-3250125
Isopropylbenzene (Cumene)103 ug/L 06/19/24 16:01 98-82-862.5 125
Methylene Chloride ND ug/L 06/19/24 16:01 75-09-2250125
Methyl-tert-butyl ether ND ug/L 06/19/24 16:01 1634-04-462.5 125
Naphthalene 538 ug/L 06/19/24 16:01 91-20-3250125
n-Propylbenzene 279 ug/L 06/19/24 16:01 103-65-162.5 125
Styrene ND ug/L 06/19/24 16:01 100-42-562.5 125
1,1,1,2-Tetrachloroethane ND ug/L 06/19/24 16:01 630-20-662.5 125
1,1,2,2-Tetrachloroethane ND ug/L 06/19/24 16:01 79-34-562.5 125
Tetrachloroethene ND ug/L 06/19/24 16:01 127-18-462.5 125
Toluene 16900 ug/L 06/19/24 16:01 108-88-362.5 125
1,2,3-Trichlorobenzene ND ug/L 06/19/24 16:01 87-61-6250125
1,2,4-Trichlorobenzene ND ug/L 06/19/24 16:01 120-82-1250125
1,1,1-Trichloroethane ND ug/L 06/19/24 16:01 71-55-662.5 125
1,1,2-Trichloroethane ND ug/L 06/19/24 16:01 79-00-562.5 125
Trichloroethene ND ug/L 06/19/24 16:01 79-01-662.5 125
Trichlorofluoromethane ND ug/L 06/19/24 16:01 75-69-4125125
1,2,3-Trichloropropane ND ug/L 06/19/24 16:01 96-18-462.5 125
1,2,4-Trimethylbenzene 2250 ug/L 06/19/24 16:01 95-63-662.5 125
1,3,5-Trimethylbenzene 509 ug/L 06/19/24 16:01 108-67-862.5 125
Vinyl chloride ND ug/L 06/19/24 16:01 75-01-4125125
m&p-Xylene 10200 ug/L 06/19/24 16:01 179601-23-1125125
o-Xylene 4130 ug/L 06/19/24 16:01 95-47-662.5 125
Surrogates
1,2-Dichloroethane-d4 (S)97 %06/19/24 16:01 17060-07-070-130 125
4-Bromofluorobenzene (S)98 %06/19/24 16:01 460-00-470-130 125
Toluene-d8 (S)96 %06/19/24 16:01 2037-26-570-130 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
862156
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92736862001, 92736862002, 92736862003, 92736862004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4445801
Associated Lab Samples:92736862001, 92736862002, 92736862003, 92736862004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/18/24 13:52
1,1,1-Trichloroethane ug/L ND 0.50 06/18/24 13:52
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/18/24 13:52
1,1,2-Trichloroethane ug/L ND 0.50 06/18/24 13:52
1,1-Dichloroethane ug/L ND 0.50 06/18/24 13:52
1,1-Dichloroethene ug/L ND 0.50 06/18/24 13:52
1,1-Dichloropropene ug/L ND 0.50 06/18/24 13:52
1,2,3-Trichlorobenzene ug/L ND 2.0 06/18/24 13:52
1,2,3-Trichloropropane ug/L ND 0.50 06/18/24 13:52
1,2,4-Trichlorobenzene ug/L ND 2.0 06/18/24 13:52
1,2,4-Trimethylbenzene ug/L ND 0.50 06/18/24 13:52
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/18/24 13:52
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/18/24 13:52
1,2-Dichlorobenzene ug/L ND 0.50 06/18/24 13:52
1,2-Dichloroethane ug/L ND 0.50 06/18/24 13:52
1,2-Dichloropropane ug/L ND 0.50 06/18/24 13:52
1,3,5-Trimethylbenzene ug/L ND 0.50 06/18/24 13:52
1,3-Dichlorobenzene ug/L ND 0.50 06/18/24 13:52
1,3-Dichloropropane ug/L ND 0.50 06/18/24 13:52
1,4-Dichlorobenzene ug/L ND 0.50 06/18/24 13:52
2,2-Dichloropropane ug/L ND 0.50 06/18/24 13:52
2-Chlorotoluene ug/L ND 0.50 06/18/24 13:52
4-Chlorotoluene ug/L ND 0.50 06/18/24 13:52
Benzene ug/L ND 0.50 06/18/24 13:52
Bromobenzene ug/L ND 0.50 06/18/24 13:52
Bromochloromethane ug/L ND 0.50 06/18/24 13:52
Bromodichloromethane ug/L ND 0.50 06/18/24 13:52
Bromoform ug/L ND 0.50 06/18/24 13:52
Bromomethane ug/L ND 5.0 06/18/24 13:52
Carbon tetrachloride ug/L ND 0.50 06/18/24 13:52
Chlorobenzene ug/L ND 0.50 06/18/24 13:52
Chloroethane ug/L ND 1.0 06/18/24 13:52
Chloroform ug/L ND 0.50 06/18/24 13:52
Chloromethane ug/L ND 1.0 06/18/24 13:52
cis-1,2-Dichloroethene ug/L ND 0.50 06/18/24 13:52
cis-1,3-Dichloropropene ug/L ND 0.50 06/18/24 13:52
Dibromochloromethane ug/L ND 0.50 06/18/24 13:52
Dibromomethane ug/L ND 0.50 06/18/24 13:52
Dichlorodifluoromethane ug/L ND 0.50 06/18/24 13:52
Diisopropyl ether ug/L ND 0.50 06/18/24 13:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4445801
Associated Lab Samples:92736862001, 92736862002, 92736862003, 92736862004
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 06/18/24 13:52
Hexachloro-1,3-butadiene ug/L ND 2.0 06/18/24 13:52
Isopropylbenzene (Cumene)ug/L ND 0.50 06/18/24 13:52
m&p-Xylene ug/L ND 1.0 06/18/24 13:52
Methyl-tert-butyl ether ug/L ND 0.50 06/18/24 13:52
Methylene Chloride ug/L ND 2.0 06/18/24 13:52
n-Butylbenzene ug/L ND 0.50 06/18/24 13:52
n-Propylbenzene ug/L ND 0.50 06/18/24 13:52
Naphthalene ug/L ND 2.0 06/18/24 13:52
o-Xylene ug/L ND 0.50 06/18/24 13:52
sec-Butylbenzene ug/L ND 0.50 06/18/24 13:52
Styrene ug/L ND 0.50 06/18/24 13:52
tert-Butylbenzene ug/L ND 0.50 06/18/24 13:52
Tetrachloroethene ug/L ND 0.50 06/18/24 13:52
Toluene ug/L ND 0.50 06/18/24 13:52
trans-1,2-Dichloroethene ug/L ND 0.50 06/18/24 13:52
trans-1,3-Dichloropropene ug/L ND 0.50 06/18/24 13:52
Trichloroethene ug/L ND 0.50 06/18/24 13:52
Trichlorofluoromethane ug/L ND 1.0 06/18/24 13:52
Vinyl chloride ug/L ND 1.0 06/18/24 13:52
1,2-Dichloroethane-d4 (S)%96 70-130 06/18/24 13:52
4-Bromofluorobenzene (S)%99 70-130 06/18/24 13:52
Toluene-d8 (S)%100 70-130 06/18/24 13:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4445802LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.920 110 60-140
1,1,1-Trichloroethane ug/L 20.920 104 60-140
1,1,2,2-Tetrachloroethane ug/L 20.420 102 60-140
1,1,2-Trichloroethane ug/L 21.520 107 60-140
1,1-Dichloroethane ug/L 20.920 105 60-140
1,1-Dichloroethene ug/L 21.120 105 60-140
1,1-Dichloropropene ug/L 20.820 104 60-140
1,2,3-Trichlorobenzene ug/L 20.720 103 60-140
1,2,3-Trichloropropane ug/L 20.920 105 60-140
1,2,4-Trichlorobenzene ug/L 21.120 105 60-140
1,2,4-Trimethylbenzene ug/L 21.120 105 60-140
1,2-Dibromo-3-chloropropane ug/L 19.120 96 60-140
1,2-Dibromoethane (EDB)ug/L 21.120 105 60-140
1,2-Dichlorobenzene ug/L 21.820 109 60-140
1,2-Dichloroethane ug/L 21.220 106 60-140
1,2-Dichloropropane ug/L 21.920 109 60-140
1,3,5-Trimethylbenzene ug/L 21.320 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4445802LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 22.420 112 60-140
1,3-Dichloropropane ug/L 21.020 105 60-140
1,4-Dichlorobenzene ug/L 21.820 109 60-140
2,2-Dichloropropane ug/L 20.120 101 60-140
2-Chlorotoluene ug/L 21.720 109 60-140
4-Chlorotoluene ug/L 21.820 109 60-140
Benzene ug/L 21.720 109 60-140
Bromobenzene ug/L 21.620 108 60-140
Bromochloromethane ug/L 21.720 109 60-140
Bromodichloromethane ug/L 21.320 106 60-140
Bromoform ug/L 21.220 106 60-140
Bromomethane ug/L 20.120 100 60-140
Carbon tetrachloride ug/L 22.320 111 60-140
Chlorobenzene ug/L 22.020 110 60-140
Chloroethane ug/L 20.020 100 60-140
Chloroform ug/L 20.920 104 60-140
Chloromethane ug/L 19.520 98 60-140
cis-1,2-Dichloroethene ug/L 20.720 104 60-140
cis-1,3-Dichloropropene ug/L 20.520 102 60-140
Dibromochloromethane ug/L 21.520 107 60-140
Dibromomethane ug/L 22.520 112 60-140
Dichlorodifluoromethane ug/L 20.020 100 60-140
Diisopropyl ether ug/L 19.620 98 60-140
Ethylbenzene ug/L 21.520 108 60-140
Hexachloro-1,3-butadiene ug/L 22.220 111 60-140
Isopropylbenzene (Cumene)ug/L 21.720 108 60-140
m&p-Xylene ug/L 42.940 107 60-140
Methyl-tert-butyl ether ug/L 19.520 97 60-140
Methylene Chloride ug/L 19.220 96 60-140
n-Butylbenzene ug/L 21.120 105 60-140
n-Propylbenzene ug/L 21.420 107 60-140
Naphthalene ug/L 19.620 98 60-140
o-Xylene ug/L 21.820 109 60-140
sec-Butylbenzene ug/L 21.820 109 60-140
Styrene ug/L 21.520 108 60-140
tert-Butylbenzene ug/L 18.220 91 60-140
Tetrachloroethene ug/L 21.020 105 60-140
Toluene ug/L 21.720 108 60-140
trans-1,2-Dichloroethene ug/L 20.820 104 60-140
trans-1,3-Dichloropropene ug/L 20.820 104 60-140
Trichloroethene ug/L 22.920 114 60-140
Trichlorofluoromethane ug/L 22.220 111 60-140
Vinyl chloride ug/L 19.620 98 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4445803MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92736862001
4445804
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 98 60-140108 1020ND19.6 21.7
1,1,1-Trichloroethane ug/L 20 101 60-140113 1120ND20.2 22.5
1,1,2,2-Tetrachloroethane ug/L 20 91 60-140102 1120ND18.1 20.3
1,1,2-Trichloroethane ug/L 20 97 60-140107 1020ND19.3 21.4
1,1-Dichloroethane ug/L 20 100 60-140110 920ND20.0 22.0
1,1-Dichloroethene ug/L 20 108 60-140119 920ND21.7 23.7
1,1-Dichloropropene ug/L 20 105 60-140116 1020ND20.9 23.1
1,2,3-Trichlorobenzene ug/L 20 95 60-140107 1220ND18.9 21.3
1,2,3-Trichloropropane ug/L 20 95 60-140103 820ND19.1 20.7
1,2,4-Trichlorobenzene ug/L 20 99 60-140107 720ND19.8 21.3
1,2,4-Trimethylbenzene ug/L 20 106 60-140116 920ND21.2 23.2
1,2-Dibromo-3-chloropropane ug/L 20 79 60-14091 1420ND15.9 18.2
1,2-Dibromoethane (EDB)ug/L 20 97 60-140108 1220ND19.3 21.7
1,2-Dichlorobenzene ug/L 20 105 60-140115 1020ND20.9 23.1
1,2-Dichloroethane ug/L 20 97 60-140107 1020ND19.3 21.3
1,2-Dichloropropane ug/L 20 103 60-140112 820ND20.6 22.3
1,3,5-Trimethylbenzene ug/L 20 108 60-140117 920ND21.5 23.4
1,3-Dichlorobenzene ug/L 20 108 60-140119 1020ND21.7 23.9
1,3-Dichloropropane ug/L 20 97 60-140107 1120ND19.3 21.5
1,4-Dichlorobenzene ug/L 20 106 60-140117 1020ND21.2 23.4
2,2-Dichloropropane ug/L 20 100 60-140111 1020ND20.0 22.1
2-Chlorotoluene ug/L 20 109 60-140120 1020ND21.7 24.0
4-Chlorotoluene ug/L 20 109 60-140120 1020ND21.7 23.9
Benzene ug/L 20 104 60-140115 1020ND20.9 23.0
Bromobenzene ug/L 20 107 60-140117 920ND21.4 23.4
Bromochloromethane ug/L 20 99 60-140108 920ND19.8 21.6
Bromodichloromethane ug/L 20 95 60-140105 1020ND19.0 21.0
Bromoform ug/L 20 84 60-14095 1220ND16.9 19.0
Bromomethane ug/L 20 103 60-140111 720ND20.7 22.2
Carbon tetrachloride ug/L 20 107 60-140117 920ND21.4 23.4
Chlorobenzene ug/L 20 105 60-140115 920ND21.0 23.1
Chloroethane ug/L 20 102 60-140113 1020ND20.3 22.6
Chloroform ug/L 20 99 60-140107 6204.3 24.1 25.6
Chloromethane ug/L 20 104 60-140117 1220ND20.7 23.4
cis-1,2-Dichloroethene ug/L 20 99 60-140108 920ND19.8 21.6
cis-1,3-Dichloropropene ug/L 20 93 60-140102 920ND18.6 20.3
Dibromochloromethane ug/L 20 93 60-140104 1220ND18.5 20.8
Dibromomethane ug/L 20 100 60-140109 920ND19.9 21.8
Dichlorodifluoromethane ug/L 20 120 60-140131 920ND24.0 26.2
Diisopropyl ether ug/L 20 91 60-140101 1020ND18.1 20.1
Ethylbenzene ug/L 20 107 60-140116 920ND21.3 23.3
Hexachloro-1,3-butadiene ug/L 20 114 60-140123 820ND22.8 24.6
Isopropylbenzene (Cumene)ug/L 20 106 60-140117 920ND21.3 23.3
m&p-Xylene ug/L 40 105 60-140115 940ND42.2 46.0
Methyl-tert-butyl ether ug/L 20 87 60-14096 1020ND17.5 19.2
Methylene Chloride ug/L 20 90 60-140100 1120ND17.9 20.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4445803MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92736862001
4445804
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 111 60-140120 820ND22.1 23.9
n-Propylbenzene ug/L 20 109 60-140120 1020ND21.9 24.1
Naphthalene ug/L 20 89 60-140100 1220ND17.8 19.9
o-Xylene ug/L 20 103 60-140115 1120ND20.5 23.0
sec-Butylbenzene ug/L 20 112 60-140121 820ND22.4 24.3
Styrene ug/L 20 102 60-140112 1020ND20.4 22.5
tert-Butylbenzene ug/L 20 93 60-140102 1020ND18.6 20.4
Tetrachloroethene ug/L 20 106 60-140117 1020ND21.2 23.4
Toluene ug/L 20 103 60-140113 1020ND20.6 22.7
trans-1,2-Dichloroethene ug/L 20 103 60-140114 1020ND20.6 22.8
trans-1,3-Dichloropropene ug/L 20 92 60-140103 1120ND18.5 20.6
Trichloroethene ug/L 20 111 60-140121 920ND22.2 24.2
Trichlorofluoromethane ug/L 20 117 60-140127 820ND23.4 25.3
Vinyl chloride ug/L 20 106 60-140115 920ND21.2 23.1
1,2-Dichloroethane-d4 (S)%93 70-13093
4-Bromofluorobenzene (S)%98 70-13098
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
862432
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92736862005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4447214
Associated Lab Samples:92736862005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/19/24 10:37
1,1,1-Trichloroethane ug/L ND 0.50 06/19/24 10:37
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/19/24 10:37
1,1,2-Trichloroethane ug/L ND 0.50 06/19/24 10:37
1,1-Dichloroethane ug/L ND 0.50 06/19/24 10:37
1,1-Dichloroethene ug/L ND 0.50 06/19/24 10:37
1,1-Dichloropropene ug/L ND 0.50 06/19/24 10:37
1,2,3-Trichlorobenzene ug/L ND 2.0 06/19/24 10:37
1,2,3-Trichloropropane ug/L ND 0.50 06/19/24 10:37
1,2,4-Trichlorobenzene ug/L ND 2.0 06/19/24 10:37
1,2,4-Trimethylbenzene ug/L ND 0.50 06/19/24 10:37
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/19/24 10:37
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/19/24 10:37
1,2-Dichlorobenzene ug/L ND 0.50 06/19/24 10:37
1,2-Dichloroethane ug/L ND 0.50 06/19/24 10:37
1,2-Dichloropropane ug/L ND 0.50 06/19/24 10:37
1,3,5-Trimethylbenzene ug/L ND 0.50 06/19/24 10:37
1,3-Dichlorobenzene ug/L ND 0.50 06/19/24 10:37
1,3-Dichloropropane ug/L ND 0.50 06/19/24 10:37
1,4-Dichlorobenzene ug/L ND 0.50 06/19/24 10:37
2,2-Dichloropropane ug/L ND 0.50 06/19/24 10:37
2-Chlorotoluene ug/L ND 0.50 06/19/24 10:37
4-Chlorotoluene ug/L ND 0.50 06/19/24 10:37
Benzene ug/L ND 0.50 06/19/24 10:37
Bromobenzene ug/L ND 0.50 06/19/24 10:37
Bromochloromethane ug/L ND 0.50 06/19/24 10:37
Bromodichloromethane ug/L ND 0.50 06/19/24 10:37
Bromoform ug/L ND 0.50 06/19/24 10:37
Bromomethane ug/L ND 5.0 06/19/24 10:37
Carbon tetrachloride ug/L ND 0.50 06/19/24 10:37
Chlorobenzene ug/L ND 0.50 06/19/24 10:37
Chloroethane ug/L ND 1.0 06/19/24 10:37
Chloroform ug/L ND 0.50 06/19/24 10:37
Chloromethane ug/L ND 1.0 06/19/24 10:37
cis-1,2-Dichloroethene ug/L ND 0.50 06/19/24 10:37
cis-1,3-Dichloropropene ug/L ND 0.50 06/19/24 10:37
Dibromochloromethane ug/L ND 0.50 06/19/24 10:37
Dibromomethane ug/L ND 0.50 06/19/24 10:37
Dichlorodifluoromethane ug/L ND 0.50 06/19/24 10:37
Diisopropyl ether ug/L ND 0.50 06/19/24 10:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4447214
Associated Lab Samples:92736862005
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 06/19/24 10:37
Hexachloro-1,3-butadiene ug/L ND 2.0 06/19/24 10:37
Isopropylbenzene (Cumene)ug/L ND 0.50 06/19/24 10:37
m&p-Xylene ug/L ND 1.0 06/19/24 10:37
Methyl-tert-butyl ether ug/L ND 0.50 06/19/24 10:37
Methylene Chloride ug/L ND 2.0 06/19/24 10:37
n-Butylbenzene ug/L ND 0.50 06/19/24 10:37
n-Propylbenzene ug/L ND 0.50 06/19/24 10:37
Naphthalene ug/L ND 2.0 06/19/24 10:37
o-Xylene ug/L ND 0.50 06/19/24 10:37
sec-Butylbenzene ug/L ND 0.50 06/19/24 10:37
Styrene ug/L ND 0.50 06/19/24 10:37
tert-Butylbenzene ug/L ND 0.50 06/19/24 10:37
Tetrachloroethene ug/L ND 0.50 06/19/24 10:37
Toluene ug/L ND 0.50 06/19/24 10:37
trans-1,2-Dichloroethene ug/L ND 0.50 06/19/24 10:37
trans-1,3-Dichloropropene ug/L ND 0.50 06/19/24 10:37
Trichloroethene ug/L ND 0.50 06/19/24 10:37
Trichlorofluoromethane ug/L ND 1.0 06/19/24 10:37
Vinyl chloride ug/L ND 1.0 06/19/24 10:37
1,2-Dichloroethane-d4 (S)%96 70-130 06/19/24 10:37
4-Bromofluorobenzene (S)%97 70-130 06/19/24 10:37
Toluene-d8 (S)%99 70-130 06/19/24 10:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4447215LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 17.520 88 60-140
1,1,1-Trichloroethane ug/L 20.320 101 60-140
1,1,2,2-Tetrachloroethane ug/L 20.120 101 60-140
1,1,2-Trichloroethane ug/L 19.220 96 60-140
1,1-Dichloroethane ug/L 19.020 95 60-140
1,1-Dichloroethene ug/L 19.220 96 60-140
1,1-Dichloropropene ug/L 20.820 104 60-140
1,2,3-Trichlorobenzene ug/L 21.120 105 60-140
1,2,3-Trichloropropane ug/L 19.620 98 60-140
1,2,4-Trichlorobenzene ug/L 21.720 109 60-140
1,2,4-Trimethylbenzene ug/L 21.120 106 60-140
1,2-Dibromo-3-chloropropane ug/L 20.120 100 60-140
1,2-Dibromoethane (EDB)ug/L 20.720 103 60-140
1,2-Dichlorobenzene ug/L 21.620 108 60-140
1,2-Dichloroethane ug/L 19.820 99 60-140
1,2-Dichloropropane ug/L 18.020 90 60-140
1,3,5-Trimethylbenzene ug/L 21.020 105 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4447215LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 20.820 104 60-140
1,3-Dichloropropane ug/L 21.120 105 60-140
1,4-Dichlorobenzene ug/L 20.920 104 60-140
2,2-Dichloropropane ug/L 20.220 101 60-140
2-Chlorotoluene ug/L 21.920 109 60-140
4-Chlorotoluene ug/L 21.420 107 60-140
Benzene ug/L 19.320 97 60-140
Bromobenzene ug/L 20.520 102 60-140
Bromochloromethane ug/L 21.220 106 60-140
Bromodichloromethane ug/L 20.420 102 60-140
Bromoform ug/L 17.220 86 60-140
Bromomethane ug/L 14.920 75 60-140
Carbon tetrachloride ug/L 20.720 103 60-140
Chlorobenzene ug/L 19.720 99 60-140
Chloroethane ug/L 18.020 90 60-140
Chloroform ug/L 19.520 97 60-140
Chloromethane ug/L 20.520 103 60-140
cis-1,2-Dichloroethene ug/L 19.820 99 60-140
cis-1,3-Dichloropropene ug/L 16.720 83 60-140
Dibromochloromethane ug/L 17.220 86 60-140
Dibromomethane ug/L 19.720 99 60-140
Dichlorodifluoromethane ug/L 19.220 96 60-140
Diisopropyl ether ug/L 18.420 92 60-140
Ethylbenzene ug/L 20.120 101 60-140
Hexachloro-1,3-butadiene ug/L 22.420 112 60-140
Isopropylbenzene (Cumene)ug/L 20.320 101 60-140
m&p-Xylene ug/L 39.540 99 60-140
Methyl-tert-butyl ether ug/L 18.020 90 60-140
Methylene Chloride ug/L 19.020 95 60-140
n-Butylbenzene ug/L 21.620 108 60-140
n-Propylbenzene ug/L 21.120 105 60-140
Naphthalene ug/L 20.620 103 60-140
o-Xylene ug/L 20.720 104 60-140
sec-Butylbenzene ug/L 21.920 110 60-140
Styrene ug/L 20.020 100 60-140
tert-Butylbenzene ug/L 17.320 87 60-140
Tetrachloroethene ug/L 21.120 105 60-140
Toluene ug/L 18.820 94 60-140
trans-1,2-Dichloroethene ug/L 19.920 99 60-140
trans-1,3-Dichloropropene ug/L 16.520 82 60-140
Trichloroethene ug/L 20.820 104 60-140
Trichlorofluoromethane ug/L 17.320 87 60-140
Vinyl chloride ug/L 17.620 88 60-140
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4447216MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92737143005
4447217
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 103 60-140110 620ND20.6 22.0
1,1,1-Trichloroethane ug/L 20 127 60-140140 1020ND25.4 28.1
1,1,2,2-Tetrachloroethane ug/L 20 114 60-140123 820ND22.7 24.6
1,1,2-Trichloroethane ug/L 20 115 60-140124 720ND23.1 24.7
1,1-Dichloroethane ug/L 20 119 60-140131 1020ND23.8 26.2
1,1-Dichloroethene ug/L 20 116 60-140130 1120ND23.2 26.0
1,1-Dichloropropene ug/L 20 129 60-140139 720ND25.8 27.8
1,2,3-Trichlorobenzene ug/L 20 125 60-140130 420ND25.1 26.0
1,2,3-Trichloropropane ug/L 20 114 60-140122 720ND22.7 24.4
1,2,4-Trichlorobenzene ug/L 20 127 60-140133 420ND25.5 26.5
1,2,4-Trimethylbenzene ug/L 20 123 60-140128 420ND24.6 25.6
1,2-Dibromo-3-chloropropane ug/L 20 117 60-140124 620ND23.5 24.8
1,2-Dibromoethane (EDB)ug/L 20 121 60-140132 820ND24.3 26.4
1,2-Dichlorobenzene ug/L 20 120 60-140125 420ND24.0 25.0
1,2-Dichloroethane ug/L 20 119 60-140134 1220ND23.9 26.8
1,2-Dichloropropane ug/L 20 110 60-140117 620ND22.1 23.4
1,3,5-Trimethylbenzene ug/L 20 125 60-140129 420ND25.0 25.9
1,3-Dichlorobenzene ug/L 20 119 60-140124 420ND23.8 24.8
1,3-Dichloropropane ug/L 20 122 60-140133 820ND24.5 26.5
1,4-Dichlorobenzene ug/L 20 118 60-140124 420ND23.7 24.7
2,2-Dichloropropane ug/L M12013260-140143 820ND26.4 28.6
2-Chlorotoluene ug/L 20 126 60-140131 420ND25.3 26.2
4-Chlorotoluene ug/L 20 121 60-140128 520ND24.3 25.5
Benzene ug/L 20 120 60-140128 620ND23.9 25.5
Bromobenzene ug/L 20 116 60-140122 520ND23.2 24.4
Bromochloromethane ug/L 20 126 60-140137 920ND25.2 27.5
Bromodichloromethane ug/L 20 124 60-140132 620ND24.9 26.4
Bromoform ug/L 20 96 60-140105 820ND19.3 20.9
Bromomethane ug/L 20 76 60-14084 1120ND15.1 16.9
Carbon tetrachloride ug/L 20 132 60-140140 520ND26.4 27.9
Chlorobenzene ug/L 20 115 60-140122 620ND23.0 24.3
Chloroethane ug/L 20 109 60-140116 720ND21.7 23.2
Chloroform ug/L 20 119 60-140132 1020ND23.8 26.4
Chloromethane ug/L 20 115 60-140126 920ND23.0 25.3
cis-1,2-Dichloroethene ug/L 20 121 60-140133 1020ND24.2 26.6
cis-1,3-Dichloropropene ug/L 20 101 60-140109 820ND20.1 21.8
Dibromochloromethane ug/L 20 102 60-140109 620ND20.4 21.7
Dibromomethane ug/L 20 123 60-140132 720ND24.6 26.4
Dichlorodifluoromethane ug/L M12013060-140143 1020ND26.0 28.6
Diisopropyl ether ug/L 20 110 60-140122 1020ND22.0 24.4
Ethylbenzene ug/L 20 121 60-140129 720ND24.2 25.9
Hexachloro-1,3-butadiene ug/L M12013560-140144 620ND27.1 28.9
Isopropylbenzene (Cumene)ug/L 20 122 60-140129 620ND24.3 25.8
m&p-Xylene ug/L 40 119 60-140126 640ND47.5 50.4
Methyl-tert-butyl ether ug/L 20 109 60-140120 920ND21.9 24.0
Methylene Chloride ug/L 20 107 60-140118 1020ND21.3 23.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
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[phone]
Page 27 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4447216MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92737143005
4447217
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M12013660-140142 420ND27.2 28.3
n-Propylbenzene ug/L 20 126 60-140132 520ND25.2 26.4
Naphthalene ug/L 20 125 60-140130 420ND25.7 26.9
o-Xylene ug/L 20 120 60-140131 920ND24.2 26.4
sec-Butylbenzene ug/L 20 129 60-140135 520ND25.8 27.1
Styrene ug/L 20 116 60-140125 720ND23.2 24.9
tert-Butylbenzene ug/L 20 104 60-140108 420ND20.7 21.6
Tetrachloroethene ug/L 20 129 60-140132 220ND25.7 26.3
Toluene ug/L 20 112 60-140121 820ND22.4 24.3
trans-1,2-Dichloroethene ug/L 20 122 60-140134 920ND24.4 26.8
trans-1,3-Dichloropropene ug/L 20 99 60-140104 620ND19.7 20.9
Trichloroethene ug/L 20 127 60-140138 820ND25.4 27.6
Trichlorofluoromethane ug/L 20 118 60-140130 1020ND23.6 26.0
Vinyl chloride ug/L 20 112 60-140120 720ND22.3 24.0
1,2-Dichloroethane-d4 (S)%104 70-130101
4-Bromofluorobenzene (S)%103 70-130101
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
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Asheville, NC 28804
[phone]
Page 28 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
862245
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92736862001, 92736862002, 92736862003, 92736862004, 92736862005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4446379
Associated Lab Samples:92736862001, 92736862002, 92736862003, 92736862004, 92736862005
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 06/19/24 13:28
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 06/19/24 13:28
2,4,6-Trichlorophenol ug/L ND 10.0 06/19/24 13:28
2,4-Dichlorophenol ug/L ND 5.0 06/19/24 13:28
2,4-Dimethylphenol ug/L ND 10.0 06/19/24 13:28
2,4-Dinitrophenol ug/L ND 50.0 06/19/24 13:28
2,4-Dinitrotoluene ug/L ND 5.0 06/19/24 13:28
2,6-Dinitrotoluene ug/L ND 5.0 06/19/24 13:28
2-Chloronaphthalene ug/L ND 5.0 06/19/24 13:28
2-Chlorophenol ug/L ND 5.0 06/19/24 13:28
2-Nitrophenol ug/L ND 5.0 06/19/24 13:28
3,3'-Dichlorobenzidine ug/L ND 10.0 06/19/24 13:28
4,6-Dinitro-2-methylphenol ug/L ND 10.0 06/19/24 13:28
4-Bromophenylphenyl ether ug/L ND 5.0 06/19/24 13:28
4-Chloro-3-methylphenol ug/L ND 5.0 06/19/24 13:28
4-Chlorophenylphenyl ether ug/L ND 5.0 06/19/24 13:28
4-Nitrophenol ug/L ND 10.0 06/19/24 13:28
Acenaphthene ug/L ND 5.0 06/19/24 13:28
Acenaphthylene ug/L ND 5.0 06/19/24 13:28
Anthracene ug/L ND 5.0 06/19/24 13:28
Benzo(a)anthracene ug/L ND 5.0 06/19/24 13:28
Benzo(a)pyrene ug/L ND 5.0 06/19/24 13:28
Benzo(b)fluoranthene ug/L ND 5.0 06/19/24 13:28
Benzo(g,h,i)perylene ug/L ND 5.0 06/19/24 13:28
Benzo(k)fluoranthene ug/L ND 5.0 06/19/24 13:28
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/19/24 13:28
bis(2-Chloroethyl) ether ug/L ND 5.0 06/19/24 13:28
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 06/19/24 13:28
Butylbenzylphthalate ug/L ND 5.0 06/19/24 13:28
Chrysene ug/L ND 5.0 06/19/24 13:28
Di-n-butylphthalate ug/L ND 5.0 06/19/24 13:28
Di-n-octylphthalate ug/L ND 5.0 06/19/24 13:28
Dibenz(a,h)anthracene ug/L ND 5.0 06/19/24 13:28
Diethylphthalate ug/L ND 5.0 06/19/24 13:28
Dimethylphthalate ug/L ND 5.0 06/19/24 13:28
Fluoranthene ug/L ND 5.0 06/19/24 13:28
Fluorene ug/L ND 5.0 06/19/24 13:28
Hexachloro-1,3-butadiene ug/L ND 5.0 06/19/24 13:28
Hexachlorobenzene ug/L ND 5.0 06/19/24 13:28
Hexachlorocyclopentadiene ug/L ND 10.0 06/19/24 13:28
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
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Asheville, NC 28804
[phone]
Page 29 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4446379
Associated Lab Samples:92736862001, 92736862002, 92736862003, 92736862004, 92736862005
Matrix:Water
Analyzed
Hexachloroethane ug/L ND 5.0 06/19/24 13:28
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 06/19/24 13:28
Isophorone ug/L ND 10.0 06/19/24 13:28
N-Nitroso-di-n-propylamine ug/L ND 5.0 06/19/24 13:28
N-Nitrosodimethylamine ug/L ND 5.0 06/19/24 13:28
N-Nitrosodiphenylamine ug/L ND 10.0 06/19/24 13:28
Naphthalene ug/L ND 5.0 06/19/24 13:28
Nitrobenzene ug/L ND 5.0 06/19/24 13:28
Pentachlorophenol ug/L ND 10.0 06/19/24 13:28
Phenanthrene ug/L ND 5.0 06/19/24 13:28
Phenol ug/L ND 5.0 06/19/24 13:28
Pyrene ug/L ND 5.0 06/19/24 13:28
2,4,6-Tribromophenol (S)%127 10-137 06/19/24 13:28
2-Fluorobiphenyl (S)%66 15-120 06/19/24 13:28
2-Fluorophenol (S)%79 10-120 06/19/24 13:28
Nitrobenzene-d5 (S)%99 10-120 06/19/24 13:28
Phenol-d6 (S)%64 10-120 06/19/24 13:28
Terphenyl-d14 (S)%141 11-131 S306/19/24 13:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4446380LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 29.050 58 44-142
2,2'-Oxybis(1-chloropropane)ug/L 39.450 79 36-166
2,4,6-Trichlorophenol ug/L 42.250 84 37-144
2,4-Dichlorophenol ug/L 38.850 78 1-191
2,4-Dimethylphenol ug/L 39.750 79 32-119
2,4-Dinitrophenol ug/L 296250 118 1-181
2,4-Dinitrotoluene ug/L 47.150 94 39-139
2,6-Dinitrotoluene ug/L 45.450 91 50-158
2-Chloronaphthalene ug/L 38.550 77 60-118
2-Chlorophenol ug/L 38.350 77 23-134
2-Nitrophenol ug/L 42.350 85 29-182
3,3'-Dichlorobenzidine ug/L 87.6100 88 1-262
4,6-Dinitro-2-methylphenol ug/L 111100 111 1-181
4-Bromophenylphenyl ether ug/L 42.750 85 53-127
4-Chloro-3-methylphenol ug/L 78.5100 78 22-147
4-Chlorophenylphenyl ether ug/L 40.750 81 25-158
4-Nitrophenol ug/L 143250 57 1-132
Acenaphthene ug/L 40.450 81 47-145
Acenaphthylene ug/L 42.150 84 33-145
Anthracene ug/L 44.250 88 1-166
Benzo(a)anthracene ug/L 46.750 93 33-143
Benzo(a)pyrene ug/L 47.350 95 17-163
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4446380LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 47.450 95 24-159
Benzo(g,h,i)perylene ug/L 43.650 87 1-219
Benzo(k)fluoranthene ug/L 46.950 94 11-162
bis(2-Chloroethoxy)methane ug/L 40.750 81 33-184
bis(2-Chloroethyl) ether ug/L 40.650 81 12-158
bis(2-Ethylhexyl)phthalate ug/L 50.750 101 8-158
Butylbenzylphthalate ug/L 51.150 102 1-152
Chrysene ug/L 45.550 91 17-168
Di-n-butylphthalate ug/L 47.850 96 1-118
Di-n-octylphthalate ug/L 50.450 101 4-146
Dibenz(a,h)anthracene ug/L 43.150 86 1-227
Diethylphthalate ug/L 44.550 89 1-114
Dimethylphthalate ug/L 42.650 85 1-112
Fluoranthene ug/L 44.950 90 26-137
Fluorene ug/L 41.450 83 59-121
Hexachloro-1,3-butadiene ug/L 26.150 52 24-116
Hexachlorobenzene ug/L 42.450 85 1-152
Hexachlorocyclopentadiene ug/L 35.250 70 25-150
Hexachloroethane ug/L 22.150 44 40-113
Indeno(1,2,3-cd)pyrene ug/L 42.850 86 1-171
Isophorone ug/L 42.350 85 21-196
N-Nitroso-di-n-propylamine ug/L 45.150 90 1-230
N-Nitrosodimethylamine ug/L 34.050 68 25-150
N-Nitrosodiphenylamine ug/L 43.850 88 25-150
Naphthalene ug/L 33.550 67 21-133
Nitrobenzene ug/L 38.450 77 35-180
Pentachlorophenol ug/L 106100 106 14-176
Phenanthrene ug/L 43.350 87 54-120
Phenol ug/L 24.350 49 5-112
Pyrene ug/L 48.750 97 52-115
2,4,6-Tribromophenol (S)%109 10-137
2-Fluorobiphenyl (S)%82 15-120
2-Fluorophenol (S)%68 10-120
Nitrobenzene-d5 (S)%91 10-120
Phenol-d6 (S)%54 10-120
Terphenyl-d14 (S)%111 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4446381MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92730657014
4446382
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M183.3 39 44-14235 1083.3ND 32.2 29.2
2,2'-Oxybis(1-chloropropane)ug/L 83.3 73 36-16661 1783.3ND 60.7 51.0
2,4,6-Trichlorophenol ug/L M183.3 0 37-144083.3ND ND ND
2,4-Dichlorophenol ug/L 83.3 9 1-191483.3ND 7.1J 3.6J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4446381MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92730657014
4446382
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dimethylphenol ug/L 83.3 74 32-11960 2183.3ND 61.8 49.9
2,4-Dinitrophenol ug/L M141731-1810417NDNDND
2,4-Dinitrotoluene ug/L 83.3 109 39-13990 1883.3ND 90.7 75.4
2,6-Dinitrotoluene ug/L 83.3 97 50-15877 2383.3ND 80.7 64.3
2-Chloronaphthalene ug/L M183.3 49 60-11844 1083.3ND 40.8 36.8
2-Chlorophenol ug/L M183.3 10 23-134883.3ND ND 6.6J
2-Nitrophenol ug/L M183.3 0 29-182083.3ND ND ND
3,3'-Dichlorobenzidine ug/L 167 129 1-262109 17167ND215181
4,6-Dinitro-2-methylphenol ug/L 167 15 1-18111 28167ND24.3 18.3
4-Bromophenylphenyl ether ug/L 83.3 85 53-12777 983.3ND 70.6 64.3
4-Chloro-3-methylphenol ug/L R11677322-14743 52167ND12271.6
4-Chlorophenylphenyl ether ug/L 83.3 74 25-15864 1683.3ND 61.9 53.0
4-Nitrophenol ug/L M141701-1320417NDNDND
Acenaphthene ug/L 83.3 60 47-14555 1083.3ND 50.3 45.7
Acenaphthylene ug/L 83.3 64 33-14557 1183.3ND 53.1 47.6
Anthracene ug/L 83.3 109 1-16698 1183.3ND 90.7 81.4
Benzo(a)anthracene ug/L 83.3 128 33-143106 1983.3ND 107 88.0
Benzo(a)pyrene ug/L 83.3 134 17-163116 1483.3ND 112 96.7
Benzo(b)fluoranthene ug/L 83.3 129 24-159108 1783.3ND 108 90.4
Benzo(g,h,i)perylene ug/L 83.3 145 1-219130 1183.3ND 121 108
Benzo(k)fluoranthene ug/L 83.3 129 11-162109 1783.3ND 108 90.7
bis(2-Chloroethoxy)methane ug/L 83.3 83 33-18470 1883.3ND 69.5 58.1
bis(2-Chloroethyl) ether ug/L 83.3 86 12-15872 1883.3ND 71.3 59.8
bis(2-Ethylhexyl)phthalate ug/L 83.3 135 8-158115 1683.3ND 113 95.8
Butylbenzylphthalate ug/L 83.3 137 1-152114 1883.3ND 114 95.1
Chrysene ug/L 83.3 123 17-168107 1483.3ND 103 89.2
Di-n-butylphthalate ug/L M183.3 130 1-118116 1183.3ND 108 96.7
Di-n-octylphthalate ug/L M183.3 151 4-146131 1583.3ND 126 109
Dibenz(a,h)anthracene ug/L 83.3 144 1-227127 1383.3ND 120 105
Diethylphthalate ug/L 83.3 104 1-11487 1783.3ND 86.3 72.6
Dimethylphthalate ug/L 83.3 87 1-11274 1683.3ND 72.3 61.8
Fluoranthene ug/L 83.3 132 26-137118 1183.3ND 110 98.4
Fluorene ug/L 83.3 74 59-12166 1183.3ND 61.6 55.1
Hexachloro-1,3-butadiene ug/L 83.3 36 24-11632 1283.3ND 30.2 26.9
Hexachlorobenzene ug/L 83.3 96 1-15281 1783.3ND 80.0 67.5
Hexachlorocyclopentadiene ug/L 83.3 28 25-15026 783.3ND 23.0 21.4
Hexachloroethane ug/L M183.3 35 40-11330 1483.3ND 29.1 25.3
Indeno(1,2,3-cd)pyrene ug/L 83.3 138 1-171119 1583.3ND 115 99.2
Isophorone ug/L 83.3 88 21-19672 1983.3ND 73.3 60.3
N-Nitroso-di-n-propylamine ug/L 83.3 83 1-23070 1783.3ND 68.9 58.1
N-Nitrosodimethylamine ug/L 83.3 70 25-15058 1983.3ND 58.4 48.5
N-Nitrosodiphenylamine ug/L 83.3 105 25-15092 1383.3ND 87.1 76.5
Naphthalene ug/L 83.3 47 21-13342 1183.3ND 39.2 35.2
Nitrobenzene ug/L 83.3 75 35-18064 1783.3ND 62.9 53.2
Pentachlorophenol ug/L M1167014-1760167NDNDND
Phenanthrene ug/L 83.3 111 54-12094 1783.3ND 92.8 78.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
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Asheville, NC 28804
[phone]
Page 32 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4446381MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92730657014
4446382
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol ug/L 83.3 23 5-11220 1483.3ND 19.0 16.4
Pyrene ug/L 83.3 114 52-11599 1483.3ND 95.3 82.8
2,4,6-Tribromophenol (S)%S0010-1370
2-Fluorobiphenyl (S)%63 15-12050
2-Fluorophenol (S)%S0210-1202
Nitrobenzene-d5 (S)%81 10-12064
Phenol-d6 (S)%15 10-12013
Terphenyl-d14 (S)%115 11-13196
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
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Asheville, NC 28804
[phone]
Page 33 of 38
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92736862
BOC- Amboy Road
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 38
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92736862
BOC- Amboy Road
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92736862001 862245 862443MW - 7 EPA 625.1 EPA 625.1
92736862002 862245 862443MW - 2 EPA 625.1 EPA 625.1
92736862003 862245 862443MW - 4 EPA 625.1 EPA 625.1
92736862004 862245 862443MW - 6 EPA 625.1 EPA 625.1
92736862005 862245 862443MW - 3 EPA 625.1 EPA 625.1
92736862001 862156MW - 7 SM 6200B
92736862002 862156MW - 2 SM 6200B
92736862003 862156MW - 4 SM 6200B
92736862004 862156MW - 6 SM 6200B
92736862005 862432MW - 3 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/21/2024 03:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 38
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