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NCD044447589_20230801_0064_Blue Ridge Plating Site_Letter Report (August 2023)_Final (1)
1955 Evergreen Blvd., Suite 300, Duluth, GA 30096 Tel 678.775.3080 Fax 678.775.3138 www.tetratech.com August 22, 2023 Mr. Craig Zeller Remedial Project Manager U.S. Environmental Protection Agency, Region 4 61 Forsyth Street, SW Atlanta, Georgia 30303 Subject: Letter Report Blue Ridge Plating Arden, Buncombe County, North Carolina EPA Contract No.: 68HE0419F0064 Task Order: 68HE0419F0064, Subtask 04 Dear Mr. Zeller: The Tetra Tech, Inc. Superfund Technical Assessment and Response Team (START) submits this letter report summarizing activities associated with the Blue Ridge Plating site (the site) in Arden, Buncombe County, North Carolina, conducted on February 28 through March 1, 2022. This report includes five enclosures and two attachments. Enclosure 1 contains figures illustrating the site location, site layout, and sampling locations. Enclosure 2 includes data summary tables. Enclosure 3 contains the photographic log. Enclosure 4 contains the monitoring well sampling forms. Enclosure 5 contains the Tetra Tech review of field quality control samples. Attachment 1 contains the laboratory data packages. Attachment 2 contains the EPA Regional Screening Levels (RSL) (target cancer risk TR=1E-06, target hazard quotient THQ=0.1) for residential soil to groundwater (May 2023). Background The Blue Ridge Plating (BRP) site is located at 171 Glenn Bridge Road, Arden, Buncombe County, North Carolina and occupies 3.06 acres. See Figure 1 in Enclosure 1. No structures remain on the property due to the EPA’s emergency response action (December 2014 through May 2015). The site is bounded to the north by Glenn Bridge Road; to the east by Business Park Circle and several commercial establishments; to the south and west by wooded areas and an auto repair business that is also along Business Park Circle; and to the west by Beale Road, including the intersection of Glenn Bridge Road and Beale Road and residential housing beyond. See Figure 2 in Enclosure 1. BRP was a metal plating company, which operated from 1974 to 2014. It used black oxide, cadmium, chromium, copper, cyanide, tin, and zinc in the electroplating processes. From 1974 to 1985, electroplating wastes were collected in drums located in the basement of a former structure where plating sludges were filtered out and the wastewater was directed to a 70,000-gallon in-ground concrete lagoon located behind the shop. Plating sludges were shipped off site for disposal and the wastewater was either sprayed on the ground or reused as process water. Between 1985 and 1990, the wastewater was discharged to the local municipal sewer system. In 1990, the municipality suspended access to the sewer system because BRP was not meeting pretreatment Mr. C. Zeller Page 2 August 22, 2023 requirements. After that suspension, BRP employed a closed loop reclamation system, which was in the basement of the former structure. Trip Description On January 24, 2023, EPA tasked START to locate and collect groundwater samples from ten previously installed off-site monitoring wells associated with the BRP site. The ten monitoring wells to be sampled are designated as follows, where “S” refers to shallow wells and “D” refers to deep wells: MW13S/13D, MW15S/15D, MW16S/16D, MW17S/17D, MW18D, and MW20D. Along with sampling, basic water data including depth to groundwater table, pH, DO, ORP, and water temperature were collected. These parameters and other information gathered during the sampling event were recorded on the monitoring well sampling forms included in Enclosure 4. Between February 28 and March 1, 2023, START David Reed and Julian Rizzi traveled to the site, located the ten monitoring wells, and collected groundwater samples from each well for analysis. See Figure 3 in Enclosure 1 and Enclosure 3. Prior to, and during well purging, a Herron dipper-T was used to monitor the depth to ground water, and a Horiba Water Quality Monitor was used to collect basic water data and ensure proper well stabilization prior to sampling. A Mega-Monsoon water sampling pump with an adjustable flow rate was used to purge all ten monitoring wells and collect samples. After sampling activities were concluded, Tetra Tech START processed, packaged, and shipped all samples to the EPA Region 4 Laboratory Services and Applied Science Division (LSASD) Laboratory Services Branch (LSB) in Athens, Georgia, for volatile and semivolatile organic compound, and metals analysis. The LSB analyzed all samples for volatile organic compounds by Method CLP SFAM01.1, semivolatile organic compounds by Method CLP SFAM01.1 B, total metals by Method CLP SFAM01.1 MS, and total mercury by Method CLP SFAM01.1 CV. Tables of the EPA-validated analytical results can be found in Enclosure 2. A summary of Tetra Tech’s review of field quality control samples is contained in Enclosure 5. The laboratory data packages can be found in Attachment 1. Analytical Results All analytical results were compared to the maximum contaminant level allowed in drinking water (MCL). MCLs were extracted from the EPA RSL tables contained in Attachment 2. Results for 1,1-dichloroethene exceeded the MCL two samples, MW13D and MW15S. Mr. C. Zeller Page 3 August 22, 2023 If you have any questions or need additional copies of this report, please call me at (803) 238-5485. Sincerely, David Reed Andrew F. Johnson START V Task Manager START V Project/Program Manager Enclosures (5) Attachment (2) cc: Katrina Jones, EPA Project Officer Angel Reed, START V Document Control Coordinator ENCLOSURE 1 FIGURES (3 Pages) City:State:County: United StatesEnvironmental Protection Agency Region 4 7/18/2023 Date: nathan.warren Analyst: Legend Site Location Map Source: USGS 7.5 Minute Topographic Quadrangle Maps: Skyland, NC 1979. / 0 1,500 3,000 Feet File: C:\Users\nathan.warren\Documents\ArcGIS\Projects\Blue Ridge Plating 0054\Blue Ridge Plating 0054.aprx Arden Blue Ridge Plating North CarolinaBuncombe 0054 FIGURE 1 Site Location TO No.: Site Name: Blue Ridge Plating 171 Glenn Bridge Road Arden, NC, Buncombe County 82.5284°W 35.46253°N Buncombe County United StatesEnvironmental Protection AgencyRegion 4 State:County:City: 7/17/2023 Date: nathan.warren Analyst: Legend Site Boundary Map Source:Bing Hybrid Imagery File: C:\Users\nathan.warren\Documents\ArcGIS\Projects\Blue Ridge Plating 0054\Blue Ridge Plating 0054.aprx / 0 100 200 Feet FIGURE 2 0054 Blue Ridge Plating Site Location TO No.: Site Name: North CarolinaBuncombeArden RockwoodRd OldShoalsRd AirportRd United StatesEnvironmental Protection AgencyRegion 4 State:County:City: 7/18/2023 Date: nathan.warren Analyst: MW13S/13D MW15S/15D MW16S/16D MW17S/17D MW18D MW20D Legend Site Boundary Monitoring Well Locations Map Source:Bing Hybrid Imagery File: C:\Users\nathan.warren\Documents\ArcGIS\Projects\Blue Ridge Plating 0054\Blue Ridge Plating 0054.aprx / 0 100 200 Feet FIGURE 3 0054 Blue Ridge Plating Monitoring Well Locations TO No.: Site Name: North CarolinaBuncombeArden RockwoodRd OldShoalsRd AirportRd ENCLOSURE 2 MONITORING WELL SAMPLING DATA SUMMARY TABLES (15 Pages) TABLE 1 LABORATORY ANALYTICAL RESULTS VOLATILE ORGANIC COMPOUNDS EPA MCL (m- and/or p-)Xylene 10000 0.5 U 0.5 U 0.044 J 0.5 U 1,1,1-Trichloroethane 200 0.55 0.5 U 0.72 9.8 1,1,2,2-Tetrachloroethane NA 0.5 U 0.5 U 0.5 U 0.5 U 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)NA 0.5 U 0.5 U 0.5 U 0.5 U 1,1,2-Trichloroethane 5 0.5 U 0.5 U 0.5 U 1.1 1,1-Dichloroethane NA 2.7 0.31 J 1.9 5.3 1,1-Dichloroethene (1,1-Dichloroethylene)7 8.7 0.5 U 6.2 47 1,2,3-Trichlorobenzene NA 0.5 U 0.5 U 0.5 U 0.5 U 1,2,3-Trichloropropane NA 0.5 U 0.5 U 0.5 U 0.5 U 1,2,4-Trichlorobenzene 70 0.5 U 0.5 U 0.5 U 0.5 U 1,2,4-Trimethylbenzene NA 0.5 U 0.5 U 0.5 U 0.5 U 1,2-Dibromo-3-Chloropropane (DBCP)0.2 0.5 U 0.5 U 0.5 U 0.5 U 1,2-Dibromoethane (EDB)0.05 0.5 U 0.5 U 0.5 U 0.5 U 1,2-Dichlorobenzene 600 0.5 U 0.5 U 0.5 U 0.5 U 1,2-Dichloroethane 5 0.5 U 0.5 U 0.5 U 0.5 U 1,2-Dichloropropane 5 0.5 UJ 0.5 UJ 0.5 UJ 0.5 UJ 1,3,5-Trimethylbenzene NA 0.5 U 0.5 U 0.5 U 0.5 U 1,3-Dichlorobenzene NA 0.5 U 0.5 U 0.5 U 0.5 U 1,4-Dichlorobenzene 75 0.5 U 0.5 U 0.5 U 0.5 U Acetone NA 5 UR 5 UR 5 UR 5 UR Benzene 5 0.5 U 0.5 U 0.5 U 0.5 U Bromochloromethane NA 0.5 U 0.5 U 0.5 U 0.5 U Bromodichloromethane 80 0.5 U 0.5 U 0.5 U 0.5 U Bromoform 80 0.5 U 0.5 U 0.5 U 0.5 U Bromomethane NA 0.5 UR 0.5 UR 0.5 UR 0.5 UR Carbon disulfide NA 0.5 U 0.5 U 0.5 U 0.5 U Carbon Tetrachloride 5 0.5 U 0.5 U 0.5 U 0.5 U Chlorobenzene 100 0.5 U 0.5 U 0.5 U 0.5 U Chloroethane NA 0.5 U 0.5 U 0.5 U 0.5 U Chloroform 80 0.27 J 0.5 U 0.5 U 0.5 U Chloromethane NA 0.5 U 0.5 U 0.5 U 0.5 U cis-1,2-Dichloroethene 70 0.34 J 0.23 J 0.19 J 0.55 cis-1,3-Dichloropropene NA 0.5 U 0.5 U 0.5 U 0.5 U Cyclohexane NA 0.5 U 0.5 U 0.5 U 0.5 U Dibromochloromethane 80 0.5 U 0.5 U 0.5 U 0.5 U Dichlorodifluoromethane (Freon 12)NA 0.5 U 0.5 U 0.5 U 0.5 U Ethyl Benzene 700 0.5 U 0.5 U 0.5 U 0.5 U Isopropylbenzene NA 0.5 U 0.5 U 0.5 U 0.5 U Methyl Acetate NA 0.5 UJ 0.5 UJ 0.5 UJ 0.5 UJ Methyl Butyl Ketone NA 5 U 5 U 5 U 5 U Methyl Ethyl Ketone NA 5 U 5 U 5 U 5 U Methyl Isobutyl Ketone NA 5 U 5 U 5 U 5 U Methyl T-Butyl Ether (MTBE)NA 0.35 J 0.5 U 0.48 J 0.5 U Methylcyclohexane NA 0.5 U 0.5 U 0.5 U 0.5 U Methylene Chloride 5 0.5 U 0.5 U 0.5 U 0.5 U o-Xylene 10000 0.5 U 0.5 U 0.5 U 0.5 U Styrene NA 0.5 U 0.5 U 0.5 U 5 U Tetrachloroethene (Tetrachloroethylene)5 13 0.15 J 9.6 26 Toluene 1000 0.069 J 0.036 J 0.11 J 0.05 J trans-1,2-Dichloroethene 100 0.5 U 0.5 U 0.5 U 0.42 J trans-1,3-Dichloropropene NA 0.5 U 0.5 U 0.5 U 0.5 U Trichloroethene (Trichloroethylene)5 1.1 0.38 J 0.62 2.8 Trichlorofluoromethane (Freon 11)NA 0.5 U 0.5 U 0.5 U 0.5 U Analyte MW13D MW13S MW15D MW15S Page 1 of 15 Blue Ridge Plating TABLE 1 LABORATORY ANALYTICAL RESULTS VOLATILE ORGANIC COMPOUNDS EPA MCL (m- and/or p-)Xylene 10000 1,1,1-Trichloroethane 200 1,1,2,2-Tetrachloroethane NA 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)NA 1,1,2-Trichloroethane 5 1,1-Dichloroethane NA 1,1-Dichloroethene (1,1-Dichloroethylene)7 1,2,3-Trichlorobenzene NA 1,2,3-Trichloropropane NA 1,2,4-Trichlorobenzene 70 1,2,4-Trimethylbenzene NA 1,2-Dibromo-3-Chloropropane (DBCP)0.2 1,2-Dibromoethane (EDB)0.05 1,2-Dichlorobenzene 600 1,2-Dichloroethane 5 1,2-Dichloropropane 5 1,3,5-Trimethylbenzene NA 1,3-Dichlorobenzene NA 1,4-Dichlorobenzene 75 Acetone NA Benzene 5 Bromochloromethane NA Bromodichloromethane 80 Bromoform 80 Bromomethane NA Carbon disulfide NA Carbon Tetrachloride 5 Chlorobenzene 100 Chloroethane NA Chloroform 80 Chloromethane NA cis-1,2-Dichloroethene 70 cis-1,3-Dichloropropene NA Cyclohexane NA Dibromochloromethane 80 Dichlorodifluoromethane (Freon 12)NA Ethyl Benzene 700 Isopropylbenzene NA Methyl Acetate NA Methyl Butyl Ketone NA Methyl Ethyl Ketone NA Methyl Isobutyl Ketone NA Methyl T-Butyl Ether (MTBE)NA Methylcyclohexane NA Methylene Chloride 5 o-Xylene 10000 Styrene NA Tetrachloroethene (Tetrachloroethylene)5 Toluene 1000 trans-1,2-Dichloroethene 100 trans-1,3-Dichloropropene NA Trichloroethene (Trichloroethylene)5 Trichlorofluoromethane (Freon 11)NA Analyte 0.5 U 0.5 U 0.049 J 0.5 U 0.23 J 0.5 U 0.11 J 0.13 J 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 2.2 0.5 U 0.46 J 0.17 J 4.7 0.5 U 1.2 0.75 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 UJ 0.5 UJ 0.5 UJ 0.5 UJ 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 5 UR 5 UR 5 UR 5 UR 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 UR 0.5 UR 0.5 UR 0.5 UR 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.85 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 UJ 0.5 UJ 0.5 UJ 0.5 UJ 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 0.5 U 0.5 U 0.36 J 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 5 U 5 U 0.5 U 1.9 0.5 U 2.5 0.47 J 0.036 J 0.5 U 0.15 J 0.041 J 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 7.4 0.5 U 0.11 J 0.12 J 0.5 U 0.5 U 0.5 U 0.5 U MW16S MW17D MW17SMW16D Page 2 of 15 Blue Ridge Plating TABLE 1 LABORATORY ANALYTICAL RESULTS VOLATILE ORGANIC COMPOUNDS EPA MCL (m- and/or p-)Xylene 10000 1,1,1-Trichloroethane 200 1,1,2,2-Tetrachloroethane NA 1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)NA 1,1,2-Trichloroethane 5 1,1-Dichloroethane NA 1,1-Dichloroethene (1,1-Dichloroethylene)7 1,2,3-Trichlorobenzene NA 1,2,3-Trichloropropane NA 1,2,4-Trichlorobenzene 70 1,2,4-Trimethylbenzene NA 1,2-Dibromo-3-Chloropropane (DBCP)0.2 1,2-Dibromoethane (EDB)0.05 1,2-Dichlorobenzene 600 1,2-Dichloroethane 5 1,2-Dichloropropane 5 1,3,5-Trimethylbenzene NA 1,3-Dichlorobenzene NA 1,4-Dichlorobenzene 75 Acetone NA Benzene 5 Bromochloromethane NA Bromodichloromethane 80 Bromoform 80 Bromomethane NA Carbon disulfide NA Carbon Tetrachloride 5 Chlorobenzene 100 Chloroethane NA Chloroform 80 Chloromethane NA cis-1,2-Dichloroethene 70 cis-1,3-Dichloropropene NA Cyclohexane NA Dibromochloromethane 80 Dichlorodifluoromethane (Freon 12)NA Ethyl Benzene 700 Isopropylbenzene NA Methyl Acetate NA Methyl Butyl Ketone NA Methyl Ethyl Ketone NA Methyl Isobutyl Ketone NA Methyl T-Butyl Ether (MTBE)NA Methylcyclohexane NA Methylene Chloride 5 o-Xylene 10000 Styrene NA Tetrachloroethene (Tetrachloroethylene)5 Toluene 1000 trans-1,2-Dichloroethene 100 trans-1,3-Dichloropropene NA Trichloroethene (Trichloroethylene)5 Trichlorofluoromethane (Freon 11)NA Analyte 0.5 U 0.5 U 0.5 U 0.36 J 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.13 J 1.5 0.25 J 5.9 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 UJ 0.5 UJ 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 5 UR 5 UR 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 UR 0.5 UR 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.67 0.5 U 0.5 U 0.16 J 0.71 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 UJ 0.5 UJ 5 U 5 U 5 U 5 U 5 U 5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 5 U 0.5 U 0.5 U 2.7 0.04 J 0.043 J 0.5 U 0.5 U 0.5 U 0.5 U 0.15 J 4.9 0.5 U 0.5 U MW18D MW20D Page 3 of 15 Blue Ridge Plating Notes:BOLD A highlighted result indicates the concentration exceeded the most restrictive comparison criteria listed in the EPA MCLs for groundwater with a 10^-6 risk level for carcinogens or a Hazard Quotient of 0.1 for non-carcinogens, dated May 2023. BOLD:Indicates analyte was positively identified at the associated value. D:Deep EPA:U.S. Environmental Protection Agency J: The analyte was positively identified; the associated value is the approximate concentration of the analyte in the sample. MCL:Maximum contaminant level mmddyy:month, day, year MW Monitoring Well NA:No MCL has been established for this analyte. UJ:The analyte was analyzed for, but was not detected at or above the associated value (reporting limit), which ug/L Micrograms per liter Page 4 of 15 Blue Ridge Plating TABLE 2 LABORATORY ANALYTICAL RESULTS SEMIVOLATILE ORGANIC COMPOUNDS EPA MCL (3-and/or 4-)Methylphenol NA 9.6 U 10 U 10 U 10 U 1,1-Biphenyl NA 4.8 U 5 U 5.2 U 5.2 U 1,2,4,5-Tetrachlorobenzene NA 4.8 U 5 U 5.2 U 5.2 U 1,4-Dioxane NA 7.4 2 U 4.4 1.6 J 1-Methylnaphthalene NA 4.8 U 4 J 5.2 U 10 J 2,3,4,6-Tetrachlorophenol NA 4.8 U 5 U 5.2 U 5.2 U 2,4,5-Trichlorophenol NA 4.8 UJ 5 U 5.2 UJ 5.2 U 2,4,6-Trichlorophenol NA 4.8 U 5 UJ 5.2 U 5.2 UJ 2,4-Dichlorophenol NA 4.8 U 5 U 5.2 U 5.2 U 2,4-Dimethylphenol NA 4.8 U 5 U 5.2 U 5.2 U 2,4-Dinitrophenol NA 9.6 UJ 5 U 10 UJ 5.2 U 2,4-Dinitrotoluene NA 4.8 U 10 UJ 5.2 U 10 UJ 2,6-Dinitrotoluene NA 4.8 U 5 U 5.2 U 5.2 U 2-Chloronaphthalene NA 4.8 U 5 U 5.2 U 5.2 U 2-Chlorophenol NA 4.8 U 5 U 5.2 U 5.2 U 2-Methyl-4,6-dinitrophenol NA 9.6 U 5 U 10 U 5.2 U 2-Methylnaphthalene NA 4.8 U 10 U 5.2 U 10 U 2-Methylphenol NA 9.6 U 5 U 10 U 5.2 U 2-Nitroaniline NA 4.8 U 10 U 5.2 U 10 U 2-Nitrophenol NA 4.8 U 5 U 5.2 U 5.2 U 3,3'-Dichlorobenzidine NA 9.6 UJ 5 U 10 UJ 5.2 U 3-Nitroaniline NA 9.6 U 10 UJ 10 U 10 UJ 4-Bromophenyl phenyl ether NA 4.8 U 10 U 5.2 U 10 U 4-Chloro-3-methylphenol NA 4.8 U 5 U 5.2 U 5.2 U 4-Chloroaniline NA 9.6 U 5 U 10 U 5.2 U 4-Chlorophenyl phenyl ether NA 4.8 U 10 U 5.2 U 10 U 4-Nitroaniline NA 9.6 UJ 5 U 10 UJ 5.2 U 4-Nitrophenol NA 9.6 UR 10 UJ 10 UR 10 UJ Acenaphthene NA 4.8 U 10 UR 5.2 U 10 UR Acenaphthylene NA 4.8 U 5 U 5.2 U 5.2 U Acetophenone NA 9.6 U 5 U 10 U 5.2 U Anthracene NA 4.8 U 10 U 5.2 U 10 U Atrazine 3 9.6 U 5 U 10 U 5.2 U Benzaldehyde NA 9.6 U 10 U 10 U 10 U Benzo(a)anthracene NA 4.8 U 10 U 5.2 U 10 U Benzo(a)pyrene 0.2 4.8 U 5 U 5.2 U 5.2 U Benzo(b)fluoranthene NA 4.8 U 5 U 5.2 U 5.2 U Benzo(g,h,i)perylene NA 4.8 U 5 U 5.2 U 5.2 U Benzo(k)fluoranthene NA 4.8 U 5 U 5.2 U 5.2 U Benzyl butyl phthalate NA 4.8 U 5 U 5.2 U 5.2 U Bis(2-chloro-1-methylethyl) ether NA 9.6 U 5 U 10 U 5.2 U Bis(2-chloroethoxy)methane NA 4.8 U 10 U 5.2 U 10 U bis(2-Chloroethyl) Ether NA 9.6 U 5 U 10 U 5.2 U Bis(2-ethylhexyl) phthalate 6 4.8 U 10 U 5.2 U 10 U Caprolactam NA 9.6 U 5 U 10 U 5.2 U Carbazole NA 9.6 U 10 U 10 U 10 U Chrysene NA 4.8 U 10 U 5.2 U 10 U Dibenzo(a,h)anthracene NA 4.8 U 5 U 5.2 U 5.2 U Dibenzofuran NA 4.8 U 5 U 5.2 U 5.2 U Diethyl phthalate NA 4.8 U 5 U 5.2 U 5.2 U Dimethyl phthalate NA 4.8 U 5 U 5.2 U 5.2 U Di-n-butylphthalate NA 4.8 U 5 U 5.2 U 5.2 U Di-n-octylphthalate NA 9.6 U 5 U 10 U 5.2 U Analyte MW13D MW13S MW15D MW15S Page 5 of 15 Blue Ridge Plating TABLE 2 LABORATORY ANALYTICAL RESULTS SEMIVOLATILE ORGANIC COMPOUNDS EPA MCLAnalyte MW13D MW13S MW15D MW15S Fluorene NA 4.8 U 5 U 5.2 U 5.2 U Hexachlorobenzene (HCB)1 4.8 U 5 U 5.2 U 5.2 U Hexachlorobutadiene NA 4.8 U 5 U 5.2 U 5.2 U Hexachlorocyclopentadiene (HCCP)50 9.6 UJ 5 U 10 UJ 5.2 U Hexachloroethane NA 4.8 U 10 UJ 5.2 U 10 UJ Indeno (1,2,3-cd) pyrene NA 4.8 U 5 U 5.2 U 5.2 U Isophorone NA 4.8 U 5 U 5.2 U 5.2 U Naphthalene NA 4.8 U 5 U 5.2 U 5.2 U Nitrobenzene NA 4.8 U 5 U 5.2 U 5.2 U n-Nitroso di-n-Propylamine NA 4.8 U 5 U 5.2 U 5.2 U n-Nitrosodiphenylamine/Diphenylamine NA 4.8 UJ 5 U 5.2 UJ 5.2 U Pentachlorophenol 1 9.6 UJ 5 UJ 10 UJ 5.2 UJ Phenanthrene NA 4.8 U 10 UJ 5.2 U 10 UJ Phenol NA 9.6 U 5 U 10 U 5.2 U Pyrene NA 4.8 U 10 U 5.2 U 10 U Page 6 of 15 Blue Ridge Plating TABLE 2 LABORATORY ANALYTICAL RESULTS SEMIVOLATILE ORGANIC COMPOUNDS EPA MCL (3-and/or 4-)Methylphenol NA 1,1-Biphenyl NA 1,2,4,5-Tetrachlorobenzene NA 1,4-Dioxane NA 1-Methylnaphthalene NA 2,3,4,6-Tetrachlorophenol NA 2,4,5-Trichlorophenol NA 2,4,6-Trichlorophenol NA 2,4-Dichlorophenol NA 2,4-Dimethylphenol NA 2,4-Dinitrophenol NA 2,4-Dinitrotoluene NA 2,6-Dinitrotoluene NA 2-Chloronaphthalene NA 2-Chlorophenol NA 2-Methyl-4,6-dinitrophenol NA 2-Methylnaphthalene NA 2-Methylphenol NA 2-Nitroaniline NA 2-Nitrophenol NA 3,3'-Dichlorobenzidine NA 3-Nitroaniline NA 4-Bromophenyl phenyl ether NA 4-Chloro-3-methylphenol NA 4-Chloroaniline NA 4-Chlorophenyl phenyl ether NA 4-Nitroaniline NA 4-Nitrophenol NA Acenaphthene NA Acenaphthylene NA Acetophenone NA Anthracene NA Atrazine 3 Benzaldehyde NA Benzo(a)anthracene NA Benzo(a)pyrene 0.2 Benzo(b)fluoranthene NA Benzo(g,h,i)perylene NA Benzo(k)fluoranthene NA Benzyl butyl phthalate NA Bis(2-chloro-1-methylethyl) ether NA Bis(2-chloroethoxy)methane NA bis(2-Chloroethyl) Ether NA Bis(2-ethylhexyl) phthalate 6 Caprolactam NA Carbazole NA Chrysene NA Dibenzo(a,h)anthracene NA Dibenzofuran NA Diethyl phthalate NA Dimethyl phthalate NA Di-n-butylphthalate NA Di-n-octylphthalate NA Analyte 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 2 2 U 1.4 J 2 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 UJ 5 UJ 5 UJ 5 UJ 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 UJ 10 UJ 10 UJ 10 UJ 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 UJ 10 UJ 10 UJ 10 UJ 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 10 UJ 10 UJ 10 U 10 U 10 UR 10 UR 10 UR 10 UR 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U MW16D MW16S MW17D MW17S Page 7 of 15 Blue Ridge Plating TABLE 2 LABORATORY ANALYTICAL RESULTS SEMIVOLATILE ORGANIC COMPOUNDS EPA MCL Analyte Fluorene NA Hexachlorobenzene (HCB)1 Hexachlorobutadiene NA Hexachlorocyclopentadiene (HCCP)50 Hexachloroethane NA Indeno (1,2,3-cd) pyrene NA Isophorone NA Naphthalene NA Nitrobenzene NA n-Nitroso di-n-Propylamine NA n-Nitrosodiphenylamine/Diphenylamine NA Pentachlorophenol 1 Phenanthrene NA Phenol NA Pyrene NA MW16D MW16S MW17D MW17S 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 UJ 10 UJ 10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 UJ 5 UJ 5 UJ 5 UJ 10 UJ 10 UJ 10 UJ 10 UJ 5 U 5 U 5 U 5 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U Page 8 of 15 Blue Ridge Plating TABLE 2 LABORATORY ANALYTICAL RESULTS SEMIVOLATILE ORGANIC COMPOUNDS EPA MCL (3-and/or 4-)Methylphenol NA 1,1-Biphenyl NA 1,2,4,5-Tetrachlorobenzene NA 1,4-Dioxane NA 1-Methylnaphthalene NA 2,3,4,6-Tetrachlorophenol NA 2,4,5-Trichlorophenol NA 2,4,6-Trichlorophenol NA 2,4-Dichlorophenol NA 2,4-Dimethylphenol NA 2,4-Dinitrophenol NA 2,4-Dinitrotoluene NA 2,6-Dinitrotoluene NA 2-Chloronaphthalene NA 2-Chlorophenol NA 2-Methyl-4,6-dinitrophenol NA 2-Methylnaphthalene NA 2-Methylphenol NA 2-Nitroaniline NA 2-Nitrophenol NA 3,3'-Dichlorobenzidine NA 3-Nitroaniline NA 4-Bromophenyl phenyl ether NA 4-Chloro-3-methylphenol NA 4-Chloroaniline NA 4-Chlorophenyl phenyl ether NA 4-Nitroaniline NA 4-Nitrophenol NA Acenaphthene NA Acenaphthylene NA Acetophenone NA Anthracene NA Atrazine 3 Benzaldehyde NA Benzo(a)anthracene NA Benzo(a)pyrene 0.2 Benzo(b)fluoranthene NA Benzo(g,h,i)perylene NA Benzo(k)fluoranthene NA Benzyl butyl phthalate NA Bis(2-chloro-1-methylethyl) ether NA Bis(2-chloroethoxy)methane NA bis(2-Chloroethyl) Ether NA Bis(2-ethylhexyl) phthalate 6 Caprolactam NA Carbazole NA Chrysene NA Dibenzo(a,h)anthracene NA Dibenzofuran NA Diethyl phthalate NA Dimethyl phthalate NA Di-n-butylphthalate NA Di-n-octylphthalate NA Analyte 10 U 10 U 5 U 5 U 5 U 5 U 2 U 2.7 5 U 5 U 5 U 5 U 5 UJ 5 UJ 5 U 5 U 5 U 5 U 5 U 5 U 10 UJ 10 UJ 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U 5 U 5 U 10 U 10 U 5 U 5 U 5 U 5 U 10 UJ 10 UJ 10 U 10 U 5 U 5 U 5 U 5 U 10 U 10 U 5 U 5 U 10 U 10 U 10 UR 10 UR 5 U 5 U 5 U 5 U 10 U 10 U 5 U 5 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U 5 U 5 U 10 U 10 U 5 U 5 U 10 U 10 U 10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U MW18D MW20D Page 9 of 15 Blue Ridge Plating TABLE 2 LABORATORY ANALYTICAL RESULTS SEMIVOLATILE ORGANIC COMPOUNDS EPA MCL Analyte Fluorene NA Hexachlorobenzene (HCB)1 Hexachlorobutadiene NA Hexachlorocyclopentadiene (HCCP)50 Hexachloroethane NA Indeno (1,2,3-cd) pyrene NA Isophorone NA Naphthalene NA Nitrobenzene NA n-Nitroso di-n-Propylamine NA n-Nitrosodiphenylamine/Diphenylamine NA Pentachlorophenol 1 Phenanthrene NA Phenol NA Pyrene NA MW18D MW20D 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 UJ 5 UJ 10 UJ 10 UJ 5 U 5 U 10 U 10 U 5 U 5 U Page 10 of 15 Blue Ridge Plating Notes:BOLD A highlighted result indicates the concentration exceeded the most restrictive comparison criteria listed in the EPA MCLs for groundwater with a 10^-6 risk level for carcinogens or a Hazard Quotient of 0.1 for non-carcinogens, dated May 2023. BOLD:Indicates analyte was positively identified at the associated value. D:Deep EPA:U.S. Environmental Protection Agency J: The analyte was positively identified; the associated value is the approximate concentration of the analyte in the sample. MCL:Maximum contaminant level mmddyy:month, day, year MW Monitoring Well NA:No MCL has been established for this analyte. UJ:The analyte was analyzed for, but was not detected at or above the associated value (reporting limit), which ug/L Micrograms per liter Page 11 of 15 Blue Ridge Plating TABLE 3 LABORATORY ANALYTICAL RESULTS METALS EPA MCL Aluminum NA 550 J 96 J 230 J 1000 J Antimony 6 2 U 2 U 2 U 2 U Arsenic 10 1 U 1 U 1 U 1.1 Barium 2000 34 36 26 390 Beryllium 4 1 U 1 U 1 U 1 U Cadmium 5 0.17 J 1 U 1 U 1 U Calcium NA 5900 280 J 2800 110 J Chromium 100 7.1 0.97 J 1.1 J 1.1 J Cobalt NA 3.3 1.8 1 U 4.8 Copper 1300 1.1 J 2 U 2 U 4.2 Iron NA 900 310 590 1300 Lead 15 1 U 1 U 1 U 1 U Magnesium NA 1300 1200 810 2100 Manganese NA 180 70 65 110 Mercury 2 0.2 U 0.2 U 0.2 U 0.2 U Nickel NA 4.7 1.9 0.63 J 6.9 Potassium NA 1500 1000 1500 3900 Selenium 50 5 U 2 J 5 U 5 U Silver NA 1 U 1 U 1 U 1 U Sodium NA 4900 26000 2400 15000 Thallium 2 1 U 0.057 J 1 U 0.15 J Vanadium NA 0.88 J 5 U 0.58 J 1.3 J Zinc NA 6 9.9 17 45 Analyte MW13D MW13S MW15D MW15S Page 12 of 15 Blue Ridge Plating TABLE 3 LABORATORY ANALYTICAL RESULTS METALS EPA MCL Aluminum NA Antimony 6 Arsenic 10 Barium 2000 Beryllium 4 Cadmium 5 Calcium NA Chromium 100 Cobalt NA Copper 1300 Iron NA Lead 15 Magnesium NA Manganese NA Mercury 2 Nickel NA Potassium NA Selenium 50 Silver NA Sodium NA Thallium 2 Vanadium NA Analyte 390 J 660 J 360 J 4600 J 2 U 2 U 2 U 2 U 1 U 0.77 J 1 U 0.67 J 140 57 23 120 1 U 2.1 U,O 1 U 1 U 0.22 J 2.2 1 U 1 U 14000 7300 3300 10000 1.2 J 2.3 2 7.5 2.5 19 1 U 7.9 2 U 2 U 1.1 J 4.7 570 4500 660 7100 1 U 0.83 J 1 U 2.5 6400 5800 920 9500 630 450 45 400 0.2 U 0.2 U 0.2 U 0.2 U 5.9 14 1.3 10 2900 1500 1300 2900 5 U 5 U 5 U 1 J 1 U 1 U 1 U 1 U 6800 8600 4700 7900 1 U 0.72 J 1 U 0.18 J 0.95 J 2.8 J 1.2 J 6.3 MW16S MW17D MW17SMW16D Page 13 of 15 Blue Ridge Plating TABLE 3 LABORATORY ANALYTICAL RESULTS METALS EPA MCL Aluminum NA Antimony 6 Arsenic 10 Barium 2000 Beryllium 4 Cadmium 5 Calcium NA Chromium 100 Cobalt NA Copper 1300 Iron NA Lead 15 Magnesium NA Manganese NA Mercury 2 Nickel NA Potassium NA Selenium 50 Silver NA Sodium NA Thallium 2 Vanadium NA Analyte 870 J 930 J 2 U 2 U 5.7 1 U 110 37 4.1 U 1 U 1 U 1 U 8800 7600 2.5 1.8 J 3.4 1 U 2 U 1.3 J 110000 1600 1.3 0.99 J 4700 2400 100 26 0.2 U 0.2 U 1.4 2.5 2300 2400 3.8 J 5 U 1 U 1 U 11000 6300 0.17 J 1 U 4.4 J 1.9 J MW18D MW20D Page 14 of 15 Blue Ridge Plating Notes: BOLD A highlighted result indicates the concentration exceeded the most restrictive comparison criteria listed in the EPA MCLs for groundwater with a 10^-6 risk level for carcinogens or a Hazard Quotient of 0.1 for non-carcinogens, dated May 2023.BOLD:Indicates analyte was positively identified at the associated value. D:Deep EPA:U.S. Environmental Protection Agency J: The analyte was positively identified; the associated value is the approximate concentration of the analyte in the sample. MCL:Maximum contaminant level mmddyy:month, day, year MW:Monitoring Well NA:No MCL has been established for this analyte. UJ:The analyte was analyzed for, but was not detected at or above the associated value (reporting limit), which is approximate due to deficiencies in one or more quality control criteria. ug/L Micrograms per liter Page 15 of 15 Blue Ridge Plating ENCLOSURE 3 PHOTOGRAPHIC LOG (7 Pages) C-1 Task Order 0064 Blue Ridge Plating OFFICIAL PHOTOGRAPH NO. 1 U.S. ENVIRONMENTAL PROTECTION AGENCY Task Order: Location: Buncombe County Orientation: Date: Photographer: Superfund Technical Assessment and Response Witness: Subject: C-2 Task Order 0064 Blue Ridge Plating OFFICIAL PHOTOGRAPH NO. 2 U.S. ENVIRONMENTAL PROTECTION AGENCY Task Order: Location: Buncombe County Orientation: Date: Photographer:Witness: Subject: C-3 Task Order 0064 Blue Ridge Plating OFFICIAL PHOTOGRAPH NO. 3 U.S. ENVIRONMENTAL PROTECTION AGENCY Task Order: Location: Buncombe County Orientation: Date: Photographer:Witness: Subject: C-4 Task Order 0064 Blue Ridge Plating OFFICIAL PHOTOGRAPH NO. 4 U.S. ENVIRONMENTAL PROTECTION AGENCY Task Order: Location: Buncombe County Orientation: Date: Photographer:Witness: Subject: C-5 Task Order 0064 Blue Ridge Plating OFFICIAL PHOTOGRAPH NO. 5 U.S. ENVIRONMENTAL PROTECTION AGENCY Task Order: Location: Buncombe County Orientation: Date: Photographer:Witness: Subject: C-6 Task Order 0064 Blue Ridge Plating OFFICIAL PHOTOGRAPH NO. 6 U.S. ENVIRONMENTAL PROTECTION AGENCY Task Order: Location: Buncombe County Orientation: Date: Photographer:Witness: Subject: C-7 Task Order 0064 Blue Ridge Plating OFFICIAL PHOTOGRAPH NO. 7 U.S. ENVIRONMENTAL PROTECTION AGENCY Task Order: Location: Buncombe County Orientation: Date: Photographer:Witness: Subject: ENCLOSURE 4 MONITORING WELL SAMPLING FORMS AND FIELD NOTES (10 Pages) ENCLOSURE 5 TETRA TECH REVIEW OF FIELD QUAILTY CONTROL SAMPLES (1 Page) 1 TO No. 68HE0421F0064 Sampling and Analysis Support (Blue Ridge Plating) Review of Field Quality Control Samples Date: June 21, 2023 Project No.: Project Name: Reviewer Name: The following is a summary of the review performed by Tetra Tech for the Contract Laboratory Program (CLP) analytical data packages for groundwater samples collected between February 28 and March 1, 2023 at the Blue Ridge Plating site. This review was performed on the following field quality control (QC) samples: field blanks, trip blanks, and field duplicate samples. The review of the field QC samples was performed in accordance with the Quality Assurance Project Plan, Superfund Technical Assessment and Response Team (START V), EPA Region 4, Revision 2 (February 2021), the EPA National Functional Guidelines (NFG) for Organic Superfund Methods Data Review (November 2020), and the EPA NFGs for Inorganic Superfund Methods Data Review (November 2020). This review was performed because the U.S. Environmental Protection Agency, Region 4, Laboratory Services and Applied Science Division, Office of Quality Assurance does not review these types of field QC samples as part of their validation effort. This policy was stated during a data validation webinar held on February 17, 2011. The webinar was attended by personnel from all 10 EPA Regions, as well as personnel from various agencies that utilize the EPA CLP and Regional Laboratories for analytical support. Field Blanks: Field blanks are generally aqueous samples that are exposed to the sampling environment or equipment at the time of sampling. Typically, one field blank is collected per field event of one week or less per lot of high-purity water used; for field events longer than one week, field blanks are collected at a frequency of one per week per lot of high-purity water used. One field blank was collected during the field sampling event. The field blank BRP-FL-01 had a detection of mercury. However, all associated samples were non-detect and no qualifications were applied. Trip Blanks: Trip blanks are used to assess the potential for sample contamination during handling, shipment, and storage. One trip blank was included within every shipping cooler of liquid or solid samples to be analyzed for VOCs. One trip blank, BRP-TW-01, was utilized for the sampling event for this project and no analytes were detected. Field Duplicate Samples: Field duplicate collection frequencies (one per twenty samples for each matrix) were met for this data set. A total of one groundwater field duplicate pair was collected for this sampling event. Analytical results for each analyte in field duplicate aqueous sample pairs must fall within less than or equal to 50 percent (%) relative percent difference (RPD). However, if at least one of the two results of the pair is below its minimum reporting limit (MRL) or one of the results is non-detect, then the absolute difference between the two results must be less than or equal to the MRL (using the MRL in the difference for the non-detect results). When results for a field duplicate sample pair fall outside the control limit for a particular analyte, the results for that analyte are qualified as estimated (flagged J or UJ) with an undetermined bias in both the parent sample and its field duplicate sample. For the field duplicate sample pair analyzed, all results met the acceptance criteria discussed above. ATTACHMENT 1 LABORATORY ANALYTICAL DATA PACKAGES (109 Pages) D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth May 24, 2023 MEMORANDUM SUBJECT: FROM: FINAL Analytical Report Project: 23-0155, Blue Ridge Plating 4LSASD-QAPSB Jeffrey Wilmoth Quality Assurance Section, Chemist Quality Assurance Section Keith Harris, ChiefTHRU: TO:Craig Zeller Attached are the final results for the analytical groups listed below. These analyses were performed in accordance with the associated contract Statement Of Work (SOW). In general, project data quality objectives have not been used to evaluate these data prior to release by the Quality Assurance Section. For a listing of specific data qualifiers and explanations, please refer to the Data Qualifier Definitions included in this report. Analyses Included in this report:Method Used: Semi Volatile Organics (SVOA) Semivolatile organic compounds CLP BNA (Water) Volatile Organics (VOA) Volatile organic compounds CLP VOA (Water) 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 1 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Report Narrative for Work Order: C231105 Analysis: SVOA Subject: Organic Data Review and Validation Report Site Name: Blue Ridge Plating, Arden NC Case No.: 50606, Project No.: 23-0155, Work Order Nos.: C231105, C231103 (PES) ELEMENT Sample I.D. Nos.: C231105-01-13, C231103-01-02 (PES) Sampling Date(s): 2/28/23, 3/1/23 Validated Time of Sample Receipt: 3/3/23 Laboratory Performing Organic Analyses: Eurofins Burlington, South Burlington VT Date Received from Lab: 3/23/23 (at SMO portal) Analyses conducted : Trace Volatiles, Semivolatile Extractables The ESAT Work Team has reviewed the above-captioned CLP data package consisting of 13 water samples for Trace Volatiles and Semivolatile Extractables according to the contract Statement of Work SFAM01.1 (SOW) and EPA guidelines. The analytical results were reported in one sample delivery group (SDG) by the laboratory. In addition to the field samples, the laboratory analyzed two performance evaluation samples (PESs) for evaluating the laboratory’s performance with using the methods. A Stage 4 validation consisting of an electronic/manual review (S4VEM) was performed on the organic samples submitted for this case. The data package presents acceptable technical performance with qualifications. The laboratory satisfied all contractual and technical holding time limits. All results associated with erratic initial calibration (ICAL) and/or continuing calibration (CCAL) performance were flagged “J” with the appropriate Element® qualifiers (CLP16 and/or QC-1). The percent difference between an ICAL and a second source verification standard exceeded 20% for 3,3’-Dichlorobenzidine. The associated results were qualified “J” (QC-3). Deuterated Monitoring Compounds (DMCs) were used as surrogates in each sample for GC/MS analysis to monitor extraction efficiency. Pertinent data quality factors are discussed below. Trace Volatiles 1.The PES recoveries analyzed for Trace Volatiles were scored within limits by the web-based SPS Web software except for 1,2-Dichloropropane, which was scored Warning Low. Associated results were all non-detected and were qualified “UJ” (CLP-25). 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 2 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth 2.The laboratory encountered poor instrument responses for Acetone and Bromomethane in ICALs and/or CCALs. All associated results were non-detected and were qualified “UR” (CLP17 and/or CLP32). Semivolatile Extractables 1.The PES recoveries analyzed for Semivolatile Extractables were scored within limits by the web-based SPS Web software. Therefore, no qualifiers were applied based on these criteria. 2.The laboratory encountered poor instrument response for 4-Nitrophenol in CCALs. All associated results were non-detected and were qualified “UR” (CLP32). Data qualification factors are explained by the Region 4 - specific qualifier definitions which are included elsewhere in this report. Further details are provided in the complete data review report, which is on file in the Region 4 LSASD Records Center. cc: Nardina Turner 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 3 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Date CollectedMatrixLaboratory IDSample ID SAMPLES INCLUDED IN THIS REPORT Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 MD#D# CAB2CAB2BRP-FL-01 C231105-01 Field Blank 2/28/23 17:00 CAB1BRP-TW-01 C231105-02 Trip Blank - Water 2/28/23 15:00 CAA1CAA1BRP-MW13D-022823 C231105-03 Groundwater 2/28/23 18:15 CAA0CAA0BRP-MW13S-030123 C231105-04 Groundwater 3/1/23 08:10 CAA3CAA3BRP-MW15D-030123 C231105-05 Groundwater 3/1/23 10:00 CAA2CAA2BRP-MW15S-030123 C231105-06 Groundwater 3/1/23 09:15 CAA5CAA5BRP-MW16D-022823 C231105-07 Groundwater 2/28/23 16:50 CAA4CAA4BRP-MW16S-022823 C231105-08 Groundwater 2/28/23 16:10 CAB0CAB0BRP-MW16S-022823-DUP C231105-09 Groundwater 2/28/23 16:10 CAA6CAA6BRP-MW17D-030123 C231105-10 Groundwater 3/1/23 10:50 CAA9CAA9BRP-MW17S-030123 C231105-11 Groundwater 3/1/23 12:55 CAA8CAA8BRP-MW18D-022823 C231105-12 Groundwater 2/28/23 14:50 CAA7CAA7BRP-MW20D-022823 C231105-13 Groundwater 2/28/23 13:40 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 4 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth DATA QUALIFIER DEFINITIONS U The analyte was not detected at or above the reporting limit. CLP01 Concentration reported is less than the lowest standard on calibration curve CLP15 TIC Results Reported as Identified by Lab - IDs Not Verified CLP16 Initial Calibration Response Erratic CLP17 Initial Calibration Relative Response Outside Method Control Limits CLP25 PE sample recovery scored as warning-low. CLP32 Continuing Calibration Relative Response Outside Method Control Limits J The identification of the analyte is acceptable; the reported value is an estimate. N There is presumptive evidence that the analyte is present; the analyte is reported as a tentative identification. NJ Presumptive evidence that analyte is present; reported as a tentative identification with an estimated value. QC-1 Analyte concentration low in continuing calibration verification standard QC-3 Analyte calibration criteria not met R The presence or absence of the analyte can not be determined from the data due to severe quality control problems. The data are rejected and considered unusable. ACRONYMS AND ABBREVIATIONS CAS Chemical Abstracts Service Note: Analytes with no known CAS identifiers have been assigned codes beginning with "E", the EPA ID as assigned by the EPA Substance Registry System (www.epa.gov/srs), or beginning with "R4-", a unique identifier assigned by the EPA Region 4 laboratory. MDL Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and reported with a 99% confidence that the analyte concentration is greater than zero. MRL Minimum Reporting Limit - Analyte concentration that corresponds to the lowest demonstrated level of acceptable quantitation. The MRL is sample-specific and accounts for preparation weights and volumes, dilutions, and moisture content of soil/sediments. TIC Tentatively Identified Compound - An analyte identified based on a match with the instrument software's mass spectral library. A calibration standard has not been analyzed to confirm the compound's identification or the estimated concentration reported. 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 5 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-FL-01 C231105-01 Matrix:Field Blank Date Collected:2/28/23 17:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB2 ETB MD No: CAB2 ETB Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U71-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U75-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.10.50 U75-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 6 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-FL-01 C231105-01 Matrix:Field Blank Date Collected:2/28/23 17:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB2 ETB MD No: CAB2 ETB Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.10.50 U127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.50 U108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.10.50 U79-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 7 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-FL-01 C231105-01 Matrix:Field Blank Date Collected:2/28/23 17:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB2 ETB MD No: CAB2 ETB Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 5 3/08/23 CLP SFAM01.13/08/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 8 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-FL-01 C231105-01 Matrix:Field Blank Date Collected:2/28/23 17:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB2 ETB MD No: CAB2 ETB Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U1319-77-3 5.0 3/06/231,1-Biphenyl ug/L 3/16/23 CLP SFAM01.1 B5.0 U92-52-4 5.0 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-94-3 2.0 3/06/231,4-Dioxane ug/L 3/16/23 CLP SFAM01.1 B2.0 U123-91-1 5.0 3/06/231-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U90-12-0 5.0 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U58-90-2 5.0 3/06/232,4,5-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-195-95-4 5.0 3/06/232,4,6-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-06-2 5.0 3/06/232,4-Dichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U120-83-2 5.0 3/06/232,4-Dimethylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.0 3/06/232,4-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U121-14-2 5.0 3/06/232,6-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U606-20-2 5.0 3/06/232-Chloronaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-58-7 5.0 3/06/232-Chlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U534-52-1 5.0 3/06/232-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-57-6 10 3/06/232-Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U95-48-7 5.0 3/06/232-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-74-4 5.0 3/06/232-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/16/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U99-09-2 5.0 3/06/234-Bromophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U101-55-3 5.0 3/06/234-Chloro-3-methylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/16/23 CLP SFAM01.1 B10U106-47-8 5.0 3/06/234-Chlorophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U100-01-6 10 3/06/234-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 9 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-FL-01 C231105-01 Matrix:Field Blank Date Collected:2/28/23 17:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB2 ETB MD No: CAB2 ETB Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.0 3/06/23Acenaphtheneug/L 3/16/23 CLP SFAM01.1 B5.0 U83-32-9 5.0 3/06/23Acenaphthyleneug/L 3/16/23 CLP SFAM01.1 B5.0 U208-96-8 10 3/06/23Acetophenoneug/L 3/16/23 CLP SFAM01.1 B10U98-86-2 5.0 3/06/23Anthraceneug/L 3/16/23 CLP SFAM01.1 B5.0 U120-12-7 10 3/06/23Atrazineug/L 3/16/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/16/23 CLP SFAM01.1 B10U100-52-7 5.0 3/06/23Benzo(a)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U56-55-3 5.0 3/06/23Benzo(a)pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U50-32-8 5.0 3/06/23Benzo(b)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U205-99-2 5.0 3/06/23Benzo(g,h,i)perylene ug/L 3/16/23 CLP SFAM01.1 B5.0 U191-24-2 5.0 3/06/23Benzo(k)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U207-08-9 5.0 3/06/23Benzyl butyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/16/23 CLP SFAM01.1 B10U108-60-1 5.0 3/06/23Bis(2-chloroethoxy)methane ug/L 3/16/23 CLP SFAM01.1 B5.0 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/16/23 CLP SFAM01.1 B10U111-44-4 5.0 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U117-81-7 10 3/06/23Caprolactamug/L 3/16/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/16/23 CLP SFAM01.1 B10U86-74-8 5.0 3/06/23Chryseneug/L 3/16/23 CLP SFAM01.1 B5.0 U218-01-9 5.0 3/06/23Dibenzo(a,h)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U53-70-3 5.0 3/06/23Dibenzofuranug/L 3/16/23 CLP SFAM01.1 B5.0 U132-64-9 5.0 3/06/23Diethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-66-2 5.0 3/06/23Dimethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U131-11-3 5.0 3/06/23Di-n-butylphthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/16/23 CLP SFAM01.1 B10U117-84-0 5.0 3/06/23Fluorantheneug/L 3/16/23 CLP SFAM01.1 B5.0 U206-44-0 5.0 3/06/23Fluoreneug/L 3/16/23 CLP SFAM01.1 B5.0 U86-73-7 5.0 3/06/23Hexachlorobenzene (HCB)ug/L 3/16/23 CLP SFAM01.1 B5.0 U118-74-1 5.0 3/06/23Hexachlorobutadieneug/L 3/16/23 CLP SFAM01.1 B5.0 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 10 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-FL-01 C231105-01 Matrix:Field Blank Date Collected:2/28/23 17:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB2 ETB MD No: CAB2 ETB Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/16/23 CLP SFAM01.1 B10U77-47-4 5.0 3/06/23Hexachloroethaneug/L 3/16/23 CLP SFAM01.1 B5.0 U67-72-1 5.0 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U193-39-5 5.0 3/06/23Isophoroneug/L 3/16/23 CLP SFAM01.1 B5.0 U78-59-1 5.0 3/06/23Naphthaleneug/L 3/16/23 CLP SFAM01.1 B5.0 U91-20-3 5.0 3/06/23Nitrobenzeneug/L 3/16/23 CLP SFAM01.1 B5.0 U98-95-3 5.0 3/06/23n-Nitroso di-n-Propylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U621-64-7 5.0 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.0 3/06/23Phenanthreneug/L 3/16/23 CLP SFAM01.1 B5.0 U85-01-8 10 3/06/23Phenolug/L 3/16/23 CLP SFAM01.1 B10U108-95-2 5.0 3/06/23Pyreneug/L 3/16/23 CLP SFAM01.1 B5.0 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/16/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 11 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-TW-01 C231105-02 Matrix:Trip Blank - Water Date Collected:2/28/23 15:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB1 ETB MD No: Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U71-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U75-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.10.50 U75-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 12 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-TW-01 C231105-02 Matrix:Trip Blank - Water Date Collected:2/28/23 15:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB1 ETB MD No: Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.10.50 U127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.50 U108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.10.50 U79-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 13 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-TW-01 C231105-02 Matrix:Trip Blank - Water Date Collected:2/28/23 15:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB1 ETB MD No: Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 3/08/23 3/08/23 CLP SFAM01.1Petroleum Product N, CLP15R4-6500 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 14 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW13D-022823 C231105-03 Matrix:Groundwater Date Collected:2/28/23 18:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA1 ETB MD No: CAA1 ETB Station ID:MW13D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.5571-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.12.775-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.18.775-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP32, CLP17 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 15 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW13D-022823 C231105-03 Matrix:Groundwater Date Collected:2/28/23 18:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA1 ETB MD No: CAA1 ETB Station ID:MW13D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.27 J, CLP0167-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.34 J, CLP01156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.35 J, CLP011634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.113127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.069 J, CLP01108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.11.179-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 16 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW13D-022823 C231105-03 Matrix:Groundwater Date Collected:2/28/23 18:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA1 ETB MD No: CAA1 ETB Station ID:MW13D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 3/08/23 3/08/23 CLP SFAM01.1Petroleum Product N, CLP15R4-6500 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 17 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW13D-022823 C231105-03 Matrix:Groundwater Date Collected:2/28/23 18:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA1 ETB MD No: CAA1 ETB Station ID:MW13D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 9.6 3/06/23(3-and/or 4-)Methylphenol ug/L 3/10/23 CLP SFAM01.1 B9.6 U1319-77-3 4.8 3/06/231,1-Biphenyl ug/L 3/10/23 CLP SFAM01.1 B4.8 U92-52-4 4.8 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/10/23 CLP SFAM01.1 B4.8 U95-94-3 1.9 3/06/231,4-Dioxane ug/L 3/10/23 CLP SFAM01.1 B7.4123-91-1 4.8 3/06/231-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B4.8 U90-12-0 4.8 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/10/23 CLP SFAM01.1 B4.8 U58-90-2 4.8 3/06/232,4,5-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B4.8 U, J, QC-195-95-4 4.8 3/06/232,4,6-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B4.8 U88-06-2 4.8 3/06/232,4-Dichlorophenol ug/L 3/10/23 CLP SFAM01.1 B4.8 U120-83-2 4.8 3/06/232,4-Dimethylphenol ug/L 3/10/23 CLP SFAM01.1 B4.8 U105-67-9 9.6 3/06/232,4-Dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B9.6 U, J, CLP16, QC-1 51-28-5 4.8 3/06/232,4-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B4.8 U121-14-2 4.8 3/06/232,6-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B4.8 U606-20-2 4.8 3/06/232-Chloronaphthalene ug/L 3/10/23 CLP SFAM01.1 B4.8 U91-58-7 4.8 3/06/232-Chlorophenol ug/L 3/10/23 CLP SFAM01.1 B4.8 U95-57-8 9.6 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B9.6 U534-52-1 4.8 3/06/232-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B4.8 U91-57-6 9.6 3/06/232-Methylphenol ug/L 3/10/23 CLP SFAM01.1 B9.6 U95-48-7 4.8 3/06/232-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B4.8 U88-74-4 4.8 3/06/232-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B4.8 U88-75-5 9.6 3/06/233,3'-Dichlorobenzidine ug/L 3/10/23 CLP SFAM01.1 B9.6 U, J, QC-391-94-1 9.6 3/06/233-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B9.6 U99-09-2 4.8 3/06/234-Bromophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B4.8 U101-55-3 4.8 3/06/234-Chloro-3-methylphenol ug/L 3/10/23 CLP SFAM01.1 B4.8 U59-50-7 9.6 3/06/234-Chloroaniline ug/L 3/10/23 CLP SFAM01.1 B9.6 U106-47-8 4.8 3/06/234-Chlorophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B4.8 U7005-72-3 9.6 3/06/234-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B9.6 U, J, QC-1100-01-6 9.6 3/06/234-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B9.6 U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 18 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW13D-022823 C231105-03 Matrix:Groundwater Date Collected:2/28/23 18:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA1 ETB MD No: CAA1 ETB Station ID:MW13D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 4.8 3/06/23Acenaphtheneug/L 3/10/23 CLP SFAM01.1 B4.8 U83-32-9 4.8 3/06/23Acenaphthyleneug/L 3/10/23 CLP SFAM01.1 B4.8 U208-96-8 9.6 3/06/23Acetophenoneug/L 3/10/23 CLP SFAM01.1 B9.6 U98-86-2 4.8 3/06/23Anthraceneug/L 3/10/23 CLP SFAM01.1 B4.8 U120-12-7 9.6 3/06/23Atrazineug/L 3/10/23 CLP SFAM01.1 B9.6 U1912-24-9 9.6 3/06/23Benzaldehydeug/L 3/10/23 CLP SFAM01.1 B9.6 U100-52-7 4.8 3/06/23Benzo(a)anthracene ug/L 3/10/23 CLP SFAM01.1 B4.8 U56-55-3 4.8 3/06/23Benzo(a)pyrene ug/L 3/10/23 CLP SFAM01.1 B4.8 U50-32-8 4.8 3/06/23Benzo(b)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B4.8 U205-99-2 4.8 3/06/23Benzo(g,h,i)perylene ug/L 3/10/23 CLP SFAM01.1 B4.8 U191-24-2 4.8 3/06/23Benzo(k)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B4.8 U207-08-9 4.8 3/06/23Benzyl butyl phthalate ug/L 3/10/23 CLP SFAM01.1 B4.8 U85-68-7 9.6 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/10/23 CLP SFAM01.1 B9.6 U108-60-1 4.8 3/06/23Bis(2-chloroethoxy)methane ug/L 3/10/23 CLP SFAM01.1 B4.8 U111-91-1 9.6 3/06/23bis(2-Chloroethyl) Ether ug/L 3/10/23 CLP SFAM01.1 B9.6 U111-44-4 4.8 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/10/23 CLP SFAM01.1 B4.8 U117-81-7 9.6 3/06/23Caprolactamug/L 3/10/23 CLP SFAM01.1 B9.6 U105-60-2 9.6 3/06/23Carbazoleug/L 3/10/23 CLP SFAM01.1 B9.6 U86-74-8 4.8 3/06/23Chryseneug/L 3/10/23 CLP SFAM01.1 B4.8 U218-01-9 4.8 3/06/23Dibenzo(a,h)anthracene ug/L 3/10/23 CLP SFAM01.1 B4.8 U53-70-3 4.8 3/06/23Dibenzofuranug/L 3/10/23 CLP SFAM01.1 B4.8 U132-64-9 4.8 3/06/23Diethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B4.8 U84-66-2 4.8 3/06/23Dimethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B4.8 U131-11-3 4.8 3/06/23Di-n-butylphthalate ug/L 3/10/23 CLP SFAM01.1 B4.8 U84-74-2 9.6 3/06/23Di-n-octylphthalate ug/L 3/10/23 CLP SFAM01.1 B9.6 U117-84-0 4.8 3/06/23Fluorantheneug/L 3/10/23 CLP SFAM01.1 B4.8 U206-44-0 4.8 3/06/23Fluoreneug/L 3/10/23 CLP SFAM01.1 B4.8 U86-73-7 4.8 3/06/23Hexachlorobenzene (HCB)ug/L 3/10/23 CLP SFAM01.1 B4.8 U118-74-1 4.8 3/06/23Hexachlorobutadieneug/L 3/10/23 CLP SFAM01.1 B4.8 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 19 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW13D-022823 C231105-03 Matrix:Groundwater Date Collected:2/28/23 18:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA1 ETB MD No: CAA1 ETB Station ID:MW13D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 9.6 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/10/23 CLP SFAM01.1 B9.6 U, J, QC-177-47-4 4.8 3/06/23Hexachloroethaneug/L 3/10/23 CLP SFAM01.1 B4.8 U67-72-1 4.8 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/10/23 CLP SFAM01.1 B4.8 U193-39-5 4.8 3/06/23Isophoroneug/L 3/10/23 CLP SFAM01.1 B4.8 U78-59-1 4.8 3/06/23Naphthaleneug/L 3/10/23 CLP SFAM01.1 B4.8 U91-20-3 4.8 3/06/23Nitrobenzeneug/L 3/10/23 CLP SFAM01.1 B4.8 U98-95-3 4.8 3/06/23n-Nitroso di-n-Propylamine ug/L 3/10/23 CLP SFAM01.1 B4.8 U621-64-7 4.8 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/10/23 CLP SFAM01.1 B4.8 U, J, QC-1122-39-4 9.6 3/06/23Pentachlorophenolug/L 3/10/23 CLP SFAM01.1 B9.6 U, J, QC-1, CLP16 87-86-5 4.8 3/06/23Phenanthreneug/L 3/10/23 CLP SFAM01.1 B4.8 U85-01-8 9.6 3/06/23Phenolug/L 3/10/23 CLP SFAM01.1 B9.6 U108-95-2 4.8 3/06/23Pyreneug/L 3/10/23 CLP SFAM01.1 B4.8 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/10/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 20 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW13S-030123 C231105-04 Matrix:Groundwater Date Collected:3/1/23 8:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA0 ETB MD No: CAA0 ETB Station ID:MW13S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U71-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.31 J, CLP0175-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.10.50 U75-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP32, CLP17 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 21 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW13S-030123 C231105-04 Matrix:Groundwater Date Collected:3/1/23 8:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA0 ETB MD No: CAA0 ETB Station ID:MW13S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.23 J, CLP01156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.10.15 J, CLP01127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.036 J, CLP01108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.10.38 J, CLP0179-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 22 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW13S-030123 C231105-04 Matrix:Groundwater Date Collected:3/1/23 8:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA0 ETB MD No: CAA0 ETB Station ID:MW13S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 3/08/23 3/08/23 CLP SFAM01.1Petroleum Product N, CLP15R4-6500 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 23 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW13S-030123 C231105-04 Matrix:Groundwater Date Collected:3/1/23 8:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA0 ETB MD No: CAA0 ETB Station ID:MW13S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U1319-77-3 5.0 3/06/231,1-Biphenyl ug/L 3/10/23 CLP SFAM01.1 B5.0 U92-52-4 5.0 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/10/23 CLP SFAM01.1 B5.0 U95-94-3 2.0 3/06/231,4-Dioxane ug/L 3/10/23 CLP SFAM01.1 B2.0 U123-91-1 5.0 3/06/231-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.0 U90-12-0 5.0 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U58-90-2 5.0 3/06/232,4,5-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U, J, QC-195-95-4 5.0 3/06/232,4,6-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U88-06-2 5.0 3/06/232,4-Dichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U120-83-2 5.0 3/06/232,4-Dimethylphenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.0 3/06/232,4-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.0 U121-14-2 5.0 3/06/232,6-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.0 U606-20-2 5.0 3/06/232-Chloronaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.0 U91-58-7 5.0 3/06/232-Chlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U534-52-1 5.0 3/06/232-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.0 U91-57-6 10 3/06/232-Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U95-48-7 5.0 3/06/232-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B5.0 U88-74-4 5.0 3/06/232-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U99-09-2 5.0 3/06/234-Bromophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.0 U101-55-3 5.0 3/06/234-Chloro-3-methylphenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/10/23 CLP SFAM01.1 B10U106-47-8 5.0 3/06/234-Chlorophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.0 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-1100-01-6 10 3/06/234-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 24 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW13S-030123 C231105-04 Matrix:Groundwater Date Collected:3/1/23 8:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA0 ETB MD No: CAA0 ETB Station ID:MW13S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.0 3/06/23Acenaphtheneug/L 3/10/23 CLP SFAM01.1 B5.0 U83-32-9 5.0 3/06/23Acenaphthyleneug/L 3/10/23 CLP SFAM01.1 B5.0 U208-96-8 10 3/06/23Acetophenoneug/L 3/10/23 CLP SFAM01.1 B10U98-86-2 5.0 3/06/23Anthraceneug/L 3/10/23 CLP SFAM01.1 B5.0 U120-12-7 10 3/06/23Atrazineug/L 3/10/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/10/23 CLP SFAM01.1 B10U100-52-7 5.0 3/06/23Benzo(a)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.0 U56-55-3 5.0 3/06/23Benzo(a)pyrene ug/L 3/10/23 CLP SFAM01.1 B5.0 U50-32-8 5.0 3/06/23Benzo(b)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.0 U205-99-2 5.0 3/06/23Benzo(g,h,i)perylene ug/L 3/10/23 CLP SFAM01.1 B5.0 U191-24-2 5.0 3/06/23Benzo(k)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.0 U207-08-9 5.0 3/06/23Benzyl butyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/10/23 CLP SFAM01.1 B10U108-60-1 5.0 3/06/23Bis(2-chloroethoxy)methane ug/L 3/10/23 CLP SFAM01.1 B5.0 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/10/23 CLP SFAM01.1 B10U111-44-4 5.0 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U117-81-7 10 3/06/23Caprolactamug/L 3/10/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/10/23 CLP SFAM01.1 B10U86-74-8 5.0 3/06/23Chryseneug/L 3/10/23 CLP SFAM01.1 B5.0 U218-01-9 5.0 3/06/23Dibenzo(a,h)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.0 U53-70-3 5.0 3/06/23Dibenzofuranug/L 3/10/23 CLP SFAM01.1 B5.0 U132-64-9 5.0 3/06/23Diethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U84-66-2 5.0 3/06/23Dimethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U131-11-3 5.0 3/06/23Di-n-butylphthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/10/23 CLP SFAM01.1 B10U117-84-0 5.0 3/06/23Fluorantheneug/L 3/10/23 CLP SFAM01.1 B5.0 U206-44-0 5.0 3/06/23Fluoreneug/L 3/10/23 CLP SFAM01.1 B5.0 U86-73-7 5.0 3/06/23Hexachlorobenzene (HCB)ug/L 3/10/23 CLP SFAM01.1 B5.0 U118-74-1 5.0 3/06/23Hexachlorobutadieneug/L 3/10/23 CLP SFAM01.1 B5.0 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 25 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW13S-030123 C231105-04 Matrix:Groundwater Date Collected:3/1/23 8:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA0 ETB MD No: CAA0 ETB Station ID:MW13S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-177-47-4 5.0 3/06/23Hexachloroethaneug/L 3/10/23 CLP SFAM01.1 B5.0 U67-72-1 5.0 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/10/23 CLP SFAM01.1 B5.0 U193-39-5 5.0 3/06/23Isophoroneug/L 3/10/23 CLP SFAM01.1 B5.0 U78-59-1 5.0 3/06/23Naphthaleneug/L 3/10/23 CLP SFAM01.1 B5.0 U91-20-3 5.0 3/06/23Nitrobenzeneug/L 3/10/23 CLP SFAM01.1 B5.0 U98-95-3 5.0 3/06/23n-Nitroso di-n-Propylamine ug/L 3/10/23 CLP SFAM01.1 B5.0 U621-64-7 5.0 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/10/23 CLP SFAM01.1 B5.0 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.0 3/06/23Phenanthreneug/L 3/10/23 CLP SFAM01.1 B5.0 U85-01-8 10 3/06/23Phenolug/L 3/10/23 CLP SFAM01.1 B10U108-95-2 5.0 3/06/23Pyreneug/L 3/10/23 CLP SFAM01.1 B5.0 U129-00-0 Tentatively Identified Compounds: 3/06/23 CLP SFAM01.1 B3/10/23ug/L413-Docosenamide, (Z)-NJ, CLP15112-84-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 26 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW15D-030123 C231105-05 Matrix:Groundwater Date Collected:3/1/23 10:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA3 ETB MD No: CAA3 ETB Station ID:MW15D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.044 J, CLP01R4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.7271-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.11.975-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.16.275-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 27 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW15D-030123 C231105-05 Matrix:Groundwater Date Collected:3/1/23 10:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA3 ETB MD No: CAA3 ETB Station ID:MW15D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.19 J, CLP01156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.48 J, CLP011634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.19.6127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.11 J, CLP01108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.10.6279-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 28 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW15D-030123 C231105-05 Matrix:Groundwater Date Collected:3/1/23 10:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA3 ETB MD No: CAA3 ETB Station ID:MW15D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 3/08/23 3/08/23 CLP SFAM01.1Petroleum Product N, CLP15R4-6500 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 29 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW15D-030123 C231105-05 Matrix:Groundwater Date Collected:3/1/23 10:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA3 ETB MD No: CAA3 ETB Station ID:MW15D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U1319-77-3 5.2 3/06/231,1-Biphenyl ug/L 3/10/23 CLP SFAM01.1 B5.2 U92-52-4 5.2 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/10/23 CLP SFAM01.1 B5.2 U95-94-3 2.1 3/06/231,4-Dioxane ug/L 3/10/23 CLP SFAM01.1 B4.4123-91-1 5.2 3/06/231-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.2 U90-12-0 5.2 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U58-90-2 5.2 3/06/232,4,5-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U, J, QC-195-95-4 5.2 3/06/232,4,6-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U88-06-2 5.2 3/06/232,4-Dichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U120-83-2 5.2 3/06/232,4-Dimethylphenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.2 3/06/232,4-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.2 U121-14-2 5.2 3/06/232,6-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.2 U606-20-2 5.2 3/06/232-Chloronaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.2 U91-58-7 5.2 3/06/232-Chlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U534-52-1 5.2 3/06/232-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.2 U91-57-6 10 3/06/232-Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U95-48-7 5.2 3/06/232-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B5.2 U88-74-4 5.2 3/06/232-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U99-09-2 5.2 3/06/234-Bromophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.2 U101-55-3 5.2 3/06/234-Chloro-3-methylphenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/10/23 CLP SFAM01.1 B10U106-47-8 5.2 3/06/234-Chlorophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.2 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-1100-01-6 10 3/06/234-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 30 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW15D-030123 C231105-05 Matrix:Groundwater Date Collected:3/1/23 10:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA3 ETB MD No: CAA3 ETB Station ID:MW15D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.2 3/06/23Acenaphtheneug/L 3/10/23 CLP SFAM01.1 B5.2 U83-32-9 5.2 3/06/23Acenaphthyleneug/L 3/10/23 CLP SFAM01.1 B5.2 U208-96-8 10 3/06/23Acetophenoneug/L 3/10/23 CLP SFAM01.1 B10U98-86-2 5.2 3/06/23Anthraceneug/L 3/10/23 CLP SFAM01.1 B5.2 U120-12-7 10 3/06/23Atrazineug/L 3/10/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/10/23 CLP SFAM01.1 B10U100-52-7 5.2 3/06/23Benzo(a)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.2 U56-55-3 5.2 3/06/23Benzo(a)pyrene ug/L 3/10/23 CLP SFAM01.1 B5.2 U50-32-8 5.2 3/06/23Benzo(b)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.2 U205-99-2 5.2 3/06/23Benzo(g,h,i)perylene ug/L 3/10/23 CLP SFAM01.1 B5.2 U191-24-2 5.2 3/06/23Benzo(k)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.2 U207-08-9 5.2 3/06/23Benzyl butyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/10/23 CLP SFAM01.1 B10U108-60-1 5.2 3/06/23Bis(2-chloroethoxy)methane ug/L 3/10/23 CLP SFAM01.1 B5.2 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/10/23 CLP SFAM01.1 B10U111-44-4 5.2 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U117-81-7 10 3/06/23Caprolactamug/L 3/10/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/10/23 CLP SFAM01.1 B10U86-74-8 5.2 3/06/23Chryseneug/L 3/10/23 CLP SFAM01.1 B5.2 U218-01-9 5.2 3/06/23Dibenzo(a,h)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.2 U53-70-3 5.2 3/06/23Dibenzofuranug/L 3/10/23 CLP SFAM01.1 B5.2 U132-64-9 5.2 3/06/23Diethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U84-66-2 5.2 3/06/23Dimethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U131-11-3 5.2 3/06/23Di-n-butylphthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/10/23 CLP SFAM01.1 B10U117-84-0 5.2 3/06/23Fluorantheneug/L 3/10/23 CLP SFAM01.1 B5.2 U206-44-0 5.2 3/06/23Fluoreneug/L 3/10/23 CLP SFAM01.1 B5.2 U86-73-7 5.2 3/06/23Hexachlorobenzene (HCB)ug/L 3/10/23 CLP SFAM01.1 B5.2 U118-74-1 5.2 3/06/23Hexachlorobutadieneug/L 3/10/23 CLP SFAM01.1 B5.2 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 31 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW15D-030123 C231105-05 Matrix:Groundwater Date Collected:3/1/23 10:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA3 ETB MD No: CAA3 ETB Station ID:MW15D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-177-47-4 5.2 3/06/23Hexachloroethaneug/L 3/10/23 CLP SFAM01.1 B5.2 U67-72-1 5.2 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/10/23 CLP SFAM01.1 B5.2 U193-39-5 5.2 3/06/23Isophoroneug/L 3/10/23 CLP SFAM01.1 B5.2 U78-59-1 5.2 3/06/23Naphthaleneug/L 3/10/23 CLP SFAM01.1 B5.2 U91-20-3 5.2 3/06/23Nitrobenzeneug/L 3/10/23 CLP SFAM01.1 B5.2 U98-95-3 5.2 3/06/23n-Nitroso di-n-Propylamine ug/L 3/10/23 CLP SFAM01.1 B5.2 U621-64-7 5.2 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/10/23 CLP SFAM01.1 B5.2 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.2 3/06/23Phenanthreneug/L 3/10/23 CLP SFAM01.1 B5.2 U85-01-8 10 3/06/23Phenolug/L 3/10/23 CLP SFAM01.1 B10U108-95-2 5.2 3/06/23Pyreneug/L 3/10/23 CLP SFAM01.1 B5.2 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/10/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 32 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW15S-030123 C231105-06 Matrix:Groundwater Date Collected:3/1/23 9:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA2 ETB MD No: CAA2 ETB Station ID:MW15S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.19.871-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.11.179-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.15.375-34-3 2.5 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.14775-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 33 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW15S-030123 C231105-06 Matrix:Groundwater Date Collected:3/1/23 9:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA2 ETB MD No: CAA2 ETB Station ID:MW15S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.55156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 2.5 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.126127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.050 J, CLP01108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.42 J, CLP01156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.12.879-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 34 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW15S-030123 C231105-06 Matrix:Groundwater Date Collected:3/1/23 9:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA2 ETB MD No: CAA2 ETB Station ID:MW15S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 5 3/08/23 CLP SFAM01.13/08/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 35 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW15S-030123 C231105-06 Matrix:Groundwater Date Collected:3/1/23 9:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA2 ETB MD No: CAA2 ETB Station ID:MW15S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U1319-77-3 5.2 3/06/231,1-Biphenyl ug/L 3/10/23 CLP SFAM01.1 B5.2 U92-52-4 5.2 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/10/23 CLP SFAM01.1 B5.2 U95-94-3 2.1 3/06/231,4-Dioxane ug/L 3/10/23 CLP SFAM01.1 B1.6 J, CLP01123-91-1 5.2 3/06/231-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.2 U90-12-0 5.2 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U58-90-2 5.2 3/06/232,4,5-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U, J, QC-195-95-4 5.2 3/06/232,4,6-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U88-06-2 5.2 3/06/232,4-Dichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U120-83-2 5.2 3/06/232,4-Dimethylphenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.2 3/06/232,4-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.2 U121-14-2 5.2 3/06/232,6-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.2 U606-20-2 5.2 3/06/232-Chloronaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.2 U91-58-7 5.2 3/06/232-Chlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U534-52-1 5.2 3/06/232-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.2 U91-57-6 10 3/06/232-Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U95-48-7 5.2 3/06/232-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B5.2 U88-74-4 5.2 3/06/232-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U99-09-2 5.2 3/06/234-Bromophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.2 U101-55-3 5.2 3/06/234-Chloro-3-methylphenol ug/L 3/10/23 CLP SFAM01.1 B5.2 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/10/23 CLP SFAM01.1 B10U106-47-8 5.2 3/06/234-Chlorophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.2 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-1100-01-6 10 3/06/234-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 36 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW15S-030123 C231105-06 Matrix:Groundwater Date Collected:3/1/23 9:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA2 ETB MD No: CAA2 ETB Station ID:MW15S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.2 3/06/23Acenaphtheneug/L 3/10/23 CLP SFAM01.1 B5.2 U83-32-9 5.2 3/06/23Acenaphthyleneug/L 3/10/23 CLP SFAM01.1 B5.2 U208-96-8 10 3/06/23Acetophenoneug/L 3/10/23 CLP SFAM01.1 B10U98-86-2 5.2 3/06/23Anthraceneug/L 3/10/23 CLP SFAM01.1 B5.2 U120-12-7 10 3/06/23Atrazineug/L 3/10/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/10/23 CLP SFAM01.1 B10U100-52-7 5.2 3/06/23Benzo(a)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.2 U56-55-3 5.2 3/06/23Benzo(a)pyrene ug/L 3/10/23 CLP SFAM01.1 B5.2 U50-32-8 5.2 3/06/23Benzo(b)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.2 U205-99-2 5.2 3/06/23Benzo(g,h,i)perylene ug/L 3/10/23 CLP SFAM01.1 B5.2 U191-24-2 5.2 3/06/23Benzo(k)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.2 U207-08-9 5.2 3/06/23Benzyl butyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/10/23 CLP SFAM01.1 B10U108-60-1 5.2 3/06/23Bis(2-chloroethoxy)methane ug/L 3/10/23 CLP SFAM01.1 B5.2 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/10/23 CLP SFAM01.1 B10U111-44-4 5.2 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U117-81-7 10 3/06/23Caprolactamug/L 3/10/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/10/23 CLP SFAM01.1 B10U86-74-8 5.2 3/06/23Chryseneug/L 3/10/23 CLP SFAM01.1 B5.2 U218-01-9 5.2 3/06/23Dibenzo(a,h)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.2 U53-70-3 5.2 3/06/23Dibenzofuranug/L 3/10/23 CLP SFAM01.1 B5.2 U132-64-9 5.2 3/06/23Diethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U84-66-2 5.2 3/06/23Dimethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U131-11-3 5.2 3/06/23Di-n-butylphthalate ug/L 3/10/23 CLP SFAM01.1 B5.2 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/10/23 CLP SFAM01.1 B10U117-84-0 5.2 3/06/23Fluorantheneug/L 3/10/23 CLP SFAM01.1 B5.2 U206-44-0 5.2 3/06/23Fluoreneug/L 3/10/23 CLP SFAM01.1 B5.2 U86-73-7 5.2 3/06/23Hexachlorobenzene (HCB)ug/L 3/10/23 CLP SFAM01.1 B5.2 U118-74-1 5.2 3/06/23Hexachlorobutadieneug/L 3/10/23 CLP SFAM01.1 B5.2 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 37 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW15S-030123 C231105-06 Matrix:Groundwater Date Collected:3/1/23 9:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA2 ETB MD No: CAA2 ETB Station ID:MW15S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-177-47-4 5.2 3/06/23Hexachloroethaneug/L 3/10/23 CLP SFAM01.1 B5.2 U67-72-1 5.2 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/10/23 CLP SFAM01.1 B5.2 U193-39-5 5.2 3/06/23Isophoroneug/L 3/10/23 CLP SFAM01.1 B5.2 U78-59-1 5.2 3/06/23Naphthaleneug/L 3/10/23 CLP SFAM01.1 B5.2 U91-20-3 5.2 3/06/23Nitrobenzeneug/L 3/10/23 CLP SFAM01.1 B5.2 U98-95-3 5.2 3/06/23n-Nitroso di-n-Propylamine ug/L 3/10/23 CLP SFAM01.1 B5.2 U621-64-7 5.2 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/10/23 CLP SFAM01.1 B5.2 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.2 3/06/23Phenanthreneug/L 3/10/23 CLP SFAM01.1 B5.2 U85-01-8 10 3/06/23Phenolug/L 3/10/23 CLP SFAM01.1 B10U108-95-2 5.2 3/06/23Pyreneug/L 3/10/23 CLP SFAM01.1 B5.2 U129-00-0 Tentatively Identified Compounds: 3/06/23 CLP SFAM01.1 B3/10/23ug/L1013-Docosenamide, (Z)-NJ, CLP15112-84-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 38 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW16D-022823 C231105-07 Matrix:Groundwater Date Collected:2/28/23 16:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA5 ETB MD No: CAA5 ETB Station ID:MW16D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.23 J, CLP0171-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.12.275-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.14.775-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 39 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW16D-022823 C231105-07 Matrix:Groundwater Date Collected:2/28/23 16:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA5 ETB MD No: CAA5 ETB Station ID:MW16D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.85156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.11.9127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.036 J, CLP01108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.17.479-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 40 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW16D-022823 C231105-07 Matrix:Groundwater Date Collected:2/28/23 16:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA5 ETB MD No: CAA5 ETB Station ID:MW16D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 3/08/23 3/08/23 CLP SFAM01.1Petroleum Product N, CLP15R4-6500 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 41 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW16D-022823 C231105-07 Matrix:Groundwater Date Collected:2/28/23 16:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA5 ETB MD No: CAA5 ETB Station ID:MW16D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U1319-77-3 5.0 3/06/231,1-Biphenyl ug/L 3/10/23 CLP SFAM01.1 B5.0 U92-52-4 5.0 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/10/23 CLP SFAM01.1 B5.0 U95-94-3 2.0 3/06/231,4-Dioxane ug/L 3/10/23 CLP SFAM01.1 B2.0123-91-1 5.0 3/06/231-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.0 U90-12-0 5.0 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U58-90-2 5.0 3/06/232,4,5-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U, J, QC-195-95-4 5.0 3/06/232,4,6-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U88-06-2 5.0 3/06/232,4-Dichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U120-83-2 5.0 3/06/232,4-Dimethylphenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.0 3/06/232,4-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.0 U121-14-2 5.0 3/06/232,6-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.0 U606-20-2 5.0 3/06/232-Chloronaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.0 U91-58-7 5.0 3/06/232-Chlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U534-52-1 5.0 3/06/232-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.0 U91-57-6 10 3/06/232-Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U95-48-7 5.0 3/06/232-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B5.0 U88-74-4 5.0 3/06/232-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U99-09-2 5.0 3/06/234-Bromophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.0 U101-55-3 5.0 3/06/234-Chloro-3-methylphenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/10/23 CLP SFAM01.1 B10U106-47-8 5.0 3/06/234-Chlorophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.0 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-1100-01-6 10 3/06/234-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 42 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW16D-022823 C231105-07 Matrix:Groundwater Date Collected:2/28/23 16:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA5 ETB MD No: CAA5 ETB Station ID:MW16D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.0 3/06/23Acenaphtheneug/L 3/10/23 CLP SFAM01.1 B5.0 U83-32-9 5.0 3/06/23Acenaphthyleneug/L 3/10/23 CLP SFAM01.1 B5.0 U208-96-8 10 3/06/23Acetophenoneug/L 3/10/23 CLP SFAM01.1 B10U98-86-2 5.0 3/06/23Anthraceneug/L 3/10/23 CLP SFAM01.1 B5.0 U120-12-7 10 3/06/23Atrazineug/L 3/10/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/10/23 CLP SFAM01.1 B10U100-52-7 5.0 3/06/23Benzo(a)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.0 U56-55-3 5.0 3/06/23Benzo(a)pyrene ug/L 3/10/23 CLP SFAM01.1 B5.0 U50-32-8 5.0 3/06/23Benzo(b)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.0 U205-99-2 5.0 3/06/23Benzo(g,h,i)perylene ug/L 3/10/23 CLP SFAM01.1 B5.0 U191-24-2 5.0 3/06/23Benzo(k)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.0 U207-08-9 5.0 3/06/23Benzyl butyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/10/23 CLP SFAM01.1 B10U108-60-1 5.0 3/06/23Bis(2-chloroethoxy)methane ug/L 3/10/23 CLP SFAM01.1 B5.0 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/10/23 CLP SFAM01.1 B10U111-44-4 5.0 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U117-81-7 10 3/06/23Caprolactamug/L 3/10/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/10/23 CLP SFAM01.1 B10U86-74-8 5.0 3/06/23Chryseneug/L 3/10/23 CLP SFAM01.1 B5.0 U218-01-9 5.0 3/06/23Dibenzo(a,h)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.0 U53-70-3 5.0 3/06/23Dibenzofuranug/L 3/10/23 CLP SFAM01.1 B5.0 U132-64-9 5.0 3/06/23Diethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U84-66-2 5.0 3/06/23Dimethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U131-11-3 5.0 3/06/23Di-n-butylphthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/10/23 CLP SFAM01.1 B10U117-84-0 5.0 3/06/23Fluorantheneug/L 3/10/23 CLP SFAM01.1 B5.0 U206-44-0 5.0 3/06/23Fluoreneug/L 3/10/23 CLP SFAM01.1 B5.0 U86-73-7 5.0 3/06/23Hexachlorobenzene (HCB)ug/L 3/10/23 CLP SFAM01.1 B5.0 U118-74-1 5.0 3/06/23Hexachlorobutadieneug/L 3/10/23 CLP SFAM01.1 B5.0 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 43 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW16D-022823 C231105-07 Matrix:Groundwater Date Collected:2/28/23 16:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA5 ETB MD No: CAA5 ETB Station ID:MW16D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-177-47-4 5.0 3/06/23Hexachloroethaneug/L 3/10/23 CLP SFAM01.1 B5.0 U67-72-1 5.0 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/10/23 CLP SFAM01.1 B5.0 U193-39-5 5.0 3/06/23Isophoroneug/L 3/10/23 CLP SFAM01.1 B5.0 U78-59-1 5.0 3/06/23Naphthaleneug/L 3/10/23 CLP SFAM01.1 B5.0 U91-20-3 5.0 3/06/23Nitrobenzeneug/L 3/10/23 CLP SFAM01.1 B5.0 U98-95-3 5.0 3/06/23n-Nitroso di-n-Propylamine ug/L 3/10/23 CLP SFAM01.1 B5.0 U621-64-7 5.0 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/10/23 CLP SFAM01.1 B5.0 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.0 3/06/23Phenanthreneug/L 3/10/23 CLP SFAM01.1 B5.0 U85-01-8 10 3/06/23Phenolug/L 3/10/23 CLP SFAM01.1 B10U108-95-2 5.0 3/06/23Pyreneug/L 3/10/23 CLP SFAM01.1 B5.0 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/10/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 44 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823 C231105-08 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA4 ETB MD No: CAA4 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U71-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U75-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.10.50 U75-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 45 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823 C231105-08 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA4 ETB MD No: CAA4 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.10.50 U127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.50 U108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.10.50 U79-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 46 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823 C231105-08 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA4 ETB MD No: CAA4 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 5 3/08/23 CLP SFAM01.13/08/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 47 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823 C231105-08 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA4 ETB MD No: CAA4 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U1319-77-3 5.0 3/06/231,1-Biphenyl ug/L 3/10/23 CLP SFAM01.1 B5.0 U92-52-4 5.0 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/10/23 CLP SFAM01.1 B5.0 U95-94-3 2.0 3/06/231,4-Dioxane ug/L 3/10/23 CLP SFAM01.1 B2.0 U123-91-1 5.0 3/06/231-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.0 U90-12-0 5.0 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U58-90-2 5.0 3/06/232,4,5-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U, J, QC-195-95-4 5.0 3/06/232,4,6-Trichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U88-06-2 5.0 3/06/232,4-Dichlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U120-83-2 5.0 3/06/232,4-Dimethylphenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.0 3/06/232,4-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.0 U121-14-2 5.0 3/06/232,6-Dinitrotoluene ug/L 3/10/23 CLP SFAM01.1 B5.0 U606-20-2 5.0 3/06/232-Chloronaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.0 U91-58-7 5.0 3/06/232-Chlorophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U534-52-1 5.0 3/06/232-Methylnaphthalene ug/L 3/10/23 CLP SFAM01.1 B5.0 U91-57-6 10 3/06/232-Methylphenol ug/L 3/10/23 CLP SFAM01.1 B10U95-48-7 5.0 3/06/232-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B5.0 U88-74-4 5.0 3/06/232-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U99-09-2 5.0 3/06/234-Bromophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.0 U101-55-3 5.0 3/06/234-Chloro-3-methylphenol ug/L 3/10/23 CLP SFAM01.1 B5.0 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/10/23 CLP SFAM01.1 B10U106-47-8 5.0 3/06/234-Chlorophenyl phenyl ether ug/L 3/10/23 CLP SFAM01.1 B5.0 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-1100-01-6 10 3/06/234-Nitrophenol ug/L 3/10/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 48 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823 C231105-08 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA4 ETB MD No: CAA4 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.0 3/06/23Acenaphtheneug/L 3/10/23 CLP SFAM01.1 B5.0 U83-32-9 5.0 3/06/23Acenaphthyleneug/L 3/10/23 CLP SFAM01.1 B5.0 U208-96-8 10 3/06/23Acetophenoneug/L 3/10/23 CLP SFAM01.1 B10U98-86-2 5.0 3/06/23Anthraceneug/L 3/10/23 CLP SFAM01.1 B5.0 U120-12-7 10 3/06/23Atrazineug/L 3/10/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/10/23 CLP SFAM01.1 B10U100-52-7 5.0 3/06/23Benzo(a)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.0 U56-55-3 5.0 3/06/23Benzo(a)pyrene ug/L 3/10/23 CLP SFAM01.1 B5.0 U50-32-8 5.0 3/06/23Benzo(b)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.0 U205-99-2 5.0 3/06/23Benzo(g,h,i)perylene ug/L 3/10/23 CLP SFAM01.1 B5.0 U191-24-2 5.0 3/06/23Benzo(k)fluoranthene ug/L 3/10/23 CLP SFAM01.1 B5.0 U207-08-9 5.0 3/06/23Benzyl butyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/10/23 CLP SFAM01.1 B10U108-60-1 5.0 3/06/23Bis(2-chloroethoxy)methane ug/L 3/10/23 CLP SFAM01.1 B5.0 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/10/23 CLP SFAM01.1 B10U111-44-4 5.0 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U117-81-7 10 3/06/23Caprolactamug/L 3/10/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/10/23 CLP SFAM01.1 B10U86-74-8 5.0 3/06/23Chryseneug/L 3/10/23 CLP SFAM01.1 B5.0 U218-01-9 5.0 3/06/23Dibenzo(a,h)anthracene ug/L 3/10/23 CLP SFAM01.1 B5.0 U53-70-3 5.0 3/06/23Dibenzofuranug/L 3/10/23 CLP SFAM01.1 B5.0 U132-64-9 5.0 3/06/23Diethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U84-66-2 5.0 3/06/23Dimethyl phthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U131-11-3 5.0 3/06/23Di-n-butylphthalate ug/L 3/10/23 CLP SFAM01.1 B5.0 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/10/23 CLP SFAM01.1 B10U117-84-0 5.0 3/06/23Fluorantheneug/L 3/10/23 CLP SFAM01.1 B5.0 U206-44-0 5.0 3/06/23Fluoreneug/L 3/10/23 CLP SFAM01.1 B5.0 U86-73-7 5.0 3/06/23Hexachlorobenzene (HCB)ug/L 3/10/23 CLP SFAM01.1 B5.0 U118-74-1 5.0 3/06/23Hexachlorobutadieneug/L 3/10/23 CLP SFAM01.1 B5.0 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 49 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823 C231105-08 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA4 ETB MD No: CAA4 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/10/23 CLP SFAM01.1 B10U, J, QC-177-47-4 5.0 3/06/23Hexachloroethaneug/L 3/10/23 CLP SFAM01.1 B5.0 U67-72-1 5.0 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/10/23 CLP SFAM01.1 B5.0 U193-39-5 5.0 3/06/23Isophoroneug/L 3/10/23 CLP SFAM01.1 B5.0 U78-59-1 5.0 3/06/23Naphthaleneug/L 3/10/23 CLP SFAM01.1 B5.0 U91-20-3 5.0 3/06/23Nitrobenzeneug/L 3/10/23 CLP SFAM01.1 B5.0 U98-95-3 5.0 3/06/23n-Nitroso di-n-Propylamine ug/L 3/10/23 CLP SFAM01.1 B5.0 U621-64-7 5.0 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/10/23 CLP SFAM01.1 B5.0 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/10/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.0 3/06/23Phenanthreneug/L 3/10/23 CLP SFAM01.1 B5.0 U85-01-8 10 3/06/23Phenolug/L 3/10/23 CLP SFAM01.1 B10U108-95-2 5.0 3/06/23Pyreneug/L 3/10/23 CLP SFAM01.1 B5.0 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/10/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 50 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823-DUP C231105-09 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB0 ETB MD No: CAB0 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U71-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U75-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.10.50 U75-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 51 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823-DUP C231105-09 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB0 ETB MD No: CAB0 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.10.50 U127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.50 U108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.10.50 U79-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 52 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823-DUP C231105-09 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB0 ETB MD No: CAB0 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 5 3/08/23 CLP SFAM01.13/08/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 53 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823-DUP C231105-09 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB0 ETB MD No: CAB0 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U1319-77-3 5.2 3/06/231,1-Biphenyl ug/L 3/16/23 CLP SFAM01.1 B5.2 U92-52-4 5.2 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/16/23 CLP SFAM01.1 B5.2 U95-94-3 2.1 3/06/231,4-Dioxane ug/L 3/16/23 CLP SFAM01.1 B2.1 U123-91-1 5.2 3/06/231-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.2 U90-12-0 5.2 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.2 U58-90-2 5.2 3/06/232,4,5-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.2 U, J, QC-195-95-4 5.2 3/06/232,4,6-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.2 U88-06-2 5.2 3/06/232,4-Dichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.2 U120-83-2 5.2 3/06/232,4-Dimethylphenol ug/L 3/16/23 CLP SFAM01.1 B5.2 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.2 3/06/232,4-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.2 U121-14-2 5.2 3/06/232,6-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.2 U606-20-2 5.2 3/06/232-Chloronaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.2 U91-58-7 5.2 3/06/232-Chlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.2 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U534-52-1 5.2 3/06/232-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.2 U91-57-6 10 3/06/232-Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U95-48-7 5.2 3/06/232-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B5.2 U88-74-4 5.2 3/06/232-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B5.2 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/16/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U99-09-2 5.2 3/06/234-Bromophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.2 U101-55-3 5.2 3/06/234-Chloro-3-methylphenol ug/L 3/16/23 CLP SFAM01.1 B5.2 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/16/23 CLP SFAM01.1 B10U106-47-8 5.2 3/06/234-Chlorophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.2 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U100-01-6 10 3/06/234-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 54 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823-DUP C231105-09 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB0 ETB MD No: CAB0 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.2 3/06/23Acenaphtheneug/L 3/16/23 CLP SFAM01.1 B5.2 U83-32-9 5.2 3/06/23Acenaphthyleneug/L 3/16/23 CLP SFAM01.1 B5.2 U208-96-8 10 3/06/23Acetophenoneug/L 3/16/23 CLP SFAM01.1 B10U98-86-2 5.2 3/06/23Anthraceneug/L 3/16/23 CLP SFAM01.1 B5.2 U120-12-7 10 3/06/23Atrazineug/L 3/16/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/16/23 CLP SFAM01.1 B10U100-52-7 5.2 3/06/23Benzo(a)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.2 U56-55-3 5.2 3/06/23Benzo(a)pyrene ug/L 3/16/23 CLP SFAM01.1 B5.2 U50-32-8 5.2 3/06/23Benzo(b)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.2 U205-99-2 5.2 3/06/23Benzo(g,h,i)perylene ug/L 3/16/23 CLP SFAM01.1 B5.2 U191-24-2 5.2 3/06/23Benzo(k)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.2 U207-08-9 5.2 3/06/23Benzyl butyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.2 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/16/23 CLP SFAM01.1 B10U108-60-1 5.2 3/06/23Bis(2-chloroethoxy)methane ug/L 3/16/23 CLP SFAM01.1 B5.2 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/16/23 CLP SFAM01.1 B10U111-44-4 5.2 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/16/23 CLP SFAM01.1 B5.2 U117-81-7 10 3/06/23Caprolactamug/L 3/16/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/16/23 CLP SFAM01.1 B10U86-74-8 5.2 3/06/23Chryseneug/L 3/16/23 CLP SFAM01.1 B5.2 U218-01-9 5.2 3/06/23Dibenzo(a,h)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.2 U53-70-3 5.2 3/06/23Dibenzofuranug/L 3/16/23 CLP SFAM01.1 B5.2 U132-64-9 5.2 3/06/23Diethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.2 U84-66-2 5.2 3/06/23Dimethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.2 U131-11-3 5.2 3/06/23Di-n-butylphthalate ug/L 3/16/23 CLP SFAM01.1 B5.2 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/16/23 CLP SFAM01.1 B10U117-84-0 5.2 3/06/23Fluorantheneug/L 3/16/23 CLP SFAM01.1 B5.2 U206-44-0 5.2 3/06/23Fluoreneug/L 3/16/23 CLP SFAM01.1 B5.2 U86-73-7 5.2 3/06/23Hexachlorobenzene (HCB)ug/L 3/16/23 CLP SFAM01.1 B5.2 U118-74-1 5.2 3/06/23Hexachlorobutadieneug/L 3/16/23 CLP SFAM01.1 B5.2 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 55 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW16S-022823-DUP C231105-09 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB0 ETB MD No: CAB0 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/16/23 CLP SFAM01.1 B10U77-47-4 5.2 3/06/23Hexachloroethaneug/L 3/16/23 CLP SFAM01.1 B5.2 U67-72-1 5.2 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/16/23 CLP SFAM01.1 B5.2 U193-39-5 5.2 3/06/23Isophoroneug/L 3/16/23 CLP SFAM01.1 B5.2 U78-59-1 5.2 3/06/23Naphthaleneug/L 3/16/23 CLP SFAM01.1 B5.2 U91-20-3 5.2 3/06/23Nitrobenzeneug/L 3/16/23 CLP SFAM01.1 B5.2 U98-95-3 5.2 3/06/23n-Nitroso di-n-Propylamine ug/L 3/16/23 CLP SFAM01.1 B5.2 U621-64-7 5.2 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/16/23 CLP SFAM01.1 B5.2 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.2 3/06/23Phenanthreneug/L 3/16/23 CLP SFAM01.1 B5.2 U85-01-8 10 3/06/23Phenolug/L 3/16/23 CLP SFAM01.1 B10U108-95-2 5.2 3/06/23Pyreneug/L 3/16/23 CLP SFAM01.1 B5.2 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/16/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 56 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW17D-030123 C231105-10 Matrix:Groundwater Date Collected:3/1/23 10:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA6 ETB MD No: CAA6 ETB Station ID:MW17D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.049 J, CLP01R4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.11 J, CLP0171-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.46 J, CLP0175-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.11.275-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 57 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW17D-030123 C231105-10 Matrix:Groundwater Date Collected:3/1/23 10:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA6 ETB MD No: CAA6 ETB Station ID:MW17D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.36 J, CLP011634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.12.5127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.15 J, CLP01108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.10.11 J, CLP0179-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 58 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW17D-030123 C231105-10 Matrix:Groundwater Date Collected:3/1/23 10:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA6 ETB MD No: CAA6 ETB Station ID:MW17D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 5 3/08/23 CLP SFAM01.13/08/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 59 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW17D-030123 C231105-10 Matrix:Groundwater Date Collected:3/1/23 10:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA6 ETB MD No: CAA6 ETB Station ID:MW17D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U1319-77-3 5.0 3/06/231,1-Biphenyl ug/L 3/16/23 CLP SFAM01.1 B5.0 U92-52-4 5.0 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-94-3 2.0 3/06/231,4-Dioxane ug/L 3/16/23 CLP SFAM01.1 B1.4 J, CLP01123-91-1 5.0 3/06/231-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U90-12-0 5.0 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U58-90-2 5.0 3/06/232,4,5-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-195-95-4 5.0 3/06/232,4,6-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-06-2 5.0 3/06/232,4-Dichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U120-83-2 5.0 3/06/232,4-Dimethylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.0 3/06/232,4-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U121-14-2 5.0 3/06/232,6-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U606-20-2 5.0 3/06/232-Chloronaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-58-7 5.0 3/06/232-Chlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U534-52-1 5.0 3/06/232-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-57-6 10 3/06/232-Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U95-48-7 5.0 3/06/232-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-74-4 5.0 3/06/232-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/16/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U99-09-2 5.0 3/06/234-Bromophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U101-55-3 5.0 3/06/234-Chloro-3-methylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/16/23 CLP SFAM01.1 B10U106-47-8 5.0 3/06/234-Chlorophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U100-01-6 10 3/06/234-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 60 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW17D-030123 C231105-10 Matrix:Groundwater Date Collected:3/1/23 10:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA6 ETB MD No: CAA6 ETB Station ID:MW17D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.0 3/06/23Acenaphtheneug/L 3/16/23 CLP SFAM01.1 B5.0 U83-32-9 5.0 3/06/23Acenaphthyleneug/L 3/16/23 CLP SFAM01.1 B5.0 U208-96-8 10 3/06/23Acetophenoneug/L 3/16/23 CLP SFAM01.1 B10U98-86-2 5.0 3/06/23Anthraceneug/L 3/16/23 CLP SFAM01.1 B5.0 U120-12-7 10 3/06/23Atrazineug/L 3/16/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/16/23 CLP SFAM01.1 B10U100-52-7 5.0 3/06/23Benzo(a)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U56-55-3 5.0 3/06/23Benzo(a)pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U50-32-8 5.0 3/06/23Benzo(b)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U205-99-2 5.0 3/06/23Benzo(g,h,i)perylene ug/L 3/16/23 CLP SFAM01.1 B5.0 U191-24-2 5.0 3/06/23Benzo(k)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U207-08-9 5.0 3/06/23Benzyl butyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/16/23 CLP SFAM01.1 B10U108-60-1 5.0 3/06/23Bis(2-chloroethoxy)methane ug/L 3/16/23 CLP SFAM01.1 B5.0 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/16/23 CLP SFAM01.1 B10U111-44-4 5.0 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U117-81-7 10 3/06/23Caprolactamug/L 3/16/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/16/23 CLP SFAM01.1 B10U86-74-8 5.0 3/06/23Chryseneug/L 3/16/23 CLP SFAM01.1 B5.0 U218-01-9 5.0 3/06/23Dibenzo(a,h)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U53-70-3 5.0 3/06/23Dibenzofuranug/L 3/16/23 CLP SFAM01.1 B5.0 U132-64-9 5.0 3/06/23Diethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-66-2 5.0 3/06/23Dimethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U131-11-3 5.0 3/06/23Di-n-butylphthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/16/23 CLP SFAM01.1 B10U117-84-0 5.0 3/06/23Fluorantheneug/L 3/16/23 CLP SFAM01.1 B5.0 U206-44-0 5.0 3/06/23Fluoreneug/L 3/16/23 CLP SFAM01.1 B5.0 U86-73-7 5.0 3/06/23Hexachlorobenzene (HCB)ug/L 3/16/23 CLP SFAM01.1 B5.0 U118-74-1 5.0 3/06/23Hexachlorobutadieneug/L 3/16/23 CLP SFAM01.1 B5.0 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 61 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW17D-030123 C231105-10 Matrix:Groundwater Date Collected:3/1/23 10:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA6 ETB MD No: CAA6 ETB Station ID:MW17D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/16/23 CLP SFAM01.1 B10U77-47-4 5.0 3/06/23Hexachloroethaneug/L 3/16/23 CLP SFAM01.1 B5.0 U67-72-1 5.0 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U193-39-5 5.0 3/06/23Isophoroneug/L 3/16/23 CLP SFAM01.1 B5.0 U78-59-1 5.0 3/06/23Naphthaleneug/L 3/16/23 CLP SFAM01.1 B5.0 U91-20-3 5.0 3/06/23Nitrobenzeneug/L 3/16/23 CLP SFAM01.1 B5.0 U98-95-3 5.0 3/06/23n-Nitroso di-n-Propylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U621-64-7 5.0 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.0 3/06/23Phenanthreneug/L 3/16/23 CLP SFAM01.1 B5.0 U85-01-8 10 3/06/23Phenolug/L 3/16/23 CLP SFAM01.1 B10U108-95-2 5.0 3/06/23Pyreneug/L 3/16/23 CLP SFAM01.1 B5.0 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/16/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 62 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW17S-030123 C231105-11 Matrix:Groundwater Date Collected:3/1/23 12:55 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA9 ETB MD No: CAA9 ETB Station ID:MW17S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.13 J, CLP0171-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.17 J, CLP0175-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.10.7575-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 63 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW17S-030123 C231105-11 Matrix:Groundwater Date Collected:3/1/23 12:55 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA9 ETB MD No: CAA9 ETB Station ID:MW17S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.10.47 J, CLP01127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.041 J, CLP01108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.10.12 J, CLP0179-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 64 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW17S-030123 C231105-11 Matrix:Groundwater Date Collected:3/1/23 12:55 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA9 ETB MD No: CAA9 ETB Station ID:MW17S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 3/08/23 3/08/23 CLP SFAM01.1Petroleum Product N, CLP15R4-6500 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 65 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW17S-030123 C231105-11 Matrix:Groundwater Date Collected:3/1/23 12:55 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA9 ETB MD No: CAA9 ETB Station ID:MW17S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U1319-77-3 5.0 3/06/231,1-Biphenyl ug/L 3/16/23 CLP SFAM01.1 B5.0 U92-52-4 5.0 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-94-3 2.0 3/06/231,4-Dioxane ug/L 3/16/23 CLP SFAM01.1 B2.0 U123-91-1 5.0 3/06/231-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U90-12-0 5.0 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U58-90-2 5.0 3/06/232,4,5-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-195-95-4 5.0 3/06/232,4,6-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-06-2 5.0 3/06/232,4-Dichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U120-83-2 5.0 3/06/232,4-Dimethylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.0 3/06/232,4-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U121-14-2 5.0 3/06/232,6-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U606-20-2 5.0 3/06/232-Chloronaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-58-7 5.0 3/06/232-Chlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U534-52-1 5.0 3/06/232-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-57-6 10 3/06/232-Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U95-48-7 5.0 3/06/232-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-74-4 5.0 3/06/232-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/16/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U99-09-2 5.0 3/06/234-Bromophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U101-55-3 5.0 3/06/234-Chloro-3-methylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/16/23 CLP SFAM01.1 B10U106-47-8 5.0 3/06/234-Chlorophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U100-01-6 10 3/06/234-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 66 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW17S-030123 C231105-11 Matrix:Groundwater Date Collected:3/1/23 12:55 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA9 ETB MD No: CAA9 ETB Station ID:MW17S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.0 3/06/23Acenaphtheneug/L 3/16/23 CLP SFAM01.1 B5.0 U83-32-9 5.0 3/06/23Acenaphthyleneug/L 3/16/23 CLP SFAM01.1 B5.0 U208-96-8 10 3/06/23Acetophenoneug/L 3/16/23 CLP SFAM01.1 B10U98-86-2 5.0 3/06/23Anthraceneug/L 3/16/23 CLP SFAM01.1 B5.0 U120-12-7 10 3/06/23Atrazineug/L 3/16/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/16/23 CLP SFAM01.1 B10U100-52-7 5.0 3/06/23Benzo(a)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U56-55-3 5.0 3/06/23Benzo(a)pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U50-32-8 5.0 3/06/23Benzo(b)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U205-99-2 5.0 3/06/23Benzo(g,h,i)perylene ug/L 3/16/23 CLP SFAM01.1 B5.0 U191-24-2 5.0 3/06/23Benzo(k)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U207-08-9 5.0 3/06/23Benzyl butyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/16/23 CLP SFAM01.1 B10U108-60-1 5.0 3/06/23Bis(2-chloroethoxy)methane ug/L 3/16/23 CLP SFAM01.1 B5.0 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/16/23 CLP SFAM01.1 B10U111-44-4 5.0 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U117-81-7 10 3/06/23Caprolactamug/L 3/16/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/16/23 CLP SFAM01.1 B10U86-74-8 5.0 3/06/23Chryseneug/L 3/16/23 CLP SFAM01.1 B5.0 U218-01-9 5.0 3/06/23Dibenzo(a,h)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U53-70-3 5.0 3/06/23Dibenzofuranug/L 3/16/23 CLP SFAM01.1 B5.0 U132-64-9 5.0 3/06/23Diethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-66-2 5.0 3/06/23Dimethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U131-11-3 5.0 3/06/23Di-n-butylphthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/16/23 CLP SFAM01.1 B10U117-84-0 5.0 3/06/23Fluorantheneug/L 3/16/23 CLP SFAM01.1 B5.0 U206-44-0 5.0 3/06/23Fluoreneug/L 3/16/23 CLP SFAM01.1 B5.0 U86-73-7 5.0 3/06/23Hexachlorobenzene (HCB)ug/L 3/16/23 CLP SFAM01.1 B5.0 U118-74-1 5.0 3/06/23Hexachlorobutadieneug/L 3/16/23 CLP SFAM01.1 B5.0 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 67 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW17S-030123 C231105-11 Matrix:Groundwater Date Collected:3/1/23 12:55 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA9 ETB MD No: CAA9 ETB Station ID:MW17S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/16/23 CLP SFAM01.1 B10U77-47-4 5.0 3/06/23Hexachloroethaneug/L 3/16/23 CLP SFAM01.1 B5.0 U67-72-1 5.0 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U193-39-5 5.0 3/06/23Isophoroneug/L 3/16/23 CLP SFAM01.1 B5.0 U78-59-1 5.0 3/06/23Naphthaleneug/L 3/16/23 CLP SFAM01.1 B5.0 U91-20-3 5.0 3/06/23Nitrobenzeneug/L 3/16/23 CLP SFAM01.1 B5.0 U98-95-3 5.0 3/06/23n-Nitroso di-n-Propylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U621-64-7 5.0 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.0 3/06/23Phenanthreneug/L 3/16/23 CLP SFAM01.1 B5.0 U85-01-8 10 3/06/23Phenolug/L 3/16/23 CLP SFAM01.1 B10U108-95-2 5.0 3/06/23Pyreneug/L 3/16/23 CLP SFAM01.1 B5.0 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/16/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 68 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW18D-022823 C231105-12 Matrix:Groundwater Date Collected:2/28/23 14:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA8 ETB MD No: CAA8 ETB Station ID:MW18D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U71-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.13 J, CLP0175-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.10.25 J, CLP0175-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 69 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW18D-022823 C231105-12 Matrix:Groundwater Date Collected:2/28/23 14:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA8 ETB MD No: CAA8 ETB Station ID:MW18D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.50 U67-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.16 J, CLP01156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.10.50 U127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.040 J, CLP01108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.10.15 J, CLP0179-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 70 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW18D-022823 C231105-12 Matrix:Groundwater Date Collected:2/28/23 14:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA8 ETB MD No: CAA8 ETB Station ID:MW18D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 5 3/08/23 CLP SFAM01.13/08/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 71 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW18D-022823 C231105-12 Matrix:Groundwater Date Collected:2/28/23 14:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA8 ETB MD No: CAA8 ETB Station ID:MW18D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U1319-77-3 5.0 3/06/231,1-Biphenyl ug/L 3/16/23 CLP SFAM01.1 B5.0 U92-52-4 5.0 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-94-3 2.0 3/06/231,4-Dioxane ug/L 3/16/23 CLP SFAM01.1 B2.0 U123-91-1 5.0 3/06/231-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U90-12-0 5.0 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U58-90-2 5.0 3/06/232,4,5-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-195-95-4 5.0 3/06/232,4,6-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-06-2 5.0 3/06/232,4-Dichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U120-83-2 5.0 3/06/232,4-Dimethylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.0 3/06/232,4-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U121-14-2 5.0 3/06/232,6-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U606-20-2 5.0 3/06/232-Chloronaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-58-7 5.0 3/06/232-Chlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U534-52-1 5.0 3/06/232-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-57-6 10 3/06/232-Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U95-48-7 5.0 3/06/232-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-74-4 5.0 3/06/232-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/16/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U99-09-2 5.0 3/06/234-Bromophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U101-55-3 5.0 3/06/234-Chloro-3-methylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/16/23 CLP SFAM01.1 B10U106-47-8 5.0 3/06/234-Chlorophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U100-01-6 10 3/06/234-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 72 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW18D-022823 C231105-12 Matrix:Groundwater Date Collected:2/28/23 14:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA8 ETB MD No: CAA8 ETB Station ID:MW18D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.0 3/06/23Acenaphtheneug/L 3/16/23 CLP SFAM01.1 B5.0 U83-32-9 5.0 3/06/23Acenaphthyleneug/L 3/16/23 CLP SFAM01.1 B5.0 U208-96-8 10 3/06/23Acetophenoneug/L 3/16/23 CLP SFAM01.1 B10U98-86-2 5.0 3/06/23Anthraceneug/L 3/16/23 CLP SFAM01.1 B5.0 U120-12-7 10 3/06/23Atrazineug/L 3/16/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/16/23 CLP SFAM01.1 B10U100-52-7 5.0 3/06/23Benzo(a)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U56-55-3 5.0 3/06/23Benzo(a)pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U50-32-8 5.0 3/06/23Benzo(b)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U205-99-2 5.0 3/06/23Benzo(g,h,i)perylene ug/L 3/16/23 CLP SFAM01.1 B5.0 U191-24-2 5.0 3/06/23Benzo(k)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U207-08-9 5.0 3/06/23Benzyl butyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/16/23 CLP SFAM01.1 B10U108-60-1 5.0 3/06/23Bis(2-chloroethoxy)methane ug/L 3/16/23 CLP SFAM01.1 B5.0 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/16/23 CLP SFAM01.1 B10U111-44-4 5.0 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U117-81-7 10 3/06/23Caprolactamug/L 3/16/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/16/23 CLP SFAM01.1 B10U86-74-8 5.0 3/06/23Chryseneug/L 3/16/23 CLP SFAM01.1 B5.0 U218-01-9 5.0 3/06/23Dibenzo(a,h)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U53-70-3 5.0 3/06/23Dibenzofuranug/L 3/16/23 CLP SFAM01.1 B5.0 U132-64-9 5.0 3/06/23Diethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-66-2 5.0 3/06/23Dimethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U131-11-3 5.0 3/06/23Di-n-butylphthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/16/23 CLP SFAM01.1 B10U117-84-0 5.0 3/06/23Fluorantheneug/L 3/16/23 CLP SFAM01.1 B5.0 U206-44-0 5.0 3/06/23Fluoreneug/L 3/16/23 CLP SFAM01.1 B5.0 U86-73-7 5.0 3/06/23Hexachlorobenzene (HCB)ug/L 3/16/23 CLP SFAM01.1 B5.0 U118-74-1 5.0 3/06/23Hexachlorobutadieneug/L 3/16/23 CLP SFAM01.1 B5.0 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 73 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW18D-022823 C231105-12 Matrix:Groundwater Date Collected:2/28/23 14:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA8 ETB MD No: CAA8 ETB Station ID:MW18D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/16/23 CLP SFAM01.1 B10U77-47-4 5.0 3/06/23Hexachloroethaneug/L 3/16/23 CLP SFAM01.1 B5.0 U67-72-1 5.0 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U193-39-5 5.0 3/06/23Isophoroneug/L 3/16/23 CLP SFAM01.1 B5.0 U78-59-1 5.0 3/06/23Naphthaleneug/L 3/16/23 CLP SFAM01.1 B5.0 U91-20-3 5.0 3/06/23Nitrobenzeneug/L 3/16/23 CLP SFAM01.1 B5.0 U98-95-3 5.0 3/06/23n-Nitroso di-n-Propylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U621-64-7 5.0 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.0 3/06/23Phenanthreneug/L 3/16/23 CLP SFAM01.1 B5.0 U85-01-8 10 3/06/23Phenolug/L 3/16/23 CLP SFAM01.1 B10U108-95-2 5.0 3/06/23Pyreneug/L 3/16/23 CLP SFAM01.1 B5.0 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/16/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 74 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW20D-022823 C231105-13 Matrix:Groundwater Date Collected:2/28/23 13:40 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA7 ETB MD No: CAA7 ETB Station ID:MW20D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23(m- and/or p-)Xylene ug/L 3/08/23 CLP SFAM01.10.50 UR4-7156 0.50 3/08/231,1,1-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.36 J, CLP0171-55-6 0.50 3/08/231,1,2,2-Tetrachloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-34-5 0.50 3/08/231,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113) ug/L 3/08/23 CLP SFAM01.10.50 U76-13-1 0.50 3/08/231,1,2-Trichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U79-00-5 0.50 3/08/231,1-Dichloroethane ug/L 3/08/23 CLP SFAM01.11.575-34-3 0.50 3/08/231,1-Dichloroethene (1,1-Dichloroethylene) ug/L 3/08/23 CLP SFAM01.15.975-35-4 0.50 3/08/231,2,3-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U87-61-6 0.50 3/08/231,2,3-Trichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U96-18-4 0.50 3/08/231,2,4-Trichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U120-82-1 0.50 3/08/231,2,4-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-63-6 0.50 3/08/231,2-Dibromo-3-Chloropropane (DBCP)ug/L 3/08/23 CLP SFAM01.10.50 U96-12-8 0.50 3/08/231,2-Dibromoethane (EDB)ug/L 3/08/23 CLP SFAM01.10.50 U106-93-4 0.50 3/08/231,2-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U95-50-1 0.50 3/08/231,2-Dichloroethane ug/L 3/08/23 CLP SFAM01.10.50 U107-06-2 0.50 3/08/231,2-Dichloropropane ug/L 3/08/23 CLP SFAM01.10.50 U, J, CLP2578-87-5 0.50 3/08/231,3,5-Trimethylbenzene ug/L 3/08/23 CLP SFAM01.10.50 U108-67-8 0.50 3/08/231,3-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U541-73-1 0.50 3/08/231,4-Dichlorobenzene ug/L 3/08/23 CLP SFAM01.10.50 U106-46-7 5.0 3/08/23Acetoneug/L 3/08/23 CLP SFAM01.15.0 U, R, CLP17, CLP32 67-64-1 0.50 3/08/23Benzeneug/L 3/08/23 CLP SFAM01.10.50 U71-43-2 0.50 3/08/23Bromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-97-5 0.50 3/08/23Bromodichloromethaneug/L 3/08/23 CLP SFAM01.10.50 U75-27-4 0.50 3/08/23Bromoformug/L 3/08/23 CLP SFAM01.10.50 U75-25-2 0.50 3/08/23Bromomethaneug/L 3/08/23 CLP SFAM01.10.50 U, R, CLP1774-83-9 0.50 3/08/23Carbon disulfide ug/L 3/08/23 CLP SFAM01.10.50 U75-15-0 0.50 3/08/23Carbon Tetrachloride ug/L 3/08/23 CLP SFAM01.10.50 U56-23-5 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 75 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW20D-022823 C231105-13 Matrix:Groundwater Date Collected:2/28/23 13:40 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA7 ETB MD No: CAA7 ETB Station ID:MW20D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.50 3/08/23Chlorobenzeneug/L 3/08/23 CLP SFAM01.10.50 U108-90-7 0.50 3/08/23Chloroethaneug/L 3/08/23 CLP SFAM01.10.50 U75-00-3 0.50 3/08/23Chloroformug/L 3/08/23 CLP SFAM01.10.6767-66-3 0.50 3/08/23Chloromethaneug/L 3/08/23 CLP SFAM01.10.50 U74-87-3 0.50 3/08/23cis-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.71156-59-2 0.50 3/08/23cis-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-01-5 0.50 3/08/23Cyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U110-82-7 0.50 3/08/23Dibromochloromethaneug/L 3/08/23 CLP SFAM01.10.50 U124-48-1 0.50 3/08/23Dichlorodifluoromethane (Freon 12)ug/L 3/08/23 CLP SFAM01.10.50 U75-71-8 0.50 3/08/23Ethyl Benzene ug/L 3/08/23 CLP SFAM01.10.50 U100-41-4 0.50 3/08/23Isopropylbenzeneug/L 3/08/23 CLP SFAM01.10.50 U98-82-8 0.50 3/08/23Methyl Acetate ug/L 3/08/23 CLP SFAM01.10.50 U, J, QC-179-20-9 5.0 3/08/23Methyl Butyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U591-78-6 5.0 3/08/23Methyl Ethyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U78-93-3 5.0 3/08/23Methyl Isobutyl Ketone ug/L 3/08/23 CLP SFAM01.15.0 U108-10-1 0.50 3/08/23Methyl T-Butyl Ether (MTBE)ug/L 3/08/23 CLP SFAM01.10.50 U1634-04-4 0.50 3/08/23Methylcyclohexaneug/L 3/08/23 CLP SFAM01.10.50 U108-87-2 0.50 3/08/23Methylene Chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-09-2 0.50 3/08/23o-Xylene ug/L 3/08/23 CLP SFAM01.10.50 U95-47-6 0.50 3/08/23Styreneug/L 3/08/23 CLP SFAM01.10.50 U100-42-5 0.50 3/08/23Tetrachloroethene (Tetrachloroethylene)ug/L 3/08/23 CLP SFAM01.12.7127-18-4 0.50 3/08/23Tolueneug/L 3/08/23 CLP SFAM01.10.043 J, CLP01108-88-3 0.50 3/08/23trans-1,2-Dichloroethene ug/L 3/08/23 CLP SFAM01.10.50 U156-60-5 0.50 3/08/23trans-1,3-Dichloropropene ug/L 3/08/23 CLP SFAM01.10.50 U10061-02-6 0.50 3/08/23Trichloroethene (Trichloroethylene)ug/L 3/08/23 CLP SFAM01.14.979-01-6 0.50 3/08/23Trichlorofluoromethane (Freon 11)ug/L 3/08/23 CLP SFAM01.10.50 U75-69-4 0.50 3/08/23Vinyl chloride ug/L 3/08/23 CLP SFAM01.10.50 U75-01-4 Tentatively Identified Compounds: 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 76 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Volatile Organics Sample ID:Lab ID: BRP-MW20D-022823 C231105-13 Matrix:Groundwater Date Collected:2/28/23 13:40 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA7 ETB MD No: CAA7 ETB Station ID:MW20D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method Tentatively Identified Compounds: 3/08/23 3/08/23 CLP SFAM01.1Petroleum Product N, CLP15R4-6500 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 77 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW20D-022823 C231105-13 Matrix:Groundwater Date Collected:2/28/23 13:40 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA7 ETB MD No: CAA7 ETB Station ID:MW20D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23(3-and/or 4-)Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U1319-77-3 5.0 3/06/231,1-Biphenyl ug/L 3/16/23 CLP SFAM01.1 B5.0 U92-52-4 5.0 3/06/231,2,4,5-Tetrachlorobenzene ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-94-3 2.0 3/06/231,4-Dioxane ug/L 3/16/23 CLP SFAM01.1 B2.7123-91-1 5.0 3/06/231-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U90-12-0 5.0 3/06/232,3,4,6-Tetrachlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U58-90-2 5.0 3/06/232,4,5-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-195-95-4 5.0 3/06/232,4,6-Trichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-06-2 5.0 3/06/232,4-Dichlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U120-83-2 5.0 3/06/232,4-Dimethylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U105-67-9 10 3/06/232,4-Dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 51-28-5 5.0 3/06/232,4-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U121-14-2 5.0 3/06/232,6-Dinitrotoluene ug/L 3/16/23 CLP SFAM01.1 B5.0 U606-20-2 5.0 3/06/232-Chloronaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-58-7 5.0 3/06/232-Chlorophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U95-57-8 10 3/06/232-Methyl-4,6-dinitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U534-52-1 5.0 3/06/232-Methylnaphthalene ug/L 3/16/23 CLP SFAM01.1 B5.0 U91-57-6 10 3/06/232-Methylphenol ug/L 3/16/23 CLP SFAM01.1 B10U95-48-7 5.0 3/06/232-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-74-4 5.0 3/06/232-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U88-75-5 10 3/06/233,3'-Dichlorobenzidine ug/L 3/16/23 CLP SFAM01.1 B10U, J, QC-391-94-1 10 3/06/233-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U99-09-2 5.0 3/06/234-Bromophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U101-55-3 5.0 3/06/234-Chloro-3-methylphenol ug/L 3/16/23 CLP SFAM01.1 B5.0 U59-50-7 10 3/06/234-Chloroaniline ug/L 3/16/23 CLP SFAM01.1 B10U106-47-8 5.0 3/06/234-Chlorophenyl phenyl ether ug/L 3/16/23 CLP SFAM01.1 B5.0 U7005-72-3 10 3/06/234-Nitroaniline ug/L 3/16/23 CLP SFAM01.1 B10U100-01-6 10 3/06/234-Nitrophenol ug/L 3/16/23 CLP SFAM01.1 B10U, R, CLP32100-02-7 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 78 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW20D-022823 C231105-13 Matrix:Groundwater Date Collected:2/28/23 13:40 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA7 ETB MD No: CAA7 ETB Station ID:MW20D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 5.0 3/06/23Acenaphtheneug/L 3/16/23 CLP SFAM01.1 B5.0 U83-32-9 5.0 3/06/23Acenaphthyleneug/L 3/16/23 CLP SFAM01.1 B5.0 U208-96-8 10 3/06/23Acetophenoneug/L 3/16/23 CLP SFAM01.1 B10U98-86-2 5.0 3/06/23Anthraceneug/L 3/16/23 CLP SFAM01.1 B5.0 U120-12-7 10 3/06/23Atrazineug/L 3/16/23 CLP SFAM01.1 B10U1912-24-9 10 3/06/23Benzaldehydeug/L 3/16/23 CLP SFAM01.1 B10U100-52-7 5.0 3/06/23Benzo(a)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U56-55-3 5.0 3/06/23Benzo(a)pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U50-32-8 5.0 3/06/23Benzo(b)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U205-99-2 5.0 3/06/23Benzo(g,h,i)perylene ug/L 3/16/23 CLP SFAM01.1 B5.0 U191-24-2 5.0 3/06/23Benzo(k)fluoranthene ug/L 3/16/23 CLP SFAM01.1 B5.0 U207-08-9 5.0 3/06/23Benzyl butyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U85-68-7 10 3/06/23Bis(2-chloro-1-methylethyl) ether ug/L 3/16/23 CLP SFAM01.1 B10U108-60-1 5.0 3/06/23Bis(2-chloroethoxy)methane ug/L 3/16/23 CLP SFAM01.1 B5.0 U111-91-1 10 3/06/23bis(2-Chloroethyl) Ether ug/L 3/16/23 CLP SFAM01.1 B10U111-44-4 5.0 3/06/23Bis(2-ethylhexyl) phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U117-81-7 10 3/06/23Caprolactamug/L 3/16/23 CLP SFAM01.1 B10U105-60-2 10 3/06/23Carbazoleug/L 3/16/23 CLP SFAM01.1 B10U86-74-8 5.0 3/06/23Chryseneug/L 3/16/23 CLP SFAM01.1 B5.0 U218-01-9 5.0 3/06/23Dibenzo(a,h)anthracene ug/L 3/16/23 CLP SFAM01.1 B5.0 U53-70-3 5.0 3/06/23Dibenzofuranug/L 3/16/23 CLP SFAM01.1 B5.0 U132-64-9 5.0 3/06/23Diethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-66-2 5.0 3/06/23Dimethyl phthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U131-11-3 5.0 3/06/23Di-n-butylphthalate ug/L 3/16/23 CLP SFAM01.1 B5.0 U84-74-2 10 3/06/23Di-n-octylphthalate ug/L 3/16/23 CLP SFAM01.1 B10U117-84-0 5.0 3/06/23Fluorantheneug/L 3/16/23 CLP SFAM01.1 B5.0 U206-44-0 5.0 3/06/23Fluoreneug/L 3/16/23 CLP SFAM01.1 B5.0 U86-73-7 5.0 3/06/23Hexachlorobenzene (HCB)ug/L 3/16/23 CLP SFAM01.1 B5.0 U118-74-1 5.0 3/06/23Hexachlorobutadieneug/L 3/16/23 CLP SFAM01.1 B5.0 U87-68-3 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 79 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Jeffrey Wilmoth Semi Volatile Organics Sample ID:Lab ID: BRP-MW20D-022823 C231105-13 Matrix:Groundwater Date Collected:2/28/23 13:40 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA7 ETB MD No: CAA7 ETB Station ID:MW20D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 10 3/06/23Hexachlorocyclopentadiene (HCCP)ug/L 3/16/23 CLP SFAM01.1 B10U77-47-4 5.0 3/06/23Hexachloroethaneug/L 3/16/23 CLP SFAM01.1 B5.0 U67-72-1 5.0 3/06/23Indeno (1,2,3-cd) pyrene ug/L 3/16/23 CLP SFAM01.1 B5.0 U193-39-5 5.0 3/06/23Isophoroneug/L 3/16/23 CLP SFAM01.1 B5.0 U78-59-1 5.0 3/06/23Naphthaleneug/L 3/16/23 CLP SFAM01.1 B5.0 U91-20-3 5.0 3/06/23Nitrobenzeneug/L 3/16/23 CLP SFAM01.1 B5.0 U98-95-3 5.0 3/06/23n-Nitroso di-n-Propylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U621-64-7 5.0 3/06/23n-Nitrosodiphenylamine/Diphenylamine ug/L 3/16/23 CLP SFAM01.1 B5.0 U, J, QC-1122-39-4 10 3/06/23Pentachlorophenolug/L 3/16/23 CLP SFAM01.1 B10U, J, CLP16, QC-1 87-86-5 5.0 3/06/23Phenanthreneug/L 3/16/23 CLP SFAM01.1 B5.0 U85-01-8 10 3/06/23Phenolug/L 3/16/23 CLP SFAM01.1 B10U108-95-2 5.0 3/06/23Pyreneug/L 3/16/23 CLP SFAM01.1 B5.0 U129-00-0 Tentatively Identified Compounds: 5 3/06/23 CLP SFAM01.1 B3/16/23ug/L5Tentatively Identified Compounds UR4-0000 5/24/23 11:31C231105 SVOA VOA FINAL 05 24 23 1131Page 80 of 80 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard May 18, 2023 MEMORANDUM SUBJECT: FROM: FINAL Analytical Report Project: 23-0155, Blue Ridge Plating 4LSASD-QAPSB Denise Goddard Quality Assurance Section, Chemist Quality Assurance Section Keith Harris, ChiefTHRU: TO:Craig Zeller Attached are the final results for the analytical groups listed below. These analyses were performed in accordance with the associated contract Statement Of Work (SOW). In general, project data quality objectives have not been used to evaluate these data prior to release by the Quality Assurance Section. For a listing of specific data qualifiers and explanations, please refer to the Data Qualifier Definitions included in this report. Analyses Included in this report:Method Used: Total Metals (TMTL) Total Mercury CLP Inorganics (Water) Total Metals CLP Inorganics (Water) 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 1 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Report Narrative for Work Order: C231105 Analysis: TMTL Inorganic Data Review and Validation Report Site Name: Blue Ridge Plating, Arden NC Case No.: 50606, Project No.: 23-0155, Work Order Nos.: C231105, C231104 (PES) ELEMENT Sample IDs.: C231105-01, 03-13, C231104-01-02 (PES) Sampling Date(s): 2/28/23, 3/1/23 Validated Time of Sample Receipt: 3/3/23 Laboratory Performing Inorganic Analyses: Eurofins Burlington, South Burlington VT Date Received from Lab: 3/24/23 (SMO portal) Analyses conducted: Total Metals (ICP-MS), Mercury The ESAT Work Team has reviewed the above-captioned CLP data package consisting of 14 water samples analyzed for total metals by ICP-MS and for mercury by CVAA according to the contract Statement of Work SFAM01.1 (SOW) and EPA guidelines. This package presents acceptable contractual and technical performance with qualifications. Additional details are provided below. Examination of laboratory blank samples revealed apparent low-level contamination for beryllium. Reported detection limits were adjusted as high as ten times the blank levels to discount possible false positives due to contamination in laboratory blanks. ICP-MS Analysis (Total Metals) PE Sample Results The PES recoveries for metals in soil by ICP-MS were scored as within limits by the web-based SPS Web software. Therefore, no data qualifiers were applied to the sample results based on these criteria. Other QA/QC Results Serial dilution % difference was above the acceptance limit for aluminum (18%) in SDG MDBAB7. All aluminum results in SDG MDBAB7 were considered estimated and “J” qualified. Mercury PE Sample Results The PES recovery for mercury was scored as within limits by the web-based SPS Web software. Therefore, no data qualifiers were applied to the sample results based on these criteria. Other QA/QC Results 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 2 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard There were no QA/QC problems observed for mercury analysis. Therefore, no data qualifiers were applied to the sample results for arsenic based on these criteria. A Stage 4 validation consisting of manual review was performed on the inorganic samples submitted for this case. 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 3 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Date CollectedMatrixLaboratory IDSample ID SAMPLES INCLUDED IN THIS REPORT Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 MD#D# CAB2CAB2BRP-FL-01 C231105-01 Field Blank 2/28/23 17:00 CAA1CAA1BRP-MW13D-022823 C231105-03 Groundwater 2/28/23 18:15 CAA0CAA0BRP-MW13S-030123 C231105-04 Groundwater 3/1/23 08:10 CAA3CAA3BRP-MW15D-030123 C231105-05 Groundwater 3/1/23 10:00 CAA2CAA2BRP-MW15S-030123 C231105-06 Groundwater 3/1/23 09:15 CAA5CAA5BRP-MW16D-022823 C231105-07 Groundwater 2/28/23 16:50 CAA4CAA4BRP-MW16S-022823 C231105-08 Groundwater 2/28/23 16:10 CAB0CAB0BRP-MW16S-022823-DUP C231105-09 Groundwater 2/28/23 16:10 CAA6CAA6BRP-MW17D-030123 C231105-10 Groundwater 3/1/23 10:50 CAA9CAA9BRP-MW17S-030123 C231105-11 Groundwater 3/1/23 12:55 CAA8CAA8BRP-MW18D-022823 C231105-12 Groundwater 2/28/23 14:50 CAA7CAA7BRP-MW20D-022823 C231105-13 Groundwater 2/28/23 13:40 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 4 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard DATA QUALIFIER DEFINITIONS U The analyte was not detected at or above the reporting limit. B-4 Level in blank impacts MRLs. J The identification of the analyte is acceptable; the reported value is an estimate. Q-2 Result greater than MDL but less than MRL. Q-5 Serial dilution precision outside method control limits ACRONYMS AND ABBREVIATIONS CAS Chemical Abstracts Service Note: Analytes with no known CAS identifiers have been assigned codes beginning with "E", the EPA ID as assigned by the EPA Substance Registry System (www.epa.gov/srs), or beginning with "R4-", a unique identifier assigned by the EPA Region 4 laboratory. MDL Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and reported with a 99% confidence that the analyte concentration is greater than zero. MRL Minimum Reporting Limit - Analyte concentration that corresponds to the lowest demonstrated level of acceptable quantitation. The MRL is sample-specific and accounts for preparation weights and volumes, dilutions, and moisture content of soil/sediments. TIC Tentatively Identified Compound - An analyte identified based on a match with the instrument software's mass spectral library. A calibration standard has not been analyzed to confirm the compound's identification or the estimated concentration reported. 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 5 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-FL-01 C231105-01 Matrix:Field Blank Date Collected:2/28/23 17:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB2 ETB MD No: CAB2 ETB Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.12 J, Q-27439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 20 U, J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 10 U7440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 500 U7440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 200 U7439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 500 U7439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 500 U7440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 500 U7440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 6 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-FL-01 C231105-01 Matrix:Field Blank Date Collected:2/28/23 17:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB2 ETB MD No: CAB2 ETB Station ID: CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 7 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW13D-022823 C231105-03 Matrix:Groundwater Date Collected:2/28/23 18:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA1 ETB MD No: CAA1 ETB Station ID:MW13D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 550 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 347440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 0.17 J, Q-27440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 59007440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 7.17440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 3.37440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 1.1 J, Q-27440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 9007439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 13007439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 1807439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 4.77440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 15007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 49007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 8 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW13D-022823 C231105-03 Matrix:Groundwater Date Collected:2/28/23 18:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA1 ETB MD No: CAA1 ETB Station ID:MW13D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 0.88 J, Q-27440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 6.07440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 9 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW13S-030123 C231105-04 Matrix:Groundwater Date Collected:3/1/23 8:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA0 ETB MD No: CAA0 ETB Station ID:MW13S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 96 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 367440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 280 J, Q-27440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 0.97 J, Q-27440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 1.87440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 3107439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 12007439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 707439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 1.97440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 10007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 2.0 J, Q-27782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 260007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 10 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW13S-030123 C231105-04 Matrix:Groundwater Date Collected:3/1/23 8:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA0 ETB MD No: CAA0 ETB Station ID:MW13S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 0.057 J, Q-27440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 9.97440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 11 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW15D-030123 C231105-05 Matrix:Groundwater Date Collected:3/1/23 10:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA3 ETB MD No: CAA3 ETB Station ID:MW15D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 230 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 267440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 28007440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 1.1 J, Q-27440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 5907439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 8107439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 657439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 0.63 J, Q-27440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 15007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 24007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 12 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW15D-030123 C231105-05 Matrix:Groundwater Date Collected:3/1/23 10:00 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA3 ETB MD No: CAA3 ETB Station ID:MW15D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 0.58 J, Q-27440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 177440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 13 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW15S-030123 C231105-06 Matrix:Groundwater Date Collected:3/1/23 9:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA2 ETB MD No: CAA2 ETB Station ID:MW15S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 1000 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 1.17440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 3907440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 110 J, Q-27440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 1.1 J, Q-27440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 4.87440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 4.27440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 13007439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 21007439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 1107439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 6.97440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 39007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 150007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 14 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW15S-030123 C231105-06 Matrix:Groundwater Date Collected:3/1/23 9:15 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA2 ETB MD No: CAA2 ETB Station ID:MW15S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 0.15 J, Q-27440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 1.3 J, Q-27440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 457440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 15 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW16D-022823 C231105-07 Matrix:Groundwater Date Collected:2/28/23 16:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA5 ETB MD No: CAA5 ETB Station ID:MW16D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 390 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 1407440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 0.22 J, Q-27440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 140007440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 1.2 J, Q-27440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 2.57440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 5707439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 64007439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 6307439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 5.97440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 29007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 68007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 16 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW16D-022823 C231105-07 Matrix:Groundwater Date Collected:2/28/23 16:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA5 ETB MD No: CAA5 ETB Station ID:MW16D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 0.95 J, Q-27440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 7.97440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 17 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW16S-022823 C231105-08 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA4 ETB MD No: CAA4 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 660 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 0.77 J, Q-27440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 577440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 2.1 U, B-47440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 2.27440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 73007440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 2.37440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 197440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 45007439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 0.83 J, Q-27439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 58007439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 4507439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 147440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 15007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 86007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 18 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW16S-022823 C231105-08 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA4 ETB MD No: CAA4 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 0.72 J, Q-27440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 2.8 J, Q-27440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 2407440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 19 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW16S-022823-DUP C231105-09 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB0 ETB MD No: CAB0 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 630 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 0.69 J, Q-27440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 597440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 2.1 U, B-47440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 2.47440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 77007440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 197440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 35007439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 0.68 J, Q-27439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 61007439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 4707439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 147440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 15007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 91007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 20 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW16S-022823-DUP C231105-09 Matrix:Groundwater Date Collected:2/28/23 16:10 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAB0 ETB MD No: CAB0 ETB Station ID:MW16S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 0.75 J, Q-27440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 2.1 J, Q-27440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 2607440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 21 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW17D-030123 C231105-10 Matrix:Groundwater Date Collected:3/1/23 10:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA6 ETB MD No: CAA6 ETB Station ID:MW17D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 360 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 237440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 33007440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 2.07440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 1.1 J, Q-27440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 6607439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 9207439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 457439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 1.37440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 13007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 47007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 22 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW17D-030123 C231105-10 Matrix:Groundwater Date Collected:3/1/23 10:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA6 ETB MD No: CAA6 ETB Station ID:MW17D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 1.2 J, Q-27440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 6.57440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 23 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW17S-030123 C231105-11 Matrix:Groundwater Date Collected:3/1/23 12:55 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA9 ETB MD No: CAA9 ETB Station ID:MW17S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 4600 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 0.67 J, Q-27440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 1207440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 100007440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 7.57440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 7.97440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 4.77440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 71007439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 2.57439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 95007439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 4007439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 107440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 29007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 1.0 J, Q-27782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 79007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 24 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW17S-030123 C231105-11 Matrix:Groundwater Date Collected:3/1/23 12:55 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA9 ETB MD No: CAA9 ETB Station ID:MW17S CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 0.18 J, Q-27440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 6.37440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 377440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 25 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW18D-022823 C231105-12 Matrix:Groundwater Date Collected:2/28/23 14:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA8 ETB MD No: CAA8 ETB Station ID:MW18D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 870 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 5.77440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 1107440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 4.1 U, B-47440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 88007440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 2.57440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 3.47440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 1100007439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 1.37439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 47007439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 1007439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 1.47440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 23007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 3.8 J, Q-27782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 110007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 26 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW18D-022823 C231105-12 Matrix:Groundwater Date Collected:2/28/23 14:50 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA8 ETB MD No: CAA8 ETB Station ID:MW18D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 0.17 J, Q-27440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 4.4 J, Q-27440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 117440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 27 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW20D-022823 C231105-13 Matrix:Groundwater Date Collected:2/28/23 13:40 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA7 ETB MD No: CAA7 ETB Station ID:MW20D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 0.20 3/15/23Mercuryug/L 3/15/23 CLP SFAM01.1 CV 0.20 U7439-97-6 20 3/15/23Aluminumug/L 3/23/23 CLP SFAM01.1 MS 930 J, Q-57429-90-5 2.0 3/15/23Antimonyug/L 3/23/23 CLP SFAM01.1 MS 2.0 U7440-36-0 1.0 3/15/23Arsenicug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-38-2 10 3/15/23Bariumug/L 3/23/23 CLP SFAM01.1 MS 377440-39-3 1.0 3/15/23Berylliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-41-7 1.0 3/15/23Cadmiumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-43-9 500 3/15/23Calciumug/L 3/23/23 CLP SFAM01.1 MS 76007440-70-2 2.0 3/15/23Chromiumug/L 3/23/23 CLP SFAM01.1 MS 1.8 J, Q-27440-47-3 1.0 3/15/23Cobaltug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-48-4 2.0 3/15/23Copperug/L 3/23/23 CLP SFAM01.1 MS 1.3 J, Q-27440-50-8 200 3/15/23Ironug/L 3/23/23 CLP SFAM01.1 MS 16007439-89-6 1.0 3/15/23Leadug/L 3/23/23 CLP SFAM01.1 MS 0.99 J, Q-27439-92-1 500 3/15/23Magnesiumug/L 3/23/23 CLP SFAM01.1 MS 24007439-95-4 1.0 3/15/23Manganeseug/L 3/23/23 CLP SFAM01.1 MS 267439-96-5 1.0 3/15/23Nickelug/L 3/23/23 CLP SFAM01.1 MS 2.57440-02-0 500 3/15/23Potassiumug/L 3/23/23 CLP SFAM01.1 MS 24007440-09-7 5.0 3/15/23Seleniumug/L 3/23/23 CLP SFAM01.1 MS 5.0 U7782-49-2 1.0 3/15/23Silverug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-22-4 500 3/15/23Sodiumug/L 3/23/23 CLP SFAM01.1 MS 63007440-23-5 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 28 of 29 D.A.R.T. Id: 23-0155 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Laboratory Services and Applied Science Division 980 College Station Road, Athens, Georgia 30605-2700 Project: 23-0155, Blue Ridge Plating - Reported by Denise Goddard Total Metals Sample ID:Lab ID: BRP-MW20D-022823 C231105-13 Matrix:Groundwater Date Collected:2/28/23 13:40 Project: 23-0155, Blue Ridge Plating Contract Lab Case: 50606 D No: CAA7 ETB MD No: CAA7 ETB Station ID:MW20D CAS Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method 1.0 3/15/23Thalliumug/L 3/23/23 CLP SFAM01.1 MS 1.0 U7440-28-0 5.0 3/15/23Vanadiumug/L 3/23/23 CLP SFAM01.1 MS 1.9 J, Q-27440-62-2 5.0 3/15/23Zincug/L 3/23/23 CLP SFAM01.1 MS 6.37440-66-6 5/18/23 16:11C231105 TMTL FINAL 05 18 23 1611Page 29 of 29 ATTACHMENT 2 EPA RSL TABLES FOR RESIDENTIAL SOIL TO GROUNDWATER, MAY 2023 (10 Pages) Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 1 of 10 TR= 1 E - 0 6 THQ = 0 . 1 Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 2 of 10 TR= 1 E - 0 6 THQ = 0 . 1 Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 3 of 10 TR= 1 E - 0 6 THQ = 0 . 1 Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 4 of 10 TR= 1 E - 0 6 THQ = 0 . 1 Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 5 of 10 TR= 1 E - 0 6 THQ = 0 . 1 Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 6 of 10 TR= 1 E - 0 6 THQ = 0 . 1 Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 7 of 10 TR= 1 E - 0 6 THQ = 0 . 1 Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 8 of 10 TR= 1 E - 0 6 THQ = 0 . 1 Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 9 of 10 TR= 1 E - 0 6 THQ = 0 . 1 Regional Screening Level (RSL) Resident Soil to GW Table (TR=1E-06, HQ=0.1) May 2023 SFO -1 ke IUR3 ke RfDo ke RfCi 3 ke vo log Kow Ingestion SLTR=1E-06 Dermal SLTR=1E-06 Inhalation SLTR=1E-06 Carcinogenic SLTR=1E-06 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHQ=0.1 ChildTHI=0.1 MCL Risk-basedSSL MCL-basedSSL Key: I = IRIS; P = PPRTV; O = OPP; A = ATSDR; C = Cal EPA; X = PPRTV Screening Level; H = HEAST; D = OW; W = TEF applied; E = RPF applied; G = see user's guide; U = user provided; c = cancer; n = noncancer; * = where: nc SL < 100X ca SL; ** = where nc SL < 10X ca SL; SSL values are based on DAF=1; m = ceiling limit exceeded; s = Csat exceeded; V = Page 10 of 10 TR= 1 E - 0 6 THQ = 0 . 1