AS-88075_88075_CA_MRP_20230912

AND SURFACE WATER
SAMPLING AND ANALYSIS:
September 2022

Prepared For:
MB HAYNES CORPORATION 187 DEAVERVIEW ROAD ASHEVILLE, NORTH CAROLINA
BLE Project Number J22-5293-22B
September 12, 2023

September 12, 2023 MB Haynes Corporation 187 Deaverview Road Asheville, North Carolina 28806
Attention: Mr. Fred Lewis
Subject: Report of Groundwater and Surface Water Sampling and Analysis: September 2022 MB Haynes Corporation
187 Deaverview Road Asheville, North Carolina BLE Project Number J22-5293-22B Incident No. 88075 Dear Mr. Lewis: As authorized by your acceptance of our Proposal Number J22-5293-22B, dated September 2, 2022, Bunnell Lammons Engineering, Inc. (BLE) has completed the groundwater and surface water sampling event for September 2022. The purpose of the work was to monitor groundwater quality and to evaluate effectiveness of the ongoing remedial measures as part of DWM approved plan for a Notice of Residual
Petroleum (NORP). The enclosed report describes the work performed and presents the results obtained. Sincerely,

BUNNELL LAMMONS ENGINEERING INC.

Thomas A. O’Shea Andrew W. Alexander, P.G. RSM Project Geologist Consultant Geologist Registered, North Carolina #2830 Registered, North Carolina #1475
cc: Ms. Caroline LaFond – NCDWM - UST Section, Asheville, NC
Groundwater and Surface Water Sampling – September 2022 September 12, 2023
MB Haynes Corporation, Asheville, NC BLE Project No. J22-5296-22B
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TABLE OF CONTENTS

1.0 PROJECT INFORMATION ........................................................................................................ 1
2.0 SCOPE OF SERVICES ................................................................................................................. 3 2.1 Groundwater Sampling .................................................................................................................... 3 2.2 Surface Water Sampling .................................................................................................................. 3
3.0 SAMPLING RESULTS ................................................................................................................. 4 3.1 Groundwater Results ........................................................................................................................ 4 3.2 Surface Water Results ...................................................................................................................... 4
4.0 SUMMARY OF REMEDIATION PROGRESS ......................................................................... 5 4.1 Aggressive Fluid Vapor Recovery (AFVR)..................................................................................... 5 4.2 Passive Product Skimmer ................................................................................................................ 5
4.3 Product Recovery from the Interceptor Trench ............................................................................... 5 4.4 Soil Vapor Extraction (SVE) System............................................................................................... 6
5.0 FUTURE COMPLIANCE MONITORING & REMEDIATION EFFECTIVENESS ........... 7 5.1 Product Recovery & SVE Operations .............................................................................................. 7 5.2 Groundwater .................................................................................................................................... 7 5.3 Surface Water .................................................................................................................................. 8 5.4 Incident Closure and Future Monitoring and Remediation.............................................................. 8
6.0 QUALIFICATION OF REPORT ................................................................................................ 9 Tables Tables 1 through 19 and SVE System Plots Figures
Figures 1 through 4 Appendices
Appendix A Groundwater Sampling Procedures and Sampling Logs Appendix B Laboratory Data Appendix C Historical Groundwater Summary Tables and Plots Appendix D Historical Surface Water Summary Table and Plots
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MB Haynes Corporation, Asheville, NC BLE Project No. J22-5296-22B
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1.0 PROJECT INFORMATION
The subject site is located at 187 Deaverview Road in Asheville, North Carolina (Figure 1). MB Haynes Corporation (MB Haynes) operates a multi-discipline construction services company on the property. The facility includes a vehicle fueling operation with one above ground diesel and one above ground gasoline storage tank with a single dispenser pump for each fuel type. The property slopes from Deaverview Road to the north and terminates at a tributary to Smith Mill Creek. The fueling area is located near the top of the slope approximately 150 feet from Deaverview Road.
We understand that on April 30, 2007, a discharge of gasoline into a tributary of Smith Mill Creek was discovered on the subject property. The local fire department conducted an emergency response action by
deploying oil absorbent booms at the point of discharge and further downstream. MB Haynes personnel investigated the incident by excavating a small trench near the discharge point. MB Haynes confirmed the presence of gasoline in the trench’s shallow groundwater. MB Haynes deployed absorbent materials in the
trench as part of an emergency remedial action. Further investigation by MB Haynes revealed that a flexible hose coupling at their gasoline dispenser pump had failed resulting in a release of gasoline. The hose was replaced by a contractor working for MB Haynes and the leak was terminated. On May 1, 2007, MB Haynes contacted the Asheville Regional Office of the North Carolina Department of Environment and Natural Resources (NCDENR) [now the NCDEQ] to report the incident. The NCDENR assigned the Department of Waste Management (DWM) as the regulatory authority for the incident. The DWM conducted a site visit on May 2, 2007 and subsequently issued a Notice of Violation (NOV) letter on May 4, 2007. The NOV assigned an incident number (88075) and required MB Haynes to perform assessment and remedial actions.
The aforementioned NOV requires the performance of a Comprehensive Site Assessment (CSA) followed by a Corrective Action Plan (CAP). MB Haynes retained BLE to perform the CSA and to implement interim remedial actions.
A soil assessment in the release area was conducted in 2007 and 2008. The limits of contaminated soil were defined and a mobile source remediation unit (soil vapor extraction [SVE] system) was deployed in
2008 as an interim remedial action as approved by the DWM. The SVE system concluded operations in 2020 per DWM approval. Seventeen groundwater monitoring wells were installed by BLE from 2007 through 2009 to establish the horizontal limits of the free-product and dissolved phase gasoline. The wells were designated MW-27 through TMW-43. The limits of the gasoline contaminants were defined. Please note that a groundwater monitoring well designated MW-26 was already present on the MB Haynes property and was installed as part of the neighboring Andrex groundwater incident. Groundwater monitoring well MW-26 has been designated as the upgradient well for the MB Haynes groundwater incident. Additionally, BLE conducted surface water sampling in Smith Mill Creek Tributary and in Smith Mill Creek which are the receiving waters for the MB Haynes groundwater discharge. The surface water impacts were also substantially
defined by this assessment. Free-phase (free-product) gasoline was present near the release area (gas pump) and near Smith Mill Creek Tributary. BLE initiated product removal in 2008 utilizing a passive downhole skimmer in several affected wells. Product recovery from the skimmer was performed by MB Haynes. Aggressive fluid vapor recovery (AFVR) was also performed in affected wells by a contractor retained by MB Haynes in 2007 and 2008.
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A free-product interceptor trench was designed by BLE and installed by MB Haynes in February 2009 near Smith Mill Creek Tributary. Product recovery from the trench was performed by MB Haynes from November 2009 until December 2020 when the DWM approved termination of remedial actions. Several groundwater and surface water sampling events have been conducted as part of the CSA. As required by the DWM we conducted one site-wide groundwater and surface water sampling event in January 2010 to establish baseline water quality conditions. The results of the 2010 event have been
submitted to the DWM. The DWM required that MB Haynes perform subsequent annual sampling events to monitor groundwater quality and to evaluate effectiveness of the ongoing remedial measures. Annual sampling events have been conducted each winter or early spring from 2010 through March 2022.
On December 10, 2020, Ms. Caroline LaFond of the DWM communicated with MB Haynes and BLE concerning a request for site closure. Ms. LaFond outlined an approach for the site to quality for a NORP.
The approach included termination of remedial actions (SVE and Product Recovery in December 2020) and the performance of four (4) semi-annual water quality sampling events to be conducted in 2021 and 2022. The schedule and sampling plan was documented in a letter dated December 16, 2020 from BLE to the DWM on behalf of MB Haynes. As of January 2021, all remedial actions have been terminated. Sampling will be performed in accordance with the DWM approved 2020-2022 Sampling Matrix (Table 1A). This report describes the final semi-annual required sampling event to comply with the DWM requirements.
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2.0 SCOPE OF SERVICES
2.1 Groundwater Sampling On September 26, 2022, groundwater levels were measured in the monitoring wells (Table 1B). Please note that monitoring wells MW-7, MW-17, and MW-23 were installed on off-site properties as part of an assessment at the neighboring former Andrex Industries facility. Water levels are measured in those wells for preparation of a groundwater elevation map. The wells are not part of the MB Haynes groundwater incident and are not sampled. A groundwater elevation map was prepared from the data (Figure 2).
Groundwater at the site flows to the north from Deaverview Road to the Smith Mill Creek Tributary (discharge location).
On September 27, 2022, groundwater samples were collected from groundwater monitoring wells specified on Table 1A. Seventeen (17) groundwater samples and one trip blank were submitted to Pace Analytical Services LLC (Pace) in West Columbia, SC for analysis of volatile organic compounds (VOCs) with IPE
and MTBE by EPA Method 8260D. Groundwater monitoring well MW-36 had an insufficient volume of water and could not be sampled. Sampling procedures and groundwater sampling logs are provided in Appendix A. 2.2 Surface Water Sampling On September 28, 2022, eight (8) surface water samples and one trip blank were collected and submitted to Pace for analysis of VOCs with IPE and MTBE by EPA Method 8260D. The samples were collected from Smith Mill Creek Tributary and from Smith Mill Creek at locations established in previous sampling events as specified on Table 1A.
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3.0 SAMPLING RESULTS
3.1 Groundwater Results The groundwater laboratory data is included in Appendix B and is summarized on Table 2. A plume map has been prepared from the data (Figure 3). Historical summary tables and plots are included in Appendix C for reference. The summary plots include bottom and top of screen elevation and historical groundwater elevations.
The current laboratory analytical results indicate that concentrations of several petroleum hydrocarbons have been detected which exceed the North Carolina NC2L groundwater standards (Table 2). Additionally, benzene was detected in exceedance of the DWM Gross Contamination Levels for Groundwater (GCL) Rev.
10/8/2020 in MW-28. The data shows that the dissolved phase gasoline plume originates near the fuel pump (release area) and travels to the north and northeast until discharging into Smith Mill Creek Tributary. Historically, hydrocarbon compounds have not been detected on the opposite side of the tributary (MW-39)
and sampling was discontinued in that well in 2017. Concentrations of dissolved phase hydrocarbons which indicate near free-product conditions are present in MW-28, MW-29, MW-35, and TMW-43. General declining concentration trends are observed in all monitoring wells. It is noted that monitoring wells MW-40 and MW-41 reached non-detect levels for the first time in 2017 however both rebounded slightly in 2018 to 2020. The groundwater impacts as the result of the MB Haynes release have been defined and are limited in extent to the MB Haynes property. The data indicates that the no off-site properties have been impacted by the release. The historical summary plots indicate that groundwater levels have risen in every well since 2007 to historical highs in 2016 and 2021 (Appendix C). 3.2 Surface Water Results The surface water laboratory data is included in Appendix B and summarized on Table 3. Please note that
any chlorinated solvent compounds detected in the samples are the results of the Andrex groundwater incident and those data have not been summarized on Table 3. The surface water sampling locations are designated SMT-1 through SMT-13 (Figure 4). Historical summary tables are included in Appendix D for reference.
Plots of historical total VOC concentrations are also included in Appendix D. The plots show decreasing or stable surface water concentration trends at most locations. The results indicate a slight increase in total VOC concentrations at SMT-7 since 2017 however, concentrations at this sampling location are declining overall.
No detected concentration of VOCs related to the MB Haynes incident exceed the North Carolina NC2B surface water standards in September 2022. The data shows that the gasoline-derived compounds discharge near the SMT-8 location and migrate downstream towards Smith Mill Creek to the east. The petroleum hydrocarbons reach non-detect levels at the SMT-1 location. It is noted that sampling is no longer performed downstream of SMT-4 per the approved matrix (Table 1B). Any petroleum hydrocarbon impacts in Smith Mill Creek and specifically further downstream of SMT-13 (which are not sampled as part of this monitoring program) cannot be directly attributed to the release at MB Haynes since numerous retail gasoline stations are present in these areas. The surface water impacts, as the result of the MB Haynes incident, have been substantially defined by this assessment.
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4.0 SUMMARY OF REMEDIATION PROGRESS
4.1 Aggressive Fluid Vapor Recovery (AFVR) AFVR was implemented as an interim remedial measure in December 2007 and was discontinued in November 2008. A total of seven single-day AFVR events were conducted as follows:
Date Duration and Location Recovery

The AFVR events recovered a total of approximately 250 gallons of free-product gasoline. AFVR events continued until replaced with alternate remedial technologies discussed below. 4.2 Passive Product Skimmer Gasoline product was skimmed from several wells via a downhole gravity-feed passive product skimmer from January 24, 2008 to February 22, 2010. The skimmer was deployed in MW-30, MW-35, and MW-
40. Total product recoveries via skimmer were as follows: MW-30 (0.15 gallons), MW-35 (56.94 gallons), MW-40 (0.02 gallons). Detailed product recovery records are shown on Tables 4 & 5. Product recovery via skimmer was discontinued after product was no longer present in sufficient quantities for operation of the skimmer. Product recovery continued at other locations via alternate technologies discussed below. 4.3 Product Recovery from the Interceptor Trench
A free-product interceptor trench was designed by BLE and installed by MB Haynes in February 2009 near Smith Mill Creek Tributary (Figures 2 & 3). The trench consists of 10 trench extraction pipes designated TEP-1 through TEP-10 installed in a 100-foot-long gravel-filled trench. A short gravel filled trench branch (installed in Fall 2009) also extends to MW-28 from the trench proper.
Product thickness measurements were collected by BLE from February 2009 through November 2009 at which time sufficient product had accumulated and product recovery was initiated by MB Haynes. Product recovery from the trench has been performed since November 17, 2009 and continued through 2020 as
approved. Product was initially recovered via a surface operated peristaltic pump utilizing tubing and a foam float.
This process was changed in late 2010 to a surface operated vacuum system with tubing and foam float. Product was transferred into steel drums and subsequently disposed by a licensed waste hauler/disposer retained by MB Haynes. A total of approximately 797.6 gallons of gasoline have been recovered from the trench from November 17, 2009 to the beginning of 2017. Detailed trench recovery records are included on Table 6A & 6B. Only 108 ounces of free product were recovered from the trench in 2014 during one event in October 2014. Product gauging indicates that insufficient product accumulated (typically <0.02 feet) for recovery efforts to be effective from October 2014 to present using the vacuum system. Please note that product recovery from MW-28 has also been performed by MB Haynes since November 2009. However, less than three
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gallons of product has been recovered from the well. The product recovery history from MW-28 is not included on Table 6. On February 17, 2017, MB Haynes implemented product recovery efforts in all ten TEPs utilizing floating oil absorbent skimmers. The skimmers are constructed of hydrophobic polypropylene and are 3-inch diameter and 18-inches long. The first operational trial was from February 17, 2017 to July 5, 2017. Based on the data collected we determined that a 3-month operational period (replacement schedule) was optimal
during the operational trial. The second operational period of skimmer deployment was from July 5, 2017 to October 4, 2017. New absorbent skimmers were deployed on October 4, 2017. BLE was retained by MB Haynes to perform quarterly inspections of the skimmers and to gauge product thickness. The
approximate saturation level of skimmers was visually identified each quarter by BLE and the skimmers were replaced by MB Haynes, as needed. A replacement schedule of more than 3 months was implemented. Spent skimmers were collected by MB Haynes for disposal by a licensed disposal contractor. The use of
absorbent skimmers was terminated at the end of the 2020 calendar year as approved. 4.4 Soil Vapor Extraction (SVE) System As part of the DWM approved interim remedial actions, a SVE system (mobile source remediation unit) was placed in operation in 2008 to remediate contaminated soil in the source area. Vacuum was applied to four SVE wells designated SVE-1 through SVE-4 (Figures 2 & 3) connected to a mobile enclosed-trailer system (near MW-34; location not shown). The extraction wells’ screen zones span the vadose zone of the source area. The system was deployed from July 1, 2008 to June 30, 2012 (4 years) as described above. The SVE system performance records for four operational years are shown on Table 7 (July 1, 2008 to June 30, 2009), Table 8 (July 1, 2009 to June 30, 2010), Table 9 (July 1, 2010 to June 30, 2011), and Table 10 (July 1, 2011 to June 30, 2012).
On July 2, 2012, the system was disconnected from the SVE wells and connected to the interceptor trench (TEP-5) and to monitoring wells MW-28 and MW-35. On July 9, 2012, the system was disconnected from TEP-5 and connected to TEP-3. It was determined that TEP-5 had insufficient screen exposed to the vadose
zone for effective vapor extraction. The SVE system performance records for one operational year are shown on Table 11 (July 2, 2012 to June 30, 2013). On June 28, 2013, the SVE system was reconnected to the SVE wells in the source area and was in operation using this configuration until the end of the 2020 calendar year per approval. In November 2014, the SVE system was also connected to MW-35. SVE system performance records for these periods are shown on Table 12 (June 28, 2013 to June 30, 2014), Table 13 (June 30, 2014 to June 30, 2015), Table 14 (June 30, 2015 to June 30, 2016), Table 15 (June 30, 2016 to June 30, 2017), Table 16 (June 30, 2017 to June 30, 2018), Table 17 (June 30, 2018 to June 30, 2019), Table 18 (June 30, 2019 to March 30, 2020), and Table 19 (June 30, 2020 to December 31, 2020). A total of 25 gallons of gasoline was recovered during the last operational 6-month period ending December 21, 2020.
Approximately 3,749 gallons of gasoline have been recovered by the SVE system operating in the source area through December 31, 2020. An additional 293 gallons of gasoline were recovered from SVE operation in the interceptor trench area from July 2, 2012 to June 28, 2013. Plots of the stack emissions and gasoline recovery in each area are included in the tables section of this report.
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5.0 FUTURE COMPLIANCE MONITORING & REMEDIATION EFFECTIVENESS
5.1 Product Recovery & SVE Operations Product recovery records from the interceptor trench and SVE system indicate that these technologies are effective. Product has not been present in the interceptor trench in sufficient quantities for significant recovery since May 2012. However, groundwater levels have risen significantly since trench installation. Groundwater levels are at or above the top of screen in the TEPs. Product gauging was performed every three months until terminated in December 2020. The SVE system extracted approximately 293 gallons of
gasoline from the interceptor trench area until reaching asymptotic low levels in approximately February 2013.
The SVE system operations in the release area has been very effective, removing almost 3,750 gallons of gasoline from the soil and groundwater in 12.5 years of operation. SVE operations appear to have reached asymptotic recovery levels. Operation of the SVE system was terminated in December 2020 and the mobile
SVE unit has been removed from the facility. 5.2 Groundwater Groundwater has reached compliance limits at the MW-30 and MW-34 locations in the release area in 2011 and these conditions were confirmed in 2012 and 2013. However, a slight rebound (below 2L Standards) was observed in MW-30 in 2013. The groundwater in the release area is in compliance as of March 2014 and these wells were no longer sampled as of 2017 as part of the annual sampling program established at that time. Total VOC concentrations at downgradient locations (MW-27, MW-29, MW-32, MW-35, MW-40, MW-41, and TMW-42) have shown decreasing trends. Groundwater in monitoring well MW-32 reached
compliance limits in March 2016. Groundwater in monitoring wells MW-40 and MW-41 reached compliance limits in March 2016 and reached ND status in March 2017. However, a slight rebound occurred in 2018 and 2019 and benzene exceeded NC2L standards in MW-40 in September 2022.
Near free-product concentrations have been observed in the groundwater at the MW-28, MW-29, MW-35, and possibly TMW-43 locations. Total VOC concentrations declined substantially in MW-28 since 2018
as groundwater levels rose above the top of the well screen, with the lowest concentrations to-date in March 2022. In September 2022, total VOC concentrations rebounded in MW-28, with the concentration of
benzene (6,800 µg/l) in exceedance of the GCL of 5,000 µg/l. The total VOC concentrations have declined in MW-29 and MW-35 and groundwater levels remain below the top of the well screens. It should be noted that the groundwater in monitoring well MW-36 exhibited near free-product concentrations (above 5,000
µg/l) in March 2015 and prior but concentrations have decreased significantly (to 141 µg/l) in March 2022. The results of the groundwater assessment demonstrate general stability (either stable or continued downward concentration trends). Additionally, only benzene was detected in exceedance of the GCL in MW-28 in September 2022.

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5.3 Surface Water Overall surface water contaminant concentration trends are decreasing at most locations. Slight increases of total VOC concentrations were observed in SMT-5, SMT-6, and SMT-7 from 2017 through March 2021 however, in September 2022, total VOC concentrations at SMT-6 reached the lowest concentrations to-date and SMT-5 reached ND status for the first time. Surface water collected at SMT-8 reached ND status in September 2021 and again in September 2022 after a very slight rebound in March 2022. In September 2022, VOCs were not detected downstream of SMT-6. The surface water sampling in 2022 is the fifth year that
a reduced DWM approved surface water sampling matrix is being used for the site. The matrix eliminated consistent non-detect surface water sample locations SMT-9 and SMT-10 (upstream) and SMT-11, SMT-12, and SMT-13 (downstream). There were no detections of MB Haynes incident VOCs at the sampled
locations in September 2022 which exceed NC2B standards for Class C freshwater. 5.4 Incident Closure and Future Monitoring and Remediation
It is noted that off-site groundwater has not been impacted by the release at MB Haynes. It is also noted that no VOC concentrations in the surface water from the release at MB Haynes exceed the NC2B standards for Class C freshwater. In May 2020 we requested that the DWM review the March 2020 report and determine if the incident at the site qualifies for closure under the NC General Statutes 130A-310.65 through 310.77 for risk-based remediation. Furthermore, we requested that the DWM provide guidance on any actions (supplemental to the 2020 report) required by MB Haynes to evaluate site conditions to achieve closure. We recommended that operation of the SVE system be discontinued if authorized by the DWM. We also recommended that the other existing interim remedial measures (product recovery via absorbent skimmers)
be discontinued, if authorized by the DWM. On December 10, 2020, Ms. Caroline LaFond of the DWM communicated with MB Haynes and BLE
concerning a request for site closure. Ms. LaFond outlined an approach for the site to qualify for a NORP. The approach included termination of remedial actions (SVE and Product Recovery in December 2020) and the performance of four (4) semi-annual water quality sampling events to be conducted in 2021 and 2022.
The schedule and sampling plan was documented in a letter dated December 16, 2020 from BLE to the DWM on behalf of MB Haynes. Remedial operations were terminated in December 2020 as approved by the DWM. BLE performed the fourth of the four required semi-annual sampling events during September 2022 documented herein. The results indicated that the detected concentration of benzene in MW-28 exceeded the GCL. BLE contacted Ms. LaFond to discuss the findings on November 30, 2022. Ms. LaFond stated that the DWM cannot complete an NORP with GCL exceedances. The DWM suggested that MB Haynes perform a single day 8-hour duration AFVR event in MW-28 to attempt to remove residual product and potentially lower the benzene concentration to below the GCL. The DWM also specified a post-AFVR sampling frequency for 2023 to demonstrate compliance for the NORP. The remediation and monitoring activities suggested by
the DWM began in January 2023 and are ongoing. Documentation of those activities will be provided under separate cover.
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6.0 QUALIFICATION OF REPORT
The activities and evaluative approaches used in this assessment are consistent with those normally employed in environmental assessment projects of this type. Our evaluation of the site conditions was based on the unique project information and data obtained. This report has been prepared on behalf of and exclusively for the use of MB Haynes Corporation, Asheville, North Carolina. This report and the findings contained herein are not intended to be relied upon
by any other party without BLE’s prior written consent.

Tables and SVE System Plots

Table 1A
2021-2022 Sampling Matrix
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. 5293-21/22
March 2021 September 2021 March 2022 September 2022
St
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t
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n
VO
C
s
Wa
t
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r

L
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l
VO
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s
Wa
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L
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Wa
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L
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l
VO
C
s
Wa
t
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L
e
v
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l
Groundwater
MW-26 No Yes Yes Yes No Yes Yes Yes
MW-27 Yes Yes Yes Yes Yes Yes Yes Yes
MW-28 Yes Yes Yes Yes Yes Yes Yes Yes
MW-29 Yes Yes Yes Yes Yes Yes Yes Yes
MW-30 No Yes Yes Yes No Yes Yes Yes
MW-31 No Yes Yes Yes No Yes Yes Yes
MW-32 Yes Yes Yes Yes Yes Yes Yes Yes
MW-33 No Yes Yes Yes No Yes Yes Yes
MW-34 No Yes Yes Yes No Yes Yes Yes
MW-35 Yes Yes Yes Yes Yes Yes Yes Yes
MW-36 Yes Yes Yes Yes Yes Yes Yes Yes
MW-37 No Yes Yes Yes No Yes Yes Yes
MW-38 No Yes Yes Yes No Yes Yes Yes
MW-39 No Yes Yes Yes No Yes Yes Yes
MW-40 Yes Yes Yes Yes Yes Yes Yes Yes
MW-41 Yes Yes Yes Yes Yes Yes Yes Yes
TMW-42 Yes Yes Yes Yes Yes Yes Yes Yes
TMW-43 Yes Yes Yes Yes Yes Yes Yes Yes
Surface Water
SMT-1 Yes --Yes --Yes --Yes --
SMT-2 Yes --Yes --Yes --Yes --
SMT-3 Yes --Yes --Yes --Yes --
SMT-4 Yes --Yes --Yes --Yes --
SMT-5 Yes --Yes --Yes --Yes --
SMT-6 Yes --Yes --Yes --Yes --
SMT-7 Yes --Yes --Yes --Yes --
SMT-8 Yes --Yes --Yes --Yes --
SMT-9 No --No --No --No --
SMT-10 No --No --No --No --
SMT-11 No --No --No --No --
SMT-12 No --No --No --No --
SMT-13 No --No --No --No --
Notes:
VOC analyses performed by EPA Method 8260D
Matrix approved by DEQ via email on December 10, 2020
Table 1A Matrix 2021-2022 of 5293-22B MB Haynes Sept 2022 Tables 1-3.xlsx
Prepared by: AWA
Checked by: TJB
Table 1B
Well Construction and Groundwater Elevation Data
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
September 26, 2022
Meas. Pt.Gnd. Surface Depth to Product Depth to Water Product *Total Borehole *Screen Well Well *Top of Rock *Top of
Well Northing Easting Latitude (N) Longitude (W)Elevation Elevation Product (bmp)Elevation Water (bmp)Elevation Thickness Depth (bgs)Depth (bgs)Type Monitors Depth (bgs)Rock Elev.
MW-7**NM NM 35.580866 -82.613866 2218.35 2218.60 NE NE 26.29 2192.06 NE 35.0 24.5 -34.5 2194.1 -2184.1 II BR 12.0 2206.6
MW-17**NM NM NM NM 2094.64 2094.74 NE NE 3.89 2090.75 NE 14.2 4.0 -14.0 2090.7 -2080.7 II SAP 14.2 2080.5
MW-23**NM NM 35.582017 -82.611985 2145.05 2145.20 NE NE 26.90 2118.15 NE 41.5 31.0 -41.5 2114.2 -2103.7 IIIo BR 30.0 2115.2
MW-26**685997.54 925050.12 35.581075 -82.616078 2207.46 2207.62 NE NE 29.71 2177.75 NE 51.5 41.0 -51.0 2166.6 -2156.6 II PWR/BR 42.0 2165.6
MW-27 686556.74 925676.60 35.582724 -82.614065 2112.81 2109.61 NE NE 6.64 2106.17 NE 6.7 2.5 -6.5 2107.1 -2103.1 II SAP 6.7 2102.9
MW-28 686494.52 925600.75 35.582562 -82.614284 2124.58 2121.01 *NE**NE*13.21 2111.37 *NE*15.2 10.0 -15.0 2111.0 -2106.0 II SAP 15.2 2105.8
MW-29 686550.60 925562.06 35.582689 -82.614399 2117.15 2113.90 *NE**NE*7.47 2109.68 *NE*12.2 2.5 -12.0 2111.4 -2101.9 II SAP 12.2 2101.7
MW-30 686251.99 925425.59 35.581801 -82.614833 2195.78 2196.05 NE NE 46.42 2149.36 NE 61.0 46.0 -61.0 2150.1 -2135.1 II PWR/BR 61.0 2135.1
MW-31 686357.35 925684.35 35.582113 -82.613992 2187.25 2187.43 NE NE 55.83 2131.42 NE 75.0 55.3 -70.3 2132.1 -2117.1 II SAP/PWR 60.0 2127.4
MW-32 686357.66 925495.94 35.582112 -82.614624 2183.85 2184.03 NE NE 52.24 2131.61 NE 82.0 49.0 -64.0 2135.0 -2120.0 II PWR 64.0 2120.0
MW-33 686450.60 925403.22 35.582386 -82.614939 2177.77 2177.94 NE NE 52.43 2125.34 NE 102.0 46.8 -61.8 2131.1 -2116.1 II SAP/PWR 76.0 2101.9
MW-34 686254.86 925514.28 35.581852 -82.614618 2195.27 2195.50 NE NE 53.16 2142.11 NE 67.0 51.6 -66.6 2143.9 -2128.9 II PWR/BR 50.0 2145.5
MW-35 686379.00 925570.41 35.582192 -82.614384 2190.64 2187.89 *NE**NE*65.20 2125.44 *NE*75.0 59.6 -74.6 2128.3 -2113.3 II PWR/BR 61.0 2126.9
MW-36 686595.67 925819.16 35.582841 -82.613573 2112.76 2109.49 NE NE 8.44 2104.32 NE 6.0 3.0 -6.0 2106.5 -2103.5 II Alluvium 6.0 2103.5
MW-37 686627.42 925425.50 35.582904 -82.614894 2123.88 2120.91 NE NE 11.90 2111.98 NE 20.0 6.0 -16.0 2114.9 -2104.9 II Alluvium NE NE
MW-38 686668.05 926046.46 35.583090 -82.612765 2110.25 2107.44 NE NE 11.38 2098.87 NE 16.5 6.3 -16.3 2101.1 -2091.1 II PWR/BR 16.0 2091.4
MW-39 686641.86 925619.36 35.582932 -82.614240 2116.44 2113.54 NE NE 6.49 2109.95 NE 12.0 2.2 -10.7 2111.4 -2102.9 II PWR NE NE
MW-40 686505.12 925709.83 35.582558 -82.613866 2136.28 2133.68 *NE**NE*25.53 2110.75 *NE*36.0 18.8 -33.8 2114.9 -2099.9 II PWR/BR 21.0 2112.7
MW-41 686539.44 925750.14 35.582658 -82.613806 2133.14 2130.34 NE NE 25.31 2107.83 NE 36.0 15.8 -30.8 2114.5 -2099.5 II PWR/BR 20.0 2110.3
TMW-42 686593.54 925761.00 35.582848 -82.613775 2111.44 2109.16 NE NE 6.45 2104.99 NE 11.0 2.8 -7.8 2106.4 -2101.4 II ALLV/SAP 11.0 2098.2
TMW-43 686621.59 925823.58 35.582880 -82.613575 2110.48 2108.24 NE NE 6.38 2104.10 NE 8.0 2.8 -7.8 2105.4 -2100.4 II ALLV/SAP NE NE
Notes:
*Values rounded to the nearest 0.1-ft.Water levels measured on 9/26/2022.II = Type II well.
NM = Not Measured.Measuring Point Elevation is top of casing.IIIo = Type III open bedrock well.
NE = Not Encountered.bgs = below ground surface.BR & PWR = Bedrock & Partially Weathered Rock.
Northing and Easting in feet (NC Grid 1983).bmp = below measuring point.SAP = Saprolite.
Latitude and longitude measured by hand-held GPS in March 2014.ALLV = Alluvium.
**Upgradient or sidegradient wells installed as part of Andrex Groundwater Incident No. 6586.Water elevations corrected for product thickness using a specific gravity of 0.70 for product.
*Screen
Elevation
Table 1B Well Sept 2022 of 5293-22B MB Haynes Sept 2022 Tables 1-3.xlsx
Prepared by: TAO
Checked by: ___
Table 2
Laboratory Analytical Results of Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
GCL 5,000 5,900 8,800 14,750 70,000 80,000 30,500 11,700 20,000 6,000 26,100 260,000 28,500 NE 24,100 50,000 NE
9/27/2022 MW-26 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 MW-27 2.0 ND 3.3 ND 0.68 ND 0.44 ND 15 ND ND ND ND NT ND ND 21
9/27/2022 MW-28 6,800 ND ND ND ND 2,300 48 ND 100 280 130 18,000 1,200 NT 280 8,700 37,838
9/27/2022 MW-29 600 ND 12 ND ND 1,500 85 8.4 4.2 330 280 1,300 2,500 NT 640 3,400 10,660
9/27/2022 MW-30 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2022 MW-31 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2022 MW-32 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2022 MW-33 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2022 MW-34 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2022 MW-35 1,000 31 14 ND ND 620 83 12 23 300 230 110 560 NT 290 380 3,653
NS MW-36 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 MW-37 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2022 MW-38 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2022 MW-39 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2022 MW-40 4.2 1.1 1.0 ND ND ND 2.5 ND 0.56 4.6 ND ND ND NT ND ND 14.0
9/27/2022 MW-41 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2022 TMW-42 8.3 1.9 2.9 0.44 ND 29 6.9 0.81 6.3 5.0 14 1.0 14 NT ND 3.5 94
9/27/2022 TMW-43 1.8 ND 19 0.63 ND 130 60 14 1.2 130 200 7.5 1,200 NT 430 350 2,544
Notes:
VOC analyses performed by EPA Method 8260D.
Units in mg/l or parts per billion (ppb).
Concentrations of Chloroform detected in March 2022 are presumed laboratory error and are not shown on this table.
Refer to laboratory data for concentrations corresponding to "J" and "H" values.
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022). Note: Standard for p-Isopropyltoluene is an IMAC.
GCL = North Carolina Gross Contaminant Levels for Groundwater revised October 8, 2020.
NS = not sampled; well removed from the sampling matrix per DEQ approval on October 26, 2017, via email.
NE = not established.
ND = not detected at laboratory detection limit.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
MW-23 was dry at the time of sampling
1,200 = concentration exceeds NC2L Standard
6,000 = concentration exceeds GCL Standard
5293-22B MB Haynes Sept 2022 Tables 1-3.xlsx
Table 2 GW Sept 2022
Prepared by: RLB
Checked by: ACJ/TAO
Table 3
Laboratory Analytical Results of Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2B 51 20,000 97 320 1,500 12 80 11 390 NE 215 670 NE
9/28/2022 SMT-1 35.584589 -82.610554 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2022 SMT-2 35.585910 -82.609740 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2022 SMT-3 35.586844 -82.608658 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2022 SMT-4 35.587431 -82.608079 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2022 SMT-5 35.583409 -82.611893 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2022 SMT-6 35.583170 -82.612799 0.56 ND ND ND ND ND ND 0.68 ND NT ND ND 1.2
9/28/2022 SMT-7 35.583050 -82.613437 6.0 ND 2.0 ND ND 0.75 ND 7.2 1.5 NT 0.50 5.4 23.4
9/28/2022 SMT-8 35.582619 -82.614182 ND ND ND ND ND ND ND ND ND NT ND ND ND
NS SMT-9 35.583249 -82.615234 NS NS NS NS NS NS NS NS NS NS NS NS NS
NS SMT-10 35.583399 -82.615677 NS NS NS NS NS NS NS NS NS NS NS NS NS
NS SMT-11 35.588768 -82.606153 NS NS NS NS NS NS NS NS NS NS NS NS NS
NS SMT-12 35.589361 -82.601256 NS NS NS NS NS NS NS NS NS NS NS NS NS
NS SMT-13 35.587746 -82.598367 NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
VOC analyses performed by EPA Method 8260D.
Units in mg/l or parts per billion (ppb).
Detected concentrations of chlorinated solvents (if detected) are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021).
Latitude and longitude measured by hand-held GPS in March 2014.
Refer to laboratory data for concentrations corresponding to "J" values.
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
2.0 = concentration exceeds NC2B Standard.
5293-22B MB Haynes Sept 2022 Tables 1-3.xlsx
Table 3 SW Sept 2022
Prepared by: RLB
Checked by: ACJ/TAO
Table 4
Product Skimmer Recovery History
MW-30 and MW-35
January 2008 through May 2009
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
MW-30 (Jan. to Sept. 2008)MW-35 (September 2008)MW-35 (October 2008)MW-35 (November 2008)MW-35 (December 2008)
Date Time Volume Date Time Volume Date Time Volume Date Time Volume Date Time Volume
1/24/2008 900 8.0 9/9/2008 1530 30.0 10/1/2008 730 32.0 11/3/2008 830 32.0 12/1/2008 1100 32.0
1/28/2008 1340 8.0 9/10/2008 930 32.0 10/2/2008 1040 32.0 11/4/2008 800 32.0 12/2/2008 900 32.0
1/30/2008 1415 0.0 9/11/2008 1430 32.0 10/3/2008 800 32.0 11/5/2008 1330 32.0 12/3/2008 1430 32.0
2/1/2008 1051 0.0 9/12/2008 900 32.0 10/4/2008 730 32.0 11/6/2008 1300 32.0 12/4/2008 1430 32.0
2/6/2008 838 0.0 9/15/2008 1130 32.0 10/6/2008 730 32.0 11/7/2008 930 32.0 12/5/2008 830 32.0
2/11/2008 1050 1.0 9/16/2008 900 32.0 10/7/2008 730 32.0 11/8/2008 1030 32.0 12/6/2008 930 32.0
2/18/2008 330 1.0 9/17/2008 930 32.0 10/8/2008 730 32.0 11/9/2008 1330 32.0 12/7/2008 1320 32.0
2/27/2008 940 1.0 9/18/2008 1000 32.0 10/9/2008 800 32.0 11/10/2008 1430 32.0 12/8/2008 1330 32.0
2/29/2008 1015 0.25 9/19/2008 900 32.0 10/13/2008 1345 32.0 11/11/2008 1500 32.0 12/9/2008 1000 32.0
3/5/2008 1423 0.0 9/22/2008 1400 32.0 10/14/2008 1345 32.0 11/12/2008 1300 32.0 12/10/2008 1300 32.0
3/13/2008 1033 0.0 9/23/2008 1330 32.0 10/15/2008 1345 32.0 11/13/2008 1530 32.0 12/11/2008 1100 32.0
3/18/2008 1441 0.0 9/24/2008 900 32.0 10/16/2008 1335 32.0 11/14/2008 900 32.0 12/12/2008 1200 32.0
3/25/2008 1430 0.0 9/25/2008 900 32.0 10/17/2008 815 32.0 11/15/2008 1000 32.0 12/15/2008 1100 32.0
3/31/2008 900 0.0 9/26/2008 1000 32.0 10/20/2008 830 32.0 11/16/2008 1000 32.0 12/16/2008 1230 32.0
4/7/2008 1440 0.0 9/27/2008 1030 32.0 10/21/2008 1000 32.0 11/17/2008 1115 32.0 12/17/2008 910 32.0
4/21/2008 900 0.0 9/28/2008 1100 32.0 10/22/2008 1345 32.0 11/18/2008 1050 32.0 12/18/2008 800 32.0
4/28/2008 1450 0.0 9/29/2008 1500 32.0 10/23/2008 1500 32.0 11/19/2008 1418 32.0 12/19/2008 850 32.0
5/5/2008 722 0.0 9/30/2008 730 32.0 10/24/2008 900 32.0 11/20/2008 1000 32.0 12/22/2008 1030 32.0
5/12/2008 1005 0.0 10/27/2008 1500 32.0 11/21/2008 1300 32.0 12/23/2008 1400 32.0
5/20/2008 1230 0.0 10/28/2008 1500 32.0 11/24/2008 1030 32.0 12/24/2008 830 32.0
5/30/2008 730 0.0 10/29/2008 1500 32.0 11/25/2008 1430 32.0 12/29/2008 750 32.0
7/25/2008 1043 0.0 10/30/2008 810 32.0 11/26/2008 1200 32.0 12/30/2008 1525 32.0
8/1/2008 1100 0.0 10/31/2008 800 32.0 11/27/2008 900 32.0 12/31/2008 800 32.0
8/26/2008 1100 0.0 11/28/2008 800 32.0
9/8/2008 0.0
Total Recovery (ounces)19.25 Total Recovery (ounces)574 Total Recovery (ounces)736 Total Recovery (ounces)768 Total Recovery (ounces)736
Total Recovery (gals)0.15 Total Recovery (gals)4.48 Total Recovery (gals)5.75 Total Recovery (gals)6.00 Total Recovery (gals)5.75
MW-35 (January 2009)MW-35 (February 2009)MW-35 (March 2009)MW-35 (April 2009)MW-35 (May 2009)
Date Time Volume Date Time Volume Date Time Volume Date Time Volume Date Time Volume
1/5/2009 1500 32.0 2/2/2009 900 32.0 3/2/2009 1000 32.0 4/1/2009 700 32.0 5/1/2009 900 32.0
1/6/2009 1300 32.0 2/3/2009 730 32.0 3/3/2009 1300 32.0 4/2/2009 1430 32.0 5/4/2009 1100 32.0
1/7/2009 1000 32.0 2/4/2009 830 32.0 3/4/2009 1400 32.0 4/3/2009 1035 32.0 5/5/2009 1300 32.0
1/8/2009 1430 32.0 2/5/2009 825 32.0 3/5/2009 800 32.0 4/6/2009 1300 32.0 5/6/2009 1000 32.0
1/9/2009 900 32.0 2/6/2009 1015 32.0 3/6/2009 900 32.0 4/7/2009 930 32.0 5/7/2009 800 32.0
1/12/2009 1100 32.0 2/9/2009 100 32.0 3/9/2009 1100 32.0 4/8/2009 900 32.0 5/8/2009 1300 32.0
1/13/2009 1033 32.0 2/10/2009 800 32.0 3/10/2009 1200 32.0 4/9/2009 945 32.0 5/11/2009 900 32.0
1/14/2009 1450 32.0 2/11/2009 730 32.0 3/11/2009 1300 32.0 4/10/2009 1015 32.0 5/12/2009 1100 32.0
1/15/2009 735 32.0 2/12/2009 800 32.0 3/12/2009 1400 32.0 4/13/2009 900 32.0 5/13/2009 1400 32.0
1/19/2009 915 32.0 2/13/2009 800 32.0 3/13/2009 1000 32.0 4/14/2009 1330 32.0 5/14/2009 800 32.0
1/20/2009 820 32.0 2/16/2009 710 32.0 3/16/2009 800 32.0 4/15/2009 1000 32.0 5/15/2009 1100 32.0
1/21/2009 1300 32.0 2/17/2009 1518 32.0 3/17/2009 800 32.0 4/16/2009 900 32.0 5/18/2009 900 32.0
1/22/2009 800 32.0 2/18/2009 1430 32.0 3/18/2009 830 32.0 4/17/2009 800 32.0 5/19/2009 1400 32.0
1/23/2009 800 32.0 2/19/2009 900 32.0 3/19/2009 1400 32.0 4/20/2009 800 32.0 5/20/2009 923 32.0
1/26/2009 830 32.0 2/20/2009 1000 32.0 3/23/2009 800 32.0 4/21/2009 930 32.0 5/21/2009 1000 32.0
1/27/2009 900 32.0 2/23/2009 830 32.0 3/24/2009 1550 32.0 4/22/2009 1400 32.0 5/26/2009 800 32.0
1/28/2009 1130 32.0 2/24/2009 730 32.0 3/25/2009 1320 32.0 4/23/2009 800 32.0 5/27/2009 1300 32.0
1/29/2009 800 32.0 2/25/2009 1500 32.0 3/26/2009 1330 32.0 4/24/2009 1330 32.0 5/28/2009 900 32.0
1/30/2009 800 32.0 2/26/2009 715 32.0 3/27/2009 900 32.0 4/27/2009 800 32.0
2/27/2009 800 32.0 3/30/2009 1300 32.0 4/28/2009 1030 32.0
3/31/2009 730 32.0 4/29/2009 1430 32.0
4/30/2009 1353 32.0
Total Recovery (ounces)608 Total Recovery (ounces)640 Total Recovery (ounces)672 Total Recovery (ounces)704 Total Recovery (ounces)576
Total Recovery (gals)4.75 Total Recovery (gals)5.00 Total Recovery (gals)5.25 Total Recovery (gals)5.50 Total Recovery (gals)4.50
Notes:
Volume in ounces unless specified otherwise
Maximum capacity of skimmer reservior is 32 ounces
Skimmer deployed in MW-30 on 1/24/08; Skimmer deployed in MW-35 on 9/8/08; Skimmer deployed in MW-40 on 12/1/09
Skimmer removed from MW-30 on 9/8/08; Skimmer removed from MW-35 on 11/30/09; Skimmer removed from MW-40 on 2/22/10
Table 4 Skim Rec Jan 08 May 09 of 5293-22B MB Haynes September 2022 Tables 4-5.xlsx
Prepared by: AWA/EJR
Checked by: IAI
Table 5
Product Skimmer Recovery History
MW-35 and MW-40
June 2009 through February 2010
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
MW-35 (June 2009)MW-35 (July 2009)MW-35 (August 2009)MW-35 (September 2009)MW-35 (October 2009)
Date Time Volume Date Time Volume Date Time Volume Date Time Volume Date Time Volume
6/1/2009 1105 32.0 7/1/2009 715 32.0 8/3/2009 800 0.0 9/1/2009 730 0.0 10/1/2009 1400 0.0
6/2/2009 900 32.0 7/1/2009 1600 11.0 8/4/2009 800 0.0 9/2/2009 800 0.0 10/5/2009 930 3.0
6/3/2009 1000 32.0 7/2/2009 700 12.0 8/5/2009 1100 0.0 9/3/2009 900 4.0 10/12/2009 730 0.0
6/4/2009 1100 32.0 7/2/2009 1100 12.0 8/6/2009 1255 0.0 9/14/2009 300 0.0 10/19/2009 1505 0.0
6/8/2009 900 32.0 7/2/2009 1630 12.0 8/10/2009 1325 2.0 9/21/2009 950 32.0 10/26/2009 745 0.0
6/9/2009 800 32.0 7/3/2009 700 32.0 8/11/2009 725 0.0 9/22/2009 700 32.0
6/10/2009 1000 32.0 7/3/2009 1150 15.0 8/12/2009 800 0.0 9/23/2009 1330 32.0
6/11/2009 815 32.0 7/3/2009 1630 15.0 8/13/2009 800 0.0 9/24/2009 700 18.0
6/15/2009 720 32.0 7/6/2009 630 32.0 8/17/2009 800 2.0 9/28/2009 930 12.0
6/15/2009 1200 32.0 7/6/2009 1130 15.0 8/18/2009 700 0.0 9/29/2009 700 12.0
6/15/2009 1500 32.0 7/6/2009 1630 15.0 8/19/2009 700 0.0 9/30/2009 730 12.0
6/16/2009 800 32.0 7/7/2009 730 4.0 8/20/2009 630 0.0
6/16/2009 1200 12.0 7/7/2009 1330 0.0 8/24/2009 700 0.0
6/17/2009 800 32.0 7/8/2009 800 0.0 8/25/2009 1300 0.0
6/17/2009 1415 32.0 7/8/2009 1330 0.0 8/31/2009 820 0.0
6/18/2009 730 32.0 7/9/2009 900 0.0
6/18/2009 1130 18.0 7/9/2009 1400 0.0
6/18/2009 1430 12.0 7/13/2009 1100 2.0
6/22/2009 700 32.0 7/14/2009 830 2.0
6/22/2009 1330 18.0 7/15/2009 800 2.0
6/23/2009 645 32.0 7/16/2009 700 2.0
6/23/2009 1415 32.0 7/20/2009 805 2.0
6/23/2009 1650 12.0 7/21/2009 700 0.0
6/24/2009 650 32.0 7/22/2009 815 0.0
6/24/2009 1000 12.0 7/23/2009 800 0.0
6/24/2009 1630 15.0 7/27/2009 1100 0.0
6/25/2009 630 32.0 7/28/2009 800 0.0
6/25/2009 1600 32.0 7/29/2009 1500 0.0
6/29/2009 1100 32.0 7/30/2009 800 0.0
6/29/2009 1600 32.0
6/30/2009 630 32.0
6/30/2009 1200 15.0
6/30/2009 1615 15.0
Total Recovery (ounces)897.00 Total Recovery (ounces)217 Total Recovery (ounces)4 Total Recovery (ounces)154 Total Recovery (ounces)3
Total Recovery (gals)7.01 Total Recovery (gals)1.70 Total Recovery (gals)0.03 Total Recovery (gals)1.20 Total Recovery (gals)0.02
MW-35 (November 2009)MW-40 (December 2009)MW-40 (January 2010)
Date Time Volume Date Time Volume Date Time Volume Date Time Volume
11/2/2009 1220 0.0 12/10/2009 900 2.0 1/19/2010 1500 0.0 2/5/2010 1300 0.0
11/9/2009 1400 0.0 12/17/2009 1500 0.0 2/14/2010 1100 0.0
11/16/2009 900 0.0 12/30/2009 1300 0.0
11/23/2009 1100 0.0
11/30/2009 800 0.0
Total Recovery (ounces)0 Total Recovery (ounces)2 Total Recovery (ounces)0 Total Recovery (ounces)0
Total Recovery (gals)0.00 Total Recovery (gals)0.02 Total Recovery (gals)0.00 Total Recovery (gals)0.00
Notes:
Volume in ounces unless specified otherwise
Maximum capacity of skimmer reservior is 32 ounces
Skimmer deployed in MW-30 on 1/24/08; Skimmer deployed in MW-35 on 9/8/08; Skimmer deployed in MW-40 on 12/1/09
Skimmer removed from MW-30 on 9/8/08; Skimmer removed from MW-35 on 11/30/09; Skimmer removed from MW-40 on 2/22/10
MW-40 (February 2010)
Table 5 Skim Rec Jun 09 Feb 10 of 5293-22B MB Haynes September 2022 Tables 4-5.xlsx
Prepared by: AWA
Checked by: BPN
Table 6A
Trench Extraction Pipe (TEP) Product Recovery History -- November 17, 2009 through December 31, 2020
TEP-1 through TEP-5
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J08-5293-08
TEP-1 TEP-2 TEP-3 TEP-4 TEP-5
Date Volume Date Volume Date Volume Date Volume Date Volume
11/17/2009 3.0 11/17/2009 0.0 11/17/2009 32.0 11/17/2009 0.0 11/17/2009 4.0
12/1/2009 8.0 12/1/2009 4.0 12/1/2009 16.0 12/1/2009 250.0 12/1/2009 12.0
12/10/2009 0.0 12/10/2009 0.0 12/10/2009 4.0 12/10/2009 6.0 12/10/2009 0.0
1/14/2010 10.0 1/14/2010 8.0 1/14/2010 40.0 1/14/2010 608.0 1/14/2010
1/19/2010 0.0 1/19/2010 1/19/2010 1/19/2010 1/19/2010 8.0
2/8/2010 0.0 2/8/2010 0.0 2/8/2010 0.0 2/8/2010 0.0 2/8/2010 0.0
2/24/2010 0.0 2/24/2010 24.0 2/24/2010 58.0 2/24/2010 0.0 2/24/2010 40.0
3/25/2010 0.0 3/25/2010 0.0 3/25/2010 8.0 3/25/2010 8.0 3/25/2010 32.0
4/21/2010 4/21/2010 4/21/2010 4/21/2010 4/21/2010 640.0
4/22/2010 4/22/2010 4/22/2010 4/22/2010 4/22/2010 128.0
5/7/2010 0.0 5/7/2010 12.0 5/7/2010 192.0 5/7/2010 192.0 5/7/2010 256.0
5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 640.0
5/28/2010 5/28/2010 5/28/2010 640.0 5/28/2010 960.0 5/28/2010 1280.0
6/11/2010 6/11/2010 6/11/2010 6/11/2010 960.0 6/11/2010 640.0
7/1/2010 768.0 7/1/2010 7/1/2010 1424.0 7/1/2010 7/1/2010 1280.0
7/22/2010 7/22/2010 7/22/2010 640.0 7/22/2010 7040.0 7/22/2010
7/30/2010 7/30/2010 7/30/2010 7/30/2010 7/30/2010
8/25/2010 1484.0 8/25/2010 48.0 8/25/2010 832.0 8/25/2010 8/25/2010
8/26/2010 8/26/2010 8/26/2010 680.0 8/26/2010 2304.0 8/26/2010
9/2/2010 9/2/2010 9/2/2010 9/2/2010 9/2/2010
9/7/2010 1840.0 9/7/2010 58.0 9/7/2010 280.0 9/7/2010 1280.0 9/7/2010
10/7/2010 10/7/2010 512.0 10/7/2010 744.0 10/6/2010 704.0 10/6/2010 1216.0
10/20/2010 808.0 10/20/2010 52.0 10/20/2010 108.0 10/20/2010 832.0 10/20/2010 832.0
11/9/2010 640.0 11/9/2010 640.0 11/9/2010 256.0 11/9/2010 1664.0 11/9/2010 512.0
11/17/2010 512.0 11/17/2010 128.0 11/17/2010 256.0 11/17/2010 896.0 11/17/2010 256.0
11/23/2010 512.0 11/23/2010 256.0 11/23/2010 256.0 11/23/2010 256.0 11/23/2010 256.0
12/7/2010 0.0 12/7/2010 0.0 12/7/2010 0.0 12/7/2010 128.0 12/7/2010 128.0
12/16/2010 0.0 12/16/2010 0.0 12/16/2010 0.0 12/16/2010 128.0 12/16/2010 128.0
12/21/2010 12/21/2010 12/21/2010 0.0 12/21/2010 64.0 12/21/2010 128.0
1/11/2011 0.0 1/11/2011 64.0 1/11/2011 0.0 1/11/2011 128.0 1/11/2011 64.0
1/20/2011 0.0 1/20/2011 0.0 1/20/2011 384.0 1/20/2011 640.0 1/20/2011 384.0
1/26/2011 0.0 1/26/2011 0.0 1/26/2011 512.0 1/26/2011 384.0 1/26/2011 512.0
2/3/2011 0.0 2/3/2011 0.0 2/3/2011 640.0 2/3/2011 768.0 2/3/2011 896.0
2/10/2011 128.0 2/10/2011 0.0 2/10/2011 512.0 2/10/2011 512.0 2/10/2011 384.0
2/16/2011 0.0 2/16/2011 0.0 2/16/2011 256.0 2/16/2011 128.0 2/16/2011 512.0
2/21/2011 0.0 2/21/2011 0.0 2/21/2011 512.0 2/21/2011 256.0 2/21/2011 384.0
2/28/2011 0.0 2/28/2011 0.0 2/28/2011 0.0 2/28/2011 128.0 2/28/2011 0.0
3/8/2011 0.0 3/8/2011 0.0 3/8/2011 0.0 3/8/2011 0.0 3/8/2011 0.0
3/17/2011 0.0 3/17/2011 0.0 3/17/2011 0.0 3/17/2011 0.0 3/17/2011 0.0
3/24/2011 0.0 3/24/2011 0.0 3/24/2011 128.0 3/24/2011 0.0 3/24/2011 0.0
3/31/2011 0.0 3/31/2011 0.0 3/31/2011 128.0 3/31/2011 0.0 3/31/2011 0.0
4/5/2011 64.0 4/5/2011 0.0 4/5/2011 0.0 4/5/2011 0.0 4/5/2011 128.0
4/13/2011 0.0 4/13/2011 0.0 4/13/2011 0.0 4/13/2011 0.0 4/13/2011 0.0
4/19/2011 128.0 4/19/2011 0.0 4/19/2011 0.0 4/19/2011 0.0 4/19/2011 0.0
4/28/2011 0.0 4/28/2011 0.0 4/28/2011 0.0 4/28/2011 0.0 4/28/2011 0.0
5/5/2011 0.0 5/5/2011 0.0 5/5/2011 0.0 5/5/2011 0.0 5/5/2011 64.0
5/11/2011 0.0 5/11/2011 0.0 5/11/2011 0.0 5/11/2011 0.0 5/11/2011 64.0
5/19/2011 0.0 5/19/2011 0.0 5/19/2011 0.0 5/19/2011 0.0 5/19/2011 0.0
5/26/2011 0.0 5/26/2011 0.0 5/26/2011 0.0 5/26/2011 0.0 5/26/2011 64.0
6/2/2011 0.0 6/2/2011 0.0 6/2/2011 0.0 6/2/2011 0.0 6/2/2011 64.0
6/9/2011 0.0 6/9/2011 0.0 6/9/2011 128.0 6/9/2011 128.0 6/9/2011 128.0
6/16/2011 0.0 6/16/2011 0.0 6/16/2011 0.0 6/16/2011 64.0 6/16/2011 0.0
6/23/2011 0.0 6/23/2011 0.0 6/23/2011 0.0 6/23/2011 0.0 6/23/2011 64.0
6/30/2011 0.0 6/30/2011 0.0 6/30/2011 64.0 6/30/2011 0.0 6/30/2011 0.0
7/7/2011 0.0 7/7/2011 0.0 7/7/2011 0.0 7/7/2011 0.0 7/7/2011 64.0
7/14/2011 0.0 7/14/2011 0.0 7/14/2011 0.0 7/14/2011 0.0 7/14/2011 0.0
7/21/2011 0.0 7/21/2011 0.0 7/21/2011 64.0 7/21/2011 0.0 7/21/2011 0.0
7/28/2011 0.0 7/28/2011 0.0 7/28/2011 0.0 7/28/2011 0.0 7/28/2011 0.0
8/4/2011 512.0 8/4/2011 512.0 8/4/2011 512.0 8/4/2011 0.0 8/4/2011 256.0
8/11/2011 128.0 8/11/2011 64.0 8/11/2011 256.0 8/11/2011 0.0 8/11/2011 64.0
8/18/2011 256.0 8/18/2011 256.0 8/18/2011 128.0 8/18/2011 0.0 8/18/2011 256.0
8/25/2011 384.0 8/25/2011 384.0 8/25/2011 384.0 8/25/2011 384.0 8/25/2011 0.0
8/31/2011 256.0 8/31/2011 256.0 8/31/2011 128.0 8/31/2011 64.0 8/31/2011 0.0
9/8/2011 0.0 9/8/2011 256.0 9/8/2011 128.0 9/8/2011 128.0 9/8/2011 0.0
9/16/2011 128.0 9/16/2011 128.0 9/16/2011 64.0 9/16/2011 64.0 9/16/2011 128.0
9/22/2011 0.0 9/22/2011 128.0 9/22/2011 256.0 9/22/2011 384.0 9/22/2011 384.0
9/29/2011 0.0 9/29/2011 128.0 9/29/2011 512.0 9/29/2011 128.0 9/29/2011 384.0
10/6/2011 0.0 10/6/2011 0.0 10/6/2011 640.0 10/6/2011 0.0 10/6/2011 640.0
10/13/2011 0.0 10/13/2011 256.0 10/13/2011 512.0 10/13/2011 512.0 10/13/2011 256.0
10/20/2011 512.0 10/20/2011 256.0 10/20/2011 384.0 10/20/2011 384.0 10/20/2011 0.0
10/27/2011 384.0 10/27/2011 384.0 10/27/2011 384.0 10/27/2011 384.0 10/27/2011 0.0
11/3/2011 384.0 11/3/2011 128.0 11/3/2011 128.0 11/3/2011 384.0 11/3/2011 512.0
11/10/2011 256.0 11/10/2011 0.0 11/10/2011 512.0 11/10/2011 128.0 11/10/2011 512.0
11/17/2011 128.0 11/17/2011 0.0 11/17/2011 384.0 11/17/2011 256.0 11/17/2011 384.0
11/23/2011 256.0 11/23/2011 128.0 11/23/2011 512.0 11/23/2011 128.0 11/23/2011 512.0
12/1/2011 256.0 12/1/2011 0.0 12/1/2011 512.0 12/1/2011 128.0 12/1/2011 640.0
12/8/2011 128.0 12/8/2011 0.0 12/8/2011 0.0 12/8/2011 128.0 12/8/2011 128.0
12/15/2011 384.0 12/15/2011 0.0 12/15/2011 256.0 12/15/2011 0.0 12/15/2011 640.0
12/22/2011 128.0 12/22/2011 0.0 12/22/2011 256.0 12/22/2011 0.0 12/22/2011 128.0
12/28/2011 256.0 12/28/2011 0.0 12/28/2011 384.0 12/28/2011 0.0 12/28/2011 384.0
1/5/2012 0.0 1/5/2012 0.0 1/5/2012 256.0 1/5/2012 128.0 1/5/2012 256.0
1/12/2012 0.0 1/12/2012 0.0 1/12/2012 0.0 1/12/2012 0.0 1/12/2012 0.0
1/19/2012 0.0 1/19/2012 0.0 1/19/2012 0.0 1/19/2012 128.0 1/19/2012 0.0
1/26/2012 0.0 1/26/2012 0.0 1/26/2012 0.0 1/26/2012 0.0 1/26/2012 0.0
2/2/2012 0.0 2/2/2012 0.0 2/2/2012 0.0 2/2/2012 0.0 2/2/2012 0.0
1 of 4
Table 6A 1-5 Trench Recovery of 5293-21A MB Haynes Trench Recovery Table 6A and B.xlsx
Prepared by: BPN
Checked by: AWA
Table 6A
Trench Extraction Pipe (TEP) Product Recovery History -- November 17, 2009 through December 31, 2020
TEP-1 through TEP-5
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J08-5293-08
TEP-1 TEP-2 TEP-3 TEP-4 TEP-5
Date Volume Date Volume Date Volume Date Volume Date Volume
2/9/2012 0.0 2/9/2012 0.0 2/9/2012 0.0 2/9/2012 0.0 2/9/2012 0.0
2/16/2012 0.0 2/16/2012 0.0 2/16/2012 0.0 2/16/2012 0.0 2/16/2012 0.0
2/21/2012 0.0 2/21/2012 0.0 2/21/2012 0.0 2/21/2012 0.0 2/21/2012 0.0
2/29/2012 0.0 2/29/2012 0.0 2/29/2012 0.0 2/29/2012 0.0 2/29/2012 0.0
3/8/2012 0.0 3/8/2012 0.0 3/8/2012 0.0 3/8/2012 0.0 3/8/2012 0.0
3/14/2012 0.0 3/14/2012 0.0 3/14/2012 0.0 3/14/2012 0.0 3/14/2012 128.0
3/22/2012 0.0 3/22/2012 0.0 3/22/2012 0.0 3/22/2012 64.0 3/22/2012 64.0
3/29/2012 0.0 3/29/2012 0.0 3/29/2012 0.0 3/29/2012 128.0 3/29/2012 128.0
4/5/2012 0.0 4/5/2012 0.0 4/5/2012 0.0 4/5/2012 128.0 4/5/2012 128.0
4/11/2012 0.0 4/11/2012 0.0 4/11/2012 64.0 4/11/2012 64.0 4/11/2012 128.0
4/19/2012 0.0 4/19/2012 0.0 4/19/2012 0.0 4/19/2012 0.0 4/19/2012 0.0
4/26/2012 0.0 4/26/2012 0.0 4/26/2012 0.0 4/26/2012 0.0 4/26/2012 0.0
5/3/2012 0.0 5/3/2012 0.0 5/3/2012 0.0 5/3/2012 0.0 5/3/2012 0.0
5/15/2012 0.0 5/15/2012 0.0 5/15/2012 0.0 5/15/2012 0.0 5/15/2012 0.0
5/24/2012 0.0 5/24/2012 0.0 5/24/2012 0.0 5/24/2012 0.0 5/24/2012 64.0
5/31/2012 0.0 5/31/2012 0.0 5/31/2012 0.0 5/31/2012 0.0 5/31/2012 0.0
6/7/2012 0.0 6/7/2012 0.0 6/7/2012 0.0 6/7/2012 0.0 6/7/2012 0.0
6/14/2012 0.0 6/14/2012 0.0 6/14/2012 0.0 6/14/2012 0.0 6/14/2012 0.0
6/20/2012 0.0 6/20/2012 0.0 6/20/2012 0.0 6/20/2012 0.0 6/20/2012 0.0
6/27/2012 0.0 6/27/2012 0.0 6/27/2012 0.0 6/27/2012 0.0 6/27/2012 0.0
7/3/2012 0.0 7/3/2012 0.0 7/3/2012 0.0 7/3/2012 0.0 7/3/2012 0.0
7/11/2012 0.0 7/11/2012 0.0 7/11/2012 0.0 7/11/2012 0.0 7/11/2012 0.0
7/16/2012 0.0 7/16/2012 0.0 7/16/2012 0.0 7/16/2012 0.0 7/16/2012 0.0
7/23/2012 0.0 7/23/2012 0.0 7/23/2012 0.0 7/23/2012 0.0 7/23/2012 0.0
7/30/2012 0.0 7/30/2012 0.0 7/30/2012 0.0 7/30/2012 0.0 7/30/2012 0.0
8/6/2012 0.0 8/6/2012 0.0 8/6/2012 0.0 8/6/2012 0.0 8/6/2012 0.0
8/13/2012 0.0 8/13/2012 0.0 8/13/2012 0.0 8/13/2012 0.0 8/13/2012 0.0
8/20/2012 0.0 8/20/2012 0.0 8/20/2012 0.0 8/20/2012 0.0 8/20/2012 0.0
8/27/2012 0.0 8/27/2012 0.0 8/27/2012 0.0 8/27/2012 0.0 8/27/2012 0.0
9/4/2012 0.0 9/4/2012 0.0 9/4/2012 0.0 9/4/2012 0.0 9/4/2012 0.0
9/18/2012 0.0 9/18/2012 0.0 9/18/2012 0.0 9/18/2012 0.0 9/18/2012 0.0
10/1/2012 0.0 10/1/2012 0.0 10/1/2012 0.0 10/1/2012 0.0 10/1/2012 0.0
10/17/2012 0.0 10/17/2012 0.0 10/17/2012 0.0 10/17/2012 0.0 10/17/2012 0.0
11/7/2012 0.0 11/7/2012 0.0 11/7/2012 0.0 11/7/2012 0.0 11/7/2012 0.0
11/21/2012 0.0 11/21/2012 0.0 11/21/2012 0.0 11/21/2012 0.0 11/21/2012 0.0
12/6/2012 0.0 12/6/2012 0.0 12/6/2012 0.0 12/6/2012 0.0 12/6/2012 0.0
12/20/2012 0.0 12/20/2012 0.0 12/20/2012 0.0 12/20/2012 0.0 12/20/2012 0.0
1/7/2013 0.0 1/7/2013 0.0 1/7/2013 0.0 1/7/2013 0.0 1/7/2013 0.0
12/9/2013 16.0 12/9/2013 16.0 12/9/2013 16.0 12/9/2013 0.0 12/9/2013 0.0
12/16/2013 0.0 12/16/2013 0.0 12/16/2013 0.0 12/16/2013 0.0 12/16/2013 0.0
6/30/2014 0.0 6/30/2014 0.0 6/30/2014 0.0 6/30/2014 0.0 6/30/2014 0.0
10/2/2014 0.0 10/2/2014 0.0 10/2/2014 0.0 10/2/2014 8.0 10/2/2014 0.0
4/23/2015 0.0 4/23/2015 0.0 4/23/2015 0.0 4/23/2015 0.0 4/23/2015 0.0
9/28/2015 0.0 9/28/2015 0.0 9/28/2015 0.0 9/28/2015 0.0 9/28/2015 0.0
6/27/2016 0.0 6/27/2016 0.0 6/27/2016 0.0 6/27/2016 0.0 6/27/2016 0.0
6/30/2017 0.0 6/30/2017 0.0 6/30/2017 0.0 6/30/2017 0.0 6/30/2017 0.0
6/30/2018 0.0 6/30/2018 0.0 6/30/2018 0.0 6/30/2018 0.0 6/30/2018 0.0
6/30/2019 0.0 6/30/2019 0.0 6/30/2019 0.0 6/30/2019 0.0 6/30/2019 0.0
4/30/2020 0.0 4/30/2020 0.0 4/30/2020 0.0 4/30/2020 0.0 4/30/2020 0.0
12/31/2020 0.0 12/31/2020 0.0 12/31/2020 0.0 12/31/2020 0.0 12/31/2020 0.0
Total Recovery (ounces)11,657 Total Recovery (ounces)5,086 Total Recovery (ounces)17,362 Total Recovery (ounces)25,648 Total Recovery (ounces)19,296
2009 Recovery (gals)0.1 2009 Recovery (gals)0.0 2009 Recovery (gals)0.4 2009 Recovery (gals)2.0 2009 Recovery (gals)0.1
2010 Recovery (gals)51.4 2010 Recovery (gals)13.6 2010 Recovery (gals)50.1 2010 Recovery (gals)140.8 2010 Recovery (gals)65.6
2011 Recovery (gals)39.5 2011 Recovery (gals)26.0 2011 Recovery (gals)82.5 2011 Recovery (gals)52.5 2011 Recovery (gals)78.0
2012 Recovery (gals)0.0 2012 Recovery (gals)0.0 2012 Recovery (gals)2.5 2012 Recovery (gals)5.0 2012 Recovery (gals)7.0
2013 Recovery (gals)0.1 2013 Recovery (gals)0.1 2013 Recovery (gals)0.1 2013 Recovery (gals)0.0 2013 Recovery (gals)0.0
2014 Recovery (gals)0.0 2014 Recovery (gals)0.0 2014 Recovery (gals)0.0 2014 Recovery (gals)0.1 2014 Recovery (gals)0.0
2015 Recovery (gals)0.0 2015 Recovery (gals)0.0 2015 Recovery (gals)0.0 2015 Recovery (gals)0.0 2015 Recovery (gals)0.0
2016 Recovery (gals)0.0 2016 Recovery (gals)0.0 2016 Recovery (gals)0.0 2016 Recovery (gals)0.0 2016 Recovery (gals)0.0
2017 Recovery (gals)0.0 2017 Recovery (gals)0.0 2017 Recovery (gals)0.0 2017 Recovery (gals)0.0 2017 Recovery (gals)0.0
2018 Recovery (gals)0.0 2018 Recovery (gals)0.0 2018 Recovery (gals)0.0 2018 Recovery (gals)0.0 2018 Recovery (gals)0.0
2019 Recovery (gals)0.0 2019 Recovery (gals)0.0 2019 Recovery (gals)0.0 2019 Recovery (gals)0.0 2019 Recovery (gals)0.0
2020 Recovery (gals)0.0 2020 Recovery (gals)0.0 2020 Recovery (gals)0.0 2020 Recovery (gals)0.0 2020 Recovery (gals)0.0
Total Recovery (gals)91.1 Total Recovery (gals)39.7 Total Recovery (gals)135.6 Total Recovery (gals)200.4 Total Recovery (gals)150.8
Notes:
Volume in ounces unless specified otherwise
Product pumped via manually operated peristaltic pump or vacuum pump with float
Product removal via absorbent socks began on February 17, 2017. Recovery volumes cannot be estimated.
Product removal via absorbent socks discontinued on Decmeber 31, 2020 per DWM approval.
2 of 4
Table 6A 1-5 Trench Recovery of 5293-21A MB Haynes Trench Recovery Table 6A and B.xlsx
Prepared by: BPN
Checked by: AWA
Table 6B
Trench Extraction Pipe (TEP) Product Recovery History -- November 17, 2009 through December 31, 2020
TEP-6 through TEP-10
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J08-5293-08
TEP-6 TEP-7 TEP-8 TEP-9 TEP-10
Date Volume Date Volume Date Volume Date Volume Date Volume
11/17/2009 0.0 11/17/2009 0.0 11/17/2009 8.0 11/17/2009 32.0 11/17/2009 32.0
12/1/2009 3.0 12/1/2009 3.0 12/1/2009 8.0 12/1/2009 48.0 12/1/2009 212.0
12/10/2009 0.0 12/10/2009 0.0 12/10/2009 0.0 12/10/2009 4.0 12/10/2009 144.0
1/14/2010 1/14/2010 1/14/2010 1/14/2010 1/14/2010
1/19/2010 0.0 1/19/2010 0.0 1/19/2010 0.0 1/19/2010 80.0 1/19/2010 16.0
2/8/2010 0.0 2/8/2010 0.0 2/8/2010 0.0 2/8/2010 0.0 2/8/2010 10.0
2/24/2010 0.0 2/24/2010 8.0 2/24/2010 6.0 2/24/2010 8.0 2/24/2010 24.0
3/25/2010 6.0 3/25/2010 6.0 3/25/2010 32.0 3/25/2010 208.0 3/25/2010 256.0
4/21/2010 8.0 4/21/2010 16.0 4/21/2010 12.0 4/21/2010 48.0 4/21/2010 326.0
4/22/2010 4/22/2010 4/22/2010 4/22/2010 4/22/2010
5/7/2010 5/7/2010 5/7/2010 5/7/2010 5/7/2010
5/14/2010 32.0 5/14/2010 32.0 5/14/2010 24.0 5/14/2010 48.0 5/14/2010 32.0
5/28/2010 5/28/2010 5/28/2010 5/28/2010 5/28/2010
6/11/2010 6/11/2010 6/11/2010 6/11/2010 6/11/2010
7/1/2010 7/1/2010 7/1/2010 7/1/2010 7/1/2010
7/22/2010 7/22/2010 7/22/2010 7/22/2010 7/22/2010
7/30/2010 496.0 7/30/2010 336.0 7/30/2010 104.0 7/30/2010 24.0 7/30/2010 48.0
8/25/2010 8/25/2010 8/25/2010 8/25/2010 8/25/2010
8/26/2010 656.0 8/26/2010 8/26/2010 8/26/2010 8/26/2010
9/2/2010 9/2/2010 40.0 9/2/2010 84.0 9/2/2010 24.0 9/2/2010 16.0
9/7/2010 9/7/2010 9/7/2010 9/7/2010 9/7/2010
10/6/2010 960.0 10/6/2010 56.0 10/6/2010 8.0 10/6/2010 40.0 10/6/2010 16.0
10/20/2010 10/20/2010 10/20/2010 10/20/2010 10/20/2010
11/10/2010 896.0 11/10/2010 512.0 11/10/2010 320.0 11/10/2010 0.0 11/10/2010 0.0
11/17/2010 256.0 11/18/2010 64.0 11/18/2010 64.0 11/18/2010 64.0 11/18/2010 0.0
11/23/2010 0.0 11/23/2010 0.0 11/23/2010 0.0 11/23/2010 0.0 11/23/2010 0.0
12/7/2010 0.0 12/7/2010 128.0 12/7/2010 0.0 12/7/2010 0.0 12/7/2010 0.0
12/16/2010 64.0 12/16/2010 0.0 12/16/2010 64.0 12/16/2010 0.0 12/16/2010 0.0
12/29/2010 128.0 12/29/2010 64.0 12/29/2010 64.0 12/29/2010 0.0 12/29/2010 0.0
1/11/2011 128.0 1/11/2011 128.0 1/11/2011 0.0 1/11/2011 0.0 1/11/2011 0.0
1/20/2011 256.0 1/20/2011 0.0 1/20/2011 256.0 1/20/2011 128.0 1/20/2011 128.0
1/26/2011 0.0 1/26/2011 256.0 1/26/2011 0.0 1/26/2011 640.0 1/26/2011 0.0
2/3/2011 896.0 2/3/2011 0.0 2/3/2011 0.0 2/3/2011 0.0 2/3/2011 0.0
2/10/2011 256.0 2/10/2011 0.0 2/10/2011 0.0 2/10/2011 0.0 2/10/2011 0.0
2/16/2011 256.0 2/16/2011 0.0 2/16/2011 0.0 2/16/2011 0.0 2/16/2011 0.0
2/21/2011 256.0 2/21/2011 128.0 2/21/2011 128.0 2/21/2011 128.0 2/21/2011 0.0
2/28/2011 128.0 2/28/2011 128.0 2/28/2011 0.0 2/28/2011 0.0 2/28/2011 0.0
3/8/2011 0.0 3/8/2011 0.0 3/8/2011 128.0 3/8/2011 0.0 3/8/2011 0.0
3/17/2011 0.0 3/17/2011 0.0 3/17/2011 128.0 3/17/2011 128.0 3/17/2011 128.0
3/24/2011 0.0 3/24/2011 0.0 3/24/2011 128.0 3/24/2011 128.0 3/24/2011 128.0
3/31/2011 0.0 3/31/2011 0.0 3/31/2011 128.0 3/31/2011 128.0 3/31/2011 128.0
4/5/2011 0.0 4/5/2011 0.0 4/5/2011 64.0 4/5/2011 0.0 4/5/2011 0.0
4/13/2011 0.0 4/13/2011 0.0 4/13/2011 0.0 4/13/2011 128.0 4/13/2011 128.0
4/19/2011 0.0 4/19/2011 0.0 4/19/2011 0.0 4/19/2011 128.0 4/19/2011 128.0
4/28/2011 0.0 4/28/2011 0.0 4/28/2011 64.0 4/28/2011 0.0 4/28/2011 64.0
5/5/2011 0.0 5/5/2011 0.0 5/5/2011 0.0 5/5/2011 0.0 5/5/2011 64.0
5/11/2011 0.0 5/11/2011 0.0 5/11/2011 0.0 5/11/2011 0.0 5/11/2011 64.0
5/19/2011 0.0 5/19/2011 0.0 5/19/2011 0.0 5/19/2011 0.0 5/19/2011 64.0
5/26/2011 0.0 5/26/2011 0.0 5/26/2011 0.0 5/26/2011 0.0 5/26/2011 64.0
6/2/2011 0.0 6/2/2011 0.0 6/2/2011 0.0 6/2/2011 0.0 6/2/2011 64.0
6/9/2011 0.0 6/9/2011 0.0 6/9/2011 0.0 6/9/2011 128.0 6/9/2011 128.0
6/16/2011 0.0 6/16/2011 0.0 6/16/2011 0.0 6/16/2011 0.0 6/16/2011 0.0
6/23/2011 0.0 6/23/2011 0.0 6/23/2011 0.0 6/23/2011 0.0 6/23/2011 0.0
6/30/2011 0.0 6/30/2011 0.0 6/30/2011 0.0 6/30/2011 0.0 6/30/2011 0.0
7/7/2011 0.0 7/7/2011 0.0 7/7/2011 0.0 7/7/2011 0.0 7/7/2011 0.0
7/14/2011 0.0 7/14/2011 0.0 7/14/2011 0.0 7/14/2011 0.0 7/14/2011 64.0
7/21/2011 0.0 7/21/2011 0.0 7/21/2011 0.0 7/21/2011 0.0 7/21/2011 0.0
7/28/2011 64.0 7/28/2011 0.0 7/28/2011 0.0 7/28/2011 0.0 7/28/2011 0.0
8/4/2011 0.0 8/4/2011 0.0 8/4/2011 0.0 8/4/2011 0.0 8/4/2011 256.0
8/11/2011 0.0 8/11/2011 0.0 8/11/2011 0.0 8/11/2011 0.0 8/11/2011 0.0
8/18/2011 0.0 8/18/2011 0.0 8/18/2011 0.0 8/18/2011 0.0 8/18/2011 0.0
8/25/2011 0.0 8/25/2011 0.0 8/25/2011 0.0 8/25/2011 0.0 8/25/2011 0.0
8/31/2011 64.0 8/31/2011 0.0 8/31/2011 128.0 8/31/2011 0.0 8/31/2011 0.0
9/8/2011 128.0 9/8/2011 0.0 9/8/2011 128.0 9/8/2011 0.0 9/8/2011 128.0
9/16/2011 0.0 9/16/2011 0.0 9/16/2011 128.0 9/16/2011 128.0 9/16/2011 128.0
9/22/2011 256.0 9/22/2011 0.0 9/22/2011 0.0 9/22/2011 128.0 9/22/2011 0.0
9/29/2011 384.0 9/29/2011 0.0 9/29/2011 0.0 9/29/2011 0.0 9/29/2011 0.0
10/6/2011 0.0 10/6/2011 0.0 10/6/2011 0.0 10/6/2011 0.0 10/6/2011 0.0
10/13/2011 128.0 10/13/2011 0.0 10/13/2011 0.0 10/13/2011 0.0 10/13/2011 0.0
10/20/2011 0.0 10/20/2011 0.0 10/20/2011 0.0 10/20/2011 0.0 10/20/2011 0.0
10/27/2011 0.0 10/27/2011 0.0 10/27/2011 0.0 10/27/2011 0.0 10/27/2011 0.0
11/3/2011 256.0 11/3/2011 0.0 11/3/2011 0.0 11/3/2011 0.0 11/3/2011 0.0
11/10/2011 128.0 11/10/2011 0.0 11/10/2011 0.0 11/10/2011 0.0 11/10/2011 0.0
11/17/2011 128.0 11/17/2011 0.0 11/17/2011 0.0 11/17/2011 0.0 11/17/2011 0.0
11/23/2011 128.0 11/23/2011 0.0 11/23/2011 0.0 11/23/2011 0.0 11/23/2011 0.0
12/1/2011 256.0 12/1/2011 0.0 12/1/2011 0.0 12/1/2011 0.0 12/1/2011 512.0
12/8/2011 0.0 12/8/2011 0.0 12/8/2011 0.0 12/8/2011 0.0 12/8/2011 0.0
12/15/2011 0.0 12/15/2011 0.0 12/15/2011 0.0 12/15/2011 0.0 12/15/2011 256.0
12/22/2011 0.0 12/22/2011 0.0 12/22/2011 0.0 12/22/2011 0.0 12/22/2011 0.0
12/28/2011 0.0 12/28/2011 0.0 12/28/2011 0.0 12/28/2011 0.0 12/28/2011 0.0
1/5/2012 0.0 1/5/2012 0.0 1/5/2012 0.0 1/5/2012 0.0 1/5/2012 128.0
1/12/2012 0.0 1/12/2012 0.0 1/12/2012 0.0 1/12/2012 128.0 1/12/2012 384.0
1/19/2012 0.0 1/19/2012 0.0 1/19/2012 0.0 1/19/2012 128.0 1/19/2012 256.0
1/26/2012 0.0 1/26/2012 0.0 1/26/2012 0.0 1/26/2012 0.0 1/26/2012 256.0
2/2/2012 0.0 2/2/2012 0.0 2/2/2012 0.0 2/2/2012 0.0 2/2/2012 256.0
3 of 4
Table 6B 6-10 Trench Recovery of 5293-21A MB Haynes Trench Recovery Table 6A and B.xlsx
Prepared by: BPN
Checked by: AWA
Table 6B
Trench Extraction Pipe (TEP) Product Recovery History -- November 17, 2009 through December 31, 2020
TEP-6 through TEP-10
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J08-5293-08
TEP-6 TEP-7 TEP-8 TEP-9 TEP-10
Date Volume Date Volume Date Volume Date Volume Date Volume
2/9/2012 0.0 2/9/2012 0.0 2/9/2012 0.0 2/9/2012 128.0 2/9/2012 128.0
2/16/2012 0.0 2/16/2012 0.0 2/16/2012 0.0 2/16/2012 0.0 2/16/2012 128.0
2/21/2012 0.0 2/21/2012 0.0 2/21/2012 0.0 2/21/2012 0.0 2/21/2012 128.0
2/29/2012 0.0 2/29/2012 0.0 2/29/2012 0.0 2/29/2012 0.0 2/29/2012 64.0
3/8/2012 0.0 3/8/2012 0.0 3/8/2012 0.0 3/8/2012 0.0 3/8/2012 128.0
3/14/2012 0.0 3/14/2012 0.0 3/14/2012 0.0 3/14/2012 0.0 3/14/2012 128.0
3/22/2012 0.0 3/22/2012 0.0 3/22/2012 0.0 3/22/2012 0.0 3/22/2012 128.0
3/29/2012 0.0 3/29/2012 0.0 3/29/2012 0.0 3/29/2012 0.0 3/29/2012 128.0
4/5/2012 0.0 4/5/2012 0.0 4/5/2012 0.0 4/5/2012 0.0 4/5/2012 128.0
4/11/2012 0.0 4/11/2012 0.0 4/11/2012 0.0 4/11/2012 0.0 4/11/2012 256.0
4/19/2012 0.0 4/19/2012 0.0 4/19/2012 0.0 4/19/2012 0.0 4/19/2012 256.0
4/26/2012 128.0 4/26/2012 0.0 4/26/2012 0.0 4/26/2012 0.0 4/26/2012 128.0
5/3/2012 64.0 5/3/2012 0.0 5/3/2012 0.0 5/3/2012 0.0 5/3/2012 256.0
5/15/2012 0.0 5/15/2012 0.0 5/15/2012 0.0 5/15/2012 0.0 5/15/2012 192.0
5/24/2012 0.0 5/24/2012 0.0 5/24/2012 0.0 5/24/2012 0.0 5/24/2012 192.0
5/31/2012 0.0 5/31/2012 0.0 5/31/2012 0.0 5/31/2012 0.0 5/31/2012 128.0
6/7/2012 0.0 6/7/2012 0.0 6/7/2012 0.0 6/7/2012 0.0 6/7/2012 192.0
6/14/2012 0.0 6/14/2012 0.0 6/14/2012 0.0 6/14/2012 0.0 6/14/2012 128.0
6/20/2012 0.0 6/20/2012 0.0 6/20/2012 0.0 6/20/2012 0.0 6/20/2012 128.0
6/27/2012 0.0 6/27/2012 0.0 6/27/2012 0.0 6/27/2012 0.0 6/27/2012 64.0
7/3/2012 0.0 7/3/2012 0.0 7/3/2012 0.0 7/3/2012 0.0 7/3/2012 64.0
7/11/2012 0.0 7/11/2012 0.0 7/11/2012 0.0 7/11/2012 0.0 7/11/2012 0.0
7/16/2012 0.0 7/16/2012 0.0 7/16/2012 0.0 7/16/2012 0.0 7/16/2012 0.0
7/23/2012 0.0 7/23/2012 0.0 7/23/2012 0.0 7/23/2012 0.0 7/23/2012 0.0
7/30/2012 0.0 7/30/2012 0.0 7/30/2012 0.0 7/30/2012 0.0 7/30/2012 0.0
8/6/2012 0.0 8/6/2012 0.0 8/6/2012 0.0 8/6/2012 0.0 8/6/2012 0.0
8/13/2012 0.0 8/13/2012 0.0 8/13/2012 0.0 8/13/2012 0.0 8/13/2012 0.0
8/20/2012 0.0 8/20/2012 0.0 8/20/2012 0.0 8/20/2012 0.0 8/20/2012 0.0
8/27/2012 0.0 8/27/2012 0.0 8/27/2012 0.0 8/27/2012 0.0 8/27/2012 0.0
9/4/2012 0.0 9/4/2012 0.0 9/4/2012 0.0 9/4/2012 0.0 9/4/2012 0.0
9/18/2012 0.0 9/18/2012 0.0 9/18/2012 0.0 9/18/2012 0.0 9/18/2012 0.0
10/1/2012 0.0 10/1/2012 0.0 10/1/2012 0.0 10/1/2012 0.0 10/1/2012 0.0
10/17/2012 0.0 10/17/2012 0.0 10/17/2012 0.0 10/17/2012 0.0 10/17/2012 0.0
11/7/2012 0.0 11/7/2012 0.0 11/7/2012 0.0 11/7/2012 0.0 11/7/2012 0.0
11/21/2012 0.0 11/21/2012 0.0 11/21/2012 0.0 11/21/2012 0.0 11/21/2012 0.0
12/6/2012 0.0 12/6/2012 0.0 12/6/2012 0.0 12/6/2012 0.0 12/6/2012 0.0
12/20/2012 0.0 12/20/2012 0.0 12/20/2012 0.0 12/20/2012 0.0 12/20/2012 0.0
1/7/2013 0.0 1/7/2013 0.0 1/7/2013 0.0 1/7/2013 0.0 1/7/2013 0.0
12/9/2013 0.0 12/9/2013 0.0 12/9/2013 0.0 12/9/2013 0.0 12/9/2013 0.0
12/16/2013 0.0 12/16/2013 0.0 12/16/2013 0.0 12/16/2013 0.0 12/16/2013 0.0
6/30/2014 0.0 6/30/2014 0.0 6/30/2014 0.0 6/30/2014 0.0 6/30/2014 0.0
10/2/2014 50.0 10/2/2014 50.0 10/2/2014 0.0 10/2/2014 0.0 10/2/2014 0.0
4/23/2015 0.0 4/23/2015 0.0 4/23/2015 0.0 4/23/2015 0.0 4/23/2015 0.0
9/28/2015 0.0 9/28/2015 0.0 9/28/2015 0.0 9/28/2015 0.0 9/28/2015 0.0
6/27/2016 0.0 6/27/2016 0.0 6/27/2016 0.0 6/27/2016 0.0 6/27/2016 0.0
6/30/2017 0.0 6/30/2017 0.0 6/30/2017 0.0 6/30/2017 0.0 6/30/2017 0.0
6/30/2018 0.0 6/30/2018 0.0 6/30/2018 0.0 6/30/2018 0.0 6/30/2018 0.0
6/30/2019 0.0 6/30/2019 0.0 6/30/2019 0.0 6/30/2019 0.0 6/30/2019 0.0
4/30/2020 0.0 4/30/2020 0.0 4/30/2020 0.0 4/30/2020 0.0 4/30/2020 0.0
12/31/2020 0.0 12/31/2020 0.0 12/31/2020 0.0 12/31/2020 0.0 12/31/2020 0.0
Total Recovery (ounces)7,843 Total Recovery (ounces)1,955 Total Recovery (ounces)2,206 Total Recovery (ounces)2,932 Total Recovery (ounces)8,108
2009 Recovery (gals)0.0 2009 Recovery (gals)0.0 2009 Recovery (gals)0.1 2009 Recovery (gals)0.7 2009 Recovery (gals)3.0
2010 Recovery (gals)27.4 2010 Recovery (gals)9.9 2010 Recovery (gals)6.1 2010 Recovery (gals)4.3 2010 Recovery (gals)5.8
2011 Recovery (gals)32.0 2011 Recovery (gals)5.0 2011 Recovery (gals)11.0 2011 Recovery (gals)15.0 2011 Recovery (gals)20.5
2012 Recovery (gals)1.5 2012 Recovery (gals)0.0 2012 Recovery (gals)0.0 2012 Recovery (gals)3.0 2012 Recovery (gals)34.0
2013 Recovery (gals)0.0 2013 Recovery (gals)0.0 2013 Recovery (gals)0.0 2013 Recovery (gals)0.0 2013 Recovery (gals)0.0
2014 Recovery (gals)0.4 2014 Recovery (gals)0.4 2014 Recovery (gals)0.0 2014 Recovery (gals)0.0 2014 Recovery (gals)0.0
2015 Recovery (gals)0.0 2015 Recovery (gals)0.0 2015 Recovery (gals)0.0 2015 Recovery (gals)0.0 2015 Recovery (gals)0.0
2016 Recovery (gals)0.0 2016 Recovery (gals)0.0 2016 Recovery (gals)0.0 2016 Recovery (gals)0.0 2016 Recovery (gals)0.0
2017 Recovery (gals)0.0 2017 Recovery (gals)0.0 2017 Recovery (gals)0.0 2017 Recovery (gals)0.0 2017 Recovery (gals)0.0
2018 Recovery (gals)0.0 2018 Recovery (gals)0.0 2018 Recovery (gals)0.0 2018 Recovery (gals)0.0 2018 Recovery (gals)0.0
2019 Recovery (gals)0.0 2019 Recovery (gals)0.0 2019 Recovery (gals)0.0 2019 Recovery (gals)0.0 2019 Recovery (gals)0.0
2020 Recovery (gals)0.0 2020 Recovery (gals)0.0 2020 Recovery (gals)0.0 2020 Recovery (gals)0.0 2020 Recovery (gals)0.0
Total Recovery (gals)61.3 Total Recovery (gals)15.3 Total Recovery (gals)17.2 Total Recovery (gals)22.9 Total Recovery (gals)63.3
Notes:
Volume in ounces unless specified otherwise
Product pumped via manually operated peristaltic pump or vacuum pump with float
Product removal via absorbent socks began on February 17, 2017. Recovery volumes cannot be estimated.
Product removal via absorbent socks discontinued on Decmeber 31, 2020 per DWM approval.
4 of 4
Table 6B 6-10 Trench Recovery of 5293-21A MB Haynes Trench Recovery Table 6A and B.xlsx
Prepared by: BPN
Checked by: AWA
Table 7
Air Emissions and Gasoline Recovery Data
Operational Year 7/1/2008 to 6/30/2009
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
8/29/2008 2.4 1,130 4 98 30.0 650 0 91.02 666 2,665 4 1,329.93 8.30E-05 0.45 0.52 0.0 0.073 0.0
9/2/2008 2.7 1,130 4 98 30.0 890 4 91.02 912 3,650 4 1,820.98 1.14E-04 0.62 0.72 70.2 0.099 9.7
9/5/2008 2.8 1,130 4 98 30.0 1,000 7 91.02 1,025 4,101 4 2,046.05 1.28E-04 0.70 0.81 59.5 0.112 8.2
11/4/2008 2.8 1,130 4 98 30.0 1,700 67 91.02 1,743 6,971 4 3,478.28 2.17E-04 1.19 1.37 1,971.9 0.190 272.6
12/3/2008 2.8 1,130 4 98 30.0 1,700 96 91.02 1,743 6,971 4 3,478.28 2.17E-04 1.19 1.37 959.7 0.190 132.7
1/5/2009 2.9 1,130 4 112 30.0 1,970 129 88.79 2,020 8,078 4 4,030.71 2.52E-04 1.34 1.55 1,224.1 0.214 169.2
2/9/2009 3.4 1,216 4 112 24.3 1,850 164 95.58 1,897 7,586 4 3,785.18 2.36E-04 1.36 1.57 1,322.1 0.217 182.8
3/5/2009 3.4 1,014 4 112 29.7 2,550 188 79.68 2,614 10,457 4 5,217.42 3.26E-04 1.56 1.80 1,033.1 0.249 142.8
4/13/2009 3.2 1,364 4 112 32.0 1,865 227 107.21 1,912 7,648 4 3,815.87 2.38E-04 1.53 1.77 1,659.0 0.245 229.4
5/5/2009 3.1 1,332 4 118 26.2 1,275 249 103.60 1,307 5,228 4 2,608.71 1.63E-04 1.01 1.17 617.7 0.162 85.4
6/1/2009 3.2 1,345 4 130 29.7 1,400 276 102.46 1,435 5,741 4 2,864.46 1.79E-04 1.10 1.27 826.7 0.176 114.3
6/30/2009 3.2 1,345 4 130 29.7 1,400 306 102.46 1,435 5,741 4 2,864.46 1.79E-04 1.10 1.27 902.4 0.176 124.8
Bws 0.025 Bwsw 0.0148
9,199
1,472
NOTES:
SVE system was started on August 29, 2008.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: TJB/AWA
Checked By: TZS
Table 8
Air Emissions and Gasoline Recovery Data
Operational Year 7/1/2009 to 6/30/2010
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
7/1/2009 3.2 1,308 4 125 28.5 1,180 0 100.47 1,210 4,839 4 2,414.33 1.51E-04 0.91 1.05 0.0 0.145 0.0
7/2/2009 3.2 1,308 4 125 28.5 1,180 1 100.47 1,210 4,839 4 2,414.33 1.51E-04 0.91 1.05 34.7 0.145 4.8
8/7/2009 3.2 1,521 4 130 20.0 1,050 37 115.87 1,076 4,306 4 2,148.35 1.34E-04 0.93 1.08 934.6 0.149 129.2
9/3/2009 3.2 1,420 4 127 13.5 820 64 108.73 841 3,362 4 1,677.76 1.05E-04 0.68 0.79 511.6 0.109 70.7
10/6/2009 3.4 1,189 4 124 26.0 920 97 91.53 943 3,773 4 1,882.36 1.18E-04 0.65 0.75 591.6 0.103 81.8
11/9/2009 3.4 1,013 4 118 26.5 1,005 132 78.80 1,030 4,121 4 2,056.28 1.28E-04 0.61 0.70 576.0 0.097 79.6
12/1/2009 3.5 1,111 4 108 26.2 1,075 153 87.91 1,102 4,408 4 2,199.50 1.37E-04 0.72 0.84 430.9 0.116 59.6
1/20/2010 3.4 1,033 4 110 22.7 935 203 81.46 959 3,834 4 1,913.05 1.19E-04 0.58 0.68 810.6 0.093 112.1
2/4/2010 3.5 1,052 4 108 22.5 1,100 218 83.25 1,128 4,511 4 2,250.65 1.41E-04 0.70 0.81 292.4 0.112 40.4
3/6/2010 3.5 1,404 4 106 23.5 800 248 111.49 820 3,280 4 1,636.84 1.02E-04 0.68 0.79 569.6 0.109 78.7
4/5/2010 3.2 1,428 4 130 30.0 615 278 108.79 630 2,522 4 1,258.32 7.86E-05 0.51 0.59 427.3 0.082 59.1
5/10/2010 3.3 1,267 4 118 33.0 506 313 98.52 519 2,075 4 1,035.30 6.46E-05 0.38 0.44 371.4 0.061 51.4
6/9/2010 3.3 1,033 4 130 29.4 466 343 78.69 478 1,911 4 953.46 5.95E-05 0.28 0.33 234.2 0.045 32.4
6/30/2010 3.3 1,033 4 130 29.4 466 364 78.69 478 1,911 4 953.46 5.95E-05 0.28 0.33 163.9 0.045 22.7
Bws 0.025 Bwsw 0.0148
5,140
822
NOTES:
SVE system was started on August 29, 2008.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Prepared By: TJB/AWA
Checked By: TZS
Table 9
Air Emissions and Gasoline Recovery Data
Operational Year 7/1/2010 to 6/30/2011
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
7/1/2010 3.2 1,111 4 130 18.4 440 0 84.64 451 1,804 4 900.26 5.62E-05 0.29 0.33 0.0 0.046 0.0
8/2/2010 3.2 1,052 4 125 21.3 511 32 80.83 524 2,095 4 1,045.53 6.53E-05 0.32 0.37 285.4 0.051 39.5
9/7/2010 3.2 1,092 4 135 16.9 465 68 82.49 477 1,907 4 951.41 5.94E-05 0.29 0.34 293.6 0.047 40.6
10/4/2010 3.4 1,326 4 115 28.7 500 95 103.65 513 2,050 4 1,023.02 6.39E-05 0.40 0.46 293.3 0.064 40.5
11/8/2010 3.5 1,033 4 112 26.2 588 131 81.17 603 2,411 4 1,203.07 7.51E-05 0.37 0.42 361.5 0.059 50.0
12/21/2010 3.4 1,033 4 100 27.3 592 173 82.91 607 2,428 4 1,211.26 7.56E-05 0.38 0.44 443.2 0.060 61.3
1/14/2011 3.4 1,111 4 102 24.6 430 197 88.85 441 1,763 4 879.80 5.49E-05 0.29 0.34 195.2 0.047 27.0
2/16/2011 3.4 1,267 4 110 23.5 430 230 99.91 441 1,763 4 879.80 5.49E-05 0.33 0.38 301.8 0.053 41.7
3/8/2011 3.4 1,072 4 106 27.1 445 250 85.13 456 1,825 4 910.49 5.68E-05 0.29 0.34 161.3 0.046 22.3
4/13/2011 3.2 1,111 4 130 23.5 350 286 84.64 359 1,435 4 716.12 4.47E-05 0.23 0.26 227.0 0.036 31.4
5/13/2011 3.2 1,072 4 125 19.4 351 316 82.36 360 1,439 4 718.16 4.48E-05 0.22 0.26 184.6 0.035 25.5
6/6/2011 3.2 1,052 4 125 16.3 320 340 80.83 328 1,312 4 654.73 4.09E-05 0.20 0.23 132.1 0.032 18.3
6/30/2011 3.2 1,052 4 125 16.3 320 364 80.83 328 1,312 4 654.73 4.09E-05 0.20 0.23 132.1 0.032 18.3
Bws 0.025 Bwsw 0.0148
2,602
416
NOTES:
SVE system was started on August 29, 2008.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB
Table 10
Air Emissions and Gasoline Recovery Data
Operational Year 7/1/2011 to 6/30/2012
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
7/1/2011 3.2 1,072 4 125 19.2 275 0 82.36 282 1,128 4 562.66 3.51E-05 0.17 0.20 0.0 0.028 0.0
7/5/2011 3.2 1,072 4 125 19.2 275 4 82.36 282 1,128 4 562.66 3.51E-05 0.17 0.20 21.5 0.028 3.0
8/8/2011 3.2 1,067 4 125 16.7 250 38 81.98 256 1,025 4 511.51 3.19E-05 0.16 0.18 167.8 0.025 23.2
9/7/2011 3.2 1,267 4 125 23.2 345 68 97.35 354 1,415 4 705.89 4.41E-05 0.26 0.30 214.2 0.041 29.6
10/5/2011 3.2 1,247 4 125 20.8 295 96 95.81 302 1,210 4 603.58 3.77E-05 0.22 0.25 166.0 0.035 22.9
11/3/2011 3.2 1,189 4 125 26.1 320 126 91.35 328 1,312 4 654.73 4.09E-05 0.22 0.26 184.1 0.036 25.5
12/8/2011 3.4 1,140 4 121 26.5 365 160 88.19 374 1,497 4 746.81 4.66E-05 0.25 0.29 235.8 0.039 32.6
1/4/2012 3.4 1,130 4 122 25.9 350 187 87.27 359 1,435 4 716.12 4.47E-05 0.23 0.27 175.5 0.037 24.3
2/9/2012 3.4 1,140 4 121 24.2 362 223 88.19 371 1,484 4 740.67 4.62E-05 0.24 0.28 244.7 0.039 33.8
3/6/2012 3.4 1,072 4 121 25.4 282 249 82.93 289 1,156 4 576.98 3.60E-05 0.18 0.21 129.4 0.029 17.9
4/17/2012 3.2 1,052 4 125 19.2 228 291 80.83 234 935 4 466.50 2.91E-05 0.14 0.16 164.8 0.023 22.8
5/8/2012 3.2 1,150 4 125 22.3 254 312 88.36 260 1,042 4 519.70 3.24E-05 0.17 0.20 100.3 0.028 13.9
6/11/2012 3.2 1,120 4 125 20.2 221 346 86.05 227 906 4 452.18 2.82E-05 0.15 0.17 137.6 0.023 19.0
6/30/2012 3.2 1,120 4 125 20.2 221 365 86.05 227 906 4 452.18 2.82E-05 0.15 0.17 76.9 0.023 10.6
Bws 0.025 Bwsw 0.0148
1,744
279
NOTES:
SVE system was started on August 29, 2008.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB
Table 11
Air Emissions and Gasoline Recovery Data
Operational Year 7/2/2012 to 6/28/2013
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
7/2/2012 3.2 1,112 4 120 28.0 1,200 0 86.17 1,230 4,921 4 2,455.36 1.53E-04 0.79 0.92 0.0 0.127 0.0
7/3/2012 3.2 1,072 4 125 26.2 1,405 1 82.36 1,440 5,762 4 2,874.82 1.79E-04 0.89 1.03 25.7 0.142 3.5
7/5/2012 2.9 1,243 4 125 26.5 1,530 3 95.50 1,569 6,274 4 3,130.59 1.95E-04 1.12 1.30 56.6 0.179 7.8
7/9/2012 2.9 1,072 4 125 24.8 1,209 7 82.36 1,239 4,958 4 2,473.78 1.54E-04 0.76 0.88 90.4 0.122 12.5
8/1/2012 2.5 1,170 4 125 36.5 640 30 89.89 656 2,625 4 1,309.53 8.18E-05 0.44 0.51 280.7 0.071 38.8
9/10/2012 3.4 1,170 4 125 24.1 845 70 89.89 866 3,465 4 1,728.98 1.08E-04 0.58 0.67 648.8 0.093 89.7
10/10/2012 2.5 1,232 4 103 31.5 384 100 98.35 394 1,575 4 785.72 4.91E-05 0.29 0.33 241.4 0.046 33.4
11/6/2012 2.5 1,286 4 84 28.8 390 127 106.25 400 1,599 4 797.99 4.98E-05 0.32 0.37 238.0 0.051 32.9
1/2/2013 2.5 1,200 4 90 21.5 266 184 98.06 273 1,091 4 544.27 3.40E-05 0.20 0.23 315.3 0.032 43.6
2/11/2013 2.5 1,072 4 96 26.4 64 224 86.66 66 263 4 131.16 8.19E-06 0.04 0.05 47.3 0.007 6.5
3/14/2013 2.5 1,130 4 88 14.6 70 255 92.68 72 288 4 143.64 8.97E-06 0.05 0.06 42.8 0.008 5.9
4/17/2013 2.5 1,130 4 92 30.5 63 289 92.01 65 260 4 129.52 8.09E-06 0.04 0.05 42.2 0.007 5.8
5/16/2013 1.6 1,170 4 103 23.1 42 318 93.40 43 173 4 86.14 5.38E-06 0.03 0.03 24.5 0.005 3.4
6/28/2013 1.5 1,130 4 100 34.9 78 361 90.69 79 318 4 158.58 9.90E-06 0.05 0.06 63.9 0.009 8.8
Bws 0.025 Bwsw 0.0148
1,830
293
NOTES:
SVE system was started on July 2, 2012.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: TEP-3, MW-28, and MW-35
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Prepared By: AWA
Checked By: TJB/PJVH
Table 12
Air Emissions and Gasoline Recovery Data
Operational Year 6/28/2013 to 6/30/2014
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
6/28/2013 2.9 1,130 4 100 34.9 566 0 92.14 571 2,284 4 1,139.85 7.12E-05 0.39 0.46 0.0 0.063 0.0
7/1/2013 2.8 1,033 4 118 22.4 404 3 81.61 408 1,631 4 813.60 5.08E-05 0.25 0.29 20.7 0.040 2.9
7/3/2013 2.8 1,052 4 118 27.5 312 5 83.11 315 1,259 4 628.33 3.92E-05 0.20 0.23 10.9 0.031 1.5
7/5/2013 2.8 1,073 4 115 28.2 352 7 85.21 355 1,421 4 708.88 4.43E-05 0.23 0.26 12.4 0.036 1.7
7/10/2013 2.8 1,033 4 122 24.6 328 12 81.05 331 1,324 4 660.55 4.12E-05 0.20 0.23 27.9 0.032 3.9
7/12/2013 2.8 1,032 4 119 23.3 309 14 81.39 312 1,247 4 622.29 3.88E-05 0.19 0.22 10.4 0.030 1.4
8/15/2013 2.8 1,130 4 120 23.4 202 48 88.97 204 815 4 406.80 2.54E-05 0.14 0.16 129.2 0.022 17.9
9/16/2013 2.8 1,286 4 125 21.4 211 80 100.38 213 852 4 424.93 2.65E-05 0.16 0.18 141.6 0.026 19.6
10/14/2013 2.8 1,033 4 122 26.1 225 108 81.05 227 908 4 453.12 2.83E-05 0.14 0.16 107.0 0.022 14.8
11/13/2013 2.9 1,032 4 105 25.8 301 138 83.41 304 1,215 4 606.18 3.78E-05 0.19 0.22 158.1 0.030 21.9
12/20/2013 2.8 1,070 4 120 22.0 216 175 84.24 218 872 4 435.00 2.72E-05 0.14 0.16 140.7 0.022 19.5
1/15/2014 2.8 1,032 4 102 29.5 412 201 83.85 416 1,663 4 829.72 5.18E-05 0.26 0.30 188.4 0.042 26.0
3/3/2014 2.8 1,033 4 102 28.4 324 248 83.93 327 1,308 4 652.50 4.07E-05 0.21 0.24 268.6 0.033 37.1
4/10/2014 2.8 1,170 4 99 33.4 178 286 95.58 180 718 4 358.47 2.24E-05 0.13 0.15 134.4 0.021 18.6
5/14/2014 2.8 1,111 4 124 20.9 216 320 86.87 218 872 4 435.00 2.72E-05 0.14 0.16 134.6 0.023 18.6
6/20/2014 2.6 954 4 125 19.5 201 357 74.47 203 811 4 404.79 2.53E-05 0.11 0.13 116.0 0.018 16.0
6/30/2014 2.6 954 4 125 19.5 201 368 74.47 203 811 4 404.79 2.53E-05 0.11 0.13 32.6 0.018 4.5
Bws 0.009 Bwsw 0.0054
1,411
226
NOTES:
SVE system was started on June 28, 2013.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB/PJVH
Table 13
Air Emissions and Gasoline Recovery Data
Operational Year 6/30/2014 to 6/30/2015
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
6/30/2014 2.6 954 4 125 19.5 201 0 74.43 203 812 4 405.01 2.53E-05 0.11 0.13 0.0 0.018 0.0
7/24/2014 2.8 1,150 4 125 20.9 195 24 89.72 197 787 4 392.92 2.45E-05 0.13 0.15 88.7 0.021 12.3
8/29/2014 2.8 1,130 4 125 20.4 224 60 88.16 226 905 4 451.35 2.82E-05 0.15 0.17 149.3 0.024 20.6
9/25/2014 2.8 1,111 4 125 25.3 250 87 86.68 252 1,010 4 503.74 3.14E-05 0.16 0.19 122.7 0.026 17.0
10/24/2014 2.8 1,013 4 120 28.8 175 116 79.71 177 707 4 352.62 2.20E-05 0.11 0.12 84.4 0.017 11.7
11/20/2014 2.4 1,206 4 120 26.5 99 143 94.90 100 401 4 199.88 1.25E-05 0.07 0.08 53.4 0.011 7.4
12/23/2014 2.4 1,033 4 112 31.1 82 176 82.42 83 331 4 165.23 1.03E-05 0.05 0.06 46.5 0.008 6.4
1/30/2015 2.4 1,033 4 88 29.1 86 214 86.03 87 347 4 173.29 1.08E-05 0.06 0.06 59.1 0.009 8.2
2/27/2015 2.4 1,209 4 88 22.9 92 242 100.69 93 373 4 185.98 1.16E-05 0.07 0.08 54.4 0.011 7.5
3/27/2015 2.4 1,033 4 92 37.4 76 270 85.41 76 305 4 152.33 9.51E-06 0.05 0.06 38.1 0.008 5.3
4/23/2015 2.4 1,111 4 115 29.8 165 297 88.18 167 666 4 332.47 2.08E-05 0.11 0.13 82.6 0.018 11.4
5/29/2015 2.4 1,033 4 115 30.5 120 333 81.99 121 485 4 241.80 1.51E-05 0.07 0.09 73.7 0.012 10.2
6/30/2015 2.4 1,033 4 112 27.0 75 365 82.42 75 301 4 150.32 9.38E-06 0.05 0.05 41.3 0.007 5.7
Bws 0.009 Bwsw 0.0057
773
124
NOTES:
SVE system was started on June 28, 2013.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume SVE system connected to SVE-1 through SVE-4 and MW-35 starting November 2014.
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4 (and MW-35 starting November 2014)
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB
Table 14
Air Emissions and Gasoline Recovery Data
Operational Year 6/30/2015 to 6/30/2016
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
6/30/2015 1.3 1,052 4 110 25.7 3 0 84.25 3 14 4 6.85 4.28E-07 0.00 0.00 0.0 0.000 0.0
7/21/2015 1.5 1,092 4 98 34.0 0 21 89.34 0 0 4 0.00 0.00E+00 0.00 0.00 0.0 0.000 0.0
8/7/2015 1.5 1,033 4 102 38.4 0 38 83.91 0 0 4 0.00 0.00E+00 0.00 0.00 0.0 0.000 0.0
9/28/2015 2.5 1,052 4 100 31.2 100 90 85.79 101 404 4 201.45 1.26E-05 0.06 0.07 93.6 0.010 12.9
10/29/2015 2.5 984 4 101 36.4 97 121 80.07 98 393 4 196.01 1.22E-05 0.06 0.07 50.6 0.009 7.0
11/30/2015 2.1 1,032 4 102 27.4 90 153 83.83 90 362 4 180.50 1.13E-05 0.06 0.07 50.3 0.009 7.0
12/30/2015 2.2 1,013 4 105 32.5 79 183 81.85 80 320 4 159.55 9.96E-06 0.05 0.06 41.1 0.008 5.7
1/29/2016 2.4 1,022 4 99 28.4 123 213 83.46 124 498 4 248.38 1.55E-05 0.08 0.09 64.1 0.012 8.9
3/31/2016 2.1 1,033 4 115 20.1 108 275 82.01 109 436 4 217.56 1.36E-05 0.07 0.08 115.6 0.011 16.0
4/29/2016 2.1 892 4 118 17.4 98 304 70.45 99 397 4 198.22 1.24E-05 0.05 0.06 42.1 0.008 5.8
5/31/2016 2.1 1,032 4 125 24.2 78 336 80.53 79 317 4 157.93 9.86E-06 0.05 0.06 42.2 0.008 5.8
6/27/2016 2.1 1,052 4 125 27.1 85 363 82.09 85 342 4 170.62 1.07E-05 0.05 0.06 39.6 0.008 5.5
6/30/2016 2.1 1,052 4 125 26.1 72 366 82.09 73 292 4 145.85 9.11E-06 0.04 0.05 3.4 0.007 0.5
Bws 0.009 Bwsw 0.0056
469
75
NOTES:
SVE system was started on June 28, 2013.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: MW-35 (June 30, 2015 to August 7, 2015) & SVE-1 through SVE-4 (August 7, 2015 to June 30, 2016)
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB
Table 15
Air Emissions and Gasoline Recovery Data
Operational Year 6/30/2016 to 6/30/2017
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
6/30/2016 2.1 1,052 4 125 26.1 72 0 82.19 73 292 4 145.68 9.09E-06 0.04 0.05 0.0 0.007 0.0
7/29/2016 2.1 1,033 4 125 28.4 87 29 80.70 87 349 4 174.25 1.09E-05 0.05 0.06 42.6 0.008 5.9
8/31/2016 2.1 1,755 4 125 18.8 83 62 137.11 84 336 4 167.81 1.05E-05 0.09 0.10 79.1 0.014 10.9
9/30/2016 2.1 1,618 4 112 26.3 100 92 129.28 101 405 4 202.02 1.26E-05 0.10 0.11 81.2 0.016 11.2
10/31/2016 2.1 1,735 4 122 18.2 81 123 136.25 82 327 4 163.19 1.02E-05 0.08 0.10 72.0 0.013 10.0
12/30/2016 1.9 1,833 4 88 31.5 76 183 152.87 77 306 4 152.92 9.55E-06 0.09 0.10 146.0 0.014 20.2
6/30/2017 1.0 1,735 4 93 34.8 32 365 143.39 33 131 4 65.19 4.07E-06 0.04 0.04 177.0 0.006 24.5
Bws 0.008 Bwsw 0.0049
517
83
NOTES:
SVE system was started on June 28, 2013.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB
Table 16
Air Emissions and Gasoline Recovery Data
Operational Year 6/30/2017 to 6/30/2018
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
6/30/2017 1.0 1,735 4 93 34.8 32 0 143.03 33 131 4 65.36 4.08E-06 0.04 0.04 0.0 0.006 0.0
10/6/2017 1.8 1,501 4 115 26.1 60 98 119.00 61 243 4 121.44 7.58E-06 0.05 0.06 147.5 0.009 20.4
12/29/2017 1.8 1,592 4 89 32.1 62 182 132.19 63 251 4 125.47 7.83E-06 0.06 0.07 144.9 0.010 20.0
3/30/2018 2.4 1,477 4 92 28.7 60 273 121.98 61 242 4 120.84 7.54E-06 0.06 0.06 139.7 0.009 19.3
6/30/2018 1.9 1,541 4 110 21.5 56 365 123.25 57 228 4 113.77 7.10E-06 0.05 0.06 134.2 0.008 18.6
Bws 0.011 Bwsw 0.0064
489
78
NOTES:
SVE system was started on June 28, 2013.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB
Table 17
Air Emissions and Gasoline Recovery Data
Operational Year 6/30/2018 to 6/30/2019
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
6/30/2018 1.9 1,541 4 110 21.5 56 0 123.56 57 227 4 113.48 7.08E-06 0.05 0.06 0.0 0.008 0.0
9/28/2018 2.1 1,443 4 125 26.5 66 90 112.74 66 265 4 132.00 8.24E-06 0.06 0.06 139.6 0.009 19.3
12/27/2018 1.9 1,562 4 94 26.7 92 180 128.86 93 371 4 185.32 1.16E-05 0.09 0.10 223.6 0.014 30.9
3/29/2019 1.8 1,501 4 99 23.6 68 272 122.70 69 276 4 137.63 8.59E-06 0.06 0.07 161.6 0.010 22.3
6/30/2019 1.9 1,364 4 118 26.1 69 365 107.85 70 279 4 139.44 8.71E-06 0.06 0.07 145.4 0.009 20.1
Bws 0.008 Bwsw 0.0049
579
93
NOTES:
SVE system was started on June 28, 2013.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB
Table 18
Air Emissions and Gasoline Recovery Data
Operational Year 6/30/2019 to 6/30/2020
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
6/30/2019 1.9 1,364 4 118 26.1 69 0 107.58 70 280 4 139.80 8.73E-06 0.06 0.07 0.0 0.009 0.0
9/30/2019 1.8 1,326 4 122 27.3 51 92 103.86 51 205 4 102.48 6.40E-06 0.04 0.05 101.9 0.006 14.1
12/31/2019 1.5 1,404 4 89 38.4 50 184 116.58 50 202 4 100.67 6.28E-06 0.04 0.05 112.3 0.007 15.5
3/30/2020 1.6 1,345 4 105 28.3 42 274 108.52 43 171 4 85.13 5.31E-06 0.03 0.04 86.7 0.006 12.0
6/30/2020 1.6 1,306 4 101 31.1 52 366 106.12 53 211 4 105.10 6.56E-06 0.04 0.05 106.5 0.007 14.7
Bws 0.011 Bwsw 0.0064
352
56
NOTES:
SVE system was started on June 28, 2013.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB
Table 19
Air Emissions and Gasoline Recovery Data
Operational Year 6/30/2020 to 12/31/2020
Soil Vapor Extraction System
MB Haynes
Asheville, North Carolina
BLE Job Number J08-5293-08
Vacuum Velocity Pipe D Temp Rel. Humidity PPMmeasured Qstd PPMd PPMc K Ccm Cc PMRc PMRg PMRg
(in. Hg)(ft/min)(in)(F)(%)(ppm)(DSCFM)(mg/dsm3)(lb/dscf)(lb/hr)(lb/hr)(gal/hr)
6/30/2020 1.6 1,306 4 101 31.1 52 0 105.66 53 212 4 105.56 6.59E-06 0.04 0.05 0.0 0.007 0.0
10/30/2020 1.8 1,328 4 90 38.0 52 122 109.59 53 212 4 105.56 6.59E-06 0.04 0.05 146.7 0.007 20.3
12/31/2020 1.2 1,224 4 86 57.4 28 184 101.75 29 115 4 57.14 3.57E-06 0.02 0.03 37.6 0.003 5.2
Bws 0.015 Bwsw 0.009
159
25
NOTES:
SVE system was started on June 28, 2013.PPMc - volumetric concentration of VOC emissions as carbon, dry basis, at STP
Vapor concentrations were measured using a portable MiniRAE® 2000 Photo-Ionization Detector (PID).K - number of carbons in calibration gas
inches of Hg - inches of mercury Ccm - mass concentration of VOC emissions as carbon
ppm - parts per million Cc - mass concentration of VOC emmisions as carbon, dry basis, at STP
Qstd - flow at DSCFM STP - standard temperature and pressure
DSCFM - Dry Standard Cubic Feet per Minute PMRc - pollutant mass removal of VOCs as carbon
PPMd - "dry" concentration PMRg - pollutant mass removal of VOCs as gasoline
Bwsw - lb of water per lb of dry air
Bws - water vapor % by volume
Calculations based on formulas published in North Carolina Department of Natural Resources, Division of Waste Management, Underground Storage Tank Section, Guidelines for Assessment and Corrective Action, Appendix B, July 21, 2001.
Cumulative Total Pounds of Gasoline Recovered as Emissions:
Cumulative Total Gallons of Gasoline Recovered as Emissions:
EXTRACTION WELLS: SVE-1 through SVE-4
SVE FIELD MEASUREMENTS EMISSION CALCULATIONS
Date
Elapsed
Days
Total Pounds
of Gasoline
Recovered
Total Gallons
of Gasoline
Recovered
Prepared By: AWA
Checked By: TJB
0.000
0.050
0.100
0.150
0.200
0.250
0.300
0
500
1,000
1,500
2,000
2,500
3,000
Ga
s
o
l
i
n
e

R
e
c
o
v
e
r
y

(
g
a
l
/
h
r
)
Va
p
o
r

C
o
n
c
e
n
t
r
a
t
i
o
n

(
p
p
m
)

Air Emissions and Gasoline Recovery Data (SVE-1 to SVE-4 & MW-35 for short periods)
Four Operational Periods 7/1/2008 to 6/30/2012 and 7.5 Operational Periods 6/28/13 to 12/30/20
Soil Vapor Extraction System --MB Haynes Asheville, North Carolina
(ppm)
(gal/hr)
Year One:
1,472 gallons
gasoline
recovered
Year Two:
822 gallons
gasoline
recovered
Year Three:
416 gallons
gasoline
recovered
Year Four:
279 gallons
gasoline
recovered
Year Five:
System Plumbed
to Trench
293 gallons recovered
Year Six:
226 gallons
gasoline
recovered
Year Seven:
124 gallons
gasoline
recovered
Year Eight:
75 gallons
gasoline
recovered
Year Nine:
83 gallons
gasoline
recovered
Year Ten:
78 gallons
gasoline
recovered
Year Eleven:
93 gallons
gasoline
recovered
Year Twelve:
56 gallons
gasoline
recovered
Year Thirteen:
25 gallons
gasoline
recovered
(6 months)
0.000
0.050
0.100
0.150
0.200
0.250
0.300
0
500
1,000
1,500
2,000
2,500
3,000
3/30/2012 6/29/2012 9/28/2012 12/28/2012 3/30/2013 6/29/2013 9/28/2013
Ga
s
o
l
i
n
e

R
e
c
o
v
e
r
y

(
g
a
l
/
h
r
)
Va
p
o
r

C
o
n
c
e
n
t
r
a
t
i
o
n

(
p
p
m
)

Air Emissions and Gasoline Recovery Data (TP-3, MW-28, & MW-35)
One Operational Period 7/2/2012 to 6/28/2013
Soil Vapor Extraction System --MB Haynes Asheville, North Carolina
BLE Job Number J08-5293-08
(ppm)
(gal/hr)
Year One (12 Months):
293 gallons gasoline recovered
Switch from TEP-5 to TEP-3

Figures

SITE
1
SMI
T
H
MILL
CRE
E
K
TRIBU
T
A
R
Y
SANITARY SEWER MANHOLE
(TYPICAL)
SANITARY SEWER CLEANOUT
(TYPICAL)
APPROXIMATE LOCATION OF
SANITARY SEWER LINES
SEWER LINE
PROPERTY LINES
PR
O
P
E
R
T
Y

L
I
N
E
S
PR
O
P
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R
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Y

L
I
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PROPERTY L
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PROP
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T
Y

L
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S
PR
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P
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R
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Y

L
I
N
E
S
HAYNES
100 50 100 200
CORP.TEMPORARY
INTERCEPTOR
TRENCH
FORMER
SANITARY
(FLO
W

)
SMIT
H
MIL
L
CRE
E
K
TRIB
U
T
A
R
Y
(FL
O
W

)
SANITARY SEWER MANHOLE
(TYPICAL)
SANITARY SEWER CLEANOUT
(TYPICAL)
APPROXIMATE LOCATION OF
SANITARY SEWER LINES
SANITARY SEWER LINE
PROPERTY LINES
PR
O
P
E
R
T
Y

L
I
N
E
S
PR
O
P
E
R
T
Y

L
I
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E
S
PROPERT
Y

L
I
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S
PROP
E
R
T
Y

L
I
N
E
S
PR
O
P
E
R
T
Y

L
I
N
E
S
HAYNES CORP.
FORMER TEMPORARY INTERCEPTOR TRENCH
SMI
T
H
MILL
CRE
E
K
TRIBU
T
A
R
Y
(FLO
W

)
SMIT
H
MIL
L
CRE
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TRIB
U
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A
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Y
(FL
O
W

)
4

APPENDIX A
Groundwater Sampling Procedures and
Sampling Logs

APPENDIX A

Monitoring Well Purging and Sampling Procedures
The monitoring wells were purged prior to sample collection to remove stagnant water from the wells so that the samples collected would be representative of the groundwater quality in the vicinity of each well.
For wells that recovered quickly, a minimum of three volumes of water were purged. Specific conductance, pH, and water temperature were measured periodically during well evacuation using daily calibrated instruments. Wells that were purged to dryness with less than three well volumes being removed were
sampled as soon as they had recovered enough to yield sufficient volume for a sample. The monitoring wells were sampled using disposable bailers constructed of a 3-foot long, 1.6-inch diameter bailer attached to unused polypropylene cord. A smaller bailer may be used for wells with restricted access.
The samples were placed in glass containers with Teflon-lined lids. Samples were maintained at <4°C until
analysis at the laboratory. Appropriate chain-of-custody records were maintained.
BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2207.46
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):Flushmount
Well ID #:MW-26 Land Surface Elevation (ft msl):2207.62
Downgradient:No Screened Interval (ft bgs):41.0 - 51.0
Upgradient:Yes Dedicated Pump or Bailer:no
Weather Conditions:Steel Guard Pipe Around Casing:no
Air Temperature:Locking Cap:yes
Total Well Depth in feet (TWD) =50.91 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =29.71 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =21.20 Well Yield (subjective):high
1 Casing Volume in gallons (CV) = LWC x 0.17 = 3.60 Sample Date and Time:9/27/22 @ 8:40AM
Standard Evacuation Volume (3 casing volumes) =10.81
Method of Well Evacuation:Disp. Bailer Remarks:
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):11.0
FIELD ANALYSIS
Volume Purged (gallons)-3.6 7.2 11.0
Time (military)0818 0825 0833 0840
pH (S.U.)5.58 5.93 6.04 6.66
Sp. Cond. (umhos/cm)51.63 55.42 57.21 58.19
Water Temp. (°C)16.0 16.1 16.3 16.1
Turbidity (subjective)*5.4 NTU 15.8 NTU 23.9 NTU 25.0 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 2.3 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2112.81
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):3.20
Well ID #:MW-27 Land Surface Elevation (ft msl):2109.61
Downgradient:Yes Screened Interval (ft bgs):2.5 - 6.5
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:Sunny Steel Guard Pipe Around Casing:no
Air Temperature:67 F Locking Cap:yes
Total Well Depth in feet (TWD) =9.30 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =6.64 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =2.66 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 0.45 Sample Date and Time:9/27/22 @14:40
Standard Evacuation Volume (3 casing volumes) =1.6
Method of Well Evacuation:Disp. Bailer Remarks: Dry at 2.0 gallons
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):2.0
FIELD ANALYSIS
Volume Purged (gallons)-1.0 2.0
Time (military)1430 1433 1436
pH (S.U.)6.63 6.74 6.78
Sp. Cond. (umhos/cm)569.7 576.4 578.2
Water Temp. (°C)17.1 17.0 17.1
Turbidity (subjective)*20.3 NTU 231 NTU 248 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 1.5 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2124.58
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):3.57
Well ID #:MW-28 Land Surface Elevation (ft msl):2121.01
Downgradient:Yes Screened Interval (ft bgs):10.0 - 15.0
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:sunny Steel Guard Pipe Around Casing:yes
Air Temperature:67 F Locking Cap:no
Total Well Depth in feet (TWD) =17.77 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =13.21 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =4.56 Well Yield (subjective):
1 Casing Volume in gallons (CV) = LWC x 0.17 = 0.78 Sample Date and Time:9/27/22 @ 12:30
Standard Evacuation Volume (3 casing volumes) =2.3
Method of Well Evacuation:Disp. Bailer Remarks: Dry at 2.5 gallons
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):2.5
FIELD ANALYSIS
Volume Purged (gallons)-1.0 2.5
Time (military)1215 1220 1230
pH (S.U.)5.57 5.35 5.47
Sp. Cond. (umhos/cm)1070 988.6 976.7
Water Temp. (°C)16.3 16.2 16.1
Turbidity (subjective)*15.6 NTU 39.6 NTU 44.7 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 1.8 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2117.15
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):3.25
Well ID #:MW-29 Land Surface Elevation (ft msl):2113.90
Downgradient:Yes Screened Interval (ft bgs):2.5 - 12.0
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:sunny Steel Guard Pipe Around Casing:yes
Air Temperature:67 F Locking Cap:yes
Total Well Depth in feet (TWD) =15.60 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =7.47 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =8.13 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 1.38 Sample Date and Time:9/27/22 @ 12:00
Standard Evacuation Volume (3 casing volumes) =4.1
Method of Well Evacuation:Disp. Bailer Remarks:
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):4.5
FIELD ANALYSIS
Volume Purged (gallons)-1.5 3.0 4.5
Time (military)1145 1150 1155 1200
pH (S.U.)6.64 6.79 6.85 7.03
Sp. Cond. (umhos/cm)666.2 643.2 640.1 639.6
Water Temp. (°C)16.5 16.1 16.1 16.0
Turbidity (subjective)*2 3 3 2
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 2.5 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2195.78
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):Flushmount
Well ID #:MW-30 Land Surface Elevation (ft msl):2196.05
Downgradient:Yes Screened Interval (ft bgs):46.0 - 61.0
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:sunny Steel Guard Pipe Around Casing:no
Air Temperature:67 F Locking Cap:yes
Total Well Depth in feet (TWD) =59.40 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =46.42 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =12.98 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 2.2 Sample Date and Time:9/27/22 @ 8:59
Standard Evacuation Volume (3 casing volumes) =6.6
Method of Well Evacuation:Disp. Bailer Remarks:
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):7.0
FIELD ANALYSIS
Volume Purged (gallons)-2.5 5.0 7.0
Time (military)0845 0850 0854 0859
pH (S.U.)6.10 5.79 5.67 5.60
Sp. Cond. (umhos/cm)286.1 270.5 264.3 261.5
Water Temp. (°C)17.1 16.5 16.8 16.9
Turbidity (subjective)*1.85 NTU 48.9 NTU 66.8 NTU 77.3 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 2.2 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2187.25
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):Flushmount
Well ID #:MW-31 Land Surface Elevation (ft msl):2187.43
Downgradient:Yes Screened Interval (ft bgs):55.3 - 70.3
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:Steel Guard Pipe Around Casing:no
Air Temperature:Locking Cap:yes
Total Well Depth in feet (TWD) =70.30 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =55.83 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =14.47 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 2.46 Sample Date and Time:9/27/22 @9:25
Standard Evacuation Volume (3 casing volumes) =7.38
Method of Well Evacuation:Disp. Bailer Remarks: Kink in the well, grab with 1-inch bailer
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):
FIELD ANALYSIS
Volume Purged (gallons)-
Time (military)0925
pH (S.U.)5.61
Sp. Cond. (umhos/cm)430.2
Water Temp. (°C)14.3
Turbidity (subjective)*35.6 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 1.6 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2183.85
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):Flushmount
Well ID #:MW-32 Land Surface Elevation (ft msl):2184.03
Downgradient:Yes Screened Interval (ft bgs):49.0 - 64.0
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:sunny Steel Guard Pipe Around Casing:no
Air Temperature:67 F Locking Cap:yes
Total Well Depth in feet (TWD) =64.00 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =52.24 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =11.76 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.65 = 7.64 Sample Date and Time:9/27/22 @ 10:00
Standard Evacuation Volume (3 casing volumes) =22.9
Method of Well Evacuation:Disp Bailer Remarks: Expandable pipe cap broken
Method of Sample Collection:Disp Bailer Dry at 20 gallons
Total Volume of Water Removed (gallons):20.0
FIELD ANALYSIS
Volume Purged (gallons)-8.0 16.0 20.0
Time (military)0935 0945 0955 1000
pH (S.U.)6.31 5.82 5.74 5.77
Sp. Cond. (umhos/cm)277.1 270.2 270.9 271.6
Water Temp. (°C)15.7 15.8 16.1 16.3
Turbidity (subjective)*12.5 NTU 25.2 NTU 33.8 NTU 145.7 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 2.6 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2177.77
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):Flushmount
Well ID #:MW-33 Land Surface Elevation (ft msl):2177.94
Downgradient:Yes Screened Interval (ft bgs):46.8 - 61.8
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:sunny Steel Guard Pipe Around Casing:no
Air Temperature:67 F Locking Cap:yes
Total Well Depth in feet (TWD) =61.80 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =52.43 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =9.4 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 1.6 Sample Date and Time:9/27/22 @ 10:55
Standard Evacuation Volume (3 casing volumes) =4.8
Method of Well Evacuation:Disp Bailer Remarks:
Method of Sample Collection:Disp Bailer
Total Volume of Water Removed (gallons):6.0
FIELD ANALYSIS
Volume Purged (gallons)-2.0 4.0 6.0
Time (military)1030 1036 1043 1055
pH (S.U.)6.05 5.92 5.91 5.90
Sp. Cond. (umhos/cm)161.5 154.3 155.6 158.3
Water Temp. (°C)16.9 16.2 16.0 16.1
Turbidity (subjective)*40.6 NTU 520.2 NTU 552 NTU 588 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 2.1 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2195.27
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):Flushmount
Well ID #:MW-34 Land Surface Elevation (ft msl):2195.50
Downgradient:Yes Screened Interval (ft bgs):51.6 - 66.6
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:sunny Steel Guard Pipe Around Casing:no
Air Temperature:67 F Locking Cap:yes
Total Well Depth in feet (TWD) =66.80 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =53.16 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =13.64 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 2.3 Sample Date and Time:9/27/22 @ 9:20
Standard Evacuation Volume (3 casing volumes) =7.0
Method of Well Evacuation:Disp. Bailer Remarks:
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):7.5
FIELD ANALYSIS
Volume Purged (gallons)-2.5 5.0 7.5
Time (military)0902 0910 0915 0920
pH (S.U.)5.60 5.63 5.67 5.71
Sp. Cond. (umhos/cm)424.0 426.8 431.4 494.1
Water Temp. (°C)16.4 16.7 15.9 15.7
Turbidity (subjective)*18.4 NTU 52.5 NTU 85.3 NTU 130.4 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 3.0 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2190.64
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):2.75
Well ID #:MW-35 Land Surface Elevation (ft msl):2187.89
Downgradient:Yes Screened Interval (ft bgs):59.6 - 74.6
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:sunny Steel Guard Pipe Around Casing:yes
Air Temperature:67 F Locking Cap:yes
Total Well Depth in feet (TWD) =76.70 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =65.20 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =11.50 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 1.96 Sample Date and Time:9/27/22 @ 9:30
Standard Evacuation Volume (3 casing volumes) =5.9
Method of Well Evacuation:Disp. Bailer Remarks: Kink in well at approximately 15 to 20 ft btoc.
Method of Sample Collection:Disp. Bailer Grab sample with 1-inch bailer.
Total Volume of Water Removed (gallons):
FIELD ANALYSIS
Volume Purged (gallons)-
Time (military)0930
pH (S.U.)6.50
Sp. Cond. (umhos/cm)523.5
Water Temp. (°C)14.3
Turbidity (subjective)*3.55 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 3.2 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name: MB Haynes Measuring Point Elevation (ft msl):2112.76
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):3.27
Well ID #:MW-36 Land Surface Elevation (ft msl):2109.49
Downgradient:Yes Screened Interval (ft bgs):3.0 - 6.0
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:sunny Steel Guard Pipe Around Casing:yes
Air Temperature:67 F Locking Cap:yes
Total Well Depth in feet (TWD) =9.50 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =8.44 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =1.06 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 0.2 Sample Date and Time:0:00
Standard Evacuation Volume (3 casing volumes) =0.5
Method of Well Evacuation:Disp. Bailer Remarks: Dry
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):
FIELD ANALYSIS
Volume Purged (gallons)-
Time (military)
pH (S.U.)
Sp. Cond. (umhos/cm)
Water Temp. (°C)
Turbidity (subjective)*
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2123.88
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):2.97
Well ID #:MW-37 Land Surface Elevation (ft msl):2120.91
Downgradient:Yes Screened Interval (ft bgs):6.0 - 16.0
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:Steel Guard Pipe Around Casing:yes
Air Temperature:Locking Cap:yes
Total Well Depth in feet (TWD) =19.00 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =11.90 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =7.10 Well Yield (subjective):low
1 Casing Volume in gallons (CV) = LWC x 0.17 = 1.2 Sample Date and Time:9/27/22 @11:30
Standard Evacuation Volume (3 casing volumes) =3.6
Method of Well Evacuation:Disp. Bailer Remarks:
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):4.5
FIELD ANALYSIS
Volume Purged (gallons)-1.5 3.0 4.5
Time (military)1115 1120 1125 1130
pH (S.U.)5.99 5.91 5.86 5.89
Sp. Cond. (umhos/cm)41.04 43.35 44.70 45.62
Water Temp. (°C)16.0 16.3 16.2 16.3
Turbidity (subjective)*25.5 NTU 32.8 NTU 44.1 NTU 48.7 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 2.0 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name: MB Haynes Measuring Point Elevation (ft msl):2110.25
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):2.81
Well ID #:MW-38 Land Surface Elevation (ft msl):2107.44
Downgradient:Yes Screened Interval (ft bgs):6.3 - 16.3
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:sunny Steel Guard Pipe Around Casing:yes
Air Temperature:67 F Locking Cap:yes
Total Well Depth in feet (TWD) =19.60 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =11.38 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =8.22 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 1.4 Sample Date and Time:9/27/22 @ 13:30
Standard Evacuation Volume (3 casing volumes) =4.2
Method of Well Evacuation:Disp. Bailer Remarks:
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):4.5
FIELD ANALYSIS
Volume Purged (gallons)-1.5 3.5 4.5
Time (military)1300 1306 1312 1330
pH (S.U.)5.85 5.83 5.70 5.66
Sp. Cond. (umhos/cm)304.2 309.7 303.1 300.5
Water Temp. (°C)16.5 16.3 16.3 16.0
Turbidity (subjective)*7.86 NTU 90.7 NTU 215 NTU 325 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 1.3 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name: MB Haynes Measuring Point Elevation (ft msl):2116.44
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):2.90
Well ID #:MW-39 Land Surface Elevation (ft msl):2113.54
Downgradient:Yes Screened Interval (ft bgs):2.2 - 10.7
Upgradient:No Dedicated Pump or Bailer:no
Weather Conditions:Steel Guard Pipe Around Casing:yes
Air Temperature:Locking Cap:yes
Total Well Depth in feet (TWD) =13.50 Protective Post/Abutment:no
Depth to Ground Water in feet (DGW) =6.49 Well Integrity Satisfactory:yes
Length of Water Column (LWC) = TWD - DGW =7.01 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 1.2 Sample Date and Time:9/27/22 @ 12:52
Standard Evacuation Volume (3 casing volumes) =3.6
Method of Well Evacuation:Disp. Bailer Remarks:
Method of Sample Collection:Disp. Bailer
Total Volume of Water Removed (gallons):4.5
FIELD ANALYSIS
Volume Purged (gallons)-1.5 3.0 4.5
Time (military)1235 1240 1246 1252
pH (S.U.)7.06 7.10 7.07 7.08
Sp. Cond. (umhos/cm)183.0 182.7 180.1 182.5
Water Temp. (°C)16.3 16.7 16.8 17.0
Turbidity (subjective)*1.64 NTU 11.7 NTU 19.6 NTU 28.9 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 2.1 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2136.28
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):2.60
Well ID #:MW-40 Land Surface Elevation (ft msl):2133.68
Downgradient:Yes Screened Interval (ft bgs):18.8 - 33.8
Upgradient:No Dedicated Pump or Bailer:No
Weather Conditions:Steel Guard Pipe Around Casing:Yes
Air Temperature:Locking Cap:Yes
Total Well Depth in feet (TWD) =36.80 Protective Post/Abutment:No
Depth to Ground Water in feet (DGW) =25.53 Well Integrity Satisfactory:Yes
Length of Water Column (LWC) = TWD - DGW =11.27 Well Yield (subjective):
1 Casing Volume in gallons (CV) = LWC x 0.17 = 1.9 Sample Date and Time:9/27/22 @ 15:58
Standard Evacuation Volume (3 casing volumes) =5.7
Method of Well Evacuation:Disp Bailer Remarks:
Method of Sample Collection:Disp Bailer
Total Volume of Water Removed (gallons):6.0
FIELD ANALYSIS
Volume Purged (gallons)-2.0 4.0 6.0
Time (military)1526 1533 1542 1558
pH (S.U.)5.85 5.91 5.98 6.02
Sp. Cond. (umhos/cm)430.4 438.4 436.8 439.3
Water Temp. (°C)16.2 16.2 16.3 16.5
Turbidity (subjective)*10.6 NTU 29.7 NTU 127.3 NTU 145.6 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 1.8 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2133.14
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):2.80
Well ID #:MW-41 Land Surface Elevation (ft msl):2130.34
Downgradient:Yes Screened Interval (ft bgs):15.8 - 30.8
Upgradient:No Dedicated Pump or Bailer:No
Weather Conditions:sunny Steel Guard Pipe Around Casing:Yes
Air Temperature:67 F Locking Cap:Yes
Total Well Depth in feet (TWD) =33.70 Protective Post/Abutment:No
Depth to Ground Water in feet (DGW) =25.31 Well Integrity Satisfactory:Yes
Length of Water Column (LWC) = TWD - DGW =8.39 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 1.43 Sample Date and Time:9/27/22 @ 1520
Standard Evacuation Volume (3 casing volumes) =4.3
Method of Well Evacuation:Disp Bailer Remarks:
Method of Sample Collection:Disp Bailer
Total Volume of Water Removed (gallons):4.5
FIELD ANALYSIS
Volume Purged (gallons)-1.5 3.0 4.5
Time (military)1500 1505 1512 1520
pH (S.U.)6.26 6.00 5.93 5.90
Sp. Cond. (umhos/cm)376.4 382.9 380 376.7
Water Temp. (°C)16.8 16.7 16.1 16.5
Turbidity (subjective)*5.81 NTU 20.3 NTU 102.1 NTU 115.2 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 0.4 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2111.44
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):2.28
Well ID #:TMW-42 Land Surface Elevation (ft msl):2109.16
Downgradient:Yes Screened Interval (ft bgs):2.8 - 7.8
Upgradient:No Dedicated Pump or Bailer:No
Weather Conditions:sunny Steel Guard Pipe Around Casing:No
Air Temperature:67 F Locking Cap:Yes
Total Well Depth in feet (TWD) =10.30 Protective Post/Abutment:No
Depth to Ground Water in feet (DGW) =6.45 Well Integrity Satisfactory:Yes
Length of Water Column (LWC) = TWD - DGW =3.85 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 0.65 Sample Date and Time:9/27/22 @ 14:25
Standard Evacuation Volume (3 casing volumes) =2.0
Method of Well Evacuation:Disp Bailer Remarks: Dry at 2.5 gallons
Method of Sample Collection:Disp Bailer
Total Volume of Water Removed (gallons):2.5
FIELD ANALYSIS
Volume Purged (gallons)-1 2
Time (military)1412 1415 1420
pH (S.U.)6.51 6.57 6.62
Sp. Cond. (umhos/cm)492.9 523.6 534.7
Water Temp. (°C)16.5 16.1 16.0
Turbidity (subjective)*18.6 NTU 108 NTU 121 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 1.0 mg/L

BUNNELL-LAMMONS ENGINEERING, INC.
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Page 1 of 1
Date:Sep. 27, 2022 Casing Diameter:2 inches
Field Personnel:IAI Casing Material:PVC
Site Name:MB Haynes Measuring Point Elevation (ft msl):2110.48
BLE Job #:J22-5293-22 Height of Riser (ft above land surface):2.24
Well ID #:TMW-43 Land Surface Elevation (ft msl):2108.24
Downgradient:Yes Screened Interval (ft bgs):2.8 - 7.8
Upgradient:No Dedicated Pump or Bailer:No
Weather Conditions:Steel Guard Pipe Around Casing:No
Air Temperature:Locking Cap:Yes
Total Well Depth in feet (TWD) =10.30 Protective Post/Abutment:No
Depth to Ground Water in feet (DGW) =5.39 Well Integrity Satisfactory:Yes
Length of Water Column (LWC) = TWD - DGW =4.91 Well Yield (subjective):sufficient
1 Casing Volume in gallons (CV) = LWC x 0.17 = 0.83 Sample Date and Time:9/27/22 @ 14:08
Standard Evacuation Volume (3 casing volumes) =2.5
Method of Well Evacuation:Disp Bailer Remarks:
Method of Sample Collection:Disp Bailer
Total Volume of Water Removed (gallons):3.0
FIELD ANALYSIS
Volume Purged (gallons)-1.0 2.0 3.0
Time (military)1400 1402 1404 1408
pH (S.U.)6.20 6.21 6.20 6.31
Sp. Cond. (umhos/cm)341.7 342.8 347.1 349.7
Water Temp. (°C)16.6 16.3 16.2 16.9
Turbidity (subjective)*10.7 NTU 108.7 NTU 131 NTU 218.7 NTU
* (1) Clear (2) Slight (3) Moderate (4) High
COMMENTS/OBSERVATIONS:DO= 1.2 mg/L

APPENDIX B
Laboratory Data

The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC.
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Report of Analysis
Bunnell-Lammons Engineering,Inc.
6004 Ponders Court
Greenville,SC 29615
Attention:Andy Alexander
Project Name:MB Haynes MW
Project Number:5293-22
Lot Number:XI30005
Date Completed:11/03/2022
11/04/2022 11:03 AM
Approved and released by:
Project Manager II:Lucas Odom
Page 1 of 66
PACE ANALYTICAL SERVICES,LLC
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Bunnell-Lammons Engineering,Inc.
Lot Number:XI30005
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.Where
sampling is conducted by the client,results relate to the accuracy of the information provided,and as the
samples are received.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace")
Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to
the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory;however,the following analyses are currently not listed on our TNI
scope of accreditation:Drinking Water:VOC (excluding BTEX,MTBE,Naphthalene,&1,2-
dichloroethane)EPA 524.2,E.coli and Total coliforms SM 9223 B-2004,Solid Chemical Material:TOC
Walkley-Black,Biological Tissue:All,Non-Potable Water:SGT-HEM EPA 1664B,Silica EPA 200.7,
Boron,Calcium,Silicon,Strontium EPA 200.8,Bicarbonate,Carbonate,and Hydroxide Alkalinity SM 2320
B-2011,SM 9221 C E-2006 &SM 9222D-2006,Strontium SW-846 6010D,VOC SM 6200 B-2011,Fecal
Coliform Colilert-18.
If you have any questions regarding this report,please contact the Pace Project Manager listed on the
cover page.
VOCs by GC/MS
The laboratory control sample (LCS)and /or laboratory control sample duplicate (LCSD)for analytical
batch 56004 and 56114exceeded acceptance criteria for Bromomethane.These analytes were biased
high and were not detected in the samples affected.
The following samples were received with headspace in the sample vial:XI30005-003,XI30005-004.The
vial containing the least amount of headspace has been used for analysis.
Reanalysis of the following samples was performed outside of the analytical holding time for trans-1,4-
dichloro-2-butene:XI30005-002,XI30005-016,XI30005-018.This compound failed calibration on the R1
instrument,therefore trans-1,4-dichloro-2-butene is not valid in the R1.
Page 2 of 66
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: XI30005

Sample Number Sample ID Matrix Date Sampled Date Received
001 09/27/2022 0840MW-26 Aqueous 09/29/2022
002 09/27/2022 1436MW-27 Aqueous 09/29/2022
003 09/27/2022 1230MW-28 Aqueous 09/29/2022
004 09/27/2022 1200MW-29 Aqueous 09/29/2022
005 09/27/2022 0859MW-30 Aqueous 09/29/2022
006 09/27/2022 0925MW-31 Aqueous 09/29/2022
007 09/27/2022 1000MW-32 Aqueous 09/29/2022
008 09/27/2022 1055MW-33 Aqueous 09/29/2022
009 09/27/2022 0920MW-34 Aqueous 09/29/2022
010 09/27/2022 0930MW-35 Aqueous 09/29/2022
011 09/27/2022 1130MW-37 Aqueous 09/29/2022
012 09/27/2022 1330MW-38 Aqueous 09/29/2022
013 09/27/2022 1252MW-39 Aqueous 09/29/2022
014 09/27/2022 1558MW-40 Aqueous 09/29/2022
015 09/27/2022 1520MW-41 Aqueous 09/29/2022
016 09/27/2022 1425TMW-42 Aqueous 09/29/2022
017 09/27/2022 1408TMW-43 Aqueous 09/29/2022
018 09/27/2022Trip Blank Aqueous 09/29/2022
(18 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 66
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: XI30005

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 MW-26 Aqueous Acetone 8260D 7.6 J ug/L 8
001 MW-26 Aqueous 2-Butanone (MEK)8260D 3.6 J ug/L 8
002 MW-27 Aqueous Benzene 8260D 2.0 ug/L 10
002 MW-27 Aqueous sec-Butylbenzene 8260D 3.3 ug/L 10
002 MW-27 Aqueous Diisopropyl ether (IPE)8260D 0.68 J ug/L 10
002 MW-27 Aqueous Isopropylbenzene 8260D 0.44 J ug/L 11
002 MW-27 Aqueous Methyl tertiary butyl ether 8260D 15 ug/L 11
003 MW-28 Aqueous Benzene 8260D 6800 ug/L 12
003 MW-28 Aqueous Ethylbenzene 8260D 2300 ug/L 12
003 MW-28 Aqueous Isopropylbenzene 8260D 48 ug/L 13
003 MW-28 Aqueous Methyl tertiary butyl ether 8260D 100 ug/L 13
003 MW-28 Aqueous Naphthalene 8260D 280 ug/L 13
003 MW-28 Aqueous n-Propylbenzene 8260D 130 ug/L 13
003 MW-28 Aqueous Toluene 8260D 18000 ug/L 13
003 MW-28 Aqueous 1,2,4-Trimethylbenzene 8260D 1200 ug/L 13
003 MW-28 Aqueous 1,3,5-Trimethylbenzene 8260D 280 ug/L 13
003 MW-28 Aqueous Xylenes (total)8260D 8700 ug/L 13
004 MW-29 Aqueous Benzene 8260D 600 ug/L 14
004 MW-29 Aqueous sec-Butylbenzene 8260D 12 ug/L 14
004 MW-29 Aqueous Ethylbenzene 8260D 1500 ug/L 14
004 MW-29 Aqueous Isopropylbenzene 8260D 85 ug/L 15
004 MW-29 Aqueous p-Isopropyltoluene 8260D 8.4 ug/L 15
004 MW-29 Aqueous Methyl tertiary butyl ether 8260D 4.2 J ug/L 15
004 MW-29 Aqueous Naphthalene 8260D 330 ug/L 15
004 MW-29 Aqueous n-Propylbenzene 8260D 280 ug/L 15
004 MW-29 Aqueous Toluene 8260D 1300 ug/L 15
004 MW-29 Aqueous 1,2,4-Trimethylbenzene 8260D 2500 ug/L 15
004 MW-29 Aqueous 1,3,5-Trimethylbenzene 8260D 640 ug/L 15
004 MW-29 Aqueous Xylenes (total)8260D 3400 ug/L 15
005 MW-30 Aqueous Chloroform 8260D 1.6 ug/L 16
007 MW-32 Aqueous Chloroform 8260D 1.5 ug/L 20
008 MW-33 Aqueous Chloroform 8260D 2.6 ug/L 22
009 MW-34 Aqueous Chloroform 8260D 0.93 J ug/L 24
010 MW-35 Aqueous Benzene 8260D 1000 ug/L 26
010 MW-35 Aqueous n-Butylbenzene 8260D 31 ug/L 26
010 MW-35 Aqueous sec-Butylbenzene 8260D 14 ug/L 26
010 MW-35 Aqueous Ethylbenzene 8260D 620 ug/L 26
010 MW-35 Aqueous 2-Hexanone 8260D 11 ug/L 27
010 MW-35 Aqueous Isopropylbenzene 8260D 83 ug/L 27
010 MW-35 Aqueous p-Isopropyltoluene 8260D 12 ug/L 27
010 MW-35 Aqueous Methyl tertiary butyl ether 8260D 23 ug/L 27
010 MW-35 Aqueous Naphthalene 8260D 300 ug/L 27
010 MW-35 Aqueous n-Propylbenzene 8260D 230 ug/L 27
010 MW-35 Aqueous Toluene 8260D 110 ug/L 27
010 MW-35 Aqueous 1,2,4-Trimethylbenzene 8260D 560 ug/L 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 66
Detection Summary (Continued)
Lot Number: XI30005
Sample Sample ID Matrix Parameter Method Result Q Units Page
010 MW-35 Aqueous 1,3,5-Trimethylbenzene 8260D 290 ug/L 27
010 MW-35 Aqueous Xylenes (total)8260D 380 ug/L 27
014 MW-40 Aqueous Benzene 8260D 4.2 ug/L 34
014 MW-40 Aqueous n-Butylbenzene 8260D 1.1 ug/L 34
014 MW-40 Aqueous sec-Butylbenzene 8260D 1.0 ug/L 34
014 MW-40 Aqueous Chloroform 8260D 0.47 J ug/L 34
014 MW-40 Aqueous Isopropylbenzene 8260D 2.5 ug/L 35
014 MW-40 Aqueous Methyl tertiary butyl ether 8260D 0.56 J ug/L 35
014 MW-40 Aqueous Naphthalene 8260D 4.6 ug/L 35
016 TMW-42 Aqueous Benzene 8260D 8.3 ug/L 38
016 TMW-42 Aqueous n-Butylbenzene 8260D 1.9 ug/L 38
016 TMW-42 Aqueous sec-Butylbenzene 8260D 2.9 ug/L 38
016 TMW-42 Aqueous tert-Butylbenzene 8260D 0.44 J ug/L 38
016 TMW-42 Aqueous Ethylbenzene 8260D 29 ug/L 38
016 TMW-42 Aqueous Isopropylbenzene 8260D 6.9 ug/L 39
016 TMW-42 Aqueous p-Isopropyltoluene 8260D 0.81 J ug/L 39
016 TMW-42 Aqueous Methyl tertiary butyl ether 8260D 6.3 ug/L 39
016 TMW-42 Aqueous Naphthalene 8260D 5.0 ug/L 39
016 TMW-42 Aqueous n-Propylbenzene 8260D 14 ug/L 39
016 TMW-42 Aqueous Toluene 8260D 1.0 ug/L 39
016 TMW-42 Aqueous 1,2,4-Trimethylbenzene 8260D 14 ug/L 39
016 TMW-42 Aqueous Xylenes (total)8260D 3.5 ug/L 39
017 TMW-43 Aqueous Benzene 8260D 1.8 ug/L 40
017 TMW-43 Aqueous sec-Butylbenzene 8260D 19 ug/L 40
017 TMW-43 Aqueous tert-Butylbenzene 8260D 0.63 J ug/L 40
017 TMW-43 Aqueous Ethylbenzene 8260D 130 ug/L 40
017 TMW-43 Aqueous Isopropylbenzene 8260D 60 ug/L 41
017 TMW-43 Aqueous p-Isopropyltoluene 8260D 14 ug/L 41
017 TMW-43 Aqueous Methyl tertiary butyl ether 8260D 1.2 ug/L 41
017 TMW-43 Aqueous Naphthalene 8260D 130 ug/L 41
017 TMW-43 Aqueous n-Propylbenzene 8260D 200 ug/L 41
017 TMW-43 Aqueous Toluene 8260D 7.5 ug/L 41
017 TMW-43 Aqueous 1,2,4-Trimethylbenzene 8260D 1200 ug/L 41
017 TMW-43 Aqueous 1,3,5-Trimethylbenzene 8260D 430 ug/L 41
017 TMW-43 Aqueous Xylenes (total)8260D 350 ug/L 41
(80 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-26
XI30005-001
09/27/2022 0840
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/04/2022 1841 CDA 56004
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D 7.6 J 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D 3.6 J 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-26
XI30005-001
09/27/2022 0840
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/04/2022 1841 CDA 56004
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 94 70-130
1,2-Dichloroethane-d4 109 70-130
Toluene-d8 105 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-27
XI30005-002
09/27/2022 1436
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/06/2022 2302 SDC 56308
2 5030B 8260D 1 11/03/2022 0149 JMM2 59017
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D 2.0 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D 3.3 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND H 2ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D 0.68 J 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-27
XI30005-002
09/27/2022 1436
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/06/2022 2302 SDC 56308
2 5030B 8260D 1 11/03/2022 0149 JMM2 59017
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D 0.44 J 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D 15 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 107 70-130 H 100 70-130
1,2-Dichloroethane-d4 101 70-130 H 97 70-130
Toluene-d8 106 70-130 H 100 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-28
XI30005-003
09/27/2022 1230
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 20 10/05/2022 1756 CDA 56114
2 5030B 8260D 200 10/07/2022 0705 JMM2 56315
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L100400
Benzene 71-43-2 8260D 6800 2ug/L80200
Bromobenzene 108-86-1 8260D ND 1ug/L8.020
Bromochloromethane 74-97-5 8260D ND 1ug/L8.020
Bromoform 75-25-2 8260D ND 1ug/L8.020
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L8.040
2-Butanone (MEK)78-93-3 8260D ND 1ug/L40200
n-Butylbenzene 104-51-8 8260D ND 1ug/L8.020
sec-Butylbenzene 135-98-8 8260D ND 1ug/L8.020
tert-Butylbenzene 98-06-6 8260D ND 1ug/L8.020
Carbon tetrachloride 56-23-5 8260D ND 1ug/L8.020
Chlorobenzene 108-90-7 8260D ND 1ug/L8.020
Chloroethane 75-00-3 8260D ND 1ug/L8.040
Chloroform 67-66-3 8260D ND 1ug/L8.020
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L1020
2-Chlorotoluene 95-49-8 8260D ND 1ug/L8.020
4-Chlorotoluene 106-43-4 8260D ND 1ug/L8.020
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L8.020
Dibromochloromethane 124-48-1 8260D ND 1ug/L8.020
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L8.020
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L8.020
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L1040
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L8.020
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L8.020
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L8.020
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L1240
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L8.020
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L8.020
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L8.020
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L8.020
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L8.020
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L8.020
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L8.020
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L8.020
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L8.040
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L8.020
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L8.020
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L8.020
Ethylbenzene 100-41-4 8260D 2300 1ug/L8.020
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-28
XI30005-003
09/27/2022 1230
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 20 10/05/2022 1756 CDA 56114
2 5030B 8260D 200 10/07/2022 0705 JMM2 56315
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L8.020
2-Hexanone 591-78-6 8260D ND 1ug/L40200
Isopropylbenzene 98-82-8 8260D 48 1ug/L8.020
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L8.020
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D 100 1ug/L8.020
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L40200
Methylene chloride 75-09-2 8260D ND 1ug/L8.020
Naphthalene 91-20-3 8260D 280 1ug/L8.020
n-Propylbenzene 103-65-1 8260D 130 1ug/L8.020
Styrene 100-42-5 8260D ND 1ug/L8.220
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L8.020
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L8.020
Tetrachloroethene 127-18-4 8260D ND 1ug/L8.020
Toluene 108-88-3 8260D 18000 2ug/L80200
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L8.420
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L8.020
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L8.020
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L8.020
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L8.020
Trichloroethene 79-01-6 8260D ND 1ug/L8.020
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L8.020
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L8.020
1,2,4-Trimethylbenzene 95-63-6 8260D 1200 1ug/L8.020
1,3,5-Trimethylbenzene 108-67-8 8260D 280 1ug/L8.020
Vinyl chloride 75-01-4 8260D ND 1ug/L8.020
Xylenes (total)1330-20-7 8260D 8700 2ug/L80200
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 95 70-130 97 70-130
1,2-Dichloroethane-d4 99 70-130 96 70-130
Toluene-d8 103 70-130 95 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-29
XI30005-004
09/27/2022 1200
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 5 10/05/2022 1706 CDA 56114
2 5030B 8260D 50 10/07/2022 0640 JMM2 56315
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L25100
Benzene 71-43-2 8260D 600 1ug/L2.05.0
Bromobenzene 108-86-1 8260D ND 1ug/L2.05.0
Bromochloromethane 74-97-5 8260D ND 1ug/L2.05.0
Bromoform 75-25-2 8260D ND 1ug/L2.05.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L2.010
2-Butanone (MEK)78-93-3 8260D ND 1ug/L1050
n-Butylbenzene 104-51-8 8260D ND 1ug/L2.05.0
sec-Butylbenzene 135-98-8 8260D 12 1ug/L2.05.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L2.05.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L2.05.0
Chlorobenzene 108-90-7 8260D ND 1ug/L2.05.0
Chloroethane 75-00-3 8260D ND 1ug/L2.010
Chloroform 67-66-3 8260D ND 1ug/L2.05.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L2.55.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L2.05.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L2.05.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L2.05.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L2.05.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L2.05.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L2.05.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L2.510
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L2.05.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L2.05.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L2.05.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L3.010
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L2.05.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L2.05.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L2.05.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L2.05.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L2.05.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L2.05.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L2.05.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L2.05.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L2.010
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L2.05.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L2.05.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L2.05.0
Ethylbenzene 100-41-4 8260D 1500 2ug/L2050
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-29
XI30005-004
09/27/2022 1200
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 5 10/05/2022 1706 CDA 56114
2 5030B 8260D 50 10/07/2022 0640 JMM2 56315
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L2.05.0
2-Hexanone 591-78-6 8260D ND 1ug/L1050
Isopropylbenzene 98-82-8 8260D 85 1ug/L2.05.0
p-Isopropyltoluene 99-87-6 8260D 8.4 1ug/L2.05.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D 4.2 J 1ug/L2.05.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L1050
Methylene chloride 75-09-2 8260D ND 1ug/L2.05.0
Naphthalene 91-20-3 8260D 330 1ug/L2.05.0
n-Propylbenzene 103-65-1 8260D 280 1ug/L2.05.0
Styrene 100-42-5 8260D ND 1ug/L2.15.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L2.05.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L2.05.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L2.05.0
Toluene 108-88-3 8260D 1300 2ug/L2050
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L2.15.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L2.05.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L2.05.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L2.05.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L2.05.0
Trichloroethene 79-01-6 8260D ND 1ug/L2.05.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L2.05.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L2.05.0
1,2,4-Trimethylbenzene 95-63-6 8260D 2500 2ug/L2050
1,3,5-Trimethylbenzene 108-67-8 8260D 640 1ug/L2.05.0
Vinyl chloride 75-01-4 8260D ND 1ug/L2.05.0
Xylenes (total)1330-20-7 8260D 3400 2ug/L2050
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 101 70-130 98 70-130
1,2-Dichloroethane-d4 97 70-130 92 70-130
Toluene-d8 107 70-130 92 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-30
XI30005-005
09/27/2022 0859
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1253 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D 1.6 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-30
XI30005-005
09/27/2022 0859
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1253 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 94 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 103 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-31
XI30005-006
09/27/2022 0925
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1319 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 16 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-31
XI30005-006
09/27/2022 0925
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1319 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 94 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 103 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 17 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-32
XI30005-007
09/27/2022 1000
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1344 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D 1.5 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 18 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-32
XI30005-007
09/27/2022 1000
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1344 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 104 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 19 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-33
XI30005-008
09/27/2022 1055
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1409 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D 2.6 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 20 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-33
XI30005-008
09/27/2022 1055
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1409 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 96 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 103 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 21 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-34
XI30005-009
09/27/2022 0920
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1435 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D 0.93 J 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 22 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-34
XI30005-009
09/27/2022 0920
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1435 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 91 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 102 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 23 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-35
XI30005-010
09/27/2022 0930
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1912 CDA 56114
2 5030B 8260D 10 10/07/2022 0447 SDC 56308
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D 1000 2ug/L4.010
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D 31 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D 14 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D 620 2ug/L4.010
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 24 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-35
XI30005-010
09/27/2022 0930
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1912 CDA 56114
2 5030B 8260D 10 10/07/2022 0447 SDC 56308
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D 11 1ug/L2.010
Isopropylbenzene 98-82-8 8260D 83 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D 12 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D 23 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D 300 2ug/L4.010
n-Propylbenzene 103-65-1 8260D 230 2ug/L4.010
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D 110 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D 560 2ug/L4.010
1,3,5-Trimethylbenzene 108-67-8 8260D 290 2ug/L4.010
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D 380 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 101 70-130 106 70-130
1,2-Dichloroethane-d4 90 70-130 104 70-130
Toluene-d8 105 70-130 105 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 25 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-37
XI30005-011
09/27/2022 1130
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1500 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 26 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-37
XI30005-011
09/27/2022 1130
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1500 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 102 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 27 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-38
XI30005-012
09/27/2022 1330
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1525 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 28 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-38
XI30005-012
09/27/2022 1330
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1525 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 93 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 103 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 29 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-39
XI30005-013
09/27/2022 1252
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1551 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 30 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-39
XI30005-013
09/27/2022 1252
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1551 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 102 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 31 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-40
XI30005-014
09/27/2022 1558
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1616 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D 4.2 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D 1.1 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D 1.0 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D 0.47 J 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 32 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-40
XI30005-014
09/27/2022 1558
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1616 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D 2.5 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D 0.56 J 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D 4.6 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 97 70-130
1,2-Dichloroethane-d4 103 70-130
Toluene-d8 106 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 33 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-41
XI30005-015
09/27/2022 1520
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1641 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 34 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
MW-41
XI30005-015
09/27/2022 1520
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1641 CDA 56114
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 109 70-130
Toluene-d8 104 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 35 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
TMW-42
XI30005-016
09/27/2022 1425
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/06/2022 2325 SDC 56308
2 5030B 8260D 1 11/03/2022 0214 JMM2 59017
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D 8.3 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D 1.9 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D 2.9 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D 0.44 J 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND H 2ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D 29 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 36 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
TMW-42
XI30005-016
09/27/2022 1425
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/06/2022 2325 SDC 56308
2 5030B 8260D 1 11/03/2022 0214 JMM2 59017
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D 6.9 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D 0.81 J 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D 6.3 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D 5.0 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D 14 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D 1.0 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D 14 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D 3.5 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 112 70-130 H 96 70-130
1,2-Dichloroethane-d4 103 70-130 H 91 70-130
Toluene-d8 105 70-130 H 96 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 37 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
TMW-43
XI30005-017
09/27/2022 1408
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1847 CDA 56114
2 5030B 8260D 10 10/07/2022 0615 JMM2 56315
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D 1.8 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND L 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D 19 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D 0.63 J 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D 130 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 38 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
TMW-43
XI30005-017
09/27/2022 1408
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/05/2022 1847 CDA 56114
2 5030B 8260D 10 10/07/2022 0615 JMM2 56315
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D 60 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D 14 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D 1.2 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D 130 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D 200 2ug/L4.010
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D 7.5 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D 1200 2ug/L4.010
1,3,5-Trimethylbenzene 108-67-8 8260D 430 2ug/L4.010
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D 350 2ug/L4.010
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 104 70-130 98 70-130
1,2-Dichloroethane-d4 92 70-130 93 70-130
Toluene-d8 106 70-130 93 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 39 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
Trip Blank
XI30005-018
09/27/2022
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/06/2022 2240 SDC 56308
2 5030B 8260D 1 11/03/2022 0125 JMM2 59017
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND H 2ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 40 of 66
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
Trip Blank
XI30005-018
09/27/2022
09/29/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/06/2022 2240 SDC 56308
2 5030B 8260D 1 11/03/2022 0125 JMM2 59017
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 108 70-130 H 100 70-130
1,2-Dichloroethane-d4 103 70-130 H 98 70-130
Toluene-d8 105 70-130 H 100 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 41 of 66
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 42 of 66
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56004-001
56004 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 10/04/2022 1041205.0 ug/L1
Benzene ND 10/04/2022 10411.0 0.40 ug/L1
Bromobenzene ND 10/04/2022 10411.0 0.40 ug/L1
Bromochloromethane ND 10/04/2022 10411.0 0.40 ug/L1
Bromoform ND 10/04/2022 10411.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 10/04/2022 10412.0 0.40 ug/L1
2-Butanone (MEK)ND 10/04/2022 1041102.0 ug/L1
n-Butylbenzene ND 10/04/2022 10411.0 0.40 ug/L1
sec-Butylbenzene ND 10/04/2022 10411.0 0.40 ug/L1
tert-Butylbenzene ND 10/04/2022 10411.0 0.40 ug/L1
Carbon tetrachloride ND 10/04/2022 10411.0 0.40 ug/L1
Chlorobenzene ND 10/04/2022 10411.0 0.40 ug/L1
Chloroethane ND 10/04/2022 10412.0 0.40 ug/L1
Chloroform ND 10/04/2022 10411.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 10/04/2022 10411.0 0.50 ug/L1
2-Chlorotoluene ND 10/04/2022 10411.0 0.40 ug/L1
4-Chlorotoluene ND 10/04/2022 10411.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 10/04/2022 10411.0 0.40 ug/L1
Dibromochloromethane ND 10/04/2022 10411.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 10/04/2022 10411.0 0.40 ug/L1
Dibromomethane (Methylene bromide)ND 10/04/2022 10411.0 0.40 ug/L1
trans-1,4-Dichloro-2-butene ND 10/04/2022 10412.0 0.50 ug/L1
1,2-Dichlorobenzene ND 10/04/2022 10411.0 0.40 ug/L1
1,3-Dichlorobenzene ND 10/04/2022 10411.0 0.40 ug/L1
1,4-Dichlorobenzene ND 10/04/2022 10411.0 0.40 ug/L1
Dichlorodifluoromethane ND 10/04/2022 10412.0 0.60 ug/L1
1,1-Dichloroethane ND 10/04/2022 10411.0 0.40 ug/L1
1,2-Dichloroethane ND 10/04/2022 10411.0 0.40 ug/L1
1,1-Dichloroethene ND 10/04/2022 10411.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 10/04/2022 10411.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 10/04/2022 10411.0 0.40 ug/L1
1,2-Dichloropropane ND 10/04/2022 10411.0 0.40 ug/L1
1,3-Dichloropropane ND 10/04/2022 10411.0 0.40 ug/L1
2,2-Dichloropropane ND 10/04/2022 10411.0 0.40 ug/L1
1,1-Dichloropropene ND 10/04/2022 10412.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 10/04/2022 10411.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 10/04/2022 10411.0 0.40 ug/L1
Diisopropyl ether (IPE)ND 10/04/2022 10411.0 0.40 ug/L1
Ethylbenzene ND 10/04/2022 10411.0 0.40 ug/L1
Hexachlorobutadiene ND 10/04/2022 10411.0 0.40 ug/L1
2-Hexanone ND 10/04/2022 1041102.0 ug/L1
Isopropylbenzene ND 10/04/2022 10411.0 0.40 ug/L1
p-Isopropyltoluene ND 10/04/2022 10411.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 10/04/2022 10411.0 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 43 of 66
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56004-001
56004 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
4-Methyl-2-pentanone ND 10/04/2022 1041102.0 ug/L1
Methylene chloride ND 10/04/2022 10411.0 0.40 ug/L1
Naphthalene ND 10/04/2022 10411.0 0.40 ug/L1
n-Propylbenzene ND 10/04/2022 10411.0 0.40 ug/L1
Styrene ND 10/04/2022 10411.0 0.41 ug/L1
1,1,1,2-Tetrachloroethane ND 10/04/2022 10411.0 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 10/04/2022 10411.0 0.40 ug/L1
Tetrachloroethene ND 10/04/2022 10411.0 0.40 ug/L1
Toluene ND 10/04/2022 10411.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10/04/2022 10411.0 0.42 ug/L1
1,2,3-Trichlorobenzene ND 10/04/2022 10411.0 0.40 ug/L1
1,2,4-Trichlorobenzene ND 10/04/2022 10411.0 0.40 ug/L1
1,1,1-Trichloroethane ND 10/04/2022 10411.0 0.40 ug/L1
1,1,2-Trichloroethane ND 10/04/2022 10411.0 0.40 ug/L1
Trichloroethene ND 10/04/2022 10411.0 0.40 ug/L1
Trichlorofluoromethane ND 10/04/2022 10411.0 0.40 ug/L1
1,2,3-Trichloropropane ND 10/04/2022 10411.0 0.40 ug/L1
1,2,4-Trimethylbenzene ND 10/04/2022 10411.0 0.40 ug/L1
1,3,5-Trimethylbenzene ND 10/04/2022 10411.0 0.40 ug/L1
Vinyl chloride ND 10/04/2022 10411.0 0.40 ug/L1
Xylenes (total)ND 10/04/2022 10411.0 0.40 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 96 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 44 of 66
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56004-002
56004 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Acetone 130 10/04/2022 093413010060-1401
Benzene 59 10/04/2022 09341175070-1301
Bromobenzene 54 10/04/2022 09341085070-1301
Bromochloromethane 58 10/04/2022 09341165070-1301
Bromoform 51 10/04/2022 09341035070-1301
Bromomethane (Methyl bromide)66 10/04/2022 0934N1335070-1301
2-Butanone (MEK)110 10/04/2022 093410710070-1301
n-Butylbenzene 60 10/04/2022 09341195070-1301
sec-Butylbenzene 58 10/04/2022 09341175070-1301
tert-Butylbenzene 57 10/04/2022 09341145070-1301
Carbon tetrachloride 56 10/04/2022 09341125070-1301
Chlorobenzene 55 10/04/2022 09341105070-1301
Chloroethane 58 10/04/2022 09341165070-1301
Chloroform 56 10/04/2022 09341125070-1301
Chloromethane (Methyl chloride)56 10/04/2022 09341135060-1401
2-Chlorotoluene 58 10/04/2022 09341155070-1301
4-Chlorotoluene 55 10/04/2022 09341095070-1301
1,2-Dibromo-3-chloropropane (DBCP)51 10/04/2022 09341015070-1301
Dibromochloromethane 54 10/04/2022 09341085070-1301
1,2-Dibromoethane (EDB)54 10/04/2022 09341075070-1301
Dibromomethane (Methylene bromide)55 10/04/2022 09341095070-1301
trans-1,4-Dichloro-2-butene 41 10/04/2022 0934825070-1301
1,2-Dichlorobenzene 57 10/04/2022 09341145070-1301
1,3-Dichlorobenzene 56 10/04/2022 09341135070-1301
1,4-Dichlorobenzene 55 10/04/2022 09341115070-1301
Dichlorodifluoromethane 57 10/04/2022 09341145060-1401
1,1-Dichloroethane 59 10/04/2022 09341185070-1301
1,2-Dichloroethane 52 10/04/2022 09341045070-1301
1,1-Dichloroethene 56 10/04/2022 09341135070-1301
cis-1,2-Dichloroethene 59 10/04/2022 09341185070-1301
trans-1,2-Dichloroethene 57 10/04/2022 09341145070-1301
1,2-Dichloropropane 58 10/04/2022 09341175070-1301
1,3-Dichloropropane 56 10/04/2022 09341115070-1301
2,2-Dichloropropane 55 10/04/2022 09341105070-1301
1,1-Dichloropropene 55 10/04/2022 09341095070-1301
cis-1,3-Dichloropropene 56 10/04/2022 09341125070-1301
trans-1,3-Dichloropropene 54 10/04/2022 09341075070-1301
Diisopropyl ether (IPE)55 10/04/2022 09341105070-1301
Ethylbenzene 54 10/04/2022 09341085070-1301
Hexachlorobutadiene 61 10/04/2022 09341215060-1401
2-Hexanone 120 10/04/2022 093411710070-1301
Isopropylbenzene 56 10/04/2022 09341135070-1301
p-Isopropyltoluene 57 10/04/2022 09341155070-1301
Methyl tertiary butyl ether (MTBE)53 10/04/2022 09341065070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 45 of 66
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56004-002
56004 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
4-Methyl-2-pentanone 100 10/04/2022 093410510070-1301
Methylene chloride 62 10/04/2022 09341235070-1301
Naphthalene 50 10/04/2022 09341005070-1301
n-Propylbenzene 59 10/04/2022 09341175070-1301
Styrene 55 10/04/2022 09341095070-1301
1,1,1,2-Tetrachloroethane 53 10/04/2022 09341065070-1301
1,1,2,2-Tetrachloroethane 56 10/04/2022 09341125070-1301
Tetrachloroethene 56 10/04/2022 09341135070-1301
Toluene 56 10/04/2022 09341125070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 56 10/04/2022 09341125070-1301
1,2,3-Trichlorobenzene 51 10/04/2022 09341025070-1301
1,2,4-Trichlorobenzene 51 10/04/2022 09341015070-1301
1,1,1-Trichloroethane 54 10/04/2022 09341085070-1301
1,1,2-Trichloroethane 55 10/04/2022 09341105070-1301
Trichloroethene 57 10/04/2022 09341145070-1301
Trichlorofluoromethane 57 10/04/2022 09341155070-1301
1,2,3-Trichloropropane 55 10/04/2022 09341095070-1301
1,2,4-Trimethylbenzene 58 10/04/2022 09341175070-1301
1,3,5-Trimethylbenzene 58 10/04/2022 09341165070-1301
Vinyl chloride 63 10/04/2022 09341265070-1301
Xylenes (total)110 10/04/2022 093410610070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 105 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 46 of 66
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56114-001
56114 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 10/05/2022 1046205.0 ug/L1
Benzene ND 10/05/2022 10461.0 0.40 ug/L1
Bromobenzene ND 10/05/2022 10461.0 0.40 ug/L1
Bromochloromethane ND 10/05/2022 10461.0 0.40 ug/L1
Bromoform ND 10/05/2022 10461.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 10/05/2022 10462.0 0.40 ug/L1
2-Butanone (MEK)ND 10/05/2022 1046102.0 ug/L1
n-Butylbenzene ND 10/05/2022 10461.0 0.40 ug/L1
sec-Butylbenzene ND 10/05/2022 10461.0 0.40 ug/L1
tert-Butylbenzene ND 10/05/2022 10461.0 0.40 ug/L1
Carbon tetrachloride ND 10/05/2022 10461.0 0.40 ug/L1
Chlorobenzene ND 10/05/2022 10461.0 0.40 ug/L1
Chloroethane ND 10/05/2022 10462.0 0.40 ug/L1
Chloroform ND 10/05/2022 10461.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 10/05/2022 10461.0 0.50 ug/L1
2-Chlorotoluene ND 10/05/2022 10461.0 0.40 ug/L1
4-Chlorotoluene ND 10/05/2022 10461.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 10/05/2022 10461.0 0.40 ug/L1
Dibromochloromethane ND 10/05/2022 10461.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 10/05/2022 10461.0 0.40 ug/L1
Dibromomethane (Methylene bromide)ND 10/05/2022 10461.0 0.40 ug/L1
trans-1,4-Dichloro-2-butene ND 10/05/2022 10462.0 0.50 ug/L1
1,2-Dichlorobenzene ND 10/05/2022 10461.0 0.40 ug/L1
1,3-Dichlorobenzene ND 10/05/2022 10461.0 0.40 ug/L1
1,4-Dichlorobenzene ND 10/05/2022 10461.0 0.40 ug/L1
Dichlorodifluoromethane ND 10/05/2022 10462.0 0.60 ug/L1
1,1-Dichloroethane ND 10/05/2022 10461.0 0.40 ug/L1
1,2-Dichloroethane ND 10/05/2022 10461.0 0.40 ug/L1
1,1-Dichloroethene ND 10/05/2022 10461.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 10/05/2022 10461.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 10/05/2022 10461.0 0.40 ug/L1
1,2-Dichloropropane ND 10/05/2022 10461.0 0.40 ug/L1
1,3-Dichloropropane ND 10/05/2022 10461.0 0.40 ug/L1
2,2-Dichloropropane ND 10/05/2022 10461.0 0.40 ug/L1
1,1-Dichloropropene ND 10/05/2022 10462.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 10/05/2022 10461.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 10/05/2022 10461.0 0.40 ug/L1
Diisopropyl ether (IPE)ND 10/05/2022 10461.0 0.40 ug/L1
Ethylbenzene ND 10/05/2022 10461.0 0.40 ug/L1
Hexachlorobutadiene ND 10/05/2022 10461.0 0.40 ug/L1
2-Hexanone ND 10/05/2022 1046102.0 ug/L1
Isopropylbenzene ND 10/05/2022 10461.0 0.40 ug/L1
p-Isopropyltoluene ND 10/05/2022 10461.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 10/05/2022 10461.0 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 47 of 66
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56114-001
56114 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
4-Methyl-2-pentanone ND 10/05/2022 1046102.0 ug/L1
Methylene chloride ND 10/05/2022 10461.0 0.40 ug/L1
Naphthalene ND 10/05/2022 10461.0 0.40 ug/L1
n-Propylbenzene ND 10/05/2022 10461.0 0.40 ug/L1
Styrene ND 10/05/2022 10461.0 0.41 ug/L1
1,1,1,2-Tetrachloroethane ND 10/05/2022 10461.0 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 10/05/2022 10461.0 0.40 ug/L1
Tetrachloroethene ND 10/05/2022 10461.0 0.40 ug/L1
Toluene ND 10/05/2022 10461.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10/05/2022 10461.0 0.42 ug/L1
1,2,3-Trichlorobenzene ND 10/05/2022 10461.0 0.40 ug/L1
1,2,4-Trichlorobenzene ND 10/05/2022 10461.0 0.40 ug/L1
1,1,1-Trichloroethane ND 10/05/2022 10461.0 0.40 ug/L1
1,1,2-Trichloroethane ND 10/05/2022 10461.0 0.40 ug/L1
Trichloroethene ND 10/05/2022 10461.0 0.40 ug/L1
Trichlorofluoromethane ND 10/05/2022 10461.0 0.40 ug/L1
1,2,3-Trichloropropane ND 10/05/2022 10461.0 0.40 ug/L1
1,2,4-Trimethylbenzene ND 10/05/2022 10461.0 0.40 ug/L1
1,3,5-Trimethylbenzene ND 10/05/2022 10461.0 0.40 ug/L1
Vinyl chloride ND 10/05/2022 10461.0 0.40 ug/L1
Xylenes (total)ND 10/05/2022 10461.0 0.40 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 93 70-130
1,2-Dichloroethane-d4 103 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 48 of 66
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56114-002
56114 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Acetone 76 10/05/2022 09367610060-1401
Benzene 59 10/05/2022 09361185070-1301
Bromobenzene 51 10/05/2022 09361035070-1301
Bromochloromethane 56 10/05/2022 09361115070-1301
Bromoform 52 10/05/2022 09361045070-1301
Bromomethane (Methyl bromide)66 10/05/2022 0936N1315070-1301
2-Butanone (MEK)86 10/05/2022 09368610070-1301
n-Butylbenzene 57 10/05/2022 09361145070-1301
sec-Butylbenzene 56 10/05/2022 09361135070-1301
tert-Butylbenzene 54 10/05/2022 09361095070-1301
Carbon tetrachloride 56 10/05/2022 09361135070-1301
Chlorobenzene 54 10/05/2022 09361075070-1301
Chloroethane 57 10/05/2022 09361145070-1301
Chloroform 55 10/05/2022 09361095070-1301
Chloromethane (Methyl chloride)54 10/05/2022 09361085060-1401
2-Chlorotoluene 55 10/05/2022 09361105070-1301
4-Chlorotoluene 52 10/05/2022 09361055070-1301
1,2-Dibromo-3-chloropropane (DBCP)50 10/05/2022 0936995070-1301
Dibromochloromethane 53 10/05/2022 09361075070-1301
1,2-Dibromoethane (EDB)53 10/05/2022 09361055070-1301
Dibromomethane (Methylene bromide)54 10/05/2022 09361095070-1301
trans-1,4-Dichloro-2-butene 45 10/05/2022 0936905070-1301
1,2-Dichlorobenzene 54 10/05/2022 09361075070-1301
1,3-Dichlorobenzene 54 10/05/2022 09361085070-1301
1,4-Dichlorobenzene 53 10/05/2022 09361065070-1301
Dichlorodifluoromethane 57 10/05/2022 09361145060-1401
1,1-Dichloroethane 58 10/05/2022 09361155070-1301
1,2-Dichloroethane 52 10/05/2022 09361055070-1301
1,1-Dichloroethene 58 10/05/2022 09361155070-1301
cis-1,2-Dichloroethene 58 10/05/2022 09361165070-1301
trans-1,2-Dichloroethene 58 10/05/2022 09361165070-1301
1,2-Dichloropropane 59 10/05/2022 09361175070-1301
1,3-Dichloropropane 55 10/05/2022 09361095070-1301
2,2-Dichloropropane 60 10/05/2022 09361205070-1301
1,1-Dichloropropene 55 10/05/2022 09361105070-1301
cis-1,3-Dichloropropene 57 10/05/2022 09361145070-1301
trans-1,3-Dichloropropene 53 10/05/2022 09361075070-1301
Diisopropyl ether (IPE)55 10/05/2022 09361095070-1301
Ethylbenzene 54 10/05/2022 09361075070-1301
Hexachlorobutadiene 55 10/05/2022 09361115060-1401
2-Hexanone 110 10/05/2022 093611510070-1301
Isopropylbenzene 56 10/05/2022 09361115070-1301
p-Isopropyltoluene 55 10/05/2022 09361115070-1301
Methyl tertiary butyl ether (MTBE)53 10/05/2022 09361075070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 49 of 66
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56114-002
56114 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
4-Methyl-2-pentanone 110 10/05/2022 093611010070-1301
Methylene chloride 60 10/05/2022 09361215070-1301
Naphthalene 48 10/05/2022 0936965070-1301
n-Propylbenzene 57 10/05/2022 09361145070-1301
Styrene 54 10/05/2022 09361095070-1301
1,1,1,2-Tetrachloroethane 51 10/05/2022 09361035070-1301
1,1,2,2-Tetrachloroethane 56 10/05/2022 09361125070-1301
Tetrachloroethene 56 10/05/2022 09361125070-1301
Toluene 55 10/05/2022 09361115070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 59 10/05/2022 09361175070-1301
1,2,3-Trichlorobenzene 49 10/05/2022 0936985070-1301
1,2,4-Trichlorobenzene 49 10/05/2022 0936975070-1301
1,1,1-Trichloroethane 54 10/05/2022 09361095070-1301
1,1,2-Trichloroethane 54 10/05/2022 09361085070-1301
Trichloroethene 55 10/05/2022 09361105070-1301
Trichlorofluoromethane 58 10/05/2022 09361155070-1301
1,2,3-Trichloropropane 54 10/05/2022 09361085070-1301
1,2,4-Trimethylbenzene 55 10/05/2022 09361115070-1301
1,3,5-Trimethylbenzene 56 10/05/2022 09361125070-1301
Vinyl chloride 62 10/05/2022 09361255070-1301
Xylenes (total)110 10/05/2022 093610610070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 105 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 50 of 66
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56308-001
56308 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 10/06/2022 2148205.0 ug/L1
Benzene ND 10/06/2022 21481.0 0.40 ug/L1
Bromobenzene ND 10/06/2022 21481.0 0.40 ug/L1
Bromochloromethane ND 10/06/2022 21481.0 0.40 ug/L1
Bromoform ND 10/06/2022 21481.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 10/06/2022 21482.0 0.40 ug/L1
2-Butanone (MEK)ND 10/06/2022 2148102.0 ug/L1
n-Butylbenzene ND 10/06/2022 21481.0 0.40 ug/L1
sec-Butylbenzene ND 10/06/2022 21481.0 0.40 ug/L1
tert-Butylbenzene ND 10/06/2022 21481.0 0.40 ug/L1
Carbon tetrachloride ND 10/06/2022 21481.0 0.40 ug/L1
Chlorobenzene ND 10/06/2022 21481.0 0.40 ug/L1
Chloroethane ND 10/06/2022 21482.0 0.40 ug/L1
Chloroform ND 10/06/2022 21481.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 10/06/2022 21481.0 0.50 ug/L1
2-Chlorotoluene ND 10/06/2022 21481.0 0.40 ug/L1
4-Chlorotoluene ND 10/06/2022 21481.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 10/06/2022 21481.0 0.40 ug/L1
Dibromochloromethane ND 10/06/2022 21481.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 10/06/2022 21481.0 0.40 ug/L1
Dibromomethane (Methylene bromide)ND 10/06/2022 21481.0 0.40 ug/L1
1,2-Dichlorobenzene ND 10/06/2022 21481.0 0.40 ug/L1
1,3-Dichlorobenzene ND 10/06/2022 21481.0 0.40 ug/L1
1,4-Dichlorobenzene ND 10/06/2022 21481.0 0.40 ug/L1
Dichlorodifluoromethane ND 10/06/2022 21482.0 0.60 ug/L1
1,1-Dichloroethane ND 10/06/2022 21481.0 0.40 ug/L1
1,2-Dichloroethane ND 10/06/2022 21481.0 0.40 ug/L1
1,1-Dichloroethene ND 10/06/2022 21481.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 10/06/2022 21481.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 10/06/2022 21481.0 0.40 ug/L1
1,2-Dichloropropane ND 10/06/2022 21481.0 0.40 ug/L1
1,3-Dichloropropane ND 10/06/2022 21481.0 0.40 ug/L1
2,2-Dichloropropane ND 10/06/2022 21481.0 0.40 ug/L1
1,1-Dichloropropene ND 10/06/2022 21482.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 10/06/2022 21481.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 10/06/2022 21481.0 0.40 ug/L1
Diisopropyl ether (IPE)ND 10/06/2022 21481.0 0.40 ug/L1
Ethylbenzene ND 10/06/2022 21481.0 0.40 ug/L1
Hexachlorobutadiene ND 10/06/2022 21481.0 0.40 ug/L1
2-Hexanone ND 10/06/2022 2148102.0 ug/L1
Isopropylbenzene ND 10/06/2022 21481.0 0.40 ug/L1
p-Isopropyltoluene ND 10/06/2022 21481.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 10/06/2022 21481.0 0.40 ug/L1
4-Methyl-2-pentanone ND 10/06/2022 2148102.0 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 51 of 66
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56308-001
56308 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Methylene chloride ND 10/06/2022 21481.0 0.40 ug/L1
Naphthalene ND 10/06/2022 21481.0 0.40 ug/L1
n-Propylbenzene ND 10/06/2022 21481.0 0.40 ug/L1
Styrene ND 10/06/2022 21481.0 0.41 ug/L1
1,1,1,2-Tetrachloroethane ND 10/06/2022 21481.0 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 10/06/2022 21481.0 0.40 ug/L1
Tetrachloroethene ND 10/06/2022 21481.0 0.40 ug/L1
Toluene ND 10/06/2022 21481.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10/06/2022 21481.0 0.42 ug/L1
1,2,3-Trichlorobenzene ND 10/06/2022 21481.0 0.40 ug/L1
1,2,4-Trichlorobenzene ND 10/06/2022 21481.0 0.40 ug/L1
1,1,1-Trichloroethane ND 10/06/2022 21481.0 0.40 ug/L1
1,1,2-Trichloroethane ND 10/06/2022 21481.0 0.40 ug/L1
Trichloroethene ND 10/06/2022 21481.0 0.40 ug/L1
Trichlorofluoromethane ND 10/06/2022 21481.0 0.40 ug/L1
1,2,3-Trichloropropane ND 10/06/2022 21481.0 0.40 ug/L1
1,2,4-Trimethylbenzene ND 10/06/2022 21481.0 0.40 ug/L1
1,3,5-Trimethylbenzene ND 10/06/2022 21481.0 0.40 ug/L1
Vinyl chloride ND 10/06/2022 21481.0 0.40 ug/L1
Xylenes (total)ND 10/06/2022 21481.0 0.40 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 111 70-130
1,2-Dichloroethane-d4 99 70-130
Toluene-d8 105 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 52 of 66
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56308-002
56308 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Acetone 100 10/06/2022 185410510060-1401
Benzene 47 10/06/2022 1854955070-1301
Bromobenzene 47 10/06/2022 1854945070-1301
Bromochloromethane 44 10/06/2022 1854885070-1301
Bromoform 51 10/06/2022 18541025070-1301
Bromomethane (Methyl bromide)49 10/06/2022 1854985070-1301
2-Butanone (MEK)96 10/06/2022 18549610070-1301
n-Butylbenzene 50 10/06/2022 18541015070-1301
sec-Butylbenzene 47 10/06/2022 1854945070-1301
tert-Butylbenzene 46 10/06/2022 1854935070-1301
Carbon tetrachloride 49 10/06/2022 1854995070-1301
Chlorobenzene 48 10/06/2022 1854955070-1301
Chloroethane 40 10/06/2022 1854805070-1301
Chloroform 46 10/06/2022 1854925070-1301
Chloromethane (Methyl chloride)48 10/06/2022 1854955060-1401
2-Chlorotoluene 45 10/06/2022 1854915070-1301
4-Chlorotoluene 48 10/06/2022 1854965070-1301
1,2-Dibromo-3-chloropropane (DBCP)44 10/06/2022 1854895070-1301
Dibromochloromethane 46 10/06/2022 1854925070-1301
1,2-Dibromoethane (EDB)46 10/06/2022 1854925070-1301
Dibromomethane (Methylene bromide)46 10/06/2022 1854925070-1301
1,2-Dichlorobenzene 46 10/06/2022 1854915070-1301
1,3-Dichlorobenzene 48 10/06/2022 1854955070-1301
1,4-Dichlorobenzene 47 10/06/2022 1854935070-1301
Dichlorodifluoromethane 45 10/06/2022 1854915060-1401
1,1-Dichloroethane 47 10/06/2022 1854955070-1301
1,2-Dichloroethane 45 10/06/2022 1854905070-1301
1,1-Dichloroethene 52 10/06/2022 18541035070-1301
cis-1,2-Dichloroethene 46 10/06/2022 1854915070-1301
trans-1,2-Dichloroethene 47 10/06/2022 1854945070-1301
1,2-Dichloropropane 46 10/06/2022 1854925070-1301
1,3-Dichloropropane 47 10/06/2022 1854935070-1301
2,2-Dichloropropane 50 10/06/2022 18541005070-1301
1,1-Dichloropropene 49 10/06/2022 1854985070-1301
cis-1,3-Dichloropropene 52 10/06/2022 18541035070-1301
trans-1,3-Dichloropropene 50 10/06/2022 1854995070-1301
Diisopropyl ether (IPE)44 10/06/2022 1854875070-1301
Ethylbenzene 49 10/06/2022 1854985070-1301
Hexachlorobutadiene 49 10/06/2022 1854995060-1401
2-Hexanone 110 10/06/2022 185410510070-1301
Isopropylbenzene 48 10/06/2022 1854965070-1301
p-Isopropyltoluene 47 10/06/2022 1854945070-1301
Methyl tertiary butyl ether (MTBE)42 10/06/2022 1854845070-1301
4-Methyl-2-pentanone 96 10/06/2022 18549610070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 53 of 66
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56308-002
56308 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Methylene chloride 46 10/06/2022 1854925070-1301
Naphthalene 44 10/06/2022 1854895070-1301
n-Propylbenzene 51 10/06/2022 18541015070-1301
Styrene 51 10/06/2022 18541025070-1301
1,1,1,2-Tetrachloroethane 44 10/06/2022 1854895070-1301
1,1,2,2-Tetrachloroethane 44 10/06/2022 1854885070-1301
Tetrachloroethene 50 10/06/2022 18541005070-1301
Toluene 48 10/06/2022 1854965070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 50 10/06/2022 18541015070-1301
1,2,3-Trichlorobenzene 45 10/06/2022 1854905070-1301
1,2,4-Trichlorobenzene 45 10/06/2022 1854905070-1301
1,1,1-Trichloroethane 45 10/06/2022 1854915070-1301
1,1,2-Trichloroethane 45 10/06/2022 1854905070-1301
Trichloroethene 48 10/06/2022 1854975070-1301
Trichlorofluoromethane 51 10/06/2022 18541015070-1301
1,2,3-Trichloropropane 45 10/06/2022 1854905070-1301
1,2,4-Trimethylbenzene 47 10/06/2022 1854955070-1301
1,3,5-Trimethylbenzene 47 10/06/2022 1854935070-1301
Vinyl chloride 45 10/06/2022 1854905070-1301
Xylenes (total)96 10/06/2022 18549610070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 92 70-130
Toluene-d8 96 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 54 of 66
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:XI30005-010MS
56308 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Acetone 920 10/07/2022 051092100060-140ND10
Benzene 1600 10/07/2022 051010950070-130100010
Bromobenzene 530 10/07/2022 051010650070-130ND10
Bromochloromethane 510 10/07/2022 051010150070-130ND10
Bromoform 420 10/07/2022 05108450070-130ND10
Bromomethane (Methyl bromide)440 10/07/2022 05108850070-130ND10
2-Butanone (MEK)930 10/07/2022 051093100070-130ND10
n-Butylbenzene 640 10/07/2022 051012250070-1303310
sec-Butylbenzene 580 10/07/2022 051011450070-1301410
tert-Butylbenzene 570 10/07/2022 051011350070-130ND10
Carbon tetrachloride 590 10/07/2022 051011850070-130ND10
Chlorobenzene 530 10/07/2022 051010650070-130ND10
Chloroethane 640 10/07/2022 051012950070-130ND10
Chloroform 530 10/07/2022 051010650070-130ND10
Chloromethane (Methyl chloride)540 10/07/2022 051010750060-140ND10
2-Chlorotoluene 620 10/07/2022 051012550070-130ND10
4-Chlorotoluene 540 10/07/2022 051010850070-130ND10
1,2-Dibromo-3-chloropropane (DBCP)520 10/07/2022 051010450070-130ND10
Dibromochloromethane 450 10/07/2022 05108950070-130ND10
1,2-Dibromoethane (EDB)500 10/07/2022 051010050070-130ND10
Dibromomethane (Methylene bromide)520 10/07/2022 051010450070-130ND10
1,2-Dichlorobenzene 540 10/07/2022 051010750070-130ND10
1,3-Dichlorobenzene 530 10/07/2022 051010650070-130ND10
1,4-Dichlorobenzene 520 10/07/2022 051010450070-130ND10
Dichlorodifluoromethane 460 10/07/2022 05109350060-140ND10
1,1-Dichloroethane 530 10/07/2022 051010750070-130ND10
1,2-Dichloroethane 520 10/07/2022 051010450070-130ND10
1,1-Dichloroethene 510 10/07/2022 051010250070-130ND10
cis-1,2-Dichloroethene 510 10/07/2022 051010350070-130ND10
trans-1,2-Dichloroethene 510 10/07/2022 051010250070-130ND10
1,2-Dichloropropane 520 10/07/2022 051010350070-130ND10
1,3-Dichloropropane 510 10/07/2022 051010250070-130ND10
2,2-Dichloropropane 530 10/07/2022 051010650070-130ND10
1,1-Dichloropropene 570 10/07/2022 051011450070-130ND10
cis-1,3-Dichloropropene 550 10/07/2022 051011050070-130ND10
trans-1,3-Dichloropropene 520 10/07/2022 051010450070-130ND10
Diisopropyl ether (IPE)510 10/07/2022 051010150070-130ND10
Ethylbenzene 1200 10/07/2022 051011650070-13062010
Hexachlorobutadiene 530 10/07/2022 051010650060-140ND10
2-Hexanone 1100 10/07/2022 0510111100070-130ND10
Isopropylbenzene 650 10/07/2022 051011250070-1308710
p-Isopropyltoluene 570 10/07/2022 051011150070-1301210
Methyl tertiary butyl ether (MTBE)470 10/07/2022 05109050070-1302310
4-Methyl-2-pentanone 1100 10/07/2022 0510106100070-130ND10
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 55 of 66
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:XI30005-010MS
56308 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Methylene chloride 470 10/07/2022 05109450070-130ND10
Naphthalene 850 10/07/2022 051011050070-13030010
n-Propylbenzene 820 10/07/2022 051011850070-13023010
Styrene 560 10/07/2022 051011250070-130ND10
1,1,1,2-Tetrachloroethane 530 10/07/2022 051010550070-130ND10
1,1,2,2-Tetrachloroethane 510 10/07/2022 051010150070-130ND10
Tetrachloroethene 560 10/07/2022 051011350070-130ND10
Toluene 670 10/07/2022 051011050070-13011010
1,1,2-Trichloro-1,2,2-Trifluoroethane 600 10/07/2022 051012150070-130ND10
1,2,3-Trichlorobenzene 500 10/07/2022 051010150070-130ND10
1,2,4-Trichlorobenzene 500 10/07/2022 051010050070-130ND10
1,1,1-Trichloroethane 560 10/07/2022 051011150070-130ND10
1,1,2-Trichloroethane 510 10/07/2022 051010150070-130ND10
Trichloroethene 550 10/07/2022 051011150070-130ND10
Trichlorofluoromethane 590 10/07/2022 051011950070-130ND10
1,2,3-Trichloropropane 510 10/07/2022 051010250070-130ND10
1,2,4-Trimethylbenzene 1100 10/07/2022 051011450070-13056010
1,3,5-Trimethylbenzene 860 10/07/2022 051011350070-13029010
Vinyl chloride 500 10/07/2022 051010050070-130ND10
Xylenes (total)1500 10/07/2022 0510110100070-13041010
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 113 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 56 of 66
Volatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Sample ID:XI30005-010MD
56308 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Acetone 970 10/07/2022 053397100060-1404.5 20ND10
Benzene 1600 10/07/2022 053310650070-1301.2 20100010
Bromobenzene 560 10/07/2022 053311250070-1305.2 20ND10
Bromochloromethane 500 10/07/2022 053310150070-1300.21 20ND10
Bromoform 440 10/07/2022 05338950070-1305.7 20ND10
Bromomethane (Methyl bromide)450 10/07/2022 05338950070-1301.1 20ND10
2-Butanone (MEK)990 10/07/2022 053399100070-1306.5 20ND10
n-Butylbenzene 660 10/07/2022 053312550070-1301.9 203310
sec-Butylbenzene 590 10/07/2022 053311650070-1301.9 201410
tert-Butylbenzene 580 10/07/2022 053311650070-1302.9 20ND10
Carbon tetrachloride 580 10/07/2022 053311650070-1301.9 20ND10
Chlorobenzene 550 10/07/2022 053310950070-1302.9 20ND10
Chloroethane 560 10/07/2022 053311250070-13014 20ND10
Chloroform 530 10/07/2022 053310550070-1301.3 20ND10
Chloromethane (Methyl chloride)480 10/07/2022 05339550060-14012 20ND10
2-Chlorotoluene 650 10/07/2022 0533N13150070-1304.6 20ND10
4-Chlorotoluene 570 10/07/2022 053311450070-1305.4 20ND10
1,2-Dibromo-3-chloropropane (DBCP)520 10/07/2022 053310550070-1301.2 20ND10
Dibromochloromethane 470 10/07/2022 05339450070-1305.8 20ND10
1,2-Dibromoethane (EDB)520 10/07/2022 053310550070-1304.7 20ND10
Dibromomethane (Methylene bromide)540 10/07/2022 053310750070-1303.2 20ND10
1,2-Dichlorobenzene 550 10/07/2022 053311050070-1302.4 20ND10
1,3-Dichlorobenzene 550 10/07/2022 053311050070-1304.1 20ND10
1,4-Dichlorobenzene 540 10/07/2022 053310850070-1303.3 20ND10
Dichlorodifluoromethane 440 10/07/2022 05338750060-1406.4 20ND10
1,1-Dichloroethane 530 10/07/2022 053310550070-1301.1 20ND10
1,2-Dichloroethane 530 10/07/2022 053310650070-1301.4 20ND10
1,1-Dichloroethene 510 10/07/2022 053310250070-1300.72 20ND10
cis-1,2-Dichloroethene 510 10/07/2022 053310150070-1301.6 20ND10
trans-1,2-Dichloroethene 500 10/07/2022 053310050070-1302.2 20ND10
1,2-Dichloropropane 530 10/07/2022 053310650070-1302.3 20ND10
1,3-Dichloropropane 530 10/07/2022 053310750070-1304.6 20ND10
2,2-Dichloropropane 540 10/07/2022 053310850070-1301.3 20ND10
1,1-Dichloropropene 570 10/07/2022 053311450070-1300.17 20ND10
cis-1,3-Dichloropropene 560 10/07/2022 053311250070-1301.5 20ND10
trans-1,3-Dichloropropene 540 10/07/2022 053310850070-1304.2 20ND10
Diisopropyl ether (IPE)500 10/07/2022 053310050070-1301.1 20ND10
Ethylbenzene 1200 10/07/2022 053311850070-1300.64 2062010
Hexachlorobutadiene 550 10/07/2022 053311150060-1403.8 20ND10
2-Hexanone 1200 10/07/2022 0533119100070-1306.6 20ND10
Isopropylbenzene 660 10/07/2022 053311550070-1302.1 208710
p-Isopropyltoluene 580 10/07/2022 053311450070-1302.3 201210
Methyl tertiary butyl ether (MTBE)480 10/07/2022 05339050070-1300.050 202310
4-Methyl-2-pentanone 1100 10/07/2022 0533110100070-1304.3 20ND10
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 57 of 66
Volatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Sample ID:XI30005-010MD
56308 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Methylene chloride 460 10/07/2022 05339250070-1301.9 20ND10
Naphthalene 840 10/07/2022 053310750070-1301.4 2030010
n-Propylbenzene 850 10/07/2022 053312450070-1303.8 2023010
Styrene 570 10/07/2022 053311550070-1302.9 20ND10
1,1,1,2-Tetrachloroethane 540 10/07/2022 053310750070-1302.0 20ND10
1,1,2,2-Tetrachloroethane 540 10/07/2022 053310750070-1305.7 20ND10
Tetrachloroethene 580 10/07/2022 053311750070-1303.2 20ND10
Toluene 690 10/07/2022 053311450070-1302.9 2011010
1,1,2-Trichloro-1,2,2-Trifluoroethane 570 10/07/2022 053311350070-1306.5 20ND10
1,2,3-Trichlorobenzene 510 10/07/2022 053310350070-1302.0 20ND10
1,2,4-Trichlorobenzene 500 10/07/2022 053310050070-1300.41 20ND10
1,1,1-Trichloroethane 540 10/07/2022 053310850070-1303.2 20ND10
1,1,2-Trichloroethane 520 10/07/2022 053310450070-1302.6 20ND10
Trichloroethene 560 10/07/2022 053311150070-1300.40 20ND10
Trichlorofluoromethane 570 10/07/2022 053311450070-1304.5 20ND10
1,2,3-Trichloropropane 540 10/07/2022 053310850070-1305.5 20ND10
1,2,4-Trimethylbenzene 1100 10/07/2022 053311650070-1300.59 2056010
1,3,5-Trimethylbenzene 880 10/07/2022 053311850070-1302.5 2029010
Vinyl chloride 440 10/07/2022 05338950070-13012 20ND10
Xylenes (total)1500 10/07/2022 0533113100070-1302.0 2041010
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 112 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 111 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56315-001
56315 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Benzene ND 10/06/2022 22391.0 0.40 ug/L1
Ethylbenzene ND 10/06/2022 22391.0 0.40 ug/L1
n-Propylbenzene ND 10/06/2022 22391.0 0.40 ug/L1
Toluene ND 10/06/2022 22391.0 0.40 ug/L1
1,2,4-Trimethylbenzene ND 10/06/2022 22391.0 0.40 ug/L1
1,3,5-Trimethylbenzene ND 10/06/2022 22391.0 0.40 ug/L1
Xylenes (total)ND 10/06/2022 22391.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 99 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56315-002
56315 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Benzene 48 10/06/2022 2135975070-1301
Ethylbenzene 50 10/06/2022 2135995070-1301
n-Propylbenzene 52 10/06/2022 21351045070-1301
Toluene 48 10/06/2022 2135975070-1301
1,2,4-Trimethylbenzene 53 10/06/2022 21351055070-1301
1,3,5-Trimethylbenzene 52 10/06/2022 21351045070-1301
Xylenes (total)99 10/06/2022 21359910070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 97 70-130
Toluene-d8 95 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ59017-001
59017 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
trans-1,4-Dichloro-2-butene ND 11/02/2022 22592.0 0.50 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 96 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 97 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ59017-002
59017 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
trans-1,4-Dichloro-2-butene 55 11/02/2022 21551105070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
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Chain of Custody
and
Miscellaneous Documents
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PACE ANALYTICAL SERVICES, LLC

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC.
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Report of Analysis
Bunnell-Lammons Engineering,Inc.
6004 Ponders Court
Greenville,SC 29615
Attention:Andy Alexander
Project Name:MB Haynes SW
Lot Number:XI30096
Date Completed:10/31/2022
11/02/2022 1:33 PM
Approved and released by:
Project Manager II:Lucas Odom
Page 1 of 40
PACE ANALYTICAL SERVICES,LLC
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Bunnell-Lammons Engineering,Inc.
Lot Number:XI30096
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.Where
sampling is conducted by the client,results relate to the accuracy of the information provided,and as the
samples are received.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace")
Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to
the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory;however,the following analyses are currently not listed on our TNI
scope of accreditation:Drinking Water:VOC (excluding BTEX,MTBE,Naphthalene,&1,2-
dichloroethane)EPA 524.2,E.coli and Total coliforms SM 9223 B-2004,Solid Chemical Material:TOC
Walkley-Black,Biological Tissue:All,Non-Potable Water:SGT-HEM EPA 1664B,Silica EPA 200.7,
Boron,Calcium,Silicon,Strontium EPA 200.8,Bicarbonate,Carbonate,and Hydroxide Alkalinity SM 2320
B-2011,SM 9221 C E-2006 &SM 9222D-2006,Strontium SW-846 6010D,VOC SM 6200 B-2011,Fecal
Coliform Colilert-18.
If you have any questions regarding this report,please contact the Pace Project Manager listed on the
cover page.
VOCs by GC/MS
The matrix spike and matrix spike duplicate (MS/MSD)was not reported in BATCH:XQ56807 due to
analyst prep error.The CCV and LCS passed acceptance criteria,therefore the data has been reported
The laboratory control sample (LCS)and /or laboratory control sample duplicate (LCSD)for analytical
batch 56807 exceeded acceptance criteria for the following analytes:methyl acetate,cyclohexane,2-
hexanone and tetrahydrofuran.These analytes were biased high and were not detected in the samples
affected.
The laboratory control sample (LCS)for analytical batch 56747 exceeded acceptance criteria for the
following analytes:Acetone.These analytes were biased high and were not detected in the samples
affected.
Reanalysis of the following sample was performed outside of the analytical holding time:XI30096-004,
XI30096-005,XI30096-006,XI30096-007,XI30096-008,XI30096-009.Run 1 had been analyzed on an
instrument that was invalid for trans-1,4-dichloro-2-butene.Run 2 passes criteria for the compound.
Report run 2 for only Trans-1,4-Dichloro-2-Butene.
The laboratory control sample (LCS)for analytical batch 57160 exceeded acceptance criteria for 1,2,4-
Trichlorobenzene,1,2,3-Trichlorobenzene,Hexachlorobutadiene,and Naphthalene.These analytes were
biased high and were not detected in the samples affected
Page 2 of 40
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: XI30096

Sample Number Sample ID Matrix Date Sampled Date Received
001 09/28/2022 1040SMT-1 Aqueous 09/30/2022
002 09/28/2022 1015SMT-2 Aqueous 09/30/2022
003 09/28/2022 1000SMT-3 Aqueous 09/30/2022
004 09/28/2022 0950SMT-4 Aqueous 09/30/2022
005 09/28/2022 1130SMT-5 Aqueous 09/30/2022
006 09/28/2022 1145SMT-6 Aqueous 09/30/2022
007 09/28/2022 1405SMT-7 Aqueous 09/30/2022
008 09/28/2022 1410SMT-8 Aqueous 09/30/2022
009 09/28/2022Trip Blank Aqueous 09/30/2022
(9 samples)
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PACE ANALYTICAL SERVICES, LLC
Detection Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: XI30096

Sample Sample ID Matrix Parameter Method Result Q Units Page
003 SMT-3 Aqueous Chloroform 8260D 0.64 J ug/L 11
004 SMT-4 Aqueous Chloroform 8260D 0.72 J ug/L 13
006 SMT-6 Aqueous Benzene 8260D 0.56 J ug/L 17
006 SMT-6 Aqueous Toluene 8260D 0.68 J ug/L 18
007 SMT-7 Aqueous Benzene 8260D 6.0 H ug/L 19
007 SMT-7 Aqueous Ethylbenzene 8260D 2.0 H ug/L 19
007 SMT-7 Aqueous Naphthalene 8260D 0.75 HJL ug/L 20
007 SMT-7 Aqueous Toluene 8260D 7.2 H ug/L 20
007 SMT-7 Aqueous 1,2,4-Trimethylbenzene 8260D 1.5 H ug/L 20
007 SMT-7 Aqueous 1,3,5-Trimethylbenzene 8260D 0.50 HJ ug/L 20
007 SMT-7 Aqueous Xylenes (total)8260D 5.4 H ug/L 20
(11 detections)
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Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-1
XI30096-001
09/28/2022 1040
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 0511 JMM2 56747
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND L 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
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Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-1
XI30096-001
09/28/2022 1040
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 0511 JMM2 56747
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 103 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
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Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-2
XI30096-002
09/28/2022 1015
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 0536 JMM2 56747
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND L 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-2
XI30096-002
09/28/2022 1015
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 0536 JMM2 56747
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 103 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-3
XI30096-003
09/28/2022 1000
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 0601 JMM2 56747
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND L 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D 0.64 J 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND 1ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-3
XI30096-003
09/28/2022 1000
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 0601 JMM2 56747
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 94 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 104 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-4
XI30096-004
09/28/2022 0950
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1458 CDA 56807
2 5030B 8260D 1 10/30/2022 2026 JMM2 58673
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D 0.72 J 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND H 2ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-4
XI30096-004
09/28/2022 0950
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1458 CDA 56807
2 5030B 8260D 1 10/30/2022 2026 JMM2 58673
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND L 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 108 70-130 H 94 70-130
1,2-Dichloroethane-d4 127 70-130 H 95 70-130
Toluene-d8 107 70-130 H 103 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-5
XI30096-005
09/28/2022 1130
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1520 CDA 56807
2 5030B 8260D 1 10/30/2022 2049 JMM2 58673
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND H 2ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-5
XI30096-005
09/28/2022 1130
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1520 CDA 56807
2 5030B 8260D 1 10/30/2022 2049 JMM2 58673
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND L 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 110 70-130 H 91 70-130
1,2-Dichloroethane-d4 129 70-130 H 95 70-130
Toluene-d8 108 70-130 H 98 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-6
XI30096-006
09/28/2022 1145
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1543 CDA 56807
2 5030B 8260D 1 10/15/2022 0209 JM1 57160
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D 0.56 J 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND H 2ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-6
XI30096-006
09/28/2022 1145
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1543 CDA 56807
2 5030B 8260D 1 10/15/2022 0209 JM1 57160
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND L 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D 0.68 J 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 109 70-130 H 103 70-130
1,2-Dichloroethane-d4 127 70-130 H 94 70-130
Toluene-d8 105 70-130 H 106 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 16 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-7
XI30096-007
09/28/2022 1405
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 5030B 8260D 1 10/15/2022 0231 JM1 57160
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND H 2ug/L5.020
Benzene 71-43-2 8260D 6.0 H 2ug/L0.401.0
Bromobenzene 108-86-1 8260D ND H 2ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND H 2ug/L0.401.0
Bromoform 75-25-2 8260D ND H 2ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND HL 2ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND H 2ug/L2.010
n-Butylbenzene 104-51-8 8260D ND H 2ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND H 2ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND H 2ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND H 2ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND H 2ug/L0.401.0
Chloroethane 75-00-3 8260D ND HL 2ug/L0.402.0
Chloroform 67-66-3 8260D ND H 2ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND H 2ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND H 2ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND H 2ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND H 2ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND H 2ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND H 2ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND H 2ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND H 2ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND H 2ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND H 2ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND H 2ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND H 2ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND H 2ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND H 2ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND H 2ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND H 2ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND H 2ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND H 2ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND H 2ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND H 2ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND H 2ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND H 2ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND H 2ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND H 2ug/L0.401.0
Ethylbenzene 100-41-4 8260D 2.0 H 2ug/L0.401.0
Hexachlorobutadiene 87-68-3 8260D ND HL 2ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 17 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-7
XI30096-007
09/28/2022 1405
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 5030B 8260D 1 10/15/2022 0231 JM1 57160
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260D ND H 2ug/L2.010
Isopropylbenzene 98-82-8 8260D ND H 2ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND H 2ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND H 2ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND H 2ug/L2.010
Methylene chloride 75-09-2 8260D ND H 2ug/L0.401.0
Naphthalene 91-20-3 8260D 0.75 HJL 2ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND H 2ug/L0.401.0
Styrene 100-42-5 8260D ND H 2ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND H 2ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND H 2ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND H 2ug/L0.401.0
Toluene 108-88-3 8260D 7.2 H 2ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND H 2ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND HL 2ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND HL 2ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND H 2ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND H 2ug/L0.401.0
Trichloroethene 79-01-6 8260D ND H 2ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND H 2ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND H 2ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D 1.5 H 2ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D 0.50 HJ 2ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND HL 2ug/L0.401.0
Xylenes (total)1330-20-7 8260D 5.4 H 2ug/L0.401.0
AcceptanceRun 2
Surrogate Q % Recovery Limits
Bromofluorobenzene H 100 70-130
1,2-Dichloroethane-d4 H 96 70-130
Toluene-d8 H 102 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 18 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-8
XI30096-008
09/28/2022 1410
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1629 CDA 56807
2 5030B 8260D 1 10/15/2022 0254 JM1 57160
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND H 2ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 19 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
SMT-8
XI30096-008
09/28/2022 1410
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1629 CDA 56807
2 5030B 8260D 1 10/15/2022 0254 JM1 57160
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND L 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 117 70-130 H 105 70-130
1,2-Dichloroethane-d4 130 70-130 H 94 70-130
Toluene-d8 109 70-130 H 106 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 20 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
Trip Blank
XI30096-009
09/28/2022
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1327 CDA 56807
2 5030B 8260D 1 10/15/2022 0317 JM1 57160
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromobenzene 108-86-1 8260D ND 1ug/L0.401.0
Bromochloromethane 74-97-5 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
n-Butylbenzene 104-51-8 8260D ND 1ug/L0.401.0
sec-Butylbenzene 135-98-8 8260D ND 1ug/L0.401.0
tert-Butylbenzene 98-06-6 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
2-Chlorotoluene 95-49-8 8260D ND 1ug/L0.401.0
4-Chlorotoluene 106-43-4 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
Dibromomethane (Methylene bromide)74-95-3 8260D ND 1ug/L0.401.0
trans-1,4-Dichloro-2-butene 110-57-6 8260D ND H 2ug/L0.502.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
1,3-Dichloropropane 142-28-9 8260D ND 1ug/L0.401.0
2,2-Dichloropropane 594-20-7 8260D ND 1ug/L0.401.0
1,1-Dichloropropene 563-58-6 8260D ND 1ug/L0.402.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 21 of 40
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Bunnell-Lammons Engineering, Inc.
Trip Blank
XI30096-009
09/28/2022
09/30/2022
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 10/12/2022 1327 CDA 56807
2 5030B 8260D 1 10/15/2022 0317 JM1 57160
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexachlorobutadiene 87-68-3 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND L 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
p-Isopropyltoluene 99-87-6 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Naphthalene 91-20-3 8260D ND 1ug/L0.401.0
n-Propylbenzene 103-65-1 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,1,2-Tetrachloroethane 630-20-6 8260D ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,3-Trichlorobenzene 87-61-6 8260D ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
1,2,3-Trichloropropane 96-18-4 8260D ND 1ug/L0.401.0
1,2,4-Trimethylbenzene 95-63-6 8260D ND 1ug/L0.401.0
1,3,5-Trimethylbenzene 108-67-8 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 112 70-130 H 104 70-130
1,2-Dichloroethane-d4 128 70-130 H 95 70-130
Toluene-d8 106 70-130 H 106 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 22 of 40
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 23 of 40
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56747-001
56747 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 10/12/2022 0023205.0 ug/L1
Benzene ND 10/12/2022 00231.0 0.40 ug/L1
Bromobenzene ND 10/12/2022 00231.0 0.40 ug/L1
Bromochloromethane ND 10/12/2022 00231.0 0.40 ug/L1
Bromoform ND 10/12/2022 00231.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 10/12/2022 00232.0 0.40 ug/L1
2-Butanone (MEK)ND 10/12/2022 0023102.0 ug/L1
n-Butylbenzene ND 10/12/2022 00231.0 0.40 ug/L1
sec-Butylbenzene ND 10/12/2022 00231.0 0.40 ug/L1
tert-Butylbenzene ND 10/12/2022 00231.0 0.40 ug/L1
Carbon tetrachloride ND 10/12/2022 00231.0 0.40 ug/L1
Chlorobenzene ND 10/12/2022 00231.0 0.40 ug/L1
Chloroethane ND 10/12/2022 00232.0 0.40 ug/L1
Chloroform ND 10/12/2022 00231.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 10/12/2022 00231.0 0.50 ug/L1
2-Chlorotoluene ND 10/12/2022 00231.0 0.40 ug/L1
4-Chlorotoluene ND 10/12/2022 00231.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 10/12/2022 00231.0 0.40 ug/L1
Dibromochloromethane ND 10/12/2022 00231.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 10/12/2022 00231.0 0.40 ug/L1
Dibromomethane (Methylene bromide)ND 10/12/2022 00231.0 0.40 ug/L1
trans-1,4-Dichloro-2-butene ND 10/12/2022 00232.0 0.50 ug/L1
1,2-Dichlorobenzene ND 10/12/2022 00231.0 0.40 ug/L1
1,3-Dichlorobenzene ND 10/12/2022 00231.0 0.40 ug/L1
1,4-Dichlorobenzene ND 10/12/2022 00231.0 0.40 ug/L1
Dichlorodifluoromethane ND 10/12/2022 00232.0 0.60 ug/L1
1,1-Dichloroethane ND 10/12/2022 00231.0 0.40 ug/L1
1,2-Dichloroethane ND 10/12/2022 00231.0 0.40 ug/L1
1,1-Dichloroethene ND 10/12/2022 00231.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 10/12/2022 00231.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 10/12/2022 00231.0 0.40 ug/L1
1,2-Dichloropropane ND 10/12/2022 00231.0 0.40 ug/L1
1,3-Dichloropropane ND 10/12/2022 00231.0 0.40 ug/L1
2,2-Dichloropropane ND 10/12/2022 00231.0 0.40 ug/L1
1,1-Dichloropropene ND 10/12/2022 00232.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 10/12/2022 00231.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 10/12/2022 00231.0 0.40 ug/L1
Diisopropyl ether (IPE)ND 10/12/2022 00231.0 0.40 ug/L1
Ethylbenzene ND 10/12/2022 00231.0 0.40 ug/L1
Hexachlorobutadiene ND 10/12/2022 00231.0 0.40 ug/L1
2-Hexanone ND 10/12/2022 0023102.0 ug/L1
Isopropylbenzene ND 10/12/2022 00231.0 0.40 ug/L1
p-Isopropyltoluene ND 10/12/2022 00231.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 10/12/2022 00231.0 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 24 of 40
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56747-001
56747 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
4-Methyl-2-pentanone ND 10/12/2022 0023102.0 ug/L1
Methylene chloride ND 10/12/2022 00231.0 0.40 ug/L1
Naphthalene ND 10/12/2022 00231.0 0.40 ug/L1
n-Propylbenzene ND 10/12/2022 00231.0 0.40 ug/L1
Styrene ND 10/12/2022 00231.0 0.41 ug/L1
1,1,1,2-Tetrachloroethane ND 10/12/2022 00231.0 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 10/12/2022 00231.0 0.40 ug/L1
Tetrachloroethene ND 10/12/2022 00231.0 0.40 ug/L1
Toluene ND 10/12/2022 00231.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10/12/2022 00231.0 0.42 ug/L1
1,2,3-Trichlorobenzene ND 10/12/2022 00231.0 0.40 ug/L1
1,2,4-Trichlorobenzene ND 10/12/2022 00231.0 0.40 ug/L1
1,1,1-Trichloroethane ND 10/12/2022 00231.0 0.40 ug/L1
1,1,2-Trichloroethane ND 10/12/2022 00231.0 0.40 ug/L1
Trichloroethene ND 10/12/2022 00231.0 0.40 ug/L1
Trichlorofluoromethane ND 10/12/2022 00231.0 0.40 ug/L1
1,2,3-Trichloropropane ND 10/12/2022 00231.0 0.40 ug/L1
1,2,4-Trimethylbenzene ND 10/12/2022 00231.0 0.40 ug/L1
1,3,5-Trimethylbenzene ND 10/12/2022 00231.0 0.40 ug/L1
Vinyl chloride ND 10/12/2022 00231.0 0.40 ug/L1
Xylenes (total)ND 10/12/2022 00231.0 0.40 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 91 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 25 of 40
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56747-002
56747 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Acetone 170 10/11/2022 2227N16810060-1401
Benzene 44 10/11/2022 2227875070-1301
Bromobenzene 48 10/11/2022 2227965070-1301
Bromochloromethane 45 10/11/2022 2227905070-1301
Bromoform 47 10/11/2022 2227945070-1301
Bromomethane (Methyl bromide)52 10/11/2022 22271045070-1301
2-Butanone (MEK)120 10/11/2022 222711810070-1301
n-Butylbenzene 51 10/11/2022 22271035070-1301
sec-Butylbenzene 52 10/11/2022 22271045070-1301
tert-Butylbenzene 51 10/11/2022 22271035070-1301
Carbon tetrachloride 43 10/11/2022 2227875070-1301
Chlorobenzene 46 10/11/2022 2227915070-1301
Chloroethane 43 10/11/2022 2227865070-1301
Chloroform 40 10/11/2022 2227795070-1301
Chloromethane (Methyl chloride)42 10/11/2022 2227845060-1401
2-Chlorotoluene 48 10/11/2022 2227965070-1301
4-Chlorotoluene 50 10/11/2022 22271005070-1301
1,2-Dibromo-3-chloropropane (DBCP)49 10/11/2022 2227995070-1301
Dibromochloromethane 47 10/11/2022 2227955070-1301
1,2-Dibromoethane (EDB)48 10/11/2022 2227965070-1301
Dibromomethane (Methylene bromide)45 10/11/2022 2227915070-1301
trans-1,4-Dichloro-2-butene 39 10/11/2022 2227785070-1301
1,2-Dichlorobenzene 47 10/11/2022 2227935070-1301
1,3-Dichlorobenzene 47 10/11/2022 2227945070-1301
1,4-Dichlorobenzene 45 10/11/2022 2227905070-1301
Dichlorodifluoromethane 52 10/11/2022 22271045060-1401
1,1-Dichloroethane 42 10/11/2022 2227855070-1301
1,2-Dichloroethane 44 10/11/2022 2227885070-1301
1,1-Dichloroethene 43 10/11/2022 2227855070-1301
cis-1,2-Dichloroethene 43 10/11/2022 2227855070-1301
trans-1,2-Dichloroethene 43 10/11/2022 2227865070-1301
1,2-Dichloropropane 44 10/11/2022 2227885070-1301
1,3-Dichloropropane 46 10/11/2022 2227925070-1301
2,2-Dichloropropane 43 10/11/2022 2227855070-1301
1,1-Dichloropropene 41 10/11/2022 2227815070-1301
cis-1,3-Dichloropropene 47 10/11/2022 2227935070-1301
trans-1,3-Dichloropropene 48 10/11/2022 2227955070-1301
Diisopropyl ether (IPE)47 10/11/2022 2227935070-1301
Ethylbenzene 49 10/11/2022 2227975070-1301
Hexachlorobutadiene 49 10/11/2022 2227975060-1401
2-Hexanone 100 10/11/2022 222710010070-1301
Isopropylbenzene 50 10/11/2022 22271015070-1301
p-Isopropyltoluene 53 10/11/2022 22271065070-1301
Methyl tertiary butyl ether (MTBE)45 10/11/2022 2227895070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 26 of 40
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56747-002
56747 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
4-Methyl-2-pentanone 97 10/11/2022 22279710070-1301
Methylene chloride 41 10/11/2022 2227825070-1301
Naphthalene 48 10/11/2022 2227965070-1301
n-Propylbenzene 50 10/11/2022 22271005070-1301
Styrene 51 10/11/2022 22271025070-1301
1,1,1,2-Tetrachloroethane 47 10/11/2022 2227945070-1301
1,1,2,2-Tetrachloroethane 46 10/11/2022 2227925070-1301
Tetrachloroethene 47 10/11/2022 2227955070-1301
Toluene 48 10/11/2022 2227965070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 43 10/11/2022 2227865070-1301
1,2,3-Trichlorobenzene 51 10/11/2022 22271035070-1301
1,2,4-Trichlorobenzene 51 10/11/2022 22271025070-1301
1,1,1-Trichloroethane 43 10/11/2022 2227875070-1301
1,1,2-Trichloroethane 46 10/11/2022 2227925070-1301
Trichloroethene 45 10/11/2022 2227905070-1301
Trichlorofluoromethane 46 10/11/2022 2227935070-1301
1,2,3-Trichloropropane 49 10/11/2022 2227985070-1301
1,2,4-Trimethylbenzene 53 10/11/2022 22271055070-1301
1,3,5-Trimethylbenzene 52 10/11/2022 22271055070-1301
Vinyl chloride 45 10/11/2022 2227915070-1301
Xylenes (total)98 10/11/2022 22279810070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 88 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 27 of 40
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56807-001
56807 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 10/12/2022 1234205.0 ug/L1
Benzene ND 10/12/2022 12341.0 0.40 ug/L1
Bromobenzene ND 10/12/2022 12341.0 0.40 ug/L1
Bromochloromethane ND 10/12/2022 12341.0 0.40 ug/L1
Bromoform ND 10/12/2022 12341.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 10/12/2022 12342.0 0.40 ug/L1
2-Butanone (MEK)ND 10/12/2022 1234102.0 ug/L1
n-Butylbenzene ND 10/12/2022 12341.0 0.40 ug/L1
sec-Butylbenzene ND 10/12/2022 12341.0 0.40 ug/L1
tert-Butylbenzene ND 10/12/2022 12341.0 0.40 ug/L1
Carbon tetrachloride ND 10/12/2022 12341.0 0.40 ug/L1
Chlorobenzene ND 10/12/2022 12341.0 0.40 ug/L1
Chloroethane ND 10/12/2022 12342.0 0.40 ug/L1
Chloroform ND 10/12/2022 12341.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 10/12/2022 12341.0 0.50 ug/L1
2-Chlorotoluene ND 10/12/2022 12341.0 0.40 ug/L1
4-Chlorotoluene ND 10/12/2022 12341.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 10/12/2022 12341.0 0.40 ug/L1
Dibromochloromethane ND 10/12/2022 12341.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 10/12/2022 12341.0 0.40 ug/L1
Dibromomethane (Methylene bromide)ND 10/12/2022 12341.0 0.40 ug/L1
1,2-Dichlorobenzene ND 10/12/2022 12341.0 0.40 ug/L1
1,3-Dichlorobenzene ND 10/12/2022 12341.0 0.40 ug/L1
1,4-Dichlorobenzene ND 10/12/2022 12341.0 0.40 ug/L1
Dichlorodifluoromethane ND 10/12/2022 12342.0 0.60 ug/L1
1,1-Dichloroethane ND 10/12/2022 12341.0 0.40 ug/L1
1,2-Dichloroethane ND 10/12/2022 12341.0 0.40 ug/L1
1,1-Dichloroethene ND 10/12/2022 12341.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 10/12/2022 12341.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 10/12/2022 12341.0 0.40 ug/L1
1,2-Dichloropropane ND 10/12/2022 12341.0 0.40 ug/L1
1,3-Dichloropropane ND 10/12/2022 12341.0 0.40 ug/L1
2,2-Dichloropropane ND 10/12/2022 12341.0 0.40 ug/L1
1,1-Dichloropropene ND 10/12/2022 12342.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 10/12/2022 12341.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 10/12/2022 12341.0 0.40 ug/L1
Diisopropyl ether (IPE)ND 10/12/2022 12341.0 0.40 ug/L1
Ethylbenzene ND 10/12/2022 12341.0 0.40 ug/L1
Hexachlorobutadiene ND 10/12/2022 12341.0 0.40 ug/L1
2-Hexanone ND 10/12/2022 1234102.0 ug/L1
Isopropylbenzene ND 10/12/2022 12341.0 0.40 ug/L1
p-Isopropyltoluene ND 10/12/2022 12341.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 10/12/2022 12341.0 0.40 ug/L1
4-Methyl-2-pentanone ND 10/12/2022 1234102.0 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 28 of 40
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ56807-001
56807 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Methylene chloride ND 10/12/2022 12341.0 0.40 ug/L1
Naphthalene ND 10/12/2022 12341.0 0.40 ug/L1
n-Propylbenzene ND 10/12/2022 12341.0 0.40 ug/L1
Styrene ND 10/12/2022 12341.0 0.41 ug/L1
1,1,1,2-Tetrachloroethane ND 10/12/2022 12341.0 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 10/12/2022 12341.0 0.40 ug/L1
Tetrachloroethene ND 10/12/2022 12341.0 0.40 ug/L1
Toluene ND 10/12/2022 12341.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10/12/2022 12341.0 0.42 ug/L1
1,2,3-Trichlorobenzene ND 10/12/2022 12341.0 0.40 ug/L1
1,2,4-Trichlorobenzene ND 10/12/2022 12341.0 0.40 ug/L1
1,1,1-Trichloroethane ND 10/12/2022 12341.0 0.40 ug/L1
1,1,2-Trichloroethane ND 10/12/2022 12341.0 0.40 ug/L1
Trichloroethene ND 10/12/2022 12341.0 0.40 ug/L1
Trichlorofluoromethane ND 10/12/2022 12341.0 0.40 ug/L1
1,2,3-Trichloropropane ND 10/12/2022 12341.0 0.40 ug/L1
1,2,4-Trimethylbenzene ND 10/12/2022 12341.0 0.40 ug/L1
1,3,5-Trimethylbenzene ND 10/12/2022 12341.0 0.40 ug/L1
Vinyl chloride ND 10/12/2022 12341.0 0.40 ug/L1
Xylenes (total)ND 10/12/2022 12341.0 0.40 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 127 70-130
Toluene-d8 109 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 29 of 40
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56807-002
56807 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Acetone 140 10/12/2022 092913810060-1401
Benzene 52 10/12/2022 09291045070-1301
Bromobenzene 49 10/12/2022 0929975070-1301
Bromochloromethane 46 10/12/2022 0929915070-1301
Bromoform 44 10/12/2022 0929885070-1301
Bromomethane (Methyl bromide)48 10/12/2022 0929965070-1301
2-Butanone (MEK)110 10/12/2022 092910810070-1301
n-Butylbenzene 60 10/12/2022 09291205070-1301
sec-Butylbenzene 54 10/12/2022 09291085070-1301
tert-Butylbenzene 52 10/12/2022 09291045070-1301
Carbon tetrachloride 58 10/12/2022 09291155070-1301
Chlorobenzene 48 10/12/2022 0929965070-1301
Chloroethane 47 10/12/2022 0929945070-1301
Chloroform 56 10/12/2022 09291135070-1301
Chloromethane (Methyl chloride)58 10/12/2022 09291165060-1401
2-Chlorotoluene 57 10/12/2022 09291145070-1301
4-Chlorotoluene 51 10/12/2022 09291035070-1301
1,2-Dibromo-3-chloropropane (DBCP)57 10/12/2022 09291145070-1301
Dibromochloromethane 46 10/12/2022 0929935070-1301
1,2-Dibromoethane (EDB)48 10/12/2022 0929975070-1301
Dibromomethane (Methylene bromide)51 10/12/2022 09291015070-1301
1,2-Dichlorobenzene 46 10/12/2022 0929935070-1301
1,3-Dichlorobenzene 48 10/12/2022 0929975070-1301
1,4-Dichlorobenzene 47 10/12/2022 0929945070-1301
Dichlorodifluoromethane 45 10/12/2022 0929905060-1401
1,1-Dichloroethane 61 10/12/2022 09291215070-1301
1,2-Dichloroethane 60 10/12/2022 09291205070-1301
1,1-Dichloroethene 51 10/12/2022 09291025070-1301
cis-1,2-Dichloroethene 50 10/12/2022 09291005070-1301
trans-1,2-Dichloroethene 50 10/12/2022 09291015070-1301
1,2-Dichloropropane 55 10/12/2022 09291095070-1301
1,3-Dichloropropane 54 10/12/2022 09291095070-1301
2,2-Dichloropropane 61 10/12/2022 09291225070-1301
1,1-Dichloropropene 61 10/12/2022 09291225070-1301
cis-1,3-Dichloropropene 58 10/12/2022 09291155070-1301
trans-1,3-Dichloropropene 59 10/12/2022 09291185070-1301
Diisopropyl ether (IPE)50 10/12/2022 09291015070-1301
Ethylbenzene 50 10/12/2022 09291005070-1301
Hexachlorobutadiene 45 10/12/2022 0929905060-1401
2-Hexanone 150 10/12/2022 0929N14610070-1301
Isopropylbenzene 50 10/12/2022 09291005070-1301
p-Isopropyltoluene 52 10/12/2022 09291045070-1301
Methyl tertiary butyl ether (MTBE)49 10/12/2022 0929985070-1301
4-Methyl-2-pentanone 130 10/12/2022 092912810070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 30 of 40
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ56807-002
56807 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Methylene chloride 48 10/12/2022 0929965070-1301
Naphthalene 46 10/12/2022 0929935070-1301
n-Propylbenzene 62 10/12/2022 09291245070-1301
Styrene 51 10/12/2022 09291015070-1301
1,1,1,2-Tetrachloroethane 45 10/12/2022 0929915070-1301
1,1,2,2-Tetrachloroethane 55 10/12/2022 09291095070-1301
Tetrachloroethene 46 10/12/2022 0929915070-1301
Toluene 53 10/12/2022 09291055070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 58 10/12/2022 09291155070-1301
1,2,3-Trichlorobenzene 42 10/12/2022 0929845070-1301
1,2,4-Trichlorobenzene 42 10/12/2022 0929845070-1301
1,1,1-Trichloroethane 55 10/12/2022 09291095070-1301
1,1,2-Trichloroethane 49 10/12/2022 0929975070-1301
Trichloroethene 45 10/12/2022 0929905070-1301
Trichlorofluoromethane 55 10/12/2022 09291105070-1301
1,2,3-Trichloropropane 54 10/12/2022 09291085070-1301
1,2,4-Trimethylbenzene 55 10/12/2022 09291095070-1301
1,3,5-Trimethylbenzene 55 10/12/2022 09291105070-1301
Vinyl chloride 50 10/12/2022 09291005070-1301
Xylenes (total)97 10/12/2022 09299710070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 105 70-130
1,2-Dichloroethane-d4 117 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 31 of 40
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ57160-001
57160 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 10/15/2022 0003205.0 ug/L1
Benzene ND 10/15/2022 00031.0 0.40 ug/L1
Bromobenzene ND 10/15/2022 00031.0 0.40 ug/L1
Bromochloromethane ND 10/15/2022 00031.0 0.40 ug/L1
Bromoform ND 10/15/2022 00031.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 10/15/2022 00032.0 0.40 ug/L1
2-Butanone (MEK)ND 10/15/2022 0003102.0 ug/L1
n-Butylbenzene ND 10/15/2022 00031.0 0.40 ug/L1
sec-Butylbenzene ND 10/15/2022 00031.0 0.40 ug/L1
tert-Butylbenzene ND 10/15/2022 00031.0 0.40 ug/L1
Carbon tetrachloride ND 10/15/2022 00031.0 0.40 ug/L1
Chlorobenzene ND 10/15/2022 00031.0 0.40 ug/L1
Chloroethane ND 10/15/2022 00032.0 0.40 ug/L1
Chloroform ND 10/15/2022 00031.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 10/15/2022 00031.0 0.50 ug/L1
2-Chlorotoluene ND 10/15/2022 00031.0 0.40 ug/L1
4-Chlorotoluene ND 10/15/2022 00031.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 10/15/2022 00031.0 0.40 ug/L1
Dibromochloromethane ND 10/15/2022 00031.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 10/15/2022 00031.0 0.40 ug/L1
Dibromomethane (Methylene bromide)ND 10/15/2022 00031.0 0.40 ug/L1
trans-1,4-Dichloro-2-butene ND 10/15/2022 00032.0 0.50 ug/L1
1,2-Dichlorobenzene ND 10/15/2022 00031.0 0.40 ug/L1
1,3-Dichlorobenzene ND 10/15/2022 00031.0 0.40 ug/L1
1,4-Dichlorobenzene ND 10/15/2022 00031.0 0.40 ug/L1
Dichlorodifluoromethane ND 10/15/2022 00032.0 0.60 ug/L1
1,1-Dichloroethane ND 10/15/2022 00031.0 0.40 ug/L1
1,2-Dichloroethane ND 10/15/2022 00031.0 0.40 ug/L1
1,1-Dichloroethene ND 10/15/2022 00031.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 10/15/2022 00031.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 10/15/2022 00031.0 0.40 ug/L1
1,2-Dichloropropane ND 10/15/2022 00031.0 0.40 ug/L1
1,3-Dichloropropane ND 10/15/2022 00031.0 0.40 ug/L1
2,2-Dichloropropane ND 10/15/2022 00031.0 0.40 ug/L1
1,1-Dichloropropene ND 10/15/2022 00032.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 10/15/2022 00031.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 10/15/2022 00031.0 0.40 ug/L1
Diisopropyl ether (IPE)ND 10/15/2022 00031.0 0.40 ug/L1
Ethylbenzene ND 10/15/2022 00031.0 0.40 ug/L1
Hexachlorobutadiene 0.99 10/15/2022 0003J1.0 0.40 ug/L1
2-Hexanone ND 10/15/2022 0003102.0 ug/L1
Isopropylbenzene ND 10/15/2022 00031.0 0.40 ug/L1
p-Isopropyltoluene ND 10/15/2022 00031.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 10/15/2022 00031.0 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 32 of 40
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ57160-001
57160 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
4-Methyl-2-pentanone ND 10/15/2022 0003102.0 ug/L1
Methylene chloride ND 10/15/2022 00031.0 0.40 ug/L1
Naphthalene ND 10/15/2022 00031.0 0.40 ug/L1
n-Propylbenzene ND 10/15/2022 00031.0 0.40 ug/L1
Styrene ND 10/15/2022 00031.0 0.41 ug/L1
1,1,1,2-Tetrachloroethane ND 10/15/2022 00031.0 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 10/15/2022 00031.0 0.40 ug/L1
Tetrachloroethene ND 10/15/2022 00031.0 0.40 ug/L1
Toluene ND 10/15/2022 00031.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10/15/2022 00031.0 0.42 ug/L1
1,2,3-Trichlorobenzene ND 10/15/2022 00031.0 0.40 ug/L1
1,2,4-Trichlorobenzene ND 10/15/2022 00031.0 0.40 ug/L1
1,1,1-Trichloroethane ND 10/15/2022 00031.0 0.40 ug/L1
1,1,2-Trichloroethane ND 10/15/2022 00031.0 0.40 ug/L1
Trichloroethene ND 10/15/2022 00031.0 0.40 ug/L1
Trichlorofluoromethane ND 10/15/2022 00031.0 0.40 ug/L1
1,2,3-Trichloropropane ND 10/15/2022 00031.0 0.40 ug/L1
1,2,4-Trimethylbenzene ND 10/15/2022 00031.0 0.40 ug/L1
1,3,5-Trimethylbenzene ND 10/15/2022 00031.0 0.40 ug/L1
Vinyl chloride ND 10/15/2022 00031.0 0.40 ug/L1
Xylenes (total)ND 10/15/2022 00031.0 0.40 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 92 70-130
Toluene-d8 108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 33 of 40
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ57160-002
57160 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
Acetone 94 10/14/2022 23019410060-1401
Benzene 47 10/14/2022 2301955070-1301
Bromobenzene 58 10/14/2022 23011165070-1301
Bromochloromethane 47 10/14/2022 2301945070-1301
Bromoform 52 10/14/2022 23011035070-1301
Bromomethane (Methyl bromide)34 10/14/2022 2301N675070-1301
2-Butanone (MEK)95 10/14/2022 23019510070-1301
n-Butylbenzene 55 10/14/2022 23011095070-1301
sec-Butylbenzene 55 10/14/2022 23011095070-1301
tert-Butylbenzene 55 10/14/2022 23011105070-1301
Carbon tetrachloride 50 10/14/2022 2301995070-1301
Chlorobenzene 52 10/14/2022 23011045070-1301
Chloroethane 34 10/14/2022 2301N695070-1301
Chloroform 44 10/14/2022 2301885070-1301
Chloromethane (Methyl chloride)33 10/14/2022 2301665060-1401
2-Chlorotoluene 52 10/14/2022 23011045070-1301
4-Chlorotoluene 53 10/14/2022 23011055070-1301
1,2-Dibromo-3-chloropropane (DBCP)56 10/14/2022 23011135070-1301
Dibromochloromethane 49 10/14/2022 2301985070-1301
1,2-Dibromoethane (EDB)53 10/14/2022 23011075070-1301
Dibromomethane (Methylene bromide)49 10/14/2022 2301985070-1301
trans-1,4-Dichloro-2-butene 54 10/14/2022 23011085070-1301
1,2-Dichlorobenzene 54 10/14/2022 23011075070-1301
1,3-Dichlorobenzene 55 10/14/2022 23011105070-1301
1,4-Dichlorobenzene 53 10/14/2022 23011065070-1301
Dichlorodifluoromethane 42 10/14/2022 2301845060-1401
1,1-Dichloroethane 46 10/14/2022 2301935070-1301
1,2-Dichloroethane 45 10/14/2022 2301915070-1301
1,1-Dichloroethene 49 10/14/2022 2301995070-1301
cis-1,2-Dichloroethene 47 10/14/2022 2301945070-1301
trans-1,2-Dichloroethene 48 10/14/2022 2301955070-1301
1,2-Dichloropropane 50 10/14/2022 2301995070-1301
1,3-Dichloropropane 52 10/14/2022 23011035070-1301
2,2-Dichloropropane 48 10/14/2022 2301955070-1301
1,1-Dichloropropene 47 10/14/2022 2301935070-1301
cis-1,3-Dichloropropene 54 10/14/2022 23011075070-1301
trans-1,3-Dichloropropene 56 10/14/2022 23011125070-1301
Diisopropyl ether (IPE)50 10/14/2022 2301995070-1301
Ethylbenzene 53 10/14/2022 23011075070-1301
Hexachlorobutadiene 81 10/14/2022 2301N1625060-1401
2-Hexanone 120 10/14/2022 230111710070-1301
Isopropylbenzene 56 10/14/2022 23011115070-1301
p-Isopropyltoluene 56 10/14/2022 23011135070-1301
Methyl tertiary butyl ether (MTBE)49 10/14/2022 2301975070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 34 of 40
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ57160-002
57160 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
4-Methyl-2-pentanone 110 10/14/2022 230111010070-1301
Methylene chloride 47 10/14/2022 2301935070-1301
Naphthalene 71 10/14/2022 2301N1425070-1301
n-Propylbenzene 53 10/14/2022 23011075070-1301
Styrene 49 10/14/2022 2301985070-1301
1,1,1,2-Tetrachloroethane 55 10/14/2022 23011105070-1301
1,1,2,2-Tetrachloroethane 52 10/14/2022 23011045070-1301
Tetrachloroethene 59 10/14/2022 23011175070-1301
Toluene 51 10/14/2022 23011035070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 49 10/14/2022 2301985070-1301
1,2,3-Trichlorobenzene 79 10/14/2022 2301N1585070-1301
1,2,4-Trichlorobenzene 70 10/14/2022 2301N1415070-1301
1,1,1-Trichloroethane 47 10/14/2022 2301935070-1301
1,1,2-Trichloroethane 51 10/14/2022 23011025070-1301
Trichloroethene 56 10/14/2022 23011115070-1301
Trichlorofluoromethane 48 10/14/2022 2301955070-1301
1,2,3-Trichloropropane 50 10/14/2022 23011005070-1301
1,2,4-Trimethylbenzene 54 10/14/2022 23011085070-1301
1,3,5-Trimethylbenzene 54 10/14/2022 23011085070-1301
Vinyl chloride 30 10/14/2022 2301N595070-1301
Xylenes (total)110 10/14/2022 230110910070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 84 70-130
Toluene-d8 96 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 35 of 40
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:XQ58673-001
58673 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
trans-1,4-Dichloro-2-butene ND 10/30/2022 14112.0 0.50 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 91 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 36 of 40
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:XQ58673-002
58673 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ug/L)(ug/L)
trans-1,4-Dichloro-2-butene 44 10/30/2022 1306895070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 84 70-130
Toluene-d8 93 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 37 of 40
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 38 of 40
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 40 of 40

APPENDIX C
Historical Groundwater Summary Tables and Plots

Laboratory Analytical Results of MW-26 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
September 18, 2007 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
9/18/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/28/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1/18/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/9/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/6/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/18/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/3/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/16/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/21/2017 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/28/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/26/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/19/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/21/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-26 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-27 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
September 18, 2007 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
9/18/2007 340 ND ND ND 22 21 ND 88 2,300 ND ND 25 14 ND ND 60 2,870
10/28/2008 130 ND ND ND 16 7.1 ND 3.6 1,400 ND 1.2 7.8 9.2 2.0 1.6 33 1,612
1/13/2010 1,100 ND ND ND 64 35 10 1.0 2,700 20 8.1 51 22 5.7 5.1 87 4,109
2/10/2011 2,300 ND ND ND 51 52 34 ND 1,600 ND 28 ND 43 ND ND 140 4,248
2/7/2012 1,700 5.6 3.3 ND 33 34 33 2.2 260 17 24 26 22 6.0 4.2 53 2,223
2/20/2013 720 5.9 3.8 ND 30 18 34 ND 180 6.9 15 13 5.5 2.1 1.7 11 1,047
3/4/2014 420 5.4 5.1 ND 19 7.0 37 ND 250 ND 7.9 ND ND ND ND ND 751
3/26/2015 140 3.8 4.4 ND 20 2.6 20 ND 130 ND 3.9 ND ND ND ND ND 325
3/17/2016 61 ND 2.4 ND 11 6.9 5.0 ND 103 ND 1.8 ND 1.45 ND ND 4.19 197
3/21/2017 20.4 ND 2.77 ND 12.9 ND 2.74 ND 51.4 ND ND ND ND ND ND ND 90
3/27/2018 16 ND 3.1 ND 7.5 2.0 2.1 ND 48 0.73 0.66 0.53 0.63 NT ND 0.97 82
3/29/2019 13 ND 2.8 ND 2.6 3.6 1.7 ND 32 0.89 0.90 1.1 1.4 NT ND 2.9 63
3/26/2020 29 1.4 4.5 ND 3.4 3.8 3.3 ND 31 0.82 0.96 1.1 1.6 NT ND 5.6 86
3/19/2021 25 ND 4.3 ND 2.0 1.7 2.3 ND 24 1.40 0.74 0.93 0.81 NT ND 3.6 67
9/27/2021 5.6 ND 3.0 ND 0.88 ND 1.0 ND 19 ND ND 0.63 0.97 NT ND 1.4 32
3/21/2022 11 ND 3.6 ND 0.87 0.95 1.2 ND 17 ND 0.50 0.62 0.57 NT ND 2.3 39
9/27/2022 2 ND 3.3 ND 0.68 ND 0.4 ND 15 ND ND ND ND NT ND ND 21
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-27 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-28 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
September 18, 2007 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
9/18/2007 27,000 ND ND ND 1,000 3,200 ND ND 130,000 ND ND 39,000 2,500 710 680 16,000 220,090
10/28/2008 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
1/18/2010 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
2/9/2011 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
2/6/2012 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
2/20/2013 11,000 ND ND ND ND 3,300 ND ND ND ND ND 29,000 2,800 660 740 17,000 64,500
3/4/2014 17,000 ND ND ND ND 3,200 ND ND 740 ND 380 33,000 2,700 600 700 15,000 73,320
3/26/2015 19,000 ND ND ND 310 4,100 ND ND 11,000 ND 380 45,000 3,000 780 730 21,000 105,300
3/17/2016 8,490 92 ND ND ND 2,230 115 ND ND 444 430 18,800 2,500 715 710 10,000 44,526
3/22/2017 20,900 ND ND ND 382 5,020 226 ND 9,670 ND 778 3,960 5,160 1,370 1,490 25,600 74,556
3/28/2018 7,800 ND 99 ND ND 3,700 270 ND ND 640 1,000 23,000 6,200 NT 1,800 17,000 61,509
3/29/2019 4,400 ND ND ND ND 1,100 ND ND ND 180 190 12,000 1,200 NT 360 4,000 23,430
3/26/2020 91 130 23 ND ND 450 40 34 ND 88 180 1,300 1,000 NT 320 1,100 4,756
3/19/2021 86 51 14 ND ND 560 34 9.1 ND 120 140 1,400 860 NT 250 1,300 4,824
9/27/2021 5,000 ND ND ND ND 2,100 55 ND 56 320 150 12,000 1,200 NT 280 6,400 27,561
3/21/2022 10 ND 4.3 ND ND 350 23 ND ND 61 82 110 520 NT 140 860 2,160
9/27/2022 6,800 ND ND ND ND 2,300 48 ND 100 280 130 18,000 1,200 NT 280 8,700 37,838
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-28 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: TAO
Checked by: IAI
Laboratory Analytical Results of MW-29 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
September 18, 2007 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
9/18/2007 3,600 ND ND ND ND 1,200 ND ND 130 ND 140 10,000 1,100 330 310 6,900 23,710
10/28/2008 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
1/14/2010 9,900 ND ND ND ND 3,200 110 ND 890 560 300 33,000 2,300 630 610 17,000 68,500
2/10/2011 4,800 ND ND ND ND 2,600 ND ND 1,400 ND 290 22,000 2,500 550 600 15,000 49,740
2/7/2012 *FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP*
2/20/2013 5,100 ND ND ND ND 2,300 ND ND 130 ND 260 17,000 2,200 570 550 12,000 40,110
3/4/2014 5,700 ND ND ND ND 2,800 110 ND 310 ND 280 18,000 2,300 550 600 15,000 45,650
3/26/2015 5,100 25 ND ND 35 3,000 130 ND 680 630 370 12,000 2,900 790 740 14,000 40,400
3/17/2016 1,330 19.9 11.5 ND ND 2,260 97.7 5.87 27.3 424 279 6,980 2,990 820 662 10,500 26,407
3/22/2017 2,710 ND ND ND ND 2,000 93.4 ND 558 564 287 2,130 2,720 755 649 8,510 20,976
3/28/2018 1,600 ND ND ND ND 1,700 96.0 ND ND 420 260 2,200 3,300 NT 1,000 9,600 20,176
3/29/2019 610 ND ND ND ND 1,600 81 ND ND 380 230 460 2,800 NT 820 5,200 12,181
3/26/2020 540 ND 24 ND ND 1,500 120 42 ND 370 360 580 3,300 NT 910 3,000 10,746
3/19/2021 500 91 36 ND ND 1,300 130 28 ND 420 490 1,000 3,700 NT 1,100 2,200 10,995
9/27/2021 510 ND 16 ND ND 1,200 81 14 5.7 340 270 1,300 2,600 NT 680 2,400 9,417
3/21/2022 250 ND 12 ND ND 1,100 82 9.2 ND 320 260 190 2,400 NT 580 1,600 6,803
9/27/2022 600 ND 12 ND ND 1,500 85 8.4 4.2 330 280 1,300 2,500 NT 640 3,400 10,660
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-29 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-30 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
September 18, 2007 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
9/18/2007 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/28/2008 ND ND ND ND ND 110 ND ND 57 ND 65 370 460 84 140 750 2,036
1/14/2010 44 ND ND ND ND 7.9 ND ND 4.8 ND 2.3 63 17 4.1 5.3 51 199
2/9/2011 ND 3.6 1.8 ND ND ND ND 5.1 ND ND 2.7 ND 18 2.4 8.3 6.3 48
2/7/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/19/2013 ND ND ND ND ND 1.9 ND ND 1.8 ND 1.0 ND 11 3.5 4.9 24 48
3/3/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/25/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/16/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/21/2017 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/28/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/26/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/19/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/21/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-30 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-31 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
September 18, 2007 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
9/18/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/28/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1/13/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/9/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/6/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/19/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/3/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/25/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/16/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/21/2017 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/28/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/26/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/19/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/28/2021 ND ND ND ND ND ND ND ND ND 1.5 ND ND 0.87 NT ND ND 2.4
3/21/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-31 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-32 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
September 18, 2007 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
9/18/2007 580 33 33 ND 33 110 ND ND 3,300 ND 14 1,100 100 27 29 620 5,979
10/28/2008 1,200 28 28 ND 28 140 ND ND 2,400 ND ND 1,700 180 48 49 1,300 7,101
1/14/2010 220 ND ND ND ND 33 ND ND 1,100 ND ND 350 33 ND ND 260 1,996
2/10/2011 120 ND ND ND ND 72 ND ND 490 ND 12 300 130 34 37 550 1,745
2/7/2012 370 ND ND ND ND 180 8.5 ND 310 47 23 1,100 220 63 55 1,000 3,377
2/19/2013 110 3.3 1.5 ND 3.1 190 11 3.5 140 86 28 580 420 87 68 1,400 3,131
3/4/2014 2.0 ND ND ND ND 2.4 ND ND 1.3 ND ND ND 14 4.6 1.8 24 50
3/26/2015 1.4 ND ND ND ND 2.3 1.4 ND ND 5.9 ND ND 26 8.7 2.2 24 72
3/17/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/22/2017 ND ND ND ND ND ND ND ND ND ND ND ND 5.22 1.16 ND 5.2 11.5
3/27/2018 ND ND ND ND ND ND 0.79 ND ND 1.8 ND ND 10 NT ND 7.7 20.3
3/28/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/26/2020 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/19/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/21/2022 ND ND ND ND ND ND ND ND ND ND ND ND 0.85 NT ND ND 0.85
9/27/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-32 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-33 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
September 18, 2007 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
9/18/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/28/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1/13/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/9/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/7/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/19/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/3/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/25/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/16/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/21/2017 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/28/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/26/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/19/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/21/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-33 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-34 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
March 18, 2008 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
3/18/2008 82 ND ND ND ND 3.9 ND ND 4.7 ND ND 98 3.7 1.3 1.3 11 206
10/28/2008 ND ND ND ND ND ND ND ND 4.4 ND ND ND ND ND ND ND 4.4
1/13/2010 ND ND ND ND ND ND ND ND 11 ND ND ND ND ND ND ND 11
2/9/2011 ND ND ND ND ND ND ND ND 2.0 ND ND ND ND ND ND ND 2.0
2/7/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/19/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/3/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/25/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/17/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/21/2017 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/28/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/26/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/19/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/21/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-34 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-35 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
March 18, 2008 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
3/18/2008 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/28/2008 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
1/13/2010 *FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP*
2/9/2011 *FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP*
2/7/2012 *FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP*
2/19/2013 1,500 ND ND ND ND 1,400 ND ND 1,200 ND ND 9,900 2,300 ND ND 8,300 24,600
3/4/2014 3,100 ND ND ND ND 2,100 97 ND 1,500 360 250 10,000 2,400 610 710 12,000 33,127
3/26/2015 1,300 32 ND ND ND 1,600 100 ND 220 410 330 6,000 2,600 730 730 9,200 23,252
3/17/2016 1,610 22 13 ND ND 2,070 109 ND 98 672 341 3,380 2,720 795 702 9,200 21,732
3/22/2017 1,910 ND ND ND ND 1,740 ND ND ND ND 399 2,170 2,540 755 723 6,690 16,927
3/27/2018 1,200 ND ND ND ND 2,200 200 ND ND 640 660 1,500 4,100 NT 1300 7,300 19,100
3/29/2019 630 29 15 ND ND 960 86 10 33 430 270 420 1,800 NT 560 2,800 8,043
3/26/2020 1,200 ND 22 ND ND 710 100 18 23 340 310 300 1,400 NT 530 2,200 7,153
3/19/2021 1,400 51 21 ND ND 610 99 21 26 390 320 210 1,200 NT 520 1,400 6,268
9/28/2021 1,200 30 23 ND ND 560 75 21 20 290 200 140 660 NT 340 710 4,269
3/22/2022 920 24 13 ND ND 520 75 11 21 250 200 110 540 NT 260 540 3,484
9/27/2022 1,000 31 14 ND ND 620 83 12 23 300 230 110 560 NT 290 380 3,653
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-35 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-36 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
March 18, 2008 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
3/18/2008 ND ND ND ND 410 1,400 ND ND 22,000 ND ND 19,000 1,200 400 320 9,800 54,530
10/28/2008 12,000 ND ND ND 330 1400 ND ND 20,000 ND ND 20,000 1,500 420 420 10,000 66,070
1/14/2010 4,000 ND ND ND ND 780 ND ND 2,100 ND ND 10,000 950 260 330 6,600 25,020
2/10/2011 4,100 ND ND ND ND 880 ND ND 1,500 ND ND 10,000 850 220 250 5,800 23,600
2/8/2012 1,200 ND ND ND 10 230 9.2 67 200 45 24 2,800 350 110 110 2,500 7,655
2/20/2013 520 ND ND ND ND 340 ND ND ND ND ND 2,600 410 120 140 2,800 6,930
3/4/2014 300 ND ND ND ND 710 27 ND ND 130 71 5,400 740 200 210 5,000 12,788
3/26/2015 110 4.3 1.9 ND ND 660 16 28 4.7 120 42 3,500 670 210 120 4,600 10,087
3/17/2016 ND ND ND ND ND 29 1.8 4.9 ND 7.3 4.3 57 62 ND 37 203 407
3/21/2017 ND ND ND ND ND 555 ND ND ND ND 52.8 578 415 119 113 2,800 4,633
3/27/2018 ND ND ND ND ND 79 4.1 7.1 ND 9.1 10 33 67 NT 15 310 534
3/29/2019 ND 0.73 0.40 ND ND 15 1.8 ND ND 3.4 2.6 0.52 20 NT ND 37 81
3/26/2020 ND ND ND ND ND 2.5 ND ND ND 0.54 0.47 ND 2.1 NT 1.3 4.4 11
3/19/2021 ND ND ND ND ND 0.82 ND ND ND ND ND ND ND NT ND ND 0.82
9/27/2021 ND ND ND ND ND 390 22 10 ND 66 48 49 410 NT 81 1,500 2,576
3/21/2022 ND 1.20 0.60 ND ND 51 3.8 0.55 ND 7 11 0.89 19 NT 0.84 45 141
9/27/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-36 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-37 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
March 18, 2008 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
3/18/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
10/28/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1/18/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/9/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/6/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/18/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/4/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/25/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/17/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/21/2017 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/28/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/26/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/19/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/21/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-37 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-38 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
August 8, 2008 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
8/6/2008 ND ND ND ND ND ND ND ND 2.6 ND ND ND ND ND ND ND 2.6
10/28/2008 ND ND ND ND ND ND ND ND 5.3 ND ND ND ND ND ND ND 5.3
1/13/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/9/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/7/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/18/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/3/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/16/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/21/2017 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/28/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/26/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/19/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/21/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-38 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-39 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
August 8, 2008 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
8/6/2008 ND ND ND ND ND ND ND ND 2.0 ND ND ND ND ND ND ND 2.0
10/28/2008 ND ND ND ND ND ND ND ND 1.6 ND ND ND ND ND ND ND 1.6
1/13/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/9/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/6/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
2/18/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/4/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/25/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/17/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/21/2017 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/28/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/26/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/19/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/21/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
9/27/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-39 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-40 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
March 31, 2009 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
3/31/2009 1,100 ND ND ND ND 120 ND ND 680 ND 52 1,300 610 130 130 1,500 5,622
1/13/2010 *FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP*
2/9/2011 *FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP*
2/6/2012 *FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP**FP*
2/20/2013 33 7.0 4.0 ND ND 9.5 16 9.3 16 39 16 ND 93 23 32 39 337
3/4/2014 77 5.1 2.6 ND ND ND 13 ND 12 19 8.2 ND 43 2.5 3.2 4.5 190
3/26/2015 17 4.1 2.9 ND ND ND 6.3 1.1 4.7 8.1 2.6 ND 12 1.4 4.5 ND 65
3/17/2016 ND ND ND ND ND ND ND ND 1.7 ND ND ND 2.8 ND ND 7.0 11
3/21/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/27/2018 3.5 1.0 1.4 ND ND ND 3.2 ND 1.5 1.8 ND ND 0.53 NT ND 0.69 13.6
3/28/2019 1.4 1.4 1.1 ND ND ND 2.1 ND 0.75 1.8 0.57 ND 0.96 NT ND 1.4 11.5
3/26/2020 7.7 1.7 1.6 ND ND ND 2.5 ND 0.97 3.0 ND ND 1.0 NT ND 1.7 20.2
3/19/2021 7.8 1.1 1.0 ND ND ND 1.6 ND 0.86 4.2 ND ND 1.6 NT ND 1.2 19.4
9/28/2021 5.8 1.1 1.4 ND ND ND 2.2 ND 0.73 2.7 ND ND 0.94 NT ND 0.87 15.7
3/21/2022 5.8 1.3 1.3 ND ND ND 2.4 ND 0.76 4.3 ND ND 0.56 NT ND 0.43 16.9
9/27/2022 4.2 1.1 1.0 ND ND ND 2.5 ND 0.56 4.6 ND ND ND NT ND ND 14.0
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-40 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of MW-41 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
March 31, 2009 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
3/31/2009 1,100 ND ND ND 21 210 15 ND 1,000 ND 85 1,500 520 150 110 2,000 6,711
1/14/2010 1,100 ND ND ND ND 160 24 ND 270 ND 45 1,000 300 54 70 740 3,763
2/10/2011 430 ND ND ND ND 52 16 ND 330 ND 22 ND 16 ND ND 31 897
2/8/2012 130 1.1 2.0 ND 1.6 28 15 ND 91 12 14 ND 8.2 ND 4.6 12 320
2/20/2013 44 2.7 2.2 ND ND 23 13 ND 25 16 13 ND 16 ND 10 15 180
3/4/2014 26 ND 1.2 ND ND 3.0 2.5 ND 29 ND 1.6 ND ND ND ND ND 63
3/25/2015 12 ND 1.4 ND ND 1.6 1.1 ND 13 ND ND ND ND ND ND ND 29
3/17/2016 ND ND ND ND ND ND ND ND 1.68 ND ND ND ND ND ND ND 1.68
3/21/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
3/27/2018 ND ND ND ND ND ND ND ND 1.8 ND ND ND ND NT ND ND 1.8
3/28/2019 ND ND ND ND ND ND ND ND 0.40 ND ND ND ND NT ND ND 0.40
3/26/2020 ND ND ND ND ND ND ND ND 0.42 ND ND ND ND NT ND ND 0.42
3/19/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
3/21/2022 ND ND ND ND ND ND ND ND 0.46 ND ND ND ND NT ND ND 0.46
9/27/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
MW-41 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of TMW-42 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
March 31, 2009 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
3/31/2009 6,500 140 140 ND 140 660 ND ND 8,500 ND ND 4,600 570 150 130 2,900 24,430
1/14/2010 8,800 ND ND ND ND 1,200 ND ND 4,600 ND 150 9,600 700 130 180 4,400 29,760
2/10/2011 5,300 ND ND ND ND 600 ND ND 2,700 ND ND 2,700 250 ND ND 1,200 12,750
2/8/2012 480 ND ND ND ND 69 ND ND 110 ND ND 320 ND ND ND ND 979
2/20/2013 3,000 ND ND ND ND 960 ND ND 360 ND 120 4,800 530 100 150 3,100 13,120
3/4/2014 1,800 10 ND ND ND 770 74 ND 160 160 130 1,900 420 87 130 2,100 7,741
3/25/2015 730 7.2 5.1 ND 3.8 510 54 1.6 110 100 86 400 280 50 86 950 3,374
3/17/2016 145 9.2 6.0 ND ND 266 35 2.8 9.18 120 73 243 618 ND 341 1,890 3,758
3/21/2017 60.1 ND ND ND ND 125 ND ND ND ND ND 41.5 72.9 ND 27.9 203 530
3/27/2018 40 ND 4.4 ND ND 160 21 ND 15 55 38 90 130 NT 46 310 909
3/28/2019 5.4 2.3 2.5 32 ND 56 8.1 1.4 0.60 25 13 15 200 NT 2.3 320 684
3/26/2020 4.5 ND 2.5 ND ND 73 9.6 ND ND 27 19 14 180 NT 8.9 210 549
3/19/2021 2.7 ND 3.6 0.48 ND 71 12 1.1 1.1 24 24 8.5 140 NT 13 160 461
9/28/2021 2.4 ND 3.3 1.1 ND 14 5.4 1.1 2.4 3.9 9.4 0.68 5.4 NT ND 5.3 54
3/21/2022 1.7 ND 2.9 0.49 ND 7.8 4.1 ND 1.8 2.9 5.2 0.66 6.1 NT ND 4.7 38
9/27/2022 8.3 1.9 2.9 0.44 ND 29 6.9 0.81 6.3 5.0 14 1.0 14 NT ND 3.5 94
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
TMW-42 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of TMW-43 Groundwater Samples
Detected Petroleum Hydrocarbon Compounds Only
March 31, 2009 to September 27, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2L 1 70 70 70 70 600 70 25 20 6 70 600 400 NE 400 500 NE
3/31/2009 5,500 ND ND ND ND 1,400 ND ND 4,100 ND ND 12,000 2,200 530 560 11,000 37,290
1/14/2010 9,100 ND ND ND ND 2,800 ND ND 3,600 ND 280 23,000 2,200 500 560 14,000 56,040
2/10/2011 3,200 ND ND ND ND 1,700 ND ND 2,300 ND 570 7,400 3,500 750 1,000 8,500 28,920
2/8/2012 2,600 ND ND ND ND 1,400 69 ND 970 250 180 8,400 1,300 320 340 7,200 23,029
2/20/2013 1,000 ND ND ND ND 1,700 ND ND ND ND ND 8,900 1,700 400 450 9,800 23,950
3/4/2014 590 22 13 ND ND 1,900 140 ND 41 520 380 6,900 2,800 820 820 14,000 28,946
3/26/2015 380 33 17 ND ND 1,900 130 ND 140 420 390 4,500 2,500 870 880 12,000 24,160
3/17/2016 35 ND ND ND ND 1,450 106 ND ND 366 297 2,150 2,650 ND 713 9,860 17,627
3/21/2017 ND ND ND ND ND 1,030 ND ND ND ND 317 807 2,580 722 754 7,620 13,830
3/27/2018 ND ND ND ND ND 560 91 ND ND 190 310 140 2,300 NT 760 4,100 8,451
3/29/2019 ND 37 21 ND ND 390 71 ND ND 160 260 67 2,000 NT 630 2,800 6,436
3/26/2020 ND 49 9.4 ND ND 120 31 27 ND 64 110 8.0 850 NT 250 670 2,188
3/19/2021 ND ND 13 ND ND 170 48 9.3 ND 130 170 8.1 1,500 NT 400 880 3,328
9/28/2021 ND ND 17 ND ND 190 49 14 ND 160 200 25 1,600 NT 500 990 3,745
3/21/2022 ND 64 15 ND ND 84 35 9.3 ND 83 160 4.0 930 NT 310 360 2,054
9/27/2022 1.8 ND 19 0.63 ND 130 60 14 1.2 130 200 7.5 1,200 NT 430 350 2,544
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in mg/l (April 1, 2022).
NE = not established.
NT = not tested
ND = not detected at laboratory detection limit.
NS = not sampled.
FP = Free Product gasoline present; monitoring well was not sampled.
*FP* = A sheen of free product gasoline present but not measurable; monitoring well was not sampled.
12,000 = concentration exceeds NC2L Standard
TMW-43 of 2022B 5293 MB Haynes Historic Groundwater Results.xlsx
Prepared by: ACJ
Checked by: TAO
2,155
2,160
2,165
2,170
2,175
2,180
2,185
0
1
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(
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Total VOC Concentration ‐‐ MW‐26
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,102
2,103
2,104
2,105
2,106
2,107
2,108
0
500
1,000
1,500
2,000
2,500
3,000
3,500
4,000
4,500
5,000
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(
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Total VOC Concentration ‐‐ MW‐27
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,105
2,106
2,107
2,108
2,109
2,110
2,111
2,112
2,113
2,114
2,115
2,116
0
50,000
100,000
150,000
200,000
250,000
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(
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Total VOC Concentration ‐‐ MW‐28
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,100
2,102
2,104
2,106
2,108
2,110
2,112
0
10,000
20,000
30,000
40,000
50,000
60,000
70,000
80,000
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(
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Total VOC Concentration ‐‐ MW‐29
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,134
2,136
2,138
2,140
2,142
2,144
2,146
2,148
2,150
2,152
2,154
0
5,000
10,000
15,000
20,000
25,000
30,000
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(
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Total VOC Concentration ‐‐ MW‐30
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,116
2,118
2,120
2,122
2,124
2,126
2,128
2,130
2,132
2,134
2,136
0
1
2
3
4
5
6
7
8
9
10
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(
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Total VOC Concentration ‐‐ MW‐31
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,118
2,120
2,122
2,124
2,126
2,128
2,130
2,132
2,134
2,136
0
1,000
2,000
3,000
4,000
5,000
6,000
7,000
8,000
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(
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Total VOC Concentration ‐‐ MW‐32
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,114
2,116
2,118
2,120
2,122
2,124
2,126
2,128
2,130
2,132
0
1
2
3
4
5
6
7
8
9
10
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(
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Total VOC Concentration ‐‐ MW‐33
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,128
2,130
2,132
2,134
2,136
2,138
2,140
2,142
2,144
2,146
0
50
100
150
200
250
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(
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Total VOC Concentration ‐‐ MW‐34
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,112
2,114
2,116
2,118
2,120
2,122
2,124
2,126
2,128
2,130
0
5,000
10,000
15,000
20,000
25,000
30,000
35,000
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(
g/
L
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Total VOC Concentration ‐‐ MW‐35
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,103
2,104
2,105
2,106
2,107
0
10,000
20,000
30,000
40,000
50,000
60,000
70,000
El
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(
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Total VOC Concentration ‐‐ MW‐36
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,104
2,106
2,108
2,110
2,112
2,114
2,116
0
1
2
3
4
5
6
7
8
9
10
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(
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(
g/
L
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Total VOC Concentration ‐‐ MW‐37
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,090
2,092
2,094
2,096
2,098
2,100
2,102
2,104
0
1
2
3
4
5
6
7
8
9
10
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(
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Total VOC Concentration ‐‐ MW‐38
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,102
2,103
2,104
2,105
2,106
2,107
2,108
2,109
2,110
2,111
2,112
0
1
2
3
4
5
6
7
8
9
10
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(
f
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t

a
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s
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)
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t
a
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V
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C
o
n
c
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t
r
a
t
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n

(
g/
L
)
Total VOC Concentration ‐‐ MW‐39
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,098
2,100
2,102
2,104
2,106
2,108
2,110
2,112
2,114
2,116
0
1,000
2,000
3,000
4,000
5,000
6,000
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(
g/
L
)
Total VOC Concentration ‐‐ MW‐40
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,098
2,100
2,102
2,104
2,106
2,108
2,110
2,112
2,114
2,116
0
1,000
2,000
3,000
4,000
5,000
6,000
7,000
8,000
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f
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(
g/
L
)
Total VOC Concentration ‐‐ MW‐41
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,101
2,102
2,103
2,104
2,105
2,106
2,107
0
5,000
10,000
15,000
20,000
25,000
30,000
35,000
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f
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(
g/
L
)
Total VOC Concentration ‐‐ TMW‐42
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation
2,100
2,101
2,102
2,103
2,104
2,105
2,106
0
10,000
20,000
30,000
40,000
50,000
60,000
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(
g/
L
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Total VOC Concentration ‐‐ TMW‐43
Total VOC Concentration
Top Screen Elevation
Groundwater Elevation
Bottom Screen Elevation

APPENDIX D
Historical Surface Water Summary Tables and Plots
Laboratory Analytical Results of SMT-1 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
October 29, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
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D
E
T
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T
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D
NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
10/29/2008 2.3 ND ND ND 94 ND ND ND ND ND ND ND 96
1/15/2010 7.5 ND ND ND 51 ND ND ND ND ND ND 5.4 64
2/11/2011 4.9 ND ND ND 57 ND ND ND ND ND ND 4.4 66
2/9/2012 ND ND ND ND 17 ND ND ND ND ND ND ND 17
2/21/2013 1.5 ND ND ND 11 ND ND ND ND ND ND ND 13
3/5/2014 1.0 ND ND ND 7.6 ND ND ND ND ND ND ND 8.6
3/24/2015 ND ND ND ND 4.6 ND ND ND ND ND ND ND 4.6
3/18/2016 ND ND ND ND 3.2 ND ND ND ND ND ND ND 3.2
3/24/2017 ND ND ND ND 1.23 ND ND ND ND ND ND ND 1.2
3/29/2018 ND ND ND ND 0.91 ND ND ND ND NT ND ND 0.91
3/29/2019 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/27/2020 0.49 ND ND ND ND ND ND 0.57 ND NT ND 0.63 1.69
3/22/2021 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/29/2021 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/22/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-1 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-2 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
November 11, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
t
e

S
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D
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T
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T
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D
NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
11/11/2008 ND ND ND ND 70 ND ND ND ND ND ND ND 70
1/15/2010 3.2 ND ND ND 51 ND ND ND ND ND ND ND 54
2/11/2011 1.2 ND ND ND 38 ND ND ND ND ND ND ND 39
2/9/2012 ND ND ND ND 10 ND ND ND ND ND ND ND 10
2/21/2013 ND ND ND ND 7.9 ND ND ND ND ND ND ND 7.9
3/5/2014 ND ND ND ND 4.9 ND ND ND ND ND ND ND 4.9
3/24/2015 ND ND ND ND 3.1 ND ND ND ND ND ND ND 3.1
3/18/2016 ND ND ND ND 2.2 ND ND ND ND ND ND ND 2.2
3/24/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/29/2018 ND ND ND ND 0.74 ND ND ND ND NT ND ND 0.74
3/29/2019 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/27/2020 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/22/2021 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/29/2021 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/22/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-2 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-3 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
November 11, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
t
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S
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D
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NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
11/11/2008 ND ND ND ND 42 ND ND ND ND ND ND ND 42
1/15/2010 ND ND ND ND 35 ND ND ND ND ND ND ND 35
2/11/2011 ND ND ND ND 31 ND ND ND ND ND ND ND 31
2/9/2012 ND ND ND ND 6.5 ND ND ND ND ND ND ND 6.5
2/21/2013 ND ND ND ND 5.6 ND ND ND ND ND ND ND 5.6
3/5/2014 ND ND ND ND 4.0 ND ND ND ND ND ND ND 4.0
3/24/2015 ND ND ND ND 2.0 ND ND ND ND ND ND ND 2.0
3/18/2016 ND ND ND ND 1.1 ND ND ND ND ND ND ND 1.1
3/24/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/29/2018 ND ND ND ND 0.52 ND ND ND ND NT ND ND 0.52
3/29/2019 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/27/2020 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/22/2021 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/29/2021 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/22/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-3 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-4 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
November 11, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
t
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S
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NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
11/11/2008 ND ND ND ND 29 ND ND ND ND ND ND ND 29
1/15/2010 ND ND ND ND 32 ND ND ND ND ND ND ND 32
2/11/2011 ND ND ND ND 24 ND ND ND ND ND ND ND 24
2/9/2012 ND ND ND ND 5.2 ND ND ND ND ND ND ND 5.2
2/21/2013 ND ND ND ND 4.9 ND ND ND ND ND ND ND 4.9
3/5/2014 ND ND ND ND 3.3 ND ND ND ND ND ND ND 3.3
3/24/2015 ND ND ND ND 1.5 ND ND ND ND ND ND ND 1.5
3/18/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/29/2018 ND ND ND ND 0.47 ND ND ND ND NT ND ND 0.47
3/29/2019 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/27/2020 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/22/2021 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/29/2021 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/22/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
9/28/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-4 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-5 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
October 29, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
t
e

S
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D
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T
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T
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D
NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
10/29/2008 40 ND 2.4 ND 210 ND ND 21 3.3 1.5 1.2 16 295
1/15/2010 45 1.0 4.0 ND 82 ND ND 38 4.9 1.7 1.8 32 210
2/11/2011 32.0 1.1 3.4 ND 79 ND ND 28 5.9 3.1 2.0 25 180
2/9/2012 6.8 ND ND ND 27 ND ND 6.4 ND ND ND 5.9 46
2/21/2013 7.3 ND 2.0 ND 14 ND ND 9.2 1.8 1.1 ND 11 46
3/5/2014 5.0 ND 1.6 ND 11 ND ND 5.7 1.1 ND ND 7.7 32
3/24/2015 1.3 ND ND ND 8.4 ND ND ND ND ND ND 3.1 12.8
3/18/2016 ND ND ND ND 3.8 ND ND ND ND ND ND 3.7 7.5
3/24/2017 ND ND ND ND 2.42 ND ND 1.06 ND ND ND ND 3.48
3/29/2018 0.72 ND 0.45 ND 1.6 ND ND 0.83 0.49 NT ND 1.8 5.9
3/29/2019 1.1 ND 0.46 ND 0.54 ND ND 1.2 0.58 NT ND 1.2 5.1
3/27/2020 2.0 ND 1.2 ND ND 0.44 ND 2.3 1.4 NT ND 3.5 10.8
3/22/2021 1.7 ND 0.82 ND ND 0.42 ND 2.2 1.2 NT 0.46 2.8 9.6
9/29/2021 0.40 ND ND ND ND ND ND ND ND NT ND ND 0.40
3/22/2022 0.84 ND ND ND ND ND ND 1.1 0.43 NT ND 1.2 3.6
9/28/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-5 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-6 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
October 29, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
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S
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D
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T
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C
T
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D
NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
10/29/2008 84 2.2 5.9 ND 300 ND ND 43 7.7 2.5 2.5 34 482
1/15/2010 59 1.1 6.0 ND 76 ND ND 51 6.9 2.1 2.2 41 245
2/11/2011 52 1.4 6.7 ND 92 6.6 1.2 47 12.0 4.2 3.0 43 269
2/9/2012 16 ND 2.5 ND 30 ND ND 15 2.3 1.2 ND 14 81
2/21/2013 14 ND 3.9 ND 16 ND ND 17 3.4 1.6 1.2 19 76
3/5/2014 8.8 ND 3.0 ND 12 ND ND 9.4 2.2 ND ND 12 47
3/24/2015 4.2 ND 2.1 ND 11 ND ND 5.9 1.9 ND ND 9.7 35
3/18/2016 8.8 ND 2.8 ND 5.7 ND ND 10.3 2.2 ND ND 11.1 40.8
3/24/2017 2.35 ND 1.25 ND 2.86 ND ND 2.85 1.68 ND ND 5.90 16.89
3/29/2018 1.9 ND 1.2 ND 1.9 0.51 ND 2.3 1.5 NT 0.65 5.2 15.2
3/29/2019 2.7 ND 1.2 ND 0.67 0.52 ND 2.9 1.6 NT 0.57 4.1 14.3
3/27/2020 3.7 ND 2.1 ND ND 0.64 ND 4.3 2.7 NT 0.83 6.3 20.6
3/22/2021 3.6 ND 1.7 ND ND 0.66 ND 4.8 2.6 NT 0.93 6.0 20.3
9/29/2021 1.2 ND 0.50 ND ND ND ND 1.2 0.54 NT ND 1.6 5.0
3/22/2022 1.7 ND 0.70 ND ND 0.56 ND 2.3 0.88 NT ND 2.4 8.5
9/28/2022 0.6 ND ND ND ND ND ND 0.7 ND NT ND ND 1.2
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-6 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-7 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
October 29, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
10/29/2008 22 1.0 2.4 ND 78 ND ND 20 4.6 1.9 1.5 16 147
1/15/2010 34 ND 4.7 ND 43 ND ND 39 5.3 1.6 1.7 30 159
2/11/2011 28 ND 4.5 ND 47 ND ND 30 4.5 1.8 1.3 25 142
2/9/2012 12 ND 2.5 ND 20 ND ND 11 1.8 1.2 1.1 10 60
2/21/2013 16 ND 5.4 ND 14 ND ND 27 4.6 1.9 1.3 26 96
3/5/2014 15 ND 3.3 ND 13 ND ND 13 2.2 ND ND 13 60
3/24/2015 8.7 ND 2.7 ND 11 ND ND 8.7 1.9 ND ND 9.6 43
3/18/2016 17.3 ND 3.4 ND 5.2 ND ND 18.8 2.2 ND ND 12.5 59.5
3/24/2017 5.33 ND 1.33 ND 2.90 ND ND 4.71 1.45 ND ND 6.29 22.01
3/29/2018 4.6 ND 1.9 ND 1.9 0.58 ND 4.8 1.7 NT 0.62 6.2 22.3
3/29/2019 5.2 ND 1.9 ND 0.66 0.60 ND 5.4 2.1 NT 0.69 5.7 22.3
3/27/2020 5.9 ND 2.8 ND ND 0.75 0.48 6.5 3.0 NT 0.85 7.2 27.5
3/22/2021 6.4 ND 2.5 ND ND 0.73 0.45 7.9 3.2 NT 0.98 7.9 30.1
9/29/2021 3.5 ND 1.2 ND ND 0.50 ND 4.3 1.1 NT 0.40 3.9 14.9
3/22/2022 4.3 ND 1.7 ND ND 0.78 ND 5.8 2.0 NT 0.73 5.6 20.9
9/28/2022 6.0 ND 2.0 ND ND 0.75 ND 7.2 1.5 NT 0.50 5.4 23.4
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-7 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-8 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
October 29, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
10/29/2008 11 ND ND ND 20 ND ND 8.9 ND ND ND 3.4 43
1/15/2010 12 ND 2.2 ND 4.5 ND ND 17 1.8 ND ND 12 50
2/11/2011 25 ND 4.2 ND 13 ND ND 29 5.0 1.8 1.2 22 101
2/9/2012 49 ND 11 ND 23 ND ND 74 7.7 2.6 2.0 49 218
2/21/2013 25 ND 7.0 ND 6.7 ND ND 30 5.3 1.9 1.4 29 106
3/5/2014 19 ND 4.8 ND 4.0 ND ND 26 2.7 ND ND 19 76
3/24/2015 29 ND 7.5 ND 11 ND ND 42 6.5 2.2 1.8 31 131
3/18/2016 ND ND 1.3 ND ND ND ND ND ND ND ND ND 1.3
3/24/2017 8.84 ND 1.98 ND 1.41 ND ND 8.62 2.11 ND ND 7.11 30.07
3/29/2018 34 ND 9.6 ND 3.8 1.5 1.0 44 6.9 NT 1.9 29 132
3/29/2019 8.4 ND 3.2 ND ND 0.72 ND 11 2.7 NT 0.75 8.9 36
3/27/2020 5.6 ND 3.6 ND ND 0.64 0.44 8.4 3.4 NT 0.85 8.2 31.1
3/22/2021 14 ND 6.9 ND ND 1.2 0.82 29 7.0 NT 1.9 23 84
9/29/2021 ND ND ND ND ND ND ND ND ND NT ND ND ND
3/22/2022 ND ND 0.41 ND ND ND ND ND 0.74 NT ND 0.64 1.79
9/28/2022 ND ND ND ND ND ND ND ND ND NT ND ND ND
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-8 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-9 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
October 29, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
10/29/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND
1/15/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND
2/11/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND
2/9/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND
2/21/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/5/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/18/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/29/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/29/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/29/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/28/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Concentrations of Acetone and Chloroform detected in March 2018 are presumed laboratory error and are not shown on this table.
Concentration of Isopropylbenzene (0.41 J mg/l in SMT-8) detected in March 2018 but presumed transient and is not shown on this table.
Detected concentrations of chlorinated solvents (if detected) are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-9 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-10 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
October 29, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
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NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
10/29/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND
1/15/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND
2/11/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND
2/9/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND
2/21/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/5/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/18/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/29/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/29/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/29/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/28/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-10 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-11 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
December 8, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
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NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
12/8/2008 ND ND ND ND 14 ND ND ND ND ND ND ND 14
1/15/2010 ND ND ND ND 22 ND ND ND ND ND ND ND 22
2/11/2011 ND ND ND ND 17 ND ND ND ND ND ND ND 17
2/9/2012 ND ND ND ND 3.1 ND ND ND ND ND ND ND 3.1
2/21/2013 ND ND ND ND 3.4 ND ND ND ND ND ND ND 3.4
3/5/2014 ND ND ND ND 2.5 ND ND ND ND ND ND ND 2.5
3/24/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/18/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/29/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/29/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/29/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/28/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-11 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-12 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
December 8, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
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NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
12/8/2008 ND ND ND ND 2.2 ND ND ND ND ND ND ND 2.2
1/15/2010 ND ND ND ND 2.9 ND ND ND ND ND ND ND 2.9
2/11/2011 ND ND ND ND 3.2 ND ND ND ND ND ND ND 3.2
2/9/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND
2/21/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/5/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/18/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/29/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/29/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/29/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/28/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-12 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
Laboratory Analytical Results of SMT-13 Surface Water Samples
Detected Petroleum Hydrocarbon Compounds Only
December 8, 2008 to September 28, 2022
MB Haynes Corp.
Asheville, North Carolina
NCDEQ Incident Number 88705
BLE Project No. J22-5293-22B
Da
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D
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T
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D
NC2B 51 20,000 130 320 1,500 12 80 11 390 NE 215 670 NE
12/8/2008 ND ND ND ND 1.8 ND ND ND ND ND ND ND 1.8
1/15/2010 ND ND ND ND 2.6 ND ND ND ND ND ND ND 2.6
2/11/2011 ND ND ND ND 2.7 ND ND ND ND ND ND ND 2.7
2/9/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND
2/21/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/5/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/18/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/24/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND
3/29/2018 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/29/2019 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2020 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/29/2021 NS NS NS NS NS NS NS NS NS NS NS NS NS
3/22/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
9/28/2022 NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
VOC analyses performed by EPA Method 8260B or 8260D
Units in mg/l or parts per billion (ppb)
Detected concentrations of chlorinated solvents are related to the Andrex incident and are not included on this table.
NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In-Stream Target Values (Workbook Dated 7-26-2021)
NE = not established.
ND = not detected at laboratory detection limit.
NT = not tested.
NS = not sampled.
40 = concentration exceeds NC2B Standard
SMT-13 of 2022B 5293 MB Haynes Historic Surface Water Results.xlsx
Prepared by: ACJ
Checked by: TAO
0
20
40
60
80
100
120
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-1
0
10
20
30
40
50
60
70
80
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-2
0
5
10
15
20
25
30
35
40
45
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-3
0
5
10
15
20
25
30
35
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-4
0
50
100
150
200
250
300
350
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-5
0
100
200
300
400
500
600
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-6
0
20
40
60
80
100
120
140
160
180
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-7
0
50
100
150
200
250
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-8
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.0
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-9
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.0
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-10
0
5
10
15
20
25
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-11
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-12
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
8/
3
1
/
0
7
2/
2
9
/
0
8
8/
3
0
/
0
8
2/
2
8
/
0
9
8/
3
0
/
0
9
3/
1
/
1
0
8/
3
0
/
1
0
3/
1
/
1
1
8/
3
1
/
1
1
2/
2
9
/
1
2
8/
3
0
/
1
2
2/
2
8
/
1
3
8/
3
0
/
1
3
3/
1
/
1
4
8/
3
0
/
1
4
3/
1
/
1
5
8/
3
1
/
1
5
2/
2
9
/
1
6
8/
3
0
/
1
6
2/
2
8
/
1
7
8/
3
0
/
1
7
3/
1
/
1
8
8/
3
0
/
1
8
3/
1
/
1
9
8/
3
1
/
1
9
2/
2
9
/
2
0
8/
3
0
/
2
0
2/
2
8
/
2
1
8/
3
0
/
2
1
3/
1
/
2
2
8/
3
0
/
2
2
3/
1
/
2
3
8/
3
1
/
2
3
Co
n
c
e
n
t
r
a
t
i
o
n

mg/
L
Total VOC Concentration --SMT-13