26036_LSA and 20 Day Report_19980824

ENVIRONMENTAL INC.
August 24, 1998
North Carolina Department of Environment and Natural Resources
Division of Waste Management
UST Section
3800 Barrett Drive
Raleigh, North Carolina 27609
Reference: Limited Site Assessment and 20 Day Report
Uzzle Cadillac and Oldsmobile Facility
Facility ID No. 0-0 15 266
Dear Sir/Madam:
The following Limited Site Assessment (LSA) and 20 Day Report has been prepared for the
Uzzle Cadillac, Oldsmobile facility located on 3737 Chapel Hill Boulevard in Durham. This LSA
has'been prepared for the assessment of three former underground storage tank (UST)
excavations. The USTs were reportedly removed on June 6, 1991. The USTs that were removed
included a 2,000 gallon capacity tank that variously held diesel and gasoline, a 550 waste oil UST
and a 550 virgin oil UST.
Please review this report and contact the undersigned if you have any questions or comments.
Sincerely,
EMS Environmental Inc.
James Stahling
Senior Geologist
117 South Hoover Road ■ Durham, North Carolina 27703 • [phone] ■ FaxL{9ll}.596-0578.''
_

' Limited Site Assessment Report and 20 Day Report
Uzzle Cadillac-Oldsmobile-GMC Truck, Inc.
' Durham, North Carolina
August 24, 1998
Site Name: Uzzle Cadillac-Oldsmobile-GMC Truck, Inc.
Location: 3737 Chapel Hill Boulevard, Durham, North Carolina
GW Incident Number: Not assigned
' Facility ID Number: 0-015266
Risk Classification: Not assigned
Land Use Category: Proposed as Industrial Commercial
' UST Owner: Uzzle Cadillac-Olds-GMC Truck, Inc, c/o Brown and Bunch, 101
North Columbia Street, Chapel HiII, North Carolina, 27514,
(9I 9) 968-1 11 1
' Consultant: EMS Environmental, Inc., 117 South Hoover Road, Durham,
North Carolina 27703, [phone]
Date Release
' Discovered: Unknown
Estimated Quantity
Released: Unknown
Cause and Source of
Release: Diesel/gasoline UST system _ f ' `-j
Size and Contents of
' UST System: 1-2,000 gallon gasoline/diesel UST with associated dispenser.1 - :7
550 gallon waste oil UST, 1-550 gallon virgin oil UST.
Latitude/Longitude: 35058'15"/7905T8" rn
Prepared by: �� GARS/ Reviewed by: l J _
James M. Stahl , 1063 ti James J. Dodson, L.G.
' Senior Geoiogts F,r+ F4{p(',``' p�� Operations Manager
1
ENVIRONMENTAL INC.

TABLE OF CONTENTS
1.0 SITE HISTORY............................................................................................ 1
1.1 UST System Information
1.2 UST System Ownership
' 1.3 Abatement Activities
1.4 Previous Investigations
' 2.0 RISK CHARACTERIZATION..................................................................... 3
2.1 Limited Site Assessment Risk Classification and Land Use Form
3.0 RECEPTOR INFORMATION...................................................................... 7
3.1 Water Supply Wells
3.2 Public Water Supplies
' 3.3 Surface Water
3.4 Subsurface Structures
3.5 Land Use
' 3.6 Property Owners and Occupants
4.0 SITE INVESTIGATION................................................................................ g
' 4.1 Soil Boring Investigation
4.2 Soil Sampling
' 43 Monitoring Well Installation
4.4 Monitoring Well Sample Collection
4.5 Site Measurements
' 5.0 SITE GEOLOGY AND HYDROGEOLOGY............................................. 11
5.1 Site Geology
' 5.2 Site Hydrogeology
6.0 SAMPLING RESULTS .... ................. ......................... ............ 4".................. 12
' 6.1 Soil Quality
6,1.1 Virgin Oil UST Location
6,1.2 Waste Oil UST Location
6,13 Diesel/Gasoline UST Location
6.1.4 Monitoring Wells MW-4 and MW-6
6.2 Groundwater Quality
' 6.2.1 Virgin Oil UST Location, Monitoring Well MW-2
6.2.2 Waste ail UST Location, Monitoring Well MW-3
6.2.3 Diesel/Gasoline UST Location, Monitoring Well MW-5
' 6.2.4 Monitoring Well Locations MW-4 and MW-6
7.0 CONCLUSIONS AND RECOMMENDATIONS ....................................... 15
' 7.1 Site Rank
7.2 Soil Cleanup Levels
1

TABLE OF CONTENTS (CONTINUED)
T3 Virgin Oil UST Location
7.4 Waste Oil UST Location
T5 Diesel/gasoline UST Location
LIST OF TABLES
' Table 1. UST Information
Table 2, Monitoring Well Installation Specifications
Table 3. Depth to Groundwater and Groundwater Elevations
Table 4, Summary of Volatile Organic Concentrations (VOC) and Soil Analytical Results
Table 5. Groundwater Analytical Results
FIGURES
Figure 1. Site Vicinity Map
Figure 2. Site Plan
Figure 3. Land Use Map
Figure 4. Former Virgin Oil UST Excavation
' Figure 5. Former Waste Oil UST Excavation
Figure b. Former Gasoline and Diesel UST Excavation
' Figure 7, Groundwater Surface -July 14, 1998
LIST OF APPENDICES
' Appendix A: Soil Laboratory Analytical Results -UST Removal and Geoprobe Samples
Appendix B: Soil Analytical Results
1 Appendix C: Zoning Districts and Land Use Statement
Appendix D: Monitoring Well Logs and Well Completion Records
Appendix E: Groundwater Analytical Results
1

1.0 SITE HISTORY
' The site is an operating retail sales and repair facility for Cadillac and Oldsmobile automobiles.
The facility is located on a 4.75 acre lot on Route 15-501 in west Durham as shown on Figure 1.
Two buildings are located on the property. The main building consists of showroom and sales
' department, a service reception area, a body and paint shop and a service area. A smaller building
used for storage is located at the southeast property corner. These areas are shown in Figure 2.
I UST System Information
Three USTs were installed at the facility in 1969. The USTs included a 2,000 gallon capacity tank
' that variously held diesel and gasoline, a 550 waste oil UST and a 550 virgin oil UST. According
to a database from the North Carolina Environment, Health and Natural Resources, the USTs
were removed on June 13, 1991. Information listed by NCDENHR is attached in Table 1.
' An additional UST that stored gasoline and had a 10,000 capacity was installed on May 2, 1981
and removed on December 15, 1992. A closure report was submitted to the NCDENHR for the
' UST and the assessment of the former UST location is not a part of this investigation.
1.2 UST System Ownership
' The USTs were owned b Uzzle Cadillac-Oldsmobile-GMC Truck Inc. when the were
Y � Y
' removed. The business is currently owned and operated as Durham Oldsmobile -Cadillac, Inc.
13 Abatement Activities
No information was obtained during the investigation concerning the necessity or conductance of
abatement activities at the time of UST removal.
1.4 Previous Investigations
' Soil samples were collected from the excavations by Boswell Plumbing following the removal of
the USTs on June 13, 1991. One soil sample identified as sample 1 was collected from the diesel -
gasoline UST excavation and analyzed for Total Petroleum Hydrocarbons by Gas Chromatograph
' (TPH-GC). Soil samples were collected from the waste oil (sample 2) and virgin oil (sample 3)
UST excavations and analyzed for Total Petroleum Hydrocarbons by Infra Red (TPH-IR). The
chain -of -custody for the laboratory samples do not indicate the sample collection depth.
' The results of laboratory analysis reported a 27 milligram per kilogram (mg/Kg) concentration of
No. 2 fuel oil and a i 1 mg[Kg concentration of gasoline in sample 1. Samples 2 and 3 contained
TPH-IR concentrations of 27 and 920 mg/Kg, respectively. Copies of the analytical results are
attached in Appendix A.
1

' A monitoring well identified as MW-I was installed to investigate the groundwater quality
adjacent to the former 10,000 gallon gasoline UST, Petroleum hydrocarbon compounds from
' MW-I were not detected, however lead was detected and appeared to be naturally occurring.
A Geoprobe soil boring investigation was performed by Fluor Daniel GTI in November -December
' 1997. In the investigation, Geoprobe boreholes were advanced at the former locations of the
virgin ail UST (identified as LIST-2) and diesel/gasoline UST (UST-4 & 4A). The soil samples
were collected from each borehole at the respective depths of 4, 9.5 and 10 feet below ground
surface (BGS). Sample UST-2 was analyzed for Oil and Grease by EPA method 9071, Volatile
Organics by EPA method 8021 and TCLP metals by 1311. Of these analyses only Oil and Grease
was detected at a reported concentration of 46.6 mg/Kg and barium with a TCLP concentration
' 1.4 mg/L.
Samples UST-4 and 4A were analyzed for Total Petroleum Hydrocarbons by GC using methods
' 3550 and 5030. TPH was detected as gasoline in UST-4 and 4A in concentrations of 18.3 and
178 mg/Kg. TPH was detected as diesel fuel in UST-4 and 4A in concentrations of 17 and 14.6
mg/Kg.
1
2

2.0 RISK CHARACTERIZATION
2.1 Limited Site Assessment Risk Classification and Land Use Form
Part I-Groundwater/Surface waterNapor Impacts
1. Has The discharge or release contaminated any water supply well including any used for non -
drinking purposes?
No.
2. Is there a water supply well used for drinking water located within 1000 feet of the source area
of the discharge or release?
No.
3. Is a water supply well used for any purpose (e,g., irrigation, washing cars, industrial cooling
' water, filling swimming pools) located within 250 feet of the source area of the discharge or
release?
I
No.
4. Does groundwater within 500 feet of the source area of the discharge or release have the
potential for future use in that there is no other source of water supply other than the
groundwater?
No.
' 5, Do vapors from the discharge or release pose a threat of explosion because of the accumulation
of the vapors in a confined space or pose any other serious threat to public health, public safety or
the environment?
' No.
5. Are there any other factors that would cause the discharge or release to pose any immanent
danger to public health, public safety, or the environment?
' No
INTERMEDIATE RISK
7. Is a surface water body located within 500 feet of the discharge or release?
1
3

t
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
A stream was formerly located near the north property boundary. During construction of kt. 15-
501 the stream was enclosed within piping and runs along the north property boundary as shown
on Figure 2. This former stream is located approximately 180 feet north of the former
diesel/gasoline UST location. The former waste oil and virgin oil UST locations are present within
300 feet of the buried stream. This buried stream drains into an unnamed tributary of Sandy
Creek. A drainage ditch is located along the east property boundary. The virgin oil, waste oil and
diesel/gasoline UST locations are located approximately 400, 500 and 600 feet from this ditch.
If yes, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in I5A NCAC 2B .0200 by a factor of 10?
No. The buried stream has a classification of CNSW. Surface water standards that are applicable
to CNSW for samples collected from the site monitoring wells are listed on Table 5. As shown on
the table, two compounds, Iead and chromium, were detected in the wells that have CNSW
standards. Both lead and chromium were detected in concentrations at less than 4 times the
CNSW standards in well MW-5 installed adjacent to the dieseVgasoline UST location.
8. Is the source area of the discharge or release located within a designated wellhead protection
area as defined in 42 USC 300-h-7(e)?
No.
9. Is the discharge or release located in the Coastal Plain Physiographic Region as designated on a
map entitled "Geology of North Carolina" published by the Department in 1985?
No.
10. ❑❑ the levels of groundwater contamination for any contaminant exceed the gross
contamination levels established (see Table 7, NCDENR 1/98, Vol. I1, p. 60)?
No.
Based on the results of this questionnaire, it appears the site ranking is Low.
Part II -Land Use
Property Containing Source Area of Discharge of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more secondary residences (permanent or temporary)?
No.
2. Does the property contain a school, day care center, hospital, playground, park, recreation
4

area, church, nursing home, or other place of public assembly?
No.
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g,, manufacturing, utilities, industrial research and development, chemical/petroleum
bulk storage, etc.) enterprise, an inactive commercial or industrial enterprise, or is the land
undeveloped?
The property contains a commercial (automotive retail and service) facility.
4. Do children visit the property?
Yes. Children likely visit the property during business hours.
5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)?
Yes, the area located behind the service area and body shop if fenced with an industrial grade
chain link fence and locking gates.
6. Do pavement, buildings, or other structures cap the contaminated soil?
Yes. All of the former excavations and surrounding soils are capped with concrete paving.
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future.
It is likely the concrete paving will remain in place as long as the site remains an automotive retail
and service facility.
7. What is the zoning status of the property?
General Commercial District (GC}
8. Is the use of the property likely to change in the next twenty years?
One cannot forecast with any certainty the future use of the property within a twenty year time
period, however the property has been used as an automobile retail facility for 29 years and it a
reasonable assumption that the use will not change in the immediate future, This is further
supported by a statement of land use prepared by Charles Gordon Brown, an attorney for Uzzle
Cadillac. This statement is attached in Appendix C.
5

(EMS note -questions 9 and 10 are not included within the DWQ document)
Property SulloundirnS!Qurc?,� &ea !af Discharge or Rellea$e
The questions below pertain to the area within 1500 feet of the source area of the discharge or
release (excludes property containing source area of the release):
11. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?
Based on the 7.5 minute topographical map, a portion of the Royal Oak apartments is located
approximately 1,000 feet southeast from former location of the diesel fuel/gasoline UST. The
apartments are located uphill and likely hydraulically upgradient from the facility.
12. What is the distance from the source area of the release to the nearest school, day care center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?
A Kinder Care day care facility is located on University Drive, approximately 1,700 feet south of
the source area. This facility is also located uphill and upgradient of the facility. South Square, a
mall, is located approximately 1,100 feet west from the former location of the diesel fueVgasoline
UST.
13. What is the zoning status of properties in the surrounding area?
Various zoning classifications are used for the property located within 1,500 feet of the site.
These include General Commercial District (GC), Neighborhood Commercial District (NC),
Shopping Center District (SC}, Planned Density Residential (PDR), Transitional Office and
Institutional District (0I-1), General Office and Institutional District (0&1-2) and Multifamily
Residential District (RW-12). Maps and summaries of local zoning districts are attached in
Appendix B.
14. Briefly characterize the use and activities of the land in the surrounding area.
Commercial properties are located adjacent to the site boundaries. Car dealerships are located
west across Auto Drive; restaurants are located south of the site; a car wash, office building and
real estate company are situated east-southeast of the facility. Shopping centers, a car rental
facility and restaurants are located across Rt. 15-501 from the site. The land use of the
surrounding area is show in Figure 3.
Based on the Iocal land use, EMS recommends the Industrial/Commercial Maximum Soil
Contaminant Concentrations (MSCQ for the applicable cleanup levels at the site.
511

3.0 RECEPTOR INFORMATION
3,1 Water Supply Wells
A drive -by reconnaissance was performed to locate potable water wells within 1,500 feet of the
site. The closest potable well is located approximately 1,500 feet north of the site at the private
residence of Cary Pickett on 2814 Pickett Road. According to Mr. Pickett, the well is 125 feet
deep. The location of the well is shown on Figure 3.
3.2 Public Water Supplies
The site and vicinity is served by a municipal water supply. The source of the municipal water is
Lake Michie, located northeast of the site near Butner.
3.3 Surface Water
A surface water drainage ditch is located along the east property line between the site and the
' Durham Ritz Car Wash, The stream is channeled into a below ground culvert which runs parallel
to the access road that borders the north property boundary. Other than this stream and a pond
located across Rt. 15-50I no other surface water is present within 1,500 feet of the site. Surface
' water at the site appears to eventually discharge to an intermittent stream of Sandy Creek which
empties into New Hope Creek.
' 3.4 Subsurface Structures
Subsurface utilities include the following:
-Storm sewers
-Sanitary sewer
-Water line
-Electric line
-Natural gas line
No basements are located at the facility. Vapors would not likely pose a problem from a release of
waste oil or virgin oil as volatile organic compounds (VOCs) are not typically associated with
these petroleum hydrocarbons. Volatile organic compounds (VOCs) are typically associated with
gasoline and can also be detected in diesel fuel in minor levels. A VOC concentration of 16.3
parts per million (ppm) was detected at sample depth 4-5.5 feet in MW-5 installed adjacent to the
diesel/gasoline UST location. Sanitary and storm sewers are located near the former UST
location. No VOCs were detected by olfactory methods within the lines,
7

1 3.4 Land Use
The zoning of the property, GC, is used for a wide variety of commercial activities that among
others includes banks, business services, car washes, convenience stores, day care facilities, night
clubs, offices, hotels, retail stores, vehicle sales, drive-in theaters, schools, boarding houses, heavy
equipment sales, printing establishments and transmission towers.
The release site is covered with concrete paving and exposure to petroleum hydrocarbons in the
soil would only occur through the removal of the paving and excavating to the affected zone.
3.5 Property Owners and Occupants
■ Based on surface topography it appears migration of dissolved phase hydrocarbons would occur
downgradient (north) of the former UST locations. ❑owngradient migration in the shallow water
' table from the source area(s) could be intercepted by buried sanitary and/or storm sewers. If side
gradient migration occurred from the former dieseVgasoline UST location it would likely travel
under Auto Drive and Land Volkswagen. Land Volkswagen is owned by Harry Land and located
' on 3823 Chapel Hill Blvd.
E:l

4.0 SITE INVESTIGATION
4.1 Soil Boring Investigation
The former UST locations were evaluated on July 6-7, 1998 by the installation of soil borings and
monitoring wells by American Environmental Drilling Services (REDS). Five monitoring wells
were installed, however only three (MW-2, MW-3 and MW-5) were installed to evaluate the
former underground storage tank locations. Gravel was found to be present in the virgin oil UST
location, therefore the borings were advanced at locations adjacent to the former UST
excavations.
The remaining two monitoring wells (MW-4 and MW-6) were installed to evaluate potential
releases of hydraulic fluid for below ground vehicle lifts and were not part of this investigation.
Monitoring well MW-2 was installed adjacent to the virgin oil UST location, MW-3 was installed
adjacent to the waste oil UST location and MW-5 was installed adjacent to the diesel -gasoline
UST location. Well identification was started at MW-2 as a monitoring well MW-I is located on
the site from the previous investigation of 10,000 gasoline UST. Two additional wells identified
as MW-4 and MW-6 were installed at locations downgradient of the virgin oil and waste oil USTs
and service department. The wells were installed at the locations shown in Figure 2.
Initial drilling was conducted with an Ingersoll-Rand drilling rig (model T-300) using 4 1/4-inch
inner diameter hollow stem augers. Bedrock was encountered in the MW-2 boring location which
required the conversion to air rotary drilling. Remaining wells MW-3 through MW-6 were
installed using a 6-inch diameter roller cone bit, Soil samples were collected with a 2-foot long, 2"
outside diameter split spoon sampling device at approximate 5 foot sampling intervals. The drill
bit, drill rod and split spoon sampling device were cleaned between borings with a high pressure
steam cleaner.
4.2 Soil Sampling
' Soil samples were field scanned for volatile organic compounds (VOCs) with a photoionization
detector (PID) as a semi -quantitative indicator of the presence of petroleum hydrocarbons. Field
scanning was performed by placing the soil sample in a new resealable plastic bag and allowing
' the organic vapors to equilibrate in the headspace for a minimum of fifteen minutes. The PID
probe was then inserted into the bag and the highest VOC reading was obtained.
Soil laboratory analytical samples were collected to estimate the vertical extent of soil adsorbed
petroleum hydrocarbons. Samples were prepared from split spoon samples that were at shallowest
sample collection depth or were from above the estimated water table. The samples were
collected for laboratory analysis listed in the "Groundwater Section Guidelines for the
Investigation and Remediation of Soil and Groundwater, January 2, 1998" (North Carolina
Division of Water Quality).
0

All soil samples were placed in laboratory supplied sample containers and stored in coolers chilled
with ice. The samples were relinquished by overnight carrier to Toxikon located in Bedford
Massachusetts. Soil laboratory results are included in Appendix A.
4.3 Monitoring Well Installation
Following the completion of soil boring activity, boreholes MW-2 through MW-6 were converted
into monitoring wells. Monitoring wells were constructed utilizing 10 feet of 2-inch ID 0.010 inch
slotted PVC screen with 1-2 feet of schedule 40 PVC riser pipe, Medium grained filter sand was
added to the borehole and a bentonite pellet seal was added to the annulus above the sand. The
remainder of each borehole was grouted with cement and finished with a boltdown manhole and
cover. Well installation details are included with the boring logs and well completion records
(GW-1 form) in Appendix ❑. Well installation details are attached in Table 2.
4.4 Monitoring Well Sample Collection
Groundwater samples were collected from the monitoring wells on July 14, 1998. The monitoring
wells were purged a minimum of 3 well volumes before sample collection. Well purging was
performed using new nylon line and single use disposable polyethylene bailers. Samples were
poured into laboratory supplied sample containers, placed in chilled coolers and delivered by
overnight freight to Toxikon Corporation located in Bedford, Massachusetts.
Samples collected from MW-2 installed adjacent to the former virgin oil UST excavation were
' analyzed by EPA Method 625 expanded to include tentatively identified compounds (TIC) and
the Massachusetts Department of Environmental Protection Extractable Petroleum Hydrocarbons
' (MADEP EPH). Samples collected from MW-3 installed adjacent to the former waste oil UST
excavation include SM 621 OD, MADEP EPH, MADEP Volatile Petroleum Hydrocarbons
(VPH), EPA 625 with TICs and lead and chromium by 3030C. A sample was collected from
' MW-5 installed adjacent to the diesel -gasoline UST excavation and analyzed by EPA 601-602
expanded to include MTBE and IPE, ethylene dibromide by EPA method 504.2, MADEP EPH
and VPH, EPA 625 including TICS and lead and chromium by 3030C. Monitoring well MW-1
' installed hydraulically sidegradient was sampled for laboratory analysis by EPA 601-602 expanded
to include MTBE and IPE.
' 4.5 Site Measurements
The monitoring wells were gauged for depth to water on the date of sample collection with a
t Keck oil -water interface probe. Monitoring well elevations and placement were measured by EMS
personnel on July 15-16, 1998 utilizing a surveying level and rod, and measurement wheel. Well
elevations are included with fluid level measurements in Table 2.
10

5.0 SITE GEOLOGY AND HYDROGEOLOGY
5.1 Site Geology
The soil borings encountered clay, silt and sand that overlies siltstone. The clay is red -brown to
brown and is occasionally silty and sandy. The sands are clayey, grey and predominantly fine.
Siltstone was encountered at 10 feet BGS in MW-2 and MW-5.
5.2 Site Hydrogeology
Groundwater was encountered at depths that ranged from 2.2 feet BGS in MW-2 to 5.32 feet
BGS in MW-4. Groundwater is oriented towards the north and likely drains into the buried creek
Iocated at the north property boundary.

6.0 SAMPLING RESULTS
' 6.1 Soil Quality
Petroleum hydrocarbons were either not detected in the soil samples or were detected below
' DWQ Industrial/Commercial Maximum Soil Contaminant Concentrations (MSCC). Complete
analytical results are described below. Analytical results are attached in Table 4 and Appendix B.
6.1.1 Virgin Gil UST Location
A Geoprobe sample collected from 4 feet BGS in borehole UST-2 by Fluor Daniel GTI exhibited
an Oil and Grease concentration of46.6 mg/Kg, The DWQ action level for oil and grease in 250
mg/Kg.
A sample was collected from MW-2 for analysis by MADEP EPH and EPA 8270. Petroleum
hydrocarbons were detected by MADEP EPH analysis at the sample depth of 0, 5-1.5 feet below
ground surface (BGS). Petroleum hydrocarbons with the range of C9-C 18 were detected in a
concentration or 1 10 milligrams per kilogram (mg,/Kg) and C19-06 range with a concentration
of 13,000. The DWQ Industrial/Commercial Maximum Soil Contaminant Concentrations
(MSCC) for the C9-C18 range is 245,280 mg/Kg, The C19-C36 Industrial/Commercial range is
does not have an established MSCC. Volatile petroleum hydrocarbons (VPH) were detected in a
concentration of 510 mglKg for the C 11-C22 range. This is below the IndustriallCommercial
MSCC of 12,264 mg/Kg.
' 6.1.2 Waste nil UST Location
A sample was collected from the depth of 3.5-5 feet BGS from MW-3 and analyzed by EPA
' method 8080, lead and chromium by EPA method 3050, EPA method 8270, MADEP VPH and
EPH and EPA 8260 expanded to include IPE and MTBE. Lead and chromium were detected in
concentrations of 2.74 and 4.62 mg/Kg. These levels are below the DWQ MSCC of 270 and 27
' mg/Kg for lead and chromium, respectively. No compounds were detected for MADEP VPH,
EPH, EPA 8260 and EPA 8270. Holding times were exceeded for the EPH and 8270 analysis,
' 6.1.3 Diesel/Gasoline UST Location
MADEP VPH and EPH were not detected in a sample collected from MW-5 at 4-5.5 feet BGS.
' Xylenes (total p,m,o) were detected in a concentration of 0.0118 mg/Kg. This is below the MSCC
for xyienes of 5 mglKg.
' The detection of Oil and grease in Geoprobe samples UST4 and UST4A during the Fluor Daniel
GTI investigation and not in sample MW-5 (MADEP EPH-VPH) may represent the sample
collection depth in the Geoprobe boreholes. The oil and grease samples were likely collected
12

below the groundwater table and may actually represent groundwater impact and not soil impact.
6.1.4 Monitoring Wells MW-4 and MW-6
Soil samples were collected from MW-4 and MW-6 at the respective depths of 2-3 and 4-5.5 feet
BGS and submitted for laboratory analysis by EPA method 8270 and MADEP EPH, Of these
analysis, a 100 mg/Kg concentration of C 19-06 was detected in MW4. It appears these
compounds originated from impact from leaky hydraulic lifts which are not part of this
investigation.
6.2 Groundwater Quality
Groundwater impacted above interim groundwater standards and Gross Contaminant Levels
(GCL) was not detected in the monitoring wells. Analytical results are attached in Table 5 and
Appendix E.
6.2.1 Virgin Oil UST Location, Monitoring Well MW-2
A groundwater sample was collected for analysis by MADEP EPH, EPA 8270 with tentatively
identified compounds. MADEP detected C9-C 18 EPH in a concentration of 162 ug/L and C I I -
C22 VPH with a concentration of 180 ug/L. These concentrations are lower then the respective
interim groundwater standards of 4,200 uglL for C9-C 18 and 210 ug1L, for C9-C22.
6.2.2 Waste Gil LIST Location, Monitoring Well MW-3
A sample was collected for analysis by MADEP EPH, VPH, EPA 625 with tentatively identified
compounds and SM 6230D. MADEP detected C9-C18 EPH in a concentration of 169 ug/L and
C 11-C22 VPH with a concentration of 121 ug/L. These concentrations are lower then the
respective groundwater standards of4,200 ug/L for C9-C18 and 210 ug/L for C9-C22.
MTBE was detected in a concentration of 4 ug/L; lead was detected in a concentration of 17 ug/L
and chromium with a concentration of 28 ug1L. These concentrations are lower than the
applicable DWQ Gross Contaminant Levels of 200,000, 15,000 and 50,000 ug/L,
6,23 DiesellGasoiine UST Location, Monitoring Well MW-5
A sample was collected for analysis by MADEP EPH, VPH, EPA 625 with tentatively identified
compounds, EPA 601, 602 with IPE and MTBE, EDB by EPA 504, chromium and lead. MADEP
detected the following compounds. C5-C8 VPH, C9-C 12 VPH, C9-C 18 VPH, C9-C 10 VPH,
benzene, toluene, ethylbenzene, xylenes, EDB, lead chromium and naphthalene.
❑WQ guidelines require the additional assessment of a LIST release if the compounds detected
exceed 10 times the interim-21- groundwater standards. The following compounds were detected
13

' with levels greater than 10 times the interim-21, standards: benzene, ethylbenzene and EDB. The
remaining compounds were below applicable NC interim-2L standards.
' 6.2.4 Monitoring Well Locations MW-4 and MW-6
' Monitoring wells MW4 and MW-6 were installed downgradient of the former virgin oil and
waste oil UST locations. Samples were collected for analysis by MADEP EPH and EPA 625 with
tentatively identified compounds. MADEP detected C9-C 18 EPH in MW-4 and MW-6 in
' respective concentrations of 154 and 156 ug/L. C11-C22 VPH was detected in MW-4 with a
concentration of 106 uglL. These concentrations are lower then the respective groundwater
standards of 4,200 for C9-C 18 and 210 ug/L for C9-C22 VPH.
1
14

7.0 CONCLUSIONS AND RECOMMENDATIONS
7.1 Site Rank
The site appears to fall within the low risk category due to the following factors:
-Levels of groundwater impact do not exceed the GCLs.
-Levels of groundwater impact do not exceed surface water quality standards by a factor
of 10.
-Potable water wells are not located within 1,000 feet of the site.
-No explosive petroleum hydrocarbon vapors were detected.
7.2 Soil Cleanup Levels
The site previously held USTs that stored virgin oil, waste oil and gasoline/diesel fuel. The site is
situated within a commercial area and the closest residential housing is located approximately
1,000 feet upgradient of the site. Therefore, EMS recommends the application of
industrial/Commercial cleanup levels to the site soils due to the site location.
7.3 Virgin Oil UST Location
Soil impact exceeding DWQ guidelines was not detected in boring MW-2. Groundwater impact
was also not detected above 10 times the N C interim-2L groundwater standards. It appears no
further assessment is necessary at this location,
7.4 Waste ail UST Location
Soil impact exceeding DWQ guidelines was not detected in boring MW-3. Groundwater impact
was also not detected above 10 times the N C interim-2L groundwater standards. It appears no
further assessment is necessary at this location.
' 7.5 Diesel/gasoline UST Location
Soil impacted with petroleum hydrocarbons was previously detected in Geoprobe borings UST-4
' and UST-4A by TPH analysis at concentrations of 18.3 and 178 mg/Kg (EPA method 5030) and
17 and 14.6 mg/Kg (EPA method 3550). Soil impact exceeding DWQ guidelines was not
detected in boring MW-5. All samples were collected below the water table and it appears the
' Geoprobe samples may actually represent groundwater impact. Utilizing the analytical results
from MW-5 it appears no further soil assessment is necessary at this location.
' Groundwater impact was detected at levels above 10 times the NC interim-21- groundwater
standards. The DWQ will require the installation of four monitoring wells to assess the release.
Two monitoring wells should be installed below the release source, one monitoring well should be
1
15
1

' installed upgradient of the release source and one deep monitoring well should be installed in the
impacted area. Groundwater samples will need to be collected from the monitoring wells for
' analysis of petroleum hydrocarbon compounds by MADEP VPH-EPH, EPA methods 601, 602,
610 and the metals lead and chromium.
R.

Table 1
Underground Storage Tank Specifications
Uzzle Cadillac-Oldsmobile-GMC Truck, Inc.
3737 Chapel Hill Boulevard, Durham, North Carolina
UST Contents
Capacity
Date Installed
Date Removed
UST Material
Virgin Oil
550
515169
6/13/91
Steel
Waste Oil
550
515169
6/13/91
Steel
❑iesellGasoline
2,000
515189
6/13/91
Steel
Gasoline
10,000
512181
12/15/92
Steel
Data from DWQ UST database with the exception of 2,000 gallon UST
contents which was supplied by site personnel,

Table 2
Monitoring Well Construction Summary
Uzzle Cadillac-Oldsmobile-GMC Truck, Inc.
3737 Chapel Nils Boulevard, Durham, North Carolina
Death Below Ground Surface
MW-2
2
0.010
0.5-1.3
1.3-11.3
MW-3
2
0.010
0.3-1.1
1.1-11.1
MW-4
2
0.010
0.3-2.5
2.5-12.5
MW-5
2
0.010
0.3-2.1
2.1-12.1
MW-6
2
0.010
0.3-2.3
2.3-12.3

Table 3
Depth to Groundwater and Groundwater Elevations
Uzzle Cadillac-Oldsmobile-GMC Truck, Inc.
3737 Chapel Hill Boulevard, Durham, North Carolina
MW-1
MW-2
MW-3
MW-4
MW-5
MW-6
Water
Water
Water
Water
Water
Water
Date
Depth
Depth
Depth
Depth
Depth
Depth
7/14/98
3.35
1,72
1.85
5.00
1.92
4.34
MW-1
MW-2
MW-3
MW-4
MW-5
MW-6
G5 Elevation
98.46
99.84
100.00
99.69
98.00
99.80
TOC Elevation
97.82
99.36
99.73
99.37
97.70
99.55
Water
Water
Water
Water
Water
Water
Date
Elevation
Elevation
Elevation
Elevation
Elevation
Elevation
7/14198
94.47
97.64
97.88
94.37
95.78
95.21
' All measurements are in feet and are referenced to a elevation of 100.00
ft. at the ground surface of MW-3.

Table 4
Summary of Volatile
Organic Concentrations (VOC) and
Soil Analytical Results
Uzzle
Cadillac-Oldsmobile-GMC Truck, Inc.
3737 Chapel Hill Boulevard,
Durham, North Carolina
Sample Location
MW-2
MW-3
MW-4
MW-5 MW-6 MSCC
Sample ID
MW-2A
MW-3
MW-4A
MW-5A MW-6A (mg/Kg)
Date Sampled
716198
716198
717/98
717198 7I7198
Sample Depth
0.5-1.5
3.5-5
2-3
4-5.5 4-5.5
PID (ppm)
10
2.6
7.8
16.3 3.4
MADEP Aliphatics
C5-C8 VPH
NS
ND
NS
N❑ NS 24528
C9-C12 VPH
NS
NO
NS
N❑ NS 245280
C9-C18 EPH
110
NO
NO
N❑ ND 245280*
C19-C36 EPH
13000
ND
100
ND ND -
MADEP Aromatics
C9-C10(VPH)
NS
ND
NS
ND NS 12264
C1 i-C22(VPH)
510
NO
NO
N❑ ND 12264*
EPA 8080
NS
N❑
NS
ND NS Varies
EPA 3050 (Pb, Cr)
Pb (mg/Kg)
NS
2.74
NS
NS NS 270
Cr (mg/Kg)
NS
4.62
NS
NS NS 27
EPA 8270
N❑
ND
N❑
N❑ ND Varies
EPA 8260, IPE, MTBE
8260 (mg/Kg)
NS
ND
NS
0.0118 (xylene) NS 5 (xylene)
IPE (mg/Kg)
NS
ND
NS
ND NS 0.37
MTBE (mg/Kg)
NS
ND
NS
ND NS 0.92
Analytical results reported in mgfKg.
ND denotes not detected.
NS denotes not sampled.
Maximum soil contaminant
concentrations
(MSCC) are Industrial/Commercial levels.
C19-C36 MSCC is Health Based
Level>100%
*C9-C12 VPH and C9-C18
EPH
are combined for No. 2 fuel oil maximum soil contaminant concentration.
*C9-Cl0 VPH and C11-C22 EPH aromatics are combined
for No. 2 fuel oil maximum soil contaminant concentra

Table 6
Groundwater Analytical Results
Uzzle
Cadillac-Oldsmobile-GMC Truck, Inc.
Chapel Hill Boulevard, Durham, North
Carolina
July 14, 1998 Sampling Event
00
E
o
E
r
U
2
Q
Q
a
2
¢
..
2
�
=
U
a.
w
I
�
w
2
w
N
G
E
N
w
CO
a
N
OD
Cq
d
N
N c
Gam]
H
2
CU
U U
U
U
U
U
U
r
CAI y
U c �
CD
o�
uj
E
UC d)
U U
�
U
U
r
U
W
U
U
W 4� O
U m H
W
T
x
uJ
0.
O
W
`°
-j
U
C
Z
Sample
Location
MW-1 NS NS
NS
-
NS
NS
NS
NS ND N❑
ND
N❑
ND
N❑
NS
NS
NS
NS
MW-2 NS NS
162
-
ND
NS
180
180 NS NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-3 ND N❑
169
-
ND
ND
121
121 N❑ N❑
ND
ND
4
NS
NS
17
28
N❑
MW-4 NS NS
154
-
ND
NS
106
106 NS NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-5 1,020 5,200
1,070
6,270
ND
2,140
ND
ND 211 1,900
409
2,980
N❑
ND
0.29
94
119
113
MW-6 NS NS
156
-
ND
NS
N❑
ND NS NS
NS
NS
NS
NS
NS
NS
NS
NS
2L & Interim
Standards 420 NGWS
4,200
4,200
42,000
NGWS
NGWS
210 1 1,000
29
530
200
70
0,0004
15
50
21
2B (CSNW)
Standards NSWS NSWS
NSWS
NSWS
NSWS
NSWS
NSWS
NSWS NSWS NSWS NSWS
NSWS
NSWS
NSWS
NSWS
25
50
NSWS
Anayltical results reported in ugfKg.
ND denotes not detected.
NS denotes not sampled.
NGWS denotes no groundwater standard.
NSWS denotes no surface water standard

N
i�!
1,590 FOOT RADIUS FROM SITE
1,000 FOOT RADIUS FROM SITE
PORTION OF THE SOUTHWEST DURHAM, NORTH CAROLINA, TOPOGRAPHICAL MAP
USGS, 1973, PHOTOREVISE❑ IN 1987
CONTOUR INTERVAL=IC FEET
SITE AND VICINITY TOPOGRAPHICAL MAP FIGURE: 1
UZZLE CADILLAC, OLDSMOBILE, GMC DATE: 8/13/98
-- 3737 CHAPEL HILL BOULEVARD SCALE: 1"=2,000'
ENVIRONMENTAL, INC-❑URHAM, NORTH CAROLINA I PROJECT NO: 7239

I
J RT. 15-501 SERVICE ROAD j FORMER STREAM
- - - - -1-- -�� ------ - -—;�-�•-�-ice-_- -� - ■
r
H I
PAVING ��
PAVING
�
I..... SI�''LK..........
i
SHOW ROOM
f
SALES DEPT.
,
FORMER DIESEL
MW�
SERVICE
PAVING
MW� FUElJGASOLlNE
RECEPTION
MW$
_
---
UST LOCATION
--------- ---------- -
......,,.........
-------------------------'--
............................................................
MW-1
SERVICE DEFT.
BODY SHOP
PARTS
`
DEPARTMENT
`ti`
yp
��'
STORAGE,_ ---
MW-3 MW_2 FORMER VIRGIN OIL
��
��
_51-0G,-
-----
FORMER WASTE OIL _- UST LOCATION ---------------
UST LD(.ATIDN
EWRONMENTAL, INC.
FENCE
EMBANKMENT
LEGEND UTILITIES
(APPROXIMATE LOCATION)
s MONITORING WELL ---- STORM SEWER
SLOPE - - SANITARY SEWER
- - - WATER LINE
SCALE (APPROXIMATE)
ELECTRIC LINE
- - NATURAL GAS LINE
- - STREAM
010 30 50 70 So 103 O MANHOLE
FEET • UTILITY POLE ® CATCH BASIN
SITE PLAN PROJECT NO., 7239
UZZLE CADILLAC OLDSMOBILE FACILITY SCALE: NOT TO SCALE
RT. 15-501, DURHAM, NORTH CAROLINA DAZE:8/13198

N
JL
RESIDENCE
RESIDENCE ❑ 1' © 0 FOREST AT DUKE
(VACANT) ❑ RETIREMENT VILLAGE
PICKETT ROAD
❑ RESIDENCE
(VACANT)
o
CONIFER GLENN APT. HOMES
"- WATER WELL m (] m w
(APPROXIMATELY I.MO FT. FROM FORMER DIESELASASOUJNE UST LOCATK]N) A 0 5 ~ r
C 7)
q0 r
T OGLE w g m rFri
m
D7 TENDEO STAY A}IERICA COMMERCIAL SHOPPING RENTAL INNN� ~ cl
Q
CENTERS Q Q
MUSIC
NCOLN•IRCURY��
G� 3MA
GOLDS ST E Lit OURfWM 101SVBlSf11
GYM CAR GEALERSHI P
RPM N)SSAN CAR
PRECISION TUNE R REAL ESTAT
MCDOHALDS RESTAURANT DEALERSHIP
THE OURHAI,L ❑ OFFICE BLUE.
❑ CD
RITZ CAR WASH ❑ �
VOL KSWAGON CAR UZ7LE CADIA.AC ❑
DEALERSHIP
DAIYIRIB$ ROYAL OAK
ON3
o ❑ RESTCH' SOUTH SQUARER APARTMENTS
g OFFICE BLDG. rj
g CHUCK E RESTAURANT V Lj
CHEE2E'8REST.71 ❑
v PONTLAC CAR L��1 D ❑
DEALERSHIP
OFFICE DEPOT O
BD570N MARKET RESTAURANT
F
PFARLE `" ROYAL OAK APARTMENTS
SOUTH SQUARE MA
CENTER SERVICE MERCHANDISE
❑ PLAZA SHOPPING
CENTER
IJ R£37AURAN7 O
SIT
BLOCKBUSTER VIDEO MEDICAL OFFICE SWTH SQUARE i
0 CD OFFICE BLDG.
RESTAURANT IVAGKINDERvAR
LfJI DRY
CLEANERS DAY CAR
OFFICE BLDG r'l E BIOG UOFFICE COMPLCK
RESIDENCES
REAL
AM MOTOR ESTATE
CLUB OFFICE
FIRST UNION MYRq SMEET
LAND USE MAP
' UZZLE CADILLAC, OLDSMOBILE, GMC TRUCK
E:WFZONMENTAL.INC. DURHAM, NORTH CAROLINA
RESIDENCE
CD
RESIDENCE
FIGURE: 3
DATE: 7/24/98
SCALE: NOT TO SCALE
PROJECT NO: 7239

r r r r r rr rr r� r r r ■r rr �■■� ■r r r r r
BUILDING
LfMITS OF FORMER EXCAVATION
---------------- -�
MW-2 1 f
I I
_-
MADEP EPH C19-C36: 13,000 MGIKG I
MADEP EPH C9-C18: 110 MG/KG I
MADEP VPH Cl i-C22: 510 MG1KG
SAMPLE DEPTH: 0.5-1.5 FT. BGS
� k
� I .
I I
l
UST-2
OIL&GREASE: 48-6 MGIKG LEGEND
SAMPLE DEPTH: 4 FT. SGS
SCALE (FEET)
1- 2 3 4- 5 1❑
GEOPROBE BOREHOLE INSTALLED BY FLUOR DANIEL GTI
FORMER VIRGIN OIL UST EXCAVATION
UZZLE CADILLAC OLDSMOBILE FACILITY
E"RONMENTAL, INC- RT. 15-501, ❑URHAM, NORTH CAROLINA
3
'
MONITORING WELL
i
WI SOIL ANALYTICAL RESULTS
GEOPROBE BOREHOLE
WI SOIL ANALYTICAL RESULTS
FIGURE: 4
PROJECT NO: 7239
SCALE. NOT TO SCALE
DATE: 7/22/98

BUILDING
USED ANTIFREEZE AS
WASTE OIL AST p
MW-3 �{--- - - - - -- ---_
PB: 2.74 MG/KG
CR: 4.62 MG/KG
SAMPLE DEPTH: 3.5-5 FT, BGS
FORMER WASTE OIL UST EXCAVATION
I I
I I
I I
I I
I I
----------------------------I
LEGEND
' MONITORING WELL
WI SOIL ANALYTICAL RESULTS
(MG/KG)
SCALE (FEET)
t
0 1 2 3 4 5 10
GEOPROBE BOREHOLE INSTALLED BY FLUOR DANIEL GTI
FORMER WASTE OIL UST EXCAVATION FIGURE: 5
PROJECT NO: 7239
UZZLE CADILLAC OLDSMOBILE FACILITY SCALE: NOT TO SCALE
EWRON MENTAL, INC. RT. 15-501, DURHAM, NORTH CAROLINA DATE: 8/10/98

N
BUILDING
❑ L
FORMER DISPENSER LOCATION
DIESEL AND GASOLINE UST LOCATION
UST-4A - - - - - - - - - -
TPH-5030:178 MGfKG I
TPH-3550: 14.6 MG1KG I {
SAMPLE DEPTH: 10 FT. B4 I
I
I" I
UST-4 ,I i I
MW-5
I
TRH-5030: 18.3 MG/KG I I
TPH-3550: 17 MGIKG 8260: 0.0116 I
SAMPLE DEPTH: 9.5 FT. BGKG XYLENESI I
AMPLE DEPTH: I I
4-5.5 FT. SGS I I
I
I
----- r
LEGEN❑
-�I�-
MONFFORING WELL
Wl SOIL ANALYTICAL RESULTS
(MG/KG)
GEOPROBE BOREHOLE
F
WI SOIL ANALYTICAL RESULTS
�- -
(MG/KG)
_._
SCALE (FEET)
GEOPROBE BOREHOLES INSTALLED BY FLUOR DANIEL GTI - 5 10
FORMER DIESEL AND GASOLINE UST EXCAVATION FIGURE: B
PROJECT NO: 7239
UZZLE CADILLAC OLDSMOBILE FACILITY SCALE; NOT TO SCALE
EWRONMENT►—VaC. RT. 15-501, DURHAM, NORTH CAROLINA DATE: 8/10►98

RT. 15-501 SERVICE ROAD
v
O PAVING SIDEWALK
� ...........................
lul
r - FORMER DIESEL
MW�-i -FUEUGASOLINE MW-4
96 - - -174L UST LOLAT �! 94.37
~ ..............
97 ..VCEDE
.............
-3 97AS
FORMER WASTE OIL
EMBANKMENT
SLOPE
SHOW ROOM
AND
SALES KEPT.
SERVICE
RECEPTION
PARTS
MW-2 FORMERVIR&il&L
97.64 UST LOCATION
97
FENCE
SCALE (APPROXIMATE)
10 %W
%
30 50 70 90 100
FEET
PAVING
95.21 �
SHOP
11 96
+ N
PAVING } -
MW-1
+ _
94.47 -
STORA�Ut~ -
BLDG. -
LEGEND
4- MONITORING WELL
WI GROUNDWATER ELEVATION (FT)
/99.00 GROUNDWATER SURFACE (FT)
GROUNDWATER FLOW DIRECTION
GROUNDWATER FLOW DIRECTION-JULY 14, 1998 FIGURE:7
PROJECT NO: 7239
- UZZLE CADILLAC OLDSMOBILE FACILITY SCALE: NOT TO SCALE
ENVIRONMENTAL, INC- RT. 15-501, ❑URHAM, NORTH CAROLINA
DATE: 8113198

)ECIAL.IZED ASSAYS, INC.
50 Foster Creighton Dr.
3. 3ox 40566
shviIlc. TN 37204-0566
one 1-615•71-6-01 7
r-:p CAfl_�_ r,T1 :�E1
_0'6TH .:Tf
66Zi0;
. ❑ject. 10143,7
i d j e C Y Na I. �Ly CAD!:-,.�C
.3mp 1 a FZENEE Lz,;RY
pn-alp{te
i'lil an,4 6rPa5a
x'liiiriTT3 E ?e5;,si, 19 5L'
3enTehe
ifrCndBefl2el:e
il-:fUCg3,�ehZerse
t2rt-:{UC'31�Pi�tOffE
:,;iorobenzp�e
?-E�lorgtoluene
4-r�larvtoiaene
t 2-;aichloroaenaene
i,3-gichloraoer��ene
1, 4_D i chlr.,rc Je nz e re
ELaazege
1��,praligi�enxe�:e
a-isooroault�luene
aa�r�thalene
9-?"oDglh°il�enA
St�rgae
_ IOIUe?!e
11?,3-iricRlorflGen�ene
2 s_rr t,,lvrtloen�ene
,2,�?-TrinAt:,ulhen�ene
,3,� Tr?:•:eLf�ylhenZefie
n, �-:#ylAaeS
a-kyze�e
Be:t ao hlorohut s¢i a rye
.ironoehltlronethar�e
ifrtlnodichloronet:sahe
Oronororn
Bronankhane
Union tetraciloride
rhlorcebane
C;sloroforn
�i25Eri� li[4lC:
C6.
1�D
'tD
�D
D
AD
O
'{D
AD
sD
{[
1D
�D
3D
ID
�D
aD
aD
AD
AD
.�D
4D
�?D
�D
:{D
RD
�U
XD
RD
in"ka
nglkg
ngi kg
ngrkg
YglKy
nq/k�
ygrkg
r: c.)k
y 01?? 0
yglLg
nglkg
ygA,q
�g11�
:wive
:dAg
f,0AI
ngAg
nglkg
nglkg
mg/kg
naA
ngAg
-IgAg
mg/kg
nglkg
mg/kg
AhiALYT 2 C AL R I=-P OR T
Lat Number: ??-A1�75861
Sainp l J 1 D: US ! -2
Sample Type: S`7
1D:
Da16a Coliected: 11�'l?��T
T i-e 11 15
LI a t-' IRece:ved: 11 r'•?Lr`wi
Time Ra_eiWed: 7:00
Re?ort quan Di=
i:nit l_:t1i` r 3C•'.�r
bite
Tlne
Anal'jSt
MetIQd
If3tch
11r261W
16,53
J.Mitehell
?071A
508
a.102
0. i7a1a
J
11, �61�f7
:t.
°'sQr�u
! , a0ia
11r'i'ur :�'!
0.
CCSi!
0. g0i0
__, ga197
U.'OKO
0.001C
1i!26r 7
a.'}02
0.GB1G
1i126197
0.00SO
0.0010
a
1,12b1ry7
0,
IIKO
0,0019
s
1,125197
0.305D
0.0010
5
11126e'?7
0.+10.'3
a.00i�
5
i1r'261?7
s�.
�105:1
il. uCiU
..
11126i?d
1.
C. O
'J. j IV
�
_li--f .
a.002
0.0010
5
11126197
a.
1f1' 6197
O.'30E0
.5. 001a
.1126:97
.3.
AI Eu
0. 001u
111261?7
0.0o50
0.0010
11I26197
a.105u
a.u010
1ill 261?7
0.
n050
0. S13010
5
i11264,197
0.
OfiSO
0,12010
11/26/97
0.9050
0.0010
11/26/97
a.0050
O.QOiO
5
'!126197
0.005a
0.0010
5
11/26/97
0.9G5u
0.0610
i1.'251r�7
0.9010
0.0910
L126197
0.0050
0.0010
5
ii126197
0-
90SO
6. a01G
11�26r97
0.002
0.01016
s
11t26197
0.0050
0.0010
5
11/26/97
r Imege0 and Confidential
6 firedatt4m,rifcmSeI
0: 34
E. sn: t3
s0"L13
•`si:6
0: J4
..; 1'i 1 Cif
7jrzl,
ryry
0l{A
0: i�
r.::iii t7
$li21iS
6iE6
li: i4
t. `sistih
a0;i
6il5
0: 39
E. Snit*
a02ilf
6u6
0:34
E.inith
30219
606
0
!th
302i0
606
0: 34
E. Sn i t,�
30213
u0c
0: 34
L Sn i tit
30M
606
G: ;4
E. ]ri3 t1
30='i3
506
9: 34
t. sns ,`�
$/Lt3
.G6
1 f
so 6
0:34
}.Snith
30713
60ti
D: 34
E. smith
301 B
606
a: 31
E. Snl t
302iB
606
0: 4
E.::nith
SO.j
606
0: 34
E. Snit i
80L,3
636
0::.
_. Snit:,
aa2i3
606
0:34
E.Sr,itI
90213
606
a:3-
E. Smith
302'_�
606
0: 34
E. Srsi th
30:' l
606
0: 34
E. Smith
K215
666
0: 34
E. Srsith
UZ.B
606
0:34
E.Snith
3021E
bah
0: 34
E. Snith
90=
606
0: 34
E. Sni th
wm
606
0: 34
E. Snit!
302J
606
a: A
E.Snith
d02L9
606
0: 34
E.Smith
MI
606
0: 34
E.Smith
mm
606

SPECIALIZED ASSAYS, INC.
2960 Foster Creighton Dr.
P.O. Sox 40566
Vashvine.TN 3720-t--0566
Phone [phone]
V-
7
•� Fiiral'�tL
ReSUi_ t
Chloromethane
.4D
Qi;romoch?:rvrecisar[e
:+.D
ilraHGmet.`[ar,e
sU
?,?-Frsc,�rQprQparre
XD
:jo
oichlorodi'1Uor hkhaiie
�D
1,1-Dichlaroit}tone
'D
5_J1C�rlor:fCl'dnr
r
��
1 orol gene
•�
trsn5-1ChIorcci: efsc
' I,2-Dir;ni,orcr,r00ane
�D
1Qnnr
-,3-Di a ,rapat�e
aJ
' ., •„
. �: ? ,1-+aivi�iorvproflene
�ir
iethyiene
1,I,Z�"-?etrachlflroetaane
:!;>
Tet7-ichtl: rc.elcaene
`?D
c':crve::ane
�G
iric:i�rvec'.ene
'iD
ir;t:�icrvr_;;oraner�arre
���
i,�-Ol�rOno-�-C'sl3rQDrOp;ne a0
rIM13i;lC?
•-------------------------
125U�.
-'"-------
01rirum
1. io
*� C; dniUm
i 1I.1�i
Chrnnium
{ i}• p
L aan'ur rrl
Selenium
(r7.10
Mver
TrLI" EX.r czz -)n
Conplete^
HD =Rot detected at the
report lint.
AI�7ALYT I C AL R l-=P ©R T
L_a+bar.etur.y Number: q7-A105601
S. mfl i e I i5: 1J [
°ay- 2
ne�ort
ncian
J:l
unit_
? i;jit
Limit
rac*ar
Ma
Tine
Ar[alvst
�leuod
--
[;atvit
ner'J3
Mora
D. M6
0: 34
c. Snith
80=,3
606
0.JCr3
h. ]mitre
8621
606
nvA
0.+]D v
0- iolJ
5
I1I2aiO7
U: 34
E.Sm:t3
2V-13
606
nglJ_]
U,IIU;U
0.00io
r
I.V1.6trI7
U: 44
E- nitl
302iri
606
nit "=?
J. Kroo
0.:IDID
.1rA197
0: 34
E--Hitt
a0m
606
rSsYr{y
t;.30E3
tit. M
.�, _ii9f
0: 3�
k.'sstit
dD �3
Sib
nnik9
0.OV�o
O.ODIG
J
I 216r:71
U: i4
�.'attiL'[
6Ui:
b05
0,0010
I11?6r 97
U: i4
E. iHi t`r
aG�_D
5U5
ngr'
D. KO
0,0010
5
I: .61197
0:134
E. Smith
3D?'_.TS
606
Y�i=:
U. Kra
D.3D10
s
._.':6r'fs
0:.1 s
_.SfS:tr!
D.00re.
0. DOitii
:I,'Sr''7
0:
E.3n:t1
30""Q
60c
YL:.=
D.'�GwG
I] :il�.iU
0::4
8�:_3
So6
H4r=:q
U.OD�O
D.itD1D
I112619
0:34
11-3mitn
80i it
606
.000
0,.1
1�•.�i?i
�i:..
�. ,r'.ft::l
'J�:... r'
�31+a
is
sE.'Jufu
J. f10: i
^i'r.v
U. 111i�D
0.11010
r
11/26iV
D: 34
E. zmit�
Ek�clb'
6D6
�rtiti[
f3�M3
Su
[0. 7L..tl
L�. sD1!t
:f
:ll �'-�! : f
�.
. �ni Li[
�ll�
:7LiC
'O.13KO
10610
:'_ _ar`'7
0; 34
E. tsi:7
sclt -
U. 0L�`0
0. DDzU
_,'S6197
0:4
E. vn; t�
8D: §
506
8D`D
0.0G10
3D 'e_is
$D6
nal �
D. Does
"v. 00IU
_1f:'sr97
0: 37
E. Snit'r
DD'y.
606
Sn;
0. 0Df0
e1.'!{t11
0: ss
-- YititI
aDc
1).0f :D
r1.]al D
]8`0
u.70Iu
'._; ='� ''
1: _4j
`nits
30L1
Gab
1�
_..'With
90?=3
606
:Sdi !;u
U. f][k;•.0
�. DDiD
v
.;,zi5i''i
il: 34
�. �nl iR
1,4
5D5
1It-ie
m 1r`?
1. ?3
ab
11l26r'9;
6010t,
11116d 9l
6010F,
'S?r i
i3.'�0
1ti�
1Il�6:`?7
147i
nDi ?
1. 41
11�
11?26i97
60100
ii:126I97
60100
1112f!?7
1311
rive 32ced and Cciieleriliai
•rpoacedd#the Re of„um

SPECIALIZED ASSAYS. INC.
1960 Foster Creighton Dr.
P.Q. Box 40566
Vashville, 14 37.04-0566
Phone [phone]
Surrogate ----
a
PID 2Ilrr. , "s, 3 r 3-.^:f!-ilratoi leRe
R;l rurr. C:!IflTUDPeIe
l i?ecover j
102
74.
^M^L.`fT I CAL. R 1rP ©R T
Lahoratcrg Number:
Sample ID: 1JSi-2'
rag= 3
E rge, r%noe
R e p a r h0pr0v4d 1s ReDor' Da ke: I /"I q7
tiiec—,icr-e J. Oue-i c, Ph. D. , (1. A. 0i2.0i_ar
ei
" 3. Ie, 5. , Liccrit,:ry Df st:-cr
.'s l it i_ 1"f a ii
'taocra iorrj Cer tifiica pion r�umner: t10229
f lvlf eg$dand Cei,, r,or,f 13t
•redafad at thaReques:Lf Cum!
rnvv 1

SPECIALIZED ASSAYS, INC.
2960 Fas=er Creighton Dr.
P.a. Box 40566
Nashvidec TN37204.0=66
Phone [phone]
" LIJCF' Dni•! T EL GT T Loc
5010 WEST 106TH c T RESET
TNE.K's 662 ; ..
�s
rre ject: 101, .."2
^o.jec t P4 a m e : I,ZZL E t,r.L _LL
AC
amp I er • RENEE LE =RY
Aa�lyca fiesait
--------- -------------- -----------
ilni[s
i� got LPr= .27 it C:,e"�JG•"L 1.. �.
� Single EXtnct'wl 7iC3
QC
hRD
ARiAL'�FT I CAL R�PC]RT
Lab Number: 97—A-'G57y9
Sample 10: UST-4
Sample Type. Sa i l
5i to 1D
Ti-m' Ca'_ I ec`ed 1 3 C.(D
Dare 4eceivej 11f2G��'
Tine Rece i% ed 00
E:11it �.lTii` FiL'tf:r
Oan fime Anall{,t Iietnod 01co,1
ni .vl5i :f:56 Hol; ngurth 8015M/UM 53'
S��rragat: ties��er, lr_'.e' R3oge
---------------------------
3TEX/GRG Sur:, , 1, 1.1-t7..Iuorc.._._.._
'� ��i�,lYu :IS �E1ri' ...•i:�1'.ii� 4f :I�- .:.U.
1 neplr . A4ar:vea y: ZeQCTL . ^e .a �_.`_c; q7
�henore Dunn,J- DueI_�, r, 4. D. �. rj Ur=ica,.
�i Dn, ,"1. , Te' Ski -: Ji
f �ccr ��or+y Cer'._,.va: Cl iiLdlf}er: E10272'
?reparedattttaR�:sBs�Gf�ts<u 58�
rngv i

SPECIALIZED ASSAYS, INC.
2960 Foszer Creighton Dr.
P. D. Box 40566
Nashville. TV 37204-0566
Phone [phone]
..:C 10 WEST 1 06TH
j—,', j aC t Na,ne: i.17'GLIE Cr=LS ILLLAC
mp i er . RENEE I_-- I-,
------ --_—.-------- ----------- ------
[0R6nHTL' P41n'UlFL:'k *
TP4 (SasolEne ;;si-}e) '?� ; Igiltg
d
RD - Pot der?czed at ii[e repot 1..".S
Sarlole Extrict;-)a data
Jb:ff }�tr3C'.?7 ti i?'i Yf +it ext-v-e" :
r`y n
:FOrTt'4 i1 :ar"i icai t.ine
AIVALY'T" 2 C AL R IEP C3R T
Lab �•iumber: 97—A105800
Sample ID: UST--?;,
Sa mp ? e Tup e: Sc) i l
i LC lid.
r-a'e Cc? lected: 11/11?!97
T�-Tle C.,s 1 a c: t ed 17:3Q
Time Receavad: 9: CQ
gepoi t 4uan Dll
Linir Linit Fait�r
J. lU _. %]V .�
.. n2'riQc r rj
1
Date time Rullst hetho'i uatci
,1:'<<,17? 16: M yoli ngUrth 801`ll.'�0'.0 537
�.y- •� - �- .: r
._. _Sr _:96 �. a iixTja del:
R'epor ; "Approved 34: Recur t
71 char=: H. Ounn, ii. J
M. S. r Labc're v D 6c::.a^
LaGui'3�:t,i+� 3�e1'._fi�•3r1+]tl P1iJinb?r: �<<�ww'?
-jreOlfed at the Ropes,ritCunsel

ROM: SPECIALIZED ASSAYS FAX NO.;
SPECIALIZED ASSAYS
- ENVIRONMENTAL
Sit 725 3404
12-02-97 03:32P P.02
7A- 010390
-
REFERRING CLIENT296o
rt
Fasics Ccehcon Dora
Na4wiile, 74 37204
' r
d15-7_6-ai77
FAX [phone]
N(3 CpSTROL NUMSER (FOR LiB LSE ONLY1
�
PROJECT •
P.fl-
3.3
S 15wnarure-Fhaic Prinil /
LSUamM+
� PROJECT NAME
Tx
Q Q.
•
LA8LSdNLy
ACr
PE ❑E5GtlPT ON
DATE
TTr
AtiAL.LYS1;S� ELQrL
TPO
��
�•
5F? -9c-1
71OL
t
6� r- c?a 7
rI47j
r car;
'
I ERjF boa-; Irt c 'o
too1G-'.3��
i D5� !
ANs�
%
!
I II
�I
tii SL �J/ ��7 r
{ D
1
I
I
19
�� - �—rz
J 5 I l*
G 1p A- "70-7'
1
—
11"tf4tow raY
I su Y' Tiztir
Krv'rmr.II :ys rSigmtarr)
Lawrnwry "i Due I Time
5j�tr
Uahed by, [FMs=
Dos / iunc
�17cccsma m [Si nitumP
�enusa
uishcd M {$i�setUno
aau / Time
Flcm+ed by! (Sknaturcl
IgU,M d try. (5WsMM)
0 nm
IR crvcd try. (5i&Mtvrcl r
For Nriher Lssistsnee in completing the chain of custody farm please refer to the instructions found on the opposite s
1469t6datthe Requestol ccal.-e1

';FxoR: -SPECIALIZED ASSAYS FAX NO.: 615 726�3484 �12-02-97 83:32P P6 3
SPECIALIZED ASSAYS
ENVIRONMENTAL
REFERRING CLIENT
Fvsrer Creston Drirc
Nuhvitk T,;1 37304
ACCOU nt : 6081
615-1.5-0171
Fluor Daniel GTI+x
at5�7:s•a�aa
Mike T naham �
JM Y:
15010 West 106th St.
Lenexa, Kansas 66215
tGp�h, 913-599--o262 Fax= 913--599-1043
Specialized Assays: [phone]
CUNTR M NUMBER (FOR LAB USE ONLY)
���
P1tt7MEC: a At
J {/
1
I
� � I H s✓'I fJ 1
UAS (spawm—Plow Prints
PAc1ECT NAME
L�LZlt C-CaLU 0,C- p tdV Tn I IZ-ay)r-
s USE ONLY
t
�
SAMPLE pESCRIp']ON
{]ATE
T7h1E
?r
ANALYSIS 9EQUESTED
.� �rf-�il'
I
i!
f
a ed �,n [swlAtm)
anc / -,=e �ActrNed 7Y: {S6=iUrr; !
I I
24eei o Laoorstmy 9y:
Due z ilmr
�lJ i
L y
4a(thed Lys j ianFWra
' pyts / Timc
Rccara] ay: iSrfnifurcl I
remark;
k
1�
Lomquaftd Or, (S;[ft1[Ura)
Duc y rum
R=csved
(SusnLmrc)
�Yr (Sivatume
Cats / T:me
Sr; (Sivarure)
For further assistance in completing the chain of custody Term please refer to the instructions found on the apposite si
ri fla sd and Cc ?` ?,Ortiai
r'R�aiCt;� lE1e�G��a�Ji VLttfi'r���

an environmental tesVn,_,aomQany
Research 7fian !� Parr. Flarth Cargllnq 27709
191918rTOg90
FAX f91916 ir -0417
.Tune 24, 199•1
1
uax Bas-we1,
Bcauel l C:.-aina n _r , _nC .
Route 6, Box Goa
'
Durhan, `7C
1
Re, de encq
Lear
-ECS'.:2=_' - -- - -
_=3:5�-----� .....__.._.._ .:._3 _..c �__--__� -- -•... ace ,...
- - - - - ---
,.::2 _�- ?
. cur
?lease 3c? z :e ar..C_ :se4' -?^Cr -S f:.- - :i_z raz :_ :3.
�:n C3
'
State Caz-,!:_fticatLon :
Alabama - #4021C Yew Jersev - 467719 Scutt
Caroli:ia - #9902i
Georgia - #815 Tennessee - 4CO296 Yor'rh
Carolina - 137720
'
Kansas Virginia - 400179
484
utlnra�,
Liiramar, Scha... rite pdandCCr{"~■i. t(]�`6
lYh�o+Rr.
C�nn�ttleue
r'vnds ] rr 7 - { Q�Q�lJ
New .«ate Y.mc•t
;S3•285-459
Ci[ri�
..,1-r89-0948
3St.A."8-8181 1�a78.513!

0
• .. - ^� '"::�-=� 'tiff_ - ��{,. _':,'
_ .ya; Pet_ _aua :vd=cca='cr. ;-nai rss
_3A S&r.L,_e Nc:
Ci _er- Sa.: c a `dc . :
NO:
Daze Sar.:nled: 76-12-91
Dame Recsi•red:
Daze Dx�accec:
.:c_rac —nn (SW ana_;s_s r- =_el cil,'te_c5a^e,,�_��_.
Came A^a_- =ed.
9am—c a ....._za_:: s d t'rdiccaztcn d
C�:=e^ _ :
a::._ _rah (SW 846 zasc__ :e .
` to a; ~ a .._.._a_-s a cep_ _eL hvczcc3cccft ._a.^.c •4;_.. a »_ZZ___am_z .
Cz ent:
�..�r•�ren ff nr-�r^rti�
a i '
Prq-EacattheReques4ciCiCunse

1
t
1
t
e
' luanraa.
C'�nnral}cul
:07�5:-3:LT0
.... •y�:�.. I - - - ....v tom' ' -:r+-a:-•. - - .�r..w.an environmental testh�./co npanp
R.O' Box 12946 1 -
Reseamm Triangle_ ParkyNonlf Carolina 27709_
0191 677.0090 1
FAX f9191 a77-4427 1
July 8, 1991
max 9cswe__ `
scswei_ ?;..._ __,c Cc..,ca _n c.
Rcute 6, 3cx 5--';�3
Curham, XC 27705
i
?!ease see .: a ercwcsec� 'Ocorts vc•�_ rest_=s.
I
State
1
Alabama - #4C210 New .Tersev - 467719. scut'. ca Ii :a - tQ9C,2_
vacrgia - :815 =eninessee - 100296 Nc=h Casciiaa - z37720
Kansas - 4E--Z-=2 VSrginia - t00179 484
al
�rJi h aa j{ rc UPS
M ifernar. SC'I4umhufg. N, 31114nca. WhIapany Efagx;unc:lcrl.
flarlda 1111nnu 6lassaClluaatis Na Jn]n Vermanl
407.309-J979 9a•7p5-�7aa 51T-27I•5:17 :01-+�a•asas Sa�•67S.S�:a

i?A LABCRATOR'! RESULTS
i
-r?. Project J:
1146-005(0)
'
Client :Ta=e _
3cswey_ P?-xnb1ng Ccm=an.,, Inc.
Date
Client 10
Parameter
Results
Ar:aly=ec
Pet=,.._eum 1=-Yd--oca---'-cns by ;R 27 mg/kg
07/01/91
2
3
Petr:oleum�Sydrocartvns by IA 920 mg/kg
07/01/91
1
1
1�
`
1
jr� c�I�C atteRec-L?:ii of 1.

S11 41iV�l "Nt %"V ow momy Pwcdi L� _ .•
J j tZlirt3 �}�
3000 ``JE51 ot1 I'K1'VY. : • ' � • I ' + i" • � � � 20,91
t
CAIIY, N.G. 27613
I N111lIkIfIfi WAIl'i1 E_1 FIG fIA 011tE:R
.[- A r _ [- -- -
-- ._ - J}++'AA:r:': �1N •:►:.1'-.�'��; 1•� ;l: ,e. ��GQUSTED•P1��r�MG 17Ff �J�• i f ••, Ci
k.
Im
7 .+ i $ EA71f7id I[}CAEit7Pl.';' y ,
--
i
vwa
AA
dID
++ +
t
r co
-`,;Ln E.; r':=,�i_ _ IiEt:E IV_EF] F3Y t]A7E' �flE,1E_ + . }
P.
E! It }UiSF EFl Ei SIGP7.4T11R1 hAl-F 'IRA ";: RE('.E IVF0 FOR I A I BY — DA1 E _7ir,� +
09
(t.l i n 1.r. ri1:I.iAfi!(`;
f�r�'._ f 1• f•r1 � •

Page 1
Received: 07/09/98
TOXIKON CORP. REPORT
REPORT EMS ENVIRONMENTAL SERVICES
TO 117 S. HOOVER RD
DURHAM NC 27703
L919)596-0470_FAX _0578
ATTEN JIM STAH ING
1
CLIENT EMS NC SAMPLES 6
COMPANY EMS ENVIRONMENTAL SERVICES
FACILITY 117 S. HOOVER RD
DURHAM NC 27703
WORK ID U22LE CADILLAC
TAKEN 7 -7 7 98
TRANS
TYPE LQJ L
P.D. # 7m9
INV. # D6 914
SAMPLE IDENTIFICATION
01 KW-2A
02 M►d-3
03 MW-4A
04 MLI-5A
05 Mu-6A
06 TRIP BLANK
08/04/98 10:43.51
PREPARED TOXIKDN CORPORATION
BY 15 WIGGINS AVE
BEDFORD MA 01730
ATTEN PAUL LETBERG
PHONE [phone] .
work Order 0 98-07-178
�
�Iwlw
CERF IED BY
CONTACT MARKETING
MA CERT # M-MA064: TRACE METALS. SULFATE.CYANIDE.RES. FRE
CHLORINE Ca TOTAL ALK., TDS pH, THMs VOC PEST. NUTRIENTS.
DEMAND_. O&G, PHENOLICS, PCBs__. CT DHS #PH-0563, NY #10778
FL HRS E87143 NJ DE '5i9538 HC-DNR2866",, C 88002 NH 204091•C.
�r
VERIFIED BY:
Previously Reported on_07/ 0 98. _ ...
TEST CODES and NAMES used an this workorder
8260 PURGEABLE ORGANICS VOA
8270 A 6N EXTRACTABLES
CR CHROMIUM
EPHNC EXTRACTABLE PHC
PIPE MS ISOPROPYL ETHER
MEX TS METALS TOTAL EXT., SOIL
MOIST % MOISTURE
;Pa LEAD
�PPCSS PESTICIDES/PCB (SOIL)
VPHNC VOLATILE PHC

.1
' Page 2 TO)iam CARP. REPORT Hark Order 8 98-07-178
Received: 07/09/98 Resuits by Sample
' SAMPLE ID NLI-2A FRACTION OIA TEST CODE 8270 NAME A/HN E)TRACTARLES
Date 8 Time Collected 07 06 98 14:30:00 Category SOIL
RESULT
LIMIT
RESULT
LIMIT
BASE NEUTRAL. EXTRACTABLES
bis(-2-Chtoroethyl) ether
ND
360
Chrysene
ND
360
} 1,3-Dichlarobenzene
ND
360
Di-n-octyL phthalate
NO
360
1,4-Dichlorobenzene
ND
360
Benzo(b)f(uoranthene
ND
360
1,2-Oichlorobenzene
ND
360
Benzo(k)fLuaranthene
ND
360
bis(2-Chloraisopropyl) ether
1
ND
360
Benzo(a)pyrene
ND
360
N-Nitroso-Di-N-Propylamine
NO
360
Indeno(1,2,3-cd)pyrene
ND
360
Hexachloroethene
NO
360
Dibenz(a,h)anthracene
NO
360
Nitrobenzene
1
No
360
Benzo(g,h,i)perytene
ND
360
Isophorone
ND
360
2-Methy(naphthalene
ND
360
bis(2-Chlaroethoxy) methane
NO
360
Benzidine
ND
360
1,2,4-TrichLorobenzene
NO
360
Dibenzofuran
NO
360
Naphthalene
ND
360
Hexachlorobutadiene
ND
360
ACID EXTRACTABLES
Nexachlorocyclopentadiene
NO
360
Phenol
ND
360
2-ChLoranaphthaLene
ND
360
2-ChiorcphenoL
ND
360
Dimethyt phthalate
ND
360
BenzyL Alcohol
ND
730
AcenaphthyLene
ND
360
2-MethyLphenol
ND
360
Acenaphthene
ND
360
4-Methylpheno(
ND
360
2,4-Dinitrotoluene
ND
360
2-Nitrophenoi
ND
360
2,6-Dinitrotoluene
ND
360
2,4-DimethyIphenol
ND
360
Diethylphthalate
ND
360
Benzoic Acid
ND
1800
4-Chlorophenyl phenyl ether
ND
360
2,4-DichlorophenaL
NO
360
FLuorene
ND
360
4-Chloroaniline
ND
360
N-Nitrosodiphenylamine
ND
360
4-Chtoro-3-methylphenoL
AD
360
4-Bromophenyl phenyl ether
NO
360
2,4,6-Trichlarophenol
ND
360
HexacM orobenzene
ND
360
2,4,5-Trichlorophenol
ND
360
Phenanthrene
ND
360
2-NitroaniLine
ND
910
Anthracene
ND
360
3-NitroaniLine
NO
910
Di-n-butylphthalate
ND
360
2,4-DinitraphenoL
ND
910
Fluoranthene
ND
360
4-Nitrophenot
ND
910
Pyrene
ND
360
4-NitroaniLine
ND
910
Butyl benzyl phthalate
ND
360
4,6-Dinitro-2-methylphenol
ND
910
3,31-Dichlorobenzidine
ND
730
Pentachlarophenol
ND
910
Benzo (a) anthracene
ND
360
3-Methylphenoi
ND
910
bis (2-ethylhexy()phthaLate
ND
360
2,6- Dichlorophenol
ND
910
Notes
and Definitions
for this Report:
UNITS:
u9/K9
EXTRACTED:
07,/13/98
DATE
RUN:
0711419
ANALYST:
PAC
` INSTRUMENT:
C
1 DIL.
FACTOR:
1
NO = not detected at detection Limit

Page 3 TOxIKOM CORP. REPORT York Order 0 98-07-17B
Received: 07109/98 1 Results by Saute
SAMPLE ID RW-2A FRACTION 01A TEST CODE EPHNC NAME EXTRACTABLE PHC
Date 8 Time Collected 07 06 $ 4. 0. 0 Category SOIL
EXTRACTABLE PETROLEUM HYDROCARONS
REPORTING
RESULT
LIMIT
C9-Ci$ Aliphatics 110
100
C19-06 Atiphatics 13000
10e
C11-C22 Aromatics 510
100
I
Surrogates %Recovery Surrogate Limits
Aliphatic Surrogate ENT 40 -
140
Aliphatic Fractionation Surrogate 64.5 40 -
140
Aromatic Surrogate 81.6 40 -
140
I
Aromatic Fractionation Surrogate 75.2 40 -
140
Notes and Definitions for this Report:
EXTRACTED 07113 98
DATE RUN 07/18/98
ANALYST CK
INSTRUMENT HP7
DIL. FACTOR: 1
UNITS O Ka
"TRIX:
DRY WEIGHT: 91.2
1I
NO = not detected at detection limit
0 = diluted out
i
INT = matrix interference
Hydrocarbon Range data exclude concentrations of surrogate(s) eluting in that range
Hydrocarbon Range data are unadjusted for target analytes
I
I
1
1
1
1
1

Page 4 TCDLIlCOM CORP. REPORT York order # 98-07-178
Received: 07/09/98 ` Results by SampLe
SAMPLE ID MY-3 1 SAMPLE 9 02 FRACTIONS: A
Date d Time Collected 07/06/98 15:30:00 Category SOIL, '
CR 4.62 IPE_MS MO MOIST 8.40 P8 2.74
mg/Kg 0L=0.507 ug/Kg 0L=10 % mg/Kg 0L=2.55

1
I
Page 5 ILMIKOW CORP. REPORT Work Order it 98-07-178
Received: 07/09/98 ResuLts by Sample
SAMPLE ID KW-3 FRACTION D2A TEST CODE 8260 NAME PURGEABLE ORGANICS VOA
Date 8 Time Collected 07106/98 15-30.00 Category SOIL
1
EPA 8260 PQRGEABLE ❑RGANICS
RESULT
LIMIT
RESULT
LIMIT
Chioromethane
HD
10
❑-Xylene
NO
5.0
Bromomethane
ND
5.0
m+p-Xylene
NO
5.0
Vinyl Chloride
ND
2.0
1,2-Dichlorobenzene
No
5.0
Chloroethane
ND
10
1,3-Dichlorobenzene
ND
5.0
Methylene Chloride
No
10
1,4-Dichlorobenzene
ND
5.0
1,1-oichloroethene
No
5.0
Naphthalene
ND
10
Trichlorofluoromethone
-No
10
n-Propylbenzene
ND
10
1,1-Oichloroethane
No
5.0
Browbenzene
ND
5.0
Trans-1,2-Dichloroethene
NO
5.0
Bromchloremethane
ND
5.o
Chloroform
No
5.0
n-Butylbenzene
NO
10
1,2-Dichlaroethane
No
5.0
sec-Butylbenzene
N0
10
1,1,1-Trichloroethane
No
5.0
tert-Butylbenzene
ND
10
Carbon Tetrachloride
No
5.0
2-Chlorotoluene
NO
5.0
Bromodichloromethane
No
5.0
4-Chlorotoluene
No
5.0
1,2.Oichioropropene
NO
5.0
1,2-Dibromo-3-chloropropane
No
5.0
Trichlaroethene
No
5.0
1,2-Dibromomethane
No
5.0
Dibromochloromethane
No
5.0
Dibromomethane
No
5,0
1,1,2-Trichloroethane
1 No
5.D
Dichlorodifluoromethane
No
10
Benzene
NO
5.0
cis-1,2-Dichloreethene
NO
5.0
1,1-Dichtoropropene
AND
5.D
1,3-Dichloroprapane
NO
5.0
2-2-Dichtorpropene
IND
5.0
1,1,1,2-Tetrachloroethane
ND
5.0
Bromoform
AND
5.D
1,2,3-TrichLorobenzene
No
5.0
Hexachiarobutadiene
IND
10
1,1,2,2-Tetrachloroethane
No
5.0
Isopropytbenzene
AND
10
1,2,4-Trichlorcbenzene
No
5.0
Tetrachtoroethene
AND
5.0
1,2,3-Trichloropropane
No
5.0
Methyl tertiary butyl ether
AND
5.0
1,2,4-Trimethylbenzene
No
10
Totuene
IND
5.0
1,3,5-Trimethylbenzene
NO
10
Chlorobenzene
AND
5.0
cis-1,3-Dichloropropene
No
5.0
Ethyl Benzene
IND
5.0
trans-1,3-Dichloropropene
No
5.0
p-Isopropyltoluene
AND
l
10
Styrene
No
5.0
Notes and definitions for this report:
DATE RUN 07/17/98
ANALYST JPM
INSTRUMENT G
DIL. FACTOR 1
UNITS 22lKS
COMMENTS
RD = Not detected at detection Limit

Page 6
Received: 07/09/98
ISAMPLE ID M11-
TOXIKOX CORP. REPORT York order * 98-07-178
1 Results by Sample
BASE NEUTRAL EXTRACTABLES
1 FRACTION 02A TEST CDDE 8270 NAME A/BN _EXTRACTABLES
I Date & Time Collected OZZ06/98 15:30:00 Category SOIL
RESULT LIMIT
bis(-2-ChloroethyL) ether
ND
360
Chrysene
1,3-Oichlorobenzene
NO
360
Di-n-octyt phthalate
1,4-Dichlorobenzene
ND
360
Benzo(b)fluoranthene
1,2-Dichlorobenzene
NO
360
Benzo(k)fluoranthene
'
bis(2-Chloroisopropyt) ether
ND
360
Benzo(a)pyrene
N-Nitroso-Di-N-Propytamine
ND
360
Indeno(1,2,3-cd)pyrene
Hexachloroethane
NO
360
Dibenz(a,h)anthracene
Nitrobenzene
ND
360
Benzo(g,h,i)peryiene
Isophorone
NO
360
2-Methylnaphthalene
bis(2-Chloroethoxy) methane
Nfl
360
Benzidine
1,2,4-Trichlorobenzene
ND
360
Dibenzofuran
Naphthalene
HD
360
Hexachlorobutadiene
ND
360
ACID EXTRACTABLES
Hexachlorocyctopentediene
HD
360
Phenol
2-Chloronaphthatene
ND
360
2-ChlorophenoL
DimethyL phthalate
ND
360
Benzyl AlcohoL
Acenaphthylene
ND
360
2-Methylphenol
Acenaphthene
ND
360
4-Methylphenol
2,4-Dinitrotoluene
HD
360
2-NitrophenoL
2,6-DtnitrotoLuene
ND
360
2,4-Dimethylphenol
DiethyLphthalate
NO
360
Benzoic Acid
4-Chtorophenyl phenyl ether
NO
360
2,4-Dichlorophenol
Fluorene
NO
360
4-Chtoroanitine
N-Nitrosodipheny(amine
NO
360
4-Chloro-3-methylphenol
4-BromophenyL phenyl ether
ND
360
2,4,6-TrichlorophenoL
Hexachiorobenzene
ND
360
2,4,5-TrichlorophenoL
Phenanthrene
NO
360
2-Nitroaniline
Anthracene
NO
360
3-Nitroaniline
Di-n-butytphthalate
NO
360
2,4-0initrophenol
Fluoranthene
ND
360
4-Nitrophenol
Pyrene
ND
360
4-Nitroaniline
Butyl benzyl phthalate
I
ND
360
4,6-Dinitro-2-methyiphenot
3,31-DichEorobenzidine
ND
720
Pentachlorephenol
Benzo (a) anthracene
HD
360
3-Methylphenol
. his (2-ethylhexy0phthalate
ND
360
2,6- Dichlorophenol
Notes and Definitions for this Report:
UNITS: ug/Kg
EXTRACTED: 07/ 9I98
DATE RUN: 07/31198
ANALYST: PAC
INSTRUMENT: F
DEL. FACTOR: 1
ND a not detected at detection Eimit
RESULT LIMIT
NO
ND
NO
NO
No
NO
NO
NO
ND
bin
NO
HD
ND
ND
ND
ND
No
ND
NO
ND
ND
un
ND
ND
NO
NO
NO
40
ND
NO
NO
No
!10
360
360
360
360
360
360
360
360
360
360
360
360
360
720
360
360
360
360
1800
360
360
360
un
360
900
900
onn
900
900
900
900
900
900

' Page 7
Received: 07/09/98
SAMPLE ID -3
1
TO)(IKO1I CORP. REPORT
Work order 9 98-07-178
Resuits by Sample
FRACTION 03A TEST CODE P£ HHC HARE EXTRACTABLE PHC
Date 8 Time Collected 07/06/98 15-30:02 Category S21L
EXTRACTABLE PETROLEUM HYDROCARONS
REPORTING
RESULT
LIMIT
C9-C18 Atiphatics N0
100
C19-C36 ALipfatics NO
100
1
C11-C22 Aromatics No
100
Surrogates %Recovery Surrogate Limits
,
Aliphatic Surrogate 79.2 40 -
140
Aliphatic Fractionation Surrogate 82.8 40 -
140
Aromatic Surrogate 61.3 40 -
140
Aromatic Fractionation Surrogate 73.1 40 -
140
1
Notes and Definitions for this Report:
EXTRACTED 07/28 98
DATE RUN 08/01 98
ANALYST CK
,
INSTRUMENT HP7
DIL.` FACTOR: 1
UNITS mglKg
MATRIX:
DRY WEIGHT: 91.6
I
NO = not detected at detection limit
0 = diluted out
1
INT = matrix interference
Hydrocarbon Range data exclude concentrations of surrogate(s) eluting in that range
Hydrocarbon Range data are unadjusted for target anaLytes

Page 8 TOC(IK011 CORP. REPORT York Order i# 98-07-17B
Received: 07/09/98 Results by Sample
SIMPLE ID MY-3 FRACTION 02A TEST CODE PPCBS NAME PESTICIDES/PCS (SOIL)
Date & Time Collected 07 06 98 15.30:00 Category SOIL
PESTICIDES
RESULT LIMIT
Alpha-BHC
Gamme-BHC (Lindane)
Beta-BHC
HeptachLor
Deita-BHC
Atdrin
HeptachLor Epoxide
Endosulfan I
4,4'-DDE
Dieldrin
Endrin
4,4--DDD
Endosulfan II
4,41-DDT
Endrin Aldehyde
Endosutfan SuLfate
Chlordane
Toxaphene
MethoxychLor
ND 0.010 Arocior 1016
ND 0.010 Arocior 1221
NO 0.010 Arocior 1232
NO 0.010 Arocior 1242
NO 0.010 Arocior 1248
ND 0.010 Arocior 1254
NO 0.010 Arocior 1260
HD 0.010
NO 0.010
ND 0.010
NO 0.010
ND 0.010
N4 0.010
ND 0.010
ND 0.010
NO 0.010
ND 0.010
HD 0.010
NO 0.010
Notes and Definitions for this Report:
EXTRACTED: 07114198
UNITS: mglKg
DATE RUN: 07�15198
ANALYST: CK
INSTRUMENT: HP2
DIL. FACTOR: 1
HD = not detected at detection Limit
PCB
RESULT LIMIT
ND 0.50
NO 0.50
ND 0.50
ND 0.50
HD 0.50
NO 0.50
HD 0.50

Page 9 TCXION CORP. REPORT York order 0 98-07-178
Received-. 07/09/98 Results by SampLe
SAMPLE ID MY-3 FRACTION 02A TEST CODE VPHNC NAME VOLATILE PHC
Date & Time Collected 07 06 98 15:30:00 Category SOIL
VOLATILE PETROLEUM HYDROCARBONS
REPORTING
RESULT
LIMIT
CS -CS ALiphatics (FID)
NO
1.0
C9-C12 ALiphatlics (FID)
NO
1.0
C9-C10 Aromatics (PID)
NO
1.0
TARGETIVPH AHALYTES
Surrogates % Recovery Surrogate Limits
FID Surrogate 76 70 - 130
PID Surrogate 77 70 - 130
Motes and Definitions for this Report:
I
UNITS: _mg/kg
DATE RUN: 07116/9
EXTRACTED:
ANALYST: SEP
INSTRUMENT: ____ V3
DIL. FACTOR: 1
DRY WEIGHT: 91.6
I
HD = not detected at detection Limit
D = diiuted out
1NT = matrix interference
Hydrocarbon Range data exclude concentrations of surrogate(s) eluting in that range
Hydrocarbon Range data are unadjusted for target analytes

Pape TO TOXI" CORP. REPORT Llark Order # 98-07-178
Received: 07/09/98 1 Results by Sample
SAMPLE ID fIN-4A I FRACTIDN 03A TEST CODE 827U NAME A BN EXTRACTABLES
Date 8 Time Cottected 07/07/98 09.15.00 Category SOIL
BASE NEUTRAL E)(TRACTABLES
bis(-2-Chtoroethyl) ether
1,3-Dichiorobenzene
1,4-Dichlorobenzene
1,2-DichLorobenzene
bis(2-ChtoroisopropyL) ether
N-Nitroso-Di-N-Propylamine
HexachLoroethane
Nitrobenzene
Isopharone
bis(2-Chtoroethoxy) methane
1,2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
Hexachiorocyclopentadiene
2-ChloronaphthaLene
Dimethyt phthalate
AcenaphthyLene
Acenaphthene
2,4-Dinitrotoluene
2,6-0initrototuene
Diethytphthalate
4-Chlorophenyl phenyl ether
FLuorene
N-Nitrosodiphenytamine
4-Bromopheny( phenyl ether
Hexachiorabenzene
Phenanthrene
Anthracene
Di-n-butylphthalate
Fluoranthene
Pyrene
Butyl benzyt phthalate
3,31-Dichlorobenzidine
Benz❑ (a) anthracene
bis (2-ethylhexy0phthaiate
RESULT LIMIT
ND
380
Chrysene
NO
380
Di-n-octyl phthalate
No
380
Benzo(b)fluoranthene
ND
380
Benzo(k)fluoranthene
No
380
Benzo(a)pyrene
ND
380
Indeno(1,2,3-cd)pyrene
No
380
Dibenz(a,h)anthracene
ND
380
Benza(g,h,i)perylene
ND
380
2-Methylnaphthalene
No
380
Benzidine
ND
380
Dibenzofuran
ND
380
ND
380
ACID EXTRACTABLES
ND
380
Phenot
No
380
2-ChlorophenoL
ND
380
Benzyt Alcohol
ND
380
2-Methy(phenol
No
380
4-Methy(phenoL
ND
380
2-Nitrophenol
N0
380
2,4-DimethyLphenot
NO
380
Benzoic Acid
ND
380
2,4-Dichlarophenot
No
380
4-Chloroaniiine
NO
380
4-Chloro-3-methytpheno(
ND
380
2,4,6-Trichlorophenol
NO
380
2,4,5-Trichloraphenot
ND
380
2-Nitroaniline
No
380
3-Nitroaniline
No
380
2,4-DinitraphenoL
ND
380
4-Nitrophenol
NO
380
4-Nitroaniline
ND
380
4,6-Dinitro-2-methylphenoL
ND
760
PentachLorophenol
No
380
3-Methylphenoi
ND
380
2,6- Dichlarophenol
Notes and Definitions for this Report:
UNITS: _ v4/K9
EXTRACTED: 07,.,/13/98
DATE RUN: 07^ /14/98
ANALYST: PAC
INSTRUMENT: C
OIL. FACTOR: 1
No = not detected at detection limit
RESULT LIMIT
kin tvn
NO
380
ND
380
ND
380
NO
380
ND
380
No
380
No
380
NO
380
kin
xvn
ND 380
NO
380
ND
380
ND
760
No
380
ND
380
ND
380
ND
380
No
1900
ND
380
HD
380
ND
380
NO
380
NO
380
ND
950
No
950
No
950
ND
950
NO
—
950
ncn
ND 950
NO 950
NO 950

I
1
Page 11 TCO[IKp[ CORP. REPORT
Received: 07/D9/98 Resuits by saple
Work Order # 98-07-178
SAMPLE lD 1ILI-4A FRACTION OA TEST CODE EPHNC NAME EXTRACTABLE PHC
Data & Time CoLLected 07 07 98 09:15:00 Category SOIL
EXTRACTABLE PETROLEUM HYDROCARONS
REPORTING
RESULT LIMIT
C9-C18 Aliphatics HD 100
C19-C36 ALiphatics 100 100
C11-C22 Aromatics ND 100
Surrogates %Recovery Surrogate Limits
Aliphatic Surrogate 61.6 40 140
Aliphatic Fractionation Surrogate 57.2 40 - 140
Aromatic Surrogate 62.0 40 - 140
Aromatic Fractionation Surrogate 77.a 40 - 140
Notes and Definitions for this Report:
EXTRACTED 07/13198
DATE RUN 07/18/98
ANALYST CK
INSTRUMENT r HP7
DIL. FACTOR: 1
UNITS m91K9
MATRIX:
DRY WEIGHT: 86.9
ND = not detected at detection limit
D diluted out
i
INT = matrix interference
Hydrocarbon Range data exclude ccncintrations of surrogate(s) eluting in that range
Hydrocarbon Range data are unadjusted for target analytes

Page 12 TOXI1<N CORP. REPORT York Order 1 98-07-178
Received: 07/091" Results by SaWLe
J SAMPLE ID MY-5A - SAMPLE # 04 FRACTIONS: A -
Date & Time Collected 07/07/98 10:45:00 Category SOIL
IPE MS RD MOIST 17.6
' ug/Kg DL=10 %

Page 13 TOXIXDk CORP. REPORT York Order 9 98-07-178
Received: 07/09/98 Results by Sample
SAMPLE ID NW-5A -
FRACTION D4A TEST CODE 8260 NAME PURGEABLE ORGANICS VDA
Date & Time CoLlected 07107/98_10:45:00 Category SOIL
EPA 8260
PURGEABLE ORGANICS
1
RESULTf
LIMIT
RESULT
LIMIT
Chioromethane {
ND
10
o-Xylene
ND
5.0
Bromomethane
ND
5.0
m+p-Xylene
11.8
5.0
Yinyi Chloride
ND
2.0
1,2-Dichlorobenzene
ND
5.0
ChLoroethane
ND
10
1,3-Dichlorobenzene
NO
5.0
Methylene Chloride I
HD
10
1,4-Dichlorobenzene
ND
5.0
1,1-Dichloroethene
ND
5.0
Naphthalene
ND
10
Trichlorofluaromethane
ND
10
n-Propylbenzene
ND
10
1,1-Oichlaroethane I
NO
5.0
Bromabenzene
ND
5.0
Trans-1,2-Dichlaroethene
NO
5.0
Bromchloromethone
NO
5.0
Chloroform I
NO
5.0
n-Butylbenzene
NO
10
1,2-Dichloroethene I
NO
5.0
sec-ButyLbenzene
ND
10
1,1,1-Trichioroethane I
ND
5.0
tert-Butylbenzene
NO
10
Carbon Tetrachiaride I
ND
5.0
2-Chlorotoluene
ND
5.0
Bromodichioromethene I
ND
5.0
4-Chlorotoluene
NO
5-0
1,2-Dichlaropropane I
NO
5.0
1,2-Dibromo-3-chlaropropane
NO
5.0
Trichloroethene I
NO
5.0
1,2-Dibromamethane
NO
5.0
Dibromachlaromethane I
NO
5.0
Dibromomethane
ND
5.0
1,1,2-Trichiorcethane I
NO
5.0
Dichlorodifluoromethane
ND
10
Benzene I
ND
5.0
cis-1,2-Oichloroethene
ND
5.0
1,1-Dichloropropene I
NO 5.0
1,3-Dichloropropane
N4
5.0
2-2-Dichlorpropane I
ND
5.0
1,1,1,2-Tetrachloraethene
ND
5.0
Bromoform I
ND
5.0
1,2,3-TrichLorobenzene
ND
5.0
Hexachlorobutadiene
ND
10
1,1,2,2-Tetrachloroethane
ND
5.0
IsopropyLbenzene
NO
10
1,2,4-TrichLarobenzene
HD
5.0
Tetrachloroethene
NO
5.0
1,2,3-Trichloropropane
NO
5.0
Methyl tertiary butyl ether
ND
5.0
1,2,4-Trimethylbenzene
ND
10
Toluene
ND
5.0
1,3,5-Trimethytbenzene
ND
10
Chlorobenzene
NO
5.0
cis-1,3-Dichtoroprcpene
ND
5.0
Ethyl Benzene
NO
5.0
trans-1,3-DichLoropropene
ND
5.0
p-Isopropyltoluene
RD
10
Styrene
ND
5.0
Notes and definitions for this report:
DATE RUN 07/17/98
ANALYST JPM
INSTRUMENT r G
DIL. FACTOR 1
UNITS u9/Kg
COMMENTS
ND a Not detected at detection Limit

' Page 14
Received: 07/09M
MIXON CORP. REPORT
Results by Sample
York Order # 98-OT-178
SAMPLE ID mw-5A _ FRACTION 04A TEST CODE B270 NAME A/BN EXTRACTABLES
Date 8 Time Collected 07 O7 98 10:45:00 Category SOIL
BASE NEUTRAL EXTRACTABLES
bis(-2-Chloroethyl) ether
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
bis(2-ChloroisoprapyL) ether
N-Nitroso-Di-N-Propylamine
Rexachloreethane
Hitrobenzene
Isophorone
bis(2-Chlaroethoxy) methane
1,2,4-Trichlorobenzene
Naphthalene
Nexachlorobutadiene
Nexachlorocyclopentodiene
2-Chloronaphthalene
Dimethyl phthalate
Acenaphthylene
Acenaphthene
2,4-Dinitrotatuene
2,6-Dinitrototuene
Diethylphthatate
4-Chlorophenyt phenyt ether
Ftuorene
N-Nitrosodiphenyiamine
4-Bromophenyt phenyl ether
Hexachlorobenzene
Phenanthrene
Anthracene
Di-n-buty(phtha{ate
Fluoranthene
Pyrene
Butyl benzyt phthalate
3,31-Dichlorobenzidine
Benzo (a) anthracene
bis (2-ethylhexyl)phthalate
RESULT LIMIT
ND
410
Chrysene
ND
410
Di-n-octyt phthalate
ND
410
Benzo(b)ftuoranthene
NO
410
Benzo(Oftuoranthene
ND
410
Benzc(a)pyrene
ND
410
Indeno(1,2,3-cd)pyrene
HD
410
Dibenz(a,h)anthracene
ND
410
Benzo(g,h,i)pery(ene
NO
410
2-Methylnaphthalene
ND
410
Benzidine
ND
410
Dibenzofuran
ND
410
HD
410
ACID EXTRACTABLES
ND
410
Phenol
ND
410
2-Chlorophenol
ND
410
BenzyL ALcohoL
No
410
2-MethylphenoL
NO
410
4-Methylphenol
NO
410
2-Hitrophenol
NO
410
2,4-Dimethylphenol
NO
410
Senzoic Acid
NO
410
2,4-Dichlorophenol
ND
410
4-Chtoroaniline
ND
410
4-ChLoro-3-methytphenol
ND
410
2,4,6-Trichloraphenot
NO
410
2,4,5-Trichlorophenot
NO
410
2-Nitroaniline
NO
410
3-Nitroanitine
NO
410
2,4-Dinitrophenol
ND
410
4-Nitrophenol
NO
410
4-Nitroaniline
NO
410
4,6-Dinitro-2-methylphenol
NO
810
Pentachtoropheno(
NO
410
3-Methytphenol
NO
410
2,6- Dichtorophenol
Notes and Definitions for this Report:
UNITS: ucIK9
EXTRACTED: 07/ 3/98
DATE RUN: 07/ 4/98
ANALYST: PAC
INSTRUMENT: C
DIL. FACTOR: 1
ND = not detected at detection limit
RESULT LIMIT
NO 410
NO 410
,in 1 4A
NO
410
ND
410
ND
410
NO
410
NO
410
NO
410
ND
410
ND
410
NO
410
NO
410
No
810
Lin
.,n
No
410
ND
410
HD
410
HD
2000
HD
410
NO
410
HD
410
NO
410
Q
410
NO
1000
NO
1000
NO
1000
NO
1000
NO
1000
NO
1000
NO
Lin
1000
i Anil
ND 1000

Page 15 TOxnioN CORP. REPORT Work Order # 98-07-178
Received: 07/09/98 Results by SaWte
' SAMPLE ID MY-5A FRACTION 04A TEST CODE EPRNC NAME EXTRACTABLE PHC
Date & Time Collected 07/07/98 10:45:00 Category SOIL
' EXTRACTABLE PETROLEUM HYDROCARONS
REPORTING
RESULT LIMIT
C9-C18 ALiphatics No 100
C19-C36 ALiphatics NO 100
C11-C22 Aromatics HD 100
Surrogates %Recovery Surrogate Limits
Aliphatic Surrogate 71.7 40 - 140
' Aliphatic Fractionation Surrogate 51.6 40 140
Aromatic Surrogate 61.9 40 140
Aromatic fractionation Surrogate 69.7 40 - 140
' Notes and Definitions for this Report:
EXTRACTED 07113L98
DATE RUN 07_ 118/98
' ANALYST CK
INSTRUMENT HP7
DEL. FACTOR: 1
UNITS m4/Kg
MATRIX:
DRY HEIGHT: 82.4
' ND = not detected at detection limit
D diluted cut
iNT = matrix interference
Hydrocarbon Range data exclude concentrations of surrogate(s) eluting in that range
Hydrocarbon Range data are unadjusted for target ane(ytes
I

Page 16 TO1(II(OM CORP. REPORT York Order 0 98-07-178
Received: 07/09/98 Results by SaWle
SAMPLE ID MY-5A - FRACTFDN 04A TEST CODE PPCHS NAME PESTICIDES PC8 SOIL
Date 8 Time Collected 07/07/98 10-45:00 Category SOIL
PESTICIDES
PCB
RESULT
LIMIT
RESULT
LIMIT
Alpha-gHC
ND
0,010
Aroclor
1016
HD
0.50
Gamma-BHC (Lindane)
ND
0.010
Aroclor
1221
ND
0.50
Beta-gHC
ND
0.010
Aroclor
1232
HD
0.50
Heptachlor
HD
0.010
Aroclor
1242
ND
0.50
Delta-BHC
ND
0.010
Aroclor
1248
HD
0.50
Aldrin
ND
0.010
Aroclor
1254
ND
0.50
Heptachlor Epoxide
No
0.010
Aroclor
1260
ND
0.50
Endosulfan 1
ND
0.010
4,4'-DDE
NO
0.010
Dieidrin
ND
0.010
Endrin
ND
D.D10
4,4'-DDD
ND
0.010
Endosulfan II
ND
0.010
4,41-DDT
NO
0.010
Endrin Aldehyde
ND
0.010
Endosulfan Sulfate
ND
O.010
Chlordane
ND
0,010
Toxaphene
ND
0.010
Methoxychlor
ND
0.010
Notes and Definitions for this Report:
EXTRACTED: 07/ 4198
UNITS: mg/Kg
DATE RUN: 07/15/48
ANALYST: CK
INSTRUMENT: HP2
DIL. FACTOR: 1
ND = not detected at detection limit

Page 17 TOXI10
Received: 07/09/98
SAMPLE ID NY-5A -
N CORP. REPORT Doric Order # 98-07-178
Results by Sample
FRACTION 04A TEST CODE VPHNC NAME VOLATILE PHC
Date & Time Collected 07/07/98 10:45:9D Category SOIL________
VOLATILE PETROLEUM HYDROCARBONS
REPORTING
RESULT LIMIT
C5-C8 Aliphatits (FID) ND 1.0
C9-C12 Aliphatics (FID) ND 1.0
C9-CIO Aromatics (PID) ND 1.0
TARGETJVPH ANALYTES
Surrogates % Recovery Surrogate Limits
FID Surrogate 82 70 - 130
PID Surrogate 83 70 - 130
Notes and Definitions for this Report:
UNITS: -- nLkg
DATE RUN: 07/16/98
EXTRACTED:
r
ANALYST: SEP
INSTRUMENT: V3
DIL. FACTOR: 1
ORY WEIGHT: 82.4
HD = not detected at detection limit
0 = diluted out
INT = matrix interference
Hydrocarbon Range data exclude concIntrations of surrogate(s) eluting in that range
I
Hydrocarbon Range data are unadjusted for target analytes

Page 1S
Received: 07/09M
SAMPLE ID
TOXIKON CORP. REPORT York Order # 98-07-178
Results by Sample
FRACTION 05A TEST CODE 8270 NAME AIBR EXTRACTABLES
Date & Time Cotlected 07/07/98 13:20:00 Category SOIL
BASE NEUTRAL EXTRACTABLES
bis(-2-ChtoroethyL) ether
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-DichLorobenzene
bis(2-Chloroisopropyl) ether
N-Nitroso-Di-N-PropyLamine
Hexachloroethane
Nitrobenzene
lsophorone
bis(2-Chlaroethoxy) methane
1,2,4-Trichlorobenzene
Naphthalene
Hexachlorobutadiene
Nexachlorocyclopentadiene
2-Chloronaphthelene
DimethyL phthalate
Acenaphthylene
Acenaphthene
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl phenyl ether
Fluorene
N-NitrosodiphenyLamine
4-gromophenyL phenyl ether
Hexachlorobenzene
Phenanthrene
Anthracene
Di-n-butyiphthalate
Fluoranthene
Pyrene
Butyl benzyl phthalate
3,31-Dichlorobenzidine
Benzo (a) anthracene
bis (2-ethylhexyl)phthalate
Note
RESULT LIMIT RESULT LIMIT
NO
390
Chrysene
ND
390
ND
390
Di-n-octyt phthalate
ND
39D
ND
390
Benzo(b)ftuoranthene
RD
390
ND
390
Senzo(k)ftuoranthene
.ND
390
ND
390
Senzo(a)pyrene
ND
390
ND
390
Indena(1,2,3-cd)pyrene
ND
390
ND
390
Dibenz(a,h)anthracene
ND
390
NO
390
Benzo(g,h,i)peryLene
ND
390
NO
390
2-Methytnaphthalene
NO
390
ND
390
Benzidine
ND
390
HD
390
Dibenzofuran
ND
390
ND
390
NO
390
ACID EXTRACTABLES
RD
390
PhenoL
NO
390
NO
390
2•ChtorophenoL
NO
390
ND
390
BenzyL Alcohol
ND
780
ND
390
2-NethyLphenoL
ND
390
ND
390
4-Methylphenol
NQ
390
ND
390
2-Nitrophenot
NO
390
NO
390
2,4-Dimethylphenal
NO
390
NO
390
Benzoic Acid
NO
1900
NO
390
2,4-Dichlorophenol
NO
390
ND
390
4-ChLoraaniLine
NO
390
NO
390
4•Chlorc-3-methylphenot
NO
390
ND
390
2,4,6-Trichlorophenot
NO
390
NO
390
2,4,5-Trichlorophenol
ND
390
ND
390
2-Nitroaniline
RD
970
No
390
3-Nitroaniline
NO
970
NO
390
2,4-Dinitrophenol
ND
970
NO
390
4-Nitrophenol
ND
970
ND
390
4-Nitroaniline
ND
970
NO
390
4,6-Dinitro-2-methylphenoL
ND
970
ND
780
Pentachtorophenol
ND
970
ND
390
3-Methylphenol
ND
970
ND
390
2,6- Dichlorophenol
NO
970
s and Definitions for this Report:
UNITS: u4/Kg
EXTRACTED: 07
DATE RUN: 0714Z98
ANALYST: PAC
INSTRUMENT: C
OIL. FACTOR: 1
NO = not detected at detection Limit

Page 19 TOXIKi
Received: 07/09/98
SAMPLE ID 1IY-6A
W CORP. REPORT York order # 98-07-173
Results by Sample
FRACTION 05A TEST CODE EPRNC NAME EXTRACTABLE PHC
Date & Time Collected 07/07/98 13.20, Category SOIL
EXTRACTABLE PETROLEUM SYDROCARONS
REPORTING
RESULT LIMIT
C9-C18 Aliphatics ND 100
C19-C36 ALiphatics ND 100
F
C11-C22 Aromatics ND 100
Surrogates %Recovery Surrogate Limits
Aliphatic Surrogate 52.2 40 - 140
Aliphatic Fractionation Surrogate 66.9 40 - 140
Aromatic Surrogate 51.4 40 - 140
Aromatic Fractionation Surrogate 66-4 40 - 140
Notes and Definitions for this Report:
EXTRACTED 07_ / 3/98
DATE RUN 07/18/98
ANALYST CK
INSTRUMENT HP7
DIL. FACTOR: 1
UNITS m41K4
NATRIx:
DRY WEIGHT: 85.1
1
HD = not detected at detection limit
D diluted out
INT = matrix interference
Hydrocarbon Range data exclude concentrations of surrogate(s) eiuting in that range
Hydrocarbon Range data are unadjusted for target analytes

Page 20 TQXlK0K CORP. REPORT York Order # 98-07-178
Received: 07/09/98 Results by Sample
SAMPLE ID TRIP ULM FRACTION D6A TEST CODE VPHNC NAME VOLATILE PHC
Date & Time Collected not specified _ Category NETHAiiOL
VOLATILE PETROLEUM HYDROCARBONS
REPORTING
RESULT LIMIT
C5-C8 Aliphatics (FID) NO 1.0
C9-C12 Aliphatics (FID) ND 1.0
C9-C10 Aromatics (PID) ND 1.0
TARGETIVPH ANALYTES
Surrogates % Recovery Surrogate Limits
FED Surrogate 72 70 - 130
PID Surrogate 70 70 130
Notes and Definitions for this Report:
UNITS: mg/kq
DATE RUN: 07/16/98
E%TRACTED:
ANALYST: SEP
INSTRUMENT: V3
DIL. FACTOR: 1
DRY WEIGHT:
ND a not detected at detection Limit
D = diluted out
INT ■ matrix interference
Hydrocarbon Range data exclude concentrations of surrogate(s) eluting in that range
Hydrocarbon Range data are unadjusted for target analytes

Page 21
Received: 0709/98
TOXIKOII CORP. REPORT
I Test Methodology
TEST CODE 8260 NAME PUR GEABLE ORGANICS VOA
Work Order # 98-07-178
EPA METHOD: 8260B: Gas Chromatography/Mass Spectrometry for Volatile Organics.
Reference: Test Methods for Evaluating SoLid Wastes: PhysicaL/ChemicaL Methods.
1 EPA SW-846 Final Update IIII, 1996. office of SoLid Waste, USEPA.
4
SOIL RESULTS ARE REPORTED ON A DRY WEIGHT BASIS.
TEST CODE 8M NAME A/SM EXTRACTABLES
EPA METHOD: 8270: Gas Chromatography)/ Mass Spectrometry for SemivoLatile
Organics; Capillary Calumn Technique.
I
Reference: Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods.
EPA SW-846 (Third Edition) 1986. Office of solid Waste, USEPA.
I
TEST CODE EPHNC NAME E][TRILCIABLE INC
METHOD:EXTRACTABLE PETROLEUM HYDROCARBONS
1
REFERENCE:METHOD FOR THE OE TERMINATION OF EXTRACTABLE PETROLEUM
HYDROCARBONS (EPH), MADEP-EPH-98-I
MASSACHUSETTS DEPARTMENT OF � ENVIRONMENTAL PROTECTION
JANUARY 1998
FOLLOWING THE GUIDELINES OF THE NORTH CAROLINA DEHR
TEST CODE IPE MS NAME ISOPROPTL ETHER
EPA METHOD: 624 Modified Volatile Aromatic Compounds
Reference: Methods for Organic Chemical Analysis of Municipal and
1
Industrial Wastewater. Appendix A. 40CFR Part 136.
Federal Register Vol. 49, No. 209, 1984.
I
TEST CODE MEX TS NAME METALS TOTAL EXT
REFERENCE:
EPA METHOD 3050: Acid Digestion of Sediments, Sludges and SoiLs. Test
Methods for Evaluating SoLid Waste Physical/ChemicaL Methods. SW 846,
3rd Edition.
' Analytical Method fvr [CP:6010A
' TEST CODE MOIST NAME 11 MOISTURE
EPA METHOD 160.2
Reference: Methods for Chemical Analysis of Water and Wastes.
EPA 600/4-79-020 (Revised, March 1983). EPA/EMSL, Cincinnati,
OR. I
ASTM METHOD D-2216 Moisture Content)

Page 22 TORIKON CORP. REPORT
Received: 07/09/98 Test Methodology
TEST CODE PPCBS NAME PESTTCI➢ES/PCI (SOIL)
EPA Method: 8080
Reference: Test Methods for Evaluating Sofid Waste: Physical/Chemical
Methods. EPA SW-M (Third Edition) 1986.
Office of Soiid Waste, USEPA.
TEST CODE VPHNC NAME VOLATILE PHC
I
METHOD:VOLATILE PETROLEUM HT➢ROCAR80H5
REFERENCE:METHOO FOR THE DETERMINATION ❑F VOLATILE PETROLEUM
HYDROCARBONS. MADEP-VPH-98-1
MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION
JANUARY 1998 I
FOLLOWING THE GUIDELINES OF THE NORTH CAROLINA DENR
Work Order # 98-07-178

Attachment 3
EPH Laboratory Reporting Form
r
Initial Calibration Date
Calibration Ranqds and Limits
'
N
C9 -C18 Aliphatics I
I l l 33 / o 0
C19 - C36 Aliphatics
I I a5 140
C11 -C22 Aromatics I
I L( 1 I / v U
NOTE: Please inc;ude units as accrooriate
Method of ❑uantitation (circle c e): Curve Average Response Factor
Calibration Concentration Levels
' _ . �; •:rya%
:/.;;;i:;' '::',•:+'''C•.x-'
'>s[;y,,
✓A-
}�c, .^1tp.�+4-'F%yF:1.��"
r T��yF�k%<:'c`,�'-•'?S.t]--ice'
L
N' • - !I .T
'�1/:'
C9 -C18
Aliphatics
3 I � ►�
300 1
C19 -C36
Aliphatics
col � i
[ d;
o t7 I 1
tau
16r;U i
C11 -C22
Aromatics
r-- i
340
5-[O I
1 7 00
3'fo V
NOTE Please indicate units as apcqjeGr[2te.
Calibration Check Date l
Calibration Check l
,..
S' are e
C9 -C18 Aliphatics I
3 o Q I
C19 - C36 Aliphatics
y o 0 I ,
C11 -C22 Aromatics
d ;S 0 1 L ILL
MDL = Method ❑eteCion Limit
ML = Mimimum Limit
RL = Reportable Limit
RPD = Relative Percent Difference
%FZSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve

EPHNPH Certification
l
Toxikon Order G 7�
VPH Soil Sample Collection Option
Option 1 = Fill line on vial Option 2 = Sampling Device Option 3 = Field weight of soil
Were all QAIQC procedures REQUIRED by the VPH method followed? Yes_ No
Were all QA/QC procedures REQUIRED by the EPH method followed? Yes_, --No,
Were all performancelacceptance standards for the required QAIQC Yeso
procedures achieved?
Details regarding any answer of "No" above are provided below.
' Were any significant modifications made to the EPHNPH methods
I
as specified in Section �11.3?
Yes_ No X
1 attest under the pains and penalties of perjury that, based upon my inquiry of those
individuals immediately responsible for obtaining the information, the material contained
in this report is. to the best of my knowledge and belief, accurate and complete.
Position: C f7
Signature: � �.. � w a,-� urr
Printed Name: 1�, , s�s 5p� y Date:T 5 I�l�
i

' I
PROJECT CHANGE ORDER
f
WORK ORDER # 9 Yb -� f 79 APPROVED tJ'
DATE OF REQUEST ? I �.196 DATE OF APPROV Z
CLIENT NAME TOX EMPLOYEE
CLIENT EMPLOYEE 5
BY PHONE FAX
THE FOLLOWING CHANGES ARE TO BE MADE BY TOXIKON:
110- -,?7 o eel
I
1 i �
1
i .
e

SUtiIIINIIRY OF ZONING DISTRICTS
NC: (Neighborhood Commercial District) provides for commercial centers in close proximity to
residential areas, offering limited commercial uses to satisfy the needs of the surrounding
1.
neighborhood. A 20,000 sq. ft. project floor area maximum applies. Permitted uses, some requiring
use permits, include: retail stores, medical clinics, day care centers, restaurants, convenience stores,
offices, banks, schools, car washes, residences, service stations, indoor commercial recreation, and
hotels.
GC: (General Commercial District) provides for a wide variety of commercial activities that are
' designed to be served by major thoroughfares. It is the intent of this district to provide sufficient size
and depth of property to meet business needs yet maintain safe traffic flows. Permitted uses, some
requiring use permits, include banks, business services, car washes, convenience stores, day care
facilities, night clubs, offices, hotels, retail stores, vehicle sales, drive-in theaters, schools, boarding
houses, heavy equipment sales, printing establishments and transmission towers.
SC: Sho > >ing Center District provides for orderly development of commercial services in a
unified grouping and encouragement of innovative development that is appropriately integrated with
adjacent uses. It is not the intent+of this district to encourage strip commercial areas, but rather a -
concentration of commercial activities with an overall design scheme. The district is intended to
provide a wide range of retail and service activities that serve many neighborhoods. The district is also
established to miniinize traffic impact; its use is intended for large lot developments and locations along
thoroughfares and at major intersections that are capable of handling the proposed traffic.
CBD: (Central Business District) is established to encourage intense development and pedestrian
activity through a mixture of uses appropriate to the downtown area. The standards of this district are
established to provide for a vital downtown economy that maintains Durham's focus as a commercial,
cultural and entertainment hub of the region while increasiniz livability. This district is intended to work
in tandem with the Historic Overlay District found in portions of downtown Durham. Permitted uses
include'artist galleries, studios, auditonums and exhibition buildings, banks, bed and breakfast inns,
boarding houses, business incubators, business services, colleges, convenience stores, retail, health
clubs, clinics, theaters, multifamily dwellings, mixed resldentlal/commercial projects, museums, night
clubs, offices, restaurants, transmission towers, and convalescent centers.
CT: (Co inntercial Trades District} provides for a limited selection of commercial and light industrial
activities that primarily serve other retail service or industrial businesses. The district is intended to
allow support services to these businesses, and to provide for uses with a retail component, but also
requiring outside storage. Permitted uses include: boat sales, business services, offices, warehousing,
travel trailer sales, transmission towers, contractors offices, freight terminals, heavy equipment sales,
commercial recreational facilities (indoor), retail fabrication businesses, storage yards, and vehicle
repair shops.

' SUMMARY OF ZONING DISTRICTS
01-1: ffransitioria[ Off -ice and Institutional Districts provides standards for Iow intensity office and
institutional uses inclose proximity to lower density residential areas to assure compatibility. Permitted
uses, some requiring use permits, include business services, single family dwellings, duplex and triplex
dwellings, offices, medical clinics places of worship, banks, bed and breakfast inns, convalescent
centers, day c facilities, retirement centers and schools.
0&I-2: (General Office and Innstitutional District) is established for employment and commurrity
service activities. Some support facilities and residential uses are also allowed when compatible with
surrounding uses. The district is designed for uses on sites near thoroughfares, since development of
' moderate to high intensity is allowed. Permitted uses, some requiring use permits, include artist
galleries, banks, business services, funeral homes, medical clinics, offices, bed and breakfast inns,
convalescent centers, day care facilities, transmission towers, boarding houses and hotels.
MU:(Mixed Use District rlides for integration of diverse but compatible uses into a single
' development that is unified by distinguishable design features. In addition to a mixture of compatible
uses, developments in this district, shall provide amenities and wallcways to increase pedestrian activity,
decrease reliance on individual vehicles, foster transit usage, enhance the attractiveness of Durham City
and County, improve the overall, quality of life, and provide for the welfare of the citizens. At least
' three use categories, each representing a minimum 20% of the total project, are required. A
Development Plan and a Phasing Plan are required as part of the rezoning application for the mixed use
1 district. The district is intended for implementation within the boundaries of the Urban Growth Area.
RSCH:(Research Park District provides an area for scientific research and development, for
1 training, and for production of p�ototype products, plans or designs. The purpose of such production
is limited to research development or evaluation of the merits of those products, plans, or designs. No
production for sale or use in production at a location off the premises is permitted. Offices and support
services are allowed. An initial threshold of 100 contiguous acres is required in order to create a
research park setting; however; additions to the zone may be made in increments of any size.
Permitted Uses include laboratories, passenger transportation terminals, pilot plants, research and
development facilities, restaurants, technical schools, small shopping centers, and transmission towers.
RAD: (Research Applications District) provides sites for research facilities and related
manufacturing, business and scientific activities. The district is intended to accommodate research
facilities, pilot plants, prototype production facilities and other manufacturing operations that require
the continual or recurrent application of research knowledge and activity as an integral part of the
manufacturing process. Tract size of 100 contiguous acres minimum is required, but additions may be
made in increments of any size. Permitted uses include laboratories, research related manufacturing,
passenger terminals, pilot plants, prototype production, research and development facilities,
restaurants, technical schools, and transmission towers.
I

SUMMARY GF ZGNING DISTRICTS
I-1: Industrial P:urk District provides for orderly development of manufacturing, research and
support activities in a unified setting. The district is intended to insure development which is
compatible with adjacent uses, and provides for a range of uses to be developed within an overall
1 design scheme as shown on an approved Development Plan, Permitted uses, some requiring use
permits, include banks, boat sales1 business incubator centers, commercial laundries, limited food
processing, hotels, laboratories, light industry, offices, research and development, transmission towers,
warehousing, passenger terminals, 1 d commercial recreation.
1-2: Light Industrial District provides for a wide range of light manufacturing, warehousing, and
wholesaling activities as well as offices and some support services. Standards of this district are
designed to minimize impacts on the environment and to assure compatibility with the surrounding
area. It is the intent of this district to offer sites for those industries whose operations, exposure,
' location or traffic have minimal impact on adjacent properties. Some permitted uses are: hospitals,
kennels, clinics, warehouses, night clubs, storage freight ternunals, labs, industries, offices,
transportation terminals, transmission towers, hotels, and recycling centers.
1
1-3: Ileayy Industrial District provides sites for activities which involve major transportation
1 terminals, and manufacturing facilities that have a greater impact on surrounding area than industries
found in the I-2 District. It is the intent of this district to provide an environment for industries that is
unencumbered by nearby residential) or commercial development. Permitted uses, some requiring use
permits, include foundries, freight terminals, industry, junkyards, transmission towers, warehousing,
' landfills and quarries.
D: A development plan designation (D) may be added to any rezoning request to indicate that the
physical layout of the site as indicated on the Development Plan (submitted with the rezoning request)
is a part of the rezoning petition. `Any significant change in the plan would require a new zoning
petition. A development plan is required in PDR, SC, and I-1 zones.
RD: Rural District allows agric ulturai operations and single family residences at low densities as
principal uses. For a single family divellirig, a 30,000 sq. ft., 100' wide lot is required. Permitted uses,
some requiring use permits, include kennels, manufactured homes, rest homes, plant nursery, riding
academy, transmission tower.
R-20: (Residential 20) is a single family residential zoning requiring a 20,000 square feet, 100' wide
lot for a single family dwelling with public utilities. (A 30,000 sq. ft. lot is required where public
utilities are not available.) Pernutted uses include: detached single family dwellings, public parks,
transmission towers less than 35 ft, in height, home occupations and family care homes. Major Special
Uses, such as convalescent centers, schools, and govemment facilities, are allowed subject to approval
by the governing body; and Minor Special Uses, such as day care facilities, group homes, transmission
3

SUMMARY OF ZONING DISTRICTS
towers between 35.- 200 ft. in height and places of worship, are permitted subject to approval by the
Board of Adjustment.
R-15: (Resid i'tial 15) is a single family residential district, with regulations designed to promote
single family development and to discourage uses that would be detrimental to single family detached
dwellings. A minimum 15,000 sq. ft., 90' wide lot is required for a single family dwelling. Permitted
uses include: detached single farrd dwellings, public parks. Uses allowed with a special use permit
include day care facilities, group horries, places of worship, convalescent centers and schools.
R-10: aResulentinI 10 District) is a single family residential zoning requiring a 10,000 square feet, 75'
wide lot for a single family dwelling. Permitted uses include: detached single family dwellings, home
occupations and family care homes. Major Special Uses, such as schools, are allowed subject to
approval by the City Council; and Minor Special Uses, such as day care facilities, group homes and
places of worship are permitted subject to approval by the Board of Adjustment (BOA).
1
R-8: (Residential 8 District) is a single family residential zoning for detached dwellings of a medium
density and requiring a minimum 8,000 sq. ft., 75' wide lot for each unit. The regulations are designed
to promote single family development and to discourage uses that would be detrimental to single family
detached dwellings. Permitted uses, some requiring special use permits, include parrs, day care
centers, group homes, places of worship and schools.
R-5: Mesidential 5 District) is a single family zoning for detached dwellings of a medium density and
requiring a 5,000 sq. ft., 50' wide nnnimum lot. The regulations are designed to promote residential
development and to discourage uses that would be detrimental to residential dwellings. Permitted uses,
some requiring special use permits, include parks, day care center group homes, places of worship and
schools. I
R-3: (Residen(hil 3 District) requires a 5,000 sq. ft., 50 ft. wide lot for a single family dwelling unit;
3,000 sq. fl. and 30 feet lot width per dwelling unit for a duplex, and 3,000 sq, ft. and 20 ft. lot width
per dwelling unit for a triplex. Permitted uses, some requiring use permits, include day care facilities,
places of worship, group homes, schools, bed acid breakfast inns, and the like.
1
PDR: (Planned Densi(v Residential) allows for design flexibility and is intended to encourage
efficient use of land and public services, promote high quality design that will provide a variety of
dwelling types as well as adequate support services and open space for residents of the development.
The district is intended to ensure irinavative development that is integrated with proposed adjacent uses
and compatible with existing patterns of development. The number folloNVIng the "PDR" is the
maximum density proposed for the site.
4

SUMMARY OF ZONING DISTRICTS
RIVI-12: (1Vlultifamily Residential District, maximum of 12 dwelling units per acre)
provides for multifamily dwellings at a maximum density of 12 units per acre. Other permitted uses
include single family, duplex and triplex dwellings, family care homes, public parks and home
occupations. Minor Special Uses such as bed and breakfast inns, boarding and rooming houses,
conference centers, convalescent centers, day care facilities, group homes, health clubs, retirement
centers and places of worship, are 1 ernvtted subject to approval by Board of Adjustment (BOA); and
Major Special Uses, such as colleges, commercial dorms, schools, and government facilities, are
permitted subject to approval by the governing body. - Changes to 20, 16, 12, 8
F/J-B Overlay: The requested site is located within the FIJ-B (Falls/Jordan Protected Area)
watershed protection overlay arealand the Urban Growth Area (UGA). Within the UGr, the
impervious surface limitation is 24% without stormwater controls; projects developed under the
High Density Option have designe{d and constructed to control the first inch of stormwater runoff.
tiITC: Major Transportation Corridor District is an overlay zone that establishes development
and planning standards, but does not affect the allowable land use as determined by the underlying
district. It is intended to enhance the economic and aesthetic appeal and orderly development of
lands adjacent to major transportation corridors. In each MTC district, a vegetative buffer is
required, the width of which is established at the time of MTC overlay establishment.
4
5

r� rr rr r s - . r■ rr ■r� �■ �■■i r r �r r� �r r■ r r■ r�
f
am
LEGEND.
vY{..a. C.T• ~4 •uaw
OT—a rY..u/. L—Ts
Y{!.. G.Q.TM •A!a
1O... a {QYAl Aar •��•-�
r •Aa4 F—S. CG*A- ....../
�•+iel.lo {oYsa.. +a•a•r
NOTICE TO LISERS-
Zoning Boundaries May
Change: Please Verify
Currant ZoNrg
eotxrdades, Stre¢t +
Names, 7,odiKm , and
Stream I at Data Wlth
Available Staff Persons -
PREPARED d MAINTAINE
THE DURHAM CITYICOUt
PLANNING DEPARTMEI`
60.3 1 60.4 51.3
703 1 70.4 j 71.3
Y • i
SCALE. 1'. fDO faat
1.600O
4+Ph "COO
a' �.4
is 94
SHEET: 74 2

q-G-18-1998 16=09
919 %8 1444 P.02i02
MAalb 0011 a+ MOW
wluAA 1 W. 11UNC71, III
wHAAA d U. lsavo=
A. MANY IRVl7F
MARINA LEANN Nemv..
WIL"" IL WEAnvau 0m, IIL
'"iTT 11. r.IUMgxxW
•�rJ Coaxed =Peew1. 1n aw.i.
pl.—" .wA Eiek+t. L...
BROWN & BUNCH
BROWN & BuNc"
ATTORNM. - AND COUNSELORS AT LAW
101 North Columbia Street
Chanel 1111 North Carolina ZT314
(919) 9ho-I11I
Paallailk: (919) 9(A1444
August 18, 1998
VIA TELECQPIE.R 919.596.0578
11lSIl68l.!?tYli.6
3101, Triwihi *x)IxVAtU1
Uri[YGICMTT TOWER. VIM r"R
(4nv) 4-m-y7no)
FA[7 WLE (919141901IF.
iV1l1!tt:M [IF'i'Sf:l'
7Y[I(1 NCIRTIIPAA7[
4"0 FALI %CAr Till[ row.11R Ht "M1, tt:71! Ilr1
(STAKNT afr LUDIS Z7609)
IKXT 0MCE Do% 14(C9
ItAf. CH. NOWnI CAROLMA 2%39.9M09
(41v) MTH.W vu
FAC861ILE I719" STPLA)GI
Mr. Fames Stahling, L.G.
Senior Geologist
EMS Environmental, Inc.
117 South Hoover Road
Durham, NC 27703
RE: 3737 Chapel Hill Boulevard, Durham, NC
(former location of Uzzle Cadillac-oidsmobile-GMC
Truck, Inc.)
Dear Mr. Stahling:
You have requested some additional information concerning the
historical and anticipated use of 3737 Chapel Hill Boulevard (the
"Site"). The Site is zoned "general commercial"" Historically, it
has been used as a new and used automobile dealership and for
ancillary services suchlas automobile repair, service and painting.
To my best information, this Site has been so used for
approximately 30 years! In addition, all contiguous parcels as
well as tracts in the immediate vicinity are as similarly zoned and
are all in industrial/commercial use. We are not aware of any
residential use of any lot at or below the gradient of the Site
within 1,500 feet.
There is no present or anticipated plan to
' any purpose other than* automobile dealership.
there is no plan, at present or anticipated, to
into a daycare, motel or residential use.
I hope this letter, is helpful. Please let me
' any additional information.
ccs/cf
' cc: Dan W. Uzzle, Jr.
Granville L. Uzzle
11667/02\L\033STAHL
very truly yours,
usa the Site for
In particular,
convert the Site
know if you need
WN & +BH
ar es rown
TOTAL P,022

MONITORING WELL INSTALLATION LOG
MONITORING WELL ID: MW-2 INSTALLS❑ BY: REDS -DRILLERS
_ I
EMS PROJECT* 7239 NO. 1436
I
SITE LOCATION: UZZLE CADILLAC-OLDSMOBILE DRILLING METHOD: 4 1I4" IQ HSA
DRILLING
LOCATION: ADJACEN I TO FORMER VIRGIN OIL LIST DATE INSTALLED: 716198
BORING LOG
MONITORING WELL
DEPTH
DESCRIPTION OF
PID
(FT.)
LITHOLOGY
(ppM)
.FLUSH -MOUNT
MANHOLE COVER
0.0
CONCRETE
LOCKING CAP
GREEN SANDY SILT
10.4
BROWN SILT
r
GRCUNCWATER DEPTH 23 FEET
BELOW GROUND SURFACE ON
CEMENT
i114M
�
CONSTRUCTION NOTES
Pvc
I
5.0
CASING /�
{
I RED -BROWN SILTSTONE
1
CASING TYPE PVC
6.4
CASING I.D. 2"
/ I /
SCREEN TYPE PVC
E
aeNTONITE PELLET - j i-
v.1=
SCREEN I.D. 2"
I
�[
SEAL - "mJ1I mI
I
SCREEN INLET SIZE
�10.0
-———— — — — — ——
•--
CEMENT GS TO 1
�^
BENTONITE I TO 13
GREY SANDY SILTSTCNE
SAND 1.3 TO 13.6
PVC RISER 0.411 TO :.37
SANG PACK
f SCREEN 13, TO 113,
TERMINATED BORING AT
13 FEET
.
7 5.0
1
PVC SCREEN —�
�J
NOTE: MONITORING
WELL NOT TO SCALE
{ ALL MEASUREMENTS
REFERENCED FROM
GROUND SURFACE

1
' NORTH CAROUNA OEPARrwwr of NATt1RAL RESOURCES At�43 CD/.OAROrY DEVIELOPMDrr
orvLVON OF ENVtR0NL4ENfAL 1MNAGDAENr - GPOUNDWATS; SECTION
P.O. BOX 77687 - RALEIGKIII.C. 27a1 i. PHONE (91a) 733-sow
WELL CONSTRUCTION RECORD ���- _Z
FOR OFFICE USE 014LY
Quad. No. Serial No.
LaL Long- Pt
Minor Basin
Basin Code
Header Ent. GW-1 Ent
DRILUNG CONTRACTOR �5 D S 1 - — -
% 3 G'
STATE WET CONS T RCfCTiQN
RfLLc t REGISTRATION NUMBER '
i
PERMIT NUMBER:
WELL
1. LOCATION: (Show SkelCh of The location betl w)
Nearest Town: -Tx• r-.
County:
3737�C ,r 1 hl: !l y31y�
-
Oeom DRILLING LOG
(road, Community, or Subdivision and Lot NOJ
From To Formation ❑escriation
OWNER - _ [J� Z,l� ['�.k�'fl,�
rJ1�s,�1cly, J.a_.
3 7 -7 C. L . � l �F�,-/I .3/wa'
G D. �c) C,Iz
AODRESS _
(Street or „ ute No.)
City or Town state
ZiD Code
L S r f'
3. OATE DRILLED USE OF WELL.
Al
TO TA, DEPTH l�• 3, CJi iiNGS COLLECITED 0-Yes F% No
I
.DOES WELL REPLACE EXISTING WELL? ❑ Yes FU NO
STATIC WATER LEVEL: 72 FT. C above TOP ❑F CASING.
' ;;11i � 2j below
SQ
TOP OF CASING IS _,__`F T. APeYG LAND SURFACE.
bo!100
,. YIELD (gpmh METHOD OF TES.
f
tWATE- ZCNES Weotti):
-
CHLORINATION: Tyoe Amount
`] CASING:
Wall Thickness
tf additional SRace is needed use tack of ldrrr.
❑eoth Diameter or We1g'1VFL Material
G. ��' 1 •z �7c ���C
- -
_4oc.� T IoN sK�g�
From ' To , =L I
(Shaw direction and ais:ance from at least two State Roacs,
From T❑ ct I
or •omer mao reference points)
From To Ft.
GROUT.
I
Gealh Material MetnoC
From _Cr_:5� ToFt_ CX7
r^vrrL
Frdm To� Ft.^
' Cen:n Diameter
Slot Size Malenal
+
y
From 1.31 To 1 / 3r F,,
in. JrL
Frzr.n To F;
From ToFt. RL rL
:2. GRAVEL
PACK:
Deom Size
malerial
=rom A 3 4�F G v
t.
:P
111 T'�w'3 L/v�e✓' Z
T
II
`rrpm Td F;
'a. REMARKS:
1 DO HEaEEY CERTIFY WAS
THAT THIS WELL CONSTRUCTED IN
ACCOROANCE WITH 15 NCAC 2C. WELL. CONSTRUCTION—
ST aNpARpS• AND THAT q COPY OF TH15 RECORD HAS BEEN�FPROVIOED TO WELL OWNER.�Jr3
9 $SIGNATLIRE-OFACT
R AGENT DATE

MONITORING WELL INSTALLATION LOG
I
MONITORING -WELL ID: MW-3 INSTALLED BY: REDS -DRILLERS
I
EMS PROJECT #: 7239 NO. 1436
1
SITE LOCATION: UZZLE CADILLAC-OLOSMOBiLE DRILLING METHOD: AIR ROTARY
DRILLING t6" ROLLER CONE)
LOCATION: ADJACENT TO FORMER WASTE all. UST DATE INSTALLED: 716198
BORING LOG MONITORING WELL
DEPTH DESCRIPTION OF
(FT-) LITHOLOGY PID FLUSH -MOUNT
0,0 (PQM) f MANHOLE COVER
j CQNCRE7 f ��_ _LOCKING CAP k
7/ GRDUNDWATER DEPTH 2.12 FEET
BELOW GROUND SURFACE ON
7l14M
PINK TO BROWN SILTY
FINE TO MEDIUM SAND,
50 TRACE COARSE SAND
RED -BROWN SIL 1 Y CLA
I
2.6
i
CEMENT
PVC
CASING
5EN70NI7E PELLET
SEAL
I SAND PACK
BORING TERMINATED AT 13 FEET
alowYeW=1=12i
f f
CONSTRUCTION NOTE:
CASING TYPE
PVC
i
CASING I.O"
2"
f/
i
ff
SCREEN TYPE
PVC
�=
{ r n
SCRreN I.D.
2"
�lr
{I
SCREEN INLET SIZE
0,01..
CEMENT GSTq
0.5
" f _
BENTONITE 0 5
TO �• I
SAND 1.1 TO
13
'
027
TO 1.10
]PVCRISER
SCREEN t i0T0
.t0
.�ti.
NOTE: MONITORING WELL NOT TO SCALD
ALL MEASUREMENTS REFERENCED FROM
GROUND SURFACE

I
' 14ORTH CAROU A DEPARTMENT OF NAn1RAL RESOURCES AND C)M&A"-rY DEVELOP1.1ENT
DrAVON OF EWRONMENTAL MANAGEMENT - OROUNOWATER SECTION
P.O. BOX 27567 , p/X.FIG1-I.,N.C, 27G1:. PHONE LatOy 733-60E.7
1 I _
WELL. CONSTRUCTION RECORD �� 3
FOR OFFICE USE 04LY
Quad. No. Serial No.
Let. Long_ pc
Minot, Basin
Basin Code
Header Ent. GW-1 Ent.
S
pR1LLIFtG CONTRACTOR
I
S I A I ti WCI- L CONSTI=iU'vi iQN .
tRILLER REGISTRATION NUMBER � � �3 � _
PERMIT NUMBER:
1. WELL LOCATION: (Snow skettr:t at me location below)
�t..1
Nearest Town: _ _
County:
373'7 c4 x I w`II 31Y
--- - _ w
—
Depm DRILLING LOG
{Road, Community, or SubdiVisi and No.]
From To Formation Description
y�Lo(
�. OWNER �� fr��S.. r'� L - ©1 �C$�� �D� _
ADDRESS 3 �3� C �t 1 fir,"ll rlr�_._-
C7 .,, C� S.•L�iz-f __�_
LStreel or cute No!1
r• 1 �Jrai�/ 5H
City or Town State
Zip Code
3. DATE DRILLED r g USE OF WELL•
foR
!Tc[cr Or! 1.
�- TOTAL DEPTH 11. 1 CUTTINGS COLLECTED 0 Yes I.a
i
_1,3 •7.L9'
:. DOES WELL REPLACE EXISTING WELL? C1 Yes No
STATIC WATER LEVEL: %. FT. C aooYe
l
TOP OF CASING.
TOP OF CASING 1S �, G �_ . i A OVE low
r oe
SURFAC_
i. YIELD (vrrt}: METHOD OF TEST
'. WATc= ZONES (aeoth): I
I
-
�C`4LORINATION-, Tyne
7 CASING:
Amount
-f Death Diameter
From Z I To /, rO FL •Z "
From Tp Ft.
Wait I Thickness
or Weignt/FL Materfaf
_ Ic l yam' v'G
From T❑ Ft.
GRGU i
Depm Material Method
=rom 6S To 7 =t. �l'tr pot. -I "
' Oeutn Diameter slot Sits Maleriai
=ram 0 C? To KL I �' c+r' in. Fv[
F rJ r:'I a Ft. in. I -
From i O fi% in_ irL
:a. GRAVEL PAC`{:
If additional space is needed use back of lot=
LOCATION SKETCH
(Show direction and distance from at least two State Roads,
or otn r map reference pointz)
S r �
51r o e �-
IY
rY
C
' Denln Size material
Prom -�, 7o 1.3 Ft.- 1►lt+6 r51;/Ild_12
Prom To Ft.
's. REMARKZZ
I D❑ HEREBY CERTIFY THAT THfS WELL WAS CONSTRUCTED IN ACCQR'--ANCE WITH 15 NCAC 2C, WELL -CONSTRUCTION._
' STANDAROS. AND THAT A COPY OF THIS RECORD HAS BEE RQVIQED TO 71-IE WELL. OWNER,
4
SIGNATU85bF CONTRACTOR OR AGENT DA T E

MONITORING WELL INSTALLATION LOG
f
MONITORING -WELL lD: MW"4 INSTALLED By: AEDS-DRILLERS
EMS PROJECT #: 1239 NO. 1436
1
SITE LOCATION: UZZLE CADILLAC-OLDSMOBILE DRILLING METHOD: AIR ROTARY
DRILLING 1 6" ROLLER CONE
LOCATION: ADJACENT TO SERVICE DEPARTMENT DATE INSTALLED: 7r7198
BORING LOG
MONITORING WELL
DEPTH
DESCRIPTION OF
PID
(FT.)
LITHOLOGY
(PpM)
FLUSH -MOUNT
MANHOLE COVER
0.�
CCNCRET>: - I LACKING CAP
1 I 1
RED -BROWN SILTY CLAY
7.8 I/
AND CLAYEY SILT CEMENT - f
PVC l� V CONSTRUCTION NOTES
5. o\
CASING / /
+
I
GROUNOWATER DEPTH 5.32 FEET ` / CASING TYPE PVC
BROW GROUN❑ SURFACE ON 7114M
cAslNc I. D. 2"
I
Ir1rI � SCREEN 'YaE PVC
{
GREY FINE SAND 15.1 J� BENTON TE PELLET — { I SCREEN I.D• 2"
I "Irl
SCREEN INLET SIZE 0,01"
10_0
CEMENT GS TO 1
BENTONITE 1 TO 2
• - SAN❑ 2 TO 14 5
_� _
— — — — T — II � - PVC RISER 03- Tp 2.a9
_
SAr1p PACK SCREEN 2 a9 TO 12 49
I
_
GREY FINE CLAYEY i 1
I
I
SAND 16.3
i 15.0
TERMINATED BORING AT 14.5 FEET ] �' •" _ "�
PVC SCREEN
I
I
� I •- _
I
NOTE: MONITORING WELL NOT TO SCALE
ALL MEASUREMENTS REFERENCE❑ FROM
I
GROUND SURFACE
I

' NORTH GRCLI A DEPARTMENT OF NATLrrL RE.SOURCE.S AM COLOAARXTY DEVELOPWIENT
or%gNON OF ENVtRpNPAEH TAL. mANAG T - GFICLINQWATUR 5:ECn0N
P.0). BOX 216at - RALE]GKN,C. 2751S. PHONE (7I9] 733-,60E3
WELL CQNSTRUCT1CN RECORD
DRILLING CONTRACTOR
FOR OFFICE USE Of+ LY
Cued- IJv. Serial No.
Lai. Long_ pc
Minor Basin
Basin Code
Header Ent. GW--I Ent.
j l STATE WELL CONSTRUCTION
RILLER REGiSTRA T ION NUMBER ■ � � � PERMIT NUMBER:
I '
t. WELL LOCATION: (Show Sket l of me Location below)
Neares, Town-.
--
'3�7'3�
(Road, Cornmunity, or Suadivision anC Lot No.]
aL
OWNER
ADORE SS _ 237
' {Street or Roue NoJ `
City or Town State 1 Zia Cooe
a DATE DRILLED' USE OF wE! L. /j1]� .il.�f�i
TOTAL 0E?T1 [ - - �1 CUTTINGS COLLECTED ❑ Yes 0 No
Ir�. DOES WELL REPLACE EXISTING WELL? ❑ Yes k`p No
STATIC WATER LEVEL: - FT. L� above I TOP OF CASING.
1 u below
TOP OF CASING :S =•2 FT LAND SURFACE.
'L? 0" 1
7- YIELD (earn} METHOD OF TEST I
' WATER ZONES idepth7:
CHLORINATION: Type Amount
CASING:
Wall T hiCicnaS
Depth Diameter or WeignVFL Material
1 I r
From _0 - To FL
From T❑ F,..
From -
County:
Oeorm
From To
DRILLIMr, I nr:
Formation Description
�a LT+Ii'
tf additional stance is needed use back GI IomL
LOCATION SKETCt-?
iShow Crection and distance Irom at least two State Roads,
or other man reierence points)
GRCLIT:
Dent t Materials Metnec
From
From 1 Ta L =t. `�'.7U:�le► Q �r
' f► Depth
.From �. 7�7 j p)z I � r 1.
From To Ft.
From To G;,
Diameter Slot Size Material
� rl
GRAVEL PACK:
'r Depth Size Material
From 2 To_/yS Ft. 7�,.""Ve-
From TO- Ft.
�. REMARKS;
IS
I
1 DO HE=;E3Y CERTIFY THAT THIS WELL WAS CONSTRUCTE❑ IN ACCOPOANCE WITH 15 NCAC 2C, WELL. CONSTRUCTION —
STANDARDS. AND THAT A COPY OF THIS RECORD HAS BEEN PR IDEA TO t IE WELL OWNER,
SIGNATURE-OVONTRACTOR OR AGENT DATE

i
MONITORING WELL INSTALLATION LOG
I
MONITORING -WELL ID: MW-5 INSTALLED BY: AEDS-DRILLERS
I.
EMS PROJECT #; 7239 NO, 1436
1
SITE LOCATION: LIZZLE CADILLAC-OLDSMO BILE DRILLING METHOD: AIR ROTARY
DRILLING I • (6" ROLLER CONE) _
LOCATION. ADJACENT TO FORMER FORMER DATE INSTALLED: 7f7198
DIESEUGASOLINE UST
BORING LOG
I MONITORING WELL
DEPTH
DESCRIPTION OF
p10
(FT.)
LITHOLOGY
(PPM)
/ UNT
MANHOLEFLUSH-MCOVER
0'0
CONCRETE
LOCKING CAP
GROUNDWATER DEPTH 2 22 FEET
I
9ELOW GROUND SURFACE ON 711AM
I �
F' I
CEMENT
j �
�j//
CONSTRUCTION NOTES
Pvc
5-0
RED -BROWN TO
16.3
CASING--��
'' J
F175
BROWN SILTY CLAY
I
` ;'
1V/
CASING TYPE PVC
I
CASING I.D. 2"
SCREEN TYPE PVC
I_
se4TONITE PELLET
SCREEN I.O. 2.,
I
SEAT
j
�
SCREEN INLET SIZE 0.01 "
10.0
GS 1
CEMENT TO
BENTONITE 1. TO 2
SAND 2 TO 13
PVC RISER 03 To 205
RED -BROWN
SILTSTONE
SAND PACK
SCREEN :•03 TO 12.05
_
TERMINATE D BORING ATI
i
13 FEET
15.9
PVC SCREEN
_
- -
NOTE:
WELL NOT TO SCALE
MONITORING
ALL MEASUREMENTS
REFERENCED FROM
GROUND SURFACE
i

I
NORTH CAROUNA DEPAfrnAa4T OF NATLkAL RESOURCES AM COAYAR7a4Y DEVELOP"aff
DPn&ON OF etWAGf¢WIETITAL MAHAC9A&lr - GRCLMWAi$1 SWnOM
t
A.Q. BOX 276a7 - RALEtGKH.G 2Tel t. PHONE ('Q191 733-d00.3
1 l
WELL CONSTRUCTION RECORD �n
l' ►W
DRILLING CONTRACTOR _ ,rf _
DRILLER REGISTRATION NUMBER 11136 -
I
1. WELL LOCATION: (Show Sketch OI the location below]
Heares: Town- �J f-11 I InI
37 3-2C4 �,- / ffyl
(Road, Commiini[y, or Subdivision and Lot No.) �+OWNEn uz-ZI8- (f--e , _ a/�F rTc��. /sue
ACDRE SS 3'7 -7 C 4 ,e / rI ' _
' (5Lree[ ❑ RoU[e No.
City or Town state Zip Code
2 DATE DRILL E7 �� USE OF WEL'_.
1
,. TOTAL DEPTH /2 • O CUTTINGS COLLECTED ❑ Yes & No
5. DOES WELL REPLACE EXISTING WELL? ❑ Yes [KNO
'STATIC WATER LEVEL: I. 9 L FT. 0 above TOP OF CASING,
TOP OF CAsiNG 15 Q• 3 F- A below �. A$�i�lAt�Q SURFACE
o� /swa
7. YIELD (sprt- METHOD OF TEST �
�. WATER ZONES (oedtn):
tCHLORINATION: Type Amount
CASING: I
Wall Mickness
Death Diameter or weignuFL Material
n „ L
From Q. 3 To ,Z 'as Ft� C %alp
From To Ft.
=Tom Td Ft.
I
GRCL•T: 1
Depth MaIerial Metnod
From TC � Fi. ���.144��
' From To FI. C.r✓>rrr�C'.f[j eTv/'
Ceotn Diameter Slat Size Materai
From 2 - 05 io F: 'Z ir, 61I0/ ' in.
Frdm To FL it
To Ft.
". GRAVEL PACK:
FOR OFFICE USE OfJLY
Quad. No. Serist No.
Lat. long. Pc
Minor Basin
Basin Code
Header Ent. GW-I Ent.
STATE WELL CONSTRUCTION
PERMIT NUMBER:
County:
Depth DRILLING LOG
From To Formation 06 riouon
Q, ! ., e farcku iJ
It additional space is needed use back oI lorrn..
_LOCATION SKETCH
(Shaw direction and distance tram at least two State Roads,
or other ma❑ reference points)
nnr�
•V
A4
- Ceo[h Size ,rM�aterial
From C. io I "r,IVL H..� _ [Lim L
From To F[.
14. REMARKS: V
1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCOF+7ANCE WITH 15 NCAC 2C. WELL. CONSTRUCTION—
, S T ANDAAOS. AND THAT A COPY OF THIS RECORD HAS BEE ROVIOED TO THE WELL OWNER-.
I � 4 4� 6
SIGNATURCit7F CONTRACTOR OR AGENT DATE

' WATH CAWXJP" DVARTLC?ff OF NATIAi RESOURCES "10 C0&&AU* Y IXVo.0ft4 a
OWL51CM CF ENV1WXJM 1TAL VANACEMDff - GRW40WATE R Sr --=ON
I
P.O. 5OX 27$e7 - FLAU GKS1 G I7e11. PRONE L9791 73a-E06.3
I I
WELL CCNSTRUCTIUN RECORD
FOR OFFICE USE ONLY
Quad. No. seriai No.
Lat. Long. PC
Minor Basin
Sasin Code
Header Ent. GW-I Erst.
DRILLING CONTRACTOR C
STATE WELL CONSTRUCTION
&RILLER REGISTRATION NUMBER �? � PERMIT ;ZT3 EER:
1. WELL LOCATION: {Show sketcri or The location vetoes)
(Road, Community, or Subdivision and Lot Na.}
OWNER U-
r
ADDRESS 3-73 -%7�'{
' LStre$t or Route Na.:{
1`" i. r A ", tyC. I
City or Town State I Zip Code
3_ DATE ❑RILLED - ��1 USE OF WELL- Z--1
' TOTAL DEPTH f`2 2-6: CU+TINGS COLL ECT=D Cl Yes fg
i
E. DOES WELL REPLACE EXISTING WELL? ❑ Yes ❑ No
STATIC WATER LEVEL: '3 y- = T. C above TOP OF CASING.
� 70P OF CASING IS ."-� T. A,��'SB{pw- LAND SURFACE
be /ecj
7. YIELD (��mr METHOD OF TEST
WATEP ZONES [aeotri):
I
�C`iLORiNATION: Tyne
CASING:
Amount
Deom Diameter
1 • 'J�� G yy
From '!.� To L •�
From 10 .
'. GROUT:
T a...
Coun=y: — L r4
Deorn DRILLING LOG
From To Formation Descriolion
C� (3 S Co,u I.7 t
r
Waif Thickness If additional space is needed use back of toetn.
or Weignt/FL Material
LOCATION SKcTC?I.
(Show direction and distance from at least two State Roacs,
or ,dtrier man reierence points)
�+ G Oeatn Mate_riall Metnoc
From C"rS T0FL / 1
' From To Ft. c,i-
SCREEN:
Denin Diameter Slot Size Ma,enal
7 `f 'f r� I C
rrOm Lr V� jo i'�• �•-J t. in. in.
' Frain
T6
Ft.
irL
in.
From
To
Ft.
in.
in.
". GRAVEL PAC`::
Deorn
Size
Material
From
To
Gt.
�. REMARKS:
41
' 1 DO HERESY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCO710ANCE WITH 15 NCAC IC, WILL• CONSTRI1CTtON—
STANOARpS, AND THAT A COPY OF THIS RECORD HAS EN PROVIDED TO 7HE WELL OWNER_ �7'I�'�
SIGNATkTRE'OF CONTRACTOR OR AGeNT DATE

1 -
Page 1
Received: 07/15/98
TCD[IKOV CORP: REPORT wont order 9 98-07-2A7
O7/M/98 13:44:35
REPORT EMS ENVIRONMENTAL SERVICES PREPARED TOXIKON CORPORATION
TO 117 S. HOOVER RD - BY 15 WIGGINS AVE
DURHAM HC 27703 BEDFORD, MA 01730
[phone] FAX 0578
ATTEN JIM STAHLING
CLIENT EMS NC SAMPLES 6
COMPANY ENS ENVIRONMENTAL SERVICES
FACILITY 117 S. HOOVER RD
DURHAM,_NC 27703
' WORK ID UZZLE-7239
TAKEN 7 14 98
TRANS
' TYPE WATER
P.O. #
INVOICE under se rate cover
SAMPLE IDENTIFICATION
01 MW-2
02 MW-3
13 MW•4
' 04 MW-5
05 MW-6
06 MW-3
1
CHRTIFIEQ, Y
ATTEN PAUL LF7RFRG
PHONE [phone] CONTACT MARKETING
1.
MA CEPT # M-MA064: TRACE METALS SULFATE.CYANIDE,RES. FREE
CHLORINE, Co. TOTAL ALK., TDS,PH THMs, VOC, PEST —NUTRIENTS.
DEMAND, O&Q, PHENOLICS, PCBs - CT DHS #PH-0563, NY #10778
FL HRS E87143 NJ DEP 59538 NC.D'NR 86 88002 NH 2O4091-C.
VERIFIER Y:
TEST CODES and NAMES used on this workarder
625 A/BN EXTRACTABLES WATER
CR CHROMIUM
EPHRC EXTRACTABLE PHC
MEX NC North Carolina Acid Ext.
PB LEAD
TICSV T.I.C. Semi-vo(atiles

I
Page 2 TOXIKOW CORP.
REPORT York
order # 98-07-267
Received: 07/15/98
Results by Sample
SAMPLE ID WW-2
FRACTION 01A
TEST CODE 62.5_ NAME A/BN
EXTRACTASLES_WATER
'
Date & Time Cot(ected 07114198 11:55;00
Category WATER
' PARAMETER
RESULT LIMIT
PARAMETER
RESULT LIMIT
BASE NEUTRAL EXTRACTABLES
bis(-2-ChtoroethyL) ether
ND
10
1,3-Dichlorobenzene
ND
10
Chrysene
ND
10
1,4-➢ichlorobenzene
ND
10
Di-n-octyL phthalate
ND
10
1,2-Dichlorobenzene
ND
10
Benzo(b)fluaranthene
ND
10
' bis(2-Chloroisopropyl] ether
ND
10
Benzo(k)fluoranthene
ND
10
N-Nitroso-Di-N-Propylamine
ND
10
Benzo(a)pyrene
ND
10
Hexachteroethane
NO
10
Indeno(1,2,3-cd)pyrene
ND
10
Nitrobenzene
HD
10
Dibenz(a,h)anthracene
ND
10
Isophorone
NO
10
Benzo(g,h,i)perytene
ND
10
bis(2-Chloroethoxy) methane
NO
10
ACID EXTRACTABLES
RESULT LIMIT
1,2,4-Trichloroben2ene
ND
10
'
Naphthalene
NO
10
Phenot
ND
10
Hexachlorobutadiene
NO
10
2-ChlorephenoL
No
10
Hexach[orocyciopentadiene
NO
10
BenzyL ALcohot
ND
20
' 2-Ch[oronaphthatene
NO
10
2-Methylphenot
ND
10
Dimethy( phthalate
RD
10
4-Methylphenot
ND
10
Acenaphthytene
NO
10
2-Nitraphenot
NO
10
' Acenaphthene
ND
10
2,4-Dimethylphenol
ND
10
2,4-Dinitrotoluene
_�ND
10
Benzoic Acid
ND
50
2,6-Dinitrotoluene
ND
10
2,4-Dichiorophenol
N4
10
Diethyiphthatate
ND
10
4-Ch(aroaniline
ND
20
4-Chiarophenyl phenyl ether
ND
10
4-Chtoro-3-methylphenoi
ND
10
Flourene
ND
10
2-Methylnaphthalene
ND
10
N-Nitrosodiphenylamine
ND
10
2,4,6-TrichlorophenaL
ND
10
' 4-Bromophenyt phenyl ether
NO
i0
2,4,5-TrichLorflphenal
ND
10
Hexachiorobenzene
HD
10
2-Nitroaniline
ND
25
Phenanthrene
ND
10
3-NitroaniLine
HD
25
Anthracene
ND
10
2,4-➢initrophenol
ND
10
'
Di-n-butylphthalate
ND
10
4-Nitrophenot
ND
10
Ftuoranthene
E ND
10
Dibenzofuran
ND
10
Pyrene
NO
10
4-Nitreaniline
ND
10
' Butyl benzyi phthalate
ND
10
4,6-Dinitra-2-methylphenoL ND
10
3,31-Dichlorobenzidine
RD
10
Pentachlorephenol
ND
10
Benzo (a) anthracene
ND
10
Benzidine
ND
10
' bis (2-ethythexyL)phthalate
I ND
10
N-Nitrosodimethylamine
ND
10
Additional Ana[ tes
1,2-Diphenylhydrazine
NO 10
' 3-Methytphenol (m-Cresol)
ND 10
1
Notes and Definitions
for
this Report:
Units:....
ugll
'
EXTRACTED........
--- 07116198
DATE RUN.........
07/17198
ANALYST .........
PAC
___
'
INSTRUMENT.......
F
DILUTION FACTOR..
1
ND = Not Detected at
Detection Limits.

Page 3
Received: 07/15/98
SAMPLE ID RW-2
TOXIKOK CORP: REPORT York Order R 98-07-267
1
Reesults by Sample
I
FRACTION 01A TEST CODE EPHNC NAME EXTRACTABLE PHC
Date $ Time Co[[eeted 07/14/98 11:55:00 Category PATER
EXTRACTABLE PETROLEUM HYDROCARONS
REPORTING
RESULT
LIMIT
C9-C18 Aliphatic&
162
100
C19-C36 Aliphatics ND
100
C11-C22 Aromatics 180
100
Surrogates
7.Recovery Surrogate Limits
Aliphatic Surrogate
55.8 40 -
140
Aliphatic Fractionation Surrogate
70.4 40 -
140
Aromatic Surrogate
52.9 40 -
140
Aromatic Fractionation Surrogate
61.1 40 -
140
Notes and Deflinitions for this Report:
EXTRACTED 07/ 6/9$
DATE RUN 07/27/98
ANALYST CK
INSTRUMENT HP7
DIL. FACTOR: 1
UNITS
ug/L
MATRIX:
DRY HEIGHT:
ND not detected at detection limit
I
D diluted out
INT ■ matrixlinterference
Hydrocarbon Range data exclude concentrations of surrogate(s) eluting in that range
Hydrocarbon Range data are unadjusted for target analytes

Page S TOXIXW CORP. REPORI Work Order # 98-07-267
' Received: 07/15/98 Resutts by Swpie
SAMPLE ID nW-2 FRACTION 01A TEST CODE TICSV NAME T.I.C. Semi-volatfles
' Date $ Time Collected 07/14/98 11:55.9D Category WATER
' SUMMARY OF NBS (38I700+ anaLyte version, ApH L 182)
LIBRARY SEARCH RESULTS OF NONTARGETED PEAKS WITH ESTIMATED
CONCENTRATION OF TENTATIVELY IDENTIFIED COMPOUNDS
' BASE NEUTRAL
SCAN ?LAME OF MF ASSESSMENT EST.
' NUN. COMPOUND PUR RS ISO UK CONC. CAS RT
(1) (2) # (3)
205
UNKNOWN 32 _
_ x 23.46
* 6.70
406
UNKNOWN 7 _
_ x 5.85
* 10.10
421
UNKNOWN 58
_ X 4.57
* 10.35
456
UNKNOWN 60 _
I
_ 8.66
* 10.94
Notes and Definitions for
this Report:
UNITS............. u�L
DATE............ 07/17/98
SPECTROSCOPIST... PAC
(1) RS - Reasonable Identification •
[SO- Isomer or similar compound
UK - Unknown, not in NBS Library
(2) Calculatetl vs nearest eluting internal standard
as a simple ratio / proportion.
(3) RT vs dif+Luarobiphenyl or d**10-phenanthrene.
* This shall mean the assessment of the library search
by an experienced mass spec. interpretation specialist
which would by his/her concurrence be a good identification
using WA85-J664, J680, Task V on page A-3 & Task III pg 2-3
COMMENTS

1
Page 5 TUXIXON CORPI REPORT York Order # 98-07-267
' Receivod: 07/15/98 Results by Sample
I
SAMPLE lD Hi!-3 FRACTION 02A TEST CODE 625 NAME A/BN EXTRACTABLES PATER
' Date & Time Collected 07/14/98 11:35:00 Category WATER
PARAMETER
RESULT LIMIT
PARAMETER RESULT
LIMIT
BASE NEUTRAL EXTRACTABLES
bis(-2-Chloroethyt) ether
ND
10
1,3-Dichlorobenzene
HD
10
Chrysene
ND
10
1,4-Dichlorobenzene
HD
10
Di-n-octyl phthalate
ND
10
1,2-Dichlorobenzene
ND
10
Benzo(b)fluoranthene
NO
10
t
bis(2-ChLoroisopropyl} ether
HD
10
Benzo(k)fluoranthene
ND
10
N-Nitraso-Di-N-Propyiamine
HD
10
Benzo(a)pyrene
ND
10
Hexachlaroethane
ND
10
Indeno(1,2,3-cd)pyrene
ND
10
Nitrobenzene
i ND
10
Oibenz(a,h)anthracene
No
10
Isophorone
ND
10
Benzo(g,h,i)pery(ene
NO
10
bis(2-Chloroethoxy) methane
ND
10
ACID EXTRACTABLES RESULT
LIMIT
1,2,4-Trichlorobenzene
ND
10
'
Haphthalene
ND
10
Phenol
ND
10
Hexachlorobutodiene
HD
10
2-Chlorophenol
ND
10
Hexachlarocyclopentadiene
ND
10
BenzyL Alcohol
ND
20
1
2-Chloronaphthalene
ND
10
2-MethyLphenol
ND
10
Dimethyl phthalate
i ND
10
4-MethyLphenol
Hfl
10
Acenaphthyiene
ND
10
2-Hitrophenol
ND
10
'
Acenaphthene
ND
10
2,4-Dimethy(phenoi
ND
10
2,4-Dinitratotuene
ND
10
Benzoic Acid
ND
50
2,6-Dinitrotoluene
ND
10
2,4-OichLorophenaL
ND
10
DiethyLphthalate
ND
10
4-Chlaroaniline
ND
20
'
4-ChloraphenyL phenyl ether
ND
10
4-Chloro-3-methyiphenoL
ND
10
FLourene
HD
10
2-Methylnaphthatene
ND
10
N-Nitrosodiphenytamine
ND
10
2,4,6-Trichlorophenoi
ND
10
t
4-Bromophenyl phenyl ether
ND
10
2,4,5-Trichlorophenol
HD
10
HexachLorobenzene
N0
10
2-Nitraaniline
ND
25
Phenanthrene
ND
10
3-Nitraaniline
ND
25
Anthracene
ND
10
2,4-Dinitrophenol
ND
10
'
Di-n-butylphthaLate
ND
10
4-Hitraphenol
NO
10
FLuoranthene
ND
10
Dibenzofuran
ND
10
Pyrene
ND
10
4-Nitraaniline
ND
10
Butyl benzyt phthalate
i No
10
4,6-Dinitro-2-methylphenol
ND
10
3,31-Dichlorobenzidine
HD
10
Pentachloraphenol
ND
10
Benzo (a) anthracene
ND
10
Benzidine
ND
10
'
bis (2-ethylhexyL)phthatate
ND
10
H-Nitrosodimethylamine
ND
10
Additional Anal tes
1,2-Diphenyihydrazine
ND 10
'
3-Methyiphenol (m-Cresol)
I
ND 10
Notes and Definitions for this Report:
units:....
ug/L
'
EXTRACTED........
07/16/98
DATE RUN.........
07 17 98
ANALYST!.........
PAC
'
INSTRUMENT.......
F
DILUTION FACTOR..
1
'
i
HD = Not Detected at Detection Limits.
f

1
Page 6
' Received: 07/15/98
SAMPLE ID mi-3
1 .
Tou Kom CORP: REPORT Work order A 98-07-267
Results by Sample
1
FRACTION Da TEST CODE EPHNC NAME QMZACTABLE PHC
Hate & Time Cottected 07/14/98 11:35:GG Category HATER
EXTRACTABLE PETROLEUM HYDROCARONS
REPORTING
RESULT LIMIT
C9-08 ALiphatics 169 100
C19-C36 Aliphatics ND 100
C11-C22 Aromatics 121 100
Surrogates %Recovery Surrogate Limits
Aliphatic Surrogate 58.1 40 - 140
Aliphatic Fractionation Surrogate 65.2 40 - 140
Aromatic Surrogate 48.8 40 - 140
Aromatic Fractionation Surrogate 61.8 40 - 140
Notes and Definitions for this Report:
EXTRACTED 07
HATE RUN 07/27/98
ANALYST CK
INSTRUMENT HP7
OIL. FACTOR: 1
UNITS _uglt
MATRIX:
DRY HEIGHT:
I
ND = not detected at detection Limit
t
D = diluted out
INT = matrix interference
Hydrocarbon Range data exclude concentrations of surrogates) eluting in that range
Hydrocarbon Range data are unadjusted foritarget anaLytes

Page 7 TOXIXON CORP I REPORT York Order # 98-07-267
Received: 07/15/98 Rewtts by Sample
SAMPLE ID MW-3 FRACTION 02A TEST CODE TICSV NAME T.I.C. Semi-yolatiles
Date & Time Collected 07 14 98 11.35:00 Category WATER
SUMMARY OF NOS (38;700+ analyte version, April 182)
LIBRARY SEARCH RESULTS OF NONTARGETED PEAKS WITH ESTIMATED
CONCENTRATION OF TENTATIVELY IDENTIFIED COMPOUNDS
BASE NEUTRAL
SCAN NAME OF MF ASSESSMENT EST.
HUM. COMPOUND PUR RS ISO UK CONC. CAS RT
(1) (2) N (3)
159 UNKNOWN 7 _ x 10.54 * 5.92
205 UNKNOWN 32 _ x_ 23.12 * 6.69
456 1 2-SENZENEOOIL 70 6.71 120809 10.94
Notes and Definitions for this Report:
UNITS....... .. v4/L
DATE .......... .. 07/17/98
SPECTROSCOPIST... PAC
(1) RS - Reasonable Identification
ISO- Isomer or similar compound
i
UK - Unknown, not in NBS Library
i
(2) Calculated vs nearest etuting internal standard
as a simple ratio / proportion.
(3) RT vs difluorobiphenyl or d**10-phenanthrene.
* This shall mean the assessment of the library search
by an experienced mass spec. interpretation specialist
which would by -his/her concurrence be a good identification
using WA85-J664, J680, Task V on page A-3 & Task III pg 2-3

t
Page a TOXIKOIL CORP. REPORT York Order # 98-07-267
' Received: 07/15/98 Results by SaWLe
SAMPLE ID MY-4 FRACTION 03A TEST CODE 625 NAME A N E)(TRACTABLES PATER
I
Date l Time Collected 07/14/98 12:25:00 Category WATER
I
PARAMETER RESULT LIMIT PARAMETER RESULT LIMIT
BASE NEUTRAL EXTRACTABLES
bis(-2-ChLoroethyt) ether
IND
10
1,3-Dichlorobenzene
No
10
Chrysene
No
10
1,4-oichtorebenzene
ND
10
Di-n-octyt phthalate
No
10
1,2-Dichtorobenzene
No
10
Benzo(b)ftuoranthene
ND
10
bis(2-Chloroisopropyl) ether
No
10
Benzo(k)fluoranthene
No
10
N-Nitroso-Di-N-Propylamine
No
10
Senzo(a)pyrene
NO
10
Hexachtoroethane
END
10
Indeno(1,2,3-cd)pyrene
NO
10
Nitrobenzene
IND
10
Dibenz(a,h)anthracene
ND
10
Isophorone
IND
10
Benzo(g,h,i)perylene
ND
10
bis(2-Chloroethoxy) methane
IND
10
ACID EXTRACTABLES
RESULT LIMIT
1,2,4-Trichlorobenzene
IND
10
Naphthalene
IND
10
Phenol
NO
10
Hexachiorobutediene
IND
10
2-Chlorophenol
No
10
Hexachtorocyclopentadiene
INo
10
Senzyl Alcohol
No
21
2-Chlaronaphthalene
IND
10
2-MethylphenoL
No
10
Dimethyt phthalate
No
10
4-MethylphenoL
NO
10
Acenaphthylene
No
10
2-Nitrophenol
No
10
Acenaphthene
IND
10
2,4-Dimethyiphenol
HD
10
2,4-DinitrotoLuene
No
10
Benzoic Acid
ND
,_ 5�?.
2,6-Dinitratotuene
No
10
2,4-Dichlorophenol
NO
10
Diethyiphthatate
No
10
4-Chloraaniline
HD
21
4-Chlorophenyl phenyl ether
No
10
4-Chloro-3-methylphenot
No
10
Ftourene
IND
10
2-MethyLnaphthalene
NO
10
H•Nitrasodiphenylamine
IHD
10
2,4,6-TrichtorophenaL
NO
10
4-Bromophenyl phenyl ether
IND
10
2,4,5-TrichlorophenoL
ND
10
Hexachlarobenzene
INo
10
2-Nitroaniline
HD
26
Phenanthrene
IND
10
3-Nitroaniline
HD
26
Anthracene
INO
10
2,4-Dinitrophenot
No
10
Di-n-butytphthatate
IND
10
4-Nitrophenol
No
10
FLuorenthene
IND
10
Dibenzofuran
NO
10
Pyrene
IND
10
4-Nitroaniline
No
10
Butyl benzyt phthalate
IND
10
4,6-Dinitro-2-methylphenol
HD
10
3,31-Dichlorobenzidine
IND
10
Pentachlorophenol
No
10
Benzo (a) anthracene
IHD
10
Benzidine
No
10
bis (2-ethyihexy()phthalate
IND
10
N-Hitrosodimethylamine
No
10
Additional Anattes
1,2-Diphenythydrazi ine
No 10
3-Methy(phenoL Cm -Cresol)
No 10
Notes and Definitions for
this Report:
Units:.. I ......
ug/L
EXTRACTED........
07/16198
HATE RUN.I........
07/17198
ANALTST..I ......
PAC
INSTRUMENT.......
F
i
DILUTION FACTOR.. 1.04
i
HD = Not Detected at
Detection Limits.

Page 9
' Received.- 07/15/98
SAMPLE ID XW-S
1
TOXIXCI( CORP. REPORT
Results by Sample
I
York Order ■ 98-07-267
FRACTION 03A TEST CODE EPHMC NAME EXTRACTABLE PHC
Date 8 Time CoLLeeted 07/14/98 12:25.00 Category WATER
' EXTRACTABLE PETROLEUM HYDROCARON5
REPORTING
RESULT LIMIT
C9-C18 Aliphatics 154 100
C19-06 Atiphatics ND 100
C11-C22 Aromatics1 106 100
' Surrogates XRecovery Surrogate Limits
Aliphatic Surrogate 52.3 40 - 140
Aliphatic Fractionation Surrogate 73.9 40 140
Aromatic Surrogate 47.8 40 140
Aromatic Fractionation Surrogate 50.1 40 140
' Notes and Definitions for this Report:
EXTRACTED 07/16198
DATE RUN 07127/98
ANALYSTI CK
' INSTRUMENT HP7
DIL. FACTOR: 1
UNITS ug/L
MATRIX:I
1 DRY WEIGHT:
I
' ND not detected at detection Limit
D di Luted'out
INT = matrix interference
I
' Hydrocarbon Range data exclude concentrations of surrogate(s) eiuting in that range
Hydrocarbon Range data are unadjusted for target analytes
I

Page 1D TOxiKoN CORP. REPORT York order i# 98-07-267
eReceived: 07/15/98 Results by Sample
SAMPLE ID )ell-4 FRACTIIjCN DA TEST CODE TICSV NAME T.I-C. Semi-volatiLes
' Date & Time Collected Onl4198 12.25:01) Category WATER
I
SUMMARY OF NUS 08,700+ analyte version, April 182)
LIBRARY SEARCH RESULTS OF NONTARGETED PEAKS WITH ESTIMATED
CONCENTRATION OF TENTATIVELY IDENTIFIED COMPOUNDS
BASE NEUTRAL
SCAN NAME OF MF ASSESSMENT EST.
HUM. COMPOUND PUR RS ISO UK CONC. CAS RT
(1) (2) # (3)
-- ----------------------1 .-------------- ----- -------------
159 UNKNOWN 9 _ _ 22.5 * 5.92
_ _20.5 UNKL OWN 8 _ _ X 22.18 * 6.70
267 UNKNOWN 59 _ _ % 24.68 + 7.75
i
Notes and Definitions for this Report:
UNITS....... .. u9/L
DATE........ .. 07/17/98
SPECTROSCOPIST... PAC
(1) RS - Reasonable identification
ISO- Isomer or similar compound
UK - Unknown, not in HBS Library
(2) Calcutated vs nearest eluting internal standard
as a simple ratio / proportion.
(3) RT vs difiuorobiphenyl or d**10-phenanthrene.
' This shad mean the assessment of the library search
by an experienced mass spec. interpretation specialist
which would by his/her concurrence be a good identification
using YA85-J664, J680, Task V on page A-3 & Task III pg 2-3
COMMENTS

Page 11 TOXiKON CORP.I REPORT York order 0 98-07-767
Received: 07/15/98 Re suits by sample
SAMPLE ID MY-5 FRACTION 04A TEST CODE 625 NAME A BN EXTRACTABLE& PATER
' Date B Time Collected 07/14/98 10:55:00 Category PATER
I
PARAMETER RESULT LIMIT PARAMETER
BASE NEUTRAL EXTRACTABLES
RESULT LIMIT
bis(-2-Chloroethyt) ether
I ND
10
1,3-Dichlorobenxene
AND
10
Chrysene
ND
10
1,4-Dichlorobenzene
I ND
10
Di-n-octyl phthalate
ND
10
1,2-Dichlorobenzene
I NO
10
Benzo(b)fluoranthene
ND
10
bis(2-ChloroisepropyL) ether
I NO
10
8enzo(k)fluaranthene
NO
10
N-Nitroso-Di-N-Propylamine
INO
10
Benzo(a)pyrene
ND
10
Hexachloroethane
No
10
lndeno(1,2,3-cd)pyrene
NO
10
Nitrobenzene
ND
10
Dibenz(a,h)anthracene
ND
10
Isophorone
ND
10
8enzo(g,h,i)perylene
ND
10
bis(2-Chloroethoxy) methane
ND
10
ACID EXTRACTABLES
RESULT LIMIT
1,2,4-Trichlorobenzene
I ND
10
Naphthalene
I ND
10
Phenol
NO
10
Hexachlorobutaciiene
NO
10
2-Chlorophenot
NO
10
Hexachlorocyclopentadiene
No
10
Senzyl Alcohol
No
21
2-Chtoronaphthalene
NO
10
2-Methylphenot
ND
10
Dimethyl phthalate
ND
10
4-Nethylphenot
ND
10
Acenaphthylene
NO
10
2-Nitrophenol
ND
10
Acenaphthene
I ND
10
2,4-DimethytphenoL
ND
10
2,4-Dinitrotoluene
I ND
10
Benzoic Acid
HD
52
2,6-Dinitrotoluene
I ND
10
2,4-DichlorophenoL
ND
10
Diethylphthalate
NO
10
4-Chioroaniline
ND
_..g 1
4-Chtorophenyl phenyl ether
ND
10
4-Chtoro-3-methylphenot
HD
10
Flourene
ND
10
2-Methylnaphthalene
ND
10
N-Nitrosodiphenylamine
No
10
2,4,6-Trichlorophenal
ND
10
4-Bromaphenyl phenyt ether
ND
10
2,4,5-Trichlorophenol
ND
10
Hexachlarobenzene
I ND
10
2-Nitroaniline
ND
26
Phenanthrene
I NO
10
3-Nitroaniline
ND
26
Anthracene
NO
10
2,4-Dinitraphenol
MD
10
Di-n-butylphthalate
NO
10
4-NitrophenoL
ND
10
Fluoranthene
NO
10
Dibenzofuran
NO
10
Pyrene
ND
10
4-NitroaniLine
No
10
Butyl benzyt phthalate
1 ND
10
4,6-Dinitro-2-methylphenol
HD
10
3,31-Dichlorobenzidine
I NO
10
Pentachloraphenol
NO
10
Benzo (a) anthracene
I ND
10
Benzidine
ND
10
bis (2-ethythexyO phthalate
I NO
10
N-Nitrosodimethylamine
ND
10
Additional Analytes
1,2-Diphenylhydrazine
ND 10
3-Methylphenot (m�Cresat)
HD 10
Hates
and Definitions
for
this Report:
Units:. I .......
ug/L
EXTRACTED........
07/16198
PATE RUN......
071�98
ANALTST.�....
........
PAC
INSTRUMENT.......
F
DILUTION FACTOR.. 1_04
NO = Not Detected at
Detection Limits.

' Page 12 TOXIKDII CORP. REPORT York order R 98-07-7-67
Received: 07/15/98 Results by Sample
SAMPLE ID KW-5 FRACTION 04A TEST CODE EPHHC NAME EXTRACTABLE PHC
Date B�Time Collected 07/14/98 10:55:00 Category WATER
1
' L A i iC 27 L,. L i7 n L r1 L F1 4 n LJ iJ C� V 1'1 it i L i� V L L1_it V li U
REPORTING
RESULT LIMIT
C9-C18 Aliphatics 1070 100
C19-C36 Aliphatics NO 100
C11-C22 Aromatics NO 100
eSurrogates %Recovery Surrogate Limits
Aliphatic Surrogate 50.4 40 - 140
' Aliphatic Fractionation Surrogate 87.8 40 - 140
Aromatic Surrogate 47.6 40 140
Aromatic Fractionation Surrogate 40.8 40 140
' Notes and Definitions for this Report:
EXTRACTEDR 07„ /16/98
DATE RUN 07/27/98
' ANALYST CK
INSTRUMENT HP7
DIL. FACTOR: 1
UNITS ugL
' MATRIX:
DRY WEIGHT:
' ND = not detected at detection limit
0 = diluted out
INT = matrix interference
I
Hydrocarbon Range data exclude concentrations of surrogate(s) eluting in that range
Hydrocarbon Range data are unadjusted for target analytes

Page 13
Received: 07/15/98
SAMPLE ID IOW-5
TOXI)(ON CORP: REPORT York Order # 98-07-267
I
Results by SawLe
FRACTION "A TEST CODE TICSV NAME T.I.C. Semi-voLatiles
Date & Time Collected 07/14/98 10:55:1)Q Category WATER
I
SUMMARY OF NUS (38,700+ analyte version, April 182)
LIBRARY SEARCH RESULTS DF NONTARGETED PEAKS WITH ESTIMATED
i
CONCENTRATION OF TENTATIVELY IDENTIFIED COMPOUNDS
BASE NEUTRAL
I
SCAN NAME OF MF ASSESSMENT EST.
NUM. COMPOUND PUR RS ISO UK CONC. CAS RT
(1) (2) # (3)
------------------------------ -------------- --
157 UNKNOWN 95 _ _ x 197.85 * 5.98
—j-89 UNKNOWN 91 _ _ x 120 * 6.30
249 UNKNOWN 94 _ _ ]( 56.4 * 7.44
256 UNKNOWN 96 _ _ x 25.2 * 7.56
280 UNKNOWN 96 _ _ x 70.2 7.96
308 _ UNKNOWN 96 _ _ � 26.7 8.44
322 INDANE 81 _ _ _ 12.1 496117 8.67
339 UNKNOWN 91 _ _ x 11.1 8.96
357 BENZENE. -ETHYL-DIMETHYL ISaME 91 _ x _ 11.2 * 9.27
395 UNKNOWN 91 x 6.11 * 9.91
413 ggNZENE. (1-METHYL-1-PROPENYL) 76 _ 6.31 767997 10.21
423 UNKNOWN 93 _ _ x 7,1.9 * 10.38
I
Notes and Definitions for this Report:
UNITS........ ... _ ug/L
DATE........I.. 07/17/98
SPECTROSCOPIST... PAC
(1) RS - Reasanab{e Identification
ISO- isomer or similar compound
UK - Unknown, not in NBS Library
(2) Calculated vs nearest eluting internal standard
as a simple ratio / proportion.
(3) RT vs difLuerobiphenyl or d**10-phenanthrene.
* This shall mean the assessment of the library search
by an experienced mass spec. interpretation specialist
which would by his/her concurrence be a good identification
using WA85-J664, J680, Task V on page A-3 & Task III pg 2-3
COMMENTS

Pogo 14 TOXIMN CORP. REPORT Work Order d 98-07-267
' Received: D7115/98 Results by Sample
1
SAMPLE ID M11-6 FRACTION 05A TEST CODE 625 NAME VBN EXTRACTABLES WATER
' Date & Time Collected 07/14/ 8 12.15:00 Category WATER
I
PARAMETER RESULT LIMIT PARAMETER I BASE NEUTRAL EXTRACTABLES
bis(-2-ChloroethyL) ether
AND
10
1,3-Dichlorobenzene
AND
10
Chrysene
1,4-Dichlorobenzene
AND
10
Di-n-octyl phthalate
1,2-Dichlorobenzene
No
10
Senzo(b)fluoranthene
bis(2-ChloroisopropyL) ether
NO
10
Benzo(k)fluccenthene
H-Nitroso-Di-N-Propylamine
ND
10
Senzo(a)pyrene
Nexachloroethane
ND
10
Indeno(1,2,3-cd)pyrene
Nitrobenzene
ND
10
Dibenz(a,h)anthracene
Isophorone
ND
10
Benza(g,h,i)perylene
bis(2-Chloroethoxy) methane
ND
10
ACID EXTRACTABLES
1,2,4-TrichLorobenzene
ND
10
Naphthalene
ND
10
Phenol
Hexachlorobutadiene
ND
10
2-Chlarophenot
Hexachlorocyclopentadiene
ND
10
Benzyl Aicohol
2-Chloronaphthalene
ND
10
2-Methyiphenol
DimethyL phthalate
ND
10
4-MethytphenoL
Acenaphthylene
ND
10
2-Nitrophenol
Acenaphthene
ND
10
2,4-Dimethytphenot
2,4-Dinitrotoluene
ND
10
Benzoic Acid
2,6-Dinitrotoiuene
ND
10
2,4-Dichtorophenol
Diethylphthalate
ND
10
4-Chlaronniline
4-ChlorophenyL phenyl ether
ND
10
4-Chloro-3-methyLphenoL
FLourene
ND
10
2-Methylnaphthalene
N-Nitrosodiphenytamine
No
10
2,4,6-Trichtoraphenot
4-Bromophenyl phenyl ether
ND
10
2,4,5-Trichiorophenol
Hexachlorobenzene
ND
10
2-NitroaniH ne
Phenanthrene
ND
10
3-Nitroanitine
Anthracene
ND
10
2,4-Dinitrophenol
Di-n-butylphtha(ate
ND
10
4-Nitrophenot
FLuorenthene
f ND
10
Dibenzofuran
Pyrene
ND
10
4-Nitroaniline
Butyl benzyl phthalate
ND
10
4,6-Dinitro-2-methytphenal
3,31-Oichlarobenzidine
f No
10
Pentachtorophenal
Benzo (a) anthracene
HD
10
Benzidine
bis (2-ethy(hexyl)phthatate
ND
10
N-Nitrosodimethylamine
additional Anal tes
1,2-Diphenylhydrazine
NO 10
3-Methy{phenol (m-CresoL)
I
NO 10
Notes and Definitions
for
this Report:
Units: ........
ug/L
EXTRACTED........
07 16 9$
DATE RUN.........
07L17194
ANALYST j.........
_
PAC
P
INSTRUMENT.......
F
DILUTION FACTOR..
1.04
1
ND = Not Detected at
I
Detection Limits.
RESULT LIMIT
ND 10
ND 10
ND 10
ND 10
ND 10
ND 10
ND 10
ND 10
RESULT LIMIT
ND
ND
un
ND
ND
ND
ND
ND
NO
ND
un
ND
un
ND
ND
un
ND
ND
NO
NO
NO
on
ND
ND
10
10
21
10
10
10
10
52
10
21
10
10
10
10
26
26
10
10
10
10
10
10
10
10

Page 15
Recei►red: 07115/98
SAMPLE ID MN-6
TOXIKOII CORP.' REPORT Nark Order # 98-07-267
Results by Sample
FRACTfDN 05A TEST CODE EPHNC NAME EXTRACTABLE PHC
Date & Time Collected 07/14/98 12:15:00 Category SLATER
EXTRACTABLE PETROLEUM HYDROCARONS
REPORTING
RESULT LIMIT
C9-C18 Aliphatics 156 100
C19-06 Aliphatics NO 100
Cll-C22 Aromatics No 100
Surrogates %Recovery Surrogate Limits
Aliphatic Surrogate 61.8 40 - 140
Aliphatic Fractionation Surrogate 97.0 40 - 140
Aromatic Surrogate 44.1 40 - 140
Aromatic Fractionation Surrogate 66.0 40 - 140
Notes and Definitions for this Report:
EXTRACTED 071 6/98
DATE RUN 07/27/98
ANALYST CK
INSTRUMENT HP7
DIL. FACTOR: 1
UNITS ug/L
MATRIX:
DRY SLEIGHT:
NO = not detected at detection limit
D = diluted out
INT = matrix interference
Hydrocarbon Range data exclude concentrations of surrogate(s) eluting in that range
Hydrocarbon Range data are unadjusted for target analytes

1 .
Page 16
Received: 07/15/98
TOXII(011 CORP.I REPORT Mork order # 98-07-267
Results by SampLe
SAMPLE ID All-6 FRACTION 05A TEST CODE TICSV NAME T.I.C. Semi-valatiies
' Date & Time Collected 07/14/98 12:15.00 Category HATER
I
SUMMARY OF NBS (38,700+ analyte version, April 182)
LIBRARY SEARCH RESULTS OF NONTARGETED PEAKS WITH ESTIMATED
CONCENTRATION OF TENTATIVELY IDENTIFIED COMPOUNDS
RASE NEUTRAL
SCAN NAME OF MF ASSESSMENT EST.
HUM. COMPOUND PUR RS IS❑ UK CONC. CAS RT
(1) (2) # (3)
159
UNKNOWN 7 _ _ x 19.7
*
5.92
205
UNKNOWN 27 _ _ x 22.5
*
6.69
309
UNKNOWN 49 _ x 7.33
^_
*
8.45
415
CYCLOHEYANEMETHANOL 74 _ 7.71
498817
10.25
420
UNKNOWN 98 _ _ x 22.5
r
*
10.33
457
1 2-SENZENEDiOL 87 7.99
-_ -_
120809
10.96
471
UNKNOWN 25 x 4.09
*
11.2
510
UNKNOWN 38 _ x_ 4.18
*
11.86
515
UNKNOWN 25 _ X 6.48
*
11.94
523
UNKNOWN 47 X 4.13
^_
*
12.08
608
UNKNOWN 64 x 4.17
*
13.51
724
UNKNOWN 46 _ X 6.29
*
15.48
940
P HE TACYCI.O(7.50.0(2,8).O(5,14) 90 _ _ _ 10.0
*
19.13
Notes and Definitions for this Report:
UNITS........ G4/L
DATE ........... 07/17/98
SPECTROSCOPIST!— PAC
(1) RS - Reasonable Identification
ISO- Isomer or similar compound
UK - Unknown, not in NBS Library
(2) Calculated vs nearest eluting internal
standard
as a simple ratio / proportion.
I
(3) RT vs difluorobiphenyl or d**10-phenanthrene.
* This shall mean the assessment of the library
search
by an experienced mass spec. interpretation
specialist
which would by his/her concurrence be a goad identification
using WA85-J664, J680, Task V on page A-3 &
Task III
pg 2-3
COMMENTS

Page 17 TOXICON CORP.1 REPORT York Order # 98-07-267
Received: 07/15/98 Results by Sample
SAMPLE ID NW-3 SAMPLE # 06 FRACTIONS: A
Date & Time Collected 07 14 98 10:55:00 Category WATER
CR 0.028 P9 0.017
mg/L DL=0.005 mglt DL=0.005

Page I T[ALIKOK CORP. J REPORT
Received: 07/15/98 Test Rethodology
TEST CODE 625 NAME AIBN E] MCTABLES WATER _
EPA METHOD: 625: Base I Neutral, Acids GCMS.
Reference: Methods for Organic Chemical Analysis of Municipal and
Industrial Wastewater. Appendix A. 40CFR Part 136.
FederaL Register VoL. 49, No. 209; 1984.
TEST CODE EPRNC NAME EXTRACTABLE PHC
METHOD:EXTRACTABLE PETROLEUM HYDROCARBONS
REFERENCE:METHOD FOR THE DETERMINATION OF EXTRACTABLE PETROLEUM
HYDROCARBONS (EPH), MADEP-EPH-98-11
MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION
JANUARY 1998
FOLLOWING THE GUIDELINES OF THE NOIIfRTH CAROLINA DENR
TEST CODE MEX NC NAME North Carolina Acid Ext.
1
Reference: Method 3030C. Preliminary Treate:nent for Acid Extractable
Metals. i
Standard Methods for the Examination of Water and
Wastewater, 17th Edition.
TEST CODE TICSV NAME T.I.C. Semi-Volatiles�
Method not available.
York Order # 98-07-267

EPHIVPH Certification
Toxikon Order �,
VPH Soil Sample Collection Option
I,
Option 1 = Fill line on vial Option 2 = Sampling Device Option 3 = Field weight of soil
Were all QAIQC procedures REQUIRED by the VPH method followed?
I
Were all QAIQC procedures REQUIRED by the EPH method followed?
Were all perform ancelacceptanlee standards for the required QAJQC
procedures achieved?
Details regarding any answer of "No" above are provided below.
Yes No A)11?
Yes --,NO—
Yes vNo_
Were any significant modifications made to the EPHIVPH methods Yes_ No X
I
as specified in Section 11.3?
I attest under the pains and penalties of perjury that, based upon my inquiry of those
individuals immediately responsible for obtaining the information, the material contained
in this report is, to the best of My knowledge and belief, accurate and complete.
f
I �
%"
Signature: I l ! Position:
Printed Name: �rtr Gr�"cE _ Date: IZ,

Attachment 3
EPH Laboratory Reporting Form
'K. N,
Initial Calibration Date
Calibration Ranqes and Limits
_z 7-,
------
M D
C9 -C18 Aliphatics
IIV 1 3 3
/00
C19 - C36 Aliphatics
a 5
J00
IC1 1 -C22 Aromatics
/OU
NOTE Please include units as appropriate
Method of Quantitation (circle one,)-. Curve Average Re�spon�se-Fa�CtCr
Calibration Concentration Levels
....... .........
. ............ Ra
- ---------
I r
..... ............
C9 _C18
Aliphatics
I C7 0
(9 0 C)
0
C19 -C36
Aliphatics
140
it u 0
c6 0 01
1 6 0 0'
C1 I - C22
Aromatics
I I
if
3 Y 0,
IF57 0.
NOTE: Please indicate units as appr
Calibration Check Date I)'
Calibration Check ti
e,
w
C9 -C18 Aliphatics
3 0
C19 - C36 Aliphatics
y 0 b
ICI 1 -C22 Aromatics
(3 5i 0
1 (: Z 12
IVIDL = Method Detection Limit
NIL = Mirnimum Limit
RL = Reportable Limit
RPC = Relative Percent Difference
%RSO = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve

err r �r r rr r i r. r■r r � 1" -
CHAIN OF CUSTODY RECORD RK ER
15 Wiggins Ave., Bedford, MA 01730 -
Telephone: [phone] DUE DATE 4�
Fax:[phone]
f ,
COMPANY: 1,'5_ _ _ 6:LVy rC-P V 4_ SAMPLE TYPE CONTAINER TYPE •U I ANALYSES
ADDRESS: S - Ft 1-WASTEWATER P - PLASTIC V'
z. SOIL G • GLASS �j L
PHONE #: ors 3. SLUDGE V .VOA
55 �a�19DFA}C #: � "� ��/� 4. OIL �
P.O. #: Z -3 5. DRINKING WATER
PROJECT MANAGER: ::T'" _, s- WATER tGWAA WISWj �i rV �J
PROJECT ID/LOCATION: /e__ ?.OTHER (SPECIFY
TOXIKON SAMPLE SAMPLE CONTAINER SAMPLING PRESERVATIVE �f SPECIAL
� INSTRUCTIONS/
a>« IDENTIFICATION! TYPE SIZE TYPE a DATE TIME � COMMENTS
BY:
RELINQUISHED BY:
RELINQUISHED BY.
METHOD OF SHIPMENT
DATE-. - - - N
TIME: -
DATE: -
TIME: - -
DATE: -
TIME:.
C4i111163 11812F11
f:�xsI�IT1��7:]'A
RECEIV ❑ OW
Y:
7Ile
COOLER TEMPERATURE
DATE: - _ ❑ RUSH ..... BUSINESS DAY TURN AROUND
TIME: _ KIROUTINE
DATE: 0-7 - �� _ y Sample disposal information
Are there any other known or suspected
TIME: /,.? - Z`L - contaminants in these samples other than
those listed above?
Yes No If Yes, 1st Known

08-03-98 03:02?M HOM TOXIKOH I TO 19!95960578 P002
✓ "1
Reerlwd: OYI15in
TOxIRK CORP, rapmr
1 NOUN 14:131:36
War* Or+dw # 98-07-26B
REPORT EZS MIRWjWAl jjjYjgjS I PREMED TgX: j Trr-CORPORATZ04
TO 117 S. Yr 5 r Ns AY
mm596-0470 fAx 0576 FLED BY
ArTFee rw STAw see I ATTEN EAUL LELURG—
PHONE (J1M75-3330 CONTACT MMEITING_
CLIENT EMS NC _ SAMPLES �
COMPANY Ch5 eMVI R2UJHTAL SERV[4E5, MA CEItT R R-NA064: TRACE METALS- SULFAJIXYAN10E.8ES. FREE_
FACILITY T17 S, HOOWR RD CALOgL , Cp, TOM -ALK TR5, OR- THNg.VOC� PEST, jNMENLf.
UR"Affl RC 27ml DENaue. Gtd. PHEWXIC:. PCea [7_ORs gM-9563. NY 810M
FL MRE�7143 NJ OEP j$53� MC ONRLM, SC OZ.-MR 2Wl71-C,
WORK ID vrrtE-7Z3q _
TAKEN 11419$ _ VER I Fi ED i1 CdLiGi ._ �Tr
f TRANS
TYPE WATER I
INVOICE y*r gm2r ltg cnvr
LWLE IDENTIfICATIONr TUT CODES erd RAINS 1md at this trorkordpr
n�21 ¢Ef� PMEA6LE IIALQEAUDN5
eVRSIJ.L1 hjMTjCS
c�1_ CH1tOMluM - -
Q�DELI E_Thr{title 21birolde _
.a 1M►7 S _ jPI gs IsupwgEnITHIp-
HEX KCVar?k CaroiltM Acid t
I
MTBE I- MTe
pR I L EM � - --
V_OLATTLF PHL
I ,

08-03-9$ 03:02PM FROM TOMON ?O 19i9596073 P003
H
i
paa. 2 • nAuj= CARP. SEFORT wort afdar s 9e-07-Zip
ilacalred: 07/13/" eawtts by sawle
SAMU 10 FRACTION MA TEST CODE VP MJiIMi VOUTIL9
Cate i Time Col 1ectsd.0`f14f98 n;35*QR Category 4ltTER
P T QL vM KY1)R0CA8A2N8
REPORT Il16
RESULT LIMIT
CS -CS AIIphatica (FID) k8 s0
CP-Cl? Aliphatics MO) _ N S4
s9-C10 Aromatics MD) !Y8 50
TARGET VPk AMALMS
Totuene
Na 2.0
Ethytbwzww
wn 2.
W-xy l erica
+l
0-%ytene
�o _2,Q
arroE
_ 4.2 2.4
Ilophthelone
Surrogstaa x Raeorery Surrogate Limits
FIC Surrogate 1 74 n - 130
PID Surrogate 7� TO - 130
Wotes and Definitions Tor this Report:
I
UNITS: uyl,
DATE RUM: 7� IZ6/98
ANALYST: np
Iii$TRUMEIiT: v3
CiL. FACTOR: 1
AATRix: HATER
III) ■ not detested at detection limit
0 diluted out
IIIT ■ fstrix interferenre
Hydrocarbon Range data exciude come ltrstfens of sueropere(a) clueing in that rsnpe
CS -CA Aliphatic Hydrocarbons exctuda the concentration of Target Analytea eluting In that range
C9-C12 Aliphatic Nydrocarbar+a exCluda the concentration ofTaraet Anatytes eluting in that r"a
and the Concentration of C9-00 Aromatia ilydrxerbons
I

08-03-98 03:0ZIN FROM TOMON
I
i4 19195960578 I'
P"o 3 Ti�[IR�I cow. +
k Raa�i►rorl: QTjTS/!a Result: 1lEPORi 1h,i k erd�r / 9e-G7-2m
+ by �(e
1i TA++FII is rAPlrle R _q FRACTIONS; �1 €
k € Date R Tlmd Co{[ette0 D7 05 W1 Cat
evory AM
k 'UGC."�
€ UVIL aL - 3.0 UWL UL*2.0 i
I � �

08-03-98 03:02PM FROM TOM ON
TO 19195960518 P00�
•
pw S TOXIMON CM. REPORT tlbrit n14Rr 190-07-2L6
Received: 07/111" f Results by sa.pE■
SWLE TO PY•1 FRACTION TEST CME fx11. - UK • i
Date a Thaa Co;lecled 0MT4�,m 1?:05;00Catenary IMTEK�
f •
g4RBLS_HALOCADONS
RESULT LIMIT
Chloromethane
v++
irpm[tI{IathaHI
Vtrrrt Chloride
9Ich{orodlIIuvrowthane
thtoreethetl!
4+r
x•�
Methytene Chioride
trichivrafltiproMethene
H�•
��
1.1-0fchIeraetheex
ti
1,1-41 ehE ortiathem
r:i.
7.0
[tarts-1,�-l1lrhEaraethene
6r•
7
Chtorvform
ti •
�i
1,2-01chioroetham
Hr+
2.0
1,1,1-Trlchioraethane
u,
—2.2
Carbon tetrsch[oride
tit,
2.0
8re$wdlchtorr6mthana
u+,
_ 2�
1,I•flichlornprvpana
ki•
2.4
Trans-1, 3-0fchtorvprepena
NI.
Trichtoreeth-ill
Mr
2.0
sfa-1,]-oichlorogrflpene
4r
2�
1,1,2-Trfchlorvethane
we,
nfbr'vmvcA[Ortimethsne
_��[+
? �
2-Ch(aroethyivfnyt ether
till
24
Rronoform
1,T,2.Z-TetrarhLernrthane
tar,
2=6
Tetrachlvroether+e
>ru
2^0
Chiorobanxeni
- _ uu
1,i vlchlnrvptniene
MU
1,3-Olthtvro6"One
4L
.'0
la-Mchlerobin:em
kU
2_
cla•1,2-01chlarvethem
Z-0
Mote$ en4 Gaiiniticnr for thlc Rcport
f
{I,If rS: vplL
DATC I r[UN: 07�
AMAtrsT:
1MlTR57RE1iT: +l
DIL.fFACTOR: 1
MO net detected at detection LIMIT

1
9
a
n
0
� R
y
rv.
= a
i
a ..
S
�r
x
w
SL7
O7
al
O
�C
p
tl w
w
n
g
qp�
O
Z
-
�
Q
<zr)

O8-83-98 I731 2°M FROM TH IKON TO 19195960578 PO07
r.E, a soxiacxw cuo. AEMT a/�swrk ord�� ! Qa oT ade lar.[+rati I�196 11"mits by iaapix
+ SAIIVLE 1� iNfPl6 I i'RAGff0lf5_ ..
6aea L Timm
i
I WL aL - 5.0 WL uLai.o

r� rr �■r rr rr r r rr r rr r� ■r r rr �r r r r r
cp
4?
w
71
o , �
i. �Cll ~ n
E{lI{I � ar
.r Iv to k; u }u`• � � p
�ar ry r I
iL�. LLLIt' Ir L1i LJf +f l`'.flrL I LfI �rIllL S4
L L W lvLL b W k1a LLLa Lla L W icy fu

08-03-98 03:02PM FROM TOXIHON
r
r} I
r
r
r
rE
r
r
r
r'
I
I
r
r�
I
r�
r'
i
G
r
r
ri
,
I
r�
r
r
r
TO 19195960518 F009
>�.�. RPTAT wrk Drdw.95.0-2"
f+ i
inefirrS: 9rlTSl� pwlrc b► 7saole
La[rm iv" TEST 007E OWNAlrE "�"ea�s A�IATiCS _-
SAM�LE 5i• Catewy �
lat� � Ti�w rallected o7J151��
LZA—A9-Z
EEWLT t.IM:t
SSORERE ,�t� --u
iplLtL1[S:I -� i�
�Q
EINtLSE�NIEME
VLtVtV V13FALI �Q
Sasn � GlfinSff�nb fpr Ch{R wiyala:
UNITS: UVIL
DAT[ pyiy oT 7n SI
MAov I L
IMSIM)"TfT: A
AIL. FA:TUR:
we - mi dttaetild rt dec�ccian [fmis

08-03-98 03:02PM FROM TO M ON TO 19i96960578 P0lo
:
p
Tt9 im =r. I"Mf Lvk erd.r ti 98 47 Zbb
Tt.r�l+nd: 1ST1151S1 Restults b7' SaRplr
3aatntE [9 EiACTICX � IFst CmE
Onto i tine Call.eted st►_ E. �r4� ta:5�1L� utryorr ]1�,
REPCRtIN0
RESULT L[R[t
CS Ca Atfptutfa (FIO) _---U24 -_In
G4-[72 AIiTlntios {f1v3
:2flU --X02
C;9 yin ArCaRtica, 0191 _—ZL 5yU
TARGET i
>MKIA Eft
Tolurnr
E thribansa++r
O-Xyt"
Witt p
�ph
p tAelana
PR f;XALTTEi
surrcyrtr>r X RtcaMVrY ii—rouste Limit$
FSp Srrro3iats q�70 130
o[� SurroyRte 79 1S9
RCtaa w4d Vwfinid w* Tor tAia "Por"
' LI [1St �t19LL
PATE Rut!
AtI YTT: iQ
1711.. Facrcx- ?4
V,ATX;X- WATER
ip t date tad at rjiteeticn "Elt
i p etivtad out
IIIT : matrt: interfereNc
a:clE] aiuc�n� in hEt rorrafs
HydrecVeer+ kuVr date exst3+da cene�rrtrat+grs of wrrog In "at rumor
C5-cl ,elipeaTic MydreCarbanf @MCVuee 1:1%+ cnncan[rotion 9f 7"Or ar.nirtes eVutir+4
Tr+T rau us
C9 Cti7 ,tlipn■Tfc AVdrvcarb@F4 en[lVgr rrn+ toncmerftien ott■rar tral r[ra clue i�7 in
CAa cmCet traiivn of :9•0Q ■rea+tl� pydrv:arecrc
i
i

uv vJ JQ uj.uLi:n r 6UM TV,�
TO 19195960578
Fdw to uKztm CW. ftrw wwk wolor r 96-ar-=6
e4ML01W d�- 97[15/ft
+ tewle. br "w1a
+
4 tAf�'tC ig 1�-S
unite N ¢4 ru CMS: A
i
Cate L Tire WtLacteQ .10.55:g2
Cat 99cry-
1
f
{ ualt 7t•a.aZ
i
+
f
f
I
S1J U ip W-
i
"OLI N 1* FRAC1IONS: LL
l
I
Oate Tips tetitacrwd?tiA96 f0:550
Category
1
ot■o.005 MA ot•v.aos
I
�
f
E
I f
i

v JJ.VL1:n rAvrn luil-Uh I
TO 1914,54060578
1
PM
Page AMAW StMr:8:. MC
98M KAtM Averue, Surw 100
µnr ervww• NC ZWA 0
•
Ter 1p4-BTSfCfi2
�
fax 704a7�P6;1s
GATE: 071241?8
Toaik;A
Pace Prelgrt wZber: 92495
15 Vtgy:rn AYs.
Client Project I0: 9607268
•
mf6o. m (1:130
wn: )is. Kin C�vtrlro
PtaneI• {7811275.3:s30
scliC result4 are reporte'1 mr 4 dry tr"q?rt ?as:s
i
Pir_tl $&&Vle H0: 92Y9931
Date Collrrtod: 07►;4►Q8
Mat."^z: Nator
C11rrK 5a01e 10: M"268,
Oate "ivel: 011L7l98
I
Parartery
ResullS 11rits
P;L
Analyzed v:41yct w
Fovtrotr•
I
H.l4pwrt, d ArgriatiC Yol . flrgs.
Mvthaalr 511 52361D
Prep Ikwtho4: EPA
021
11chIorod1fluot•ora V1AFr
rq
Uak
9.5
VIZV96 ON 75.71.E
Urlpntnaethsne
10
uy1L
a's
37124198 PPM 74.67.3
Ytnyl 711r110
ND
uglL
4.5
07/24/75 Pp?V M-01.4
Arafat7Aaethane
4D
uplL
0.5
01/24/98 Ppx 74.83.9
Chlortethane
%V
uglL
0.5
071241ae Pax 75.00.3
Trschi grofluorwwth+n&
as
tralL
+i.5
07/24196 P94 75•69.4
1.1.Dichi oroettwwv
MD
u, lL
0 5
;7R41% PPM 75.33.4
}IeMYlere Cllloridr,
w
u4IL
:.5
07124191! vox 75.09.2
trans 1,2 *1ch* oethene
w0
aq/L
015
07/24/99 PPx 156-60.5
I.;.0ir�ilolwthule
ND
,rjlL
0.5
07/24/98 P" 75•24.3
5fvMPtnlororietn4nr
9r
u;slL
0.5
07124/W PPn 74.97.5
ihlorafarn
1•1
us)IL
C.5
@717419U PPM 67.0.1
7.2.0101 wraparw
MD
u01L
M
0712419as PPM 594.20.1
1.2•01chi0r ftne.
ND
;pIL
0.5
07/24498 PP" IN-06•:
1.1.1-Trichi orawttor*
My
uifL
1.5
01/241% P" 71.55•6
1.I-Di chiarvpr4xnv
no
ve1L
0.5
07124r,4a PPw 553.58.E
Carbon Tetricnleride
lD
ugll
3.5
07124/96 WN 56.23.5
aibrara wthlra
MD
;s11L
0.5
071241VB PPM 74.95.3
1.2.0+chi amp -gone
%0
ti91L
0,5
07124198 PPM 70.97.5
7riolaraettrene
40
ua1L
n S
07/24/98 PP4 79.01.5
$rMO CNlOrorrtltar:e
No
G91 L
0. 5
071Z4194 pp-bt 75. v, 4
I 01-1.3.0zc1laroprovcne
10
uglL
0,5
011241g4 pPM 10D61 01.5
trms-L.3.01chi urowvven!
WD
;r91L
0.5
071Ia198 Pf" 14061.02.6
1.1,2•Trichluruethane
Ma
u5fL
0.5
1}71241% PPP 79.00.5
1.3.01010foomeane
NO
ug11
0.5
111141" 11h 147-28•9
i
,
010, ►richlwrawtMam
r
4D
t*/l
0.5
:7tzdi% rp+l 124.M-1
r
VA amn ;a&
Mc Was%+ralar S:
j
REPORT OF LABORATORY ANALYSIS
KV Cfriol" LYt:er RM
f
fJc rOr*jrq WZK ,ntL*
-,% UST :.ram
I SG 99:X'ra
IT+ s rwncrt fnali ict
be rtorodu_m r.te� A `tea,
VA Cn"kurq W42F 21
w"tA th¢ wnLI$n
-c�-
4 of P&CC tine ytG;W Sa-rrr sa 1rrC

�i
1
1
1
1
.V u 1 .7V
1.ucrm mum 1U,�1KON � TO 1919j9�Q�7Q
Fp}3
Pao Arvite"I Sinkea, Inc.
9BJ0 oxey Avenik, LW:e IGO
Pa r a A final vtir- AI llunter Olo. IC ZN70
9toIsamle fib; 9ZM31
1
Ir C1I.nt Savle ID: 45071268.:
i 9ar I+rartrrs
I I
Rol-,
j 1,2.4ibraid�vethine
ela
Teirethlaraethene
ND
j 1.1.1.2•Tetractilarvethaw,
ID
Chigrobenzom
•aranator„I
ND
f
ru
1.1.2.2•Tttr4ehlawtiv�rle
ft�
1.2.3 Trlrriiarapropane
N9
9rGe•eEenil�
ND
2 LhlarOtalu4ne
ND
4 Chlarrotaluerle
✓.9
1.] Dichlpraken:
MQ
1.4•DfchlarvDtrrw>w
IL
1.Z•Dt�hlorabertzerk
Nil
' 1.2.4i$r+7er0.317waropmparit
ND
1.2.4•Trichlarabentene
M0
}lexachlorvbsrWGterle
'G7
I 1.2.3-Trtchi cmberurrr
NO
l4owl•tert-hAY) Ether
4,5
IsaorcoYl Ether
NO
Stmcr*
No
Taluenc
M9
5tyrent
t47
I a-bleN 11,T•D1rwLhylttrrrrel V
1 so"y I fir'+ [Gwent}
MD
' N•PrvpYlbensrrle
IY7
I ..3.5•Trtminylbeni,r:x
fb
:t*t -butyl D rrmw
►i7
1.Y.4 Trlsrthylberurnr
P-D
' fill • 11jtYl �eM
'.�
D•I:Wropyltolurne
PC
rl Butylberlxnr
NO
NapntWone
1D
1•Chlarrn•3•tlucrpEerlt" 4b1
103
"►�+�A1an Careec� r �•
Hu Wazw"..w 12
NC Orinlunp WSW 3770e
Si 99CkM
T.i 7D4.876.9uV2
Fax• 704-575.909i
DATE: 9717A198
?Ii(;E: Z
Pare Projerl RwM*r-. 92495
L, bmt Prv)ect ID: 9W7268
One collwto: 0711419d Matrix-. Water
I Date. Rec41v": 071111.4
all is Quits m Malys Ana l yit :Aj fw%T mtec
' ---.. ..........
unn
0.5
07124/98
PPM
106.93.4
ugh
0.s
117124►9B
FIRM
127.18•4
AtL
0.5
07/94/98
OP"
630.V-6
u91-
0.5
47/24194
'PN
lD8.90.7
u91Li
0-5
07/24/96
PPM
M-25.2
uy1LI
v.5
071241W
PPM
79. A-5
A/L
9.5
e7124198
1>NM
96.18.4
liO1L
0.5
OVE4198
?PM
1D8.86.1
u91c
0.5
07/24/48
RPM
15.4918
wr1L
v.5
071Z41?8
FVH
106.43.4
uvll
11.5
071Z4196
N914
54:•73.1
uy1;
4.5
071241%
PPw
I06.46.7
uy1L
9.5
n71E4198
PPtt
95.5A•1
u,lt
9.5
07/24/90
?YM
96.12.8
ug/L
9.5
r17124198
P?I
120.62.1
uy1L
0.5
C7124198
PPx
87•b16.3
uu1L
0.5
"t24196
PPM
47-61.6
uo1:
0.5
071W98
Oil
1W.64.4
ug1L
9.5
07/24198
?PK
104.20.3
LWL
0.5
a7124196
P?M
71.43•?
Pig 1L
0.$
071Z41%
i1P►1
108.86.3
uuiL
0.5
071241%
PPn
100•4114
v9/L
9.5
07/24/98
PM
7816.50-0
up1L
0.5
O71Yp14B
OW
00.42.5
UgIL
0.5
9i1241'}8
"m
95.47-6
u91L
9.5
07124t%
lsux
96.82.6
rg1L
0.5
,;7;E4194
99%
1C3•(i5.1
uplL
0.5
37/24/98
"%
108.67.5
sv1L
0.5
O71Z4l98
VIM
95.06.6
4p/L
0.5
07/24/98
"+'�M
95.63.6
WWI
0.5
971UI94
PPP
13S•99.8
upll.
0.5
17124195
va.
44.57.6
u91L
).5
.? r. rya
F"
104.51.8
.dL
0.5
07/24/98
:9fl
91-20.3
J1
I
9lIZa752
�:FI
6E5.4B 9
REPORT OF LABORATORY
ANALYSIS
T hlt feMn
ov 14 be reproo,00a r­vl iZ lWi
w lhou% She wrlRen 00neera ur
Pace Arai t c7
`oNtCtr7-
:'c.
KYmiAhr
TN 138T LIe4
V4 r1r.,knp lWQf `11.4

i 08-03-98 03:02?,M FROM THIKOH
■ . E- I
!I
.i
I
IF Ma►'E5
I yp Not QvttctW
NG wt Calculable
#AL pw�e "ro nq Limit
+� [5l Sun -agate
'I
I
I
1
1'
I
1
E I j
i
! r
liCo�
nC �'�'+►ti""ee' i 7
yC ormk" WON 37706
SG 440DG
TO 19195960538 F0I4
llacv Ara+1111 i 1Z
Hvrlrs.— ., 29f77$
4acc Fra]e "fir: 92495
tivent yr ,e• c :o: W7m
REPORT OF LABORATORY ANALYSIS
MTh 7 $nail 1:1 tW rV-," aed nrrCOi �n l�,I,
w d4fOrJS 11re rrr[I:en uonso-t 0 �,xr Alra•YT7C�i �!r'CC7, ktC
Fir• 1W-673•9001
Kl' 1� �nk.na L'ktar HV[79n
.K US7 LU
', A Qfmwnp waver 21 7

vQ-u) �O U:Ev51 �XUM FOXIKON TO 1g19�960$7$ °�1�
I
EFFD PH Cmtilication
I'oxikon Dtder
i
'err all QAlQC procedures REQUIRED by the Vl'H method followed? Yes-'l;o
� � w
Were all QNQC procedurvt FLEQ TRED by the EFH method followed? YnW No
Were all acce/accepwice standards for tho required QAIQC. YC*w_No
procedures azhieved?
Detail% regardint any aaswerf "No above are provided belew-
wiere anv ilgiuficant modifications madr to the EPH , PH methods Ycs� No X
j as specified in Sec:tiol 11.3?
j
I attest under the pains and pInalties of pc jurjr that, bAwd upon my inquiry of those
individuals immediately responsibIc for ohtai=g the informatiwi, the marcriai co=ined
in this report is, to the bet of my knowledge jnd belirf, accurate and complcta.
I
Signatturc: ��--�'G ;f _ _ Pnsitiop: � . •. fr �a�� f
Yri cd.Namc: �� }=I,��' �•r Date: 5'rIY�
I
I
{
i

sat crrnvvr
Ro;jn%64pc 1rlkinKpY1+W1 !o sx +.t'+[3G SL13Gn)""Wh
!•G6.3Jh•d3Rril •7GDi':rJ41GAM
ealyal3- 3111VIM A 101ii11fLn13134 3nl 31p1 qpK[ r37ft3n31�+
fMCt<nY.1O7164lL MfSm"3/ il:irjw ooHl3w
It 3MY1 —FZW lam i331
'�14■li■+� ate+ Pp43� i '
7b- 3C� L531
•�JaEsfA3 432L '�■31N3Hr '
Pus J040A }a sn[a■uL■�■r3 iy3 io1 ■poyua pJs>y+■14
•a1tY■n
rlo■yaoJax] Play ioy auw■s��J1 hi N1v41° ']0l9t P0441W •sawJ■y■x '
rx Pt�M !i on � 7pC17 1f31
i
"at', 'iti8t 'an 'd7 '1eh Jaaasd■Y 1a�+p°i '
•9L1 a,o� u7v+ 'r x1io=Y •�a3o�a3■tll ffLJ7��P'+[
w■ 14d[.�+ni ►a aLahlruY lea}d►V7 s[' Q J31 wow :■xu,ayia
svr�fFm] SL3 IY al[3f1■h p►SaLPP% 749 cp'3ri171+ Y{7 1 '
1 '
3= 1i7a {
•Ry6■Jb�1W7JL7 ■f7 i .
a1�r. ul fe.�■c1 wad�+eo.[ol+n•S.wo+41Q•Z't '
pua uo3swJa+an,a+H W : ! �Ip041Yd]
Lx■ tq:3T wwy3o�+910 '"6L �aga■s■0 aiII :ayasa►•■ i
•�aJkl% Al11ULJn ut CPi3''
ooti�7 3Lurk3J0 yw[3■uks+a■3■p ■41 JCi 00%aal!
+ypS �¢741iLA rai
-r4.: '60Z 'OH •6Y 'Toa J■as!WL loj*" I l
7CL ,�Ld n+7p> 'Y ASpuwy -.raisM:aen 19!41VVUI
a st5I1■W la�i°at%1 71ur6J0 Jei "akp4N :aadJ000
� 1r:11sL..r,M y i
apu+od■n9 �iaL10o1Y a111olaA !Q4=Cf,lli:1+ Ydi
3ylYN ion] 1131 .�
•7e6t •dcz I 'at leh J3>■[*+a 1■,+a
aJ■d V401 'V xir,dOr 'J■a■Nli■11 i■[s3'u'AJS
pva 1rJ;3t+nw ye ■LsAl*Vf IR31"10 2W"-lp �i �°YaK+ :■awlof��
cp�r ] n+agJf�aS�X /}}lal"A t09 CWIN va
&M3 till -
ACoT ++i 7■al %vuit0=P■+Np■#
LL
�e
B�Dd 8��D9656E6I �L EF.IXU WOO �IdZG 70 86-8D-8G

•.!, w14;ins A.r clajwd. mA ol7w
Trrephonw 4701] 7&3310
Fp. [7at) _15-7472
CHAIN OF CiSTODY RECORD Y
�)
waax orm�ts; of _ a7. �)-109
DUEOATE D-J -I;'$ 9p
Y6E�
CCM PA W fkUE i/ `�v�iM� f • /
ADDREM' �_.(��_-4 t�e�rr� _ 1,
PHONE r. (ij `)) MI6°Y7D FAK #: (41 r}) aS7�7�_
P.O. #; `?% R
PRp.]EGT MANAOER:,
PROJEGI IMOCAT1014: — -7
she" rim With" R "W
, wArrU+rAM P.,Y,Snc P
2 xx a-GWISLLtit
r
' us_ v .'roA ' io to
&, a[M4MH(:ER 1() u
PiiE3ERVAIV TE �! 1 4 sPEN
�
_ � 11� �]�� �NS1 RlJGT1DHS1
Y �j 0 ! COL W14TS
mxI►ro�t
SAMPLE
%)EmTwsCA-nGN
sAMPIE
TYPE
CONTAINED
SI14PL1NG
stZE
TtiP
a
GATE
Tim
j -
-� —
u�-
s=r
-�y
.
►�
--t!z.I—.
1�
Y Leff
L
!�
Val
SAMPLED 9Y:
�, 1
Dom. - I P/ - h iT
OUOTAMN 0:
❑ RUSH ..... BUSINM DAY TURN AROUND
ROUTINE
mpre drapasa! rriror►I7atbn
W• Ihara any ci w khw^ or smowod
canrzmnairs 1n Shew *WON crier Mum
MW i"" mwva7
Yes _„�_^ Ho � tYas'zst I[erera•r ____�
TIME-, - rs v
REUNGUISHED $ .'
DATE:
RECEIVED BY.
DATE:
TI1dE,
TIME-
nEI IN4UISriED Ely:
DATE'
RECEsvEf7 FOR BY'.�')
- J -,
- {
THE
eAETHOL7OF SHIpAIENT
COOL=R TEMP RATUR
e -T

= M r r =
1 MAUR CHAIN Qf CUSTQDY RE�QRfl WDRX ORDER Ot
15 Wiggins AveL, Badlwd, AAA 01T30 _ '}
Te+ephono: (f81) 275.33W C) GY ( DUEOAIE
COMPANY: _ 4 �` I �S _ _
&XIWPLE TYPIE "
CcwrAMER TYK
ANALYSES
ADDRESS: n
1. WATER
P • a.A•s'r4[�
PHONE #: (7J- W75j33Q FAX : riS Z57
3- iiUDaE
sL
1'- L/QA
;. OIL
P.Q. #.
5. DRNMrn WATER
,
PROJECT MANAGER: • i a"A &r
C WAWA (4WA&W 9%
PROJECT IOILOCATION- �G}
7. OTHER (SPEMY
TOXIKON
skwL�r-
SAMPLE
CONTAINER
SAMPLING
PRESERV•1TiVE
SP IONS
Il�TRUDTIriHS
IDENTIFICATION
TYPE
SIZE
T"Pf
0
DATE
I TJAA
COMMEW1
1
0
-z.
la,
SAWLE D BY.
REiQlJISHED
, RELINQU W-ED
9Y
DATE: -
TIME: -
L1ATE: `7 -
TIME: -
DATE -
TWE:
- OUDTATION N:
� - RECEIVED BY.
RE E R f.AB BY. "
CDO R iE P RATURE
L7 GSI1Zp �GZrfS'.
DATE. _ _ ❑ 5uSH ...-- BUSINESS DAY TURN AROUND
TIDE: _ OUTINE
wtrl - _ Semple dsPosal information
Are there any other kno m or &AWKM W
TIME: - - pp gaily iR tlsase �Xf105 01her t?mi - -- -- - ---
- b) 0" is*d above?
yas No ____ n Yes, lit Known
ScFz-