WS-2442_3329_CA_MRP_20150814

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Via FedEx Overnight

August 14, 2015

NC DENR
Division of Waste Management/UST Section
450 Hanes Mill Road, Suite 300
Winston-Salem, NC 27105

Attention: Mr. Thomas Moore

Re: Groundwater Monitoring Report
Former One Stop Store #2
7190 Vance Road
Kernersville, North Carolina
H&H Job No. YOC-123

Dear Mr. Moore:
On behalf of YOCO, Inc., Hart & Hickman, PC (H&H) is providing the attached Groundwater
Monitoring Report for the above-referenced site.

If you have any questions or comments, please do not hesitate to contact me.

Very truly yours,
Hart & Hickman, PC
Stephen R. Libbey, PG
Project Manager

cc: Ms. Donna Draughn, YOCO, Inc.

Groundwater Monitoring Report
One Stop Store #2

YOCO, Inc.
Kernersville, North Carolina
NCDENR Groundwater Incident No. 3329

H&H Job No. YOC-123
August 14, 2015

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Groundwater Monitoring Report
One Stop Store #2
Kernersville, North Carolina
H&H Job No. YOC-123

Table of Contents

Section Page No.

1.0 Introduction ............................................................................................................................ 1
2.0 Receptor Survey Update ........................................................................................................ 6
3.0 Monitoring Well Installations ............................................................................................... 8
4.0 Groundwater Analytical Data .............................................................................................. 9
4.1 Water Levels ........................................................................................................................ 9
4.2 Monitoring Well Analytical Data ........................................................................................ 9
5.0 Conclusions and Recommendations ................................................................................... 11

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List of Tables

Table 1 Summary of Water Supply Well Information
Table 2 Summary of Water Level Data
Table 3 Summary of Groundwater Analytical Results

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Water Supply Well Map
Figure 4 Water Table Surface Map
Figure 5 Benzene Isoconcentration Map
Figure 6 MTBE Isoconcentration Map
Figure 7 Naphthalene Isoconcentration Map

List of Appendices

Appendix A Pre-2007 Groundwater Data
Appendix B Boring Logs and Well Construction Records
Appendix C Groundwater Analytical Data

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Groundwater Monitoring Report
One Stop Store #2
Kernersville, North Carolina
H&H Job No. YOC-123

1.0 Introduction

On behalf of YOCO, Inc. (YOCO), Hart & Hickman, P.C. (H&H) has prepared this Groundwater
Monitoring Report for the One Stop Store #2 facility located at 7190 Vance Road in
Kernersville, Forsyth County, North Carolina (Figure 1). A Site Map is presented as Figure 2.
The NCDENR Groundwater incident number for the site is 3329.

In July 1986, Mr. Walter James (7210 Vance Road) contacted the North Carolina Department of
Environment and Natural Resources (NCDENR) to report strong gasoline odors in water from
his water supply well. NCDENR and the Forsyth County Health Department collected water
samples from Mr. James’ well and the One Stop Store #2 water supply well. Petroleum
hydrocarbons were identified in the James’ water supply well sample.

In March 1988, NCDENR installed and sampled five shallow monitoring wells at the site.
NCDENR also collected Groundwater samples from the One Stop Store #2 water supply well
and surrounding water supply wells, including the James supply well. Petroleum hydrocarbons
were identified in two of the monitoring wells and the James supply well. The monitoring wells
were abandoned at a later date.

A Notice of Violation (NOV) for the release was issued to YOCO on February 10, 1989. In
response to the NOV, YOCO removed the leaking underground storage tank (UST) system.
YOCO currently owns and operates two 6,000-gallon gasoline and one 4,000-gallon kerosene
USTs at the site. These three USTs were installed in March 1989.

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In April and May 1990, NCDENR contracted with Geophex, Ltd. (Geophex) to complete a soil
and Groundwater assessment at the subject site. Six groundwater monitoring wells (GMW-1
through GWM-6) and ten soil borings were installed and sampled. Additionally, nine water
supply wells also were sampled. Petroleum hydrocarbons were identified in three of the water
supply wells and monitoring wells GMW-5 and GMW-6. Petroleum hydrocarbons also were
detected in seven of the soil borings.

In April of 1991, extraction well EW-1 was installed at the site in order to initiate free product
recovery. The free product recovery system operated at the site from November 1991 to 1994.
In 1994, a groundwater pump and treat system was implemented at the site. The pump and treat
system operated from November 1991 to July 2001.

In April 1998, monitoring wells GMW-7 and GMW-8 were installed because monitoring wells
GMW-3, GMW-4 and GMW-5 were repeatedly dry during sampling events. Additionally, at the
request of NCDENR, ten soil borings were installed at the site to further define the extent of soil
impacts in April 1998. Gasoline range total petroleum hydrocarbons (TPH) were detected in two
soil samples located near the existing and former dispenser islands above the NCDENR action
levels. The results of the investigation are discussed in further detail in Waters Edge
Environmental’s (Waters Edge) Soil and Groundwater Assessment Report dated January 22,
1999.

In July 2001, free product was detected in monitoring well GMW-6. Because the groundwater
pump and treat system was not designed to recover free product, it was shut down and free
product recovery using Aggressive Fluid Vapor Recovery (AFVR) was initiated in July 2001.
Three additional AFVR events were conducted in August, October and December 2001. A total
of approximately 1,101 gallons of wastewater and free product were recovered during the events.

In an attempt to locate the source of the free product, YOCO conducted tank tightness testing for
the tanks and associated piping in July 2001. All tanks and piping tested tight. The product
transfer lines were retested on August 27, 2001 and were found to be tight. Additionally, YOCO

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also excavated soils in the vicinity of the two gasoline USTs and associated piping, and
completed a geophysical survey to determine the source of the release. No obvious source of free
product was identified during the excavation and no magnetic anomalies large enough to be an
orphan UST were identified during the geophysical survey.

In November 2001, GeoChem, Inc. collected a sample of free product from GMW-6 for fuel
identification. The results of the fuel analysis indicated that the free product was fresh gasoline
less than ten years old.

Between November 2001 and September 2002, shallow aquifer monitoring wells MW-9 through
MW-13, and vertical extent well VE-1 were installed at the site to further define the extent of
impacts as part of two separate Comprehensive Site Assessment (CSA) addendums conducted by
Waters Edge. The results of the CSA addendums revealed that the groundwater hydrocarbon
plume was primarily located on-site and the adjacent downgradient James property. In both
reports, Waters Edge recommended preparing a Corrective Action Plan (CAP) Addendum to
evaluate remedial options for soil and groundwater at the site. Following submittal of the second
CSA Report Addendum dated January 16, 2003, NCDENR required the submittal of a CAP
Addendum for the site in a letter dated January 22, 2003. The letter also indicated that quarterly
monitoring should be conducted.

Waters Edge prepared a CAP and NCDENR requested CAP Addendum on March 24, 2003 and
April 8, 2003, respectively. The CAP and CAP Addendum proposed abandoning all potable and
non-potable water supply wells within 250 ft of the source area combined with source area soil
excavation.

Between February 2003 and October 2005, Waters Edge conducted quarterly groundwater
monitoring at the site as required by NCDENR. The groundwater analytical data from this
period is included in Appendix A. During this period, Waters Edge also pursued abandoning the
surrounding water supply wells within 250 ft from the source area. According to Waters Edge
August 2005 Groundwater Monitoring and Well Abandonment Report dated October 10, 2005, in

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September 2005 the on-site water supply well and three other surrounding wells were abandoned.
The report concludes that all water supply wells within 250 ft of the source area had been
abandoned and recommended that NCDENR issue a Notice of No Further Action for the incident
following preparation of a Notice of Residual Petroleum.

As requested by NCDENR, an updated receptor survey was conducted and monitoring wells
GMW-1, GMW-2, GMW-4, GMW-5, GMW-6, GMW-7, MW-9, MW-10, MW-11 and EW-1
were sampled on July 10, 2007. Laboratory analytical results indicated the presence of
petroleum-related compounds exceeding the groundwater standards in monitoring wells GMW-6,
GMW-7 and EW-1. Six water supply wells were confirmed as being used for drinking water
within 1,000-foot radius of the site at that time.

In January 2014, YOCO, Inc. contracted with EVO Corporation (EVO) of Winston-Salem, NC to
remove the gasoline (UST-6 and UST-7) and kerosene (UST-8) UST systems at the site. Prior to
the removal activities, monitoring wells GMW-6, EW-1 and VE-1 were properly abandoned.
Approximately 2,274 tons of impacted soils were excavated from the UST basin and associated
product piping and product dispenser excavation. Results of post-excavation confirmation soil
sampling indicated compound concentrations above NCDENR soil-to-groundwater maximum
soil contaminant concentrations (MSCCs), but below residential or commercial/industrial
MSCCs. The removal activities were presented in H&H’s Initial Abatement Action (IAA)
Report dated April 11, 2015.

Based on the results of the IAA activities, H&H recommended installing a new monitoring well
between former monitoring wells GMW-6 and EW-1 and conducting a comprehensive
groundwater sampling event at the site. YOCO, Inc. was also planning to evaluate connecting
the drinking water wells within 1,000 ft of the source area to the municipal water supply. If the
water supply well users are connected to the municipal water supply and groundwater VOC
concentrations are detected below NCDENR gross contamination levels (GCLs), a risk-based
closure should be warranted for the site.

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In subsequent conversations, NCDENR requested that a second monitoring well be installed in
the former UST basin. Additionally, NCDENR indicated that two groundwater sampling events
were required before a risk-based closure was considered for the site. The results of the
monitoring well installations and groundwater sampling events are presented herein.

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2.0 Receptor Survey Update

H&H conducted an initial receptor survey in July 2007 for the area within a 1,500-ft radius of the
source area. The survey was conducted by performing area reconnaissance and checking for
municipal water connections. H&H also conducted an extended survey of properties within
500 ft of the UST area, which included contacts with knowledgeable personnel at those adjacent
properties with structures present.

The results of the survey indicated that Forsyth County water is provided to the site and is
available to properties within a 1,500-foot radius of the site. Thirty-three potential water supply
wells were located within 1,000 ft of the source area at that time. An additional 13 potential
water supply wells were observed on properties located between approximately 1,000 and
1,500 ft of the source area. Of the 33 potential water supply wells within 1,000 ft of the source
area, six water supply wells were confirmed as being used for drinking water. An additional two
water supply wells were confirmed as being used for irrigation purposes only. The remaining 25
water supply wells were not active, or their use could not be confirmed. The closest active water
supply well used for drinking water was located approximately 410 ft northwest and cross-
gradient of the source area.

H&H also conducted a survey for surface water bodies in the area. No surface water bodies are
located within 500 ft of the source area. A tributary to Belews Creek is located approximately
1,900 ft east of the source area and Belews Creek is located approximately 2,500 ft northwest of
the source area.

In June 2013 and September 2014, H&H conducted receptor survey updates for the area within
1,000 ft of the source area. Thirty-three potential water supply wells are located within 1,000 ft
of the source area. Of the 33 potential water supply wells within 1,000 ft of the source area, 4
water supply wells were confirmed as being used for drinking water and 1 water supply well was
confirmed as being used for irrigation purposes only. The remaining 28 water supply wells are
not currently active.

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The water supply well locations are depicted on Figure 3, and supply well owner information and
well specifics are presented in Table 1.

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3.0 Monitoring Well Installations

On September 15, 2014, H&H oversaw the advancement of permanent monitoring wells MW-14
and MW-15 in the UST excavation basin. MW-14 was installed between former wells GMW-6
and EW-1 and MW-15 was installed in the former location of gasoline USTs (UST-6 and UST-
7). The well locations were approved by NCDENR prior to installation.

Geologic Exploration, Inc. of Statesville, North Carolina utilized a Diedrich D-120 drill rig to
advance the monitoring wells. During boring advancement, split spoon soil samples were
collected form each boring at approximate 5 ft intervals and evaluated for evidence of impacts by
visual observations, presence of odors, staining, and organic vapors as measured using a photo-
ionization detector.

Monitoring wells MW-14 and MW-15 were each installed to a depth of 34 ft. The wells were
constructed of 2-inch diameter PVC casing with a 15 ft section of 0.010-inch slot PVC screens.
The well screens were installed to bracket the water table. Monitor well construction details are
summarized in Table 2 and boring logs and well construction records are provided in
Appendix B.

After installation, the monitoring wells were developed and purged. After purging was
completed, the new wells and existing wells were sampled using a dedicated, disposable
polyethylene bailer. The sampling results are discussed in Section 4.0 below.

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4.0 Groundwater Analytical Data

4.1 Water Levels

On September 15, 2014 and July 16, 2015, H&H attempted to measure the depth to groundwater
in monitoring wells GMW-2, GMW-7, MW-9, MW-10, MW-11, MW-12, MW-13, MW-14, and
MW-15. Monitoring well MW-9 could not be located during both events and appears to have
been destroyed. Groundwater gauging data for each well is presented in Table 2. The estimated
water table surface based on July 2015 elevations indicates the groundwater flow direction is to
the east-northeast, which is consistent with the previous monitoring events (Figure 4).

4.2 Monitoring Well Analytical Data
Monitoring wells GMW-2, GMW-7, MW-10, MW-11, MW-12, MW-13, MW-14, and MW-15
were sampled on September 15, 2014 and July 16, 2015. Additionally, water supply wells
WSW-15 and WSW-18 also were sampled during the September 2014 groundwater sampling
event. Prior to sampling, monitoring wells were purged until pH, temperature, and conductivity
stabilized. Groundwater samples were then collected using dedicated polyethylene bailers,
poured in laboratory-supplied containers, marked with identifying labels, and placed in an iced
cooler for delivery under chain-of-custody to a certified laboratory for analyses. Groundwater
samples were analyzed for volatile organic compounds (VOCs) by EPA Method 6200B. The
laboratory analytical datasheets are provided in Appendix C.

September 2014 Sampling Results
September 2014 laboratory analytical results indicated the presence of petroleum-related
compounds that exceeded the groundwater standards in monitoring wells GMW-6, GMW-7,
MW-14, and MW-15 (Table 3). No compounds exceeded GCLs.

Chloroform (3.4 μg/l) was detected at a concertation below the groundwater standard in water
supply well WSW-15. Chloroform is not a typical petroleum compound; therefore, the
chloroform does not appear to be associated with the groundwater plume at the site. No

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compounds were detected above the laboratory detection limits in the sample collected from
water supply well WSW-18.

July 2015 Sampling Results
Similar to September 2014, laboratory analytical results indicated the presence of petroleum-
related compounds that exceeded the groundwater standards in monitoring wells GMW-6,
GMW-7, MW-14, and MW-15 in July 2015 (Table 3). No compounds exceeded GCLs.
Isoconcentration maps for benzene, methyl tertiary butyl ether (MTBE), and naphthalene for the
July 2015 sampling event are presented as Figure 5, 6, and 7, respectively.

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5.0 Conclusions and Recommendations

On September 15, 2014, H&H oversaw the advancement of permanent monitoring wells MW-14
and MW-15 in the UST excavation basin. MW-14 was installed between former wells GMW-6
and EW-1 and MW-15 was installed in the former location of gasoline USTs. The well locations
were approved by NCDENR prior to installation.

Monitoring wells MW-2, GMW-7, MW-10, MW-11, MW-12, MW-13, MW-14, and MW-15
were sampled on September 15, 2014 and July 16, 2015. Additionally, water supply wells
WSW-15 and WSW-18 also were sampled during the September 2014 groundwater sampling
event. Laboratory analytical results indicate the presence of petroleum-related compounds that
exceed groundwater standards in monitoring wells GMW-6, GMW-7, MW-14, and MW-15. No
compounds exceeded the GCLs.

Chloroform was detected at a concertation below the groundwater standard in water supply well
WSW-15. Chloroform is not a typical petroleum compound; therefore, it does not appear to be
associated with the groundwater plume at the site. No compounds were detected above the
laboratory detection limits in the sample collected from water supply well WSW-18.

YOCO, Inc. is planning to connect the four drinking water wells within 1,000 ft of the source
area to the municipal water supply. Following connection of the drinking water well users to the
municipal water supply, and because residual soil impacts do not exceed residential or
commercial/industrial MSCCs and site groundwater VOC concentrations do not exceed
NCDENR GCLs, a risk-based closure should be warranted for the site.

Table 1 (Page 1 of 2)Summary of Water Supply Well InformationOne Stop Store #2Kernersville, North CarolinaH Job No. YOC-123
File: S:\AAA-Master Projects\York Oil - YOC\YOC-123 One Stop Well ReplacementSampling\Data\GWdata July 2015 WSWsDate: 8/14/2015
Table 1 Page 1 of 2Hart & Hickman, PC
Map ID Parcel ID No.Owner Property Address Owner Address Owner Telephone No.Direction/Distance(ft) From Source Well/Use /Depth(ft)Casing (ft)
1 6878-83-1503 Brent Peters 1750 Kerner Rd.
Kernersville, NC 27284
1750 Kerner Rd.
Kernersville, NC 27284 Not Available South/890 Yes/Not Used Not Available Not Available
2, 3 Not Available Deborah Mccuiston 1796 Kerner Rd.
Kernersville, NC 27284 Kernersville, NC 27284 Not Available South/670 & 650 Yes; 2 observed/Not
Used Not Available Not Available
4 6878-83-3933 John Strother 1787 Kerner Rd.
Kernersville, NC 27284 Kernersville, NC 27284 336-399-3244 Southeast/520 Yes/Drinking; also
supplies 1781 6/430 150
5 6878-84-3007 Walter James 7210 Vance Road Kernersville, NC 27284 7210 Vance Road Kernersville, NC 27284 336-993-6684 Southeast/310 Yes/Not Used 6/330 Unknown
6 6878-74-7232 William Shreve, Jr.7164 Vance Road Kernersville, NC 27284 7164 Vance Road Kernersville, NC 27284 336-993-4385 West/320 Yes/Not Used 24/35 None
7, 8 6878-84-3351 Mark Auman 7220 Vance Road Kernersville, NC 27284 7220 Vance Road Kernersville, NC 27284 336-996-1849 East/280 & 300 Yes/Not Used 8 - unknown/30 Unknown
9 6878-84-4261 Virgina Ball 7230 Vance Road Kernersville, NC 27284 7230 Vance Road Kernersville, NC 27284 336-993-4039 East/420 Yes/Not Used Unknown Unknown
10 6878-84-6271 Ronnie Spivey 7250 Vance Road Kernersville, NC 27284 7250 Vance Road Kernersville, NC 27284 Not Available East/610 Yes/Not Used Not Available Not Available
11 6878-84-9260 Dott Tilley 7280 Vance Road Kernersville, NC 27284 7280 Vance Road Kernersville, NC 27284 Not Available East/940 Yes/Not Used Not Available Not Available
12 6878-84-6566 Greg Smith 7255 Vance Road Kernersville, NC 27284 7255 Vance Road Kernersville, NC 27284 336-996-1253 East-Northeast/600 Yes/Not Used Not Available Not Available
13 6878-84-3558 Danny Sell 7201 Vance Road Kernersville, NC 27284 7201 Vance Road Kernersville, NC 27284 336-996-0500 Northeast/380 Yes/Not Used 6/425 71
14 6878-84-2609 Patricia Savage 1810 Kerner Rd. Kernersville, NC 27284 182 Arthur Miller Rd. Clemmons, NC 27012 336-996-8538 North-northeast/360 Yes/Not used according to 1820 Not Available Not Available
15, 16 6878-84-2840 Bonner Ray Mccraw 1820 Kerner Rd. Kernersville, NC 27284 Kernersville, NC 27284 336-993-2323 Northeast/470 & 530 Not Used 16 - 6/108 16 - 73
17 6878-84-2971 Keith D. Sharpe 1830 Kerner Rd. Kernersville, NC 27284 Kernersville, NC 27284 336-993-8796 Northeast/600 Yes/Not Used Not Available Not Available
18 6878-84-5834 Timothy Lee Robertson 1825 Kerner Rd. Kernersville, NC 27284 Kernersville, NC 27284 Not Available Northeast/680 Yes/Drinking according to 1820 Not Available Not Available
19 6878-85-3000 Royce E. Voss 1840 Kerner Rd. Kernersville, NC 27284 910 Weavil Rd. Kernersville, NC 27284 336-788-9247 Northeast/690 Yes/Not Used Unknown Unknown
20 6878-85-3029 Stephen Ray Maness 1850 Kerner Rd. Kernersville, NC 27284 1850 Kerner Rd. Kernersville, NC 27284 336-992-0253 Northeast/790 Yes/Not Used Unknown Unknown
21 6878-85-3139 Gary Spring 1856 Kerner Rd. Kernersville, NC 27284 Kernersville, NC 27284 Not Available Northeast/890 Yes/Not Used Not Available Not Available
22 6878-74-7684 Jane Collins 110 Kerner Knolls Dr. Kernersville, NC 27284 8427 Mears Fork Road Summerfield, NC 27358 336-996-8578 Northwest/340 Yes/Not Used Unknown Unknown
23 6878-74-7794 Elmer Hackler 120 Kerner Knolls Dr. Kernersville, NC 27284 120 Kerner Knolls Dr. Kernersville, NC27284 336-996-3885 Northwest/410 Yes/Does not drink, no county water Unknown/60 Unknown
24 6878-74-8813 Kenton T. Berrier 130 Kerner Knolls Dr. Kernersville, NC 27284 130 Kerner Knolls Dr. Kernersville, NC 27284 336-996-1605 Northwest/550 Yes/Not Used Unknown/Unknown Unknown
Table 1 (Page 2 of 2)Summary of Water Supply Well InformationOne Stop Store #2Kernersville, North CarolinaH Job No. YOC-123
File: S:\AAA-Master Projects\York Oil - YOC\YOC-123 One Stop Well ReplacementSampling\Data\GWdata July 2015 WSWsDate: 8/14/2015
Table 1 Page 2 of 2Hart & Hickman, PC
Map ID Parcel ID No.Owner Property Address Owner Address Owner Telephone No.Direction/Distance(ft) From Source Well/Use /Depth(ft)Casing (ft)
25 6878-74-8934 Mary M. Lawson 140 Kerner Knolls Dr.
Kernersville, NC 27284
140 Kerner Knolls Dr.
Kernersville, NC 27284 Not Available North northwest/640 Yes/Not Used Not Available Not Available
26 6878-84-0963 Larry L. Florke 135 Kerner Knolls Dr.
Kernersville, NC 27284
135 Kerner Knolls Dr.
Kernersville, NC 27284 Not Available North/620 Yes/Not Used Not Available Not Available
27 6878-75-8039 Wayne C. Vaughn 150 Kerner Knolls Dr.
Kernersville, NC 27284
150 Kerner Knolls Dr.
Kernersville, NC 27284 336-993-5181 North Northwest/690 Yes/Not Used Unknown Unknown
28 6878-85-1014 Marlene L. Cutrell 145 Kerner Knolls Dr. Kernersville, NC 27284 145 Kerner Knolls Dr. Kernersville, NC 27284 Not Available North/680 Yes/Not Used Not Available Not Available
29 6878-85-1105 Richard E. Montgomery 155 Kerner Knolls Dr. Kernersville, NC 27284 155 Kerner Knolls Dr. Kernersville, NC 27284 336-993-1027 North/790 Yes/Irrigation Unknown Unknown
30 6878-75-8234 Chester L. Bowman 170 Kerner Knolls Dr. Kernersville, NC 27284 170 Kerner Knolls Dr. Kernersville, NC 27284 336-996-1451 Northwest/920 Yes/Not Used Unknown Unknown
31 6878-85-1217 David M. Hughes 165 Kerner Knolls Dr. Kernersville, NC 27284 Kernersville, NC 27284 336-996-1739 North/900 Yes/Not Used Not Available Not Available
32 6878-74-4626 Stephen Vanhoy 7131 Vance Road Kernersville, NC 27284 Kernersville, NC 27284 Not Available West/730 Yes/Not Used Not Available Not Available
33 6878-74-1439 Henry Vanhoy 7097 Vance Road Kernersville, NC 27284 Kernersville, NC 27284 Not Available West Northwest/975 Yes/Not Used Not Available Not Available
Timothy Bertaux 7094 Vance Road Kernersville, NC 27284 7094 Vance Road Kernersville, NC 27284
Mary Avant 7300 Vance Road Kernersville, NC 27284 632 Hopkins Road Kernersville, NC 27284
Alvin Newsome 7320 Vance Road Kernersville, NC 27284 7320 Vance Road Kernersville, NC 27284
6878-75-8661 Pamela Mitchell Teague 200 Kerner Knolls Dr. Kernersville, NC 27284 200 Kerner Knolls Dr. Kernersville, NC 27284
6878-75-8881 Charles W. Hall 220 Kerner Knolls Dr. Kernersville, NC 27284 220 Kerner Knolls Dr. Kernersville, NC 27284
6878-85-1759 Lawrence Lucas 221 Kerner Knolls Dr. Kernersville, NC 27284 FL 34133
6878-85-3249 Brian S. Goins 1862 Kerner Rd. Kernersville, NC 27284 NC 27284
6878-85-6569 Chadelyn Gidcumb 1879 Kerner Rd. Kernersville, NC 27284 NC 27284
6878-85-3760 Earl Lee Moses 1880 Kerner Rd. Kernersville, NC 27284 NC 27284
Notes:
Information based on Forsyth County GIS System data and site receptor surveys, 2014.Contiguous properties are shown on Figure 3.
File: GWdata July 2015\water levels
Date: 8/14/2015
Table 2 Page 1 of 1
Hart & Hickman, PC
Monitoring TOC Well Screen
MW-9 849.01 45.00 20 24.50 824.51 NL N/A NL N/A
MW-10 850.51 45.00 20 25.63 824.88 26.00 824.51 28.40 822.11
MW-11 846.21 45.00 20.0 21.75 824.46 22.64 823.57 24.83 821.38
MW-12 852.27 45.00 20 NM N/A 28.72 823.55 31.12 821.15
MW-13 842.57 45.00 20 21.20 821.37 21.97 820.60 23.98 818.59
GMW-1 852.80 30.25 10 NM N/A DRY N/A DRY N/A
GMW-2 835.13 15.50 10 6.11 829.02 14.88 820.25 14.65 820.48
GMW-4 846.20 20.50 10 NM N/A N/A N/A N/A N/A
GMW-5 848.51 25.25 10 NM N/A DRY N/A DRY N/A
GMW-6 848.84 28.00 10 24.66 824.18 N/A N/A N/A N/A
GMW-7 848.90 35.00 10 26.23 822.67 26.72 822.18 28.90 820.00
EW-1 NA 35.00 20 24.50 --
VE-1 849.45 70.00 5 25.01 824.44
MW-14 848.26 34.00 15 N/A N/A 27.58 820.68 27.58 820.68
MW-15 847.88 34.00 15 N/A N/A 25.12 822.76 27.43 820.45
Notes:
NS = Not Surveyed; N/A = Not Available; NL = Not Located
TOC = Top of well casing
bgs = below ground surface
Water Table
Depth TOC (ft) Elevation (ft)
Apart from MW-14 and MW-15, TOC elevations taken from Waters Edge Envrionmental's CSA Report Addendum
dated January 16, 2003. TOC elevations for MW-14 and MW-15 surveyed by H&H in September 2014.
Depth TOC (ft) Elevation (ft) Depth TOC (ft)
1 Elevation (ft)
S:\AAA-Master Projects\York Oil - YOC\YOC-123 One Stop Well ReplacementSampling\Data\GWdata July 2015GWdata July 2015
8/14/2015
Table 3 Page 1 of 2Hart & Hickman, PC
GMW-1 MW-9
7/10/2007 7/10/2007 6/10/2013 7/16/2015 7/10/2007 6/27/2013 7/10/2007 6/10/2013 9/15/2014 7/16/2015 7/10/2007 7/10/2007 9/15/2014 7/16/2015 7/10/2007 9/15/2014 7/16/2015
VOCs (6210D/6200B) (µg/l)
Acetone <0.50 <0.50 <10 NA <5.0 930 <20 <200 28 NA <0.50 <0.50 <10 NA <10 <10 NA 6,000 6,000,000
Benzene <0.50 <0.50 <0.50 <0.50 11,000 28,000 9,400 2,600 610 665 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1 5,000
Toluene <0.50 4.1 <0.50 <0.50 7,500 49,000 9,300 3,600 730 823 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 600 260,000
Ethylbenzene <0.50 <0.50 <0.50 <0.50 1,400 4,500 1,700 1,300 470 557 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 600 84,500
Isopropyl ether (IPE)<0.50 <0.50 <0.50 <0.50 1,600 1,400 930 140 39 57.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 70 70,000
Isopropylbenzene <0.50 <0.50 <0.50 <0.50 63 170 91 63 25 26.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 70 25,000
m,p-Xylenes 7,400 17,000 4,100 2,500 650 870 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 500 85,500
Methyl Tert Butyl Ether 14,000 24,000 2,900 240 51 74.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 20 20,000
Naphthalene <2.0 <2.0 <2.0 <2.0 390 690 370 230 62 125 <2.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 6 6,000
o-Xylene <0.50 <0.50 <0.50 <0.50 2,900 7,500 1,600 910 250 296 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 500 85,500
n-Butylbenzene <0.50 <0.50 <0.50 <0.50 <5.0 74 <20 18 4.1 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 70 6,900
sec-Butylbenzene <0.50 <0.50 <0.50 <0.50 12 <25 <20 45 4.9 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 70 8,500
1,2-Dichloroethane <0.50 <0.50 <0.50 <0.50 160 220 110 <10 1.2 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.4 400
p-Isopropyltoluene <0.50 <0.50 <0.50 NA 48 <25 24 34 2.9 NA <0.50 <0.50 <0.50 NA <0.50 <0.50 NA 25 11,700
n-Propylbenzene 130 480 230 180 69 69.6 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 70 30,000
1,2,4-Trimethylbenzene 2,000 3,900 1,300 1,100 260 317 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 400 28,500
1,2-Dibromoethane(EDB)<0.50 <0.50 <0.50 <0.50 7.4 84 <20 <10 <0.50 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.02 50
1,3,5-Trimethylbenzene <0.50 <0.50 <0.50 <0.50 620 1,000 370 350 120 129 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 400 25,000
Chloroform <0.50 <0.50 <0.50 <0.50 <5.0 <25 <20 <10 <0.50 <5.0 8.3 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 70 70,000
Styrene <0.50 <0.50 <0.50 <0.50 9.3 92 30 <10 0.97 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 70 70,000
EPA Method follows parameter in parenthesis.
Bold indicates concentration exceeds groundwater standard.
Bold italics indicates concentration exceeds groundwater GCL.
VOCs = Volatile Organic Compounds; GCL = Gross Contamination Levels
NA = Not analyzed
Groundwater
µg/l)
GCL (µg/l)SAMPLE ID / DATE
Table 3 (Page 1 of 2)
Summary of Groundwater Analytical ResultsOne Stop Store #2Kernersville, North Carolina
H&H Job No. YOC-123
(1)
S:\AAA-Master Projects\York Oil - YOC\YOC-123 One Stop Well ReplacementSampling\Data\GWdata July 2015GWdata July 2015
8/14/2015
Table 3 Page 2 of 2
Hart & Hickman, PC
9/15/2014 7/16/2015 6/10/2013 9/15/2014 7/16/2015 9/15/2014 7/16/2015 9/15/2014 7/16/2015 7/10/2007 6/27/2013 9/15/2014 9/15/2014
VOCs (6210D/6200B) (µg/l)
Acetone <10 NA <10 <10 NA 61 NA <10 NA <5.0 <500 <10 <10 6,000 6,000,000
Benzene <0.50 <0.50 <0.50 <0.50 <0.50 1,800 281 680 1,140 8,300 7,400 <0.50 <0.50 1 5,000
Toluene <0.50 <0.50 <0.50 <0.50 <0.50 5,100 650 5,900 9,060 6,100 4,100 <0.50 <0.50 600 260,000
Ethylbenzene 930 119 2,000 3,730 800 870 <0.50 <0.50 600 84,500
Isopropyl ether (IPE)<0.50 <0.50 <0.50 <0.50 <0.50 60 9.5 5.9 <10 480 660 <0.50 <0.50 70 70,000
Isopropylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 79 16.9 160 409 41 60 <0.50 <0.50 70 25,000
m,p-Xylenes <1.0 <1.0 <1.0 <1.0 <1.0 2,000 280 5,900 12,000 6,700 3,300 <1.0 <1.0 500 85,500
Methyl Tert Butyl Ether <1.0 <1.0 <1.0 <1.0 <1.0 910 115 27 196 11,000 14,000 <1.0 <1.0 20 20,000
Naphthalene <1.0 <1.0 <1.0 <1.0 <1.0 240 25.5 490 1,460 460 220 <1.0 <1.0 6 6,000
o-Xylene <0.50 <0.50 <0.50 <0.50 <0.50 910 119 2,300 4,830 2,600 400 <0.50 <0.50 500 85,500
n-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 23 6.1 37 288 <5.0 55 <0.50 <0.50 70 6,900
sec-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 15 5.1 25 <10 <5.0 <25 <0.50 <0.50 70 8,500
1,2-Dichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 7.1 <2.5 <0.50 <10 21 <25 <0.50 <0.50 0.4 400
p-Isopropyltoluene <0.50 NA <0.50 <0.50 NA 6.9 NA 9.7 NA 53 <25 <0.50 <0.50 25 11,700
n-Propylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 230 29.8 450 1,420 110 170 <0.50 <0.50 70 30,000
1,2,4-Trimethylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 770 86.2 2,500 6,910 2,400 1,800 <0.50 <0.50 400 28,500
1,2-Dibromoethane(EDB)<0.50 <0.50 <0.50 <0.50 <0.50 3.9 <2.5 2.0 <10 <5.0 <25 <0.50 <0.50 0.02 50
1,3,5-Trimethylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 230 28.3 710 2,470 750 420 <0.50 <0.50 400 25,000
Chloroform <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <2.5 <0.50 <10 <5.0 <25 3.4 <0.50 70 70,000
Styrene <0.50 <0.50 <0.50 <0.50 <0.50 20 <2.5 51 91.1 <5.0 <25 <0.50 <0.50 70 70,000
EPA Method follows parameter in parenthesis.
Bold indicates concentration exceeds groundwater standard.
Bold italics indicates concentration exceeds groundwater GCL.
VOCs = Volatile Organic Compounds; GCL = Gross Contamination Level
(1) Indicates that 2-Hexanone (2.6 µg/l) and Methyl Isobutyl Ketone (2.8 µg/l) detected during the September 2014 sampling event
(2) Indicates that 2-Hexanone (6 µg/l), Methyl Isobutyl Ketone (6.3 µg/l) and tert-Butylbenzene (0.88 µg/l) detected during the September 2014 sampling event
(2)(3)SAMPLE ID / DATE
Table 3 (Page 2 of 2)
Summary of Groundwater Analytical Results
One Stop Store #2
Kernersville, North CarolinaH&H Job No. YOC-123
Groundwater
µg/l)
GCL (µg/l)
TITLE
PROJECT
SITE LOCATION MAP
ONE STOP STORE #2
KERNERSVILLE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
7-15-15 0
1YOC-123
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
BELEWS CREEK, N.C. 1969 REVISED 1994
SITE

Appendix A
Pre-2007 Groundwater Data

Appendix B
Boring Logs and Well Construction Records
Asphalt and gravel
Slightly moist, brown, clayey SILT
Moist, light brown, clayey SILT (odor)
Very moist, light brown, clayey SILT (heavy odor)
Bottom of borehole at 34.0 feet.
Grout
2" PVCRiser
BentoniteSeal
Sand FilterPack2" PVC
SlottedScreen
DRAWN BY:GES
BORING COMPLETED:9/15/14
DRILLING CONTRACTOR:Geologic Exploration Remarks:
DRILL RIG/ METHOD:D-120 / HSA
SAMPLING METHOD:Cuttings Hand Auger to 5' BGS
BORING STARTED:9/15/14
LOGGED BY:GES
TOTAL DEPTH: 34 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION BORING DIAGRAM
OV
A

(
p
p
m
)
SA
M
P
.
BK
G
.
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
Sheet 1 of 1
BORING NUMBER MW-14
PROJECT:One Stop Store #2
JOB NUMBER:YOC-123
LOCATION:Kernersville, North Carolina
BO
R
I
N
G

L
O
G

-

H
A
R
T

H
I
C
K
M
A
N
.
G
D
T

-

8
/
1
0
/
1
5

1
5
:
1
8

-

S
:
\
A
A
A
-
M
A
S
T
E
R

G
I
N
T

P
R
O
J
E
C
T
S
\
Y
O
C
-
1
2
3

K
E
R
N
E
R
S
V
I
L
L
E

W
E
L
L
S
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
30
35
0
5
10
15
20
25
30
35
Asphalt and gravel
Slightly moist, brown, clayey SILT
Moist, gray, clayey SILT (odor)
Very moist, tan, clayey SILT (odor)
Bottom of borehole at 34.0 feet.
Grout
2" PVCRiser
BentoniteSeal
Sand FilterPack2" PVC
SlottedScreen
DRAWN BY:GES
BORING COMPLETED:9/15/14
DRILLING CONTRACTOR:Geologic Exploration Remarks:
DRILL RIG/ METHOD:D-120 / HSA
SAMPLING METHOD:Cuttings Hand Auger to 5' BGS
BORING STARTED:9/15/14
LOGGED BY:GES
TOTAL DEPTH: 34 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:
DE
P
T
H
(f
t
)
DE
P
T
H
(f
t
)
LI
T
H
O
L
O
G
Y
MATERIAL DESCRIPTION BORING DIAGRAM
OV
A

(
p
p
m
)
SA
M
P
.
BK
G
.
RE
C
O
V
E
R
Y

(
%
)
SA
M
P
L
E

T
Y
P
E
NU
M
B
E
R
Sheet 1 of 1
BORING NUMBER MW-15
PROJECT:One Stop Store #2
JOB NUMBER:YOC-123
LOCATION:Kernersville, North Carolina
BO
R
I
N
G

L
O
G

-

H
A
R
T

H
I
C
K
M
A
N
.
G
D
T

-

8
/
1
0
/
1
5

1
5
:
1
8

-

S
:
\
A
A
A
-
M
A
S
T
E
R

G
I
N
T

P
R
O
J
E
C
T
S
\
Y
O
C
-
1
2
3

K
E
R
N
E
R
S
V
I
L
L
E

W
E
L
L
S
.
G
P
J
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
30
35
0
5
10
15
20
25
30
35

Appendix C
Groundwater Analytical Data
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
09/22/2014
Hart & Hickman (Charlotte)
Steve Libbey
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: YOC-122 One Stop Store #2
Lab Submittal Date: 09/16/2014
Prism Work Order: 4090257
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
Data Qualifiers Key Reference:
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 29
Sample Receipt Summary
09/22/2014
Prism Work Order: 4090257
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
4090257-01 09/15/14GMW-7 09/16/14Water
4090257-02 09/15/14MW-10 09/16/14Water
4090257-03 09/15/14MW-11 09/16/14Water
4090257-04 09/15/14MW-12 09/16/14Water
4090257-05 09/15/14MW-13 09/16/14Water
4090257-06 09/16/14MW-14 09/16/14Water
4090257-07 09/16/14MW-15 09/16/14Water
4090257-08 09/15/14WSW-15 09/16/14Water
4090257-09 09/15/14WSW-18 09/16/14Water
Samples were received in good condition at 1.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 29
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 4090257
09/22/2014
Summary of Detections
260 ug/L4090257-01 GMW-7 1,2,4-Trimethylbenzene *SM6200 B
1.2 ug/L4090257-01 GMW-7 1,2-Dichloroethane *SM6200 B
120 ug/L4090257-01 GMW-7 1,3,5-Trimethylbenzene *SM6200 B
2.9 ug/L4090257-01 GMW-7 4-Isopropyltoluene *SM6200 B
28 ug/L4090257-01 GMW-7 Acetone *SM6200 B
610 ug/L4090257-01 GMW-7 Benzene *SM6200 B
470 ug/L4090257-01 GMW-7 Ethylbenzene *SM6200 B
39 ug/L4090257-01 GMW-7 Isopropyl Ether *SM6200 B
25 ug/L4090257-01 GMW-7 Isopropylbenzene (Cumene)*SM6200 B
650 ug/L4090257-01 GMW-7 m,p-Xylenes *SM6200 B
2.6 ug/L4090257-01 GMW-7 Methyl Butyl Ketone (2-Hexanone)*SM6200 B
2.8 ug/L4090257-01 GMW-7 Methyl Isobutyl Ketone *SM6200 B
51 ug/L4090257-01 GMW-7 Methyl-tert-Butyl Ether *SM6200 B
62 ug/L4090257-01 GMW-7 Naphthalene *SM6200 B
4.1 ug/L4090257-01 GMW-7 n-Butylbenzene *SM6200 B
69 ug/L4090257-01 GMW-7 n-Propylbenzene *SM6200 B
250 ug/L4090257-01 GMW-7 o-Xylene *SM6200 B
4.9 ug/L4090257-01 GMW-7 sec-Butylbenzene *SM6200 B
0.97 ug/L4090257-01 GMW-7 Styrene *SM6200 B
730 ug/L4090257-01 GMW-7 Toluene *SM6200 B
900 ug/L4090257-01 GMW-7 Xylenes, total *SM6200 B
770 ug/L4090257-06 MW-14 1,2,4-Trimethylbenzene *SM6200 B
3.9 ug/L4090257-06 MW-14 1,2-Dibromoethane *SM6200 B
7.1 ug/L4090257-06 MW-14 1,2-Dichloroethane *SM6200 B
230 ug/L4090257-06 MW-14 1,3,5-Trimethylbenzene *SM6200 B
6.9 ug/L4090257-06 MW-14 4-Isopropyltoluene *SM6200 B
61 ug/L4090257-06 MW-14 Acetone *SM6200 B
1800 ug/L4090257-06 MW-14 Benzene *SM6200 B
930 ug/L4090257-06 MW-14 Ethylbenzene *SM6200 B
60 ug/L4090257-06 MW-14 Isopropyl Ether *SM6200 B
79 ug/L4090257-06 MW-14 Isopropylbenzene (Cumene)*SM6200 B
2000 ug/L4090257-06 MW-14 m,p-Xylenes *SM6200 B
6.0 ug/L4090257-06 MW-14 Methyl Butyl Ketone (2-Hexanone)*SM6200 B
6.3 ug/L4090257-06 MW-14 Methyl Isobutyl Ketone *SM6200 B
910 ug/L4090257-06 MW-14 Methyl-tert-Butyl Ether *SM6200 B
240 ug/L4090257-06 MW-14 Naphthalene *SM6200 B
23 ug/L4090257-06 MW-14 n-Butylbenzene *SM6200 B
230 ug/L4090257-06 MW-14 n-Propylbenzene *SM6200 B
910 ug/L4090257-06 MW-14 o-Xylene *SM6200 B
15 ug/L4090257-06 MW-14 sec-Butylbenzene *SM6200 B
20 ug/L4090257-06 MW-14 Styrene *SM6200 B
0.88 ug/L4090257-06 MW-14 tert-Butylbenzene *SM6200 B
5100 ug/L4090257-06 MW-14 Toluene *SM6200 B
2900 ug/L4090257-06 MW-14 Xylenes, total *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 29
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 4090257
09/22/2014
Summary of Detections
2500 ug/L4090257-07 MW-15 1,2,4-Trimethylbenzene *SM6200 B
2.0 ug/L4090257-07 MW-15 1,2-Dibromoethane *SM6200 B
710 ug/L4090257-07 MW-15 1,3,5-Trimethylbenzene *SM6200 B
9.7 ug/L4090257-07 MW-15 4-Isopropyltoluene *SM6200 B
680 ug/L4090257-07 MW-15 Benzene *SM6200 B
2000 ug/L4090257-07 MW-15 Ethylbenzene *SM6200 B
5.9 ug/L4090257-07 MW-15 Isopropyl Ether *SM6200 B
160 ug/L4090257-07 MW-15 Isopropylbenzene (Cumene)*SM6200 B
5900 ug/L4090257-07 MW-15 m,p-Xylenes *SM6200 B
11 ug/L4090257-07 MW-15 Methyl Butyl Ketone (2-Hexanone)*SM6200 B
11 ug/L4090257-07 MW-15 Methyl Isobutyl Ketone *SM6200 B
27 ug/L4090257-07 MW-15 Methyl-tert-Butyl Ether *SM6200 B
490 ug/L4090257-07 MW-15 Naphthalene *SM6200 B
37 ug/L4090257-07 MW-15 n-Butylbenzene *SM6200 B
450 ug/L4090257-07 MW-15 n-Propylbenzene *SM6200 B
2300 ug/L4090257-07 MW-15 o-Xylene *SM6200 B
25 ug/L4090257-07 MW-15 sec-Butylbenzene *SM6200 B
51 ug/L4090257-07 MW-15 Styrene *SM6200 B
1.5 ug/L4090257-07 MW-15 tert-Butylbenzene *SM6200 B
5900 ug/L4090257-07 MW-15 Toluene *SM6200 B
8200 ug/L4090257-07 MW-15 Xylenes, total *SM6200 B
3.4 ug/L4090257-08 WSW-15 Chloroform *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: GMW-7
Prism Sample ID: 4090257-01
Prism Work Order: 4090257
Time Collected: 09/15/14 15:10
Time Submitted: 09/16/14 15:42
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0701,1,1,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0751,1,1-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0751,1,2,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0681,1,2-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0381,1-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0571,1-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0721,1-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.121,2,3-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0901,2,3-Trichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.151,2,4-Trichlorobenzene
260 *SM6200 B P4I026920109/19/14 1:43 VHLug/L 0.761,2,4-Trimethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 21:41 VHLug/L 0.591,2-Dibromo-3-chloropropane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0411,2-Dibromoethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0441,2-Dichlorobenzene
1.2 *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0541,2-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0621,2-Dichloropropane
120 *SM6200 B P4I026920109/19/14 1:43 VHLug/L 0.761,3,5-Trimethylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0701,3-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0541,3-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0591,4-Dichlorobenzene
BRL *SM6200 B P4I026912.0 9/17/14 21:41 VHLug/L 0.272,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0382-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0534-Chlorotoluene
2.9 *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.0594-Isopropyltoluene
28 *SM6200 B P4I02691109/17/14 21:41 VHLug/L 1.5Acetone
610 *SM6200 B P4I026920109/19/14 1:43 VHLug/L 1.1Benzene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.088Bromobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.050Bromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.031Bromodichloromethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.10Bromoform
BRL *SM6200 B P4I026911.0 9/17/14 21:41 VHLug/L 0.24Bromomethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.065Carbon Tetrachloride
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.025Chlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.088Chloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.053Chloroform
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.032Chloromethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.061cis-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.065cis-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.062Dibromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.044Dibromomethane
BRL *SM6200 B P4I026911.0 9/17/14 21:41 VHLug/L 0.057Dichlorodifluoromethane
BRL *SM6200 B P4I026912009/17/14 21:41 VHLCCVug/L 42Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: GMW-7
Prism Sample ID: 4090257-01
Prism Work Order: 4090257
Time Collected: 09/15/14 15:10
Time Submitted: 09/16/14 15:42
470 *SM6200 B P4I026920109/19/14 1:43 VHLug/L 1.1Ethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 21:41 VHLug/L 0.41Hexachlorobutadiene
39 *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.042Isopropyl Ether
25 *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.034Isopropylbenzene (Cumene)
650 *SM6200 B P4I026920209/19/14 1:43 VHLug/L 2.2m,p-Xylenes
2.6 *SM6200 B P4I026911.0 9/17/14 21:41 VHLug/L 0.11Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P4I026915.0 9/17/14 21:41 VHLug/L 0.83Methyl Ethyl Ketone (2-Butanone)
2.8 *SM6200 B P4I026911.0 9/17/14 21:41 VHLug/L 0.048Methyl Isobutyl Ketone
BRL *SM6200 B P4I026912.0 9/17/14 21:41 VHLug/L 0.073Methylene Chloride
51 *SM6200 B P4I026911.0 9/17/14 21:41 VHLug/L 0.056Methyl-tert-Butyl Ether
62 *SM6200 B P4I026911.0 9/17/14 21:41 VHLug/L 0.094Naphthalene
4.1 *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.059n-Butylbenzene
69 *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.059n-Propylbenzene
250 *SM6200 B P4I026920109/19/14 1:43 VHLug/L 1.3o-Xylene
4.9 *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.054sec-Butylbenzene
0.97 *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.034Styrene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.11tert-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.096Tetrachloroethylene
730 *SM6200 B P4I026920109/19/14 1:43 VHLug/L 1.1Toluene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.061trans-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.054trans-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.044Trichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.050Trichlorofluoromethane
BRL *SM6200 B P4I026915.0 9/17/14 21:41 VHLug/L 1.3Vinyl acetate
BRL *SM6200 B P4I026910.50 9/17/14 21:41 VHLug/L 0.068Vinyl chloride
900 *SM6200 B P4I026920309/19/14 1:43 VHLug/L 3.4Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-130102 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-10
Prism Sample ID: 4090257-02
Prism Work Order: 4090257
Time Collected: 09/15/14 14:45
Time Submitted: 09/16/14 15:42
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0701,1,1,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0751,1,1-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0751,1,2,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0681,1,2-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0381,1-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0571,1-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0721,1-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.121,2,3-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0901,2,3-Trichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.151,2,4-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0381,2,4-Trimethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 19:08 VHLug/L 0.591,2-Dibromo-3-chloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0411,2-Dibromoethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0441,2-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0541,2-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0621,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0381,3,5-Trimethylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0701,3-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0541,3-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0591,4-Dichlorobenzene
BRL *SM6200 B P4I026912.0 9/17/14 19:08 VHLug/L 0.272,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0382-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0534-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.0594-Isopropyltoluene
BRL *SM6200 B P4I02691109/17/14 19:08 VHLug/L 1.5Acetone
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.054Benzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.088Bromobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.050Bromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.031Bromodichloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.10Bromoform
BRL *SM6200 B P4I026911.0 9/17/14 19:08 VHLug/L 0.24Bromomethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.065Carbon Tetrachloride
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.025Chlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.088Chloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.053Chloroform
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.032Chloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.061cis-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.065cis-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.062Dibromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.044Dibromomethane
BRL *SM6200 B P4I026911.0 9/17/14 19:08 VHLug/L 0.057Dichlorodifluoromethane
BRL *SM6200 B P4I026912009/17/14 19:08 VHLCCVug/L 42Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-10
Prism Sample ID: 4090257-02
Prism Work Order: 4090257
Time Collected: 09/15/14 14:45
Time Submitted: 09/16/14 15:42
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.054Ethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 19:08 VHLug/L 0.41Hexachlorobutadiene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.042Isopropyl Ether
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.034Isopropylbenzene (Cumene)
BRL *SM6200 B P4I026911.0 9/17/14 19:08 VHLug/L 0.11m,p-Xylenes
BRL *SM6200 B P4I026911.0 9/17/14 19:08 VHLug/L 0.11Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P4I026915.0 9/17/14 19:08 VHLug/L 0.83Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P4I026911.0 9/17/14 19:08 VHLug/L 0.048Methyl Isobutyl Ketone
BRL *SM6200 B P4I026912.0 9/17/14 19:08 VHLug/L 0.073Methylene Chloride
BRL *SM6200 B P4I026911.0 9/17/14 19:08 VHLug/L 0.056Methyl-tert-Butyl Ether
BRL *SM6200 B P4I026911.0 9/17/14 19:08 VHLug/L 0.094Naphthalene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.059n-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.059n-Propylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.064o-Xylene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.054sec-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.034Styrene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.11tert-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.096Tetrachloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.057Toluene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.061trans-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.054trans-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.044Trichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.050Trichlorofluoromethane
BRL *SM6200 B P4I026915.0 9/17/14 19:08 VHLug/L 1.3Vinyl acetate
BRL *SM6200 B P4I026910.50 9/17/14 19:08 VHLug/L 0.068Vinyl chloride
BRL *SM6200 B P4I026911.5 9/17/14 19:08 VHLug/L 0.17Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-130101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-11
Prism Sample ID: 4090257-03
Prism Work Order: 4090257
Time Collected: 09/15/14 14:15
Time Submitted: 09/16/14 15:42
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0701,1,1,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0751,1,1-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0751,1,2,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0681,1,2-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0381,1-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0571,1-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0721,1-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.121,2,3-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0901,2,3-Trichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.151,2,4-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0381,2,4-Trimethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 19:34 VHLug/L 0.591,2-Dibromo-3-chloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0411,2-Dibromoethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0441,2-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0541,2-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0621,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0381,3,5-Trimethylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0701,3-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0541,3-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0591,4-Dichlorobenzene
BRL *SM6200 B P4I026912.0 9/17/14 19:34 VHLug/L 0.272,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0382-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0534-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.0594-Isopropyltoluene
BRL *SM6200 B P4I02691109/17/14 19:34 VHLug/L 1.5Acetone
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.054Benzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.088Bromobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.050Bromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.031Bromodichloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.10Bromoform
BRL *SM6200 B P4I026911.0 9/17/14 19:34 VHLug/L 0.24Bromomethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.065Carbon Tetrachloride
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.025Chlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.088Chloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.053Chloroform
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.032Chloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.061cis-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.065cis-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.062Dibromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.044Dibromomethane
BRL *SM6200 B P4I026911.0 9/17/14 19:34 VHLug/L 0.057Dichlorodifluoromethane
BRL *SM6200 B P4I026912009/17/14 19:34 VHLCCVug/L 42Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-11
Prism Sample ID: 4090257-03
Prism Work Order: 4090257
Time Collected: 09/15/14 14:15
Time Submitted: 09/16/14 15:42
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.054Ethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 19:34 VHLug/L 0.41Hexachlorobutadiene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.042Isopropyl Ether
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.034Isopropylbenzene (Cumene)
BRL *SM6200 B P4I026911.0 9/17/14 19:34 VHLug/L 0.11m,p-Xylenes
BRL *SM6200 B P4I026911.0 9/17/14 19:34 VHLug/L 0.11Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P4I026915.0 9/17/14 19:34 VHLug/L 0.83Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P4I026911.0 9/17/14 19:34 VHLug/L 0.048Methyl Isobutyl Ketone
BRL *SM6200 B P4I026912.0 9/17/14 19:34 VHLug/L 0.073Methylene Chloride
BRL *SM6200 B P4I026911.0 9/17/14 19:34 VHLug/L 0.056Methyl-tert-Butyl Ether
BRL *SM6200 B P4I026911.0 9/17/14 19:34 VHLug/L 0.094Naphthalene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.059n-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.059n-Propylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.064o-Xylene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.054sec-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.034Styrene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.11tert-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.096Tetrachloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.057Toluene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.061trans-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.054trans-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.044Trichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.050Trichlorofluoromethane
BRL *SM6200 B P4I026915.0 9/17/14 19:34 VHLug/L 1.3Vinyl acetate
BRL *SM6200 B P4I026910.50 9/17/14 19:34 VHLug/L 0.068Vinyl chloride
BRL *SM6200 B P4I026911.5 9/17/14 19:34 VHLug/L 0.17Xylenes, total
Surrogate Recovery Control Limits
70-130106 %4-Bromofluorobenzene
70-130105 %Dibromofluoromethane
70-130102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-12
Prism Sample ID: 4090257-04
Prism Work Order: 4090257
Time Collected: 09/15/14 13:50
Time Submitted: 09/16/14 15:42
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0701,1,1,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0751,1,1-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0751,1,2,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0681,1,2-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0381,1-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0571,1-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0721,1-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.121,2,3-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0901,2,3-Trichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.151,2,4-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0381,2,4-Trimethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 19:59 VHLug/L 0.591,2-Dibromo-3-chloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0411,2-Dibromoethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0441,2-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0541,2-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0621,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0381,3,5-Trimethylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0701,3-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0541,3-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0591,4-Dichlorobenzene
BRL *SM6200 B P4I026912.0 9/17/14 19:59 VHLug/L 0.272,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0382-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0534-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.0594-Isopropyltoluene
BRL *SM6200 B P4I02691109/17/14 19:59 VHLug/L 1.5Acetone
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.054Benzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.088Bromobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.050Bromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.031Bromodichloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.10Bromoform
BRL *SM6200 B P4I026911.0 9/17/14 19:59 VHLug/L 0.24Bromomethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.065Carbon Tetrachloride
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.025Chlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.088Chloroethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.053Chloroform
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.032Chloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.061cis-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.065cis-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.062Dibromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.044Dibromomethane
BRL *SM6200 B P4I026911.0 9/17/14 19:59 VHLug/L 0.057Dichlorodifluoromethane
BRL *SM6200 B P4I026912009/17/14 19:59 VHLCCVug/L 42Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-12
Prism Sample ID: 4090257-04
Prism Work Order: 4090257
Time Collected: 09/15/14 13:50
Time Submitted: 09/16/14 15:42
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.054Ethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 19:59 VHLug/L 0.41Hexachlorobutadiene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.042Isopropyl Ether
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.034Isopropylbenzene (Cumene)
BRL *SM6200 B P4I026911.0 9/17/14 19:59 VHLug/L 0.11m,p-Xylenes
BRL *SM6200 B P4I026911.0 9/17/14 19:59 VHLug/L 0.11Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P4I026915.0 9/17/14 19:59 VHLug/L 0.83Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P4I026911.0 9/17/14 19:59 VHLug/L 0.048Methyl Isobutyl Ketone
BRL *SM6200 B P4I026912.0 9/17/14 19:59 VHLug/L 0.073Methylene Chloride
BRL *SM6200 B P4I026911.0 9/17/14 19:59 VHLug/L 0.056Methyl-tert-Butyl Ether
BRL *SM6200 B P4I026911.0 9/17/14 19:59 VHLug/L 0.094Naphthalene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.059n-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.059n-Propylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.064o-Xylene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.054sec-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.034Styrene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.11tert-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.096Tetrachloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.057Toluene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.061trans-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.054trans-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.044Trichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.050Trichlorofluoromethane
BRL *SM6200 B P4I026915.0 9/17/14 19:59 VHLug/L 1.3Vinyl acetate
BRL *SM6200 B P4I026910.50 9/17/14 19:59 VHLug/L 0.068Vinyl chloride
BRL *SM6200 B P4I026911.5 9/17/14 19:59 VHLug/L 0.17Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-130103 %Dibromofluoromethane
70-130101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 4090257-05
Prism Work Order: 4090257
Time Collected: 09/15/14 13:20
Time Submitted: 09/16/14 15:42
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0701,1,1,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0751,1,1-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0751,1,2,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0681,1,2-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0381,1-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0571,1-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0721,1-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.121,2,3-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0901,2,3-Trichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.151,2,4-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0381,2,4-Trimethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 20:25 VHLug/L 0.591,2-Dibromo-3-chloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0411,2-Dibromoethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0441,2-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0541,2-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0621,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0381,3,5-Trimethylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0701,3-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0541,3-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0591,4-Dichlorobenzene
BRL *SM6200 B P4I026912.0 9/17/14 20:25 VHLug/L 0.272,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0382-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0534-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.0594-Isopropyltoluene
BRL *SM6200 B P4I02691109/17/14 20:25 VHLug/L 1.5Acetone
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.054Benzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.088Bromobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.050Bromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.031Bromodichloromethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.10Bromoform
BRL *SM6200 B P4I026911.0 9/17/14 20:25 VHLug/L 0.24Bromomethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.065Carbon Tetrachloride
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.025Chlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.088Chloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.053Chloroform
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.032Chloromethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.061cis-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.065cis-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.062Dibromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.044Dibromomethane
BRL *SM6200 B P4I026911.0 9/17/14 20:25 VHLug/L 0.057Dichlorodifluoromethane
BRL *SM6200 B P4I026912009/17/14 20:25 VHLCCVug/L 42Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-13
Prism Sample ID: 4090257-05
Prism Work Order: 4090257
Time Collected: 09/15/14 13:20
Time Submitted: 09/16/14 15:42
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.054Ethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 20:25 VHLug/L 0.41Hexachlorobutadiene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.042Isopropyl Ether
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.034Isopropylbenzene (Cumene)
BRL *SM6200 B P4I026911.0 9/17/14 20:25 VHLug/L 0.11m,p-Xylenes
BRL *SM6200 B P4I026911.0 9/17/14 20:25 VHLug/L 0.11Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P4I026915.0 9/17/14 20:25 VHLug/L 0.83Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P4I026911.0 9/17/14 20:25 VHLug/L 0.048Methyl Isobutyl Ketone
BRL *SM6200 B P4I026912.0 9/17/14 20:25 VHLug/L 0.073Methylene Chloride
BRL *SM6200 B P4I026911.0 9/17/14 20:25 VHLug/L 0.056Methyl-tert-Butyl Ether
BRL *SM6200 B P4I026911.0 9/17/14 20:25 VHLug/L 0.094Naphthalene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.059n-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.059n-Propylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.064o-Xylene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.054sec-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.034Styrene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.11tert-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.096Tetrachloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.057Toluene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.061trans-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.054trans-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.044Trichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.050Trichlorofluoromethane
BRL *SM6200 B P4I026915.0 9/17/14 20:25 VHLug/L 1.3Vinyl acetate
BRL *SM6200 B P4I026910.50 9/17/14 20:25 VHLug/L 0.068Vinyl chloride
BRL *SM6200 B P4I026911.5 9/17/14 20:25 VHLug/L 0.17Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-130101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-14
Prism Sample ID: 4090257-06
Prism Work Order: 4090257
Time Collected: 09/16/14 11:30
Time Submitted: 09/16/14 15:42
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0701,1,1,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0751,1,1-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0751,1,2,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0681,1,2-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0381,1-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0571,1-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0721,1-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.121,2,3-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0901,2,3-Trichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.151,2,4-Trichlorobenzene
770 *SM6200 B P4I026950259/17/14 23:24 VHLug/L 1.91,2,4-Trimethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 22:59 VHLug/L 0.591,2-Dibromo-3-chloropropane
3.9 *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0411,2-Dibromoethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0441,2-Dichlorobenzene
7.1 *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0541,2-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0621,2-Dichloropropane
230 *SM6200 B P4I026950259/17/14 23:24 VHLug/L 1.91,3,5-Trimethylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0701,3-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0541,3-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0591,4-Dichlorobenzene
BRL *SM6200 B P4I026912.0 9/17/14 22:59 VHLug/L 0.272,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0382-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0534-Chlorotoluene
6.9 *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.0594-Isopropyltoluene
61 *SM6200 B P4I02691109/17/14 22:59 VHLug/L 1.5Acetone
1800 *SM6200 B P4I026950259/17/14 23:24 VHLug/L 2.7Benzene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.088Bromobenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.050Bromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.031Bromodichloromethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.10Bromoform
BRL *SM6200 B P4I026911.0 9/17/14 22:59 VHLug/L 0.24Bromomethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.065Carbon Tetrachloride
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.025Chlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.088Chloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.053Chloroform
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.032Chloromethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.061cis-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.065cis-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.062Dibromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.044Dibromomethane
BRL *SM6200 B P4I026911.0 9/17/14 22:59 VHLug/L 0.057Dichlorodifluoromethane
BRL *SM6200 B P4I026912009/17/14 22:59 VHLCCVug/L 42Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-14
Prism Sample ID: 4090257-06
Prism Work Order: 4090257
Time Collected: 09/16/14 11:30
Time Submitted: 09/16/14 15:42
930 *SM6200 B P4I026950259/17/14 23:24 VHLug/L 2.7Ethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 22:59 VHLug/L 0.41Hexachlorobutadiene
60 *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.042Isopropyl Ether
79 *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.034Isopropylbenzene (Cumene)
2000 *SM6200 B P4I026950509/17/14 23:24 VHLug/L 5.4m,p-Xylenes
6.0 *SM6200 B P4I026911.0 9/17/14 22:59 VHLug/L 0.11Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P4I026915.0 9/17/14 22:59 VHLug/L 0.83Methyl Ethyl Ketone (2-Butanone)
6.3 *SM6200 B P4I026911.0 9/17/14 22:59 VHLug/L 0.048Methyl Isobutyl Ketone
BRL *SM6200 B P4I026912.0 9/17/14 22:59 VHLug/L 0.073Methylene Chloride
910 *SM6200 B P4I026950509/17/14 23:24 VHLug/L 2.8Methyl-tert-Butyl Ether
240 *SM6200 B P4I026950509/17/14 22:59 VHLug/L 4.7Naphthalene
23 *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.059n-Butylbenzene
230 *SM6200 B P4I026950259/17/14 23:24 VHLug/L 3.0n-Propylbenzene
910 *SM6200 B P4I026950259/17/14 23:24 VHLug/L 3.2o-Xylene
15 *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.054sec-Butylbenzene
20 *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.034Styrene
0.88 *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.11tert-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.096Tetrachloroethylene
5100 *SM6200 B P4I026950259/17/14 22:59 VHLug/L 2.8Toluene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.061trans-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.054trans-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.044Trichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.050Trichlorofluoromethane
BRL *SM6200 B P4I026915.0 9/17/14 22:59 VHLug/L 1.3Vinyl acetate
BRL *SM6200 B P4I026910.50 9/17/14 22:59 VHLug/L 0.068Vinyl chloride
2900 *SM6200 B P4I026950759/17/14 23:24 VHLug/L 8.6Xylenes, total
Surrogate Recovery Control Limits
70-130105 %4-Bromofluorobenzene
70-130105 %Dibromofluoromethane
70-13088 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-15
Prism Sample ID: 4090257-07
Prism Work Order: 4090257
Time Collected: 09/16/14 10:50
Time Submitted: 09/16/14 15:42
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0701,1,1,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0751,1,1-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0751,1,2,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0681,1,2-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0381,1-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0571,1-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0721,1-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.121,2,3-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0901,2,3-Trichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.151,2,4-Trichlorobenzene
2500 *SM6200 B P4I0269100509/18/14 17:14 VHLug/L 3.81,2,4-Trimethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 22:07 VHLug/L 0.591,2-Dibromo-3-chloropropane
2.0 *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0411,2-Dibromoethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0441,2-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0541,2-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0621,2-Dichloropropane
710 *SM6200 B P4I0269100509/18/14 17:14 VHLug/L 3.81,3,5-Trimethylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0701,3-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0541,3-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0591,4-Dichlorobenzene
BRL *SM6200 B P4I026912.0 9/17/14 22:07 VHLug/L 0.272,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0382-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0534-Chlorotoluene
9.7 *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.0594-Isopropyltoluene
BRL *SM6200 B P4I02691109/17/14 22:07 VHLug/L 1.5Acetone
680 *SM6200 B P4I0269100509/18/14 17:14 VHLug/L 5.4Benzene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.088Bromobenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.050Bromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.031Bromodichloromethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.10Bromoform
BRL *SM6200 B P4I026911.0 9/17/14 22:07 VHLug/L 0.24Bromomethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.065Carbon Tetrachloride
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.025Chlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.088Chloroethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.053Chloroform
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.032Chloromethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.061cis-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.065cis-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.062Dibromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.044Dibromomethane
BRL *SM6200 B P4I026911.0 9/17/14 22:07 VHLug/L 0.057Dichlorodifluoromethane
BRL *SM6200 B P4I026912009/17/14 22:07 VHLCCVug/L 42Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: MW-15
Prism Sample ID: 4090257-07
Prism Work Order: 4090257
Time Collected: 09/16/14 10:50
Time Submitted: 09/16/14 15:42
2000 *SM6200 B P4I0269100509/18/14 17:14 VHLug/L 5.4Ethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 22:07 VHLug/L 0.41Hexachlorobutadiene
5.9 *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.042Isopropyl Ether
160 *SM6200 B P4I0269100509/18/14 17:14 VHLug/L 3.4Isopropylbenzene (Cumene)
5900 *SM6200 B P4I02691001009/18/14 17:14 VHLug/L 11m,p-Xylenes
11 *SM6200 B P4I026911.0 9/17/14 22:07 VHLug/L 0.11Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P4I026915.0 9/17/14 22:07 VHLug/L 0.83Methyl Ethyl Ketone (2-Butanone)
11 *SM6200 B P4I026911.0 9/17/14 22:07 VHLug/L 0.048Methyl Isobutyl Ketone
BRL *SM6200 B P4I026912.0 9/17/14 22:07 VHLug/L 0.073Methylene Chloride
27 *SM6200 B P4I026911.0 9/17/14 22:07 VHLug/L 0.056Methyl-tert-Butyl Ether
490 *SM6200 B P4I02691001009/17/14 22:07 VHLug/L 9.4Naphthalene
37 *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.059n-Butylbenzene
450 *SM6200 B P4I0269100509/18/14 17:14 VHLug/L 5.9n-Propylbenzene
2300 *SM6200 B P4I0269100509/18/14 17:14 VHLug/L 6.4o-Xylene
25 *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.054sec-Butylbenzene
51 *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.034Styrene
1.5 *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.11tert-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.096Tetrachloroethylene
5900 *SM6200 B P4I0269100509/18/14 17:14 VHLug/L 5.7Toluene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.061trans-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.054trans-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.044Trichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.050Trichlorofluoromethane
BRL *SM6200 B P4I026915.0 9/17/14 22:07 VHLug/L 1.3Vinyl acetate
BRL *SM6200 B P4I026910.50 9/17/14 22:07 VHLug/L 0.068Vinyl chloride
8200 *SM6200 B P4I02691001509/18/14 17:14 VHLug/L 17Xylenes, total
Surrogate Recovery Control Limits
70-130118 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-13089 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: WSW-15
Prism Sample ID: 4090257-08
Prism Work Order: 4090257
Time Collected: 09/15/14 12:15
Time Submitted: 09/16/14 15:42
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0701,1,1,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0751,1,1-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0751,1,2,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0681,1,2-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0381,1-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0571,1-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0721,1-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.121,2,3-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0901,2,3-Trichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.151,2,4-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0381,2,4-Trimethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 20:50 VHLug/L 0.591,2-Dibromo-3-chloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0411,2-Dibromoethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0441,2-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0541,2-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0621,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0381,3,5-Trimethylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0701,3-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0541,3-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0591,4-Dichlorobenzene
BRL *SM6200 B P4I026912.0 9/17/14 20:50 VHLug/L 0.272,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0382-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0534-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.0594-Isopropyltoluene
BRL *SM6200 B P4I02691109/17/14 20:50 VHLug/L 1.5Acetone
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.054Benzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.088Bromobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.050Bromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.031Bromodichloromethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.10Bromoform
BRL *SM6200 B P4I026911.0 9/17/14 20:50 VHLug/L 0.24Bromomethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.065Carbon Tetrachloride
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.025Chlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.088Chloroethane
3.4 *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.053Chloroform
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.032Chloromethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.061cis-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.065cis-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.062Dibromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.044Dibromomethane
BRL *SM6200 B P4I026911.0 9/17/14 20:50 VHLug/L 0.057Dichlorodifluoromethane
BRL *SM6200 B P4I026912009/17/14 20:50 VHLug/L 42Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: WSW-15
Prism Sample ID: 4090257-08
Prism Work Order: 4090257
Time Collected: 09/15/14 12:15
Time Submitted: 09/16/14 15:42
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.054Ethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 20:50 VHLug/L 0.41Hexachlorobutadiene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.042Isopropyl Ether
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.034Isopropylbenzene (Cumene)
BRL *SM6200 B P4I026911.0 9/17/14 20:50 VHLug/L 0.11m,p-Xylenes
BRL *SM6200 B P4I026911.0 9/17/14 20:50 VHLug/L 0.11Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P4I026915.0 9/17/14 20:50 VHLug/L 0.83Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P4I026911.0 9/17/14 20:50 VHLug/L 0.048Methyl Isobutyl Ketone
BRL *SM6200 B P4I026912.0 9/17/14 20:50 VHLug/L 0.073Methylene Chloride
BRL *SM6200 B P4I026911.0 9/17/14 20:50 VHLug/L 0.056Methyl-tert-Butyl Ether
BRL *SM6200 B P4I026911.0 9/17/14 20:50 VHLug/L 0.094Naphthalene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.059n-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.059n-Propylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.064o-Xylene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.054sec-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.034Styrene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.11tert-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.096Tetrachloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.057Toluene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.061trans-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.054trans-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.044Trichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.050Trichlorofluoromethane
BRL *SM6200 B P4I026915.0 9/17/14 20:50 VHLug/L 1.3Vinyl acetate
BRL *SM6200 B P4I026910.50 9/17/14 20:50 VHLug/L 0.068Vinyl chloride
BRL *SM6200 B P4I026911.5 9/17/14 20:50 VHLug/L 0.17Xylenes, total
Surrogate Recovery Control Limits
70-130106 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-130104 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: WSW-18
Prism Sample ID: 4090257-09
Prism Work Order: 4090257
Time Collected: 09/15/14 12:00
Time Submitted: 09/16/14 15:42
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0701,1,1,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0751,1,1-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0751,1,2,2-Tetrachloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0681,1,2-Trichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0381,1-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0571,1-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0721,1-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.121,2,3-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0901,2,3-Trichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.151,2,4-Trichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0381,2,4-Trimethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 21:16 VHLug/L 0.591,2-Dibromo-3-chloropropane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0411,2-Dibromoethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0441,2-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0541,2-Dichloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0621,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0381,3,5-Trimethylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0701,3-Dichlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0541,3-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0591,4-Dichlorobenzene
BRL *SM6200 B P4I026912.0 9/17/14 21:16 VHLug/L 0.272,2-Dichloropropane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0382-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0534-Chlorotoluene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.0594-Isopropyltoluene
BRL *SM6200 B P4I02691109/17/14 21:16 VHLug/L 1.5Acetone
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.054Benzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.088Bromobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.050Bromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.031Bromodichloromethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.10Bromoform
BRL *SM6200 B P4I026911.0 9/17/14 21:16 VHLug/L 0.24Bromomethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.065Carbon Tetrachloride
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.025Chlorobenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.088Chloroethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.053Chloroform
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.032Chloromethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.061cis-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.065cis-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.062Dibromochloromethane
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.044Dibromomethane
BRL *SM6200 B P4I026911.0 9/17/14 21:16 VHLug/L 0.057Dichlorodifluoromethane
BRL *SM6200 B P4I026912009/17/14 21:16 VHLug/L 42Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 29
Laboratory Report
09/22/2014
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Sample Matrix: Water
Client Sample ID: WSW-18
Prism Sample ID: 4090257-09
Prism Work Order: 4090257
Time Collected: 09/15/14 12:00
Time Submitted: 09/16/14 15:42
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.054Ethylbenzene
BRL *SM6200 B P4I026912.0 9/17/14 21:16 VHLug/L 0.41Hexachlorobutadiene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.042Isopropyl Ether
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.034Isopropylbenzene (Cumene)
BRL *SM6200 B P4I026911.0 9/17/14 21:16 VHLug/L 0.11m,p-Xylenes
BRL *SM6200 B P4I026911.0 9/17/14 21:16 VHLug/L 0.11Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P4I026915.0 9/17/14 21:16 VHLug/L 0.83Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P4I026911.0 9/17/14 21:16 VHLug/L 0.048Methyl Isobutyl Ketone
BRL *SM6200 B P4I026912.0 9/17/14 21:16 VHLug/L 0.073Methylene Chloride
BRL *SM6200 B P4I026911.0 9/17/14 21:16 VHLug/L 0.056Methyl-tert-Butyl Ether
BRL *SM6200 B P4I026911.0 9/17/14 21:16 VHLug/L 0.094Naphthalene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.059n-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.059n-Propylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.064o-Xylene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.054sec-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.034Styrene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.11tert-Butylbenzene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.096Tetrachloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.057Toluene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.061trans-1,2-Dichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.054trans-1,3-Dichloropropylene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.044Trichloroethylene
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.050Trichlorofluoromethane
BRL *SM6200 B P4I026915.0 9/17/14 21:16 VHLug/L 1.3Vinyl acetate
BRL *SM6200 B P4I026910.50 9/17/14 21:16 VHLug/L 0.068Vinyl chloride
BRL *SM6200 B P4I026911.5 9/17/14 21:16 VHLug/L 0.17Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-130102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 29
9/22/14
Level II QC Report
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 4090257
Time Submitted: 9/16/2014 3:42:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P4I0269 - SM6200 B
Blank (P4I0269-BLK1)Prepared & Analyzed: 09/17/14
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 29
9/22/14
Level II QC Report
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 4090257
Time Submitted: 9/16/2014 3:42:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P4I0269 - SM6200 B
Blank (P4I0269-BLK1)Prepared & Analyzed: 09/17/14
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10552.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10753.6
ug/L 50.00 70-130Surrogate: Toluene-d8 10351.4
LCS (P4I0269-BS1)Prepared & Analyzed: 09/17/14
1,1,1,2-Tetrachloroethane ug/L21.3 0.50 20.00 70-130107
1,1,1-Trichloroethane ug/L21.5 0.50 20.00 70-130108
1,1,2,2-Tetrachloroethane ug/L21.9 0.50 20.00 70-130110
1,1,2-Trichloroethane ug/L20.7 0.50 20.00 70-130104
1,1-Dichloroethane ug/L20.9 0.50 20.00 70-130104
1,1-Dichloroethylene ug/L24.1 0.50 20.00 70-130120
1,1-Dichloropropylene ug/L21.8 0.50 20.00 70-130109
1,2,3-Trichlorobenzene ug/L23.4 0.50 20.00 70-130117
1,2,3-Trichloropropane ug/L21.3 0.50 20.00 70-130107
1,2,4-Trichlorobenzene ug/L20.6 0.50 20.00 70-130103
1,2,4-Trimethylbenzene ug/L21.0 0.50 20.00 70-130105
1,2-Dibromo-3-chloropropane ug/L21.1 2.0 20.00 70-130106
1,2-Dibromoethane ug/L20.8 0.50 20.00 70-130104
1,2-Dichlorobenzene ug/L20.7 0.50 20.00 70-130104
1,2-Dichloroethane ug/L19.9 0.50 20.00 70-13099
1,2-Dichloropropane ug/L20.6 0.50 20.00 70-130103
1,3,5-Trimethylbenzene ug/L21.0 0.50 20.00 70-130105
1,3-Dichlorobenzene ug/L21.3 0.50 20.00 70-130107
1,3-Dichloropropane ug/L21.3 0.50 20.00 70-130107
1,4-Dichlorobenzene ug/L21.5 0.50 20.00 70-130107
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 29
9/22/14
Level II QC Report
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 4090257
Time Submitted: 9/16/2014 3:42:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P4I0269 - SM6200 B
LCS (P4I0269-BS1)Prepared & Analyzed: 09/17/14
2,2-Dichloropropane ug/L23.6 2.0 20.00 70-130118
2-Chlorotoluene ug/L22.0 0.50 20.00 70-130110
4-Chlorotoluene ug/L21.6 0.50 20.00 70-130108
4-Isopropyltoluene ug/L21.5 0.50 20.00 70-130108
Acetone ug/L43.7 10 40.00 40-160109
Benzene ug/L21.7 0.50 20.00 70-130109
Bromobenzene ug/L21.5 0.50 20.00 70-130108
Bromochloromethane ug/L19.9 0.50 20.00 70-13099
Bromodichloromethane ug/L21.4 0.50 20.00 70-130107
Bromoform ug/L21.5 0.50 20.00 70-130108
Bromomethane ug/L21.4 1.0 20.00 60-140107
Carbon Tetrachloride ug/L22.7 0.50 20.00 70-130113
Chlorobenzene ug/L21.0 0.50 20.00 70-130105
Chloroethane ug/L21.7 0.50 20.00 60-140108
Chloroform ug/L21.4 0.50 20.00 70-130107
Chloromethane ug/L16.3 0.50 20.00 60-14082
cis-1,2-Dichloroethylene ug/L20.8 0.50 20.00 70-130104
cis-1,3-Dichloropropylene ug/L20.5 0.50 20.00 70-130103
Dibromochloromethane ug/L20.4 0.50 20.00 70-130102
Dibromomethane ug/L21.0 0.50 20.00 70-130105
Dichlorodifluoromethane ug/L19.0 1.0 20.00 60-14095
Ethanol ug/L646 200 500.0 60-140129
Ethylbenzene ug/L21.2 0.50 20.00 70-130106
Hexachlorobutadiene ug/L23.2 2.0 20.00 70-130116
Isopropyl Ether ug/L19.3 0.50 20.00 70-13096
Isopropylbenzene (Cumene)ug/L22.5 0.50 20.00 70-130113
m,p-Xylenes ug/L43.5 1.0 40.00 70-130109
Methyl Butyl Ketone (2-Hexanone)ug/L18.8 1.0 20.00 60-14094
Methyl Ethyl Ketone (2-Butanone)ug/L21.2 5.0 20.00 60-140106
Methyl Isobutyl Ketone ug/L18.5 1.0 20.00 60-14093
Methylene Chloride ug/L21.9 2.0 20.00 70-130109
Methyl-tert-Butyl Ether ug/L19.4 1.0 20.00 70-13097
Naphthalene ug/L19.2 1.0 20.00 70-13096
n-Butylbenzene ug/L22.2 0.50 20.00 70-130111
n-Propylbenzene ug/L22.9 0.50 20.00 70-130115
o-Xylene ug/L21.0 0.50 20.00 70-130105
sec-Butylbenzene ug/L22.0 0.50 20.00 70-130110
Styrene ug/L21.2 0.50 20.00 70-130106
tert-Butylbenzene ug/L22.0 0.50 20.00 70-130110
Tetrachloroethylene ug/L22.8 0.50 20.00 70-130114
Toluene ug/L21.1 0.50 20.00 70-130106
trans-1,2-Dichloroethylene ug/L21.6 0.50 20.00 70-130108
trans-1,3-Dichloropropylene ug/L21.5 0.50 20.00 70-130107
Trichloroethylene ug/L21.6 0.50 20.00 70-130108
Trichlorofluoromethane ug/L22.9 0.50 20.00 60-140115
Vinyl acetate ug/L22.9 5.0 20.00 60-140115
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 29
9/22/14
Level II QC Report
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 4090257
Time Submitted: 9/16/2014 3:42:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P4I0269 - SM6200 B
LCS (P4I0269-BS1)Prepared & Analyzed: 09/17/14
Vinyl chloride ug/L19.8 0.50 20.00 60-14099
Xylenes, total ug/L64.5 1.5 60.00 70-130107
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10451.8
ug/L 50.00 70-130Surrogate: Toluene-d8 10351.3
LCS Dup (P4I0269-BSD1)Prepared & Analyzed: 09/17/14
1,1,1,2-Tetrachloroethane ug/L20.5 0.50 20.00 2070-130102 4
1,1,1-Trichloroethane ug/L20.5 0.50 20.00 2070-130103 5
1,1,2,2-Tetrachloroethane ug/L21.3 0.50 20.00 2070-130106 3
1,1,2-Trichloroethane ug/L20.1 0.50 20.00 2070-130100 3
1,1-Dichloroethane ug/L20.1 0.50 20.00 2070-130101 4
1,1-Dichloroethylene ug/L21.7 0.50 20.00 2070-130108 10
1,1-Dichloropropylene ug/L20.1 0.50 20.00 2070-130100 8
1,2,3-Trichlorobenzene ug/L23.4 0.50 20.00 2070-130117 0.3
1,2,3-Trichloropropane ug/L20.4 0.50 20.00 2070-130102 4
1,2,4-Trichlorobenzene ug/L20.5 0.50 20.00 2070-130102 0.7
1,2,4-Trimethylbenzene ug/L20.5 0.50 20.00 2070-130102 2
1,2-Dibromo-3-chloropropane ug/L20.2 2.0 20.00 2070-130101 4
1,2-Dibromoethane ug/L20.1 0.50 20.00 2070-130101 3
1,2-Dichlorobenzene ug/L20.4 0.50 20.00 2070-130102 1
1,2-Dichloroethane ug/L19.1 0.50 20.00 2070-13095 4
1,2-Dichloropropane ug/L19.7 0.50 20.00 2070-13099 4
1,3,5-Trimethylbenzene ug/L20.6 0.50 20.00 2070-130103 2
1,3-Dichlorobenzene ug/L21.0 0.50 20.00 2070-130105 1
1,3-Dichloropropane ug/L20.5 0.50 20.00 2070-130102 4
1,4-Dichlorobenzene ug/L20.8 0.50 20.00 2070-130104 3
2,2-Dichloropropane ug/L21.8 2.0 20.00 2070-130109 8
2-Chlorotoluene ug/L21.3 0.50 20.00 2070-130106 3
4-Chlorotoluene ug/L21.2 0.50 20.00 2070-130106 2
4-Isopropyltoluene ug/L20.4 0.50 20.00 2070-130102 5
Acetone ug/L41.4 10 40.00 2040-160103 6
Benzene ug/L21.0 0.50 20.00 2070-130105 3
Bromobenzene ug/L20.9 0.50 20.00 2070-130104 3
Bromochloromethane ug/L19.6 0.50 20.00 2070-13098 2
Bromodichloromethane ug/L20.2 0.50 20.00 2070-130101 5
Bromoform ug/L20.7 0.50 20.00 2070-130103 4
Bromomethane ug/L21.4 1.0 20.00 2060-140107 0.09
Carbon Tetrachloride ug/L20.5 0.50 20.00 2070-130102 10
Chlorobenzene ug/L20.4 0.50 20.00 2070-130102 3
Chloroethane ug/L20.4 0.50 20.00 2060-140102 6
Chloroform ug/L21.7 0.50 20.00 2070-130109 2
Chloromethane ug/L15.6 0.50 20.00 2060-14078 4
cis-1,2-Dichloroethylene ug/L20.2 0.50 20.00 2070-130101 3
cis-1,3-Dichloropropylene ug/L20.1 0.50 20.00 2070-130100 2
Dibromochloromethane ug/L19.7 0.50 20.00 2070-13098 4
Dibromomethane ug/L20.0 0.50 20.00 2070-130100 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 29
9/22/14
Level II QC Report
2923 South Tryon St. Ste 100
Project: YOC-122 One Stop Store #2Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Steve Libbey
Prism Work Order: 4090257
Time Submitted: 9/16/2014 3:42:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P4I0269 - SM6200 B
LCS Dup (P4I0269-BSD1)Prepared & Analyzed: 09/17/14
Dichlorodifluoromethane ug/L16.0 1.0 20.00 2060-14080 17
Ethanol ug/L542 200 500.0 2060-140108 18
Ethylbenzene ug/L20.4 0.50 20.00 2070-130102 4
Hexachlorobutadiene ug/L21.4 2.0 20.00 2070-130107 8
Isopropyl Ether ug/L18.8 0.50 20.00 2070-13094 3
Isopropylbenzene (Cumene)ug/L21.4 0.50 20.00 2070-130107 5
m,p-Xylenes ug/L41.7 1.0 40.00 2070-130104 4
Methyl Butyl Ketone (2-Hexanone)ug/L18.4 1.0 20.00 2060-14092 2
Methyl Ethyl Ketone (2-Butanone)ug/L19.5 5.0 20.00 2060-14098 8
Methyl Isobutyl Ketone ug/L18.0 1.0 20.00 2060-14090 3
Methylene Chloride ug/L20.9 2.0 20.00 2070-130104 5
Methyl-tert-Butyl Ether ug/L18.8 1.0 20.00 2070-13094 3
Naphthalene ug/L18.9 1.0 20.00 2070-13094 2
n-Butylbenzene ug/L21.1 0.50 20.00 2070-130106 5
n-Propylbenzene ug/L21.8 0.50 20.00 2070-130109 5
o-Xylene ug/L20.1 0.50 20.00 2070-130101 4
sec-Butylbenzene ug/L20.7 0.50 20.00 2070-130103 6
Styrene ug/L20.5 0.50 20.00 2070-130102 3
tert-Butylbenzene ug/L20.8 0.50 20.00 2070-130104 5
Tetrachloroethylene ug/L21.2 0.50 20.00 2070-130106 8
Toluene ug/L20.3 0.50 20.00 2070-130102 4
trans-1,2-Dichloroethylene ug/L20.8 0.50 20.00 2070-130104 4
trans-1,3-Dichloropropylene ug/L20.5 0.50 20.00 2070-130103 5
Trichloroethylene ug/L20.0 0.50 20.00 2070-130100 8
Trichlorofluoromethane ug/L20.0 0.50 20.00 2060-140100 14
Vinyl acetate ug/L23.6 5.0 20.00 2060-140118 3
Vinyl chloride ug/L17.9 0.50 20.00 2060-14089 10
Xylenes, total ug/L61.8 1.5 60.00 2070-130103 4
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10250.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10251.0
ug/L 50.00 70-130Surrogate: Toluene-d8 10351.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 29
Sample Extraction Data
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P4I02694090257-01 09/17/14 8:4610 10mL mL
P4I02694090257-01 09/17/14 8:4610 10mL mL
P4I02694090257-02 09/17/14 8:4610 10mL mL
P4I02694090257-03 09/17/14 8:4610 10mL mL
P4I02694090257-04 09/17/14 8:4610 10mL mL
P4I02694090257-05 09/17/14 8:4610 10mL mL
P4I02694090257-06 09/17/14 8:4610 10mL mL
P4I02694090257-06 09/17/14 8:4610 10mL mL
P4I02694090257-07 09/17/14 8:4610 10mL mL
P4I02694090257-07 09/17/14 8:4610 10mL mL
P4I02694090257-08 09/17/14 8:4610 10mL mL
P4I02694090257-09 09/17/14 8:4610 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 29
Page 29 of 29
#=CL#
July 27, 2015
LIMS USE: FR - STEVE LIBBEY
LIMS OBJECT ID: 92259124
92259124
Project:
Pace Project No.:
RE:
Mr. Steve Libbey
Hart & Hickman
2923 South Tryon Street
Charlotte, NC 28203
ONE STOP STORE #2
Dear Mr. Libbey:
Enclosed are the analytical results for sample(s) received by the laboratory on July 16, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 2 of 32
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Lab ID Sample ID Matrix Date Collected Date Received
92259124001 GMW-2 Water 07/16/15 11:30 07/16/15 16:00
92259124002 GMW-7 Water 07/16/15 13:40 07/16/15 16:00
92259124003 MW-10 Water 07/16/15 12:30 07/16/15 16:00
92259124004 MW-11 Water 07/16/15 13:10 07/16/15 16:00
92259124005 MW-12 Water 07/16/15 11:55 07/16/15 16:00
92259124006 MW-13 Water 07/16/15 11:10 07/16/15 16:00
92259124007 MW-14 Water 07/16/15 14:45 07/16/15 16:00
92259124008 MW-15 Water 07/16/15 14:10 07/16/15 16:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Page 3 of 32
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92259124001 GMW-2 SM 6200B 63 PASI-CCAH
92259124002 GMW-7 SM 6200B 63 PASI-CCAH
92259124003 MW-10 SM 6200B 63 PASI-CCAH
92259124004 MW-11 SM 6200B 63 PASI-CCAH
92259124005 MW-12 SM 6200B 63 PASI-CCAH
92259124006 MW-13 SM 6200B 63 PASI-CCAH
92259124007 MW-14 SM 6200B 63 PASI-CCAH
92259124008 MW-15 SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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[phone]
Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:GMW-2 Lab ID:92259124001 Collected:07/16/15 11:30 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 07/20/15 18:17 71-43-20.50 1
Bromobenzene ND ug/L 07/20/15 18:17 108-86-10.50 1
Bromochloromethane ND ug/L 07/20/15 18:17 74-97-50.50 1
Bromodichloromethane ND ug/L 07/20/15 18:17 75-27-40.50 1
Bromoform ND ug/L 07/20/15 18:17 75-25-20.50 1
Bromomethane ND ug/L 07/20/15 18:17 74-83-95.0 1
n-Butylbenzene ND ug/L 07/20/15 18:17 104-51-80.50 1
sec-Butylbenzene ND ug/L 07/20/15 18:17 135-98-80.50 1
tert-Butylbenzene ND ug/L 07/20/15 18:17 98-06-60.50 1
Carbon tetrachloride ND ug/L 07/20/15 18:17 56-23-50.50 1
Chlorobenzene ND ug/L 07/20/15 18:17 108-90-70.50 1
Chloroethane ND ug/L 07/20/15 18:17 75-00-31.0 1
Chloroform ND ug/L 07/20/15 18:17 67-66-30.50 1
Chloromethane ND ug/L 07/20/15 18:17 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/20/15 18:17 95-49-80.50 1
4-Chlorotoluene ND ug/L 07/20/15 18:17 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 07/20/15 18:17 96-12-81.0 1
Dibromochloromethane ND ug/L 07/20/15 18:17 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 07/20/15 18:17 106-93-40.50 1
Dibromomethane ND ug/L 07/20/15 18:17 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 07/20/15 18:17 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 07/20/15 18:17 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 07/20/15 18:17 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 07/20/15 18:17 75-71-80.50 1
1,1-Dichloroethane ND ug/L 07/20/15 18:17 75-34-30.50 1
1,2-Dichloroethane ND ug/L 07/20/15 18:17 107-06-20.50 1
1,1-Dichloroethene ND ug/L 07/20/15 18:17 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 07/20/15 18:17 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 07/20/15 18:17 156-60-50.50 1
1,2-Dichloropropane ND ug/L 07/20/15 18:17 78-87-50.50 1
1,3-Dichloropropane ND ug/L 07/20/15 18:17 142-28-90.50 1
2,2-Dichloropropane ND ug/L 07/20/15 18:17 594-20-70.50 1
1,1-Dichloropropene ND ug/L 07/20/15 18:17 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 07/20/15 18:17 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 07/20/15 18:17 10061-02-60.50 1
Diisopropyl ether ND ug/L 07/20/15 18:17 108-20-30.50 1
Ethylbenzene ND ug/L 07/20/15 18:17 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 07/20/15 18:17 87-68-3 L32.0 1
Isopropylbenzene (Cumene)ND ug/L 07/20/15 18:17 98-82-80.50 1
Methylene Chloride ND ug/L 07/20/15 18:17 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 07/20/15 18:17 1634-04-40.50 1
Naphthalene ND ug/L 07/20/15 18:17 91-20-32.0 1
n-Propylbenzene ND ug/L 07/20/15 18:17 103-65-10.50 1
Styrene ND ug/L 07/20/15 18:17 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 07/20/15 18:17 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 07/20/15 18:17 79-34-50.50 1
Tetrachloroethene ND ug/L 07/20/15 18:17 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:GMW-2 Lab ID:92259124001 Collected:07/16/15 11:30 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 07/20/15 18:17 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 07/20/15 18:17 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 07/20/15 18:17 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 07/20/15 18:17 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 07/20/15 18:17 79-00-50.50 1
Trichloroethene ND ug/L 07/20/15 18:17 79-01-60.50 1
Trichlorofluoromethane ND ug/L 07/20/15 18:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/20/15 18:17 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 07/20/15 18:17 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 07/20/15 18:17 108-67-80.50 1
Vinyl chloride ND ug/L 07/20/15 18:17 75-01-41.0 1
m&p-Xylene ND ug/L 07/20/15 18:17 179601-23-11.0 1
o-Xylene ND ug/L 07/20/15 18:17 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)122 %07/20/15 18:17 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %07/20/15 18:17 460-00-470-130 1
Toluene-d8 (S)103 %07/20/15 18:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:GMW-7 Lab ID:92259124002 Collected:07/16/15 13:40 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 665 ug/L 07/20/15 19:56 71-43-25.0 10
Bromobenzene ND ug/L 07/20/15 19:56 108-86-15.0 10
Bromochloromethane ND ug/L 07/20/15 19:56 74-97-55.0 10
Bromodichloromethane ND ug/L 07/20/15 19:56 75-27-45.0 10
Bromoform ND ug/L 07/20/15 19:56 75-25-25.0 10
Bromomethane ND ug/L 07/20/15 19:56 74-83-950.0 10
n-Butylbenzene ND ug/L 07/20/15 19:56 104-51-85.0 10
sec-Butylbenzene ND ug/L 07/20/15 19:56 135-98-85.0 10
tert-Butylbenzene ND ug/L 07/20/15 19:56 98-06-65.0 10
Carbon tetrachloride ND ug/L 07/20/15 19:56 56-23-55.0 10
Chlorobenzene ND ug/L 07/20/15 19:56 108-90-75.0 10
Chloroethane ND ug/L 07/20/15 19:56 75-00-310.0 10
Chloroform ND ug/L 07/20/15 19:56 67-66-35.0 10
Chloromethane ND ug/L 07/20/15 19:56 74-87-310.0 10
2-Chlorotoluene ND ug/L 07/20/15 19:56 95-49-85.0 10
4-Chlorotoluene ND ug/L 07/20/15 19:56 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 07/20/15 19:56 96-12-810.0 10
Dibromochloromethane ND ug/L 07/20/15 19:56 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 07/20/15 19:56 106-93-45.0 10
Dibromomethane ND ug/L 07/20/15 19:56 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 07/20/15 19:56 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 07/20/15 19:56 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 07/20/15 19:56 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 07/20/15 19:56 75-71-85.0 10
1,1-Dichloroethane ND ug/L 07/20/15 19:56 75-34-35.0 10
1,2-Dichloroethane ND ug/L 07/20/15 19:56 107-06-25.0 10
1,1-Dichloroethene ND ug/L 07/20/15 19:56 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 07/20/15 19:56 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 07/20/15 19:56 156-60-55.0 10
1,2-Dichloropropane ND ug/L 07/20/15 19:56 78-87-55.0 10
1,3-Dichloropropane ND ug/L 07/20/15 19:56 142-28-95.0 10
2,2-Dichloropropane ND ug/L 07/20/15 19:56 594-20-75.0 10
1,1-Dichloropropene ND ug/L 07/20/15 19:56 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 07/20/15 19:56 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 07/20/15 19:56 10061-02-65.0 10
Diisopropyl ether 57.6 ug/L 07/20/15 19:56 108-20-35.0 10
Ethylbenzene 557 ug/L 07/20/15 19:56 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 07/20/15 19:56 87-68-3 L320.0 10
Isopropylbenzene (Cumene)26.6 ug/L 07/20/15 19:56 98-82-85.0 10
Methylene Chloride 29.6 ug/L 07/20/15 19:56 75-09-2 C920.0 10
Methyl-tert-butyl ether 74.6 ug/L 07/20/15 19:56 1634-04-45.0 10
Naphthalene 125 ug/L 07/20/15 19:56 91-20-320.0 10
n-Propylbenzene 69.6 ug/L 07/20/15 19:56 103-65-15.0 10
Styrene ND ug/L 07/20/15 19:56 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 07/20/15 19:56 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 07/20/15 19:56 79-34-55.0 10
Tetrachloroethene ND ug/L 07/20/15 19:56 127-18-45.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 7 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:GMW-7 Lab ID:92259124002 Collected:07/16/15 13:40 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 823 ug/L 07/20/15 19:56 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 07/20/15 19:56 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 07/20/15 19:56 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 07/20/15 19:56 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 07/20/15 19:56 79-00-55.0 10
Trichloroethene ND ug/L 07/20/15 19:56 79-01-65.0 10
Trichlorofluoromethane ND ug/L 07/20/15 19:56 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 07/20/15 19:56 96-18-45.0 10
1,2,4-Trimethylbenzene 317 ug/L 07/20/15 19:56 95-63-65.0 10
1,3,5-Trimethylbenzene 129 ug/L 07/20/15 19:56 108-67-85.0 10
Vinyl chloride ND ug/L 07/20/15 19:56 75-01-410.0 10
m&p-Xylene 870 ug/L 07/20/15 19:56 179601-23-110.0 10
o-Xylene 296 ug/L 07/20/15 19:56 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)124 %07/20/15 19:56 17060-07-070-130 10
4-Bromofluorobenzene (S)96 %07/20/15 19:56 460-00-470-130 10
Toluene-d8 (S)103 %07/20/15 19:56 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-10 Lab ID:92259124003 Collected:07/16/15 12:30 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 07/20/15 18:34 71-43-20.50 1
Bromobenzene ND ug/L 07/20/15 18:34 108-86-10.50 1
Bromochloromethane ND ug/L 07/20/15 18:34 74-97-50.50 1
Bromodichloromethane ND ug/L 07/20/15 18:34 75-27-40.50 1
Bromoform ND ug/L 07/20/15 18:34 75-25-20.50 1
Bromomethane ND ug/L 07/20/15 18:34 74-83-95.0 1
n-Butylbenzene ND ug/L 07/20/15 18:34 104-51-80.50 1
sec-Butylbenzene ND ug/L 07/20/15 18:34 135-98-80.50 1
tert-Butylbenzene ND ug/L 07/20/15 18:34 98-06-60.50 1
Carbon tetrachloride ND ug/L 07/20/15 18:34 56-23-50.50 1
Chlorobenzene ND ug/L 07/20/15 18:34 108-90-70.50 1
Chloroethane ND ug/L 07/20/15 18:34 75-00-31.0 1
Chloroform ND ug/L 07/20/15 18:34 67-66-30.50 1
Chloromethane ND ug/L 07/20/15 18:34 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/20/15 18:34 95-49-80.50 1
4-Chlorotoluene ND ug/L 07/20/15 18:34 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 07/20/15 18:34 96-12-81.0 1
Dibromochloromethane ND ug/L 07/20/15 18:34 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 07/20/15 18:34 106-93-40.50 1
Dibromomethane ND ug/L 07/20/15 18:34 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 07/20/15 18:34 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 07/20/15 18:34 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 07/20/15 18:34 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 07/20/15 18:34 75-71-80.50 1
1,1-Dichloroethane ND ug/L 07/20/15 18:34 75-34-30.50 1
1,2-Dichloroethane ND ug/L 07/20/15 18:34 107-06-20.50 1
1,1-Dichloroethene ND ug/L 07/20/15 18:34 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 07/20/15 18:34 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 07/20/15 18:34 156-60-50.50 1
1,2-Dichloropropane ND ug/L 07/20/15 18:34 78-87-50.50 1
1,3-Dichloropropane ND ug/L 07/20/15 18:34 142-28-90.50 1
2,2-Dichloropropane ND ug/L 07/20/15 18:34 594-20-70.50 1
1,1-Dichloropropene ND ug/L 07/20/15 18:34 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 07/20/15 18:34 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 07/20/15 18:34 10061-02-60.50 1
Diisopropyl ether ND ug/L 07/20/15 18:34 108-20-30.50 1
Ethylbenzene ND ug/L 07/20/15 18:34 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 07/20/15 18:34 87-68-3 L32.0 1
Isopropylbenzene (Cumene)ND ug/L 07/20/15 18:34 98-82-80.50 1
Methylene Chloride ND ug/L 07/20/15 18:34 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 07/20/15 18:34 1634-04-40.50 1
Naphthalene ND ug/L 07/20/15 18:34 91-20-32.0 1
n-Propylbenzene ND ug/L 07/20/15 18:34 103-65-10.50 1
Styrene ND ug/L 07/20/15 18:34 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 07/20/15 18:34 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 07/20/15 18:34 79-34-50.50 1
Tetrachloroethene ND ug/L 07/20/15 18:34 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-10 Lab ID:92259124003 Collected:07/16/15 12:30 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 07/20/15 18:34 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 07/20/15 18:34 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 07/20/15 18:34 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 07/20/15 18:34 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 07/20/15 18:34 79-00-50.50 1
Trichloroethene ND ug/L 07/20/15 18:34 79-01-60.50 1
Trichlorofluoromethane ND ug/L 07/20/15 18:34 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/20/15 18:34 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 07/20/15 18:34 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 07/20/15 18:34 108-67-80.50 1
Vinyl chloride ND ug/L 07/20/15 18:34 75-01-41.0 1
m&p-Xylene ND ug/L 07/20/15 18:34 179601-23-11.0 1
o-Xylene ND ug/L 07/20/15 18:34 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)126 %07/20/15 18:34 17060-07-070-130 1
4-Bromofluorobenzene (S)92 %07/20/15 18:34 460-00-470-130 1
Toluene-d8 (S)103 %07/20/15 18:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-11 Lab ID:92259124004 Collected:07/16/15 13:10 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 07/20/15 18:50 71-43-20.50 1
Bromobenzene ND ug/L 07/20/15 18:50 108-86-10.50 1
Bromochloromethane ND ug/L 07/20/15 18:50 74-97-50.50 1
Bromodichloromethane ND ug/L 07/20/15 18:50 75-27-40.50 1
Bromoform ND ug/L 07/20/15 18:50 75-25-20.50 1
Bromomethane ND ug/L 07/20/15 18:50 74-83-95.0 1
n-Butylbenzene ND ug/L 07/20/15 18:50 104-51-80.50 1
sec-Butylbenzene ND ug/L 07/20/15 18:50 135-98-80.50 1
tert-Butylbenzene ND ug/L 07/20/15 18:50 98-06-60.50 1
Carbon tetrachloride ND ug/L 07/20/15 18:50 56-23-50.50 1
Chlorobenzene ND ug/L 07/20/15 18:50 108-90-70.50 1
Chloroethane ND ug/L 07/20/15 18:50 75-00-31.0 1
Chloroform ND ug/L 07/20/15 18:50 67-66-30.50 1
Chloromethane ND ug/L 07/20/15 18:50 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/20/15 18:50 95-49-80.50 1
4-Chlorotoluene ND ug/L 07/20/15 18:50 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 07/20/15 18:50 96-12-81.0 1
Dibromochloromethane ND ug/L 07/20/15 18:50 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 07/20/15 18:50 106-93-40.50 1
Dibromomethane ND ug/L 07/20/15 18:50 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 07/20/15 18:50 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 07/20/15 18:50 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 07/20/15 18:50 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 07/20/15 18:50 75-71-80.50 1
1,1-Dichloroethane ND ug/L 07/20/15 18:50 75-34-30.50 1
1,2-Dichloroethane ND ug/L 07/20/15 18:50 107-06-20.50 1
1,1-Dichloroethene ND ug/L 07/20/15 18:50 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 07/20/15 18:50 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 07/20/15 18:50 156-60-50.50 1
1,2-Dichloropropane ND ug/L 07/20/15 18:50 78-87-50.50 1
1,3-Dichloropropane ND ug/L 07/20/15 18:50 142-28-90.50 1
2,2-Dichloropropane ND ug/L 07/20/15 18:50 594-20-70.50 1
1,1-Dichloropropene ND ug/L 07/20/15 18:50 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 07/20/15 18:50 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 07/20/15 18:50 10061-02-60.50 1
Diisopropyl ether ND ug/L 07/20/15 18:50 108-20-30.50 1
Ethylbenzene ND ug/L 07/20/15 18:50 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 07/20/15 18:50 87-68-3 L32.0 1
Isopropylbenzene (Cumene)ND ug/L 07/20/15 18:50 98-82-80.50 1
Methylene Chloride ND ug/L 07/20/15 18:50 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 07/20/15 18:50 1634-04-40.50 1
Naphthalene ND ug/L 07/20/15 18:50 91-20-32.0 1
n-Propylbenzene ND ug/L 07/20/15 18:50 103-65-10.50 1
Styrene ND ug/L 07/20/15 18:50 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 07/20/15 18:50 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 07/20/15 18:50 79-34-50.50 1
Tetrachloroethene ND ug/L 07/20/15 18:50 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-11 Lab ID:92259124004 Collected:07/16/15 13:10 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 07/20/15 18:50 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 07/20/15 18:50 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 07/20/15 18:50 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 07/20/15 18:50 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 07/20/15 18:50 79-00-50.50 1
Trichloroethene ND ug/L 07/20/15 18:50 79-01-60.50 1
Trichlorofluoromethane ND ug/L 07/20/15 18:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/20/15 18:50 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 07/20/15 18:50 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 07/20/15 18:50 108-67-80.50 1
Vinyl chloride ND ug/L 07/20/15 18:50 75-01-41.0 1
m&p-Xylene ND ug/L 07/20/15 18:50 179601-23-11.0 1
o-Xylene ND ug/L 07/20/15 18:50 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)123 %07/20/15 18:50 17060-07-070-130 1
4-Bromofluorobenzene (S)91 %07/20/15 18:50 460-00-470-130 1
Toluene-d8 (S)103 %07/20/15 18:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-12 Lab ID:92259124005 Collected:07/16/15 11:55 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 07/20/15 19:07 71-43-20.50 1
Bromobenzene ND ug/L 07/20/15 19:07 108-86-10.50 1
Bromochloromethane ND ug/L 07/20/15 19:07 74-97-50.50 1
Bromodichloromethane ND ug/L 07/20/15 19:07 75-27-40.50 1
Bromoform ND ug/L 07/20/15 19:07 75-25-20.50 1
Bromomethane ND ug/L 07/20/15 19:07 74-83-95.0 1
n-Butylbenzene ND ug/L 07/20/15 19:07 104-51-80.50 1
sec-Butylbenzene ND ug/L 07/20/15 19:07 135-98-80.50 1
tert-Butylbenzene ND ug/L 07/20/15 19:07 98-06-60.50 1
Carbon tetrachloride ND ug/L 07/20/15 19:07 56-23-50.50 1
Chlorobenzene ND ug/L 07/20/15 19:07 108-90-70.50 1
Chloroethane ND ug/L 07/20/15 19:07 75-00-31.0 1
Chloroform ND ug/L 07/20/15 19:07 67-66-30.50 1
Chloromethane ND ug/L 07/20/15 19:07 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/20/15 19:07 95-49-80.50 1
4-Chlorotoluene ND ug/L 07/20/15 19:07 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 07/20/15 19:07 96-12-81.0 1
Dibromochloromethane ND ug/L 07/20/15 19:07 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 07/20/15 19:07 106-93-40.50 1
Dibromomethane ND ug/L 07/20/15 19:07 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 07/20/15 19:07 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 07/20/15 19:07 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 07/20/15 19:07 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 07/20/15 19:07 75-71-80.50 1
1,1-Dichloroethane ND ug/L 07/20/15 19:07 75-34-30.50 1
1,2-Dichloroethane ND ug/L 07/20/15 19:07 107-06-20.50 1
1,1-Dichloroethene ND ug/L 07/20/15 19:07 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 07/20/15 19:07 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 07/20/15 19:07 156-60-50.50 1
1,2-Dichloropropane ND ug/L 07/20/15 19:07 78-87-50.50 1
1,3-Dichloropropane ND ug/L 07/20/15 19:07 142-28-90.50 1
2,2-Dichloropropane ND ug/L 07/20/15 19:07 594-20-70.50 1
1,1-Dichloropropene ND ug/L 07/20/15 19:07 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 07/20/15 19:07 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 07/20/15 19:07 10061-02-60.50 1
Diisopropyl ether ND ug/L 07/20/15 19:07 108-20-30.50 1
Ethylbenzene ND ug/L 07/20/15 19:07 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 07/20/15 19:07 87-68-3 L32.0 1
Isopropylbenzene (Cumene)ND ug/L 07/20/15 19:07 98-82-80.50 1
Methylene Chloride ND ug/L 07/20/15 19:07 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 07/20/15 19:07 1634-04-40.50 1
Naphthalene ND ug/L 07/20/15 19:07 91-20-32.0 1
n-Propylbenzene ND ug/L 07/20/15 19:07 103-65-10.50 1
Styrene ND ug/L 07/20/15 19:07 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 07/20/15 19:07 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 07/20/15 19:07 79-34-50.50 1
Tetrachloroethene ND ug/L 07/20/15 19:07 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-12 Lab ID:92259124005 Collected:07/16/15 11:55 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 07/20/15 19:07 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 07/20/15 19:07 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 07/20/15 19:07 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 07/20/15 19:07 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 07/20/15 19:07 79-00-50.50 1
Trichloroethene ND ug/L 07/20/15 19:07 79-01-60.50 1
Trichlorofluoromethane ND ug/L 07/20/15 19:07 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/20/15 19:07 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 07/20/15 19:07 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 07/20/15 19:07 108-67-80.50 1
Vinyl chloride ND ug/L 07/20/15 19:07 75-01-41.0 1
m&p-Xylene ND ug/L 07/20/15 19:07 179601-23-11.0 1
o-Xylene ND ug/L 07/20/15 19:07 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)126 %07/20/15 19:07 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %07/20/15 19:07 460-00-470-130 1
Toluene-d8 (S)103 %07/20/15 19:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-13 Lab ID:92259124006 Collected:07/16/15 11:10 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 07/20/15 19:23 71-43-20.50 1
Bromobenzene ND ug/L 07/20/15 19:23 108-86-10.50 1
Bromochloromethane ND ug/L 07/20/15 19:23 74-97-50.50 1
Bromodichloromethane ND ug/L 07/20/15 19:23 75-27-40.50 1
Bromoform ND ug/L 07/20/15 19:23 75-25-20.50 1
Bromomethane ND ug/L 07/20/15 19:23 74-83-95.0 1
n-Butylbenzene ND ug/L 07/20/15 19:23 104-51-80.50 1
sec-Butylbenzene ND ug/L 07/20/15 19:23 135-98-80.50 1
tert-Butylbenzene ND ug/L 07/20/15 19:23 98-06-60.50 1
Carbon tetrachloride ND ug/L 07/20/15 19:23 56-23-50.50 1
Chlorobenzene ND ug/L 07/20/15 19:23 108-90-70.50 1
Chloroethane ND ug/L 07/20/15 19:23 75-00-31.0 1
Chloroform ND ug/L 07/20/15 19:23 67-66-30.50 1
Chloromethane ND ug/L 07/20/15 19:23 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/20/15 19:23 95-49-80.50 1
4-Chlorotoluene ND ug/L 07/20/15 19:23 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 07/20/15 19:23 96-12-81.0 1
Dibromochloromethane ND ug/L 07/20/15 19:23 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 07/20/15 19:23 106-93-40.50 1
Dibromomethane ND ug/L 07/20/15 19:23 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 07/20/15 19:23 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 07/20/15 19:23 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 07/20/15 19:23 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 07/20/15 19:23 75-71-80.50 1
1,1-Dichloroethane ND ug/L 07/20/15 19:23 75-34-30.50 1
1,2-Dichloroethane ND ug/L 07/20/15 19:23 107-06-20.50 1
1,1-Dichloroethene ND ug/L 07/20/15 19:23 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 07/20/15 19:23 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 07/20/15 19:23 156-60-50.50 1
1,2-Dichloropropane ND ug/L 07/20/15 19:23 78-87-50.50 1
1,3-Dichloropropane ND ug/L 07/20/15 19:23 142-28-90.50 1
2,2-Dichloropropane ND ug/L 07/20/15 19:23 594-20-70.50 1
1,1-Dichloropropene ND ug/L 07/20/15 19:23 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 07/20/15 19:23 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 07/20/15 19:23 10061-02-60.50 1
Diisopropyl ether ND ug/L 07/20/15 19:23 108-20-30.50 1
Ethylbenzene ND ug/L 07/20/15 19:23 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 07/20/15 19:23 87-68-3 L32.0 1
Isopropylbenzene (Cumene)ND ug/L 07/20/15 19:23 98-82-80.50 1
Methylene Chloride ND ug/L 07/20/15 19:23 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 07/20/15 19:23 1634-04-40.50 1
Naphthalene ND ug/L 07/20/15 19:23 91-20-32.0 1
n-Propylbenzene ND ug/L 07/20/15 19:23 103-65-10.50 1
Styrene ND ug/L 07/20/15 19:23 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 07/20/15 19:23 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 07/20/15 19:23 79-34-50.50 1
Tetrachloroethene ND ug/L 07/20/15 19:23 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
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Page 15 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-13 Lab ID:92259124006 Collected:07/16/15 11:10 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 07/20/15 19:23 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 07/20/15 19:23 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 07/20/15 19:23 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 07/20/15 19:23 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 07/20/15 19:23 79-00-50.50 1
Trichloroethene ND ug/L 07/20/15 19:23 79-01-60.50 1
Trichlorofluoromethane ND ug/L 07/20/15 19:23 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/20/15 19:23 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 07/20/15 19:23 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 07/20/15 19:23 108-67-80.50 1
Vinyl chloride ND ug/L 07/20/15 19:23 75-01-41.0 1
m&p-Xylene ND ug/L 07/20/15 19:23 179601-23-11.0 1
o-Xylene ND ug/L 07/20/15 19:23 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)127 %07/20/15 19:23 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %07/20/15 19:23 460-00-470-130 1
Toluene-d8 (S)103 %07/20/15 19:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
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Page 16 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-14 Lab ID:92259124007 Collected:07/16/15 14:45 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 281 ug/L 07/21/15 10:33 71-43-22.5 5
Bromobenzene ND ug/L 07/21/15 10:33 108-86-12.5 5
Bromochloromethane ND ug/L 07/21/15 10:33 74-97-52.5 5
Bromodichloromethane ND ug/L 07/21/15 10:33 75-27-42.5 5
Bromoform ND ug/L 07/21/15 10:33 75-25-22.5 5
Bromomethane ND ug/L 07/21/15 10:33 74-83-925.0 5
n-Butylbenzene 6.1 ug/L 07/21/15 10:33 104-51-82.5 5
sec-Butylbenzene 5.1 ug/L 07/21/15 10:33 135-98-82.5 5
tert-Butylbenzene ND ug/L 07/21/15 10:33 98-06-62.5 5
Carbon tetrachloride ND ug/L 07/21/15 10:33 56-23-52.5 5
Chlorobenzene ND ug/L 07/21/15 10:33 108-90-72.5 5
Chloroethane ND ug/L 07/21/15 10:33 75-00-35.0 5
Chloroform ND ug/L 07/21/15 10:33 67-66-32.5 5
Chloromethane ND ug/L 07/21/15 10:33 74-87-35.0 5
2-Chlorotoluene ND ug/L 07/21/15 10:33 95-49-82.5 5
4-Chlorotoluene ND ug/L 07/21/15 10:33 106-43-42.5 5
1,2-Dibromo-3-chloropropane ND ug/L 07/21/15 10:33 96-12-85.0 5
Dibromochloromethane ND ug/L 07/21/15 10:33 124-48-12.5 5
1,2-Dibromoethane (EDB)ND ug/L 07/21/15 10:33 106-93-42.5 5
Dibromomethane ND ug/L 07/21/15 10:33 74-95-32.5 5
1,2-Dichlorobenzene ND ug/L 07/21/15 10:33 95-50-12.5 5
1,3-Dichlorobenzene ND ug/L 07/21/15 10:33 541-73-12.5 5
1,4-Dichlorobenzene ND ug/L 07/21/15 10:33 106-46-72.5 5
Dichlorodifluoromethane ND ug/L 07/21/15 10:33 75-71-82.5 5
1,1-Dichloroethane ND ug/L 07/21/15 10:33 75-34-32.5 5
1,2-Dichloroethane ND ug/L 07/21/15 10:33 107-06-22.5 5
1,1-Dichloroethene ND ug/L 07/21/15 10:33 75-35-42.5 5
cis-1,2-Dichloroethene ND ug/L 07/21/15 10:33 156-59-22.5 5
trans-1,2-Dichloroethene ND ug/L 07/21/15 10:33 156-60-52.5 5
1,2-Dichloropropane ND ug/L 07/21/15 10:33 78-87-52.5 5
1,3-Dichloropropane ND ug/L 07/21/15 10:33 142-28-92.5 5
2,2-Dichloropropane ND ug/L 07/21/15 10:33 594-20-72.5 5
1,1-Dichloropropene ND ug/L 07/21/15 10:33 563-58-62.5 5
cis-1,3-Dichloropropene ND ug/L 07/21/15 10:33 10061-01-52.5 5
trans-1,3-Dichloropropene ND ug/L 07/21/15 10:33 10061-02-62.5 5
Diisopropyl ether 9.5 ug/L 07/21/15 10:33 108-20-32.5 5
Ethylbenzene 119 ug/L 07/21/15 10:33 100-41-42.5 5
Hexachloro-1,3-butadiene ND ug/L 07/21/15 10:33 87-68-310.0 5
Isopropylbenzene (Cumene)16.9 ug/L 07/21/15 10:33 98-82-82.5 5
Methylene Chloride ND ug/L 07/21/15 10:33 75-09-210.0 5
Methyl-tert-butyl ether 115 ug/L 07/21/15 10:33 1634-04-42.5 5
Naphthalene 25.5 ug/L 07/21/15 10:33 91-20-310.0 5
n-Propylbenzene 29.8 ug/L 07/21/15 10:33 103-65-12.5 5
Styrene ND ug/L 07/21/15 10:33 100-42-52.5 5
1,1,1,2-Tetrachloroethane ND ug/L 07/21/15 10:33 630-20-62.5 5
1,1,2,2-Tetrachloroethane ND ug/L 07/21/15 10:33 79-34-52.5 5
Tetrachloroethene ND ug/L 07/21/15 10:33 127-18-42.5 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
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Page 17 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-14 Lab ID:92259124007 Collected:07/16/15 14:45 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 650 ug/L 07/21/15 10:33 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 07/21/15 10:33 87-61-610.0 5
1,2,4-Trichlorobenzene ND ug/L 07/21/15 10:33 120-82-110.0 5
1,1,1-Trichloroethane ND ug/L 07/21/15 10:33 71-55-62.5 5
1,1,2-Trichloroethane ND ug/L 07/21/15 10:33 79-00-52.5 5
Trichloroethene ND ug/L 07/21/15 10:33 79-01-62.5 5
Trichlorofluoromethane ND ug/L 07/21/15 10:33 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 07/21/15 10:33 96-18-42.5 5
1,2,4-Trimethylbenzene 86.2 ug/L 07/21/15 10:33 95-63-62.5 5
1,3,5-Trimethylbenzene 28.3 ug/L 07/21/15 10:33 108-67-82.5 5
Vinyl chloride ND ug/L 07/21/15 10:33 75-01-45.0 5
m&p-Xylene 280 ug/L 07/21/15 10:33 179601-23-15.0 5
o-Xylene 119 ug/L 07/21/15 10:33 95-47-62.5 5
Surrogates
1,2-Dichloroethane-d4 (S)110 %07/21/15 10:33 17060-07-070-130 5
4-Bromofluorobenzene (S)98 %07/21/15 10:33 460-00-470-130 5
Toluene-d8 (S)100 %07/21/15 10:33 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-15 Lab ID:92259124008 Collected:07/16/15 14:10 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 1140 ug/L 07/20/15 20:29 71-43-210.0 20
Bromobenzene ND ug/L 07/20/15 20:29 108-86-110.0 20
Bromochloromethane ND ug/L 07/20/15 20:29 74-97-510.0 20
Bromodichloromethane ND ug/L 07/20/15 20:29 75-27-410.0 20
Bromoform ND ug/L 07/20/15 20:29 75-25-210.0 20
Bromomethane ND ug/L 07/20/15 20:29 74-83-910020
n-Butylbenzene 288 ug/L 07/20/15 20:29 104-51-810.0 20
sec-Butylbenzene ND ug/L 07/20/15 20:29 135-98-810.0 20
tert-Butylbenzene ND ug/L 07/20/15 20:29 98-06-610.0 20
Carbon tetrachloride ND ug/L 07/20/15 20:29 56-23-510.0 20
Chlorobenzene ND ug/L 07/20/15 20:29 108-90-710.0 20
Chloroethane ND ug/L 07/20/15 20:29 75-00-320.0 20
Chloroform ND ug/L 07/20/15 20:29 67-66-310.0 20
Chloromethane ND ug/L 07/20/15 20:29 74-87-320.0 20
2-Chlorotoluene ND ug/L 07/20/15 20:29 95-49-810.0 20
4-Chlorotoluene ND ug/L 07/20/15 20:29 106-43-410.0 20
1,2-Dibromo-3-chloropropane ND ug/L 07/20/15 20:29 96-12-820.0 20
Dibromochloromethane ND ug/L 07/20/15 20:29 124-48-110.0 20
1,2-Dibromoethane (EDB)ND ug/L 07/20/15 20:29 106-93-410.0 20
Dibromomethane ND ug/L 07/20/15 20:29 74-95-310.0 20
1,2-Dichlorobenzene ND ug/L 07/20/15 20:29 95-50-110.0 20
1,3-Dichlorobenzene ND ug/L 07/20/15 20:29 541-73-110.0 20
1,4-Dichlorobenzene ND ug/L 07/20/15 20:29 106-46-710.0 20
Dichlorodifluoromethane ND ug/L 07/20/15 20:29 75-71-810.0 20
1,1-Dichloroethane ND ug/L 07/20/15 20:29 75-34-310.0 20
1,2-Dichloroethane ND ug/L 07/20/15 20:29 107-06-210.0 20
1,1-Dichloroethene ND ug/L 07/20/15 20:29 75-35-410.0 20
cis-1,2-Dichloroethene ND ug/L 07/20/15 20:29 156-59-210.0 20
trans-1,2-Dichloroethene ND ug/L 07/20/15 20:29 156-60-510.0 20
1,2-Dichloropropane ND ug/L 07/20/15 20:29 78-87-510.0 20
1,3-Dichloropropane ND ug/L 07/20/15 20:29 142-28-910.0 20
2,2-Dichloropropane ND ug/L 07/20/15 20:29 594-20-710.0 20
1,1-Dichloropropene ND ug/L 07/20/15 20:29 563-58-610.0 20
cis-1,3-Dichloropropene ND ug/L 07/20/15 20:29 10061-01-510.0 20
trans-1,3-Dichloropropene ND ug/L 07/20/15 20:29 10061-02-610.0 20
Diisopropyl ether ND ug/L 07/20/15 20:29 108-20-310.0 20
Ethylbenzene 3730 ug/L 07/20/15 20:29 100-41-410.0 20
Hexachloro-1,3-butadiene ND ug/L 07/20/15 20:29 87-68-3 L340.0 20
Isopropylbenzene (Cumene)409 ug/L 07/20/15 20:29 98-82-810.0 20
Methylene Chloride ND ug/L 07/20/15 20:29 75-09-240.0 20
Methyl-tert-butyl ether 196 ug/L 07/20/15 20:29 1634-04-410.0 20
Naphthalene 1460 ug/L 07/20/15 20:29 91-20-340.0 20
n-Propylbenzene 1420 ug/L 07/20/15 20:29 103-65-110.0 20
Styrene 91.1 ug/L 07/20/15 20:29 100-42-510.0 20
1,1,1,2-Tetrachloroethane ND ug/L 07/20/15 20:29 630-20-610.0 20
1,1,2,2-Tetrachloroethane ND ug/L 07/20/15 20:29 79-34-510.0 20
Tetrachloroethene ND ug/L 07/20/15 20:29 127-18-410.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
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Huntersville, NC 28078
[phone]
Page 19 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Sample:MW-15 Lab ID:92259124008 Collected:07/16/15 14:10 Received:07/16/15 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 9060 ug/L 07/23/15 16:13 108-88-350.0 100
1,2,3-Trichlorobenzene ND ug/L 07/20/15 20:29 87-61-640.0 20
1,2,4-Trichlorobenzene ND ug/L 07/20/15 20:29 120-82-140.0 20
1,1,1-Trichloroethane ND ug/L 07/20/15 20:29 71-55-610.0 20
1,1,2-Trichloroethane ND ug/L 07/20/15 20:29 79-00-510.0 20
Trichloroethene ND ug/L 07/20/15 20:29 79-01-610.0 20
Trichlorofluoromethane ND ug/L 07/20/15 20:29 75-69-420.0 20
1,2,3-Trichloropropane ND ug/L 07/20/15 20:29 96-18-410.0 20
1,2,4-Trimethylbenzene 6910 ug/L 07/23/15 16:13 95-63-650.0 100
1,3,5-Trimethylbenzene 2470 ug/L 07/20/15 20:29 108-67-810.0 20
Vinyl chloride ND ug/L 07/20/15 20:29 75-01-420.0 20
m&p-Xylene 12000 ug/L 07/23/15 16:13 179601-23-1100100
o-Xylene 4830 ug/L 07/23/15 16:13 95-47-650.0 100
Surrogates
1,2-Dichloroethane-d4 (S)125 %07/20/15 20:29 17060-07-070-130 20
4-Bromofluorobenzene (S)96 %07/20/15 20:29 460-00-470-130 20
Toluene-d8 (S)102 %07/20/15 20:29 2037-26-570-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32632
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92259124001, 92259124002, 92259124003, 92259124004, 92259124005, 92259124006, 92259124008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1512541
Associated Lab Samples:92259124001, 92259124002, 92259124003, 92259124004, 92259124005, 92259124006, 92259124008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 07/20/15 16:21
1,1,1-Trichloroethane ug/L ND 0.50 07/20/15 16:21
1,1,2,2-Tetrachloroethane ug/L ND 0.50 07/20/15 16:21
1,1,2-Trichloroethane ug/L ND 0.50 07/20/15 16:21
1,1-Dichloroethane ug/L ND 0.50 07/20/15 16:21
1,1-Dichloroethene ug/L ND 0.50 07/20/15 16:21
1,1-Dichloropropene ug/L ND 0.50 07/20/15 16:21
1,2,3-Trichlorobenzene ug/L ND 2.0 07/20/15 16:21
1,2,3-Trichloropropane ug/L ND 0.50 07/20/15 16:21
1,2,4-Trichlorobenzene ug/L ND 2.0 07/20/15 16:21
1,2,4-Trimethylbenzene ug/L ND 0.50 07/20/15 16:21
1,2-Dibromo-3-chloropropane ug/L ND 1.0 07/20/15 16:21
1,2-Dibromoethane (EDB)ug/L ND 0.50 07/20/15 16:21
1,2-Dichlorobenzene ug/L ND 0.50 07/20/15 16:21
1,2-Dichloroethane ug/L ND 0.50 07/20/15 16:21
1,2-Dichloropropane ug/L ND 0.50 07/20/15 16:21
1,3,5-Trimethylbenzene ug/L ND 0.50 07/20/15 16:21
1,3-Dichlorobenzene ug/L ND 0.50 07/20/15 16:21
1,3-Dichloropropane ug/L ND 0.50 07/20/15 16:21
1,4-Dichlorobenzene ug/L ND 0.50 07/20/15 16:21
2,2-Dichloropropane ug/L ND 0.50 07/20/15 16:21
2-Chlorotoluene ug/L ND 0.50 07/20/15 16:21
4-Chlorotoluene ug/L ND 0.50 07/20/15 16:21
Benzene ug/L ND 0.50 07/20/15 16:21
Bromobenzene ug/L ND 0.50 07/20/15 16:21
Bromochloromethane ug/L ND 0.50 07/20/15 16:21
Bromodichloromethane ug/L ND 0.50 07/20/15 16:21
Bromoform ug/L ND 0.50 07/20/15 16:21
Bromomethane ug/L ND 5.0 07/20/15 16:21
Carbon tetrachloride ug/L ND 0.50 07/20/15 16:21
Chlorobenzene ug/L ND 0.50 07/20/15 16:21
Chloroethane ug/L ND 1.0 07/20/15 16:21
Chloroform ug/L ND 0.50 07/20/15 16:21
Chloromethane ug/L ND 1.0 07/20/15 16:21
cis-1,2-Dichloroethene ug/L ND 0.50 07/20/15 16:21
cis-1,3-Dichloropropene ug/L ND 0.50 07/20/15 16:21
Dibromochloromethane ug/L ND 0.50 07/20/15 16:21
Dibromomethane ug/L ND 0.50 07/20/15 16:21
Dichlorodifluoromethane ug/L ND 0.50 07/20/15 16:21
Diisopropyl ether ug/L ND 0.50 07/20/15 16:21
Ethylbenzene ug/L ND 0.50 07/20/15 16:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1512541
Associated Lab Samples:92259124001, 92259124002, 92259124003, 92259124004, 92259124005, 92259124006, 92259124008
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 07/20/15 16:21
Isopropylbenzene (Cumene)ug/L ND 0.50 07/20/15 16:21
m&p-Xylene ug/L ND 1.0 07/20/15 16:21
Methyl-tert-butyl ether ug/L ND 0.50 07/20/15 16:21
Methylene Chloride ug/L ND 2.0 07/20/15 16:21
n-Butylbenzene ug/L ND 0.50 07/20/15 16:21
n-Propylbenzene ug/L ND 0.50 07/20/15 16:21
Naphthalene ug/L ND 2.0 07/20/15 16:21
o-Xylene ug/L ND 0.50 07/20/15 16:21
sec-Butylbenzene ug/L ND 0.50 07/20/15 16:21
Styrene ug/L ND 0.50 07/20/15 16:21
tert-Butylbenzene ug/L ND 0.50 07/20/15 16:21
Tetrachloroethene ug/L ND 0.50 07/20/15 16:21
Toluene ug/L ND 0.50 07/20/15 16:21
trans-1,2-Dichloroethene ug/L ND 0.50 07/20/15 16:21
trans-1,3-Dichloropropene ug/L ND 0.50 07/20/15 16:21
Trichloroethene ug/L ND 0.50 07/20/15 16:21
Trichlorofluoromethane ug/L ND 1.0 07/20/15 16:21
Vinyl chloride ug/L ND 1.0 07/20/15 16:21
1,2-Dichloroethane-d4 (S)%113 70-130 07/20/15 16:21
4-Bromofluorobenzene (S)%98 70-130 07/20/15 16:21
Toluene-d8 (S)%101 70-130 07/20/15 16:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1512542LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.350 105 60-140
1,1,1-Trichloroethane ug/L 61.150 122 60-140
1,1,2,2-Tetrachloroethane ug/L 57.850 116 60-140
1,1,2-Trichloroethane ug/L 54.450 109 60-140
1,1-Dichloroethane ug/L 62.150 124 60-140
1,1-Dichloroethene ug/L 64.950 130 60-140
1,1-Dichloropropene ug/L 65.050 130 60-140
1,2,3-Trichlorobenzene ug/L 51.450 103 60-140
1,2,3-Trichloropropane ug/L 54.750 109 60-140
1,2,4-Trichlorobenzene ug/L 51.850 104 60-140
1,2,4-Trimethylbenzene ug/L 54.350 109 60-140
1,2-Dibromo-3-chloropropane ug/L 55.150 110 60-140
1,2-Dibromoethane (EDB)ug/L 55.850 112 60-140
1,2-Dichlorobenzene ug/L 54.550 109 60-140
1,2-Dichloroethane ug/L 56.550 113 60-140
1,2-Dichloropropane ug/L 57.550 115 60-140
1,3,5-Trimethylbenzene ug/L 55.050 110 60-140
1,3-Dichlorobenzene ug/L 55.050 110 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1512542LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 56.550 113 60-140
1,4-Dichlorobenzene ug/L 53.650 107 60-140
2,2-Dichloropropane ug/L 62.550 125 60-140
2-Chlorotoluene ug/L 54.150 108 60-140
4-Chlorotoluene ug/L 55.550 111 60-140
Benzene ug/L 57.250 114 60-140
Bromobenzene ug/L 55.450 111 60-140
Bromochloromethane ug/L 64.150 128 60-140
Bromodichloromethane ug/L 59.450 119 60-140
Bromoform ug/L 49.650 99 60-140
Bromomethane ug/L 61.050 122 60-140
Carbon tetrachloride ug/L 56.250 112 60-140
Chlorobenzene ug/L 54.750 109 60-140
Chloroethane ug/L 55.750 111 60-140
Chloroform ug/L 59.950 120 60-140
Chloromethane ug/L 58.350 117 60-140
cis-1,2-Dichloroethene ug/L 61.750 123 60-140
cis-1,3-Dichloropropene ug/L 58.150 116 60-140
Dibromochloromethane ug/L 54.050 108 60-140
Dibromomethane ug/L 55.150 110 60-140
Dichlorodifluoromethane ug/L 54.050 108 60-140
Diisopropyl ether ug/L 64.050 128 60-140
Ethylbenzene ug/L 54.150 108 60-140
Hexachloro-1,3-butadiene ug/L 75.4 L05015160-140
Isopropylbenzene (Cumene)ug/L 55.750 111 60-140
m&p-Xylene ug/L 109100 109 60-140
Methyl-tert-butyl ether ug/L 63.550 127 60-140
Methylene Chloride ug/L 66.650 133 60-140
n-Butylbenzene ug/L 57.650 115 60-140
n-Propylbenzene ug/L 56.950 114 60-140
Naphthalene ug/L 51.250 102 60-140
o-Xylene ug/L 53.750 107 60-140
sec-Butylbenzene ug/L 58.150 116 60-140
Styrene ug/L 56.050 112 60-140
tert-Butylbenzene ug/L 44.850 90 60-140
Tetrachloroethene ug/L 49.950 100 60-140
Toluene ug/L 55.550 111 60-140
trans-1,2-Dichloroethene ug/L 62.350 125 60-140
trans-1,3-Dichloropropene ug/L 59.550 119 60-140
Trichloroethene ug/L 53.450 107 60-140
Trichlorofluoromethane ug/L 53.750 107 60-140
Vinyl chloride ug/L 60.050 120 60-140
1,2-Dichloroethane-d4 (S)%114 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32634
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92259124007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1512567
Associated Lab Samples:92259124007
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 07/20/15 23:47
1,1,1-Trichloroethane ug/L ND 0.50 07/20/15 23:47
1,1,2,2-Tetrachloroethane ug/L ND 0.50 07/20/15 23:47
1,1,2-Trichloroethane ug/L ND 0.50 07/20/15 23:47
1,1-Dichloroethane ug/L ND 0.50 07/20/15 23:47
1,1-Dichloroethene ug/L ND 0.50 07/20/15 23:47
1,1-Dichloropropene ug/L ND 0.50 07/20/15 23:47
1,2,3-Trichlorobenzene ug/L ND 2.0 07/20/15 23:47
1,2,3-Trichloropropane ug/L ND 0.50 07/20/15 23:47
1,2,4-Trichlorobenzene ug/L ND 2.0 07/20/15 23:47
1,2,4-Trimethylbenzene ug/L ND 0.50 07/20/15 23:47
1,2-Dibromo-3-chloropropane ug/L ND 1.0 07/20/15 23:47
1,2-Dibromoethane (EDB)ug/L ND 0.50 07/20/15 23:47
1,2-Dichlorobenzene ug/L ND 0.50 07/20/15 23:47
1,2-Dichloroethane ug/L ND 0.50 07/20/15 23:47
1,2-Dichloropropane ug/L ND 0.50 07/20/15 23:47
1,3,5-Trimethylbenzene ug/L ND 0.50 07/20/15 23:47
1,3-Dichlorobenzene ug/L ND 0.50 07/20/15 23:47
1,3-Dichloropropane ug/L ND 0.50 07/20/15 23:47
1,4-Dichlorobenzene ug/L ND 0.50 07/20/15 23:47
2,2-Dichloropropane ug/L ND 0.50 07/20/15 23:47
2-Chlorotoluene ug/L ND 0.50 07/20/15 23:47
4-Chlorotoluene ug/L ND 0.50 07/20/15 23:47
Benzene ug/L ND 0.50 07/20/15 23:47
Bromobenzene ug/L ND 0.50 07/20/15 23:47
Bromochloromethane ug/L ND 0.50 07/20/15 23:47
Bromodichloromethane ug/L ND 0.50 07/20/15 23:47
Bromoform ug/L ND 0.50 07/20/15 23:47
Bromomethane ug/L ND 5.0 07/20/15 23:47
Carbon tetrachloride ug/L ND 0.50 07/20/15 23:47
Chlorobenzene ug/L ND 0.50 07/20/15 23:47
Chloroethane ug/L ND 1.0 07/20/15 23:47
Chloroform ug/L ND 0.50 07/20/15 23:47
Chloromethane ug/L ND 1.0 07/20/15 23:47
cis-1,2-Dichloroethene ug/L ND 0.50 07/20/15 23:47
cis-1,3-Dichloropropene ug/L ND 0.50 07/20/15 23:47
Dibromochloromethane ug/L ND 0.50 07/20/15 23:47
Dibromomethane ug/L ND 0.50 07/20/15 23:47
Dichlorodifluoromethane ug/L ND 0.50 07/20/15 23:47
Diisopropyl ether ug/L ND 0.50 07/20/15 23:47
Ethylbenzene ug/L ND 0.50 07/20/15 23:47
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
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[phone]
Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1512567
Associated Lab Samples:92259124007
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 07/20/15 23:47
Isopropylbenzene (Cumene)ug/L ND 0.50 07/20/15 23:47
m&p-Xylene ug/L ND 1.0 07/20/15 23:47
Methyl-tert-butyl ether ug/L ND 0.50 07/20/15 23:47
Methylene Chloride ug/L ND 2.0 07/20/15 23:47
n-Butylbenzene ug/L ND 0.50 07/20/15 23:47
n-Propylbenzene ug/L ND 0.50 07/20/15 23:47
Naphthalene ug/L ND 2.0 07/20/15 23:47
o-Xylene ug/L ND 0.50 07/20/15 23:47
sec-Butylbenzene ug/L ND 0.50 07/20/15 23:47
Styrene ug/L ND 0.50 07/20/15 23:47
tert-Butylbenzene ug/L ND 0.50 07/20/15 23:47
Tetrachloroethene ug/L ND 0.50 07/20/15 23:47
Toluene ug/L ND 0.50 07/20/15 23:47
trans-1,2-Dichloroethene ug/L ND 0.50 07/20/15 23:47
trans-1,3-Dichloropropene ug/L ND 0.50 07/20/15 23:47
Trichloroethene ug/L ND 0.50 07/20/15 23:47
Trichlorofluoromethane ug/L ND 1.0 07/20/15 23:47
Vinyl chloride ug/L ND 1.0 07/20/15 23:47
1,2-Dichloroethane-d4 (S)%114 70-130 07/20/15 23:47
4-Bromofluorobenzene (S)%93 70-130 07/20/15 23:47
Toluene-d8 (S)%100 70-130 07/20/15 23:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1512568LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.950 102 60-140
1,1,1-Trichloroethane ug/L 59.750 119 60-140
1,1,2,2-Tetrachloroethane ug/L 57.650 115 60-140
1,1,2-Trichloroethane ug/L 54.150 108 60-140
1,1-Dichloroethane ug/L 60.350 121 60-140
1,1-Dichloroethene ug/L 63.750 127 60-140
1,1-Dichloropropene ug/L 61.850 124 60-140
1,2,3-Trichlorobenzene ug/L 51.850 104 60-140
1,2,3-Trichloropropane ug/L 53.550 107 60-140
1,2,4-Trichlorobenzene ug/L 51.450 103 60-140
1,2,4-Trimethylbenzene ug/L 53.350 107 60-140
1,2-Dibromo-3-chloropropane ug/L 56.450 113 60-140
1,2-Dibromoethane (EDB)ug/L 55.250 110 60-140
1,2-Dichlorobenzene ug/L 55.150 110 60-140
1,2-Dichloroethane ug/L 56.050 112 60-140
1,2-Dichloropropane ug/L 56.550 113 60-140
1,3,5-Trimethylbenzene ug/L 54.150 108 60-140
1,3-Dichlorobenzene ug/L 54.650 109 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1512568LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 54.450 109 60-140
1,4-Dichlorobenzene ug/L 52.050 104 60-140
2,2-Dichloropropane ug/L 52.050 104 60-140
2-Chlorotoluene ug/L 54.050 108 60-140
4-Chlorotoluene ug/L 54.650 109 60-140
Benzene ug/L 54.650 109 60-140
Bromobenzene ug/L 58.050 116 60-140
Bromochloromethane ug/L 64.050 128 60-140
Bromodichloromethane ug/L 56.850 114 60-140
Bromoform ug/L 46.150 92 60-140
Bromomethane ug/L 56.350 113 60-140
Carbon tetrachloride ug/L 53.750 107 60-140
Chlorobenzene ug/L 53.550 107 60-140
Chloroethane ug/L 52.950 106 60-140
Chloroform ug/L 59.150 118 60-140
Chloromethane ug/L 59.750 119 60-140
cis-1,2-Dichloroethene ug/L 60.550 121 60-140
cis-1,3-Dichloropropene ug/L 53.950 108 60-140
Dibromochloromethane ug/L 52.150 104 60-140
Dibromomethane ug/L 53.150 106 60-140
Dichlorodifluoromethane ug/L 54.250 108 60-140
Diisopropyl ether ug/L 66.050 132 60-140
Ethylbenzene ug/L 51.750 103 60-140
Hexachloro-1,3-butadiene ug/L 65.850 132 60-140
Isopropylbenzene (Cumene)ug/L 52.850 106 60-140
m&p-Xylene ug/L 104100 104 60-140
Methyl-tert-butyl ether ug/L 61.450 123 60-140
Methylene Chloride ug/L 64.750 129 60-140
n-Butylbenzene ug/L 53.550 107 60-140
n-Propylbenzene ug/L 54.850 110 60-140
Naphthalene ug/L 54.050 108 60-140
o-Xylene ug/L 52.350 105 60-140
sec-Butylbenzene ug/L 55.450 111 60-140
Styrene ug/L 54.650 109 60-140
tert-Butylbenzene ug/L 44.150 88 60-140
Tetrachloroethene ug/L 47.750 95 60-140
Toluene ug/L 52.350 105 60-140
trans-1,2-Dichloroethene ug/L 59.950 120 60-140
trans-1,3-Dichloropropene ug/L 56.750 113 60-140
Trichloroethene ug/L 51.050 102 60-140
Trichlorofluoromethane ug/L 50.350 101 60-140
Vinyl chloride ug/L 58.950 118 60-140
1,2-Dichloroethane-d4 (S)%114 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1512569MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92259099002
1512570
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 100 60-140107 7 3020ND20.0 21.4
1,1,1-Trichloroethane ug/L 20 122 60-140129 6 3020ND24.5 25.9
1,1,2,2-Tetrachloroethane ug/L 20 114 60-140115 1 3020ND22.8 23.0
1,1,2-Trichloroethane ug/L 20 109 60-140116 6 3020ND21.7 23.1
1,1-Dichloroethane ug/L 20 120 60-140126 5 3020ND24.0 25.2
1,1-Dichloroethene ug/L 20 131 60-140138 6 3020ND26.1 27.7
1,1-Dichloropropene ug/L 20 126 60-140132 4 3020ND25.3 26.4
1,2,3-Trichlorobenzene ug/L 20 99 60-140100 2 3020ND19.7 20.0
1,2,3-Trichloropropane ug/L 20 109 60-140112 3 3020ND21.7 22.3
1,2,4-Trichlorobenzene ug/L 20 91 60-140100 10 3020ND18.1 20.0
1,2,4-Trimethylbenzene ug/L 20 106 60-140112 5 3020ND21.3 22.5
1,2-Dibromo-3-
chloropropane ug/L 20 97 60-140101 5 3020ND19.4 20.3
1,2-Dibromoethane (EDB)ug/L 20 112 60-140113 1 3020ND22.5 22.6
1,2-Dichlorobenzene ug/L 20 110 60-140115 4 3020ND22.1 23.1
1,2-Dichloroethane ug/L 20 108 60-140114 5 3020ND21.7 22.9
1,2-Dichloropropane ug/L 20 116 60-140121 4 3020ND23.2 24.2
1,3,5-Trimethylbenzene ug/L 20 109 60-140116 6 3020ND21.9 23.1
1,3-Dichlorobenzene ug/L 20 108 60-140117 8 3020ND21.6 23.4
1,3-Dichloropropane ug/L 20 114 60-140117 3 3020ND22.8 23.4
1,4-Dichlorobenzene ug/L 20 104 60-140112 7 3020ND20.8 22.3
2,2-Dichloropropane ug/L M1203060-14032 7 3020ND5.9 6.3
2-Chlorotoluene ug/L 20 110 60-140118 6 3020ND22.1 23.5
4-Chlorotoluene ug/L 20 109 60-140117 7 3020ND21.8 23.3
Benzene ug/L 20 118 60-140123 4 3020ND23.5 24.5
Bromobenzene ug/L 20 113 60-140118 4 3020ND22.6 23.5
Bromochloromethane ug/L 20 124 60-140132 7 3020ND24.8 26.5
Bromodichloromethane ug/L 20 110 60-140117 6 3020ND22.1 23.5
Bromoform ug/L 20 76 60-14084 9 3020ND15.2 16.7
Bromomethane ug/L 20 81 60-14098 18 3020ND16.3 19.6
Carbon tetrachloride ug/L 20 112 60-140119 7 3020ND22.4 23.9
Chlorobenzene ug/L 20 112 60-140118 5 3020ND22.3 23.5
Chloroethane ug/L 20 111 60-140120 7 3020ND22.3 23.9
Chloroform ug/L 20 119 60-140126 6 3020ND23.7 25.1
Chloromethane ug/L 20 125 60-140132 5 3020ND25.1 26.4
cis-1,2-Dichloroethene ug/L 20 118 60-140127 8 3020ND23.6 25.4
cis-1,3-Dichloropropene ug/L 20 84 60-14088 6 3020ND16.7 17.7
Dibromochloromethane ug/L 20 93 60-140102 9 3020ND18.6 20.4
Dibromomethane ug/L 20 107 60-140116 7 3020ND21.5 23.1
Dichlorodifluoromethane ug/L 20 117 60-140125 6 3020ND23.4 25.0
Diisopropyl ether ug/L 20 127 60-140134 5 3020ND25.5 26.8
Ethylbenzene ug/L 20 110 60-140116 5 3020ND22.0 23.2
Hexachloro-1,3-butadiene ug/L 20 101 60-140128 24 3020ND20.2 25.6
Isopropylbenzene (Cumene)ug/L 20 110 60-140115 4 3020ND22.0 22.9
m&p-Xylene ug/L 40 108 60-140113 5 3040ND43.2 45.3
Methyl-tert-butyl ether ug/L 20 118 60-140124 5 30201.9 25.5 26.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1512569MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92259099002
1512570
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 117 60-140124 5 3020ND23.4 24.7
n-Butylbenzene ug/L 20 94 60-140104 10 3020ND18.7 20.8
n-Propylbenzene ug/L 20 110 60-140117 6 3020ND22.0 23.4
Naphthalene ug/L 20 108 60-140107 1 3020ND21.6 21.4
o-Xylene ug/L 20 109 60-140114 4 3020ND21.8 22.8
sec-Butylbenzene ug/L 20 108 60-140118 8 3020ND21.7 23.6
Styrene ug/L 20 92 60-14094 3 3020ND18.3 18.8
tert-Butylbenzene ug/L 20 92 60-14096 5 3020ND18.3 19.2
Tetrachloroethene ug/L 20 103 60-140108 5 3020ND20.5 21.6
Toluene ug/L 20 112 60-140116 4 3020ND22.5 23.3
trans-1,2-Dichloroethene ug/L 20 117 60-140130 10 3020ND23.5 26.0
trans-1,3-Dichloropropene ug/L 20 86 60-14091 6 3020ND17.1 18.2
Trichloroethene ug/L 20 108 60-140114 5 3020ND21.6 22.8
Trichlorofluoromethane ug/L 20 107 60-140113 5 3020ND21.4 22.5
Vinyl chloride ug/L 20 118 60-140128 8 3020ND23.5 25.6
1,2-Dichloroethane-d4 (S)%105 70-130105
4-Bromofluorobenzene (S)%99 70-13098
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92259124
ONE STOP STORE #2
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92259124001 MSV/32632GMW-2 SM 6200B
92259124002 MSV/32632GMW-7 SM 6200B
92259124003 MSV/32632MW-10 SM 6200B
92259124004 MSV/32632MW-11 SM 6200B
92259124005 MSV/32632MW-12 SM 6200B
92259124006 MSV/32632MW-13 SM 6200B
92259124007 MSV/32634MW-14 SM 6200B
92259124008 MSV/32632MW-15 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 08:30 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 32
Page 31 of 32
Page 32 of 32