MO-86246_86246_CA_MRP_20231103_Reinhardt Heating & Air

CES of NC, PLLC
1701 Shenandoah Ave NW
Roanoke, Virginia 24017
540.343.6256 [office]
540.343.6259 [facsimile]

November 3, 2023

Mr. Ryan Mills
North Carolina Department of Environmental Quality
DWM/UST Section
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115

RE: 2023 Groundwater Monitoring Report
Reinhardt Heating and Air Conditioning (Energy Dispatch)
3003 Highway 27 East
Lincolnton, Lincoln County, North Carolina
NCDEQ AST Incident No: 86246

Dear Mr. Mills:

Enclosed please find one copy of the Annual 2023 Groundwater Monitoring Report completed by CES of
NC, PLLC on behalf of Energy Dispatch, LLC. The report was prepared in accordance with North Carolina
Department of Environmental Quality (NCDEQ) directives and is being delivered to the NCDEQ
Mooresville Regional Office. Should you have questions regarding the enclosed material, or if additional
information is required, please feel free to contact the undersigned at [phone].

Best Regards,

Marshall Adam Flora Daniel J. Fisher, PMP
Senior Project Manager Operations Manager

Enclosure

cc: Energy Dispatch, LLC

2023 GROUNDWATER MONITORING REPORT

Site Information

Date of Report: November 3, 2023

Site Identification
Site Name: Reinhardt Heating and Air Conditioning (Energy Dispatch)
Street Address: 3003 Highway 27 East
Lincolnton, North Carolina
County: Lincoln
Facility I.D.: NA AST Incident Number: 86246 AST Number: NA
Risk Rank:
Latitude: 35°28'53.9"N Longitude: 81°11'42.5"W Source: Google Earth
Description of Geographical Data Point: SE corner of building

Site Contact Information
Responsible Party: Energy Dispatch, LLC
Address: 3225 Cumberland Blvd. Suite 100
Atlanta, Georgia 30309
Telephone: Not Available
Email: Not Available

Property Property
Owner: Reinhardt Heating & Air Inc Occupant: Reinhardt Heating and Air
Address: 3003 E Hwy 27 Conditioning
Lincolnton, North Carolina 28092 3003 Highway 27 East
Lincolnton, North Carolina
Telephone: Not Available Not Available

Consultant: CES of NC, PLLC State
Address: 1701 Shenandoah Ave NW License No. C-550
Roanoke, Virginia 24017
Telephone: [phone]
Email: [e-mail]

Analytical State
Laboratory: Pace Analytical Services, LLC Certification No. 5342
Address: 9800 Kincey Ave, Suite 100
Huntersville, NC 28078_
Telephone: [phone]
Email: [e-mail]

Release Information
Release Date: July 17, 2001
Estimated Quantity: Approximately 9,200-gallons
Cause of Release: Gasoline tanker truck overturned
Source of Release: Gasoline tanker truck

2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT i
TABLE OF CONTENTS
List of Figures ................................................................................................................................................ i
List of Tables ................................................................................................................................................. i
List of Appendices ......................................................................................................................................... i
1.0 Introduction ....................................................................................................................................... 1
1.1 Site Identification .......................................................................................................................... 1
1.2 Site Description ............................................................................................................................. 1
1.3 Site History ................................................................................................................................... 1
2.0 Receptor Survey ................................................................................................................................ 3
2.1 Water Supply Wells ...................................................................................................................... 4
2.2 Public Water Supplies ................................................................................................................... 4
2.3 Surface Water ................................................................................................................................ 4
2.4 Wellhead Protection Area ............................................................................................................. 4
2.5 Surrounding Land Use .................................................................................................................. 4
2.6 Subsurface Structures .................................................................................................................... 4
2.7 Regional Geology/Hydrology ....................................................................................................... 4
2.8 Deep Aquifers in the Coastal Plain Physiographic Province ........................................................ 4
3.0 Recent Site Activities ........................................................................................................................ 5
3.1 Groundwater Sampling ............................................................................................................. 5
3.2 Groundwater Occurrence & Flow Direction ............................................................................. 5
3.3 Analytical Results ..................................................................................................................... 5
3.4 Investigative Derived Waste ..................................................................................................... 6
3.5 Quality Assurance & Quality Control ....................................................................................... 6
4.0 Groundwater Monitoring Report Summary ...................................................................................... 6
5.0 Statements and Certification .............................................................................................................. 7

LIST OF FIGURES
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Potential Receptor Location Map
Figure 4A Potentiometric Map (3/30/2023)
Figure 4B Potentiometric Map (10/19/2023)
Figure 5 Analytical Results Map (2023)

LIST OF TABLES
Table 1 Summary of Soil Analytical Results
Table 2 Summary of Water Supply Well Information
Table 3 Groundwater Elevation Data
Table 4 Summary of Groundwater Quality Data

LIST OF APPENDICES
Appendix A Groundwater Sampling Logs
Appendix B Laboratory Analytical Reports and Chain-of-Custody Documentation

2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT 1
1.0 INTRODUCTION
CES of NC, PLLC (CES) has completed this 2023 Groundwater Monitoring Report (GMR) to document
additional environmental assessment activities associated with a confirmed petroleum release from a
gasoline transport vehicle accident on State Highway 27 proximal to Lincolnton, North Carolina. This
report was prepared on behalf of Energy Dispatch, LLC in accordance with North Carolina Department of
Environmental Quality (NCDEQ) correspondence and is being delivered to the NCDEQ Mooresville, North
Carolina regional office.

1.1 SITE IDENTIFICATION
The incident area is located at 3003 NC Highway 27 East in Lincolnton, NC (site) as indicated on the
topographic site vicinity map included as Figure 1. The site is identified by the NCDEQ as Reinhardt
Heating and Air Conditioning and above-ground storage tank (AST) incident number 86246.

1.2 SITE DESCRIPTION
The site is in a mixed-use area within the jurisdictional limits of Lincolnton, North Carolina. The site is
improved with a one-story commercial building currently serving as Reinhardt Heating and Air
Conditioning, an active commercial service business. The site further is improved with a gravel
parking/access area and chain link fencing. The property is bordered to the west by Nandina Trail and to
the south by Highway 27. Residential properties border the subject site to the north and a commercial
storage unit facility borders the site to the east. A site map depicting pertinent features of the subject
property is provided as Figure 2.

1.3 SITE HISTORY
July 2001:
On July 17, 2001, a gasoline tanker truck traveling west on Highway 27 overturned proximal to the Reinhart
Heating & Air Conditioning facility. The truck came to rest on the north side of Highway 27 with a ruptured
gasoline storage tank. As a result, approximately 9,200-gallons of gasoline were discharge to the ground
surface. The release followed the topographic gradient to an ephemeral stream that discharged to Hoyle
Creek approximately 280-feet south of the release. As part of emergency response activities, a vacuum
truck was dispatched to the subject site and approximately 1,650-gallons of free-phase petroleum were
recovered.

December 2001:
As a result of the release, HEPACO, Inc. excavated approximately 175-tons of petroleum impacted material
from the southern drainage ditch trending Highway 27. The impacted material was transported off-site for
proper disposal and the excavation was backfilled with native fill material. Activities were reported to the
NCDEQ by Terraine, Inc. (Terraine) in a Soil Remediation Report dated March 11, 2002.

April 2003:
In accordance with North Carolina Department of Environment and Natural Resources (NCDENR),
directives (now known as the NCDEQ), Terraine completed a Comprehensive Site Assessment (CSA) at
the subject site. As part of the CSA, Terraine installed four (4) monitoring wells. Results of the subsequent
dissolved-phase sampling event yielded analytical results above groundwater quality standards defined in
Title 15A of the North Carolina Administrative Code, Subchapter 2L, Section .0202 (2L Standards),
however free product was not detected.

2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT 2
August 2003:
In response to data obtained during CSA activities, a Corrective Action Plan (CAP) was submitted to
NCDENR on August 22, 2003. Based on review of the CAP and subsequent pilot study, NCDENR
personnel requested that the remedial technique be modified to include periodic Mobile Multi-Phase
Extraction (MMPE) events followed by monitoring and natural attenuation. Site specific target levels
(SSTLs) also were established for benzene, toluene, ethylbenzene, and xylenes during the CAP phase.

February 2004 - July 2006:
In accordance with the modified CAP, Terraine conducted six (6) 90-hour MMPE events at the subject site.
The MMPE events performed at MW-1 consisted of a sustained negative pressure of approximately 21
inches of mercury (inHg) for a duration of 90-hours. Subsequent sampling events yielded the efficient and
effective removal of dissolved-phase contaminants.

August 2006:
During the August 2006 sampling event, Terraine personnel discovered an additional gasoline tanker had
overturned on August 30, 2006. Terraine personnel observed that emergency response measures were being
conducted by Spill Group, Inc. (Spill Group). Spill Group indicated that the resulting fire prohibited the
calculation of the actual volume released/discharged, however, the tanker reportedly was hauling
approximately 9,000-gallons of gasoline. The tankers final location following the incident was immediately
west of the Reinhardt Heating and Air parcel. Monitoring well MW-3 was not able to be located during
subsequent monitoring events. It is presumed that monitoring well MW-3 was destroyed during the
previously mentioned emergency response excavation event.

May 2007
A seventh MMPE event was performed May 14 to 18, 2007 by Shamrock Environmental Corporation. Four
follow-up sampling events conducted three to fifty days post MMPE indicated exceedances of 2L
Standards.

July 2007 through May 2010
In accordance with the approved CAP, five groundwater monitoring events were performed to monitor for
natural attenuation. Exceedances of 2L Standards continued to persist in site monitoring wells.

August 2010:
In accordance with NCDENR directives, Terraine mobilized to the subject site on August 31, 2010 to install
monitoring well MW-1R. Monitoring well MW-1R was installed following evidence that MW-1 had been
destroyed prior to a groundwater monitoring event that occurred in April 2010.

April 2011:
In accordance with the approved CAP, Terraine mobilized to the subject site to perform a groundwater
monitoring event. Terraine collected groundwater samples from monitoring wells MW-1R, MW-2, and
MW-4. Terraine was unable to locate monitoring well MW-3, therefore a sample was not collected. Results
of the analytical results yielded multiple 2L Standard violations, however, xylenes observed in the sample
collected from MW-1R were the only compound that exceeded the SSTLs.

October & November 2012:
In accordance with the approved work plan, CES initiated chemical and biological injections on October
22, 2012 to stimulate in-situ biodegradation of the observed contaminants. As part of corrective action
activities, CES installed four (4) injection wells and injected approximately 5,700-gallons of chemical and
biological amendments. Subsequent groundwater monitoring performed on November 15, 2012 indicated
significant reduction of dissolved-phase compounds in monitoring well MW-1R.
2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT 3
January through April 2013:
In accordance with the approved work plan, CES remobilized to the subject site on January 7, 2013 to
perform an additional biological injection. As part of corrective action activities, CES injected
approximately 2,250-gallons of biological amendments. Post injection groundwater monitoring performed
on January 30, 2013 indicated a substantial decrease in dissolved-phase compounds in monitoring well
MW-1R. An additional groundwater monitoring event performed on April 26, 2013 indicated relatively
static concentrations of dissolved-phase compounds when compared to the previous monitoring event.

July & August 2013:
In accordance with the approved work plan, CES remobilized to the subject site to perform an additional
chemical oxidation injection event. As part of corrective action activities, CES injected approximately
2,200-gallons of a 3.0 – 5.0% hydrogen peroxide solution to the network of injection wells. Post injection
groundwater monitoring performed on August 22, 2013 indicated a decrease on dissolved-phase
compounds. As noted in the October 29, 2013 Groundwater Monitoring Report, additional source area
remediation would no longer be possible due to construction of a stormwater retention pond proximal to
the former release area associated with a road widening project for Highway 27. In preparation of this
project, monitoring well MW-1R and injection wells IN-1, IN-2, IN-3, and IN-4 were properly abandoned.

August 2015 through December 2018:
Three groundwater monitoring events were performed on roughly an annual basis utilizing the only
remaining site monitoring well (MW-2) and/or nearby water supply wells WSW-1 and WSW-2. No
exceedances of 2L Standards were reported. Following completion of the Highway 27 road widening
project, replacement of monitoring wells MW-1R and MW-4 was suggested.

July 2020:
After approval of an encroachment permit by the NC Department of Transportation (NCDOT) and issuance
of well permits by the NCDEQ Division of Water Resources (DWR), CES installed two replacement
groundwater monitoring wells (MW-1R2 and MW-4R) on July 8, 2020. Soil samples collected during
installation of the monitoring wells indicated exceedances of the NCDEQ Soil-to-Groundwater maximum
soil contaminant concentrations (MSCCs), but no exceedances of the Residential Cleanup Level MSCCs
were reported as summarized in Table 1. Groundwater sampling was performed on July 9, 2020 and
indicated exceedances of 2L Standards, with total xylenes exceeding the SSTLs. An additional MMPE
event was recommended to remediate contaminated groundwater to concentrations below the SSTLs.

June 2022:
A groundwater sampling event was conducted on June 28, 2022. Laboratory analysis of the groundwater
sample collected from monitoring well MW-1R2 continued to yield results above the 2L Standards;
however, only the total xylenes concentration exceeded the SSTL. In addition, laboratory analysis of
groundwater samples collected from MW-2, MW-4R, WSW-1, and WSW-2 were either below laboratory
reporting limits or below 2L Standards.

2.0 RECEPTOR SURVEY
CES evaluated potential receptors based on historically available information and current site conditions as
discussed below. Historically, Terraine completed receptor survey activities as part of CSA activities. In
addition to site reconnaissance performed on August 9, 2012, CES personnel have completed windshield
surveys during subsequent site visits to identify potential receptors located within a 1,000-foot radius of the
subject property and provided updated receptor information as required. CES confirmed the presence of
potential receptors located within the search radius.
2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT 4
2.1 WATER SUPPLY WELLS
Visual inspections were performed for evidence indicating the presence of supply wells/springs. Six (6)
water supply wells have been identified within 1,500 feet of the site as summarized in Table 2 and shown
on Figure 3. Note that not all identified supply wells are operational.

2.2 PUBLIC WATER SUPPLIES
Municipal water service is available to the vicinity of the site by the Lincoln County Department of Public
Works under Public Water System ID NC 01-55-035. The source of water is surface water from Lake
Norman which is part of the Catawba River basin. No public water supply intakes are located near the site.

2.3 SURFACE WATER
The nearest natural surface water body is an unnamed tributary of Hoyle Creek located approximately 300-
feet west of the site. An intermittent drainage ditch is located immediately adjacent to the west of the site
which also appears to drain into the unnamed tributary of Hoyle Creek.

2.4 WELLHEAD PROTECTION AREA
According to the North Carolina Division of Water Quality, the site is not located within an approved
wellhead protection area as defined by 42 USC 300h-7(e).

2.5 SURROUNDING LAND USE
Land use in the vicinity of the site is primarily residential and commercial. Single family homes are located
sporadically in the area with primarily commercial development along the NC Highway 27 corridor.
Owners and occupants of adjacent properties have been provided in previous submittals.

2.6 SUBSURFACE STRUCTURES
Numerous subsurface utilities are buried in the surrounding area including electric, municipal water, storm
sewer, and communications as shown on Figure 2. The burial depths of the subsurface utilities are not
expected to intercept the water table. No subsurface structures such as basements or utility vaults have been
identified in the vicinity of the release.

2.7 REGIONAL GEOLOGY/HYDROLOGY
Based on the published 1985 Geologic Map of North Carolina, the site is located within the Kings Mountain
Belt of the Piedmont Physiographic Province. More specifically, the site is underlain by the Blacksburg
Formation characterized primarily by metamorphic rocks which consist of sericite schist, graphite, phyllite,
quartzite, banded marble, amphibolite, and minor calc-silicate rock.

In the piedmont, groundwater is generally accumulated from direct precipitation. Saturated conditions
typically occur in the undisturbed primary permeability within the saprolite weathered from the parent
bedrock. Groundwater also occurs within secondary permeability of the crystalline bedrock through joints,
fractures, and cleavage plains. Groundwater recharge occurs in interstream areas, while discharge is into
streams, lakes, and mash areas.

2.8 DEEP AQUIFERS IN THE COASTAL PLAIN PHYSIOGRAPHIC PROVINCE
The site is not located within the Coastal Plain Physiographic Province.

2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT 5
3.0 RECENT SITE ACTIVITIES
CES performed groundwater monitoring events at the subject site in March 2023 and in October 2023 in
accordance with NCDEQ directives.

3.1 GROUNDWATER SAMPLING
CES mobilized to the site on March 30, 2023 and October 19, 2023 for collection of groundwater samples
from monitoring wells MW-1R2, MW-2, and MW-4R. Depth to water and total well depth in each
monitoring well were measured with an electronic oil/water interface probe. Prior to sampling, a minimum
of three well volumes were purged from each well using a dedicated, disposable PVC bailer and nylon cord.
The bailer was gently lowered into the well and allowed to fill with water, then raised to the surface and
evacuated. This process was repeated until the necessary volume of water had been removed. During
purging activities, groundwater physical parameters were recorded by a calibrated groundwater multi-
parameter meter at regular intervals. Purge volumes, sample times, and physical parameters recorded during
the sampling events are included on the groundwater sampling logs provided in Appendix A. Groundwater
samples were also collected from water supply wells WSW-1 and WSW-2 following purging the supply
wells for a minimum of 10 minutes.

Subsequent to purging the necessary volume of water, groundwater samples were slowly poured from the
bailer into laboratory provided containers pre-filled with appropriate preservatives, labeled with indelible
ink, entered into chain-of-custody, and immediately placed on wet ice in a chilled cooler maintained at
approximately 4° C. The samples were transported under chain-of-custody protocol and submitted to Pace
Analytical Services, LLC in Huntersville, NC and Pace Analytical National in Mount Juliet, TN for
chemical analysis. The groundwater samples were analyzed for VOCs by Standard Methods 8260/6200,
polyaromatic hydrocarbons (PAHs) by Standard Methods 8270, and VPH aliphatic and aromatic carbon
chain fractions by MADEP methods.

3.2 GROUNDWATER OCCURRENCE & FLOW DIRECTION
On March 30, 2023, measured depth to water in the site monitoring wells ranged from 3.87-feet below top
of casing (TOC) in MW-2 to 8.05-feet below TOC in MW-1R2. Groundwater elevations were calculated
to range from 90.78-feet in monitoring well MW-1R2 to 96.42-feet in monitoring well MW-2. Based on
this data, shallow groundwater flow direction was interpreted to trend towards the southwest as shown on
Figure 4A. Groundwater gauging and elevation data is summarized in Table 3.

On October 19, 2023, measured depth to water in the site monitoring wells ranged from 15.40-feet below
top of casing (TOC) in MW-4R to 15.81-feet below TOC in MW-1R2. Groundwater elevations were
calculated to range from 83.02-feet in monitoring well MW-1R2 to 84.69-feet in monitoring well MW-2.
Based on this data, shallow groundwater flow direction was interpreted to trend towards the west-southwest
as shown on Figure 4B. Groundwater gauging and elevation data is summarized in Table 3.

3.3 ANALYTICAL RESULTS
Groundwater analytical results were compared to the 2L Standards and previously determined SSTLs. The
March 2023 and October 2023 laboratory analytical reports are provided in Appendix B with groundwater
analytical detections summarized in Table 4. Groundwater analytical results from 2023 are also illustrated
on Figure 5. Results flagged with a “J” indicate that the analyte was positively identified but the
concentration was between the method detection limit and laboratory reporting limit, therefore those values
are estimated. Further, results flagged with a “B” indicate that the same analyte was positively identified in
the associated blank.

2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT 6
Laboratory analysis of groundwater samples collected during March 2023 and October 2023 from MW-
1R2 and WSW-1 yielded VOC concentrations above 2L Standards. However, the groundwater samples
collected from MW-2, MW-4R, and WSW-2 were reported to be below laboratory reporting limits or below
the 2L Standards. Further, no exceedances to the SSTLs were observed during the March 2023 or October
2023 sampling events. Following receipt of the October 2023 laboratory analytical report, CES reported
the limited VOC concentrations within WSW-1 to the property owner and the NCDEQ case manager on
November 1, 2023. WSW-1 provides water to the Bodylines Towing & Auto Body Repair (Former Downs
Garage) facility addressed as 3010 Highway 27 East in Lincolnton, NC. The property owner confirmed
WSW-1 is used to provide water to a bathroom and the well is not utilized for potable water. Please note,
laboratory analysis of the October 2023 groundwater samples yielded measurable C9-C10 aromatics in
MW-1R2, MW-2, MW-4R, WSW-1, and WSW-2. However, these results were flagged with B qualifiers
indicating C9-C10 aromatics were observed in the method blank.

3.4 INVESTIGATIVE DERIVED WASTE
Purge water generated from the monitoring wells was disposed of on permeable surfaces near the well of
generation as a deemed permitted waste in accordance with NCDEQ guidelines.

3.5 QUALITY ASSURANCE & QUALITY CONTROL
To reduce the potential of cross contamination, dedicated disposable nitrile gloves were worn during all
phases of soil and groundwater sample handling. Field monitoring equipment such as water quality
instruments were calibrated to manufacturer specifications prior to each day of use. All samples were
maintained under strict chain-of-custody protocol as documented in Appendix B.

As part of CES’s quality assurance and quality control (QA/QC) measures, a data review of the laboratory
reports was conducted. During the review, it was found that the samples were received by the laboratory in
acceptable condition and properly preserved. The samples were analyzed within applicable holding times
and the chain-of-custody was properly completed by all parties. The laboratory QC reports show that
internal blanks were analyzed for each method that was used for the original samples. The laboratory
method blank, laboratory control sample, and associated matrix spike and matrix spike duplicate data results
were also provided for each analytical method. Refer to Appendix B for details regarding QA results for
the laboratory samples and any noted exceptions. Overall, CES concludes that the laboratory results are of
sufficient quality for use in this assessment and any exceptions do not significantly impact the conclusions
presented in this report.

4.0 GROUNDWATER MONITORING REPORT SUMMARY
Laboratory analytical results from the March 2023 and October 2023 groundwater sampling events
exceeded 2L Standards; however, no exceedances were observed above the SSTLs. In fact, exceedances to
the SSTLs have not been observed at the subject site since June 2022. It should be noted, limited VOC
concentrations were observed within offsite supply well WSW-1 during the 2023 sampling events;
however, WSW-1 reportedly only provides water to a bathroom and is not utilized for potable water. The
presence of VOCs in WSW-1 was reported to the property owner and the NCDEQ on November 1, 2023.
Based on the information presented in this report and the lack of exceedances to groundwater SSTLs for
over one (1) year, CES recommends closure of Incident 86246 by filing a Notice of Residual Petroleum for
the site and public notice.

2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT 7
5.0 STATEMENTS AND CERTIFICATION

1 Enter the date the monitoring report was due. No established due date Will this report be
submitted after the established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain what was
missing and why.

3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the
Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and outline
proposed remedies. (This should be described in more detail in the report text above.)
Not applicable, milestones have not been determined for the site.

4 Does any known or suspected source zone soil contamination or free product remain outside of the
assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #6 or #7 is “YES”, generally describe in this cell any actions recommended to
further assess or clean up this known or suspected source. (This should be described in more detail in the report text
above.)
6 Certification:
I Rachel A. Raines, a Licensed Geologist for CES of NC, PLLC, do certify that the information contained in this report
is correct and accurate to the best of my knowledge.

Rachel A. Raines, L.G.
Geologist
NC Licensed Geologist #2739

CES of NC, PLLC. is licensed to practice geology in North Carolina. The certification number of the company or
corporation is C-550.

2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT

FIGURES

FIGURE 1
Site Location Map
Reinhardt Heating and Air (Energy Dispatch)
3003 NC-27
Lincolnton, North Carolina
Lincolnton, North Carolina Project: 2023 Groundwater
Monitoring Report
Client: Racetrac Petroleum
CES NC Job #: 7.0914
Date: 11/2/2023
Latitude:
35°28'54.3"N
Longitude:
81°11'42.4"W
U.S.G.S Topographic Map of the
Lincolnton East Quadrangle, North
Carolina, 7.5 Minute Series (2019)
Scale: 1:24,000 Contour Interval: 20 Feet
Source:
National Geodetic Vertical
Datum 1988
Horizontal Datum:North American Datum 1983
Vertical Datum:
5104 Reagan Drive, Suite 7
Charlotte, NC 28206
540-343-6256 (office) 540-343-6259 (fax)
Site Location
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C
C
C
C C
MW-1R
WM
W
W
WSW-1
0 20'40'80'
1 inch equals 40 feet
Reinhardt Heating and Air (Energy Dispatch)
Site Map
2023 Groundwater Monitoring Report
Figure 23003 NC-27
Lincolnton, North Carolina
Racetrac Petroleum
Legend
Monitoring Well Location
Former Well Location
Approximate Property Lines
Approximate Right-of-Way Line
Overhead Electric Line
Underground Electric Line
Communications Line
Water Line
Storm Sewer Line
Fence
Utility Pole
Storm Drain
CLIENT:
LOCATION:
x
ROW
C
W
5104 Reagan Drive, Suite 7
Charlotte, NC 28206
540-343-6256 (office) 540-343-6259 (fax)
FIGURE 3
Potential Receptors Map
Reinhardt Heating and Air (Energy Dispatch)
3003 NC-27
Lincolnton, North Carolina
Legend
Client: Racetrac Petroleum
CES NC Job #: 7.0914
Date: 11/2/2023
Water Supply Well Location
Creek
0 175'350'700'
1 inch equals 350 feet
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
WSW-6
1,000-feet
Site
Project: 2023 Groundwater
Monitoring Report
x
x
x x x x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
Reinhardt
Heating
and Air
Downs
Garage
Self
Storage
Facility
NC-27
Su
n
n
y

H
i
l
l

D
r
i
v
e
Na
n
d
i
n
a

T
r
a
i
l
NC-27
MW-2
MW-1
MW-3
IN-1
IN-2 IN-3
IN-4
Dit
c
h
Dit
c
h
Cu
l
v
e
r
t
Sig
n
gravel
parking area
grass
grass
grass
grass
grass
grass
MW-4
MW-1R2
MW-4R
gate
edge of p
a
v
e
m
e
n
t
edge of pa
v
e
m
e
n
t
edge of p
a
v
e
m
e
n
t
edge of pa
v
e
m
e
n
t
edge of pave
m
e
n
t
edge of pavement
ROW
ROW
ROW
ROW
ROW
septic
tank
MW-1R
WM
WSW-1
0 20'40'80'
1 inch equals 40 feet
Reinhardt Heating and Air (Energy Dispatch)
Potentiometric Map (3/30/2023)
Figure 4A3003 NC-27
Lincolnton, North Carolina
Racetrac Petroleum
Legend
Monitoring Well Location
Former Well Location
Approximate Property Lines
Approximate Right-of-Way Line
Fence
Utility Pole
Storm Drain
Groundwater Elevation (feet)
Groundwater Elevation Contour
Groundwater Flow Direction
CLIENT:
LOCATION:
x
ROW
(94.38)
2023 Groundwater Monitoring Report
(90.78)
(96.42)
(92.24)
91.00
92.00
93.00
94.00
95.00
96.00
91.00
92.00
93.00
94.00
95.00
96.00
x
x
x x x x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
Reinhardt
Heating
and Air
Downs
Garage
Self
Storage
Facility
NC-27
Su
n
n
y

H
i
l
l

D
r
i
v
e
Na
n
d
i
n
a

T
r
a
i
l
NC-27
MW-2
MW-1
MW-3
IN-1
IN-2 IN-3
IN-4
Dit
c
h
Dit
c
h
Cu
l
v
e
r
t
Sig
n
gravel
parking area
grass
grass
grass
grass
grass
grass
MW-4
MW-1R2
MW-4R
gate
edge of p
a
v
e
m
e
n
t
edge of pa
v
e
m
e
n
t
edge of p
a
v
e
m
e
n
t
edge of pa
v
e
m
e
n
t
edge of pave
m
e
n
t
edge of pavement
ROW
ROW
ROW
ROW
ROW
septic
tank
MW-1R
WM
WSW-1
0 20'40'80'
1 inch equals 40 feet
Reinhardt Heating and Air (Energy Dispatch)
Potentiometric Map (10/19/2023)
Figure 4B3003 NC-27
Lincolnton, North Carolina
Racetrac Petroleum
Legend
Monitoring Well Location
Former Well Location
Approximate Property Lines
Approximate Right-of-Way Line
Fence
Utility Pole
Storm Drain
Groundwater Elevation (feet)
Groundwater Elevation Contour
Groundwater Flow Direction
CLIENT:
LOCATION:
x
ROW
(94.38)
2023 Groundwater Monitoring Report
(83.02)
(84.69)
(84.09)
84.50
84.00
83.50
84.50
84.00
83.50
x
x
x x x x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
Reinhardt
Heating
and Air
Downs
Garage
Self
Storage
Facility
NC-27
Su
n
n
y

H
i
l
l

D
r
i
v
e
Na
n
d
i
n
a

T
r
a
i
l
NC-27
MW-2
MW-1
MW-3
IN-1
IN-2 IN-3
IN-4
Dit
c
h
Dit
c
h
Cu
l
v
e
r
t
Sig
n
gravel
parking area
grass
grass
grass
grass
grass
grass
MW-4
MW-1R2
MW-4R
gate
edge of p
a
v
e
m
e
n
t
edge of pa
v
e
m
e
n
t
edge of p
a
v
e
m
e
n
t
edge of pa
v
e
m
e
n
t
edge of pave
m
e
n
t
edge of pavement
ROW
ROW
ROW
ROW
ROW
septic
tank
MW-1R
WM
WSW-1
0 20'40'80'
1 inch equals 40 feet
Reinhardt Heating and Air (Energy Dispatch)
Analytical Results 2023
Figure 53003 NC-27
Lincolnton, North Carolina
Racetrac Petroleum
Legend
Monitoring Well Location
Former Well Location
Approximate Property Lines
Approximate Right-of-Way Line
Fence
Utility Pole
Storm Drain
CLIENT:
LOCATION:
x
ROW
Groundwater
Data in ug/L (micrograms per Liter)
Bold indicates exceedance of 2L Standard
Shading indicates exceedance of SSTL
2023 Groundwater Monitoring Report
WSW-2 located
approximately 250
feet south-southwest
of WSW-1
2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT

TABLES

MW-1R2-5 MW-1R2-11 MW-1R2-15 MW-4R-5 MW-4R-13 MW-4R-15
7/8/2020 7/8/2020 7/8/2020 7/8/2020 7/8/2020 7/8/2020
5 11 15 5 13 15
STW Residential Ind/Comm
68 939 24,528 104 202 51.9 <7.90 <19.8 <10.2
540 1,500 40,000 76.7 115 82.2 <7.90 <19.8 <10.2
31 469 12,264 69.7 123 80.5 <7.90 <19.8 3.46 J
24 14,000 3.6 E5 <0.29 <0.74 0.086 J <0.23 <0.24 0.32 J
0.0056 18 164 <0.015 <0.037 <0.0011 <0.012 <0.012 <0.019
16 9,385 245,280 0.22 J <0.74 <0.22 <0.012 0.11 J 0.29 J
4.9 1,560 40,000 0.22 3.6 0.20 0.013 <0.012 <0.019
1.7 1,564 40,880 <0.015 0.51 <0.011 <0.012 <0.012 <0.019
0.12 100 4,000 0.092 <0.037 <0.011 <0.012 <0.012 <0.019
0.02 85 763 0.024 J <0.15 <0.044 <0.047 <0.049 <0.019
0.091 350 3,100 <0.015 <0.037 <0.011 <0.012 <0.012 <0.019
0.16 313 8,176 0.31 2.2 1.0 <0.012 <0.012 <0.019
1.7 626 16,350 0.31 <0.037 <0.011 <0.012 <0.012 <0.019
4.3 1,200 32,000 <0.015 <0.037 <0.011 0.026 0.016 0.019
8.5 782 20,440 2.6 16.5 7.7 0.015 0.012 0.024
8.3 782 20,440 0.83 5.0 2.2 <0.012 <0.012 <0.019
4.6 3,129 81,760 0.82 8.6 0.90 0.054 0.042 0.044
TABLE 1
SUMMARY OF SOIL ANALYTICAL RESULTS
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
Acetone
Benzene
2-Butanone (MEK)
C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C10 Aromatics
Isopropylbenzene (Cumene)
p-Isopropyltoluene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Analytical
Method
INCIDENT NO. 86246
mg/kg
EPA
Method
8260
Analyte
NCDEQ MSCC's
Sample ID
Sample Date
Sample Depth (ft BGS)
MADEP
VPH
Xylenes, Total
Toluene
Methylene Chloride
Methyl-tert Butyl Ether
Naphthalene
n-propylbenzene
Ethylbenzene
MW-1R2-5 MW-1R2-11 MW-1R2-15 MW-4R-5 MW-4R-13 MW-4R-15
7/8/2020 7/8/2020 7/8/2020 7/8/2020 7/8/2020 7/8/2020
5 11 15 5 13 15
STW Residential Ind/Comm
TABLE 1
SUMMARY OF SOIL ANALYTICAL RESULTS
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
Analytical
Method
INCIDENT NO. 86246
mg/kg
Analyte
NCDEQ MSCC's
Sample ID
Sample Date
Sample Depth (ft BGS)
8.2 940 24,000 0.0027 J <0.153 0.00062 J 0.00072 J <0.0131 <0.0144
11 469 12,264 <0.0138 <0.153 <0.0123 0.0013 J <0.0131 <0.0144
1,000 4,600 122,000 0.0011 J <0.153 <0.0123 0.0026 J <0.0131 <0.0144
0.34 0.88 8 <0.0138 <0.153 0.001 J 0.0099 J <0.0131 <0.0144
0.091 0.088 0.78 <0.0138 <0.153 0.0018 J 0.0089 J <0.0131 <0.0144
1.2 0.88 8 <0.0138 <0.153 0.0021 J 0.0136 <0.0131 <0.0144
6720 469 12,264 <0.0138 <0.153 0.0021 J 0.0071 J <0.0131 <0.0144
12 9 78 <0.0138 <0.153 0.00081 J 0.0071 J <0.0131 <0.0144
38 88 780 <0.0138 <0.153 0.0013 J 0.0104 J <0.0131 <0.0144
0.17 0.088 0.078 <0.0138 <0.153 <0.0123 0.0026 J <0.0131 <0.0144
276 620 16,400 0.0045 J <0.153 <0.0123 0.0194 <0.0131 <0.0144
44 620 16,400 0.0025 J 0.90 J 0.00056 J 0.001 J <0.0131 <0.0144
NE NE NE <0.0138 <0.153 0.0011 J 0.0058 J <0.0131 <0.0144
0.004 20 100 0.0801 0.063 0.0393 <0.0125 <0.0131 <0.0144
3.6 63 1,635 0.174 0.137 0.0862 <0.0125 <0.0131 <0.0144
0.16 313 8,176 0.229 0.264 0.11 <0.0125 <0.0131 <0.0144
56 469 12,264 0.0068 J <0.153 <0.0123 0.0115 J <0.0131 <0.0144
270 469 12,264 0.0033 J <0.153 0.0014 J 0.0166 <0.0131 <0.0144
Analytes not shown were below reporting limits in all samples. Refer to laboratory report for complete analytical suite.
MSCC = maximum soil contaminant concentration
STW = Soil-to-Groundwater
ft BGS = feet below ground surface
Results in mg/kg
J - Estimated value between method detection & reporting limits.
Bold face type indicates exceedance of most stringent regulatory limit.
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluorathene
Benzo(g,h,I)perylene
Benzo(k)fluoranthene
Dibenz(a,h)anthracene
ChryseneEPA
Method
8270
2-Methylnapthalene
Naphthalene
Phenanthrene
Pyrene
Indeno(1,2,3-cd)pyrene
1-Methylnapthalene
Fluoranthene
Fluorene
WELL ID PROPERTY OWNER PROPERTY ADDRESS MAILING ADDRESS WATER USE
DISTANCE
FROM
SOURCE AREA
(ft.)
WSW-1 Downs, Gilber 3010 E. HWY 27 3010 E. HWY 27 Potable (Inactive) 217 SE
WSW-2 Downs, Grayson 138 Lenhaven Trail 1905 Smith Farm Rd. Potable 586 SE
WSW-3 McGee, Pearl 152 Lenhaven Trail 331 Hill Road Potable 701 SE
WSW-4 McGee Todd 156 Lenhaven Trail 156 Lenhaven Trail Potable 813 SE
WSW-5 McGee David 158 Lenhaven Trail 158 Lenhaven Trail Potable 950 S
WSW-6 Dixon Beal 2921 E Hwy 27 2921 E Hwy 27 Disconnected 828 W
Unless otherwise noted, all addresses are located in Lincolnton, NC 28092
TABLE 2
SUMMARY OF WATER SUPPLY WELL INFORMATION
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
Well
Identification
Top of
Casing
Elevation1
(feet)
Screened
Interval Date
Depth to
Water
(feet)
Depth to
Free
Product
(feet)
Free-
Product
Thickness
(feet)
Groundwater
Elevation
9/3/2002 6.11 93.89
2/14/2003 4.99 95.01
10/21/2003 6.52 93.48
3/5/2004 5.05 94.95
5/27/2004 5.9 94.1
11/30/2004 4.55 95.45
3/4/2005 4.21 95.79
9/6/2005 8.5 91.5
7/10/2006 8.76 91.24
7/17/2006 9.92 90.08
7/31/2006 10.98 89.02
8/31/2006 5.49 94.51
2/15/2007 4.93 95.07
5/27/2007 6.81 93.19
6/5/2007 7.74 92.26
7/6/2007 9.73 90.27
2/27/2008 8.69 91.31
9/18/2008 8.4 91.6
2/17/2009 9.31 90.69
4/6/2010
9/7/2010 16 84.84
4/12/2011 5.49 95.35
6/5/2012 10.53 90.31
11/5/2012 14.07 86.77
1/30/2013 8.98 91.86
4/26/2013 7.63 93.21
8/22/2013 6.15 94.69
7/9/2020 9.45 89.38
11/16/2020 5.97 92.86
6/28/2022 13.67 85.16
3/30/2023 8.05 90.78
10/19/2023 15.81 83.02
TABLE 3
GROUNDWATER ELEVATION DATA
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
NA
NA
Abandoned 08/31/13
NA
NA
NA
NA
NA
NA
NA
NA
NA
Destroyed
MW-1R 100.84
MW-1 100
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
MW-1R2 98.83 5 - 20
NA
NA
NA
NA
Well
Identification
Top of
Casing
Elevation1
(feet)
Screened
Interval Date
Depth to
Water
(feet)
Depth to
Free
Product
(feet)
Free-
Product
Thickness
(feet)
Groundwater
Elevation
TABLE 3
GROUNDWATER ELEVATION DATA
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
2/14/2003 8.22 96.42
9/6/2005 10.48 94.16
7/31/2006 13.87 90.77
5/21/2007 9.21 95.43
6/5/2007 10.77 93.87
7/6/2007 12.71 91.93
2/27/2008 12.81 91.83
9/18/2008 12.53 92.11
2/17/2009 12.95 91.69
4/6/2010 6.20 98.44
6/5/2012 12.24 92.4
11/5/2012 16.36 88.28
1/30/2013 11.40 93.24
4/26/2013 9.63 95.01
8/22/2013 7.95 96.69
8/13/2015 10.24 94.40
11/23/2016 16.91 87.73
1/9/2018 15.22 89.42
7/9/2020 8.07 92.22
11/16/2020 4.84 95.45
6/28/2022 13.14 87.15
3/30/2023 3.87 96.42
10/19/2023 15.60 84.69
NA
NA
NA
NA
NA
NA
104.64
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
MW-2
100.29
NA
NA
NA
NA
NA
Well
Identification
Top of
Casing
Elevation1
(feet)
Screened
Interval Date
Depth to
Water
(feet)
Depth to
Free
Product
(feet)
Free-
Product
Thickness
(feet)
Groundwater
Elevation
TABLE 3
GROUNDWATER ELEVATION DATA
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
4/14/2003 10.31 92.04
3/4/2005 10.12 92.23
9/6/2005 12.09 90.26
7/31/2006 14.2 88.15
2/15/2007 NM NM
5/21/2007 NM NM
6/5/2007 NM NM
7/6/2007 NM NM
2/27/2008 NM NM
9/18/2008 NM NM
2/17/2009 NM NM
4/6/2010 NM NM
6/5/2012 NM NM
11/5/2012 NM NM
1/30/2013
8/22/2013
4/14/2003 3.49 79.2
3/4/2005 2.74 79.95
9/6/2005 7.01 75.68
7/31/2006 9.63 73.06
2/15/2007 3.61 79.08
5/21/2007 5.42 77.27
6/5/2007 6.78 75.91
7/6/2007 8 74.69
2/27/2008 5.96 76.73
9/18/2008 6.79 75.9
2/17/2009 7.27 75.42
4/6/2010 2.87 79.82
6/5/2012 NM NM
11/5/2012 NM NM
1/30/2013
8/22/2013
MW-3 102.35
MW-4 82.69
NA
NA
NA
NA
NA
NA
NA
Unable to Locate
Unable to Locate
Unable to Locate - Presumed Destroyed
NA
NA
NA
NA
Unable to Locate - Presumed Destroyed
NA
NA
NA
NA
NA
NA
NA
NA
NA
Unable to Locate
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Well
Identification
Top of
Casing
Elevation1
(feet)
Screened
Interval Date
Depth to
Water
(feet)
Depth to
Free
Product
(feet)
Free-
Product
Thickness
(feet)
Groundwater
Elevation
TABLE 3
GROUNDWATER ELEVATION DATA
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
7/9/2020 8.41 91.08
11/16/2020 2.38 97.11
6/28/2022 13.02 86.47
3/30/2023 7.25 92.24
10/19/2023 15.40 84.09
4/26/2013 7.94 NA
8/22/2013 6.54 NA
4/26/2013 8.09 NA
8/22/2013 6.52 NA
4/26/2013 8.58 NA
8/22/2013 6.72 NA
4/26/2013 8.23 NA
8/22/2013 5.81 NA
1. Historical elevations measured by CES on June 15, 2012, relative to the site elevation of 100.00 feet.
2020 elevations measured by CES on July 9, 2020 relative to storm sewer drop inlet grate east of MW-1R2 assigned an arbitrary elevation of 100.00-feet.
NA – Not applicable
NM - Not measured
NA
IN-4 NA
NAIN-3
IN-2 NA
NA
Abandoned 08/31/13
NA
NA
NA
NA
NA
Abandoned 08/31/13
Abandoned 08/31/13
NA
5 - 20
NA
5 - 20
MW-4R 99.49 5 - 20
NA
NA
NA
NAIN-1 5 - 20
5 - 20
Abandoned 08/31/13
NA
Sample
I.D.Sample Date
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1.0 600.0 600.0 500.0 0.02 70.0 70.0 70.0 70.0 NE 6.0 70.0 400.0 400.0 20.0 70.0 20.0 3.0 400.0 700.0 200.0 NA NA NA NA NA NA
4,500.0 10,000.0 4,650.0 7,400.0 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NA NA NA NA NA NA
2/14/2003 19,500 44,500 2,550 13,600 ND2 ND ND ND 55.0 ND 410.0 170.0 1,420.0 405.0 11,000.0 300.0 ND NA3 NA NA NA NA NA NA NA NA NA
3/4/2005 3,400 16,600 1,890 13,400 ND 56.9 13.6 ND 64.7 9.7 587.0 166.0 2,780.0 785.0 NA NA ND NA NA NA NA NA NA NA NA NA NA
9/6/2005 11,200 32,700 1,940 10,600 ND 40.5 ND 194.0 75.5 ND 448.0 174.0 1,690.0 462.0 2,840.0 86.5 ND NA NA NA NA NA NA NA NA NA NA
7/10/2006 886 2,700 1,050 5,510 ND ND ND ND 54.0 42.4 720.0 161.0 2,490.0 726.0 214.0 ND ND NA NA NA NA NA NA NA NA NA NA
7/17/2006 12,600 36,500 1,950 14,400 ND ND ND ND 36.0 19.6 538.0 133.0 1,820.0 484.0 3,120.0 NA ND NA NA NA NA NA NA NA NA NA NA
7/31/2006 4,940 15,700 641 14,100 ND ND ND ND 20.4 4.6 366.0 54.3 1,550.0 475.0 719.0 NA ND NA NA NA NA NA NA NA NA NA NA
8/31/2006 1,330 7,150 1,290 10,500 ND ND 8.6 ND 43.6 ND 634.0 123.0 2,680.0 898.0 384.0 8.9 ND NA NA NA NA NA NA NA NA NA NA
2/15/2007 1,010 2,090 1,140 5,510 ND ND ND ND 54.9 10.1 566.0 167.0 2,070.0 684.0 170.0 5.6 ND NA NA NA NA NA NA NA NA NA NA
5/21/2007 10,400 32,800 2,250 12,800 ND 37.1 9.2 ND 59.6 5.4 428.0 150.0 1,590.0 397.0 1,790.0 76.0 ND NA NA NA NA NA NA NA NA NA NA
6/5/2007 1,600 6,980 723 5,840 ND 49.8 ND ND 30.0 5.5 540.0 81.4 1,620.0 509.0 346.0 10.4 ND NA NA NA NA NA NA NA NA NA NA
7/6/2007 477 1,470 255 3,200 ND ND ND ND 11.4 16.8 329.0 31.8 1,240.0 365.0 181.0 ND ND NA NA NA NA NA NA NA NA NA NA
2/27/2008 150 376 648 3,860 ND 67.2 ND ND 40.7 9.3 462.0 113.0 2,200.0 676.0 42.5 ND ND NA NA NA NA NA NA NA NA NA NA
9/18/2008 393 1,210 892 5,790 ND 54.5 6.8 ND 40.4 7.5 732.0 115.0 2,210.0 619.0 63.3 1.9 ND NA NA NA NA NA NA NA NA NA NA
2/17/2009 155 105 730 2,340 ND ND 13.7 ND 43.1 ND 329.0 122.0 2,260.0 652.0 31.8 ND ND NA NA NA NA NA NA NA NA NA NA
4/6/2010 NS4 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS ND NA NS NS NS NA NA NA NA NA NA
6/5/2012 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS ND NA NS NS NS NA NA NA NA NA NA
11/5/2012 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS ND NA NS NS NS NA NA NA NA NA NA
9/7/2010 1,000 11,900 1,780 13,970 ND ND ND ND 53.3 ND 430.0 ND 2,170.0 494.0 80.0 ND ND 55.2 27,300.0 81,700.0 6,410.0 NA NA NA NA NA NA
4/12/2011 408 5,980 1,620 10,710 ND ND ND ND 33.6 ND 319.0 125.0 1,450.0 415.0 14.0 ND ND NA NA NA NA NA NA NA NA NA NA
6/5/2012 1,830 260 160 585.3 ND ND ND ND 20.0 ND 166.0 ND 389.0 144.0 266.0 8.7 ND NA NA NA NA NA NA NA NA NA NA
11/5/2012 26.0 60.0 88.0 370.0 ND 2.2 ND ND 1.9 ND 24.0 7.3 110.0 27.0 0.6 ND ND NA NA NA NA NA NA NA NA NA NA
4/26/2013 160 150 0.6 810.0 ND ND ND ND 1.1 ND 110.0 0.7 410.0 82.0 9.4 ND ND NA NA NA NA NA 460.0 <0.1 0.66 7.24 190
8/22/2013 24.0 21.0 17.0 147.0 ND 5.9 0.7 ND 3.4 1.4 17.0 5.5 120.0 54.0 6.4 0.19J ND NA NA NA NA NA 63.0 0.92j 4.3 NM 129.3
7/9/2020 596 2,110 2,220 11,890 <0.020 <20.0 <20.0 <20.0 56.1 NA 443 170 1,500 352 <20.0 <20.0 <20.0 NA 16,500 20,600 6,080 <5.0 NA NA 4.96 6.60 201
11/16/2020 24.0 282 1,150 4,900 <10.0 <10.0 <10.0 NA 60.9 <10.0 412 <10.0 1,860 <10.0 <10.0 <10.0 <10.0 NA 6,000 <100 6,210 NA NA NA 2.36 6.17 -52
6/28/2022 130 1,000 2,400 10,100 <40 <40 <40 <40 98 <40 650 330 3,000 750 <40 <40 <40 NA 17,000 15,000 10,000 NA NA NA NA NA NA
3/30/2023 99.1 545 1,790 5,400 <20.0 NA NA NA NA NA 517 NA NA NA <20.0 NA <20.0 NA 26,000 <2,000 9,400 NA NA NA 2.58 6.67 -67.8
10/19/2023 97.3 J 447 2,200 6,976 <12.6 68.2 J 18.5 J <12.7 85.5 J <12.0 556 351 2,740 686 <10.1 <10.5 <10.7 NA 15,600 11,200 9,900 B J NA NA NA NA NA NA
TABLE 4
SUMMARY OF GROUNDWATER QUALITY DATA
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
Unable to Locate - Presumed Destroyed
MW-1R
MW-1R2
SSTL
2L Standard
Abandoned 08/31/2013
MW-1
Sample
I.D.Sample Date
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m
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(
s
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OR
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(
m
V
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1.0 600.0 600.0 500.0 0.02 70.0 70.0 70.0 70.0 NE 6.0 70.0 400.0 400.0 20.0 70.0 20.0 3.0 400.0 700.0 200.0 NA NA NA NA NA NA
4,500.0 10,000.0 4,650.0 7,400.0 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NA NA NA NA NA NA
TABLE 4
SUMMARY OF GROUNDWATER QUALITY DATA
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
SSTL
2L Standard
2/14/2003 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
3/4/2005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
9/6/2005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
7/31/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
2/15/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
5/21/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.8 ND ND NA NA NA NA NA NA NA NA NA NA
6/5/2007 ND ND ND ND ND ND ND ND ND ND 13.4 ND 9.5 3.0 ND ND ND NA NA NA NA NA NA NA NA NA NA
7/6/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
2/27/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
9/18/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
2/17/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
4/6/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
4/12/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
6/5/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
11/5/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
4/26/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA ND ND 2.1 6.1 185.0
8/22/2013 ND 0.16 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA 0.4 2.8 2.5 NM 115.2
11/22/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NM NM
8/13/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NM NM
11/23/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NM NM
1/9/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NM NM
12/28/2018
7/9/2020 <0.50 <0.50 <0.50 <1.50 <0.020 <0.50 <0.50 <0.50 <0.50 NA <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA 38.3 J <100 <100 <5.0 NA NA 3.98 6.10 244
11/16/2020 <0.50 <0.50 <0.50 <1.50 <0.50 <0.50 <0.50 NA <0.50 NA <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <100 <100 <100 NA NA NA 0.55 5.98 30
6/28/2022 <0.40 <0.40 <0.40 <0.80 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 NA <15 <15 <5.0 NA NA NA NA NA NA
3/30/2023 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA <1.0 NA NA NA <1.0 NA <1.0 NA <100 <100 <100 NA NA NA 3.99 6.44 95.8
10/19/2023 <0.0941 <0.278 <0.137 <3.0 <0.126 <0.157 <0.125 <0.127 <0.105 <0.120 <1.0 <0.0993 <0.322 <0.104 <0.101 <0.105 <0.107 NA <33.3 <33.3 52.0 B J NA NA NA NA NA NA
MW-2
Not Sampled
Sample
I.D.Sample Date
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m
V
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1.0 600.0 600.0 500.0 0.02 70.0 70.0 70.0 70.0 NE 6.0 70.0 400.0 400.0 20.0 70.0 20.0 3.0 400.0 700.0 200.0 NA NA NA NA NA NA
4,500.0 10,000.0 4,650.0 7,400.0 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NA NA NA NA NA NA
TABLE 4
SUMMARY OF GROUNDWATER QUALITY DATA
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
SSTL
2L Standard
2/14/2003 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
3/4/2005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
9/6/2005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
7/31/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
2/15/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA
5/21/2007 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
6/5/2007 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
7/6/2007 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
2/27/2008 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
9/18/2008 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
2/17/2009 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
4/6/2010 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
4/12/2011 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
6/5/2012 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
11/5/2012 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
2/14/2003 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
3/4/2005 8.0 ND ND 14.0 ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
9/6/2005 9.7 ND ND 11.3 ND ND ND ND ND ND ND ND 3.0 ND 2.1 ND ND ND NA NA NA NA NA NA NA NA NA
7/31/2006 1.7 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
2/15/2007 4.3 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.0 ND ND ND NA NA NA NA NA NA NA NA NA
5/21/2007 1.5 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.4 ND ND ND NA NA NA NA NA NA NA NA NA
6/5/2007 1.3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
7/6/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
2/27/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
9/18/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
2/17/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
4/6/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
4/12/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA
6/5/2012 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
11/5/2012 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NA NA NA NA NA NA
Presumed Destroyed
MW-4
MW-3
Presumed Destroyed
Sample
I.D.Sample Date
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x
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n

(
m
g
/
L
)
pH

(
s
u
)
OR
P

(
m
V
)
1.0 600.0 600.0 500.0 0.02 70.0 70.0 70.0 70.0 NE 6.0 70.0 400.0 400.0 20.0 70.0 20.0 3.0 400.0 700.0 200.0 NA NA NA NA NA NA
4,500.0 10,000.0 4,650.0 7,400.0 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NA NA NA NA NA NA
TABLE 4
SUMMARY OF GROUNDWATER QUALITY DATA
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
SSTL
2L Standard
7/9/2020 1.6 1.3 1.2 1.47 <0.020 <0.50 0.73 <0.50 1.5 NA 0.69 J 1.4 <0.50 <0.50 1.3 <0.50 <0.50 NA 172 95.0 J <100 <5.0 NA NA 7.63 6.70 111
11/16/2020 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <100 <100 <100 NA NA NA 4.17 5.64 129
6/28/2022 0.64 <0.40 <0.40 <0.80 <0.40 <0.40 0.53 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 NA 93 <15 14 J NA NA NA NA NA NA
3/30/2023 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA <1.0 NA NA NA <1.0 NA <1.0 NA <100 <100 <100 NA NA NA 3.10 6.11 70.5
10/19/2023 0.785 J 0.365 J 0.148 J <3.0 <0.126 <0.157 0.585 J <0.127 0.326 J <0.120 <1.0 0.185 J <0.322 <0.104 0.385 J <0.105 <0.107 NA 128 <33.3 45.8 B J NA NA NA NA NA NA
8/22/2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 46.0 71.0 6.8 NM 140.8
4/26/2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1,000.0 ND 1.0 6.9 181.0
8/22/2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 360.0 270.0 2.6 NM 129.1
4/26/2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 190.0 ND 0.8 6.1 199.0
8/22/2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 93.0 470.0 1.8 NM 110.3
4/26/2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 66.0 0.63 1.2 6.17 253.00
8/22/2013 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 23.0 280.00 2.9 NM 107.90
11/22/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.8 NA NA NA NA NA NA NA NM NM NM
8/13/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NM NM NM
11/23/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.4 NA NA NA NA NA NA NA NM NM NM
1/9/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.6 NA NA NA NA NA NA NA NM NM NM
12/28/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.6 NA NA NA NA NA NA NA NM NM NM
7/9/2020
11/16/2020
6/28/2022 <0.40 <0.40 <0.40 <0.80 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 NA 21 J <15 <5.0 NA NA NA NA NA NA
3/30/2023 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA <1.0 NA NA NA 10.3 NA <1.0 NA <100 <100 <100 NA NA NA 5.92 6.35 53.0
10/19/2023 1.54 <0.278 <0.137 0.808 J <0.126 <0.157 <0.125 <0.127 0.267 J <0.120 <1.0 0.0994 J <0.322 <0.104 0.409 J <0.105 0.321 J NA <33.3 <33.3 51.1 B J NA NA NA NA NA NA
11/22/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NM NM NM
8/13/2015
11/23/2016
1/9/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NM NM NM
12/28/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NM NM NM
7/9/2020
11/16/2020 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 NA <0.50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <100 <100 <100 NA NA NA 0.62 7.04 137
6/28/2022 <0.40 <0.40 <0.40 <0.80 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 NA <15 <15 <5.0 NA NA NA NA NA NA
3/30/2023 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA <1.0 NA NA NA <1.0 NA <1.0 NA <100 <100 <100 NA NA NA 5.05 6.18 86.2
10/19/2023 <0.0941 <0.278 <0.137 <3.0 <0.126 <0.157 <0.125 <0.127 <0.105 <0.120 <1.0 <0.0993 <0.322 <0.104 <0.101 <0.105 <0.107 NA <33.3 <33.3 50.6 B J NA NA NA NA NA NA
Abandoned 08/31/2013
IN-1
IN-3
Abandoned 08/31/2013
Abandoned 08/31/2013
MW-4R
WSW-1
WSW-2
Not Sampled - Well Not in Operation
Unable to contact.
Not Sampled
Not Sampled
Unable to contact.
IN-2
IN-4
Abandoned 08/31/2013
Sample
I.D.Sample Date
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1.0 600.0 600.0 500.0 0.02 70.0 70.0 70.0 70.0 NE 6.0 70.0 400.0 400.0 20.0 70.0 20.0 3.0 400.0 700.0 200.0 NA NA NA NA NA NA
4,500.0 10,000.0 4,650.0 7,400.0 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NA NA NA NA NA NA
TABLE 4
SUMMARY OF GROUNDWATER QUALITY DATA
REINHARDT HEATING AND AIR
LINCOLNTON, LINCOLN COUNTY
INCIDENT NO. 86246
SSTL
2L Standard
All results reported in micrograms per liter (µg/L) unless otherwise noted.
1 VOCs, MTBE, & IPE analysis via Standard Method 6200B.
2 Non-Detect
3 Not Analyzed
4 Not Sampled
SSTL - Site Specific Target Level
*Total PAHs include: acenapthene, acenpahtylene, anthracene, benzo(a)anthracene, beno(a)pyrene, benzo(b)fluoranthene, benzo(g,h.i)perylene, benzo(k)fluoranthene, chrysene, dibenz(a,h)anthracene, fluoranthene, fluorene, ideno(1,2,3-cd)pyrene, phenanthrene, and pyrene via EPA Method 625. Value shown is maximum laboratory reporting limit.
EDB analysis July 2020 via EPA Method 504.1, November 2020 via SM 6200.
Aliphatics and aromatics carbon fractions via analytical method MADEP VPH.
Bold font indicates detection above laboratory reporting limit.
Bold Red font and highligted cell indicates detection above SSTL.
Dissolved oxygen, pH, & ORP collected in-situ by field instrumentation post 2020.
2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT

APPENDIX A
Groundwater Sampling Logs

2023 GROUNDWATER MONITORING REPORT
REINHARDT HEATING AND AIR CONDITIONING (ENERGY DISPATCH)
LINCOLNTON, NORTH CAROLINA
AST INCIDENT #86246

REINHARDT HEATING AND AIR CONDITIONING - 2023 GROUNDWATER MONITORING REPORT

APPENDIX B
Laboratory Analytical Report & Chain of Custody Documentation

#=CL#
April 18, 2023
LIMS USE: FR - DAN FISHER
LIMS OBJECT ID: 92659938
92659938
Project:
Pace Project No.:
RE:
Mr. Dan Fisher
Crawford Environmental Services, Inc.
15 Church Avenue, SW
Roanoke, VA 24011
RACE TRACK PETRO
Dear Mr. Fisher:
Enclosed are the analytical results for sample(s) received by the laboratory on March 31, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
cc:James Coleman, Crawford Environmental
Carol Goss, Crawford Environmental Services, Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 49
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 49
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92659938001 MW-1R EPA 8270E 21 PASI-CPKS
EPA 8260D 63 PASI-CTMH
92659938002 MW-2 EPA 8270E 21 PASI-CPKS
EPA 8260D 63 PASI-CTMH
92659938003 MW-4 EPA 8270E 21 PASI-CPKS
EPA 8260D 63 PASI-CTMH
92659938004 WSW-1 EPA 8270E 21 PASI-CPKS
EPA 8260D 63 PASI-CTMH
92659938005 WSW-2 EPA 8270E 21 PASI-CPKS
EPA 8260D 63 PASI-CTMH
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:MW-1R Lab ID:92659938001 Collected:03/30/23 11:35 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene ND ug/L 04/06/23 16:13 83-32-904/05/23 13:279.8 1
Acenaphthylene ND ug/L 04/06/23 16:13 208-96-804/05/23 13:279.8 1
Anthracene ND ug/L 04/06/23 16:13 120-12-704/05/23 13:279.8 1
Benzo(a)anthracene ND ug/L 04/06/23 16:13 56-55-304/05/23 13:279.8 1
Benzo(a)pyrene ND ug/L 04/06/23 16:13 50-32-804/05/23 13:279.8 1
Benzo(b)fluoranthene ND ug/L 04/06/23 16:13 205-99-204/05/23 13:279.8 1
Benzo(g,h,i)perylene ND ug/L 04/06/23 16:13 191-24-2 L104/05/23 13:279.8 1
Benzo(k)fluoranthene ND ug/L 04/06/23 16:13 207-08-904/05/23 13:279.8 1
Chrysene ND ug/L 04/06/23 16:13 218-01-904/05/23 13:279.8 1
Dibenz(a,h)anthracene ND ug/L 04/06/23 16:13 53-70-304/05/23 13:279.8 1
Fluoranthene ND ug/L 04/06/23 16:13 206-44-004/05/23 13:279.8 1
Fluorene ND ug/L 04/06/23 16:13 86-73-704/05/23 13:279.8 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/06/23 16:13 193-39-504/05/23 13:279.8 1
1-Methylnaphthalene 57.5 ug/L 04/06/23 16:13 90-12-004/05/23 13:279.8 1
2-Methylnaphthalene 115 ug/L 04/06/23 16:13 91-57-604/05/23 13:279.8 1
Naphthalene 482 ug/L 04/06/23 16:13 91-20-304/05/23 13:279.8 1
Phenanthrene ND ug/L 04/06/23 16:13 85-01-804/05/23 13:279.8 1
Pyrene ND ug/L 04/06/23 16:13 129-00-004/05/23 13:279.8 1
Surrogates
Nitrobenzene-d5 (S)118 %04/06/23 16:13 4165-60-004/05/23 13:2759-144 1
2-Fluorobiphenyl (S)86 %04/06/23 16:13 321-60-804/05/23 13:2757-152 1
Terphenyl-d14 (S)92 %04/06/23 16:13 1718-51-004/05/23 13:2710-162 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 624 ug/L 04/13/23 07:01 67-64-150020
Benzene 99.1 ug/L 04/13/23 07:01 71-43-220.0 20
Bromobenzene ND ug/L 04/13/23 07:01 108-86-120.0 20
Bromochloromethane ND ug/L 04/13/23 07:01 74-97-520.0 20
Bromodichloromethane ND ug/L 04/13/23 07:01 75-27-420.0 20
Bromoform ND ug/L 04/13/23 07:01 75-25-220.0 20
Bromomethane ND ug/L 04/13/23 07:01 74-83-940.0 20
2-Butanone (MEK)ND ug/L 04/13/23 07:01 78-93-310020
Carbon tetrachloride ND ug/L 04/13/23 07:01 56-23-520.0 20
Chlorobenzene ND ug/L 04/13/23 07:01 108-90-720.0 20
Chloroethane ND ug/L 04/13/23 07:01 75-00-320.0 20
Chloroform ND ug/L 04/13/23 07:01 67-66-320.0 20
Chloromethane 41.5 ug/L 04/13/23 07:01 74-87-320.0 20
2-Chlorotoluene ND ug/L 04/13/23 07:01 95-49-820.0 20
4-Chlorotoluene ND ug/L 04/13/23 07:01 106-43-420.0 20
1,2-Dibromo-3-chloropropane ND ug/L 04/13/23 07:01 96-12-840.0 20
Dibromochloromethane ND ug/L 04/13/23 07:01 124-48-120.0 20
1,2-Dibromoethane (EDB)ND ug/L 04/13/23 07:01 106-93-420.0 20
Dibromomethane ND ug/L 04/13/23 07:01 74-95-320.0 20
1,2-Dichlorobenzene ND ug/L 04/13/23 07:01 95-50-120.0 20
1,3-Dichlorobenzene ND ug/L 04/13/23 07:01 541-73-120.0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:MW-1R Lab ID:92659938001 Collected:03/30/23 11:35 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,4-Dichlorobenzene ND ug/L 04/13/23 07:01 106-46-720.0 20
Dichlorodifluoromethane ND ug/L 04/13/23 07:01 75-71-820.0 20
1,1-Dichloroethane ND ug/L 04/13/23 07:01 75-34-320.0 20
1,2-Dichloroethane ND ug/L 04/13/23 07:01 107-06-220.0 20
1,1-Dichloroethene ND ug/L 04/13/23 07:01 75-35-420.0 20
cis-1,2-Dichloroethene ND ug/L 04/13/23 07:01 156-59-220.0 20
trans-1,2-Dichloroethene ND ug/L 04/13/23 07:01 156-60-520.0 20
1,2-Dichloropropane ND ug/L 04/13/23 07:01 78-87-520.0 20
1,3-Dichloropropane ND ug/L 04/13/23 07:01 142-28-920.0 20
2,2-Dichloropropane ND ug/L 04/13/23 07:01 594-20-720.0 20
1,1-Dichloropropene ND ug/L 04/13/23 07:01 563-58-620.0 20
cis-1,3-Dichloropropene ND ug/L 04/13/23 07:01 10061-01-520.0 20
trans-1,3-Dichloropropene ND ug/L 04/13/23 07:01 10061-02-620.0 20
Diisopropyl ether ND ug/L 04/13/23 07:01 108-20-320.0 20
Ethylbenzene 1790 ug/L 04/13/23 07:01 100-41-420.0 20
Hexachloro-1,3-butadiene ND ug/L 04/13/23 07:01 87-68-340.0 20
2-Hexanone ND ug/L 04/13/23 07:01 591-78-610020
p-Isopropyltoluene ND ug/L 04/13/23 07:01 99-87-620.0 20
Methylene Chloride 461 ug/L 04/13/23 07:01 75-09-2 L1,v110020
4-Methyl-2-pentanone (MIBK)ND ug/L 04/13/23 07:01 108-10-110020
Methyl-tert-butyl ether ND ug/L 04/13/23 07:01 1634-04-420.0 20
Naphthalene 517 ug/L 04/13/23 07:01 91-20-320.0 20
Styrene ND ug/L 04/13/23 07:01 100-42-520.0 20
1,1,1,2-Tetrachloroethane ND ug/L 04/13/23 07:01 630-20-620.0 20
1,1,2,2-Tetrachloroethane ND ug/L 04/13/23 07:01 79-34-520.0 20
Tetrachloroethene ND ug/L 04/13/23 07:01 127-18-420.0 20
Toluene 545 ug/L 04/13/23 07:01 108-88-320.0 20
1,2,3-Trichlorobenzene ND ug/L 04/13/23 07:01 87-61-620.0 20
1,2,4-Trichlorobenzene ND ug/L 04/13/23 07:01 120-82-120.0 20
1,1,1-Trichloroethane ND ug/L 04/13/23 07:01 71-55-620.0 20
1,1,2-Trichloroethane ND ug/L 04/13/23 07:01 79-00-520.0 20
Trichloroethene ND ug/L 04/13/23 07:01 79-01-620.0 20
Trichlorofluoromethane ND ug/L 04/13/23 07:01 75-69-420.0 20
1,2,3-Trichloropropane ND ug/L 04/13/23 07:01 96-18-420.0 20
Vinyl acetate ND ug/L 04/13/23 07:01 108-05-440.0 20
Vinyl chloride ND ug/L 04/13/23 07:01 75-01-420.0 20
Xylene (Total)5400 ug/L 04/13/23 07:01 1330-20-720.0 20
m&p-Xylene 4510 ug/L 04/13/23 07:01 179601-23-140.0 20
o-Xylene 885 ug/L 04/13/23 07:01 95-47-620.0 20
Surrogates
4-Bromofluorobenzene (S)97 %04/13/23 07:01 460-00-4 HS70-130 20
1,2-Dichloroethane-d4 (S)98 %04/13/23 07:01 17060-07-070-130 20
Toluene-d8 (S)100 %04/13/23 07:01 2037-26-570-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:MW-2 Lab ID:92659938002 Collected:03/30/23 11:00 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene ND ug/L 04/06/23 16:39 83-32-904/05/23 13:279.6 1
Acenaphthylene ND ug/L 04/06/23 16:39 208-96-804/05/23 13:279.6 1
Anthracene ND ug/L 04/06/23 16:39 120-12-704/05/23 13:279.6 1
Benzo(a)anthracene ND ug/L 04/06/23 16:39 56-55-304/05/23 13:279.6 1
Benzo(a)pyrene ND ug/L 04/06/23 16:39 50-32-804/05/23 13:279.6 1
Benzo(b)fluoranthene ND ug/L 04/06/23 16:39 205-99-204/05/23 13:279.6 1
Benzo(g,h,i)perylene ND ug/L 04/06/23 16:39 191-24-2 L104/05/23 13:279.6 1
Benzo(k)fluoranthene ND ug/L 04/06/23 16:39 207-08-904/05/23 13:279.6 1
Chrysene ND ug/L 04/06/23 16:39 218-01-904/05/23 13:279.6 1
Dibenz(a,h)anthracene ND ug/L 04/06/23 16:39 53-70-304/05/23 13:279.6 1
Fluoranthene ND ug/L 04/06/23 16:39 206-44-004/05/23 13:279.6 1
Fluorene ND ug/L 04/06/23 16:39 86-73-704/05/23 13:279.6 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/06/23 16:39 193-39-504/05/23 13:279.6 1
1-Methylnaphthalene ND ug/L 04/06/23 16:39 90-12-004/05/23 13:279.6 1
2-Methylnaphthalene ND ug/L 04/06/23 16:39 91-57-604/05/23 13:279.6 1
Naphthalene ND ug/L 04/06/23 16:39 91-20-304/05/23 13:279.6 1
Phenanthrene ND ug/L 04/06/23 16:39 85-01-804/05/23 13:279.6 1
Pyrene ND ug/L 04/06/23 16:39 129-00-004/05/23 13:279.6 1
Surrogates
Nitrobenzene-d5 (S)108 %04/06/23 16:39 4165-60-004/05/23 13:2759-144 1
2-Fluorobiphenyl (S)81 %04/06/23 16:39 321-60-804/05/23 13:2757-152 1
Terphenyl-d14 (S)86 %04/06/23 16:39 1718-51-004/05/23 13:2710-162 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/13/23 06:26 67-64-125.0 1
Benzene ND ug/L 04/13/23 06:26 71-43-21.0 1
Bromobenzene ND ug/L 04/13/23 06:26 108-86-11.0 1
Bromochloromethane ND ug/L 04/13/23 06:26 74-97-51.0 1
Bromodichloromethane ND ug/L 04/13/23 06:26 75-27-41.0 1
Bromoform ND ug/L 04/13/23 06:26 75-25-21.0 1
Bromomethane ND ug/L 04/13/23 06:26 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/13/23 06:26 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/13/23 06:26 56-23-51.0 1
Chlorobenzene ND ug/L 04/13/23 06:26 108-90-71.0 1
Chloroethane ND ug/L 04/13/23 06:26 75-00-31.0 1
Chloroform ND ug/L 04/13/23 06:26 67-66-31.0 1
Chloromethane ND ug/L 04/13/23 06:26 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/13/23 06:26 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/13/23 06:26 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/13/23 06:26 96-12-82.0 1
Dibromochloromethane ND ug/L 04/13/23 06:26 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 04/13/23 06:26 106-93-41.0 1
Dibromomethane ND ug/L 04/13/23 06:26 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/13/23 06:26 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/13/23 06:26 541-73-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:MW-2 Lab ID:92659938002 Collected:03/30/23 11:00 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,4-Dichlorobenzene ND ug/L 04/13/23 06:26 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/13/23 06:26 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/13/23 06:26 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/13/23 06:26 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/13/23 06:26 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/13/23 06:26 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/13/23 06:26 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/13/23 06:26 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/13/23 06:26 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/13/23 06:26 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/13/23 06:26 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/13/23 06:26 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/13/23 06:26 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/13/23 06:26 108-20-31.0 1
Ethylbenzene ND ug/L 04/13/23 06:26 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/13/23 06:26 87-68-32.0 1
2-Hexanone ND ug/L 04/13/23 06:26 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/13/23 06:26 99-87-61.0 1
Methylene Chloride ND ug/L 04/13/23 06:26 75-09-2 L1,v15.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/13/23 06:26 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 04/13/23 06:26 1634-04-41.0 1
Naphthalene ND ug/L 04/13/23 06:26 91-20-31.0 1
Styrene ND ug/L 04/13/23 06:26 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/13/23 06:26 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/13/23 06:26 79-34-51.0 1
Tetrachloroethene ND ug/L 04/13/23 06:26 127-18-41.0 1
Toluene ND ug/L 04/13/23 06:26 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/13/23 06:26 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/13/23 06:26 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/13/23 06:26 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/13/23 06:26 79-00-51.0 1
Trichloroethene ND ug/L 04/13/23 06:26 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/13/23 06:26 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/13/23 06:26 96-18-41.0 1
Vinyl acetate ND ug/L 04/13/23 06:26 108-05-42.0 1
Vinyl chloride ND ug/L 04/13/23 06:26 75-01-41.0 1
Xylene (Total)ND ug/L 04/13/23 06:26 1330-20-71.0 1
m&p-Xylene ND ug/L 04/13/23 06:26 179601-23-12.0 1
o-Xylene ND ug/L 04/13/23 06:26 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %04/13/23 06:26 460-00-4 HS70-130 1
1,2-Dichloroethane-d4 (S)98 %04/13/23 06:26 17060-07-070-130 1
Toluene-d8 (S)98 %04/13/23 06:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:MW-4 Lab ID:92659938003 Collected:03/30/23 11:50 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene ND ug/L 04/06/23 14:53 83-32-904/05/23 13:27101
Acenaphthylene ND ug/L 04/06/23 14:53 208-96-804/05/23 13:27101
Anthracene ND ug/L 04/06/23 14:53 120-12-704/05/23 13:27101
Benzo(a)anthracene ND ug/L 04/06/23 14:53 56-55-304/05/23 13:27101
Benzo(a)pyrene ND ug/L 04/06/23 14:53 50-32-804/05/23 13:27101
Benzo(b)fluoranthene ND ug/L 04/06/23 14:53 205-99-204/05/23 13:27101
Benzo(g,h,i)perylene ND ug/L 04/06/23 14:53 191-24-2 L104/05/23 13:27101
Benzo(k)fluoranthene ND ug/L 04/06/23 14:53 207-08-904/05/23 13:27101
Chrysene ND ug/L 04/06/23 14:53 218-01-904/05/23 13:27101
Dibenz(a,h)anthracene ND ug/L 04/06/23 14:53 53-70-304/05/23 13:27101
Fluoranthene ND ug/L 04/06/23 14:53 206-44-004/05/23 13:27101
Fluorene ND ug/L 04/06/23 14:53 86-73-704/05/23 13:27101
Indeno(1,2,3-cd)pyrene ND ug/L 04/06/23 14:53 193-39-504/05/23 13:27101
1-Methylnaphthalene ND ug/L 04/06/23 14:53 90-12-004/05/23 13:27101
2-Methylnaphthalene ND ug/L 04/06/23 14:53 91-57-604/05/23 13:27101
Naphthalene ND ug/L 04/06/23 14:53 91-20-304/05/23 13:27101
Phenanthrene ND ug/L 04/06/23 14:53 85-01-804/05/23 13:27101
Pyrene ND ug/L 04/06/23 14:53 129-00-004/05/23 13:27101
Surrogates
Nitrobenzene-d5 (S)115 %04/06/23 14:53 4165-60-004/05/23 13:2759-144 1
2-Fluorobiphenyl (S)81 %04/06/23 14:53 321-60-804/05/23 13:2757-152 1
Terphenyl-d14 (S)97 %04/06/23 14:53 1718-51-004/05/23 13:2710-162 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/13/23 06:44 67-64-125.0 1
Benzene ND ug/L 04/13/23 06:44 71-43-21.0 1
Bromobenzene ND ug/L 04/13/23 06:44 108-86-11.0 1
Bromochloromethane ND ug/L 04/13/23 06:44 74-97-51.0 1
Bromodichloromethane ND ug/L 04/13/23 06:44 75-27-41.0 1
Bromoform ND ug/L 04/13/23 06:44 75-25-21.0 1
Bromomethane ND ug/L 04/13/23 06:44 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/13/23 06:44 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/13/23 06:44 56-23-51.0 1
Chlorobenzene ND ug/L 04/13/23 06:44 108-90-71.0 1
Chloroethane ND ug/L 04/13/23 06:44 75-00-31.0 1
Chloroform ND ug/L 04/13/23 06:44 67-66-31.0 1
Chloromethane ND ug/L 04/13/23 06:44 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/13/23 06:44 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/13/23 06:44 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/13/23 06:44 96-12-82.0 1
Dibromochloromethane ND ug/L 04/13/23 06:44 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 04/13/23 06:44 106-93-41.0 1
Dibromomethane ND ug/L 04/13/23 06:44 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/13/23 06:44 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/13/23 06:44 541-73-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:MW-4 Lab ID:92659938003 Collected:03/30/23 11:50 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,4-Dichlorobenzene ND ug/L 04/13/23 06:44 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/13/23 06:44 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/13/23 06:44 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/13/23 06:44 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/13/23 06:44 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/13/23 06:44 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/13/23 06:44 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/13/23 06:44 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/13/23 06:44 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/13/23 06:44 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/13/23 06:44 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/13/23 06:44 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/13/23 06:44 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/13/23 06:44 108-20-31.0 1
Ethylbenzene ND ug/L 04/13/23 06:44 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/13/23 06:44 87-68-32.0 1
2-Hexanone ND ug/L 04/13/23 06:44 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/13/23 06:44 99-87-61.0 1
Methylene Chloride ND ug/L 04/13/23 06:44 75-09-2 L1,v15.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/13/23 06:44 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 04/13/23 06:44 1634-04-41.0 1
Naphthalene ND ug/L 04/13/23 06:44 91-20-31.0 1
Styrene ND ug/L 04/13/23 06:44 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/13/23 06:44 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/13/23 06:44 79-34-51.0 1
Tetrachloroethene ND ug/L 04/13/23 06:44 127-18-41.0 1
Toluene ND ug/L 04/13/23 06:44 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/13/23 06:44 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/13/23 06:44 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/13/23 06:44 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/13/23 06:44 79-00-51.0 1
Trichloroethene ND ug/L 04/13/23 06:44 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/13/23 06:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/13/23 06:44 96-18-41.0 1
Vinyl acetate ND ug/L 04/13/23 06:44 108-05-42.0 1
Vinyl chloride ND ug/L 04/13/23 06:44 75-01-41.0 1
Xylene (Total)ND ug/L 04/13/23 06:44 1330-20-71.0 1
m&p-Xylene ND ug/L 04/13/23 06:44 179601-23-12.0 1
o-Xylene ND ug/L 04/13/23 06:44 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %04/13/23 06:44 460-00-4 HS70-130 1
1,2-Dichloroethane-d4 (S)99 %04/13/23 06:44 17060-07-070-130 1
Toluene-d8 (S)99 %04/13/23 06:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:WSW-1 Lab ID:92659938004 Collected:03/30/23 12:10 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene ND ug/L 04/06/23 15:19 83-32-904/05/23 13:279.7 1
Acenaphthylene ND ug/L 04/06/23 15:19 208-96-804/05/23 13:279.7 1
Anthracene ND ug/L 04/06/23 15:19 120-12-704/05/23 13:279.7 1
Benzo(a)anthracene ND ug/L 04/06/23 15:19 56-55-304/05/23 13:279.7 1
Benzo(a)pyrene ND ug/L 04/06/23 15:19 50-32-804/05/23 13:279.7 1
Benzo(b)fluoranthene ND ug/L 04/06/23 15:19 205-99-204/05/23 13:279.7 1
Benzo(g,h,i)perylene ND ug/L 04/06/23 15:19 191-24-2 L104/05/23 13:279.7 1
Benzo(k)fluoranthene ND ug/L 04/06/23 15:19 207-08-904/05/23 13:279.7 1
Chrysene ND ug/L 04/06/23 15:19 218-01-904/05/23 13:279.7 1
Dibenz(a,h)anthracene ND ug/L 04/06/23 15:19 53-70-304/05/23 13:279.7 1
Fluoranthene ND ug/L 04/06/23 15:19 206-44-004/05/23 13:279.7 1
Fluorene ND ug/L 04/06/23 15:19 86-73-704/05/23 13:279.7 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/06/23 15:19 193-39-504/05/23 13:279.7 1
1-Methylnaphthalene ND ug/L 04/06/23 15:19 90-12-004/05/23 13:279.7 1
2-Methylnaphthalene ND ug/L 04/06/23 15:19 91-57-604/05/23 13:279.7 1
Naphthalene ND ug/L 04/06/23 15:19 91-20-304/05/23 13:279.7 1
Phenanthrene ND ug/L 04/06/23 15:19 85-01-804/05/23 13:279.7 1
Pyrene ND ug/L 04/06/23 15:19 129-00-004/05/23 13:279.7 1
Surrogates
Nitrobenzene-d5 (S)116 %04/06/23 15:19 4165-60-004/05/23 13:2759-144 1
2-Fluorobiphenyl (S)81 %04/06/23 15:19 321-60-804/05/23 13:2757-152 1
Terphenyl-d14 (S)86 %04/06/23 15:19 1718-51-004/05/23 13:2710-162 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/12/23 18:39 67-64-125.0 1
Benzene ND ug/L 04/12/23 18:39 71-43-21.0 1
Bromobenzene ND ug/L 04/12/23 18:39 108-86-11.0 1
Bromochloromethane ND ug/L 04/12/23 18:39 74-97-51.0 1
Bromodichloromethane ND ug/L 04/12/23 18:39 75-27-41.0 1
Bromoform ND ug/L 04/12/23 18:39 75-25-21.0 1
Bromomethane ND ug/L 04/12/23 18:39 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/12/23 18:39 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/12/23 18:39 56-23-51.0 1
Chlorobenzene ND ug/L 04/12/23 18:39 108-90-71.0 1
Chloroethane ND ug/L 04/12/23 18:39 75-00-31.0 1
Chloroform ND ug/L 04/12/23 18:39 67-66-31.0 1
Chloromethane ND ug/L 04/12/23 18:39 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/12/23 18:39 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/12/23 18:39 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/12/23 18:39 96-12-82.0 1
Dibromochloromethane ND ug/L 04/12/23 18:39 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 04/12/23 18:39 106-93-41.0 1
Dibromomethane ND ug/L 04/12/23 18:39 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/12/23 18:39 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/12/23 18:39 541-73-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:WSW-1 Lab ID:92659938004 Collected:03/30/23 12:10 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,4-Dichlorobenzene ND ug/L 04/12/23 18:39 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/12/23 18:39 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/12/23 18:39 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/12/23 18:39 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/12/23 18:39 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/12/23 18:39 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/12/23 18:39 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/12/23 18:39 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/12/23 18:39 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/12/23 18:39 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/12/23 18:39 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/12/23 18:39 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/12/23 18:39 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/12/23 18:39 108-20-31.0 1
Ethylbenzene ND ug/L 04/12/23 18:39 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/12/23 18:39 87-68-32.0 1
2-Hexanone ND ug/L 04/12/23 18:39 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/12/23 18:39 99-87-61.0 1
Methylene Chloride ND ug/L 04/12/23 18:39 75-09-2 L1,v15.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/12/23 18:39 108-10-15.0 1
Methyl-tert-butyl ether 10.3 ug/L 04/12/23 18:39 1634-04-41.0 1
Naphthalene ND ug/L 04/12/23 18:39 91-20-31.0 1
Styrene ND ug/L 04/12/23 18:39 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/12/23 18:39 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/12/23 18:39 79-34-51.0 1
Tetrachloroethene ND ug/L 04/12/23 18:39 127-18-41.0 1
Toluene ND ug/L 04/12/23 18:39 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/12/23 18:39 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/12/23 18:39 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/12/23 18:39 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/12/23 18:39 79-00-51.0 1
Trichloroethene ND ug/L 04/12/23 18:39 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/12/23 18:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/12/23 18:39 96-18-41.0 1
Vinyl acetate ND ug/L 04/12/23 18:39 108-05-42.0 1
Vinyl chloride ND ug/L 04/12/23 18:39 75-01-41.0 1
Xylene (Total)ND ug/L 04/12/23 18:39 1330-20-71.0 1
m&p-Xylene ND ug/L 04/12/23 18:39 179601-23-12.0 1
o-Xylene ND ug/L 04/12/23 18:39 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %04/12/23 18:39 460-00-4 HS70-130 1
1,2-Dichloroethane-d4 (S)102 %04/12/23 18:39 17060-07-070-130 1
Toluene-d8 (S)98 %04/12/23 18:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:WSW-2 Lab ID:92659938005 Collected:03/30/23 12:20 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3511
Pace Analytical Services - Charlotte
8270E PAH Low Volume
Acenaphthene ND ug/L 04/06/23 19:00 83-32-904/05/23 13:279.9 1
Acenaphthylene ND ug/L 04/06/23 19:00 208-96-804/05/23 13:279.9 1
Anthracene ND ug/L 04/06/23 19:00 120-12-704/05/23 13:279.9 1
Benzo(a)anthracene ND ug/L 04/06/23 19:00 56-55-304/05/23 13:279.9 1
Benzo(a)pyrene ND ug/L 04/06/23 19:00 50-32-804/05/23 13:279.9 1
Benzo(b)fluoranthene ND ug/L 04/06/23 19:00 205-99-204/05/23 13:279.9 1
Benzo(g,h,i)perylene ND ug/L 04/06/23 19:00 191-24-2 L104/05/23 13:279.9 1
Benzo(k)fluoranthene ND ug/L 04/06/23 19:00 207-08-904/05/23 13:279.9 1
Chrysene ND ug/L 04/06/23 19:00 218-01-904/05/23 13:279.9 1
Dibenz(a,h)anthracene ND ug/L 04/06/23 19:00 53-70-304/05/23 13:279.9 1
Fluoranthene ND ug/L 04/06/23 19:00 206-44-004/05/23 13:279.9 1
Fluorene ND ug/L 04/06/23 19:00 86-73-704/05/23 13:279.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/06/23 19:00 193-39-504/05/23 13:279.9 1
1-Methylnaphthalene ND ug/L 04/06/23 19:00 90-12-004/05/23 13:279.9 1
2-Methylnaphthalene ND ug/L 04/06/23 19:00 91-57-604/05/23 13:279.9 1
Naphthalene ND ug/L 04/06/23 19:00 91-20-304/05/23 13:279.9 1
Phenanthrene ND ug/L 04/06/23 19:00 85-01-804/05/23 13:279.9 1
Pyrene ND ug/L 04/06/23 19:00 129-00-004/05/23 13:279.9 1
Surrogates
Nitrobenzene-d5 (S)118 %04/06/23 19:00 4165-60-004/05/23 13:2759-144 1
2-Fluorobiphenyl (S)87 %04/06/23 19:00 321-60-804/05/23 13:2757-152 1
Terphenyl-d14 (S)99 %04/06/23 19:00 1718-51-004/05/23 13:2710-162 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/12/23 18:56 67-64-125.0 1
Benzene ND ug/L 04/12/23 18:56 71-43-21.0 1
Bromobenzene ND ug/L 04/12/23 18:56 108-86-11.0 1
Bromochloromethane ND ug/L 04/12/23 18:56 74-97-51.0 1
Bromodichloromethane ND ug/L 04/12/23 18:56 75-27-41.0 1
Bromoform ND ug/L 04/12/23 18:56 75-25-21.0 1
Bromomethane ND ug/L 04/12/23 18:56 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/12/23 18:56 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/12/23 18:56 56-23-51.0 1
Chlorobenzene ND ug/L 04/12/23 18:56 108-90-71.0 1
Chloroethane ND ug/L 04/12/23 18:56 75-00-31.0 1
Chloroform ND ug/L 04/12/23 18:56 67-66-31.0 1
Chloromethane ND ug/L 04/12/23 18:56 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/12/23 18:56 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/12/23 18:56 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/12/23 18:56 96-12-82.0 1
Dibromochloromethane ND ug/L 04/12/23 18:56 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 04/12/23 18:56 106-93-41.0 1
Dibromomethane ND ug/L 04/12/23 18:56 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/12/23 18:56 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/12/23 18:56 541-73-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Sample:WSW-2 Lab ID:92659938005 Collected:03/30/23 12:20 Received:03/31/23 12:15 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,4-Dichlorobenzene ND ug/L 04/12/23 18:56 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/12/23 18:56 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/12/23 18:56 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/12/23 18:56 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/12/23 18:56 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/12/23 18:56 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/12/23 18:56 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/12/23 18:56 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/12/23 18:56 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/12/23 18:56 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/12/23 18:56 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/12/23 18:56 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/12/23 18:56 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/12/23 18:56 108-20-31.0 1
Ethylbenzene ND ug/L 04/12/23 18:56 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/12/23 18:56 87-68-32.0 1
2-Hexanone ND ug/L 04/12/23 18:56 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/12/23 18:56 99-87-61.0 1
Methylene Chloride ND ug/L 04/12/23 18:56 75-09-2 L1,v15.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/12/23 18:56 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 04/12/23 18:56 1634-04-41.0 1
Naphthalene ND ug/L 04/12/23 18:56 91-20-31.0 1
Styrene ND ug/L 04/12/23 18:56 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/12/23 18:56 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/12/23 18:56 79-34-51.0 1
Tetrachloroethene ND ug/L 04/12/23 18:56 127-18-41.0 1
Toluene ND ug/L 04/12/23 18:56 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/12/23 18:56 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/12/23 18:56 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/12/23 18:56 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/12/23 18:56 79-00-51.0 1
Trichloroethene ND ug/L 04/12/23 18:56 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/12/23 18:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/12/23 18:56 96-18-41.0 1
Vinyl acetate ND ug/L 04/12/23 18:56 108-05-42.0 1
Vinyl chloride ND ug/L 04/12/23 18:56 75-01-41.0 1
Xylene (Total)ND ug/L 04/12/23 18:56 1330-20-71.0 1
m&p-Xylene ND ug/L 04/12/23 18:56 179601-23-12.0 1
o-Xylene ND ug/L 04/12/23 18:56 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %04/12/23 18:56 460-00-4 HS70-130 1
1,2-Dichloroethane-d4 (S)100 %04/12/23 18:56 17060-07-070-130 1
Toluene-d8 (S)100 %04/12/23 18:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
767419
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92659938004, 92659938005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3984612
Associated Lab Samples:92659938004, 92659938005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 04/12/23 09:52
1,1,1-Trichloroethane ug/L ND 1.0 04/12/23 09:52
1,1,2,2-Tetrachloroethane ug/L ND 1.0 04/12/23 09:52
1,1,2-Trichloroethane ug/L ND 1.0 04/12/23 09:52
1,1-Dichloroethane ug/L ND 1.0 04/12/23 09:52
1,1-Dichloroethene ug/L ND 1.0 04/12/23 09:52
1,1-Dichloropropene ug/L ND 1.0 04/12/23 09:52
1,2,3-Trichlorobenzene ug/L ND 1.0 04/12/23 09:52
1,2,3-Trichloropropane ug/L ND 1.0 04/12/23 09:52
1,2,4-Trichlorobenzene ug/L ND 1.0 04/12/23 09:52
1,2-Dibromo-3-chloropropane ug/L ND 2.0 04/12/23 09:52
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/12/23 09:52
1,2-Dichlorobenzene ug/L ND 1.0 04/12/23 09:52
1,2-Dichloroethane ug/L ND 1.0 04/12/23 09:52
1,2-Dichloropropane ug/L ND 1.0 04/12/23 09:52
1,3-Dichlorobenzene ug/L ND 1.0 04/12/23 09:52
1,3-Dichloropropane ug/L ND 1.0 04/12/23 09:52
1,4-Dichlorobenzene ug/L ND 1.0 04/12/23 09:52
2,2-Dichloropropane ug/L ND 1.0 04/12/23 09:52
2-Butanone (MEK)ug/L ND 5.0 04/12/23 09:52
2-Chlorotoluene ug/L ND 1.0 04/12/23 09:52
2-Hexanone ug/L ND 5.0 04/12/23 09:52
4-Chlorotoluene ug/L ND 1.0 04/12/23 09:52
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 04/12/23 09:52
Acetone ug/L ND 25.0 04/12/23 09:52
Benzene ug/L ND 1.0 04/12/23 09:52
Bromobenzene ug/L ND 1.0 04/12/23 09:52
Bromochloromethane ug/L ND 1.0 04/12/23 09:52
Bromodichloromethane ug/L ND 1.0 04/12/23 09:52
Bromoform ug/L ND 1.0 04/12/23 09:52
Bromomethane ug/L ND 2.0 04/12/23 09:52
Carbon tetrachloride ug/L ND 1.0 04/12/23 09:52
Chlorobenzene ug/L ND 1.0 04/12/23 09:52
Chloroethane ug/L ND 1.0 04/12/23 09:52
Chloroform ug/L ND 1.0 04/12/23 09:52
Chloromethane ug/L ND 1.0 04/12/23 09:52
cis-1,2-Dichloroethene ug/L ND 1.0 04/12/23 09:52
cis-1,3-Dichloropropene ug/L ND 1.0 04/12/23 09:52
Dibromochloromethane ug/L ND 1.0 04/12/23 09:52
Dibromomethane ug/L ND 1.0 04/12/23 09:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3984612
Associated Lab Samples:92659938004, 92659938005
Matrix:Water
Analyzed
Dichlorodifluoromethane ug/L ND 1.0 04/12/23 09:52
Diisopropyl ether ug/L ND 1.0 04/12/23 09:52
Ethylbenzene ug/L ND 1.0 04/12/23 09:52
Hexachloro-1,3-butadiene ug/L ND 2.0 04/12/23 09:52
m&p-Xylene ug/L ND 2.0 04/12/23 09:52
Methyl-tert-butyl ether ug/L ND 1.0 04/12/23 09:52
Methylene Chloride ug/L ND 5.0 v104/12/23 09:52
Naphthalene ug/L ND 1.0 04/12/23 09:52
o-Xylene ug/L ND 1.0 04/12/23 09:52
p-Isopropyltoluene ug/L ND 1.0 04/12/23 09:52
Styrene ug/L ND 1.0 04/12/23 09:52
Tetrachloroethene ug/L ND 1.0 04/12/23 09:52
Toluene ug/L ND 1.0 04/12/23 09:52
trans-1,2-Dichloroethene ug/L ND 1.0 04/12/23 09:52
trans-1,3-Dichloropropene ug/L ND 1.0 04/12/23 09:52
Trichloroethene ug/L ND 1.0 04/12/23 09:52
Trichlorofluoromethane ug/L ND 1.0 04/12/23 09:52
Vinyl acetate ug/L ND 2.0 04/12/23 09:52
Vinyl chloride ug/L ND 1.0 04/12/23 09:52
Xylene (Total)ug/L ND 1.0 04/12/23 09:52
1,2-Dichloroethane-d4 (S)%99 70-130 04/12/23 09:52
4-Bromofluorobenzene (S)%101 70-130 04/12/23 09:52
Toluene-d8 (S)%102 70-130 04/12/23 09:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3984613LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.520 103 70-130
1,1,1-Trichloroethane ug/L 19.920 99 70-130
1,1,2,2-Tetrachloroethane ug/L 20.520 103 70-130
1,1,2-Trichloroethane ug/L 20.520 102 70-130
1,1-Dichloroethane ug/L 20.220 101 70-130
1,1-Dichloroethene ug/L 19.820 99 70-130
1,1-Dichloropropene ug/L 21.320 106 70-130
1,2,3-Trichlorobenzene ug/L 20.220 101 70-130
1,2,3-Trichloropropane ug/L 20.120 101 70-130
1,2,4-Trichlorobenzene ug/L 19.820 99 70-130
1,2-Dibromo-3-chloropropane ug/L 19.520 97 70-131
1,2-Dibromoethane (EDB)ug/L 20.320 101 70-130
1,2-Dichlorobenzene ug/L 20.720 103 70-130
1,2-Dichloroethane ug/L 20.820 104 70-130
1,2-Dichloropropane ug/L 20.620 103 70-130
1,3-Dichlorobenzene ug/L 20.620 103 70-130
1,3-Dichloropropane ug/L 20.020 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3984613LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 20.320 101 70-130
2,2-Dichloropropane ug/L 18.920 94 68-135
2-Butanone (MEK)ug/L 35.440 89 70-134
2-Chlorotoluene ug/L 20.420 102 70-130
2-Hexanone ug/L 38.040 95 70-131
4-Chlorotoluene ug/L 20.820 104 70-130
4-Methyl-2-pentanone (MIBK)ug/L 37.140 93 70-130
Acetone ug/L 38.540 96 70-133
Benzene ug/L 20.320 101 70-130
Bromobenzene ug/L 20.220 101 70-130
Bromochloromethane ug/L 20.420 102 70-130
Bromodichloromethane ug/L 20.620 103 70-130
Bromoform ug/L 19.920 100 70-130
Bromomethane ug/L 16.420 82 45-151
Carbon tetrachloride ug/L 20.620 103 70-130
Chlorobenzene ug/L 19.920 100 70-130
Chloroethane ug/L 19.820 99 39-152
Chloroform ug/L 20.320 101 70-130
Chloromethane ug/L 21.320 107 58-130
cis-1,2-Dichloroethene ug/L 19.720 98 70-130
cis-1,3-Dichloropropene ug/L 20.020 100 70-130
Dibromochloromethane ug/L 20.320 102 70-130
Dibromomethane ug/L 19.320 97 70-130
Dichlorodifluoromethane ug/L 20.720 103 54-133
Diisopropyl ether ug/L 18.220 91 70-130
Ethylbenzene ug/L 19.720 98 70-130
Hexachloro-1,3-butadiene ug/L 19.820 99 70-135
m&p-Xylene ug/L 39.340 98 70-130
Methyl-tert-butyl ether ug/L 19.020 95 70-130
Methylene Chloride ug/L 37.3 L1,v12018766-130
Naphthalene ug/L 21.120 106 70-130
o-Xylene ug/L 19.620 98 70-130
p-Isopropyltoluene ug/L 20.620 103 70-130
Styrene ug/L 19.820 99 70-130
Tetrachloroethene ug/L 18.620 93 70-130
Toluene ug/L 19.720 99 70-130
trans-1,2-Dichloroethene ug/L 19.920 99 70-130
trans-1,3-Dichloropropene ug/L 20.020 100 70-130
Trichloroethene ug/L 20.020 100 70-130
Trichlorofluoromethane ug/L 17.720 89 62-130
Vinyl acetate ug/L 40.740 102 70-144
Vinyl chloride ug/L 16.820 84 62-130
Xylene (Total)ug/L 59.060 98 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3984614MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92659785001
3984615
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 92 70-14197 520ND18.4 19.4
1,1,1-Trichloroethane ug/L 20 97 70-150101 420ND19.3 20.2
1,1,2,2-Tetrachloroethane ug/L 20 92 69-14294 220ND18.4 18.7
1,1,2-Trichloroethane ug/L 20 95 70-13897 220ND19.0 19.5
1,1-Dichloroethane ug/L 20 98 70-150101 320ND19.6 20.2
1,1-Dichloroethene ug/L 20 94 70-156100 620ND18.8 20.0
1,1-Dichloropropene ug/L 20 97 70-150101 520ND19.4 20.2
1,2,3-Trichlorobenzene ug/L 20 83 70-14884 120ND16.6 16.7
1,2,3-Trichloropropane ug/L 20 91 70-14092 120ND18.3 18.5
1,2,4-Trichlorobenzene ug/L 20 79 70-14683 420ND15.9 16.6
1,2-Dibromo-3-chloropropane ug/L 20 84 68-14687 320ND16.9 17.4
1,2-Dibromoethane (EDB)ug/L 20 95 70-13898 320ND19.0 19.5
1,2-Dichlorobenzene ug/L 20 87 70-14188 220ND17.3 17.7
1,2-Dichloroethane ug/L 20 95 69-143100 520ND19.1 19.9
1,2-Dichloropropane ug/L 20 96 68-15697 120ND19.2 19.5
1,3-Dichlorobenzene ug/L 20 85 70-14387 320ND17.0 17.5
1,3-Dichloropropane ug/L 20 93 70-13899 620ND18.7 19.8
1,4-Dichlorobenzene ug/L 20 86 70-14288 220ND17.2 17.6
2,2-Dichloropropane ug/L 20 86 52-17091 620ND17.2 18.2
2-Butanone (MEK)ug/L 40 88 60-15791 340ND35.2 36.5
2-Chlorotoluene ug/L 20 87 70-14789 220ND17.4 17.8
2-Hexanone ug/L 40 88 68-14694 640ND35.3 37.6
4-Chlorotoluene ug/L 20 86 70-14288 320ND17.1 17.6
4-Methyl-2-pentanone (MIBK)ug/L 40 86 70-14190 440ND34.6 35.8
Acetone ug/L 40 85 58-15795 1040ND34.2 37.9
Benzene ug/L 20 97 70-142100 320ND19.4 19.9
Bromobenzene ug/L 20 90 70-14393 320ND18.0 18.5
Bromochloromethane ug/L 20 95 70-14697 320ND18.9 19.4
Bromodichloromethane ug/L 20 97 70-13998 120ND19.4 19.6
Bromoform ug/L 20 87 64-14092 620ND17.3 18.3
Bromomethane ug/L 20 88 28-19286 320ND17.7 17.2
Carbon tetrachloride ug/L 20 98 70-148100 220ND19.6 20.0
Chlorobenzene ug/L 20 91 70-14195 520ND18.1 19.0
Chloroethane ug/L 20 96 58-191102 620ND19.2 20.3
Chloroform ug/L 20 93 70-14897 3205.5 24.2 25.0
Chloromethane ug/L 20 98 43-162103 420ND19.6 20.5
cis-1,2-Dichloroethene ug/L 20 92 68-15199 720ND18.5 19.9
cis-1,3-Dichloropropene ug/L 20 93 70-13994 020ND18.7 18.7
Dibromochloromethane ug/L 20 93 70-14495 320ND18.5 19.0
Dibromomethane ug/L 20 91 70-13996 520ND18.3 19.2
Dichlorodifluoromethane ug/L 20 105 39-171116 1020ND21.0 23.2
Diisopropyl ether ug/L 20 85 67-14289 420ND17.1 17.8
Ethylbenzene ug/L 20 89 70-14393 520ND17.7 18.6
Hexachloro-1,3-butadiene ug/L 20 84 64-16387 420ND16.8 17.4
m&p-Xylene ug/L 40 84 70-14490 640ND33.8 35.9
Methyl-tert-butyl ether ug/L 20 87 65-14389 220ND17.9 18.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3984614MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92659785001
3984615
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L v1209362-14996 420ND18.5 19.2
Naphthalene ug/L 20 90 67-14790 120ND17.9 18.1
o-Xylene ug/L 20 87 70-14591 520ND17.3 18.2
p-Isopropyltoluene ug/L 20 83 70-14788 520ND16.6 17.5
Styrene ug/L 20 85 70-14386 120ND17.0 17.2
Tetrachloroethene ug/L 20 77 70-14583 720ND16.1 17.4
Toluene ug/L 20 91 70-14292 220ND18.1 18.5
trans-1,2-Dichloroethene ug/L 20 90 70-151100 1120ND17.9 20.0
trans-1,3-Dichloropropene ug/L 20 92 70-13993 220ND18.3 18.7
Trichloroethene ug/L 20 92 62-14694 320ND18.9 19.4
Trichlorofluoromethane ug/L 20 91 63-153102 1220ND18.2 20.5
Vinyl acetate ug/L 40 81 61-16281 040ND32.4 32.5
Vinyl chloride ug/L 20 80 61-16387 820ND15.9 17.4
Xylene (Total)ug/L 60 85 70-14390 660ND51.1 54.1
1,2-Dichloroethane-d4 (S)%99 70-130103
4-Bromofluorobenzene (S)%99 70-130101
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
767703
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92659938001, 92659938002, 92659938003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3986135
Associated Lab Samples:92659938001, 92659938002, 92659938003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 04/12/23 23:59
1,1,1-Trichloroethane ug/L ND 1.0 04/12/23 23:59
1,1,2,2-Tetrachloroethane ug/L ND 1.0 04/12/23 23:59
1,1,2-Trichloroethane ug/L ND 1.0 04/12/23 23:59
1,1-Dichloroethane ug/L ND 1.0 04/12/23 23:59
1,1-Dichloroethene ug/L ND 1.0 04/12/23 23:59
1,1-Dichloropropene ug/L ND 1.0 04/12/23 23:59
1,2,3-Trichlorobenzene ug/L ND 1.0 04/12/23 23:59
1,2,3-Trichloropropane ug/L ND 1.0 04/12/23 23:59
1,2,4-Trichlorobenzene ug/L ND 1.0 04/12/23 23:59
1,2-Dibromo-3-chloropropane ug/L ND 2.0 04/12/23 23:59
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/12/23 23:59
1,2-Dichlorobenzene ug/L ND 1.0 04/12/23 23:59
1,2-Dichloroethane ug/L ND 1.0 04/12/23 23:59
1,2-Dichloropropane ug/L ND 1.0 04/12/23 23:59
1,3-Dichlorobenzene ug/L ND 1.0 04/12/23 23:59
1,3-Dichloropropane ug/L ND 1.0 04/12/23 23:59
1,4-Dichlorobenzene ug/L ND 1.0 04/12/23 23:59
2,2-Dichloropropane ug/L ND 1.0 04/12/23 23:59
2-Butanone (MEK)ug/L ND 5.0 04/12/23 23:59
2-Chlorotoluene ug/L ND 1.0 04/12/23 23:59
2-Hexanone ug/L ND 5.0 04/12/23 23:59
4-Chlorotoluene ug/L ND 1.0 04/12/23 23:59
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 04/12/23 23:59
Acetone ug/L ND 25.0 04/12/23 23:59
Benzene ug/L ND 1.0 04/12/23 23:59
Bromobenzene ug/L ND 1.0 04/12/23 23:59
Bromochloromethane ug/L ND 1.0 04/12/23 23:59
Bromodichloromethane ug/L ND 1.0 04/12/23 23:59
Bromoform ug/L ND 1.0 04/12/23 23:59
Bromomethane ug/L ND 2.0 04/12/23 23:59
Carbon tetrachloride ug/L ND 1.0 04/12/23 23:59
Chlorobenzene ug/L ND 1.0 04/12/23 23:59
Chloroethane ug/L ND 1.0 04/12/23 23:59
Chloroform ug/L ND 1.0 04/12/23 23:59
Chloromethane ug/L ND 1.0 04/12/23 23:59
cis-1,2-Dichloroethene ug/L ND 1.0 04/12/23 23:59
cis-1,3-Dichloropropene ug/L ND 1.0 04/12/23 23:59
Dibromochloromethane ug/L ND 1.0 04/12/23 23:59
Dibromomethane ug/L ND 1.0 04/12/23 23:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
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[phone]
Page 19 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3986135
Associated Lab Samples:92659938001, 92659938002, 92659938003
Matrix:Water
Analyzed
Dichlorodifluoromethane ug/L ND 1.0 04/12/23 23:59
Diisopropyl ether ug/L ND 1.0 04/12/23 23:59
Ethylbenzene ug/L ND 1.0 04/12/23 23:59
Hexachloro-1,3-butadiene ug/L ND 2.0 04/12/23 23:59
m&p-Xylene ug/L ND 2.0 04/12/23 23:59
Methyl-tert-butyl ether ug/L ND 1.0 04/12/23 23:59
Methylene Chloride ug/L ND 5.0 v104/12/23 23:59
Naphthalene ug/L ND 1.0 04/12/23 23:59
o-Xylene ug/L ND 1.0 04/12/23 23:59
p-Isopropyltoluene ug/L ND 1.0 04/12/23 23:59
Styrene ug/L ND 1.0 04/12/23 23:59
Tetrachloroethene ug/L ND 1.0 04/12/23 23:59
Toluene ug/L ND 1.0 04/12/23 23:59
trans-1,2-Dichloroethene ug/L ND 1.0 04/12/23 23:59
trans-1,3-Dichloropropene ug/L ND 1.0 04/12/23 23:59
Trichloroethene ug/L ND 1.0 04/12/23 23:59
Trichlorofluoromethane ug/L ND 1.0 04/12/23 23:59
Vinyl acetate ug/L ND 2.0 04/12/23 23:59
Vinyl chloride ug/L ND 1.0 04/12/23 23:59
Xylene (Total)ug/L ND 1.0 04/12/23 23:59
1,2-Dichloroethane-d4 (S)%101 70-130 04/12/23 23:59
4-Bromofluorobenzene (S)%100 70-130 04/12/23 23:59
Toluene-d8 (S)%101 70-130 04/12/23 23:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3986136LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.220 96 70-130
1,1,1-Trichloroethane ug/L 18.720 93 70-130
1,1,2,2-Tetrachloroethane ug/L 19.520 98 70-130
1,1,2-Trichloroethane ug/L 18.620 93 70-130
1,1-Dichloroethane ug/L 19.020 95 70-130
1,1-Dichloroethene ug/L 19.220 96 70-130
1,1-Dichloropropene ug/L 20.420 102 70-130
1,2,3-Trichlorobenzene ug/L 19.020 95 70-130
1,2,3-Trichloropropane ug/L 18.420 92 70-130
1,2,4-Trichlorobenzene ug/L 19.120 95 70-130
1,2-Dibromo-3-chloropropane ug/L 18.020 90 70-131
1,2-Dibromoethane (EDB)ug/L 19.720 98 70-130
1,2-Dichlorobenzene ug/L 19.620 98 70-130
1,2-Dichloroethane ug/L 19.920 100 70-130
1,2-Dichloropropane ug/L 19.320 96 70-130
1,3-Dichlorobenzene ug/L 19.520 98 70-130
1,3-Dichloropropane ug/L 19.120 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3986136LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 19.520 98 70-130
2,2-Dichloropropane ug/L 19.420 97 68-135
2-Butanone (MEK)ug/L 35.640 89 70-134
2-Chlorotoluene ug/L 19.320 97 70-130
2-Hexanone ug/L 39.240 98 70-131
4-Chlorotoluene ug/L 19.220 96 70-130
4-Methyl-2-pentanone (MIBK)ug/L 37.140 93 70-130
Acetone ug/L 38.840 97 70-133
Benzene ug/L 19.220 96 70-130
Bromobenzene ug/L 19.120 96 70-130
Bromochloromethane ug/L 19.120 95 70-130
Bromodichloromethane ug/L 18.820 94 70-130
Bromoform ug/L 18.520 93 70-130
Bromomethane ug/L 16.520 83 45-151
Carbon tetrachloride ug/L 18.920 94 70-130
Chlorobenzene ug/L 18.920 94 70-130
Chloroethane ug/L 18.520 92 39-152
Chloroform ug/L 18.020 90 70-130
Chloromethane ug/L 18.720 93 58-130
cis-1,2-Dichloroethene ug/L 18.120 91 70-130
cis-1,3-Dichloropropene ug/L 19.120 95 70-130
Dibromochloromethane ug/L 19.420 97 70-130
Dibromomethane ug/L 17.920 90 70-130
Dichlorodifluoromethane ug/L 19.620 98 54-133
Diisopropyl ether ug/L 17.820 89 70-130
Ethylbenzene ug/L 19.020 95 70-130
Hexachloro-1,3-butadiene ug/L 19.620 98 70-135
m&p-Xylene ug/L 37.340 93 70-130
Methyl-tert-butyl ether ug/L 18.420 92 70-130
Methylene Chloride ug/L 48.4 L1,v12024266-130
Naphthalene ug/L 20.020 100 70-130
o-Xylene ug/L 18.620 93 70-130
p-Isopropyltoluene ug/L 19.520 98 70-130
Styrene ug/L 18.620 93 70-130
Tetrachloroethene ug/L 18.120 90 70-130
Toluene ug/L 18.220 91 70-130
trans-1,2-Dichloroethene ug/L 19.220 96 70-130
trans-1,3-Dichloropropene ug/L 19.020 95 70-130
Trichloroethene ug/L 19.120 96 70-130
Trichlorofluoromethane ug/L 17.420 87 62-130
Vinyl acetate ug/L 42.440 106 70-144
Vinyl chloride ug/L 15.220 76 62-130
Xylene (Total)ug/L 56.060 93 70-130
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3986138MATRIX SPIKE SAMPLE:
MSSpike
Result
92659938003
1,1,1,2-Tetrachloroethane ug/L 21.720 109 70-141ND
1,1,1-Trichloroethane ug/L 22.520 112 70-150ND
1,1,2,2-Tetrachloroethane ug/L 20.420 102 69-142ND
1,1,2-Trichloroethane ug/L 21.420 107 70-138ND
1,1-Dichloroethane ug/L 21.220 106 70-150ND
1,1-Dichloroethene ug/L 22.220 111 70-156ND
1,1-Dichloropropene ug/L 24.220 121 70-150ND
1,2,3-Trichlorobenzene ug/L 20.820 104 70-148ND
1,2,3-Trichloropropane ug/L 20.320 102 70-140ND
1,2,4-Trichlorobenzene ug/L 20.620 103 70-146ND
1,2-Dibromo-3-chloropropane ug/L 19.220 96 68-146ND
1,2-Dibromoethane (EDB)ug/L 21.620 108 70-138ND
1,2-Dichlorobenzene ug/L 21.820 109 70-141ND
1,2-Dichloroethane ug/L 21.120 106 69-143ND
1,2-Dichloropropane ug/L 22.020 110 68-156ND
1,3-Dichlorobenzene ug/L 22.120 111 70-143ND
1,3-Dichloropropane ug/L 21.220 106 70-138ND
1,4-Dichlorobenzene ug/L 21.920 110 70-142ND
2,2-Dichloropropane ug/L 22.920 114 52-170ND
2-Butanone (MEK)ug/L 39.140 98 60-157ND
2-Chlorotoluene ug/L 22.220 111 70-147ND
2-Hexanone ug/L 39.540 99 68-146ND
4-Chlorotoluene ug/L 22.220 111 70-142ND
4-Methyl-2-pentanone (MIBK)ug/L 40.440 101 70-141ND
Acetone ug/L 41.640 104 58-157ND
Benzene ug/L 22.720 113 70-142ND
Bromobenzene ug/L 21.820 109 70-143ND
Bromochloromethane ug/L 20.920 104 70-146ND
Bromodichloromethane ug/L 21.520 107 70-139ND
Bromoform ug/L 19.020 95 64-140ND
Bromomethane ug/L 21.420 107 28-192ND
Carbon tetrachloride ug/L 23.520 118 70-148ND
Chlorobenzene ug/L 21.420 107 70-141ND
Chloroethane ug/L 22.120 111 58-191ND
Chloroform ug/L 21.620 108 70-148ND
Chloromethane ug/L 21.820 109 43-162ND
cis-1,2-Dichloroethene ug/L 21.320 106 68-151ND
cis-1,3-Dichloropropene ug/L 21.320 106 70-139ND
Dibromochloromethane ug/L 20.920 104 70-144ND
Dibromomethane ug/L 20.320 102 70-139ND
Dichlorodifluoromethane ug/L 25.2 v12012639-171ND
Diisopropyl ether ug/L 19.620 98 67-142ND
Ethylbenzene ug/L 21.620 108 70-143ND
Hexachloro-1,3-butadiene ug/L 21.620 108 64-163ND
m&p-Xylene ug/L 42.140 105 70-144ND
Methyl-tert-butyl ether ug/L 20.120 101 65-143ND
Methylene Chloride ug/L 19.9 v12010062-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3986138MATRIX SPIKE SAMPLE:
MSSpike
Result
92659938003
Naphthalene ug/L 21.220 106 67-147ND
o-Xylene ug/L 21.120 106 70-145ND
p-Isopropyltoluene ug/L 22.020 110 70-147ND
Styrene ug/L 21.020 105 70-143ND
Tetrachloroethene ug/L 20.920 105 70-145ND
Toluene ug/L 21.720 108 70-142ND
trans-1,2-Dichloroethene ug/L 21.920 110 70-151ND
trans-1,3-Dichloropropene ug/L 21.020 105 70-139ND
Trichloroethene ug/L 23.120 115 62-146ND
Trichlorofluoromethane ug/L 22.220 111 63-153ND
Vinyl acetate ug/L 44.3 v14011161-162ND
Vinyl chloride ug/L 18.520 93 61-163ND
Xylene (Total)ug/L 63.260 105 70-143ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%HS9770-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92659938002
3986137SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92659938002
3986137SAMPLE DUPLICATE:
Benzene ug/L NDND
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L ND v1ND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L ND v1ND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L ND v1ND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%10198
4-Bromofluorobenzene (S)%99 HS97
Toluene-d8 (S)%9898
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
766023
EPA 3511
EPA 8270E
8270E PAH Low Volume
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92659938001, 92659938002, 92659938003, 92659938004, 92659938005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3977233
Associated Lab Samples:92659938001, 92659938002, 92659938003, 92659938004, 92659938005
Matrix:Water
Analyzed
1-Methylnaphthalene ug/L ND 10.0 04/05/23 15:27
2-Methylnaphthalene ug/L ND 10.0 04/05/23 15:27
Acenaphthene ug/L ND 10.0 04/05/23 15:27
Acenaphthylene ug/L ND 10.0 04/05/23 15:27
Anthracene ug/L ND 10.0 04/05/23 15:27
Benzo(a)anthracene ug/L ND 10.0 04/05/23 15:27
Benzo(a)pyrene ug/L ND 10.0 04/05/23 15:27
Benzo(b)fluoranthene ug/L ND 10.0 04/05/23 15:27
Benzo(g,h,i)perylene ug/L ND 10.0 04/05/23 15:27
Benzo(k)fluoranthene ug/L ND 10.0 04/05/23 15:27
Chrysene ug/L ND 10.0 04/05/23 15:27
Dibenz(a,h)anthracene ug/L ND 10.0 04/05/23 15:27
Fluoranthene ug/L ND 10.0 04/05/23 15:27
Fluorene ug/L ND 10.0 04/05/23 15:27
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 04/05/23 15:27
Naphthalene ug/L ND 10.0 04/05/23 15:27
Phenanthrene ug/L ND 10.0 04/05/23 15:27
Pyrene ug/L ND 10.0 04/05/23 15:27
2-Fluorobiphenyl (S)%77 57-152 04/05/23 15:27
Nitrobenzene-d5 (S)%100 59-144 04/05/23 15:27
Terphenyl-d14 (S)%98 10-162 04/05/23 15:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3977234LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/L 68.162.5 109 70-130
2-Methylnaphthalene ug/L 61.562.5 98 70-130
Acenaphthene ug/L 68.162.5 109 70-130
Acenaphthylene ug/L 65.762.5 105 70-130
Anthracene ug/L 62.562.5 100 70-130
Benzo(a)anthracene ug/L 67.462.5 108 70-130
Benzo(a)pyrene ug/L 63.162.5 101 70-130
Benzo(b)fluoranthene ug/L 60.462.5 97 70-130
Benzo(g,h,i)perylene ug/L 85.2 L162.5 136 70-130
Benzo(k)fluoranthene ug/L 58.262.5 93 70-130
Chrysene ug/L 66.862.5 107 70-130
Dibenz(a,h)anthracene ug/L 79.862.5 128 70-130
Fluoranthene ug/L 68.062.5 109 70-130
Fluorene ug/L 70.062.5 112 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3977234LABORATORY CONTROL SAMPLE:
LCSSpike
Indeno(1,2,3-cd)pyrene ug/L 80.262.5 128 70-130
Naphthalene ug/L 57.962.5 93 70-130
Phenanthrene ug/L 68.262.5 109 70-130
Pyrene ug/L 67.662.5 108 70-130
2-Fluorobiphenyl (S)%94 57-152
Nitrobenzene-d5 (S)%103 59-144
Terphenyl-d14 (S)%105 10-162
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3977235MATRIX SPIKE SAMPLE:
MSSpike
Result
92659938004
1-Methylnaphthalene ug/L 70.962 114 56-169ND
2-Methylnaphthalene ug/L 64.962 105 52-169ND
Acenaphthene ug/L 65.362 105 58-172ND
Acenaphthylene ug/L 65.662 106 59-168ND
Anthracene ug/L 63.362 102 39-173ND
Benzo(a)anthracene ug/L 65.562 106 51-169ND
Benzo(a)pyrene ug/L 64.162 103 52-170ND
Benzo(b)fluoranthene ug/L 63.862 103 48-172ND
Benzo(g,h,i)perylene ug/L 69.162 111 53-172ND
Benzo(k)fluoranthene ug/L 67.462 109 53-178ND
Chrysene ug/L 69.362 112 57-172ND
Dibenz(a,h)anthracene ug/L 67.462 109 51-171ND
Fluoranthene ug/L 75.862 122 49-170ND
Fluorene ug/L 70.462 113 57-174ND
Indeno(1,2,3-cd)pyrene ug/L 67.062 108 52-170ND
Naphthalene ug/L 62.662 101 55-172ND
Phenanthrene ug/L 69.062 111 54-171ND
Pyrene ug/L 59.962 97 47-178ND
2-Fluorobiphenyl (S)%85 57-152
Nitrobenzene-d5 (S)%114 59-144
Terphenyl-d14 (S)%88 10-162
Parameter Units
Dup
Result QualifiersRPDResult
92659938005
3977236SAMPLE DUPLICATE:
1-Methylnaphthalene ug/L NDND
2-Methylnaphthalene ug/L NDND
Acenaphthene ug/L NDND
Acenaphthylene ug/L NDND
Anthracene ug/L NDND
Benzo(a)anthracene ug/L NDND
Benzo(a)pyrene ug/L NDND
Benzo(b)fluoranthene ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92659938005
3977236SAMPLE DUPLICATE:
Benzo(g,h,i)perylene ug/L NDND
Benzo(k)fluoranthene ug/L NDND
Chrysene ug/L NDND
Dibenz(a,h)anthracene ug/L NDND
Fluoranthene ug/L NDND
Fluorene ug/L NDND
Indeno(1,2,3-cd)pyrene ug/L NDND
Naphthalene ug/L NDND
Phenanthrene ug/L NDND
Pyrene ug/L NDND
2-Fluorobiphenyl (S)%8887
Nitrobenzene-d5 (S)%109118
Terphenyl-d14 (S)%8999
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 49
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).HS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 49
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92659938
RACE TRACK PETRO
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92659938001 766023 766182MW-1R EPA 3511 EPA 8270E
92659938002 766023 766182MW-2 EPA 3511 EPA 8270E
92659938003 766023 766182MW-4 EPA 3511 EPA 8270E
92659938004 766023 766182WSW-1 EPA 3511 EPA 8270E
92659938005 766023 766182WSW-2 EPA 3511 EPA 8270E
92659938001 767703MW-1R EPA 8260D
92659938002 767703MW-2 EPA 8260D
92659938003 767703MW-4 EPA 8260D
92659938004 767419WSW-1 EPA 8260D
92659938005 767419WSW-2 EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/18/2023 10:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 49
Page 30 of 49
Page 31 of 49
Pa
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e

3
2

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4
9
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 12, 2023
Taylor Cannon
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: Race Track Petro
Client Job Number:
Project Number: 92659938
Laboratory Work Order Number: 23D0499
Enclosed are results of analyses for samples as received by the laboratory on April 5, 2023. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 17
Table of Contents
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Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23D0499-01 5
23D0499-02 6
23D0499-03 7
23D0499-04 8
23D0499-05 9
Sample Preparation Information 10
QC Data 11
Petroleum Hydrocarbons Analyses - VPH 11
B336504 11
Flag/Qualifier Summary 13
Certifications 14
Chain of Custody/Sample Receipt 15
Page 2 of 17
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/12/2023
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
ATTN: Taylor Cannon
92659938
23D0499
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Race Track Petro
MW-1R 23D0499-01 Water MADEP-VPH-Feb
2018 Rev 2.1
MW-2 23D0499-02 Water MADEP-VPH-Feb
2018 Rev 2.1
MW-4 23D0499-03 Water MADEP-VPH-Feb
2018 Rev 2.1
WSW-1 23D0499-04 Water MADEP-VPH-Feb
2018 Rev 2.1
WSW-2 23D0499-05 Water MADEP-VPH-Feb
2018 Rev 2.1
[TOC_1]Sample Summary[TOC]
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CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
For VPH analysis, the average of the three marker compounds passes criteria.
Analyte & Samples(s) Qualified:
V-37
2-Methylpentane
S085831-CCV1
Butylcyclohexane
S085831-CCV1
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
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Date Received: 4/5/2023
Work Order: 23D0499Sample Description:Project Location: Race Track Petro
Sample ID: 23D0499-01
Field Sample #: MW-1R
Sample Matrix: Water
Sampled: 3/30/2023 11:35
[TOC_2]23D0499-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
27000 2000 4/8/23 2:57 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
20Unadjusted C5-C8 Aliphatics
26000 2000 4/8/23 2:57 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
20C5-C8 Aliphatics
18000 2000 4/8/23 2:57 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
20Unadjusted C9-C12 Aliphatics
ND 2000 4/8/23 2:57 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
20C9-C12 Aliphatics
9400 2000 4/8/23 2:57 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
20C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)105 4/8/23 2:5770-130
2,5-Dibromotoluene (PID)107 4/8/23 2:5770-130
[TOC_1]Sample Results[TOC]
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Date Received: 4/5/2023
Work Order: 23D0499Sample Description:Project Location: Race Track Petro
Sample ID: 23D0499-02
Field Sample #: MW-2
Sample Matrix: Water
Sampled: 3/30/2023 11:00
[TOC_2]23D0499-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 4/7/23 17:21 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 4/7/23 17:21 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 4/7/23 17:21 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 4/7/23 17:21 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 4/7/23 17:21 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)82.8 4/7/23 17:2170-130
2,5-Dibromotoluene (PID)86.4 4/7/23 17:2170-130
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Date Received: 4/5/2023
Work Order: 23D0499Sample Description:Project Location: Race Track Petro
Sample ID: 23D0499-03
Field Sample #: MW-4
Sample Matrix: Water
Sampled: 3/30/2023 11:50
[TOC_2]23D0499-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 4/7/23 18:01 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 4/7/23 18:01 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 4/7/23 18:01 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 4/7/23 18:01 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 4/7/23 18:01 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)79.4 4/7/23 18:0170-130
2,5-Dibromotoluene (PID)86.0 4/7/23 18:0170-130
Page 7 of 17
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Date Received: 4/5/2023
Work Order: 23D0499Sample Description:Project Location: Race Track Petro
Sample ID: 23D0499-04
Field Sample #: WSW-1
Sample Matrix: Water
Sampled: 3/30/2023 12:10
[TOC_2]23D0499-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 4/7/23 18:40 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 4/7/23 18:40 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 4/7/23 18:40 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 4/7/23 18:40 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 4/7/23 18:40 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)86.1 4/7/23 18:4070-130
2,5-Dibromotoluene (PID)91.9 4/7/23 18:4070-130
Page 8 of 17
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Date Received: 4/5/2023
Work Order: 23D0499Sample Description:Project Location: Race Track Petro
Sample ID: 23D0499-05
Field Sample #: WSW-2
Sample Matrix: Water
Sampled: 3/30/2023 12:20
[TOC_2]23D0499-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 4/7/23 19:18 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 4/7/23 19:18 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 4/7/23 19:18 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 4/7/23 19:18 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 4/7/23 19:18 EEHµg/L 4/7/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)89.3 4/7/23 19:1870-130
2,5-Dibromotoluene (PID)99.3 4/7/23 19:1870-130
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Sample Extraction Data
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B336504 04/07/230.25 5.0023D0499-01 [MW-1R]
B336504 04/07/235 5.0023D0499-02 [MW-2]
B336504 04/07/235 5.0023D0499-03 [MW-4]
B336504 04/07/235 5.0023D0499-04 [WSW-1]
B336504 04/07/235 5.0023D0499-05 [WSW-2]
[TOC_1]Sample Preparation Information[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B336504 - MA VPH
[TOC_3]B336504[TOC]
Blank (B336504-BLK1) Prepared & Analyzed: 04/07/23
Unadjusted C5-C8 Aliphatics µg/L100ND
C5-C8 Aliphatics µg/L100ND
Unadjusted C9-C12 Aliphatics µg/L100ND
C9-C12 Aliphatics µg/L100ND
C9-C10 Aromatics µg/L100ND
Benzene µg/L1.0ND
Butylcyclohexane µg/L1.0ND
Decane µg/L1.0ND
Ethylbenzene µg/L1.0ND
Methyl tert-Butyl Ether (MTBE)µg/L1.0ND
2-Methylpentane µg/L1.0ND
Naphthalene µg/L5.0ND
Nonane µg/L1.0ND
Pentane µg/L1.0ND
Toluene µg/L1.0ND
1,2,4-Trimethylbenzene µg/L1.0ND
2,2,4-Trimethylpentane µg/L1.0ND
m+p Xylene µg/L2.0ND
o-Xylene µg/L1.0ND
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)84.433.7
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)93.637.4
LCS (B336504-BS1) Prepared & Analyzed: 04/07/23
Unadjusted C5-C8 Aliphatics µg/L100 150 70-13089.7135
Unadjusted C9-C12 Aliphatics µg/L100 150 70-130121181
C9-C10 Aromatics µg/L100 50.0 70-13087.143.6
Benzene µg/L1.0 50.0 70-13097.148.6
Butylcyclohexane µg/L1.0 50.0 70-13012863.8
Decane µg/L1.0 50.0 70-13010954.6
Ethylbenzene µg/L1.0 50.0 70-13085.642.8
Methyl tert-Butyl Ether (MTBE)µg/L1.0 50.0 70-13080.040.0
2-Methylpentane µg/L1.0 50.0 70-13096.248.1
Naphthalene µg/L5.0 50.0 70-13011055.0
Nonane µg/L1.0 50.0 70-13012663.1
Pentane µg/L1.0 50.0 70-13092.846.4
Toluene µg/L1.0 50.0 70-13085.142.5
1,2,4-Trimethylbenzene µg/L1.0 50.0 70-13087.143.6
2,2,4-Trimethylpentane µg/L1.0 50.0 70-13080.140.0
m+p Xylene µg/L2.0 100 70-13087.187.1
o-Xylene µg/L1.0 50.0 70-13087.843.9
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10642.4
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10542.0
[TOC_1]QC Data[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B336504 - MA VPH
LCS Dup (B336504-BSD1) Prepared & Analyzed: 04/07/23
Unadjusted C5-C8 Aliphatics µg/L100 150 2570-13093.3 3.91140
Unadjusted C9-C12 Aliphatics µg/L100 150 2570-130123 1.58184
C9-C10 Aromatics µg/L100 50.0 2570-13087.6 0.59743.8
Benzene µg/L1.0 50.0 2570-13097.5 0.44048.8
Butylcyclohexane µg/L1.0 50.0 2570-130129 1.0764.5
Decane µg/L1.0 50.0 2570-130110 1.0955.2
Ethylbenzene µg/L1.0 50.0 2570-13087.4 2.0943.7
Methyl tert-Butyl Ether (MTBE)µg/L1.0 50.0 2570-13088.4 9.9844.2
2-Methylpentane µg/L1.0 50.0 2570-130101 5.0550.6
Naphthalene µg/L5.0 50.0 2570-130119 8.0959.6
Nonane µg/L1.0 50.0 2570-130129 2.5064.7
Pentane µg/L1.0 50.0 2570-13090.3 2.7245.2
Toluene µg/L1.0 50.0 2570-13087.0 2.1943.5
1,2,4-Trimethylbenzene µg/L1.0 50.0 2570-13087.6 0.59743.8
2,2,4-Trimethylpentane µg/L1.0 50.0 2570-13088.3 9.7844.1
m+p Xylene µg/L2.0 100 2570-13089.4 2.6489.4
o-Xylene µg/L1.0 50.0 2570-13089.9 2.4445.0
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10140.5
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11144.5
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
For VPH analysis, the average of the three marker compounds passes criteria.V-37
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Water
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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ANALYTICAL REPORT
October 31, 2023
Crawford Environmental Services
Sample Delivery Group:L1669213
Samples Received:10/21/2023
Project Number:
Description:Energy Dispatch
Report To:James Coleman
1701 Shenandoah Ave., NW
Roanoke, VA 24017
Entire Report Reviewed By:
October 31, 2023
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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October 31, 2023
Heather J Wagner
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-1R2 L1669213-01 5
MW-2 L1669213-02 7
MW-4R L1669213-03 9
WSW-1 L1669213-04 11
WSW-2 L1669213-05 13
Qc: Quality Control Summary 15
Volatile Petroleum Hydrocarbons by Method MADEPV 15
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 16
Gl: Glossary of Terms 24
Al: Accreditations & Locations 25
Sc: Sample Chain of Custody 26
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1R2 L1669213-01 GW Jacob Wagner 10/19/23 14:20 10/21/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG2159944 100 10/29/23 06:32 10/29/23 06:32 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2159937 100 10/28/23 22:03 10/28/23 22:03 JBE Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1669213-02 GW Jacob Wagner 10/19/23 13:45 10/21/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG2159944 1 10/29/23 03:27 10/29/23 03:27 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2159937 1 10/28/23 16:56 10/28/23 16:56 JBE Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4R L1669213-03 GW Jacob Wagner 10/19/23 14:40 10/21/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG2159944 1 10/29/23 04:04 10/29/23 04:04 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2159937 1 10/28/23 17:18 10/28/23 17:18 JBE Mt. Juliet, TN
Collected by Collected date/time Received date/time
WSW-1 L1669213-04 GW Jacob Wagner 10/19/23 15:20 10/21/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG2159944 1 10/29/23 04:41 10/29/23 04:41 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2159937 1 10/28/23 17:40 10/28/23 17:40 JBE Mt. Juliet, TN
Collected by Collected date/time Received date/time
WSW-2 L1669213-05 GW Jacob Wagner 10/19/23 15:50 10/21/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG2159944 1 10/29/23 05:18 10/29/23 05:18 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2159937 1 10/28/23 18:02 10/28/23 18:02 JBE Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Heather J Wagner
Project Manager
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SAMPLE RESULTS - 01
L1669213
MW-1R2
Collected date/time: 10/19/23 14:20
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 15600 3330 10000 100 10/29/2023 06:32 WG2159944
Unadjusted C9-C12 Aliphatics 11200 3330 10000 100 10/29/2023 06:32 WG2159944
Unadjusted C9-C10 Aromatics 9900 B J 3330 10000 100 10/29/2023 06:32 WG2159944
Total VPH 36700 B 3330 10000 100 10/29/2023 06:32 WG2159944
(S) 2,5-Dibromotoluene(FID)85.5 70.0-130 10/29/2023 06:32 WG2159944
(S) 2,5-Dibromotoluene(PID)73.9 70.0-130 10/29/2023 06:32 WG2159944
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 1130 5000 100 10/28/2023 22:03 WG2159937
Acrolein U 254 5000 100 10/28/2023 22:03 WG2159937
Acrylonitrile U 67.1 1000 100 10/28/2023 22:03 WG2159937
Benzene 97.3 J 9.41 100 100 10/28/2023 22:03 WG2159937
Bromobenzene U 11.8 100 100 10/28/2023 22:03 WG2159937
Bromodichloromethane U 13.6 100 100 10/28/2023 22:03 WG2159937
Bromoform U 12.9 100 100 10/28/2023 22:03 WG2159937
Bromomethane U 60.5 500 100 10/28/2023 22:03 WG2159937
n-Butylbenzene 68.2 J 15.7 100 100 10/28/2023 22:03 WG2159937
sec-Butylbenzene 18.5 J 12.5 100 100 10/28/2023 22:03 WG2159937
tert-Butylbenzene U 12.7 100 100 10/28/2023 22:03 WG2159937
Carbon tetrachloride U 12.8 100 100 10/28/2023 22:03 WG2159937
Chlorobenzene U 11.6 100 100 10/28/2023 22:03 WG2159937
Chlorodibromomethane U 14.0 100 100 10/28/2023 22:03 WG2159937
Chloroethane U 19.2 500 100 10/28/2023 22:03 WG2159937
Chloroform U 11.1 500 100 10/28/2023 22:03 WG2159937
Chloromethane U 96.0 250 100 10/28/2023 22:03 WG2159937
2-Chlorotoluene U 10.6 100 100 10/28/2023 22:03 WG2159937
4-Chlorotoluene U 11.4 100 100 10/28/2023 22:03 WG2159937
1,2-Dibromo-3-Chloropropane U 27.6 500 100 10/28/2023 22:03 WG2159937
1,2-Dibromoethane U 12.6 100 100 10/28/2023 22:03 WG2159937
Dibromomethane U 12.2 100 100 10/28/2023 22:03 WG2159937
1,2-Dichlorobenzene U 10.7 100 100 10/28/2023 22:03 WG2159937
1,3-Dichlorobenzene U 11.0 100 100 10/28/2023 22:03 WG2159937
1,4-Dichlorobenzene U 12.0 100 100 10/28/2023 22:03 WG2159937
Dichlorodifluoromethane U 37.4 500 100 10/28/2023 22:03 WG2159937
1,1-Dichloroethane U 10.0 100 100 10/28/2023 22:03 WG2159937
1,2-Dichloroethane U 8.19 100 100 10/28/2023 22:03 WG2159937
1,1-Dichloroethene U 18.8 100 100 10/28/2023 22:03 WG2159937
cis-1,2-Dichloroethene U 12.6 100 100 10/28/2023 22:03 WG2159937
trans-1,2-Dichloroethene U 14.9 100 100 10/28/2023 22:03 WG2159937
1,2-Dichloropropane U 14.9 100 100 10/28/2023 22:03 WG2159937
1,1-Dichloropropene U 14.2 100 100 10/28/2023 22:03 WG2159937
1,3-Dichloropropane U 11.0 100 100 10/28/2023 22:03 WG2159937
2,2-Dichloropropane U 16.1 100 100 10/28/2023 22:03 WG2159937
Di-isopropyl ether U 10.5 100 100 10/28/2023 22:03 WG2159937
Ethylbenzene 2220 13.7 100 100 10/28/2023 22:03 WG2159937
Hexachloro-1,3-butadiene U 33.7 100 100 10/28/2023 22:03 WG2159937
Isopropylbenzene 85.8 J 10.5 100 100 10/28/2023 22:03 WG2159937
p-Isopropyltoluene U 12.0 100 100 10/28/2023 22:03 WG2159937
2-Butanone (MEK)U 119 1000 100 10/28/2023 22:03 WG2159937
Methylene Chloride U 43.0 500 100 10/28/2023 22:03 WG2159937
4-Methyl-2-pentanone (MIBK)U 47.8 1000 100 10/28/2023 22:03 WG2159937
Methyl tert-butyl ether U 10.1 100 100 10/28/2023 22:03 WG2159937
Naphthalene 556 100 500 100 10/28/2023 22:03 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1669213
MW-1R2
Collected date/time: 10/19/23 14:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
n-Propylbenzene 351 9.93 100 100 10/28/2023 22:03 WG2159937
Styrene U 11.8 100 100 10/28/2023 22:03 WG2159937
1,1,1,2-Tetrachloroethane U 14.7 100 100 10/28/2023 22:03 WG2159937
1,1,2,2-Tetrachloroethane U 13.3 100 100 10/28/2023 22:03 WG2159937
Tetrachloroethene U 30.0 100 100 10/28/2023 22:03 WG2159937
Toluene 447 27.8 100 100 10/28/2023 22:03 WG2159937
1,2,3-Trichlorobenzene U 23.0 100 100 10/28/2023 22:03 WG2159937
1,2,4-Trichlorobenzene U 48.1 100 100 10/28/2023 22:03 WG2159937
1,1,1-Trichloroethane U 14.9 100 100 10/28/2023 22:03 WG2159937
1,1,2-Trichloroethane U 15.8 100 100 10/28/2023 22:03 WG2159937
Trichloroethene U 19.0 100 100 10/28/2023 22:03 WG2159937
Trichlorofluoromethane U 16.0 500 100 10/28/2023 22:03 WG2159937
1,2,3-Trichloropropane U 23.7 250 100 10/28/2023 22:03 WG2159937
1,2,4-Trimethylbenzene 2740 32.2 100 100 10/28/2023 22:03 WG2159937
1,3,5-Trimethylbenzene 686 10.4 100 100 10/28/2023 22:03 WG2159937
Vinyl chloride U 23.4 100 100 10/28/2023 22:03 WG2159937
o-Xylene 796 17.4 100 100 10/28/2023 22:03 WG2159937
m&p-Xylenes 6180 43.0 200 100 10/28/2023 22:03 WG2159937
(S) Toluene-d8 102 80.0-120 10/28/2023 22:03 WG2159937
(S) 4-Bromofluorobenzene 95.6 77.0-126 10/28/2023 22:03 WG2159937
(S) 1,2-Dichloroethane-d4 102 70.0-130 10/28/2023 22:03 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1669213
MW-2
Collected date/time: 10/19/23 13:45
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics U 33.3 100 1 10/29/2023 03:27 WG2159944
Unadjusted C9-C12 Aliphatics U 33.3 100 1 10/29/2023 03:27 WG2159944
Unadjusted C9-C10 Aromatics 52.0 B J 33.3 100 1 10/29/2023 03:27 WG2159944
Total VPH 52.0 B J 33.3 100 1 10/29/2023 03:27 WG2159944
(S) 2,5-Dibromotoluene(FID)87.0 70.0-130 10/29/2023 03:27 WG2159944
(S) 2,5-Dibromotoluene(PID)75.1 70.0-130 10/29/2023 03:27 WG2159944
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 11.3 50.0 1 10/28/2023 16:56 WG2159937
Acrolein U 2.54 50.0 1 10/28/2023 16:56 WG2159937
Acrylonitrile U 0.671 10.0 1 10/28/2023 16:56 WG2159937
Benzene U 0.0941 1.00 1 10/28/2023 16:56 WG2159937
Bromobenzene U 0.118 1.00 1 10/28/2023 16:56 WG2159937
Bromodichloromethane U 0.136 1.00 1 10/28/2023 16:56 WG2159937
Bromoform U 0.129 1.00 1 10/28/2023 16:56 WG2159937
Bromomethane U 0.605 5.00 1 10/28/2023 16:56 WG2159937
n-Butylbenzene U 0.157 1.00 1 10/28/2023 16:56 WG2159937
sec-Butylbenzene U 0.125 1.00 1 10/28/2023 16:56 WG2159937
tert-Butylbenzene U 0.127 1.00 1 10/28/2023 16:56 WG2159937
Carbon tetrachloride U 0.128 1.00 1 10/28/2023 16:56 WG2159937
Chlorobenzene U 0.116 1.00 1 10/28/2023 16:56 WG2159937
Chlorodibromomethane U 0.140 1.00 1 10/28/2023 16:56 WG2159937
Chloroethane U 0.192 5.00 1 10/28/2023 16:56 WG2159937
Chloroform U 0.111 5.00 1 10/28/2023 16:56 WG2159937
Chloromethane U 0.960 2.50 1 10/28/2023 16:56 WG2159937
2-Chlorotoluene U 0.106 1.00 1 10/28/2023 16:56 WG2159937
4-Chlorotoluene U 0.114 1.00 1 10/28/2023 16:56 WG2159937
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 10/28/2023 16:56 WG2159937
1,2-Dibromoethane U 0.126 1.00 1 10/28/2023 16:56 WG2159937
Dibromomethane U 0.122 1.00 1 10/28/2023 16:56 WG2159937
1,2-Dichlorobenzene U 0.107 1.00 1 10/28/2023 16:56 WG2159937
1,3-Dichlorobenzene U 0.110 1.00 1 10/28/2023 16:56 WG2159937
1,4-Dichlorobenzene U 0.120 1.00 1 10/28/2023 16:56 WG2159937
Dichlorodifluoromethane U 0.374 5.00 1 10/28/2023 16:56 WG2159937
1,1-Dichloroethane U 0.100 1.00 1 10/28/2023 16:56 WG2159937
1,2-Dichloroethane U 0.0819 1.00 1 10/28/2023 16:56 WG2159937
1,1-Dichloroethene U 0.188 1.00 1 10/28/2023 16:56 WG2159937
cis-1,2-Dichloroethene U 0.126 1.00 1 10/28/2023 16:56 WG2159937
trans-1,2-Dichloroethene U 0.149 1.00 1 10/28/2023 16:56 WG2159937
1,2-Dichloropropane U 0.149 1.00 1 10/28/2023 16:56 WG2159937
1,1-Dichloropropene U 0.142 1.00 1 10/28/2023 16:56 WG2159937
1,3-Dichloropropane U 0.110 1.00 1 10/28/2023 16:56 WG2159937
2,2-Dichloropropane U 0.161 1.00 1 10/28/2023 16:56 WG2159937
Di-isopropyl ether U 0.105 1.00 1 10/28/2023 16:56 WG2159937
Ethylbenzene U 0.137 1.00 1 10/28/2023 16:56 WG2159937
Hexachloro-1,3-butadiene U 0.337 1.00 1 10/28/2023 16:56 WG2159937
Isopropylbenzene U 0.105 1.00 1 10/28/2023 16:56 WG2159937
p-Isopropyltoluene U 0.120 1.00 1 10/28/2023 16:56 WG2159937
2-Butanone (MEK)U 1.19 10.0 1 10/28/2023 16:56 WG2159937
Methylene Chloride U 0.430 5.00 1 10/28/2023 16:56 WG2159937
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 10/28/2023 16:56 WG2159937
Methyl tert-butyl ether U 0.101 1.00 1 10/28/2023 16:56 WG2159937
Naphthalene U 1.00 5.00 1 10/28/2023 16:56 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1669213
MW-2
Collected date/time: 10/19/23 13:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
n-Propylbenzene U 0.0993 1.00 1 10/28/2023 16:56 WG2159937
Styrene U 0.118 1.00 1 10/28/2023 16:56 WG2159937
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 10/28/2023 16:56 WG2159937
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 10/28/2023 16:56 WG2159937
Tetrachloroethene U 0.300 1.00 1 10/28/2023 16:56 WG2159937
Toluene U 0.278 1.00 1 10/28/2023 16:56 WG2159937
1,2,3-Trichlorobenzene U 0.230 1.00 1 10/28/2023 16:56 WG2159937
1,2,4-Trichlorobenzene U 0.481 1.00 1 10/28/2023 16:56 WG2159937
1,1,1-Trichloroethane U 0.149 1.00 1 10/28/2023 16:56 WG2159937
1,1,2-Trichloroethane U 0.158 1.00 1 10/28/2023 16:56 WG2159937
Trichloroethene U 0.190 1.00 1 10/28/2023 16:56 WG2159937
Trichlorofluoromethane U 0.160 5.00 1 10/28/2023 16:56 WG2159937
1,2,3-Trichloropropane U 0.237 2.50 1 10/28/2023 16:56 WG2159937
1,2,4-Trimethylbenzene U 0.322 1.00 1 10/28/2023 16:56 WG2159937
1,3,5-Trimethylbenzene U 0.104 1.00 1 10/28/2023 16:56 WG2159937
Vinyl chloride U 0.234 1.00 1 10/28/2023 16:56 WG2159937
o-Xylene U 0.174 1.00 1 10/28/2023 16:56 WG2159937
m&p-Xylenes U 0.430 2.00 1 10/28/2023 16:56 WG2159937
(S) Toluene-d8 103 80.0-120 10/28/2023 16:56 WG2159937
(S) 4-Bromofluorobenzene 99.8 77.0-126 10/28/2023 16:56 WG2159937
(S) 1,2-Dichloroethane-d4 102 70.0-130 10/28/2023 16:56 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 03
L1669213
MW-4R
Collected date/time: 10/19/23 14:40
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 128 33.3 100 1 10/29/2023 04:04 WG2159944
Unadjusted C9-C12 Aliphatics U 33.3 100 1 10/29/2023 04:04 WG2159944
Unadjusted C9-C10 Aromatics 45.8 B J 33.3 100 1 10/29/2023 04:04 WG2159944
Total VPH 174 B 33.3 100 1 10/29/2023 04:04 WG2159944
(S) 2,5-Dibromotoluene(FID)86.4 70.0-130 10/29/2023 04:04 WG2159944
(S) 2,5-Dibromotoluene(PID)74.6 70.0-130 10/29/2023 04:04 WG2159944
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 11.3 50.0 1 10/28/2023 17:18 WG2159937
Acrolein U 2.54 50.0 1 10/28/2023 17:18 WG2159937
Acrylonitrile U 0.671 10.0 1 10/28/2023 17:18 WG2159937
Benzene 0.785 J 0.0941 1.00 1 10/28/2023 17:18 WG2159937
Bromobenzene U 0.118 1.00 1 10/28/2023 17:18 WG2159937
Bromodichloromethane U 0.136 1.00 1 10/28/2023 17:18 WG2159937
Bromoform U 0.129 1.00 1 10/28/2023 17:18 WG2159937
Bromomethane U 0.605 5.00 1 10/28/2023 17:18 WG2159937
n-Butylbenzene U 0.157 1.00 1 10/28/2023 17:18 WG2159937
sec-Butylbenzene 0.585 J 0.125 1.00 1 10/28/2023 17:18 WG2159937
tert-Butylbenzene U 0.127 1.00 1 10/28/2023 17:18 WG2159937
Carbon tetrachloride U 0.128 1.00 1 10/28/2023 17:18 WG2159937
Chlorobenzene U 0.116 1.00 1 10/28/2023 17:18 WG2159937
Chlorodibromomethane U 0.140 1.00 1 10/28/2023 17:18 WG2159937
Chloroethane U 0.192 5.00 1 10/28/2023 17:18 WG2159937
Chloroform U 0.111 5.00 1 10/28/2023 17:18 WG2159937
Chloromethane U 0.960 2.50 1 10/28/2023 17:18 WG2159937
2-Chlorotoluene U 0.106 1.00 1 10/28/2023 17:18 WG2159937
4-Chlorotoluene U 0.114 1.00 1 10/28/2023 17:18 WG2159937
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 10/28/2023 17:18 WG2159937
1,2-Dibromoethane U 0.126 1.00 1 10/28/2023 17:18 WG2159937
Dibromomethane U 0.122 1.00 1 10/28/2023 17:18 WG2159937
1,2-Dichlorobenzene U 0.107 1.00 1 10/28/2023 17:18 WG2159937
1,3-Dichlorobenzene U 0.110 1.00 1 10/28/2023 17:18 WG2159937
1,4-Dichlorobenzene U 0.120 1.00 1 10/28/2023 17:18 WG2159937
Dichlorodifluoromethane U 0.374 5.00 1 10/28/2023 17:18 WG2159937
1,1-Dichloroethane U 0.100 1.00 1 10/28/2023 17:18 WG2159937
1,2-Dichloroethane U 0.0819 1.00 1 10/28/2023 17:18 WG2159937
1,1-Dichloroethene U 0.188 1.00 1 10/28/2023 17:18 WG2159937
cis-1,2-Dichloroethene U 0.126 1.00 1 10/28/2023 17:18 WG2159937
trans-1,2-Dichloroethene U 0.149 1.00 1 10/28/2023 17:18 WG2159937
1,2-Dichloropropane U 0.149 1.00 1 10/28/2023 17:18 WG2159937
1,1-Dichloropropene U 0.142 1.00 1 10/28/2023 17:18 WG2159937
1,3-Dichloropropane U 0.110 1.00 1 10/28/2023 17:18 WG2159937
2,2-Dichloropropane U 0.161 1.00 1 10/28/2023 17:18 WG2159937
Di-isopropyl ether U 0.105 1.00 1 10/28/2023 17:18 WG2159937
Ethylbenzene 0.148 J 0.137 1.00 1 10/28/2023 17:18 WG2159937
Hexachloro-1,3-butadiene U 0.337 1.00 1 10/28/2023 17:18 WG2159937
Isopropylbenzene 0.326 J 0.105 1.00 1 10/28/2023 17:18 WG2159937
p-Isopropyltoluene U 0.120 1.00 1 10/28/2023 17:18 WG2159937
2-Butanone (MEK)U 1.19 10.0 1 10/28/2023 17:18 WG2159937
Methylene Chloride U 0.430 5.00 1 10/28/2023 17:18 WG2159937
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 10/28/2023 17:18 WG2159937
Methyl tert-butyl ether 0.385 J 0.101 1.00 1 10/28/2023 17:18 WG2159937
Naphthalene U 1.00 5.00 1 10/28/2023 17:18 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 03
L1669213
MW-4R
Collected date/time: 10/19/23 14:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
n-Propylbenzene 0.185 J 0.0993 1.00 1 10/28/2023 17:18 WG2159937
Styrene U 0.118 1.00 1 10/28/2023 17:18 WG2159937
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 10/28/2023 17:18 WG2159937
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 10/28/2023 17:18 WG2159937
Tetrachloroethene U 0.300 1.00 1 10/28/2023 17:18 WG2159937
Toluene 0.365 J 0.278 1.00 1 10/28/2023 17:18 WG2159937
1,2,3-Trichlorobenzene U 0.230 1.00 1 10/28/2023 17:18 WG2159937
1,2,4-Trichlorobenzene U 0.481 1.00 1 10/28/2023 17:18 WG2159937
1,1,1-Trichloroethane U 0.149 1.00 1 10/28/2023 17:18 WG2159937
1,1,2-Trichloroethane U 0.158 1.00 1 10/28/2023 17:18 WG2159937
Trichloroethene U 0.190 1.00 1 10/28/2023 17:18 WG2159937
Trichlorofluoromethane U 0.160 5.00 1 10/28/2023 17:18 WG2159937
1,2,3-Trichloropropane U 0.237 2.50 1 10/28/2023 17:18 WG2159937
1,2,4-Trimethylbenzene U 0.322 1.00 1 10/28/2023 17:18 WG2159937
1,3,5-Trimethylbenzene U 0.104 1.00 1 10/28/2023 17:18 WG2159937
Vinyl chloride U 0.234 1.00 1 10/28/2023 17:18 WG2159937
o-Xylene U 0.174 1.00 1 10/28/2023 17:18 WG2159937
m&p-Xylenes U 0.430 2.00 1 10/28/2023 17:18 WG2159937
(S) Toluene-d8 103 80.0-120 10/28/2023 17:18 WG2159937
(S) 4-Bromofluorobenzene 98.3 77.0-126 10/28/2023 17:18 WG2159937
(S) 1,2-Dichloroethane-d4 104 70.0-130 10/28/2023 17:18 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1669213
WSW-1
Collected date/time: 10/19/23 15:20
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics U 33.3 100 1 10/29/2023 04:41 WG2159944
Unadjusted C9-C12 Aliphatics U 33.3 100 1 10/29/2023 04:41 WG2159944
Unadjusted C9-C10 Aromatics 51.1 B J 33.3 100 1 10/29/2023 04:41 WG2159944
Total VPH 51.1 B J 33.3 100 1 10/29/2023 04:41 WG2159944
(S) 2,5-Dibromotoluene(FID)86.5 70.0-130 10/29/2023 04:41 WG2159944
(S) 2,5-Dibromotoluene(PID)74.7 70.0-130 10/29/2023 04:41 WG2159944
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 11.3 50.0 1 10/28/2023 17:40 WG2159937
Acrolein U 2.54 50.0 1 10/28/2023 17:40 WG2159937
Acrylonitrile U 0.671 10.0 1 10/28/2023 17:40 WG2159937
Benzene 1.54 0.0941 1.00 1 10/28/2023 17:40 WG2159937
Bromobenzene U 0.118 1.00 1 10/28/2023 17:40 WG2159937
Bromodichloromethane U 0.136 1.00 1 10/28/2023 17:40 WG2159937
Bromoform U 0.129 1.00 1 10/28/2023 17:40 WG2159937
Bromomethane U 0.605 5.00 1 10/28/2023 17:40 WG2159937
n-Butylbenzene U 0.157 1.00 1 10/28/2023 17:40 WG2159937
sec-Butylbenzene U 0.125 1.00 1 10/28/2023 17:40 WG2159937
tert-Butylbenzene U 0.127 1.00 1 10/28/2023 17:40 WG2159937
Carbon tetrachloride U 0.128 1.00 1 10/28/2023 17:40 WG2159937
Chlorobenzene U 0.116 1.00 1 10/28/2023 17:40 WG2159937
Chlorodibromomethane U 0.140 1.00 1 10/28/2023 17:40 WG2159937
Chloroethane U 0.192 5.00 1 10/28/2023 17:40 WG2159937
Chloroform 1.06 J 0.111 5.00 1 10/28/2023 17:40 WG2159937
Chloromethane U 0.960 2.50 1 10/28/2023 17:40 WG2159937
2-Chlorotoluene U 0.106 1.00 1 10/28/2023 17:40 WG2159937
4-Chlorotoluene U 0.114 1.00 1 10/28/2023 17:40 WG2159937
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 10/28/2023 17:40 WG2159937
1,2-Dibromoethane U 0.126 1.00 1 10/28/2023 17:40 WG2159937
Dibromomethane U 0.122 1.00 1 10/28/2023 17:40 WG2159937
1,2-Dichlorobenzene 0.321 J 0.107 1.00 1 10/28/2023 17:40 WG2159937
1,3-Dichlorobenzene U 0.110 1.00 1 10/28/2023 17:40 WG2159937
1,4-Dichlorobenzene U 0.120 1.00 1 10/28/2023 17:40 WG2159937
Dichlorodifluoromethane U 0.374 5.00 1 10/28/2023 17:40 WG2159937
1,1-Dichloroethane U 0.100 1.00 1 10/28/2023 17:40 WG2159937
1,2-Dichloroethane U 0.0819 1.00 1 10/28/2023 17:40 WG2159937
1,1-Dichloroethene U 0.188 1.00 1 10/28/2023 17:40 WG2159937
cis-1,2-Dichloroethene U 0.126 1.00 1 10/28/2023 17:40 WG2159937
trans-1,2-Dichloroethene U 0.149 1.00 1 10/28/2023 17:40 WG2159937
1,2-Dichloropropane U 0.149 1.00 1 10/28/2023 17:40 WG2159937
1,1-Dichloropropene U 0.142 1.00 1 10/28/2023 17:40 WG2159937
1,3-Dichloropropane U 0.110 1.00 1 10/28/2023 17:40 WG2159937
2,2-Dichloropropane U 0.161 1.00 1 10/28/2023 17:40 WG2159937
Di-isopropyl ether U 0.105 1.00 1 10/28/2023 17:40 WG2159937
Ethylbenzene U 0.137 1.00 1 10/28/2023 17:40 WG2159937
Hexachloro-1,3-butadiene U 0.337 1.00 1 10/28/2023 17:40 WG2159937
Isopropylbenzene 0.267 J 0.105 1.00 1 10/28/2023 17:40 WG2159937
p-Isopropyltoluene U 0.120 1.00 1 10/28/2023 17:40 WG2159937
2-Butanone (MEK)U 1.19 10.0 1 10/28/2023 17:40 WG2159937
Methylene Chloride U 0.430 5.00 1 10/28/2023 17:40 WG2159937
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 10/28/2023 17:40 WG2159937
Methyl tert-butyl ether 0.409 J 0.101 1.00 1 10/28/2023 17:40 WG2159937
Naphthalene U 1.00 5.00 1 10/28/2023 17:40 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 04
L1669213
WSW-1
Collected date/time: 10/19/23 15:20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
n-Propylbenzene 0.0994 J 0.0993 1.00 1 10/28/2023 17:40 WG2159937
Styrene U 0.118 1.00 1 10/28/2023 17:40 WG2159937
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 10/28/2023 17:40 WG2159937
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 10/28/2023 17:40 WG2159937
Tetrachloroethene U 0.300 1.00 1 10/28/2023 17:40 WG2159937
Toluene U 0.278 1.00 1 10/28/2023 17:40 WG2159937
1,2,3-Trichlorobenzene U 0.230 1.00 1 10/28/2023 17:40 WG2159937
1,2,4-Trichlorobenzene U 0.481 1.00 1 10/28/2023 17:40 WG2159937
1,1,1-Trichloroethane U 0.149 1.00 1 10/28/2023 17:40 WG2159937
1,1,2-Trichloroethane U 0.158 1.00 1 10/28/2023 17:40 WG2159937
Trichloroethene U 0.190 1.00 1 10/28/2023 17:40 WG2159937
Trichlorofluoromethane U 0.160 5.00 1 10/28/2023 17:40 WG2159937
1,2,3-Trichloropropane U 0.237 2.50 1 10/28/2023 17:40 WG2159937
1,2,4-Trimethylbenzene U 0.322 1.00 1 10/28/2023 17:40 WG2159937
1,3,5-Trimethylbenzene U 0.104 1.00 1 10/28/2023 17:40 WG2159937
Vinyl chloride U 0.234 1.00 1 10/28/2023 17:40 WG2159937
o-Xylene 0.808 J 0.174 1.00 1 10/28/2023 17:40 WG2159937
m&p-Xylenes U 0.430 2.00 1 10/28/2023 17:40 WG2159937
(S) Toluene-d8 103 80.0-120 10/28/2023 17:40 WG2159937
(S) 4-Bromofluorobenzene 96.8 77.0-126 10/28/2023 17:40 WG2159937
(S) 1,2-Dichloroethane-d4 103 70.0-130 10/28/2023 17:40 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1669213
WSW-2
Collected date/time: 10/19/23 15:50
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics U 33.3 100 1 10/29/2023 05:18 WG2159944
Unadjusted C9-C12 Aliphatics U 33.3 100 1 10/29/2023 05:18 WG2159944
Unadjusted C9-C10 Aromatics 50.6 B J 33.3 100 1 10/29/2023 05:18 WG2159944
Total VPH 50.6 B J 33.3 100 1 10/29/2023 05:18 WG2159944
(S) 2,5-Dibromotoluene(FID)85.0 70.0-130 10/29/2023 05:18 WG2159944
(S) 2,5-Dibromotoluene(PID)73.5 70.0-130 10/29/2023 05:18 WG2159944
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 11.3 50.0 1 10/28/2023 18:02 WG2159937
Acrolein U 2.54 50.0 1 10/28/2023 18:02 WG2159937
Acrylonitrile U 0.671 10.0 1 10/28/2023 18:02 WG2159937
Benzene U 0.0941 1.00 1 10/28/2023 18:02 WG2159937
Bromobenzene U 0.118 1.00 1 10/28/2023 18:02 WG2159937
Bromodichloromethane U 0.136 1.00 1 10/28/2023 18:02 WG2159937
Bromoform U 0.129 1.00 1 10/28/2023 18:02 WG2159937
Bromomethane U 0.605 5.00 1 10/28/2023 18:02 WG2159937
n-Butylbenzene U 0.157 1.00 1 10/28/2023 18:02 WG2159937
sec-Butylbenzene U 0.125 1.00 1 10/28/2023 18:02 WG2159937
tert-Butylbenzene U 0.127 1.00 1 10/28/2023 18:02 WG2159937
Carbon tetrachloride U 0.128 1.00 1 10/28/2023 18:02 WG2159937
Chlorobenzene U 0.116 1.00 1 10/28/2023 18:02 WG2159937
Chlorodibromomethane U 0.140 1.00 1 10/28/2023 18:02 WG2159937
Chloroethane U 0.192 5.00 1 10/28/2023 18:02 WG2159937
Chloroform 0.138 J 0.111 5.00 1 10/28/2023 18:02 WG2159937
Chloromethane U 0.960 2.50 1 10/28/2023 18:02 WG2159937
2-Chlorotoluene U 0.106 1.00 1 10/28/2023 18:02 WG2159937
4-Chlorotoluene U 0.114 1.00 1 10/28/2023 18:02 WG2159937
1,2-Dibromo-3-Chloropropane U 0.276 5.00 1 10/28/2023 18:02 WG2159937
1,2-Dibromoethane U 0.126 1.00 1 10/28/2023 18:02 WG2159937
Dibromomethane U 0.122 1.00 1 10/28/2023 18:02 WG2159937
1,2-Dichlorobenzene U 0.107 1.00 1 10/28/2023 18:02 WG2159937
1,3-Dichlorobenzene U 0.110 1.00 1 10/28/2023 18:02 WG2159937
1,4-Dichlorobenzene U 0.120 1.00 1 10/28/2023 18:02 WG2159937
Dichlorodifluoromethane U 0.374 5.00 1 10/28/2023 18:02 WG2159937
1,1-Dichloroethane U 0.100 1.00 1 10/28/2023 18:02 WG2159937
1,2-Dichloroethane U 0.0819 1.00 1 10/28/2023 18:02 WG2159937
1,1-Dichloroethene U 0.188 1.00 1 10/28/2023 18:02 WG2159937
cis-1,2-Dichloroethene U 0.126 1.00 1 10/28/2023 18:02 WG2159937
trans-1,2-Dichloroethene U 0.149 1.00 1 10/28/2023 18:02 WG2159937
1,2-Dichloropropane U 0.149 1.00 1 10/28/2023 18:02 WG2159937
1,1-Dichloropropene U 0.142 1.00 1 10/28/2023 18:02 WG2159937
1,3-Dichloropropane U 0.110 1.00 1 10/28/2023 18:02 WG2159937
2,2-Dichloropropane U 0.161 1.00 1 10/28/2023 18:02 WG2159937
Di-isopropyl ether U 0.105 1.00 1 10/28/2023 18:02 WG2159937
Ethylbenzene U 0.137 1.00 1 10/28/2023 18:02 WG2159937
Hexachloro-1,3-butadiene U 0.337 1.00 1 10/28/2023 18:02 WG2159937
Isopropylbenzene U 0.105 1.00 1 10/28/2023 18:02 WG2159937
p-Isopropyltoluene U 0.120 1.00 1 10/28/2023 18:02 WG2159937
2-Butanone (MEK)U 1.19 10.0 1 10/28/2023 18:02 WG2159937
Methylene Chloride U 0.430 5.00 1 10/28/2023 18:02 WG2159937
4-Methyl-2-pentanone (MIBK)U 0.478 10.0 1 10/28/2023 18:02 WG2159937
Methyl tert-butyl ether U 0.101 1.00 1 10/28/2023 18:02 WG2159937
Naphthalene U 1.00 5.00 1 10/28/2023 18:02 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 05
L1669213
WSW-2
Collected date/time: 10/19/23 15:50
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
n-Propylbenzene U 0.0993 1.00 1 10/28/2023 18:02 WG2159937
Styrene U 0.118 1.00 1 10/28/2023 18:02 WG2159937
1,1,1,2-Tetrachloroethane U 0.147 1.00 1 10/28/2023 18:02 WG2159937
1,1,2,2-Tetrachloroethane U 0.133 1.00 1 10/28/2023 18:02 WG2159937
Tetrachloroethene U 0.300 1.00 1 10/28/2023 18:02 WG2159937
Toluene U 0.278 1.00 1 10/28/2023 18:02 WG2159937
1,2,3-Trichlorobenzene U 0.230 1.00 1 10/28/2023 18:02 WG2159937
1,2,4-Trichlorobenzene U 0.481 1.00 1 10/28/2023 18:02 WG2159937
1,1,1-Trichloroethane U 0.149 1.00 1 10/28/2023 18:02 WG2159937
1,1,2-Trichloroethane U 0.158 1.00 1 10/28/2023 18:02 WG2159937
Trichloroethene U 0.190 1.00 1 10/28/2023 18:02 WG2159937
Trichlorofluoromethane U 0.160 5.00 1 10/28/2023 18:02 WG2159937
1,2,3-Trichloropropane U 0.237 2.50 1 10/28/2023 18:02 WG2159937
1,2,4-Trimethylbenzene U 0.322 1.00 1 10/28/2023 18:02 WG2159937
1,3,5-Trimethylbenzene U 0.104 1.00 1 10/28/2023 18:02 WG2159937
Vinyl chloride U 0.234 1.00 1 10/28/2023 18:02 WG2159937
o-Xylene U 0.174 1.00 1 10/28/2023 18:02 WG2159937
m&p-Xylenes U 0.430 2.00 1 10/28/2023 18:02 WG2159937
(S) Toluene-d8 103 80.0-120 10/28/2023 18:02 WG2159937
(S) 4-Bromofluorobenzene 95.1 77.0-126 10/28/2023 18:02 WG2159937
(S) 1,2-Dichloroethane-d4 102 70.0-130 10/28/2023 18:02 WG2159937
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG2159944
Volatile Petroleum Hydrocarbons by Method MADEPV L1669213-01,02,03,04,05
Method Blank (MB)
(MB) R3992524-3 10/28/23 16:20
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics 55.6 J 33.3 100
Total VPH 55.6 J 33.3 100
(S) 2,5-Dibromotoluene(FID)83.5 70.0-130
(S) 2,5-Dibromotoluene(PID)75.3 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3992524-1 10/28/23 13:52 • (LCSD) R3992524-2 10/28/23 14:29
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1180 1150 98.3 95.8 70.0-130 2.58 25
Unadjusted C9-C12 Aliphatics 1400 1220 1180 87.1 84.3 70.0-130 3.33 25
Unadjusted C9-C10 Aromatics 200 197 205 98.5 103 70.0-130 3.98 25
Total VPH 2800 2600 2540 92.9 90.7 70.0-130 2.33 25
(S) 2,5-Dibromotoluene(FID) 109 89.1 70.0-130
(S) 2,5-Dibromotoluene(PID) 99.4 80.6 70.0-130
L1670300-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1670300-02 10/28/23 17:34 • (MS) R3992524-4 10/28/23 20:39 • (MSD) R3992524-5 10/28/23 21:16
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 U 1050 1050 87.5 87.5 1 70.0-130 0.000 25
Unadjusted C9-C12 Aliphatics 1400 U 1070 991 76.4 70.8 1 70.0-130 7.67 25
Unadjusted C9-C10 Aromatics 200 U 176 169 88.0 84.5 1 70.0-130 4.06 25
Total VPH 2800 U 2300 2210 82.1 78.9 1 70.0-130 3.99 25
(S) 2,5-Dibromotoluene(FID) 80.8 83.2 70.0-130
(S) 2,5-Dibromotoluene(PID) 73.4 75.5 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2159937
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1669213-01,02,03,04,05
Method Blank (MB)
(MB) R3993206-4 10/28/23 14:35
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2159937
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1669213-01,02,03,04,05
Method Blank (MB)
(MB) R3993206-4 10/28/23 14:35
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
2-Butanone (MEK)U 1.19 10.0
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
(S) Toluene-d8 105 80.0-120
(S) 4-Bromofluorobenzene 94.8 77.0-126
(S) 1,2-Dichloroethane-d4 101 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3993206-1 10/28/23 12:23 • (LCSD) R3993206-2 10/28/23 12:45
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 24.8 24.5 99.2 98.0 19.0-160 1.22 27
Acrolein 25.0 21.0 22.8 84.0 91.2 10.0-160 8.22 26
Acrylonitrile 25.0 22.8 23.1 91.2 92.4 55.0-149 1.31 20
Benzene 5.00 5.04 5.15 101 103 70.0-123 2.16 20
Bromobenzene 5.00 5.28 5.47 106 109 73.0-121 3.53 20
Bromodichloromethane 5.00 5.15 5.40 103 108 75.0-120 4.74 20
Bromoform 5.00 4.42 4.37 88.4 87.4 68.0-132 1.14 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2159937
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1669213-01,02,03,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3993206-1 10/28/23 12:23 • (LCSD) R3993206-2 10/28/23 12:45
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 5.13 5.33 103 107 10.0-160 3.82 25
n-Butylbenzene 5.00 4.77 4.92 95.4 98.4 73.0-125 3.10 20
sec-Butylbenzene 5.00 5.12 5.14 102 103 75.0-125 0.390 20
tert-Butylbenzene 5.00 5.16 5.18 103 104 76.0-124 0.387 20
Carbon tetrachloride 5.00 4.90 5.16 98.0 103 68.0-126 5.17 20
Chlorobenzene 5.00 4.82 4.90 96.4 98.0 80.0-121 1.65 20
Chlorodibromomethane 5.00 5.30 5.38 106 108 77.0-125 1.50 20
Chloroethane 5.00 5.53 5.63 111 113 47.0-150 1.79 20
Chloroform 5.00 5.03 5.24 101 105 73.0-120 4.09 20
Chloromethane 5.00 4.61 4.69 92.2 93.8 41.0-142 1.72 20
2-Chlorotoluene 5.00 5.42 5.36 108 107 76.0-123 1.11 20
4-Chlorotoluene 5.00 5.23 5.36 105 107 75.0-122 2.46 20
1,2-Dibromo-3-Chloropropane 5.00 4.51 4.78 90.2 95.6 58.0-134 5.81 20
1,2-Dibromoethane 5.00 4.80 4.86 96.0 97.2 80.0-122 1.24 20
Dibromomethane 5.00 5.18 5.41 104 108 80.0-120 4.34 20
1,2-Dichlorobenzene 5.00 5.10 5.11 102 102 79.0-121 0.196 20
1,3-Dichlorobenzene 5.00 5.13 5.19 103 104 79.0-120 1.16 20
1,4-Dichlorobenzene 5.00 5.28 5.25 106 105 79.0-120 0.570 20
Dichlorodifluoromethane 5.00 5.96 5.97 119 119 51.0-149 0.168 20
1,1-Dichloroethane 5.00 4.60 4.86 92.0 97.2 70.0-126 5.50 20
1,2-Dichloroethane 5.00 5.06 5.17 101 103 70.0-128 2.15 20
1,1-Dichloroethene 5.00 5.19 5.49 104 110 71.0-124 5.62 20
cis-1,2-Dichloroethene 5.00 4.88 5.02 97.6 100 73.0-120 2.83 20
trans-1,2-Dichloroethene 5.00 4.92 5.16 98.4 103 73.0-120 4.76 20
1,2-Dichloropropane 5.00 4.93 5.02 98.6 100 77.0-125 1.81 20
1,1-Dichloropropene 5.00 5.35 5.52 107 110 74.0-126 3.13 20
1,3-Dichloropropane 5.00 5.16 5.23 103 105 80.0-120 1.35 20
2,2-Dichloropropane 5.00 4.15 4.36 83.0 87.2 58.0-130 4.94 20
Di-isopropyl ether 5.00 4.27 4.47 85.4 89.4 58.0-138 4.58 20
Ethylbenzene 5.00 4.77 4.85 95.4 97.0 79.0-123 1.66 20
Hexachloro-1,3-butadiene 5.00 4.60 4.76 92.0 95.2 54.0-138 3.42 20
Isopropylbenzene 5.00 4.80 4.88 96.0 97.6 76.0-127 1.65 20
p-Isopropyltoluene 5.00 5.11 5.08 102 102 76.0-125 0.589 20
2-Butanone (MEK)25.0 22.4 23.1 89.6 92.4 44.0-160 3.08 20
Methylene Chloride 5.00 4.94 5.15 98.8 103 67.0-120 4.16 20
4-Methyl-2-pentanone (MIBK)25.0 21.5 22.3 86.0 89.2 68.0-142 3.65 20
Methyl tert-butyl ether 5.00 4.84 5.06 96.8 101 68.0-125 4.44 20
Naphthalene 5.00 4.88 4.99 97.6 99.8 54.0-135 2.23 20
n-Propylbenzene 5.00 5.42 5.48 108 110 77.0-124 1.10 20
Styrene 5.00 4.36 4.36 87.2 87.2 73.0-130 0.000 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2159937
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1669213-01,02,03,04,05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3993206-1 10/28/23 12:23 • (LCSD) R3993206-2 10/28/23 12:45
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
1,1,1,2-Tetrachloroethane 5.00 4.61 4.68 92.2 93.6 75.0-125 1.51 20
1,1,2,2-Tetrachloroethane 5.00 5.60 5.58 112 112 65.0-130 0.358 20
Tetrachloroethene 5.00 4.88 4.86 97.6 97.2 72.0-132 0.411 20
Toluene 5.00 5.09 5.06 102 101 79.0-120 0.591 20
1,2,3-Trichlorobenzene 5.00 4.69 4.75 93.8 95.0 50.0-138 1.27 20
1,2,4-Trichlorobenzene 5.00 4.39 4.69 87.8 93.8 57.0-137 6.61 20
1,1,1-Trichloroethane 5.00 5.59 5.84 112 117 73.0-124 4.37 20
1,1,2-Trichloroethane 5.00 5.15 5.31 103 106 80.0-120 3.06 20
Trichloroethene 5.00 4.65 5.18 93.0 104 78.0-124 10.8 20
Trichlorofluoromethane 5.00 5.54 5.46 111 109 59.0-147 1.45 20
1,2,3-Trichloropropane 5.00 5.48 5.53 110 111 73.0-130 0.908 20
1,2,4-Trimethylbenzene 5.00 5.04 5.06 101 101 76.0-121 0.396 20
1,3,5-Trimethylbenzene 5.00 5.04 5.15 101 103 76.0-122 2.16 20
Vinyl chloride 5.00 5.17 5.26 103 105 67.0-131 1.73 20
o-Xylene 5.00 4.49 4.49 89.8 89.8 80.0-122 0.000 20
m&p-Xylenes 10.0 9.63 9.63 96.3 96.3 80.0-122 0.000 20
(S) Toluene-d8 103 103 80.0-120
(S) 4-Bromofluorobenzene 98.2 95.8 77.0-126
(S) 1,2-Dichloroethane-d4 104 106 70.0-130
L1668931-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1668931-13 10/28/23 16:34 • (MS) R3993206-5 10/28/23 23:09 • (MSD) R3993206-6 10/28/23 23:31
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acetone 25.0 74.7 126 121 205 185 1 10.0-160 J5 J5 4.05 35
Acrolein 25.0 12.0 38.8 40.8 107 115 1 10.0-160 5.03 39
Acrylonitrile 25.0 U 24.1 24.3 96.4 97.2 1 21.0-160 0.826 32
Benzene 5.00 U 2.81 2.90 56.2 58.0 1 17.0-158 3.15 27
Bromobenzene 5.00 U 3.52 4.55 70.4 91.0 1 30.0-149 V3 V3 25.5 28
Bromodichloromethane 5.00 U 2.66 2.94 53.2 58.8 1 31.0-150 10.0 27
Bromoform 5.00 U 3.00 3.13 60.0 62.6 1 29.0-150 4.24 29
Bromomethane 5.00 U 2.02 2.05 40.4 41.0 1 10.0-160 1.47 38
n-Butylbenzene 5.00 U 2.83 3.47 56.6 69.4 1 31.0-150 V3 V3 20.3 30
sec-Butylbenzene 5.00 U 2.88 3.88 57.6 77.6 1 33.0-155 V3 J3 V3 29.6 29
tert-Butylbenzene 5.00 U 2.82 3.74 56.4 74.8 1 34.0-153 V3 V3 28.0 28
Carbon tetrachloride 5.00 U 2.55 2.75 51.0 55.0 1 23.0-159 7.55 28
Chlorobenzene 5.00 U 2.26 2.49 45.2 49.8 1 33.0-152 9.68 27
Chlorodibromomethane 5.00 U 3.10 3.28 62.0 65.6 1 37.0-149 5.64 27
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2159937
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1669213-01,02,03,04,05
L1668931-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1668931-13 10/28/23 16:34 • (MS) R3993206-5 10/28/23 23:09 • (MSD) R3993206-6 10/28/23 23:31
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Chloroethane 5.00 U 3.56 3.46 71.2 69.2 1 10.0-160 2.85 30
Chloroform 5.00 U 2.85 3.04 57.0 60.8 1 29.0-154 6.45 28
Chloromethane 5.00 3.60 4.40 4.73 16.0 22.6 1 10.0-160 7.23 29
2-Chlorotoluene 5.00 U 3.20 4.10 64.0 82.0 1 32.0-153 V3 V3 24.7 28
4-Chlorotoluene 5.00 U 2.99 4.00 59.8 80.0 1 32.0-150 V3 J3 V3 28.9 28
1,2-Dibromo-3-Chloropropane 5.00 U 8.53 10.8 171 216 1 22.0-151 J5 V3 J5 V3 23.5 34
1,2-Dibromoethane 5.00 U 3.02 3.30 60.4 66.0 1 34.0-147 8.86 27
Dibromomethane 5.00 U 2.80 3.21 56.0 64.2 1 30.0-151 13.6 27
1,2-Dichlorobenzene 5.00 U 3.05 4.07 61.0 81.4 1 34.0-149 V3 J3 V3 28.7 28
1,3-Dichlorobenzene 5.00 U 2.93 3.84 58.6 76.8 1 36.0-146 V3 V3 26.9 27
1,4-Dichlorobenzene 5.00 U 2.99 3.93 59.8 78.6 1 35.0-142 V3 J3 V3 27.2 27
Dichlorodifluoromethane 5.00 U 3.31 3.68 66.2 73.6 1 10.0-160 10.6 29
1,1-Dichloroethane 5.00 U 2.83 2.87 56.6 57.4 1 25.0-158 1.40 27
1,2-Dichloroethane 5.00 U 2.70 2.94 54.0 58.8 1 29.0-151 8.51 27
1,1-Dichloroethene 5.00 U 2.91 3.09 58.2 61.8 1 11.0-160 6.00 29
cis-1,2-Dichloroethene 5.00 U 2.74 2.86 54.8 57.2 1 10.0-160 4.29 27
trans-1,2-Dichloroethene 5.00 U 2.72 2.71 54.4 54.2 1 17.0-153 0.368 27
1,2-Dichloropropane 5.00 U 2.64 2.93 52.8 58.6 1 30.0-156 10.4 27
1,1-Dichloropropene 5.00 U 2.65 2.60 53.0 52.0 1 25.0-158 1.90 27
1,3-Dichloropropane 5.00 U 3.13 3.49 62.6 69.8 1 38.0-147 10.9 27
2,2-Dichloropropane 5.00 0.294 1.98 1.82 33.7 30.5 1 24.0-152 8.42 29
Di-isopropyl ether 5.00 U 2.47 2.56 49.4 51.2 1 21.0-160 3.58 28
Ethylbenzene 5.00 U 1.94 2.19 38.8 43.8 1 30.0-155 12.1 27
Hexachloro-1,3-butadiene 5.00 U 3.95 4.91 79.0 98.2 1 20.0-154 V3 V3 21.7 34
Isopropylbenzene 5.00 U 1.61 2.00 32.2 40.0 1 28.0-157 21.6 27
p-Isopropyltoluene 5.00 U 2.77 3.69 55.4 73.8 1 30.0-154 V3 V3 28.5 29
2-Butanone (MEK)25.0 13.8 45.5 47.6 127 135 1 10.0-160 4.51 32
Methylene Chloride 5.00 U 2.56 2.83 51.2 56.6 1 23.0-144 10.0 28
4-Methyl-2-pentanone (MIBK)25.0 0.524 26.7 28.8 105 113 1 29.0-160 7.57 29
Methyl tert-butyl ether 5.00 U 2.49 2.62 49.8 52.4 1 28.0-150 5.09 29
Naphthalene 5.00 U 3.86 5.00 77.2 100 1 12.0-156 25.7 35
n-Propylbenzene 5.00 U 3.01 3.89 60.2 77.8 1 31.0-154 V3 V3 25.5 28
Styrene 5.00 U 1.68 1.88 33.6 37.6 1 33.0-155 11.2 28
1,1,1,2-Tetrachloroethane 5.00 U 2.47 2.65 49.4 53.0 1 36.0-151 7.03 29
1,1,2,2-Tetrachloroethane 5.00 U 6.40 7.75 128 155 1 33.0-150 V3 J5 V3 19.1 28
Tetrachloroethene 5.00 U 2.12 2.34 42.4 46.8 1 10.0-160 9.87 27
Toluene 5.00 U 2.84 2.92 56.8 58.4 1 26.0-154 2.78 28
1,2,3-Trichlorobenzene 5.00 U 2.84 4.08 56.8 81.6 1 17.0-150 V3 V3 35.8 36
1,2,4-Trichlorobenzene 5.00 U 2.69 3.78 53.8 75.6 1 24.0-150 V3 J3 V3 33.7 33
1,1,1-Trichloroethane 5.00 U 3.04 3.14 60.8 62.8 1 23.0-160 3.24 28
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2159937
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1669213-01,02,03,04,05
L1668931-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1668931-13 10/28/23 16:34 • (MS) R3993206-5 10/28/23 23:09 • (MSD) R3993206-6 10/28/23 23:31
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
1,1,2-Trichloroethane 5.00 U 3.18 3.40 63.6 68.0 1 35.0-147 6.69 27
Trichloroethene 5.00 U 2.36 2.51 47.2 50.2 1 10.0-160 6.16 25
Trichlorofluoromethane 5.00 U 2.77 3.17 55.4 63.4 1 17.0-160 13.5 31
1,2,3-Trichloropropane 5.00 U 7.11 8.60 142 172 1 34.0-151 V3 J5 V3 19.0 29
1,2,4-Trimethylbenzene 5.00 U 2.78 3.67 55.6 73.4 1 26.0-154 V3 J3 V3 27.6 27
1,3,5-Trimethylbenzene 5.00 U 2.81 3.62 56.2 72.4 1 28.0-153 V3 V3 25.2 27
Vinyl chloride 5.00 U 3.18 3.24 63.6 64.8 1 10.0-160 1.87 27
o-Xylene 5.00 U 1.76 2.06 35.2 41.2 1 45.0-144 J6 J6 15.7 26
m&p-Xylenes 10.0 U 3.80 4.18 38.0 41.8 1 43.0-146 J6 J6 9.52 26
(S) Toluene-d8 113 114 80.0-120
(S) 4-Bromofluorobenzene 80.4 82.3 77.0-126
(S) 1,2-Dichloroethane-d4 104 102 70.0-130
L1670989-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1670989-05 10/28/23 20:57 • (MS) R3993206-7 10/28/23 23:52 • (MSD) R3993206-8 10/29/23 00:14
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acetone 25.0 U 18.2 19.1 72.8 76.4 1 10.0-160 4.83 35
Acrolein 25.0 U 21.0 25.4 84.0 102 1 10.0-160 19.0 39
Acrylonitrile 25.0 U 16.7 18.3 66.8 73.2 1 21.0-160 9.14 32
Benzene 5.00 U 4.10 4.42 82.0 88.4 1 17.0-158 7.51 27
Bromobenzene 5.00 U 4.34 4.52 86.8 90.4 1 30.0-149 4.06 28
Bromodichloromethane 5.00 U 4.07 4.50 81.4 90.0 1 31.0-150 10.0 27
Bromoform 5.00 U 3.46 3.68 69.2 73.6 1 29.0-150 6.16 29
Bromomethane 5.00 U 4.18 4.63 83.6 92.6 1 10.0-160 10.2 38
n-Butylbenzene 5.00 U 3.94 3.99 78.8 79.8 1 31.0-150 1.26 30
sec-Butylbenzene 5.00 U 4.32 4.56 86.4 91.2 1 33.0-155 5.41 29
tert-Butylbenzene 5.00 U 4.34 4.53 86.8 90.6 1 34.0-153 4.28 28
Carbon tetrachloride 5.00 U 4.36 4.70 87.2 94.0 1 23.0-159 7.51 28
Chlorobenzene 5.00 U 3.89 4.25 77.8 85.0 1 33.0-152 8.85 27
Chlorodibromomethane 5.00 U 4.10 4.37 82.0 87.4 1 37.0-149 6.38 27
Chloroethane 5.00 U 4.51 4.91 90.2 98.2 1 10.0-160 8.49 30
Chloroform 5.00 U 4.22 4.53 84.4 90.6 1 29.0-154 7.09 28
Chloromethane 5.00 U 3.86 3.96 77.2 79.2 1 10.0-160 2.56 29
2-Chlorotoluene 5.00 U 4.53 4.62 90.6 92.4 1 32.0-153 1.97 28
4-Chlorotoluene 5.00 U 4.29 4.54 85.8 90.8 1 32.0-150 5.66 28
1,2-Dibromo-3-Chloropropane 5.00 U 3.68 3.80 73.6 76.0 1 22.0-151 3.21 34
1,2-Dibromoethane 5.00 U 3.79 3.99 75.8 79.8 1 34.0-147 5.14 27
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2159937
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1669213-01,02,03,04,05
L1670989-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1670989-05 10/28/23 20:57 • (MS) R3993206-7 10/28/23 23:52 • (MSD) R3993206-8 10/29/23 00:14
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Dibromomethane 5.00 U 4.16 4.40 83.2 88.0 1 30.0-151 5.61 27
1,2-Dichlorobenzene 5.00 U 4.21 4.36 84.2 87.2 1 34.0-149 3.50 28
1,3-Dichlorobenzene 5.00 U 4.23 4.46 84.6 89.2 1 36.0-146 5.29 27
1,4-Dichlorobenzene 5.00 U 4.22 4.35 84.4 87.0 1 35.0-142 3.03 27
Dichlorodifluoromethane 5.00 U 4.87 5.60 97.4 112 1 10.0-160 13.9 29
1,1-Dichloroethane 5.00 U 3.84 4.13 76.8 82.6 1 25.0-158 7.28 27
1,2-Dichloroethane 5.00 U 4.01 4.23 80.2 84.6 1 29.0-151 5.34 27
1,1-Dichloroethene 5.00 U 4.56 4.77 91.2 95.4 1 11.0-160 4.50 29
cis-1,2-Dichloroethene 5.00 U 4.01 4.30 80.2 86.0 1 10.0-160 6.98 27
trans-1,2-Dichloroethene 5.00 U 4.06 4.43 81.2 88.6 1 17.0-153 8.72 27
1,2-Dichloropropane 5.00 U 3.90 4.26 78.0 85.2 1 30.0-156 8.82 27
1,1-Dichloropropene 5.00 U 4.65 4.91 93.0 98.2 1 25.0-158 5.44 27
1,3-Dichloropropane 5.00 U 4.10 4.29 82.0 85.8 1 38.0-147 4.53 27
2,2-Dichloropropane 5.00 U 3.40 3.88 68.0 77.6 1 24.0-152 13.2 29
Di-isopropyl ether 5.00 U 3.42 3.71 68.4 74.2 1 21.0-160 8.13 28
Ethylbenzene 5.00 U 3.93 4.16 78.6 83.2 1 30.0-155 5.69 27
Hexachloro-1,3-butadiene 5.00 U 3.75 4.20 75.0 84.0 1 20.0-154 11.3 34
Isopropylbenzene 5.00 U 3.97 4.19 79.4 83.8 1 28.0-157 5.39 27
p-Isopropyltoluene 5.00 U 4.19 4.42 83.8 88.4 1 30.0-154 5.34 29
2-Butanone (MEK)25.0 U 17.2 18.0 68.8 72.0 1 10.0-160 4.55 32
Methylene Chloride 5.00 U 3.81 4.16 76.2 83.2 1 23.0-144 8.78 28
4-Methyl-2-pentanone (MIBK)25.0 U 17.1 18.2 68.4 72.8 1 29.0-160 6.23 29
Methyl tert-butyl ether 5.00 U 3.61 4.10 72.2 82.0 1 28.0-150 12.7 29
Naphthalene 5.00 U 3.91 4.17 78.2 83.4 1 12.0-156 6.44 35
n-Propylbenzene 5.00 U 4.49 4.74 89.8 94.8 1 31.0-154 5.42 28
Styrene 5.00 U 3.45 3.71 69.0 74.2 1 33.0-155 7.26 28
1,1,1,2-Tetrachloroethane 5.00 U 3.78 3.96 75.6 79.2 1 36.0-151 4.65 29
1,1,2,2-Tetrachloroethane 5.00 U 4.58 4.80 91.6 96.0 1 33.0-150 4.69 28
Tetrachloroethene 5.00 U 4.15 4.27 83.0 85.4 1 10.0-160 2.85 27
Toluene 5.00 U 4.13 4.40 82.6 88.0 1 26.0-154 6.33 28
1,2,3-Trichlorobenzene 5.00 U 3.81 4.03 76.2 80.6 1 17.0-150 5.61 36
1,2,4-Trichlorobenzene 5.00 U 3.64 3.88 72.8 77.6 1 24.0-150 6.38 33
1,1,1-Trichloroethane 5.00 U 4.64 5.09 92.8 102 1 23.0-160 9.25 28
1,1,2-Trichloroethane 5.00 U 3.94 4.31 78.8 86.2 1 35.0-147 8.97 27
Trichloroethene 5.00 U 4.15 4.28 83.0 85.6 1 10.0-160 3.08 25
Trichlorofluoromethane 5.00 U 4.80 5.42 96.0 108 1 17.0-160 12.1 31
1,2,3-Trichloropropane 5.00 U 4.26 4.54 85.2 90.8 1 34.0-151 6.36 29
1,2,4-Trimethylbenzene 5.00 U 4.14 4.29 82.8 85.8 1 26.0-154 3.56 27
1,3,5-Trimethylbenzene 5.00 U 4.24 4.47 84.8 89.4 1 28.0-153 5.28 27
Vinyl chloride 5.00 U 4.51 4.76 90.2 95.2 1 10.0-160 5.39 27
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2159937
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1669213-01,02,03,04,05
L1670989-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1670989-05 10/28/23 20:57 • (MS) R3993206-7 10/28/23 23:52 • (MSD) R3993206-8 10/29/23 00:14
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
o-Xylene 5.00 U 3.64 3.87 72.8 77.4 1 45.0-144 6.13 26
m&p-Xylenes 10.0 U 7.85 8.31 78.5 83.1 1 43.0-146 5.69 26
(S) Toluene-d8 103 101 80.0-120
(S) 4-Bromofluorobenzene 95.1 96.8 77.0-126
(S) 1,2-Dichloroethane-d4 103 103 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
V3 The internal standard exhibited poor recovery due to sample matrix interference. The analytical results will be biased
high. BDL results will be unaffected.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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