Loading...
HomeMy WebLinkAboutMO-85747_85747_CA_MRP_20230628_Groundwater Monitoring ReportApex Companies, LLC  5900 Northwoods Business Parkway, Suite 5900‐O  Charlotte, NC 28269  T 704.799.6390  apexcos.com  June 28, 2023 Mr. Ryan Mills North Carolina Department of Environmental Quality Division of Waste Management UST Section - Corrective Action Branch 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 Re: 2023 Annual Groundwater Monitoring Report Freeze Road Site Enochville, Rowan County, North Carolina NCDEQ Incident Number 85747 Dear Mr. Mills: On behalf of Colonial Pipeline Company, Apex Companies, LLC (Apex, dba Maryland Apex Engineering, P.C.) has prepared the attached 2023 Annual Groundwater Monitoring Report for the Colonial Pipeline Company’s Freeze Road site covering the period of May 2022 through May 2023. If you have any questions or concerns, please do not hesitate to contact the undersigned at (704) 799-6390. Sincerely, Apex Companies, LLC Andrew Street, CHMM, RSM Tom Naumann P.G. Senior Project Manager Project Manager NC License No. 2405 Enclosure cc: Maribeth Hughes, Colonial Pipeline Company Jeff Morrison, Colonial Pipeline Company Prepared for: Colonial Pipeline Company P.O. Box 87 Paw Creek, North Carolina 25130 2023 Annual Groundwater Monitoring Report May 2022 - May 2023 Freeze Road Site Enochville, North Carolina NCDEQ lncident No. 85747 ,,.\ APEX 5900 North Woods Business Parkway, Suite O Charlotte, North Carolina 28269 ,."-l ! !r ,. a -{ t //U /'?' .)..= j-' /'t.-_ Jamie Humphrey Scientist lll Reviewed By: ,./ "/ -/ t,_// .. j'i'/,. u/,r, / Andrew Street, CHMM, RSM Senior Project Manager Project Manager NC License No.2405 2405 96AFAA.6 June28,2023 Colonial Pipeline Company – Freeze Road Site June 28 20, 23 Annual Groundwater Monitoring Report Page i Table of Contents 1.0 INTRODUCTION .................................................................................................................................... 1  2.0 FIELD ACTIVITIES ................................................................................................................................ 1  2.1 Groundwater Gauging .............................................................................................................. 2  2.2 Groundwater Sampling and Analysis ....................................................................................... 2  3.0 FINDINGS ............................................................................................................................................... 3  3.1 Well Gauging Results and Groundwater Flow ......................................................................... 3  3.2 Groundwater Analytical Results ............................................................................................... 3  4.0 REMEDIATION SYSTEM OPERATION ............................................................................................... 3  5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................................... 4  Tables Table 1: Groundwater Monitoring and Analysis Program Table 2: Summary of Groundwater Elevation Data Table 3: Summary of Groundwater Analytical Results Figures Figure 1: Site Location Map Figure 2: Site Vicinity Map Figure 3: Site Plan with Well Locations Figure 4: Groundwater Potentiometric Surface Map Surficial Saprolite Unit (May 2023) Figure 5: Groundwater Potentiometric Surface Map Bedrock Unit (May 2023) Figure 6: Distribution of LNAPL May 2023 Figure 7: Benzene in Groundwater May 2023 Figure 8: Naphthalene in Groundwater May 2023 Appendices Appendix A: Groundwater Sampling Field Logs Appendix B: Laboratory Analytical Report Colonial Pipeline Company – Freeze Road Site June 28 20, 23 Annual Groundwater Monitoring Report Page 1 1.0 INTRODUCTION This report presents the results of the May 2023 annual groundwater monitoring event performed at the Colonial Pipeline Company (CPC) Freeze Road site located approximately 1.3 miles west of downtown Enochville, North Carolina (the ‘site’). Apex Companies, LLC (Apex, dba Maryland Apex Engineering, P.C.), prepared this report on behalf of CPC for submittal to the North Carolina Department of Environmental Quality (NCDEQ). A Site Location Map is provided as Figure 1. A Site Vicinity Map, with property boundaries, is provided as Figure 2. The site is located along a CPC right-of-way in a rural, residential area west of Enochville, North Carolina. On May 30, 2001, CPC discovered a crack in the 36-inch No. 2 distillate line running through the site. Approximately 400 barrels (16,800 gallons) of diesel and jet fuel were released from the line, resulting in impacts to surrounding soil and groundwater. A Site Plan showing the locations of the release, monitoring wells, recovery wells, and nearby water supply wells is included as Figure 3. Following discovery of the release, Progressive Engineering and Construction, Inc. (Progressive) performed initial abatement and assessment activities at the site in 2001. The investigation activities are summarized in the Comprehensive Site Assessment Report dated October 11, 2001. Based on the results of the assessment activities, a Corrective Action Plan (CAP) was submitted to NCDEQ on December 21, 2001. The CAP was subsequently approved by NCDEQ on January 14, 2002. The CAP describes corrective actions at the facility to be conducted under North Carolina 15A NCAC 2L, .0106 (c) groundwater standards (2L Standards). The corrective action objectives for the site as described in the CAP are to: i) prevent off-site migration to downgradient receptors; ii) remove light non-aqueous phase liquid (LNAPL) fuel to the extent practical; and iii) remediate source area soils. Based on the risk-based rules established in October 2015 under House Bill 765, Risk Based Corrective Action (RBCA) Rules that were previously established for releases from petroleum underground storage tanks (USTs) became applicable to non-UST releases of petroleum. Under the RBCA framework, corrective action objectives for impacted groundwater at the site are based on risk classification criteria and the associated remedial goals established under North Carolina 15A NCAC 2L .0506 regulations. The risk classification for a site is based on several factors, including the distance from the source area of a release to receptors such as surface water bodies and water supply wells. At present, the risk classification for the site is high risk due to the presence of multiple water supply wells within 1,000 feet (ft.) of the release. Groundwater remediation goals for sites classified as high risk are the 2L Standards. This report summarizes the results of annual groundwater monitoring activities completed at the site in May 2023 and provides a summary of groundwater remediation activities during the annual reporting period. 2.0 FIELD ACTIVITIES The following sections provide a summary of the field methods for the annual groundwater monitoring event conducted in May 2023. Field logs documenting the groundwater sample collection Colonial Pipeline Company – Freeze Road Site June 28 20, 23 Annual Groundwater Monitoring Report Page 2 are provided in Appendix A. During the May 2023 sampling event, groundwater samples were collected and analyzed for benzene, toluene, ethylbenzene, total xylenes (BTEX), methyl tert-butyl ether (MTBE), and naphthalene. The current groundwater monitoring program is summarized in Table 1. The current groundwater monitoring program for the site was approved by NCDEQ in a letter dated June 14, 2012. Groundwater elevation data and laboratory analytical results for the May 2023 groundwater monitoring event are summarized in Table 2 and Table 3, respectively. 2.1 Groundwater Gauging Prior to sampling, groundwater monitoring wells were gauged to measure the depth to groundwater and LNAPL, if present. Upon arriving at the site, wells were opened and allowed to equilibrate. Wells were gauged in accordance with the United States Environmental Protection Agency (EPA) Region IV Science and Ecosystem Support Division Field Branches Quality System and Technical Procedures. Depths to groundwater and LNAPL (if present) were measured using an electronic oil/water interface probe capable of measuring to an accuracy of 0.01 ft. The interface probe was thoroughly decontaminated before collecting measurements at each subsequent monitoring well. A total of 26 monitoring wells and 25 recovery wells were gauged on May 9, 2023. Monitoring wells MW-15, MW-18D, MW-19, MW-20D, MW-31, MW-33, and MW-40, were not gauged because they could not be accessed or located. Monitoring well MW-41 was not gauged because the well was covered by a wood debris pile. Recovery well RW-10 was not gauged because the lid could not be opened. Monitoring well locations are shown on Figure 3. Well construction details are provided in Table 1. Well gauging results are discussed in Section 3.1 and summarized in Table 2 of this report. 2.2 Groundwater Sampling and Analysis Groundwater samples were collected from 13 of the 14 planned monitoring wells on May 9-10, 2023. MW-30 was not sampled because the current resident would not answer the door and permission to access the property was not granted. At each monitoring well, a baseline set of water quality stabilization data was measured and recorded, including conductivity, dissolved oxygen (DO), pH, oxidation-reduction potential (ORP), turbidity, and temperature. The monitoring wells were purged and sampled using a decontaminated stainless-steel submersible pump with disposable polyethylene tubing that was changed between wells. Pump tubing was set approximately one to two feet below the water table for the wells screened across the water table, and at mid-point of the screened interval for deeper wells. Water quality parameters were considered stable when specific conductance stabilized within 3 percent, pH stabilized within 0.1 units, ORP stabilized within 10 millivolts (mV), DO stabilized within 0.3 micrograms per liter (mg/L), and turbidity stabilized within 10 percent over three consecutive measurements. Field logs documenting the groundwater purging and sample collection are provided in Appendix A. Once purging was completed, samples were collected in the laboratory supplied bottleware and stored on ice in a cooler. Groundwater samples were submitted under chain of custody procedures to Pace Analytical, Inc., a North Carolina certified laboratory. Groundwater samples were analyzed for BTEX, MTBE, and naphthalene by EPA Method SM 6200B. Colonial Pipeline Company – Freeze Road Site June 28 20, 23 Annual Groundwater Monitoring Report Page 3 As part of the groundwater sampling program, quality assurance/quality control (QA/QC) samples were collected and submitted for laboratory analysis. Specifically, two blind duplicate samples, two equipment rinse blanks, and one trip blank were submitted for laboratory analysis. Analytical results are summarized in Table 3 and a copy of the laboratory report is provided in Appendix B. 3.0 FINDINGS 3.1 Well Gauging Results and Groundwater Flow Groundwater gauging results from the May 2023 gauging event are summarized in Table 2. Depth to water and top of well casing elevation data from the monitoring wells were used to calculate groundwater potentiometric elevations relative to an on-site benchmark referenced to mean sea level (MSL) datum. For shallow wells that are screened across the water table surface, the groundwater potentiometric surface is approximately equal to the water table elevation. Potentiometric surface maps for the surficial and bedrock aquifer units were developed for the site based on the May 2023 gauging data and are presented as Figure 4 and Figure 5, respectively. The calculated horizontal groundwater gradient for the surficial saprolite unit during the May 2023 monitoring event is approximately 0.027 ft. per foot using gauging data from the 832 ft. MSL and 844 ft. MSL equipotential contour lines in the vicinity of monitoring wells MW-35 and MW-36, respectively. The surficial groundwater flow is generally towards the west and bedrock groundwater flow is generally towards the northwest. The groundwater elevations and flow results observed in May 2023 were consistent with those observed during historical observations. The distribution of LNAPL recorded during the May 2023 gauging event is depicted in Figure 6. LNAPL was detected in two recovery wells, RW-3 and RW-8, with thicknesses of 0.02 ft and 0.05 ft respectively. Table 2 provides the top of screen elevation for each monitoring well and recovery well and indicates if each well screen was submerged during the May 2023 gauging event. Downgradient migration of the LNAPL plume was not indicated by the May 2023 gauging data from the leading- edge monitoring wells. The distribution and thickness of LNAPL across the site has decreased significantly since monitoring began in 2001. 3.2 Groundwater Analytical Results Groundwater analytical results from the May 2023 monitoring event are summarized in Table 3. The laboratory analytical data report and chain of custody records for the May 2023 sampling event are provided in Appendix B. The distribution of benzene and naphthalene in groundwater for the May 2023 sampling event are presented in Figure 7 and Figure 8, respectively. All other constituents of concern that were detected during the May 2023 sampling event were below their applicable 2L Standards. 4.0 REMEDIATION SYSTEM OPERATION The biosparging system has operated at the site since 2004 to enhance hydrocarbon degradation rates and prevent downgradient migration of dissolved-phase petroleum constituents. Low volumes of air are injected into 32 converted recovery wells operating as biosparge wells. The recovery wells Colonial Pipeline Company – Freeze Road Site June 28 20, 23 Annual Groundwater Monitoring Report Page 4 were converted to biosparge wells by removing the LNAPL recovery tubing and associated air supply hoses and connecting to an existing high-density polyethylene (HDPE) branch stub-up for compressed air. Each converted well head is equipped with a flow shutoff valve, a variable area flow meter/controller, and a liquid filled pressure gauge. A galvanized drop pipe fitted with a 4-inch diameter packer is installed in each biosparge well, which forces compressed air through the formation and prevents short-circuiting of air through the well casing. The flow rate of the air into the system ranges from 0.5 cubic ft. per minute (cfm) to 2 cfm. Apex performed a site visit on April 22, 2022 to determine the operational status of the system at the Freeze Road Site. The system was run for a total of two hours, but due to high temp alarms Apex personnel shut the system down pending repairs and service. Following servicing, the system was restarted on March 16, 2023 and ran through the end of the reporting period. 5.0 CONCLUSIONS AND RECOMMENDATIONS Five of 14 monitoring wells sampled (MW-8, MW-22, MW-28, MW-29D, and MW-34) exhibited benzene and/or naphthalene concentrations above 2L Standards. Measurable LNAPL was detected in two wells within the footprint of the historical LNAPL plume area with a maximum thickness of 0.05 feet. The groundwater monitoring data indicates that the LNAPL plume continues to decrease in horizontal extent and thickness, and the remaining LNAPL is not migrating. Continued operation of the biosparge system is recommended to enhance biodegradation of dissolved-phase hydrocarbons in groundwater, to bioremediate sorbed and residual LNAPL hydrocarbons in the phreatic zone soils, and to prevent the migration of the hydrocarbon plume. TABLES Table 1 Groundwater Monitoring and Analysis Program Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Hydraulic Monitoring Water Quality Monitoring Annually Annually Depth to Water / LNAPL BTEX, MTBE, & Naphthalene MW-2 40 25 - 40 MW-3 41 21 - 41 MW-4D 70 50 - 70 MW-5 25 13 - 25 MW-7D 100 80 - 100 MW-8 55 35 - 55 MW-9 50 25 - 50 MW-10 40 23 - 40 MW-11D 122 102 - 122 MW-12D 70 50 - 70 MW-13D 70 50 - 70 MW-14D 200 180 - 200 MW-15 31 21 - 31 MW-16D 75 55 - 75 MW-17D 105 75 - 105 MW-18D 215 175 - 215 MW-19 35 20 - 35 MW-20D 182 162 - 182 MW-21 54 24 - 54 MW-22 36.5 26.5 - 36.5 MW-28 49 19 - 49 MW-29D 70 50 - 70 MW-30 50 25 - 50 MW-31 50 25 - 50 MW-32 50 25 - 50 MW-33 50 20 - 50 MW-34 71 21 - 71 MW-35 46 21 - 46 MW-36 31 16 - 31 MW-37 48 28 - 48 MW-38 55 25 - 55 MW-39 55 25 - 55 MW-40 50 20 - 50 MW-41 50 25 - 55 MW-1 35 25 - 35 MW-6 40 24 - 34 * MW-23 30 20 - 30 MW-24 29 19 - 29 * MW-25 35 20 - 35 MW-26 40 20 - 40 * MW-27 45 20 - 45 * RW-1 40 20 - 40 RW-2 45 25 - 45 RW-3 40 20 - 40 RW-4 45 20 - 40 RW-5 34 24 - 34 RW-6 45 20 - 45 RW-7 46 21 - 41 * Well ID Total Well Depth (ft. bgs) Screened Interval (ft. bgs) Monitoring Wells Product Recovery Wells Page 1 of 2 Table 1 Groundwater Monitoring and Analysis Program Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Hydraulic Monitoring Water Quality Monitoring Annually Annually Depth to Water / LNAPL BTEX, MTBE, & Naphthalene Well ID Total Well Depth (ft. bgs) Screened Interval (ft. bgs) RW-8 46 21 - 41 RW-9 41 16 - 36 RW-10 50 25 - 45 RW-11 48 23 - 48 RW-12 46 21 - 41 RW-13 46 21 - 41 RW-14 46 21 - 41 * RW-15 43 18 - 43 RW-16 46 21 - 41 RW-17 43 23 - 43 * RW-18 39 19 - 39 RW-19 41 21 - 41 RW-20 50 20 - 50 * RW-21 40 20 - 40 RW-22 39 19 - 39 RW-23 43 23 - 43 * RW-24 40 20 - 40 * RW-25 40 25 - 40 * RW-26 40 20 - 40 * RW-27 38 18 - 38 RW-28 41 21 - 41 * RW-29 35 15 - 35 * RW-30 41 21 - 41 RW-31 42 22 - 42 * RW-32 33 13 - 33 * RW-33 34 14 - 34 * RW-34 50 20 - 50 * RW-35 58 8 - 58 * RW-36 42 22 - 42 * RW-37 54 24 - 54 RW-38 53 13 - 53 * RW-39 58 13 - 58 RW-40 55 15 - 55 * RW-41 45 25 - 45 RW-42 50 10 - 50 * RW-43 45 15 - 45 * RW-44 54 14 - 54 * RW-45 44 19 - 44 * RW-47 45 15 - 45 * RW-48 43 23 - 43 * RW-49 57 22 - 57 * RW-50 52 27 - 52 * RW-51 38 23 - 38 * Notes: ID - Identification ft. bgs - feet below grade surface LNAPL - Light Non-Aqueous Phase Liquid BTEX - benzene, toluene, ethylbenzene, and xylenes MTBE - Methyl Tertiary Butyl Ether Water quality samples will be analyzed for BTEX, MTBE, and Naphthalene via EPA Method 602 by SM 6200B. * Well is equipped with a packer or pump and cannot be gauged Monitoring Plan approved via June 14, 2012 letter from North Carolina Department of Environment and Natural Resources (NCDENR) Page 2 of 2 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged 859.10 834.1 40.0 8/28/2001 ND 27.01 NA 832.09 No 11/27/2001 ND 27.27 NA 831.83 No 5/15/2002 ND 26.23 NA 832.87 No 11/13/2002 ND 26.45 NA 832.65 No 5/23/2003 ND 18.75 NA 840.35 Yes 11/24/2003 ND 18.87 NA 840.23 Yes 5/12/2004 ND 19.36 NA 839.74 Yes 11/10/2004 ND 19.97 NA 839.13 Yes 5/31/2005 ND 18.67 NA 840.43 Yes 11/15/2005 ND 21.29 NA 837.81 Yes 5/22/2006 ND 20.50 NA 838.60 Yes 11/22/2006 ND 20.44 NA 838.66 Yes 5/22/2007 ND 18.97 NA 840.13 Yes 11/13/2007 ND 24.10 NA 835.00 Yes 5/28/2008 ND 23.18 NA 835.92 Yes 11/18/2008 ND 24.73 NA 834.37 Yes 5/13/2009 ND 21.07 NA 838.03 Yes 11/18/2009 ND 24.56 NA 834.54 Yes 5/11/2010 ND 18.78 NA 840.32 Yes 11/16/2010 ND 21.37 NA 837.73 Yes 5/25/2011 ND 21.76 NA 837.34 Yes 11/17/2011 ND 26.07 NA 833.03 No 5/2/2012 ND 22.98 NA 836.12 Yes 11/21/2012 ND 26.39 NA 832.71 No 5/30/2013 ND 22.80 NA 836.30 Yes 5/27/2014 ND 18.75 NA 840.35 Yes 5/26/2015 ND 21.59 NA 837.51 Yes 5/11/2016 ND 19.63 NA 839.47 Yes 5/23/2017 ND 22.90 NA 836.20 Yes 5/9/2018 ND 23.59 NA 835.51 Yes 5/28/2019 5/14/2020 ND 18.29 NA 840.81 Yes 5/4/2021 ND 15.91 NA 843.19 Yes 5/11/2022 ND 21.98 NA 837.12 Yes 5/9/2023 ND 18.88 NA 840.22 Yes Groundwater Elevation (ft. MSL) Monitoring Wells Could Not Open Lock On Vault MW-2 Page 1 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.53 841.5 41.0 8/28/2001 ND 30.87 NA 831.66 No 11/28/2001 ND 31.70 NA 830.83 No 5/15/2002 NM 31.40*NM NM NM 11/13/2002 NM 32.00*NM NM NM 5/23/2003 ND 22.30 NA 840.23 No 11/17/2003 ND 21.00 NA 841.53 Yes 5/12/2004 ND 22.38 NA 840.15 No 11/10/2004 NM 22.83*NM NM NM 5/31/2005 ND 21.50 NA 841.03 No 11/15/2005 NM 24.53*NM NM NM 5/22/2006 ND 23.01 NA 839.52 No 5/7/2007 ND 22.32 NA 840.21 No 11/13/2007 NM 26.50*NM NM NM 11/18/2008 ND 27.70 NA 834.83 No 5/13/2009 ND 25.06 NA 837.47 No 11/16/2009 ND 27.21 NA 835.32 No 5/30/2013 ND 27.11 NA 835.42 No 5/27/2014 ND 19.19 NA 843.34 Yes 5/26/2015 ND 24.98 NA 837.55 No 5/11/2016 ND 22.84 NA 839.69 No 5/23/2017 26.83 26.88 0.05 835.69 **No 5/9/2018 27.33 27.34 0.01 835.20 **No 5/28/2019 ND 20.04 NA 842.49 Yes 5/14/2020 ND 21.46 NA 841.07 No 5/4/2021 ND 19.02 NA 843.51 Yes 5/11/2022 ND 27.02 NA 835.51 No 5/9/2023 ND 23.47 NA 839.06 No MW-3 Page 2 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.78 812.8 70.0 8/28/2001 ND 32.70 NA 830.08 NA 11/28/2001 ND 33.48 NA 829.30 NA 5/15/2002 ND 32.46 NA 830.32 NA 11/13/2002 ND 34.30 NA 828.48 NA 5/23/2003 ND 27.20 NA 835.58 NA 11/24/2003 ND 24.38 NA 838.40 NA 5/12/2004 ND 25.42 NA 837.36 NA 11/10/2004 ND 25.90 NA 836.88 NA 5/31/2005 ND 24.84 NA 837.94 NA 11/15/2005 ND 27.39 NA 835.39 NA 5/22/2006 ND 26.00 NA 836.78 NA 11/22/2006 ND 24.03 NA 838.75 NA 5/22/2007 ND 23.75 NA 839.03 NA 11/13/2007 ND 29.25 NA 833.53 NA 5/28/2008 ND 28.45 NA 834.33 NA 11/18/2008 ND 29.42 NA 833.36 NA 5/13/2009 ND 26.50 NA 836.28 NA 11/16/2009 ND 28.34 NA 834.44 NA 5/12/2010 ND 23.98 NA 838.80 NA 11/18/2010 ND 26.11 NA 836.67 NA 5/25/2011 ND 26.52 NA 836.26 NA 11/18/2011 ND 29.32 NA 833.46 NA 11/20/2012 ND 30.13 NA 832.65 NA 5/30/2013 ND 28.27 NA 834.51 NA 5/27/2014 ND 23.75 NA 839.03 NA 5/26/2015 ND 26.35 NA 836.43 NA 5/11/2016 ND 24.27 NA 838.51 NA 5/23/2017 ND 28.21 NA 834.57 NA 5/9/2018 ND 28.63 NA 834.15 NA 5/28/2019 ND 21.22 NA 841.56 NA 5/14/2020 ND 22.85 NA 839.93 NA 5/4/2021 ND 19.86 NA 842.92 NA 5/11/2022 ND 27.03 NA 835.75 NA 5/9/2023 ND 24.88 NA 837.90 NA MW-4D Page 3 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 854.95 842.0 25.0 8/28/2001 ND 15.30 NA 839.65 No 11/27/2001 ND 16.25 NA 838.70 No 5/15/2002 ND 15.25 NA 839.70 No 11/13/2002 ND 15.23 NA 839.72 No 5/23/2003 ND 9.30 NA 845.65 Yes 5/12/2004 ND 9.05 NA 845.90 Yes 11/10/2004 ND 10.34 NA 844.61 Yes 5/31/2005 ND 9.32 NA 845.63 Yes 11/15/2005 ND 11.32 NA 843.63 Yes 5/22/2006 ND 10.75 NA 844.20 Yes 11/22/2006 NM NM NM NM NM 5/22/2007 ND 10.02 NA 844.93 Yes 11/13/2007 ND 13.05 NA 841.90 No 5/28/2008 ND 12.30 NA 842.65 Yes 11/20/2008 ND 13.32 NA 841.63 No 5/13/2009 ND 11.79 NA 843.16 Yes 11/18/2009 ND 11.73 NA 843.22 Yes 5/30/2013 ND 12.48 NA 842.47 Yes 5/26/2015 ND 11.99 NA 842.96 Yes 5/11/2016 ND 9.86 NA 845.09 Yes 5/23/2017 ND 12.33 NA 842.62 Yes 5/9/2018 ND 12.40 NA 842.55 Yes 5/28/2019 ND 7.86 NA 847.09 Yes 5/14/2020 ND 8.93 NA 846.02 Yes 5/4/2021 ND 5.58 NA 849.37 Yes 5/11/2022 ND 11.54 NA 843.41 Yes 5/9/2023 ND 5.53 NA 849.42 Yes MW-5 Page 4 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 861.62 781.6 100.0 8/28/2001 ND 35.07 NA 826.55 NA 11/28/2001 ND 36.48 NA 825.14 NA 5/15/2002 ND 34.12 NA 827.50 NA 11/13/2002 ND 35.45 NA 826.17 NA 5/23/2003 ND 27.20 NA 834.42 NA 11/24/2003 ND 27.78 NA 833.84 NA 5/12/2004 ND 27.20 NA 834.42 NA 11/10/2004 ND 28.20 NA 833.42 NA 5/31/2005 ND 27.19 NA 834.43 NA 11/15/2005 ND 29.58 NA 832.04 NA 5/22/2006 ND 28.80 NA 832.82 NA 11/22/2006 ND 21.95 NA 839.67 NA 5/22/2007 ND 27.92 NA 833.70 NA 11/13/2007 ND 29.80 NA 831.82 NA 5/28/2008 ND 31.05 NA 830.57 NA 11/18/2008 ND 31.91 NA 829.71 NA 5/13/2009 ND 30.17 NA 831.45 NA 11/16/2009 ND 15.99 NA 845.63 NA 5/11/2010 ND 27.98 NA 833.64 NA 11/16/2010 ND 30.31 NA 831.31 NA 5/25/2011 ND 30.34 NA 831.28 NA 3/20/2012 ND 31.46 NA 830.16 NA 5/2/2012 ND 31.26 NA 830.36 NA 11/21/2012 NM NM NM NM NM 5/30/2013 ND 31.15 NA 830.47 NA 5/27/2014 ND 27.69 NA 833.93 NA 5/26/2015 ND 29.94 NA 831.68 NA 5/11/2016 ND 28.50 NA 833.12 NA 5/23/2017 ND 31.40 NA 830.22 NA 5/9/2018 ND 28.61 NA 833.01 NA 5/28/2019 ND 25.87 NA 835.75 NA 5/14/2020 ND 27.49 NA 834.13 NA 5/4/2021 ND 24.50 NA 837.12 NA 5/11/2022 5/9/2023 ND 25.74 NA 835.88 NA Could Not Locate MW-7D Page 5 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 864.19 829.2 55.0 8/28/2001 ND 33.77 NA 830.42 Yes 11/28/2001 ND 34.55 NA 829.64 Yes 5/15/2002 ND 33.57 NA 830.62 Yes 11/13/2002 ND 35.50 NA 828.69 No 5/23/2003 ND 27.05 NA 837.14 Yes 11/24/2003 ND 25.31 NA 838.88 Yes 5/12/2004 ND 26.45 NA 837.74 Yes 11/10/2004 ND 27.07 NA 837.12 Yes 5/31/2005 ND 25.74 NA 838.45 Yes 11/15/2005 ND 28.43 NA 835.76 Yes 5/22/2006 ND 27.93 NA 836.26 Yes 11/22/2006 ND 28.50 NA 835.69 Yes 5/22/2007 ND 26.28 NA 837.91 Yes 11/13/2007 ND 30.50 NA 833.69 Yes 5/28/2008 ND 30.70 NA 833.49 Yes 11/18/2008 ND 31.48 NA 832.71 Yes 5/13/2009 ND 28.95 NA 835.24 Yes 11/16/2009 ND 30.94 NA 833.25 Yes 5/12/2010 ND 26.21 NA 837.98 Yes 11/18/2010 ND 28.87 NA 835.32 Yes 5/25/2011 ND 29.17 NA 835.02 Yes 11/17/2011 ND 31.89 NA 832.30 Yes 5/3/2012 ND 30.23 NA 833.96 Yes 11/19/2012 ND 32.67 NA 831.52 Yes 5/30/2013 ND 31.08 NA 833.11 Yes 5/27/2014 ND 26.60 NA 837.59 Yes 5/26/2015 ND 29.11 NA 835.08 Yes 5/11/2016 ND 26.94 NA 837.25 Yes 5/23/2017 ND 31.01 NA 833.18 Yes 5/9/2018 ND 31.42 NA 832.77 Yes 5/28/2019 ND 23.84 NA 840.35 Yes 5/14/2020 ND 25.61 NA 838.58 Yes 5/4/2021 ND 22.58 NA 841.61 Yes 5/11/2022 ND 29.85 NA 834.34 Yes 5/9/2023 ND 27.91 NA 836.28 Yes MW-8 Page 6 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 849.57 824.6 50.0 8/28/2001 ND 17.78 NA 831.79 Yes 11/27/2001 ND 18.50 NA 831.07 Yes 5/15/2002 ND 17.80 NA 831.77 Yes 11/13/2002 ND 19.52 NA 830.05 Yes 5/23/2003 ND 10.65 NA 838.92 Yes 11/24/2003 ND 9.06 NA 840.51 Yes 5/12/2004 ND 10.34 NA 839.23 Yes 11/10/2004 ND 10.79 NA 838.78 Yes 5/31/2005 ND 9.73 NA 839.84 Yes 11/15/2005 ND 12.37 NA 837.20 Yes 5/22/2006 ND 11.80 NA 837.77 Yes 11/22/2006 ND 12.18 NA 837.39 Yes 5/22/2007 ND 10.37 NA 839.20 Yes 11/13/2007 ND 14.37 NA 835.20 Yes 5/28/2008 ND 14.75 NA 834.82 Yes 11/19/2008 ND 15.55 NA 834.02 Yes 5/13/2009 ND 13.15 NA 836.42 Yes 11/17/2009 ND 14.61 NA 834.96 Yes 5/30/2013 ND 15.13 NA 834.44 Yes 5/27/2014 ND 10.92 NA 838.65 Yes 5/26/2015 ND 13.22 NA 836.35 Yes 5/11/2016 ND 10.92 NA 838.65 Yes 5/23/2017 ND 14.90 NA 834.67 Yes 5/9/2018 ND 15.15 NA 834.42 Yes 5/28/2019 ND 7.77 NA 841.80 Yes 5/14/2020 ND 9.57 NA 840.00 Yes 5/4/2021 ND 6.53 NA 843.04 Yes 5/11/2022 ND 13.70 NA 835.87 Yes 5/9/2023 ND 11.71 NA 837.86 Yes MW-9 Page 7 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 853.01 830.0 40.0 8/28/2001 ND 21.96 NA 831.05 Yes 11/27/2001 ND 22.78 NA 830.23 Yes 5/15/2002 ND 21.95 NA 831.06 Yes 11/13/2002 ND 23.68 NA 829.33 No 5/23/2003 ND 14.45 NA 838.56 Yes 11/24/2003 ND 13.56 NA 839.45 Yes 5/12/2004 ND 14.79 NA 838.22 Yes 11/10/2004 ND 15.34 NA 837.67 Yes 5/31/2005 ND 14.19 NA 838.82 Yes 11/15/2005 ND 16.79 NA 836.22 Yes 5/22/2006 ND 16.25 NA 836.76 Yes 11/22/2006 ND 16.60 NA 836.41 Yes 5/22/2007 ND 14.86 NA 838.15 Yes 11/13/2007 ND 18.95 NA 834.06 Yes 5/28/2008 ND 19.17 NA 833.84 Yes 11/19/2008 ND 19.98 NA 833.03 Yes 5/13/2009 ND 17.45 NA 835.56 Yes 11/17/2009 ND 19.17 NA 833.84 Yes 5/30/2013 ND 19.41 NA 833.60 Yes 5/27/2014 ND 15.29 NA 837.72 Yes 5/26/2015 ND 17.58 NA 835.43 Yes 5/11/2016 ND 15.51 NA 837.50 Yes 5/23/2017 ND 19.32 NA 833.69 Yes 5/9/2018 ND 19.55 NA 833.46 Yes 5/28/2019 ND 12.34 NA 840.67 Yes 5/14/2020 ND 14.16 NA 838.85 Yes 5/4/2021 ND 11.16 NA 841.85 Yes 5/11/2022 ND 18.20 NA 834.81 Yes 5/9/2023 ND 16.16 NA 836.85 Yes MW-10 Page 8 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 852.61 750.6 122.0 8/28/2001 ND 20.74 NA 831.87 NA 11/27/2001 ND 21.70 NA 830.91 NA 5/15/2002 ND 20.90 NA 831.71 NA 11/13/2002 ND 22.07 NA 830.54 NA 5/23/2003 ND 14.50 NA 838.11 NA 11/24/2003 ND 12.59 NA 840.02 NA 5/12/2004 ND 13.70 NA 838.91 NA 11/10/2004 ND 14.48 NA 838.13 NA 5/31/2005 ND 13.27 NA 839.34 NA 11/15/2005 ND 15.81 NA 836.80 NA 5/22/2006 ND 15.20 NA 837.41 NA 11/22/2006 ND 15.35 NA 837.26 NA 5/22/2007 ND 13.88 NA 838.73 NA 11/13/2007 ND 17.95 NA 834.66 NA 5/28/2008 ND 18.08 NA 834.53 NA 11/19/2008 ND 19.57 NA 833.04 NA 5/13/2009 ND 17.06 NA 835.55 NA 11/17/2009 ND 16.30 NA 836.31 NA 5/13/2010 ND 13.81 NA 838.80 NA 11/16/2010 ND 16.28 NA 836.33 NA 5/26/2011 ND 16.61 NA 836.00 NA 11/22/2011 ND 19.10 NA 833.51 NA 5/4/2012 ND 17.69 NA 834.92 NA 11/21/2012 ND 20.04 NA 832.57 NA 5/31/2013 ND 18.43 NA 834.18 NA 5/27/2014 ND 14.38 NA 838.23 NA 5/26/2015 ND 16.51 NA 836.10 NA 5/11/2016 ND 14.41 NA 838.20 NA 5/23/2017 ND 17.95 NA 834.66 NA 5/9/2018 ND 18.15 NA 834.46 NA 5/28/2019 ND 10.53 NA 842.08 NA 5/14/2020 ND 12.67 NA 839.94 NA 5/4/2021 ND 9.88 NA 842.73 NA 5/11/2022 ND 16.89 NA 835.72 NA 5/9/2023 ND 14.07 NA 838.54 NA MW-11D Page 9 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 852.38 802.4 70.0 8/28/2001 ND 20.65 NA 831.73 NA 11/27/2001 ND 21.52 NA 830.86 NA 5/15/2002 ND 20.70 NA 831.68 NA 11/13/2002 ND 22.13 NA 830.25 NA 5/23/2003 ND 12.15 NA 840.23 NA 11/24/2003 ND 12.37 NA 840.01 NA 5/12/2004 ND 13.53 NA 838.85 NA 11/10/2004 ND 14.23 NA 838.15 NA 5/31/2005 ND 13.04 NA 839.34 NA 11/15/2005 ND 15.59 NA 836.79 NA 5/22/2006 ND 15.05 NA 837.33 NA 11/22/2006 ND 15.05 NA 837.33 NA 5/22/2007 ND 13.64 NA 838.74 NA 11/13/2007 ND 17.74 NA 834.64 NA 5/28/2008 ND 17.90 NA 834.48 NA 11/19/2008 ND 18.67 NA 833.71 NA 5/13/2009 ND 16.26 NA 836.12 NA 11/17/2009 ND 17.52 NA 834.86 NA 5/30/2013 ND 18.22 NA 834.16 NA 5/27/2014 ND 14.14 NA 838.24 NA 5/26/2015 ND 16.25 NA 836.13 NA 5/11/2016 ND 14.23 NA 838.15 NA 5/23/2017 ND 17.92 NA 834.46 NA 5/9/2018 ND 18.10 NA 834.28 NA 5/28/2019 ND 10.97 NA 841.41 NA 5/14/2020 ND 12.82 NA 839.56 NA 5/4/2021 ND 9.99 NA 842.39 NA 5/11/2022 ND 16.86 NA 835.52 NA 5/9/2023 ND 14.88 NA 837.50 NA MW-12D Page 10 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 849.49 799.5 70.0 8/28/2001 ND 18.06 NA 831.43 NA 11/27/2001 ND 18.92 NA 830.57 NA 5/15/2002 ND 18.15 NA 831.34 NA 11/13/2002 ND 19.80 NA 829.69 NA 5/23/2003 ND 10.53 NA 838.96 NA 11/24/2003 ND 9.65 NA 839.84 NA 5/12/2004 ND 10.90 NA 838.59 NA 11/10/2004 ND 11.49 NA 838.00 NA 5/31/2005 ND 10.35 NA 839.14 NA 11/15/2005 ND 12.92 NA 836.57 NA 5/22/2006 ND 12.34 NA 837.15 NA 11/22/2006 ND 12.68 NA 836.81 NA 5/22/2007 ND 10.99 NA 838.50 NA 11/13/2007 ND 15.05 NA 834.44 NA 5/28/2008 ND 15.30 NA 834.19 NA 11/19/2008 ND 16.10 NA 833.39 NA 5/13/2009 ND 13.66 NA 835.83 NA 11/17/2009 ND 15.17 NA 834.32 NA 5/30/2013 ND 15.60 NA 833.89 NA 5/27/2014 ND 11.49 NA 838.00 NA 5/26/2015 ND 13.77 NA 835.72 NA 5/11/2016 ND 11.63 NA 837.86 NA 5/23/2017 ND 15.45 NA 834.04 NA 5/9/2018 ND 15.70 NA 833.79 NA 5/28/2019 ND 8.44 NA 841.05 NA 5/14/2020 ND 10.26 NA 839.23 NA 5/4/2021 ND 7.29 NA 842.20 NA 5/11/2022 ND 14.32 NA 835.17 NA 5/9/2023 ND 12.30 NA 837.19 NA MW-13D Page 11 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 849.08 669.1 200.0 8/28/2001 ND 1.71 NA 847.37 NA 11/27/2001 ND 7.83 NA 841.25 NA 5/15/2002 ND 29.95 NA 819.13 NA 11/13/2002 ND 20.55 NA 828.53 NA 5/23/2003 ND 12.60 NA 836.48 NA 11/24/2003 ND 14.33 NA 834.75 NA 5/12/2004 ND 0.10 NA 848.98 NA 11/10/2004 NM NM NM NM NA 5/31/2005 ND 5.34 NA 843.74 NA 11/15/2005 ND 6.96 NA 842.12 NA 5/22/2006 ND 7.90 NA 841.18 NA 11/22/2006 ND 12.34 NA 836.74 NA 5/22/2007 ND 13.80 NA 835.28 NA 11/13/2007 ND 11.70 NA 837.38 NA 5/28/2008 ND 14.70 NA 834.38 NA 11/19/2008 ND 18.35 NA 830.73 NA 5/13/2009 ND 17.71 NA 831.37 NA 11/17/2009 ND 17.03 NA 832.05 NA 5/30/2013 ND 13.35 NA 835.73 NA 5/26/2015 ND 17.51 NA 831.57 NA 5/11/2016 ND 13.50 NA 835.58 NA 5/23/2017 ND 13.85 NA 835.23 NA 5/9/2018 ND 18.12 NA 830.96 NA 5/28/2019 ND 11.26 NA 837.82 NA 5/14/2020 ND 13.94 NA 835.14 NA 5/4/2021 ND 11.29 NA 837.79 NA 5/11/2022 ND 14.33 NA 834.75 NA 5/9/2023 ND 15.51 NA 833.57 NA MW-14D Page 12 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 835.28 814.3 31.0 8/28/2001 ND 12.52 NA 822.76 Yes 11/29/2001 ND 12.87 NA 822.41 Yes 5/15/2002 ND 11.91 NA 823.37 Yes 11/13/2002 ND 12.55 NA 822.73 Yes 5/23/2003 ND 8.62 NA 826.66 Yes 11/24/2003 ND 8.53 NA 826.75 Yes 5/12/2004 ND 8.64 NA 826.64 Yes 11/10/2004 ND 9.03 NA 826.25 Yes 5/31/2005 ND 8.22 NA 827.06 Yes 11/15/2005 ND 9.91 NA 825.37 Yes 5/22/2006 ND 9.20 NA 826.08 Yes 11/22/2006 ND 8.88 NA 826.40 Yes 5/22/2007 ND 8.47 NA 826.81 Yes 11/13/2007 ND 11.47 NA 823.81 Yes 5/28/2008 ND 10.40 NA 824.88 Yes 11/18/2008 ND 10.98 NA 824.30 Yes 5/13/2009 ND 9.42 NA 825.86 Yes 11/16/2009 ND 10.69 NA 824.59 Yes 5/13/2010 ND 8.54 NA 826.74 Yes 11/17/2010 ND 10.40 NA 824.88 Yes 5/25/2011 ND 10.13 NA 825.15 Yes 11/18/2011 ND 11.76 NA 823.52 Yes 5/2/2012 ND 10.30 NA 824.98 Yes 11/19/2012 ND 12.11 NA 823.17 Yes 5/30/2013 ND 10.01 NA 825.27 Yes 5/27/2014 ND 8.37 NA 826.91 Yes 5/26/2015 ND 9.95 NA 825.33 Yes 5/11/2016 ND 8.95 NA 826.33 Yes 5/23/2017 ND 10.53 NA 824.75 Yes 5/9/2018 ND 10.41 NA 824.87 Yes 5/28/2019 ND 7.22 NA 828.06 Yes 5/14/2020 ND 8.12 NA 827.16 Yes 5/4/2021 ND 6.32 NA 828.96 Yes 5/11/2022 ND 10.04 NA 825.24 Yes 5/9/2023 Could Not Locate MW-15 Page 13 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 835.44 780.4 75.0 8/28/2001 ND 12.62 NA 822.82 NA 11/26/2001 ND 13.14 NA 822.30 NA 5/15/2002 ND 11.60 NA 823.84 NA 11/13/2002 ND 12.20 NA 823.24 NA 5/23/2003 ND 6.90 NA 828.54 NA 11/24/2003 ND 8.90 NA 826.54 NA 5/12/2004 ND 9.03 NA 826.41 NA 11/10/2004 NM NM NM NM NM 5/31/2005 ND 8.67 NA 826.77 NA 11/15/2005 ND 10.22 NA 825.22 NA 5/22/2006 ND 9.62 NA 825.82 NA 11/22/2006 ND 9.34 NA 826.10 NA 5/22/2007 ND 8.92 NA 826.52 NA 11/13/2007 ND 11.82 NA 823.62 NA 5/28/2008 ND 10.75 NA 824.69 NA 11/18/2008 ND 11.27 NA 824.17 NA 5/13/2009 ND 9.81 NA 825.63 NA 11/16/2009 ND 10.99 NA 824.45 NA 5/30/2013 ND 11.15 NA 824.29 NA 5/27/2014 ND 8.51 NA 826.93 NA 5/26/2015 ND 10.34 NA 825.10 NA 5/11/2016 ND 9.38 NA 826.06 NA 5/23/2017 ND 10.89 NA 824.55 NA 5/9/2018 ND 10.38 NA 825.06 NA 5/28/2019 ND 7.71 NA 827.73 NA 5/14/2020 ND 8.60 NA 826.84 NA 5/4/2021 ND 6.90 NA 828.54 NA 5/11/2022 ND 10.40 NA 825.04 NA 5/9/2023 ND 9.76 NA 825.68 NA MW-16D Page 14 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 836.11 761.1 105.0 8/28/2001 ND 13.27 NA 822.84 NA 11/26/2001 ND 13.72 NA 822.39 NA 5/15/2002 ND 12.45 NA 823.66 NA 11/13/2002 ND 12.95 NA 823.16 NA 5/23/2003 ND 7.70 NA 828.41 NA 11/24/2003 ND 9.43 NA 826.68 NA 5/12/2004 ND 9.80 NA 826.31 NA 11/10/2004 ND 10.00 NA 826.11 NA 5/31/2005 ND 9.31 NA 826.80 NA 11/15/2005 ND 10.62 NA 825.49 NA 5/22/2006 ND 10.27 NA 825.84 NA 11/22/2006 ND 10.11 NA 826.00 NA 5/22/2007 ND 9.60 NA 826.51 NA 11/13/2007 ND 12.12 NA 823.99 NA 5/28/2008 ND 11.44 NA 824.67 NA 11/18/2008 ND 12.15 NA 823.96 NA 5/13/2009 ND 10.52 NA 825.59 NA 11/16/2009 ND 11.75 NA 824.36 NA 5/30/2013 ND 10.35 NA 825.76 NA 5/27/2014 NM NM NM NM NM 5/26/2015 ND 10.97 NA 825.14 NA 5/11/2016 ND 10.00 NA 826.11 NA 5/23/2017 ND 11.53 NA 824.58 NA 5/9/2018 ND 11.50 NA 824.61 NA 5/28/2019 ND 8.32 NA 827.79 NA 5/14/2020 ND 9.20 NA 826.91 NA 5/4/2021 ND 7.51 NA 828.60 NA 5/11/2022 ND 11.08 NA 825.03 NA 5/9/2023 ND 5.59 NA 830.52 NA MW-17D Page 15 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 835.72 660.7 215.0 8/28/2001 ND 12.52 NA 823.20 NA 11/26/2001 ND 13.56 NA 822.16 NA 5/15/2002 ND 11.40 NA 824.32 NA 11/13/2002 ND 12.00 NA 823.72 NA 5/23/2003 ND 0.10 NA 835.62 NA 11/24/2003 ND 9.07 NA 826.65 NA 5/12/2004 ND 0.50 NA 835.22 NA 11/10/2004 ND 6.12 NA 829.60 NA 5/31/2005 ND 6.17 NA 829.55 NA 11/15/2005 ND 8.39 NA 827.33 NA 5/22/2006 ND 4.80 NA 830.92 NA 11/22/2006 ND 9.74 NA 825.98 NA 5/22/2007 ND 9.24 NA 826.48 NA 11/13/2007 ND 7.40 NA 828.32 NA 5/28/2008 ND 9.44 NA 826.28 NA 11/18/2008 ND 11.82 NA 823.90 NA 5/13/2009 ND 12.05 NA 823.67 NA 11/16/2009 ND 9.49 NA 826.23 NA 5/13/2010 ND 7.99 NA 827.73 NA 11/17/2010 ND 10.07 NA 825.65 NA 5/26/2011 ND 10.90 NA 824.82 NA 11/18/2011 ND 7.78 NA 827.94 NA 5/4/2012 ND 15.83 NA 819.89 NA 11/20/2012 ND 16.57 NA 819.15 NA 5/30/2013 ND 14.64 NA 821.08 NA 5/26/2015 ND 5.99 NA 829.73 NA 5/11/2016 ND 6.58 NA 829.14 NA 5/23/2017 ND 3.04 NA 832.68 NA 5/9/2018 ND 4.38 NA 831.34 NA 5/28/2019 ND 4.35 NA 831.37 NA 5/14/2020 ND 4.25 NA 831.47 NA 5/4/2021 ND 4.32 NA 831.40 NA 5/11/2022 ND 4.80 NA 830.92 NA 5/9/2023 Could Not Locate MW-18D Page 16 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 865.15 845.2 35.0 8/28/2001 ND 26.04 NA 839.11 No 11/26/2001 ND 26.79 NA 838.36 No 5/15/2002 ND 26.50 NA 838.65 No 11/13/2002 ND 27.88 NA 837.27 No 5/23/2003 ND 19.50 NA 845.65 Yes 11/24/2003 ND 17.83 NA 847.32 Yes 5/12/2004 ND 17.82 NA 847.33 Yes 11/10/2004 ND 18.79 NA 846.36 Yes 5/31/2005 ND 17.33 NA 847.82 Yes 11/15/2005 ND 19.92 NA 845.23 Yes 5/22/2006 ND 19.50 NA 845.65 Yes 11/22/2006 ND 20.19 NA 844.96 No 5/22/2007 ND 18.13 NA 847.02 Yes 11/13/2007 ND 22.05 NA 843.10 No 5/28/2008 ND 22.25 NA 842.90 No 11/19/2008 ND 23.62 NA 841.53 No 5/13/2009 ND 21.35 NA 843.80 No 11/17/2009 ND 22.98 NA 842.17 No 5/30/2013 ND 23.60 NA 841.55 No 5/27/2014 ND 19.81 NA 845.34 Yes 5/26/2015 ND 21.91 NA 843.24 No 5/11/2016 5/23/2017 5/9/2018 5/28/2019 5/14/2020 ND 18.18 NA 846.97 Yes 5/4/2021 ND 15.12 NA 850.03 Yes 5/11/2022 ND 21.38 NA 843.77 No 5/9/2023 Could Not Locate Could Not Locate Could Not Locate Could Not Locate Could Not Locate MW-19 Page 17 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 864.63 702.6 182.0 8/28/2001 ND 29.60 NA 835.03 NA 11/26/2001 ND 26.83 NA 837.80 NA 5/15/2002 ND 26.70 NA 837.93 NA 11/13/2002 ND 30.68 NA 833.95 NA 5/23/2003 ND 27.00 NA 837.63 NA 11/24/2003 ND 17.56 NA 847.07 NA 5/12/2004 ND 17.45 NA 847.18 NA 11/10/2004 ND 18.42 NA 846.21 NA 5/31/2005 ND 16.82 NA 847.81 NA 11/15/2005 ND 19.29 NA 845.34 NA 5/22/2006 ND 19.05 NA 845.58 NA 11/22/2006 ND 20.09 NA 844.54 NA 5/22/2007 ND 17.74 NA 846.89 NA 11/13/2007 ND 21.60 NA 843.03 NA 5/28/2008 ND 22.25 NA 842.38 NA 11/19/2008 ND 24.08 NA 840.55 NA 5/13/2009 ND 22.00 NA 842.63 NA 11/17/2009 ND 22.84 NA 841.79 NA 5/14/2010 ND 18.88 NA 845.75 NA 11/18/2010 ND 20.65 NA 843.98 NA 5/26/2011 ND 21.18 NA 843.45 NA 11/18/2011 ND 23.50 NA 841.13 NA 5/4/2012 ND 23.67 NA 840.96 NA 11/20/2012 ND 24.63 NA 840.00 NA 5/30/2013 ND 23.42 NA 841.21 NA 5/26/2015 ND 21.79 NA 842.84 NA 5/11/2016 ND 19.95 NA 844.68 NA 5/23/2017 5/9/2018 ND 24.41 NA 840.22 NA 5/28/2019 5/14/2020 ND 17.91 NA 846.72 NA 5/4/2021 ND 14.77 NA 849.86 NA 5/11/2022 ND 21.31 NA 843.32 NA 5/9/2023 Could Not Locate MW-20D Could Not Locate Could Not Locate Page 18 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 864.75 840.8 54.0 8/28/2001 ND 33.45 NA 831.30 No 11/27/2001 ND 34.28 NA 830.47 No 5/15/2002 ND 33.50 NA 831.25 No 11/13/2002 ND 34.95 NA 829.80 No 5/23/2003 ND 26.00 NA 838.75 No 11/24/2003 ND 24.88 NA 839.87 No 5/12/2004 ND 26.15 NA 838.60 No 11/10/2004 ND 26.56 NA 838.19 No 5/31/2005 ND 25.44 NA 839.31 No 11/15/2005 ND 28.07 NA 836.68 No 5/22/2006 ND 27.60 NA 837.15 No 11/22/2006 ND 21.15 NA 843.60 Yes 5/22/2007 ND 26.09 NA 838.66 No 11/13/2007 ND 30.20 NA 834.55 No 5/28/2008 ND 30.56 NA 834.19 No 11/19/2008 ND 31.37 NA 833.38 No 5/13/2009 ND 28.76 NA 835.99 No 11/16/2009 ND 30.53 NA 834.22 No 5/30/2013 ND 38.80 NA 825.95 No 5/27/2014 ND 26.51 NA 838.24 No 5/26/2015 ND 28.91 NA 835.84 No 5/11/2016 ND 26.73 NA 838.02 No 5/23/2017 ND 30.70 NA 834.05 No 5/9/2018 ND 31.03 NA 833.72 No 5/28/2019 ND 23.51 NA 841.24 Yes 5/14/2020 ND 25.32 NA 839.43 No 5/4/2021 ND 22.22 NA 842.53 Yes 5/11/2022 ND 29.47 NA 835.28 No 5/9/2023 ND 27.48 NA 837.27 No MW-21 Page 19 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 858.41 831.9 36.5 8/28/2001 ND 26.37 NA 832.04 Yes 11/26/2001 ND 27.25 NA 831.16 No 5/15/2002 ND 26.52 NA 831.89 No 11/13/2002 ND 28.20 NA 830.21 No 5/23/2003 ND 20.12 NA 838.29 Yes 11/24/2003 ND 17.73 NA 840.68 Yes 5/12/2004 ND 19.00 NA 839.41 Yes 11/10/2004 ND 19.53 NA 838.88 Yes 5/31/2005 ND 18.35 NA 840.06 Yes 11/15/2005 ND 20.67 NA 837.74 Yes 5/22/2006 ND 20.45 NA 837.96 Yes 11/22/2006 ND 20.90 NA 837.51 Yes 5/22/2007 ND 19.04 NA 839.37 Yes 11/13/2007 ND 23.05 NA 835.36 Yes 5/28/2008 ND 23.45 NA 834.96 Yes 11/19/2008 ND 24.17 NA 834.24 Yes 5/13/2009 ND 21.80 NA 836.61 Yes 11/16/2009 ND 23.31 NA 835.10 Yes 5/12/2010 ND 19.04 NA 839.37 Yes 11/17/2010 ND 21.38 NA 837.03 Yes 5/25/2011 ND 21.79 NA 836.62 Yes 11/18/2011 ND 24.59 NA 833.82 Yes 5/3/2012 ND 23.04 NA 835.37 Yes 11/19/2012 ND 25.23 NA 833.18 Yes 5/30/2013 ND 25.55 NA 832.86 Yes 5/27/2014 ND 19.57 NA 838.84 Yes 5/26/2015 ND 21.89 NA 836.52 Yes 5/11/2016 ND 19.64 NA 838.77 Yes 5/23/2017 ND 23.58 NA 834.83 Yes 5/9/2018 ND 23.91 NA 834.50 Yes 5/28/2019 ND 16.40 NA 842.01 Yes 5/14/2020 ND 18.17 NA 840.24 Yes 5/4/2021 ND 15.19 NA 843.22 Yes 5/11/2022 ND 22.31 NA 836.10 Yes 5/9/2023 ND 20.42 NA 837.99 Yes MW-22 Page 20 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 860.18 841.2 49.0 8/28/2001 ND 27.12 NA 833.06 No 11/26/2001 ND 27.94 NA 832.24 No 5/15/2002 ND 27.43 NA 832.75 No 11/13/2002 ND 30.68 NA 829.50 No 5/23/2003 ND 21.14 NA 839.04 No 11/24/2003 ND 18.23 NA 841.95 Yes 5/12/2004 ND 19.45 NA 840.73 No 11/10/2004 ND 19.97 NA 840.21 No 5/31/2005 ND 18.76 NA 841.42 Yes 11/15/2005 ND 21.31 NA 838.87 No 5/22/2006 ND 20.85 NA 839.33 No 11/22/2006 ND 21.43 NA 838.75 No 5/22/2007 ND 19.36 NA 840.82 No 11/13/2007 ND 23.35 NA 836.83 No 5/28/2008 ND 23.90 NA 836.28 No 11/19/2008 ND 24.75 NA 835.43 No 5/13/2009 ND 22.34 NA 837.84 No 11/16/2009 ND 23.99 NA 836.19 No 5/12/2010 ND 19.53 NA 840.65 No 11/18/2010 ND 21.81 NA 838.37 No 5/26/2011 ND 22.21 NA 837.97 No 11/18/2011 ND 25.11 NA 835.07 No 5/2/2012 ND 23.60 NA 836.58 No 11/20/2012 ND 25.78 NA 834.40 No 5/30/2013 ND 24.50 NA 835.68 No 5/27/2014 ND 19.99 NA 840.19 No 5/26/2015 ND 22.32 NA 837.86 No 5/11/2016 ND 20.05 NA 840.13 No 5/23/2017 ND 23.97 NA 836.21 No 5/9/2018 ND 24.41 NA 835.77 No 5/28/2019 ND 16.71 NA 843.47 Yes 5/14/2020 ND 18.36 NA 841.82 Yes 5/4/2021 ND 15.41 NA 844.77 Yes 5/11/2022 ND 22.63 NA 837.55 No 5/9/2023 ND 20.74 NA 839.44 No MW-28 Page 21 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 860.24 810.2 70.0 8/28/2001 ND 27.11 NA 833.13 NA 11/28/2001 ND 27.97 NA 832.27 NA 5/15/2002 ND 27.44 NA 832.80 NA 11/13/2002 ND 29.15 NA 831.09 NA 5/23/2003 ND 20.70 NA 839.54 NA 11/24/2003 ND 18.31 NA 841.93 NA 5/12/2004 ND 19.49 NA 840.75 NA 11/10/2004 ND 20.01 NA 840.23 NA 5/31/2005 ND 18.78 NA 841.46 NA 11/15/2005 ND 21.45 NA 838.79 NA 5/22/2006 ND 20.65 NA 839.59 NA 11/22/2006 ND 21.51 NA 838.73 NA 5/22/2007 ND 19.40 NA 840.84 NA 11/13/2007 ND 23.45 NA 836.79 NA 5/28/2008 ND 23.75 NA 836.49 NA 11/19/2008 ND 24.79 NA 835.45 NA 5/13/2009 ND 22.35 NA 837.89 NA 11/16/2009 ND 23.96 NA 836.28 NA 5/13/2010 ND 19.50 NA 840.74 NA 11/18/2010 ND 21.85 NA 838.39 NA 5/26/2011 ND 22.24 NA 838.00 NA 11/18/2011 ND 25.13 NA 835.11 NA 5/4/2012 ND 23.59 NA 836.65 NA 11/20/2012 ND 25.81 NA 834.43 NA 5/31/2013 ND 24.65 NA 835.59 NA 5/27/2014 ND 22.89 NA 837.35 NA 5/26/2015 ND 22.31 NA 837.93 NA 5/11/2016 ND 20.15 NA 840.09 NA 5/23/2017 ND 23.68 NA 836.56 NA 5/9/2018 ND 24.45 NA 835.79 NA 5/28/2019 ND 16.84 NA 843.40 NA 5/14/2020 ND 18.39 NA 841.85 NA 5/4/2021 ND 15.51 NA 844.73 NA 5/11/2022 ND 22.48 NA 837.76 NA 5/9/2023 ND 20.77 NA 839.47 NA MW-29D Page 22 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 868.27 843.3 50.0 8/28/2001 ND 30.50 NA 837.77 No 11/26/2001 ND 31.21 NA 837.06 No 5/15/2002 ND 30.93 NA 837.34 No 11/13/2002 ND 32.75 NA 835.52 No 5/23/2003 ND 25.03 NA 843.24 No 11/24/2003 ND 22.30 NA 845.97 Yes 5/12/2004 ND 22.50 NA 845.77 Yes 11/10/2004 ND 23.41 NA 844.86 Yes 5/31/2005 ND 21.85 NA 846.42 Yes 11/15/2005 ND 23.58 NA 844.69 Yes 5/22/2006 ND 24.10 NA 844.17 Yes 11/22/2006 ND 25.03 NA 843.24 No 5/22/2007 ND 22.62 NA 845.65 Yes 11/13/2007 ND 26.70 NA 841.57 No 5/28/2008 ND 27.30 NA 840.97 No 11/19/2008 ND 28.26 NA 840.01 No 5/13/2009 ND 25.77 NA 842.50 No 11/17/2009 ND 27.95 NA 840.32 No 5/13/2010 ND 23.43 NA 844.84 Yes 11/16/2010 ND 25.88 NA 842.39 No 5/26/2011 ND 25.98 NA 842.29 No 11/22/2011 ND 28.55 NA 839.72 No 5/3/2012 ND 27.42 NA 840.85 No 11/21/2012 ND 29.20 NA 839.07 No 5/30/2013 ND 28.36 NA 839.91 No 5/27/2014 ND 24.31 NA 843.96 Yes 5/26/2015 ND 26.42 NA 841.85 No 5/11/2016 ND 24.62 NA 843.65 Yes 5/23/2017 ND 27.97 NA 840.30 No 5/9/2018 ND 28.53 NA 839.74 No 5/28/2019 ND 21.34 NA 846.93 Yes 5/14/2020 ND 22.67 NA 845.60 Yes 5/4/2021 ND 19.43 NA 848.84 Yes 5/11/2022 ND 25.92 NA 842.35 No 5/9/2023 ND 25.67 NA 842.60 No MW-30 Page 23 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 868.83 843.8 50.0 8/28/2001 ND 31.64 NA 837.19 No 11/26/2001 ND 32.33 NA 836.50 No 5/15/2002 ND 32.07 NA 836.76 No 11/13/2002 ND 33.97 NA 834.86 No 5/23/2003 ND 25.56 NA 843.27 No 11/24/2003 ND 23.49 NA 845.34 Yes 5/12/2004 ND 23.68 NA 845.15 Yes 11/10/2004 ND 24.60 NA 844.23 Yes 5/31/2005 ND 23.07 NA 845.76 Yes 11/15/2005 ND 25.87 NA 842.96 No 5/22/2006 11/22/2006 ND 26.15 NA 842.68 No 5/22/2007 11/13/2007 5/28/2008 5/13/2009 ND 27.02 NA 841.81 No 11/17/2009 ND 29.22 NA 839.61 No 5/30/2013 5/27/2014 5/26/2015 ND 27.60 NA 841.23 No 5/11/2016 ND 25.77 NA 843.06 No 5/23/2017 ND 29.22 NA 839.61 No 5/9/2018 ND 29.75 NA 839.08 No 5/28/2019 5/14/2020 ND 23.88 NA 844.95 Yes 5/4/2021 ND 20.69 NA 848.14 Yes 5/11/2022 ND 27.16 NA 841.67 No 5/9/2023 Could Not Access Well MW-31 Could Not Access Well Could Not Access Well Could Not Access Well Could Not Access Well Could Not Access Well Could Not Access Well Could Not Access Well Page 24 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 868.95 844.0 50.0 8/28/2001 ND 32.38 NA 836.57 No 11/26/2001 ND 33.10 NA 835.85 No 5/15/2002 ND 32.83 NA 836.12 No 11/13/2002 ND 34.75 NA 834.20 No 5/23/2003 ND 26.77 NA 842.18 No 11/24/2003 ND 24.28 NA 844.67 Yes 5/12/2004 ND 24.63 NA 844.32 Yes 11/10/2004 ND 25.49 NA 843.46 No 5/31/2005 ND 24.00 NA 844.95 Yes 11/15/2005 ND 26.75 NA 842.20 No 5/22/2006 ND 26.14 NA 842.81 No 11/22/2006 NM NM NM NM NM 5/22/2007 ND 24.71 NA 844.24 Yes 11/13/2007 ND 28.80 NA 840.15 No 5/28/2008 ND 28.80 NA 840.15 No 11/19/2008 ND 30.13 NA 838.82 No 5/13/2009 ND 27.81 NA 841.14 No 11/17/2009 ND 30.03 NA 838.92 No 5/30/2013 ND 33.30 NA 835.65 No 5/26/2015 ND 28.40 NA 840.55 No 5/11/2016 ND 26.58 NA 842.37 No 5/23/2017 ND 30.00 NA 838.95 No 5/9/2018 ND 30.50 NA 838.45 No 5/28/2019 ND 23.42 NA 845.53 Yes 5/14/2020 ND 24.74 NA 844.21 Yes 5/4/2021 ND 21.60 NA 847.35 Yes 5/11/2022 ND 26.03 NA 842.92 No 5/9/2023 ND 27.47 NA 841.48 No MW-32 Page 25 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 864.98 845.0 50.0 8/28/2001 ND 31.58 NA 833.40 No 11/26/2001 ND 32.37 NA 832.61 No 5/15/2002 ND 31.90 NA 833.08 No 11/13/2002 ND 33.67 NA 831.31 No 5/23/2003 ND 25.00 NA 839.98 No 5/12/2004 ND 23.74 NA 841.24 No 11/10/2004 ND 24.38 NA 840.60 No 5/31/2005 ND 23.01 NA 841.97 No 11/15/2005 ND 25.67 NA 839.31 No 5/22/2006 ND 25.15 NA 839.83 No 11/22/2006 5/22/2007 ND 23.71 NA 841.27 No 11/13/2007 ND 27.80 NA 837.18 No 5/28/2008 11/20/2008 ND 29.21 NA 835.77 No 5/13/2009 ND 26.81 NA 838.17 No 11/17/2009 ND 28.61 NA 836.37 No 5/30/2013 ND 28.94 NA 836.04 No 5/27/2014 ND 24.59 NA 840.39 No 5/26/2015 ND 26.81 NA 838.17 No 5/11/2016 ND 24.63 NA 840.35 No 5/23/2017 5/9/2018 5/28/2019 5/14/2020 5/4/2021 ND 19.86 NA 845.12 Yes 5/11/2022 ND 27.00 NA 837.98 No 5/9/2023 Could Not Locate MW-33 Could Not Locate Could Not Locate Could Not Locate Could Not Locate Could Not Locate Could Not Locate Page 26 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 853.95 833.0 71.0 8/28/2001 ND 21.67 NA 832.28 No 11/26/2001 ND 22.46 NA 831.49 No 5/15/2002 ND 21.84 NA 832.11 No 11/13/2002 ND 23.55 NA 830.40 No 5/23/2003 ND 14.67 NA 839.28 Yes 11/24/2003 ND 12.89 NA 841.06 Yes 5/12/2004 ND 14.27 NA 839.68 Yes 11/10/2004 ND 14.73 NA 839.22 Yes 5/31/2005 ND 13.57 NA 840.38 Yes 11/15/2005 ND 16.00 NA 837.95 Yes 5/22/2006 ND 15.60 NA 838.35 Yes 11/22/2006 ND 16.00 NA 837.95 Yes 5/22/2007 ND 14.20 NA 839.75 Yes 11/13/2007 ND 18.15 NA 835.80 Yes 5/28/2008 ND 18.76 NA 835.19 Yes 11/19/2008 ND 19.42 NA 834.53 Yes 5/13/2009 ND 17.04 NA 836.91 Yes 11/17/2009 ND 18.52 NA 835.43 Yes 5/12/2010 ND 14.21 NA 839.74 Yes 11/16/2010 ND 16.48 NA 837.47 Yes 5/26/2011 ND 16.10 NA 837.85 Yes 11/22/2011 ND 18.89 NA 835.06 Yes 3/20/2012 ND 18.50 NA 835.45 Yes 5/4/2012 ND 18.18 NA 835.77 Yes 11/21/2012 ND 20.35 NA 833.60 Yes 5/30/2013 ND 19.10 NA 834.85 Yes 5/27/2014 ND 14.79 NA 839.16 Yes 5/26/2015 ND 16.99 NA 836.96 Yes 5/11/2016 ND 14.76 NA 839.19 Yes 5/23/2017 ND 18.66 NA 835.29 Yes 5/9/2018 ND 19.02 NA 834.93 Yes 5/28/2019 ND 11.50 NA 842.45 Yes 5/14/2020 ND 13.19 NA 840.76 Yes 5/4/2021 ND 10.27 NA 843.68 Yes 5/11/2022 ND 17.42 NA 836.53 Yes 5/9/2023 ND 15.48 NA 838.47 Yes MW-34 Page 27 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 852.75 831.8 46.0 8/28/2001 ND 26.66 NA 826.09 No 11/29/2001 ND 27.32 NA 825.43 No 5/15/2002 ND 25.52 NA 827.23 No 11/13/2002 ND 27.27 NA 825.48 No 5/23/2003 ND 8.62 NA 844.13 Yes 11/24/2003 ND 19.63 NA 833.12 Yes 5/12/2004 ND 20.20 NA 832.55 Yes 11/10/2004 ND 20.95 NA 831.80 Yes 5/31/2005 ND 19.57 NA 833.18 Yes 11/15/2005 ND 22.35 NA 830.40 No 5/22/2006 ND 21.48 NA 831.27 No 11/22/2006 ND 21.78 NA 830.97 No 5/22/2007 ND 20.03 NA 832.72 Yes 11/13/2007 ND 24.63 NA 828.12 No 5/28/2008 ND 23.32 NA 829.43 No 11/18/2008 ND 24.82 NA 827.93 No 5/13/2009 ND 21.77 NA 830.98 No 11/17/2009 ND 24.62 NA 828.13 No 5/13/2010 ND 19.96 NA 832.79 Yes 11/17/2010 ND 23.16 NA 829.59 No 5/26/2011 ND 22.67 NA 830.08 No 11/17/2011 ND 25.82 NA 826.93 No 3/20/2012 ND 23.42 NA 829.33 No 5/3/2012 ND 23.17 NA 829.58 No 11/19/2012 ND 26.05 NA 826.70 No 5/31/2013 ND 23.22 NA 829.53 No 5/27/2014 ND 18.85 NA 833.90 Yes 5/26/2015 ND 22.60 NA 830.15 No 5/11/2016 ND 20.86 NA 831.89 Yes 5/23/2017 ND 23.50 NA 829.25 No 5/9/2018 ND 24.02 NA 828.73 No 5/28/2019 ND 18.09 NA 834.66 Yes 5/14/2020 ND 19.69 NA 833.06 Yes 5/4/2021 ND 16.75 NA 836.00 Yes 5/11/2022 ND 23.07 NA 829.68 No 5/9/2023 ND 20.93 NA 831.82 Yes MW-35 Page 28 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 857.08 841.1 31.0 8/28/2001 ND 17.55 NA 839.53 No 11/27/2001 ND 18.43 NA 838.65 No 5/15/2002 ND 17.38 NA 839.70 No 11/13/2002 ND 17.58 NA 839.50 No 5/23/2003 ND 11.40 NA 845.68 Yes 11/24/2003 ND 12.75 NA 844.33 Yes 5/12/2004 ND 12.79 NA 844.29 Yes 11/10/2004 ND 13.37 NA 843.71 Yes 5/31/2005 ND 12.51 NA 844.57 Yes 11/15/2005 ND 14.55 NA 842.53 Yes 5/22/2006 ND 13.85 NA 843.23 Yes 11/22/2006 ND 9.84 NA 847.24 Yes 5/22/2007 ND 13.21 NA 843.87 Yes 11/13/2007 ND 15.90 NA 841.18 Yes 5/28/2008 ND 15.40 NA 841.68 Yes 11/20/2008 ND 16.00 NA 841.08 Yes 5/13/2009 ND 14.52 NA 842.56 Yes 11/17/2009 ND 14.84 NA 842.24 Yes 5/30/2013 ND 14.93 NA 842.15 Yes 5/27/2014 ND 12.61 NA 844.47 Yes 5/26/2015 ND 14.73 NA 842.35 Yes 5/11/2016 ND 13.23 NA 843.85 Yes 5/23/2017 ND 14.88 NA 842.20 Yes 5/9/2018 ND 14.87 NA 842.21 Yes 5/28/2019 ND 11.07 NA 846.01 Yes 5/14/2020 ND 12.13 NA 844.95 Yes 5/4/2021 ND 10.14 NA 846.94 Yes 5/11/2022 ND 14.41 NA 842.67 Yes 5/9/2023 ND 12.61 NA 844.47 Yes MW-36 Page 29 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 861.25 833.3 48.0 11/13/2002 ND 33.05 NA 828.20 No 5/23/2003 ND 22.22 NA 839.03 Yes 11/24/2003 ND 23.43 NA 837.82 Yes 5/12/2004 ND 24.30 NA 836.95 Yes 11/10/2004 NM NM NM NM NM 5/31/2005 ND 23.75 NA 837.50 Yes 11/15/2005 NM 26.88*NM NM NM 5/22/2006 NM 25.91*NM NM NM 11/22/2006 NM 26.37*NM NM NM 5/22/2007 ND 24.39 NA 836.86 Yes 11/13/2007 NM NM NM NM NM 5/28/2008 NM 28.45*NM NM NM 11/18/2008 ND 29.98 NA 831.27 No 5/13/2009 NM 26.57*NM NM NM 11/16/2009 ND 29.43 NA 831.82 No 5/30/2013 NM NM NM NM NM 5/26/2015 ND 27.34 NA 833.91 Yes 5/11/2016 NM NM NM NM NM 5/23/2017 ND 28.92 NA 832.33 No 5/9/2018 ND 29.27 NA 831.98 No 5/28/2019 ND 21.66 NA 839.59 Yes 5/14/2020 ND 23.64 NA 837.61 Yes 5/4/2021 ND 20.20 NA 841.05 Yes 5/11/2022 ND 28.06 NA 833.19 No 5/9/2023 ND 25.11 NA 836.14 Yes MW-37 Page 30 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 863.93 838.9 55.0 11/13/2002 ND 33.95 NA 829.98 No 5/23/2003 ND 24.90 NA 839.03 Yes 11/24/2003 ND 23.20 NA 840.73 Yes 5/12/2004 ND 24.49 NA 839.44 Yes 11/10/2004 ND 24.94 NA 838.99 Yes 5/31/2005 ND 23.69 NA 840.24 Yes 11/15/2005 ND 26.27 NA 837.66 No 5/22/2006 NM NM NM NM NM 11/22/2006 ND 26.45 NA 837.48 No 5/22/2007 ND 24.27 NA 839.66 Yes 11/13/2007 NM NM NM NM NM 5/28/2008 NM NM NM NM NM 11/20/2008 ND 29.65 NA 834.28 No 5/13/2009 ND 27.14 NA 836.79 No 11/16/2009 ND 28.90 NA 835.03 No 5/30/2013 ND 29.29 NA 834.64 No 5/26/2015 ND 27.19 NA 836.74 No 5/11/2016 ND 24.94 NA 838.99 Yes 5/23/2017 ND 29.06 NA 834.87 No 5/9/2018 ND 29.51 NA 834.42 No 5/28/2019 ND 21.64 NA 842.29 Yes 5/14/2020 ND 23.58 NA 840.35 Yes 5/4/2021 ND 20.40 NA 843.53 Yes 5/11/2022 5/9/2023 ND 25.84 NA 838.09 No MW-38 Dry Page 31 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) NM NM 55.0 11/13/2002 ND 33.35*NM NM NM 5/28/2003 ND 23.53 NA NA NM 11/17/2003 ND 21.68 NA NA NM 5/12/2004 ND 23.28*NM NM NM 5/27/2005 ND 22.43 NA NA NM 5/31/2005 ND 22.49*NM NM NM 11/15/2005 ND 21.07*NM NM NM 5/22/2006 ND 20.66*NM NM NM 5/7/2007 ND 18.91*NM NM NM 11/13/2007 ND 27.11 NA NA NM 5/9/2008 ND 27.85*NM NM NM 11/20/2008 ND 28.45 NA NA NM 5/13/2009 ND 25.95 NA NA NM 11/16/2009 ND 27.66 NA NA NM 5/30/2013 5/26/2015 ND 25.97 NA NA NM 5/11/2016 ND 23.70 NA NA NM 5/23/2017 ND 27.78 NA NA NM 5/9/2018 5/28/2019 5/14/2020 5/4/2021 ND 19.14 NA NA NM 5/11/2022 5/9/2023 ND 24.46 NA NA NM MW-39 Could Not Locate Could Not Locate Could Not Locate Could Not Locate Could Not Locate Page 32 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 859.27 839.3 50.0 11/13/2002 ND 28.85 NA 830.42 No 5/23/2003 ND 19.45 NA 839.82 Yes 11/24/2003 ND 17.91 NA 841.36 Yes 5/12/2004 ND 19.30 NA 839.97 Yes 11/10/2004 ND 19.72 NA 839.55 Yes 5/31/2005 ND 18.51 NA 840.76 Yes 11/15/2005 ND 21.09 NA 838.18 No 5/22/2006 NM NM NM NM NM 11/22/2006 NM NM NM NM NM 5/22/2007 ND 19.11 NA 840.16 Yes 11/13/2008 NM NM NM NM NM 5/28/2008 NM NM NM NM NM 11/20/2008 ND 24.48 NA 834.79 No 5/13/2009 ND 22.02 NA 837.25 No 11/16/2009 ND 23.69 NA 835.58 No 5/2/2012 ND 27.61 NA 831.66 No 5/30/2013 NM NM NM NM NM 5/27/2014 ND 19.55 NA 839.72 Yes 5/26/2015 ND 22.03 NA 837.24 No 5/11/2016 ND 19.73 NA 839.54 Yes 5/23/2017 ND 23.77 NA 835.50 No 5/9/2018 NM NM NM NM NM 5/28/2019 ND 16.42 NA 842.85 Yes 5/14/2020 ND 18.27 NA 841.00 Yes 5/4/2021 ND 15.19 NA 844.08 Yes 5/11/2022 ND 22.55 NA 836.72 No 5/9/2023 Could Not Locate MW-40 Page 33 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 857.75 832.8 50.0 11/13/2002 NM 27.12*NM NM NM 5/23/2003 ND 17.83 NA 839.92 Yes 11/24/2003 ND 15.97 NA 841.78 Yes 5/12/2004 ND 17.28 NA 840.47 Yes 11/10/2004 ND 17.72 NA 840.03 Yes 5/31/2005 ND 16.51 NA 841.24 Yes 11/15/2005 NM 19.05*NM NM NM 5/22/2006 NM 18.63*NM NM NM 5/7/2007 ND 18.61 NA 839.14 Yes 11/13/2007 ND 21.18 NA 836.57 Yes 5/9/2008 ND 21.90 NA 835.85 Yes 11/19/2008 ND 22.56 NA 835.19 Yes 5/13/2009 ND 20.15 NA 837.60 Yes 11/17/2009 ND 21.75 NA 836.00 Yes 5/30/2013 NM NM NM NM NM 5/27/2014 NM NM NM NM NM 5/26/2015 NM NM NM NM NM 5/11/2016 17.75 18.02 0.27 839.92 **Yes 5/23/2017 5/9/2018 5/28/2019 5/14/2020 5/4/2021 5/11/2022 5/9/2023 MW-41 Well Under Wood Pile Well Under Wood Pile Well Under Wood Pile Well Under Wood Pile Well Under Wood Pile Well Under Wood Pile Well Under Wood Pile Page 34 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 864.26 839.3 35.0 5/15/2002 31.20 32.25 1.05 832.77 **No 11/13/2002 32.80 33.85 1.05 831.17 **No 5/28/2003 23.15 25.40 2.25 840.48 **Yes 11/17/2003 21.40 21.42 0.02 842.85 **Yes 5/12/2004 22.95 22.97 0.02 841.30 **Yes 11/10/2004 23.39 23.44 0.05 840.86 **Yes 5/27/2005 ND 22.05 NA 842.21 Yes 11/15/2005 24.67 25.43 0.76 839.38 **Yes 5/22/2006 24.28 24.82 0.54 839.83 **Yes 11/22/2006 24.63 25.24 0.61 839.46 **Yes 5/7/2007 22.50 22.95 0.45 841.63 **Yes 11/13/2007 26.90 27.45 0.55 837.21 **No 5/9/2008 28.28 28.30 0.02 835.97 **No 5/27/2014 22.63 22.67 0.04 841.62 **Yes 5/11/2016 23.02 23.03 0.01 841.24 **Yes 5/23/2017 ND 27.19 NA 837.07 No 5/9/2018 27.78 27.82 0.04 836.47 **No 5/28/2019 19.74 20.02 0.28 844.44 **Yes 5/14/2020 21.41 21.90 0.49 842.71 **Yes 5/5/2021 18.41 18.54 0.13 845.81 **Yes 5/11/2022 ND 25.96 NA 838.30 Yes 5/9/2023 ND 23.72 NA 840.54 Yes MW-1 Recovery Wells Page 35 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 864.90 844.9 30.0 5/15/2002 ND 31.30 NA 833.6 No 11/13/2002 32.95 32.96 0.01 831.95 **No 5/28/2003 ND 23.90 NA 841.00 No 11/17/2003 ND 21.88 NA 843.02 No 5/12/2004 23.34 23.35 0.01 841.56 **No 5/27/2005 ND 22.58 NA 842.32 No 11/15/2005 25.25 25.26 0.01 839.65 **No 5/22/2006 ND 24.70 NA 840.20 No 11/22/2006 ND 25.15 NA 839.75 No 5/7/2007 23.01 23.02 0.01 841.89 **No 11/13/2007 27.29 27.29 0.00 837.61 **No 5/9/2008 ND 28.00 NA 836.90 No 5/27/2014 ND 23.12 NA 841.78 No 5/27/2015 ND 25.85 NA 839.05 No 5/11/2016 ND 23.53 NA 841.37 No 5/23/2017 ND 27.48 NA 837.42 No 5/9/2018 ND 28.00 NA 836.90 No 5/28/2019 ND 20.22 NA 844.68 No 5/14/2020 ND 21.90 NA 843.00 No 5/5/2021 ND 18.95 NA 845.95 Yes 5/11/2022 5/9/2023 ND 24.17 NA 840.73 No MW-23 Could Not Locate Page 36 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 864.56 844.6 35.0 5/15/2002 30.32 31.15 0.83 834.01 **No 11/13/2002 31.43 33.62 2.19 832.52 **No 5/28/2003 23.6 24.33 0.73 840.76 **No 11/17/2003 21.33 21.43 0.10 843.20 **No 5/12/2004 22.6 22.92 0.32 841.87 **No 11/10/2004 23.08 23.55 0.47 841.35 **No 5/27/2005 21.81 22.96 1.15 842.43 **No 11/15/2005 24.26 24.39 0.13 840.26 **No 5/22/2006 23.73 23.96 0.23 840.77 **No 11/22/2006 24.4 24.53 0.13 840.12 **No 5/7/2007 22.28 22.29 0.01 842.28 **No 11/13/2007 25.9 26.58 0.68 838.47 **No 5/9/2008 ND 26.53 NA 838.03 No 11/21/2012 ND DRY NA NA NA 5/27/2014 ND 22.37 NA 842.19 No 5/27/2015 ND 24.41 NA 840.15 No 5/11/2016 22.62 22.63 0.01 841.94 **No 5/23/2017 ND 25.83 NA 838.73 No 5/9/2018 ND 26.33 NA 838.23 No 5/28/2019 5/14/2020 ND 21.13 NA 843.43 No 5/5/2021 ND 18.42 NA 846.14 Yes 5/11/2022 5/9/2023 ND 23.39 NA 841.17 No MW-25 Could Not Open Lock On Vault Could Not Open Lock On Vault Page 37 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 863.46 843.5 40.0 5/15/2002 30.25 31.65 1.4 832.82 **No 11/13/2002 31.9 32.75 0.85 831.32 **No 5/28/2003 22.3 23.54 1.24 840.81 **No 11/17/2003 ND 20.50 NA 842.96 No 5/12/2004 21.98 22.20 0.22 841.42 **No 11/10/2004 22.51 22.71 0.2 840.89 **No 5/27/2005 21.12 21.32 0.2 842.28 **No 11/15/2005 23.94 24.20 0.26 839.45 **No 5/22/2006 23.4 23.46 0.06 840.04 **No 11/22/2006 23.75 23.76 0.01 839.71 **No 5/7/2007 21.74 21.76 0.02 841.71 **No 11/13/2007 25.97 26.17 0.2 837.43 **No 5/9/2008 26.96 27.10 0.14 836.46 **No 11/16/2010 ND 24.31 NA 839.15 No 11/22/2011 27.75 27.89 0.14 835.67 **No 11/21/2012 28.43 28.83 0.4 834.92 **No 5/27/2014 ND 21.85 NA 841.61 No 5/11/2016 Trace 22.64 Trace 840.82 No 5/23/2017 ND 26.57 NA 836.89 No 5/9/2018 ND 27.12 NA 836.34 No 5/28/2019 19.00 19.02 0.02 844.44 **Yes 5/14/2020 20.74 20.76 0.02 842.71 **No 5/5/2021 ND 18.15 NA 845.31 Yes 5/11/2022 ND 25.29 NA 838.17 No 5/9/2023 ND 23.13 NA 840.33 No RW-1 Page 38 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.34 837.3 45.0 5/15/2002 29.95 30.65 0.70 832.19 **No 11/13/2002 31.30 33.95 2.65 830.30 **No 5/28/2003 22.45 23.75 1.30 839.53 **Yes 11/17/2003 20.25 20.31 0.06 842.07 **Yes 5/12/2004 21.80 21.97 0.17 840.49 **Yes 11/10/2004 22.40 22.43 0.03 839.93 **Yes 5/27/2005 20.95 21.02 0.07 841.37 **Yes 11/15/2005 23.57 23.92 0.35 838.67 **Yes 5/22/2006 23.25 23.42 0.17 839.04 **Yes 11/22/2006 23.60 23.80 0.20 838.68 **Yes 5/7/2007 21.58 21.74 0.16 840.72 **Yes 11/13/2007 25.78 26.13 0.35 836.46 **No 5/9/2008 ND 26.49 NA 835.85 No 11/21/2012 28.27 28.28 0.01 834.07 **No 5/27/2014 22.05 22.07 0.02 840.28 **Yes 5/27/2015 24.70 24.75 0.05 837.63 **Yes 5/11/2016 Trace 22.60 Trace 839.74 Yes 5/23/2017 ND 26.52 NA 835.82 No 5/9/2018 ND 26.95 NA 835.39 No 5/28/2019 ND 19.69 NA 842.65 Yes 5/14/2020 ND 20.82 NA 841.52 Yes 5/5/2021 ND 18.28 NA 844.06 Yes 5/11/2022 ND 25.20 NA 837.14 No 5/9/2023 ND 23.23 NA 839.11 Yes RW-2 Page 39 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.37 842.4 40.0 5/15/2002 29.60 32.10 2.50 832.07 **No 11/13/2002 31.20 34.50 3.30 830.25 **No 5/28/2003 21.95 23.60 1.65 839.96 **No 11/17/2003 20.07 21.20 1.13 841.98 **No 5/12/2004 21.60 22.35 0.75 840.56 **No 11/10/2004 22.05 22.80 0.75 840.11 **No 11/15/2005 23.56 23.67 0.11 838.78 **No 5/22/2006 23.10 23.28 0.18 839.22 **No 11/22/2006 23.14 23.15 0.01 839.23 **No 5/7/2007 21.34 21.36 0.02 841.02 **No 11/13/2007 25.73 26.21 0.48 837.60 **No 5/9/2008 ND 27.20 NA 835.17 No 11/16/2010 ND 23.91 NA 838.46 No 11/22/2011 ND 27.41 NA 834.96 No 11/21/2012 28.27 28.47 0.20 835.13 **No 5/27/2014 22.07 22.08 0.01 841.39 **No 5/11/2016 22.36 22.37 0.01 841.10 **No 5/23/2017 Trace 26.38 NA 835.99 No 5/9/2018 ND 26.90 NA 835.47 No 5/28/2019 18.85 18.89 0.04 844.60 **Yes 5/14/2020 ND 20.98 NA 841.39 No 5/5/2021 17.64 17.71 0.07 845.80 **Yes 5/11/2022 25.02 25.22 0.20 838.38 **No 5/9/2023 23.00 23.02 0.02 840.45 **No RW-3 Page 40 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 863.73 843.7 45.0 5/15/2002 29.3 30.05 0.75 834.22 **No 11/13/2002 31.08 31.28 0.20 832.59 **No 5/28/2003 ND 21.75 NA 841.98 No 11/17/2003 20.1 20.14 0.04 843.62 **No 5/12/2004 21.6 21.78 0.18 842.08 **No 11/10/2004 22.18 22.21 0.03 841.54 **No 5/27/2005 ND 20.55 NA 843.18 No 11/15/2005 23.24 23.62 0.38 840.38 **No 5/22/2006 22.84 22.98 0.14 840.85 **No 11/22/2006 23.22 23.24 0.02 840.50 **No 5/7/2007 21.11 21.13 0.02 842.61 **No 11/13/2007 25.56 25.63 0.07 838.15 **No 5/9/2008 25.86 25.88 0.02 837.86 **No 11/16/2009 ND 25.88 NA 837.85 No 5/1/2010 ND 21.74 NA 841.99 No 11/21/2012 26.98 27.02 0.04 836.74 **No 5/27/2014 20.72 20.73 0.01 843.01 **No 5/27/2015 ND 23.37 NA 840.36 No 5/11/2016 NM NM NM NM NM 5/23/2017 25.28 25.31 0.03 838.44 **No 5/9/2018 ND 25.76 NA 837.97 No 5/28/2019 18.40 18.43 0.03 845.30 **Yes 5/14/2020 20.03 20.05 0.02 843.69 **No 5/5/2021 ND 17.40 NA 846.33 Yes 5/11/2022 ND 24.42 NA 839.31 No 5/9/2023 ND 22.22 NA 841.51 No RW-4 Page 41 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.22 838.2 34.0 5/15/2002 29.25 29.80 0.55 832.82 **No 11/13/2002 30.90 31.00 0.10 831.29 **No 5/28/2003 21.40 22.00 0.60 840.22 **Yes 11/17/2003 ND 19.60 NA 842.62 Yes 5/12/2004 21.02 21.19 0.17 841.15 **Yes 11/10/2004 21.51 21.55 0.04 840.70 **Yes 5/27/2005 20.16 20.23 0.07 842.04 **Yes 11/15/2005 23.10 23.42 0.32 839.03 **Yes 5/22/2006 22.58 22.60 0.02 839.63 **Yes 11/22/2006 22.60 22.61 0.01 839.62 **Yes 5/7/2007 20.65 20.66 0.01 841.57 **Yes 11/13/2007 25.07 25.38 0.31 837.06 **No 5/9/2008 25.89 25.96 0.07 836.31 **No 5/27/2014 ND 20.57 NA 841.65 Yes 5/27/2015 ND 23.28 NA 838.94 Yes 5/11/2016 ND 21.11 NA 841.11 Yes 5/23/2017 ND 25.13 NA 837.09 No 5/9/2018 ND 25.74 NA 836.48 No 5/28/2019 ND 17.95 NA 844.27 Yes 5/14/2020 ND 19.60 NA 842.62 Yes 5/5/2021 ND 16.66 NA 845.56 Yes 5/11/2022 ND 23.90 NA 838.32 Yes 5/9/2023 ND 21.61 NA 840.61 Yes RW-5 Page 42 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 861.84 841.8 45.0 5/15/2002 29.15 31.75 2.60 831.96 **No 11/13/2002 30.87 33.90 3.03 830.12 **No 5/28/2003 ND 21.90 NA 839.94 No 11/17/2003 19.95 19.98 0.03 841.88 **Yes 5/12/2004 21.39 22.39 1.00 840.17 **No 11/10/2004 21.95 21.97 0.02 839.88 **No 5/27/2005 20.65 20.81 0.16 841.15 **No 11/15/2005 23.25 23.73 0.48 838.46 **No 5/22/2006 ND 22.81 NA 839.03 No 11/22/2006 ND 23.70 NA 838.14 No 5/7/2007 ND 21.15 NA 840.69 No 11/13/2007 25.4 25.70 0.30 836.36 **No 5/9/2008 26.2 27.33 1.13 835.32 **No 11/18/2009 ND 26.11 NA 835.73 No 11/16/2010 ND 23.58 NA 838.26 No 11/17/2011 27.19 27.32 0.13 834.61 **No 11/21/2012 27.88 28.03 0.15 833.92 **No 5/30/2013 ND 26.40 NA 835.44 No 5/27/2014 ND 21.78 NA 840.06 No 5/27/2015 ND 24.40 NA 837.44 No 5/11/2016 ND 22.04 NA 839.80 No 5/23/2017 ND 25.13 NA 836.71 No 5/9/2018 ND 26.58 NA 835.26 No 5/28/2019 ND 18.67 NA 843.17 Yes 5/14/2020 ND 20.50 NA 841.34 No 5/5/2021 ND 18.43 NA 843.41 Yes 5/11/2022 ND 24.90 NA 836.94 No 5/9/2023 ND 22.75 NA 839.09 No RW-6 Page 43 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.09 841.1 48.0 5/15/2002 28.70 29.50 0.80 833.17 **No 11/13/2002 30.40 30.72 0.32 831.60 **No 5/28/2003 ND 21.10 NA 840.99 No 11/17/2003 19.48 19.50 0.02 842.60 **Yes 5/12/2004 20.76 20.78 0.02 841.32 **Yes 11/10/2004 21.02 21.03 0.01 841.07 **No 5/27/2005 19.98 20.00 0.02 842.10 **Yes 11/15/2005 22.64 22.72 0.08 839.43 **No 5/22/2006 22.13 22.14 0.01 839.96 **No 11/22/2006 22.19 22.20 0.01 839.90 **No 5/7/2007 20.43 20.45 0.02 841.65 **Yes 11/13/2007 24.69 24.78 0.09 837.37 **No 5/9/2008 25.23 25.24 0.01 836.86 **No 11/21/2012 ND 26.60 NA 835.49 No 5/27/2014 ND 20.25 NA 841.84 Yes 5/27/2015 23.02 23.03 0.01 839.07 **No 5/11/2016 20.88 20.90 0.02 841.2 **Yes 5/23/2017 24.69 24.86 0.17 837.35 **No 5/9/2018 25.42 25.57 0.15 836.63 **No 5/28/2019 5/14/2020 5/5/2021 16.59 16.67 0.08 845.48 **Yes 5/11/2022 5/9/2023 21.29 21.34 0.05 840.79 **No RW-8 Could Not Open Vault Could Not Open Vault Could Not Open Vault Page 44 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.91 846.9 41.0 5/15/2002 28.95 31.30 2.35 833.30 **No 11/13/2002 30.7 32.65 1.95 831.66 **No 5/28/2003 21.1 22.80 1.70 841.33 **No 11/17/2003 19.4 19.60 0.20 843.45 **No 5/12/2004 21.8 22.40 0.60 840.94 **No 11/10/2004 21.3 21.50 0.20 841.55 **No 5/27/2005 20.1 20.16 0.06 842.79 **No 11/15/2005 22.8 22.99 0.19 840.06 **No 5/22/2006 22.27 22.33 0.06 840.62 **No 11/22/2006 ND 20.94 NA 841.97 No 5/7/2007 20.5 20.51 0.01 842.41 **No 11/13/2007 24 25.29 1.29 838.55 **No 5/9/2008 25.69 25.70 0.01 837.22 **No 11/19/2009 25.63 25.64 0.01 837.28 **No 11/16/2010 ND 23.04 NA 839.87 No 11/22/2011 ND 26.90 NA 836.01 No 11/21/2012 ND 27.49 NA 835.42 No 5/30/2013 ND 25.70 NA 837.21 No 5/27/2014 21.61 21.64 0.03 841.29 **No 5/27/2015 ND 23.63 NA 839.28 No 5/11/2016 ND 21.28 NA 841.63 No 5/23/2017 ND 25.54 NA 837.37 No 5/9/2018 ND 26.06 NA 836.85 No 5/28/2019 17.94 17.95 0.01 844.96 **No 5/14/2020 ND 19.61 NA 843.30 No 5/5/2021 ND 16.66 NA 846.25 No 5/11/2022 ND 24.03 NA 838.88 No 5/9/2023 ND 21.73 NA 841.18 No RW-9 Page 45 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 861.38 836.4 50.0 5/15/2002 28.60 31.20 2.60 832.05 **No 11/13/2002 30.23 33.40 3.17 830.26 **No 5/28/2003 ND 21.13 NA 840.25 Yes 11/17/2003 ND 19.22 NA 842.16 Yes 5/12/2004 20.69 20.74 0.05 840.68 **Yes 11/10/2004 21.16 21.20 0.04 840.21 **Yes 5/27/2005 19.80 19.86 0.06 841.56 **Yes 11/15/2005 22.56 22.58 0.02 838.81 **Yes 5/22/2006 22.08 22.10 0.02 839.29 **Yes 11/22/2006 21.52 21.54 0.02 839.85 **Yes 5/7/2007 20.24 20.26 0.02 841.13 **Yes 11/13/2007 24.72 24.81 0.09 836.63 **Yes 5/9/2008 25.54 25.64 0.10 835.81 **No 11/21/2012 27.34 27.38 0.04 834.03 **No 5/27/2014 ND 20.73 NA 840.65 Yes 5/27/2015 23.00 23.65 0.65 838.20 **Yes 5/11/2016 ND 21.25 NA 840.13 Yes 5/23/2017 25.31 25.34 0.03 836.06 **No 5/9/2018 ND 25.88 NA 835.50 No 5/28/2019 17.96 17.98 0.02 843.41 **Yes 5/14/2020 19.67 19.73 0.06 841.69 **Yes 5/5/2021 ND 16.68 NA 844.70 Yes 5/11/2022 23.99 24.01 0.02 837.37 **Yes 5/9/2023 Could Not Open Vault RW-10 Page 46 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 863.02 840.0 48.0 5/15/2002 30.5 32.90 2.40 831.85 **No 11/13/2002 32.03 35.65 3.62 829.98 **No 5/28/2003 23.2 24.05 0.85 839.58 **No 11/17/2003 21.29 21.39 0.10 841.70 **Yes 5/12/2004 22.85 23.00 0.15 840.13 **Yes 11/10/2004 23.41 23.60 0.19 839.56 **No 5/27/2005 22.00 22.28 0.28 840.94 **Yes 11/15/2005 24.78 24.95 0.17 838.19 **No 5/22/2006 24.25 24.44 0.19 838.72 **No 11/22/2006 24.45 24.57 0.12 838.54 **No 5/7/2007 22.63 22.64 0.01 840.39 **Yes 11/13/2007 26.83 27.36 0.53 836.04 **No 5/9/2008 NM NM NM NM NM 11/21/2012 29.28 29.39 0.11 833.71 **No 5/27/2014 22.92 22.94 0.02 840.09 **Yes 5/27/2015 ND 24.04 NA 838.98 No 5/11/2016 Trace 23.75 Trace 839.27 No 5/23/2017 27.50 27.84 0.34 835.42 **No 5/9/2018 27.98 28.02 0.04 835.03 **No 5/28/2019 20.10 20.30 0.20 842.86 **Yes 5/14/2020 22.00 22.07 0.07 841.00 **Yes 5/5/2021 ND 19.50 NA 843.52 Yes 5/11/2022 26.53 26.72 0.19 836.30 **No 5/9/2023 ND 24.44 NA 838.58 No RW-11 Page 47 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 860.89 839.9 46.0 5/15/2002 28.12 30.70 2.58 832.05 **No 11/13/2002 30.05 31.11 1.06 830.54 **No 5/28/2003 ND 22.88 NA 838.01 No 11/17/2003 18.84 18.85 0.01 842.05 **Yes 5/12/2004 20.24 20.25 0.01 840.65 **Yes 11/10/2004 20.68 20.69 0.01 840.21 **Yes 5/27/2005 ND 20.33 NA 840.56 Yes 11/15/2005 22.04 22.23 0.19 838.80 **No 5/22/2006 21.6 21.61 0.01 839.29 **No 11/22/2006 25.03 25.04 0.01 835.86 **No 5/7/2007 19.78 19.80 0.02 841.10 **Yes 11/13/2007 24.23 24.39 0.16 836.62 **No 5/9/2008 24.84 24.85 0.01 836.05 **No 11/21/2012 ND 26.92 NA 833.97 No 5/27/2014 22.92 22.94 0.02 837.96 **No 5/27/2015 ND 23.08 NA 837.81 No 5/11/2016 ND 20.75 NA 840.14 Yes 5/23/2017 ND 24.77 NA 836.12 No 5/9/2018 ND 25.33 NA 835.56 No 5/28/2019 ND 17.49 NA 843.40 Yes 5/14/2020 ND 19.17 NA 841.72 Yes 5/5/2021 ND 16.21 NA 844.68 Yes 5/11/2022 ND 23.48 NA 837.41 No 5/9/2023 ND 21.13 NA 839.76 No RW-12 Page 48 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 861.32 840.3 46.0 5/15/2002 28.55 29.50 0.95 832.50 **No 11/13/2002 30.25 30.40 0.15 831.03 **No 5/28/2003 20.5 20.65 0.15 840.78 **Yes 11/17/2003 19.1 19.20 0.10 842.19 **Yes 5/12/2004 20.35 20.36 0.01 840.97 **Yes 11/10/2004 20.8 20.82 0.02 840.51 **Yes 5/27/2005 19.45 19.54 0.09 841.84 **Yes 11/15/2005 22.15 22.44 0.29 839.09 **No 5/22/2006 21.75 21.85 0.10 839.54 **No 5/7/2007 19.9 19.92 0.02 841.41 **Yes 11/13/2007 24.35 24.58 0.23 836.91 **No 5/9/2008 24.98 25.00 0.02 836.33 **No 11/16/2009 25.1 25.11 0.01 836.22 **No 11/21/2012 ND 26.93 NA 834.39 No 5/30/2013 ND 24.95 NA 836.37 No 5/27/2014 ND 20.05 NA 841.27 Yes 5/27/2015 ND 22.98 NA 838.34 No 5/11/2016 NM NM NM NM NA 5/23/2017 ND 24.08 NA 837.24 No 5/9/2018 ND 25.29 NA 836.03 No 5/28/2019 ND 17.54 NA 843.78 Yes 5/14/2020 ND 19.15 NA 842.17 Yes 5/5/2021 ND 16.24 NA 845.08 Yes 5/11/2022 ND 23.42 NA 837.90 No 5/9/2023 ND 20.99 NA 840.33 Yes RW-13 Page 49 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.27 844.3 43.0 5/15/2002 29.6 32.10 2.50 831.97 **No 11/13/2002 31.15 34.77 3.62 830.11 **No 5/28/2003 22.05 24.10 2.05 839.65 **No 11/17/2003 20.33 20.63 0.30 841.86 **No 5/12/2004 21.85 22.00 0.15 840.38 **No 11/10/2004 22.42 22.65 0.23 839.79 **No 5/27/2005 21.01 21.12 0.11 841.23 **No 11/15/2005 23.82 23.91 0.09 838.42 **No 5/22/2006 23.28 23.30 0.02 838.98 **No 5/7/2007 21.52 21.54 0.02 840.74 **No 11/13/2007 25.83 26.30 0.47 836.31 **No 5/9/2008 26.6 26.69 0.09 835.64 **No 11/16/2009 ND 26.21 NA 836.06 No 11/16/2010 ND 23.62 NA 838.65 No 11/22/2011 ND 27.06 NA 835.21 No 11/21/2012 28.01 28.08 0.07 834.24 **No 5/30/2013 ND 26.70 NA 835.57 No 5/27/2014 ND 21.59 NA 840.68 No 5/27/2015 ND 24.30 NA 837.97 No 5/11/2016 Trace 22.30 Trace 839.97 No 5/23/2017 ND 26.18 NA 836.09 No 5/9/2018 ND 26.61 NA 835.66 No 5/28/2019 18.86 18.87 0.01 843.40 **No 5/14/2020 ND 20.61 NA 841.66 No 5/5/2021 ND 18.39 NA 843.88 No 5/11/2022 25.37 25.50 0.13 836.77 **No 5/9/2023 ND 23.18 NA 839.09 No RW-15 Page 50 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.50 841.5 46.0 5/15/2002 29.7 31.90 2.20 832.18 **No 11/13/2002 31.4 34.00 2.60 830.37 **No 5/28/2003 22.35 23.55 1.20 839.81 **No 11/17/2003 20.22 20.65 0.43 842.16 **Yes 5/12/2004 21.86 21.87 0.01 840.64 **No 11/10/2004 22.39 22.41 0.02 840.10 **No 5/27/2005 21.12 21.14 0.02 841.37 **No 11/15/2005 23.63 23.88 0.25 838.80 **No 5/22/2006 23.29 23.43 0.14 839.17 **No 11/22/2006 23.63 23.72 0.09 838.84 **No 5/7/2007 21.55 21.58 0.03 840.94 **No 11/13/2007 25.86 25.97 0.11 836.61 **No 5/9/2008 26.6 27.10 0.50 835.76 **No 11/18/2009 ND 26.61 NA 835.89 No 11/16/2010 ND 24.27 NA 838.23 No 11/17/2011 ND 27.67 NA 834.83 No 11/21/2012 28.3 28.31 0.01 834.20 **No 5/30/2013 ND 27.00 NA 835.50 No 5/27/2014 ND 22.19 NA 840.31 No 5/27/2015 ND 20.35 NA 842.15 Yes 5/11/2016 ND 22.52 NA 839.98 No 5/23/2017 ND 26.52 NA 835.98 No 5/9/2018 ND 26.97 NA 835.53 No 5/28/2019 ND 19.61 NA 842.89 Yes 5/14/2020 ND 20.80 NA 841.70 Yes 5/5/2021 ND 17.85 NA 844.65 Yes 5/11/2022 ND 25.38 NA 837.12 No 5/9/2023 ND 23.10 NA 839.40 No RW-16 Page 51 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 863.07 844.1 39.0 15/05/2002 29.8 30.40 0.6 833.10 **No 13/11/2002 31.54 31.75 0.21 831.47 **No 28/05/2003 ND 22.20 NA 840.87 No 17/11/2003 20.11 20.21 0.1 842.93 **No 12/05/2004 21.68 21.76 0.08 841.37 **No 10/11/2004 22.17 22.18 0.01 840.90 **No 27/05/2005 20.85 20.87 0.02 842.21 **No 15/11/2005 23.5 23.60 0.1 839.54 **No 22/05/2006 23.02 23.04 0.02 840.04 **No 22/11/2006 23.41 23.42 0.01 839.66 **No 7/05/2007 21.3 21.31 0.01 841.77 **No 13/11/2007 25.64 25.79 0.15 837.39 **No 9/05/2008 26.42 26.50 0.08 836.63 **No 17/11/2009 ND 26.32 NA 836.75 No 16/11/2010 ND 23.78 NA 839.29 No 17/11/2011 27.41 27.54 0.13 835.62 **No 21/11/2012 28.09 28.18 0.09 834.95 **No 30/05/2013 ND 26.60 NA 836.47 No 27/05/2014 ND 21.83 NA 841.24 No 5/11/2016 ND 22.12 NA 840.95 No 5/23/2017 ND 26.24 NA 836.83 No 5/9/2018 ND 26.73 NA 836.34 No 5/28/2019 ND 18.71 NA 844.36 Yes 5/14/2020 ND 20.52 NA 842.55 No 5/5/2021 ND 17.42 NA 845.65 Yes 5/11/2022 ND 25.04 NA 838.03 No 5/9/2023 ND 22.83 NA 840.24 No RW-18 Page 52 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 859.85 818.9 41.0 5/15/2002 26.85 29.10 2.25 832.37 **Yes 11/13/2002 28.35 31.92 3.57 830.50 **Yes 5/28/2003 19.3 21.40 2.10 839.96 **Yes 11/17/2003 17.53 17.67 0.14 842.28 **Yes 5/12/2004 19.05 19.15 0.10 840.77 **Yes 11/10/2004 19.53 19.74 0.21 840.26 **Yes 5/27/2005 18.21 18.41 0.20 841.58 **Yes 11/15/2005 21.87 21.92 0.05 837.97 **Yes 5/22/2006 20.41 20.42 0.01 839.44 **Yes 11/22/2006 20.76 20.77 0.01 839.09 **Yes 5/7/2007 18.65 18.66 0.01 841.20 **Yes 11/13/2007 23.07 23.18 0.11 836.75 **Yes 5/9/2008 23.75 23.90 0.15 836.06 **Yes 5/27/2014 ND 19.37 NA 840.48 Yes 5/27/2015 ND 21.99 NA 837.86 Yes 5/11/2016 ND 19.62 NA 840.23 Yes 5/23/2017 ND 23.65 NA 836.20 Yes 5/9/2018 ND 24.16 NA 835.69 Yes 5/28/2019 ND 16.30 NA 843.55 Yes 5/14/2020 ND 18.07 NA 841.78 Yes 5/5/2021 ND 15.05 NA 844.80 Yes 5/11/2022 ND 22.39 NA 837.46 Yes 5/9/2023 ND 20.25 NA 839.60 Yes RW-19 Page 53 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 864.63 844.6 40.0 5/15/2002 31.2 31.35 0.15 833.39 **No 11/13/2002 32.85 33.00 0.15 831.74 **No 5/28/2003 ND 23.79 NA 840.84 No 11/17/2003 ND 21.84 NA 842.79 No 5/12/2004 ND 23.20 NA 841.43 No 11/10/2004 ND 23.69 NA 840.94 No 5/27/2005 ND 22.40 NA 842.23 No 11/15/2005 25.06 25.07 0.01 839.57 **No 5/22/2006 24.57 24.70 0.13 840.02 **No 5/7/2007 22.94 22.96 0.02 841.68 **No 11/13/2007 26.98 27.15 0.17 837.60 **No 5/9/2008 27.58 27.59 0.01 837.05 **No 11/21/2012 28.99 29.04 0.05 835.63 **No 5/27/2014 22.73 22.74 0.01 841.90 **No 5/27/2015 ND 19.90 NA 844.73 Yes 5/11/2016 ND 23.40 NA 841.23 No 5/23/2017 ND 26.79 NA 837.84 No 5/9/2018 ND 27.43 NA 837.20 No 5/28/2019 ND 20.22 NA 844.41 No 5/14/2020 ND 21.85 NA 842.78 No 5/5/2021 ND 18.97 NA 845.66 Yes 5/11/2022 ND 25.83 NA 838.80 No 5/9/2023 ND 23.83 NA 840.80 No RW-21 Page 54 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 864.61 845.6 39.0 5/15/2002 31.35 31.80 0.45 833.13 **No 11/13/2002 33.03 33.20 0.17 831.53 **No 5/28/2003 ND 23.90 NA 840.71 No 11/17/2003 21.90 21.94 0.04 842.70 **No 5/12/2004 23.30 23.48 0.18 841.26 **No 11/10/2004 23.78 23.96 0.18 840.78 **No 5/27/2005 22.47 22.51 0.04 842.13 **No 11/15/2005 25.68 25.85 0.17 838.88 **No 5/22/2006 24.72 24.79 0.07 839.87 **No 11/22/2006 25.13 25.14 0.01 839.48 **No 5/7/2007 22.96 22.97 0.01 841.65 **No 11/13/2007 27.25 27.88 0.63 837.18 **No 5/9/2008 ND 27.94 NA 836.67 No 11/21/2012 29.30 29.33 0.03 835.30 **No 5/27/2014 ND 22.73 NA 841.88 No 5/27/2015 ND 25.45 NA 839.16 No 5/11/2016 ND 23.25 NA 841.36 No 5/23/2017 ND 26.98 NA 837.63 No 5/9/2018 ND 27.22 NA 837.39 No 5/28/2019 ND 20.19 NA 844.42 No 5/14/2020 ND 21.86 NA 842.75 No 5/5/2021 ND 18.90 NA 845.71 Yes 5/11/2022 ND 26.04 NA 838.57 No 5/9/2023 ND 23.92 NA 840.69 No RW-22 Page 55 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 861.81 843.8 38.0 5/15/2002 28.82 31.75 2.93 832.17 **No 11/13/2002 31.00 31.50 0.50 830.67 **No 5/28/2003 ND 21.65 NA 840.16 No 11/17/2003 20.21 20.34 0.13 841.56 **No 5/12/2004 21.31 21.41 0.10 840.47 **No 11/10/2004 21.70 21.72 0.02 840.10 **No 5/27/2005 ND 20.36 NA 841.45 No 11/15/2005 23.04 23.21 0.17 838.72 **No 5/22/2006 22.60 22.62 0.02 839.20 **No 5/7/2007 20.91 20.92 0.01 840.90 **No 11/13/2007 25.15 25.36 0.21 836.60 **No 5/9/2008 25.84 25.88 0.04 835.96 **No 5/27/2014 ND 21.30 NA 840.51 No 5/27/2015 ND 24.10 NA 837.71 No 5/11/2016 ND 21.78 NA 840.03 No 5/23/2017 ND 25.80 NA 836.01 No 5/9/2018 ND 26.34 NA 835.47 No 5/28/2019 ND 18.53 NA 843.28 No 5/14/2020 ND 20.25 NA 841.56 No 5/5/2021 ND 17.27 NA 844.54 Yes 5/11/2022 ND 24.58 NA 837.23 No 5/9/2023 ND 22.39 NA 839.42 No RW-27 Page 56 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 863.75 842.8 41.0 15/05/2002 29.65 31.85 2.2 833.48 **No 13/11/2002 31.58 32.15 0.57 832.01 **No 28/05/2003 22.30 22.69 0.39 841.34 **No 17/11/2003 20.20 20.60 0.4 843.44 **Yes 12/05/2004 21.81 22.05 0.24 841.87 **No 10/11/2004 22.31 22.40 0.09 841.41 **No 27/05/2005 21.00 21.04 0.04 842.74 **No 15/11/2005 23.60 23.95 0.35 840.05 **No 22/05/2006 23.20 23.30 0.1 840.52 **No 22/11/2006 23.60 23.61 0.01 840.15 **No 7/05/2007 21.48 21.50 0.02 842.26 **No 13/11/2007 25.78 25.96 0.18 837.92 **No 9/05/2008 26.24 26.25 0.01 837.51 **No 17/11/2009 26.09 26.10 0.01 837.66 **No 16/11/2010 ND 23.58 NA 840.17 No 17/11/2011 27.15 27.41 0.26 836.53 **No 21/11/2012 ND 27.82 NA 835.93 No 27/05/2014 ND 21.76 NA 841.99 No 5/11/2016 ND 22.08 NA 841.67 No 5/23/2017 ND 26.06 NA 837.69 No 5/9/2018 ND 26.48 NA 837.27 No 5/28/2019 ND 18.65 NA 845.10 Yes 5/14/2020 ND 20.35 NA 843.40 Yes 5/5/2021 ND 17.34 NA 846.41 Yes 5/11/2022 ND 24.78 NA 838.97 No 5/9/2023 ND 22.64 NA 841.11 No RW-30 Page 57 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.61 838.6 54.0 5/15/2002 28.80 30.10 1.30 833.45 **No 11/13/2002 30.53 31.80 1.27 831.72 **No 5/28/2003 ND 21.19 NA 841.42 Yes 11/17/2003 19.70 19.72 0.02 842.90 **Yes 5/12/2004 21.10 21.14 0.04 841.50 **Yes 11/10/2004 21.55 21.56 0.01 841.06 **Yes 5/27/2005 ND 20.20 NA 842.41 Yes 11/15/2005 22.94 22.95 0.01 839.67 **Yes 5/22/2006 22.23 22.25 0.02 840.37 **Yes 5/7/2007 ND 22.25 NA 840.36 Yes 11/13/2007 ND 25.03 NA 837.58 No 5/9/2008 25.53 25.54 0.01 837.08 **No 11/21/2012 27.51 27.68 0.17 835.05 **No 5/27/2014 ND 21.01 NA 841.60 Yes 5/27/2015 ND 23.82 NA 838.79 Yes 5/11/2016 ND 21.53 NA 841.08 Yes 5/23/2017 ND 25.50 NA 837.11 No 5/9/2018 ND 26.04 NA 836.57 No 5/28/2019 ND 18.36 NA 844.25 Yes 5/14/2020 ND 20.03 NA 842.58 Yes 5/5/2021 ND 17.15 NA 845.46 Yes 5/11/2022 ND 24.31 NA 838.30 No 5/9/2023 ND 22.05 NA 840.56 Yes RW-37 Page 58 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 863.98 851.0 58.0 15/05/2002 31.00 32.10 1.10 832.67 **No 13/11/2002 32.87 33.24 0.37 831.01 **No 28/05/2003 ND 23.73 NA 840.25 No 17/11/2003 21.83 21.85 0.02 842.14 **No 12/05/2004 22.23 22.90 0.67 841.56 **No 10/11/2004 23.83 23.89 0.06 840.13 **No 27/05/2005 22.46 22.50 0.04 841.51 **No 15/11/2005 25.04 25.65 0.61 838.77 **No 22/05/2006 24.45 24.47 0.02 839.52 **No 22/11/2006 24.70 24.71 0.01 839.28 **No 7/05/2007 22.94 22.95 0.01 841.04 **No 13/11/2007 27.29 27.31 0.02 836.68 **No 9/05/2008 27.9 27.93 0.03 836.07 **No 16/11/2010 ND 24.90 NA 839.08 No 22/11/2011 28.69 28.78 0.09 835.26 **No 21/11/2012 29.23 29.27 0.04 834.74 **No 27/05/2014 ND 28.04 NA 835.94 No 5/11/2016 ND 23.42 NA 840.56 No 5/23/2017 ND 27.61 NA 836.37 No 5/9/2018 ND 28.01 NA 835.97 No 5/28/2019 ND 20.19 NA 843.79 No 5/14/2020 ND 21.96 NA 842.02 No 5/5/2021 ND 19.03 NA 844.95 No 5/11/2022 ND 26.35 NA 837.63 No 5/9/2023 ND 24.21 NA 839.77 No RW-39 Page 59 of 60 Table 2 Summary of Groundwater Elevation Data Freeze Road Site Colonial Pipeline Company Enochville, North Carolina Well Top of Casing Elevation (ft. MSL) Top of Screened Interval (MSL) Well Depth (ft. BGS) Date Measured Depth to LNAPL (ft. BTOC) Depth to Water (ft. BTOC) LNAPL Thickness (ft.) Well Screen Submerged Groundwater Elevation (ft. MSL) 862.71 837.7 45.0 5/15/2002 29.6 30.30 0.70 832.91 **No 11/13/2002 31.35 31.53 0.18 831.31 **No 5/28/2003 ND 22.00 NA 840.71 Yes 11/17/2003 ND 20.46 NA 842.25 Yes 5/12/2004 ND 21.83 NA 840.88 Yes 11/10/2004 22.29 22.30 0.01 840.42 **Yes 5/27/2005 ND 20.94 NA 841.77 Yes 11/15/2005 23.65 23.66 0.01 839.06 **Yes 5/22/2006 22.93 22.94 0.01 839.78 **Yes 11/22/2006 22.68 22.69 0.01 840.03 **Yes 5/7/2007 21.55 21.56 0.01 841.16 **Yes 11/13/2007 25.9 25.97 0.07 836.79 **No 5/9/2008 ND 27.01 NA 835.70 No 5/27/2014 ND 21.76 NA 840.95 Yes 5/27/2015 ND 24.52 NA 838.19 Yes 5/11/2016 ND 22.26 NA 840.45 Yes 5/23/2017 ND 26.23 NA 836.48 No 5/9/2018 ND 26.76 NA 835.95 No 5/28/2019 ND 19.11 NA 843.60 Yes 5/14/2020 ND 20.75 NA 841.96 Yes 5/5/2021 ND 17.92 NA 844.79 Yes 5/11/2022 ND 25.01 NA 837.70 No 5/9/2023 ND 22.81 NA 839.90 Yes Notes: MSL - Mean Sea Level NM - Not Measured BGS - Below Grade Surface ND - None Detected BTOC - Below Top of Casing NA - Not Applicable ft. - Feet LNAPL - Light Non-Aqueous Phase Liquid ("Free Product") Trace - Trace amount of LNAPL observed on probe * - LNAPL was historically detected in the well (thickness not measured) ** Value represents Corrected Groundwater Elevation (Groundwater Elevation = TOC - DTW + (LNAPL Thickness x 0.72)) RW-41 Page 60 of 60 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6 6/11/2001 <1 <1 <1 <3 <5 NA 11/27/2001 <1 <1 <1 <1 <1 NA 5/16/2002 <1 <1 <1 <1 <1 <10 11/14/2002 <1 <1 <1 <1 <1 NA 5/22/2003 <1 <1 <1 <3 <5 <10 11/18/2003 <1 <1 <1 <3 <5 <5 5/13/2004 <1 <1 <1 <3 <5 <5 11/10/2004 <1 <1 <1 <3 <5 <5 6/1/2005 <1 <1 <1 <3 <5 <5 11/15/2005 <1 <1 <1 <3 <5 <5 5/23/2006 <1 <1 <1 <3 <5 <5 5/22/2007 <1 <1 <1 <3 <5 <5 5/28/2008 <1 <1 <1 <3 <5 <5 5/13/2009 <1 <1 <1 <3 <1 <1 5/11/2010 <1 <1 <1 <3 <1 <2 5/25/2011 <0.5 <0.5 <0.5 <1 <0.5 <2 5/2/2012 <1 <1 <1 <2 <1 <2 5/30/2013 1.2 <1 <1 <2 <1 <2 5/28/2014 <1 <1 <1 <2 <1 <2 5/27/2015 <1 <1 <1 <2 <1 <2 5/12/2016 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/23/2017 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/10/2018 <0.50 <0.50 <0.50 <0.50 <0.50 1.3 5/29/2019 5/15/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/4/2021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/11/2022 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/9/2023 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 6/11/2001 6.9 <1 4.6 58 220 NA 11/28/2001 66.0 85.4 95.9 528 30.2 114 5/29/2014 <10 <10 <10 <20 <10 <20 5/27/2015 1.2 <1 36.8 151 <1 157 5/11/2016 0.29 J <0.50 4.7 22 <0.50 25 5/23/2017 5/9/2018 5/29/2019 <0.50 <0.50 2.1 4.2 <0.50 11 5/15/2020 <0.50 <0.50 1.8 3.5 <0.50 7.9 5/4/2021 <0.50 <0.50 0.88 1.9 <0.50 5.1 5/12/2022 <0.50 H <0.50 H 0.77 H 2.4 H <0.50 H 4.4 H 5/9/2023 <0.50 <0.50 0.68 1.8 <0.50 5.7 MW-3 MW-2 NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds LNAPL Could Not Open Lock On Vault LNAPL Page 1 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 6/19/2001 <1 <1 <1 <3 <5 NA 11/28/2001 <1 <1 1.1 14.7 47.6 NA 5/16/2002 2.5 <1 3.2 29.4 43 <10 11/14/2002 15.0 1.2 12.9 120 66.9 NA 5/22/2003 <1 <1 <1 <3 <5 <10 9/10/2003 <1 <1 <1 4.9 11 NA 11/18/2003 <1 <1 <1 37 <5 26 5/12/2004 2.2 <1 <1 36 2.7 J 35 11/10/2004 2.7 <1 <1 84 8.4 120 6/1/2005 1.5 <1 <1 75 <5 56 11/16/2005 1.1 <1 <1 91 6.0 85 5/23/2006 <1 <1 <1 6.8 <5 6.4 11/21/2006 <1 <1 <1 1.7 5.2 5.8 5/22/2007 <1 <1 <1 8.9 <5 44 11/13/2007 <1 <1 <1 <3 <5 8.4 5/28/2008 <1 <1 <1 <3 <5 <5 11/18/2008 <0.5 <1 <1 <3 <5 <1 5/13/2009 <1 <1 <1 <3 <1 1.9 11/16/2009 <1 <1 <1 <2 <1 <1 5/12/2010 <1 <1 <1 <3 <1 <2 11/18/2010 <1 <1 <1 <3 <1 <2 5/25/2011 <0.5 <0.5 <0.5 <1 <0.5 <2 11/18/2011 <1 <1 <1 <3 <1 <2 5/2/2012 <1 <1 <1 <2 <1 <2 11/20/2012 <1 <1 <1 <2 <1 <1 5/31/2013 <1 <1 <1 <2 <1 <2 5/28/2014 <1 <1 <1 <2 <1 6 5/27/2015 <1 <1 <1 <2 <1 <2 5/12/2016 <0.50 <0.50 <0.50 <0.50 <0.50 1.4 B 5/24/2017 <0.50 <0.50 <0.50 <0.50 <0.50 0.56 5/9/2018 <0.50 <0.50 <0.50 <0.50 <0.50 0.54 5/29/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/15/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/4/2021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/12/2022 <0.50 H <0.50 H <0.50 H <0.50 H <0.50 H <0.50 H 5/9/2023 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 MW-4D Page 2 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 6/11/2001 <1 <1 <1 <3 <5 NA 11/28/2001 <1 <1 <1 <1 <1 NA 5/15/2002 <1 <1 <1 <1 <1 <10 11/14/2002 <1 <1 <1 2.5 <1 NA 5/22/2003 <1 <1 <1 <3 <5 <10 11/18/2003 10.0 2.8 56 200 74 97 12/8/2003 2.7 1.1 20 200 93 53 5/12/2004 20.0 0.86 J 39 210 210 110 11/10/2004 79.0 3.8 100 320 440 340 2/9/2005 72.0 4.1 71 197 230 140 6/1/2005 76.0 2.5 81 380 1400 260 11/15/2005 86.0 <1 77 430 1800 250 5/23/2006 77.0 <4 71 500 1600 230 11/21/2006 6.0 <1 1.4 35.1 140 11 5/22/2007 69.0 <1 24 386 740 230 11/13/2007 41.0 <4 5.5 550 360 280 5/29/2008 33.0 <4 6.2 411 260 260 11/20/2008 69.0 <4 14 490 520 300 5/15/2009 121.0 1.7 13.2 342 752 251 5/12/2010 134.0 <2.5 8.5 338 346 229 11/18/2010 102.0 <5 5.3 326 234 309 5/25/2011 104.0 5.0 6.5 359 133 218 11/17/2011 1.4 1.9 <1 7.9 1.9 7.8 5/3/2012 88.3 <2 7.3 290 71.3 201 11/19/2012 122.0 2.7 9.2 344 65.3 277 5/30/2013 52.4 <2 2.2 94.3 25.4 77.5 5/28/2014 144.0 2.9 3.1 114 19 163 5/27/2015 68.3 <1 1.6 60.4 6.2 113 5/11/2016 98 2.2 J 4.2 140 6.0 230 B 5/23/2017 49 0.78 0.55 13 <0.50 44 5/9/2018 20 <0.50 <0.50 11 <0.50 23 5/29/2019 75 0.73 0.52 13 <0.50 66 5/15/2020 130 1.1 1.3 21 <0.50 190 5/4/2021 69 <0.50 <0.50 5.5 <0.50 85 5/12/2022 64 H <2.5 H <2.5 H 5.3 H <2.5 H 130 H 5/9/2023 5.6 <0.50 <0.50 <1.5 <0.50 8.8 MW-8 Page 3 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 6/11/2001 <1 <1 <1 <3 <5 NA 11/27/2001 <1 <1 <1 <1 <1 NA 5/29/2014 <1 <1 <1 <2 <1 <2 5/28/2015 <1 <1 <1 <2 <1 <2 5/12/2016 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/24/2017 <0.50 <0.50 <0.50 <0.50 <0.50 0.42 J 5/10/2018 <0.50 <0.50 <0.50 <0.50 <0.50 0.54 5/29/2019 <0.50 <0.50 <0.50 <0.50 <0.50 1.1 5/15/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/5/2021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/11/2022 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/10/2023 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 6/11/2001 <1 <1 <1 <3 <5 NA 8/27/2001 NA NA NA NA NA <5 11/27/2001 <1 <1 <1 <1 <1 NA 5/29/2014 <1 <1 <1 <2 <1 <2 5/28/2015 <1 <1 <1 <2 <1 <2 5/12/2016 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/24/2017 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/10/2018 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/29/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/15/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/5/2021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/11/2022 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/10/2023 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 MW-10 MW-9 Page 4 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 6/15/2001 <1 <1 <1 <3 <5 NA 11/26/2001 <1 <1 <1 <1 <1 NA 5/29/2008 <1 <1 <1 30.5 <5 28 5/28/2014 <1 <1 <1 <2 <1 <2 5/27/2015 <1 <1 <1 <2 <1 <2 5/11/2016 <0.50 7.4 <0.50 <0.50 <0.50 0.41 J B 5/24/2017 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/10/2018 <0.50 <0.50 <0.50 <0.50 0.53 0.41 J 5/29/2019 0.40 J <0.50 <0.50 <0.50 1.0 1.3 5/15/2020 <0.50 0.60 <0.50 <0.50 <0.50 1.0 5/5/2021 1.3 <0.50 <0.50 <0.50 1.7 4.0 5/11/2022 <0.50 <0.50 <0.50 <0.50 0.55 1.9 5/9/2023 <0.50 <0.50 0.33 J <1.5 <0.50 1.6 J 6/14/2001 <1 <1 <1 <3 <5 NA 11/27/2001 <1 <1 <1 <1 <1 NA 11/16/2005 <1 <1 <1 <3 <5 <5 5/29/2014 <1 <1 <1 <2 <1 <2 5/28/2015 <1 <1 <1 <2 <1 <2 5/12/2016 <0.50 <0.50 <0.50 <0.50 0.24 J 0.50 B 5/24/2017 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/10/2018 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/29/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/15/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/5/2021 <0.50 <0.50 <0.50 <0.50 <0.50 0.57 5/11/2022 0.71 <0.50 <0.50 <0.50 <0.50 3.6 5/10/2023 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 MW-21 MW-16D Page 5 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 6/14/2001 <1 <1 <1 <3 <5 NA 11/26/2001 <1 <1 <1 <1 <1 NA 5/16/2002 <1 <1 <1 <1 <1 <10 11/14/2002 <1 <1 <1 <1 <1 NA 5/21/2003 <1 <1 <1 <3 <5 <10 11/18/2003 <1 <1 <1 <3 <5 <5 5/13/2004 <1 <1 <1 <3 <5 <5 11/10/2004 <1 <1 <1 <3 <5 <5 6/2/2005 <1 <1 <1 <3 <5 <5 11/16/2005 <1 <1 <1 <3 <5 <5 5/23/2006 <1 <1 <1 <3 <5 <5 11/21/2006 <1 <1 <1 <3 <5 <5 5/22/2007 15.0 <1 1.6 47.7 5.9 76 11/13/2007 21.0 <1 <1 62 11 110 5/29/2008 9.8 <1 <1 21.3 20 38 11/19/2008 21.0 <1 <1 117 16 100 5/15/2009 16.2 <2 <2 69.8 14.3 90.6 11/16/2009 4.0 <1 <1 27.6 5.4 16.4 5/12/2010 14.5 <1 <1 49.1 11.4 60.3 11/17/2010 17.4 <1 <1 10.9 18.5 51.7 5/25/2011 21.5 <0.5 <0.5 72.9 14.2 71.8 11/18/2011 14.8 <1 <1 39.6 12.3 53 5/3/2012 21.1 <1 <1 55.4 11.3 67 11/19/2012 18.2 <1 <1 20.8 11.5 54.2 5/30/2013 13.9 <1 <1 24.5 6.5 48.6 5/29/2014 9.9 <1 <1 32.5 1.5 31.3 5/28/2015 5.6 <1 <1 15.4 1.2 18.4 5/11/2016 10 <0.50 <0.50 26 0.62 33 5/24/2017 2.6 <0.50 <0.50 6.0 <0.50 8.3 5/10/2018 0.69 <0.50 <0.50 0.60 <0.50 1.9 5/29/2019 3.1 <0.50 <0.50 5.5 <0.50 12 5/15/2020 3.8 <0.50 <0.50 8.7 <0.50 19 5/5/2021 2.7 <0.50 <0.50 5.7 <0.50 15 5/11/2022 1.3 H <0.50 H <0.50 H 2.3 H <0.50 H 7.2 H 5/10/2023 1.8 <0.50 <0.50 2.4 <0.50 14.8 MW-22 Page 6 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 6/19/2001 <1 <1 <1 <3 <5 NA 11/26/2001 <1 <1 <1 <1 <1 NA 5/16/2002 <1 <1 <1 <1 <1 <10 5/21/2003 <1 <1 <1 <3 9.1 <10 9/10/2003 8.9 1.2 4.3 76 4.0 J NA 11/18/2003 14.0 1.8 29 170 <5 86 5/13/2004 9.8 <1 7.5 120 <5 64 11/11/2004 5.5 <1 5.0 119 <5 75 6/1/2005 17.0 <1 11.0 260 20 170 11/16/2005 2.5 <1 4.0 134 <5 97 5/23/2006 12.0 <1 4.7 155 13 79 11/21/2006 <1 <1 2.7 110 <5 55 5/22/2007 9.5 <1 6.5 327 6.4 J 210 11/13/2007 <1 <1 4.3 419 <5 390 5/29/2008 4.5 <1 3.7 295 <5 240 11/19/2008 12.0 <1 5.1 440 <5 330 5/13/2009 10.5 <5 <5 244.8 <5 233 6/28/2010 <1 1.4 <1 34 <1 25.4 11/18/2010 <1 <1 <1 32.3 <1 37.1 5/26/2011 2.0 <1 <1 139 <1 112 11/18/2011 2.0 <1 <1 201 <1 166 5/2/2012 3.7 <1 <1 153 <1 146 11/20/2012 2.8 <1 <1 181 <1 181 5/30/2013 2.7 <1 <1 117 <1 119 5/29/2014 2.0 <1 <1 170 <1 167 5/28/2015 3.3 <1 <1 92.6 <1 215 5/12/2016 1.6 J <2.5 <2.5 130 <2.5 180 5/23/2017 <2.5 <2.5 <2.5 89 <2.5 150 5/10/2018 2.3 <0.50 <0.50 1.5 <0.50 87 5/29/2019 <0.50 <0.50 <0.50 7.0 <0.50 27 5/15/2020 0.71 <0.50 <0.50 67 <0.50 150 5/4/2021 0.66 <0.50 <0.50 47 <0.50 140 5/12/2022 <0.50 H <0.50 H <0.50 H 36 H <0.50 H 110 H 5/10/2023 <0.50 <0.50 <0.50 20 <0.50 90.6 MW-28 Page 7 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 6/19/2001 <1 <1 <1 <3 <5 NA 8/24/2001 NA NA NA NA NA <5 11/28/2001 <1 <1 <1 <1 7.5 NA 5/16/2002 <1 <1 <1 <1 <1 <10 11/14/2002 <1 <1 <1 <1 39.2 NA 5/23/2003 <1 <1 <1 <3 <5 <10 9/10/2003 <1 <1 <1 <3 2.4 J NA 11/18/2003 <1 <1 <1 <3 <5 <5 5/13/2004 <1 1.5 <1 <3 <5 <5 11/11/2004 17.0 <1 5.3 28 210 29 6/1/2005 54.0 <1 3.0 116 300 80 11/16/2005 97.0 <1 3.0 257 270 220 5/23/2006 43.0 <1 <1 121 76 97 11/21/2006 43.0 <1 1.8 173 58 180 5/22/2007 18.0 <1 <1 59 16 57 11/13/2007 18.0 <1 <1 105 13 100 5/29/2008 <1 <1 <1 2.3 8.8 <5 11/20/2008 23.0 <1 1.4 167 6.6 150 5/14/2009 13.7 <2 <2 60.1 3.3 95.2 6/28/2010 <1 2.3 <1 11.2 <1 46.2 11/18/2010 4.4 <1 <1 2.9 <1 93.4 5/26/2011 3.0 <0.5 <0.5 3.9 <0.5 51 11/18/2011 2.7 <1 <1 11.6 <1 34.9 5/4/2012 3.3 <1 <1 14.4 <1 86.7 11/20/2012 4.4 <1 <1 21.1 <1 125 5/31/2013 4.2 <1 <1 22.3 <1 130 5/29/2014 6.2 <1 <1 16.5 <1 146 5/28/2015 3.4 <1 <1 7.5 <1 122 5/12/2016 6.4 <2.5 <2.5 3.3 <2.5 180 5/23/2017 3.2 <0.50 <0.50 3.5 <0.50 150 5/10/2018 1.0 <0.50 <0.50 90 <0.50 180 5/29/2019 2.0 <0.50 <0.50 0.54 <0.50 83 5/15/2020 2.6 <0.50 <0.50 0.68 <0.50 92 5/5/2021 1.7 <0.50 <0.50 1.0 <0.50 64 5/12/2022 1.1 H <0.50 H <0.50 H <0.50 H <0.50 H 100 H 5/10/2023 0.90 <0.50 <0.50 <1.5 <0.50 69.8 MW-29D Page 8 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 6/19/2001 <1 <1 <1 <3 <5 NA 11/26/2001 <1 <1 <1 <1 <1 NA 5/15/2002 <1 <1 <1 <1 <1 <14.3 11/14/2002 <1 <1 <1 <1 <1 NA 5/21/2003 <1 <1 <1 <3 <5 <10 11/18/2003 <1 <1 <1 <3 <5 <5 5/12/2004 <1 <1 <1 <3 <5 <5 11/11/2004 <1 <1 <1 <3 <5 6.1 6/2/2005 <1 <1 <1 <3 <5 <5 11/16/2005 <1 <1 <1 <3 <5 <5 5/23/2006 <1 <1 <1 <3 <5 <5 5/22/2007 <1 <1 <1 <3 <5 2.7 J 5/29/2008 <1 <1 <1 <3 <5 <5 5/15/2009 <1 <1 <1 <3 <1 <1 5/12/2010 <1 <1 <1 <3 <1 <2 5/26/2011 <0.5 <0.5 <0.5 <1 <0.5 <2 5/3/2012 <1 <1 <1 <2 <1 <2 5/30/2013 <1 <1 <1 <2 <1 <2 5/29/2014 <1 <1 <1 <2 <1 <2 5/27/2015 <1 <1 <1 <2 <1 <2 5/12/2016 <0.50 <0.50 <0.50 <0.50 <0.50 0.69 5/24/2017 <0.50 <0.50 <0.50 <0.50 <0.50 0.51 5/10/2018 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/29/2019 <0.50 <0.50 <0.50 <0.50 <0.50 0.54 5/15/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/5/2021 <0.50 <0.50 <0.50 <0.50 <0.50 0.77 5/12/2022 <0.50 H <0.50 H <0.50 H <0.50 H <0.50 H <0.50 H 5/10/2023 Not Sampled - Could Not Access Well MW-30 Page 9 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 8/24/2001 <1 <1 <1 <2 <5 <5 11/28/2001 <1 <1 <1 <1 <1 NA 1/25/2006 4.0 <1 2.9 20.1 9.0 6.9 5/23/2006 3.5 <1 3.2 16.8 12 8.1 5/22/2007 7.5 <1 8.8 37 1.8 J 15 5/28/2008 20.0 1.3 19 118 14 66 5/14/2009 40.4 <1 40.1 219.6 11.3 120 5/12/2010 16.7 <1 17.8 129.9 1.1 58.9 5/26/2011 6.8 <0.5 1.8 65.6 <0.5 13.7 5/4/2012 19.5 <1 3.4 196 <1 73.5 5/30/2013 15.4 <1 7.5 213 <1 96.5 5/29/2014 18.9 <1 4.2 235 <1 140 5/28/2015 8.9 <1 3.5 144.5 <1 95.7 5/12/2016 3.8 <0.50 0.88 62 <0.50 40 5/24/2017 1.6 <0.50 <0.50 24 <0.50 20 5/10/2018 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 5/29/2019 <0.50 <0.50 <0.50 9.1 <0.50 3.5 5/15/2020 2.6 <0.50 <0.50 29 <0.50 60 5/5/2021 2.3 <0.50 <0.50 33 <0.50 86 5/11/2022 1.5 <0.50 <0.50 22 <0.50 86 5/10/2023 1.2 <0.50 <0.50 30 <0.50 116 MW-34 Page 10 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds 6/27/2001 <1 <1 <1 <2 18 <5 11/29/2001 <1 <1 <1 <1 20.5 NA 5/15/2002 2.2 <1 <1 33.1 21.2 <10 11/14/2002 12.6 1.2 6 147 23 NA 3/10/2003 17.0 4.5 19 230 <5 NA 5/23/2003 3.3 1.3 8.3 73 <5 <10 11/18/2003 <1 <1 <1 <3 <5 <5 12/8/2003 <1 <1 <1 <3 <5 <5 5/12/2004 0.54 J <1 <1 41 <5 25 11/10/2004 1.5 <1 <1 94 <5 100 6/1/2005 1.2 <1 <1 140 <5 160 11/15/2005 <1 <1 <1 107 <5 98 5/23/2006 <1 <1 <1 29.8 <5 33 11/22/2006 <1 <1 <1 42 <5 60 5/22/2007 <1 <1 <1 15.8 <5 65 11/13/2007 <1 <1 <1 48.4 <5 99 5/29/2008 <1 <1 <1 11.9 J <5 94 11/18/2008 <0.5 <1 <1 9.9 <5 140 5/15/2009 <1 <1 <1 1.7 <1 90.6 6/29/2010 <1 <1 <1 <3 <1 41 11/17/2010 <1 <1 <1 <3 <1 5.1 5/26/2011 <0.5 <0.5 <0.5 <1 <0.5 16.8 11/17/2011 <1 <1 <1 <2 <1 50.1 5/3/2012 <1 <1 <1 <2 <1 34.9 11/19/2012 <1 <1 <1 <2 <1 64.9 5/31/2013 <1 <1 <1 <2 <1 33.6 5/28/2014 <1 <1 <1 <2 <1 39.9 5/27/2015 <1 <1 <1 <2 <1 <2 5/11/2016 <0.50 <0.50 <0.50 <0.50 <0.50 25 5/24/2017 <0.50 <0.50 <0.50 <0.50 <0.50 15 5/10/2018 <0.50 <0.50 <0.50 <0.50 <0.50 5.3 5/29/2019 <0.50 <0.50 <0.50 <0.50 <0.50 3.3 5/15/2020 <0.50 <0.50 <0.50 <0.50 <0.50 12 5/5/2021 <0.50 <0.50 <0.50 <0.50 <0.50 3.7 5/11/2022 <0.50 <0.50 <0.50 <0.50 <0.50 1.1 5/9/2023 <0.50 <0.50 <0.50 <1.5 <0.50 5.8 MW-35 Page 11 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds Blind Duplicate 1 MW-29D 5/23/2017 3.3 <0.50 <0.50 3.3 <0.50 160 Blind Duplicate 2 MW-22 5/24/2017 2.8 <0.50 <0.50 5.7 <0.50 7.7 Blind Duplicate 1 DUP050918 MW-4D 5/9/2018 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Blind Duplicate 2 DUP051018 MW-28 5/10/2018 1.0 <0.50 <0.50 90 <0.50 190 DUP-1 5/29/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 DUP-1 MW-3 5/15/2020 <0.50 <0.50 1.9 3.2 <0.50 8.9 DUP-1 MW-28 5/4/2021 0.63 <0.50 <0.50 50 <0.50 140 DUP-2 MW-10 5/5/2021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 DUP-1 (MW-16D)5/11/2022 <0.50 H <0.50 H <0.50 H <0.50 H 0.65 H 2.2 H DUP-2 (MW-03)5/12/2022 69 H <0.50 H <0.50 H 6.2 H <0.50 H 170 H DUP-1 (MW-16D)5/9/2023 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 DUP-2 (MW-34)5/10/2023 1.4 <0.50 <0.50 31.3 <0.50 114 Equipment Blank 1 5/23/2017 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Equipment Blank 2 5/24/2017 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Equipment Blank 1 EB050918 5/9/2018 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Equipment Blank 2 EB051018 5/10/2018 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 EB05292019 5/29/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 EB-1 5/15/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Equipment Blank 5/4/2021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Equip Blank-2 5/5/2021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 EB-1 5/11/2022 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 EB-2 5/12/2022 <0.50 H <0.50 H <0.50 H <0.50 H <0.50 H 1.8 H EB-1 5/9/2023 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 EB-2 5/10/2023 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 QA/QC Samples Page 12 of 13 Table 3 Summary of Groundwater Analytical Results Freeze Road Site Colonial Pipeline Company Enochville, North Carolina B e n z e n e T o l u e n e E t h y l b e n z e n e T o t a l X y l e n e s M T B E N a p h t h a l e n e 1 600 600 500 20 6NCAC 2L Groundwater Standard Sample ID Sampling Date Volatile Organic Compounds Trip Blank 5/24/2017 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Trip Blank 5/10/2018 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Trip Blank 5/29/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Trip Blank 5/15/2020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Trip Blank 5/4/2021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Trip Blank 5/11/2022 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 Trip Blank 5/10/2023 <0.50 <0.50 <0.50 <1.5 <0.50 <2.0 Notes: Units reported in micrograms per liter (µg/L) NCAC - North Carolina Administrative Code QA/QC - Quality Assurance Quality Control MTBE - Methyl tertiary butyl ether LNAPL - Liqht Non-Aqueous Phase Liquid detected in well NA - Not Analyzed / Not Applicable J - Estimated concentration below laboratory reporting limit B - Analyte detected in laboratory method blank E - Quantitation of compound exceeded the calibration range H - Out of holding time < - Value not detected above practical quantitation limit Bold text indicates the value meets or exceeds the 2L Standards Groundwater samples analyzed for BTEX, MTBE, and Naphthalene via EPA Method 602 by SM 6200B. Page 13 of 13 FIGURES Sources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS, FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, Esri Japan, METI, Esri China (Hong Kong), (c) OpenStreetMap contributors, and the GIS User Community CHECK BY: AS DRAWN BY: CW DATE: 5/25/23 SCALE: 1 in = 2,000 ft CAD NO.: COL054-0314051 PRJ NO.: COL054-0314051 1 FIGURE SITE LOCATION MAP FREEZE ROAD SITE COLONIAL PIPELINE COMPANY ENOCHVILLE, NORTH CAROLINA ¯ 0 1,000 2,000 Feet SITE LOCATION APPENDIX A GROUNDWATER SAMPLING FIELD LOGS APPENDIX B LABORATORY ANALYTICAL REPORT #=CL# May 22, 2023 LIMS USE: FR - ANDREW STREET LIMS OBJECT ID: 92667049 92667049 Project: Pace Project No.: RE: Andrew Street Apex Companies 5900-O Northwoods Business Parkway Charlotte, NC 28269 COL054-0314051-23004620 Dear Andrew Street: Enclosed are the analytical results for sample(s) received by the laboratory on May 10, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Charlotte A revised report is being submitted on 5/22/23 due to a compound list error. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com Project Manager (704)875-9092 Enclosures cc:Kaitlyn Nootens, Apex Companies REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 26 #=CP# CERTIFICATIONS Pace Project No.: Project: 92667049 COL054-0314051-23004620 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 26 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92667049 COL054-0314051-23004620 Lab ID Sample ID Matrix Date Collected Date Received 92667049001 MW-2 Water 05/09/23 12:05 05/10/23 16:32 92667049002 MW-3 Water 05/09/23 14:00 05/10/23 16:32 92667049003 MW-4D Water 05/09/23 14:45 05/10/23 16:32 92667049004 MW-8 Water 05/09/23 15:35 05/10/23 16:32 92667049005 MW-9 Water 05/10/23 09:25 05/10/23 16:32 92667049006 MW-10 Water 05/10/23 08:40 05/10/23 16:32 92667049007 MW-16D Water 05/09/23 10:10 05/10/23 16:32 92667049008 MW-21 Water 05/10/23 12:10 05/10/23 16:32 92667049009 MW-22 Water 05/10/23 11:30 05/10/23 16:32 92667049010 MW-28 Water 05/10/23 11:25 05/10/23 16:32 92667049011 MW-29D Water 05/10/23 10:00 05/10/23 16:32 92667049012 MW-34 Water 05/10/23 10:45 05/10/23 16:32 92667049013 MW-35 Water 05/10/23 11:00 05/10/23 16:32 92667049014 EB-1 Water 05/09/23 17:30 05/10/23 16:32 92667049015 EB-2 Water 05/10/23 12:40 05/10/23 16:32 92667049016 DUP-1 Water 05/09/23 00:00 05/10/23 16:32 92667049017 DUP-2 Water 05/10/23 00:00 05/10/23 16:32 92667049018 TRIP BLANK Water 05/10/23 00:00 05/10/23 16:32 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 26 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92667049 COL054-0314051-23004620 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92667049001 MW-2 SM 6200B 10 PASI-CSAS 92667049002 MW-3 SM 6200B 10 PASI-CSAS 92667049003 MW-4D SM 6200B 10 PASI-CSAS 92667049004 MW-8 SM 6200B 10 PASI-CSAS 92667049005 MW-9 SM 6200B 10 PASI-CSAS 92667049006 MW-10 SM 6200B 10 PASI-CSAS 92667049007 MW-16D SM 6200B 10 PASI-CSAS 92667049008 MW-21 SM 6200B 10 PASI-CSAS 92667049009 MW-22 SM 6200B 10 PASI-CSAS 92667049010 MW-28 SM 6200B 10 PASI-CSAS 92667049011 MW-29D SM 6200B 10 PASI-CSAS 92667049012 MW-34 SM 6200B 10 PASI-CSAS 92667049013 MW-35 SM 6200B 10 PASI-CSAS 92667049014 EB-1 SM 6200B 10 PASI-CSAS 92667049015 EB-2 SM 6200B 10 PASI-CSAS 92667049016 DUP-1 SM 6200B 10 PASI-CSAS 92667049017 DUP-2 SM 6200B 10 PASI-CSAS 92667049018 TRIP BLANK SM 6200B 10 PASI-CSAS PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 26 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92667049 COL054-0314051-23004620 Sample:MW-2 Lab ID:92667049001 Collected:05/09/23 12:05 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/17/23 16:46 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 16:46 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 16:46 1634-04-40.50 0.42 1 Naphthalene <2.0 ug/L 05/17/23 16:46 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 16:46 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 16:46 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/17/23 16:46 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)112 %05/17/23 16:46 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %05/17/23 16:46 460-00-470-130 1 Toluene-d8 (S)103 %05/17/23 16:46 2037-26-570-130 1 Sample:MW-3 Lab ID:92667049002 Collected:05/09/23 14:00 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/18/23 15:13 71-43-20.50 0.34 1 Ethylbenzene 0.68 ug/L 05/18/23 15:13 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/18/23 15:13 1634-04-40.50 0.42 1 Naphthalene 5.7 ug/L 05/18/23 15:13 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/18/23 15:13 108-88-30.50 0.24 1 m&p-Xylene 1.8 ug/L 05/18/23 15:13 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/18/23 15:13 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)88 %05/18/23 15:13 17060-07-070-130 1 4-Bromofluorobenzene (S)104 %05/18/23 15:13 460-00-470-130 1 Toluene-d8 (S)107 %05/18/23 15:13 2037-26-570-130 1 Sample:MW-4D Lab ID:92667049003 Collected:05/09/23 14:45 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/17/23 17:04 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 17:04 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 17:04 1634-04-40.50 0.42 1 Naphthalene <2.0 ug/L 05/17/23 17:04 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 17:04 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 17:04 179601-23-11.0 0.71 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 26 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92667049 COL054-0314051-23004620 Sample:MW-4D Lab ID:92667049003 Collected:05/09/23 14:45 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV o-Xylene <0.50 ug/L 05/17/23 17:04 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)113 %05/17/23 17:04 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %05/17/23 17:04 460-00-470-130 1 Toluene-d8 (S)103 %05/17/23 17:04 2037-26-570-130 1 Sample:MW-8 Lab ID:92667049004 Collected:05/09/23 15:35 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 5.6 ug/L 05/17/23 17:22 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 17:22 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 17:22 1634-04-40.50 0.42 1 Naphthalene 8.8 ug/L 05/17/23 17:22 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 17:22 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 17:22 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/17/23 17:22 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)114 %05/17/23 17:22 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %05/17/23 17:22 460-00-470-130 1 Toluene-d8 (S)102 %05/17/23 17:22 2037-26-570-130 1 Sample:MW-9 Lab ID:92667049005 Collected:05/10/23 09:25 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/17/23 22:41 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 22:41 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 22:41 1634-04-40.50 0.42 1 Naphthalene <2.0 ug/L 05/17/23 22:41 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 22:41 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 22:41 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/17/23 22:41 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)114 %05/17/23 22:41 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %05/17/23 22:41 460-00-470-130 1 Toluene-d8 (S)102 %05/17/23 22:41 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 26 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92667049 COL054-0314051-23004620 Sample:MW-10 Lab ID:92667049006 Collected:05/10/23 08:40 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/17/23 22:59 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 22:59 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 22:59 1634-04-40.50 0.42 1 Naphthalene <2.0 ug/L 05/17/23 22:59 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 22:59 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 22:59 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/17/23 22:59 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)114 %05/17/23 22:59 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %05/17/23 22:59 460-00-470-130 1 Toluene-d8 (S)102 %05/17/23 22:59 2037-26-570-130 1 Sample:MW-16D Lab ID:92667049007 Collected:05/09/23 10:10 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/18/23 15:26 71-43-20.50 0.34 1 Ethylbenzene 0.33J ug/L 05/18/23 15:26 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/18/23 15:26 1634-04-40.50 0.42 1 Naphthalene 1.6J ug/L 05/18/23 15:26 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/18/23 15:26 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/18/23 15:26 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/18/23 15:26 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)111 %05/18/23 15:26 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %05/18/23 15:26 460-00-470-130 1 Toluene-d8 (S)102 %05/18/23 15:26 2037-26-570-130 1 Sample:MW-21 Lab ID:92667049008 Collected:05/10/23 12:10 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/17/23 23:17 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 23:17 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 23:17 1634-04-40.50 0.42 1 Naphthalene <2.0 ug/L 05/17/23 23:17 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 23:17 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 23:17 179601-23-11.0 0.71 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 26 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92667049 COL054-0314051-23004620 Sample:MW-21 Lab ID:92667049008 Collected:05/10/23 12:10 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV o-Xylene <0.50 ug/L 05/17/23 23:17 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)112 %05/17/23 23:17 17060-07-070-130 1 4-Bromofluorobenzene (S)95 %05/17/23 23:17 460-00-470-130 1 Toluene-d8 (S)103 %05/17/23 23:17 2037-26-570-130 1 Sample:MW-22 Lab ID:92667049009 Collected:05/10/23 11:30 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 1.8 ug/L 05/17/23 23:35 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 23:35 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 23:35 1634-04-40.50 0.42 1 Naphthalene 14.8 ug/L 05/17/23 23:35 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 23:35 108-88-30.50 0.24 1 m&p-Xylene 1.1 ug/L 05/17/23 23:35 179601-23-11.0 0.71 1 o-Xylene 1.3 ug/L 05/17/23 23:35 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)115 %05/17/23 23:35 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %05/17/23 23:35 460-00-470-130 1 Toluene-d8 (S)103 %05/17/23 23:35 2037-26-570-130 1 Sample:MW-28 Lab ID:92667049010 Collected:05/10/23 11:25 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/18/23 15:31 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/18/23 15:31 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/18/23 15:31 1634-04-40.50 0.42 1 Naphthalene 90.6 ug/L 05/18/23 15:31 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/18/23 15:31 108-88-30.50 0.24 1 m&p-Xylene 4.4 ug/L 05/18/23 15:31 179601-23-11.0 0.71 1 o-Xylene 15.6 ug/L 05/18/23 15:31 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)84 %05/18/23 15:31 17060-07-070-130 1 4-Bromofluorobenzene (S)104 %05/18/23 15:31 460-00-470-130 1 Toluene-d8 (S)102 %05/18/23 15:31 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 26 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92667049 COL054-0314051-23004620 Sample:MW-29D Lab ID:92667049011 Collected:05/10/23 10:00 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 0.90 ug/L 05/17/23 23:52 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 23:52 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 23:52 1634-04-40.50 0.42 1 Naphthalene 69.8 ug/L 05/17/23 23:52 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 23:52 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 23:52 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/17/23 23:52 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)115 %05/17/23 23:52 17060-07-070-130 1 4-Bromofluorobenzene (S)99 %05/17/23 23:52 460-00-470-130 1 Toluene-d8 (S)104 %05/17/23 23:52 2037-26-570-130 1 Sample:MW-34 Lab ID:92667049012 Collected:05/10/23 10:45 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 1.2 ug/L 05/18/23 15:49 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/18/23 15:49 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/18/23 15:49 1634-04-40.50 0.42 1 Naphthalene 116 ug/L 05/18/23 15:49 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/18/23 15:49 108-88-30.50 0.24 1 m&p-Xylene 8.4 ug/L 05/18/23 15:49 179601-23-11.0 0.71 1 o-Xylene 21.1 ug/L 05/18/23 15:49 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)85 %05/18/23 15:49 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %05/18/23 15:49 460-00-470-130 1 Toluene-d8 (S)110 %05/18/23 15:49 2037-26-570-130 1 Sample:MW-35 Lab ID:92667049013 Collected:05/10/23 11:00 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/18/23 00:10 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/18/23 00:10 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/18/23 00:10 1634-04-40.50 0.42 1 Naphthalene 5.8 ug/L 05/18/23 00:10 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/18/23 00:10 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/18/23 00:10 179601-23-11.0 0.71 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 26 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92667049 COL054-0314051-23004620 Sample:MW-35 Lab ID:92667049013 Collected:05/10/23 11:00 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV o-Xylene <0.50 ug/L 05/18/23 00:10 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)114 %05/18/23 00:10 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %05/18/23 00:10 460-00-470-130 1 Toluene-d8 (S)102 %05/18/23 00:10 2037-26-570-130 1 Sample:EB-1 Lab ID:92667049014 Collected:05/09/23 17:30 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/17/23 21:48 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 21:48 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 21:48 1634-04-40.50 0.42 1 Naphthalene <2.0 ug/L 05/17/23 21:48 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 21:48 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 21:48 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/17/23 21:48 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)112 %05/17/23 21:48 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %05/17/23 21:48 460-00-470-130 1 Toluene-d8 (S)102 %05/17/23 21:48 2037-26-570-130 1 Sample:EB-2 Lab ID:92667049015 Collected:05/10/23 12:40 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/17/23 22:05 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 22:05 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 22:05 1634-04-40.50 0.42 1 Naphthalene <2.0 ug/L 05/17/23 22:05 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 22:05 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 22:05 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/17/23 22:05 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)112 %05/17/23 22:05 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %05/17/23 22:05 460-00-470-130 1 Toluene-d8 (S)102 %05/17/23 22:05 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 26 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92667049 COL054-0314051-23004620 Sample:DUP-1 Lab ID:92667049016 Collected:05/09/23 00:00 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/18/23 13:43 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/18/23 13:43 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/18/23 13:43 1634-04-4 R10.50 0.42 1 Naphthalene <2.0 ug/L 05/18/23 13:43 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/18/23 13:43 108-88-3 R10.50 0.24 1 m&p-Xylene <1.0 ug/L 05/18/23 13:43 179601-23-11.0 0.71 1 o-Xylene <0.50 ug/L 05/18/23 13:43 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)89 %05/18/23 13:43 17060-07-070-130 1 4-Bromofluorobenzene (S)103 %05/18/23 13:43 460-00-470-130 1 Toluene-d8 (S)105 %05/18/23 13:43 2037-26-570-130 1 Sample:DUP-2 Lab ID:92667049017 Collected:05/10/23 00:00 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene 1.4 ug/L 05/18/23 14:14 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/18/23 14:14 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/18/23 14:14 1634-04-40.50 0.42 1 Naphthalene 114 ug/L 05/18/23 14:14 91-20-3 M12.0 0.64 1 Toluene <0.50 ug/L 05/18/23 14:14 108-88-30.50 0.24 1 m&p-Xylene 9.0 ug/L 05/18/23 14:14 179601-23-11.0 0.71 1 o-Xylene 22.3 ug/L 05/18/23 14:14 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)115 %05/18/23 14:14 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %05/18/23 14:14 460-00-470-130 1 Toluene-d8 (S)103 %05/18/23 14:14 2037-26-570-130 1 Sample:TRIP BLANK Lab ID:92667049018 Collected:05/10/23 00:00 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene <0.50 ug/L 05/17/23 22:23 71-43-20.50 0.34 1 Ethylbenzene <0.50 ug/L 05/17/23 22:23 100-41-40.50 0.30 1 Methyl-tert-butyl ether <0.50 ug/L 05/17/23 22:23 1634-04-40.50 0.42 1 Naphthalene <2.0 ug/L 05/17/23 22:23 91-20-32.0 0.64 1 Toluene <0.50 ug/L 05/17/23 22:23 108-88-30.50 0.24 1 m&p-Xylene <1.0 ug/L 05/17/23 22:23 179601-23-11.0 0.71 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 26 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92667049 COL054-0314051-23004620 Sample:TRIP BLANK Lab ID:92667049018 Collected:05/10/23 00:00 Received:05/10/23 16:32 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV o-Xylene <0.50 ug/L 05/17/23 22:23 95-47-60.50 0.34 1 Surrogates 1,2-Dichloroethane-d4 (S)113 %05/17/23 22:23 17060-07-070-130 1 4-Bromofluorobenzene (S)96 %05/17/23 22:23 460-00-470-130 1 Toluene-d8 (S)102 %05/17/23 22:23 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 26 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92667049 COL054-0314051-23004620 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 775001 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92667049001, 92667049003, 92667049004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4021669 Associated Lab Samples:92667049001, 92667049003, 92667049004 Matrix:Water AnalyzedMDL Benzene ug/L <0.50 0.50 05/17/23 10:500.34 Ethylbenzene ug/L <0.50 0.50 05/17/23 10:500.30 m&p-Xylene ug/L <1.0 1.0 05/17/23 10:500.71 Methyl-tert-butyl ether ug/L <0.50 0.50 05/17/23 10:500.42 Naphthalene ug/L <2.0 2.0 05/17/23 10:500.64 o-Xylene ug/L <0.50 0.50 05/17/23 10:500.34 Toluene ug/L <0.50 0.50 05/17/23 10:500.24 1,2-Dichloroethane-d4 (S)%108 70-130 05/17/23 10:50 4-Bromofluorobenzene (S)%97 70-130 05/17/23 10:50 Toluene-d8 (S)%102 70-130 05/17/23 10:50 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4021670LABORATORY CONTROL SAMPLE: LCSSpike Benzene ug/L 22.520 112 60-140 Ethylbenzene ug/L 21.520 108 60-140 m&p-Xylene ug/L 42.440 106 60-140 Methyl-tert-butyl ether ug/L 20.920 105 60-140 Naphthalene ug/L 20.720 104 60-140 o-Xylene ug/L 21.020 105 60-140 Toluene ug/L 20.920 104 60-140 1,2-Dichloroethane-d4 (S)%107 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%101 70-130 Parameter Units MS Result % Rec Limits Qual% RecConc. 4021671MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92666177007 4021672 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 20 136 60-140134 1 3020ND27.1 26.9 Ethylbenzene ug/L 20 126 60-140125 1 3020ND25.3 25.0 m&p-Xylene ug/L 40 123 60-140123 0 3040ND49.2 49.1 Methyl-tert-butyl ether ug/L 20 125 60-140124 0 3020ND25.0 24.9 Naphthalene ug/L 20 113 60-140117 3 3020ND22.6 23.3 o-Xylene ug/L 20 122 60-140121 1 3020ND24.4 24.1 Toluene ug/L 20 124 60-140123 1 3020ND24.8 24.5 1,2-Dichloroethane-d4 (S)%108 70-130108 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 26 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92667049 COL054-0314051-23004620 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4021671MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92666177007 4021672 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 4-Bromofluorobenzene (S)%99 70-13099 Toluene-d8 (S)%99 70-130100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 26 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92667049 COL054-0314051-23004620 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 775007 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92667049005, 92667049006, 92667049008, 92667049009, 92667049011, 92667049013, 92667049014, 92667049015, 92667049018 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4021692 Associated Lab Samples:92667049005, 92667049006, 92667049008, 92667049009, 92667049011, 92667049013, 92667049014, 92667049015, 92667049018 Matrix:Water AnalyzedMDL Benzene ug/L <0.50 0.50 05/17/23 21:300.34 Ethylbenzene ug/L <0.50 0.50 05/17/23 21:300.30 m&p-Xylene ug/L <1.0 1.0 05/17/23 21:300.71 Methyl-tert-butyl ether ug/L <0.50 0.50 05/17/23 21:300.42 Naphthalene ug/L <2.0 2.0 05/17/23 21:300.64 o-Xylene ug/L <0.50 0.50 05/17/23 21:300.34 Toluene ug/L <0.50 0.50 05/17/23 21:300.24 1,2-Dichloroethane-d4 (S)%110 70-130 05/17/23 21:30 4-Bromofluorobenzene (S)%98 70-130 05/17/23 21:30 Toluene-d8 (S)%103 70-130 05/17/23 21:30 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4021693LABORATORY CONTROL SAMPLE: LCSSpike Benzene ug/L 22.820 114 60-140 Ethylbenzene ug/L 21.320 106 60-140 m&p-Xylene ug/L 41.840 104 60-140 Methyl-tert-butyl ether ug/L 21.520 107 60-140 Naphthalene ug/L 20.720 103 60-140 o-Xylene ug/L 20.720 104 60-140 Toluene ug/L 20.820 104 60-140 1,2-Dichloroethane-d4 (S)%109 70-130 4-Bromofluorobenzene (S)%99 70-130 Toluene-d8 (S)%101 70-130 Parameter Units MS Result % Rec Limits Qual% RecConc. 4021694MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92667049005 4021695 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 20 139 60-140134 4 3020<0.50 27.8 26.8 Ethylbenzene ug/L 20 132 60-140128 3 3020<0.50 26.3 25.6 m&p-Xylene ug/L 40 128 60-140124 3 3040<1.0 51.3 49.7 Methyl-tert-butyl ether ug/L 20 126 60-140119 5 3020<0.50 25.2 23.9 Naphthalene ug/L 20 115 60-140113 2 3020<2.0 23.0 22.7 o-Xylene ug/L 20 126 60-140123 3 3020<0.50 25.2 24.6 Toluene ug/L 20 129 60-140122 6 3020<0.50 25.7 24.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 26 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92667049 COL054-0314051-23004620 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4021694MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92667049005 4021695 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,2-Dichloroethane-d4 (S)%109 70-130109 4-Bromofluorobenzene (S)%99 70-13099 Toluene-d8 (S)%100 70-130100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 26 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92667049 COL054-0314051-23004620 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 775332 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92667049002, 92667049010, 92667049012, 92667049016 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4023369 Associated Lab Samples:92667049002, 92667049010, 92667049012, 92667049016 Matrix:Water AnalyzedMDL Benzene ug/L <0.50 0.50 05/18/23 13:250.34 Ethylbenzene ug/L <0.50 0.50 05/18/23 13:250.30 m&p-Xylene ug/L <1.0 1.0 05/18/23 13:250.71 Methyl-tert-butyl ether ug/L <0.50 0.50 05/18/23 13:250.42 Naphthalene ug/L <2.0 2.0 05/18/23 13:250.64 o-Xylene ug/L <0.50 0.50 05/18/23 13:250.34 Toluene ug/L <0.50 0.50 05/18/23 13:250.24 1,2-Dichloroethane-d4 (S)%84 70-130 05/18/23 13:25 4-Bromofluorobenzene (S)%85 70-130 05/18/23 13:25 Toluene-d8 (S)%103 70-130 05/18/23 13:25 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4023370LABORATORY CONTROL SAMPLE: LCSSpike Benzene ug/L 24.620 123 60-140 Ethylbenzene ug/L 20.120 100 60-140 m&p-Xylene ug/L 40.540 101 60-140 Methyl-tert-butyl ether ug/L 17.420 87 60-140 Naphthalene ug/L 19.820 99 60-140 o-Xylene ug/L 25.420 127 60-140 Toluene ug/L 19.420 97 60-140 1,2-Dichloroethane-d4 (S)%101 70-130 4-Bromofluorobenzene (S)%125 70-130 Toluene-d8 (S)%100 70-130 Parameter Units MS Result % Rec Limits Qual% RecConc. 4023371MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92667049016 4023372 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 20 104 60-14081 25 3020<0.50 20.9 16.2 Ethylbenzene ug/L 20 108 60-14083 26 3020<0.50 21.6 16.6 m&p-Xylene ug/L 40 106 60-14082 26 3040<1.0 42.4 32.7 Methyl-tert-butyl ether ug/L R1209960-14060 48 3020<0.50 19.8 12.1 Naphthalene ug/L 20 100 60-14083 18 3020<2.0 20.0 16.6 o-Xylene ug/L 20 106 60-14083 25 3020<0.50 21.3 16.5 Toluene ug/L R12010160-14067 41 3020<0.50 20.3 13.4 1,2-Dichloroethane-d4 (S)%104 70-130105 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 26 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92667049 COL054-0314051-23004620 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4023371MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92667049016 4023372 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 4-Bromofluorobenzene (S)%103 70-130101 Toluene-d8 (S)%99 70-13096 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 26 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92667049 COL054-0314051-23004620 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 775382 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92667049007, 92667049017 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4023606 Associated Lab Samples:92667049007, 92667049017 Matrix:Water AnalyzedMDL Benzene ug/L <0.50 0.50 05/18/23 13:560.34 Ethylbenzene ug/L <0.50 0.50 05/18/23 13:560.30 m&p-Xylene ug/L <1.0 1.0 05/18/23 13:560.71 Methyl-tert-butyl ether ug/L <0.50 0.50 05/18/23 13:560.42 Naphthalene ug/L <2.0 2.0 05/18/23 13:560.64 o-Xylene ug/L <0.50 0.50 05/18/23 13:560.34 Toluene ug/L <0.50 0.50 05/18/23 13:560.24 1,2-Dichloroethane-d4 (S)%113 70-130 05/18/23 13:56 4-Bromofluorobenzene (S)%96 70-130 05/18/23 13:56 Toluene-d8 (S)%102 70-130 05/18/23 13:56 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4023607LABORATORY CONTROL SAMPLE: LCSSpike Benzene ug/L 22.820 114 60-140 Ethylbenzene ug/L 21.920 110 60-140 m&p-Xylene ug/L 43.540 109 60-140 Methyl-tert-butyl ether ug/L 21.320 106 60-140 Naphthalene ug/L 21.320 106 60-140 o-Xylene ug/L 21.520 108 60-140 Toluene ug/L 21.120 105 60-140 1,2-Dichloroethane-d4 (S)%110 70-130 4-Bromofluorobenzene (S)%98 70-130 Toluene-d8 (S)%100 70-130 Parameter Units MS Result % Rec Limits Qual% RecConc. 4023608MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92667049017 4023609 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 20 122 60-140130 6 30201.4 25.9 27.4 Ethylbenzene ug/L 20 120 60-140127 6 3020<0.50 24.0 25.4 m&p-Xylene ug/L 40 120 60-140127 5 30409.0 56.8 59.8 Methyl-tert-butyl ether ug/L 20 109 60-140116 6 3020<0.50 21.8 23.1 Naphthalene ug/L M12010860-140158 7 3020114136146 o-Xylene ug/L 20 123 60-140129 3 302022.3 46.8 48.0 Toluene ug/L 20 113 60-140120 6 3020<0.50 22.6 24.0 1,2-Dichloroethane-d4 (S)%109 70-130109 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 26 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92667049 COL054-0314051-23004620 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 4023608MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92667049017 4023609 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 4-Bromofluorobenzene (S)%98 70-13097 Toluene-d8 (S)%99 70-13099 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 26 #=QL# QUALIFIERS Pace Project No.: Project: 92667049 COL054-0314051-23004620 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 26 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92667049 COL054-0314051-23004620 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92667049001 775001MW-2 SM 6200B 92667049002 775332MW-3 SM 6200B 92667049003 775001MW-4D SM 6200B 92667049004 775001MW-8 SM 6200B 92667049005 775007MW-9 SM 6200B 92667049006 775007MW-10 SM 6200B 92667049007 775382MW-16D SM 6200B 92667049008 775007MW-21 SM 6200B 92667049009 775007MW-22 SM 6200B 92667049010 775332MW-28 SM 6200B 92667049011 775007MW-29D SM 6200B 92667049012 775332MW-34 SM 6200B 92667049013 775007MW-35 SM 6200B 92667049014 775007EB-1 SM 6200B 92667049015 775007EB-2 SM 6200B 92667049016 775332DUP-1 SM 6200B 92667049017 775382DUP-2 SM 6200B 92667049018 775007TRIP BLANK SM 6200B REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 26 Page 23 of 26 Page 24 of 26 Page 25 of 26 Page 26 of 26