MO-30292_49318_CA_CLO_20231211_JPS Composites

7606 Whitehall Executive Center Drive, Suite 800 Charlotte, NC 28273 Tel: [phone] Fax: [phone] www.oneatlas.com

LETTER OF TRANSMITTAL

November 15, 2023

TO: FROM:
NCDEQ, DWM, UST Section Mr. Al Quarles, L.G.
Attn: Ryan Mills ATC Associates of North Carolina, P.C.
610 East Center Avenue, Suite 301 7606 Whitehall Exec Ctr Dr, Ste 800
Mooresville, NC 28115 Charlotte, NC 28732

PROJECT/SUBJECT INFORMATION:

Project Name: JPS Composite Materials, Inc.
Facility ID: 00-0-0000009583
UST #: MO-86090
Address: 535 Connor Street
Statesville, Iredell Co, NC 25677

Submittal Date Description
UST Closure Report 12/11/2023 UST Closure Report for UST #5 and #6

Comments:
The attached report is associated with the closure of two registered USTs (UST-5 and UST-6).
Closed on August 23, 2023 (UST-5) and October 9, 2023 (UST-6). The delay in closure UST-
6 was due to the need to sample soil and groundwater to evaluate a potential release. No
release was indicated from UST-6. No sampling was required for UST-5. Monitoring well MW-
1 is still present and will be abandoned following issuance of a Notice of No Further Action or
other guidance from NCDEQ.

Copy to: Ms. Tina Alexander, JPS Composite Materials

Signature:

UST Closure Report
JPS Composite Materials, Inc.

December 11, 2023

535 Connor Street,
Statesvill, Iredell County, North Carolina
NCDEQ Facility ID # 00-0-0000009583
UST # MO-86090

Prepared for:
JPS Composite Materials, Inc.
535 Connor Street,
Statesville, NC 28677
Prepared by:
ATC Associates of North Carolina, P.C.
7606 Whitehall Executive Center Dr., Suite 800
Charlotte, NC 28204

UST Closure Report ATC Associates of North Carolina, P.C. JPS Composite Materials, Inc., UST # MO-86090, Statesville, NC December 11, 2023

TABLE OF CONTENTS

1.0 Site Information ...................................................................................................................... 1
2.0 Executive Summary ................................................................................................................ 2
3.0 Site History and Characterization ......................................................................................... 3
3.1 UST/AST Information .................................................................................................. 4
3.2 UST/AST Owner/Operator and Other Responsible Party Information ........................ 4
4.0 UST Closure Procedures ....................................................................................................... 4
4.1 Preparations for UST Closure ..................................................................................... 4
4.2 Closure Activities ........................................................................................................ 5
5.0 UST-6 Closure Assessment ................................................................................................... 5
5.1 Soil Sampling Information ........................................................................................... 5
5.2 Groundwater Sampling Information ............................................................................ 6
5.3 Quality Assurance/Quality Control .............................................................................. 7
5.4 Soil and Groundwater Investigation Results ............................................................... 7
6.0 Summary and Conclusions ................................................................................................... 7

Tables
Table B-1 Site History – UST/AST Owner/Operator and Other
Table B-2 Site History – UST/AST System and Other Release Information Table B-3 Soil Analytical Results Table B-4 Groundwater Analytical Results

Figures

Figure 1 Topographic Map Figure 2 Site Map Figure 3 Soil Analytical Results Figure 4 Dissolved Analytical Results
Appendices Appendix A Bill of Laden/Material (Waste Disposal) Manifests
Appendix B 24-Hour Release and UST Leak Reporting Form (UST-61); Site Investigation Report for Permanent Closure or Change-in-Service of UST (UST-2A Form) Appendix C Soil Compaction Field Log and Testing Results
Appendix D Soil Boring Logs and Well Construction Record Appendix E Laboratory Reports
UST Closure Report ATC Associates of North Carolina, P.C.
JPS Composite Materials, Inc. , UST# MO-86090, Statesville, NC December 11, 2023
1.0 SITE INFORMATION
1.1 Site Identification
Date of Report: December 11, 2023 Site Risk: unknown
Facility 1.0.: 00-0-0000009583 UST Incident Number (if known): MO-86090
Site Name: JPS Composite Materials, Inc.
Street Address: 535 Connor Street
City/Town: Charlotte Zip Code: 28677 County: Iredell
Description of Geographical Data Point (e.g., diesel fill port): UST-6 (30.000-gallon UST)
Location Method (GPS, topographical map, other): Google Earth
Latitude (decimal degrees): 35.774171 ° N Longitude (decimal degrees): 80.893723° w
1.2 Information about Contacts Associated with the Leaking UST System.
UST/AST Owner: JPS Composite Materials, Inc. Email: T [e-mail]
Address: 535 Connor St., Statesville, NC 28677 Tel: [phone]
UST/AST Operator: Same as above Email: Same as above
Address: Same as above Tel: Same as above
Property Owner: Same as above Email: Same as above
Address: Same as above Tel: Same as above
Property Occupant: Same as above Email: Same as above
Address: Same as above Tel: Same as above
ConsultanUContractor: ATC Associates of North Carolina, P.C.
Address: 7606 Whitehall Exec. Center Dr., Ste 800, Charlotte, NC 28204
Email: [e-mail] Tel: [phone]
Analytical Laboratory: PACE Analytical, Huntersville State Certification No: .12.
Address: 9800 Kincey Ave# 100, Huntersville, NC 28078 Tel: [phone]
1.3 Information about Release
Date Discovered: not applicable; no release confirmed
Estimated Quantity of Release: not applicable
Cause of Release: not applicable
Source of Release (e.g., Dispenser/Piping/UST): not applicable
Sizes and Contents of Tanks or Other Containment from which the Release Occurred: not applicable
5. Certification
I, Al Quarles, a Licensed Geologist for ATC Associates of North Carolina,
P.C., do certify that the information contained in this report is correct and
accurate to the best of my knowledge.
ATC Associates of North Carolina, P.C. is licensed to practice engineering
and geology in North Carolina. The certification number of the company or
corporation for engineering is C-1598. The certification number of the
company or corporation for geology is C-294.
Page 1 of 8
UST Closure Report ATC Associates of North Carolina, P.C. JPS Composite Materials, Inc. , UST # MO-86090, Statesville, NC December 11, 2023
Page 2 of 8
2.0 EXECUTIVE SUMMARY
JPS Composite Materials, Inc. (JPS), has operated as a fiberglass materials manufacturing facility since the late 1880s. The site is located at 535 Connor Street, Statesville, Iredell County, North
Carolina. Two underground storage tanks (USTs) were recently closed in place: one 20,000-gallon UST (UST-5) and one 30,000-gallon UST (UST-6). The USTs contained fuel oil for on-site heating, and are registered as Commercial, Non-Regulated USTs by the North Carolina Department of Environmental Quality (NCDEQ), Division of Waste Management, UST Section. The USTs and their appurtenances are owned by JPS. Between August 14, 2023, and October 9, 2023, UST-5 and UST-
6, and their appurtenances, were closed in place by ATC Associates of North Carolina, P.C. (ATC), in accordance with NCDEQ, DWM, UST Section Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement (STIRA Guidelines).
UST-5 is located in a loading dock in the western portion of the facility. UST-6 is located adjacent to another loading dock in the southeastern portion of the property. Both tanks are registered with
NCDEQ and classified as unregulated, commercial USTs. UST-5 was closed in place on August 23, 2023. No unusual operating conditions or suspected
releases were observed during closure of UST-5, and therefore, no soil or groundwater sampling was required as a part of closure activities.
During closure activities for UST-6, several holes were observed in the bottom of the UST after emptying and cleaning the UST, and water was observed to be entering the UST from the holes. UST Closure activities were suspended, and the unusual operating condition was reported to the UST Section of NCDEQ on August 23, 2023. Following observation of holes in the bottom of the 30,000-gallon UST, a soil and groundwater sampling was conducted in accordance with NCDEQ STIRA Guidelines. From September 18 to September 19, 2023, Fourteen (14) soil samples (SB-1 through SB-14) were advanced around the
perimeter of the 30,000 gallon UST. Additionally, one permanent monitoring well (MW-1) was installed on the downgradient side of the UST in order to collect a groundwater sample. Soil samples were analyzed by EPA Method 8015 for Total Petroleum Hydrocarbons – Diesel Range Organics
(TPH-DRO). The groundwater sample was analyzed for semi-volatile organic compounds (SVOCs) by EPA Method 625 and for Extractable Petroleum Hydrocarbons (EPH) by the MADEP Method. Sampling was conducted to document environmental conditions and determine if a release from the
UST had occurred. Laboratory analytical results of the soil samples collected around UST-6 indicated no detections
above the NCDEQ action level for TPH DRO. Laboratory analytical results of the groundwater sample collected from monitoring well MW-1 near UST-6 indicated no detections of SVOCs and no exceedances of the 15A NCAC 02L .0202 groundwater quality standards (2L Standards) for the EPH compounds. Based on the soil and groundwater results, UST-6 was closed in-place on October 9, 2023.
Based on the soil and groundwater analytical results, no further action appears to be warranted for UST-5 and UST-6.
UST Closure Report ATC Associates of North Carolina, P.C. JPS Composite Materials, Inc. , UST # MO-86090, Statesville, NC December 11, 2023
Page 3 of 8
3.0 SITE HISTORY AND CHARACTERIZATION
JPS Composite Materials, Inc., has operated as a fiberglass materials manufacturing facility since the late 1880s. The site is located at 535 Connor Street, Statesville, Iredell County, North Carolina.
The subject property is located in mixed manufacturing and residential zone of Iredell County. The subject facility is zoned for manufacturing purposes. The surrounding area is zoned as a mixture of commercial and residential. Public water supply for the area is provided by the City of Statesville. During the recent assessment activities conducted by ATC, two water supply wells were identified
within 1,500 feet of the subject facility. The water supply wells are out of use, but were historically used as non-potable supply wells for facility operations. A topographic map of the area is presented as Figure 1, and a site map is presented as Figure 2. UST Owner/Operator and system information
are summarized in Section 3.1 and Section 3.2 below. Review of historical reports reveal that previously, four 30,000-gallon USTs (Registered as UST-1
through UST-4), one 10,000-gallon UST (Registered as UST-7), and one 500-gallon UST (UST-8) were present at the facility (Table B-1). UST-1 through UST-4, UST-7, and UST-8 were all closed by removal according to the NCDEQ UST database. According the the NCDEQ UST Database, UST-1
through UST-4 were closed on August 30, 1991, UST-7 was closed on August 31, 1991, and UST-8 was closed on October 6, 1995. UST-5 (20,000-gallons) and UST-6 (30,000-gallons) were closed during this scope of work.
Owner and operator information for the USTs registered at the site and USST release information is presented in Table B-2. In 1988, following an ownership change of the facility, a site investigation was conducted by Dames & Moore (Site Investigation Report dated August 22, 1988, Dames & Moore). Releases were reported from the area of UST-1 through UST-4 and UST-7 following the investigation. The release(s) were assigned the incident number 3853 by the NCDEQ UST Section. The Site Investigation Report dated August 22, 1988, included recommendations for further assessment. As a result, an assessment was conducted by Universal Engineering Services (UES)
and the resulting report was submitted to NCDEQ in June of 1989 (Contamination Assessment Report dated June 22, 1989, UES). The Contamination Assessment Report dated June 22, 1989 confirmed soil contamination in the vicinity of UST-1 through UST-4 and groundwater contamination
in the vicinity of UST-7. The report included recommendations for these tanks to be removed and contaminated soils excavated during removal. Records revealed that UST-1 through UST-4 were removed by Four Season Industrial Services in August 1991; however a closure report could not be
located in NCDEQ Laserfiche files. Records documenting closure of UST-7 and UST-8 could not be located.
In response to the initial assessments conducted, a Notice of Regulatory Requirement (NORR) was issued from NCDEQ to Springs Industries, Inc., the tank owner at that time, that requested further assessment for incident number 3583. A Limited Site Assessment was conducted by URS Corporation (URS) and the resulting report was submitted on February 18, 2011 (Limited Site Assessment Report dated February 18, 2011, URS). The Limited Site Assessment Report concluded that no further action was warranted for the release(s). Subsequently, the NCDEQ issued a Notice of No Further Action for incident number 3853 on July 29, 2011 by NCDEQ.
UST-5 is located in the loading dock area along the central-southeastern side of the JPS facility, and is bounded by building walls on three sides. Sanitary sewer lines are present within approximately five feet of both the western and eastern sides of the UST basin. Underlying the subsurface, but
above the UST, there are a series of “I” beams providing extra support to the loading dock, as the area used to be an ending point for railcars to unload.
UST Closure Report ATC Associates of North Carolina, P.C. JPS Composite Materials, Inc. , UST # MO-86090, Statesville, NC December 11, 2023
Page 4 of 8
UST-6 is located along the southeastern portion of the JPS facility bounded by Pine Street and an active railroad to the South. Low-hanging overhead power lines run approximately 15 feet from the
western side of the UST and diagonally over the UST basin itself toward the east. An access road for JPS facility operations is located approximately 20 feet to the south of the UST. To the west, large cooling towers are present within approximately 25 feet of the UST basin. To the north, there is a
loading dock within 10 feet from the UST basin. Asphalt covers the UST and surrounding area. A Site Map included as Figure 2 and depicts the locations of UST-5 and UST-6. Between August 14, 2023, and October 9, 2023, UST-5 and UST-6 were closed in place, and a soil and groundwater sampling was conducted in accordance with NCDEQ STIRA Guidelines. The UST closure activity details are presented below in Section 4.0.
3.1 UST/AST Information

Table B-1 presents information on the registered USTs at the site, including UST-5 and UST-6
recently closed.
3.2 UST/AST Owner/Operator and Other Responsible Party Information

Table B-2 presents information regarding the UST owners and operators, and information of
previously reported UST release.
4.0 UST CLOSURE PROCEDURES
This section presents information regarding the closure in-place of the USTs and associated piping.
4.1 Preparations for UST Closure
The USTs are registered with NCDEQ as unregulated, commercial USTs. Therefore, notification to
NCDEQ for UST Closure was not required prior to the UST closure activities. Due to the USTs unregulated status, they were not required to be removed or closed via any specific procedure in accordance with NCDEQ STIRA Guidelines.
In preparation for UST Closure, ATC mobilized to the facility along with the UST Closure Contractor, A&D Environmental Services (A&D) to remove as much of the remaining product from the USTs as
possible. From August 14, 2023 to August 23, 2023, A&D removed residual fuel from the tanks, rinsed the tanks with a water mixture including Purple Power detergent and Simple Green® All-Purpose Cleaner, and diesel fuel, as needed, due to the viscosity of the UST contents, and then removed the rinsing fluids. The removed fluids were transported by A&D to a permitted facility for treatment and disposal. Copies of the non-hazardous waste manifests for all liquids removed are included in Appendix A. After cleaning of UST-6 during UST closure activities, several corrosion holes (~0.25 to 0.5 inches)
were observed in the bottom of that tank and water was noted to be entering the UST through these holes. No water was observed in the UST prior to removal of the heating oil. Residual corrosion material (e.g., rust) may have been present blocking the holes from fluid leakage from or into the
USTs. After consultation with NCDEQ, this was determined to be an unusual operating condition and thus required to be reported. Initial response actions had already been taken to remove the tank contents, clean the UST, and plug the holes to mitigate the potential for additional water entering the
tank, fulfilling the requirements for Initial Response Actions in accordance with NCAC 15A .02N, Section .0702. A UST-61 form was submitted for the 30,000-gallon UST on August 23, 2023
UST Closure Report ATC Associates of North Carolina, P.C. JPS Composite Materials, Inc. , UST # MO-86090, Statesville, NC December 11, 2023
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(Appendix A), to serve as the 24-hour notification of an unusual operating condition, in accordance with NCAC 15A .02N, Section .0601.
Due to the unusual operating condition for UST-6, environmental sampling was required as part of closing the UST, whether the UST was closed in place or removed. Fourteen soil samples and one
groundwater sample were collected to evaluate site conditions for a possible petroleum release from the UST. The results of the soil and groundwater sampling are presented in Section 5.0. In accordance with NCDEQ’s STIRA Guidelines, Section 3.7.3., In-Place Closure (or Change-in-Service) of USTs, ATC, on behalf of JPS, requested in-place closure of the UST-6 based on the belief that assessment and cleanup of any potential release would not require system removal, and that system removal would otherwise be unreasonable or impracticable. Approval was granted from NCDEQ for closure of UST-6 in-place on September 12, 2023.
On October 6, 2023, A&D Environmental removed 3,316 gallons of fluid from UST-6. A copy of the non-hazardous waste manifest is included in Appendix A.
No unusual operating conditions requiring 24-hour reporting were observed during the cleaning of UST-5 or associated lines, and therefore, the UST closure proceeded as discussed below.

4.2 Closure Activities
After the cleaning of the USTs, UST Closure in-place activities were conducted at the Site. UST-5 was closed on August 22, 2023 and UST-6 was closed on October 9, 2023. A&D performed the UST
closure activities with ATC providing oversight and project management services for the closure. All UST Closure activities were conducted in accordance with NCDEQ STIRA Guidelines. The USTs were filled in place with foam (Tailored Chemical Products, Inc. Core-Fill 500 Resin and P 500). All associated lines were capped prior to filling the USTs with foam. Electric pump equipment
was disconnected from the associated piping, loaded onto a trailer, and transported off site for proper disposal.
On October 19, 2023, A&D Environmental backfilled the manway to UST-6 with soil. A copy of the field report with compaction testing results in included in Appendix C.
Post closure information is included on the Site Investigation Report Form (UST-2), which is included in Appendix A.
5.0 UST-6 CLOSURE ASSESSMENT
5.1 Soil Sampling Information
On September 18, 2023, ATC mobilized to the site with drilling contractor EDPS (EDPS) in order to conduct the soil and groundwater sampling. Fourteen soil borings were advanced and samples were collected from the perimeter of UST-6, within five feet from the estimated ends and sides of the UST. The borings were advanced to depths of 20 feet below ground surface (ft-bgs), The locations of the borings are illustrated on Figure 3. Soil samples were collected using direct push soil sampling
methodology. Fourteen (14) soil samples (SB-1 through SB-14) were collected from the perimeter of the UST basin
to document environmental conditions. Based on the soil conditions and measurements Samples were collected from above the saturated zone, ranging from 13-15 ft-bgs to 15-17 ft-bgs, depending
UST Closure Report ATC Associates of North Carolina, P.C. JPS Composite Materials, Inc. , UST # MO-86090, Statesville, NC December 11, 2023
Page 6 of 8
on recovery of cores and saturation of the material. The estimated depth to the bottom of the UST was 15 ft-bgs. Following the collection of the soil samples, the borings were checked for the presence
of groundwater, and groundwater levels were observed at depths of 17 ft-bgs is several of the borings. Light non-aqueous phase liquid (LNAPL) was not apparent in the soil or groundwater observed in the borings. Soil boring logs are included in Appendix D.
Each soil sample selected for laboratory analysis was placed in laboratory provided sample containers and submitted for analyses by Environmental Protection Agency (EPA) Method 8015C for Total Petroleum Hydrocarbons (TPH) – Diesel Range Organics (DRO). The soil samples were placed into laboratory-approved containers, packed in ice, and delivered under chain-of-custody to Pace Analytical Services, LLC (Pace, North Carolina Certification No. 12) in Huntersville, North Carolina for analyses. The locations of the soil samples are provided in Figure 2.
5.2 Groundwater Sampling Information

Between September 18 and September 19, 2023, in accordance with NCDEQ STIRA Guidelines, a permanent monitoring well (MW-1) was installed at the site by personnel with EDPS (EDPS), a North Carolina licensed driller, under supervision of personnel from ATC. The location of monitoring well
MW-1 is depicted on Figure 2. Monitoring well MW-1 was installed by over drilling SB-1. When installing MW-1, ATC did not
encounter what was believed to be a sufficient enough water bearing zone until about 30 ft-bgs. Therefore, to ensure that there was water in the well for sampling, the well was drilled down to 32 ft-bgs. The well was installed with 15 feet of screen. The water level was measured in the newly
installed well prior to development. The water level in the well prior to well development was measured to be 22 ft-bgs in the monitoring well. The well was then properly developed and allowed to equilibrate overnight. The monitoring well was installed using hollow-stem augers and constructed of two-inch diameter
well casing made of flush-joint, threaded schedule-40 poly vinyl chloride (PVC) pipe. The PVC well screen is 0.010-inch slot with a screened interval of 15 feet. A coarse pack (filter pack) was used to backfill the well annulus to a depth of approximately one foot above the well screen. A one-foot thick
bentonite seal was placed above the filter pack, and neat cement was used to fill the remainder of the well annuli to ground surface. The well was installed as flush-mounted and was provided with a sealing and locking cap. The well construction record is included in Appendix D.
ATC personnel returned to the site on September 19, 2023, to collect the groundwater sample from the newly installed MW-1. When ATC measured the water level in the well on September 19, 2023,
it was recorded to be 11.71 ft-bgs. The monitoring well was sampled utilizing low-flow groundwater sampling techniques. The monitoring well was properly purged prior to sampling and field parameters collected from purge water every five minutes. After field parameters had stabilized, a representative groundwater sample was collected. Upon collection, the groundwater sample was placed into laboratory-approved containers, packed in ice, and delivered under chain-of-custody to Pace for analyses. The groundwater sample was analyzed by EPA Method 625 and Massachusetts Department of Environmental Protection (MADEP) methods for extractable petroleum hydrocarbons (EPH). Due to a misunderstanding of the sample containers by the field staff, two sets of containers were filled and noted as samples MW-1 and MW-1(2) on the Chain-of-Custody. The two samples are from MW-1,
and one of the samples may be considered as a duplicate of the other sample.
UST Closure Report ATC Associates of North Carolina, P.C. JPS Composite Materials, Inc. , UST # MO-86090, Statesville, NC December 11, 2023
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5.3 Quality Assurance/Quality Control
The soil and groundwater sample containers were labelled and placed on ice in a cooler pending transport to Pace. Strict chain-of-custody and sample preservation protocols were observed for shipping and delivering the samples.
5.4 Soil and Groundwater Investigation Results
Soil
TPH-DRO was reported in seven of the fourteen samples at concentrations ranging from 4.7 milligrams per kilogram (mg/kg) in sample SB-9 to 40.2 mg/kg in sample SB-5. Sample SB-1 (the boring for monitoring well MW-1) contained 8.7 mg/kg of TPH-DRO. None of the reported
concentrations exceeded the NCDEQ action level for TPH-DRO of 100 mg/kg. Table B-3 provides a summary of the soil analytical results. TPH-DRO concentrations are depicted on Figure 3. A copy of the laboratory report is included in Appendix E.

Groundwater
No EPA Method 625 constituents were reported above the laboratory reporting or detection limits. The MADEP Method results indicated low concentrations of aliphatics and aromatics at concentrations less than the 15A NCAC 02L .0202 groundwater quality standards (2L Standards). A summary of the groundwater analytical results is provided in Table B-4. Dissolved contaminants of concern are depicted on Figure 4. A copy of the laboratory report is included in Appendix E.
6.0 SUMMARY AND CONCLUSIONS
Between August 14, 2023, and October 9, 2023, two USTs, UST-5 and UST-6, and their appurtenances, were closed in place, and a soil and groundwater samples were collected around
UST-6, in accordance with NCDEQ STIRA Guidelines. UST-5 is located in a loading dock in the western portion of the facility. UST-6 is located adjacent to
another loading dock in the southeastern portion of the property. Both tanks are registered with NCDEQ and classified as unregulated, commercial USTs.
UST-5 was closed in place on August 23, 2023. No unusual operating conditions or suspected releases were observed during closure of UST-5, and therefore, no sampling was required as a part of closure activities. During closure of UST-6, after emptying and cleaning the UST, several thumb to pinky sized holes were observed in the bottom of the UST. UST Closure activities were suspended, and the unusual operating condition was reported to the UST Section of NCDEQ on August 23, 2023. Following observation of holes in the bottom of the 30,000-gallon UST, a soil and groundwater sampling was conducted in accordance with NCDEQ STIRA Guidelines. From September 18 to September 19, 2023, Fourteen (14) soil samples (SB-1 through SB-14) were advanced around the
perimeter of the 30,000 gallon UST. Additionally, one permanent monitoring well (MW-1) was installed on the downgradient side of the UST in order to collect a groundwater sample. Soil samples were analyzed by method 8015 for Total Petroleum Hydrocarbons – Diesel Range Organics (TPH-
DRO) in accordance with Table 3 of the Comprehensive Tables for Corrective Action Guidelines. Groundwater samples were analyzed for target analytes listed in table 21 of the Comprehensive Tables for Corrective Action Guidelines by EPA Method 625 and MADEP EPH. Sampling was
UST Closure Report ATC Associates of North Carolina, P.C. JPS Composite Materials, Inc. , UST # MO-86090, Statesville, NC December 11, 2023
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conducted to document environmental conditions and determine if a release had occurred to the soil and groundwater around the UST.
Laboratory analytical results of the soil samples collected during UST closure activities indicated no detections above the NCDEQ action level for TPH DRO.
Laboratory analytical results of the groundwater sample collected from monitoring well MW-1 near UST-6 indicated no detections of SVOCs and no exceedances of the 15A NCAC 02L .0202 groundwater quality standards (2L Standards) for the EPH compounds. Based on the soil and groundwater results, UST-6 was closed in-place on October 9, 2023. Based on the soil and groundwater analytical results, no further action appears to be warranted for
UST-5 and UST-6.
UST Closure and Site Investigation Report JPS Composite Materials, Inc.

TABLES

Table B-1: Site History – UST/AST System and Other Release Information Facility ID # 00-0-0000009583 JPS Composite Materials, Inc, 535 Connor Street, Statesville, Iredell County, NC 28677

UST ID
Number
Current /
Most-Recent
Contents*
Previous
Contents*
Capacity
(gallons)
Construction
Details**
Tank
Dimensions
Description
of Piping
and Pumps
Date Tank
Installed
Status of
UST***
Release
associated
with this UST
System?
UST-1 Diesel Fuel Diesel Fuel 30,000 Single Wall
Steel
unknown unknown 2/18/1973 Closed
8/30/1991
Yes
UST-2 Diesel Fuel Diesel Fuel 30,000 Single Wall
Steel
unknown unknown 2/18/1973 Closed
8/30/1991
Yes
UST-3 Diesel Fuel Diesel Fuel 30,000 Single Wall
Steel
unknown unknown 2/18/1973 Closed
8/30/1991
Yes
UST-4 Diesel Fuel Diesel Fuel 30,000 Single Wall
Steel
unknown unknown 2/18/1973 Closed
8/30/1991
Yes
UST-5 Number 5 Fuel
Oil
Number 5 Fuel
Oil
20,000 Single Wall
Steel
10.6 feet x
31 feet
Steel 2/21/1963 Closed
8/23/2023
No
UST-6 Number 5 Fuel
Oil
Number 5 Fuel
Oil
30,000 Single Wall
Steel
10.6 feet x
47 feet
Steel 2/17/1978 Closed
10/9/2023
No
UST-7

Diesel Fuel Diesel Fuel 10,000 Single Wall
Steel
unknown unknown 1/1/1964 Closed
8/30/1991
Yes
UST-8 Gasoline, gas
mix
Gasoline, gas
mix
500 Single Wall
Steel
unknown unknown 1/1/1960 Closed
10/6/1995
No

Table B-1: Site History – UST/AST System and Other Release Information (Continued)
Facility ID # 00-0-0000009583
JPS Composite Materials, Inc, 535 Connor Street, Statesville, Iredell County, NC 28677

Incident
Number
Material
Released Date of Release Description of Release
3853 Diesel Reported
August 22,
1988
A site investigation was conducted and a report submitted to NCDEQ on August 22, 1989,
which documented impacts of petroleum constituents to soil and groundwater in the areas
of UST-1 through UST-4, and groundwater in the area of UST-7. A release was confirmed
as a result of this assessment. Limited Site Assessment submitted February 18, 2011.
Notice of No Further Action issued July 29, 2011

Table B-2: Site History - UST/AST Owner/Operator and Other
Responsible Party Information Facility ID # 00-0-0000009583 JPS Composite Materials, Inc. 535 Connor Street, Statesville, Iredell County, NC 28677

UST ID Number UST-5/UST-6 Facility ID Number 00-0-0000009583
Owner Name (and Contact) Dates of Operation
(mm/dd/yy to mm/dd/yy)
JPS Composite Materials, Inc. 2/21/1963 - 8/23/2023 (UST-5)
2/17/1978 - 10/9/2023 (UST-6)
Street Address
535 Connor Street
City State Zip Telephone Number
Statesville NC 28677 704-878-8381
Operator Name Operator Contact
JPS Composite Materials, Inc. Tina Alexander
[e-mail]
Street Address
535 Connor Street
City State Zip Telephone Number
Statesville NC 28677 704-878-8381
Other Incidents Onsite or Commingled/In Close Proximity
Incident Number MO-3853 Date Incident
Occurred unknown
Name of Responsible Party
for Other Incident
Date Incident
Reported August 22, 1998
Springs Industries, Inc. (Business Withdrawn
per NC Secretary of State)
Date Incident Closed July 18, 2011
Street Address
535 Connor Street
City State Zip Telephone Number
Statesville NC 28677 N/A; Business withdrawn

535 Connor Street, Statesville, Iredell Count , NC 28677
TPH DRO (EPA
8015)
Source Area
(e.g.,
Tank Pit 1)
SB-1/ MW-1 9/18/2023 UST-6 13-15 UST Closure 8.7
SB-2 9/18/2023 UST-6 13-15 UST Closure <4.7
SB-3 9/18/2023 UST-6 13-15 UST Closure <4.7
SB-4 9/18/2023 UST-6 14-15 UST Closure 6.8
SB-5 9/18/2023 UST-6 14-15 UST Closure 40.2
SB-6 9/18/2023 UST-6 14-15 UST Closure 10
SB-7 9/18/2023 UST-6 14-15 UST Closure 12.7
SB-8 9/18/2023 UST-6 15-17 UST Closure <4.6
SB-9 9/18/2023 UST-6 15-16 UST Closure 4.7J
SB-10 9/18/2023 UST-6 15-16 UST Closure <4.6
SB-11 9/18/2023 UST-6 15-17 UST Closure <4.6
SB-12 9/18/2023 UST-6 15-17 UST Closure 33.4
SB-13 9/18/2023 UST-6 14-16 UST Closure <4.5
SB-14 9/18/2023 UST-6 15-16 UST Closure <4.7
100
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
ft-bgs: feet below ground surface
mg/kg: milligrams per kilogram
NA: Not Applicable
Facility ID # 00-0-0000009583
Table B-3: Summary of Soil Sampling Results
Action Level
TP
H

D
R
O
(m
g
/
k
g
)
JPS Composite Materials, Inc
Analytical Method
Contaminant of Concern
Sample ID
Date
Collected
(mm/dd/yy)
Sample
Depth
(ft-bgs)
Incident Phase
Incident
Phase
UST Closure
MW-1 ND 73.9J <69.3 125J
MW-1(2)ND <66.6 127J 120J
NA 700 10,000 200
Notes:
All concentrations reported in micrograms per liter (µg/L)
J: Estimated concentration between the method detection limit and reporting limit.
2L Standard: 15A NCAC 02L .0202 groundwater quality standards
ND: Not Detected
NA: Not Applicable
Sample
ID
2L Standard
9/19/2023MW-1 UST Closure
Table B-4: Summary of Groundwater and Surface Water
Sampling Results
Contaminant of Concern
Al
l

C
o
m
p
o
u
n
d
s
Al
i
p
h
a
t
i
c

(
C
1
9
-
C
3
6
)
Ar
o
m
a
t
i
c

(
C
9
-
C
2
2
)
625 MADEP
EPH
MADEP
EPHAnalytical Method MADEP
EPH
Al
i
p
h
a
t
i
c

(
C
9
-
C
1
8
)
535 Connor Street, Statesville, Iredell County, 28677
Facility ID # 00-0-0000009583
JPS Composite Materials, Inc.
Well or
SW ID
Date
Collected
(mm/dd/yy)
UST Closure and Site Investigation Report JPS Composite Materials, Inc.

FIGURES

1,500 FT.RADIUSLEGEND:
SITE PROPERTY LINE
NOTE: ALL LOCATIONS ARE APPROXIMATE
PARCEL LINE
300200100
SCALE: 1" = 300'
0
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SITE
SURFACE WATER
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WSW-1
WSW-2
APPROXIMATE LOCATION OFFORMER 20,000 GAL.(31' x 10.5' DIA)NO. 5 OIL
APPROXIMATE LOCATION OFFORMER 30,000 GAL.(47' x 10.5' DIA.)NO. 5 OIL
P
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P P P P P P
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SCALE: 1" = 40'
0 10 20 30 40
N
LEGEND:
SITE PROPERTY LINE
NOTE: ALL LOCATIONS ARE APPROXIMATE
PARCEL LINE
WSW-1 WATER SUPPLY WELL
Well Identification
P P POSSIBLE PRODUCT
PIPING, UST VENT LINE,ELECTRICAL CONDUIT
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SB-12
SB-2
MONITORING WELL
Well Identification
SOIL BORING
Boring Identification
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Figure:
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P
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LEGEND:
SITE PROPERTY LINE
NOTE: ALL LOCATIONS ARE APPROXIMATE
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Well Identification
P P POSSIBLE PRODUCTPIPING, UST VENT LINE,ELECTRICAL CONDUIT
P P P P P P P P P P P P P P P P P P P P
P
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SB-13
SB-2
SB-3
SB-4
SB-5
SB-6
SB-7SB-8
SB-9
SB-10SB-11SB-12
SB-2
MONITORING WELL
Well Identification
SOIL BORING
Boring Identification
SB-1/MW-1
SCALE: 1" = 20'
0 5 10 15 20
N
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WSW-2
APPROXIMATE LOCATION OFFORMER 30,000 GAL.(47' x 10.5' DIA.)NO. 5 OIL
P
P
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P P P P P P P P P P P P
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PPPPPPPP
LEGEND:
SITE PROPERTY LINE
NOTE: ALL LOCATIONS ARE APPROXIMATE
WSW-1 WATER SUPPLY WELL
Well Identification
P P POSSIBLE PRODUCTPIPING, UST VENT LINE,ELECTRICAL CONDUIT
P P P P P P P P P P P P P P P P P P P P
P
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P P
SB-1/MW-1
SB-14
SB-13
SB-2
SB-3
SB-4
SB-5
SB-6
SB-7SB-8
SB-9SB-10
SB-11SB-12
SB-2
MONITORING WELL
Well Identification
SOIL BORING
Boring Identification
SB-1/MW-1
SCALE: 1" = 20'
0 5 10 15 20
N
Figure:
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UST Closure and Site Investigation Report JPS Composite Materials, Inc.

APPENDIX A
Bill of Laden/Material (Waste Disposal) Manifests

UST Closure and Site Investigation Report JPS Composite Materials, Inc.

APPENDIX B
24-Hour Release and UST Leak Reporting Form (UST-61); Site
Investigation Report for Permanent Closure or Change-in-
Service of UST (UST-2 Form)

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from
in NC an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or suspected release
(DWM USE ONLY) Suspected Contamination? (Y/N) Facility ID Number Incident# Risk (H,l,L,U) Confirmed GW Contamination? (Y/N) ___ Date Leak Discovered Received On Received By Confirmed Soil Contamination ?(Y/N) ___ Comm/Non-Commercial? Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) __ Reg/Non-regulated? Region Free Product? (Y/N) __ If Yes, State Greatest Thickness
INCIDENT DESCRIPTION Incident Name:
Address: I County:
City/Town: Zip Code: I Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by: Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount OGPS of release, amount of free oroduct oresent and recoverv efforts, initial resoonses conducted, imoacts to receotors)□Topographic map
OGls Address matching
O0ther □unknown
Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one) □Release Detection Equipment or Methods Dvisual/Odor □Groundwater Contamination
ODuring UST Closure/Removal Dwater in Tank Dsurtace Water Contamination □Property Transfer Dwater Supply Well Contamination O0ther (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release T�ee of Release Product T�ee Released
(Check primary source) (Check primary cause) (Check one) (Check primary product type released)
OTank □spill D Petroleum D Gasoline/ Diesel/ 0 DieselNeg. Oil □Piping □overfill D Non-Petroleum Kerosene Blend
D Dispenser D Corrosion OBoth D Heating Oil 0 Vegetable Oil 100%
D Submersible Turbine Pump D Physical/Mechanical D Other Petroleum OE10-E20
Location Products OE21-E84 D Delivery Problem Damage (Check one) D Metals D Install Problem OE85-E99 □spill Bucket D Other □Facility D Other lnorganics D Ethanol 100% Oother D Unknown □Residence D Other Organics OE01-E09 D Unknown O0ther
Definitions presented on reverse Definitions presented on reverse
Ownershie 1.Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Oeeration Tl£ee 1.Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2
JPS Composite Materials, Inc.
535 Connor Street Iredell
Statesville 28677
x
35.774359 -80.895434
UST Closure activities at the facility began at the site on 8/14/23, for a 30,000-gallon, non-regulated commercial heating oil (#5 fuel)
tank that was used only for heating on premises. Closure activites were conducted in accordance with NCDEQ Guidelines for Site Checks,
Tank Closure, and Initial Response. After all heating oil/sludge was removed from the UST and the UST had been cleaned,
and after returning the next day to begin work, water was discovered to have collected in the UST overnight. The water was pumped out,
and the tank inspected thoroughly. Several small corrosion holes were then observed in the bottom of the UST. The holes were patched to
prevent any additional water entering the tank. Based on the thickness of the fuel in the tank, and based on regular tank level measurements
taken at the facility over time, it is not suspected that the fuel released from the tank. However, after consultation with the UST Division at
NCDEQ, this was determined to be an unusual operating condition which requires reporting. All initial response actions were taken in
accordance with 15A NCAC 2N .0601 as a response to this unusual operating condition, including but not limited to removal of all liquids
(fuel/sludge/water) for disposal off site at a permitted disposal facility, and patching the holes in the bottom of the tank to prevent additional
liquids from entering.
N
N
N
x
x
x
x
x
x
8/18/23
Commercial
Non-Regulated
00-0-0000009583
N
N/A
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2. 3.
UST SYSTEM OWNER
UST Owner/Company
Address
City I State Zip Code I Telephone Number
UST SYSTEM OPERATOR UST Operator/Company
Address
City I State Zip Code I Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT Landowner
Address
City I State Zip Code I Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page2 of2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories ( e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion ( e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion ( e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined Point of Contact
Email
Email
Email
JPS Composite Materials, Inc.Tina Alexander
[e-mail] 535 Connor St.
Statesville NC 28677 704-818-6019
JPS Composite Materials, Inc.
[e-mail] 535 Connor St.
28677 704-818-6019StatesvilleNC
JPS Composite Materials, Inc.
[e-mail]
Statesville NC 28677 704-818-6019
Ashleigh Thrash ATC Associates of NC, PC 704-972-4087
Project Manager 7606 Whitehall Executive Center Dr., Charlotte, NC 28273 8/23/23
See Attached
535 Connor St.
Approximate Location of
30,000-gallon #5 Heating Oil
UST
UST Closure and Site Investigation Report JPS Composite Materials, Inc.

APPENDIX C
Soil Compaction Field Log and Testing Results

Contractor:A&D Environmental
Weather:Sunny Temperature (°F):
Arrival Time:09:00 Departure Time:15:00
Atlas Rep:Hayes, Khristopher
Date:10/19/2023
A. Description of Work:Abandoned underground tank backfill B. Location Details:
Empty holding tank at SE corner of building under pavement.
C. Tests Performed:Soil nuclear gauge
D. Equipment and Crew:Tractor with backhoe attachment, jumping jack
E. Problems/Non­Compliance/Failing Tests
Note that no new discrepancies were reported.
Specs. Available On­Site:Yes No Plans Available On­Site:Yes No
Request for other information; specs./plans, mill certifications, details or manufacturer's literature:
Remarks or Comments:
Our representative arrived on site at 9:00am as requested by Ashleigh. Upon arriving at site, our representative checked in with
Ashleigh. Our representative was informed of work requiring testing and inspections.
Observed backfill and compaction of abandoned underground tank located in the area of the SE corner of the building in the exterior
parking lot/pavement.
This abandoned tank had a backfill area approx 4'x5' and approx 4' deep.  Contractor backfilled using imported soils from off site. 
Material is a brown gravely SAND.  Backfill was placed in lifts and compacted using jumping jack compactor.
Density tests were taken during backfill operations.  Test results show that a minimum 95% compaction was achieved.  Backfill
operations proceeded slowly due to contractor having to import additional material to complete backfill operations.
An ATC representative from our Environmental department was also on site, and inspected approved tank for backfill today.
Before departing the site, our representative notified Ashleigh of field inspection results.
✔✔
Daily Field Report DRPO-000001Report #:
ATC Associates of North Carolina, PC
(Charlotte)
7606 Whitehall Executive Center Dr
Suite 800
Charlotte, NC 28273
Phone: 704­972­4085
Client:
JPS Composite Materials
535 Connor Street
Statesville , NC 28677
Project:
199JPS2301
JPS Statesville UST Closure
535 Connor St.
Statesville, NC 28677
These test results are only based upon the actual items observed, sampled, inspected or tested as part of the
Services. Unless noted otherwise, test results comply with the acceptance criteria in the most recent client­
approved project plans and specifications. We use the simple acceptance/rejection decision rule; accordingly,
measurement uncertainty is not applied in this determination unless required by project plans and specifications
or specified by contract. This report shall not be reproduced, except in full, without prior written approval from ourcompany.
Page 1 of 4Page 1 of 3Page 1 of 4
Contractor:A&D EnvironmentalWeather:Sunny Temperature (°F):Arrival Time:09:00 Departure Time:15:00 Atlas Rep:Hayes, KhristopherDate:10/19/2023A. Description of Work:Abandoned underground tank backfill B. Location Details:Empty holding tank at SE corner of building under pavement.C. Tests Performed:Soil nuclear gaugeD. Equipment and Crew:Tractor with backhoe attachment, jumping jackE. Problems/Non­Compliance/Failing TestsNote that no new discrepancies were reported.Specs. Available On­Site:Yes No Plans Available On­Site:Yes NoRequest for other information; specs./plans, mill certifications, details or manufacturer's literature:Remarks or Comments:Our representative arrived on site at 9:00am as requested by Ashleigh. Upon arriving at site, our representative checked in withAshleigh. Our representative was informed of work requiring testing and inspections.Observed backfill and compaction of abandoned underground tank located in the area of the SE corner of the building in the exteriorparking lot/pavement.This abandoned tank had a backfill area approx 4'x5' and approx 4' deep.  Contractor backfilled using imported soils from off site. Material is a brown gravely SAND.  Backfill was placed in lifts and compacted using jumping jack compactor.Density tests were taken during backfill operations.  Test results show that a minimum 95% compaction was achieved.  Backfilloperations proceeded slowly due to contractor having to import additional material to complete backfill operations.An ATC representative from our Environmental department was also on site, and inspected approved tank for backfill today.Before departing the site, our representative notified Ashleigh of field inspection results.
Upload Image/PDF:Image/PDF Description:
Tank prior to backfill placement.  Inside of tank approve for
backfill by ATC Environmental personnel.
Upload Image/PDF:Image/PDF Description:
✔✔
Daily Field Report DRPO-000001Report #:
ATC Associates of North Carolina, PC
(Charlotte)
7606 Whitehall Executive Center Dr
Suite 800
Charlotte, NC 28273
Phone: 704­972­4085
Client:
JPS Composite Materials
535 Connor Street
Statesville , NC 28677
Project:
199JPS2301
JPS Statesville UST Closure
535 Connor St.
Statesville, NC 28677
These test results are only based upon the actual items observed, sampled, inspected or tested as part of the
Services. Unless noted otherwise, test results comply with the acceptance criteria in the most recent client­
approved project plans and specifications. We use the simple acceptance/rejection decision rule; accordingly,
measurement uncertainty is not applied in this determination unless required by project plans and specifications
or specified by contract. This report shall not be reproduced, except in full, without prior written approval from ourcompany.
Page 2 of 4Page 2 of 3Page 2 of 4
Contractor:A&D EnvironmentalWeather:Sunny Temperature (°F):Arrival Time:09:00 Departure Time:15:00 Atlas Rep:Hayes, KhristopherDate:10/19/2023A. Description of Work:Abandoned underground tank backfill B. Location Details:Empty holding tank at SE corner of building under pavement.C. Tests Performed:Soil nuclear gaugeD. Equipment and Crew:Tractor with backhoe attachment, jumping jackE. Problems/Non­Compliance/Failing TestsNote that no new discrepancies were reported.Specs. Available On­Site:Yes No Plans Available On­Site:Yes NoRequest for other information; specs./plans, mill certifications, details or manufacturer's literature:Remarks or Comments:Our representative arrived on site at 9:00am as requested by Ashleigh. Upon arriving at site, our representative checked in withAshleigh. Our representative was informed of work requiring testing and inspections.Observed backfill and compaction of abandoned underground tank located in the area of the SE corner of the building in the exteriorparking lot/pavement.This abandoned tank had a backfill area approx 4'x5' and approx 4' deep.  Contractor backfilled using imported soils from off site. Material is a brown gravely SAND.  Backfill was placed in lifts and compacted using jumping jack compactor.Density tests were taken during backfill operations.  Test results show that a minimum 95% compaction was achieved.  Backfilloperations proceeded slowly due to contractor having to import additional material to complete backfill operations.An ATC representative from our Environmental department was also on site, and inspected approved tank for backfill today.Before departing the site, our representative notified Ashleigh of field inspection results.Upload Image/PDF:Image/PDF Description:Tank prior to backfill placement.  Inside of tank approve forbackfill by ATC Environmental personnel.
Upload Image/PDF:Image/PDF Description:
Backfilled tank.
Soil Nuclear Gauge
✔✔
Daily Field Report DRPO-000001Report #:
ATC Associates of North Carolina, PC
(Charlotte)
7606 Whitehall Executive Center Dr
Suite 800
Charlotte, NC 28273
Phone: 704­972­4085
Client:
JPS Composite Materials
535 Connor Street
Statesville , NC 28677
Project:
199JPS2301
JPS Statesville UST Closure
535 Connor St.
Statesville, NC 28677
These test results are only based upon the actual items observed, sampled, inspected or tested as part of the
Services. Unless noted otherwise, test results comply with the acceptance criteria in the most recent client­
approved project plans and specifications. We use the simple acceptance/rejection decision rule; accordingly,
measurement uncertainty is not applied in this determination unless required by project plans and specifications
or specified by contract. This report shall not be reproduced, except in full, without prior written approval from ourcompany.
Page 3 of 4Page 3 of 3Page 3 of 4
Test Results
Test #
Retest
Of Test Date Proctor ID Method
Soil
Classification
Optimum
Moisture
(%)
Maximum
Dry Density
(pcf)
In Place
Moisture
(%)
In Place
Dry
Density
(pcf)
In Place
Wet
Density
(pcf)
Probe
Depth
(in)
Percent
Compaction
Min/Max
Comp.
(%)
Optimum
Moisture
Tolerance
(%)Remark
1 10/19/23 P1-Brown
SAND with
gravels,
110.5@15.
4
D698 /
T99 - C
SP-SM 15.4 110.5 12.4 108.6 122.1 8 98 95 / 103 -3 / 3 DP/MP
2 10/19/23 P1-Brown
SAND with
gravels,
110.5@15.
4
D698 /
T99 - C
SP-SM 15.4 110.5 14.5 108.4 124.1 8 98 95 / 103 -3 / 3 DP/MP
3 10/19/23 P1-Brown
SAND with
gravels,
110.5@15.
4
D698 /
T99 - C
SP-SM 15.4 110.5 13.7 108.0 122.8 8 98 95 / 103 -3 / 3 DP/MP
4 10/19/23 P1-Brown
SAND with
gravels,
110.5@15.
4
D698 /
T99 - C
SP-SM 15.4 110.5 12.9 109.4 123.5 8 99 95 / 103 -3 / 3 DP/MP
Test Information
Test #Test Location Elevation Reference
Gauge
Make / Model / SN / Calibrated Field Technician
1 Structure backfill: Empty tank -3.0 Top of adjacent
pavement
Troxler / 3430 / 76799 / Hayes, Khristopher
2 Structure backfill: Empty tank -2.0 Top of adjacent
pavement
Troxler / 3430 / 76799 / Hayes, Khristopher
3 Structure backfill: Empty tank -1.0 Top of adjacent
pavement
Troxler / 3430 / 76799 / Hayes, Khristopher
4 Structure backfill: Empty tank -0.5 Top of adjacent
pavement
Troxler / 3430 / 76799 / Hayes, Khristopher
Remarks
DP/MP: Density Pass / Moisture Pass
Comments
Tests are "Direct Transmission" (Method A) unless probe depth is noted as
"Backscatter". Gauge calibration data on file with the testing agency.
These tests were performed in accordance with ASTM D 6938, AASHTO T-310 or local DOT methods. These test results are only based upon the actual items
observed, sampled, inspected or tested as part of the Services. Unless noted otherwise, test results comply with the acceptance criteria in the most recent client-
approved project plans and specifications. We use the simple acceptance/rejection decision rule; accordingly, measurement uncertainty is not applied in this
determination unless required by project plans and specifications or specified by contract. This report shall not be reproduced, except in full, without prior written
approval from our company.
Page 1 of 1
Soil Nuclear Gauge
Test Method: See Footnote
Report #: SNG-000001
Client:
JPS Composite Materials
Statesville , NC 28677
535 Connor Street
Project:
JPS Statesville UST Closure
199JPS2301
Statesville, NC 28677
535 Connor St.
7606 Whitehall Executive Center Dr
Suite 800
Charlotte, NC 28273
Phone: [phone]
ATC Associates of North Carolina, PC (Charlotte)
Page 4 of 4
UST Closure and Site Investigation Report JPS Composite Materials, Inc.

APPENDIX D
Soil Boring Logs and Well Construction Record

10
-
0
5
-
2
0
2
3

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9
J
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2
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1

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-
1
&
S
B
-
1

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 6"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
30
35
CL
CL
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand
Moist, reddish brown to orange-brown silty CLAY to CLAY, interbedded with
brown sand. Wet at 22 ft. bgs
Wet, orange-brown CLAY mud
END OF BORING
13-15
Well: MW-1
Grout
Bentonite
Sand
Cover
2" Diameter Casing
2" Diameter Screen
10
-
0
5
-
2
0
2
3

C
:
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\
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A
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a
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k
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1
9
9
J
P
S
2
3
0
1

-

J
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S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
2

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 16 ft. bgs
END OF BORING
13-15
10
-
0
5
-
2
0
2
3

C
:
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U
s
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\
k
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.
h
a
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\
O
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-

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k
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t
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1
9
9
J
P
S
2
3
0
1

-

J
P
S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
3

B
o
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i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 16 ft. bgs
END OF BORING
13-15
10
-
0
5
-
2
0
2
3

C
:
\
U
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\
k
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.
h
a
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\
O
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D
r
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v
e

-

O
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A
t
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a
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D
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k
t
o
p
\
t
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m
p
\
1
9
9
J
P
S
2
3
0
1

-

J
P
S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
4

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 16 ft. bgs
END OF BORING
14-15
10
-
0
5
-
2
0
2
3

C
:
\
U
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\
k
y
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.
h
a
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\
O
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D
r
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v
e

-

O
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A
t
l
a
s
\
D
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s
k
t
o
p
\
t
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m
p
\
1
9
9
J
P
S
2
3
0
1

-

J
P
S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
5

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 16 ft. bgs
END OF BORING
14-15
10
-
0
5
-
2
0
2
3

C
:
\
U
s
e
r
s
\
k
y
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.
h
a
r
r
i
s
\
O
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D
r
i
v
e

-

O
n
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A
t
l
a
s
\
D
e
s
k
t
o
p
\
t
e
m
p
\
1
9
9
J
P
S
2
3
0
1

-

J
P
S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
6

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 16 ft. bgs
END OF BORING
14-15
10
-
0
5
-
2
0
2
3

C
:
\
U
s
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s
\
k
y
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.
h
a
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\
O
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D
r
i
v
e

-

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A
t
l
a
s
\
D
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s
k
t
o
p
\
t
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m
p
\
1
9
9
J
P
S
2
3
0
1

-

J
P
S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
7

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 16 ft. bgs
END OF BORING
14-15
10
-
0
5
-
2
0
2
3

C
:
\
U
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k
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h
a
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D
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a
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k
t
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\
t
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\
1
9
9
J
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2
3
0
1

-

J
P
S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
8

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 17 ft. bgs
END OF BORING
15-17
10
-
0
5
-
2
0
2
3

C
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k
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1
9
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J
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2
3
0
1

-

J
P
S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
9

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 17 ft. bgs
END OF BORING
15-16
10
-
0
5
-
2
0
2
3

C
:
\
U
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h
a
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e

-

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A
t
l
a
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D
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s
k
t
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p
\
t
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\
1
9
9
J
P
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2
3
0
1

-

J
P
S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
1
0

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
SOIL BORING: SB-10
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 17 ft. bgs
END OF BORING
15-16
10
-
0
5
-
2
0
2
3

C
:
\
U
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a
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a
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1
9
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2
3
0
1

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J
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C
o
m
p
o
s
i
t
e
s

-

S
B
-
1
1

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
SOIL BORING: SB-11
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 17 ft. bgs
END OF BORING
15-17
10
-
0
5
-
2
0
2
3

C
:
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0
1

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J
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C
o
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p
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i
t
e
s

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S
B
-
1
2

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
SOIL BORING: SB-12
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 17 ft. bgs
END OF BORING
15-17
10
-
0
5
-
2
0
2
3

C
:
\
U
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\
k
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.
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a
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\
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A
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a
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k
t
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\
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1
9
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J
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2
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0
1

-

J
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C
o
m
p
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i
t
e
s

-

S
B
-
1
3

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
Obstruction at 4 ft. bgs on first attempt. Boring moved 2 ft. West of initial location.
bgs = below ground surface
SOIL BORING: SB-13
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, interbedded with brown
sand, becoming wet at 17 ft. bgs
END OF BORING
14-16
10
-
0
5
-
2
0
2
3

C
:
\
U
s
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k
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.
h
a
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\
O
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D
r
i
v
e

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O
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A
t
l
a
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\
D
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k
t
o
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\
t
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\
1
9
9
J
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2
3
0
1

-

J
P
S

C
o
m
p
o
s
i
t
e
s

-

S
B
-
1
4

B
o
r
i
n
g

L
o
g
.
b
o
r
JPS Composite Materials, Inc.
bgs = below ground surface
SOIL BORING: SB-14
(Page 1 of 1)
Date(s) Drilled : 09/18/2023
Drilling Conractor : EDPS
Drilling Method : DPT/HSA
Boring Diameter : 2"
Logged By : Kyle Harris
Sampling Method : Macro-Core®
0
5
10
15
20
25
CL
CL
CL
DESCRIPTION
Asphalt to 8 in. bgs
Reddish brown to orange-brown silty CLAY to CLAY, some gray to white fine
sand, interbedded with brown sand
No recovery. Assumed to be CLAY
reddish brown to orange-brown silty CLAY to CLAY, becoming yellow to
yellow-gray CLAY
END OF BORING
14-16
UST Closure and Site Investigation Report JPS Composite Materials, Inc.

APPENDIX E
Laboratory Reports
#=CL#
October 06, 2023
LIMS USE: FR - ASHLEIGH THRASH
LIMS OBJECT ID: 92689078
92689078
Project:
Pace Project No.:
RE:
Ashleigh Thrash
ATC Group Services, LLC
7606 Whitehall Exceutive
Center Drive Suite 800
Charlotte, NC 28271
JPS Composite Materials
Dear Ashleigh Thrash:
Enclosed are the analytical results for sample(s) received by the laboratory on September 20, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
704-977-0943
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92689078
JPS Composite Materials
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689078
JPS Composite Materials
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92689078001 MW-1 MADEP EPH 8 PANJDG
92689078002 MW-1(2)MADEP EPH 8 PANDMG
92689078003 MW-1 EPA 625.1 58 PASI-CPKS
92689078004 MW-1(2)EPA 625.1 58 PASI-CPKS
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689078
JPS Composite Materials
Sample: MW-1 Lab ID: 92689078001 Collected: 09/19/23 10:50 Received: 09/20/23 13:52 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)73.9J ug/L 09/27/23 20:58 B,J09/25/23 19:45208 2.08
Aliphatic (C19-C36)<69.3 ug/L 09/27/23 20:5809/25/23 19:45208 2.08
Aromatic (C11-C22)125J ug/L 09/27/23 22:34 B,J09/25/23 19:45208 2.08
Total Extractable Hydrocarbons 199J ug/L 09/27/23 22:34 TPH-TEH J09/25/23 19:45208 2.08
Surrogates
o-Terphenyl (S)74.3 %09/27/23 22:34 84-15-109/25/23 19:4540.0-140 2.08
1-Chloro-octadecane (S)69.5 %09/27/23 20:58 3386-33-209/25/23 19:4540.0-140 2.08
2-Fluorobiphenyl (S)79.0 %09/27/23 22:34 321-60-809/25/23 19:4540.0-140 2.08
2-Bromonaphthalene (S)80.8 %09/27/23 22:34 580-13-209/25/23 19:4540.0-140 2.08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689078
JPS Composite Materials
Sample: MW-1(2)Lab ID: 92689078002 Collected: 09/19/23 10:53 Received: 09/20/23 13:52 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)<66.6 ug/L 10/05/23 15:46 G7,R110/03/23 16:56200 2
Aliphatic (C19-C36)127J ug/L 10/05/23 15:46 B,G7,J,
R110/03/23 16:56200 2
Aromatic (C11-C22)120J ug/L 10/05/23 05:17 B,G7,J10/03/23 16:56200 2
Total Extractable Hydrocarbons 247 ug/L 10/05/23 15:46 TPH-TEH G710/03/23 16:56200 2
Surrogates
o-Terphenyl (S)71.3 %10/05/23 05:17 84-15-110/03/23 16:5640.0-140 2
1-Chloro-octadecane (S)70.0 %10/05/23 15:46 3386-33-210/03/23 16:5640.0-140 2
2-Fluorobiphenyl (S)71.6 %10/05/23 05:17 321-60-810/03/23 16:5640.0-140 2
2-Bromonaphthalene (S)73.8 %10/05/23 05:17 580-13-210/03/23 16:5640.0-140 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689078
JPS Composite Materials
Sample: MW-1 Lab ID: 92689078003 Collected: 09/19/23 10:54 Received: 09/20/23 13:52 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene <1.7 ug/L 09/24/23 15:47 83-32-909/24/23 09:344.2 1
Acenaphthylene <1.6 ug/L 09/24/23 15:47 208-96-809/24/23 09:344.2 1
Anthracene <1.9 ug/L 09/24/23 15:47 120-12-709/24/23 09:344.2 1
Benzo(a)anthracene <2.2 ug/L 09/24/23 15:47 56-55-309/24/23 09:344.2 1
Benzo(a)pyrene <2.3 ug/L 09/24/23 15:47 50-32-809/24/23 09:344.2 1
Benzo(b)fluoranthene <2.2 ug/L 09/24/23 15:47 205-99-209/24/23 09:344.2 1
Benzo(g,h,i)perylene <2.4 ug/L 09/24/23 15:47 191-24-209/24/23 09:344.2 1
Benzo(k)fluoranthene <2.3 ug/L 09/24/23 15:47 207-08-909/24/23 09:344.2 1
4-Bromophenylphenyl ether <1.5 ug/L 09/24/23 15:47 101-55-309/24/23 09:344.2 1
Butylbenzylphthalate <2.6 ug/L 09/24/23 15:47 85-68-709/24/23 09:344.2 1
4-Chloro-3-methylphenol <2.8 ug/L 09/24/23 15:47 59-50-709/24/23 09:344.2 1
bis(2-Chloroethoxy)methane <1.5 ug/L 09/24/23 15:47 111-91-109/24/23 09:348.3 1
bis(2-Chloroethyl) ether <1.6 ug/L 09/24/23 15:47 111-44-409/24/23 09:344.2 1
2-Chloronaphthalene <1.4 ug/L 09/24/23 15:47 91-58-709/24/23 09:344.2 1
2-Chlorophenol <1.0 ug/L 09/24/23 15:47 95-57-809/24/23 09:344.2 1
4-Chlorophenylphenyl ether <1.7 ug/L 09/24/23 15:47 7005-72-309/24/23 09:344.2 1
Chrysene <2.3 ug/L 09/24/23 15:47 218-01-909/24/23 09:344.2 1
Dibenz(a,h)anthracene <2.5 ug/L 09/24/23 15:47 53-70-309/24/23 09:344.2 1
3,3'-Dichlorobenzidine <6.8 ug/L 09/24/23 15:47 91-94-109/24/23 09:348.3 1
2,4-Dichlorophenol <1.2 ug/L 09/24/23 15:47 120-83-209/24/23 09:344.2 1
Diethylphthalate <1.7 ug/L 09/24/23 15:47 84-66-209/24/23 09:344.2 1
2,4-Dimethylphenol <1.4 ug/L 09/24/23 15:47 105-67-909/24/23 09:348.3 1
Dimethylphthalate <1.8 ug/L 09/24/23 15:47 131-11-309/24/23 09:344.2 1
Di-n-butylphthalate <1.8 ug/L 09/24/23 15:47 84-74-209/24/23 09:344.2 1
4,6-Dinitro-2-methylphenol <6.5 ug/L 09/24/23 15:47 534-52-109/24/23 09:348.3 1
2,4-Dinitrophenol <21.7 ug/L 09/24/23 15:47 51-28-509/24/23 09:3441.7 1
2,4-Dinitrotoluene <1.4 ug/L 09/24/23 15:47 121-14-209/24/23 09:344.2 1
2,6-Dinitrotoluene <1.4 ug/L 09/24/23 15:47 606-20-209/24/23 09:344.2 1
Di-n-octylphthalate <3.3 ug/L 09/24/23 15:47 117-84-009/24/23 09:344.2 1
bis(2-Ethylhexyl)phthalate <3.1 ug/L 09/24/23 15:47 117-81-709/24/23 09:344.2 1
Fluoranthene <1.8 ug/L 09/24/23 15:47 206-44-009/24/23 09:344.2 1
Fluorene <1.7 ug/L 09/24/23 15:47 86-73-709/24/23 09:344.2 1
Hexachloro-1,3-butadiene <1.5 ug/L 09/24/23 15:47 87-68-309/24/23 09:344.2 1
Hexachlorobenzene <1.8 ug/L 09/24/23 15:47 118-74-109/24/23 09:344.2 1
Hexachlorocyclopentadiene <1.3 ug/L 09/24/23 15:47 77-47-409/24/23 09:348.3 1
Hexachloroethane <1.2 ug/L 09/24/23 15:47 67-72-109/24/23 09:344.2 1
Indeno(1,2,3-cd)pyrene <2.4 ug/L 09/24/23 15:47 193-39-509/24/23 09:344.2 1
Isophorone <1.4 ug/L 09/24/23 15:47 78-59-109/24/23 09:348.3 1
Naphthalene <1.7 ug/L 09/24/23 15:47 91-20-309/24/23 09:344.2 1
Nitrobenzene <1.6 ug/L 09/24/23 15:47 98-95-309/24/23 09:344.2 1
2-Nitrophenol <1.2 ug/L 09/24/23 15:47 88-75-509/24/23 09:344.2 1
4-Nitrophenol <5.5 ug/L 09/24/23 15:47 100-02-709/24/23 09:348.3 1
N-Nitrosodimethylamine <1.6 ug/L 09/24/23 15:47 62-75-909/24/23 09:344.2 1
N-Nitroso-di-n-propylamine <1.1 ug/L 09/24/23 15:47 621-64-709/24/23 09:344.2 1
N-Nitrosodiphenylamine <2.5 ug/L 09/24/23 15:47 86-30-609/24/23 09:348.3 1
2,2'-Oxybis(1-chloropropane)<0.96 ug/L 09/24/23 15:47 108-60-109/24/23 09:344.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689078
JPS Composite Materials
Sample: MW-1 Lab ID: 92689078003 Collected: 09/19/23 10:54 Received: 09/20/23 13:52 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol <3.1 ug/L 09/24/23 15:47 87-86-509/24/23 09:348.3 1
Phenanthrene <1.7 ug/L 09/24/23 15:47 85-01-809/24/23 09:344.2 1
Phenol <1.1 ug/L 09/24/23 15:47 108-95-209/24/23 09:344.2 1
Pyrene <1.8 ug/L 09/24/23 15:47 129-00-009/24/23 09:344.2 1
1,2,4-Trichlorobenzene <1.4 ug/L 09/24/23 15:47 120-82-109/24/23 09:344.2 1
2,4,6-Trichlorophenol <1.3 ug/L 09/24/23 15:47 88-06-209/24/23 09:348.3 1
Surrogates
Nitrobenzene-d5 (S)52 %09/24/23 15:47 4165-60-009/24/23 09:3410-120 1
2-Fluorobiphenyl (S)48 %09/24/23 15:47 321-60-809/24/23 09:3415-120 1
Terphenyl-d14 (S)121 %09/24/23 15:47 1718-51-009/24/23 09:3411-131 1
Phenol-d6 (S)27 %09/24/23 15:47 13127-88-309/24/23 09:3410-120 1
2-Fluorophenol (S)36 %09/24/23 15:47 367-12-409/24/23 09:3410-120 1
2,4,6-Tribromophenol (S)97 %09/24/23 15:47 118-79-609/24/23 09:3410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689078
JPS Composite Materials
Sample: MW-1(2)Lab ID: 92689078004 Collected: 09/19/23 10:55 Received: 09/20/23 13:52 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene <1.8 ug/L 09/24/23 16:13 83-32-909/24/23 09:344.5 1
Acenaphthylene <1.8 ug/L 09/24/23 16:13 208-96-809/24/23 09:344.5 1
Anthracene <2.1 ug/L 09/24/23 16:13 120-12-709/24/23 09:344.5 1
Benzo(a)anthracene <2.4 ug/L 09/24/23 16:13 56-55-309/24/23 09:344.5 1
Benzo(a)pyrene <2.5 ug/L 09/24/23 16:13 50-32-809/24/23 09:344.5 1
Benzo(b)fluoranthene <2.4 ug/L 09/24/23 16:13 205-99-209/24/23 09:344.5 1
Benzo(g,h,i)perylene <2.6 ug/L 09/24/23 16:13 191-24-209/24/23 09:344.5 1
Benzo(k)fluoranthene <2.5 ug/L 09/24/23 16:13 207-08-909/24/23 09:344.5 1
4-Bromophenylphenyl ether <1.6 ug/L 09/24/23 16:13 101-55-309/24/23 09:344.5 1
Butylbenzylphthalate <2.9 ug/L 09/24/23 16:13 85-68-709/24/23 09:344.5 1
4-Chloro-3-methylphenol <3.0 ug/L 09/24/23 16:13 59-50-709/24/23 09:344.5 1
bis(2-Chloroethoxy)methane <1.7 ug/L 09/24/23 16:13 111-91-109/24/23 09:349.1 1
bis(2-Chloroethyl) ether <1.7 ug/L 09/24/23 16:13 111-44-409/24/23 09:344.5 1
2-Chloronaphthalene <1.6 ug/L 09/24/23 16:13 91-58-709/24/23 09:344.5 1
2-Chlorophenol <1.1 ug/L 09/24/23 16:13 95-57-809/24/23 09:344.5 1
4-Chlorophenylphenyl ether <1.8 ug/L 09/24/23 16:13 7005-72-309/24/23 09:344.5 1
Chrysene <2.5 ug/L 09/24/23 16:13 218-01-909/24/23 09:344.5 1
Dibenz(a,h)anthracene <2.7 ug/L 09/24/23 16:13 53-70-309/24/23 09:344.5 1
3,3'-Dichlorobenzidine <7.4 ug/L 09/24/23 16:13 91-94-109/24/23 09:349.1 1
2,4-Dichlorophenol <1.3 ug/L 09/24/23 16:13 120-83-209/24/23 09:344.5 1
Diethylphthalate <1.9 ug/L 09/24/23 16:13 84-66-209/24/23 09:344.5 1
2,4-Dimethylphenol <1.5 ug/L 09/24/23 16:13 105-67-909/24/23 09:349.1 1
Dimethylphthalate <1.9 ug/L 09/24/23 16:13 131-11-309/24/23 09:344.5 1
Di-n-butylphthalate <2.0 ug/L 09/24/23 16:13 84-74-209/24/23 09:344.5 1
4,6-Dinitro-2-methylphenol <7.1 ug/L 09/24/23 16:13 534-52-109/24/23 09:349.1 1
2,4-Dinitrophenol <23.6 ug/L 09/24/23 16:13 51-28-509/24/23 09:3445.5 1
2,4-Dinitrotoluene <1.5 ug/L 09/24/23 16:13 121-14-209/24/23 09:344.5 1
2,6-Dinitrotoluene <1.6 ug/L 09/24/23 16:13 606-20-209/24/23 09:344.5 1
Di-n-octylphthalate <3.6 ug/L 09/24/23 16:13 117-84-009/24/23 09:344.5 1
bis(2-Ethylhexyl)phthalate <3.4 ug/L 09/24/23 16:13 117-81-709/24/23 09:344.5 1
Fluoranthene <2.0 ug/L 09/24/23 16:13 206-44-009/24/23 09:344.5 1
Fluorene <1.9 ug/L 09/24/23 16:13 86-73-709/24/23 09:344.5 1
Hexachloro-1,3-butadiene <1.6 ug/L 09/24/23 16:13 87-68-309/24/23 09:344.5 1
Hexachlorobenzene <2.0 ug/L 09/24/23 16:13 118-74-109/24/23 09:344.5 1
Hexachlorocyclopentadiene <1.4 ug/L 09/24/23 16:13 77-47-409/24/23 09:349.1 1
Hexachloroethane <1.3 ug/L 09/24/23 16:13 67-72-109/24/23 09:344.5 1
Indeno(1,2,3-cd)pyrene <2.6 ug/L 09/24/23 16:13 193-39-509/24/23 09:344.5 1
Isophorone <1.5 ug/L 09/24/23 16:13 78-59-109/24/23 09:349.1 1
Naphthalene <1.9 ug/L 09/24/23 16:13 91-20-309/24/23 09:344.5 1
Nitrobenzene <1.7 ug/L 09/24/23 16:13 98-95-309/24/23 09:344.5 1
2-Nitrophenol <1.3 ug/L 09/24/23 16:13 88-75-509/24/23 09:344.5 1
4-Nitrophenol <6.0 ug/L 09/24/23 16:13 100-02-709/24/23 09:349.1 1
N-Nitrosodimethylamine <1.7 ug/L 09/24/23 16:13 62-75-909/24/23 09:344.5 1
N-Nitroso-di-n-propylamine <1.2 ug/L 09/24/23 16:13 621-64-709/24/23 09:344.5 1
N-Nitrosodiphenylamine <2.7 ug/L 09/24/23 16:13 86-30-609/24/23 09:349.1 1
2,2'-Oxybis(1-chloropropane)<1.0 ug/L 09/24/23 16:13 108-60-109/24/23 09:344.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689078
JPS Composite Materials
Sample: MW-1(2)Lab ID: 92689078004 Collected: 09/19/23 10:55 Received: 09/20/23 13:52 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Pentachlorophenol <3.4 ug/L 09/24/23 16:13 87-86-509/24/23 09:349.1 1
Phenanthrene <1.8 ug/L 09/24/23 16:13 85-01-809/24/23 09:344.5 1
Phenol <1.2 ug/L 09/24/23 16:13 108-95-209/24/23 09:344.5 1
Pyrene <2.0 ug/L 09/24/23 16:13 129-00-009/24/23 09:344.5 1
1,2,4-Trichlorobenzene <1.6 ug/L 09/24/23 16:13 120-82-109/24/23 09:344.5 1
2,4,6-Trichlorophenol <1.4 ug/L 09/24/23 16:13 88-06-209/24/23 09:349.1 1
Surrogates
Nitrobenzene-d5 (S)82 %09/24/23 16:13 4165-60-009/24/23 09:3410-120 1
2-Fluorobiphenyl (S)72 %09/24/23 16:13 321-60-809/24/23 09:3415-120 1
Terphenyl-d14 (S)127 %09/24/23 16:13 1718-51-009/24/23 09:3411-131 1
Phenol-d6 (S)44 %09/24/23 16:13 13127-88-309/24/23 09:3410-120 1
2-Fluorophenol (S)59 %09/24/23 16:13 367-12-409/24/23 09:3410-120 1
2,4,6-Tribromophenol (S)123 %09/24/23 16:13 118-79-609/24/23 09:3410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689078
JPS Composite Materials
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2139497
MA DEP/NJ DEP
MADEP EPH
TPH by Method MADEPE
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92689078001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3978964-1
Associated Lab Samples:92689078001
Matrix: Water
Analyzed
Aliphatic (C09-C18)ug/L 63.0J 100 J09/27/23 15:44
Aliphatic (C19-C36)ug/L 49.1J 100 J09/27/23 15:44
1-Chloro-octadecane (S)%92.3 40.0-140 09/27/23 15:44
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3978964-4
Associated Lab Samples:92689078001
Matrix: Water
Analyzed
Aromatic (C11-C22)ug/L 40.1J 100 J09/27/23 16:51
o-Terphenyl (S)%96.3 40.0-140 09/27/23 16:51
2-Fluorobiphenyl (S)%99.5 40.0-140 09/27/23 16:51
2-Bromonaphthalene (S)%99.1 40.0-140 09/27/23 16:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3978964-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3978964-3
Aliphatic (C09-C18)ug/L 460600 76.7 40.0-14077.2463 0.650 25
Aliphatic (C19-C36)ug/L 825800 103 40.0-140108865 4.73 25
1-Chloro-octadecane (S)%91.9 40.0-14096.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3978964-5LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3978964-6
Aromatic (C11-C22)ug/L 17801700 105 40.0-1401051790 0.560 25
o-Terphenyl (S)%95.3 40.0-14096.9
2-Fluorobiphenyl (S)%101 40.0-140103
2-Bromonaphthalene (S)%101 40.0-140103
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3978964-7MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1657797-01
R3978964-8
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aliphatic (C09-C18)ug/L 570 69.7 40.0-14069.0 5.3861254.5 452 477
Aliphatic (C19-C36)ug/L 760 97.0 40.0-14096.8 6.4381645.5 783 835
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689078
JPS Composite Materials
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3978964-7MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1657797-01
R3978964-8
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1-Chloro-octadecane (S)%59.3 40.0-14057.2
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3978964-9MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1657797-01
R3978964-10
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aromatic (C11-C22)ug/L 1620 96.3 40.0-140108 18.11730ND1560 1870
o-Terphenyl (S)%76.2 40.0-14078.8
2-Fluorobiphenyl (S)%99.5 40.0-140104
2-Bromonaphthalene (S)%98.6 40.0-140104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689078
JPS Composite Materials
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2144707
MA DEP/NJ DEP
MADEP EPH
TPH by Method MADEPE
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92689078002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3982305-1
Associated Lab Samples:92689078002
Matrix: Water
Analyzed
Aromatic (C11-C22)ug/L 63.3J 100 J10/04/23 22:51
o-Terphenyl (S)%50.5 40.0-140 10/04/23 22:51
2-Fluorobiphenyl (S)%70.5 40.0-140 10/04/23 22:51
2-Bromonaphthalene (S)%71.5 40.0-140 10/04/23 22:51
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3982669-3
Associated Lab Samples:92689078002
Matrix: Water
Analyzed
Aliphatic (C09-C18)ug/L 42.6J 100 J10/05/23 12:44
Aliphatic (C19-C36)ug/L 81.3J 100 J10/05/23 12:44
1-Chloro-octadecane (S)%61.7 40.0-140 10/05/23 12:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3982305-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3982305-3
Aromatic (C11-C22)ug/L 10801700 63.5 40.0-14072.41230 13.0 25
o-Terphenyl (S)%60.0 40.0-14067.3
2-Fluorobiphenyl (S)%72.8 40.0-14074.8
2-Bromonaphthalene (S)%71.8 40.0-14074.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3982669-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3982669-2
Aliphatic (C09-C18)ug/L 299 R160049.8 40.0-14069.0414 32.3 25
Aliphatic (C19-C36)ug/L 604 R180075.5 40.0-140100802 28.2 25
1-Chloro-octadecane (S)%61.3 40.0-14081.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3982305-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1658612-04
R3982305-5
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aromatic (C11-C22)ug/L 1680 49.0 40.0-14052.1 5.73168057.7 881 933
o-Terphenyl (S)%57.8 40.0-14058.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
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[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689078
JPS Composite Materials
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3982305-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1658612-04
R3982305-5
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2-Fluorobiphenyl (S)%68.9 40.0-14074.7
2-Bromonaphthalene (S)%67.4 40.0-14074.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3982669-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1658612-04
R3982669-5
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aliphatic (C09-C18)ug/L ML59439.3 40.0-14051.3 23.7594ND264 335
Aliphatic (C19-C36)ug/L 792 57.9 40.0-14069.7 16.579257.3 516 609
1-Chloro-octadecane (S)%59.3 40.0-14068.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689078
JPS Composite Materials
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801641
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689078003, 92689078004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152689
Associated Lab Samples:92689078003, 92689078004
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L <1.7 5.0 09/24/23 13:47
2,2'-Oxybis(1-chloropropane)ug/L <1.2 5.0 09/24/23 13:47
2,4,6-Trichlorophenol ug/L <1.6 10.0 09/24/23 13:47
2,4-Dichlorophenol ug/L <1.4 5.0 09/24/23 13:47
2,4-Dimethylphenol ug/L <1.7 10.0 09/24/23 13:47
2,4-Dinitrophenol ug/L <26.0 50.0 09/24/23 13:47
2,4-Dinitrotoluene ug/L <1.6 5.0 09/24/23 13:47
2,6-Dinitrotoluene ug/L <1.7 5.0 09/24/23 13:47
2-Chloronaphthalene ug/L <1.7 5.0 09/24/23 13:47
2-Chlorophenol ug/L <1.2 5.0 09/24/23 13:47
2-Nitrophenol ug/L <1.4 5.0 09/24/23 13:47
3,3'-Dichlorobenzidine ug/L <8.1 10.0 09/24/23 13:47
4,6-Dinitro-2-methylphenol ug/L <7.8 10.0 09/24/23 13:47
4-Bromophenylphenyl ether ug/L <1.8 5.0 09/24/23 13:47
4-Chloro-3-methylphenol ug/L <3.3 5.0 09/24/23 13:47
4-Chlorophenylphenyl ether ug/L <2.0 5.0 09/24/23 13:47
4-Nitrophenol ug/L <6.6 10.0 09/24/23 13:47
Acenaphthene ug/L <2.0 5.0 09/24/23 13:47
Acenaphthylene ug/L <2.0 5.0 09/24/23 13:47
Anthracene ug/L <2.3 5.0 09/24/23 13:47
Benzo(a)anthracene ug/L <2.7 5.0 09/24/23 13:47
Benzo(a)pyrene ug/L <2.8 5.0 09/24/23 13:47
Benzo(b)fluoranthene ug/L <2.6 5.0 09/24/23 13:47
Benzo(g,h,i)perylene ug/L <2.8 5.0 09/24/23 13:47
Benzo(k)fluoranthene ug/L <2.7 5.0 09/24/23 13:47
bis(2-Chloroethoxy)methane ug/L <1.8 10.0 09/24/23 13:47
bis(2-Chloroethyl) ether ug/L <1.9 5.0 09/24/23 13:47
bis(2-Ethylhexyl)phthalate ug/L <3.7 5.0 09/24/23 13:47
Butylbenzylphthalate ug/L <3.1 5.0 09/24/23 13:47
Chrysene ug/L <2.8 5.0 09/24/23 13:47
Di-n-butylphthalate ug/L <2.2 5.0 09/24/23 13:47
Di-n-octylphthalate ug/L <3.9 5.0 09/24/23 13:47
Dibenz(a,h)anthracene ug/L <3.0 5.0 09/24/23 13:47
Diethylphthalate ug/L <2.0 5.0 09/24/23 13:47
Dimethylphthalate ug/L <2.1 5.0 09/24/23 13:47
Fluoranthene ug/L <2.2 5.0 09/24/23 13:47
Fluorene ug/L <2.1 5.0 09/24/23 13:47
Hexachloro-1,3-butadiene ug/L <1.8 5.0 09/24/23 13:47
Hexachlorobenzene ug/L <2.2 5.0 09/24/23 13:47
Hexachlorocyclopentadiene ug/L <1.6 10.0 09/24/23 13:47
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
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Huntersville, NC 28078
[phone]
Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689078
JPS Composite Materials
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4152689
Associated Lab Samples:92689078003, 92689078004
Matrix: Water
Analyzed
Hexachloroethane ug/L <1.4 5.0 09/24/23 13:47
Indeno(1,2,3-cd)pyrene ug/L <2.9 5.0 09/24/23 13:47
Isophorone ug/L <1.7 10.0 09/24/23 13:47
N-Nitroso-di-n-propylamine ug/L <1.3 5.0 09/24/23 13:47
N-Nitrosodimethylamine ug/L <1.9 5.0 09/24/23 13:47
N-Nitrosodiphenylamine ug/L <3.0 10.0 09/24/23 13:47
Naphthalene ug/L <2.1 5.0 09/24/23 13:47
Nitrobenzene ug/L <1.9 5.0 09/24/23 13:47
Pentachlorophenol ug/L <3.8 10.0 09/24/23 13:47
Phenanthrene ug/L <2.0 5.0 09/24/23 13:47
Phenol ug/L <1.4 5.0 09/24/23 13:47
Pyrene ug/L <2.2 5.0 09/24/23 13:47
2,4,6-Tribromophenol (S)%132 10-137 09/24/23 13:47
2-Fluorobiphenyl (S)%115 15-120 09/24/23 13:47
2-Fluorophenol (S)%82 10-120 09/24/23 13:47
Nitrobenzene-d5 (S)%113 10-120 09/24/23 13:47
Phenol-d6 (S)%59 10-120 09/24/23 13:47
Terphenyl-d14 (S)%131 11-131 09/24/23 13:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152690LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 27.150 54 44-142
2,2'-Oxybis(1-chloropropane)ug/L 29.350 59 36-166
2,4,6-Trichlorophenol ug/L 43.450 87 37-144
2,4-Dichlorophenol ug/L 40.250 80 1-191
2,4-Dimethylphenol ug/L 39.850 80 32-119
2,4-Dinitrophenol ug/L 268250 107 1-181
2,4-Dinitrotoluene ug/L 45.650 91 39-139
2,6-Dinitrotoluene ug/L 44.750 89 50-158
2-Chloronaphthalene ug/L 36.050 72 60-118
2-Chlorophenol ug/L 35.450 71 23-134
2-Nitrophenol ug/L 40.250 80 29-182
3,3'-Dichlorobenzidine ug/L 121100 121 1-262
4,6-Dinitro-2-methylphenol ug/L 114100 114 1-181
4-Bromophenylphenyl ether ug/L 44.250 88 53-127
4-Chloro-3-methylphenol ug/L 78.1100 78 22-147
4-Chlorophenylphenyl ether ug/L 41.350 83 25-158
4-Nitrophenol ug/L 147250 59 1-132
Acenaphthene ug/L 38.050 76 47-145
Acenaphthylene ug/L 38.050 76 33-145
Anthracene ug/L 42.350 85 1-166
Benzo(a)anthracene ug/L 53.150 106 33-143
Benzo(a)pyrene ug/L 53.050 106 17-163
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
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Huntersville, NC 28078
[phone]
Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689078
JPS Composite Materials
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4152690LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 65.050 130 24-159
Benzo(g,h,i)perylene ug/L 51.150 102 1-219
Benzo(k)fluoranthene ug/L 56.750 113 11-162
bis(2-Chloroethoxy)methane ug/L 37.350 75 33-184
bis(2-Chloroethyl) ether ug/L 33.350 67 12-158
bis(2-Ethylhexyl)phthalate ug/L 60.750 121 8-158
Butylbenzylphthalate ug/L 56.850 114 1-152
Chrysene ug/L 49.250 98 17-168
Di-n-butylphthalate ug/L 54.750 109 1-118
Di-n-octylphthalate ug/L 55.650 111 4-146
Dibenz(a,h)anthracene ug/L 50.950 102 1-227
Diethylphthalate ug/L 45.250 90 1-114
Dimethylphthalate ug/L 41.550 83 1-112
Fluoranthene ug/L 45.550 91 26-137
Fluorene ug/L 39.950 80 59-121
Hexachloro-1,3-butadiene ug/L 26.650 53 24-116
Hexachlorobenzene ug/L 43.150 86 1-152
Hexachlorocyclopentadiene ug/L 34.550 69 25-150
Hexachloroethane ug/L 19.850 40 40-113
Indeno(1,2,3-cd)pyrene ug/L 50.150 100 1-171
Isophorone ug/L 37.850 76 21-196
N-Nitroso-di-n-propylamine ug/L 39.150 78 1-230
N-Nitrosodimethylamine ug/L 25.350 51 25-150
N-Nitrosodiphenylamine ug/L 43.650 87 25-150
Naphthalene ug/L 30.050 60 21-133
Nitrobenzene ug/L 34.750 69 35-180
Pentachlorophenol ug/L 113100 113 14-176
Phenanthrene ug/L 41.650 83 54-120
Phenol ug/L 21.850 44 5-112
Pyrene ug/L 50.450 101 52-115
2,4,6-Tribromophenol (S)%134 10-137
2-Fluorobiphenyl (S)%94 15-120
2-Fluorophenol (S)%63 10-120
Nitrobenzene-d5 (S)%94 10-120
Phenol-d6 (S)%53 10-120
Terphenyl-d14 (S)%131 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152691MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92685024002
4152692
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 67 44-14265 3100ND66.9 65.0
2,2'-Oxybis(1-chloropropane) ug/L 100 83 36-16681 3100ND83.0 80.9
2,4,6-Trichlorophenol ug/L 100 104 37-14495 9100ND104 94.5
2,4-Dichlorophenol ug/L 100 89 1-19184 6100ND89.2 83.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689078
JPS Composite Materials
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152691MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92685024002
4152692
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2,4-Dimethylphenol ug/L 100 84 32-11979 7100ND84.1 78.8
2,4-Dinitrophenol ug/L 500 121 1-181107 12500ND605 537
2,4-Dinitrotoluene ug/L 100 109 39-13999 10100ND109 98.6
2,6-Dinitrotoluene ug/L 100 105 50-15895 10100ND105 94.9
2-Chloronaphthalene ug/L 100 79 60-11872 9100ND79.5 72.5
2-Chlorophenol ug/L 100 86 23-13483 4100ND86.2 82.6
2-Nitrophenol ug/L 100 105 29-182103 1100ND105 103
3,3'-Dichlorobenzidine ug/L 200 103 1-26294 10200ND207 187
4,6-Dinitro-2-methylphenol ug/L 200 134 1-181119 12200ND267 238
4-Bromophenylphenyl ether ug/L 100 100 53-12791 9100ND99.6 91.3
4-Chloro-3-methylphenol ug/L 200 85 22-14785 0200ND171 170
4-Chlorophenylphenyl ether ug/L 100 95 25-15888 7100ND94.7 87.9
4-Nitrophenol ug/L 500 61 1-13258 6500ND305 289
Acenaphthene ug/L 100 85 47-14581 4100ND84.6 81.5
Acenaphthylene ug/L 100 84 33-14580 5100ND83.6 79.6
Anthracene ug/L 100 96 1-16687 9100ND95.6 87.2
Benzo(a)anthracene ug/L 100 105 33-14393 12100ND105 92.5
Benzo(a)pyrene ug/L 100 106 17-16397 9100ND106 97.1
Benzo(b)fluoranthene ug/L 100 103 24-15997 6100ND103 96.6
Benzo(g,h,i)perylene ug/L 100 121 1-219112 7100ND121 112
Benzo(k)fluoranthene ug/L 100 100 11-16293 8100ND99.9 92.6
bis(2-Chloroethoxy)methane ug/L 100 86 33-18483 3100ND85.7 83.3
bis(2-Chloroethyl) ether ug/L 100 83 12-15881 3100ND83.1 80.6
bis(2-Ethylhexyl)phthalate ug/L 100 118 8-158106 11100ND118 106
Butylbenzylphthalate ug/L 100 114 1-152100 14100ND114 99.5
Chrysene ug/L 100 102 17-16891 12100ND102 90.6
Di-n-butylphthalate ug/L 100 107 1-11893 14100ND107 93.0
Di-n-octylphthalate ug/L 100 119 4-146105 12100ND119 105
Dibenz(a,h)anthracene ug/L 100 119 1-227110 8100ND119 110
Diethylphthalate ug/L 100 101 1-11492 10100ND101 92.0
Dimethylphthalate ug/L 100 95 1-11286 10100ND94.6 85.9
Fluoranthene ug/L 100 103 26-13792 11100ND103 92.3
Fluorene ug/L 100 92 59-12183 10100ND92.1 83.3
Hexachloro-1,3-butadiene ug/L 100 65 24-11660 7100ND64.8 60.3
Hexachlorobenzene ug/L 100 101 1-15293 9100ND101 92.6
Hexachlorocyclopentadiene ug/L 100 71 25-15065 8100ND70.9 65.1
Hexachloroethane ug/L 100 48 40-11354 11100ND48.5 54.0
Indeno(1,2,3-cd)pyrene ug/L 100 114 1-171104 9100ND114 104
Isophorone ug/L 100 85 21-19682 3100ND84.7 81.9
N-Nitroso-di-n-propylamine ug/L 100 84 1-23081 4100ND84.2 81.2
N-Nitrosodimethylamine ug/L 100 69 25-15068 1100ND68.6 67.8
N-Nitrosodiphenylamine ug/L 100 94 25-15082 13100ND94.3 82.4
Naphthalene ug/L 100 73 21-13371 3100ND72.7 70.8
Nitrobenzene ug/L 100 78 35-18074 6100ND77.9 73.6
Pentachlorophenol ug/L 200 133 14-176116 14200ND266 231
Phenanthrene ug/L 100 97 54-12087 11100ND97.0 86.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
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Huntersville, NC 28078
[phone]
Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689078
JPS Composite Materials
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4152691MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92685024002
4152692
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phenol ug/L 100 51 5-11253 3100ND54.4 56.4
Pyrene ug/L 100 102 52-11590 12100ND102 90.4
2,4,6-Tribromophenol (S)%S016410-137148
2-Fluorobiphenyl (S)%104 15-12095
2-Fluorophenol (S)%77 10-12077
Nitrobenzene-d5 (S)%105 10-12097
Phenol-d6 (S)%60 10-12060
Terphenyl-d14 (S)%116 11-131100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
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Huntersville, NC 28078
[phone]
Page 18 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92689078
JPS Composite Materials
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
An aliquot for analysis was taken from the original container received due to the level of sediment present in the sample.
Rinsing of the original sample container for inclusion in the sample extraction was not performed.G7
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
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Huntersville, NC 28078
[phone]
Page 19 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92689078
JPS Composite Materials
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92689078001 2139497 2139497MW-1 MA DEP/NJ DEP MADEP EPH
92689078002 2144707 2144707MW-1(2)MA DEP/NJ DEP MADEP EPH
92689078003 801641 801657MW-1 EPA 625.1 EPA 625.1
92689078004 801641 801657MW-1(2)EPA 625.1 EPA 625.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/06/2023 03:50 PM
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[phone]
Page 20 of 23
Page 21 of 23
Page 22 of 23
Pa
g
e

2
3

o
f

2
3
#=CL#
September 25, 2023
LIMS USE: FR - ASHLEIGH THRASH
LIMS OBJECT ID: 92689031
92689031
Project:
Pace Project No.:
RE:
Ashleigh Thrash
ATC Group Services, LLC
7606 Whitehall Exceutive
Center Drive Suite 800
Charlotte, NC 28271
199/PS2301
Dear Ashleigh Thrash:
Enclosed are the analytical results for sample(s) received by the laboratory on September 20, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
704-977-0943
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 1 of 27
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92689031
199/PS2301
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 27
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92689031
199/PS2301
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92689031001 SB-1/MW-1 (13-15)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031002 SB-2 (13-15)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031003 SB-3 (13-15)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031004 SB-4 (14-15)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031005 SB-5 (14-15)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031006 SB-6 (14-15)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031007 SB-7 (14-15)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031008 SB-8 (15-17)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031009 SB-9 (15-16)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031010 SB-10 (15-16)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031011 SB-11 (15-17)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031012 SB-12 (15-17)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031013 SB-13 (14-16)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
92689031014 SB-14 (15-16)EPA 8015C 2 PASI-CHH
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-1/MW-1 (13-15)Lab ID: 92689031001 Collected: 09/18/23 11:05 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)8.7 mg/kg 09/22/23 19:0309/22/23 12:546.8 1
Surrogates
n-Pentacosane (S)78 %09/22/23 19:03 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.8 %09/20/23 18:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-2 (13-15)Lab ID: 92689031002 Collected: 09/18/23 12:05 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)<4.7 mg/kg 09/22/23 19:1909/22/23 12:546.6 1
Surrogates
n-Pentacosane (S)75 %09/22/23 19:19 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.4 %09/20/23 18:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-3 (13-15)Lab ID: 92689031003 Collected: 09/18/23 12:20 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)<4.7 mg/kg 09/22/23 19:1909/22/23 12:546.6 1
Surrogates
n-Pentacosane (S)138 %09/22/23 19:19 629-99-2 S309/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.6 %09/20/23 18:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-4 (14-15)Lab ID: 92689031004 Collected: 09/18/23 12:30 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)6.8 mg/kg 09/22/23 19:3509/22/23 12:546.2 1
Surrogates
n-Pentacosane (S)65 %09/22/23 19:35 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.7 %09/20/23 18:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-5 (14-15)Lab ID: 92689031005 Collected: 09/18/23 12:35 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)40.2 mg/kg 09/22/23 19:3509/22/23 12:546.4 1
Surrogates
n-Pentacosane (S)69 %09/22/23 19:35 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.2 %09/20/23 18:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-6 (14-15)Lab ID: 92689031006 Collected: 09/18/23 14:35 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)10.0 mg/kg 09/22/23 19:5109/22/23 12:546.3 1
Surrogates
n-Pentacosane (S)73 %09/22/23 19:51 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.9 %09/21/23 15:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-7 (14-15)Lab ID: 92689031007 Collected: 09/18/23 14:40 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)12.7 mg/kg 09/22/23 19:5109/22/23 12:545.3 1
Surrogates
n-Pentacosane (S)91 %09/22/23 19:51 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 5.3 %09/21/23 15:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-8 (15-17)Lab ID: 92689031008 Collected: 09/18/23 14:45 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)<4.6 mg/kg 09/22/23 20:0609/22/23 12:546.5 1
Surrogates
n-Pentacosane (S)83 %09/22/23 20:06 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.1 %09/21/23 15:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-9 (15-16)Lab ID: 92689031009 Collected: 09/18/23 15:00 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)4.7J mg/kg 09/22/23 20:0609/22/23 12:546.6 1
Surrogates
n-Pentacosane (S)88 %09/22/23 20:06 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.8 %09/21/23 15:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-10 (15-16)Lab ID: 92689031010 Collected: 09/18/23 15:35 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)<4.6 mg/kg 09/22/23 20:2209/22/23 12:546.5 1
Surrogates
n-Pentacosane (S)81 %09/22/23 20:22 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.3 %09/21/23 15:21 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-11 (15-17)Lab ID: 92689031011 Collected: 09/18/23 16:00 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)<4.6 mg/kg 09/22/23 20:2209/22/23 12:546.5 1
Surrogates
n-Pentacosane (S)98 %09/22/23 20:22 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.3 %09/21/23 15:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-12 (15-17)Lab ID: 92689031012 Collected: 09/18/23 16:10 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)33.4 mg/kg 09/22/23 20:3709/22/23 12:546.0 1
Surrogates
n-Pentacosane (S)72 %09/22/23 20:37 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.4 %09/21/23 15:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-13 (14-16)Lab ID: 92689031013 Collected: 09/18/23 16:20 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)<4.5 mg/kg 09/22/23 20:3709/22/23 12:546.4 1
Surrogates
n-Pentacosane (S)100 %09/22/23 20:37 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.9 %09/21/23 15:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 27
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92689031
199/PS2301
Sample: SB-14 (15-16)Lab ID: 92689031014 Collected: 09/18/23 16:30 Received: 09/20/23 12:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)<4.7 mg/kg 09/22/23 20:5309/22/23 12:546.6 1
Surrogates
n-Pentacosane (S)83 %09/22/23 20:53 629-99-209/22/23 12:5410-133 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.5 %09/21/23 15:22 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689031
199/PS2301
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801401
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92689031001, 92689031002, 92689031003, 92689031004, 92689031005, 92689031006, 92689031007,
92689031008, 92689031009, 92689031010, 92689031011, 92689031012, 92689031013, 92689031014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4151033
Associated Lab Samples: 92689031001, 92689031002, 92689031003, 92689031004, 92689031005, 92689031006, 92689031007,
92689031008, 92689031009, 92689031010, 92689031011, 92689031012, 92689031013, 92689031014
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg <3.5 5.0 09/22/23 18:17
n-Pentacosane (S)%69 10-133 09/22/23 18:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4151034LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 62.266 94 43-130
n-Pentacosane (S)%83 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4151035MATRIX SPIKE SAMPLE:
MSSpike
Result
92689390002
Diesel Range Organics(C10-C28)mg/kg 76.265.8 101 15-13010.1
n-Pentacosane (S)%84 10-133
Parameter Units
Dup
Result QualifiersRPDResult
92689390004
4151036SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 9.5 1310.9
n-Pentacosane (S)%81131
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689031
199/PS2301
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
800952
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92689031001, 92689031002, 92689031003, 92689031004, 92689031005
Parameter Units
Dup
Result QualifiersRPDResult
92689008022
4148855SAMPLE DUPLICATE:
Percent Moisture %15.1 N2414.5
Parameter Units
Dup
Result QualifiersRPDResult
92688780034
4148856SAMPLE DUPLICATE:
Percent Moisture %20.7 N2321.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 27
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92689031
199/PS2301
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
801203
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92689031006, 92689031007, 92689031008, 92689031009, 92689031010, 92689031011, 92689031012,
92689031013, 92689031014
Parameter Units
Dup
Result QualifiersRPDResult
92686333001
4150135SAMPLE DUPLICATE:
Percent Moisture %20.3 N2120.5
Parameter Units
Dup
Result QualifiersRPDResult
92689194002
4150145SAMPLE DUPLICATE:
Percent Moisture %83.3 N2083.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 27
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92689031
199/PS2301
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 27
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92689031
199/PS2301
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92689031001 801401 801516SB-1/MW-1 (13-15)EPA 3546 EPA 8015C
92689031002 801401 801516SB-2 (13-15)EPA 3546 EPA 8015C
92689031003 801401 801516SB-3 (13-15)EPA 3546 EPA 8015C
92689031004 801401 801516SB-4 (14-15)EPA 3546 EPA 8015C
92689031005 801401 801516SB-5 (14-15)EPA 3546 EPA 8015C
92689031006 801401 801516SB-6 (14-15)EPA 3546 EPA 8015C
92689031007 801401 801516SB-7 (14-15)EPA 3546 EPA 8015C
92689031008 801401 801516SB-8 (15-17)EPA 3546 EPA 8015C
92689031009 801401 801516SB-9 (15-16)EPA 3546 EPA 8015C
92689031010 801401 801516SB-10 (15-16)EPA 3546 EPA 8015C
92689031011 801401 801516SB-11 (15-17)EPA 3546 EPA 8015C
92689031012 801401 801516SB-12 (15-17)EPA 3546 EPA 8015C
92689031013 801401 801516SB-13 (14-16)EPA 3546 EPA 8015C
92689031014 801401 801516SB-14 (15-16)EPA 3546 EPA 8015C
92689031001 800952SB-1/MW-1 (13-15)SW-846
92689031002 800952SB-2 (13-15)SW-846
92689031003 800952SB-3 (13-15)SW-846
92689031004 800952SB-4 (14-15)SW-846
92689031005 800952SB-5 (14-15)SW-846
92689031006 801203SB-6 (14-15)SW-846
92689031007 801203SB-7 (14-15)SW-846
92689031008 801203SB-8 (15-17)SW-846
92689031009 801203SB-9 (15-16)SW-846
92689031010 801203SB-10 (15-16)SW-846
92689031011 801203SB-11 (15-17)SW-846
92689031012 801203SB-12 (15-17)SW-846
92689031013 801203SB-13 (14-16)SW-846
92689031014 801203SB-14 (15-16)SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/25/2023 12:01 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 27
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