MO-30225_49270_CA_IAR_20231030_721 Andrews Street

REPORT OF ENVIRONMENTAL SERVICES

721 ANDREWS STREET
EAST SPENCER, ROWAN COUNTY, NORTH CAROLINA

PREPARED FOR:
WAKE HAMILTON
721 ANDREWS INDUSTRIAL OWNER, LLC
101 SOUTH KINGS DRIVE, SUITE 200
CHARLOTTE, NORTH CAROLINA 28204

PREPARED BY:
PILOT GEOLOGICAL, PLLC
PO BOX 128
KERNERSVILLE, NORTH CAROLINA 27285

OCTOBER 30, 2023
PILOT PROJECT G-10220

REPORT OF ENVIRONMENTAL SERVICES
721 ANDREWS STREET
EAST SPENCER, ROWAN COUNTY, NORTH CAROLINA

1.0 BACKGROUND INFORMATION .................................................................... 1
2.0 FIELD ACTIVITIES ........................................................................................ 1
2.1 Soil Sampling ............................................................................................ 1
3.0 RESULTS .................................................................................................... 2
3.1 Soil Sample ............................................................................................... 2
4.0 CONCLUSIONS AND RECOMMENDATIONS .................................................. 2
5.0 QUALIFICATIONS OF REPORT ...................................................................... 3

DRAWINGS
Drawing 1 USGS Topographic Map
Drawing 2 Site Map
Drawing 3 UST Areas Map
Drawing 4 Sample Location Map A
Drawing 5 Sample Location Map B

TABLE
Table 1 Summary of Soil Analytical Results

APPENDIX
Tank Disposal Manifest
Non-Hazardous Waste Manifest
Material Manifest
Laboratory Data Sheets and Chain of Custody

Report of Environmental Services
Pilot Project G-10220
October 30, 2023
Page 1

1.0 BACKGROUND INFORMATION

The site is located at 721 Andrews Street in East Spencer, Rowan County, North Carolina (Drawings
1 and 2). The site is a former residential property that is currently being redeveloped for commercial
use. One apparent 550-gallon heating oil underground storage tank (UST) and one apparent 550-
gallon gasoline UST were identified at the site.

Pilot was requested to provide UST removal services at the site. Project information is based on
conversations between Mr. Joe Kozlowski with Ironhead Construction Company, Mr. Eric
McManus with D.H. Griffin Wrecking Company, Inc. (D.H. Griffin) and Mr. Jason Ricks of Pilot.

2.0 FIELD ACTIVITIES

On October 16, 2023, one approximate 550-gallon heating oil UST and one approximate 550-
gallon gasoline UST were removed from the site by D.H. Griffin and observed by Pilot (Drawings 3
through 5). Based on observations and photoionization detector (PID) readings, an apparent
release occurred from the heating oil UST. Approximately 11.95 tons of soil was excavated from
the vicinity of the 550-gallon heating oil UST and transported to Carolina Composting of
Wadesboro, North Carolina in an effort to remediate the release. Approximately 20 gallons of
liquid were evacuated from the gasoline UST and 246 gallons were evacuated from the heating
oil UST using a vacuum truck prior to removal. Following completion of UST removal activities, the
excavations were backfilled with the overburden and surrounding soils and the USTs were
transported off-site for disposal. The USTs were located approximately 2 feet below ground surface
(bgs). Both the heating oil and the gasoline USTs were measured to be approximately 93 inches long
by 42 inches in diameter. The tank disposal manifest, Non-Hazardous Waste Manifest (impacted
soil) and Material Manifest (liquids) is included in the Appendix.

2.1 Soil Sampling

Following removal of the heating oil UST, two soil samples (S-1 and S-2, Drawing 4) were collected
from beneath both ends of the UST at an approximate depth of 7 feet bgs. Subsequently,
approximately 11.95 tons of soil was excavated from the vicinity of the UST based on an apparent
release. The impacted soil excavation measured approximately 15 foot long by 12 foot wide by
7 feet deep. Soil samples SS-1, ES-1, NS-1 and WS-1 were collected from the sidewalls and soil
sample B-1 was collected from the base of the excavation. The sidewall soil samples were
collected at a depth of approximately 8 feet bgs, while soil sample B-1 was collected at an
approximate depth of 11 feet bgs.

Following the removal of the gasoline UST, one soil sample (S-3, Drawing 5) was collected from
the approximate mid-point of the UST. This soil sample was collected at an approximate depth
of 7 feet bgs using the bucket of the excavator.

Report of Environmental Services
Pilot Project G-10220
October 30, 2023
Page 2

Pilot personnel wore a new pair of disposable nitrile gloves during the sampling process. Each
container was labeled and placed in a cooler containing ice to maintain the samples at
approximately 4 Celsius. The soil sample was transported to Pace Analytical (Pace) in
Kernersville, North Carolina for analysis. Soil samples S-1, S-2 and S-3 were analyzed for gasoline
and diesel range total petroleum hydrocarbons (TPH) using EPA Methods 8015/5035 and
8015/3550, respectively. The over-excavation soil samples SS-1, ES-1, NS-1, WS-1 and B-1 were
analyzed for volatile organic compounds (VOCs) using EPA Method 8260, for semi-volatile organic
compounds (SVOCs) using EPA Method 8270BNA, for volatile and extractable petroleum
hydrocarbons (VPH and EPH) using the Massachusetts Department of Environmental Protection
(MADEP) Methods. A chain of custody was maintained for the samples and is included in the
Appendix.

3.0 RESULTS
3.1 Soil Sample

Laboratory analysis of soil samples S-1, S-3, NS-1, ES-1, SS-1 and B-1 did not detect targeted
compounds above laboratory quantitation limits. Laboratory analysis of soil sample S-2 detected
diesel range TPH at a concentration above its North Carolina Action Level of 100 mg/Kg.
Laboratory analysis of soil sample WS-1 detected targeted compounds below their respective
Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs). A summary of the soil
analytical results is presented in Table 1. The laboratory data sheets are included in the
Appendix.

4.0 CONCLUSIONS AND RECOMMENDATIONS

Based on the results of the laboratory analysis, Pilot concludes the following:

One approximate 550-gallon heating oil UST and one approximate 550-gallon gasoline UST were
removed from the site on October 16, 2023. An apparent minor release occurred from the
heating oil UST. Approximately 11.95 tons of impacted soil were removed in an effort to
remediate the release.

Laboratory analysis of soil samples S-1, S-3, NS-1, ES-1, SS-1 and B-1 did not detect targeted
compounds above laboratory quantitation limits. Laboratory analysis of soil sample S-2 detected
diesel range TPH at a concentration above its North Carolina Action Level of 100 mg/Kg.
Laboratory analysis of soil sample WS-1 detected targeted compounds below their respective
Soil-to-Groundwater MSCCs.

Based on the release from the former heating oil UST, Pilot recommends that a copy of this report
be submitted to the North Carolina Department of Environmental Quality (NCDEQ). Based on
laboratory analysis of the over-excavation samples, it appears that the release of heating oil
should qualify for closure from the NCDEQ.

Report of Environmental Services
Pilot Project G-10220
October 30, 2023
Page 3

5.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those
normally employed in assessment projects of this type. Our evaluation of site conditions has
been based on our understanding of the project information and the data obtained during our
field activities. This report was prepared for the exclusive use of 721 Andrews Industrial Owner,
LLC, Ironhead Construction Company and D.H. Griffin.

DRAWINGS

Drawing 1 USGS Topographic Map
Drawing 2 Site Map
Drawing 3 UST Areas Map
Drawing 4 Sample Location Map A
Drawing 5 Sample Location Map B

USGS Topographic Map
721 Andrew Street
East Spencer, Rowan County, NC
Pilot Project G-10220
Drawing 1
USGS Topographic Map
Salisbury, NC Quadrangle
Scale: 1” = 2,000’
LEGEND
Site Boundary
Site Map
721 Andrew Street
East Spencer, Rowan County, NC
Pilot Project G-10220
Drawing 3
Google Earth
Interactive Mapping Software
Scale : 1”= 160’
LEGEND
Site Boundary
See Drawing 3
UST Areas Map
721 Andrew Street
East Spencer, Rowan County, NC
Pilot Project G-10220
Drawing 3
Google Earth
Interactive Mapping Software
Scale : 1”= 160’
LEGEND
Site Boundary
See Drawing 4
See Drawing 5
Sample Location Map A
721 Andrew Street
East Spencer, Rowan County, NC
Pilot Project G-10220
Drawing 4
Google Earth
Interactive Mapping Software
Scale : 1”= 10’
LEGEND
Site Boundary
Approximate Soil Sample Location
Former Heating Oil UST
Approximate Extent of
Impacted Soil Excavation
S-2
S-1
WS-1
SS-1 NS-1
ES-1
B-1
Sample Location Map B
721 Andrew Street
East Spencer, Rowan County, NC
Pilot Project G-10220
Drawing 5
Google Earth
Interactive Mapping Software
Scale : 1”= 50’
LEGEND
Site Boundary
Approximate Soil Sample Location
Former Gasoline UST
S-3

TABLE

Table 1 Summary of Soil Analytical Results

5035 3550 8270
Sample ID Approximate Sample Depth (ft.
bgs)Sample Collection Date GR
O
DR
O
Et
h
y
l
e
n
z
e
n
e
St
y
r
e
n
e
To
t
a
l

X
y
l
e
n
e
s
Ta
r
g
e
t
e
d

C
o
m
p
o
u
n
d
s
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
2
2

A
r
o
m
a
t
i
c
s
C
1
9
-
C
-
3
6

A
l
i
p
h
a
t
i
c
S-1 7 10/16/2023 ND ND NA NA NA NA NA NA NA NA
S-2 7 10/16/2023 ND 192 NA NA NA NA NA NA NA NA
S-3 7 10/16/2023 ND ND NA NA NA NA NA NA NA NA
NS-1 8 10/16/2023 NA NA ND ND ND ND ND ND ND ND
ES-1 8 10/16/2023 NA NA ND ND ND ND ND ND ND ND
SS-1 8 10/16/2023 NA NA ND ND ND ND ND ND ND ND
WS-1 8 10/16/2023 NA NA 0.015 0.011 0.072 ND ND ND ND ND
B-1 11 10/16/2023 NA NA ND ND ND ND ND ND ND ND
50 100 N/A N/A N/A N/A N/A N/A N/A N/A
N/A N/A 8 0.9 6 N/A 68 540 31 #
N/A N/A 297 46,700 46,700 N/A 9,340 23,300 7,000 467,000
= Soil Sample Above the NC Action Level
mg/Kg = Milligrams per Kilogram (analogous to parts per million)
BGS = Below Ground Surface
N/A = Not Applicable
MSCC = Maximum Soil Contaminant Concentration
NA = Not Analyzed
Industrial/Commercial Soil Cleanup Levels (mg/Kg)
Analytical Method
NC Action Level (mg/Kg)
Standards
Table 1 - Summary of Soil Analytical Results
721 Andrews Street
East Spencer, North Carolina
8260 VPH & EPH
Soil-to-Groundwater MSCC (mg/Kg)

APPENDIX

Tank Disposal Manifest
Non-Hazardous Waste Manifest
Material Manifest
Laboratory Data Sheets and Chain of Custody Document
#=CL#
October 27, 2023
LIMS USE: FR - JASON RICKS
LIMS OBJECT ID: 92693430
92693430
Project:
Pace Project No.:
RE:
Jason Ricks
Pilot Geological
P.O. Box 128
Kernersville, NC 27285
Spencer G-10220
Dear Jason Ricks:
Enclosed are the analytical results for sample(s) received by the laboratory on October 16, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
704-977-0981
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 80
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92693430
Spencer G-10220
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 80
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92693430
Spencer G-10220
Lab ID Sample ID Matrix Date Collected Date Received
92693430001 SS-1 Solid 10/16/23 10:10 10/16/23 12:38
92693430002 ES-1 Solid 10/16/23 10:14 10/16/23 12:38
92693430003 NS-1 Solid 10/16/23 10:16 10/16/23 12:38
92693430004 WS-1 Solid 10/16/23 10:18 10/16/23 12:38
92693430005 B-1 Solid 10/16/23 10:05 10/16/23 12:38
92693430006 S-1 Solid 10/16/23 11:10 10/16/23 12:38
92693430007 S-2 Solid 10/16/23 11:15 10/16/23 12:38
92693430008 S-3 Solid 10/16/23 11:30 10/16/23 12:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 3 of 80
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92693430
Spencer G-10220
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92693430001 SS-1 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92693430002 ES-1 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92693430003 NS-1 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92693430004 WS-1 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92693430005 B-1 EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92693430006 S-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92693430007 S-2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92693430008 S-3 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 4 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:SS-1 Lab ID:92693430001 Collected:10/16/23 10:10 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/25/23 00:43 83-32-910/24/23 17:140.42 1
Acenaphthylene ND mg/kg 10/25/23 00:43 208-96-810/24/23 17:140.42 1
Aniline ND mg/kg 10/25/23 00:43 62-53-310/24/23 17:140.42 1
Anthracene ND mg/kg 10/25/23 00:43 120-12-710/24/23 17:140.42 1
Benzo(a)anthracene ND mg/kg 10/25/23 00:43 56-55-310/24/23 17:140.42 1
Benzo(a)pyrene ND mg/kg 10/25/23 00:43 50-32-810/24/23 17:140.42 1
Benzo(b)fluoranthene ND mg/kg 10/25/23 00:43 205-99-210/24/23 17:140.42 1
Benzo(g,h,i)perylene ND mg/kg 10/25/23 00:43 191-24-210/24/23 17:140.42 1
Benzo(k)fluoranthene ND mg/kg 10/25/23 00:43 207-08-910/24/23 17:140.42 1
Benzoic Acid ND mg/kg 10/25/23 00:43 65-85-010/24/23 17:142.1 1
Benzyl alcohol ND mg/kg 10/25/23 00:43 100-51-610/24/23 17:140.84 1
4-Bromophenylphenyl ether ND mg/kg 10/25/23 00:43 101-55-310/24/23 17:140.42 1
Butylbenzylphthalate ND mg/kg 10/25/23 00:43 85-68-710/24/23 17:140.42 1
4-Chloro-3-methylphenol ND mg/kg 10/25/23 00:43 59-50-710/24/23 17:140.84 1
4-Chloroaniline ND mg/kg 10/25/23 00:43 106-47-810/24/23 17:140.84 1
bis(2-Chloroethoxy)methane ND mg/kg 10/25/23 00:43 111-91-110/24/23 17:140.42 1
bis(2-Chloroethyl) ether ND mg/kg 10/25/23 00:43 111-44-410/24/23 17:140.42 1
2-Chloronaphthalene ND mg/kg 10/25/23 00:43 91-58-710/24/23 17:140.42 1
2-Chlorophenol ND mg/kg 10/25/23 00:43 95-57-810/24/23 17:140.42 1
4-Chlorophenylphenyl ether ND mg/kg 10/25/23 00:43 7005-72-310/24/23 17:140.42 1
Chrysene ND mg/kg 10/25/23 00:43 218-01-910/24/23 17:140.42 1
Dibenz(a,h)anthracene ND mg/kg 10/25/23 00:43 53-70-310/24/23 17:140.42 1
Dibenzofuran ND mg/kg 10/25/23 00:43 132-64-910/24/23 17:140.42 1
1,2-Dichlorobenzene ND mg/kg 10/25/23 00:43 95-50-110/24/23 17:140.42 1
1,3-Dichlorobenzene ND mg/kg 10/25/23 00:43 541-73-110/24/23 17:140.42 1
1,4-Dichlorobenzene ND mg/kg 10/25/23 00:43 106-46-710/24/23 17:140.42 1
3,3'-Dichlorobenzidine ND mg/kg 10/25/23 00:43 91-94-1 L210/24/23 17:140.84 1
2,4-Dichlorophenol ND mg/kg 10/25/23 00:43 120-83-210/24/23 17:140.42 1
Diethylphthalate ND mg/kg 10/25/23 00:43 84-66-210/24/23 17:140.42 1
2,4-Dimethylphenol ND mg/kg 10/25/23 00:43 105-67-910/24/23 17:140.42 1
Dimethylphthalate ND mg/kg 10/25/23 00:43 131-11-310/24/23 17:140.42 1
Di-n-butylphthalate ND mg/kg 10/25/23 00:43 84-74-210/24/23 17:140.42 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/25/23 00:43 534-52-110/24/23 17:140.84 1
2,4-Dinitrophenol ND mg/kg 10/25/23 00:43 51-28-510/24/23 17:142.1 1
2,4-Dinitrotoluene ND mg/kg 10/25/23 00:43 121-14-210/24/23 17:140.42 1
2,6-Dinitrotoluene ND mg/kg 10/25/23 00:43 606-20-210/24/23 17:140.42 1
Di-n-octylphthalate ND mg/kg 10/25/23 00:43 117-84-010/24/23 17:140.42 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/25/23 00:43 117-81-710/24/23 17:140.42 1
Fluoranthene ND mg/kg 10/25/23 00:43 206-44-010/24/23 17:140.42 1
Fluorene ND mg/kg 10/25/23 00:43 86-73-710/24/23 17:140.42 1
Hexachloro-1,3-butadiene ND mg/kg 10/25/23 00:43 87-68-310/24/23 17:140.42 1
Hexachlorobenzene ND mg/kg 10/25/23 00:43 118-74-110/24/23 17:140.42 1
Hexachlorocyclopentadiene ND mg/kg 10/25/23 00:43 77-47-410/24/23 17:140.42 1
Hexachloroethane ND mg/kg 10/25/23 00:43 67-72-110/24/23 17:140.42 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/25/23 00:43 193-39-510/24/23 17:140.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 5 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:SS-1 Lab ID:92693430001 Collected:10/16/23 10:10 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND mg/kg 10/25/23 00:43 78-59-110/24/23 17:140.42 1
1-Methylnaphthalene ND mg/kg 10/25/23 00:43 90-12-010/24/23 17:140.42 1
2-Methylnaphthalene ND mg/kg 10/25/23 00:43 91-57-610/24/23 17:140.42 1
2-Methylphenol(o-Cresol)ND mg/kg 10/25/23 00:43 95-48-710/24/23 17:140.42 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/25/23 00:43 15831-10-410/24/23 17:140.42 1
Naphthalene ND mg/kg 10/25/23 00:43 91-20-310/24/23 17:140.42 1
2-Nitroaniline ND mg/kg 10/25/23 00:43 88-74-410/24/23 17:142.1 1
3-Nitroaniline ND mg/kg 10/25/23 00:43 99-09-210/24/23 17:142.1 1
4-Nitroaniline ND mg/kg 10/25/23 00:43 100-01-610/24/23 17:140.84 1
Nitrobenzene ND mg/kg 10/25/23 00:43 98-95-310/24/23 17:140.42 1
2-Nitrophenol ND mg/kg 10/25/23 00:43 88-75-510/24/23 17:140.42 1
4-Nitrophenol ND mg/kg 10/25/23 00:43 100-02-710/24/23 17:142.1 1
N-Nitrosodimethylamine ND mg/kg 10/25/23 00:43 62-75-910/24/23 17:140.42 1
N-Nitroso-di-n-propylamine ND mg/kg 10/25/23 00:43 621-64-710/24/23 17:140.42 1
N-Nitrosodiphenylamine ND mg/kg 10/25/23 00:43 86-30-610/24/23 17:140.42 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 10/25/23 00:43 108-60-110/24/23 17:140.42 1
Pentachlorophenol ND mg/kg 10/25/23 00:43 87-86-510/24/23 17:140.84 1
Phenanthrene ND mg/kg 10/25/23 00:43 85-01-810/24/23 17:140.42 1
Phenol ND mg/kg 10/25/23 00:43 108-95-2 v110/24/23 17:140.42 1
Pyrene ND mg/kg 10/25/23 00:43 129-00-010/24/23 17:140.42 1
Pyridine ND mg/kg 10/25/23 00:43 110-86-110/24/23 17:140.42 1
1,2,4-Trichlorobenzene ND mg/kg 10/25/23 00:43 120-82-110/24/23 17:140.42 1
2,4,5-Trichlorophenol ND mg/kg 10/25/23 00:43 95-95-410/24/23 17:140.42 1
2,4,6-Trichlorophenol ND mg/kg 10/25/23 00:43 88-06-210/24/23 17:140.42 1
Surrogates
Nitrobenzene-d5 (S)55 %10/25/23 00:43 4165-60-010/24/23 17:1410-130 1
2-Fluorobiphenyl (S)51 %10/25/23 00:43 321-60-810/24/23 17:1410-130 1
Terphenyl-d14 (S)63 %10/25/23 00:43 1718-51-010/24/23 17:1410-130 1
Phenol-d6 (S)55 %10/25/23 00:43 13127-88-310/24/23 17:1410-130 1
2-Fluorophenol (S)55 %10/25/23 00:43 367-12-410/24/23 17:1410-130 1
2,4,6-Tribromophenol (S)48 %10/25/23 00:43 118-79-610/24/23 17:1410-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/17/23 23:16 67-64-110/17/23 16:310.14 1
Benzene ND mg/kg 10/17/23 23:16 71-43-210/17/23 16:310.0069 1
Bromobenzene ND mg/kg 10/17/23 23:16 108-86-110/17/23 16:310.0069 1
Bromochloromethane ND mg/kg 10/17/23 23:16 74-97-510/17/23 16:310.0069 1
Bromodichloromethane ND mg/kg 10/17/23 23:16 75-27-410/17/23 16:310.0069 1
Bromoform ND mg/kg 10/17/23 23:16 75-25-210/17/23 16:310.0069 1
Bromomethane ND mg/kg 10/17/23 23:16 74-83-9 IH,IK,M110/17/23 16:310.028 1
2-Butanone (MEK)ND mg/kg 10/17/23 23:16 78-93-310/17/23 16:310.14 1
n-Butylbenzene ND mg/kg 10/17/23 23:16 104-51-810/17/23 16:310.0069 1
sec-Butylbenzene ND mg/kg 10/17/23 23:16 135-98-810/17/23 16:310.0069 1
tert-Butylbenzene ND mg/kg 10/17/23 23:16 98-06-610/17/23 16:310.0069 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 6 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:SS-1 Lab ID:92693430001 Collected:10/16/23 10:10 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND mg/kg 10/17/23 23:16 56-23-510/17/23 16:310.0069 1
Chlorobenzene ND mg/kg 10/17/23 23:16 108-90-710/17/23 16:310.0069 1
Chloroethane ND mg/kg 10/17/23 23:16 75-00-3 M110/17/23 16:310.014 1
Chloroform ND mg/kg 10/17/23 23:16 67-66-310/17/23 16:310.0069 1
Chloromethane ND mg/kg 10/17/23 23:16 74-87-310/17/23 16:310.014 1
2-Chlorotoluene ND mg/kg 10/17/23 23:16 95-49-810/17/23 16:310.0069 1
4-Chlorotoluene ND mg/kg 10/17/23 23:16 106-43-410/17/23 16:310.0069 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/17/23 23:16 96-12-810/17/23 16:310.0069 1
Dibromochloromethane ND mg/kg 10/17/23 23:16 124-48-110/17/23 16:310.0069 1
1,2-Dibromoethane (EDB)ND mg/kg 10/17/23 23:16 106-93-410/17/23 16:310.0069 1
Dibromomethane ND mg/kg 10/17/23 23:16 74-95-3 M110/17/23 16:310.0069 1
1,2-Dichlorobenzene ND mg/kg 10/17/23 23:16 95-50-110/17/23 16:310.0069 1
1,3-Dichlorobenzene ND mg/kg 10/17/23 23:16 541-73-110/17/23 16:310.0069 1
1,4-Dichlorobenzene ND mg/kg 10/17/23 23:16 106-46-710/17/23 16:310.0069 1
Dichlorodifluoromethane ND mg/kg 10/17/23 23:16 75-71-8 IH10/17/23 16:310.014 1
1,1-Dichloroethane ND mg/kg 10/17/23 23:16 75-34-310/17/23 16:310.0069 1
1,2-Dichloroethane ND mg/kg 10/17/23 23:16 107-06-210/17/23 16:310.0069 1
1,1-Dichloroethene ND mg/kg 10/17/23 23:16 75-35-410/17/23 16:310.0069 1
cis-1,2-Dichloroethene ND mg/kg 10/17/23 23:16 156-59-210/17/23 16:310.0069 1
trans-1,2-Dichloroethene ND mg/kg 10/17/23 23:16 156-60-510/17/23 16:310.0069 1
1,2-Dichloropropane ND mg/kg 10/17/23 23:16 78-87-510/17/23 16:310.0069 1
1,3-Dichloropropane ND mg/kg 10/17/23 23:16 142-28-910/17/23 16:310.0069 1
2,2-Dichloropropane ND mg/kg 10/17/23 23:16 594-20-710/17/23 16:310.0069 1
1,1-Dichloropropene ND mg/kg 10/17/23 23:16 563-58-610/17/23 16:310.0069 1
cis-1,3-Dichloropropene ND mg/kg 10/17/23 23:16 10061-01-510/17/23 16:310.0069 1
trans-1,3-Dichloropropene ND mg/kg 10/17/23 23:16 10061-02-610/17/23 16:310.0069 1
Diisopropyl ether ND mg/kg 10/17/23 23:16 108-20-310/17/23 16:310.0069 1
Ethylbenzene ND mg/kg 10/17/23 23:16 100-41-410/17/23 16:310.0069 1
Hexachloro-1,3-butadiene ND mg/kg 10/17/23 23:16 87-68-310/17/23 16:310.014 1
2-Hexanone ND mg/kg 10/17/23 23:16 591-78-610/17/23 16:310.069 1
Isopropylbenzene (Cumene)ND mg/kg 10/17/23 23:16 98-82-810/17/23 16:310.0069 1
p-Isopropyltoluene ND mg/kg 10/17/23 23:16 99-87-610/17/23 16:310.0069 1
Methylene Chloride ND mg/kg 10/17/23 23:16 75-09-210/17/23 16:310.028 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/17/23 23:16 108-10-110/17/23 16:310.069 1
Methyl-tert-butyl ether ND mg/kg 10/17/23 23:16 1634-04-410/17/23 16:310.0069 1
Naphthalene ND mg/kg 10/17/23 23:16 91-20-310/17/23 16:310.0069 1
n-Propylbenzene ND mg/kg 10/17/23 23:16 103-65-110/17/23 16:310.0069 1
Styrene ND mg/kg 10/17/23 23:16 100-42-510/17/23 16:310.0069 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/17/23 23:16 630-20-610/17/23 16:310.0069 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/17/23 23:16 79-34-510/17/23 16:310.0069 1
Tetrachloroethene ND mg/kg 10/17/23 23:16 127-18-410/17/23 16:310.0069 1
Toluene ND mg/kg 10/17/23 23:16 108-88-310/17/23 16:310.0069 1
1,2,3-Trichlorobenzene ND mg/kg 10/17/23 23:16 87-61-610/17/23 16:310.0069 1
1,2,4-Trichlorobenzene ND mg/kg 10/17/23 23:16 120-82-110/17/23 16:310.0069 1
1,1,1-Trichloroethane ND mg/kg 10/17/23 23:16 71-55-610/17/23 16:310.0069 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 7 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:SS-1 Lab ID:92693430001 Collected:10/16/23 10:10 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND mg/kg 10/17/23 23:16 79-00-510/17/23 16:310.0069 1
Trichloroethene ND mg/kg 10/17/23 23:16 79-01-610/17/23 16:310.0069 1
Trichlorofluoromethane ND mg/kg 10/17/23 23:16 75-69-4 M110/17/23 16:310.0069 1
1,2,3-Trichloropropane ND mg/kg 10/17/23 23:16 96-18-410/17/23 16:310.0069 1
1,2,4-Trimethylbenzene ND mg/kg 10/17/23 23:16 95-63-610/17/23 16:310.0069 1
1,3,5-Trimethylbenzene ND mg/kg 10/17/23 23:16 108-67-810/17/23 16:310.0069 1
Vinyl acetate ND mg/kg 10/17/23 23:16 108-05-410/17/23 16:310.069 1
Vinyl chloride ND mg/kg 10/17/23 23:16 75-01-410/17/23 16:310.014 1
Xylene (Total)ND mg/kg 10/17/23 23:16 1330-20-710/17/23 16:310.014 1
m&p-Xylene ND mg/kg 10/17/23 23:16 179601-23-110/17/23 16:310.014 1
o-Xylene ND mg/kg 10/17/23 23:16 95-47-610/17/23 16:310.0069 1
Surrogates
Toluene-d8 (S)103 %10/17/23 23:16 2037-26-510/17/23 16:3170-130 1
4-Bromofluorobenzene (S)104 %10/17/23 23:16 460-00-410/17/23 16:3170-130 1
1,2-Dichloroethane-d4 (S)102 %10/17/23 23:16 17060-07-010/17/23 16:3170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.4 %10/17/23 18:08 N20.10 1
Sample:ES-1 Lab ID:92693430002 Collected:10/16/23 10:14 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/25/23 01:33 83-32-910/24/23 17:140.42 1
Acenaphthylene ND mg/kg 10/25/23 01:33 208-96-810/24/23 17:140.42 1
Aniline ND mg/kg 10/25/23 01:33 62-53-310/24/23 17:140.42 1
Anthracene ND mg/kg 10/25/23 01:33 120-12-710/24/23 17:140.42 1
Benzo(a)anthracene ND mg/kg 10/25/23 01:33 56-55-310/24/23 17:140.42 1
Benzo(a)pyrene ND mg/kg 10/25/23 01:33 50-32-810/24/23 17:140.42 1
Benzo(b)fluoranthene ND mg/kg 10/25/23 01:33 205-99-210/24/23 17:140.42 1
Benzo(g,h,i)perylene ND mg/kg 10/25/23 01:33 191-24-210/24/23 17:140.42 1
Benzo(k)fluoranthene ND mg/kg 10/25/23 01:33 207-08-910/24/23 17:140.42 1
Benzoic Acid ND mg/kg 10/25/23 01:33 65-85-010/24/23 17:142.1 1
Benzyl alcohol ND mg/kg 10/25/23 01:33 100-51-610/24/23 17:140.83 1
4-Bromophenylphenyl ether ND mg/kg 10/25/23 01:33 101-55-310/24/23 17:140.42 1
Butylbenzylphthalate ND mg/kg 10/25/23 01:33 85-68-710/24/23 17:140.42 1
4-Chloro-3-methylphenol ND mg/kg 10/25/23 01:33 59-50-710/24/23 17:140.83 1
4-Chloroaniline ND mg/kg 10/25/23 01:33 106-47-810/24/23 17:140.83 1
bis(2-Chloroethoxy)methane ND mg/kg 10/25/23 01:33 111-91-110/24/23 17:140.42 1
bis(2-Chloroethyl) ether ND mg/kg 10/25/23 01:33 111-44-410/24/23 17:140.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 8 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:ES-1 Lab ID:92693430002 Collected:10/16/23 10:14 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2-Chloronaphthalene ND mg/kg 10/25/23 01:33 91-58-710/24/23 17:140.42 1
2-Chlorophenol ND mg/kg 10/25/23 01:33 95-57-810/24/23 17:140.42 1
4-Chlorophenylphenyl ether ND mg/kg 10/25/23 01:33 7005-72-310/24/23 17:140.42 1
Chrysene ND mg/kg 10/25/23 01:33 218-01-910/24/23 17:140.42 1
Dibenz(a,h)anthracene ND mg/kg 10/25/23 01:33 53-70-310/24/23 17:140.42 1
Dibenzofuran ND mg/kg 10/25/23 01:33 132-64-910/24/23 17:140.42 1
1,2-Dichlorobenzene ND mg/kg 10/25/23 01:33 95-50-110/24/23 17:140.42 1
1,3-Dichlorobenzene ND mg/kg 10/25/23 01:33 541-73-110/24/23 17:140.42 1
1,4-Dichlorobenzene ND mg/kg 10/25/23 01:33 106-46-710/24/23 17:140.42 1
3,3'-Dichlorobenzidine ND mg/kg 10/25/23 01:33 91-94-1 L210/24/23 17:140.83 1
2,4-Dichlorophenol ND mg/kg 10/25/23 01:33 120-83-210/24/23 17:140.42 1
Diethylphthalate ND mg/kg 10/25/23 01:33 84-66-210/24/23 17:140.42 1
2,4-Dimethylphenol ND mg/kg 10/25/23 01:33 105-67-910/24/23 17:140.42 1
Dimethylphthalate ND mg/kg 10/25/23 01:33 131-11-310/24/23 17:140.42 1
Di-n-butylphthalate ND mg/kg 10/25/23 01:33 84-74-210/24/23 17:140.42 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/25/23 01:33 534-52-110/24/23 17:140.83 1
2,4-Dinitrophenol ND mg/kg 10/25/23 01:33 51-28-510/24/23 17:142.1 1
2,4-Dinitrotoluene ND mg/kg 10/25/23 01:33 121-14-210/24/23 17:140.42 1
2,6-Dinitrotoluene ND mg/kg 10/25/23 01:33 606-20-210/24/23 17:140.42 1
Di-n-octylphthalate ND mg/kg 10/25/23 01:33 117-84-010/24/23 17:140.42 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/25/23 01:33 117-81-710/24/23 17:140.42 1
Fluoranthene ND mg/kg 10/25/23 01:33 206-44-010/24/23 17:140.42 1
Fluorene ND mg/kg 10/25/23 01:33 86-73-710/24/23 17:140.42 1
Hexachloro-1,3-butadiene ND mg/kg 10/25/23 01:33 87-68-310/24/23 17:140.42 1
Hexachlorobenzene ND mg/kg 10/25/23 01:33 118-74-110/24/23 17:140.42 1
Hexachlorocyclopentadiene ND mg/kg 10/25/23 01:33 77-47-410/24/23 17:140.42 1
Hexachloroethane ND mg/kg 10/25/23 01:33 67-72-110/24/23 17:140.42 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/25/23 01:33 193-39-510/24/23 17:140.42 1
Isophorone ND mg/kg 10/25/23 01:33 78-59-110/24/23 17:140.42 1
1-Methylnaphthalene ND mg/kg 10/25/23 01:33 90-12-010/24/23 17:140.42 1
2-Methylnaphthalene ND mg/kg 10/25/23 01:33 91-57-610/24/23 17:140.42 1
2-Methylphenol(o-Cresol)ND mg/kg 10/25/23 01:33 95-48-710/24/23 17:140.42 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/25/23 01:33 15831-10-410/24/23 17:140.42 1
Naphthalene ND mg/kg 10/25/23 01:33 91-20-310/24/23 17:140.42 1
2-Nitroaniline ND mg/kg 10/25/23 01:33 88-74-410/24/23 17:142.1 1
3-Nitroaniline ND mg/kg 10/25/23 01:33 99-09-210/24/23 17:142.1 1
4-Nitroaniline ND mg/kg 10/25/23 01:33 100-01-610/24/23 17:140.83 1
Nitrobenzene ND mg/kg 10/25/23 01:33 98-95-310/24/23 17:140.42 1
2-Nitrophenol ND mg/kg 10/25/23 01:33 88-75-510/24/23 17:140.42 1
4-Nitrophenol ND mg/kg 10/25/23 01:33 100-02-710/24/23 17:142.1 1
N-Nitrosodimethylamine ND mg/kg 10/25/23 01:33 62-75-910/24/23 17:140.42 1
N-Nitroso-di-n-propylamine ND mg/kg 10/25/23 01:33 621-64-710/24/23 17:140.42 1
N-Nitrosodiphenylamine ND mg/kg 10/25/23 01:33 86-30-610/24/23 17:140.42 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 10/25/23 01:33 108-60-110/24/23 17:140.42 1
Pentachlorophenol ND mg/kg 10/25/23 01:33 87-86-510/24/23 17:140.83 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 9 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:ES-1 Lab ID:92693430002 Collected:10/16/23 10:14 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Phenanthrene ND mg/kg 10/25/23 01:33 85-01-810/24/23 17:140.42 1
Phenol ND mg/kg 10/25/23 01:33 108-95-2 v110/24/23 17:140.42 1
Pyrene ND mg/kg 10/25/23 01:33 129-00-010/24/23 17:140.42 1
Pyridine ND mg/kg 10/25/23 01:33 110-86-110/24/23 17:140.42 1
1,2,4-Trichlorobenzene ND mg/kg 10/25/23 01:33 120-82-110/24/23 17:140.42 1
2,4,5-Trichlorophenol ND mg/kg 10/25/23 01:33 95-95-410/24/23 17:140.42 1
2,4,6-Trichlorophenol ND mg/kg 10/25/23 01:33 88-06-210/24/23 17:140.42 1
Surrogates
Nitrobenzene-d5 (S)48 %10/25/23 01:33 4165-60-010/24/23 17:1410-130 1
2-Fluorobiphenyl (S)43 %10/25/23 01:33 321-60-810/24/23 17:1410-130 1
Terphenyl-d14 (S)58 %10/25/23 01:33 1718-51-010/24/23 17:1410-130 1
Phenol-d6 (S)49 %10/25/23 01:33 13127-88-310/24/23 17:1410-130 1
2-Fluorophenol (S)48 %10/25/23 01:33 367-12-410/24/23 17:1410-130 1
2,4,6-Tribromophenol (S)40 %10/25/23 01:33 118-79-610/24/23 17:1410-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/17/23 23:34 67-64-110/17/23 16:310.15 1
Benzene ND mg/kg 10/17/23 23:34 71-43-210/17/23 16:310.0076 1
Bromobenzene ND mg/kg 10/17/23 23:34 108-86-110/17/23 16:310.0076 1
Bromochloromethane ND mg/kg 10/17/23 23:34 74-97-510/17/23 16:310.0076 1
Bromodichloromethane ND mg/kg 10/17/23 23:34 75-27-410/17/23 16:310.0076 1
Bromoform ND mg/kg 10/17/23 23:34 75-25-210/17/23 16:310.0076 1
Bromomethane ND mg/kg 10/17/23 23:34 74-83-9 IH,IK10/17/23 16:310.031 1
2-Butanone (MEK)ND mg/kg 10/17/23 23:34 78-93-310/17/23 16:310.15 1
n-Butylbenzene ND mg/kg 10/17/23 23:34 104-51-810/17/23 16:310.0076 1
sec-Butylbenzene ND mg/kg 10/17/23 23:34 135-98-810/17/23 16:310.0076 1
tert-Butylbenzene ND mg/kg 10/17/23 23:34 98-06-610/17/23 16:310.0076 1
Carbon tetrachloride ND mg/kg 10/17/23 23:34 56-23-510/17/23 16:310.0076 1
Chlorobenzene ND mg/kg 10/17/23 23:34 108-90-710/17/23 16:310.0076 1
Chloroethane ND mg/kg 10/17/23 23:34 75-00-310/17/23 16:310.015 1
Chloroform ND mg/kg 10/17/23 23:34 67-66-310/17/23 16:310.0076 1
Chloromethane ND mg/kg 10/17/23 23:34 74-87-310/17/23 16:310.015 1
2-Chlorotoluene ND mg/kg 10/17/23 23:34 95-49-810/17/23 16:310.0076 1
4-Chlorotoluene ND mg/kg 10/17/23 23:34 106-43-410/17/23 16:310.0076 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/17/23 23:34 96-12-810/17/23 16:310.0076 1
Dibromochloromethane ND mg/kg 10/17/23 23:34 124-48-110/17/23 16:310.0076 1
1,2-Dibromoethane (EDB)ND mg/kg 10/17/23 23:34 106-93-410/17/23 16:310.0076 1
Dibromomethane ND mg/kg 10/17/23 23:34 74-95-310/17/23 16:310.0076 1
1,2-Dichlorobenzene ND mg/kg 10/17/23 23:34 95-50-110/17/23 16:310.0076 1
1,3-Dichlorobenzene ND mg/kg 10/17/23 23:34 541-73-110/17/23 16:310.0076 1
1,4-Dichlorobenzene ND mg/kg 10/17/23 23:34 106-46-710/17/23 16:310.0076 1
Dichlorodifluoromethane ND mg/kg 10/17/23 23:34 75-71-8 IH10/17/23 16:310.015 1
1,1-Dichloroethane ND mg/kg 10/17/23 23:34 75-34-310/17/23 16:310.0076 1
1,2-Dichloroethane ND mg/kg 10/17/23 23:34 107-06-210/17/23 16:310.0076 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 10 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:ES-1 Lab ID:92693430002 Collected:10/16/23 10:14 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloroethene ND mg/kg 10/17/23 23:34 75-35-410/17/23 16:310.0076 1
cis-1,2-Dichloroethene ND mg/kg 10/17/23 23:34 156-59-210/17/23 16:310.0076 1
trans-1,2-Dichloroethene ND mg/kg 10/17/23 23:34 156-60-510/17/23 16:310.0076 1
1,2-Dichloropropane ND mg/kg 10/17/23 23:34 78-87-510/17/23 16:310.0076 1
1,3-Dichloropropane ND mg/kg 10/17/23 23:34 142-28-910/17/23 16:310.0076 1
2,2-Dichloropropane ND mg/kg 10/17/23 23:34 594-20-710/17/23 16:310.0076 1
1,1-Dichloropropene ND mg/kg 10/17/23 23:34 563-58-610/17/23 16:310.0076 1
cis-1,3-Dichloropropene ND mg/kg 10/17/23 23:34 10061-01-510/17/23 16:310.0076 1
trans-1,3-Dichloropropene ND mg/kg 10/17/23 23:34 10061-02-610/17/23 16:310.0076 1
Diisopropyl ether ND mg/kg 10/17/23 23:34 108-20-310/17/23 16:310.0076 1
Ethylbenzene ND mg/kg 10/17/23 23:34 100-41-410/17/23 16:310.0076 1
Hexachloro-1,3-butadiene ND mg/kg 10/17/23 23:34 87-68-310/17/23 16:310.015 1
2-Hexanone ND mg/kg 10/17/23 23:34 591-78-610/17/23 16:310.076 1
Isopropylbenzene (Cumene)ND mg/kg 10/17/23 23:34 98-82-810/17/23 16:310.0076 1
p-Isopropyltoluene ND mg/kg 10/17/23 23:34 99-87-610/17/23 16:310.0076 1
Methylene Chloride ND mg/kg 10/17/23 23:34 75-09-210/17/23 16:310.031 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/17/23 23:34 108-10-110/17/23 16:310.076 1
Methyl-tert-butyl ether ND mg/kg 10/17/23 23:34 1634-04-410/17/23 16:310.0076 1
Naphthalene ND mg/kg 10/17/23 23:34 91-20-310/17/23 16:310.0076 1
n-Propylbenzene ND mg/kg 10/17/23 23:34 103-65-110/17/23 16:310.0076 1
Styrene ND mg/kg 10/17/23 23:34 100-42-510/17/23 16:310.0076 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/17/23 23:34 630-20-610/17/23 16:310.0076 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/17/23 23:34 79-34-510/17/23 16:310.0076 1
Tetrachloroethene ND mg/kg 10/17/23 23:34 127-18-410/17/23 16:310.0076 1
Toluene ND mg/kg 10/17/23 23:34 108-88-310/17/23 16:310.0076 1
1,2,3-Trichlorobenzene ND mg/kg 10/17/23 23:34 87-61-610/17/23 16:310.0076 1
1,2,4-Trichlorobenzene ND mg/kg 10/17/23 23:34 120-82-110/17/23 16:310.0076 1
1,1,1-Trichloroethane ND mg/kg 10/17/23 23:34 71-55-610/17/23 16:310.0076 1
1,1,2-Trichloroethane ND mg/kg 10/17/23 23:34 79-00-510/17/23 16:310.0076 1
Trichloroethene ND mg/kg 10/17/23 23:34 79-01-610/17/23 16:310.0076 1
Trichlorofluoromethane ND mg/kg 10/17/23 23:34 75-69-410/17/23 16:310.0076 1
1,2,3-Trichloropropane ND mg/kg 10/17/23 23:34 96-18-410/17/23 16:310.0076 1
1,2,4-Trimethylbenzene ND mg/kg 10/17/23 23:34 95-63-610/17/23 16:310.0076 1
1,3,5-Trimethylbenzene ND mg/kg 10/17/23 23:34 108-67-810/17/23 16:310.0076 1
Vinyl acetate ND mg/kg 10/17/23 23:34 108-05-410/17/23 16:310.076 1
Vinyl chloride ND mg/kg 10/17/23 23:34 75-01-410/17/23 16:310.015 1
Xylene (Total)ND mg/kg 10/17/23 23:34 1330-20-710/17/23 16:310.015 1
m&p-Xylene ND mg/kg 10/17/23 23:34 179601-23-110/17/23 16:310.015 1
o-Xylene ND mg/kg 10/17/23 23:34 95-47-610/17/23 16:310.0076 1
Surrogates
Toluene-d8 (S)101 %10/17/23 23:34 2037-26-510/17/23 16:3170-130 1
4-Bromofluorobenzene (S)101 %10/17/23 23:34 460-00-410/17/23 16:3170-130 1
1,2-Dichloroethane-d4 (S)100 %10/17/23 23:34 17060-07-010/17/23 16:3170-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 11 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:ES-1 Lab ID:92693430002 Collected:10/16/23 10:14 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.7 %10/17/23 18:08 N20.10 1
Sample:NS-1 Lab ID:92693430003 Collected:10/16/23 10:16 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/25/23 02:24 83-32-910/24/23 17:140.45 1
Acenaphthylene ND mg/kg 10/25/23 02:24 208-96-810/24/23 17:140.45 1
Aniline ND mg/kg 10/25/23 02:24 62-53-310/24/23 17:140.45 1
Anthracene ND mg/kg 10/25/23 02:24 120-12-710/24/23 17:140.45 1
Benzo(a)anthracene ND mg/kg 10/25/23 02:24 56-55-310/24/23 17:140.45 1
Benzo(a)pyrene ND mg/kg 10/25/23 02:24 50-32-810/24/23 17:140.45 1
Benzo(b)fluoranthene ND mg/kg 10/25/23 02:24 205-99-210/24/23 17:140.45 1
Benzo(g,h,i)perylene ND mg/kg 10/25/23 02:24 191-24-210/24/23 17:140.45 1
Benzo(k)fluoranthene ND mg/kg 10/25/23 02:24 207-08-910/24/23 17:140.45 1
Benzoic Acid ND mg/kg 10/25/23 02:24 65-85-010/24/23 17:142.3 1
Benzyl alcohol ND mg/kg 10/25/23 02:24 100-51-610/24/23 17:140.90 1
4-Bromophenylphenyl ether ND mg/kg 10/25/23 02:24 101-55-310/24/23 17:140.45 1
Butylbenzylphthalate ND mg/kg 10/25/23 02:24 85-68-710/24/23 17:140.45 1
4-Chloro-3-methylphenol ND mg/kg 10/25/23 02:24 59-50-710/24/23 17:140.90 1
4-Chloroaniline ND mg/kg 10/25/23 02:24 106-47-810/24/23 17:140.90 1
bis(2-Chloroethoxy)methane ND mg/kg 10/25/23 02:24 111-91-110/24/23 17:140.45 1
bis(2-Chloroethyl) ether ND mg/kg 10/25/23 02:24 111-44-410/24/23 17:140.45 1
2-Chloronaphthalene ND mg/kg 10/25/23 02:24 91-58-710/24/23 17:140.45 1
2-Chlorophenol ND mg/kg 10/25/23 02:24 95-57-810/24/23 17:140.45 1
4-Chlorophenylphenyl ether ND mg/kg 10/25/23 02:24 7005-72-310/24/23 17:140.45 1
Chrysene ND mg/kg 10/25/23 02:24 218-01-910/24/23 17:140.45 1
Dibenz(a,h)anthracene ND mg/kg 10/25/23 02:24 53-70-310/24/23 17:140.45 1
Dibenzofuran ND mg/kg 10/25/23 02:24 132-64-910/24/23 17:140.45 1
1,2-Dichlorobenzene ND mg/kg 10/25/23 02:24 95-50-110/24/23 17:140.45 1
1,3-Dichlorobenzene ND mg/kg 10/25/23 02:24 541-73-110/24/23 17:140.45 1
1,4-Dichlorobenzene ND mg/kg 10/25/23 02:24 106-46-710/24/23 17:140.45 1
3,3'-Dichlorobenzidine ND mg/kg 10/25/23 02:24 91-94-1 L210/24/23 17:140.90 1
2,4-Dichlorophenol ND mg/kg 10/25/23 02:24 120-83-210/24/23 17:140.45 1
Diethylphthalate ND mg/kg 10/25/23 02:24 84-66-210/24/23 17:140.45 1
2,4-Dimethylphenol ND mg/kg 10/25/23 02:24 105-67-910/24/23 17:140.45 1
Dimethylphthalate ND mg/kg 10/25/23 02:24 131-11-310/24/23 17:140.45 1
Di-n-butylphthalate ND mg/kg 10/25/23 02:24 84-74-210/24/23 17:140.45 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/25/23 02:24 534-52-110/24/23 17:140.90 1
2,4-Dinitrophenol ND mg/kg 10/25/23 02:24 51-28-510/24/23 17:142.3 1
2,4-Dinitrotoluene ND mg/kg 10/25/23 02:24 121-14-210/24/23 17:140.45 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 12 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:NS-1 Lab ID:92693430003 Collected:10/16/23 10:16 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,6-Dinitrotoluene ND mg/kg 10/25/23 02:24 606-20-210/24/23 17:140.45 1
Di-n-octylphthalate ND mg/kg 10/25/23 02:24 117-84-010/24/23 17:140.45 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/25/23 02:24 117-81-710/24/23 17:140.45 1
Fluoranthene ND mg/kg 10/25/23 02:24 206-44-010/24/23 17:140.45 1
Fluorene ND mg/kg 10/25/23 02:24 86-73-710/24/23 17:140.45 1
Hexachloro-1,3-butadiene ND mg/kg 10/25/23 02:24 87-68-310/24/23 17:140.45 1
Hexachlorobenzene ND mg/kg 10/25/23 02:24 118-74-110/24/23 17:140.45 1
Hexachlorocyclopentadiene ND mg/kg 10/25/23 02:24 77-47-410/24/23 17:140.45 1
Hexachloroethane ND mg/kg 10/25/23 02:24 67-72-110/24/23 17:140.45 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/25/23 02:24 193-39-510/24/23 17:140.45 1
Isophorone ND mg/kg 10/25/23 02:24 78-59-110/24/23 17:140.45 1
1-Methylnaphthalene ND mg/kg 10/25/23 02:24 90-12-010/24/23 17:140.45 1
2-Methylnaphthalene ND mg/kg 10/25/23 02:24 91-57-610/24/23 17:140.45 1
2-Methylphenol(o-Cresol)ND mg/kg 10/25/23 02:24 95-48-710/24/23 17:140.45 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/25/23 02:24 15831-10-410/24/23 17:140.45 1
Naphthalene ND mg/kg 10/25/23 02:24 91-20-310/24/23 17:140.45 1
2-Nitroaniline ND mg/kg 10/25/23 02:24 88-74-410/24/23 17:142.3 1
3-Nitroaniline ND mg/kg 10/25/23 02:24 99-09-210/24/23 17:142.3 1
4-Nitroaniline ND mg/kg 10/25/23 02:24 100-01-610/24/23 17:140.90 1
Nitrobenzene ND mg/kg 10/25/23 02:24 98-95-310/24/23 17:140.45 1
2-Nitrophenol ND mg/kg 10/25/23 02:24 88-75-510/24/23 17:140.45 1
4-Nitrophenol ND mg/kg 10/25/23 02:24 100-02-710/24/23 17:142.3 1
N-Nitrosodimethylamine ND mg/kg 10/25/23 02:24 62-75-910/24/23 17:140.45 1
N-Nitroso-di-n-propylamine ND mg/kg 10/25/23 02:24 621-64-710/24/23 17:140.45 1
N-Nitrosodiphenylamine ND mg/kg 10/25/23 02:24 86-30-610/24/23 17:140.45 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 10/25/23 02:24 108-60-110/24/23 17:140.45 1
Pentachlorophenol ND mg/kg 10/25/23 02:24 87-86-510/24/23 17:140.90 1
Phenanthrene ND mg/kg 10/25/23 02:24 85-01-810/24/23 17:140.45 1
Phenol ND mg/kg 10/25/23 02:24 108-95-2 v110/24/23 17:140.45 1
Pyrene ND mg/kg 10/25/23 02:24 129-00-010/24/23 17:140.45 1
Pyridine ND mg/kg 10/25/23 02:24 110-86-110/24/23 17:140.45 1
1,2,4-Trichlorobenzene ND mg/kg 10/25/23 02:24 120-82-110/24/23 17:140.45 1
2,4,5-Trichlorophenol ND mg/kg 10/25/23 02:24 95-95-410/24/23 17:140.45 1
2,4,6-Trichlorophenol ND mg/kg 10/25/23 02:24 88-06-210/24/23 17:140.45 1
Surrogates
Nitrobenzene-d5 (S)62 %10/25/23 02:24 4165-60-010/24/23 17:1410-130 1
2-Fluorobiphenyl (S)57 %10/25/23 02:24 321-60-810/24/23 17:1410-130 1
Terphenyl-d14 (S)72 %10/25/23 02:24 1718-51-010/24/23 17:1410-130 1
Phenol-d6 (S)55 %10/25/23 02:24 13127-88-310/24/23 17:1410-130 1
2-Fluorophenol (S)54 %10/25/23 02:24 367-12-410/24/23 17:1410-130 1
2,4,6-Tribromophenol (S)46 %10/25/23 02:24 118-79-610/24/23 17:1410-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/18/23 00:11 67-64-110/17/23 16:310.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 13 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:NS-1 Lab ID:92693430003 Collected:10/16/23 10:16 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Benzene ND mg/kg 10/18/23 00:11 71-43-210/17/23 16:310.0064 1
Bromobenzene ND mg/kg 10/18/23 00:11 108-86-110/17/23 16:310.0064 1
Bromochloromethane ND mg/kg 10/18/23 00:11 74-97-510/17/23 16:310.0064 1
Bromodichloromethane ND mg/kg 10/18/23 00:11 75-27-410/17/23 16:310.0064 1
Bromoform ND mg/kg 10/18/23 00:11 75-25-210/17/23 16:310.0064 1
Bromomethane ND mg/kg 10/18/23 00:11 74-83-9 IH,IK10/17/23 16:310.026 1
2-Butanone (MEK)ND mg/kg 10/18/23 00:11 78-93-310/17/23 16:310.13 1
n-Butylbenzene ND mg/kg 10/18/23 00:11 104-51-810/17/23 16:310.0064 1
sec-Butylbenzene ND mg/kg 10/18/23 00:11 135-98-810/17/23 16:310.0064 1
tert-Butylbenzene ND mg/kg 10/18/23 00:11 98-06-610/17/23 16:310.0064 1
Carbon tetrachloride ND mg/kg 10/18/23 00:11 56-23-510/17/23 16:310.0064 1
Chlorobenzene ND mg/kg 10/18/23 00:11 108-90-710/17/23 16:310.0064 1
Chloroethane ND mg/kg 10/18/23 00:11 75-00-310/17/23 16:310.013 1
Chloroform ND mg/kg 10/18/23 00:11 67-66-310/17/23 16:310.0064 1
Chloromethane ND mg/kg 10/18/23 00:11 74-87-310/17/23 16:310.013 1
2-Chlorotoluene ND mg/kg 10/18/23 00:11 95-49-810/17/23 16:310.0064 1
4-Chlorotoluene ND mg/kg 10/18/23 00:11 106-43-410/17/23 16:310.0064 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/18/23 00:11 96-12-810/17/23 16:310.0064 1
Dibromochloromethane ND mg/kg 10/18/23 00:11 124-48-110/17/23 16:310.0064 1
1,2-Dibromoethane (EDB)ND mg/kg 10/18/23 00:11 106-93-410/17/23 16:310.0064 1
Dibromomethane ND mg/kg 10/18/23 00:11 74-95-310/17/23 16:310.0064 1
1,2-Dichlorobenzene ND mg/kg 10/18/23 00:11 95-50-110/17/23 16:310.0064 1
1,3-Dichlorobenzene ND mg/kg 10/18/23 00:11 541-73-110/17/23 16:310.0064 1
1,4-Dichlorobenzene ND mg/kg 10/18/23 00:11 106-46-710/17/23 16:310.0064 1
Dichlorodifluoromethane ND mg/kg 10/18/23 00:11 75-71-8 IH10/17/23 16:310.013 1
1,1-Dichloroethane ND mg/kg 10/18/23 00:11 75-34-310/17/23 16:310.0064 1
1,2-Dichloroethane ND mg/kg 10/18/23 00:11 107-06-210/17/23 16:310.0064 1
1,1-Dichloroethene ND mg/kg 10/18/23 00:11 75-35-410/17/23 16:310.0064 1
cis-1,2-Dichloroethene ND mg/kg 10/18/23 00:11 156-59-210/17/23 16:310.0064 1
trans-1,2-Dichloroethene ND mg/kg 10/18/23 00:11 156-60-510/17/23 16:310.0064 1
1,2-Dichloropropane ND mg/kg 10/18/23 00:11 78-87-510/17/23 16:310.0064 1
1,3-Dichloropropane ND mg/kg 10/18/23 00:11 142-28-910/17/23 16:310.0064 1
2,2-Dichloropropane ND mg/kg 10/18/23 00:11 594-20-710/17/23 16:310.0064 1
1,1-Dichloropropene ND mg/kg 10/18/23 00:11 563-58-610/17/23 16:310.0064 1
cis-1,3-Dichloropropene ND mg/kg 10/18/23 00:11 10061-01-510/17/23 16:310.0064 1
trans-1,3-Dichloropropene ND mg/kg 10/18/23 00:11 10061-02-610/17/23 16:310.0064 1
Diisopropyl ether ND mg/kg 10/18/23 00:11 108-20-310/17/23 16:310.0064 1
Ethylbenzene ND mg/kg 10/18/23 00:11 100-41-410/17/23 16:310.0064 1
Hexachloro-1,3-butadiene ND mg/kg 10/18/23 00:11 87-68-310/17/23 16:310.013 1
2-Hexanone ND mg/kg 10/18/23 00:11 591-78-610/17/23 16:310.064 1
Isopropylbenzene (Cumene)ND mg/kg 10/18/23 00:11 98-82-810/17/23 16:310.0064 1
p-Isopropyltoluene ND mg/kg 10/18/23 00:11 99-87-610/17/23 16:310.0064 1
Methylene Chloride ND mg/kg 10/18/23 00:11 75-09-210/17/23 16:310.026 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/18/23 00:11 108-10-110/17/23 16:310.064 1
Methyl-tert-butyl ether ND mg/kg 10/18/23 00:11 1634-04-410/17/23 16:310.0064 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 14 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:NS-1 Lab ID:92693430003 Collected:10/16/23 10:16 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Naphthalene ND mg/kg 10/18/23 00:11 91-20-310/17/23 16:310.0064 1
n-Propylbenzene ND mg/kg 10/18/23 00:11 103-65-110/17/23 16:310.0064 1
Styrene ND mg/kg 10/18/23 00:11 100-42-510/17/23 16:310.0064 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/18/23 00:11 630-20-610/17/23 16:310.0064 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/18/23 00:11 79-34-510/17/23 16:310.0064 1
Tetrachloroethene ND mg/kg 10/18/23 00:11 127-18-410/17/23 16:310.0064 1
Toluene ND mg/kg 10/18/23 00:11 108-88-310/17/23 16:310.0064 1
1,2,3-Trichlorobenzene ND mg/kg 10/18/23 00:11 87-61-610/17/23 16:310.0064 1
1,2,4-Trichlorobenzene ND mg/kg 10/18/23 00:11 120-82-110/17/23 16:310.0064 1
1,1,1-Trichloroethane ND mg/kg 10/18/23 00:11 71-55-610/17/23 16:310.0064 1
1,1,2-Trichloroethane ND mg/kg 10/18/23 00:11 79-00-510/17/23 16:310.0064 1
Trichloroethene ND mg/kg 10/18/23 00:11 79-01-610/17/23 16:310.0064 1
Trichlorofluoromethane ND mg/kg 10/18/23 00:11 75-69-410/17/23 16:310.0064 1
1,2,3-Trichloropropane ND mg/kg 10/18/23 00:11 96-18-410/17/23 16:310.0064 1
1,2,4-Trimethylbenzene ND mg/kg 10/18/23 00:11 95-63-610/17/23 16:310.0064 1
1,3,5-Trimethylbenzene ND mg/kg 10/18/23 00:11 108-67-810/17/23 16:310.0064 1
Vinyl acetate ND mg/kg 10/18/23 00:11 108-05-410/17/23 16:310.064 1
Vinyl chloride ND mg/kg 10/18/23 00:11 75-01-410/17/23 16:310.013 1
Xylene (Total)ND mg/kg 10/18/23 00:11 1330-20-710/17/23 16:310.013 1
m&p-Xylene ND mg/kg 10/18/23 00:11 179601-23-110/17/23 16:310.013 1
o-Xylene ND mg/kg 10/18/23 00:11 95-47-610/17/23 16:310.0064 1
Surrogates
Toluene-d8 (S)102 %10/18/23 00:11 2037-26-510/17/23 16:3170-130 1
4-Bromofluorobenzene (S)101 %10/18/23 00:11 460-00-410/17/23 16:3170-130 1
1,2-Dichloroethane-d4 (S)99 %10/18/23 00:11 17060-07-010/17/23 16:3170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.7 %10/17/23 18:08 N20.10 1
Sample:WS-1 Lab ID:92693430004 Collected:10/16/23 10:18 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/25/23 02:49 83-32-910/24/23 17:140.43 1
Acenaphthylene ND mg/kg 10/25/23 02:49 208-96-810/24/23 17:140.43 1
Aniline ND mg/kg 10/25/23 02:49 62-53-310/24/23 17:140.43 1
Anthracene ND mg/kg 10/25/23 02:49 120-12-710/24/23 17:140.43 1
Benzo(a)anthracene ND mg/kg 10/25/23 02:49 56-55-310/24/23 17:140.43 1
Benzo(a)pyrene ND mg/kg 10/25/23 02:49 50-32-810/24/23 17:140.43 1
Benzo(b)fluoranthene ND mg/kg 10/25/23 02:49 205-99-210/24/23 17:140.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 15 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:WS-1 Lab ID:92693430004 Collected:10/16/23 10:18 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Benzo(g,h,i)perylene ND mg/kg 10/25/23 02:49 191-24-210/24/23 17:140.43 1
Benzo(k)fluoranthene ND mg/kg 10/25/23 02:49 207-08-910/24/23 17:140.43 1
Benzoic Acid ND mg/kg 10/25/23 02:49 65-85-010/24/23 17:142.2 1
Benzyl alcohol ND mg/kg 10/25/23 02:49 100-51-610/24/23 17:140.86 1
4-Bromophenylphenyl ether ND mg/kg 10/25/23 02:49 101-55-310/24/23 17:140.43 1
Butylbenzylphthalate ND mg/kg 10/25/23 02:49 85-68-710/24/23 17:140.43 1
4-Chloro-3-methylphenol ND mg/kg 10/25/23 02:49 59-50-710/24/23 17:140.86 1
4-Chloroaniline ND mg/kg 10/25/23 02:49 106-47-810/24/23 17:140.86 1
bis(2-Chloroethoxy)methane ND mg/kg 10/25/23 02:49 111-91-110/24/23 17:140.43 1
bis(2-Chloroethyl) ether ND mg/kg 10/25/23 02:49 111-44-410/24/23 17:140.43 1
2-Chloronaphthalene ND mg/kg 10/25/23 02:49 91-58-710/24/23 17:140.43 1
2-Chlorophenol ND mg/kg 10/25/23 02:49 95-57-810/24/23 17:140.43 1
4-Chlorophenylphenyl ether ND mg/kg 10/25/23 02:49 7005-72-310/24/23 17:140.43 1
Chrysene ND mg/kg 10/25/23 02:49 218-01-910/24/23 17:140.43 1
Dibenz(a,h)anthracene ND mg/kg 10/25/23 02:49 53-70-310/24/23 17:140.43 1
Dibenzofuran ND mg/kg 10/25/23 02:49 132-64-910/24/23 17:140.43 1
1,2-Dichlorobenzene ND mg/kg 10/25/23 02:49 95-50-110/24/23 17:140.43 1
1,3-Dichlorobenzene ND mg/kg 10/25/23 02:49 541-73-110/24/23 17:140.43 1
1,4-Dichlorobenzene ND mg/kg 10/25/23 02:49 106-46-710/24/23 17:140.43 1
3,3'-Dichlorobenzidine ND mg/kg 10/25/23 02:49 91-94-1 L210/24/23 17:140.86 1
2,4-Dichlorophenol ND mg/kg 10/25/23 02:49 120-83-210/24/23 17:140.43 1
Diethylphthalate ND mg/kg 10/25/23 02:49 84-66-210/24/23 17:140.43 1
2,4-Dimethylphenol ND mg/kg 10/25/23 02:49 105-67-910/24/23 17:140.43 1
Dimethylphthalate ND mg/kg 10/25/23 02:49 131-11-310/24/23 17:140.43 1
Di-n-butylphthalate ND mg/kg 10/25/23 02:49 84-74-210/24/23 17:140.43 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/25/23 02:49 534-52-110/24/23 17:140.86 1
2,4-Dinitrophenol ND mg/kg 10/25/23 02:49 51-28-510/24/23 17:142.2 1
2,4-Dinitrotoluene ND mg/kg 10/25/23 02:49 121-14-210/24/23 17:140.43 1
2,6-Dinitrotoluene ND mg/kg 10/25/23 02:49 606-20-210/24/23 17:140.43 1
Di-n-octylphthalate ND mg/kg 10/25/23 02:49 117-84-010/24/23 17:140.43 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/25/23 02:49 117-81-710/24/23 17:140.43 1
Fluoranthene ND mg/kg 10/25/23 02:49 206-44-010/24/23 17:140.43 1
Fluorene ND mg/kg 10/25/23 02:49 86-73-710/24/23 17:140.43 1
Hexachloro-1,3-butadiene ND mg/kg 10/25/23 02:49 87-68-310/24/23 17:140.43 1
Hexachlorobenzene ND mg/kg 10/25/23 02:49 118-74-110/24/23 17:140.43 1
Hexachlorocyclopentadiene ND mg/kg 10/25/23 02:49 77-47-410/24/23 17:140.43 1
Hexachloroethane ND mg/kg 10/25/23 02:49 67-72-110/24/23 17:140.43 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/25/23 02:49 193-39-510/24/23 17:140.43 1
Isophorone ND mg/kg 10/25/23 02:49 78-59-110/24/23 17:140.43 1
1-Methylnaphthalene ND mg/kg 10/25/23 02:49 90-12-010/24/23 17:140.43 1
2-Methylnaphthalene ND mg/kg 10/25/23 02:49 91-57-610/24/23 17:140.43 1
2-Methylphenol(o-Cresol)ND mg/kg 10/25/23 02:49 95-48-710/24/23 17:140.43 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/25/23 02:49 15831-10-410/24/23 17:140.43 1
Naphthalene ND mg/kg 10/25/23 02:49 91-20-310/24/23 17:140.43 1
2-Nitroaniline ND mg/kg 10/25/23 02:49 88-74-410/24/23 17:142.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 16 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:WS-1 Lab ID:92693430004 Collected:10/16/23 10:18 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3-Nitroaniline ND mg/kg 10/25/23 02:49 99-09-210/24/23 17:142.2 1
4-Nitroaniline ND mg/kg 10/25/23 02:49 100-01-610/24/23 17:140.86 1
Nitrobenzene ND mg/kg 10/25/23 02:49 98-95-310/24/23 17:140.43 1
2-Nitrophenol ND mg/kg 10/25/23 02:49 88-75-510/24/23 17:140.43 1
4-Nitrophenol ND mg/kg 10/25/23 02:49 100-02-710/24/23 17:142.2 1
N-Nitrosodimethylamine ND mg/kg 10/25/23 02:49 62-75-910/24/23 17:140.43 1
N-Nitroso-di-n-propylamine ND mg/kg 10/25/23 02:49 621-64-710/24/23 17:140.43 1
N-Nitrosodiphenylamine ND mg/kg 10/25/23 02:49 86-30-610/24/23 17:140.43 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 10/25/23 02:49 108-60-110/24/23 17:140.43 1
Pentachlorophenol ND mg/kg 10/25/23 02:49 87-86-510/24/23 17:140.86 1
Phenanthrene ND mg/kg 10/25/23 02:49 85-01-810/24/23 17:140.43 1
Phenol ND mg/kg 10/25/23 02:49 108-95-2 v110/24/23 17:140.43 1
Pyrene ND mg/kg 10/25/23 02:49 129-00-010/24/23 17:140.43 1
Pyridine ND mg/kg 10/25/23 02:49 110-86-110/24/23 17:140.43 1
1,2,4-Trichlorobenzene ND mg/kg 10/25/23 02:49 120-82-110/24/23 17:140.43 1
2,4,5-Trichlorophenol ND mg/kg 10/25/23 02:49 95-95-410/24/23 17:140.43 1
2,4,6-Trichlorophenol ND mg/kg 10/25/23 02:49 88-06-210/24/23 17:140.43 1
Surrogates
Nitrobenzene-d5 (S)60 %10/25/23 02:49 4165-60-010/24/23 17:1410-130 1
2-Fluorobiphenyl (S)56 %10/25/23 02:49 321-60-810/24/23 17:1410-130 1
Terphenyl-d14 (S)65 %10/25/23 02:49 1718-51-010/24/23 17:1410-130 1
Phenol-d6 (S)56 %10/25/23 02:49 13127-88-310/24/23 17:1410-130 1
2-Fluorophenol (S)56 %10/25/23 02:49 367-12-410/24/23 17:1410-130 1
2,4,6-Tribromophenol (S)49 %10/25/23 02:49 118-79-610/24/23 17:1410-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/18/23 00:29 67-64-110/17/23 16:310.17 1
Benzene ND mg/kg 10/18/23 00:29 71-43-210/17/23 16:310.0086 1
Bromobenzene ND mg/kg 10/18/23 00:29 108-86-110/17/23 16:310.0086 1
Bromochloromethane ND mg/kg 10/18/23 00:29 74-97-510/17/23 16:310.0086 1
Bromodichloromethane ND mg/kg 10/18/23 00:29 75-27-410/17/23 16:310.0086 1
Bromoform ND mg/kg 10/18/23 00:29 75-25-210/17/23 16:310.0086 1
Bromomethane ND mg/kg 10/18/23 00:29 74-83-9 IH,IK10/17/23 16:310.034 1
2-Butanone (MEK)ND mg/kg 10/18/23 00:29 78-93-310/17/23 16:310.17 1
n-Butylbenzene ND mg/kg 10/18/23 00:29 104-51-810/17/23 16:310.0086 1
sec-Butylbenzene ND mg/kg 10/18/23 00:29 135-98-810/17/23 16:310.0086 1
tert-Butylbenzene ND mg/kg 10/18/23 00:29 98-06-610/17/23 16:310.0086 1
Carbon tetrachloride ND mg/kg 10/18/23 00:29 56-23-510/17/23 16:310.0086 1
Chlorobenzene ND mg/kg 10/18/23 00:29 108-90-710/17/23 16:310.0086 1
Chloroethane ND mg/kg 10/18/23 00:29 75-00-310/17/23 16:310.017 1
Chloroform ND mg/kg 10/18/23 00:29 67-66-310/17/23 16:310.0086 1
Chloromethane ND mg/kg 10/18/23 00:29 74-87-310/17/23 16:310.017 1
2-Chlorotoluene ND mg/kg 10/18/23 00:29 95-49-810/17/23 16:310.0086 1
4-Chlorotoluene ND mg/kg 10/18/23 00:29 106-43-410/17/23 16:310.0086 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 17 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:WS-1 Lab ID:92693430004 Collected:10/16/23 10:18 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dibromo-3-chloropropane ND mg/kg 10/18/23 00:29 96-12-810/17/23 16:310.0086 1
Dibromochloromethane ND mg/kg 10/18/23 00:29 124-48-110/17/23 16:310.0086 1
1,2-Dibromoethane (EDB)ND mg/kg 10/18/23 00:29 106-93-410/17/23 16:310.0086 1
Dibromomethane ND mg/kg 10/18/23 00:29 74-95-310/17/23 16:310.0086 1
1,2-Dichlorobenzene ND mg/kg 10/18/23 00:29 95-50-110/17/23 16:310.0086 1
1,3-Dichlorobenzene ND mg/kg 10/18/23 00:29 541-73-110/17/23 16:310.0086 1
1,4-Dichlorobenzene ND mg/kg 10/18/23 00:29 106-46-710/17/23 16:310.0086 1
Dichlorodifluoromethane ND mg/kg 10/18/23 00:29 75-71-8 IH10/17/23 16:310.017 1
1,1-Dichloroethane ND mg/kg 10/18/23 00:29 75-34-310/17/23 16:310.0086 1
1,2-Dichloroethane ND mg/kg 10/18/23 00:29 107-06-210/17/23 16:310.0086 1
1,1-Dichloroethene ND mg/kg 10/18/23 00:29 75-35-410/17/23 16:310.0086 1
cis-1,2-Dichloroethene ND mg/kg 10/18/23 00:29 156-59-210/17/23 16:310.0086 1
trans-1,2-Dichloroethene ND mg/kg 10/18/23 00:29 156-60-510/17/23 16:310.0086 1
1,2-Dichloropropane ND mg/kg 10/18/23 00:29 78-87-510/17/23 16:310.0086 1
1,3-Dichloropropane ND mg/kg 10/18/23 00:29 142-28-910/17/23 16:310.0086 1
2,2-Dichloropropane ND mg/kg 10/18/23 00:29 594-20-710/17/23 16:310.0086 1
1,1-Dichloropropene ND mg/kg 10/18/23 00:29 563-58-610/17/23 16:310.0086 1
cis-1,3-Dichloropropene ND mg/kg 10/18/23 00:29 10061-01-510/17/23 16:310.0086 1
trans-1,3-Dichloropropene ND mg/kg 10/18/23 00:29 10061-02-610/17/23 16:310.0086 1
Diisopropyl ether ND mg/kg 10/18/23 00:29 108-20-310/17/23 16:310.0086 1
Ethylbenzene 0.015 mg/kg 10/18/23 00:29 100-41-410/17/23 16:310.0086 1
Hexachloro-1,3-butadiene ND mg/kg 10/18/23 00:29 87-68-310/17/23 16:310.017 1
2-Hexanone ND mg/kg 10/18/23 00:29 591-78-610/17/23 16:310.086 1
Isopropylbenzene (Cumene)ND mg/kg 10/18/23 00:29 98-82-810/17/23 16:310.0086 1
p-Isopropyltoluene ND mg/kg 10/18/23 00:29 99-87-610/17/23 16:310.0086 1
Methylene Chloride ND mg/kg 10/18/23 00:29 75-09-210/17/23 16:310.034 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/18/23 00:29 108-10-110/17/23 16:310.086 1
Methyl-tert-butyl ether ND mg/kg 10/18/23 00:29 1634-04-410/17/23 16:310.0086 1
Naphthalene ND mg/kg 10/18/23 00:29 91-20-310/17/23 16:310.0086 1
n-Propylbenzene ND mg/kg 10/18/23 00:29 103-65-110/17/23 16:310.0086 1
Styrene 0.011 mg/kg 10/18/23 00:29 100-42-510/17/23 16:310.0086 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/18/23 00:29 630-20-610/17/23 16:310.0086 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/18/23 00:29 79-34-510/17/23 16:310.0086 1
Tetrachloroethene ND mg/kg 10/18/23 00:29 127-18-410/17/23 16:310.0086 1
Toluene ND mg/kg 10/18/23 00:29 108-88-310/17/23 16:310.0086 1
1,2,3-Trichlorobenzene ND mg/kg 10/18/23 00:29 87-61-610/17/23 16:310.0086 1
1,2,4-Trichlorobenzene ND mg/kg 10/18/23 00:29 120-82-110/17/23 16:310.0086 1
1,1,1-Trichloroethane ND mg/kg 10/18/23 00:29 71-55-610/17/23 16:310.0086 1
1,1,2-Trichloroethane ND mg/kg 10/18/23 00:29 79-00-510/17/23 16:310.0086 1
Trichloroethene ND mg/kg 10/18/23 00:29 79-01-610/17/23 16:310.0086 1
Trichlorofluoromethane ND mg/kg 10/18/23 00:29 75-69-410/17/23 16:310.0086 1
1,2,3-Trichloropropane ND mg/kg 10/18/23 00:29 96-18-410/17/23 16:310.0086 1
1,2,4-Trimethylbenzene ND mg/kg 10/18/23 00:29 95-63-610/17/23 16:310.0086 1
1,3,5-Trimethylbenzene ND mg/kg 10/18/23 00:29 108-67-810/17/23 16:310.0086 1
Vinyl acetate ND mg/kg 10/18/23 00:29 108-05-410/17/23 16:310.086 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 18 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:WS-1 Lab ID:92693430004 Collected:10/16/23 10:18 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl chloride ND mg/kg 10/18/23 00:29 75-01-410/17/23 16:310.017 1
Xylene (Total)0.072 mg/kg 10/18/23 00:29 1330-20-710/17/23 16:310.017 1
m&p-Xylene 0.053 mg/kg 10/18/23 00:29 179601-23-110/17/23 16:310.017 1
o-Xylene 0.019 mg/kg 10/18/23 00:29 95-47-610/17/23 16:310.0086 1
Surrogates
Toluene-d8 (S)102 %10/18/23 00:29 2037-26-510/17/23 16:3170-130 1
4-Bromofluorobenzene (S)101 %10/18/23 00:29 460-00-410/17/23 16:3170-130 1
1,2-Dichloroethane-d4 (S)100 %10/18/23 00:29 17060-07-010/17/23 16:3170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.9 %10/17/23 18:08 N20.10 1
Sample:B-1 Lab ID:92693430005 Collected:10/16/23 10:05 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 10/25/23 03:15 83-32-910/24/23 17:140.41 1
Acenaphthylene ND mg/kg 10/25/23 03:15 208-96-810/24/23 17:140.41 1
Aniline ND mg/kg 10/25/23 03:15 62-53-310/24/23 17:140.41 1
Anthracene ND mg/kg 10/25/23 03:15 120-12-710/24/23 17:140.41 1
Benzo(a)anthracene ND mg/kg 10/25/23 03:15 56-55-310/24/23 17:140.41 1
Benzo(a)pyrene ND mg/kg 10/25/23 03:15 50-32-810/24/23 17:140.41 1
Benzo(b)fluoranthene ND mg/kg 10/25/23 03:15 205-99-210/24/23 17:140.41 1
Benzo(g,h,i)perylene ND mg/kg 10/25/23 03:15 191-24-210/24/23 17:140.41 1
Benzo(k)fluoranthene ND mg/kg 10/25/23 03:15 207-08-910/24/23 17:140.41 1
Benzoic Acid ND mg/kg 10/25/23 03:15 65-85-010/24/23 17:142.1 1
Benzyl alcohol ND mg/kg 10/25/23 03:15 100-51-610/24/23 17:140.83 1
4-Bromophenylphenyl ether ND mg/kg 10/25/23 03:15 101-55-310/24/23 17:140.41 1
Butylbenzylphthalate ND mg/kg 10/25/23 03:15 85-68-710/24/23 17:140.41 1
4-Chloro-3-methylphenol ND mg/kg 10/25/23 03:15 59-50-710/24/23 17:140.83 1
4-Chloroaniline ND mg/kg 10/25/23 03:15 106-47-810/24/23 17:140.83 1
bis(2-Chloroethoxy)methane ND mg/kg 10/25/23 03:15 111-91-110/24/23 17:140.41 1
bis(2-Chloroethyl) ether ND mg/kg 10/25/23 03:15 111-44-410/24/23 17:140.41 1
2-Chloronaphthalene ND mg/kg 10/25/23 03:15 91-58-710/24/23 17:140.41 1
2-Chlorophenol ND mg/kg 10/25/23 03:15 95-57-810/24/23 17:140.41 1
4-Chlorophenylphenyl ether ND mg/kg 10/25/23 03:15 7005-72-310/24/23 17:140.41 1
Chrysene ND mg/kg 10/25/23 03:15 218-01-910/24/23 17:140.41 1
Dibenz(a,h)anthracene ND mg/kg 10/25/23 03:15 53-70-310/24/23 17:140.41 1
Dibenzofuran ND mg/kg 10/25/23 03:15 132-64-910/24/23 17:140.41 1
1,2-Dichlorobenzene ND mg/kg 10/25/23 03:15 95-50-110/24/23 17:140.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 19 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:B-1 Lab ID:92693430005 Collected:10/16/23 10:05 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,3-Dichlorobenzene ND mg/kg 10/25/23 03:15 541-73-110/24/23 17:140.41 1
1,4-Dichlorobenzene ND mg/kg 10/25/23 03:15 106-46-710/24/23 17:140.41 1
3,3'-Dichlorobenzidine ND mg/kg 10/25/23 03:15 91-94-1 L210/24/23 17:140.83 1
2,4-Dichlorophenol ND mg/kg 10/25/23 03:15 120-83-210/24/23 17:140.41 1
Diethylphthalate ND mg/kg 10/25/23 03:15 84-66-210/24/23 17:140.41 1
2,4-Dimethylphenol ND mg/kg 10/25/23 03:15 105-67-910/24/23 17:140.41 1
Dimethylphthalate ND mg/kg 10/25/23 03:15 131-11-310/24/23 17:140.41 1
Di-n-butylphthalate ND mg/kg 10/25/23 03:15 84-74-210/24/23 17:140.41 1
4,6-Dinitro-2-methylphenol ND mg/kg 10/25/23 03:15 534-52-110/24/23 17:140.83 1
2,4-Dinitrophenol ND mg/kg 10/25/23 03:15 51-28-510/24/23 17:142.1 1
2,4-Dinitrotoluene ND mg/kg 10/25/23 03:15 121-14-210/24/23 17:140.41 1
2,6-Dinitrotoluene ND mg/kg 10/25/23 03:15 606-20-210/24/23 17:140.41 1
Di-n-octylphthalate ND mg/kg 10/25/23 03:15 117-84-010/24/23 17:140.41 1
bis(2-Ethylhexyl)phthalate ND mg/kg 10/25/23 03:15 117-81-710/24/23 17:140.41 1
Fluoranthene ND mg/kg 10/25/23 03:15 206-44-010/24/23 17:140.41 1
Fluorene ND mg/kg 10/25/23 03:15 86-73-710/24/23 17:140.41 1
Hexachloro-1,3-butadiene ND mg/kg 10/25/23 03:15 87-68-310/24/23 17:140.41 1
Hexachlorobenzene ND mg/kg 10/25/23 03:15 118-74-110/24/23 17:140.41 1
Hexachlorocyclopentadiene ND mg/kg 10/25/23 03:15 77-47-410/24/23 17:140.41 1
Hexachloroethane ND mg/kg 10/25/23 03:15 67-72-110/24/23 17:140.41 1
Indeno(1,2,3-cd)pyrene ND mg/kg 10/25/23 03:15 193-39-510/24/23 17:140.41 1
Isophorone ND mg/kg 10/25/23 03:15 78-59-110/24/23 17:140.41 1
1-Methylnaphthalene ND mg/kg 10/25/23 03:15 90-12-010/24/23 17:140.41 1
2-Methylnaphthalene ND mg/kg 10/25/23 03:15 91-57-610/24/23 17:140.41 1
2-Methylphenol(o-Cresol)ND mg/kg 10/25/23 03:15 95-48-710/24/23 17:140.41 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 10/25/23 03:15 15831-10-410/24/23 17:140.41 1
Naphthalene ND mg/kg 10/25/23 03:15 91-20-310/24/23 17:140.41 1
2-Nitroaniline ND mg/kg 10/25/23 03:15 88-74-410/24/23 17:142.1 1
3-Nitroaniline ND mg/kg 10/25/23 03:15 99-09-210/24/23 17:142.1 1
4-Nitroaniline ND mg/kg 10/25/23 03:15 100-01-610/24/23 17:140.83 1
Nitrobenzene ND mg/kg 10/25/23 03:15 98-95-310/24/23 17:140.41 1
2-Nitrophenol ND mg/kg 10/25/23 03:15 88-75-510/24/23 17:140.41 1
4-Nitrophenol ND mg/kg 10/25/23 03:15 100-02-710/24/23 17:142.1 1
N-Nitrosodimethylamine ND mg/kg 10/25/23 03:15 62-75-910/24/23 17:140.41 1
N-Nitroso-di-n-propylamine ND mg/kg 10/25/23 03:15 621-64-710/24/23 17:140.41 1
N-Nitrosodiphenylamine ND mg/kg 10/25/23 03:15 86-30-610/24/23 17:140.41 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 10/25/23 03:15 108-60-110/24/23 17:140.41 1
Pentachlorophenol ND mg/kg 10/25/23 03:15 87-86-510/24/23 17:140.83 1
Phenanthrene ND mg/kg 10/25/23 03:15 85-01-810/24/23 17:140.41 1
Phenol ND mg/kg 10/25/23 03:15 108-95-2 v110/24/23 17:140.41 1
Pyrene ND mg/kg 10/25/23 03:15 129-00-010/24/23 17:140.41 1
Pyridine ND mg/kg 10/25/23 03:15 110-86-110/24/23 17:140.41 1
1,2,4-Trichlorobenzene ND mg/kg 10/25/23 03:15 120-82-110/24/23 17:140.41 1
2,4,5-Trichlorophenol ND mg/kg 10/25/23 03:15 95-95-410/24/23 17:140.41 1
2,4,6-Trichlorophenol ND mg/kg 10/25/23 03:15 88-06-210/24/23 17:140.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 20 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:B-1 Lab ID:92693430005 Collected:10/16/23 10:05 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)40 %10/25/23 03:15 4165-60-010/24/23 17:1410-130 1
2-Fluorobiphenyl (S)40 %10/25/23 03:15 321-60-810/24/23 17:1410-130 1
Terphenyl-d14 (S)56 %10/25/23 03:15 1718-51-010/24/23 17:1410-130 1
Phenol-d6 (S)39 %10/25/23 03:15 13127-88-310/24/23 17:1410-130 1
2-Fluorophenol (S)40 %10/25/23 03:15 367-12-410/24/23 17:1410-130 1
2,4,6-Tribromophenol (S)36 %10/25/23 03:15 118-79-610/24/23 17:1410-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 10/18/23 00:48 67-64-110/17/23 16:310.14 1
Benzene ND mg/kg 10/18/23 00:48 71-43-210/17/23 16:310.0069 1
Bromobenzene ND mg/kg 10/18/23 00:48 108-86-110/17/23 16:310.0069 1
Bromochloromethane ND mg/kg 10/18/23 00:48 74-97-510/17/23 16:310.0069 1
Bromodichloromethane ND mg/kg 10/18/23 00:48 75-27-410/17/23 16:310.0069 1
Bromoform ND mg/kg 10/18/23 00:48 75-25-210/17/23 16:310.0069 1
Bromomethane ND mg/kg 10/18/23 00:48 74-83-9 IH,IK10/17/23 16:310.028 1
2-Butanone (MEK)ND mg/kg 10/18/23 00:48 78-93-310/17/23 16:310.14 1
n-Butylbenzene ND mg/kg 10/18/23 00:48 104-51-810/17/23 16:310.0069 1
sec-Butylbenzene ND mg/kg 10/18/23 00:48 135-98-810/17/23 16:310.0069 1
tert-Butylbenzene ND mg/kg 10/18/23 00:48 98-06-610/17/23 16:310.0069 1
Carbon tetrachloride ND mg/kg 10/18/23 00:48 56-23-510/17/23 16:310.0069 1
Chlorobenzene ND mg/kg 10/18/23 00:48 108-90-710/17/23 16:310.0069 1
Chloroethane ND mg/kg 10/18/23 00:48 75-00-310/17/23 16:310.014 1
Chloroform ND mg/kg 10/18/23 00:48 67-66-310/17/23 16:310.0069 1
Chloromethane ND mg/kg 10/18/23 00:48 74-87-310/17/23 16:310.014 1
2-Chlorotoluene ND mg/kg 10/18/23 00:48 95-49-810/17/23 16:310.0069 1
4-Chlorotoluene ND mg/kg 10/18/23 00:48 106-43-410/17/23 16:310.0069 1
1,2-Dibromo-3-chloropropane ND mg/kg 10/18/23 00:48 96-12-810/17/23 16:310.0069 1
Dibromochloromethane ND mg/kg 10/18/23 00:48 124-48-110/17/23 16:310.0069 1
1,2-Dibromoethane (EDB)ND mg/kg 10/18/23 00:48 106-93-410/17/23 16:310.0069 1
Dibromomethane ND mg/kg 10/18/23 00:48 74-95-310/17/23 16:310.0069 1
1,2-Dichlorobenzene ND mg/kg 10/18/23 00:48 95-50-110/17/23 16:310.0069 1
1,3-Dichlorobenzene ND mg/kg 10/18/23 00:48 541-73-110/17/23 16:310.0069 1
1,4-Dichlorobenzene ND mg/kg 10/18/23 00:48 106-46-710/17/23 16:310.0069 1
Dichlorodifluoromethane ND mg/kg 10/18/23 00:48 75-71-8 IH10/17/23 16:310.014 1
1,1-Dichloroethane ND mg/kg 10/18/23 00:48 75-34-310/17/23 16:310.0069 1
1,2-Dichloroethane ND mg/kg 10/18/23 00:48 107-06-210/17/23 16:310.0069 1
1,1-Dichloroethene ND mg/kg 10/18/23 00:48 75-35-410/17/23 16:310.0069 1
cis-1,2-Dichloroethene ND mg/kg 10/18/23 00:48 156-59-210/17/23 16:310.0069 1
trans-1,2-Dichloroethene ND mg/kg 10/18/23 00:48 156-60-510/17/23 16:310.0069 1
1,2-Dichloropropane ND mg/kg 10/18/23 00:48 78-87-510/17/23 16:310.0069 1
1,3-Dichloropropane ND mg/kg 10/18/23 00:48 142-28-910/17/23 16:310.0069 1
2,2-Dichloropropane ND mg/kg 10/18/23 00:48 594-20-710/17/23 16:310.0069 1
1,1-Dichloropropene ND mg/kg 10/18/23 00:48 563-58-610/17/23 16:310.0069 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 21 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:B-1 Lab ID:92693430005 Collected:10/16/23 10:05 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND mg/kg 10/18/23 00:48 10061-01-510/17/23 16:310.0069 1
trans-1,3-Dichloropropene ND mg/kg 10/18/23 00:48 10061-02-610/17/23 16:310.0069 1
Diisopropyl ether ND mg/kg 10/18/23 00:48 108-20-310/17/23 16:310.0069 1
Ethylbenzene ND mg/kg 10/18/23 00:48 100-41-410/17/23 16:310.0069 1
Hexachloro-1,3-butadiene ND mg/kg 10/18/23 00:48 87-68-310/17/23 16:310.014 1
2-Hexanone ND mg/kg 10/18/23 00:48 591-78-610/17/23 16:310.069 1
Isopropylbenzene (Cumene)ND mg/kg 10/18/23 00:48 98-82-810/17/23 16:310.0069 1
p-Isopropyltoluene ND mg/kg 10/18/23 00:48 99-87-610/17/23 16:310.0069 1
Methylene Chloride ND mg/kg 10/18/23 00:48 75-09-210/17/23 16:310.028 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 10/18/23 00:48 108-10-110/17/23 16:310.069 1
Methyl-tert-butyl ether ND mg/kg 10/18/23 00:48 1634-04-410/17/23 16:310.0069 1
Naphthalene ND mg/kg 10/18/23 00:48 91-20-310/17/23 16:310.0069 1
n-Propylbenzene ND mg/kg 10/18/23 00:48 103-65-110/17/23 16:310.0069 1
Styrene ND mg/kg 10/18/23 00:48 100-42-510/17/23 16:310.0069 1
1,1,1,2-Tetrachloroethane ND mg/kg 10/18/23 00:48 630-20-610/17/23 16:310.0069 1
1,1,2,2-Tetrachloroethane ND mg/kg 10/18/23 00:48 79-34-510/17/23 16:310.0069 1
Tetrachloroethene ND mg/kg 10/18/23 00:48 127-18-410/17/23 16:310.0069 1
Toluene ND mg/kg 10/18/23 00:48 108-88-310/17/23 16:310.0069 1
1,2,3-Trichlorobenzene ND mg/kg 10/18/23 00:48 87-61-610/17/23 16:310.0069 1
1,2,4-Trichlorobenzene ND mg/kg 10/18/23 00:48 120-82-110/17/23 16:310.0069 1
1,1,1-Trichloroethane ND mg/kg 10/18/23 00:48 71-55-610/17/23 16:310.0069 1
1,1,2-Trichloroethane ND mg/kg 10/18/23 00:48 79-00-510/17/23 16:310.0069 1
Trichloroethene ND mg/kg 10/18/23 00:48 79-01-610/17/23 16:310.0069 1
Trichlorofluoromethane ND mg/kg 10/18/23 00:48 75-69-410/17/23 16:310.0069 1
1,2,3-Trichloropropane ND mg/kg 10/18/23 00:48 96-18-410/17/23 16:310.0069 1
1,2,4-Trimethylbenzene ND mg/kg 10/18/23 00:48 95-63-610/17/23 16:310.0069 1
1,3,5-Trimethylbenzene ND mg/kg 10/18/23 00:48 108-67-810/17/23 16:310.0069 1
Vinyl acetate ND mg/kg 10/18/23 00:48 108-05-410/17/23 16:310.069 1
Vinyl chloride ND mg/kg 10/18/23 00:48 75-01-410/17/23 16:310.014 1
Xylene (Total)ND mg/kg 10/18/23 00:48 1330-20-710/17/23 16:310.014 1
m&p-Xylene ND mg/kg 10/18/23 00:48 179601-23-110/17/23 16:310.014 1
o-Xylene ND mg/kg 10/18/23 00:48 95-47-610/17/23 16:310.0069 1
Surrogates
Toluene-d8 (S)102 %10/18/23 00:48 2037-26-510/17/23 16:3170-130 1
4-Bromofluorobenzene (S)102 %10/18/23 00:48 460-00-410/17/23 16:3170-130 1
1,2-Dichloroethane-d4 (S)100 %10/18/23 00:48 17060-07-010/17/23 16:3170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.9 %10/17/23 18:08 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 22 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:S-1 Lab ID:92693430006 Collected:10/16/23 11:10 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 10/19/23 23:1910/19/23 12:376.5 1
Surrogates
n-Pentacosane (S)48 %10/19/23 23:19 629-99-210/19/23 12:3710-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/20/23 06:1210/19/23 11:529.7 1
Surrogates
4-Bromofluorobenzene (S)98 %10/20/23 06:12 460-00-410/19/23 11:5266-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.1 %10/18/23 18:11 N20.10 1
Sample:S-2 Lab ID:92693430007 Collected:10/16/23 11:15 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)192 mg/kg 10/22/23 18:45 M110/19/23 15:136.2 1
Surrogates
n-Pentacosane (S)52 %10/22/23 18:45 629-99-210/19/23 15:1310-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/20/23 06:3810/19/23 11:5215.3 1
Surrogates
4-Bromofluorobenzene (S)92 %10/20/23 06:38 460-00-410/19/23 11:5266-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.1 %10/18/23 18:11 N20.10 1
Sample:S-3 Lab ID:92693430008 Collected:10/16/23 11:30 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)ND mg/kg 10/22/23 19:0110/19/23 15:136.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 23 of 80
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92693430
Spencer G-10220
Sample:S-3 Lab ID:92693430008 Collected:10/16/23 11:30 Received:10/16/23 12:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Surrogates
n-Pentacosane (S)50 %10/22/23 19:01 629-99-210/19/23 15:1310-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 10/18/23 07:2710/17/23 21:0210.6 1
Surrogates
4-Bromofluorobenzene (S)92 %10/18/23 07:27 460-00-410/17/23 21:0266-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.6 %10/18/23 18:11 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 24 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807100
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693430008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4179355
Associated Lab Samples:92693430008
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 10/17/23 18:35
4-Bromofluorobenzene (S)%93 66-130 10/17/23 18:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4179356LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 47.850 96 70-130
4-Bromofluorobenzene (S)%96 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4179358MATRIX SPIKE SAMPLE:
MSSpike
Result
92693328003
Gas Range Organics (C6-C10)mg/kg 132 M174.9 -1 57-154133
4-Bromofluorobenzene (S)%123 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693328002
4179357SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%9495
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 25 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807547
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693430006, 92693430007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4181587
Associated Lab Samples:92693430006, 92693430007
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 10/19/23 16:27
4-Bromofluorobenzene (S)%91 66-130 10/19/23 16:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4181588LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 47.449.9 95 70-130
4-Bromofluorobenzene (S)%93 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4181590MATRIX SPIKE SAMPLE:
MSSpike
Result
92693767030
Gas Range Organics (C6-C10)mg/kg 84.2 M15415657-154ND
4-Bromofluorobenzene (S)%94 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693767029
4181589SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%9090
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 26 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
806996
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693430001, 92693430002, 92693430003, 92693430004, 92693430005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4178904
Associated Lab Samples:92693430001, 92693430002, 92693430003, 92693430004, 92693430005
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 10/17/23 22:39
1,1,1-Trichloroethane mg/kg ND 0.0050 10/17/23 22:39
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 10/17/23 22:39
1,1,2-Trichloroethane mg/kg ND 0.0050 10/17/23 22:39
1,1-Dichloroethane mg/kg ND 0.0050 10/17/23 22:39
1,1-Dichloroethene mg/kg ND 0.0050 10/17/23 22:39
1,1-Dichloropropene mg/kg ND 0.0050 10/17/23 22:39
1,2,3-Trichlorobenzene mg/kg ND 0.0050 10/17/23 22:39
1,2,3-Trichloropropane mg/kg ND 0.0050 10/17/23 22:39
1,2,4-Trichlorobenzene mg/kg ND 0.0050 10/17/23 22:39
1,2,4-Trimethylbenzene mg/kg ND 0.0050 10/17/23 22:39
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 10/17/23 22:39
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 10/17/23 22:39
1,2-Dichlorobenzene mg/kg ND 0.0050 10/17/23 22:39
1,2-Dichloroethane mg/kg ND 0.0050 10/17/23 22:39
1,2-Dichloropropane mg/kg ND 0.0050 10/17/23 22:39
1,3,5-Trimethylbenzene mg/kg ND 0.0050 10/17/23 22:39
1,3-Dichlorobenzene mg/kg ND 0.0050 10/17/23 22:39
1,3-Dichloropropane mg/kg ND 0.0050 10/17/23 22:39
1,4-Dichlorobenzene mg/kg ND 0.0050 10/17/23 22:39
2,2-Dichloropropane mg/kg ND 0.0050 10/17/23 22:39
2-Butanone (MEK)mg/kg ND 0.10 10/17/23 22:39
2-Chlorotoluene mg/kg ND 0.0050 10/17/23 22:39
2-Hexanone mg/kg ND 0.050 10/17/23 22:39
4-Chlorotoluene mg/kg ND 0.0050 10/17/23 22:39
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 10/17/23 22:39
Acetone mg/kg ND 0.10 10/17/23 22:39
Benzene mg/kg ND 0.0050 10/17/23 22:39
Bromobenzene mg/kg ND 0.0050 10/17/23 22:39
Bromochloromethane mg/kg ND 0.0050 10/17/23 22:39
Bromodichloromethane mg/kg ND 0.0050 10/17/23 22:39
Bromoform mg/kg ND 0.0050 10/17/23 22:39
Bromomethane mg/kg ND 0.020 IH,IK10/17/23 22:39
Carbon tetrachloride mg/kg ND 0.0050 10/17/23 22:39
Chlorobenzene mg/kg ND 0.0050 10/17/23 22:39
Chloroethane mg/kg ND 0.010 10/17/23 22:39
Chloroform mg/kg ND 0.0050 10/17/23 22:39
Chloromethane mg/kg ND 0.010 10/17/23 22:39
cis-1,2-Dichloroethene mg/kg ND 0.0050 10/17/23 22:39
cis-1,3-Dichloropropene mg/kg ND 0.0050 10/17/23 22:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 27 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4178904
Associated Lab Samples:92693430001, 92693430002, 92693430003, 92693430004, 92693430005
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 10/17/23 22:39
Dibromomethane mg/kg ND 0.0050 10/17/23 22:39
Dichlorodifluoromethane mg/kg ND 0.010 IH10/17/23 22:39
Diisopropyl ether mg/kg ND 0.0050 10/17/23 22:39
Ethylbenzene mg/kg ND 0.0050 10/17/23 22:39
Hexachloro-1,3-butadiene mg/kg ND 0.010 10/17/23 22:39
Isopropylbenzene (Cumene)mg/kg ND 0.0050 10/17/23 22:39
m&p-Xylene mg/kg ND 0.010 10/17/23 22:39
Methyl-tert-butyl ether mg/kg ND 0.0050 10/17/23 22:39
Methylene Chloride mg/kg ND 0.020 10/17/23 22:39
n-Butylbenzene mg/kg ND 0.0050 10/17/23 22:39
n-Propylbenzene mg/kg ND 0.0050 10/17/23 22:39
Naphthalene mg/kg ND 0.0050 10/17/23 22:39
o-Xylene mg/kg ND 0.0050 10/17/23 22:39
p-Isopropyltoluene mg/kg ND 0.0050 10/17/23 22:39
sec-Butylbenzene mg/kg ND 0.0050 10/17/23 22:39
Styrene mg/kg ND 0.0050 10/17/23 22:39
tert-Butylbenzene mg/kg ND 0.0050 10/17/23 22:39
Tetrachloroethene mg/kg ND 0.0050 10/17/23 22:39
Toluene mg/kg ND 0.0050 10/17/23 22:39
trans-1,2-Dichloroethene mg/kg ND 0.0050 10/17/23 22:39
trans-1,3-Dichloropropene mg/kg ND 0.0050 10/17/23 22:39
Trichloroethene mg/kg ND 0.0050 10/17/23 22:39
Trichlorofluoromethane mg/kg ND 0.0050 10/17/23 22:39
Vinyl acetate mg/kg ND 0.050 10/17/23 22:39
Vinyl chloride mg/kg ND 0.010 10/17/23 22:39
Xylene (Total)mg/kg ND 0.010 10/17/23 22:39
1,2-Dichloroethane-d4 (S)%102 70-130 10/17/23 22:39
4-Bromofluorobenzene (S)%101 70-130 10/17/23 22:39
Toluene-d8 (S)%102 70-130 10/17/23 22:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4178905LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.430.5 85 70-130
1,1,1-Trichloroethane mg/kg 0.430.5 85 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.430.5 85 70-130
1,1,2-Trichloroethane mg/kg 0.430.5 86 70-130
1,1-Dichloroethane mg/kg 0.420.5 84 70-130
1,1-Dichloroethene mg/kg 0.470.5 93 70-132
1,1-Dichloropropene mg/kg 0.470.5 94 70-130
1,2,3-Trichlorobenzene mg/kg 0.470.5 93 62-136
1,2,3-Trichloropropane mg/kg 0.420.5 83 70-130
1,2,4-Trichlorobenzene mg/kg 0.430.5 85 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 28 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4178905LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 0.440.5 89 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.420.5 84 65-130
1,2-Dibromoethane (EDB)mg/kg 0.420.5 85 70-130
1,2-Dichlorobenzene mg/kg 0.420.5 85 70-130
1,2-Dichloroethane mg/kg 0.430.5 86 70-130
1,2-Dichloropropane mg/kg 0.450.5 90 70-130
1,3,5-Trimethylbenzene mg/kg 0.460.5 92 70-130
1,3-Dichlorobenzene mg/kg 0.420.5 84 70-130
1,3-Dichloropropane mg/kg 0.420.5 84 70-130
1,4-Dichlorobenzene mg/kg 0.410.5 83 70-130
2,2-Dichloropropane mg/kg 0.410.5 82 60-130
2-Butanone (MEK)mg/kg 0.861 86 66-130
2-Chlorotoluene mg/kg 0.440.5 89 70-130
2-Hexanone mg/kg 0.911 91 68-130
4-Chlorotoluene mg/kg 0.450.5 89 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.901 90 70-130
Acetone mg/kg 0.881 88 60-130
Benzene mg/kg 0.420.5 85 70-130
Bromobenzene mg/kg 0.410.5 83 70-130
Bromochloromethane mg/kg 0.440.5 88 70-130
Bromodichloromethane mg/kg 0.420.5 84 70-130
Bromoform mg/kg 0.430.5 85 70-130
Bromomethane mg/kg 0.44 IH,IK0.5 88 43-175
Carbon tetrachloride mg/kg 0.450.5 89 70-130
Chlorobenzene mg/kg 0.430.5 85 70-130
Chloroethane mg/kg 0.460.5 91 70-145
Chloroform mg/kg 0.430.5 86 70-130
Chloromethane mg/kg 0.490.5 98 66-146
cis-1,2-Dichloroethene mg/kg 0.430.5 86 70-130
cis-1,3-Dichloropropene mg/kg 0.440.5 88 70-130
Dibromochloromethane mg/kg 0.430.5 86 70-130
Dibromomethane mg/kg 0.420.5 84 70-130
Dichlorodifluoromethane mg/kg 0.78 IH0.5 155 42-197
Diisopropyl ether mg/kg 0.430.5 86 68-130
Ethylbenzene mg/kg 0.420.5 84 70-130
Hexachloro-1,3-butadiene mg/kg 0.440.5 88 70-130
Isopropylbenzene (Cumene)mg/kg 0.470.5 93 70-130
m&p-Xylene mg/kg 0.881 88 70-130
Methyl-tert-butyl ether mg/kg 0.410.5 82 70-130
Methylene Chloride mg/kg 0.450.5 89 65-130
n-Butylbenzene mg/kg 0.460.5 91 70-130
n-Propylbenzene mg/kg 0.430.5 86 70-130
Naphthalene mg/kg 0.450.5 90 65-135
o-Xylene mg/kg 0.450.5 91 70-130
p-Isopropyltoluene mg/kg 0.440.5 88 70-130
sec-Butylbenzene mg/kg 0.440.5 88 70-130
Styrene mg/kg 0.450.5 91 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 29 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4178905LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.420.5 84 70-130
Tetrachloroethene mg/kg 0.430.5 87 70-130
Toluene mg/kg 0.430.5 85 70-130
trans-1,2-Dichloroethene mg/kg 0.450.5 91 70-130
trans-1,3-Dichloropropene mg/kg 0.420.5 85 70-130
Trichloroethene mg/kg 0.440.5 88 70-130
Trichlorofluoromethane mg/kg 0.470.5 93 62-140
Vinyl acetate mg/kg 0.891 89 70-140
Vinyl chloride mg/kg 0.430.5 86 70-152
Xylene (Total)mg/kg 1.31.5 89 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4178906MATRIX SPIKE SAMPLE:
MSSpike
Result
92693430001
1,1,1,2-Tetrachloroethane mg/kg 0.210.7 31 22-166ND
1,1,1-Trichloroethane mg/kg 0.230.7 33 23-172ND
1,1,2,2-Tetrachloroethane mg/kg 0.220.7 32 21-158ND
1,1,2-Trichloroethane mg/kg 0.230.7 34 25-160ND
1,1-Dichloroethane mg/kg 0.230.7 33 22-166ND
1,1-Dichloroethene mg/kg 0.280.7 40 18-183ND
1,1-Dichloropropene mg/kg 0.250.7 36 20-181ND
1,2,3-Trichlorobenzene mg/kg 0.100.7 15 10-161ND
1,2,3-Trichloropropane mg/kg 0.210.7 31 21-147ND
1,2,4-Trichlorobenzene mg/kg 0.150.7 21 10-159ND
1,2,4-Trimethylbenzene mg/kg 0.210.7 30 17-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.200.7 29 10-135ND
1,2-Dibromoethane (EDB)mg/kg 0.230.7 34 30-154ND
1,2-Dichlorobenzene mg/kg 0.210.7 31 26-162ND
1,2-Dichloroethane mg/kg 0.250.7 36 23-161ND
1,2-Dichloropropane mg/kg 0.250.7 36 29-165ND
1,3,5-Trimethylbenzene mg/kg 0.210.7 31 20-172ND
1,3-Dichlorobenzene mg/kg 0.200.7 29 22-164ND
1,3-Dichloropropane mg/kg 0.230.7 33 27-156ND
1,4-Dichlorobenzene mg/kg 0.210.7 30 20-161ND
2,2-Dichloropropane mg/kg 0.200.7 29 10-159ND
2-Butanone (MEK)mg/kg 0.501.4 36 13-143ND
2-Chlorotoluene mg/kg 0.210.7 31 21-166ND
2-Hexanone mg/kg 0.451.4 33 19-145ND
4-Chlorotoluene mg/kg 0.210.7 31 19-163ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.481.4 35 21-151ND
Acetone mg/kg 0.401.4 29 10-133ND
Benzene mg/kg 0.240.7 35 29-156ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 30 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4178906MATRIX SPIKE SAMPLE:
MSSpike
Result
92693430001
Bromobenzene mg/kg 0.210.7 30 25-161ND
Bromochloromethane mg/kg 0.250.7 36 27-158ND
Bromodichloromethane mg/kg 0.220.7 32 23-158ND
Bromoform mg/kg 0.210.7 30 19-152ND
Bromomethane mg/kg ND IH,IK,M10.7 0 10-152ND
Carbon tetrachloride mg/kg 0.210.7 30 18-172ND
Chlorobenzene mg/kg 0.220.7 31 26-166ND
Chloroethane mg/kg 0.045 M10.7 6 10-130ND
Chloroform mg/kg 0.240.7 35 25-161ND
Chloromethane mg/kg 0.320.7 46 27-197ND
cis-1,2-Dichloroethene mg/kg 0.250.7 37 28-165ND
cis-1,3-Dichloropropene mg/kg 0.230.7 33 23-159ND
Dibromochloromethane mg/kg 0.220.7 32 21-151ND
Dibromomethane mg/kg 0.24 M10.7 34 38-158ND
Dichlorodifluoromethane mg/kg 0.46 IH0.7 67 10-200ND
Diisopropyl ether mg/kg 0.230.7 34 23-160ND
Ethylbenzene mg/kg 0.200.7 29 22-163ND
Hexachloro-1,3-butadiene mg/kg 0.180.7 26 10-192ND
Isopropylbenzene (Cumene)mg/kg 0.220.7 32 24-173ND
m&p-Xylene mg/kg 0.431.4 30 22-171ND
Methyl-tert-butyl ether mg/kg 0.220.7 32 25-153ND
Methylene Chloride mg/kg 0.290.7 41 10-165ND
n-Butylbenzene mg/kg 0.200.7 29 10-186ND
n-Propylbenzene mg/kg 0.210.7 30 16-171ND
Naphthalene mg/kg 0.120.7 17 10-159ND
o-Xylene mg/kg 0.220.7 32 23-171ND
p-Isopropyltoluene mg/kg 0.200.7 28 13-184ND
sec-Butylbenzene mg/kg 0.210.7 30 16-182ND
Styrene mg/kg 0.210.7 30 25-169ND
tert-Butylbenzene mg/kg 0.190.7 28 20-174ND
Tetrachloroethene mg/kg 0.190.7 27 14-171ND
Toluene mg/kg 0.220.7 32 24-166ND
trans-1,2-Dichloroethene mg/kg 0.250.7 37 24-170ND
trans-1,3-Dichloropropene mg/kg 0.220.7 32 22-157ND
Trichloroethene mg/kg 0.220.7 32 23-176ND
Trichlorofluoromethane mg/kg 0.034 M10.7 5 10-138ND
Vinyl acetate mg/kg 0.491.4 35 11-166ND
Vinyl chloride mg/kg 0.270.7 39 21-200ND
Xylene (Total)mg/kg 0.652.1 31 23-170ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 31 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693430002
4178907SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND IH,IK30ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND IH30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg .0054J 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 32 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693430002
4178907SAMPLE DUPLICATE:
m&p-Xylene mg/kg .012J 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%102100
4-Bromofluorobenzene (S)%102101
Toluene-d8 (S)%102101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 33 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807536
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693430006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4181504
Associated Lab Samples:92693430006
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.0 10/19/23 20:24
n-Pentacosane (S)%60 10-133 10/19/23 20:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4181505LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 45.966.4 69 43-130
n-Pentacosane (S)%71 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4181506MATRIX SPIKE SAMPLE:
MSSpike
Result
92693432001
Diesel Range Organics(C10-C28)mg/kg 50.783.5 59 15-130ND
n-Pentacosane (S)%63 10-133
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693740002
4181507SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg ND 30ND
n-Pentacosane (S)%5868
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 34 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807578
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693430007, 92693430008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4181764
Associated Lab Samples:92693430007, 92693430008
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 4.9 10/22/23 18:29
n-Pentacosane (S)%48 10-133 10/22/23 18:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4181765LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 44.466.9 66 43-130
n-Pentacosane (S)%69 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4181766MATRIX SPIKE SAMPLE:
MSSpike
Result
92693430007
Diesel Range Organics(C10-C28)mg/kg 1080 M181.6 1090 15-130192
n-Pentacosane (S)%83 10-133
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693430008
4181767SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 6.3J 30ND
n-Pentacosane (S)%6050
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 35 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
808513
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693430001, 92693430002, 92693430003, 92693430004, 92693430005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4186437
Associated Lab Samples:92693430001, 92693430002, 92693430003, 92693430004, 92693430005
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 10/24/23 20:54
1,2-Dichlorobenzene mg/kg ND 0.33 10/24/23 20:54
1,3-Dichlorobenzene mg/kg ND 0.33 10/24/23 20:54
1,4-Dichlorobenzene mg/kg ND 0.33 10/24/23 20:54
1-Methylnaphthalene mg/kg ND 0.33 10/24/23 20:54
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 10/24/23 20:54
2,4,5-Trichlorophenol mg/kg ND 0.33 10/24/23 20:54
2,4,6-Trichlorophenol mg/kg ND 0.33 10/24/23 20:54
2,4-Dichlorophenol mg/kg ND 0.33 10/24/23 20:54
2,4-Dimethylphenol mg/kg ND 0.33 10/24/23 20:54
2,4-Dinitrophenol mg/kg ND 1.6 10/24/23 20:54
2,4-Dinitrotoluene mg/kg ND 0.33 10/24/23 20:54
2,6-Dinitrotoluene mg/kg ND 0.33 10/24/23 20:54
2-Chloronaphthalene mg/kg ND 0.33 10/24/23 20:54
2-Chlorophenol mg/kg ND 0.33 10/24/23 20:54
2-Methylnaphthalene mg/kg ND 0.33 10/24/23 20:54
2-Methylphenol(o-Cresol)mg/kg ND 0.33 10/24/23 20:54
2-Nitroaniline mg/kg ND 1.6 10/24/23 20:54
2-Nitrophenol mg/kg ND 0.33 10/24/23 20:54
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 10/24/23 20:54
3,3'-Dichlorobenzidine mg/kg ND 0.66 10/24/23 20:54
3-Nitroaniline mg/kg ND 1.6 10/24/23 20:54
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 10/24/23 20:54
4-Bromophenylphenyl ether mg/kg ND 0.33 10/24/23 20:54
4-Chloro-3-methylphenol mg/kg ND 0.66 10/24/23 20:54
4-Chloroaniline mg/kg ND 0.66 10/24/23 20:54
4-Chlorophenylphenyl ether mg/kg ND 0.33 10/24/23 20:54
4-Nitroaniline mg/kg ND 0.66 10/24/23 20:54
4-Nitrophenol mg/kg ND 1.6 10/24/23 20:54
Acenaphthene mg/kg ND 0.33 10/24/23 20:54
Acenaphthylene mg/kg ND 0.33 10/24/23 20:54
Aniline mg/kg ND 0.33 10/24/23 20:54
Anthracene mg/kg ND 0.33 10/24/23 20:54
Benzo(a)anthracene mg/kg ND 0.33 10/24/23 20:54
Benzo(a)pyrene mg/kg ND 0.33 10/24/23 20:54
Benzo(b)fluoranthene mg/kg ND 0.33 10/24/23 20:54
Benzo(g,h,i)perylene mg/kg ND 0.33 10/24/23 20:54
Benzo(k)fluoranthene mg/kg ND 0.33 10/24/23 20:54
Benzoic Acid mg/kg ND 1.6 10/24/23 20:54
Benzyl alcohol mg/kg ND 0.66 10/24/23 20:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 36 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4186437
Associated Lab Samples:92693430001, 92693430002, 92693430003, 92693430004, 92693430005
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane mg/kg ND 0.33 10/24/23 20:54
bis(2-Chloroethyl) ether mg/kg ND 0.33 10/24/23 20:54
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 10/24/23 20:54
Butylbenzylphthalate mg/kg ND 0.33 10/24/23 20:54
Chrysene mg/kg ND 0.33 10/24/23 20:54
Di-n-butylphthalate mg/kg ND 0.33 10/24/23 20:54
Di-n-octylphthalate mg/kg ND 0.33 10/24/23 20:54
Dibenz(a,h)anthracene mg/kg ND 0.33 10/24/23 20:54
Dibenzofuran mg/kg ND 0.33 10/24/23 20:54
Diethylphthalate mg/kg ND 0.33 10/24/23 20:54
Dimethylphthalate mg/kg ND 0.33 10/24/23 20:54
Fluoranthene mg/kg ND 0.33 10/24/23 20:54
Fluorene mg/kg ND 0.33 10/24/23 20:54
Hexachloro-1,3-butadiene mg/kg ND 0.33 10/24/23 20:54
Hexachlorobenzene mg/kg ND 0.33 10/24/23 20:54
Hexachlorocyclopentadiene mg/kg ND 0.33 10/24/23 20:54
Hexachloroethane mg/kg ND 0.33 10/24/23 20:54
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 10/24/23 20:54
Isophorone mg/kg ND 0.33 10/24/23 20:54
N-Nitroso-di-n-propylamine mg/kg ND 0.33 10/24/23 20:54
N-Nitrosodimethylamine mg/kg ND 0.33 10/24/23 20:54
N-Nitrosodiphenylamine mg/kg ND 0.33 10/24/23 20:54
Naphthalene mg/kg ND 0.33 10/24/23 20:54
Nitrobenzene mg/kg ND 0.33 10/24/23 20:54
Pentachlorophenol mg/kg ND 0.66 10/24/23 20:54
Phenanthrene mg/kg ND 0.33 10/24/23 20:54
Phenol mg/kg ND 0.33 v110/24/23 20:54
Pyrene mg/kg ND 0.33 10/24/23 20:54
Pyridine mg/kg ND 0.33 10/24/23 20:54
2,4,6-Tribromophenol (S)%70 10-130 10/24/23 20:54
2-Fluorobiphenyl (S)%73 10-130 10/24/23 20:54
2-Fluorophenol (S)%75 10-130 10/24/23 20:54
Nitrobenzene-d5 (S)%74 10-130 10/24/23 20:54
Phenol-d6 (S)%74 10-130 10/24/23 20:54
Terphenyl-d14 (S)%90 10-130 10/24/23 20:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4186438LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 0.871.7 52 40-130
1,2-Dichlorobenzene mg/kg 0.911.7 53 37-130
1,3-Dichlorobenzene mg/kg 0.881.7 52 36-130
1,4-Dichlorobenzene mg/kg 0.871.7 52 36-130
1-Methylnaphthalene mg/kg 1.01.7 60 46-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 37 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4186438LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 0.921.7 54 12-130
2,4,5-Trichlorophenol mg/kg 1.11.7 63 49-130
2,4,6-Trichlorophenol mg/kg 1.01.7 59 48-130
2,4-Dichlorophenol mg/kg 0.961.7 57 45-130
2,4-Dimethylphenol mg/kg 1.01.7 60 45-130
2,4-Dinitrophenol mg/kg 5.98.5 70 23-130
2,4-Dinitrotoluene mg/kg 1.21.7 72 50-130
2,6-Dinitrotoluene mg/kg 1.21.7 71 53-130
2-Chloronaphthalene mg/kg 0.951.7 56 46-130
2-Chlorophenol mg/kg 0.961.7 56 39-130
2-Methylnaphthalene mg/kg 1.01.7 60 45-130
2-Methylphenol(o-Cresol)mg/kg 1.01.7 59 38-130
2-Nitroaniline mg/kg 2.33.4 69 43-130
2-Nitrophenol mg/kg 0.981.7 58 43-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.01.7 61 34-130
3,3'-Dichlorobenzidine mg/kg 2.2 L23.4 66 68-130
3-Nitroaniline mg/kg 2.33.4 68 36-130
4,6-Dinitro-2-methylphenol mg/kg 2.43.4 71 38-130
4-Bromophenylphenyl ether mg/kg 1.11.7 68 52-130
4-Chloro-3-methylphenol mg/kg 2.23.4 66 45-130
4-Chloroaniline mg/kg 2.13.4 62 41-130
4-Chlorophenylphenyl ether mg/kg 1.21.7 69 46-130
4-Nitroaniline mg/kg 2.53.4 74 40-130
4-Nitrophenol mg/kg 6.38.5 75 34-130
Acenaphthene mg/kg 1.11.7 67 47-130
Acenaphthylene mg/kg 1.11.7 67 50-130
Aniline mg/kg 0.981.7 58 33-130
Anthracene mg/kg 1.31.7 74 46-130
Benzo(a)anthracene mg/kg 1.21.7 73 49-130
Benzo(a)pyrene mg/kg 1.21.7 68 45-130
Benzo(b)fluoranthene mg/kg 1.21.7 69 45-130
Benzo(g,h,i)perylene mg/kg 1.01.7 59 44-130
Benzo(k)fluoranthene mg/kg 1.21.7 69 46-130
Benzoic Acid mg/kg 4.98.5 58 14-130
Benzyl alcohol mg/kg 2.13.4 62 39-130
bis(2-Chloroethoxy)methane mg/kg 1.01.7 59 41-130
bis(2-Chloroethyl) ether mg/kg 0.951.7 56 34-130
bis(2-Ethylhexyl)phthalate mg/kg 1.41.7 83 39-130
Butylbenzylphthalate mg/kg 1.41.7 80 48-130
Chrysene mg/kg 1.21.7 73 50-130
Di-n-butylphthalate mg/kg 1.31.7 78 46-130
Di-n-octylphthalate mg/kg 1.41.7 84 49-130
Dibenz(a,h)anthracene mg/kg 1.01.7 61 46-130
Dibenzofuran mg/kg 1.11.7 65 49-130
Diethylphthalate mg/kg 1.31.7 74 49-130
Dimethylphthalate mg/kg 1.21.7 71 50-130
Fluoranthene mg/kg 1.31.7 76 49-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 38 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4186438LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.31.7 74 47-130
Hexachloro-1,3-butadiene mg/kg 0.821.7 48 36-130
Hexachlorobenzene mg/kg 1.11.7 65 52-130
Hexachlorocyclopentadiene mg/kg 0.721.7 43 10-130
Hexachloroethane mg/kg 0.861.7 51 36-130
Indeno(1,2,3-cd)pyrene mg/kg 1.01.7 59 44-130
Isophorone mg/kg 1.11.7 65 40-130
N-Nitroso-di-n-propylamine mg/kg 1.11.7 64 34-130
N-Nitrosodimethylamine mg/kg 0.881.7 52 29-130
N-Nitrosodiphenylamine mg/kg 1.21.7 72 47-130
Naphthalene mg/kg 0.991.7 58 43-130
Nitrobenzene mg/kg 0.921.7 54 41-130
Pentachlorophenol mg/kg 2.23.4 64 35-130
Phenanthrene mg/kg 1.31.7 76 50-130
Phenol mg/kg 1.1 v11.7 62 39-130
Pyrene mg/kg 1.31.7 75 51-130
Pyridine mg/kg 0.761.7 45 21-130
2,4,6-Tribromophenol (S)%67 10-130
2-Fluorobiphenyl (S)%58 10-130
2-Fluorophenol (S)%56 10-130
Nitrobenzene-d5 (S)%56 10-130
Phenol-d6 (S)%58 10-130
Terphenyl-d14 (S)%72 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4186439MATRIX SPIKE SAMPLE:
MSSpike
Result
92693430001
1,2,4-Trichlorobenzene mg/kg 0.832.2 39 22-130ND
1,2-Dichlorobenzene mg/kg 0.922.2 42 22-130ND
1,3-Dichlorobenzene mg/kg 0.902.2 42 22-130ND
1,4-Dichlorobenzene mg/kg 0.892.2 41 21-130ND
1-Methylnaphthalene mg/kg 1.02.2 47 27-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 0.992.2 46 10-130ND
2,4,5-Trichlorophenol mg/kg 1.12.2 51 18-130ND
2,4,6-Trichlorophenol mg/kg 1.12.2 49 17-130ND
2,4-Dichlorophenol mg/kg 0.982.2 45 19-130ND
2,4-Dimethylphenol mg/kg 0.932.2 43 17-130ND
2,4-Dinitrophenol mg/kg 6.610.8 61 10-130ND
2,4-Dinitrotoluene mg/kg 1.32.2 61 31-130ND
2,6-Dinitrotoluene mg/kg 1.32.2 60 33-130ND
2-Chloronaphthalene mg/kg 0.932.2 43 26-130ND
2-Chlorophenol mg/kg 1.02.2 46 19-130ND
2-Methylnaphthalene mg/kg 1.02.2 47 26-130ND
2-Methylphenol(o-Cresol)mg/kg 1.02.2 48 19-130ND
2-Nitroaniline mg/kg 2.64.4 60 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 39 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4186439MATRIX SPIKE SAMPLE:
MSSpike
Result
92693430001
2-Nitrophenol mg/kg 0.982.2 45 16-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.12.2 52 14-130ND
3,3'-Dichlorobenzidine mg/kg 2.44.4 55 16-130ND
3-Nitroaniline mg/kg 2.84.4 64 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 2.74.4 63 10-131ND
4-Bromophenylphenyl ether mg/kg 1.22.2 54 32-130ND
4-Chloro-3-methylphenol mg/kg 2.44.4 56 26-130ND
4-Chloroaniline mg/kg 2.24.4 51 19-130ND
4-Chlorophenylphenyl ether mg/kg 1.12.2 53 29-130ND
4-Nitroaniline mg/kg 2.94.4 67 22-130ND
4-Nitrophenol mg/kg 6.810.8 63 10-130ND
Acenaphthene mg/kg 1.22.2 53 29-130ND
Acenaphthylene mg/kg 1.22.2 54 27-130ND
Aniline mg/kg 0.962.2 44 10-130ND
Anthracene mg/kg 1.32.2 59 26-130ND
Benzo(a)anthracene mg/kg 1.32.2 58 31-130ND
Benzo(a)pyrene mg/kg 1.12.2 52 24-130ND
Benzo(b)fluoranthene mg/kg 1.22.2 54 12-137ND
Benzo(g,h,i)perylene mg/kg 0.972.2 45 16-130ND
Benzo(k)fluoranthene mg/kg 1.22.2 54 27-130ND
Benzoic Acid mg/kg 4.510.8 42 10-130ND
Benzyl alcohol mg/kg 2.34.4 52 25-130ND
bis(2-Chloroethoxy)methane mg/kg 1.12.2 49 26-130ND
bis(2-Chloroethyl) ether mg/kg 1.02.2 47 23-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.42.2 66 20-130ND
Butylbenzylphthalate mg/kg 1.42.2 64 28-130ND
Chrysene mg/kg 1.22.2 58 29-130ND
Di-n-butylphthalate mg/kg 1.42.2 63 29-130ND
Di-n-octylphthalate mg/kg 1.42.2 67 30-130ND
Dibenz(a,h)anthracene mg/kg 0.982.2 46 27-130ND
Dibenzofuran mg/kg 1.12.2 53 33-130ND
Diethylphthalate mg/kg 1.32.2 62 34-130ND
Dimethylphthalate mg/kg 1.32.2 62 35-130ND
Fluoranthene mg/kg 1.32.2 59 26-130ND
Fluorene mg/kg 1.32.2 60 27-130ND
Hexachloro-1,3-butadiene mg/kg 0.752.2 34 19-130ND
Hexachlorobenzene mg/kg 1.12.2 50 31-130ND
Hexachlorocyclopentadiene mg/kg 0.662.2 31 10-130ND
Hexachloroethane mg/kg 0.892.2 41 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 0.982.2 45 16-130ND
Isophorone mg/kg 1.22.2 54 29-130ND
N-Nitroso-di-n-propylamine mg/kg 1.22.2 56 22-130ND
N-Nitrosodimethylamine mg/kg 1.02.2 48 15-130ND
N-Nitrosodiphenylamine mg/kg 1.32.2 59 30-130ND
Naphthalene mg/kg 1.02.2 47 24-130ND
Nitrobenzene mg/kg 0.942.2 43 25-130ND
Pentachlorophenol mg/kg 2.34.4 54 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 40 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4186439MATRIX SPIKE SAMPLE:
MSSpike
Result
92693430001
Phenanthrene mg/kg 1.32.2 62 28-130ND
Phenol mg/kg 1.1 v12.2 51 18-130ND
Pyrene mg/kg 1.32.2 61 27-130ND
Pyridine mg/kg 1.02.2 46 10-130ND
2,4,6-Tribromophenol (S)%56 10-130
2-Fluorobiphenyl (S)%47 10-130
2-Fluorophenol (S)%47 10-130
Nitrobenzene-d5 (S)%47 10-130
Phenol-d6 (S)%50 10-130
Terphenyl-d14 (S)%65 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693430002
4186440SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg ND 30ND
2,2'-Oxybis(1-chloropropane)mg/kg ND 30ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
2-Chlorophenol mg/kg ND 30ND
2-Methylnaphthalene mg/kg ND 30ND
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Nitroaniline mg/kg ND 30ND
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND 30ND
3-Nitroaniline mg/kg ND 30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND 30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 41 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693430002
4186440SAMPLE DUPLICATE:
Aniline mg/kg ND 30ND
Anthracene mg/kg ND 30ND
Benzo(a)anthracene mg/kg ND 30ND
Benzo(a)pyrene mg/kg ND 30ND
Benzo(b)fluoranthene mg/kg ND 30ND
Benzo(g,h,i)perylene mg/kg ND 30ND
Benzo(k)fluoranthene mg/kg ND 30ND
Benzoic Acid mg/kg ND 30ND
Benzyl alcohol mg/kg ND 30ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg ND 30ND
Butylbenzylphthalate mg/kg ND 30ND
Chrysene mg/kg ND 30ND
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg ND 30ND
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzofuran mg/kg ND 30ND
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg ND 30ND
Fluorene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND 30ND
Hexachloroethane mg/kg ND 30ND
Indeno(1,2,3-cd)pyrene mg/kg ND 30ND
Isophorone mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND 30ND
N-Nitrosodimethylamine mg/kg ND 30ND
N-Nitrosodiphenylamine mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg ND 30ND
Phenanthrene mg/kg ND 30ND
Phenol mg/kg ND v130ND
Pyrene mg/kg ND 30ND
Pyridine mg/kg ND 30ND
2,4,6-Tribromophenol (S)%4240
2-Fluorobiphenyl (S)%4743
2-Fluorophenol (S)%4648
Nitrobenzene-d5 (S)%4948
Phenol-d6 (S)%4749
Terphenyl-d14 (S)%6458
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 42 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807077
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693430001, 92693430002, 92693430003, 92693430004, 92693430005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693690003
4179169SAMPLE DUPLICATE:
Percent Moisture %19.9 N262518.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693430005
4179170SAMPLE DUPLICATE:
Percent Moisture %21.6 N292519.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 43 of 80
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92693430
Spencer G-10220
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
807403
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92693430006, 92693430007, 92693430008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92692459001
4181019SAMPLE DUPLICATE:
Percent Moisture %84.4 N202584.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92693430008
4181020SAMPLE DUPLICATE:
Percent Moisture %23.0 N232523.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 44 of 80
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92693430
Spencer G-10220
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 45 of 80
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92693430
Spencer G-10220
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92693430006 807536 807756S-1 EPA 3546 EPA 8015C
92693430007 807578 807907S-2 EPA 3546 EPA 8015C
92693430008 807578 807907S-3 EPA 3546 EPA 8015C
92693430006 807547 807615S-1 EPA 5030B EPA 8015C
92693430007 807547 807615S-2 EPA 5030B EPA 8015C
92693430008 807100 807102S-3 EPA 5030B EPA 8015C
92693430001 808513 808582SS-1 EPA 3546 EPA 8270E
92693430002 808513 808582ES-1 EPA 3546 EPA 8270E
92693430003 808513 808582NS-1 EPA 3546 EPA 8270E
92693430004 808513 808582WS-1 EPA 3546 EPA 8270E
92693430005 808513 808582B-1 EPA 3546 EPA 8270E
92693430001 806996 807104SS-1 EPA 5035A/5030B EPA 8260D
92693430002 806996 807104ES-1 EPA 5035A/5030B EPA 8260D
92693430003 806996 807104NS-1 EPA 5035A/5030B EPA 8260D
92693430004 806996 807104WS-1 EPA 5035A/5030B EPA 8260D
92693430005 806996 807104B-1 EPA 5035A/5030B EPA 8260D
92693430001 807077SS-1 SW-846
92693430002 807077ES-1 SW-846
92693430003 807077NS-1 SW-846
92693430004 807077WS-1 SW-846
92693430005 807077B-1 SW-846
92693430006 807403S-1 SW-846
92693430007 807403S-2 SW-846
92693430008 807403S-3 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/27/2023 05:23 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 46 of 80
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Page 48 of 80
Page 49 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
October 27, 2023
Stephanie Knott
Pace Analytical Services - NC
1377 South Park Dr.
Kernersville, NC 27284
Project Location: Spencer G-10220
Client Job Number:
Project Number: 92693430
Laboratory Work Order Number: 23J2282
Enclosed are results of analyses for samples as received by the laboratory on October 17, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 50 of 80
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23J2282-01 5
23J2282-02 8
23J2282-03 11
23J2282-04 14
23J2282-05 17
Sample Preparation Information 20
QC Data 21
Petroleum Hydrocarbons Analyses - EPH 21
B355453 21
Petroleum Hydrocarbons Analyses - VPH 24
B355498 24
Flag/Qualifier Summary 26
Certifications 27
Chain of Custody/Sample Receipt 28
Page 51 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
10/27/2023
Pace Analytical Services - NC
1377 South Park Dr.
Kernersville, NC 27284
ATTN: Stephanie Knott
92693430
23J2282
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Spencer G-10220
SS-1 23J2282-01 Soil MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
ES-1 23J2282-02 Soil MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
NS-1 23J2282-03 Soil MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
WS-1 23J2282-04 Soil MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
B-1 23J2282-05 Soil MADEP EPH rev 2.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
[TOC_1]Sample Summary[TOC]
Page 52 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
For method MA EPH, only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
Page 53 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:10
[TOC_2]23J2282-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 14 10/26/23 0:04 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C9-C18 Aliphatics
ND 14 10/26/23 0:04 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C19-C36 Aliphatics
ND 14 10/26/23 0:04 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
ND 14 10/26/23 0:04 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)64.5 10/26/23 0:0440-140
o-Terphenyl (OTP)84.3 10/26/23 0:0440-140
2-Bromonaphthalene 101 10/26/23 0:0440-140
2-Fluorobiphenyl 100 10/26/23 0:0440-140
[TOC_1]Sample Results[TOC]
Page 54 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.15
Petroleum Hydrocarbons Analyses - VPH
ND 15 10/18/23 14:25 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 15 10/18/23 14:25 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 15 10/18/23 14:25 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 15 10/18/23 14:25 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 15 10/18/23 14:25 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)85.9 10/18/23 14:2570-130
2,5-Dibromotoluene (PID)89.2 10/18/23 14:2570-130
Page 55 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-01
Field Sample #: SS-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
73.6 10/18/23 12:29 CCC% Wt 10/18/23SM 2540G1% Solids
Page 56 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-02
Field Sample #: ES-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:14
[TOC_2]23J2282-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 13 10/26/23 0:23 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C9-C18 Aliphatics
ND 13 10/26/23 0:23 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C19-C36 Aliphatics
ND 13 10/26/23 0:23 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
ND 13 10/26/23 0:23 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)65.4 10/26/23 0:2340-140
o-Terphenyl (OTP)65.0 10/26/23 0:2340-140
2-Bromonaphthalene 88.7 10/26/23 0:2340-140
2-Fluorobiphenyl 87.2 10/26/23 0:2340-140
Page 57 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-02
Field Sample #: ES-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:14
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 0.95
Petroleum Hydrocarbons Analyses - VPH
ND 17 10/18/23 14:54 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 17 10/18/23 14:54 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 17 10/18/23 14:54 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 17 10/18/23 14:54 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 17 10/18/23 14:54 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)77.1 10/18/23 14:5470-130
2,5-Dibromotoluene (PID)80.0 10/18/23 14:5470-130
Page 58 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-02
Field Sample #: ES-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:14
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
75.1 10/18/23 12:29 CCC% Wt 10/18/23SM 2540G1% Solids
Page 59 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-03
Field Sample #: NS-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:16
[TOC_2]23J2282-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 14 10/26/23 0:41 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C9-C18 Aliphatics
ND 14 10/26/23 0:41 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C19-C36 Aliphatics
ND 14 10/26/23 0:41 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
ND 14 10/26/23 0:41 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)78.9 10/26/23 0:4140-140
o-Terphenyl (OTP)73.6 10/26/23 0:4140-140
2-Bromonaphthalene 85.8 10/26/23 0:4140-140
2-Fluorobiphenyl 84.9 10/26/23 0:4140-140
Page 60 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-03
Field Sample #: NS-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.08
Petroleum Hydrocarbons Analyses - VPH
ND 18 10/18/23 15:24 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 18 10/18/23 15:24 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 18 10/18/23 15:24 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 18 10/18/23 15:24 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 18 10/18/23 15:24 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)82.0 10/18/23 15:2470-130
2,5-Dibromotoluene (PID)82.0 10/18/23 15:2470-130
Page 61 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-03
Field Sample #: NS-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
70.0 10/18/23 12:29 CCC% Wt 10/18/23SM 2540G1% Solids
Page 62 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-04
Field Sample #: WS-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:18
[TOC_2]23J2282-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 13 10/24/23 23:07 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C9-C18 Aliphatics
ND 13 10/24/23 23:07 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C19-C36 Aliphatics
ND 13 10/24/23 23:07 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
ND 13 10/24/23 23:07 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)60.2 10/24/23 23:0740-140
o-Terphenyl (OTP)63.7 10/24/23 23:0740-140
2-Bromonaphthalene 84.4 10/24/23 23:0740-140
2-Fluorobiphenyl 82.9 10/24/23 23:0740-140
Page 63 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-04
Field Sample #: WS-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:18
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 0.96
Petroleum Hydrocarbons Analyses - VPH
ND 17 10/18/23 15:53 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 17 10/18/23 15:53 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 17 10/18/23 15:53 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 17 10/18/23 15:53 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 17 10/18/23 15:53 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)84.7 10/18/23 15:5370-130
2,5-Dibromotoluene (PID)86.7 10/18/23 15:5370-130
Page 64 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-04
Field Sample #: WS-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:18
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
75.3 10/18/23 12:29 CCC% Wt 10/18/23SM 2540G1% Solids
Page 65 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-05
Field Sample #: B-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:05
[TOC_2]23J2282-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 13 10/26/23 19:50 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C9-C18 Aliphatics
ND 13 10/26/23 19:50 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C19-C36 Aliphatics
ND 13 10/26/23 19:50 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11Unadjusted C11-C22 Aromatics
ND 13 10/26/23 19:50 AYHmg/Kg dry 10/17/23MADEP EPH rev 2.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)61.9 10/26/23 19:5040-140
o-Terphenyl (OTP)68.3 10/26/23 19:5040-140
2-Bromonaphthalene 90.3 10/26/23 19:5040-140
2-Fluorobiphenyl 89.0 10/26/23 19:5040-140
Page 66 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-05
Field Sample #: B-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 0.99
Petroleum Hydrocarbons Analyses - VPH
ND 16 10/18/23 16:23 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 16 10/18/23 16:23 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 16 10/18/23 16:23 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 16 10/18/23 16:23 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 16 10/18/23 16:23 KDKmg/Kg dry 10/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)85.9 10/18/23 16:2370-130
2,5-Dibromotoluene (PID)90.4 10/18/23 16:2370-130
Page 67 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/17/2023
Work Order: 23J2282Sample Description:Project Location: Spencer G-10220
Sample ID: 23J2282-05
Field Sample #: B-1
Sample Matrix: Soil
Sampled: 10/16/2023 10:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
78.2 10/18/23 12:29 CCC% Wt 10/18/23SM 2540G1% Solids
Page 68 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method:SW-846 3546 Analytical Method:MADEP EPH rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B355453 10/17/2320.0 2.0023J2282-01 [SS-1]
B355453 10/17/2320.0 2.0023J2282-02 [ES-1]
B355453 10/17/2320.2 2.0023J2282-03 [NS-1]
B355453 10/17/2320.1 2.0023J2282-04 [WS-1]
B355453 10/17/2320.1 2.0023J2282-05 [B-1]
Prep Method:MA VPH Analytical Method:MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B355498 10/18/2311.4 13.023J2282-01 [SS-1]
B355498 10/18/239.47 12.423J2282-02 [ES-1]
B355498 10/18/2310.8 13.223J2282-03 [NS-1]
B355498 10/18/239.60 12.423J2282-04 [WS-1]
B355498 10/18/239.86 12.223J2282-05 [B-1]
Prep Method:% Solids Analytical Method:SM 2540G
Lab Number [Field ID]Batch Date
B355542 10/18/2323J2282-01 [SS-1]
B355542 10/18/2323J2282-02 [ES-1]
B355542 10/18/2323J2282-03 [NS-1]
B355542 10/18/2323J2282-04 [WS-1]
B355542 10/18/2323J2282-05 [B-1]
[TOC_1]Sample Preparation Information[TOC]
Page 69 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]
Batch B355453 - SW-846 3546
[TOC_3]B355453[TOC]
Blank (B355453-BLK1) Prepared: 10/17/23 Analyzed: 10/20/23
C9-C18 Aliphatics mg/Kg wet10ND
C19-C36 Aliphatics mg/Kg wet10ND
Unadjusted C11-C22 Aromatics mg/Kg wet10ND
C11-C22 Aromatics mg/Kg wet10ND
Acenaphthene mg/Kg wet0.10ND
Acenaphthylene mg/Kg wet0.10ND
Anthracene mg/Kg wet0.10ND
Benzo(a)anthracene mg/Kg wet0.10ND
Benzo(a)pyrene mg/Kg wet0.10ND
Benzo(b)fluoranthene mg/Kg wet0.10ND
Benzo(g,h,i)perylene mg/Kg wet0.10ND
Benzo(k)fluoranthene mg/Kg wet0.10ND
Chrysene mg/Kg wet0.10ND
Dibenz(a,h)anthracene mg/Kg wet0.10ND
Fluoranthene mg/Kg wet0.10ND
Fluorene mg/Kg wet0.10ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10ND
2-Methylnaphthalene mg/Kg wet0.10ND
Naphthalene mg/Kg wet0.10ND
Phenanthrene mg/Kg wet0.10ND
Pyrene mg/Kg wet0.10ND
Naphthalene-aliphatic fraction mg/Kg wet0.10ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10ND
mg/Kg wet 4.98 40-140Surrogate: Chlorooctadecane (COD)53.52.66
mg/Kg wet 4.98 40-140Surrogate: o-Terphenyl (OTP)61.33.05
mg/Kg wet 4.98 40-140Surrogate: 2-Bromonaphthalene 99.24.94
mg/Kg wet 4.98 40-140Surrogate: 2-Fluorobiphenyl 97.74.86
LCS (B355453-BS1) Prepared: 10/17/23 Analyzed: 10/20/23
C9-C18 Aliphatics mg/Kg wet9.9 29.7 40-14063.618.9
C19-C36 Aliphatics mg/Kg wet9.9 39.6 40-14075.229.8
Unadjusted C11-C22 Aromatics mg/Kg wet9.9 84.2 40-14065.955.4
Acenaphthene mg/Kg wet0.099 4.95 40-14062.13.08
Acenaphthylene mg/Kg wet0.099 4.95 40-14058.52.90
Anthracene mg/Kg wet0.099 4.95 40-14066.63.30
Benzo(a)anthracene mg/Kg wet0.099 4.95 40-14062.43.09
Benzo(a)pyrene mg/Kg wet0.099 4.95 40-14062.43.09
Benzo(b)fluoranthene mg/Kg wet0.099 4.95 40-14057.62.85
Benzo(g,h,i)perylene mg/Kg wet0.099 4.95 40-14054.22.68
Benzo(k)fluoranthene mg/Kg wet0.099 4.95 40-14055.72.76
Chrysene mg/Kg wet0.099 4.95 40-14066.13.27
Dibenz(a,h)anthracene mg/Kg wet0.099 4.95 40-14057.92.87
Fluoranthene mg/Kg wet0.099 4.95 40-14063.73.16
Fluorene mg/Kg wet0.099 4.95 40-14065.43.24
Indeno(1,2,3-cd)pyrene mg/Kg wet0.099 4.95 40-14056.92.82
2-Methylnaphthalene mg/Kg wet0.099 4.95 40-14058.42.89
Naphthalene mg/Kg wet0.099 4.95 40-14054.12.68
Phenanthrene mg/Kg wet0.099 4.95 40-14066.43.29
Pyrene mg/Kg wet0.099 4.95 40-14065.43.24
Naphthalene-aliphatic fraction mg/Kg wet0.099 4.95 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.099 4.95 0-5ND
mg/Kg wet 4.95 40-140Surrogate: Chlorooctadecane (COD)52.72.61
[TOC_1]QC Data[TOC]
Page 70 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B355453 - SW-846 3546
LCS (B355453-BS1) Prepared: 10/17/23 Analyzed: 10/20/23
mg/Kg wet 4.95 40-140Surrogate: o-Terphenyl (OTP)59.72.95
mg/Kg wet 4.95 40-140Surrogate: 2-Bromonaphthalene 98.04.85
mg/Kg wet 4.95 40-140Surrogate: 2-Fluorobiphenyl 97.94.85
LCS Dup (B355453-BSD1) Prepared: 10/17/23 Analyzed: 10/20/23
C9-C18 Aliphatics mg/Kg wet10 30.0 2540-14069.2 9.4220.8
C19-C36 Aliphatics mg/Kg wet10 40.0 2540-14077.2 3.5730.9
Unadjusted C11-C22 Aromatics mg/Kg wet10 85.0 2540-14076.5 16.065.1
Acenaphthene mg/Kg wet0.10 5.00 2540-14075.1 19.93.75
Acenaphthylene mg/Kg wet0.10 5.00 2540-14071.2 20.73.56
Anthracene mg/Kg wet0.10 5.00 2540-14078.2 17.03.91
Benzo(a)anthracene mg/Kg wet0.10 5.00 2540-14072.3 15.83.62
Benzo(a)pyrene mg/Kg wet0.10 5.00 2540-14071.6 14.73.58
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 2540-14066.4 15.13.32
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 2540-14061.6 13.73.08
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 2540-14063.8 14.53.19
Chrysene mg/Kg wet0.10 5.00 2540-14075.6 14.53.78
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 2540-14065.8 13.83.29
Fluoranthene mg/Kg wet0.10 5.00 2540-14074.2 16.13.71
Fluorene mg/Kg wet0.10 5.00 2540-14076.1 16.03.80
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 2540-14065.3 14.83.26
2-Methylnaphthalene mg/Kg wet0.10 5.00 2540-14072.6 22.73.63
Naphthalene mg/Kg wet0.10 5.00 2540-14066.5 21.63.32
Phenanthrene mg/Kg wet0.10 5.00 2540-14078.5 17.63.92
Pyrene mg/Kg wet0.10 5.00 2540-14076.0 16.13.80
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)53.22.66
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)70.13.50
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 1045.22
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 1045.19
Matrix Spike (B355453-MS1) Prepared: 10/17/23 Analyzed: 10/24/23 Source: 23J2282-04
C9-C18 Aliphatics mg/Kg dry13 39.8 40-14069.527.7 ND
C19-C36 Aliphatics mg/Kg dry13 53.1 40-14081.143.0 ND
Unadjusted C11-C22 Aromatics mg/Kg dry13 113 40-14069.278.0 ND
Acenaphthene mg/Kg dry0.13 6.64 40-14065.44.34 ND
Acenaphthylene mg/Kg dry0.13 6.64 40-14060.94.04 ND
Anthracene mg/Kg dry0.13 6.64 40-14067.84.50 ND
Benzo(a)anthracene mg/Kg dry0.13 6.64 40-14064.24.26 ND
Benzo(a)pyrene mg/Kg dry0.13 6.64 40-14065.24.33 ND
Benzo(b)fluoranthene mg/Kg dry0.13 6.64 40-14060.34.00 ND
Benzo(g,h,i)perylene mg/Kg dry0.13 6.64 40-14058.23.86 ND
Benzo(k)fluoranthene mg/Kg dry0.13 6.64 40-14058.93.91 ND
Chrysene mg/Kg dry0.13 6.64 40-14069.04.58 ND
Dibenz(a,h)anthracene mg/Kg dry0.13 6.64 40-14061.94.11 ND
Fluoranthene mg/Kg dry0.13 6.64 40-14065.64.35 ND
Fluorene mg/Kg dry0.13 6.64 40-14069.04.58 ND
Indeno(1,2,3-cd)pyrene mg/Kg dry0.13 6.64 40-14060.44.01 ND
2-Methylnaphthalene mg/Kg dry0.13 6.64 40-14064.14.26 ND
Naphthalene mg/Kg dry0.13 6.64 40-14059.43.94 ND
Phenanthrene mg/Kg dry0.13 6.64 40-14068.64.55 ND
Page 71 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B355453 - SW-846 3546
Matrix Spike (B355453-MS1) Prepared: 10/17/23 Analyzed: 10/24/23 Source: 23J2282-04
Pyrene mg/Kg dry0.13 6.64 40-14066.94.44 ND
mg/Kg dry 6.64 40-140Surrogate: Chlorooctadecane (COD)64.24.26
mg/Kg dry 6.64 40-140Surrogate: o-Terphenyl (OTP)60.54.02
mg/Kg dry 6.64 40-140Surrogate: 2-Bromonaphthalene 81.45.40
mg/Kg dry 6.64 40-140Surrogate: 2-Fluorobiphenyl 80.25.33
Matrix Spike Dup (B355453-MSD1) Prepared: 10/17/23 Analyzed: 10/24/23 Source: 23J2282-04
C9-C18 Aliphatics mg/Kg dry13 39.4 5040-14075.9 7.8529.9 ND
C19-C36 Aliphatics mg/Kg dry13 52.6 5040-14089.5 8.9247.1 ND
Unadjusted C11-C22 Aromatics mg/Kg dry13 112 5040-14087.8 22.898.1 ND
Acenaphthene mg/Kg dry0.13 6.57 5040-14082.4 22.15.42 ND
Acenaphthylene mg/Kg dry0.13 6.57 5040-14076.8 22.15.05 ND
Anthracene mg/Kg dry0.13 6.57 5040-14086.4 23.15.68 ND
Benzo(a)anthracene mg/Kg dry0.13 6.57 5040-14082.8 24.45.44 ND
Benzo(a)pyrene mg/Kg dry0.13 6.57 5040-14084.2 24.45.53 ND
Benzo(b)fluoranthene mg/Kg dry0.13 6.57 5040-14078.0 24.75.13 ND
Benzo(g,h,i)perylene mg/Kg dry0.13 6.57 5040-14075.9 25.44.99 ND
Benzo(k)fluoranthene mg/Kg dry0.13 6.57 5040-14075.7 23.94.97 ND
Chrysene mg/Kg dry0.13 6.57 5040-14088.5 23.95.82 ND
Dibenz(a,h)anthracene mg/Kg dry0.13 6.57 5040-14079.7 24.25.24 ND
Fluoranthene mg/Kg dry0.13 6.57 5040-14084.2 24.05.54 ND
Fluorene mg/Kg dry0.13 6.57 5040-14087.5 22.65.75 ND
Indeno(1,2,3-cd)pyrene mg/Kg dry0.13 6.57 5040-14078.5 25.15.16 ND
2-Methylnaphthalene mg/Kg dry0.13 6.57 5040-14080.1 21.15.26 ND
Naphthalene mg/Kg dry0.13 6.57 5040-14074.2 21.14.87 ND
Phenanthrene mg/Kg dry0.13 6.57 5040-14087.6 23.45.76 ND
Pyrene mg/Kg dry0.13 6.57 5040-14086.1 24.05.66 ND
mg/Kg dry 6.57 40-140Surrogate: Chlorooctadecane (COD)69.84.58
mg/Kg dry 6.57 40-140Surrogate: o-Terphenyl (OTP)75.54.96
mg/Kg dry 6.57 40-140Surrogate: 2-Bromonaphthalene 97.56.41
mg/Kg dry 6.57 40-140Surrogate: 2-Fluorobiphenyl 96.36.33
Page 72 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B355498 - MA VPH
[TOC_3]B355498[TOC]
Blank (B355498-BLK1) Prepared & Analyzed: 10/18/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)84.633.8
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)87.935.2
LCS (B355498-BS1) Prepared & Analyzed: 10/18/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 70-1301128.43
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 70-1301088.11
C9-C10 Aromatics mg/Kg wet10 2.50 70-1301052.63
Benzene mg/Kg wet0.050 2.50 70-1301122.80
Butylcyclohexane mg/Kg wet0.050 2.50 70-1301182.96
Decane mg/Kg wet0.050 2.50 70-13089.12.23
Ethylbenzene mg/Kg wet0.050 2.50 70-1301112.78
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 70-1301072.69
2-Methylpentane mg/Kg wet0.050 2.50 70-1301162.90
Naphthalene mg/Kg wet0.50 2.50 70-13086.72.17
Nonane mg/Kg wet0.050 2.50 30-1301172.92
Pentane mg/Kg wet0.050 2.50 70-1301122.81
Toluene mg/Kg wet0.050 2.50 70-1301122.79
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 70-1301052.63
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 70-1301092.72
m+p Xylene mg/Kg wet0.10 5.00 70-1301125.61
o-Xylene mg/Kg wet0.050 2.50 70-1301132.83
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)94.037.6
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10140.4
Page 73 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B355498 - MA VPH
LCS Dup (B355498-BSD1) Prepared & Analyzed: 10/18/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 2570-130111 1.328.32
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 2570-130109 0.5028.15
C9-C10 Aromatics mg/Kg wet10 2.50 2570-130107 1.832.68
Benzene mg/Kg wet0.050 2.50 2570-130114 1.382.84
Butylcyclohexane mg/Kg wet0.050 2.50 2570-130119 0.3622.97
Decane mg/Kg wet0.050 2.50 2570-13089.6 0.4792.24
Ethylbenzene mg/Kg wet0.050 2.50 2570-130114 2.082.84
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 2570-130108 0.2552.69
2-Methylpentane mg/Kg wet0.050 2.50 2570-130116 0.2132.91
Naphthalene mg/Kg wet0.50 2.50 2570-13087.8 1.252.19
Nonane mg/Kg wet0.050 2.50 2530-130117 0.6612.94
Pentane mg/Kg wet0.050 2.50 2570-130107 4.522.69
Toluene mg/Kg wet0.050 2.50 2570-130113 1.502.83
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 2570-130107 1.832.68
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 2570-130109 0.2682.72
m+p Xylene mg/Kg wet0.10 5.00 2570-130114 2.025.72
o-Xylene mg/Kg wet0.050 2.50 2570-130115 1.622.88
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10541.9
µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10441.7
Page 74 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
[TOC_1]Flag/Qualifier Summary[TOC]
Page 75 of 80
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP EPH rev 2.1 in Soil
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
MADEP EPH rev 2.1 in Water
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2025
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2024
Page 76 of 80
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