MO-30154_49209_CA_UST-61_20230728_Rental Uniform

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from
in NC an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or suspected release
(DWM USE ONLY) Suspected Contamination? (Y/N) Facility ID Number Incident# Risk (H,l,L,U) Confirmed GW Contamination? (Y/N) ___ Date Leak Discovered Received On Received By Confirmed Soil Contamination ?(Y/N) ___ Comm/Non-Commercial? Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) __ Reg/Non-regulated? Region Free Product? (Y/N) __ If Yes, State Greatest Thickness
INCIDENT DESCRIPTION Incident Name:
Address: I County:
City/Town: Zip Code: I Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by: Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount OGPS of release, amount of free oroduct oresent and recoverv efforts, initial resoonses conducted, imoacts to receotors)□Topographic map
OGls Address matching
O0ther □unknown
Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one) □Release Detection Equipment or Methods Dvisual/Odor □Groundwater Contamination
ODuring UST Closure/Removal Dwater in Tank Dsurtace Water Contamination □Property Transfer Dwater Supply Well Contamination O0ther (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release T�ee of Release Product T�ee Released
(Check primary source) (Check primary cause) (Check one) (Check primary product type released)
OTank □spill D Petroleum D Gasoline/ Diesel/ 0 DieselNeg. Oil □Piping □overfill D Non-Petroleum Kerosene Blend
D Dispenser D Corrosion OBoth D Heating Oil 0 Vegetable Oil 100%
D Submersible Turbine Pump D Physical/Mechanical D Other Petroleum OE10-E20
Location Products OE21-E84 D Delivery Problem Damage (Check one) D Metals D Install Problem OE85-E99 □spill Bucket D Other □Facility D Other lnorganics D Ethanol 100% Oother D Unknown □Residence D Other Organics OE01-E09 D Unknown O0ther
Definitions presented on reverse Definitions presented on reverse
Ownershie 1.Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Oeeration Tl£ee 1.Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2. 3.
UST SYSTEM OWNER
UST Owner/Company
Address
City I State Zip Code I Telephone Number
UST SYSTEM OPERATOR UST Operator/Company
Address
City I State Zip Code I Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT Landowner
Address
City I State Zip Code I Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page2 of2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories ( e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion ( e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion ( e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined Point of Contact
Email
Email
Email
FIGURE 1SAMPLE LOCATION MAP
Rental Uniform Services of Statesville1203 Barkley Road NorthStatesville, North Carolina
Project No: 241EN01007
Drawn By: AQ
Date: 7-27-23
Reviewed By: TG
Scale: 1” ~ 100’
0’100’
Scale
N
2725 E. Millbrook Rd, Ste 121Raleigh, NC 27604(919) 871-0999
Boring/Temporary Well Location
Legend
Approximate Former Gasoline UST Location (??)
TMW - 5
ANALYTICAL REPORT
June 18, 2023
ATC Group Services LLC
Sample Delivery Group:L1623264
Samples Received:06/06/2023
Project Number:
Description:Statesville ESA
Report To:Tim Grant
2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
Entire Report Reviewed By:
June 18, 2023
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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June 19, 2023
Jason Romer
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
TMW-1 (10-12) L1623264-01 5
TMW-2 (2-4) L1623264-02 7
TMW-3 (6-8) L1623264-03 9
TMW-4 (2-4) L1623264-04 11
TMW-5 (2-4) L1623264-05 13
TMW-6 (8-10) L1623264-06 16
Qc: Quality Control Summary 19
Total Solids by Method 2540 G-2011 19
Wet Chemistry by Method 3060A/7196A 20
Metals (ICP) by Method 6010D 21
Volatile Petroleum Hydrocarbons by Method MADEPV 22
Volatile Organic Compounds (GC) by Method 8015D/GRO 23
Volatile Organic Compounds (GC/MS) by Method 8260D 24
Semi-Volatile Organic Compounds (GC) by Method 8015C 28
TPH by Method MADEPE 29
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 31
Gl: Glossary of Terms 35
Al: Accreditations & Locations 36
Sc: Sample Chain of Custody 37
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TMW-1 (10-12) L1623264-01 Solid Laura De Sousa 06/03/23 12:00 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2073149 1 06/08/23 08:56 06/08/23 09:03 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2074843 1 06/03/23 12:00 06/11/23 12:43 DWR Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-2 (2-4) L1623264-02 Solid Laura De Sousa 06/03/23 12:30 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2073149 1 06/08/23 08:56 06/08/23 09:03 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2074843 1.04 06/03/23 12:30 06/11/23 13:02 DWR Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-3 (6-8) L1623264-03 Solid Laura De Sousa 06/03/23 13:00 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2073149 1 06/08/23 08:56 06/08/23 09:03 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2074843 1.03 06/03/23 13:00 06/11/23 13:21 DWR Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-4 (2-4) L1623264-04 Solid Laura De Sousa 06/03/23 14:00 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2073149 1 06/08/23 08:56 06/08/23 09:03 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2074843 1.06 06/03/23 14:00 06/11/23 13:40 DWR Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-5 (2-4) L1623264-05 Solid Laura De Sousa 06/03/23 11:30 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2073149 1 06/08/23 08:56 06/08/23 09:03 CMK Mt. Juliet, TN
Wet Chemistry by Method 3060A/7196A WG2073391 1 06/07/23 20:00 06/08/23 09:39 JAS Mt. Juliet, TN
Metals (ICP) by Method 6010D WG2073522 1 06/07/23 22:02 06/09/23 19:49 ZSA Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG2073823 4.44 06/03/23 11:30 06/17/23 14:15 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2074843 1.11 06/03/23 11:30 06/11/23 13:59 DWR Mt. Juliet, TN
TPH by Method MADEPE WG2075877 1 06/12/23 06:36 06/12/23 20:45 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2075877 1 06/12/23 06:36 06/12/23 22:14 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2075877 5 06/12/23 06:36 06/13/23 10:36 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2073649 1 06/08/23 07:40 06/08/23 21:31 AMG Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-6 (8-10) L1623264-06 Solid Laura De Sousa 06/03/23 14:20 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2073149 1 06/08/23 08:56 06/08/23 09:03 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG2074970 25 06/03/23 14:20 06/10/23 17:32 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2074843 1 06/03/23 14:20 06/11/23 14:18 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG2073289 1 06/07/23 16:23 06/07/23 22:38 KAP Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2073649 1 06/08/23 07:40 06/08/23 17:59 AMG Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
Sample Delivery Group (SDG) Narrative
Analysis was performed from an improper container for the following samples.
Lab Sample ID Project Sample ID Method
L1623264-05 TMW-5 (2-4)MADEPE
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Jason Romer
Project Manager
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SAMPLE RESULTS - 05
L1623264
TMW-5 (2-4)
Collected date/time: 06/03/23 11:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 73.1 1 06/08/2023 09:03 WG2073149
Wet Chemistry by Method 3060A/7196A
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Chromium,Hexavalent 2.17 J J6 0.876 2.74 1 06/08/2023 09:39 WG2073391
Metals (ICP) by Method 6010D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Chromium 85.2 0.182 1.37 1 06/09/2023 19:49 WG2073522
Lead 52.2 0.285 0.684 1 06/09/2023 19:49 WG2073522
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics U 12.6 37.7 4.44 06/17/2023 14:15 WG2073823
Unadjusted C9-C12 Aliphatics U 12.6 37.7 4.44 06/17/2023 14:15 WG2073823
Unadjusted C9-C10 Aromatics U 12.6 37.7 4.44 06/17/2023 14:15 WG2073823
Total VPH U 12.6 37.7 4.44 06/17/2023 14:15 WG2073823
(S) 2,5-Dibromotoluene(FID)117 70.0-130 06/17/2023 14:15 WG2073823
(S) 2,5-Dibromotoluene(PID)123 70.0-130 06/17/2023 14:15 WG2073823
Sample Narrative:
L1623264-05 WG2073823: Lowest possible dilution due to sample foaming.
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0688 0.0943 1.11 06/11/2023 13:59 WG2074843
Acrylonitrile U C3 0.00681 0.0236 1.11 06/11/2023 13:59 WG2074843
Benzene U 0.000880 0.00189 1.11 06/11/2023 13:59 WG2074843
Bromobenzene U J3 0.00170 0.0236 1.11 06/11/2023 13:59 WG2074843
Bromodichloromethane U 0.00137 0.00472 1.11 06/11/2023 13:59 WG2074843
Bromoform U 0.00221 0.0472 1.11 06/11/2023 13:59 WG2074843
Bromomethane U 0.00372 0.0236 1.11 06/11/2023 13:59 WG2074843
n-Butylbenzene U 0.00990 0.0236 1.11 06/11/2023 13:59 WG2074843
sec-Butylbenzene U 0.00544 0.0236 1.11 06/11/2023 13:59 WG2074843
tert-Butylbenzene U 0.00367 0.00943 1.11 06/11/2023 13:59 WG2074843
Carbon tetrachloride U 0.00169 0.00943 1.11 06/11/2023 13:59 WG2074843
Chlorobenzene U 0.000396 0.00472 1.11 06/11/2023 13:59 WG2074843
Chlorodibromomethane U 0.00115 0.00472 1.11 06/11/2023 13:59 WG2074843
Chloroethane U 0.00321 0.00943 1.11 06/11/2023 13:59 WG2074843
Chloroform U 0.00194 0.00472 1.11 06/11/2023 13:59 WG2074843
Chloromethane U C3 0.00820 0.0236 1.11 06/11/2023 13:59 WG2074843
2-Chlorotoluene U J3 0.00163 0.00472 1.11 06/11/2023 13:59 WG2074843
4-Chlorotoluene U J3 J4 0.000849 0.00943 1.11 06/11/2023 13:59 WG2074843
1,2-Dibromo-3-Chloropropane U 0.00735 0.0472 1.11 06/11/2023 13:59 WG2074843
1,2-Dibromoethane U 0.00122 0.00472 1.11 06/11/2023 13:59 WG2074843
Dibromomethane U 0.00141 0.00943 1.11 06/11/2023 13:59 WG2074843
1,2-Dichlorobenzene U 0.000802 0.00943 1.11 06/11/2023 13:59 WG2074843
1,3-Dichlorobenzene U 0.00113 0.00943 1.11 06/11/2023 13:59 WG2074843
1,4-Dichlorobenzene U 0.00132 0.00943 1.11 06/11/2023 13:59 WG2074843
Dichlorodifluoromethane U 0.00304 0.00472 1.11 06/11/2023 13:59 WG2074843
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 05
L1623264
TMW-5 (2-4)
Collected date/time: 06/03/23 11:30
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
1,1-Dichloroethane U 0.000926 0.00472 1.11 06/11/2023 13:59 WG2074843
1,2-Dichloroethane U 0.00122 0.00472 1.11 06/11/2023 13:59 WG2074843
1,1-Dichloroethene U 0.00114 0.00472 1.11 06/11/2023 13:59 WG2074843
cis-1,2-Dichloroethene U 0.00138 0.00472 1.11 06/11/2023 13:59 WG2074843
trans-1,2-Dichloroethene U 0.00195 0.00943 1.11 06/11/2023 13:59 WG2074843
1,2-Dichloropropane U C3 0.00268 0.00943 1.11 06/11/2023 13:59 WG2074843
1,1-Dichloropropene U 0.00153 0.00472 1.11 06/11/2023 13:59 WG2074843
1,3-Dichloropropane U 0.000944 0.00943 1.11 06/11/2023 13:59 WG2074843
cis-1,3-Dichloropropene U 0.00143 0.00472 1.11 06/11/2023 13:59 WG2074843
trans-1,3-Dichloropropene U 0.00216 0.00943 1.11 06/11/2023 13:59 WG2074843
2,2-Dichloropropane U 0.00260 0.00472 1.11 06/11/2023 13:59 WG2074843
Di-isopropyl ether U C3 0.000773 0.00189 1.11 06/11/2023 13:59 WG2074843
Ethylbenzene U 0.00139 0.00472 1.11 06/11/2023 13:59 WG2074843
Hexachloro-1,3-butadiene U C3 0.0113 0.0472 1.11 06/11/2023 13:59 WG2074843
Isopropylbenzene U 0.000802 0.00472 1.11 06/11/2023 13:59 WG2074843
p-Isopropyltoluene U 0.00481 0.00943 1.11 06/11/2023 13:59 WG2074843
2-Butanone (MEK)U C3 0.120 0.189 1.11 06/11/2023 13:59 WG2074843
Methylene Chloride U 0.0125 0.0472 1.11 06/11/2023 13:59 WG2074843
4-Methyl-2-pentanone (MIBK)U C3 0.00430 0.0472 1.11 06/11/2023 13:59 WG2074843
Methyl tert-butyl ether U 0.000661 0.00189 1.11 06/11/2023 13:59 WG2074843
Naphthalene U C3 0.00921 0.0236 1.11 06/11/2023 13:59 WG2074843
n-Propylbenzene U J3 0.00178 0.00943 1.11 06/11/2023 13:59 WG2074843
Styrene U 0.000431 0.0236 1.11 06/11/2023 13:59 WG2074843
1,1,1,2-Tetrachloroethane U 0.00178 0.00472 1.11 06/11/2023 13:59 WG2074843
1,1,2,2-Tetrachloroethane U J3 0.00131 0.00472 1.11 06/11/2023 13:59 WG2074843
1,1,2-Trichlorotrifluoroethane U 0.00142 0.00472 1.11 06/11/2023 13:59 WG2074843
Tetrachloroethene 1.40 0.00169 0.00472 1.11 06/11/2023 13:59 WG2074843
Toluene U 0.00245 0.00943 1.11 06/11/2023 13:59 WG2074843
1,2,3-Trichlorobenzene U C3 0.0138 0.0236 1.11 06/11/2023 13:59 WG2074843
1,2,4-Trichlorobenzene U C3 0.00829 0.0236 1.11 06/11/2023 13:59 WG2074843
1,1,1-Trichloroethane U 0.00173 0.00472 1.11 06/11/2023 13:59 WG2074843
1,1,2-Trichloroethane U 0.00113 0.00472 1.11 06/11/2023 13:59 WG2074843
Trichloroethene 0.0119 0.00110 0.00189 1.11 06/11/2023 13:59 WG2074843
Trichlorofluoromethane U 0.00156 0.00472 1.11 06/11/2023 13:59 WG2074843
1,2,3-Trichloropropane U J3 0.00306 0.0236 1.11 06/11/2023 13:59 WG2074843
1,2,4-Trimethylbenzene U 0.00297 0.00943 1.11 06/11/2023 13:59 WG2074843
1,2,3-Trimethylbenzene U 0.00297 0.00943 1.11 06/11/2023 13:59 WG2074843
1,3,5-Trimethylbenzene U J3 0.00377 0.00943 1.11 06/11/2023 13:59 WG2074843
Vinyl chloride U 0.00219 0.00472 1.11 06/11/2023 13:59 WG2074843
Xylenes, Total U 0.00166 0.0123 1.11 06/11/2023 13:59 WG2074843
(S) Toluene-d8 110 75.0-131 06/11/2023 13:59 WG2074843
(S) 4-Bromofluorobenzene 102 67.0-138 06/11/2023 13:59 WG2074843
(S) 1,2-Dichloroethane-d4 91.3 70.0-130 06/11/2023 13:59 WG2074843
TPH by Method MADEPE
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics 22.3 2.97 8.89 1 06/12/2023 20:45 WG2075877
Unadjusted C19-C36 Aliphatics 259 14.9 44.5 5 06/13/2023 10:36 WG2075877
Unadjusted C11-C22 Aromatics 62.8 2.97 8.89 1 06/12/2023 22:14 WG2075877
Unadjusted Total Petroleum
Hydrocarbons 343 14.9 44.5 5 06/13/2023 10:36 WG2075877
(S) o-Terphenyl 57.8 40.0-140 06/12/2023 22:14 WG2075877
(S) 1-Chloro-octadecane 56.3 40.0-140 06/13/2023 10:36 WG2075877
(S) 1-Chloro-octadecane 56.1 40.0-140 06/12/2023 20:45 WG2075877
(S) 2-Fluorobiphenyl 82.0 40.0-140 06/12/2023 22:14 WG2075877
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 05
L1623264
TMW-5 (2-4)
Collected date/time: 06/03/23 11:30
TPH by Method MADEPE
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
(S) 2-Bromonaphthalene 88.6 40.0-140 06/12/2023 22:14 WG2075877
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00737 0.0456 1 06/08/2023 21:31 WG2073649
Acenaphthylene U 0.00642 0.0456 1 06/08/2023 21:31 WG2073649
Anthracene U 0.00811 0.0456 1 06/08/2023 21:31 WG2073649
Benzidine U 0.0856 2.28 1 06/08/2023 21:31 WG2073649
Benzo(a)anthracene U 0.00803 0.0456 1 06/08/2023 21:31 WG2073649
Benzo(b)fluoranthene U 0.00850 0.0456 1 06/08/2023 21:31 WG2073649
Benzo(k)fluoranthene U 0.00810 0.0456 1 06/08/2023 21:31 WG2073649
Benzo(g,h,i)perylene U 0.00833 0.0456 1 06/08/2023 21:31 WG2073649
Benzo(a)pyrene U 0.00847 0.0456 1 06/08/2023 21:31 WG2073649
Bis(2-chlorethoxy)methane U 0.0137 0.456 1 06/08/2023 21:31 WG2073649
Bis(2-chloroethyl)ether U 0.0150 0.456 1 06/08/2023 21:31 WG2073649
2,2-Oxybis(1-Chloropropane)U 0.0197 0.456 1 06/08/2023 21:31 WG2073649
4-Bromophenyl-phenylether U 0.0160 0.456 1 06/08/2023 21:31 WG2073649
2-Chloronaphthalene U 0.00800 0.0456 1 06/08/2023 21:31 WG2073649
4-Chlorophenyl-phenylether U 0.0159 0.456 1 06/08/2023 21:31 WG2073649
Chrysene U 0.00906 0.0456 1 06/08/2023 21:31 WG2073649
Dibenz(a,h)anthracene U 0.0126 0.0456 1 06/08/2023 21:31 WG2073649
1,2-Dichlorobenzene U 0.0135 0.456 1 06/08/2023 21:31 WG2073649
1,3-Dichlorobenzene U 0.0138 0.456 1 06/08/2023 21:31 WG2073649
1,4-Dichlorobenzene U 0.0136 0.456 1 06/08/2023 21:31 WG2073649
3,3-Dichlorobenzidine U 0.0168 0.456 1 06/08/2023 21:31 WG2073649
2,4-Dinitrotoluene U 0.0131 0.456 1 06/08/2023 21:31 WG2073649
2,6-Dinitrotoluene U 0.0149 0.456 1 06/08/2023 21:31 WG2073649
Fluoranthene U 0.00822 0.0456 1 06/08/2023 21:31 WG2073649
Fluorene U 0.00741 0.0456 1 06/08/2023 21:31 WG2073649
Hexachlorobenzene U 0.0161 0.456 1 06/08/2023 21:31 WG2073649
Hexachloro-1,3-butadiene U 0.0153 0.456 1 06/08/2023 21:31 WG2073649
Hexachlorocyclopentadiene U 0.0239 0.456 1 06/08/2023 21:31 WG2073649
Hexachloroethane U 0.0179 0.456 1 06/08/2023 21:31 WG2073649
Indeno(1,2,3-cd)pyrene U 0.0129 0.0456 1 06/08/2023 21:31 WG2073649
Isophorone U 0.0140 0.456 1 06/08/2023 21:31 WG2073649
Naphthalene U 0.0114 0.0456 1 06/08/2023 21:31 WG2073649
Nitrobenzene U 0.0159 0.456 1 06/08/2023 21:31 WG2073649
n-Nitrosodimethylamine U 0.0676 0.456 1 06/08/2023 21:31 WG2073649
n-Nitrosodiphenylamine U 0.0345 0.456 1 06/08/2023 21:31 WG2073649
n-Nitrosodi-n-propylamine U 0.0152 0.456 1 06/08/2023 21:31 WG2073649
Phenanthrene U 0.00904 0.0456 1 06/08/2023 21:31 WG2073649
Benzylbutyl phthalate 0.0480 J 0.0142 0.456 1 06/08/2023 21:31 WG2073649
Bis(2-ethylhexyl)phthalate 0.160 J 0.0577 0.456 1 06/08/2023 21:31 WG2073649
Di-n-butyl phthalate U 0.0156 0.456 1 06/08/2023 21:31 WG2073649
Diethyl phthalate U 0.0150 0.456 1 06/08/2023 21:31 WG2073649
Dimethyl phthalate U 0.0966 0.456 1 06/08/2023 21:31 WG2073649
Di-n-octyl phthalate U 0.0308 0.456 1 06/08/2023 21:31 WG2073649
Pyrene U 0.00886 0.0456 1 06/08/2023 21:31 WG2073649
1,2,4-Trichlorobenzene U 0.0142 0.456 1 06/08/2023 21:31 WG2073649
(S) 2-Fluorobiphenyl 35.5 15.0-120 06/08/2023 21:31 WG2073649
(S) Nitrobenzene-d5 33.1 10.0-122 06/08/2023 21:31 WG2073649
(S) p-Terphenyl-d14 42.5 10.0-120 06/08/2023 21:31 WG2073649
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 06
L1623264
TMW-6 (8-10)
Collected date/time: 06/03/23 14:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 72.5 1 06/08/2023 09:03 WG2073149
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction U 0.970 4.46 25 06/10/2023 17:32 WG2074970
(S) a,a,a-Trifluorotoluene(FID)103 77.0-120 06/10/2023 17:32 WG2074970
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0652 0.0893 1 06/11/2023 14:18 WG2074843
Acrylonitrile U C3 0.00645 0.0223 1 06/11/2023 14:18 WG2074843
Benzene U 0.000834 0.00179 1 06/11/2023 14:18 WG2074843
Bromobenzene U J3 0.00161 0.0223 1 06/11/2023 14:18 WG2074843
Bromodichloromethane U 0.00129 0.00446 1 06/11/2023 14:18 WG2074843
Bromoform U 0.00209 0.0446 1 06/11/2023 14:18 WG2074843
Bromomethane U 0.00352 0.0223 1 06/11/2023 14:18 WG2074843
n-Butylbenzene U 0.00937 0.0223 1 06/11/2023 14:18 WG2074843
sec-Butylbenzene U 0.00514 0.0223 1 06/11/2023 14:18 WG2074843
tert-Butylbenzene U 0.00348 0.00893 1 06/11/2023 14:18 WG2074843
Carbon tetrachloride U 0.00160 0.00893 1 06/11/2023 14:18 WG2074843
Chlorobenzene U 0.000375 0.00446 1 06/11/2023 14:18 WG2074843
Chlorodibromomethane U 0.00109 0.00446 1 06/11/2023 14:18 WG2074843
Chloroethane U 0.00304 0.00893 1 06/11/2023 14:18 WG2074843
Chloroform U 0.00184 0.00446 1 06/11/2023 14:18 WG2074843
Chloromethane U C3 0.00777 0.0223 1 06/11/2023 14:18 WG2074843
2-Chlorotoluene U J3 0.00154 0.00446 1 06/11/2023 14:18 WG2074843
4-Chlorotoluene U J3 J4 0.000803 0.00893 1 06/11/2023 14:18 WG2074843
1,2-Dibromo-3-Chloropropane U 0.00696 0.0446 1 06/11/2023 14:18 WG2074843
1,2-Dibromoethane U 0.00116 0.00446 1 06/11/2023 14:18 WG2074843
Dibromomethane U 0.00134 0.00893 1 06/11/2023 14:18 WG2074843
1,2-Dichlorobenzene U 0.000759 0.00893 1 06/11/2023 14:18 WG2074843
1,3-Dichlorobenzene U 0.00107 0.00893 1 06/11/2023 14:18 WG2074843
1,4-Dichlorobenzene U 0.00125 0.00893 1 06/11/2023 14:18 WG2074843
Dichlorodifluoromethane U 0.00287 0.00446 1 06/11/2023 14:18 WG2074843
1,1-Dichloroethane U 0.000877 0.00446 1 06/11/2023 14:18 WG2074843
1,2-Dichloroethane U 0.00116 0.00446 1 06/11/2023 14:18 WG2074843
1,1-Dichloroethene U 0.00108 0.00446 1 06/11/2023 14:18 WG2074843
cis-1,2-Dichloroethene U 0.00131 0.00446 1 06/11/2023 14:18 WG2074843
trans-1,2-Dichloroethene U 0.00186 0.00893 1 06/11/2023 14:18 WG2074843
1,2-Dichloropropane U C3 0.00254 0.00893 1 06/11/2023 14:18 WG2074843
1,1-Dichloropropene U 0.00144 0.00446 1 06/11/2023 14:18 WG2074843
1,3-Dichloropropane U 0.000895 0.00893 1 06/11/2023 14:18 WG2074843
cis-1,3-Dichloropropene U 0.00135 0.00446 1 06/11/2023 14:18 WG2074843
trans-1,3-Dichloropropene U 0.00204 0.00893 1 06/11/2023 14:18 WG2074843
2,2-Dichloropropane U 0.00246 0.00446 1 06/11/2023 14:18 WG2074843
Di-isopropyl ether U C3 0.000732 0.00179 1 06/11/2023 14:18 WG2074843
Ethylbenzene U 0.00132 0.00446 1 06/11/2023 14:18 WG2074843
Hexachloro-1,3-butadiene U C3 0.0107 0.0446 1 06/11/2023 14:18 WG2074843
Isopropylbenzene U 0.000759 0.00446 1 06/11/2023 14:18 WG2074843
p-Isopropyltoluene U 0.00455 0.00893 1 06/11/2023 14:18 WG2074843
2-Butanone (MEK)U C3 0.113 0.179 1 06/11/2023 14:18 WG2074843
Methylene Chloride U 0.0119 0.0446 1 06/11/2023 14:18 WG2074843
4-Methyl-2-pentanone (MIBK)U C3 0.00407 0.0446 1 06/11/2023 14:18 WG2074843
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073149
Total Solids by Method 2540 G-2011 L1623264-01,02,03,04,05,06
Method Blank (MB)
(MB) R3934424-1 06/08/23 09:03
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00400
L1623239-12 Original Sample (OS) • Duplicate (DUP)
(OS) L1623239-12 06/08/23 09:03 • (DUP) R3934424-3 06/08/23 09:03
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 74.0 72.5 1 1.99 10
Laboratory Control Sample (LCS)
(LCS) R3934424-2 06/08/23 09:03
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 49.9 99.9 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073391
Wet Chemistry by Method 3060A/7196A L1623264-05
Method Blank (MB)
(MB) R3934168-1 06/08/23 09:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Chromium,Hexavalent U 0.640 2.00
L1623166-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1623166-01 06/08/23 09:37 • (DUP) R3934168-3 06/08/23 09:38
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Chromium,Hexavalent 1.58 U 1 200 P1 20
Laboratory Control Sample (LCS)
(LCS) R3934168-2 06/08/23 09:37
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Chromium,Hexavalent 24.0 22.8 95.1 80.0-120
L1623264-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623264-05 06/08/23 09:39 • (MS) R3934168-4 06/08/23 09:41 • (MSD) R3934168-5 06/08/23 09:42
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Chromium,Hexavalent 27.4 2.17 25.2 25.6 84.0 85.6 1 75.0-125 1.70 20
L1623264-05 Original Sample (OS) • Matrix Spike (MS)
(OS) L1623264-05 06/08/23 09:39 • (MS) R3934168-6 06/08/23 09:42
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Chromium,Hexavalent 891 2.17 626 70.3 50 75.0-125 J6
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073522
Metals (ICP) by Method 6010D L1623264-05
Method Blank (MB)
(MB) R3935280-1 06/09/23 19:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Chromium U 0.133 1.00
Lead U 0.208 0.500
Laboratory Control Sample (LCS)
(LCS) R3935280-2 06/09/23 19:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Chromium 100 99.0 99.0 80.0-120
Lead 100 97.5 97.5 80.0-120
L1623280-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623280-01 06/09/23 19:32 • (MS) R3935280-5 06/09/23 19:40 • (MSD) R3935280-6 06/09/23 19:43
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Chromium 106 19.1 128 115 103 90.1 1 75.0-125 10.9 20
Lead 106 0.434 113 101 106 94.8 1 75.0-125 11.3 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073823
Volatile Petroleum Hydrocarbons by Method MADEPV L1623264-05
Method Blank (MB)
(MB) R3938057-3 06/17/23 02:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C5-C8 Aliphatics U 1.67 5.00
Unadjusted C9-C12 Aliphatics U 1.67 5.00
Unadjusted C9-C10 Aromatics U 1.67 5.00
Total VPH U 1.67 5.00
(S) 2,5-Dibromotoluene(FID)100 70.0-130
(S) 2,5-Dibromotoluene(PID)104 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3938057-1 06/17/23 00:32 • (LCSD) R3938057-2 06/17/23 01:04
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 60.0 59.9 59.7 99.8 99.5 70.0-130 0.334 25
Unadjusted C9-C12 Aliphatics 70.0 61.5 59.7 87.9 85.3 70.0-130 2.97 25
Unadjusted C9-C10 Aromatics 10.0 9.46 9.25 94.6 92.5 70.0-130 2.24 25
Total VPH 140 131 129 93.6 92.1 70.0-130 1.54 25
(S) 2,5-Dibromotoluene(FID) 104 106 70.0-130
(S) 2,5-Dibromotoluene(PID) 113 113 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2074970
Volatile Organic Compounds (GC) by Method 8015D/GRO L1623264-06
Method Blank (MB)
(MB) R3936113-2 06/10/23 01:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction U 0.543 2.50
(S)
a,a,a-Trifluorotoluene(FID)102 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3936113-1 06/10/23 00:13
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.41 98.4 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 106 77.0-120
L1622715-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1622715-02 06/10/23 08:34 • (MS) R3936113-3 06/10/23 22:00 • (MSD) R3936113-4 06/10/23 22:23
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 202 U 234 248 116 123 27.3 10.0-151 5.59 28
(S)
a,a,a-Trifluorotoluene(FID) 111 111 77.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2074843
Volatile Organic Compounds (GC/MS) by Method 8260D L1623264-01,02,03,04,05,06
Method Blank (MB)
(MB) R3936138-3 06/11/23 07:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2074843
Volatile Organic Compounds (GC/MS) by Method 8260D L1623264-01,02,03,04,05,06
Method Blank (MB)
(MB) R3936138-3 06/11/23 07:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene 0.000400 J 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 107 75.0-131
(S) 4-Bromofluorobenzene 127 67.0-138
(S) 1,2-Dichloroethane-d4 97.4 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936138-1 06/11/23 06:43 • (LCSD) R3936138-2 06/11/23 07:02
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.530 0.536 84.8 85.8 10.0-160 1.13 31
Acrylonitrile 0.625 0.460 0.452 73.6 72.3 45.0-153 1.75 22
Benzene 0.125 0.118 0.115 94.4 92.0 70.0-123 2.58 20
Bromobenzene 0.125 0.128 0.101 102 80.8 73.0-121 J3 23.6 20
Bromodichloromethane 0.125 0.114 0.111 91.2 88.8 73.0-121 2.67 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2074843
Volatile Organic Compounds (GC/MS) by Method 8260D L1623264-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936138-1 06/11/23 06:43 • (LCSD) R3936138-2 06/11/23 07:02
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.140 0.148 112 118 64.0-132 5.56 20
Bromomethane 0.125 0.180 0.171 144 137 56.0-147 5.13 20
n-Butylbenzene 0.125 0.101 0.0969 80.8 77.5 68.0-135 4.14 20
sec-Butylbenzene 0.125 0.128 0.114 102 91.2 74.0-130 11.6 20
tert-Butylbenzene 0.125 0.127 0.107 102 85.6 75.0-127 17.1 20
Carbon tetrachloride 0.125 0.120 0.114 96.0 91.2 66.0-128 5.13 20
Chlorobenzene 0.125 0.116 0.114 92.8 91.2 76.0-128 1.74 20
Chlorodibromomethane 0.125 0.116 0.117 92.8 93.6 74.0-127 0.858 20
Chloroethane 0.125 0.118 0.124 94.4 99.2 61.0-134 4.96 20
Chloroform 0.125 0.122 0.116 97.6 92.8 72.0-123 5.04 20
Chloromethane 0.125 0.0921 0.0848 73.7 67.8 51.0-138 8.25 20
2-Chlorotoluene 0.125 0.132 0.103 106 82.4 75.0-124 J3 24.7 20
4-Chlorotoluene 0.125 0.117 0.0882 93.6 70.6 75.0-124 J3 J4 28.1 20
1,2-Dibromo-3-Chloropropane 0.125 0.113 0.114 90.4 91.2 59.0-130 0.881 20
1,2-Dibromoethane 0.125 0.119 0.120 95.2 96.0 74.0-128 0.837 20
Dibromomethane 0.125 0.126 0.119 101 95.2 75.0-122 5.71 20
1,2-Dichlorobenzene 0.125 0.114 0.113 91.2 90.4 76.0-124 0.881 20
1,3-Dichlorobenzene 0.125 0.109 0.109 87.2 87.2 76.0-125 0.000 20
1,4-Dichlorobenzene 0.125 0.110 0.107 88.0 85.6 77.0-121 2.76 20
Dichlorodifluoromethane 0.125 0.129 0.110 103 88.0 43.0-156 15.9 20
1,1-Dichloroethane 0.125 0.107 0.105 85.6 84.0 70.0-127 1.89 20
1,2-Dichloroethane 0.125 0.103 0.0952 82.4 76.2 65.0-131 7.87 20
1,1-Dichloroethene 0.125 0.112 0.105 89.6 84.0 65.0-131 6.45 20
cis-1,2-Dichloroethene 0.125 0.128 0.122 102 97.6 73.0-125 4.80 20
trans-1,2-Dichloroethene 0.125 0.127 0.124 102 99.2 71.0-125 2.39 20
1,2-Dichloropropane 0.125 0.0937 0.0938 75.0 75.0 74.0-125 0.107 20
1,1-Dichloropropene 0.125 0.120 0.110 96.0 88.0 73.0-125 8.70 20
1,3-Dichloropropane 0.125 0.123 0.123 98.4 98.4 80.0-125 0.000 20
cis-1,3-Dichloropropene 0.125 0.106 0.103 84.8 82.4 76.0-127 2.87 20
trans-1,3-Dichloropropene 0.125 0.119 0.108 95.2 86.4 73.0-127 9.69 20
2,2-Dichloropropane 0.125 0.134 0.113 107 90.4 59.0-135 17.0 20
Di-isopropyl ether 0.125 0.0861 0.0849 68.9 67.9 60.0-136 1.40 20
Ethylbenzene 0.125 0.121 0.115 96.8 92.0 74.0-126 5.08 20
Hexachloro-1,3-butadiene 0.125 0.0905 0.0760 72.4 60.8 57.0-150 17.4 20
Isopropylbenzene 0.125 0.143 0.135 114 108 72.0-127 5.76 20
p-Isopropyltoluene 0.125 0.124 0.110 99.2 88.0 72.0-133 12.0 20
2-Butanone (MEK)0.625 0.481 0.478 77.0 76.5 30.0-160 0.626 24
Methylene Chloride 0.125 0.128 0.121 102 96.8 68.0-123 5.62 20
4-Methyl-2-pentanone (MIBK)0.625 0.483 0.483 77.3 77.3 56.0-143 0.000 20
Methyl tert-butyl ether 0.125 0.143 0.141 114 113 66.0-132 1.41 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2074843
Volatile Organic Compounds (GC/MS) by Method 8260D L1623264-01,02,03,04,05,06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936138-1 06/11/23 06:43 • (LCSD) R3936138-2 06/11/23 07:02
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.0875 0.103 70.0 82.4 59.0-130 16.3 20
n-Propylbenzene 0.125 0.120 0.0972 96.0 77.8 74.0-126 J3 21.0 20
Styrene 0.125 0.123 0.129 98.4 103 72.0-127 4.76 20
1,1,1,2-Tetrachloroethane 0.125 0.127 0.127 102 102 74.0-129 0.000 20
1,1,2,2-Tetrachloroethane 0.125 0.157 0.106 126 84.8 68.0-128 J3 38.8 20
1,1,2-Trichlorotrifluoroethane 0.125 0.125 0.120 100 96.0 61.0-139 4.08 20
Tetrachloroethene 0.125 0.114 0.114 91.2 91.2 70.0-136 0.000 20
Toluene 0.125 0.116 0.113 92.8 90.4 75.0-121 2.62 20
1,2,3-Trichlorobenzene 0.125 0.0862 0.0955 69.0 76.4 59.0-139 10.2 20
1,2,4-Trichlorobenzene 0.125 0.0834 0.0842 66.7 67.4 62.0-137 0.955 20
1,1,1-Trichloroethane 0.125 0.141 0.134 113 107 69.0-126 5.09 20
1,1,2-Trichloroethane 0.125 0.125 0.123 100 98.4 78.0-123 1.61 20
Trichloroethene 0.125 0.120 0.128 96.0 102 76.0-126 6.45 20
Trichlorofluoromethane 0.125 0.125 0.128 100 102 61.0-142 2.37 20
1,2,3-Trichloropropane 0.125 0.155 0.126 124 101 67.0-129 J3 20.6 20
1,2,4-Trimethylbenzene 0.125 0.127 0.116 102 92.8 70.0-126 9.05 20
1,2,3-Trimethylbenzene 0.125 0.116 0.118 92.8 94.4 74.0-124 1.71 20
1,3,5-Trimethylbenzene 0.125 0.125 0.101 100 80.8 73.0-127 J3 21.2 20
Vinyl chloride 0.125 0.119 0.115 95.2 92.0 63.0-134 3.42 20
Xylenes, Total 0.375 0.363 0.366 96.8 97.6 72.0-127 0.823 20
(S) Toluene-d8 107 108 75.0-131
(S) 4-Bromofluorobenzene 111 105 67.0-138
(S) 1,2-Dichloroethane-d4 97.6 97.0 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073289
Semi-Volatile Organic Compounds (GC) by Method 8015C L1623264-06
Method Blank (MB)
(MB) R3934107-1 06/07/23 22:10
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction U 0.769 4.00
(S) o-Terphenyl 70.4 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3934107-2 06/07/23 22:24
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) High Fraction 50.0 36.2 72.4 50.0-150
(S) o-Terphenyl 72.2 18.0-148
L1623264-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623264-06 06/07/23 22:38 • (MS) R3934107-3 06/07/23 22:52 • (MSD) R3934107-4 06/07/23 23:06
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 67.3 U 45.2 42.1 67.2 62.5 1 50.0-150 7.27 20
(S) o-Terphenyl 66.6 63.4 18.0-148
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075877
TPH by Method MADEPE L1623264-05
Method Blank (MB)
(MB) R3935835-1 06/12/23 17:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C9-C18 Aliphatics U 2.17 6.50
Unadjusted C19-C36 Aliphatics 3.01 J 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons 3.01 J 2.17 6.50
(S) 1-Chloro-octadecane 52.8 40.0-140
Method Blank (MB)
(MB) R3935835-4 06/12/23 18:32
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C11-C22 Aromatics 2.83 J 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons 2.83 J 2.17 6.50
(S) o-Terphenyl 57.7 40.0-140
(S) 2-Fluorobiphenyl 73.7 40.0-140
(S) 2-Bromonaphthalene 80.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935835-2 06/12/23 17:48 • (LCSD) R3935835-3 06/12/23 18:10
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 39.9 25.9 25.4 64.9 63.7 40.0-140 1.95 25
Unadjusted C19-C36 Aliphatics 53.2 42.7 41.4 80.3 77.8 40.0-140 3.09 25
(S) 1-Chloro-octadecane 69.4 65.0 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935835-5 06/12/23 18:54 • (LCSD) R3935835-6 06/12/23 19:17
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 113 76.5 72.2 67.7 63.9 40.0-140 5.78 25
(S) o-Terphenyl 68.4 63.7 40.0-140
(S) 2-Fluorobiphenyl 79.7 80.5 40.0-140
(S) 2-Bromonaphthalene 86.3 87.2 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075877
TPH by Method MADEPE L1623264-05
L1622559-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1622559-01 06/13/23 04:49 • (MS) R3935835-7 06/13/23 05:11 • (MSD) R3935835-8 06/13/23 06:01
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 48.5 U 22.0 31.7 45.5 65.4 1 40.0-140 36.0 50
Unadjusted C19-C36 Aliphatics 64.6 7.30 32.9 52.7 39.6 70.3 1 40.0-140 J6 46.3 50
(S) 1-Chloro-octadecane 42.2 65.9 40.0-140
L1622559-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1622559-01 06/13/23 10:14 • (MS) R3935835-10 06/13/23 09:44 • (MSD) R3935835-9 06/13/23 09:22
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg %%%%%
Unadjusted C11-C22 Aromatics 137 2.91 81.7 90.5 57.5 63.9 1 40.0-140 10.2 50
(S) o-Terphenyl 59.1 65.7 40.0-140
(S) 2-Fluorobiphenyl 79.4 77.7 40.0-140
(S) 2-Bromonaphthalene 86.2 84.1 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073649
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1623264-05,06
Method Blank (MB)
(MB) R3934927-3 06/08/23 17:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane)U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
1,2-Dichlorobenzene U 0.00987 0.333
1,3-Dichlorobenzene U 0.0101 0.333
1,4-Dichlorobenzene U 0.00991 0.333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073649
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1623264-05,06
Method Blank (MB)
(MB) R3934927-3 06/08/23 17:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
(S) 2-Fluorobiphenyl 51.4 15.0-120
(S) Nitrobenzene-d5 48.0 10.0-122
(S) p-Terphenyl-d14 63.7 10.0-120
Laboratory Control Sample (LCS)
(LCS) R3934927-1 06/08/23 16:34
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.320 48.0 38.0-120
Acenaphthylene 0.666 0.340 51.1 40.0-120
Anthracene 0.666 0.360 54.1 42.0-120
Benzidine 1.33 0.281 21.1 10.0-120
Benzo(a)anthracene 0.666 0.383 57.5 44.0-120
Benzo(b)fluoranthene 0.666 0.361 54.2 43.0-120
Benzo(k)fluoranthene 0.666 0.378 56.8 44.0-120
Benzo(g,h,i)perylene 0.666 0.397 59.6 43.0-120
Benzo(a)pyrene 0.666 0.413 62.0 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.248 37.2 20.0-120
Bis(2-chloroethyl)ether 0.666 0.252 37.8 16.0-120
2,2-Oxybis(1-Chloropropane)0.666 0.297 44.6 23.0-120
4-Bromophenyl-phenylether 0.666 0.341 51.2 40.0-120
2-Chloronaphthalene 0.666 0.306 45.9 35.0-120
4-Chlorophenyl-phenylether 0.666 0.349 52.4 40.0-120
Chrysene 0.666 0.382 57.4 43.0-120
Dibenz(a,h)anthracene 0.666 0.404 60.7 44.0-120
1,2-Dichlorobenzene 0.666 0.301 45.2 32.0-120
1,3-Dichlorobenzene 0.666 0.273 41.0 30.0-120
1,4-Dichlorobenzene 0.666 0.284 42.6 31.0-120
3,3-Dichlorobenzidine 1.33 0.660 49.6 28.0-120
2,4-Dinitrotoluene 0.666 0.363 54.5 45.0-120
2,6-Dinitrotoluene 0.666 0.348 52.3 42.0-120
Fluoranthene 0.666 0.364 54.7 44.0-120
Fluorene 0.666 0.339 50.9 41.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073649
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1623264-05,06
Laboratory Control Sample (LCS)
(LCS) R3934927-1 06/08/23 16:34
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexachlorobenzene 0.666 0.372 55.9 39.0-120
Hexachloro-1,3-butadiene 0.666 0.261 39.2 15.0-120
Hexachlorocyclopentadiene 0.666 0.364 54.7 15.0-120
Hexachloroethane 0.666 0.281 42.2 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.369 55.4 45.0-120
Isophorone 0.666 0.264 39.6 23.0-120
Naphthalene 0.666 0.241 36.2 18.0-120
Nitrobenzene 0.666 0.228 34.2 17.0-120
n-Nitrosodimethylamine 0.666 0.216 32.4 10.0-125
n-Nitrosodiphenylamine 0.666 0.343 51.5 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.297 44.6 26.0-120
Phenanthrene 0.666 0.342 51.4 42.0-120
Benzylbutyl phthalate 0.666 0.378 56.8 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.380 57.1 41.0-120
Di-n-butyl phthalate 0.666 0.386 58.0 43.0-120
Diethyl phthalate 0.666 0.367 55.1 43.0-120
Dimethyl phthalate 0.666 0.353 53.0 43.0-120
Di-n-octyl phthalate 0.666 0.363 54.5 40.0-120
Pyrene 0.666 0.364 54.7 41.0-120
1,2,4-Trichlorobenzene 0.666 0.262 39.3 17.0-120
(S) 2-Fluorobiphenyl 46.8 15.0-120
(S) Nitrobenzene-d5 37.5 10.0-122
(S) p-Terphenyl-d14 58.9 10.0-120
L1623082-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623082-01 06/08/23 19:02 • (MS) R3934927-4 06/08/23 19:24 • (MSD) R3934927-5 06/08/23 19:45
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.641 U 0.280 0.283 43.6 42.6 1 18.0-120 1.07 32
Acenaphthylene 0.641 U 0.296 0.296 46.1 44.5 1 25.0-120 0.000 32
Anthracene 0.641 U 0.308 0.311 48.0 46.8 1 22.0-120 0.976 29
Benzidine 1.29 U 0.338 0.400 26.2 30.2 1 10.0-120 16.9 40
Benzo(a)anthracene 0.641 U 0.335 0.326 52.2 49.1 1 25.0-120 2.74 29
Benzo(b)fluoranthene 0.641 0.00914 0.322 0.312 48.7 45.6 1 19.0-122 3.17 31
Benzo(k)fluoranthene 0.641 U 0.309 0.305 48.1 45.9 1 23.0-120 1.31 30
Benzo(g,h,i)perylene 0.641 0.00670 0.330 0.318 50.4 46.9 1 10.0-120 3.73 33
Benzo(a)pyrene 0.641 U 0.354 0.349 55.2 52.6 1 24.0-120 1.43 30
Bis(2-chlorethoxy)methane 0.641 U 0.228 0.228 35.6 34.4 1 10.0-120 0.000 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073649
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1623264-05,06
L1623082-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623082-01 06/08/23 19:02 • (MS) R3934927-4 06/08/23 19:24 • (MSD) R3934927-5 06/08/23 19:45
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Bis(2-chloroethyl)ether 0.641 U 0.269 0.271 42.0 40.9 1 10.0-120 0.743 40
2,2-Oxybis(1-Chloropropane)0.641 U 0.269 0.275 42.0 41.5 1 10.0-120 2.21 40
4-Bromophenyl-phenylether 0.641 U 0.300 0.300 46.7 45.2 1 27.0-120 0.000 30
2-Chloronaphthalene 0.641 U 0.269 0.271 42.0 40.9 1 20.0-120 0.743 32
4-Chlorophenyl-phenylether 0.641 U 0.292 0.294 45.5 44.2 1 24.0-120 0.687 29
Chrysene 0.641 U 0.331 0.321 51.6 48.3 1 21.0-120 3.09 29
Dibenz(a,h)anthracene 0.641 U 0.338 0.328 52.7 49.4 1 10.0-120 3.02 32
1,2-Dichlorobenzene 0.641 U 0.287 0.276 44.7 41.7 1 10.0-120 3.57 38
1,3-Dichlorobenzene 0.641 U 0.254 0.255 39.7 38.5 1 10.0-120 0.394 40
1,4-Dichlorobenzene 0.641 U 0.260 0.257 40.6 38.8 1 10.0-120 1.17 39
3,3-Dichlorobenzidine 1.29 U 0.631 0.625 49.1 47.1 1 10.0-120 0.960 34
2,4-Dinitrotoluene 0.641 U 0.318 0.319 49.5 48.0 1 30.0-120 0.316 31
2,6-Dinitrotoluene 0.641 U 0.309 0.311 48.1 46.8 1 25.0-120 0.649 31
Fluoranthene 0.641 0.00763 0.321 0.318 48.8 46.7 1 18.0-126 0.945 32
Fluorene 0.641 U 0.288 0.289 44.8 43.5 1 25.0-120 0.349 30
Hexachlorobenzene 0.641 U 0.317 0.320 49.4 48.2 1 27.0-120 0.948 28
Hexachloro-1,3-butadiene 0.641 U 0.245 0.248 38.2 37.4 1 10.0-120 1.22 38
Hexachlorocyclopentadiene 0.641 U 0.300 0.300 46.7 45.2 1 10.0-120 0.000 40
Hexachloroethane 0.641 U 0.249 0.250 38.9 37.7 1 10.0-120 0.402 40
Indeno(1,2,3-cd)pyrene 0.641 U 0.323 0.316 50.3 47.6 1 10.0-120 2.20 32
Isophorone 0.641 U 0.237 0.241 37.0 36.4 1 13.0-120 1.68 34
Naphthalene 0.641 U 0.225 0.226 35.1 34.1 1 10.0-120 0.445 35
Nitrobenzene 0.641 U 0.211 0.214 32.9 32.3 1 10.0-120 1.42 36
n-Nitrosodimethylamine 0.641 U 0.184 0.178 28.7 26.8 1 10.0-127 3.33 40
n-Nitrosodiphenylamine 0.641 U 0.294 0.300 45.8 45.2 1 17.0-120 2.03 29
n-Nitrosodi-n-propylamine 0.641 U 0.276 0.271 43.1 40.9 1 10.0-120 1.83 37
Phenanthrene 0.641 U 0.290 0.291 45.1 43.8 1 17.0-120 0.347 31
Benzylbutyl phthalate 0.641 U 0.358 0.348 55.8 52.4 1 23.0-120 2.85 30
Bis(2-ethylhexyl)phthalate 0.641 U 0.370 0.362 57.7 54.5 1 17.0-126 2.20 30
Di-n-butyl phthalate 0.641 U 0.334 0.334 52.0 50.3 1 30.0-120 0.000 29
Diethyl phthalate 0.641 U 0.309 0.310 48.1 46.7 1 26.0-120 0.325 28
Dimethyl phthalate 0.641 U 0.305 0.302 47.5 45.5 1 25.0-120 0.995 29
Di-n-octyl phthalate 0.641 U 0.365 0.352 56.9 53.0 1 21.0-123 3.65 29
Pyrene 0.641 0.00766 0.325 0.316 49.4 46.4 1 16.0-121 2.83 32
1,2,4-Trichlorobenzene 0.641 U 0.242 0.244 37.8 36.8 1 12.0-120 0.826 37
(S) 2-Fluorobiphenyl 48.0 41.2 15.0-120
(S) Nitrobenzene-d5 40.8 35.2 10.0-122
(S) p-Terphenyl-d14 58.0 48.8 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ANALYTICAL REPORT
June 18, 2023
ATC Group Services LLC
Sample Delivery Group:L1623263
Samples Received:06/06/2023
Project Number:
Description:Statesville ESA
Report To:Tim Grant
2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
Entire Report Reviewed By:
June 18, 2023
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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June 19, 2023
Jason Romer
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
TMW-1 L1623263-01 5
TMW-2 L1623263-02 7
TMW-3 L1623263-03 9
TMW-4 L1623263-04 11
TMW-5 L1623263-05 13
TMW-6 L1623263-06 16
Qc: Quality Control Summary 19
Metals (ICP) by Method 6010D 19
Volatile Petroleum Hydrocarbons by Method MADEPV 20
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 21
Volatile Organic Compounds (GC/MS) by Method 8260D 30
TPH by Method MADEPE 39
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 40
Gl: Glossary of Terms 44
Al: Accreditations & Locations 45
Sc: Sample Chain of Custody 46
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TMW-1 L1623263-01 GW Laura De Sousa 06/03/23 12:35 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260D WG2075206 1 06/10/23 19:50 06/10/23 19:50 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2076103 200 06/14/23 03:43 06/14/23 03:43 ACG Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-2 L1623263-02 GW Laura De Sousa 06/03/23 12:50 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260D WG2075206 1 06/10/23 20:12 06/10/23 20:12 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2076103 1 06/14/23 02:38 06/14/23 02:38 ACG Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-3 L1623263-03 GW Laura De Sousa 06/03/23 13:40 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260D WG2075206 1 06/10/23 20:34 06/10/23 20:34 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2076103 1 06/14/23 03:00 06/14/23 03:00 ACG Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-4 L1623263-04 GW Laura De Sousa 06/03/23 14:20 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260D WG2075212 1 06/11/23 09:15 06/11/23 09:15 DWR Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-5 L1623263-05 GW Laura De Sousa 06/03/23 11:55 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Metals (ICP) by Method 6010D WG2073611 1 06/08/23 10:02 06/12/23 01:11 SPL Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG2078820 5 06/16/23 21:57 06/16/23 21:57 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2077679 20 06/15/23 05:06 06/15/23 05:06 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2078149 20 06/15/23 14:40 06/15/23 14:40 JHH Mt. Juliet, TN
TPH by Method MADEPE WG2074045 1.05 06/08/23 03:55 06/10/23 12:51 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2074045 1.05 06/08/23 03:55 06/11/23 17:12 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2073715 1.05 06/09/23 06:26 06/09/23 16:08 JCH Mt. Juliet, TN
Collected by Collected date/time Received date/time
TMW-6 L1623263-06 GW Laura De Sousa 06/03/23 14:40 06/06/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG2078820 1 06/16/23 21:24 06/16/23 21:24 NCC Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG2075083 2 06/11/23 03:30 06/11/23 03:30 DYW Mt. Juliet, TN
TPH by Method MADEPE WG2074045 1.18 06/08/23 03:55 06/10/23 13:13 DMG Mt. Juliet, TN
TPH by Method MADEPE WG2074045 1.18 06/08/23 03:55 06/12/23 03:04 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG2073715 1.25 06/09/23 06:26 06/09/23 16:29 JCH Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
Sample Delivery Group (SDG) Narrative
An aliquot for analysis was taken from the original container received due to the level of sediment present in the sample.
Rinsing of the original sample container for inclusion in the sample extraction was not performed.
Lab Sample ID Project Sample ID Method
L1623263-05 TMW-5 MADEPE, 625.1
L1623263-06 TMW-6 625.1
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Jason Romer
Project Manager
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SAMPLE RESULTS - 05
L1623263
TMW-5
Collected date/time: 06/03/23 11:55
Metals (ICP) by Method 6010D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Chromium 1.56 J 1.40 10.0 1 06/12/2023 01:11 WG2073611
Lead U 2.99 6.00 1 06/12/2023 01:11 WG2073611
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 1270 167 500 5 06/16/2023 21:57 WG2078820
Unadjusted C9-C12 Aliphatics 9150 167 500 5 06/16/2023 21:57 WG2078820
Unadjusted C9-C10 Aromatics 2650 167 500 5 06/16/2023 21:57 WG2078820
Total VPH 13100 167 500 5 06/16/2023 21:57 WG2078820
(S) 2,5-Dibromotoluene(FID)113 70.0-130 06/16/2023 21:57 WG2078820
(S) 2,5-Dibromotoluene(PID)112 70.0-130 06/16/2023 21:57 WG2078820
Volatile Organic Compounds (GC/MS) by Method 6200B-2011/8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 226 1000 20 06/15/2023 05:06 WG2077679
Acrolein U 50.8 1000 20 06/15/2023 05:06 WG2077679
Acrylonitrile U 13.4 200 20 06/15/2023 05:06 WG2077679
Benzene U 1.88 20.0 20 06/15/2023 05:06 WG2077679
Bromobenzene U 2.36 20.0 20 06/15/2023 05:06 WG2077679
Bromodichloromethane U 2.72 20.0 20 06/15/2023 05:06 WG2077679
Bromoform U 2.58 20.0 20 06/15/2023 05:06 WG2077679
Bromomethane U C4 12.1 100 20 06/15/2023 14:40 WG2078149
n-Butylbenzene 5.50 J 3.14 20.0 20 06/15/2023 05:06 WG2077679
sec-Butylbenzene U 2.50 20.0 20 06/15/2023 05:06 WG2077679
tert-Butylbenzene U 2.54 20.0 20 06/15/2023 05:06 WG2077679
Carbon tetrachloride U 2.56 20.0 20 06/15/2023 05:06 WG2077679
Chlorobenzene U 2.32 20.0 20 06/15/2023 05:06 WG2077679
Chlorodibromomethane U 2.80 20.0 20 06/15/2023 05:06 WG2077679
Chloroethane U 3.84 100 20 06/15/2023 05:06 WG2077679
Chloroform 5.19 J 2.22 100 20 06/15/2023 05:06 WG2077679
Chloromethane U J4 19.2 50.0 20 06/15/2023 05:06 WG2077679
2-Chlorotoluene U 2.12 20.0 20 06/15/2023 05:06 WG2077679
4-Chlorotoluene U 2.28 20.0 20 06/15/2023 05:06 WG2077679
1,2-Dibromo-3-Chloropropane U 5.52 100 20 06/15/2023 05:06 WG2077679
1,2-Dibromoethane U 2.52 20.0 20 06/15/2023 05:06 WG2077679
Dibromomethane U 2.44 20.0 20 06/15/2023 05:06 WG2077679
1,2-Dichlorobenzene U 2.14 20.0 20 06/15/2023 05:06 WG2077679
1,3-Dichlorobenzene U 2.20 20.0 20 06/15/2023 05:06 WG2077679
1,4-Dichlorobenzene U 2.40 20.0 20 06/15/2023 05:06 WG2077679
Dichlorodifluoromethane U 7.48 100 20 06/15/2023 05:06 WG2077679
1,1-Dichloroethane U 2.00 20.0 20 06/15/2023 05:06 WG2077679
1,2-Dichloroethane U 1.64 20.0 20 06/15/2023 05:06 WG2077679
1,1-Dichloroethene U 3.76 20.0 20 06/15/2023 05:06 WG2077679
cis-1,2-Dichloroethene U 2.52 20.0 20 06/15/2023 05:06 WG2077679
trans-1,2-Dichloroethene U 2.98 20.0 20 06/15/2023 05:06 WG2077679
1,2-Dichloropropane U 2.98 20.0 20 06/15/2023 05:06 WG2077679
1,1-Dichloropropene U 2.84 20.0 20 06/15/2023 05:06 WG2077679
1,3-Dichloropropane U 2.20 20.0 20 06/15/2023 05:06 WG2077679
2,2-Dichloropropane U 3.22 20.0 20 06/15/2023 05:06 WG2077679
Di-isopropyl ether 6.66 J 2.10 20.0 20 06/15/2023 05:06 WG2077679
Ethylbenzene 1100 2.74 20.0 20 06/15/2023 05:06 WG2077679
Hexachloro-1,3-butadiene U 6.74 20.0 20 06/15/2023 05:06 WG2077679
Isopropylbenzene 46.2 2.10 20.0 20 06/15/2023 05:06 WG2077679
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 05
L1623263
TMW-5
Collected date/time: 06/03/23 11:55
Volatile Organic Compounds (GC/MS) by Method 6200B-2011/8260D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
p-Isopropyltoluene 19.9 J 2.40 20.0 20 06/15/2023 05:06 WG2077679
2-Butanone (MEK)U 23.8 200 20 06/15/2023 05:06 WG2077679
Methylene Chloride U 8.60 100 20 06/15/2023 05:06 WG2077679
4-Methyl-2-pentanone (MIBK)U 9.56 200 20 06/15/2023 05:06 WG2077679
Methyl tert-butyl ether 699 2.02 20.0 20 06/15/2023 05:06 WG2077679
Naphthalene 334 20.0 100 20 06/15/2023 05:06 WG2077679
n-Propylbenzene 138 1.99 20.0 20 06/15/2023 05:06 WG2077679
Styrene U 2.36 20.0 20 06/15/2023 05:06 WG2077679
1,1,1,2-Tetrachloroethane U 2.94 20.0 20 06/15/2023 05:06 WG2077679
1,1,2,2-Tetrachloroethane U 2.66 20.0 20 06/15/2023 05:06 WG2077679
Tetrachloroethene 322 6.00 20.0 20 06/15/2023 05:06 WG2077679
Toluene 196 5.56 20.0 20 06/15/2023 05:06 WG2077679
1,2,3-Trichlorobenzene U 4.60 20.0 20 06/15/2023 05:06 WG2077679
1,2,4-Trichlorobenzene U 9.62 20.0 20 06/15/2023 05:06 WG2077679
1,1,1-Trichloroethane U 2.98 20.0 20 06/15/2023 05:06 WG2077679
1,1,2-Trichloroethane U 3.16 20.0 20 06/15/2023 05:06 WG2077679
Trichloroethene U 3.80 20.0 20 06/15/2023 05:06 WG2077679
Trichlorofluoromethane U 3.20 100 20 06/15/2023 05:06 WG2077679
1,2,3-Trichloropropane U 4.74 50.0 20 06/15/2023 05:06 WG2077679
1,2,4-Trimethylbenzene 1260 6.44 20.0 20 06/15/2023 05:06 WG2077679
1,3,5-Trimethylbenzene 442 2.08 20.0 20 06/15/2023 05:06 WG2077679
Vinyl chloride U 4.68 20.0 20 06/15/2023 05:06 WG2077679
o-Xylene 2050 3.48 20.0 20 06/15/2023 05:06 WG2077679
m&p-Xylenes 4330 8.60 40.0 20 06/15/2023 05:06 WG2077679
(S) Toluene-d8 112 80.0-120 06/15/2023 05:06 WG2077679
(S) Toluene-d8 111 80.0-120 06/15/2023 14:40 WG2078149
(S) 4-Bromofluorobenzene 98.0 77.0-126 06/15/2023 05:06 WG2077679
(S) 4-Bromofluorobenzene 95.9 77.0-126 06/15/2023 14:40 WG2078149
(S) 1,2-Dichloroethane-d4 127 70.0-130 06/15/2023 05:06 WG2077679
(S) 1,2-Dichloroethane-d4 124 70.0-130 06/15/2023 14:40 WG2078149
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics U J3 35.0 105 1.05 06/11/2023 17:12 WG2074045
Unadjusted C19-C36 Aliphatics 76.7 B J J3 35.0 105 1.05 06/11/2023 17:12 WG2074045
Unadjusted C11-C22 Aromatics 564 35.0 105 1.05 06/10/2023 12:51 WG2074045
Unadjusted Total Petroleum
Hydrocarbons 641 35.0 105 1.05 06/10/2023 12:51 WG2074045
(S) o-Terphenyl 61.8 40.0-140 06/10/2023 12:51 WG2074045
(S) 1-Chloro-octadecane 51.3 40.0-140 06/11/2023 17:12 WG2074045
(S) 2-Fluorobiphenyl 84.0 40.0-140 06/10/2023 12:51 WG2074045
(S) 2-Bromonaphthalene 84.5 40.0-140 06/10/2023 12:51 WG2074045
Sample Narrative:
L1623263-05 WG2074045: Dilution due to sample volume.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.332 1.05 1.05 06/09/2023 16:08 WG2073715
Acenaphthylene U 0.324 1.05 1.05 06/09/2023 16:08 WG2073715
Anthracene U 0.306 1.05 1.05 06/09/2023 16:08 WG2073715
Benzidine U 4.54 10.5 1.05 06/09/2023 16:08 WG2073715
Benzo(a)anthracene U 0.102 1.05 1.05 06/09/2023 16:08 WG2073715
Benzo(b)fluoranthene U 0.0941 1.05 1.05 06/09/2023 16:08 WG2073715
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 05
L1623263
TMW-5
Collected date/time: 06/03/23 11:55
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzo(k)fluoranthene U 0.373 1.05 1.05 06/09/2023 16:08 WG2073715
Benzo(g,h,i)perylene U 0.169 1.05 1.05 06/09/2023 16:08 WG2073715
Benzo(a)pyrene U 0.357 1.05 1.05 06/09/2023 16:08 WG2073715
Bis(2-chlorethoxy)methane U 0.345 10.5 1.05 06/09/2023 16:08 WG2073715
Bis(2-chloroethyl)ether U 1.70 10.5 1.05 06/09/2023 16:08 WG2073715
2,2-Oxybis(1-Chloropropane)U 0.467 10.5 1.05 06/09/2023 16:08 WG2073715
4-Bromophenyl-phenylether U 0.352 10.5 1.05 06/09/2023 16:08 WG2073715
2-Chloronaphthalene U 0.347 1.05 1.05 06/09/2023 16:08 WG2073715
4-Chlorophenyl-phenylether U 0.318 10.5 1.05 06/09/2023 16:08 WG2073715
Chrysene U 0.349 1.05 1.05 06/09/2023 16:08 WG2073715
Dibenz(a,h)anthracene U 0.293 1.05 1.05 06/09/2023 16:08 WG2073715
1,2-Dichlorobenzene U 0.357 10.5 1.05 06/09/2023 16:08 WG2073715
1,3-Dichlorobenzene U 0.383 10.5 1.05 06/09/2023 16:08 WG2073715
1,4-Dichlorobenzene U 0.338 10.5 1.05 06/09/2023 16:08 WG2073715
3,3-Dichlorobenzidine U 2.12 10.5 1.05 06/09/2023 16:08 WG2073715
2,4-Dinitrotoluene U 1.73 10.5 1.05 06/09/2023 16:08 WG2073715
2,6-Dinitrotoluene U 0.293 10.5 1.05 06/09/2023 16:08 WG2073715
Fluoranthene U 0.326 1.05 1.05 06/09/2023 16:08 WG2073715
Fluorene U 0.339 1.05 1.05 06/09/2023 16:08 WG2073715
Hexachlorobenzene U 0.358 1.05 1.05 06/09/2023 16:08 WG2073715
Hexachloro-1,3-butadiene U 0.345 10.5 1.05 06/09/2023 16:08 WG2073715
Hexachlorocyclopentadiene U 2.45 10.5 1.05 06/09/2023 16:08 WG2073715
Hexachloroethane U 0.383 10.5 1.05 06/09/2023 16:08 WG2073715
Indeno(1,2,3-cd)pyrene U 0.293 1.05 1.05 06/09/2023 16:08 WG2073715
Isophorone U 0.286 10.5 1.05 06/09/2023 16:08 WG2073715
Naphthalene 221 0.391 1.05 1.05 06/09/2023 16:08 WG2073715
Nitrobenzene U 0.385 10.5 1.05 06/09/2023 16:08 WG2073715
n-Nitrosodimethylamine U 1.32 10.5 1.05 06/09/2023 16:08 WG2073715
n-Nitrosodiphenylamine U 1.25 10.5 1.05 06/09/2023 16:08 WG2073715
n-Nitrosodi-n-propylamine U 0.423 10.5 1.05 06/09/2023 16:08 WG2073715
Phenanthrene U 0.384 1.05 1.05 06/09/2023 16:08 WG2073715
Benzylbutyl phthalate U 0.289 3.15 1.05 06/09/2023 16:08 WG2073715
Bis(2-ethylhexyl)phthalate U 0.744 3.15 1.05 06/09/2023 16:08 WG2073715
Di-n-butyl phthalate U 0.279 3.15 1.05 06/09/2023 16:08 WG2073715
Diethyl phthalate U 0.296 3.15 1.05 06/09/2023 16:08 WG2073715
Dimethyl phthalate U 0.297 3.15 1.05 06/09/2023 16:08 WG2073715
Di-n-octyl phthalate U 0.292 3.15 1.05 06/09/2023 16:08 WG2073715
Pyrene U 0.347 1.05 1.05 06/09/2023 16:08 WG2073715
1,2,4-Trichlorobenzene U 0.373 10.5 1.05 06/09/2023 16:08 WG2073715
(S) Nitrobenzene-d5 111 15.0-314 06/09/2023 16:08 WG2073715
(S) 2-Fluorobiphenyl 70.0 22.0-127 06/09/2023 16:08 WG2073715
(S) p-Terphenyl-d14 75.3 29.0-141 06/09/2023 16:08 WG2073715
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073611
Metals (ICP) by Method 6010D L1623263-05
Method Blank (MB)
(MB) R3935421-1 06/12/23 00:54
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Chromium U 1.40 10.0
Lead U 2.99 6.00
Laboratory Control Sample (LCS)
(LCS) R3935421-2 06/12/23 00:57
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Chromium 1000 1020 102 80.0-120
Lead 1000 1020 102 80.0-120
L1623457-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1623457-02 06/12/23 01:00 • (MS) R3935421-4 06/12/23 01:05 • (MSD) R3935421-5 06/12/23 01:08
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Chromium 1000 U 990 967 99.0 96.7 1 75.0-125 2.41 20
Lead 1000 U 1020 993 102 99.3 1 75.0-125 2.16 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2078820
Volatile Petroleum Hydrocarbons by Method MADEPV L1623263-05,06
Method Blank (MB)
(MB) R3937880-3 06/16/23 12:02
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID)99.5 70.0-130
(S) 2,5-Dibromotoluene(PID)107 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3937880-1 06/16/23 09:50 • (LCSD) R3937880-2 06/16/23 10:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1120 1120 93.3 93.3 70.0-130 0.000 25
Unadjusted C9-C12 Aliphatics 1400 1180 1180 84.3 84.3 70.0-130 0.000 25
Unadjusted C9-C10 Aromatics 200 187 188 93.5 94.0 70.0-130 0.533 25
Total VPH 2800 2490 2490 88.9 88.9 70.0-130 0.000 25
(S) 2,5-Dibromotoluene(FID) 103 104 70.0-130
(S) 2,5-Dibromotoluene(PID) 113 114 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075083
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1623263-06
Method Blank (MB)
(MB) R3935681-3 06/10/23 21:29
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075083
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1623263-06
Method Blank (MB)
(MB) R3935681-3 06/10/23 21:29
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
2-Butanone (MEK)U 1.19 10.0
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
(S) Toluene-d8 95.4 80.0-120
(S) 4-Bromofluorobenzene 112 77.0-126
(S) 1,2-Dichloroethane-d4 92.9 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935681-1 06/10/23 20:02 • (LCSD) R3935681-2 06/10/23 20:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 22.0 27.0 88.0 108 19.0-160 20.4 27
Acrolein 25.0 28.5 25.3 114 101 10.0-160 11.9 26
Acrylonitrile 25.0 26.2 27.4 105 110 55.0-149 4.48 20
Benzene 5.00 5.08 5.30 102 106 70.0-123 4.24 20
Bromobenzene 5.00 4.25 4.58 85.0 91.6 73.0-121 7.47 20
Bromodichloromethane 5.00 4.75 5.31 95.0 106 75.0-120 11.1 20
Bromoform 5.00 4.50 4.48 90.0 89.6 68.0-132 0.445 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075083
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1623263-06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935681-1 06/10/23 20:02 • (LCSD) R3935681-2 06/10/23 20:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 3.80 4.25 76.0 85.0 10.0-160 11.2 25
n-Butylbenzene 5.00 4.31 4.86 86.2 97.2 73.0-125 12.0 20
sec-Butylbenzene 5.00 4.50 4.77 90.0 95.4 75.0-125 5.83 20
tert-Butylbenzene 5.00 4.37 4.75 87.4 95.0 76.0-124 8.33 20
Carbon tetrachloride 5.00 5.68 5.63 114 113 68.0-126 0.884 20
Chlorobenzene 5.00 4.52 4.80 90.4 96.0 80.0-121 6.01 20
Chlorodibromomethane 5.00 4.56 4.66 91.2 93.2 77.0-125 2.17 20
Chloroethane 5.00 5.46 5.66 109 113 47.0-150 3.60 20
Chloroform 5.00 5.04 5.07 101 101 73.0-120 0.593 20
Chloromethane 5.00 4.56 4.97 91.2 99.4 41.0-142 8.60 20
2-Chlorotoluene 5.00 4.18 4.79 83.6 95.8 76.0-123 13.6 20
4-Chlorotoluene 5.00 3.99 4.53 79.8 90.6 75.0-122 12.7 20
1,2-Dibromo-3-Chloropropane 5.00 4.53 4.53 90.6 90.6 58.0-134 0.000 20
1,2-Dibromoethane 5.00 4.76 4.75 95.2 95.0 80.0-122 0.210 20
Dibromomethane 5.00 4.63 5.13 92.6 103 80.0-120 10.2 20
1,2-Dichlorobenzene 5.00 4.44 4.89 88.8 97.8 79.0-121 9.65 20
1,3-Dichlorobenzene 5.00 4.22 4.65 84.4 93.0 79.0-120 9.70 20
1,4-Dichlorobenzene 5.00 3.87 4.34 77.4 86.8 79.0-120 J4 11.4 20
Dichlorodifluoromethane 5.00 4.84 5.59 96.8 112 51.0-149 14.4 20
1,1-Dichloroethane 5.00 5.42 5.71 108 114 70.0-126 5.21 20
1,2-Dichloroethane 5.00 5.12 5.04 102 101 70.0-128 1.57 20
1,1-Dichloroethene 5.00 5.72 6.14 114 123 71.0-124 7.08 20
cis-1,2-Dichloroethene 5.00 5.27 5.34 105 107 73.0-120 1.32 20
trans-1,2-Dichloroethene 5.00 5.65 6.23 113 125 73.0-120 J4 9.76 20
1,2-Dichloropropane 5.00 5.11 5.15 102 103 77.0-125 0.780 20
1,1-Dichloropropene 5.00 5.43 5.56 109 111 74.0-126 2.37 20
1,3-Dichloropropane 5.00 5.08 5.05 102 101 80.0-120 0.592 20
2,2-Dichloropropane 5.00 4.97 5.02 99.4 100 58.0-130 1.00 20
Di-isopropyl ether 5.00 5.51 5.47 110 109 58.0-138 0.729 20
Ethylbenzene 5.00 4.44 4.69 88.8 93.8 79.0-123 5.48 20
Hexachloro-1,3-butadiene 5.00 4.50 4.77 90.0 95.4 54.0-138 5.83 20
Isopropylbenzene 5.00 4.55 5.00 91.0 100 76.0-127 9.42 20
p-Isopropyltoluene 5.00 4.55 4.94 91.0 98.8 76.0-125 8.22 20
2-Butanone (MEK)25.0 26.8 26.1 107 104 44.0-160 2.65 20
Methylene Chloride 5.00 4.94 5.66 98.8 113 67.0-120 13.6 20
4-Methyl-2-pentanone (MIBK)25.0 23.9 24.5 95.6 98.0 68.0-142 2.48 20
Methyl tert-butyl ether 5.00 5.48 5.66 110 113 68.0-125 3.23 20
Naphthalene 5.00 3.75 4.11 75.0 82.2 54.0-135 9.16 20
n-Propylbenzene 5.00 4.12 4.71 82.4 94.2 77.0-124 13.4 20
Styrene 5.00 4.51 4.82 90.2 96.4 73.0-130 6.65 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075083
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1623263-06
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935681-1 06/10/23 20:02 • (LCSD) R3935681-2 06/10/23 20:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
1,1,1,2-Tetrachloroethane 5.00 4.66 4.87 93.2 97.4 75.0-125 4.41 20
1,1,2,2-Tetrachloroethane 5.00 4.06 4.49 81.2 89.8 65.0-130 10.1 20
Tetrachloroethene 5.00 4.68 5.14 93.6 103 72.0-132 9.37 20
Toluene 5.00 4.38 4.86 87.6 97.2 79.0-120 10.4 20
1,2,3-Trichlorobenzene 5.00 4.29 4.60 85.8 92.0 50.0-138 6.97 20
1,2,4-Trichlorobenzene 5.00 3.95 4.41 79.0 88.2 57.0-137 11.0 20
1,1,1-Trichloroethane 5.00 5.75 5.62 115 112 73.0-124 2.29 20
1,1,2-Trichloroethane 5.00 4.96 4.83 99.2 96.6 80.0-120 2.66 20
Trichloroethene 5.00 5.04 5.72 101 114 78.0-124 12.6 20
Trichlorofluoromethane 5.00 5.68 6.45 114 129 59.0-147 12.7 20
1,2,3-Trichloropropane 5.00 4.35 4.77 87.0 95.4 73.0-130 9.21 20
1,2,4-Trimethylbenzene 5.00 4.27 4.80 85.4 96.0 76.0-121 11.7 20
1,3,5-Trimethylbenzene 5.00 3.97 4.66 79.4 93.2 76.0-122 16.0 20
Vinyl chloride 5.00 5.37 5.97 107 119 67.0-131 10.6 20
o-Xylene 5.00 4.73 4.92 94.6 98.4 80.0-122 3.94 20
m&p-Xylenes 10.0 8.94 9.55 89.4 95.5 80.0-122 6.60 20
(S) Toluene-d8 99.5 99.9 80.0-120
(S) 4-Bromofluorobenzene 111 112 77.0-126
(S) 1,2-Dichloroethane-d4 97.9 98.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2077679
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1623263-05
Method Blank (MB)
(MB) R3936981-3 06/14/23 22:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
2-Butanone (MEK)U 1.19 10.0
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2077679
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1623263-05
Method Blank (MB)
(MB) R3936981-3 06/14/23 22:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
o-Xylene U 0.174 1.00
m&p-Xylenes U 0.430 2.00
(S) Toluene-d8 116 80.0-120
(S) 4-Bromofluorobenzene 87.1 77.0-126
(S) 1,2-Dichloroethane-d4 120 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936981-1 06/14/23 21:19 • (LCSD) R3936981-2 06/14/23 21:40
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 24.9 26.8 99.6 107 19.0-160 7.35 27
Acrolein 25.0 17.6 18.4 70.4 73.6 10.0-160 4.44 26
Acrylonitrile 25.0 28.4 32.3 114 129 55.0-149 12.9 20
Benzene 5.00 5.21 5.35 104 107 70.0-123 2.65 20
Bromobenzene 5.00 5.33 5.35 107 107 73.0-121 0.375 20
Bromodichloromethane 5.00 5.59 5.46 112 109 75.0-120 2.35 20
Bromoform 5.00 4.49 4.28 89.8 85.6 68.0-132 4.79 20
n-Butylbenzene 5.00 5.23 5.14 105 103 73.0-125 1.74 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2077679
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1623263-05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936981-1 06/14/23 21:19 • (LCSD) R3936981-2 06/14/23 21:40
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
sec-Butylbenzene 5.00 5.39 5.47 108 109 75.0-125 1.47 20
tert-Butylbenzene 5.00 5.27 5.43 105 109 76.0-124 2.99 20
Carbon tetrachloride 5.00 6.04 5.96 121 119 68.0-126 1.33 20
Chlorobenzene 5.00 5.35 5.09 107 102 80.0-121 4.98 20
Chlorodibromomethane 5.00 5.03 5.17 101 103 77.0-125 2.75 20
Chloroethane 5.00 4.07 4.13 81.4 82.6 47.0-150 1.46 20
Chloroform 5.00 5.63 5.61 113 112 73.0-120 0.356 20
Chloromethane 5.00 6.78 7.22 136 144 41.0-142 J4 6.29 20
2-Chlorotoluene 5.00 5.44 5.51 109 110 76.0-123 1.28 20
4-Chlorotoluene 5.00 5.58 5.33 112 107 75.0-122 4.58 20
1,2-Dibromo-3-Chloropropane 5.00 4.36 4.37 87.2 87.4 58.0-134 0.229 20
1,2-Dibromoethane 5.00 4.57 4.81 91.4 96.2 80.0-122 5.12 20
Dibromomethane 5.00 4.56 4.81 91.2 96.2 80.0-120 5.34 20
1,2-Dichlorobenzene 5.00 5.31 5.39 106 108 79.0-121 1.50 20
1,3-Dichlorobenzene 5.00 5.27 5.50 105 110 79.0-120 4.27 20
1,4-Dichlorobenzene 5.00 5.40 5.38 108 108 79.0-120 0.371 20
Dichlorodifluoromethane 5.00 5.04 6.01 101 120 51.0-149 17.6 20
1,1-Dichloroethane 5.00 6.03 6.32 121 126 70.0-126 4.70 20
1,2-Dichloroethane 5.00 6.13 6.06 123 121 70.0-128 1.15 20
1,1-Dichloroethene 5.00 5.11 5.56 102 111 71.0-124 8.43 20
cis-1,2-Dichloroethene 5.00 5.28 5.37 106 107 73.0-120 1.69 20
trans-1,2-Dichloroethene 5.00 5.20 5.60 104 112 73.0-120 7.41 20
1,2-Dichloropropane 5.00 5.89 5.81 118 116 77.0-125 1.37 20
1,1-Dichloropropene 5.00 5.22 5.22 104 104 74.0-126 0.000 20
1,3-Dichloropropane 5.00 5.16 4.81 103 96.2 80.0-120 7.02 20
2,2-Dichloropropane 5.00 5.25 4.46 105 89.2 58.0-130 16.3 20
Di-isopropyl ether 5.00 6.77 6.86 135 137 58.0-138 1.32 20
Ethylbenzene 5.00 5.22 5.10 104 102 79.0-123 2.33 20
Hexachloro-1,3-butadiene 5.00 6.26 6.83 125 137 54.0-138 8.71 20
Isopropylbenzene 5.00 4.96 4.87 99.2 97.4 76.0-127 1.83 20
p-Isopropyltoluene 5.00 5.32 5.42 106 108 76.0-125 1.86 20
2-Butanone (MEK)25.0 25.2 25.8 101 103 44.0-160 2.35 20
Methylene Chloride 5.00 5.37 5.19 107 104 67.0-120 3.41 20
4-Methyl-2-pentanone (MIBK)25.0 27.8 25.8 111 103 68.0-142 7.46 20
Methyl tert-butyl ether 5.00 4.90 5.14 98.0 103 68.0-125 4.78 20
Naphthalene 5.00 3.99 4.12 79.8 82.4 54.0-135 3.21 20
n-Propylbenzene 5.00 5.41 5.44 108 109 77.0-124 0.553 20
Styrene 5.00 4.83 4.55 96.6 91.0 73.0-130 5.97 20
1,1,1,2-Tetrachloroethane 5.00 5.25 4.93 105 98.6 75.0-125 6.29 20
1,1,2,2-Tetrachloroethane 5.00 3.57 3.38 71.4 67.6 65.0-130 5.47 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2077679
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1623263-05
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936981-1 06/14/23 21:19 • (LCSD) R3936981-2 06/14/23 21:40
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Tetrachloroethene 5.00 5.86 5.49 117 110 72.0-132 6.52 20
Toluene 5.00 5.47 5.50 109 110 79.0-120 0.547 20
1,2,3-Trichlorobenzene 5.00 5.69 6.31 114 126 50.0-138 10.3 20
1,2,4-Trichlorobenzene 5.00 5.70 5.60 114 112 57.0-137 1.77 20
1,1,1-Trichloroethane 5.00 5.66 5.99 113 120 73.0-124 5.67 20
1,1,2-Trichloroethane 5.00 4.79 4.75 95.8 95.0 80.0-120 0.839 20
Trichloroethene 5.00 5.54 6.00 111 120 78.0-124 7.97 20
Trichlorofluoromethane 5.00 5.23 5.81 105 116 59.0-147 10.5 20
1,2,3-Trichloropropane 5.00 4.73 4.96 94.6 99.2 73.0-130 4.75 20
1,2,4-Trimethylbenzene 5.00 5.38 5.38 108 108 76.0-121 0.000 20
1,3,5-Trimethylbenzene 5.00 5.49 5.46 110 109 76.0-122 0.548 20
Vinyl chloride 5.00 4.81 4.88 96.2 97.6 67.0-131 1.44 20
o-Xylene 5.00 5.02 4.79 100 95.8 80.0-122 4.69 20
m&p-Xylenes 10.0 10.1 10.0 101 100 80.0-122 0.995 20
(S) Toluene-d8 116 115 80.0-120
(S) 4-Bromofluorobenzene 93.3 92.0 77.0-126
(S) 1,2-Dichloroethane-d4 124 125 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2078149
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1623263-05
Method Blank (MB)
(MB) R3937302-3 06/15/23 10:15
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Bromomethane U 0.605 5.00
(S) Toluene-d8 118 80.0-120
(S) 4-Bromofluorobenzene 92.1 77.0-126
(S) 1,2-Dichloroethane-d4 128 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3937302-1 06/15/23 08:53 • (LCSD) R3937302-2 06/15/23 09:13
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 2.58 2.85 51.6 57.0 10.0-160 9.94 25
(S) Toluene-d8 114 116 80.0-120
(S) 4-Bromofluorobenzene 91.6 92.6 77.0-126
(S) 1,2-Dichloroethane-d4 126 128 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075206
Volatile Organic Compounds (GC/MS) by Method 8260D L1623263-01,02,03
Method Blank (MB)
(MB) R3935599-3 06/10/23 14:25
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075206
Volatile Organic Compounds (GC/MS) by Method 8260D L1623263-01,02,03
Method Blank (MB)
(MB) R3935599-3 06/10/23 14:25
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
2-Butanone (MEK)U 1.19 10.0
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
1,1,2-Trichlorotrifluoroethane U 0.180 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,2,3-Trimethylbenzene U 0.104 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
Xylenes, Total U 0.174 3.00
(S) Toluene-d8 104 80.0-120
(S) 4-Bromofluorobenzene 92.6 77.0-126
(S) 1,2-Dichloroethane-d4 88.7 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3935599-1 06/10/23 12:58
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acetone 25.0 22.9 91.6 19.0-160
Acrolein 25.0 8.83 35.3 10.0-160
Acrylonitrile 25.0 22.8 91.2 55.0-149
Benzene 5.00 4.99 99.8 70.0-123
Bromobenzene 5.00 4.56 91.2 73.0-121
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075206
Volatile Organic Compounds (GC/MS) by Method 8260D L1623263-01,02,03
Laboratory Control Sample (LCS)
(LCS) R3935599-1 06/10/23 12:58
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Bromodichloromethane 5.00 4.63 92.6 75.0-120
Bromoform 5.00 4.07 81.4 68.0-132
Bromomethane 5.00 6.02 120 10.0-160
n-Butylbenzene 5.00 4.81 96.2 73.0-125
sec-Butylbenzene 5.00 4.90 98.0 75.0-125
tert-Butylbenzene 5.00 4.59 91.8 76.0-124
Carbon tetrachloride 5.00 5.29 106 68.0-126
Chlorobenzene 5.00 5.06 101 80.0-121
Chlorodibromomethane 5.00 4.49 89.8 77.0-125
Chloroethane 5.00 6.30 126 47.0-150
Chloroform 5.00 5.21 104 73.0-120
Chloromethane 5.00 6.81 136 41.0-142
2-Chlorotoluene 5.00 4.89 97.8 76.0-123
4-Chlorotoluene 5.00 4.62 92.4 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.39 87.8 58.0-134
1,2-Dibromoethane 5.00 4.89 97.8 80.0-122
Dibromomethane 5.00 4.84 96.8 80.0-120
1,2-Dichlorobenzene 5.00 4.99 99.8 79.0-121
1,3-Dichlorobenzene 5.00 5.15 103 79.0-120
1,4-Dichlorobenzene 5.00 5.02 100 79.0-120
Dichlorodifluoromethane 5.00 5.32 106 51.0-149
1,1-Dichloroethane 5.00 5.14 103 70.0-126
1,2-Dichloroethane 5.00 4.65 93.0 70.0-128
1,1-Dichloroethene 5.00 5.52 110 71.0-124
cis-1,2-Dichloroethene 5.00 5.27 105 73.0-120
trans-1,2-Dichloroethene 5.00 5.27 105 73.0-120
1,2-Dichloropropane 5.00 4.68 93.6 77.0-125
1,1-Dichloropropene 5.00 5.26 105 74.0-126
1,3-Dichloropropane 5.00 4.70 94.0 80.0-120
cis-1,3-Dichloropropene 5.00 4.27 85.4 80.0-123
trans-1,3-Dichloropropene 5.00 4.32 86.4 78.0-124
2,2-Dichloropropane 5.00 5.27 105 58.0-130
Di-isopropyl ether 5.00 4.53 90.6 58.0-138
Ethylbenzene 5.00 5.33 107 79.0-123
Hexachloro-1,3-butadiene 5.00 5.35 107 54.0-138
Isopropylbenzene 5.00 5.03 101 76.0-127
p-Isopropyltoluene 5.00 4.82 96.4 76.0-125
2-Butanone (MEK)25.0 18.9 75.6 44.0-160
Methylene Chloride 5.00 5.05 101 67.0-120
4-Methyl-2-pentanone (MIBK)25.0 21.5 86.0 68.0-142
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075206
Volatile Organic Compounds (GC/MS) by Method 8260D L1623263-01,02,03
Laboratory Control Sample (LCS)
(LCS) R3935599-1 06/10/23 12:58
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Methyl tert-butyl ether 5.00 5.00 100 68.0-125
Naphthalene 5.00 4.74 94.8 54.0-135
n-Propylbenzene 5.00 4.75 95.0 77.0-124
Styrene 5.00 4.64 92.8 73.0-130
1,1,1,2-Tetrachloroethane 5.00 5.10 102 75.0-125
1,1,2,2-Tetrachloroethane 5.00 4.83 96.6 65.0-130
1,1,2-Trichlorotrifluoroethane 5.00 5.70 114 69.0-132
Toluene 5.00 4.97 99.4 79.0-120
1,2,3-Trichlorobenzene 5.00 5.28 106 50.0-138
1,2,4-Trichlorobenzene 5.00 5.07 101 57.0-137
1,1,1-Trichloroethane 5.00 5.56 111 73.0-124
1,1,2-Trichloroethane 5.00 4.81 96.2 80.0-120
Trichloroethene 5.00 5.02 100 78.0-124
Trichlorofluoromethane 5.00 3.57 71.4 59.0-147
1,2,3-Trichloropropane 5.00 4.97 99.4 73.0-130
1,2,4-Trimethylbenzene 5.00 4.89 97.8 76.0-121
1,2,3-Trimethylbenzene 5.00 4.82 96.4 77.0-120
1,3,5-Trimethylbenzene 5.00 4.93 98.6 76.0-122
Vinyl chloride 5.00 6.37 127 67.0-131
Xylenes, Total 15.0 15.4 103 79.0-123
(S) Toluene-d8 100 80.0-120
(S) 4-Bromofluorobenzene 92.5 77.0-126
(S) 1,2-Dichloroethane-d4 88.1 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075212
Volatile Organic Compounds (GC/MS) by Method 8260D L1623263-04
Method Blank (MB)
(MB) R3936071-2 06/11/23 07:36
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 11.3 50.0
Acrolein U 2.54 50.0
Acrylonitrile U 0.671 10.0
Benzene U 0.0941 1.00
Bromobenzene U 0.118 1.00
Bromodichloromethane U 0.136 1.00
Bromoform U 0.129 1.00
Bromomethane U 0.605 5.00
n-Butylbenzene U 0.157 1.00
sec-Butylbenzene U 0.125 1.00
tert-Butylbenzene U 0.127 1.00
Carbon tetrachloride U 0.128 1.00
Chlorobenzene U 0.116 1.00
Chlorodibromomethane U 0.140 1.00
Chloroethane U 0.192 5.00
Chloroform U 0.111 5.00
Chloromethane U 0.960 2.50
2-Chlorotoluene U 0.106 1.00
4-Chlorotoluene U 0.114 1.00
1,2-Dibromo-3-Chloropropane U 0.276 5.00
1,2-Dibromoethane U 0.126 1.00
Dibromomethane U 0.122 1.00
1,2-Dichlorobenzene U 0.107 1.00
1,3-Dichlorobenzene U 0.110 1.00
1,4-Dichlorobenzene U 0.120 1.00
Dichlorodifluoromethane U 0.374 5.00
1,1-Dichloroethane U 0.100 1.00
1,2-Dichloroethane U 0.0819 1.00
1,1-Dichloroethene U 0.188 1.00
cis-1,2-Dichloroethene U 0.126 1.00
trans-1,2-Dichloroethene U 0.149 1.00
1,2-Dichloropropane U 0.149 1.00
1,1-Dichloropropene U 0.142 1.00
1,3-Dichloropropane U 0.110 1.00
cis-1,3-Dichloropropene U 0.111 1.00
trans-1,3-Dichloropropene U 0.118 1.00
2,2-Dichloropropane U 0.161 1.00
Di-isopropyl ether U 0.105 1.00
Ethylbenzene U 0.137 1.00
Hexachloro-1,3-butadiene U 0.337 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075212
Volatile Organic Compounds (GC/MS) by Method 8260D L1623263-04
Method Blank (MB)
(MB) R3936071-2 06/11/23 07:36
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Isopropylbenzene U 0.105 1.00
p-Isopropyltoluene U 0.120 1.00
2-Butanone (MEK)U 1.19 10.0
Methylene Chloride U 0.430 5.00
4-Methyl-2-pentanone (MIBK)U 0.478 10.0
Methyl tert-butyl ether U 0.101 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.0993 1.00
Styrene U 0.118 1.00
1,1,1,2-Tetrachloroethane U 0.147 1.00
1,1,2,2-Tetrachloroethane U 0.133 1.00
1,1,2-Trichlorotrifluoroethane U 0.180 1.00
Tetrachloroethene U 0.300 1.00
Toluene U 0.278 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.481 1.00
1,1,1-Trichloroethane U 0.149 1.00
1,1,2-Trichloroethane U 0.158 1.00
Trichloroethene U 0.190 1.00
Trichlorofluoromethane U 0.160 5.00
1,2,3-Trichloropropane U 0.237 2.50
1,2,4-Trimethylbenzene U 0.322 1.00
1,2,3-Trimethylbenzene U 0.104 1.00
1,3,5-Trimethylbenzene U 0.104 1.00
Vinyl chloride U 0.234 1.00
Xylenes, Total U 0.174 3.00
(S) Toluene-d8 101 80.0-120
(S) 4-Bromofluorobenzene 91.3 77.0-126
(S) 1,2-Dichloroethane-d4 92.8 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936071-1 06/11/23 06:37 • (LCSD) R3936071-3 06/11/23 14:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 17.9 21.5 71.6 86.0 19.0-160 18.3 27
Acrolein 25.0 26.4 12.5 106 50.0 10.0-160 J3 71.5 26
Acrylonitrile 25.0 23.8 25.3 95.2 101 55.0-149 6.11 20
Benzene 5.00 4.96 4.88 99.2 97.6 70.0-123 1.63 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075212
Volatile Organic Compounds (GC/MS) by Method 8260D L1623263-04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936071-1 06/11/23 06:37 • (LCSD) R3936071-3 06/11/23 14:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromobenzene 5.00 5.85 5.43 117 109 73.0-121 7.45 20
Bromodichloromethane 5.00 4.89 4.94 97.8 98.8 75.0-120 1.02 20
Bromoform 5.00 5.44 5.06 109 101 68.0-132 7.24 20
Bromomethane 5.00 4.67 4.50 93.4 90.0 10.0-160 3.71 25
n-Butylbenzene 5.00 5.01 4.89 100 97.8 73.0-125 2.42 20
sec-Butylbenzene 5.00 4.80 4.40 96.0 88.0 75.0-125 8.70 20
tert-Butylbenzene 5.00 4.84 4.44 96.8 88.8 76.0-124 8.62 20
Carbon tetrachloride 5.00 5.63 5.36 113 107 68.0-126 4.91 20
Chlorobenzene 5.00 6.10 5.71 122 114 80.0-121 J4 6.60 20
Chlorodibromomethane 5.00 5.95 5.56 119 111 77.0-125 6.78 20
Chloroethane 5.00 5.14 4.86 103 97.2 47.0-150 5.60 20
Chloroform 5.00 4.80 4.61 96.0 92.2 73.0-120 4.04 20
Chloromethane 5.00 4.31 4.04 86.2 80.8 41.0-142 6.47 20
2-Chlorotoluene 5.00 5.70 5.65 114 113 76.0-123 0.881 20
4-Chlorotoluene 5.00 5.92 5.49 118 110 75.0-122 7.54 20
1,2-Dibromo-3-Chloropropane 5.00 4.16 3.97 83.2 79.4 58.0-134 4.67 20
1,2-Dibromoethane 5.00 5.74 5.57 115 111 80.0-122 3.01 20
Dibromomethane 5.00 5.04 5.12 101 102 80.0-120 1.57 20
1,2-Dichlorobenzene 5.00 5.68 5.69 114 114 79.0-121 0.176 20
1,3-Dichlorobenzene 5.00 5.54 5.37 111 107 79.0-120 3.12 20
1,4-Dichlorobenzene 5.00 5.55 5.35 111 107 79.0-120 3.67 20
Dichlorodifluoromethane 5.00 4.92 4.67 98.4 93.4 51.0-149 5.21 20
1,1-Dichloroethane 5.00 5.28 5.18 106 104 70.0-126 1.91 20
1,2-Dichloroethane 5.00 4.91 4.74 98.2 94.8 70.0-128 3.52 20
1,1-Dichloroethene 5.00 5.75 5.60 115 112 71.0-124 2.64 20
cis-1,2-Dichloroethene 5.00 5.32 4.89 106 97.8 73.0-120 8.42 20
trans-1,2-Dichloroethene 5.00 5.27 5.07 105 101 73.0-120 3.87 20
1,2-Dichloropropane 5.00 5.17 5.23 103 105 77.0-125 1.15 20
1,1-Dichloropropene 5.00 5.52 5.21 110 104 74.0-126 5.78 20
1,3-Dichloropropane 5.00 5.62 5.56 112 111 80.0-120 1.07 20
cis-1,3-Dichloropropene 5.00 4.19 4.11 83.8 82.2 80.0-123 1.93 20
trans-1,3-Dichloropropene 5.00 5.57 5.31 111 106 78.0-124 4.78 20
2,2-Dichloropropane 5.00 4.82 4.65 96.4 93.0 58.0-130 3.59 20
Di-isopropyl ether 5.00 4.75 4.91 95.0 98.2 58.0-138 3.31 20
Ethylbenzene 5.00 5.98 5.51 120 110 79.0-123 8.18 20
Hexachloro-1,3-butadiene 5.00 4.43 4.64 88.6 92.8 54.0-138 4.63 20
Isopropylbenzene 5.00 5.05 4.75 101 95.0 76.0-127 6.12 20
p-Isopropyltoluene 5.00 4.68 4.39 93.6 87.8 76.0-125 6.39 20
2-Butanone (MEK)25.0 19.3 19.8 77.2 79.2 44.0-160 2.56 20
Methylene Chloride 5.00 5.12 4.98 102 99.6 67.0-120 2.77 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2075212
Volatile Organic Compounds (GC/MS) by Method 8260D L1623263-04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936071-1 06/11/23 06:37 • (LCSD) R3936071-3 06/11/23 14:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
4-Methyl-2-pentanone (MIBK)25.0 25.0 25.5 100 102 68.0-142 1.98 20
Methyl tert-butyl ether 5.00 4.96 4.88 99.2 97.6 68.0-125 1.63 20
Naphthalene 5.00 2.52 2.73 50.4 54.6 54.0-135 J4 8.00 20
n-Propylbenzene 5.00 5.73 5.27 115 105 77.0-124 8.36 20
Styrene 5.00 5.15 4.87 103 97.4 73.0-130 5.59 20
1,1,1,2-Tetrachloroethane 5.00 5.76 5.66 115 113 75.0-125 1.75 20
1,1,2,2-Tetrachloroethane 5.00 5.41 5.49 108 110 65.0-130 1.47 20
1,1,2-Trichlorotrifluoroethane 5.00 5.14 4.79 103 95.8 69.0-132 7.05 20
Tetrachloroethene 5.00 5.71 5.25 114 105 72.0-132 8.39 20
Toluene 5.00 5.66 5.44 113 109 79.0-120 3.96 20
1,2,3-Trichlorobenzene 5.00 2.34 2.67 46.8 53.4 50.0-138 J4 13.2 20
1,2,4-Trichlorobenzene 5.00 3.38 3.79 67.6 75.8 57.0-137 11.4 20
1,1,1-Trichloroethane 5.00 5.63 5.23 113 105 73.0-124 7.37 20
1,1,2-Trichloroethane 5.00 5.95 5.56 119 111 80.0-120 6.78 20
Trichloroethene 5.00 4.62 4.72 92.4 94.4 78.0-124 2.14 20
Trichlorofluoromethane 5.00 4.67 4.39 93.4 87.8 59.0-147 6.18 20
1,2,3-Trichloropropane 5.00 5.49 5.14 110 103 73.0-130 6.59 20
1,2,4-Trimethylbenzene 5.00 4.86 4.42 97.2 88.4 76.0-121 9.48 20
1,2,3-Trimethylbenzene 5.00 5.36 5.25 107 105 77.0-120 2.07 20
1,3,5-Trimethylbenzene 5.00 5.73 5.23 115 105 76.0-122 9.12 20
Vinyl chloride 5.00 5.24 4.91 105 98.2 67.0-131 6.50 20
Xylenes, Total 15.0 17.3 16.1 115 107 79.0-123 7.19 20
(S) Toluene-d8 103 100 80.0-120
(S) 4-Bromofluorobenzene 97.9 96.1 77.0-126
(S) 1,2-Dichloroethane-d4 92.2 94.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2076103
Volatile Organic Compounds (GC/MS) by Method 8260D L1623263-01,02,03
Method Blank (MB)
(MB) R3936566-4 06/13/23 17:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Tetrachloroethene U 0.300 1.00
(S) Toluene-d8 94.8 80.0-120
(S) 4-Bromofluorobenzene 88.8 77.0-126
(S) 1,2-Dichloroethane-d4 126 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3936566-1 06/13/23 15:49 • (LCSD) R3936566-2 06/13/23 16:11
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Tetrachloroethene 5.00 4.77 4.78 95.4 95.6 72.0-132 0.209 20
(S) Toluene-d8 92.4 91.9 80.0-120
(S) 4-Bromofluorobenzene 93.3 91.1 77.0-126
(S) 1,2-Dichloroethane-d4 122 124 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2074045
TPH by Method MADEPE L1623263-05,06
Method Blank (MB)
(MB) R3935380-1 06/09/23 14:05
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.3 100
Unadjusted C19-C36 Aliphatics 46.6 J 33.3 100
(S) 1-Chloro-octadecane 76.4 40.0-140
Method Blank (MB)
(MB) R3935515-1 06/09/23 00:08
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics U 33.3 100
(S) o-Terphenyl 69.4 40.0-140
(S) 2-Fluorobiphenyl 82.4 40.0-140
(S) 2-Bromonaphthalene 82.0 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935380-2 06/09/23 14:27 • (LCSD) R3935380-3 06/09/23 14:49
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 560 411 93.3 68.5 40.0-140 J3 30.7 25
Unadjusted C19-C36 Aliphatics 800 936 703 117 87.9 40.0-140 J3 28.4 25
(S) 1-Chloro-octadecane 75.3 71.9 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3935515-2 06/09/23 00:31 • (LCSD) R3935515-3 06/09/23 00:53
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1340 1210 78.8 71.2 40.0-140 10.2 25
(S) o-Terphenyl 73.4 66.6 40.0-140
(S) 2-Fluorobiphenyl 84.0 86.0 40.0-140
(S) 2-Bromonaphthalene 80.7 82.7 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073715
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1623263-05,06
Method Blank (MB)
(MB) R3935315-2 06/09/23 15:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene 0.151 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroethyl)ether U 1.62 10.0
2,2-Oxybis(1-Chloropropane)U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
1,2-Dichlorobenzene U 0.340 10.0
1,3-Dichlorobenzene U 0.365 10.0
1,4-Dichlorobenzene U 0.322 10.0
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 1.19 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073715
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1623263-05,06
Method Blank (MB)
(MB) R3935315-2 06/09/23 15:46
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Diethyl phthalate U 0.282 3.00
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate U 0.278 3.00
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
(S) Nitrobenzene-d5 92.5 15.0-314
(S) 2-Fluorobiphenyl 67.8 22.0-127
(S) p-Terphenyl-d14 77.9 29.0-141
Laboratory Control Sample (LCS)
(LCS) R3935315-1 06/09/23 15:25
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 38.4 76.8 47.0-145
Acenaphthylene 50.0 39.3 78.6 33.0-145
Anthracene 50.0 42.6 85.2 27.0-133
Benzidine 100 7.08 7.08 1.00-120
Benzo(a)anthracene 50.0 42.3 84.6 33.0-143
Benzo(b)fluoranthene 50.0 46.1 92.2 24.0-159
Benzo(k)fluoranthene 50.0 41.0 82.0 11.0-162
Benzo(g,h,i)perylene 50.0 37.2 74.4 1.00-219
Benzo(a)pyrene 50.0 47.3 94.6 17.0-163
Bis(2-chlorethoxy)methane 50.0 44.8 89.6 1.00-219
Bis(2-chloroethyl)ether 50.0 38.8 77.6 33.0-185
2,2-Oxybis(1-Chloropropane)50.0 34.1 68.2 36.0-166
4-Bromophenyl-phenylether 50.0 47.0 94.0 53.0-127
2-Chloronaphthalene 50.0 35.9 71.8 60.0-120
4-Chlorophenyl-phenylether 50.0 49.5 99.0 25.0-158
Chrysene 50.0 42.2 84.4 17.0-168
Dibenz(a,h)anthracene 50.0 38.1 76.2 1.00-227
1,2-Dichlorobenzene 50.0 35.3 70.6 27.0-120
1,3-Dichlorobenzene 50.0 32.1 64.2 26.0-120
1,4-Dichlorobenzene 50.0 33.1 66.2 26.0-120
3,3-Dichlorobenzidine 100 89.5 89.5 1.00-262
2,4-Dinitrotoluene 50.0 51.5 103 39.0-139
2,6-Dinitrotoluene 50.0 43.0 86.0 50.0-158
Fluoranthene 50.0 51.5 103 26.0-137
Fluorene 50.0 42.1 84.2 59.0-121
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073715
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1623263-05,06
Laboratory Control Sample (LCS)
(LCS) R3935315-1 06/09/23 15:25
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Hexachlorobenzene 50.0 47.3 94.6 1.00-152
Hexachloro-1,3-butadiene 50.0 53.4 107 24.0-120
Hexachlorocyclopentadiene 50.0 32.9 65.8 10.0-120
Hexachloroethane 50.0 37.0 74.0 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 38.6 77.2 1.00-171
Isophorone 50.0 54.0 108 21.0-196
Naphthalene 50.0 36.1 72.2 21.0-133
Nitrobenzene 50.0 48.7 97.4 35.0-180
n-Nitrosodimethylamine 50.0 26.7 53.4 10.0-120
n-Nitrosodiphenylamine 50.0 36.7 73.4 44.0-120
n-Nitrosodi-n-propylamine 50.0 48.7 97.4 1.00-230
Phenanthrene 50.0 40.6 81.2 54.0-120
Benzylbutyl phthalate 50.0 41.2 82.4 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 39.6 79.2 8.00-158
Di-n-butyl phthalate 50.0 49.3 98.6 1.00-120
Diethyl phthalate 50.0 52.7 105 1.00-120
Dimethyl phthalate 50.0 48.9 97.8 1.00-120
Di-n-octyl phthalate 50.0 36.4 72.8 4.00-146
Pyrene 50.0 37.7 75.4 52.0-120
1,2,4-Trichlorobenzene 50.0 40.9 81.8 44.0-142
(S) Nitrobenzene-d5 102 15.0-314
(S) 2-Fluorobiphenyl 73.3 22.0-127
(S) p-Terphenyl-d14 74.9 29.0-141
L1624007-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1624007-03 06/09/23 20:44 • (MS) R3935315-3 06/09/23 21:05 • (MSD) R3935315-4 06/09/23 21:27
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 U 33.2 31.0 66.4 62.0 1 47.0-145 6.85 48
Acenaphthylene 50.0 U 35.0 31.8 70.0 63.6 1 33.0-145 9.58 74
Anthracene 50.0 U 31.4 31.7 62.8 63.4 1 27.0-133 0.951 66
Benzidine 100 U 15.6 16.3 15.6 16.3 1 1.00-120 4.39 40
Benzo(a)anthracene 50.0 U 31.6 31.1 63.2 62.2 1 33.0-143 1.59 53
Benzo(b)fluoranthene 50.0 U 34.7 34.6 69.4 69.2 1 24.0-159 0.289 71
Benzo(k)fluoranthene 50.0 U 29.0 28.9 58.0 57.8 1 11.0-162 0.345 63
Benzo(g,h,i)perylene 50.0 U 26.6 27.0 53.2 54.0 1 1.00-219 1.49 97
Benzo(a)pyrene 50.0 U 34.3 35.1 68.6 70.2 1 17.0-163 2.31 72
Bis(2-chlorethoxy)methane 50.0 U 39.0 35.1 78.0 70.2 1 33.0-184 10.5 54
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2073715
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1623263-05,06
L1624007-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1624007-03 06/09/23 20:44 • (MS) R3935315-3 06/09/23 21:05 • (MSD) R3935315-4 06/09/23 21:27
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Bis(2-chloroethyl)ether 50.0 U 34.2 30.0 68.4 60.0 1 12.0-158 13.1 108
2,2-Oxybis(1-Chloropropane)50.0 U 29.6 24.5 59.2 49.0 1 36.0-166 18.9 76
4-Bromophenyl-phenylether 50.0 U 36.6 37.4 73.2 74.8 1 53.0-127 2.16 43
2-Chloronaphthalene 50.0 U 31.1 29.9 62.2 59.8 1 60.0-120 J6 3.93 24
4-Chlorophenyl-phenylether 50.0 U 38.8 38.6 77.6 77.2 1 25.0-158 0.517 61
Chrysene 50.0 U 30.7 29.9 61.4 59.8 1 17.0-168 2.64 87
Dibenz(a,h)anthracene 50.0 U 27.9 28.4 55.8 56.8 1 1.00-227 1.78 126
1,2-Dichlorobenzene 50.0 U 26.7 23.1 53.4 46.2 1 14.0-125 14.5 24
1,3-Dichlorobenzene 50.0 U 25.7 22.2 51.4 44.4 1 12.0-123 14.6 22
1,4-Dichlorobenzene 50.0 U 26.5 23.4 53.0 46.8 1 12.0-125 12.4 23
3,3-Dichlorobenzidine 100 U 56.1 56.7 56.1 56.7 1 1.00-262 1.06 108
2,4-Dinitrotoluene 50.0 U 43.9 41.5 87.8 83.0 1 39.0-139 5.62 42
2,6-Dinitrotoluene 50.0 U 40.4 36.6 80.8 73.2 1 50.0-158 9.87 48
Fluoranthene 50.0 U 37.1 38.2 74.2 76.4 1 26.0-137 2.92 66
Fluorene 50.0 U 35.8 34.0 71.6 68.0 1 59.0-121 5.16 38
Hexachlorobenzene 50.0 U 36.2 35.6 72.4 71.2 1 1.00-152 1.67 55
Hexachloro-1,3-butadiene 50.0 U 40.0 38.6 80.0 77.2 1 24.0-120 3.56 62
Hexachlorocyclopentadiene 50.0 U 23.1 23.7 46.2 47.4 1 10.0-146 2.56 34
Hexachloroethane 50.0 U 27.2 24.5 54.4 49.0 1 40.0-120 10.4 52
Indeno(1,2,3-cd)pyrene 50.0 U 27.1 27.2 54.2 54.4 1 1.00-171 0.368 99
Isophorone 50.0 U 45.8 42.9 91.6 85.8 1 21.0-196 6.54 93
Naphthalene 50.0 U 31.1 28.1 62.2 56.2 1 21.0-133 10.1 65
Nitrobenzene 50.0 U 44.3 40.0 88.6 80.0 1 35.0-180 10.2 62
n-Nitrosodimethylamine 50.0 U 25.7 19.5 51.4 39.0 1 10.0-120 27.4 40
n-Nitrosodiphenylamine 50.0 U 31.5 30.9 63.0 61.8 1 16.0-160 1.92 28
n-Nitrosodi-n-propylamine 50.0 U 41.7 36.5 83.4 73.0 1 1.00-230 13.3 87
Phenanthrene 50.0 U 32.0 30.5 64.0 61.0 1 54.0-120 4.80 39
Benzylbutyl phthalate 50.0 U 32.8 32.2 65.6 64.4 1 1.00-152 1.85 60
Bis(2-ethylhexyl)phthalate 50.0 U 30.8 29.5 61.6 59.0 1 8.00-158 4.31 82
Di-n-butyl phthalate 50.0 U 36.3 37.4 72.6 74.8 1 1.00-120 2.99 47
Diethyl phthalate 50.0 U 43.7 40.1 87.4 80.2 1 1.00-120 8.59 100
Dimethyl phthalate 50.0 U 41.2 38.6 82.4 77.2 1 1.00-120 6.52 183
Di-n-octyl phthalate 50.0 U 27.5 27.0 55.0 54.0 1 4.00-146 1.83 69
Pyrene 50.0 U 31.8 29.0 63.6 58.0 1 52.0-120 9.21 49
1,2,4-Trichlorobenzene 50.0 U 33.5 30.3 67.0 60.6 1 44.0-142 10.0 50
(S) Nitrobenzene-d5 91.4 79.7 15.0-314
(S) 2-Fluorobiphenyl 61.0 55.5 22.0-127
(S) p-Terphenyl-d14 54.6 54.8 29.0-141
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
C4 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Data is likely to show a low bias concerning the result.
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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