MO-30137_49193_CA_IAR_20230725

ONE Environmental Mid Atlantic, LLC www.oneenv.com
July 25, 2023 Mr. Bruce Stainbrook Altec Industries, Inc. 810 Franklin Court, Suite A Marietta, Georgia 30067
Re: UST Closure and Site Investigation 640 Rock Lane China Grove, Rowan County, North Carolina 28023 Dear Mr. Stainbrook: ONE Environmental Mid Atlantic, LLC (ONE) appreciates the opportunity to submit this letter report to Altec Industries, Inc. (Altec) for the closure of a non-regulated noncommercial heating oil underground storage tank (UST) and subsequent site investigation at the property located at 640 Rock Lane in China Grove, Rowan County, North Carolina (the “subject property”). The subject property is located on the northern portion of a larger parent tract that encompasses approximately 17.07 acres. The subject property contains one vacant residential structure and a detached garage. The location of the subject property is depicted on Figure 1.
UST REMOVAL On March 17, 2023, ONE mobilized to the site with a UST removal contractor, Clean Safe Technologies (CST), to excavate and remove one approximate 270-gallon former heating oil UST from the subject property. At the time of removal, there was no product inside the tank; however, the tank did contain approximately 5-6 inches of water. Upon removal, the UST was observed to be in poor condition with several holes and cracks around the bottom. The UST was cut in half, cleaned, and transported by CST to a salvage yard for destruction. A copy of the Certificate of Recycling is provided as Attachment A. Soil within the UST excavation was screened using a photoionization detector (PID). Elevated PID readings up to 15,000 parts per million (ppm) were detected in soil below the UST down to a depth of approximately 10 feet below ground surface (bgs), which was the maximum depth of the excavation equipment. Due to the significantly elevated PID readings at the bottom of the excavation, a soil sample was not collected for laboratory analysis.
Mr. Bruce Stainbrook July 25, 2023 Page 2 of 7
ONE Environmental Mid Atlantic, LLC www.oneenv.com
The excavated soil was temporarily staged on-site and covered with plastic, and orange construction fencing was placed around the excavation until it could be backfilled with clean soil. On March 27, 2023, CST returned to the subject property to haul off the impacted soil and backfill the excavation with clean soil. Approximately 5 tons of petroleum-impacted soil was transported to HAZ-MAT Environmental Services in Charlotte, North Carolina for disposal. A copy of the waste disposal manifest is provided as Attachment B.
INVESTIGATIVE PROCEDURES Prior to the introduction of the soil borings, the North Carolina 811 notification system for excavators, contractors, property owners, and drillers was contacted as required by state law to notify participating utilities of the upcoming work, so they could locate and mark their underground facilities.
Soil Investigation On April 6-7, 2023, under the direction of ONE, M&W Drilling LLC (MWD) advanced nine soil borings (EB-1 through EB-9) at the subject property using direct push technology (DPT). Environmental boring EB-1 was placed in the location of the former UST and the remaining eight borings surrounded EB-1 in a 15-foot grid pattern. The soil boring locations are depicted on Figure
2. The soil borings were advanced to depths ranging from 20-35 feet below ground surface (bgs). Soil samples obtained from the soil borings were field screened visually and with a PID. Soil samples for laboratory analysis were selected based on the field screening results. The PID results and visual observations of the soil samples are documented on the soil boring logs provided as
Attachment C. The soil samples were placed in clean laboratory-supplied containers and sent under proper chain-of custody documentation to Eurofins in Pittsburg, Pennsylvania for analysis of the following:
 Volatile organic compounds (VOCs) by EPA Method 8260
 Semivolatile organic compounds (SVOCs) by EPA Method 8270
 Volatile petroleum hydrocarbons (VPHs) by Massachusetts Department of Environmental Protection (MADEP) Methods
 Extractable petroleum hydrocarbons (EPHs) by MADEP Methods
Supplemental Soil Investigation ONE returned to the subject property on May 30-31, 2023, to collect additional soil samples and delineate soil impacts detected during the April 2023 sampling event. Under the direction of ONE,
Mr. Bruce Stainbrook July 25, 2023 Page 3 of 7
ONE Environmental Mid Atlantic, LLC www.oneenv.com
MWD advanced ten soil borings (EB-6B, EB-7B, and EB-10 through EB-17) at the subject property using direct push technology. With the exceptions of EB-16 and EB-17, which were advanced near the former residence to the east, the soil boring locations continued to follow the previous 15-foot grid pattern. Environmental borings EB-6B and EB-7B were advanced to investigate the vertical distribution of substances detected during the April 2023 sampling event. The additional soil boring locations are depicted on Figure 2. The additional soil borings were advanced to depths ranging from 5-20 feet bgs. Soil samples obtained from the soil borings were field screened visually and with a PID. Soil samples for laboratory analysis were collected from EB-6B and EB-7B at predetermined depths of 3-5 feet bgs and 8-10 feet bgs, respectively. The remaining soil samples for laboratory analysis were selected based on the field screening results. The PID results and visual observations of the soil samples are documented on the soil boring logs provided as Attachment C. The soil samples were placed in clean laboratory-supplied containers and sent under proper chain-of custody documentation to Eurofins in Pittsburg, Pennsylvania for analysis of the following:
 VOCs by EPA Method 8260
 SVOCs by EPA Method 8270
 VPHs by MADEP Methods
 EPHs by MADEP Methods
Groundwater Investigation On April 6, 2023, under the direction of ONE, MWD installed three temporary monitoring wells (TMW-1 through TMW-3) at the subject property to evaluate potential groundwater impacts relating to the former UST. Temporary monitoring well TMW-1 was installed in the location of the former UST with TMW-2 and TMW-3 approximately 30 feet to the west and south, respectively. The well locations are depicted on Figure 3. The temporary monitoring wells were constructed by inserting a 20-foot section of 1-inch diameter polyvinyl chloride (PVC) slotted screen in the 2-inch diameter borehole created by the DPT rods. One-inch PVC riser pipe extended from the top of the screen to at least 1 foot above the ground surface. The temporary monitoring wells were capped with lockable rubber stoppers and left in place to facilitate future sampling, if necessary. ONE returned to the site on April 12, 2023, to sample the temporary monitoring wells. The wells were developed utilizing a peristaltic pump with new polyethylene and silicone tubing until at least
Mr. Bruce Stainbrook July 25, 2023 Page 4 of 7
ONE Environmental Mid Atlantic, LLC www.oneenv.com
three well volumes had been removed from the well and limited fines were observed in the development water. The groundwater samples were placed in clean laboratory-supplied containers and sent under proper chain-of custody documentation to Eurofins in Pittsburg, Pennsylvania for analysis of the following:
 VOCs by EPA Method 8260
 SVOCs by EPA Method 625.1
 VPHs by MADEP Methods
 EPHs by MADEP Methods
Supplemental Groundwater Investigation On May 30-31, 2023, under the direction of ONE, MWD installed seven additional temporary monitoring wells (TMW-4 through TMW-10) at the subject property to further evaluate potential groundwater impacts relating to the former UST. The well locations are depicted on Figure 3. Except for TMW-8, the temporary monitoring wells were constructed by inserting 5 to 10-foot sections of 1-inch diameter PVC slotted screen in the 2-inch diameter boreholes created by the DPT rods. One-inch PVC riser pipe extended from the top of screens to at least 1 foot above the ground surface. The temporary monitoring wells were capped with lockable rubber stoppers and left in place to facilitate future sampling, if necessary. Please note that temporary monitoring well TMW-8 was located in the driveway and could not be left in place; therefore, a stainless-steel screenpoint sampler with a 4-foot section of stainless-steel slotted screen was used to collect a groundwater sample. Following sample collection, the screenpoint sampler was immediately removed from the ground by MWD and the borehole properly abandoned. Between May 30, 2023 and June 1, 2023, ONE collected groundwater samples from all ten on-site monitoring wells. The wells were developed utilizing a peristaltic pump with new polyethylene and silicone tubing until at least three well volumes had been removed from the well and limited fines were observed in the development water. The groundwater samples were placed in clean laboratory-supplied containers and sent under proper chain-of custody documentation to Eurofins in Pittsburg, Pennsylvania for analysis of the following:
 VOCs by EPA Method 8260
 SVOCs by EPA Method 625.1
Mr. Bruce Stainbrook July 25, 2023 Page 5 of 7
ONE Environmental Mid Atlantic, LLC www.oneenv.com
 VPHs by MADEP Methods
 EPHs by MADEP Methods In addition to collecting groundwater samples, ONE obtained relative top of casing (TOC) elevations from all on-site temporary monitoring wells, except for TMW-8. Further, depth to groundwater measurements were collected from the entire well network on June 1, 2023 using an electronic water level indicator accurate to 0.01 foot.
INVESTIGATIVE RESULTS
Soil Investigation Results The laboratory analytical results for the soil samples collected at the subject property were compared to the North Carolina Department of Environmental Quality (NCDEQ) Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs) and Residential MSCCs, whichever was lower, per 15A NCAC 02L .0411. One VOC (1,1,1-trichloroethane) was detected above the laboratory reporting limit in soil at the subject property; however, the concentrations of 1,1,1-trichloroethane were less than the applicable MSCC. Five SVOCs (benzo[a]anthracene, chrysene, fluoranthene, phenanthrene, and pyrene) were detected above laboratory reporting limits in soil at the subject property; however, the concentrations of these SVOCs were less than the applicable MSCCs. Two MADEP VPHs (C9-C12 aliphatics and C9-C10 aromatics) were detected above laboratory reporting limits in soil at the subject property. While the concentrations of C9-C12 aliphatics were below the applicable MSCCs, the concentrations of C9-C10 aromatics detected in both soil samples collected from EB-12 (2-4 feet bgs and 6-8 feet bgs) exceeded the Soil-to-Groundwater MSCC. Three MADEP EPHs (C9-C18 aliphatics, C19-C36 aliphatics, and C11-C22 aromatics) were detected above laboratory reporting limits in soil at the subject property. While the concentrations of C9-C18 aliphatics and C19-C36 aliphatics were below the applicable MSCCs, the concentrations of C11-C22 aromatics detected in the soil samples collected from EB-7 (3-5 feet bgs) and EB-12 (2-4 feet bgs) exceeded the Soil-to-Groundwater MSCC. The soil analytical results are summarized in Table 1. The complete laboratory analytical data reports are provided as Attachment D.
Groundwater Investigation Results
Mr. Bruce Stainbrook July 25, 2023 Page 6 of 7
ONE Environmental Mid Atlantic, LLC www.oneenv.com
The laboratory analytical results for the groundwater samples collected at the subject property were compared to the NCDEQ Groundwater Quality Standard (GWQS) per 15A NCAC 02L .0202. Three VOCs (benzene, toluene, and xylenes) were detected above laboratory reporting limits in groundwater at the subject property. While the concentrations of toluene and xylenes were below the GWQSs, the concentrations of benzene detected in the groundwater samples collected from temporary monitoring wells TMW-1 and TMW-3 exceeded the GWQS. Three SVOCs (1-methylnaphthalene, 2-methylnaphthalene, and naphthalene) were detected above laboratory reporting limits in groundwater at the subject property; however, the concentrations of these SVOCs were less than the GWQSs. Two MADEP VPHs (C5-C8 aliphatics and C9-C12 aliphatics) were detected above laboratory reporting limits in groundwater at the subject property; however, the concentrations of these MADEP VPHs were less than the GWQSs. Two MADEP EPHs (C9-C18 aliphatics and C11-C22 aromatics) were detected above laboratory reporting limits in groundwater at the subject property; however, the concentrations of these MADEP EPHs were less than the GWQSs. The groundwater analytical results are summarized in Table 2. The complete laboratory analytical data reports are provided as Attachment D. Based on the water table elevations measured on June 1, 2023, the groundwater flow directions in the vicinity of the former UST appear to be to the west, southwest, and south. The water table contours and estimated groundwater flow directions are depicted on Figure 4.
CONCLUSIONS AND RECOMMENDATIONS ONE collected 20 soil samples at the subject property over the course of two site visits. C11-C22 aromatics exceeded the Soil-to-Groundwater MSCC in the soil sample collected from EB-7 (2-4 feet bgs); however, a deeper soil sample collected at this location from EB-7B (8-10 feet bgs) did not exhibit any MSCC exceedances. Similarly, C11-C22 aromatics exceeded the Soil-to-Groundwater MSCC in the shallow soil sample collected from EB-12 (2-4 feet bgs) but were below the MSCC in the deeper soil sample (6-8 feet bgs). On the other hand, C9-C10 aromatics exceeded the Soil-to-Groundwater MSCC in both the shallow and deep soil samples collected from EB-12; however, it should be noted the concentration of C9-C10 aromatics in EB-12 (6-8 feet bgs) was 32.8 milligrams per kilogram (mg/kg), which is only slightly above the Soil-to-Groundwater MSCC of 31 mg/kg. To summarize, while MSCC exceedances were detected at the subject property, the soil impacts appear to be relatively minor.
Mr. Bruce Stainbrook July 25, 2023 Page 7 of 7
ONE Environmental Mid Atlantic, LLC www.oneenv.com
Benzene was the only compound detected at the subject property above the GWQS. The maximum concentration of benzene (21.4 micrograms per liter [µg/L]) was detected in TMW-1, which is in the location of the former UST. Benzene was also detected above the GWQS in the groundwater sample collected from TMW-3, which is located approximately 30 feet to the south of the former UST. This is consistent with the findings of the groundwater flow direction at this location, which is to the south. The concentration of benzene in TMW-3 was 2 µg/L in the sample collected on May 31, 2023, but it was below the laboratory reporting limit in the sample collected on April 12, 2023. This suggests that the concentration of benzene in TMW-3 fluctuates around the GWQS for benzene of 1 µg/L. Like soil, the groundwater impacts at the subject property appear to be relatively minor and do not appear to be migrating significantly. Moreover, the groundwater flow direction and analytical data suggest that the release at the subject property is not expected to impact the adjoining property to the north.
CLOSING ONE appreciates the opportunity to provide environmental consulting services to Altec. If you should have any questions or comments pertaining to the information contained herein, please do not hesitate to contact me at [phone]. Sincerely,
ONE Environmental Mid Atlantic, LLC Brad D. White, PG Senior Project Manager Enclosures: Tables Figures Attachment A – UST Certificate of Recycling Attachment B – Waste Manifest for Soil Attachment C – Soil Boring Logs and Monitoring Well Construction Diagrams Attachment D – Laboratory Analytical Data Reports
TABLES

Sample ID Date Collected Sample Depth
(feet bgs)
EB-1 4/6/2023 8-10 <0.00245 <0.0429 <0.0528 <0.0251 <0.0255 <0.0225 <5.86 <5.86 <5.86 <8.65 <17.3 <17.3 <17.3
EB-2 4/6/2023 8-10 <0.00253 <0.0453 <0.0557 <0.0265 <0.0269 <0.0238 <5.75 <5.75 <5.75 <9.04 <18.1 <18.1 <18.1
EB-3 4/6/2023 8-10 <0.00250 <0.0445 <0.0547 <0.0260 <0.0264 <0.0233 <5.91 <5.91 <5.91 <9.02 <18.0 <18.0 <18.0
EB-4 4/7/2023 8-10 <0.00237 <0.0457 <0.0561 <0.0267 <0.0272 <0.0240 <6.11 <6.11 <6.11 <8.77 <17.5 <17.5 <17.5
EB-5 4/7/2023 8-10 <0.00239 <0.0440 <0.0541 <0.0257 <0.0262 <0.0231 <5.82 <5.82 <5.82 <8.54 <17.1 <17.1 <17.1
EB-6 4/7/2023 8-10 0.0132 <0.0451 <0.0554 <0.0264 <0.0268 <0.0237 <5.79 <5.79 <5.79 <8.98 <18.0 <18.0 <18.0
EB-6B 5/30/2023 3-5 <0.00219 <0.0400 <0.0492 <0.0234 <0.0238 <0.0210 <6.59 <6.59 <6.59 <8.11 <16.2 <16.2 <16.2
EB-7 4/7/2023 3-5 0.00314 J <0.0404 <0.0496 <0.0236 <0.0240 <0.0212 7.59 J <5.46 <5.46 39.5 1300 170 164
EB-7B 5/30/2023 8-10 <0.00233 <0.0444 <0.0546 <0.0260 <0.0264 <0.0233 <6.92 <6.92 <6.92 <9.00 25 <18.0 <18.0
EB-8 4/6/2023 8-10 <0.00244 <0.0444 <0.0546 <0.0260 <0.0264 <0.0233 <5.84 <5.84 <5.84 <8.56 <17.1 <17.1 <17.1
EB-9 4/6/2023 8-10 <0.00242 <0.0443 <0.0544 <0.0259 <0.0263 <0.0232 <5.88 <5.88 <5.88 <8.73 <17.5 <17.5 <17.5
EB-10 5/30/2023 8-10 0.00586 J <0.0469 <0.0576 <0.0274 <0.0279 <0.0246 N/A N/A N/A 15.1 <19.0 <19.0 <19.0
EB-11 5/30/2023 3-5 <0.00247 <0.0453 <0.0557 <0.0265 <0.0270 <0.0238 <7.83 <7.83 <7.83 <8.74 <17.5 <17.5 <17.5
EB-12 5/31/2023 2-4 0.0166 <0.0445 <0.0547 <0.0260 <0.0264 <0.0233 186 123 61.2 39 934 49 43.6
EB-12 5/31/2023 6-8 0.0189 0.0998 0.0946 0.32 0.291 0.342 114 80.5 32.8 36.5 535 27.9 26.1
EB-13 5/31/2023 6-8 <0.00221 <0.0430 <0.0528 <0.0251 <0.0256 <0.0226 <6.33 <6.33 <6.33 <8.80 <17.6 <17.6 <17.6
EB-14 5/31/2023 8-10 <0.00237 <0.0439 <0.0540 <0.0257 <0.0261 <0.0231 <7.16 <7.16 <7.16 <8.69 <17.4 <17.4 <17.4
EB-15 5/30/2023 8-10 <0.00227 <0.0423 <0.0520 <0.0247 <0.0252 <0.0222 <15.7 <15.7 <15.7 28.3 <16.8 <16.8 <16.8
EB-16 5/31/2023 2-3 <0.00224 <0.0425 <0.0522 <0.0249 <0.0253 <0.0223 <5.30 <5.30 <5.30 <8.30 <16.6 <16.6 <16.6
EB-17 5/31/2023 8-10 <0.00252 <0.0454 <0.0558 0.164 0.141 0.133 <7.51 <7.51 <7.51 47 <17.7 <17.7 <17.7
1.2 0.17 18 330 64 210 540 540 31 540 # 31 31
31200 6.6 663 625 469 469 1560 1560 469 1560 31200 469 469
Notes:
All concentrations reported in milligrams per kilogram (mg/kg).
bgs - below ground surface
BDL - Below laboratory method detection limit for grouped parameters
Bolded values greater than laboratory reporting limit.
Concentration exceeds NCDEQ Soil-to-Groundwater Maximum Soil Contaminant Concentration (MSCC)
Concentration exceeds NCDEQ Residential MSCC
J - Result is less than laboratory reporting limit but greater than or equal to the laboratory MDL and the concentration is an approximate value.
# - Health based level > 100%
N/A - Not available
Soil-to-Groundwater MSCC
Table 1: Summary of Soil Sampling Results
640 Rock Lane
Analytical Method
Contaminant of Concern
Residential MSCC
China Grove, North Carolina
1,1,1-
Trichloroethane Pyrene C9-C10
Aromatics
C11-C22 Aromatics
(Adjusted)C19-C36 Aliphatics
EPA 8260 MADEP EPH
C9-C18
Aliphatics
C11-C22 Aromatics
(Unadjusted)
C9-C12
Aliphatics
(Adjusted)
C9-C12
Aliphatics
(Unadjusted)
MADEP VPHEPA 8270
PhenanthreneChrysene FluorantheneBenzo[a]
anthracene
Sample ID Date Collected
4/12/2023 15.3 1.12 28.7 <0.0519 <0.0574 0.0719 J 191 172 109 48.6 J <31.2 <41.6 <41.6
5/30/2023 21.4 1.36 63.2 0.37 0.361 2.15 372 341 360 154 52.5 81.7 65.2
4/12/2023 <0.596 <0.457 <0.890 <0.0609 <0.0674 <0.0641 <25.0 <25.0 <25.0 <25.0 <32.3 <43.1 <43.1
5/31/2023 <0.596 <0.457 <0.890 <0.0583 <0.0646 <0.0615 29.6 J 29.2 J <25.0 <25.0 <32.3 <43.1 <43.1
4/12/2023 <0.596 <0.457 <0.890 <0.0583 <0.0646 <0.0615 <25.0 <25.0 <25.0 <25.0 <32.1 <42.8 <42.8
5/31/2023 2 <0.457 4.2 <0.0538 <0.0596 0.0902 J 64.3 J 61.9 J <25.0 <25.0 <31.3 <41.7 <41.7
TMW-4 5/31/2023 <0.596 <0.457 <0.890 <0.0560 <0.0620 0.0958 J <25.0 <25.0 <25.0 <25.0 33.8 <44.5 <44.5
TMW-5 5/31/2023 <0.596 <0.457 <0.890 <0.0560 <0.0620 <0.0590 <25.0 <25.0 <25.0 <25.0 <31.0 <41.3 <41.3
TMW-7 6/1/2023 <0.596 <0.457 <0.890 <0.0560 <0.0620 <0.0590 57.7 J 57.4 J <25.0 <25.0 <32.1 <42.8 <42.8
TMW-8 5/31/2023 <0.596 <0.457 <0.890 <0.0560 <0.0620 <0.0590 <25.0 <25.0 <25.0 <25.0 <31.1 <41.5 <41.5
TMW-9 6/1/2023 <0.596 <0.457 <0.890 <0.0609 <0.0674 <0.0641 <25.0 <25.0 <25.0 <25.0 <31.5 <42.0 <42.0
TMW-10 6/1/2023 <0.596 <0.457 <0.890 <0.0583 <0.0646 <0.0615 <25.0 <25.0 <25.0 <25.0 <31.2 <41.6 <41.6
1 600 500 1 30 6 400 400 700 700 700 N/A N/A
Notes:
All concentrations reported in micrograms per liter (µg/L).
Bolded values greater than laboratory reporting limit.
Concentration exceeds NCDEQ Groundwater Quality Standard (GWQS) per 15A NCAC 02L .0202
J - Result is less than laboratory reporting limit but greater than or equal to the laboratory method detection limit and the concentration is an approximate value.
N/A - Not available
C11-C22 Aromatics
(Adjusted)
Analytical Method EPA 8260
Contaminant of Concern
Benzene Xylenes
GWQS
NaphthaleneToluene
C9-C12
Aliphatics
(Unadjusted)
C9-C12
Aliphatics
(Adjusted)
TMW-1
TMW-2
TMW-3
Table 2: Summary of Groundwater Sampling Results
640 Rock Lane
C5-C8
Aliphatics
(Adjusted)
C5-C8
Aliphatics
(Unadjusted)
MADEP VPH
China Grove, North Carolina
1-Methyl-
naphthalene
2-Methyl-
naphthalene
MADEP EPH
C9-C18
Aliphatics
C11-C22 Aromatics
(Unadjusted)
EPA 625
Well ID TOC Elevation Depth to Water Groundwater
Elevation
TMW-1 99.82 13.21 86.61
TMW-2 99.29 13.21 86.08
TMW-3 100.16 14.41 85.75
TMW-4 98.39 12.47 85.92
TMW-5 99.69 13.13 86.56
TMW-6 101.91 DRY --
TMW-7 103.91 17.01 86.9
TMW-9 99.36 13.24 86.12
TMW-10 99.72 13.66 86.06
Notes:
Depth to water collected on 6/1/23
Top of casing (TOC) Elevation measured relative to a predetermined benchmark of 100 feet
Table 3: Groundwater Elevation
640 Rock Lane
China Grove, NC
FIGURES

N

Figure 1 – Subject Property Location Map
640 Rock Lane
China Grove, North Carolina
Project Manager: Brad White

Subject
Property
EB-2
EB-3EB-4EB-5
EB-6/EB-6B
GARAGE
WELL HOUSE
GRAVEL
DRIVE
FORMER UST
FORMER AST
EB-10 EB-11 EB-7/EB-7B EB-12 EB-13
EB-8
EB-9
EB-1 EB-15
EB-14
EB-16
EB-17
Figure 2:
Soil Sample Location Map
640 Rock Lane
China Grove, North Carolina N
0 15 30 457.5 Feet
Legend:
Approximate Property Boundary
Structure
Former UST/AST Approximate Location
Soil Sample Location
TMW-1
TMW-3
GARAGE
WELL HOUSE
GRAVEL
DRIVE
FORMER UST
FORMER AST
TMW-10
TMW-8TMW-6
(No Sample)
TMW-4
TMW-9TMW-2
TMW-5 TMW-7
Figure 3:
Groundwater Sample Location Map
640 Rock Lane
China Grove, North Carolina N
0 15 30 457.5 Feet
Legend:
Approximate Property Boundary
Structure
Former UST/AST Approximate Location
Groundwater Sample Location
TMW-1
TMW-3
GARAGE
WELL HOUSE
GRAVEL
DRIVE
FORMER UST
FORMER AST
TMW-10
TMW-8TMW-6
(No Sample)
TMW-4
TMW-9
85.75
86.08
85.92
86.12
86.06
86.0 86.5
86.0
87.0
87.0
86.5
TMW-2
86.61
TMW-5
86.56
TMW-7
86.9
Figure 4:Water Table Map
640 Rock Lane
China Grove, North Carolina
Legend:
Approximate Property Boundary
Structure
Former UST/AST Approximate Location
Groundwater Sample Location
Presumed Groundwater Flow Direction
N
0 15 30 457.5 Feet
ATTACHMENT A
UST CERTIFICATE OF RECYCLING
P.O. Box 236
Barstow, MD 20610
[phone]
CERTIFICATE OF RECYCLING:
Issued to:
Received Date:
Bill of Lading #:
DESCRIPTION OF WASTE: Quantity Size/Type Weight

Clean Safe Technologies, Inc. certifies acceptance of the material referenced on this
document. The material has been managed/recycled in accordance with United States
Environmental Protection Agency waste management regulations.
I certify that the information contained in or accompanying this document is true,
accurate and complete as to the identification of the materials received from the waste
generating company and the processing of the waste in accordance with the United
State Environmental Protection Agency waste management regulations.
Name: DONALD LAMOND Title: PRESIDENT
Signature: Date:
JJ KANE AUCTIONEERS
May 3, 2023
640 Rock Lane
China Grove, NC
UST was Cut in Half, Cleaned & Transported to
Salvage Yard for Destruction 1 Tank 250GAL
3/28/2023
ATTACHMENT B
WASTE MANIFEST FOR SOIL
ATTACHMENT C
SOIL BORING LOGS AND MONITORING WELL CONSTRUCTION
DIAGRAMS
oNl: liNvt RoNMt:N't'AI. (;R()r.,t,
Project No.GAo1 02-0003-2 Soil Boring / Well lD EB-1/TMW-1
Site Location China Grove, NC Date Started 41612023
Client Altec Date Completed 4t6t2023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material PVC
Drilling Method Direct Push Groundwater Depth (feet)N/A Well Diameter (inches)1
Logged By BW Well Type Monitoring Temporary / Stick-Up i Flush Temporary
oo
oo
to
LOgE
G-
=guJ
.9
-o,6
oo
LOg 9^
E IE
^oe.LE
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
tI
!
=
=
4.5
14.6
50.5
104.6
183.8
Topsoil (2") and red clay from pile (backfill material for UST excavation)
EB-1 (8-10) collected at 8-10'bgs
Soil damp at 1 1' bgs
Soil wet at 25'
Soil screening ceased
Orange silty clay
Orange sofl silty clay
Tan and orange with brown streaks soft silty clay
Tan with brown veins soft clay, trace silt
Boring terminated at 35'
Project No.GAo1 02-0003-2 Soil Boring / Well lD EB-2
Site Location China Grove, NC Date Staded 4t6t2023
Client Altec Date Completed 4t6t2023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type Temporary / Stick-Up / Flush
oo
o.oo
6'LOo!6-
=gIIJ
.9
-oi;
oo
LOg 9^
E sEoEeo-u
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
NA
b.b
6.8
8.2
Iopsoil and red clav (backfill material for UST excavation)
No soil recovered from 0-2' bgs
EB-2 (8-1 0) collected at 8-1 0' bgs
Soil damp at 1 3' bgs
Soil wet at 20' bgs
Paqe 1 of 1
f,range silty clay
lrange soft silty clay
fan and orange with brown streaks soft silty clay
Ian with brown veins soft clay, trace silt
Boring terminated at 25'
N
oN Ii tiNvl RoN M uNl'Al, (;l{r}U t,
Project No.GA01 02-0003-2 Soil Boring / Well lD EB-3
Site Location China Grove, NC Date Started 41612023
Client Altec Date Completed 41612023
Drilling Company M&W Drilljng Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type Temporary / Stick-Up / Flush
o0)
o.
6Jo
ELOgE
sE
lrJ
.9
-o
=froo
LO99,^6J!tr
= KA
^oElo- x,
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
8.1
7.2
8.5
8.5
9.2
Topsoil (2") and red clay from pile (backfill material for UST excavation)
EB-3 (8-1 0) collected at 8-1 0' bgs
Soil damp at 13'bgs
Paqe 1 of 1
Orange silty clay
Orange soft silty clay
Tan and orange with brown streaks soft silty clay
Tan with brown veins soft clay, trace silt
Boring terminated at 20'
oNli liNvl RnN M liNl'At, (;ttorIP
Project No.GA01 02-0003-2 Soil Boring / Well lD EB-4
Site Location China Grove, NC Date Started 4t712023
Client Altec Date Completed 41712023
Drilling Company [/&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type Temporary / Stick-Up / Flush
o(,
d)o
o
LOgE6-
=glrJ
c
.9
-oOP
=froo
LO.9 q^
=
gE
AoELo-E
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
0.8
1.4
5.6
13.2
fopsoil and backfill material (2-3")
EB-4 (8-10) collected 8-10' bgs
Page 1 of '1
Orange clay, trace silt
silty clay
Boring terminated at 20'
Project No.GA01 02-0003-2 Soil Boring / Well lD EB-5
Site Location China Grove, NC Date Started 41712023
Client Altec Date Completed 4t7t2023
Drilling Company lil&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type Temporary / Stick-Up / Flush
oo
o.oo
EL (ll8EO-
=glrJ
c
F
-ooiBfrc
o
LOg9^
E sEoago.d
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
NA
18.3
31.6
55.6
Topsoil and backfill material (2-3")
No recovery from 0-3'bgs
EB-5 (8-10) collected at 8-10' bgs
Page 1 of 1
Orange silty clay
Boring terminated at 20'
ONE
()Nli liN\/l Rr)Nl\l liN'l Al. {;l{{)lJt,
oNI.: I.:NVl R()NM 11 N I AI. (;lt0t,l,
Project No.GA01 02-0003-2 Soil Boring / Well lD EB-6
Site Location China Grove, NC Date Started 4t712023
Client Altec Date Completed 4t712023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type Temporary / Stick-Up / Flush
oo
oo
Eo
LOgE
6r
=E
UJ
.9
-oi;
oo
!o99,^6r!tr
= Ba
^oELa-u
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
1.2
1.8
12.8
129.5
385.1
Topsoil (2") and red clay from pile (backfill material for UST excavation)
E8-6 (8-10) collected at 8-10' bgs
Petroleum odor
Paoe 1 of '1
Orange silty clay
Orange soft silty clay
Tan and orange with brown streaks soft silty clay
Tan with brown veins soft clay, trace silt
Boring terminated at 25'
Project No.GA01 02-0003-2 Soil Boring / Well lD EB.7
Site Location China Grove, NC Date Started 41712023
Client Altec Date Completed 41712023
Drilling Company [/&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type Temporary / Stick-Up / Flush
0,0,
o.oo
to
LO6)!
=glrJ
.9
-o
=6oo
LOg 9^
E IE.
^oElo-0/
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
t_J
22.1
z.o
2.0
2.8
1.9
Topsoil (2") and red clay from pile
Unidentifiable odor 3-5' bgs
EB-7 (3-5) collected at 3-5' bgs
Paqe 1 of 1
Orange silty clay
Orange soft silty clay
Tan and orange with brown streaks soft silty clay
Tan with brown veins soft clay, trace silt
Boring terminated at 25'
ON,F
ONIi INVIRONM}.:NTAI, CROUI'
Project No.GA01 02-0003-2 Soil Boring / Well lD EB-8/TMW-2
Site Location China Grove, NC Date Started 41612023
Client Altec Date Completed 41612023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material PVC
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)I
Logged By BW Well Type lVonitoring Temporary / Stick-Up / Flush Temporary
0)d)
oo
t0)LOgE6a
=g
uJ
.9
-o
=froo
L6'9a^
=
gE
^oELo-E
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
E
3.8
5.4
7.8
6.6
11.0
24.1
Topsoil (2-3")
EB-8 (8-1 0) collected at 8-1 0' bgs
Paqe 1 of 1
Orange silty clay
Orange soft silty clay
Tan and orange with brown streaks soft silty clay
Tan with brown veins soft clay, trace silt
Boring terminated at 30'
oN It tiNvl RoN M trN't'Al, (; R(tlt, I,
Project No.GA01 02-0003-2 Soil Boring / Well lD EB.g/TMW.3
Site Location China Grove, NC Date Started 4t612023
Client Altec Date Completed 41612023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material PVC
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)I
Logged By BW Well Type Monitoring Temporary / Stick-Up / Flush Temporary
oo
o.oo
o
LOgEO-
=g
llJ
o
-oOJ
=;oo
LO.g q^i 3e
^ooo- x,
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
I
NA
5.5
1'1.3
13.5
12.3
ropsoil (2-3")
No recovery from 0-2' bgs
EB-g (8-10) collected at 8-10'bgs
Soil damp at 9' bgs
Paqe 1 of 1
Orange clay, trace silt
Orange and tan silty clay
Tan and orange with brown streaks soft silty clay
Tan with brown veins soft clay, trace silt
Boring terminated at 30'
Project No.GA01 02-0003-2 Soil Boring / Well lD EB-68
Site Location China Grove, NC Date Started 5t30t2023
Client Altec Date Completed 5t30t2023
Drilling Company [/&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type Temporary / Stick-Up / Flush
od)
oo
ELOor!Or
=EuJ
c
jj
>E>a E
o
LOg 9^gEE
^oe=ovo-u
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
1.0
Iopsoil (2")
EB-6 (3-5) collected at 3-5'bgs
Paqe 1 of 1
Orange silty clay
Boring terminated at 5' bgs
ONE
oNti liNVt t,t{)NIt t.:N l Al, (;tioillt
Project No.GA01 02-0003-2 Soil Boring / Well lD E8-6B
Site Location China Grove, NC Date Started 513012023
Client Altec Date Completed 513012023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type Temporary / Stick-Up / Flush
oo
tooo
(,
LOgE
6i
=g
UJ
F-o;;tr
o
EE^EEE
= o-o- 0a
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
'1.0
Topsoil (2")
E8-6 (3-5) collected at 3-5'bgs
Page 1 of 1
Orange silty clay
Boring terminated at 5'bgs
ONE
()N t: t.:Nvt tt()N ivl t.:N l Al. (; t.toli t,
ONI: ENVIRONMTiN'I'AI, GROUP
Project No.GA01 02-0003-2 Soil Boring / Well lD EB-7B/TMW-s
Site Location China Grove, NC Date Started 5t3012023
Client Altec Date Completed 513012023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material PVC
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)1
Logged By BW Well Type Monitoring Temporary / Stick-Up / Flush Temporary
(,o
oo
oLLO9EsE
llJ
.9
-(J>E>a
oo
LO.g q^g sE
^oeAE
Soil Description and Strata Depth Comments
0
5
't0
15
20
25
30
35
40
45
s0
55.0
18.0
Topsoil (2")
EB-78 (8-1 0) collected at 8-1 0' bgs
Page 1 of 1
Orange silty clay
Orange soft silty clay
Tan and orange with brown streaks soft silty clay
Tan with brown veins soft clay, trace silt
Boring terminated at 20' bgs
oNIt t;NvIRONM tiNTAL Ctt(}t.'P
Project No.GA01 02-0003-2 Soil Boring / Well lD EB-10/TMW.4
Site Location China Grove, NC Date Started 5t30t2023
Client Altec Date Completed 5t30t2023
Drilling Gompany M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material PVC
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)1
Logged By BW Well Type Monitoring Temporary / Stick-Up / Flush Temporary
oo
oo
o)
LOgE
6-
=EIJJ
.9
-o56
oo
LOg 9^
EEEAocL
o-E
Soil Description and Strata Depth Comments
0
5
'10
15
20
25
30
35
40
45
50
I I
lt
ND
ND
Grass/vegetation and topsoil (2")
EB-10 (8-10) collected at 8-10'bgs
Paqe 1 of 1
Orange clay, trace silt
Orange and tan silty clay (soft)
Tan fine sandy silt, trace clay
Boring terminated at 20' bgs
Project No.GAo'102-0003-2 Soil Boring / Well lD EB-11
Site Location China Grove, NC Date Started 513012023
Client Altec Date Completed 513012023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type Temporary / Stick-Up / Flush
oo
EL0,o
o)
LOgE
6!
=5-o
lrJ
.9
-oOP7Ft
o(.)
LOg 9^esE
^oo= o-o-E
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
ND
ND
Grass and topsoil (2")
EB-1 1 (3-5) collected at 3-5' bgs
Paoe 1 of 1
Orange clay, trace silt
Orange and tan silty clay (soft)
Boring terminated at 10' bgs
ONE
()Nll liNvt RoNMliN't Al. (;ttot,l,
ONTi INVIRONMT'NTAI, GItOt,,P
Project No.GAo1 02-0003-2 Soil Boring / Well lD E8.12lTMW-6
Site Location China Grove, NC Date Started 513112023
Client Altec Date Completed 513112023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material PVC
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)1
Logged By BW Well Type Monitoring Temporary / Stick-Up / Flush Temporary
oo
aoo
ELOgE6r
=glrJ
.9
-oi;
oo
LO.g o^
= gE
AocL= o-o-E
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
ND
ND
Concrete (4")
EB-12 (2-4) collected at 2-4' bgs
EB-12 (6-8) collected at 6-8' bgs
Soil soft and damp at 8'bgs
Paqe 1 of 1
T
I
Red and tan clay, trace silt
Orange and tan silty clay
Boring terminated at 13'bgs
Project No.GA01 02-0003-2 Soil Boring / Well lD EB-13/TMW-7
Site Location China Grove, NC Date Started 513112023
Client Altec Date Completed 5t3112023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material PVC
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)1
Logged By BW Well Type Monitoring Temporary / Stick-Up / Flush Temporary
oo
ooo
Eo
LOo!i
d!
=ElrJ
.9
=9t;
oo
LOg 9^EsE
^ocLo.E
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
ND
2.0
Bare dirt floor in garage
EB-1 0 (8-1 0) collected at 8-1 0' bgs
Paqe 1 of 1
Orange silty clay
Orange and tan soft silty clay
Red with tan streaks silty clay
Boring terminated at 15'bgs
ONE
oNti liNVt R{)Nt\l tiN'tAl. (;r{r}lJ I'
oN t; INvt R0NM t.:N't'Al, (;t{ot,t,
Project No.GA01 02-0003-2 Soil Boring / Well lD EB.14lTMW-8
Site Location China Grove, NC Date Started 5t31t2023
Client Altec Date Completed 5t31t2023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material Stainless-Steel
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)I
Logged By BW Well Type Monitorjng femporary / Stick-Up / Flush Temporary
oo
oo
toLL (llo!6-
=EuJ
.9
-ot;
oo
LOg 9^
= ge
^oqo-E
Soil Description and Strata Depth Comments
0
5
10
't5
20
25
30
35
40
45
50
ND
ND
Gravel (2")
EB-14 (8-10) collected at B-10'bgs
Soil wet at 11' bgs
Paoe 1 of 1
Tan and orange clay, trace silt
Orange and tan silty clay
Red and tan silty clay
Boring terminated at 20' bgs
Project No.GAo1 02-0003-2 Soil Boring / Well lD EB-15/TMW-g
Site Location China Grove, NC Date Started 513012023
Client Altec Date Completed 5t30t2023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material PVC
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)I
Logged By BW Well Type l\/onitoring femporary / Stick-Up / Flush Temporary
0)o
o.oo
E
ELOQ,JE:
=gIIJ
o
-oi.b>o
oo
LO.g 9^
E sEAocl
o-E
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
I
!
I
r
ND
ND
Sparce grass and topsoil (2")
EB-1 5 (8-1 0) collected at 8-1 0' bgs
Paqe 1 of 1
Orange and tan silty clay
Tan silty clay
Red and tan clay, trace silt
Boring terminated at 20' bgs
SN E
0Nti tiNvr R0NM t.:N't'Al, (ir{()uP
Project No.GA0'102-0003-2 Soil Boring / Well lD E8.16/TMW-10
Site Location China Grove, NC Date Started 513112023
Client Altec Date Completed 513112023
Drilling Company M&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material PVC
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)I
Logged By BW Well Type Monitoring Temporary / Stick-Up / Flush Temporary
oo
o.q)o
t,o
LOo!
6!
=gIJJ
.9
-o,6
oo
LOg 9^eIE
^@ao-tr
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
ND
ND
Bare ground and topsoil (3")
Hand augered 0-5' bgs
EB-16 (2-3) collected at 2-3' bgs
Paqe 1 of 1
Orange and tan silty clay
Tan silty clay
Red and tan clay, trace silt
Boring terminated at 20' bgs
Project No.GA01 02-0003-2 Soil Boring / Well lD EB,.17
Site Location China Grove, NC Date Started 513112023
Client Altec Date Completed 513112023
Drilling Company [/&W Drilling Soil Sampling Method Dual Tube Well Screen / Riser Material
Drilling Method Direct Push Groundwater Depth (feet)Well Diameter (inches)
Logged By BW Well Type femporary / Stick-Up / Flush
oo
o(,o
Eo
LOo!
6r
=gUI
.9
-oi;
oo
LOo6i gE
^oelLE
Soil Description and Strata Depth Comments
0
5
10
15
20
25
30
35
40
45
50
ND
ND
Bare ground and topsoil (3")
Hand augered 0-5' bgs
EB-1 7 (8-1 0) collected at 8-'l 0' bgs
Page 1 of 1
Tan and orange silty clay
Boring terminated at 10' bgs
ONE
()Nli rlNvlttoNlvlriN't t, (;t.{ol,t,
ATTACHMENT D
LABORATORY ANALYTICAL DATA REPORTS
ANALYTICAL REPORT
PREPARED FOR
Attn: Mr. Bruce Stainbrook
Altec Industries, Inc
Bruce Stainbrook
810 Franklin Court, Ste A
Marietta, Georgia 30067
Generated 5/5/2023 4:28:26 PM
JOB DESCRIPTION
China Grove NC
SDG NUMBER 640 Rock Lane
JOB NUMBER
180-154769-1
See page two for job notes and contact information.
Pittsburgh PA 15238
RIDC Park
301 Alpha Drive
Eurofins Pittsburgh
Page 1 of 49
1
2
3
4
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6
7
8
Eurofins Pittsburgh
Eurofins Pittsburgh is a laboratory within Eurofins Environment Testing Northeast LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced,
except in full, without the written approval of the laboratory. This report is confidential and is intended for the sole use of
Eurofins Environment Testing Northeast, LLC Pittsburgh and its client. All questions regarding this report should be directed
to the Eurofins Environment Testing Northeast, LLC Pittsburgh Project Manager or designee who has signed this report.
PA Lab ID: 02-00416
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Pittsburgh Project Manager.
Authorization
Generated
5/5/2023 4:28:26 PM
Authorized for release by
Shali Brown, Project Manager II
[e-mail]
[phone]
Page 2 of 49 5/5/2023
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3
4
5
6
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8
Case Narrative
Client: Altec Industries, Inc Job ID: 180-154769-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-154769-1
Laboratory: Eurofins Pittsburgh
Narrative
Job Narrative
180-154769-1
Receipt
The samples were received on 4/7/2023 9:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 1.3°C
GC/MS VOA
Method 8260D: The continuing calibration verification (CCV) analyzed in 180-432477 was outside the method criteria for the following
analyte(s): Dichloro-difluoromethane and Methyl acetate (HIGH). As indicated in the reference method, sample analysis may proceed;
however, any detection for the affected analyte(s) is considered estimated.
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-432477 was outside the method criteria for the
following analyte(s): Chloromethane, 1,2-Dibromo-3-Chloropropane, 1,1,2-Trichloroethane, 2-Hexanone and 4-Methyl-2-pentanone
(LOW). A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As
indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered
estimated.
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-432477 was outside the method criteria for the
following analyte(s): 1,2-Dibromo-3-Chloropropane (RF). A CCV standard at or below the reporting limit (RL) was analyzed with the
affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any
detection for the affected analyte(s) is considered estimated.
Method 8260D: The laboratory control sample (LCS) for analytical batch 180-432477 recovered outside control limits for the following
analytes: Dichloro-difluoromethane and Methyl acetate. These analytes were biased high in the LCS and were not detected in the
associated samples; therefore, the data have been reported.
Method 8260D: The laboratory control sample duplicate (LCSD) for analytical batch 180-432477 recovered outside control limits for the
following analytes: Dichloro-difluoromethane and Methylene Chloride. These analytes were biased high in the LCSD and were not
detected in the associated samples; therefore, the data have been reported.
Method 8260D: Surrogate recovery for the following sample was outside the upper control limit: EB-1 (8-10) (180-154769-1). This sample
did not contain any target analytes; therefore, re-extraction and/or re-analysis was not performed.
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-432752 was outside the method criteria for the
following analyte(s): Acetone, 2-Hexanone and 2-Butanone (LOW). A CCV standard at or below the reporting limit (RL) was analyzed with
the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any
detection for the affected analyte(s) is considered estimated.
Method 8260D: The continuing calibration verification (CCV) analyzed in 180-432752 was outside the method criteria for the following
analyte(s): Methyl acetate, Dichloro-difluoromethane and 1,1,2-Trichloro-1,2,2-trifluoroethane (HIGH). As indicated in the reference
method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated.
Method 8260D: The laboratory control sample duplicate (LCSD) for analytical batch 180-432752 recovered outside control limits for the
following analytes: Dichloro-difluoromethane. These analytes were biased high in the LCSD and were not detected in the associated
samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
Method 8270E: The continuing calibration verification (CCV) associated with batch 180-432356 recovered above the upper control limit for
Pentachlorophenol. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been
reported. The associated sample is impacted: (CCVIS 180-432356/3).
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Case Narrative
Client: Altec Industries, Inc Job ID: 180-154769-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-154769-1 (Continued)
Laboratory: Eurofins Pittsburgh (Continued)
Method 8270E: The continuing calibration verification (CCV) associated with batch 180-432356 recovered outside acceptance criteria, low
biased, for 2,2'-oxybis[1-chloropropane]. A reporting limit (RL) standard was analyzed, and the target analytes are detected. Since the
associated samples were non-detect for the analyte(s), the data are reported.
Method 8270E: The continuing calibration verification (CCV) associated with batch 180-432297 recovered outside acceptance criteria, low
biased, for Di-n-octyl phthalate. A reporting limit (RL) standard was analyzed, and the target analytes are detected. Since the associated
samples were non-detect for the analyte(s), the data are reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
Method MAVPH: The following sample(s) were received in pre-weighed containers with a label that was added in the field, which would
cause a slight low bias in the final results. EB-1 (8-10) (180-154769-1), EB-2 (8-10) (180-154769-2), EB-3 (8-10) (180-154769-3), EB-8
(8-10) (180-154769-4) and EB-9 (8-10) (180-154769-5).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method MAEPH2.1: The breakthrough for naphthalene and 2-methylnaphthalene in the LCS and LCSD is <1%. The method requirement
for breakthrough is <5%. EB-1 (8-10) (180-154769-1), EB-2 (8-10) (180-154769-2), EB-3 (8-10) (180-154769-3), EB-8 (8-10)
(180-154769-4) and EB-9 (8-10) (180-154769-5)
Method MAEPH2.1: 1-Chlorooctadecane (Surr) recovery for the following samples were outside acceptance limits: EB-1 (8-10)
(180-154769-1), EB-8 (8-10) (180-154769-4) and (180-154822-I-1-B). The samples cannot be re-extracted and re-analyzed within method
holding time. The results have been reported per client request.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Definitions/Glossary
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
F1 MS and/or MSD recovery exceeds control limits.
F2 MS/MSD RPD exceeds control limits
S1+Surrogate recovery exceeds control limits, high biased.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
S1-Surrogate recovery exceeds control limits, low biased.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Accreditation/Certification Summary
Client: Altec Industries, Inc Job ID: 180-154769-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Laboratory: Eurofins Pittsburgh
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 434 05-03-23
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 521 12-31-23
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-1Client Sample ID: EB-1 (8-10)
Matrix: SolidDate Collected: 04/06/23 09:00
Percent Solids: 67.9Date Received: 04/07/23 09:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.32 2.45 ug/Kg ☼04/19/23 07:41 04/19/23 14:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.32 2.23 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,1,2,2-Tetrachloroethane
7.32 2.93 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
7.32 1.45 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,1,2-Trichloroethane
7.32 2.34 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,1-Dichloroethane
7.32 3.31 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,1-Dichloroethene
7.32 4.73 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,2-Dibromo-3-Chloropropane
7.32 2.46 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,2-Dichlorobenzene
7.32 2.11 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,2-Dichloroethane
7.32 1.95 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,2-Dichloropropane
7.32 3.72 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,2,4-Trichlorobenzene
7.32 4.51 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,3-Dichlorobenzene
7.32 2.20 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,4-Dichlorobenzene
7.32 3.72 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND2-Butanone (MEK)
7.32 2.30 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND2-Hexanone
7.32 2.68 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND4-Methyl-2-pentanone (MIBK)
29.3 5.71 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDAcetone
7.32 2.07 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDBenzene
7.32 3.69 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDBromoform
7.32 3.34 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDBromomethane
7.32 5.86 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDCarbon disulfide
7.32 2.97 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDCarbon tetrachloride
7.32 1.90 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDChlorobenzene
7.32 3.63 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDChlorodibromomethane
7.32 2.36 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDChloroform
7.32 2.90 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDChloromethane
7.32 4.28 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDChloroethane
7.32 2.21 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDcis-1,2-Dichloroethene
7.32 3.24 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDcis-1,3-Dichloropropene
7.32 3.41 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDDichlorobromomethane
7.32 3.65 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND *+Dichlorodifluoromethane
7.32 2.71 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDEthylbenzene
7.32 2.01 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼ND1,2-Dibromoethane
7.32 3.50 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDCyclohexane
7.32 3.81 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDIsopropylbenzene
36.6 10.8 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDMethyl acetate
7.32 2.15 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDMethyl tert-butyl ether
7.32 3.53 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDMethylcyclohexane
7.32 6.61 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDMethylene Chloride
7.32 2.20 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDStyrene
7.32 2.94 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDTetrachloroethene
7.32 2.11 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDToluene
7.32 2.56 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDtrans-1,2-Dichloroethene
7.32 3.30 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDtrans-1,3-Dichloropropene
7.32 2.30 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDTrichloroethene
7.32 6.08 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDTrichlorofluoromethane
7.32 5.27 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDVinyl chloride
14.6 10.6 ug/Kg 04/19/23 07:41 04/19/23 14:38 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-1Client Sample ID: EB-1 (8-10)
Matrix: SolidDate Collected: 04/06/23 09:00
Percent Solids: 67.9Date Received: 04/07/23 09:30
1,2-Dichloroethane-d4 (Surr)138 S1+73-135 04/19/23 07:41 04/19/23 14:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)101 04/19/23 07:41 04/19/23 14:38 160-124
Dibromofluoromethane (Surr)114 04/19/23 07:41 04/19/23 14:38 169-126
Toluene-d8 (Surr)101 04/19/23 07:41 04/19/23 14:38 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 471 174 ug/Kg ☼04/14/23 06:07 04/14/23 18:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
95.5 35.2 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2,2'-oxybis[1-chloropropane]
471 165 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2,4,5-Trichlorophenol
471 158 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2,4,6-Trichlorophenol
95.5 36.6 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2,4-Dichlorophenol
471 160 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2,4-Dimethylphenol
4710 2950 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2,4-Dinitrophenol
471 284 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2,4-Dinitrotoluene
471 185 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2,6-Dinitrotoluene
95.5 21.8 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2-Chloronaphthalene
471 175 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2-Chlorophenol
95.5 22.8 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2-Methylnaphthalene
471 136 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2-Methylphenol
2420 217 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2-Nitroaniline
471 175 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND2-Nitrophenol
471 443 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND3,3'-Dichlorobenzidine
2420 121 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND3-Nitroaniline
2420 820 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND4,6-Dinitro-2-methylphenol
471 202 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND4-Bromophenyl phenyl ether
471 167 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND4-Chloro-3-methylphenol
471 125 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND4-Chloroaniline
471 158 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND4-Chlorophenyl phenyl ether
471 140 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDMethylphenol, 3 & 4
2420 177 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND4-Nitroaniline
2420 334 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼ND4-Nitrophenol
95.5 27.4 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDAcenaphthene
95.5 20.8 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDAcenaphthylene
955 170 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDAcetophenone
95.5 24.7 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDAnthracene
955 208 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDAtrazine
955 59.0 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDBenzaldehyde
95.5 42.9 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDBenzo[a]anthracene
95.5 41.2 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDBenzo[a]pyrene
95.5 23.4 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDBenzo[b]fluoranthene
95.5 20.5 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDBenzo[g,h,i]perylene
95.5 28.5 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDBenzo[k]fluoranthene
471 174 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDBis(2-chloroethoxy)methane
95.5 17.3 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDBis(2-chloroethyl)ether
4710 506 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDBis(2-ethylhexyl) phthalate
471 327 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDButyl benzyl phthalate
2420 309 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDCaprolactam
95.5 22.2 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDCarbazole
95.5 52.8 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDChrysene
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-1Client Sample ID: EB-1 (8-10)
Matrix: SolidDate Collected: 04/06/23 09:00
Percent Solids: 67.9Date Received: 04/07/23 09:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 95.5 60.9 ug/Kg ☼04/14/23 06:07 04/14/23 18:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
471 175 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDDibenzofuran
471 167 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDDiethyl phthalate
471 188 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDDimethyl phthalate
471 208 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDDi-n-butyl phthalate
471 277 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDDi-n-octyl phthalate
95.5 25.1 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDFluoranthene
95.5 18.7 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDFluorene
95.5 34.1 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDHexachlorobenzene
95.5 27.8 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDHexachlorobutadiene
471 48.6 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDHexachlorocyclopentadiene
471 168 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDHexachloroethane
95.5 47.3 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDIndeno[1,2,3-cd]pyrene
471 178 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDIsophorone
95.5 18.5 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDNaphthalene
955 174 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDNitrobenzene
95.5 32.2 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDN-Nitrosodi-n-propylamine
471 158 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDN-Nitrosodiphenylamine
2420 764 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDPentachlorophenol
95.5 25.5 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDPhenanthrene
471 144 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDPhenol
95.5 22.5 ug/Kg 04/14/23 06:07 04/14/23 18:18 1☼NDPyrene
2,4,6-Tribromophenol (Surr)54 34-108 04/14/23 06:07 04/14/23 18:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 59 04/14/23 06:07 04/14/23 18:18 144-105
2-Fluorophenol (Surr)60 04/14/23 06:07 04/14/23 18:18 148-105
Nitrobenzene-d5 (Surr)58 04/14/23 06:07 04/14/23 18:18 146-105
Phenol-d5 (Surr)60 04/14/23 06:07 04/14/23 18:18 146-105
Terphenyl-d14 (Surr)67 04/14/23 06:07 04/14/23 18:18 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.37 1.84 mg/Kg ☼04/24/23 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 23.4 5.86 mg/Kg ☼04/16/23 20:00 04/20/23 23:35 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
23.4 5.86 mg/Kg 04/16/23 20:00 04/20/23 23:35 50☼NDC9-C10 Aromatics
23.4 5.86 mg/Kg 04/16/23 20:00 04/20/23 23:35 50☼NDC9-C12 Aliphatics (unadjusted)
23.4 5.86 mg/Kg 04/16/23 20:00 04/20/23 23:35 50☼NDC9-C12 Aliphatics (adjusted)
23.4 5.86 mg/Kg 04/16/23 20:00 04/20/23 23:35 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)117 70-130 04/16/23 20:00 04/20/23 23:35 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)107 04/16/23 20:00 04/20/23 23:35 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.3 17.3 mg/Kg ☼04/13/23 14:59 05/02/23 20:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics
17.3 17.3 mg/Kg 04/13/23 14:59 05/02/23 20:56 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-1Client Sample ID: EB-1 (8-10)
Matrix: SolidDate Collected: 04/06/23 09:00
Percent Solids: 67.9Date Received: 04/07/23 09:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 17.3 17.3 mg/Kg ☼04/13/23 14:59 05/02/23 20:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.65 8.65 mg/Kg 04/13/23 14:59 05/02/23 20:56 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)31 S1-40-140 04/13/23 14:59 05/02/23 20:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)82 04/13/23 14:59 05/02/23 20:56 140-140
o- terphenyl (Surr)67 04/13/23 14:59 05/02/23 20:56 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.7 17.7 mg/Kg ☼05/02/23 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-2Client Sample ID: EB-2 (8-10)
Matrix: SolidDate Collected: 04/06/23 10:20
Percent Solids: 66.0Date Received: 04/07/23 09:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.57 2.53 ug/Kg ☼04/17/23 07:00 04/17/23 17:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.57 2.30 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,1,2,2-Tetrachloroethane
7.57 3.03 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
7.57 1.50 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,1,2-Trichloroethane
7.57 2.42 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,1-Dichloroethane
7.57 3.42 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,1-Dichloroethene
7.57 4.89 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,2-Dibromo-3-Chloropropane
7.57 2.54 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,2-Dichlorobenzene
7.57 2.18 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,2-Dichloroethane
7.57 2.01 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,2-Dichloropropane
7.57 3.84 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,2,4-Trichlorobenzene
7.57 4.66 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,3-Dichlorobenzene
7.57 2.27 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,4-Dichlorobenzene
7.57 3.84 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND2-Butanone (MEK)
7.57 2.38 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND2-Hexanone
7.57 2.77 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND4-Methyl-2-pentanone (MIBK)
30.3 5.90 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDAcetone
7.57 2.13 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDBenzene
7.57 3.81 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDBromoform
7.57 3.45 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDBromomethane
7.57 6.05 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDCarbon disulfide
7.57 3.07 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDCarbon tetrachloride
7.57 1.97 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDChlorobenzene
7.57 3.75 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDChlorodibromomethane
7.57 2.44 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDChloroform
7.57 3.00 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDChloromethane
7.57 4.42 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDChloroethane
7.57 2.29 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDcis-1,2-Dichloroethene
7.57 3.35 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDcis-1,3-Dichloropropene
7.57 3.53 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDDichlorobromomethane
7.57 3.77 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND *+Dichlorodifluoromethane
7.57 2.80 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDEthylbenzene
7.57 2.07 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND1,2-Dibromoethane
7.57 3.62 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDCyclohexane
7.57 3.94 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDIsopropylbenzene
37.8 11.1 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND *+Methyl acetate
7.57 2.23 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDMethyl tert-butyl ether
7.57 3.65 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDMethylcyclohexane
7.57 6.83 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼ND *+Methylene Chloride
7.57 2.27 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDStyrene
7.57 3.04 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDTetrachloroethene
7.57 2.18 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDToluene
7.57 2.65 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDtrans-1,2-Dichloroethene
7.57 3.41 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDtrans-1,3-Dichloropropene
7.57 2.38 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDTrichloroethene
7.57 6.28 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDTrichlorofluoromethane
7.57 5.45 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDVinyl chloride
15.1 10.9 ug/Kg 04/17/23 07:00 04/17/23 17:11 1☼NDXylenes, Total
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-2Client Sample ID: EB-2 (8-10)
Matrix: SolidDate Collected: 04/06/23 10:20
Percent Solids: 66.0Date Received: 04/07/23 09:30
1,2-Dichloroethane-d4 (Surr)122 73-135 04/17/23 07:00 04/17/23 17:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)105 04/17/23 07:00 04/17/23 17:11 160-124
Dibromofluoromethane (Surr)119 04/17/23 07:00 04/17/23 17:11 169-126
Toluene-d8 (Surr)106 04/17/23 07:00 04/17/23 17:11 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 497 184 ug/Kg ☼04/14/23 06:07 04/14/23 18:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
101 37.2 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2,2'-oxybis[1-chloropropane]
497 175 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2,4,5-Trichlorophenol
497 167 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2,4,6-Trichlorophenol
101 38.7 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2,4-Dichlorophenol
497 169 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2,4-Dimethylphenol
4970 3120 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2,4-Dinitrophenol
497 300 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2,4-Dinitrotoluene
497 196 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2,6-Dinitrotoluene
101 23.0 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2-Chloronaphthalene
497 185 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2-Chlorophenol
101 24.1 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2-Methylnaphthalene
497 144 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2-Methylphenol
2560 229 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2-Nitroaniline
497 185 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND2-Nitrophenol
497 468 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND3,3'-Dichlorobenzidine
2560 128 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND3-Nitroaniline
2560 865 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND4,6-Dinitro-2-methylphenol
497 214 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND4-Bromophenyl phenyl ether
497 176 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND4-Chloro-3-methylphenol
497 132 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND4-Chloroaniline
497 167 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND4-Chlorophenyl phenyl ether
497 147 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDMethylphenol, 3 & 4
2560 187 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND4-Nitroaniline
2560 352 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼ND4-Nitrophenol
101 28.9 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDAcenaphthene
101 22.0 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDAcenaphthylene
1010 179 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDAcetophenone
101 26.0 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDAnthracene
1010 220 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDAtrazine
1010 62.3 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDBenzaldehyde
101 45.3 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDBenzo[a]anthracene
101 43.5 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDBenzo[a]pyrene
101 24.7 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDBenzo[b]fluoranthene
101 21.7 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDBenzo[g,h,i]perylene
101 30.1 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDBenzo[k]fluoranthene
497 184 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDBis(2-chloroethoxy)methane
101 18.2 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDBis(2-chloroethyl)ether
4970 534 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDBis(2-ethylhexyl) phthalate
497 345 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDButyl benzyl phthalate
2560 327 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDCaprolactam
101 23.5 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDCarbazole
101 55.7 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDChrysene
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-2Client Sample ID: EB-2 (8-10)
Matrix: SolidDate Collected: 04/06/23 10:20
Percent Solids: 66.0Date Received: 04/07/23 09:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 101 64.3 ug/Kg ☼04/14/23 06:07 04/14/23 18:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
497 185 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDDibenzofuran
497 176 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDDiethyl phthalate
497 199 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDDimethyl phthalate
497 220 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDDi-n-butyl phthalate
497 292 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDDi-n-octyl phthalate
101 26.5 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDFluoranthene
101 19.7 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDFluorene
101 36.0 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDHexachlorobenzene
101 29.3 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDHexachlorobutadiene
497 51.3 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDHexachlorocyclopentadiene
497 178 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDHexachloroethane
101 50.0 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDIndeno[1,2,3-cd]pyrene
497 188 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDIsophorone
101 19.6 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDNaphthalene
1010 184 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDNitrobenzene
101 34.0 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDN-Nitrosodi-n-propylamine
497 167 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDN-Nitrosodiphenylamine
2560 807 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDPentachlorophenol
101 26.9 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDPhenanthrene
497 152 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDPhenol
101 23.8 ug/Kg 04/14/23 06:07 04/14/23 18:39 1☼NDPyrene
2,4,6-Tribromophenol (Surr)55 34-108 04/14/23 06:07 04/14/23 18:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 57 04/14/23 06:07 04/14/23 18:39 144-105
2-Fluorophenol (Surr)62 04/14/23 06:07 04/14/23 18:39 148-105
Nitrobenzene-d5 (Surr)58 04/14/23 06:07 04/14/23 18:39 146-105
Phenol-d5 (Surr)62 04/14/23 06:07 04/14/23 18:39 146-105
Terphenyl-d14 (Surr)66 04/14/23 06:07 04/14/23 18:39 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.58 1.89 mg/Kg ☼04/24/23 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 23.0 5.75 mg/Kg ☼04/16/23 20:00 04/21/23 00:16 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
23.0 5.75 mg/Kg 04/16/23 20:00 04/21/23 00:16 50☼NDC9-C10 Aromatics
23.0 5.75 mg/Kg 04/16/23 20:00 04/21/23 00:16 50☼NDC9-C12 Aliphatics (unadjusted)
23.0 5.75 mg/Kg 04/16/23 20:00 04/21/23 00:16 50☼NDC9-C12 Aliphatics (adjusted)
23.0 5.75 mg/Kg 04/16/23 20:00 04/21/23 00:16 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)111 70-130 04/16/23 20:00 04/21/23 00:16 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)102 04/16/23 20:00 04/21/23 00:16 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.1 18.1 mg/Kg ☼04/13/23 14:59 05/02/23 21:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics
18.1 18.1 mg/Kg 04/13/23 14:59 05/02/23 21:19 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-2Client Sample ID: EB-2 (8-10)
Matrix: SolidDate Collected: 04/06/23 10:20
Percent Solids: 66.0Date Received: 04/07/23 09:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 18.1 18.1 mg/Kg ☼04/13/23 14:59 05/02/23 21:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
9.04 9.04 mg/Kg 04/13/23 14:59 05/02/23 21:19 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)49 40-140 04/13/23 14:59 05/02/23 21:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)76 04/13/23 14:59 05/02/23 21:19 140-140
o- terphenyl (Surr)54 04/13/23 14:59 05/02/23 21:19 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.2 18.2 mg/Kg ☼05/02/23 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-3Client Sample ID: EB-3 (8-10)
Matrix: SolidDate Collected: 04/06/23 11:45
Percent Solids: 65.9Date Received: 04/07/23 09:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.49 2.50 ug/Kg ☼04/17/23 07:00 04/17/23 17:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.49 2.28 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,1,2,2-Tetrachloroethane
7.49 3.00 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
7.49 1.48 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,1,2-Trichloroethane
7.49 2.40 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,1-Dichloroethane
7.49 3.39 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,1-Dichloroethene
7.49 4.84 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,2-Dibromo-3-Chloropropane
7.49 2.52 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,2-Dichlorobenzene
7.49 2.16 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,2-Dichloroethane
7.49 1.99 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,2-Dichloropropane
7.49 3.81 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,2,4-Trichlorobenzene
7.49 4.62 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,3-Dichlorobenzene
7.49 2.25 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,4-Dichlorobenzene
7.49 3.81 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND2-Butanone (MEK)
7.49 2.35 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND2-Hexanone
7.49 2.74 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND4-Methyl-2-pentanone (MIBK)
30.0 5.85 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDAcetone
7.49 2.11 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDBenzene
7.49 3.78 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDBromoform
7.49 3.42 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDBromomethane
7.49 6.00 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDCarbon disulfide
7.49 3.04 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDCarbon tetrachloride
7.49 1.95 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDChlorobenzene
7.49 3.72 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDChlorodibromomethane
7.49 2.41 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDChloroform
7.49 2.97 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDChloromethane
7.49 4.38 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDChloroethane
7.49 2.26 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDcis-1,2-Dichloroethene
7.49 3.31 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDcis-1,3-Dichloropropene
7.49 3.49 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDDichlorobromomethane
7.49 3.73 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND *+Dichlorodifluoromethane
7.49 2.77 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDEthylbenzene
7.49 2.05 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND1,2-Dibromoethane
7.49 3.58 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDCyclohexane
7.49 3.90 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDIsopropylbenzene
37.5 11.0 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND *+Methyl acetate
7.49 2.20 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDMethyl tert-butyl ether
7.49 3.61 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDMethylcyclohexane
7.49 6.76 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼ND *+Methylene Chloride
7.49 2.25 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDStyrene
7.49 3.01 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDTetrachloroethene
7.49 2.16 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDToluene
7.49 2.62 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDtrans-1,2-Dichloroethene
7.49 3.37 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDtrans-1,3-Dichloropropene
7.49 2.35 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDTrichloroethene
7.49 6.22 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDTrichlorofluoromethane
7.49 5.40 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDVinyl chloride
15.0 10.8 ug/Kg 04/17/23 07:00 04/17/23 17:34 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-3Client Sample ID: EB-3 (8-10)
Matrix: SolidDate Collected: 04/06/23 11:45
Percent Solids: 65.9Date Received: 04/07/23 09:30
1,2-Dichloroethane-d4 (Surr)117 73-135 04/17/23 07:00 04/17/23 17:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)101 04/17/23 07:00 04/17/23 17:34 160-124
Dibromofluoromethane (Surr)116 04/17/23 07:00 04/17/23 17:34 169-126
Toluene-d8 (Surr)106 04/17/23 07:00 04/17/23 17:34 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 488 180 ug/Kg ☼04/14/23 06:07 04/14/23 19:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
99.0 36.5 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2,2'-oxybis[1-chloropropane]
488 171 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2,4,5-Trichlorophenol
488 164 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2,4,6-Trichlorophenol
99.0 38.0 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2,4-Dichlorophenol
488 165 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2,4-Dimethylphenol
4880 3060 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2,4-Dinitrophenol
488 294 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2,4-Dinitrotoluene
488 192 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2,6-Dinitrotoluene
99.0 22.6 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2-Chloronaphthalene
488 182 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2-Chlorophenol
99.0 23.6 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2-Methylnaphthalene
488 141 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2-Methylphenol
2510 225 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2-Nitroaniline
488 182 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND2-Nitrophenol
488 460 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND3,3'-Dichlorobenzidine
2510 125 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND3-Nitroaniline
2510 850 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND4,6-Dinitro-2-methylphenol
488 210 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND4-Bromophenyl phenyl ether
488 173 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND4-Chloro-3-methylphenol
488 129 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND4-Chloroaniline
488 164 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND4-Chlorophenyl phenyl ether
488 145 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDMethylphenol, 3 & 4
2510 183 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND4-Nitroaniline
2510 346 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼ND4-Nitrophenol
99.0 28.4 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDAcenaphthene
99.0 21.6 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDAcenaphthylene
990 176 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDAcetophenone
99.0 25.6 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDAnthracene
990 216 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDAtrazine
990 61.2 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDBenzaldehyde
99.0 44.5 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDBenzo[a]anthracene
99.0 42.7 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDBenzo[a]pyrene
99.0 24.2 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDBenzo[b]fluoranthene
99.0 21.3 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDBenzo[g,h,i]perylene
99.0 29.6 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDBenzo[k]fluoranthene
488 180 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDBis(2-chloroethoxy)methane
99.0 17.9 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDBis(2-chloroethyl)ether
4880 525 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDBis(2-ethylhexyl) phthalate
488 338 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDButyl benzyl phthalate
2510 321 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDCaprolactam
99.0 23.0 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDCarbazole
99.0 54.7 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDChrysene
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-3Client Sample ID: EB-3 (8-10)
Matrix: SolidDate Collected: 04/06/23 11:45
Percent Solids: 65.9Date Received: 04/07/23 09:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 99.0 63.1 ug/Kg ☼04/14/23 06:07 04/14/23 19:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
488 182 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDDibenzofuran
488 173 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDDiethyl phthalate
488 195 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDDimethyl phthalate
488 216 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDDi-n-butyl phthalate
488 287 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDDi-n-octyl phthalate
99.0 26.0 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDFluoranthene
99.0 19.4 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDFluorene
99.0 35.3 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDHexachlorobenzene
99.0 28.8 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDHexachlorobutadiene
488 50.4 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDHexachlorocyclopentadiene
488 174 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDHexachloroethane
99.0 49.1 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDIndeno[1,2,3-cd]pyrene
488 185 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDIsophorone
99.0 19.2 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDNaphthalene
990 180 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDNitrobenzene
99.0 33.4 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDN-Nitrosodi-n-propylamine
488 164 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDN-Nitrosodiphenylamine
2510 792 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDPentachlorophenol
99.0 26.4 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDPhenanthrene
488 149 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDPhenol
99.0 23.3 ug/Kg 04/14/23 06:07 04/14/23 19:01 1☼NDPyrene
2,4,6-Tribromophenol (Surr)52 34-108 04/14/23 06:07 04/14/23 19:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 52 04/14/23 06:07 04/14/23 19:01 144-105
2-Fluorophenol (Surr)54 04/14/23 06:07 04/14/23 19:01 148-105
Nitrobenzene-d5 (Surr)53 04/14/23 06:07 04/14/23 19:01 146-105
Phenol-d5 (Surr)56 04/14/23 06:07 04/14/23 19:01 146-105
Terphenyl-d14 (Surr)60 04/14/23 06:07 04/14/23 19:01 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.58 1.90 mg/Kg ☼04/24/23 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 23.7 5.91 mg/Kg ☼04/16/23 20:00 04/21/23 00:57 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
23.7 5.91 mg/Kg 04/16/23 20:00 04/21/23 00:57 50☼NDC9-C10 Aromatics
23.7 5.91 mg/Kg 04/16/23 20:00 04/21/23 00:57 50☼NDC9-C12 Aliphatics (unadjusted)
23.7 5.91 mg/Kg 04/16/23 20:00 04/21/23 00:57 50☼NDC9-C12 Aliphatics (adjusted)
23.7 5.91 mg/Kg 04/16/23 20:00 04/21/23 00:57 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)108 70-130 04/16/23 20:00 04/21/23 00:57 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)100 04/16/23 20:00 04/21/23 00:57 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.0 18.0 mg/Kg ☼04/13/23 14:59 05/02/23 21:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics
18.0 18.0 mg/Kg 04/13/23 14:59 05/02/23 21:42 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-3Client Sample ID: EB-3 (8-10)
Matrix: SolidDate Collected: 04/06/23 11:45
Percent Solids: 65.9Date Received: 04/07/23 09:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 18.0 18.0 mg/Kg ☼04/13/23 14:59 05/02/23 21:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
9.02 9.02 mg/Kg 04/13/23 14:59 05/02/23 21:42 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)42 40-140 04/13/23 14:59 05/02/23 21:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)69 04/13/23 14:59 05/02/23 21:42 140-140
o- terphenyl (Surr)51 04/13/23 14:59 05/02/23 21:42 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.2 18.2 mg/Kg ☼05/02/23 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-4Client Sample ID: EB-8 (8-10)
Matrix: SolidDate Collected: 04/06/23 16:00
Percent Solids: 67.8Date Received: 04/07/23 09:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.31 2.44 ug/Kg ☼04/17/23 07:00 04/17/23 17:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.31 2.22 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,1,2,2-Tetrachloroethane
7.31 2.93 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
7.31 1.45 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,1,2-Trichloroethane
7.31 2.34 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,1-Dichloroethane
7.31 3.31 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,1-Dichloroethene
7.31 4.72 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,2-Dibromo-3-Chloropropane
7.31 2.46 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,2-Dichlorobenzene
7.31 2.11 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,2-Dichloroethane
7.31 1.95 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,2-Dichloropropane
7.31 3.72 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,2,4-Trichlorobenzene
7.31 4.50 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,3-Dichlorobenzene
7.31 2.19 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,4-Dichlorobenzene
7.31 3.72 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND2-Butanone (MEK)
7.31 2.30 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND2-Hexanone
7.31 2.68 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND4-Methyl-2-pentanone (MIBK)
29.3 5.70 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDAcetone
7.31 2.06 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDBenzene
7.31 3.69 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDBromoform
7.31 3.33 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDBromomethane
7.31 5.85 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDCarbon disulfide
7.31 2.97 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDCarbon tetrachloride
7.31 1.90 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDChlorobenzene
7.31 3.63 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDChlorodibromomethane
7.31 2.35 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDChloroform
7.31 2.90 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDChloromethane
7.31 4.27 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDChloroethane
7.31 2.21 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDcis-1,2-Dichloroethene
7.31 3.23 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDcis-1,3-Dichloropropene
7.31 3.41 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDDichlorobromomethane
7.31 3.64 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND *+Dichlorodifluoromethane
7.31 2.71 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDEthylbenzene
7.31 2.00 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND1,2-Dibromoethane
7.31 3.50 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDCyclohexane
7.31 3.80 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDIsopropylbenzene
36.6 10.8 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND *+Methyl acetate
7.31 2.15 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDMethyl tert-butyl ether
7.31 3.52 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDMethylcyclohexane
7.31 6.60 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼ND *+Methylene Chloride
7.31 2.19 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDStyrene
7.31 2.94 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDTetrachloroethene
7.31 2.11 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDToluene
7.31 2.56 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDtrans-1,2-Dichloroethene
7.31 3.29 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDtrans-1,3-Dichloropropene
7.31 2.30 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDTrichloroethene
7.31 6.07 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDTrichlorofluoromethane
7.31 5.27 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDVinyl chloride
14.6 10.5 ug/Kg 04/17/23 07:00 04/17/23 17:57 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-4Client Sample ID: EB-8 (8-10)
Matrix: SolidDate Collected: 04/06/23 16:00
Percent Solids: 67.8Date Received: 04/07/23 09:30
1,2-Dichloroethane-d4 (Surr)124 73-135 04/17/23 07:00 04/17/23 17:57 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)100 04/17/23 07:00 04/17/23 17:57 160-124
Dibromofluoromethane (Surr)115 04/17/23 07:00 04/17/23 17:57 169-126
Toluene-d8 (Surr)99 04/17/23 07:00 04/17/23 17:57 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 487 180 ug/Kg ☼04/14/23 06:07 04/14/23 19:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
98.9 36.5 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2,2'-oxybis[1-chloropropane]
487 171 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2,4,5-Trichlorophenol
487 164 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2,4,6-Trichlorophenol
98.9 37.9 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2,4-Dichlorophenol
487 165 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2,4-Dimethylphenol
4870 3050 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2,4-Dinitrophenol
487 294 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2,4-Dinitrotoluene
487 192 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2,6-Dinitrotoluene
98.9 22.6 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2-Chloronaphthalene
487 182 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2-Chlorophenol
98.9 23.6 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2-Methylnaphthalene
487 141 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2-Methylphenol
2510 224 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2-Nitroaniline
487 182 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND2-Nitrophenol
487 459 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND3,3'-Dichlorobenzidine
2510 125 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND3-Nitroaniline
2510 849 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND4,6-Dinitro-2-methylphenol
487 210 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND4-Bromophenyl phenyl ether
487 173 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND4-Chloro-3-methylphenol
487 129 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND4-Chloroaniline
487 164 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND4-Chlorophenyl phenyl ether
487 144 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDMethylphenol, 3 & 4
2510 183 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND4-Nitroaniline
2510 345 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼ND4-Nitrophenol
98.9 28.3 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDAcenaphthene
98.9 21.5 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDAcenaphthylene
989 176 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDAcetophenone
98.9 25.5 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDAnthracene
989 215 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDAtrazine
989 61.1 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDBenzaldehyde
98.9 44.4 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDBenzo[a]anthracene
98.9 42.7 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDBenzo[a]pyrene
98.9 24.2 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDBenzo[b]fluoranthene
98.9 21.3 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDBenzo[g,h,i]perylene
98.9 29.5 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDBenzo[k]fluoranthene
487 180 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDBis(2-chloroethoxy)methane
98.9 17.9 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDBis(2-chloroethyl)ether
4870 524 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDBis(2-ethylhexyl) phthalate
487 338 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDButyl benzyl phthalate
2510 320 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDCaprolactam
98.9 23.0 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDCarbazole
98.9 54.6 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDChrysene
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-4Client Sample ID: EB-8 (8-10)
Matrix: SolidDate Collected: 04/06/23 16:00
Percent Solids: 67.8Date Received: 04/07/23 09:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 98.9 63.0 ug/Kg ☼04/14/23 06:07 04/14/23 19:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
487 182 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDDibenzofuran
487 173 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDDiethyl phthalate
487 195 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDDimethyl phthalate
487 215 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDDi-n-butyl phthalate
487 286 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDDi-n-octyl phthalate
98.9 26.0 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDFluoranthene
98.9 19.3 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDFluorene
98.9 35.3 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDHexachlorobenzene
98.9 28.8 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDHexachlorobutadiene
487 50.3 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDHexachlorocyclopentadiene
487 174 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDHexachloroethane
98.9 49.0 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDIndeno[1,2,3-cd]pyrene
487 184 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDIsophorone
98.9 19.2 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDNaphthalene
989 180 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDNitrobenzene
98.9 33.4 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDN-Nitrosodi-n-propylamine
487 164 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDN-Nitrosodiphenylamine
2510 791 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDPentachlorophenol
98.9 26.4 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDPhenanthrene
487 149 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDPhenol
98.9 23.3 ug/Kg 04/14/23 06:07 04/14/23 19:23 1☼NDPyrene
2,4,6-Tribromophenol (Surr)45 34-108 04/14/23 06:07 04/14/23 19:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 48 04/14/23 06:07 04/14/23 19:23 144-105
2-Fluorophenol (Surr)51 04/14/23 06:07 04/14/23 19:23 148-105
Nitrobenzene-d5 (Surr)51 04/14/23 06:07 04/14/23 19:23 146-105
Phenol-d5 (Surr)52 04/14/23 06:07 04/14/23 19:23 146-105
Terphenyl-d14 (Surr)54 04/14/23 06:07 04/14/23 19:23 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.38 1.84 mg/Kg ☼04/24/23 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 23.4 5.84 mg/Kg ☼04/16/23 20:00 04/21/23 01:38 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
23.4 5.84 mg/Kg 04/16/23 20:00 04/21/23 01:38 50☼NDC9-C10 Aromatics
23.4 5.84 mg/Kg 04/16/23 20:00 04/21/23 01:38 50☼NDC9-C12 Aliphatics (unadjusted)
23.4 5.84 mg/Kg 04/16/23 20:00 04/21/23 01:38 50☼NDC9-C12 Aliphatics (adjusted)
23.4 5.84 mg/Kg 04/16/23 20:00 04/21/23 01:38 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)108 70-130 04/16/23 20:00 04/21/23 01:38 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)100 04/16/23 20:00 04/21/23 01:38 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.1 17.1 mg/Kg ☼04/13/23 14:59 05/02/23 22:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics
17.1 17.1 mg/Kg 04/13/23 14:59 05/02/23 22:04 1☼NDC11-C22 Aromatics (Adjusted)
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-4Client Sample ID: EB-8 (8-10)
Matrix: SolidDate Collected: 04/06/23 16:00
Percent Solids: 67.8Date Received: 04/07/23 09:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 17.1 17.1 mg/Kg ☼04/13/23 14:59 05/02/23 22:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.56 8.56 mg/Kg 04/13/23 14:59 05/02/23 22:04 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)38 S1-40-140 04/13/23 14:59 05/02/23 22:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)66 04/13/23 14:59 05/02/23 22:04 140-140
o- terphenyl (Surr)50 04/13/23 14:59 05/02/23 22:04 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.7 17.7 mg/Kg ☼05/02/23 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-5Client Sample ID: EB-9 (8-10)
Matrix: SolidDate Collected: 04/06/23 14:40
Percent Solids: 67.6Date Received: 04/07/23 09:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.23 2.42 ug/Kg ☼04/17/23 07:00 04/17/23 18:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.23 2.20 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,1,2,2-Tetrachloroethane
7.23 2.89 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
7.23 1.43 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,1,2-Trichloroethane
7.23 2.31 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,1-Dichloroethane
7.23 3.27 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,1-Dichloroethene
7.23 4.67 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,2-Dibromo-3-Chloropropane
7.23 2.43 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,2-Dichlorobenzene
7.23 2.08 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,2-Dichloroethane
7.23 1.92 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,2-Dichloropropane
7.23 3.67 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,2,4-Trichlorobenzene
7.23 4.45 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,3-Dichlorobenzene
7.23 2.17 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,4-Dichlorobenzene
7.23 3.67 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND2-Butanone (MEK)
7.23 2.27 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND2-Hexanone
7.23 2.65 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND4-Methyl-2-pentanone (MIBK)
28.9 5.64 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDAcetone
7.23 2.04 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDBenzene
7.23 3.64 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDBromoform
7.23 3.30 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDBromomethane
7.23 5.79 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDCarbon disulfide
7.23 2.94 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDCarbon tetrachloride
7.23 1.88 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDChlorobenzene
7.23 3.59 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDChlorodibromomethane
7.23 2.33 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDChloroform
7.23 2.86 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDChloromethane
7.23 4.22 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDChloroethane
7.23 2.18 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDcis-1,2-Dichloroethene
7.23 3.20 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDcis-1,3-Dichloropropene
7.23 3.37 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDDichlorobromomethane
7.23 3.60 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND *+Dichlorodifluoromethane
7.23 2.68 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDEthylbenzene
7.23 1.98 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND1,2-Dibromoethane
7.23 3.46 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDCyclohexane
7.23 3.76 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDIsopropylbenzene
36.2 10.6 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND *+Methyl acetate
7.23 2.13 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDMethyl tert-butyl ether
7.23 3.49 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDMethylcyclohexane
7.23 6.52 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼ND *+Methylene Chloride
7.23 2.17 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDStyrene
7.23 2.91 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDTetrachloroethene
7.23 2.08 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDToluene
7.23 2.53 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDtrans-1,2-Dichloroethene
7.23 3.25 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDtrans-1,3-Dichloropropene
7.23 2.27 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDTrichloroethene
7.23 6.00 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDTrichlorofluoromethane
7.23 5.21 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDVinyl chloride
14.5 10.4 ug/Kg 04/17/23 07:00 04/17/23 18:20 1☼NDXylenes, Total
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-5Client Sample ID: EB-9 (8-10)
Matrix: SolidDate Collected: 04/06/23 14:40
Percent Solids: 67.6Date Received: 04/07/23 09:30
1,2-Dichloroethane-d4 (Surr)91 73-135 04/17/23 07:00 04/17/23 18:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)89 04/17/23 07:00 04/17/23 18:20 160-124
Dibromofluoromethane (Surr)97 04/17/23 07:00 04/17/23 18:20 169-126
Toluene-d8 (Surr)101 04/17/23 07:00 04/17/23 18:20 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 485 179 ug/Kg ☼04/14/23 06:07 04/14/23 23:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
98.5 36.3 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2,2'-oxybis[1-chloropropane]
485 171 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2,4,5-Trichlorophenol
485 163 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2,4,6-Trichlorophenol
98.5 37.8 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2,4-Dichlorophenol
485 165 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2,4-Dimethylphenol
4850 3040 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2,4-Dinitrophenol
485 293 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2,4-Dinitrotoluene
485 191 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2,6-Dinitrotoluene
98.5 22.5 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2-Chloronaphthalene
485 181 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2-Chlorophenol
98.5 23.5 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2-Methylnaphthalene
485 141 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2-Methylphenol
2500 223 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2-Nitroaniline
485 181 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND2-Nitrophenol
485 457 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND3,3'-Dichlorobenzidine
2500 125 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND3-Nitroaniline
2500 845 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND4,6-Dinitro-2-methylphenol
485 209 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND4-Bromophenyl phenyl ether
485 172 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND4-Chloro-3-methylphenol
485 129 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND4-Chloroaniline
485 163 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND4-Chlorophenyl phenyl ether
485 144 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDMethylphenol, 3 & 4
2500 182 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND4-Nitroaniline
2500 344 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼ND4-Nitrophenol
98.5 28.2 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDAcenaphthene
98.5 21.5 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDAcenaphthylene
985 175 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDAcetophenone
98.5 25.4 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDAnthracene
985 215 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDAtrazine
985 60.9 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDBenzaldehyde
98.5 44.3 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDBenzo[a]anthracene
98.5 42.5 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDBenzo[a]pyrene
98.5 24.1 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDBenzo[b]fluoranthene
98.5 21.2 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDBenzo[g,h,i]perylene
98.5 29.4 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDBenzo[k]fluoranthene
485 179 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDBis(2-chloroethoxy)methane
98.5 17.8 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDBis(2-chloroethyl)ether
4850 522 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDBis(2-ethylhexyl) phthalate
485 337 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDButyl benzyl phthalate
2500 319 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDCaprolactam
98.5 22.9 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDCarbazole
98.5 54.4 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDChrysene
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-5Client Sample ID: EB-9 (8-10)
Matrix: SolidDate Collected: 04/06/23 14:40
Percent Solids: 67.6Date Received: 04/07/23 09:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 98.5 62.8 ug/Kg ☼04/14/23 06:07 04/14/23 23:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
485 181 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDDibenzofuran
485 172 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDDiethyl phthalate
485 194 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDDimethyl phthalate
485 215 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDDi-n-butyl phthalate
485 285 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDDi-n-octyl phthalate
98.5 25.9 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDFluoranthene
98.5 19.3 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDFluorene
98.5 35.1 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDHexachlorobenzene
98.5 28.7 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDHexachlorobutadiene
485 50.1 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDHexachlorocyclopentadiene
485 173 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDHexachloroethane
98.5 48.8 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDIndeno[1,2,3-cd]pyrene
485 184 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDIsophorone
98.5 19.1 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDNaphthalene
985 179 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDNitrobenzene
98.5 33.2 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDN-Nitrosodi-n-propylamine
485 163 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDN-Nitrosodiphenylamine
2500 788 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDPentachlorophenol
98.5 26.3 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDPhenanthrene
485 148 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDPhenol
98.5 23.2 ug/Kg 04/14/23 06:07 04/14/23 23:58 1☼NDPyrene
2,4,6-Tribromophenol (Surr)38 34-108 04/14/23 06:07 04/14/23 23:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 52 04/14/23 06:07 04/14/23 23:58 144-105
2-Fluorophenol (Surr)53 04/14/23 06:07 04/14/23 23:58 148-105
Nitrobenzene-d5 (Surr)59 04/14/23 06:07 04/14/23 23:58 146-105
Phenol-d5 (Surr)55 04/14/23 06:07 04/14/23 23:58 146-105
Terphenyl-d14 (Surr)62 04/14/23 06:07 04/14/23 23:58 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.40 1.85 mg/Kg ☼04/24/23 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 23.5 5.88 mg/Kg ☼04/16/23 20:00 04/21/23 02:19 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
23.5 5.88 mg/Kg 04/16/23 20:00 04/21/23 02:19 50☼NDC9-C10 Aromatics
23.5 5.88 mg/Kg 04/16/23 20:00 04/21/23 02:19 50☼NDC9-C12 Aliphatics (unadjusted)
23.5 5.88 mg/Kg 04/16/23 20:00 04/21/23 02:19 50☼NDC9-C12 Aliphatics (adjusted)
23.5 5.88 mg/Kg 04/16/23 20:00 04/21/23 02:19 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)117 70-130 04/16/23 20:00 04/21/23 02:19 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)109 04/16/23 20:00 04/21/23 02:19 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.5 17.5 mg/Kg ☼04/13/23 14:59 05/02/23 22:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics
17.5 17.5 mg/Kg 04/13/23 14:59 05/02/23 22:27 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154769-5Client Sample ID: EB-9 (8-10)
Matrix: SolidDate Collected: 04/06/23 14:40
Percent Solids: 67.6Date Received: 04/07/23 09:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 17.5 17.5 mg/Kg ☼04/13/23 14:59 05/02/23 22:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.73 8.73 mg/Kg 04/13/23 14:59 05/02/23 22:27 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)50 40-140 04/13/23 14:59 05/02/23 22:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)78 04/13/23 14:59 05/02/23 22:27 140-140
o- terphenyl (Surr)60 04/13/23 14:59 05/02/23 22:27 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.8 17.8 mg/Kg ☼05/02/23 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 180-432477/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477
RL MDL
1,1,1-Trichloroethane ND 5.00 1.67 ug/Kg 04/17/23 11:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.525.00 ug/Kg 04/17/23 11:13 11,1,2,2-Tetrachloroethane
ND 2.005.00 ug/Kg 04/17/23 11:13 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.9905.00 ug/Kg 04/17/23 11:13 11,1,2-Trichloroethane
ND 1.605.00 ug/Kg 04/17/23 11:13 11,1-Dichloroethane
ND 2.265.00 ug/Kg 04/17/23 11:13 11,1-Dichloroethene
ND 3.235.00 ug/Kg 04/17/23 11:13 11,2-Dibromo-3-Chloropropane
ND 1.685.00 ug/Kg 04/17/23 11:13 11,2-Dichlorobenzene
ND 1.445.00 ug/Kg 04/17/23 11:13 11,2-Dichloroethane
ND 1.335.00 ug/Kg 04/17/23 11:13 11,2-Dichloropropane
ND 2.545.00 ug/Kg 04/17/23 11:13 11,2,4-Trichlorobenzene
ND 3.085.00 ug/Kg 04/17/23 11:13 11,3-Dichlorobenzene
ND 1.505.00 ug/Kg 04/17/23 11:13 11,4-Dichlorobenzene
ND 2.545.00 ug/Kg 04/17/23 11:13 12-Butanone (MEK)
ND 1.575.00 ug/Kg 04/17/23 11:13 12-Hexanone
ND 1.835.00 ug/Kg 04/17/23 11:13 14-Methyl-2-pentanone (MIBK)
ND 3.9020.0 ug/Kg 04/17/23 11:13 1Acetone
ND 1.415.00 ug/Kg 04/17/23 11:13 1Benzene
ND 2.525.00 ug/Kg 04/17/23 11:13 1Bromoform
ND 2.285.00 ug/Kg 04/17/23 11:13 1Bromomethane
ND 4.005.00 ug/Kg 04/17/23 11:13 1Carbon disulfide
ND 2.035.00 ug/Kg 04/17/23 11:13 1Carbon tetrachloride
ND 1.305.00 ug/Kg 04/17/23 11:13 1Chlorobenzene
ND 2.485.00 ug/Kg 04/17/23 11:13 1Chlorodibromomethane
ND 1.615.00 ug/Kg 04/17/23 11:13 1Chloroform
ND 1.985.00 ug/Kg 04/17/23 11:13 1Chloromethane
ND 2.925.00 ug/Kg 04/17/23 11:13 1Chloroethane
ND 1.515.00 ug/Kg 04/17/23 11:13 1cis-1,2-Dichloroethene
ND 2.215.00 ug/Kg 04/17/23 11:13 1cis-1,3-Dichloropropene
ND 2.335.00 ug/Kg 04/17/23 11:13 1Dichlorobromomethane
ND 2.495.00 ug/Kg 04/17/23 11:13 1Dichlorodifluoromethane
ND 1.855.00 ug/Kg 04/17/23 11:13 1Ethylbenzene
ND 1.375.00 ug/Kg 04/17/23 11:13 11,2-Dibromoethane
ND 2.395.00 ug/Kg 04/17/23 11:13 1Cyclohexane
ND 2.605.00 ug/Kg 04/17/23 11:13 1Isopropylbenzene
ND 7.3625.0 ug/Kg 04/17/23 11:13 1Methyl acetate
ND 1.475.00 ug/Kg 04/17/23 11:13 1Methyl tert-butyl ether
ND 2.415.00 ug/Kg 04/17/23 11:13 1Methylcyclohexane
ND 4.515.00 ug/Kg 04/17/23 11:13 1Methylene Chloride
ND 1.505.00 ug/Kg 04/17/23 11:13 1Styrene
ND 2.015.00 ug/Kg 04/17/23 11:13 1Tetrachloroethene
ND 1.445.00 ug/Kg 04/17/23 11:13 1Toluene
ND 1.755.00 ug/Kg 04/17/23 11:13 1trans-1,2-Dichloroethene
ND 2.255.00 ug/Kg 04/17/23 11:13 1trans-1,3-Dichloropropene
ND 1.575.00 ug/Kg 04/17/23 11:13 1Trichloroethene
ND 4.155.00 ug/Kg 04/17/23 11:13 1Trichlorofluoromethane
ND 3.605.00 ug/Kg 04/17/23 11:13 1Vinyl chloride
ND 7.2110.0 ug/Kg 04/17/23 11:13 1Xylenes, Total
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-432477/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477
1,2-Dichloroethane-d4 (Surr)128 73-135 04/17/23 11:13 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
102 04/17/23 11:13 14-Bromofluorobenzene (Surr)60-124
116 04/17/23 11:13 1Dibromofluoromethane (Surr)69-126
97 04/17/23 11:13 1Toluene-d8 (Surr)67-134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432477/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477
1,1,1-Trichloroethane 40.0 44.71 ug/Kg 112 72-134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2,2-Tetrachloroethane 40.0 37.30 ug/Kg 93 36-170
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 48.29 ug/Kg 121 59-135
1,1,2-Trichloroethane 40.0 34.53 ug/Kg 86 66-128
1,1-Dichloroethane 40.0 40.09 ug/Kg 100 73-124
1,1-Dichloroethene 40.0 48.77 ug/Kg 122 55-136
1,2-Dibromo-3-Chloropropane 40.0 36.13 ug/Kg 90 30-163
1,2-Dichlorobenzene 40.0 35.44 ug/Kg 89 76-120
1,2-Dichloroethane 40.0 48.08 ug/Kg 120 64-140
1,2-Dichloropropane 40.0 34.68 ug/Kg 87 77-119
1,2,4-Trichlorobenzene 40.0 38.39 ug/Kg 96 22-170
1,3-Dichlorobenzene 40.0 36.27 ug/Kg 91 77-121
1,4-Dichlorobenzene 40.0 36.79 ug/Kg 92 79-120
2-Butanone (MEK)40.0 38.94 ug/Kg 97 39-157
2-Hexanone 40.0 37.69 ug/Kg 94 42-152
4-Methyl-2-pentanone (MIBK)40.0 35.15 ug/Kg 88 51-147
Acetone 40.0 51.10 ug/Kg 128 23-170
Benzene 40.0 39.08 ug/Kg 98 77-120
Bromoform 40.0 39.94 ug/Kg 100 37-147
Bromomethane 40.0 44.87 ug/Kg 112 47-149
Carbon disulfide 40.0 52.30 ug/Kg 131 40-156
Carbon tetrachloride 40.0 45.40 ug/Kg 114 73-130
Chlorobenzene 40.0 36.18 ug/Kg 90 79-122
Chlorodibromomethane 40.0 39.93 ug/Kg 100 60-134
Chloroform 40.0 41.55 ug/Kg 104 73-126
Chloromethane 40.0 36.83 ug/Kg 92 46-151
Chloroethane 40.0 42.11 ug/Kg 105 37-159
cis-1,2-Dichloroethene 40.0 41.19 ug/Kg 103 77-118
cis-1,3-Dichloropropene 40.0 40.06 ug/Kg 100 73-127
Dichlorobromomethane 40.0 40.08 ug/Kg 100 75-123
Dichlorodifluoromethane 40.0 66.08 *+ug/Kg 165 26-149
Ethylbenzene 40.0 35.71 ug/Kg 89 79-119
1,2-Dibromoethane 40.0 36.30 ug/Kg 91 59-137
Cyclohexane 40.0 39.20 ug/Kg 98 63-143
Isopropylbenzene 40.0 36.76 ug/Kg 92 70-125
Methyl acetate 80.0 136.5 *+ug/Kg 171 20-170
Methyl tert-butyl ether 40.0 41.29 ug/Kg 103 58-132
Methylcyclohexane 40.0 38.36 ug/Kg 96 70-125
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432477/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477
Methylene Chloride 40.0 51.39 ug/Kg 128 67-131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
m-Xylene & p-Xylene 40.0 37.66 ug/Kg 94 77-120
o-Xylene 40.0 35.87 ug/Kg 90 78-118
Styrene 40.0 36.14 ug/Kg 90 80-120
Tetrachloroethene 40.0 40.65 ug/Kg 102 71-121
Toluene 40.0 35.93 ug/Kg 90 76-120
trans-1,2-Dichloroethene 40.0 43.68 ug/Kg 109 75-122
trans-1,3-Dichloropropene 40.0 36.53 ug/Kg 91 68-133
Trichloroethene 40.0 42.52 ug/Kg 106 69-118
Trichlorofluoromethane 40.0 42.06 ug/Kg 105 32-149
Vinyl chloride 40.0 35.70 ug/Kg 89 64-134
Xylenes, Total 80.0 73.53 ug/Kg 92 78-118
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
107
LCS LCS
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)60 -124
104Dibromofluoromethane (Surr)69 -126
98Toluene-d8 (Surr)67 -134
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-432477/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477
1,1,1-Trichloroethane 40.0 48.17 ug/Kg 120 72-134 7 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 40.0 35.00 ug/Kg 87 36-170 6 23
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 49.54 ug/Kg 124 59-135 3 28
1,1,2-Trichloroethane 40.0 34.26 ug/Kg 86 66-128 1 21
1,1-Dichloroethane 40.0 43.00 ug/Kg 107 73-124 7 20
1,1-Dichloroethene 40.0 51.61 ug/Kg 129 55-136 6 21
1,2-Dibromo-3-Chloropropane 40.0 35.86 ug/Kg 90 30-163 1 34
1,2-Dichlorobenzene 40.0 35.93 ug/Kg 90 76-120 1 20
1,2-Dichloroethane 40.0 45.85 ug/Kg 115 64-140 5 20
1,2-Dichloropropane 40.0 36.16 ug/Kg 90 77-119 4 20
1,2,4-Trichlorobenzene 40.0 39.14 ug/Kg 98 22-170 2 29
1,3-Dichlorobenzene 40.0 38.44 ug/Kg 96 77-121 6 20
1,4-Dichlorobenzene 40.0 38.77 ug/Kg 97 79-120 5 20
2-Butanone (MEK)40.0 36.04 ug/Kg 90 39-157 8 33
2-Hexanone 40.0 36.74 ug/Kg 92 42-152 3 30
4-Methyl-2-pentanone (MIBK)40.0 32.73 ug/Kg 82 51-147 7 27
Acetone 40.0 49.17 ug/Kg 123 23-170 4 35
Benzene 40.0 41.64 ug/Kg 104 77-120 6 20
Bromoform 40.0 39.04 ug/Kg 98 37-147 2 23
Bromomethane 40.0 38.49 ug/Kg 96 47-149 15 25
Carbon disulfide 40.0 57.25 ug/Kg 143 40-156 9 25
Carbon tetrachloride 40.0 50.63 ug/Kg 127 73-130 11 21
Chlorobenzene 40.0 38.79 ug/Kg 97 79-122 7 20
Chlorodibromomethane 40.0 39.25 ug/Kg 98 60-134 2 40
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-432477/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477
Chloroform 40.0 43.29 ug/Kg 108 73-126 4 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloromethane 40.0 41.99 ug/Kg 105 46-151 13 33
Chloroethane 40.0 46.57 ug/Kg 116 37-159 10 25
cis-1,2-Dichloroethene 40.0 43.16 ug/Kg 108 77-118 5 20
cis-1,3-Dichloropropene 40.0 40.14 ug/Kg 100 73-127 0 20
Dichlorobromomethane 40.0 39.08 ug/Kg 98 75-123 3 20
Dichlorodifluoromethane 40.0 72.24 *+ug/Kg 181 26-149 9 24
Ethylbenzene 40.0 40.22 ug/Kg 101 79-119 12 20
1,2-Dibromoethane 40.0 35.40 ug/Kg 89 59-137 2 20
Cyclohexane 40.0 44.25 ug/Kg 111 63-143 12 25
Isopropylbenzene 40.0 40.57 ug/Kg 101 70-125 10 21
Methyl acetate 80.0 130.6 ug/Kg 163 20-170 4 33
Methyl tert-butyl ether 40.0 38.82 ug/Kg 97 58-132 6 24
Methylcyclohexane 40.0 44.27 ug/Kg 111 70-125 14 22
Methylene Chloride 40.0 61.62 *+ug/Kg 154 67-131 18 32
m-Xylene & p-Xylene 40.0 42.75 ug/Kg 107 77-120 13 20
o-Xylene 40.0 38.83 ug/Kg 97 78-118 8 20
Styrene 40.0 39.36 ug/Kg 98 80-120 9 20
Tetrachloroethene 40.0 44.63 ug/Kg 112 71-121 9 21
Toluene 40.0 39.09 ug/Kg 98 76-120 8 20
trans-1,2-Dichloroethene 40.0 46.89 ug/Kg 117 75-122 7 20
trans-1,3-Dichloropropene 40.0 36.85 ug/Kg 92 68-133 1 20
Trichloroethene 40.0 44.11 ug/Kg 110 69-118 4 20
Trichlorofluoromethane 40.0 45.89 ug/Kg 115 32-149 9 39
Vinyl chloride 40.0 40.19 ug/Kg 100 64-134 12 23
Xylenes, Total 80.0 81.58 ug/Kg 102 78-118 10 20
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
107
LCSD LCSD
Qualifier Limits%Recovery
1064-Bromofluorobenzene (Surr)60 -124
112Dibromofluoromethane (Surr)69 -126
110Toluene-d8 (Surr)67 -134
Client Sample ID: Matrix SpikeLab Sample ID: 180-154813-C-20-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477 Prep Batch: 432544
1,1,1-Trichloroethane ND 46.5 48.40 ug/Kg 104 72-134☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,1,2,2-Tetrachloroethane ND 46.5 40.14 ug/Kg 86 36-170☼
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 46.5 54.84 ug/Kg 118 59-135☼
1,1,2-Trichloroethane ND 46.5 37.05 ug/Kg 80 66-128☼
1,1-Dichloroethane ND 46.5 42.87 ug/Kg 92 73-124☼
1,1-Dichloroethene ND 46.5 54.07 ug/Kg 116 55-136☼
1,2-Dibromo-3-Chloropropane ND 46.5 41.31 ug/Kg 89 30-163☼
1,2-Dichlorobenzene ND 46.5 38.02 ug/Kg 82 76-120☼
1,2-Dichloroethane ND 46.5 49.82 ug/Kg 107 64-140☼
1,2-Dichloropropane ND 46.5 37.14 ug/Kg 80 77-119☼
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-154813-C-20-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477 Prep Batch: 432544
1,2,4-Trichlorobenzene ND 46.5 40.76 ug/Kg 88 22-170☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,3-Dichlorobenzene ND 46.5 39.18 ug/Kg 84 77-121☼
1,4-Dichlorobenzene ND 46.5 39.42 ug/Kg 85 79-120☼
2-Butanone (MEK)ND 46.5 40.64 ug/Kg 87 39-157☼
2-Hexanone ND 46.5 39.02 ug/Kg 84 42-152☼
4-Methyl-2-pentanone (MIBK)ND 46.5 36.29 ug/Kg 78 51-147☼
Acetone ND 46.5 54.44 ug/Kg 117 23-170☼
Benzene ND 46.5 41.98 ug/Kg 90 77-120☼
Bromoform ND 46.5 44.12 ug/Kg 95 37-147☼
Bromomethane ND 46.5 43.25 ug/Kg 93 47-149☼
Carbon disulfide ND 46.5 56.39 ug/Kg 121 40-156☼
Carbon tetrachloride ND 46.5 49.12 ug/Kg 106 73-130☼
Chlorobenzene ND 46.5 39.19 ug/Kg 84 79-122☼
Chlorodibromomethane ND 46.5 41.25 ug/Kg 89 60-134☼
Chloroform ND 46.5 43.28 ug/Kg 93 73-126☼
Chloromethane ND 46.5 35.07 ug/Kg 75 46-151☼
Chloroethane ND 46.5 46.09 ug/Kg 99 37-159☼
cis-1,2-Dichloroethene ND 46.5 43.66 ug/Kg 94 77-118☼
cis-1,3-Dichloropropene ND 46.5 42.60 ug/Kg 92 73-127☼
Dichlorobromomethane ND 46.5 42.92 ug/Kg 92 75-123☼
Dichlorodifluoromethane ND *+46.5 66.05 ug/Kg 142 26-149☼
Ethylbenzene ND 46.5 38.96 ug/Kg 84 79-119☼
1,2-Dibromoethane ND 46.5 36.56 ug/Kg 79 59-137☼
Cyclohexane ND 46.5 42.57 ug/Kg 92 63-143☼
Isopropylbenzene ND 46.5 39.48 ug/Kg 85 70-125☼
Methyl acetate ND *+93.0 145.6 ug/Kg 157 20-170☼
Methyl tert-butyl ether ND 46.5 42.88 ug/Kg 92 58-132☼
Methylcyclohexane ND 46.5 42.95 ug/Kg 92 70-125☼
Methylene Chloride ND *+46.5 49.09 ug/Kg 106 67-131☼
m-Xylene & p-Xylene ND 46.5 40.83 ug/Kg 88 77-120☼
o-Xylene ND 46.5 38.83 ug/Kg 83 78-118☼
Styrene ND 46.5 38.98 ug/Kg 84 80-120☼
Tetrachloroethene ND 46.5 43.68 ug/Kg 94 71-121☼
Toluene ND 46.5 38.30 ug/Kg 82 76-120☼
trans-1,2-Dichloroethene ND 46.5 46.64 ug/Kg 100 75-122☼
trans-1,3-Dichloropropene ND 46.5 38.62 ug/Kg 83 68-133☼
Trichloroethene ND 46.5 43.78 ug/Kg 94 69-118☼
Trichlorofluoromethane ND 46.5 43.95 ug/Kg 94 32-149☼
Vinyl chloride ND 46.5 35.12 ug/Kg 75 64-134☼
Xylenes, Total ND 93.0 79.66 ug/Kg 86 78-118☼
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
103
MS MS
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr)60 -124
104Dibromofluoromethane (Surr)69 -126
95Toluene-d8 (Surr)67 -134
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-154813-C-20-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477 Prep Batch: 432544
1,1,1-Trichloroethane ND 46.9 48.61 ug/Kg 104 72-134 0 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane ND 46.9 42.23 ug/Kg 90 36-170 5 23☼
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 46.9 51.24 ug/Kg 109 59-135 7 28☼
1,1,2-Trichloroethane ND 46.9 39.31 ug/Kg 84 66-128 6 21☼
1,1-Dichloroethane ND 46.9 44.04 ug/Kg 94 73-124 3 20☼
1,1-Dichloroethene ND 46.9 52.98 ug/Kg 113 55-136 2 21☼
1,2-Dibromo-3-Chloropropane ND 46.9 43.21 ug/Kg 92 30-163 5 34☼
1,2-Dichlorobenzene ND 46.9 39.17 ug/Kg 84 76-120 3 20☼
1,2-Dichloroethane ND 46.9 51.63 ug/Kg 110 64-140 4 20☼
1,2-Dichloropropane ND 46.9 39.06 ug/Kg 83 77-119 5 20☼
1,2,4-Trichlorobenzene ND 46.9 42.46 ug/Kg 91 22-170 4 29☼
1,3-Dichlorobenzene ND 46.9 40.70 ug/Kg 87 77-121 4 20☼
1,4-Dichlorobenzene ND 46.9 40.52 ug/Kg 86 79-120 3 20☼
2-Butanone (MEK)ND 46.9 43.92 ug/Kg 94 39-157 8 33☼
2-Hexanone ND 46.9 42.38 ug/Kg 90 42-152 8 30☼
4-Methyl-2-pentanone (MIBK)ND 46.9 39.30 ug/Kg 84 51-147 8 27☼
Acetone ND 46.9 53.31 ug/Kg 114 23-170 2 35☼
Benzene ND 46.9 43.74 ug/Kg 93 77-120 4 20☼
Bromoform ND 46.9 44.46 ug/Kg 95 37-147 1 23☼
Bromomethane ND 46.9 44.25 ug/Kg 94 47-149 2 25☼
Carbon disulfide ND 46.9 56.27 ug/Kg 120 40-156 0 25☼
Carbon tetrachloride ND 46.9 48.74 ug/Kg 104 73-130 1 21☼
Chlorobenzene ND 46.9 40.75 ug/Kg 87 79-122 4 20☼
Chlorodibromomethane ND 46.9 43.42 ug/Kg 93 60-134 5 40☼
Chloroform ND 46.9 45.13 ug/Kg 96 73-126 4 20☼
Chloromethane ND 46.9 37.08 ug/Kg 79 46-151 6 33☼
Chloroethane ND 46.9 42.83 ug/Kg 91 37-159 7 25☼
cis-1,2-Dichloroethene ND 46.9 45.12 ug/Kg 96 77-118 3 20☼
cis-1,3-Dichloropropene ND 46.9 44.52 ug/Kg 95 73-127 4 20☼
Dichlorobromomethane ND 46.9 44.35 ug/Kg 95 75-123 3 20☼
Dichlorodifluoromethane ND *+46.9 64.14 ug/Kg 137 26-149 3 24☼
Ethylbenzene ND 46.9 40.26 ug/Kg 86 79-119 3 20☼
1,2-Dibromoethane ND 46.9 41.39 ug/Kg 88 59-137 12 20☼
Cyclohexane ND 46.9 43.81 ug/Kg 93 63-143 3 25☼
Isopropylbenzene ND 46.9 40.75 ug/Kg 87 70-125 3 21☼
Methyl acetate ND *+93.8 154.6 ug/Kg 165 20-170 6 33☼
Methyl tert-butyl ether ND 46.9 46.05 ug/Kg 98 58-132 7 24☼
Methylcyclohexane ND 46.9 44.41 ug/Kg 95 70-125 3 22☼
Methylene Chloride ND *+46.9 49.54 ug/Kg 106 67-131 1 32☼
m-Xylene & p-Xylene ND 46.9 41.85 ug/Kg 89 77-120 2 20☼
o-Xylene ND 46.9 40.70 ug/Kg 87 78-118 5 20☼
Styrene ND 46.9 40.84 ug/Kg 87 80-120 5 20☼
Tetrachloroethene ND 46.9 44.14 ug/Kg 94 71-121 1 21☼
Toluene ND 46.9 40.58 ug/Kg 87 76-120 6 20☼
trans-1,2-Dichloroethene ND 46.9 48.48 ug/Kg 103 75-122 4 20☼
trans-1,3-Dichloropropene ND 46.9 42.10 ug/Kg 90 68-133 9 20☼
Trichloroethene ND 46.9 46.68 ug/Kg 100 69-118 6 20☼
Trichlorofluoromethane ND 46.9 42.00 ug/Kg 90 32-149 5 39☼
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-154813-C-20-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432477 Prep Batch: 432544
Vinyl chloride ND 46.9 39.55 ug/Kg 84 64-134 12 23☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Xylenes, Total ND 93.8 82.55 ug/Kg 88 78-118 4 20☼
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
108
MSD MSD
Qualifier Limits%Recovery
994-Bromofluorobenzene (Surr)60 -124
104Dibromofluoromethane (Surr)69 -126
99Toluene-d8 (Surr)67 -134
Client Sample ID: Method BlankLab Sample ID: MB 180-432752/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752
RL MDL
1,1,1-Trichloroethane ND 5.00 1.67 ug/Kg 04/19/23 12:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.525.00 ug/Kg 04/19/23 12:22 11,1,2,2-Tetrachloroethane
ND 2.005.00 ug/Kg 04/19/23 12:22 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.9905.00 ug/Kg 04/19/23 12:22 11,1,2-Trichloroethane
ND 1.605.00 ug/Kg 04/19/23 12:22 11,1-Dichloroethane
ND 2.265.00 ug/Kg 04/19/23 12:22 11,1-Dichloroethene
ND 3.235.00 ug/Kg 04/19/23 12:22 11,2-Dibromo-3-Chloropropane
ND 1.685.00 ug/Kg 04/19/23 12:22 11,2-Dichlorobenzene
ND 1.445.00 ug/Kg 04/19/23 12:22 11,2-Dichloroethane
ND 1.335.00 ug/Kg 04/19/23 12:22 11,2-Dichloropropane
ND 2.545.00 ug/Kg 04/19/23 12:22 11,2,4-Trichlorobenzene
ND 3.085.00 ug/Kg 04/19/23 12:22 11,3-Dichlorobenzene
ND 1.505.00 ug/Kg 04/19/23 12:22 11,4-Dichlorobenzene
ND 2.545.00 ug/Kg 04/19/23 12:22 12-Butanone (MEK)
ND 1.575.00 ug/Kg 04/19/23 12:22 12-Hexanone
ND 1.835.00 ug/Kg 04/19/23 12:22 14-Methyl-2-pentanone (MIBK)
ND 3.9020.0 ug/Kg 04/19/23 12:22 1Acetone
ND 1.415.00 ug/Kg 04/19/23 12:22 1Benzene
ND 2.525.00 ug/Kg 04/19/23 12:22 1Bromoform
ND 2.285.00 ug/Kg 04/19/23 12:22 1Bromomethane
ND 4.005.00 ug/Kg 04/19/23 12:22 1Carbon disulfide
ND 2.035.00 ug/Kg 04/19/23 12:22 1Carbon tetrachloride
ND 1.305.00 ug/Kg 04/19/23 12:22 1Chlorobenzene
ND 2.485.00 ug/Kg 04/19/23 12:22 1Chlorodibromomethane
ND 1.615.00 ug/Kg 04/19/23 12:22 1Chloroform
ND 1.985.00 ug/Kg 04/19/23 12:22 1Chloromethane
ND 2.925.00 ug/Kg 04/19/23 12:22 1Chloroethane
ND 1.515.00 ug/Kg 04/19/23 12:22 1cis-1,2-Dichloroethene
ND 2.215.00 ug/Kg 04/19/23 12:22 1cis-1,3-Dichloropropene
ND 2.335.00 ug/Kg 04/19/23 12:22 1Dichlorobromomethane
ND 2.495.00 ug/Kg 04/19/23 12:22 1Dichlorodifluoromethane
ND 1.855.00 ug/Kg 04/19/23 12:22 1Ethylbenzene
ND 1.375.00 ug/Kg 04/19/23 12:22 11,2-Dibromoethane
ND 2.395.00 ug/Kg 04/19/23 12:22 1Cyclohexane
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-432752/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752
RL MDL
Isopropylbenzene ND 5.00 2.60 ug/Kg 04/19/23 12:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 7.3625.0 ug/Kg 04/19/23 12:22 1Methyl acetate
ND 1.475.00 ug/Kg 04/19/23 12:22 1Methyl tert-butyl ether
ND 2.415.00 ug/Kg 04/19/23 12:22 1Methylcyclohexane
ND 4.515.00 ug/Kg 04/19/23 12:22 1Methylene Chloride
ND 1.505.00 ug/Kg 04/19/23 12:22 1Styrene
ND 2.015.00 ug/Kg 04/19/23 12:22 1Tetrachloroethene
ND 1.445.00 ug/Kg 04/19/23 12:22 1Toluene
ND 1.755.00 ug/Kg 04/19/23 12:22 1trans-1,2-Dichloroethene
ND 2.255.00 ug/Kg 04/19/23 12:22 1trans-1,3-Dichloropropene
ND 1.575.00 ug/Kg 04/19/23 12:22 1Trichloroethene
ND 4.155.00 ug/Kg 04/19/23 12:22 1Trichlorofluoromethane
ND 3.605.00 ug/Kg 04/19/23 12:22 1Vinyl chloride
ND 7.2110.0 ug/Kg 04/19/23 12:22 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)133 73-135 04/19/23 12:22 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
101 04/19/23 12:22 14-Bromofluorobenzene (Surr)60-124
120 04/19/23 12:22 1Dibromofluoromethane (Surr)69-126
101 04/19/23 12:22 1Toluene-d8 (Surr)67-134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432752/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752
1,1,1-Trichloroethane 40.0 40.85 ug/Kg 102 72-134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2,2-Tetrachloroethane 40.0 33.21 ug/Kg 83 36-170
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 45.27 ug/Kg 113 59-135
1,1,2-Trichloroethane 40.0 31.81 ug/Kg 80 66-128
1,1-Dichloroethane 40.0 35.65 ug/Kg 89 73-124
1,1-Dichloroethene 40.0 43.39 ug/Kg 108 55-136
1,2-Dibromo-3-Chloropropane 40.0 32.06 ug/Kg 80 30-163
1,2-Dichlorobenzene 40.0 32.20 ug/Kg 80 76-120
1,2-Dichloroethane 40.0 41.64 ug/Kg 104 64-140
1,2-Dichloropropane 40.0 30.98 ug/Kg 77 77-119
1,2,4-Trichlorobenzene 40.0 34.21 ug/Kg 86 22-170
1,3-Dichlorobenzene 40.0 33.00 ug/Kg 83 77-121
1,4-Dichlorobenzene 40.0 33.71 ug/Kg 84 79-120
2-Butanone (MEK)40.0 29.49 ug/Kg 74 39-157
2-Hexanone 40.0 31.12 ug/Kg 78 42-152
4-Methyl-2-pentanone (MIBK)40.0 32.55 ug/Kg 81 51-147
Acetone 40.0 42.99 ug/Kg 107 23-170
Benzene 40.0 34.73 ug/Kg 87 77-120
Bromoform 40.0 37.62 ug/Kg 94 37-147
Bromomethane 40.0 38.24 ug/Kg 96 47-149
Carbon disulfide 40.0 45.83 ug/Kg 115 40-156
Carbon tetrachloride 40.0 42.41 ug/Kg 106 73-130
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432752/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752
Chlorobenzene 40.0 33.33 ug/Kg 83 79-122
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chlorodibromomethane 40.0 35.50 ug/Kg 89 60-134
Chloroform 40.0 36.99 ug/Kg 92 73-126
Chloromethane 40.0 29.22 ug/Kg 73 46-151
Chloroethane 40.0 38.55 ug/Kg 96 37-159
cis-1,2-Dichloroethene 40.0 35.72 ug/Kg 89 77-118
cis-1,3-Dichloropropene 40.0 36.08 ug/Kg 90 73-127
Dichlorobromomethane 40.0 35.42 ug/Kg 89 75-123
Dichlorodifluoromethane 40.0 59.23 ug/Kg 148 26-149
Ethylbenzene 40.0 33.12 ug/Kg 83 79-119
1,2-Dibromoethane 40.0 32.60 ug/Kg 82 59-137
Cyclohexane 40.0 36.46 ug/Kg 91 63-143
Isopropylbenzene 40.0 33.79 ug/Kg 84 70-125
Methyl acetate 80.0 133.4 ug/Kg 167 20-170
Methyl tert-butyl ether 40.0 37.23 ug/Kg 93 58-132
Methylcyclohexane 40.0 35.39 ug/Kg 88 70-125
Methylene Chloride 40.0 37.58 ug/Kg 94 67-131
m-Xylene & p-Xylene 40.0 34.94 ug/Kg 87 77-120
o-Xylene 40.0 32.80 ug/Kg 82 78-118
Styrene 40.0 33.49 ug/Kg 84 80-120
Tetrachloroethene 40.0 38.07 ug/Kg 95 71-121
Toluene 40.0 32.84 ug/Kg 82 76-120
trans-1,2-Dichloroethene 40.0 39.08 ug/Kg 98 75-122
trans-1,3-Dichloropropene 40.0 33.81 ug/Kg 85 68-133
Trichloroethene 40.0 37.08 ug/Kg 93 69-118
Trichlorofluoromethane 40.0 37.85 ug/Kg 95 32-149
Vinyl chloride 40.0 31.53 ug/Kg 79 64-134
Xylenes, Total 80.0 67.74 ug/Kg 85 78-118
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
110
LCS LCS
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)60 -124
107Dibromofluoromethane (Surr)69 -126
101Toluene-d8 (Surr)67 -134
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-432752/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752
1,1,1-Trichloroethane 40.0 42.99 ug/Kg 107 72-134 5 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 40.0 32.80 ug/Kg 82 36-170 1 23
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 48.69 ug/Kg 122 59-135 7 28
1,1,2-Trichloroethane 40.0 32.10 ug/Kg 80 66-128 1 21
1,1-Dichloroethane 40.0 38.75 ug/Kg 97 73-124 8 20
1,1-Dichloroethene 40.0 47.69 ug/Kg 119 55-136 9 21
1,2-Dibromo-3-Chloropropane 40.0 31.76 ug/Kg 79 30-163 1 34
1,2-Dichlorobenzene 40.0 33.83 ug/Kg 85 76-120 5 20
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-432752/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752
1,2-Dichloroethane 40.0 44.30 ug/Kg 111 64-140 6 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,2-Dichloropropane 40.0 32.93 ug/Kg 82 77-119 6 20
1,2,4-Trichlorobenzene 40.0 35.97 ug/Kg 90 22-170 5 29
1,3-Dichlorobenzene 40.0 34.77 ug/Kg 87 77-121 5 20
1,4-Dichlorobenzene 40.0 35.15 ug/Kg 88 79-120 4 20
2-Butanone (MEK)40.0 30.36 ug/Kg 76 39-157 3 33
2-Hexanone 40.0 31.92 ug/Kg 80 42-152 3 30
4-Methyl-2-pentanone (MIBK)40.0 31.94 ug/Kg 80 51-147 2 27
Acetone 40.0 45.21 ug/Kg 113 23-170 5 35
Benzene 40.0 37.36 ug/Kg 93 77-120 7 20
Bromoform 40.0 37.99 ug/Kg 95 37-147 1 23
Bromomethane 40.0 42.86 ug/Kg 107 47-149 11 25
Carbon disulfide 40.0 49.37 ug/Kg 123 40-156 7 25
Carbon tetrachloride 40.0 45.83 ug/Kg 115 73-130 8 21
Chlorobenzene 40.0 35.74 ug/Kg 89 79-122 7 20
Chlorodibromomethane 40.0 36.02 ug/Kg 90 60-134 1 40
Chloroform 40.0 39.17 ug/Kg 98 73-126 6 20
Chloromethane 40.0 36.23 ug/Kg 91 46-151 21 33
Chloroethane 40.0 44.04 ug/Kg 110 37-159 13 25
cis-1,2-Dichloroethene 40.0 38.58 ug/Kg 96 77-118 8 20
cis-1,3-Dichloropropene 40.0 37.09 ug/Kg 93 73-127 3 20
Dichlorobromomethane 40.0 37.30 ug/Kg 93 75-123 5 20
Dichlorodifluoromethane 40.0 62.23 *+ug/Kg 156 26-149 5 24
Ethylbenzene 40.0 35.04 ug/Kg 88 79-119 6 20
1,2-Dibromoethane 40.0 34.31 ug/Kg 86 59-137 5 20
Cyclohexane 40.0 39.64 ug/Kg 99 63-143 8 25
Isopropylbenzene 40.0 35.84 ug/Kg 90 70-125 6 21
Methyl acetate 80.0 127.0 ug/Kg 159 20-170 5 33
Methyl tert-butyl ether 40.0 36.14 ug/Kg 90 58-132 3 24
Methylcyclohexane 40.0 38.47 ug/Kg 96 70-125 8 22
Methylene Chloride 40.0 41.08 ug/Kg 103 67-131 9 32
m-Xylene & p-Xylene 40.0 36.97 ug/Kg 92 77-120 6 20
o-Xylene 40.0 35.32 ug/Kg 88 78-118 7 20
Styrene 40.0 35.28 ug/Kg 88 80-120 5 20
Tetrachloroethene 40.0 40.77 ug/Kg 102 71-121 7 21
Toluene 40.0 35.30 ug/Kg 88 76-120 7 20
trans-1,2-Dichloroethene 40.0 41.20 ug/Kg 103 75-122 5 20
trans-1,3-Dichloropropene 40.0 35.28 ug/Kg 88 68-133 4 20
Trichloroethene 40.0 40.28 ug/Kg 101 69-118 8 20
Trichlorofluoromethane 40.0 40.65 ug/Kg 102 32-149 7 39
Vinyl chloride 40.0 33.76 ug/Kg 84 64-134 7 23
Xylenes, Total 80.0 72.29 ug/Kg 90 78-118 6 20
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)60 -124
101Dibromofluoromethane (Surr)69 -126
99Toluene-d8 (Surr)67 -134
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-154808-C-18-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752 Prep Batch: 432800
1,1,1-Trichloroethane ND 39.3 44.39 ug/Kg 113 72-134☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,1,2,2-Tetrachloroethane ND 39.3 39.82 ug/Kg 101 36-170☼
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 39.3 52.90 ug/Kg 135 59-135☼
1,1,2-Trichloroethane ND 39.3 36.68 ug/Kg 93 66-128☼
1,1-Dichloroethane ND 39.3 38.82 ug/Kg 99 73-124☼
1,1-Dichloroethene ND 39.3 47.85 ug/Kg 122 55-136☼
1,2-Dibromo-3-Chloropropane ND 39.3 39.22 ug/Kg 100 30-163☼
1,2-Dichlorobenzene ND 39.3 33.72 ug/Kg 86 76-120☼
1,2-Dichloroethane ND 39.3 48.47 ug/Kg 123 64-140☼
1,2-Dichloropropane ND 39.3 33.97 ug/Kg 87 77-119☼
1,2,4-Trichlorobenzene ND 39.3 37.06 ug/Kg 94 22-170☼
1,3-Dichlorobenzene ND 39.3 33.67 ug/Kg 86 77-121☼
1,4-Dichlorobenzene ND 39.3 34.43 ug/Kg 88 79-120☼
2-Butanone (MEK)ND 39.3 66.76 F1 ug/Kg 170 39-157☼
2-Hexanone ND 39.3 40.40 ug/Kg 103 42-152☼
4-Methyl-2-pentanone (MIBK)ND 39.3 37.48 ug/Kg 95 51-147☼
Acetone ND 39.3 56.83 ug/Kg 145 23-170☼
Benzene ND 39.3 37.77 ug/Kg 96 77-120☼
Bromoform ND 39.3 42.14 ug/Kg 107 37-147☼
Bromomethane ND 39.3 40.47 ug/Kg 103 47-149☼
Carbon disulfide ND 39.3 50.46 ug/Kg 128 40-156☼
Carbon tetrachloride ND 39.3 46.28 ug/Kg 118 73-130☼
Chlorobenzene ND 39.3 36.16 ug/Kg 92 79-122☼
Chlorodibromomethane ND 39.3 40.70 ug/Kg 104 60-134☼
Chloroform ND 39.3 39.28 ug/Kg 100 73-126☼
Chloromethane ND 39.3 33.74 ug/Kg 86 46-151☼
Chloroethane ND 39.3 41.66 ug/Kg 106 37-159☼
cis-1,2-Dichloroethene ND 39.3 39.33 ug/Kg 100 77-118☼
cis-1,3-Dichloropropene ND 39.3 39.24 ug/Kg 100 73-127☼
Dichlorobromomethane ND 39.3 40.75 ug/Kg 104 75-123☼
Dichlorodifluoromethane ND *+39.3 63.64 F1 ug/Kg 162 26-149☼
Ethylbenzene ND 39.3 35.57 ug/Kg 91 79-119☼
1,2-Dibromoethane ND 39.3 38.10 ug/Kg 97 59-137☼
Cyclohexane ND 39.3 39.55 ug/Kg 101 63-143☼
Isopropylbenzene ND 39.3 36.38 ug/Kg 93 70-125☼
Methyl acetate ND 78.5 124.4 ug/Kg 158 20-170☼
Methyl tert-butyl ether ND 39.3 43.56 ug/Kg 111 58-132☼
Methylcyclohexane ND 39.3 39.69 ug/Kg 101 70-125☼
Methylene Chloride ND 39.3 43.63 ug/Kg 111 67-131☼
m-Xylene & p-Xylene ND 39.3 37.95 ug/Kg 97 77-120☼
o-Xylene ND 39.3 35.80 ug/Kg 91 78-118☼
Styrene ND 39.3 36.16 ug/Kg 92 80-120☼
Tetrachloroethene ND 39.3 39.39 ug/Kg 100 71-121☼
Toluene ND 39.3 35.58 ug/Kg 91 76-120☼
trans-1,2-Dichloroethene ND 39.3 42.80 ug/Kg 109 75-122☼
trans-1,3-Dichloropropene ND 39.3 38.39 ug/Kg 98 68-133☼
Trichloroethene ND 39.3 40.34 ug/Kg 103 69-118☼
Trichlorofluoromethane ND 39.3 41.36 ug/Kg 105 32-149☼
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-154808-C-18-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752 Prep Batch: 432800
Vinyl chloride ND 39.3 33.16 ug/Kg 84 64-134☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Xylenes, Total ND 78.5 73.75 ug/Kg 94 78-118☼
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
113
MS MS
Qualifier Limits%Recovery
1024-Bromofluorobenzene (Surr)60 -124
109Dibromofluoromethane (Surr)69 -126
101Toluene-d8 (Surr)67 -134
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-154808-C-18-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752 Prep Batch: 432800
1,1,1-Trichloroethane ND 42.9 43.57 ug/Kg 102 72-134 2 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane ND 42.9 38.85 ug/Kg 91 36-170 2 23☼
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 42.9 48.58 ug/Kg 113 59-135 9 28☼
1,1,2-Trichloroethane ND 42.9 36.30 ug/Kg 85 66-128 1 21☼
1,1-Dichloroethane ND 42.9 38.25 ug/Kg 89 73-124 1 20☼
1,1-Dichloroethene ND 42.9 46.63 ug/Kg 109 55-136 3 21☼
1,2-Dibromo-3-Chloropropane ND 42.9 35.62 ug/Kg 83 30-163 10 34☼
1,2-Dichlorobenzene ND 42.9 34.54 ug/Kg 81 76-120 2 20☼
1,2-Dichloroethane ND 42.9 48.43 ug/Kg 113 64-140 0 20☼
1,2-Dichloropropane ND 42.9 34.93 ug/Kg 81 77-119 3 20☼
1,2,4-Trichlorobenzene ND 42.9 38.04 ug/Kg 89 22-170 3 29☼
1,3-Dichlorobenzene ND 42.9 35.96 ug/Kg 84 77-121 7 20☼
1,4-Dichlorobenzene ND 42.9 36.11 ug/Kg 84 79-120 5 20☼
2-Butanone (MEK)ND 42.9 40.33 F2 ug/Kg 94 39-157 49 33☼
2-Hexanone ND 42.9 37.18 ug/Kg 87 42-152 8 30☼
4-Methyl-2-pentanone (MIBK)ND 42.9 37.62 ug/Kg 88 51-147 0 27☼
Acetone ND 42.9 50.39 ug/Kg 117 23-170 12 35☼
Benzene ND 42.9 38.00 ug/Kg 89 77-120 1 20☼
Bromoform ND 42.9 41.09 ug/Kg 96 37-147 3 23☼
Bromomethane ND 42.9 43.33 ug/Kg 101 47-149 7 25☼
Carbon disulfide ND 42.9 49.54 ug/Kg 116 40-156 2 25☼
Carbon tetrachloride ND 42.9 45.46 ug/Kg 106 73-130 2 21☼
Chlorobenzene ND 42.9 36.37 ug/Kg 85 79-122 1 20☼
Chlorodibromomethane ND 42.9 40.51 ug/Kg 94 60-134 0 40☼
Chloroform ND 42.9 40.44 ug/Kg 94 73-126 3 20☼
Chloromethane ND 42.9 35.50 ug/Kg 83 46-151 5 33☼
Chloroethane ND 42.9 40.38 ug/Kg 94 37-159 3 25☼
cis-1,2-Dichloroethene ND 42.9 39.22 ug/Kg 91 77-118 0 20☼
cis-1,3-Dichloropropene ND 42.9 40.29 ug/Kg 94 73-127 3 20☼
Dichlorobromomethane ND 42.9 40.52 ug/Kg 94 75-123 1 20☼
Dichlorodifluoromethane ND *+42.9 60.63 ug/Kg 141 26-149 5 24☼
Ethylbenzene ND 42.9 34.78 ug/Kg 81 79-119 2 20☼
1,2-Dibromoethane ND 42.9 37.60 ug/Kg 88 59-137 1 20☼
Cyclohexane ND 42.9 39.83 ug/Kg 93 63-143 1 25☼
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-154808-C-18-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432752 Prep Batch: 432800
Isopropylbenzene ND 42.9 36.23 ug/Kg 84 70-125 0 21☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Methyl acetate ND 85.8 133.4 ug/Kg 156 20-170 7 33☼
Methyl tert-butyl ether ND 42.9 42.90 ug/Kg 100 58-132 2 24☼
Methylcyclohexane ND 42.9 39.14 ug/Kg 91 70-125 1 22☼
Methylene Chloride ND 42.9 44.03 ug/Kg 103 67-131 1 32☼
m-Xylene & p-Xylene ND 42.9 37.54 ug/Kg 88 77-120 1 20☼
o-Xylene ND 42.9 35.35 ug/Kg 82 78-118 1 20☼
Styrene ND 42.9 36.39 ug/Kg 85 80-120 1 20☼
Tetrachloroethene ND 42.9 39.50 ug/Kg 92 71-121 0 21☼
Toluene ND 42.9 35.85 ug/Kg 84 76-120 1 20☼
trans-1,2-Dichloroethene ND 42.9 43.23 ug/Kg 101 75-122 1 20☼
trans-1,3-Dichloropropene ND 42.9 38.06 ug/Kg 89 68-133 1 20☼
Trichloroethene ND 42.9 40.60 ug/Kg 95 69-118 1 20☼
Trichlorofluoromethane ND 42.9 40.26 ug/Kg 94 32-149 3 39☼
Vinyl chloride ND 42.9 34.21 ug/Kg 80 64-134 3 23☼
Xylenes, Total ND 85.8 72.89 ug/Kg 85 78-118 1 20☼
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
111
MSD MSD
Qualifier Limits%Recovery
974-Bromofluorobenzene (Surr)60 -124
105Dibromofluoromethane (Surr)69 -126
97Toluene-d8 (Surr)67 -134
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-432293/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
RL MDL
1,1'-Biphenyl ND 330 122 ug/Kg 04/14/23 06:07 04/14/23 13:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 24.767.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,2'-oxybis[1-chloropropane]
ND 116330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4,5-Trichlorophenol
ND 111330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4,6-Trichlorophenol
ND 25.767.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4-Dichlorophenol
ND 112330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4-Dimethylphenol
ND 20703300 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4-Dinitrophenol
ND 199330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4-Dinitrotoluene
ND 130330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,6-Dinitrotoluene
ND 15.367.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Chloronaphthalene
ND 123330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Chlorophenol
ND 16.067.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Methylnaphthalene
ND 95.6330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Methylphenol
ND 1521700 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Nitroaniline
ND 123330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Nitrophenol
ND 311330 ug/Kg 04/14/23 06:07 04/14/23 13:13 13,3'-Dichlorobenzidine
ND 84.81700 ug/Kg 04/14/23 06:07 04/14/23 13:13 13-Nitroaniline
ND 5751700 ug/Kg 04/14/23 06:07 04/14/23 13:13 14,6-Dinitro-2-methylphenol
ND 142330 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Bromophenyl phenyl ether
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-432293/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
RL MDL
4-Chloro-3-methylphenol ND 330 117 ug/Kg 04/14/23 06:07 04/14/23 13:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 87.5330 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Chloroaniline
ND 111330 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Chlorophenyl phenyl ether
ND 97.9330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Methylphenol, 3 & 4
ND 1241700 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Nitroaniline
ND 2341700 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Nitrophenol
ND 19.267.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Acenaphthene
ND 14.667.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Acenaphthylene
ND 119670 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Acetophenone
ND 17.367.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Anthracene
ND 146670 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Atrazine
ND 41.4670 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzaldehyde
ND 30.167.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[a]anthracene
ND 28.967.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[a]pyrene
ND 16.467.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[b]fluoranthene
ND 14.467.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[g,h,i]perylene
ND 20.067.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[k]fluoranthene
ND 122330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Bis(2-chloroethoxy)methane
ND 12.167.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Bis(2-chloroethyl)ether
ND 3553300 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Bis(2-ethylhexyl) phthalate
ND 229330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Butyl benzyl phthalate
ND 2171700 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Caprolactam
ND 15.667.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Carbazole
ND 37.067.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Chrysene
ND 42.767.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Dibenz(a,h)anthracene
ND 123330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Dibenzofuran
ND 117330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Diethyl phthalate
ND 132330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Dimethyl phthalate
ND 146330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Di-n-butyl phthalate
ND 194330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Di-n-octyl phthalate
ND 17.667.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Fluoranthene
ND 13.167.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Fluorene
ND 23.967.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Hexachlorobenzene
ND 19.567.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Hexachlorobutadiene
ND 34.1330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Hexachlorocyclopentadiene
ND 118330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Hexachloroethane
ND 33.267.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Indeno[1,2,3-cd]pyrene
ND 125330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Isophorone
ND 13.067.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Naphthalene
ND 122670 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Nitrobenzene
ND 22.667.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1N-Nitrosodi-n-propylamine
ND 111330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1N-Nitrosodiphenylamine
ND 5361700 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Pentachlorophenol
ND 17.967.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Phenanthrene
ND 101330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Phenol
ND 15.867.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Pyrene
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-432293/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
2,4,6-Tribromophenol (Surr)91 34-108 04/14/23 13:13 1
MB MB
Surrogate
04/14/23 06:07
Dil FacPreparedAnalyzedQualifierLimits%Recovery
92 04/14/23 06:07 04/14/23 13:13 12-Fluorobiphenyl 44-105
92 04/14/23 06:07 04/14/23 13:13 12-Fluorophenol (Surr)48-105
90 04/14/23 06:07 04/14/23 13:13 1Nitrobenzene-d5 (Surr)46-105
90 04/14/23 06:07 04/14/23 13:13 1Phenol-d5 (Surr)46-105
104 04/14/23 06:07 04/14/23 13:13 1Terphenyl-d14 (Surr)39-105
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432293/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
1,1'-Biphenyl 6670 5434 ug/Kg 82 50-100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,2'-oxybis[1-chloropropane]6670 5341 ug/Kg 80 30-113
2,4,5-Trichlorophenol 6670 5774 ug/Kg 87 50-104
2,4,6-Trichlorophenol 6670 5834 ug/Kg 88 50-105
2,4-Dichlorophenol 6670 5725 ug/Kg 86 53-101
2,4-Dimethylphenol 6670 5410 ug/Kg 81 51-101
2,4-Dinitrophenol 13300 10090 ug/Kg 76 33-101
2,4-Dinitrotoluene 6670 5875 ug/Kg 88 54-104
2,6-Dinitrotoluene 6670 5754 ug/Kg 86 51-106
2-Chloronaphthalene 6670 5279 ug/Kg 79 51-100
2-Chlorophenol 6670 5482 ug/Kg 82 51-100
2-Methylnaphthalene 6670 5427 ug/Kg 81 53-100
2-Methylphenol 6670 5418 ug/Kg 81 50-101
2-Nitroaniline 6670 5903 ug/Kg 89 42-123
2-Nitrophenol 6670 5964 ug/Kg 89 55-107
3,3'-Dichlorobenzidine 6670 4779 ug/Kg 72 43-100
3-Nitroaniline 6670 5989 ug/Kg 90 50-103
4,6-Dinitro-2-methylphenol 13300 9967 ug/Kg 75 51-100
4-Bromophenyl phenyl ether 6670 5413 ug/Kg 81 52-101
4-Chloro-3-methylphenol 6670 5681 ug/Kg 85 49-106
4-Chloroaniline 6670 5318 ug/Kg 80 47-100
4-Chlorophenyl phenyl ether 6670 5579 ug/Kg 84 52-100
Methylphenol, 3 & 4 6670 5699 ug/Kg 85 50-103
4-Nitroaniline 6670 5722 ug/Kg 86 52-103
4-Nitrophenol 13300 12180 ug/Kg 91 30-134
Acenaphthene 6670 5431 ug/Kg 81 50-100
Acenaphthylene 6670 5546 ug/Kg 83 52-100
Acetophenone 6670 5250 ug/Kg 79 48-100
Anthracene 6670 5633 ug/Kg 84 53-100
Atrazine 6670 5182 ug/Kg 78 49-103
Benzaldehyde 6670 3686 ug/Kg 55 23-105
Benzo[a]anthracene 6670 5225 ug/Kg 78 51-100
Benzo[a]pyrene 6670 5504 ug/Kg 83 51-100
Benzo[b]fluoranthene 6670 5286 ug/Kg 79 48-100
Benzo[g,h,i]perylene 6670 5785 ug/Kg 87 48-105
Benzo[k]fluoranthene 6670 5700 ug/Kg 86 19-100
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432293/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
Bis(2-chloroethoxy)methane 6670 5424 ug/Kg 81 49-100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Bis(2-chloroethyl)ether 6670 5375 ug/Kg 81 48-100
Bis(2-ethylhexyl) phthalate 6670 5745 ug/Kg 86 53-107
Butyl benzyl phthalate 6670 5685 ug/Kg 85 52-107
Carbazole 6670 5537 ug/Kg 83 53-100
Chrysene 6670 5071 ug/Kg 76 50-100
Dibenz(a,h)anthracene 6670 6099 ug/Kg 91 50-107
Dibenzofuran 6670 5485 ug/Kg 82 52-100
Diethyl phthalate 6670 5598 ug/Kg 84 48-104
Dimethyl phthalate 6670 5572 ug/Kg 84 53-100
Di-n-butyl phthalate 6670 5807 ug/Kg 87 57-102
Di-n-octyl phthalate 6670 5855 ug/Kg 88 41-106
Fluoranthene 6670 5649 ug/Kg 85 55-100
Fluorene 6670 5641 ug/Kg 85 52-100
Hexachlorobenzene 6670 5440 ug/Kg 82 49-100
Hexachlorobutadiene 6670 5432 ug/Kg 81 38-107
Hexachlorocyclopentadiene 6670 5272 ug/Kg 79 33-117
Hexachloroethane 6670 5412 ug/Kg 81 47-100
Indeno[1,2,3-cd]pyrene 6670 6098 ug/Kg 91 51-103
Isophorone 6670 5517 ug/Kg 83 48-105
Naphthalene 6670 5417 ug/Kg 81 51-100
Nitrobenzene 6670 5523 ug/Kg 83 44-108
N-Nitrosodi-n-propylamine 6670 5582 ug/Kg 84 45-107
N-Nitrosodiphenylamine 6670 5535 ug/Kg 83 52-100
Pentachlorophenol 13300 12500 ug/Kg 94 42-110
Phenanthrene 6670 5406 ug/Kg 81 53-100
Phenol 6670 5491 ug/Kg 82 49-100
Pyrene 6670 5181 ug/Kg 78 52-100
2,4,6-Tribromophenol (Surr)34 -108
Surrogate
80
LCS LCS
Qualifier Limits%Recovery
752-Fluorobiphenyl 44 -105
782-Fluorophenol (Surr)48 -105
75Nitrobenzene-d5 (Surr)46 -105
76Phenol-d5 (Surr)46 -105
71Terphenyl-d14 (Surr)39 -105
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-366573/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 366575 Prep Batch: 366573
RL MDL
C5-C8 Aliphatics (unadjusted)ND 5.00 1.25 mg/Kg 04/20/23 11:29 04/20/23 12:38 50
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.255.00 mg/Kg 04/20/23 11:29 04/20/23 12:38 50C9-C10 Aromatics
ND 1.255.00 mg/Kg 04/20/23 11:29 04/20/23 12:38 50C9-C12 Aliphatics (unadjusted)
ND 1.255.00 mg/Kg 04/20/23 11:29 04/20/23 12:38 50C9-C12 Aliphatics (adjusted)
ND 1.255.00 mg/Kg 04/20/23 11:29 04/20/23 12:38 50C5-C8 Aliphatics (adjusted)
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
a,a,a-Trifluorotoluene (fid)99 70-130 04/20/23 12:38 50
MB MB
Surrogate
04/20/23 11:29
Dil FacPreparedAnalyzedQualifierLimits%Recovery
91 04/20/23 11:29 04/20/23 12:38 50a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-366573/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 366575 Prep Batch: 366573
C5-C8 Aliphatics (unadjusted)7.53 6.868 mg/Kg 91 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 2.51 2.412 J mg/Kg 96 70-130
C9-C12 Aliphatics (unadjusted)7.53 6.511 mg/Kg 87 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
96a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-366573/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 366575 Prep Batch: 366573
C5-C8 Aliphatics (unadjusted)7.53 6.685 mg/Kg 89 70-130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 2.51 2.346 J mg/Kg 94 70-130 3 30
C9-C12 Aliphatics (unadjusted)7.53 6.531 mg/Kg 87 70-130 0 30
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
99
LCSD LCSD
Qualifier Limits%Recovery
93a,a,a-Trifluorotoluene (pid)70 -130
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-364138/1-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371212 Prep Batch: 364138
RL MDL
C19-C36 Aliphatics ND 12.0 12.0 mg/Kg 04/13/23 14:59 05/02/23 18:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 6.006.00 mg/Kg 04/13/23 14:59 05/02/23 18:41 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)43 40-140 05/02/23 18:41 1
MB MB
Surrogate
04/13/23 14:59
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-364138/1-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371207 Prep Batch: 364138
RL MDL
C11-C22 Aromatics ND 12.0 12.0 mg/Kg 04/13/23 14:59 05/02/23 18:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 12.012.0 mg/Kg 04/13/23 14:59 05/02/23 18:41 1C11-C22 Aromatics (Adjusted)
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154769-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-364138/1-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371207 Prep Batch: 364138
2-Fluorobiphenyl (Surr)75 40-140 05/02/23 18:41 1
MB MB
Surrogate
04/13/23 14:59
Dil FacPreparedAnalyzedQualifierLimits%Recovery
72 04/13/23 14:59 05/02/23 18:41 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-364138/2-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371212 Prep Batch: 364138
C19-C36 Aliphatics 32.1 23.54 mg/Kg 73 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 24.1 18.71 mg/Kg 78 40-140
1-Chlorooctadecane (Surr)40 -140
Surrogate
44
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-364138/2-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371207 Prep Batch: 364138
C11-C22 Aromatics 68.1 47.28 mg/Kg 69 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Fluorobiphenyl (Surr)40 -140
Surrogate
76
LCS LCS
Qualifier Limits%Recovery
70o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-364138/3-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371212 Prep Batch: 364138
C19-C36 Aliphatics 32.1 22.32 mg/Kg 69 40-140 5 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 24.1 17.96 mg/Kg 75 40-140 4 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
51
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-364138/3-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371207 Prep Batch: 364138
C11-C22 Aromatics 68.1 46.86 mg/Kg 69 40-140 1 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)40 -140
Surrogate
77
LCSD LCSD
Qualifier Limits%Recovery
68o- terphenyl (Surr)40 -140
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-154769-1
SDG Number: 640 Rock Lane
Login Number: 154769
Question Answer Comment
Creator: Abernathy, Eric L
List Source: Eurofins Pittsburgh
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-154769-1
SDG Number: 640 Rock Lane
Login Number: 154769
Question Answer Comment
Creator: Cyms, Carolyn M
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 04/10/23 10:46 AMList Number: 2
TrueThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
FalseAppropriate sample containers are used.Did not receive all required containers.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.Not present.
N/AVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
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ANALYTICAL REPORT
PREPARED FOR
Attn: Mr. Bruce Stainbrook
Altec Industries, Inc
Bruce Stainbrook
810 Franklin Court, Ste A
Marietta, Georgia 30067
Generated 5/5/2023 4:29:16 PM
JOB DESCRIPTION
China Grove NC
SDG NUMBER 640 Rock Lane
JOB NUMBER
180-154822-1
See page two for job notes and contact information.
Pittsburgh PA 15238
RIDC Park
301 Alpha Drive
Eurofins Pittsburgh
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Eurofins Pittsburgh
Eurofins Pittsburgh is a laboratory within Eurofins Environment Testing Northeast LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced,
except in full, without the written approval of the laboratory. This report is confidential and is intended for the sole use of
Eurofins Environment Testing Northeast, LLC Pittsburgh and its client. All questions regarding this report should be directed
to the Eurofins Environment Testing Northeast, LLC Pittsburgh Project Manager or designee who has signed this report.
PA Lab ID: 02-00416
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Pittsburgh Project Manager.
Authorization
Generated
5/5/2023 4:29:16 PM
Authorized for release by
Shali Brown, Project Manager II
[e-mail]
[phone]
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Case Narrative
Client: Altec Industries, Inc Job ID: 180-154822-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-154822-1
Laboratory: Eurofins Pittsburgh
Narrative
Job Narrative
180-154822-1
Receipt
The samples were received on 4/8/2023 8:35 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 2.4°C
GC/MS VOA
Method 8260D: MS & MSD was not spike and was out of tune. Minimal QC requirements were reached with LCS.(LCS 180-432587/4)
Method 8260D: The continuing calibration verification (CCV) analyzed in 180-432587 was outside the method criteria for the following
analyte(s): Dichloro-difluoromethane and Methyl acetate (HIGH). As indicated in the reference method, sample analysis may proceed;
however, any detection for the affected analyte(s) is considered estimated.
Method 8260D: The laboratory control sample (LCS) for analytical batch 180-432587 recovered outside control limits for the following
analytes: 1,1,2-Trichloro-1,2,2-trifluoroethane, Carbon disulfide, Dichloro-difluoromethane and Methyl acetate. These analytes were
biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-432587 was outside the method criteria for the
following analyte(s): Bromomethane, Chloroethane, Chloromethane, Trichlorofluoromethane and Vinyl chloride (LOW). A CCV standard at
or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference
method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
Method 8270E: The continuing calibration verification (CCV) associated with batch 180-432297 recovered outside acceptance criteria, low
biased, for Di-n-octyl phthalate. A reporting limit (RL) standard was analyzed, and the target analytes are detected. Since the associated
samples were non-detect for the analyte(s), the data are reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
Method MAVPH: The following sample(s) were received in pre-weighed containers with a label that was added in the field, which would
cause a slight low bias in the final results. EB-4 (8-10) (180-154822-1), EB-5 (8-10) (180-154822-2), EB-6 (8-10) (180-154822-3) and
EB-7 (3-5) (180-154822-4).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method MAEPH2.1: 1-Chlorooctadecane (Surr) recovery was outside acceptance limits for the following matrix spike/matrix spike duplicate
(MS/MSD) sample: (180-154822-B-1-D MSD). The parent sample's surrogate recovery was within limits and the spike recovery of the MSD
is within limits. The MS/MSD sample has been qualified and reported.
Method MAEPH2.1: The breakthrough for naphthalene and 2-methylnaphthalene in the LCS and LCSD is <1%. The method requirement
for breakthrough is <5%. EB-4 (8-10) (180-154822-1), EB-5 (8-10) (180-154822-2), EB-6 (8-10) (180-154822-3), EB-7 (3-5)
(180-154822-4), (180-154822-B-1-C MS) and (180-154822-B-1-D MSD)
Method MAEPH2.1: 1-Chlorooctadecane (Surr) recovery for the following samples were outside acceptance limits: EB-4 (8-10)
(180-154822-1) and EB-6 (8-10) (180-154822-3). The samples cannot be re-extracted and re-analyzed within method holding time. The
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Case Narrative
Client: Altec Industries, Inc Job ID: 180-154822-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-154822-1 (Continued)
Laboratory: Eurofins Pittsburgh (Continued)
results have been reported per client request.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Definitions/Glossary
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
S1-Surrogate recovery exceeds control limits, low biased.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Accreditation/Certification Summary
Client: Altec Industries, Inc Job ID: 180-154822-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Laboratory: Eurofins Pittsburgh
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 434 05-03-23
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 521 12-31-23
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-1Client Sample ID: EB-4 (8-10)
Matrix: SolidDate Collected: 04/07/23 08:45
Percent Solids: 65.9Date Received: 04/08/23 08:35
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.11 2.37 ug/Kg ☼04/18/23 07:04 04/18/23 17:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.11 2.16 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,1,2,2-Tetrachloroethane
7.11 2.84 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND *+1,1,2-Trichloro-1,2,2-trifluoroethane
7.11 1.41 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,1,2-Trichloroethane
7.11 2.27 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,1-Dichloroethane
7.11 3.21 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,1-Dichloroethene
7.11 4.59 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,2-Dibromo-3-Chloropropane
7.11 2.39 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,2-Dichlorobenzene
7.11 2.05 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,2-Dichloroethane
7.11 1.89 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,2-Dichloropropane
7.11 3.61 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,2,4-Trichlorobenzene
7.11 4.38 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,3-Dichlorobenzene
7.11 2.13 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,4-Dichlorobenzene
7.11 3.61 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND2-Butanone (MEK)
7.11 2.23 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND2-Hexanone
7.11 2.60 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND4-Methyl-2-pentanone (MIBK)
28.4 5.54 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDAcetone
7.11 2.00 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDBenzene
7.11 3.58 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDBromoform
7.11 3.24 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDBromomethane
7.11 5.69 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND *+Carbon disulfide
7.11 2.89 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDCarbon tetrachloride
7.11 1.85 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDChlorobenzene
7.11 3.53 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDChlorodibromomethane
7.11 2.29 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDChloroform
7.11 2.81 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDChloromethane
7.11 4.15 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDChloroethane
7.11 2.15 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDcis-1,2-Dichloroethene
7.11 3.14 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDcis-1,3-Dichloropropene
7.11 3.31 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDDichlorobromomethane
7.11 3.54 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND *+Dichlorodifluoromethane
7.11 2.63 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDEthylbenzene
7.11 1.95 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND1,2-Dibromoethane
7.11 3.40 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDCyclohexane
7.11 3.70 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDIsopropylbenzene
35.5 10.5 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼ND *+Methyl acetate
7.11 2.09 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDMethyl tert-butyl ether
7.11 3.43 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDMethylcyclohexane
7.11 6.41 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDMethylene Chloride
7.11 2.13 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDStyrene
7.11 2.86 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDTetrachloroethene
7.11 2.05 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDToluene
7.11 2.49 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDtrans-1,2-Dichloroethene
7.11 3.20 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDtrans-1,3-Dichloropropene
7.11 2.23 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDTrichloroethene
7.11 5.90 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDTrichlorofluoromethane
7.11 5.12 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDVinyl chloride
14.2 10.2 ug/Kg 04/18/23 07:04 04/18/23 17:50 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-1Client Sample ID: EB-4 (8-10)
Matrix: SolidDate Collected: 04/07/23 08:45
Percent Solids: 65.9Date Received: 04/08/23 08:35
1,2-Dichloroethane-d4 (Surr)115 73-135 04/18/23 07:04 04/18/23 17:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 04/18/23 07:04 04/18/23 17:50 160-124
Dibromofluoromethane (Surr)109 04/18/23 07:04 04/18/23 17:50 169-126
Toluene-d8 (Surr)98 04/18/23 07:04 04/18/23 17:50 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 501 185 ug/Kg ☼04/14/23 06:07 04/14/23 16:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
102 37.5 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2,2'-oxybis[1-chloropropane]
501 176 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2,4,5-Trichlorophenol
501 168 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2,4,6-Trichlorophenol
102 39.0 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2,4-Dichlorophenol
501 170 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2,4-Dimethylphenol
5010 3140 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2,4-Dinitrophenol
501 302 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2,4-Dinitrotoluene
501 197 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2,6-Dinitrotoluene
102 23.2 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2-Chloronaphthalene
501 187 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2-Chlorophenol
102 24.3 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2-Methylnaphthalene
501 145 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2-Methylphenol
2580 231 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2-Nitroaniline
501 187 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND2-Nitrophenol
501 472 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND3,3'-Dichlorobenzidine
2580 129 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND3-Nitroaniline
2580 873 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND4,6-Dinitro-2-methylphenol
501 215 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND4-Bromophenyl phenyl ether
501 178 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND4-Chloro-3-methylphenol
501 133 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND4-Chloroaniline
501 168 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND4-Chlorophenyl phenyl ether
501 149 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDMethylphenol, 3 & 4
2580 188 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND4-Nitroaniline
2580 355 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼ND4-Nitrophenol
102 29.1 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDAcenaphthene
102 22.2 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDAcenaphthylene
1020 181 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDAcetophenone
102 26.3 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDAnthracene
1020 222 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDAtrazine
1020 62.8 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDBenzaldehyde
102 45.7 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDBenzo[a]anthracene
102 43.9 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDBenzo[a]pyrene
102 24.9 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDBenzo[b]fluoranthene
102 21.9 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDBenzo[g,h,i]perylene
102 30.4 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDBenzo[k]fluoranthene
501 185 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDBis(2-chloroethoxy)methane
102 18.4 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDBis(2-chloroethyl)ether
5010 539 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDBis(2-ethylhexyl) phthalate
501 348 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDButyl benzyl phthalate
2580 329 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDCaprolactam
102 23.7 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDCarbazole
102 56.1 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDChrysene
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-1Client Sample ID: EB-4 (8-10)
Matrix: SolidDate Collected: 04/07/23 08:45
Percent Solids: 65.9Date Received: 04/08/23 08:35
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 102 64.8 ug/Kg ☼04/14/23 06:07 04/14/23 16:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
501 187 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDDibenzofuran
501 178 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDDiethyl phthalate
501 200 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDDimethyl phthalate
501 222 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDDi-n-butyl phthalate
501 294 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDDi-n-octyl phthalate
102 26.7 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDFluoranthene
102 19.9 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDFluorene
102 36.3 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDHexachlorobenzene
102 29.6 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDHexachlorobutadiene
501 51.7 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDHexachlorocyclopentadiene
501 179 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDHexachloroethane
102 50.4 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDIndeno[1,2,3-cd]pyrene
501 190 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDIsophorone
102 19.7 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDNaphthalene
1020 185 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDNitrobenzene
102 34.3 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDN-Nitrosodi-n-propylamine
501 168 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDN-Nitrosodiphenylamine
2580 813 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDPentachlorophenol
102 27.2 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDPhenanthrene
501 153 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDPhenol
102 24.0 ug/Kg 04/14/23 06:07 04/14/23 16:50 1☼NDPyrene
2,4,6-Tribromophenol (Surr)55 34-108 04/14/23 06:07 04/14/23 16:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 59 04/14/23 06:07 04/14/23 16:50 144-105
2-Fluorophenol (Surr)60 04/14/23 06:07 04/14/23 16:50 148-105
Nitrobenzene-d5 (Surr)59 04/14/23 06:07 04/14/23 16:50 146-105
Phenol-d5 (Surr)61 04/14/23 06:07 04/14/23 16:50 146-105
Terphenyl-d14 (Surr)65 04/14/23 06:07 04/14/23 16:50 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.59 1.90 mg/Kg ☼04/24/23 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 24.5 6.11 mg/Kg ☼04/16/23 20:00 04/21/23 03:00 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
24.5 6.11 mg/Kg 04/16/23 20:00 04/21/23 03:00 50☼NDC9-C10 Aromatics
24.5 6.11 mg/Kg 04/16/23 20:00 04/21/23 03:00 50☼NDC9-C12 Aliphatics (unadjusted)
24.5 6.11 mg/Kg 04/16/23 20:00 04/21/23 03:00 50☼NDC9-C12 Aliphatics (adjusted)
24.5 6.11 mg/Kg 04/16/23 20:00 04/21/23 03:00 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)112 70-130 04/16/23 20:00 04/21/23 03:00 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)106 04/16/23 20:00 04/21/23 03:00 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.5 17.5 mg/Kg ☼04/13/23 14:59 05/02/23 19:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
17.5 17.5 mg/Kg 04/13/23 14:59 05/02/23 19:49 1☼NDC11-C22 Aromatics (Adjusted)
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-1Client Sample ID: EB-4 (8-10)
Matrix: SolidDate Collected: 04/07/23 08:45
Percent Solids: 65.9Date Received: 04/08/23 08:35
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 17.5 17.5 mg/Kg ☼04/13/23 14:59 05/02/23 19:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.77 8.77 mg/Kg 04/13/23 14:59 05/02/23 19:49 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)23 S1-40-140 04/13/23 14:59 05/02/23 19:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)79 04/13/23 14:59 05/02/23 19:49 140-140
o- terphenyl (Surr)59 04/13/23 14:59 05/02/23 19:49 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.2 18.2 mg/Kg ☼05/02/23 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-2Client Sample ID: EB-5 (8-10)
Matrix: SolidDate Collected: 04/07/23 10:05
Percent Solids: 68.0Date Received: 04/08/23 08:35
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.17 2.39 ug/Kg ☼04/18/23 18:30 04/18/23 20:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.17 2.18 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,1,2,2-Tetrachloroethane
7.17 2.87 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND *+1,1,2-Trichloro-1,2,2-trifluoroethane
7.17 1.42 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,1,2-Trichloroethane
7.17 2.29 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,1-Dichloroethane
7.17 3.24 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,1-Dichloroethene
7.17 4.63 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,2-Dibromo-3-Chloropropane
7.17 2.41 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,2-Dichlorobenzene
7.17 2.06 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,2-Dichloroethane
7.17 1.91 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,2-Dichloropropane
7.17 3.64 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,2,4-Trichlorobenzene
7.17 4.42 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,3-Dichlorobenzene
7.17 2.15 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,4-Dichlorobenzene
7.17 3.64 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND2-Butanone (MEK)
7.17 2.25 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND2-Hexanone
7.17 2.62 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND4-Methyl-2-pentanone (MIBK)
28.7 5.59 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDAcetone
7.17 2.02 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDBenzene
7.17 3.61 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDBromoform
7.17 3.27 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDBromomethane
7.17 5.73 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND *+Carbon disulfide
7.17 2.91 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDCarbon tetrachloride
7.17 1.86 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDChlorobenzene
7.17 3.56 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDChlorodibromomethane
7.17 2.31 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDChloroform
7.17 2.84 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDChloromethane
7.17 4.19 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDChloroethane
7.17 2.16 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDcis-1,2-Dichloroethene
7.17 3.17 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDcis-1,3-Dichloropropene
7.17 3.34 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDDichlorobromomethane
7.17 3.57 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND *+Dichlorodifluoromethane
7.17 2.65 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDEthylbenzene
7.17 1.96 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND1,2-Dibromoethane
7.17 3.43 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDCyclohexane
7.17 3.73 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDIsopropylbenzene
35.8 10.6 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼ND *+Methyl acetate
7.17 2.11 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDMethyl tert-butyl ether
7.17 3.45 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDMethylcyclohexane
7.17 6.47 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDMethylene Chloride
7.17 2.15 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDStyrene
7.17 2.88 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDTetrachloroethene
7.17 2.06 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDToluene
7.17 2.51 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDtrans-1,2-Dichloroethene
7.17 3.23 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDtrans-1,3-Dichloropropene
7.17 2.25 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDTrichloroethene
7.17 5.95 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDTrichlorofluoromethane
7.17 5.16 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDVinyl chloride
14.3 10.3 ug/Kg 04/18/23 18:30 04/18/23 20:29 1☼NDXylenes, Total
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-2Client Sample ID: EB-5 (8-10)
Matrix: SolidDate Collected: 04/07/23 10:05
Percent Solids: 68.0Date Received: 04/08/23 08:35
1,2-Dichloroethane-d4 (Surr)105 73-135 04/18/23 18:30 04/18/23 20:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)73 04/18/23 18:30 04/18/23 20:29 160-124
Dibromofluoromethane (Surr)88 04/18/23 18:30 04/18/23 20:29 169-126
Toluene-d8 (Surr)70 04/18/23 18:30 04/18/23 20:29 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 482 178 ug/Kg ☼04/14/23 06:07 04/14/23 17:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
97.9 36.1 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2,2'-oxybis[1-chloropropane]
482 169 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2,4,5-Trichlorophenol
482 162 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2,4,6-Trichlorophenol
97.9 37.6 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2,4-Dichlorophenol
482 164 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2,4-Dimethylphenol
4820 3020 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2,4-Dinitrophenol
482 291 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2,4-Dinitrotoluene
482 190 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2,6-Dinitrotoluene
97.9 22.4 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2-Chloronaphthalene
482 180 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2-Chlorophenol
97.9 23.4 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2-Methylnaphthalene
482 140 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2-Methylphenol
2480 222 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2-Nitroaniline
482 180 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND2-Nitrophenol
482 454 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND3,3'-Dichlorobenzidine
2480 124 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND3-Nitroaniline
2480 840 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND4,6-Dinitro-2-methylphenol
482 207 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND4-Bromophenyl phenyl ether
482 171 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND4-Chloro-3-methylphenol
482 128 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND4-Chloroaniline
482 162 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND4-Chlorophenyl phenyl ether
482 143 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDMethylphenol, 3 & 4
2480 181 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND4-Nitroaniline
2480 342 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼ND4-Nitrophenol
97.9 28.1 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDAcenaphthene
97.9 21.3 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDAcenaphthylene
979 174 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDAcetophenone
97.9 25.3 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDAnthracene
979 213 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDAtrazine
979 60.5 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDBenzaldehyde
97.9 44.0 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDBenzo[a]anthracene
97.9 42.2 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDBenzo[a]pyrene
97.9 24.0 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDBenzo[b]fluoranthene
97.9 21.0 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDBenzo[g,h,i]perylene
97.9 29.2 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDBenzo[k]fluoranthene
482 178 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDBis(2-chloroethoxy)methane
97.9 17.7 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDBis(2-chloroethyl)ether
4820 519 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDBis(2-ethylhexyl) phthalate
482 335 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDButyl benzyl phthalate
2480 317 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDCaprolactam
97.9 22.8 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDCarbazole
97.9 54.1 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDChrysene
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-2Client Sample ID: EB-5 (8-10)
Matrix: SolidDate Collected: 04/07/23 10:05
Percent Solids: 68.0Date Received: 04/08/23 08:35
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 97.9 62.4 ug/Kg ☼04/14/23 06:07 04/14/23 17:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
482 180 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDDibenzofuran
482 171 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDDiethyl phthalate
482 193 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDDimethyl phthalate
482 213 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDDi-n-butyl phthalate
482 283 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDDi-n-octyl phthalate
97.9 25.7 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDFluoranthene
97.9 19.1 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDFluorene
97.9 34.9 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDHexachlorobenzene
97.9 28.5 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDHexachlorobutadiene
482 49.8 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDHexachlorocyclopentadiene
482 172 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDHexachloroethane
97.9 48.5 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDIndeno[1,2,3-cd]pyrene
482 183 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDIsophorone
97.9 19.0 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDNaphthalene
979 178 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDNitrobenzene
97.9 33.0 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDN-Nitrosodi-n-propylamine
482 162 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDN-Nitrosodiphenylamine
2480 783 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDPentachlorophenol
97.9 26.2 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDPhenanthrene
482 148 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDPhenol
97.9 23.1 ug/Kg 04/14/23 06:07 04/14/23 17:12 1☼NDPyrene
2,4,6-Tribromophenol (Surr)58 34-108 04/14/23 06:07 04/14/23 17:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 59 04/14/23 06:07 04/14/23 17:12 144-105
2-Fluorophenol (Surr)61 04/14/23 06:07 04/14/23 17:12 148-105
Nitrobenzene-d5 (Surr)60 04/14/23 06:07 04/14/23 17:12 146-105
Phenol-d5 (Surr)63 04/14/23 06:07 04/14/23 17:12 146-105
Terphenyl-d14 (Surr)66 04/14/23 06:07 04/14/23 17:12 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.35 1.84 mg/Kg ☼04/24/23 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 23.3 5.82 mg/Kg ☼04/16/23 20:00 04/21/23 03:41 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
23.3 5.82 mg/Kg 04/16/23 20:00 04/21/23 03:41 50☼NDC9-C10 Aromatics
23.3 5.82 mg/Kg 04/16/23 20:00 04/21/23 03:41 50☼NDC9-C12 Aliphatics (unadjusted)
23.3 5.82 mg/Kg 04/16/23 20:00 04/21/23 03:41 50☼NDC9-C12 Aliphatics (adjusted)
23.3 5.82 mg/Kg 04/16/23 20:00 04/21/23 03:41 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)114 70-130 04/16/23 20:00 04/21/23 03:41 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)107 04/16/23 20:00 04/21/23 03:41 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.1 17.1 mg/Kg ☼04/13/23 14:59 05/02/23 22:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
17.1 17.1 mg/Kg 04/13/23 14:59 05/02/23 22:49 1☼NDC11-C22 Aromatics (Adjusted)
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-2Client Sample ID: EB-5 (8-10)
Matrix: SolidDate Collected: 04/07/23 10:05
Percent Solids: 68.0Date Received: 04/08/23 08:35
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 17.1 17.1 mg/Kg ☼04/13/23 14:59 05/02/23 22:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.54 8.54 mg/Kg 04/13/23 14:59 05/02/23 22:49 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)42 40-140 04/13/23 14:59 05/02/23 22:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)74 04/13/23 14:59 05/02/23 22:49 140-140
o- terphenyl (Surr)56 04/13/23 14:59 05/02/23 22:49 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.7 17.7 mg/Kg ☼05/02/23 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-3Client Sample ID: EB-6 (8-10)
Matrix: SolidDate Collected: 04/07/23 11:00
Percent Solids: 66.3Date Received: 04/08/23 08:35
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
13.2 7.16 2.39 ug/Kg ☼04/18/23 07:04 04/18/23 18:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.16 2.18 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,1,2,2-Tetrachloroethane
7.16 2.86 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND *+1,1,2-Trichloro-1,2,2-trifluoroethane
7.16 1.42 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,1,2-Trichloroethane
7.16 2.29 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,1-Dichloroethane
7.16 3.24 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,1-Dichloroethene
7.16 4.63 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,2-Dibromo-3-Chloropropane
7.16 2.41 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,2-Dichlorobenzene
7.16 2.06 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,2-Dichloroethane
7.16 1.90 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,2-Dichloropropane
7.16 3.64 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,2,4-Trichlorobenzene
7.16 4.41 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,3-Dichlorobenzene
7.16 2.15 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,4-Dichlorobenzene
7.16 3.64 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND2-Butanone (MEK)
7.16 2.25 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND2-Hexanone
7.16 2.62 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND4-Methyl-2-pentanone (MIBK)
28.6 5.59 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDAcetone
7.16 2.02 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDBenzene
7.16 3.61 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDBromoform
7.16 3.27 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDBromomethane
7.16 5.73 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND *+Carbon disulfide
7.16 2.91 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDCarbon tetrachloride
7.16 1.86 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDChlorobenzene
7.16 3.55 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDChlorodibromomethane
7.16 2.31 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDChloroform
7.16 2.84 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDChloromethane
7.16 4.18 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDChloroethane
7.16 2.16 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDcis-1,2-Dichloroethene
7.16 3.17 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDcis-1,3-Dichloropropene
7.16 3.34 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDDichlorobromomethane
7.16 3.57 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND *+Dichlorodifluoromethane
7.16 2.65 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDEthylbenzene
7.16 1.96 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND1,2-Dibromoethane
7.16 3.42 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDCyclohexane
7.16 3.72 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDIsopropylbenzene
35.8 10.5 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼ND *+Methyl acetate
7.16 2.11 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDMethyl tert-butyl ether
7.16 3.45 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDMethylcyclohexane
7.16 6.46 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDMethylene Chloride
7.16 2.15 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDStyrene
7.16 2.88 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDTetrachloroethene
7.16 2.06 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDToluene
7.16 2.51 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDtrans-1,2-Dichloroethene
7.16 3.22 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDtrans-1,3-Dichloropropene
7.16 2.25 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDTrichloroethene
7.16 5.94 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDTrichlorofluoromethane
7.16 5.16 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDVinyl chloride
14.3 10.3 ug/Kg 04/18/23 07:04 04/18/23 18:35 1☼NDXylenes, Total
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-3Client Sample ID: EB-6 (8-10)
Matrix: SolidDate Collected: 04/07/23 11:00
Percent Solids: 66.3Date Received: 04/08/23 08:35
1,2-Dichloroethane-d4 (Surr)108 73-135 04/18/23 07:04 04/18/23 18:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)89 04/18/23 07:04 04/18/23 18:35 160-124
Dibromofluoromethane (Surr)106 04/18/23 07:04 04/18/23 18:35 169-126
Toluene-d8 (Surr)94 04/18/23 07:04 04/18/23 18:35 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 494 183 ug/Kg ☼04/14/23 06:07 04/14/23 17:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
100 37.0 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2,2'-oxybis[1-chloropropane]
494 174 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2,4,5-Trichlorophenol
494 166 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2,4,6-Trichlorophenol
100 38.5 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2,4-Dichlorophenol
494 168 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2,4-Dimethylphenol
4940 3100 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2,4-Dinitrophenol
494 298 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2,4-Dinitrotoluene
494 195 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2,6-Dinitrotoluene
100 22.9 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2-Chloronaphthalene
494 184 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2-Chlorophenol
100 24.0 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2-Methylnaphthalene
494 143 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2-Methylphenol
2550 228 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2-Nitroaniline
494 184 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND2-Nitrophenol
494 466 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND3,3'-Dichlorobenzidine
2550 127 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND3-Nitroaniline
2550 862 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND4,6-Dinitro-2-methylphenol
494 213 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND4-Bromophenyl phenyl ether
494 175 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND4-Chloro-3-methylphenol
494 131 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND4-Chloroaniline
494 166 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND4-Chlorophenyl phenyl ether
494 147 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDMethylphenol, 3 & 4
2550 186 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND4-Nitroaniline
2550 351 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼ND4-Nitrophenol
100 28.8 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDAcenaphthene
100 21.9 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDAcenaphthylene
1000 178 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDAcetophenone
100 25.9 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDAnthracene
1000 219 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDAtrazine
1000 62.0 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDBenzaldehyde
100 45.1 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDBenzo[a]anthracene
100 43.3 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDBenzo[a]pyrene
100 24.6 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDBenzo[b]fluoranthene
100 21.6 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDBenzo[g,h,i]perylene
100 30.0 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDBenzo[k]fluoranthene
494 183 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDBis(2-chloroethoxy)methane
100 18.1 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDBis(2-chloroethyl)ether
4940 532 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDBis(2-ethylhexyl) phthalate
494 343 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDButyl benzyl phthalate
2550 325 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDCaprolactam
100 23.4 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDCarbazole
100 55.4 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDChrysene
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-3Client Sample ID: EB-6 (8-10)
Matrix: SolidDate Collected: 04/07/23 11:00
Percent Solids: 66.3Date Received: 04/08/23 08:35
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 100 64.0 ug/Kg ☼04/14/23 06:07 04/14/23 17:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
494 184 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDDibenzofuran
494 175 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDDiethyl phthalate
494 198 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDDimethyl phthalate
494 219 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDDi-n-butyl phthalate
494 291 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDDi-n-octyl phthalate
100 26.4 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDFluoranthene
100 19.6 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDFluorene
100 35.8 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDHexachlorobenzene
100 29.2 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDHexachlorobutadiene
494 51.1 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDHexachlorocyclopentadiene
494 177 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDHexachloroethane
100 49.7 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDIndeno[1,2,3-cd]pyrene
494 187 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDIsophorone
100 19.5 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDNaphthalene
1000 183 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDNitrobenzene
100 33.9 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDN-Nitrosodi-n-propylamine
494 166 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDN-Nitrosodiphenylamine
2550 803 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDPentachlorophenol
100 26.8 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDPhenanthrene
494 151 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDPhenol
100 23.7 ug/Kg 04/14/23 06:07 04/14/23 17:34 1☼NDPyrene
2,4,6-Tribromophenol (Surr)50 34-108 04/14/23 06:07 04/14/23 17:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 52 04/14/23 06:07 04/14/23 17:34 144-105
2-Fluorophenol (Surr)54 04/14/23 06:07 04/14/23 17:34 148-105
Nitrobenzene-d5 (Surr)52 04/14/23 06:07 04/14/23 17:34 146-105
Phenol-d5 (Surr)54 04/14/23 06:07 04/14/23 17:34 146-105
Terphenyl-d14 (Surr)58 04/14/23 06:07 04/14/23 17:34 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.54 1.89 mg/Kg ☼04/24/23 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 23.2 5.79 mg/Kg ☼04/16/23 20:00 04/21/23 04:22 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
23.2 5.79 mg/Kg 04/16/23 20:00 04/21/23 04:22 50☼NDC9-C10 Aromatics
23.2 5.79 mg/Kg 04/16/23 20:00 04/21/23 04:22 50☼NDC9-C12 Aliphatics (unadjusted)
23.2 5.79 mg/Kg 04/16/23 20:00 04/21/23 04:22 50☼NDC9-C12 Aliphatics (adjusted)
23.2 5.79 mg/Kg 04/16/23 20:00 04/21/23 04:22 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)112 70-130 04/16/23 20:00 04/21/23 04:22 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)105 04/16/23 20:00 04/21/23 04:22 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.0 18.0 mg/Kg ☼04/13/23 14:59 05/02/23 23:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
18.0 18.0 mg/Kg 04/13/23 14:59 05/02/23 23:12 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-3Client Sample ID: EB-6 (8-10)
Matrix: SolidDate Collected: 04/07/23 11:00
Percent Solids: 66.3Date Received: 04/08/23 08:35
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 18.0 18.0 mg/Kg ☼04/13/23 14:59 05/02/23 23:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.98 8.98 mg/Kg 04/13/23 14:59 05/02/23 23:12 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)33 S1-40-140 04/13/23 14:59 05/02/23 23:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)78 04/13/23 14:59 05/02/23 23:12 140-140
o- terphenyl (Surr)57 04/13/23 14:59 05/02/23 23:12 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.1 18.1 mg/Kg ☼05/02/23 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-4Client Sample ID: EB-7 (3-5)
Matrix: SolidDate Collected: 04/07/23 12:10
Percent Solids: 73.1Date Received: 04/08/23 08:35
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
3.14 J 6.41 2.14 ug/Kg ☼04/18/23 07:04 04/18/23 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
6.41 1.95 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,1,2,2-Tetrachloroethane
6.41 2.56 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND *+1,1,2-Trichloro-1,2,2-trifluoroethane
6.41 1.27 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,1,2-Trichloroethane
6.41 2.05 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,1-Dichloroethane
6.41 2.90 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,1-Dichloroethene
6.41 4.14 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,2-Dibromo-3-Chloropropane
6.41 2.15 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,2-Dichlorobenzene
6.41 1.84 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,2-Dichloroethane
6.41 1.70 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,2-Dichloropropane
6.41 3.25 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,2,4-Trichlorobenzene
6.41 3.95 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,3-Dichlorobenzene
6.41 1.92 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,4-Dichlorobenzene
6.41 3.25 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND2-Butanone (MEK)
6.41 2.01 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND2-Hexanone
6.41 2.34 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND4-Methyl-2-pentanone (MIBK)
25.6 5.00 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDAcetone
6.41 1.81 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDBenzene
6.41 3.23 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDBromoform
6.41 2.92 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDBromomethane
6.41 5.12 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND *+Carbon disulfide
6.41 2.60 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDCarbon tetrachloride
6.41 1.67 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDChlorobenzene
6.41 3.18 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDChlorodibromomethane
6.41 2.06 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDChloroform
6.41 2.54 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDChloromethane
6.41 3.74 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDChloroethane
6.41 1.93 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDcis-1,2-Dichloroethene
6.41 2.83 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDcis-1,3-Dichloropropene
6.41 2.99 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDDichlorobromomethane
6.41 3.19 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND *+Dichlorodifluoromethane
6.41 2.37 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDEthylbenzene
6.41 1.76 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND1,2-Dibromoethane
6.41 3.06 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDCyclohexane
6.41 3.33 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDIsopropylbenzene
32.0 9.43 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼ND *+Methyl acetate
6.41 1.88 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDMethyl tert-butyl ether
6.41 3.09 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDMethylcyclohexane
6.41 5.78 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDMethylene Chloride
6.41 1.92 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDStyrene
6.41 2.58 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDTetrachloroethene
6.41 1.84 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼2.17 JToluene
6.41 2.24 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDtrans-1,2-Dichloroethene
6.41 2.88 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDtrans-1,3-Dichloropropene
6.41 2.01 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDTrichloroethene
6.41 5.32 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDTrichlorofluoromethane
6.41 4.61 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDVinyl chloride
12.8 9.24 ug/Kg 04/18/23 07:04 04/18/23 18:58 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-4Client Sample ID: EB-7 (3-5)
Matrix: SolidDate Collected: 04/07/23 12:10
Percent Solids: 73.1Date Received: 04/08/23 08:35
1,2-Dichloroethane-d4 (Surr)116 73-135 04/18/23 07:04 04/18/23 18:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)102 04/18/23 07:04 04/18/23 18:58 160-124
Dibromofluoromethane (Surr)111 04/18/23 07:04 04/18/23 18:58 169-126
Toluene-d8 (Surr)96 04/18/23 07:04 04/18/23 18:58 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 442 164 ug/Kg ☼04/14/23 06:07 04/14/23 17:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
89.8 33.1 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2,2'-oxybis[1-chloropropane]
442 156 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2,4,5-Trichlorophenol
442 149 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2,4,6-Trichlorophenol
89.8 34.5 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2,4-Dichlorophenol
442 150 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2,4-Dimethylphenol
4420 2780 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2,4-Dinitrophenol
442 267 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2,4-Dinitrotoluene
442 174 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2,6-Dinitrotoluene
89.8 20.5 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2-Chloronaphthalene
442 165 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2-Chlorophenol
89.8 21.5 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2-Methylnaphthalene
442 128 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2-Methylphenol
2280 204 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2-Nitroaniline
442 165 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND2-Nitrophenol
442 417 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND3,3'-Dichlorobenzidine
2280 114 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND3-Nitroaniline
2280 771 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND4,6-Dinitro-2-methylphenol
442 190 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND4-Bromophenyl phenyl ether
442 157 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND4-Chloro-3-methylphenol
442 117 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND4-Chloroaniline
442 149 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND4-Chlorophenyl phenyl ether
442 131 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDMethylphenol, 3 & 4
2280 166 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND4-Nitroaniline
2280 314 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼ND4-Nitrophenol
89.8 25.7 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDAcenaphthene
89.8 19.6 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDAcenaphthylene
898 160 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDAcetophenone
89.8 23.2 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDAnthracene
898 196 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDAtrazine
898 55.5 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDBenzaldehyde
89.8 40.4 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDBenzo[a]anthracene
89.8 38.7 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDBenzo[a]pyrene
89.8 22.0 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDBenzo[b]fluoranthene
89.8 19.3 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDBenzo[g,h,i]perylene
89.8 26.8 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDBenzo[k]fluoranthene
442 164 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDBis(2-chloroethoxy)methane
89.8 16.2 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDBis(2-chloroethyl)ether
4420 476 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDBis(2-ethylhexyl) phthalate
442 307 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDButyl benzyl phthalate
2280 291 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDCaprolactam
89.8 20.9 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDCarbazole
89.8 49.6 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDChrysene
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-4Client Sample ID: EB-7 (3-5)
Matrix: SolidDate Collected: 04/07/23 12:10
Percent Solids: 73.1Date Received: 04/08/23 08:35
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 89.8 57.2 ug/Kg ☼04/14/23 06:07 04/14/23 17:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
442 165 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDDibenzofuran
442 157 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDDiethyl phthalate
442 177 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDDimethyl phthalate
442 196 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDDi-n-butyl phthalate
442 260 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDDi-n-octyl phthalate
89.8 23.6 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDFluoranthene
89.8 17.6 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDFluorene
89.8 32.0 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDHexachlorobenzene
89.8 26.1 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDHexachlorobutadiene
442 45.7 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDHexachlorocyclopentadiene
442 158 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDHexachloroethane
89.8 44.5 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDIndeno[1,2,3-cd]pyrene
442 168 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDIsophorone
89.8 17.4 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDNaphthalene
898 164 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDNitrobenzene
89.8 30.3 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDN-Nitrosodi-n-propylamine
442 149 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDN-Nitrosodiphenylamine
2280 719 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDPentachlorophenol
89.8 24.0 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDPhenanthrene
442 135 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDPhenol
89.8 21.2 ug/Kg 04/14/23 06:07 04/14/23 17:56 1☼NDPyrene
2,4,6-Tribromophenol (Surr)59 34-108 04/14/23 06:07 04/14/23 17:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 58 04/14/23 06:07 04/14/23 17:56 144-105
2-Fluorophenol (Surr)56 04/14/23 06:07 04/14/23 17:56 148-105
Nitrobenzene-d5 (Surr)57 04/14/23 06:07 04/14/23 17:56 146-105
Phenol-d5 (Surr)57 04/14/23 06:07 04/14/23 17:56 146-105
Terphenyl-d14 (Surr)60 04/14/23 06:07 04/14/23 17:56 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
7.59 6.84 1.71 mg/Kg ☼04/24/23 09:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 21.8 5.46 mg/Kg ☼04/16/23 20:00 04/21/23 05:02 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
21.8 5.46 mg/Kg 04/16/23 20:00 04/21/23 05:02 50☼NDC9-C10 Aromatics
21.8 5.46 mg/Kg 04/16/23 20:00 04/21/23 05:02 50☼7.59 JC9-C12 Aliphatics (unadjusted)
21.8 5.46 mg/Kg 04/16/23 20:00 04/21/23 05:02 50☼NDC9-C12 Aliphatics (adjusted)
21.8 5.46 mg/Kg 04/16/23 20:00 04/21/23 05:02 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)113 70-130 04/16/23 20:00 04/21/23 05:02 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)107 04/16/23 20:00 04/21/23 05:02 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
170 16.2 16.2 mg/Kg ☼04/13/23 14:59 05/02/23 23:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
16.2 16.2 mg/Kg 04/13/23 14:59 05/02/23 23:34 1☼164C11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-154822-4Client Sample ID: EB-7 (3-5)
Matrix: SolidDate Collected: 04/07/23 12:10
Percent Solids: 73.1Date Received: 04/08/23 08:35
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
39.5 8.12 8.12 mg/Kg ☼04/13/23 14:59 05/02/23 23:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C9-C18 Aliphatics
1-Chlorooctadecane (Surr)52 40-140 04/13/23 14:59 05/02/23 23:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)77 04/13/23 14:59 05/02/23 23:34 140-140
o- terphenyl (Surr)56 04/13/23 14:59 05/02/23 23:34 140-140
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - DL
RL MDL
1300 81.2 81.2 mg/Kg ☼04/13/23 14:59 05/03/23 18:53 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
1-Chlorooctadecane (Surr)51 40-140 04/13/23 14:59 05/03/23 18:53 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
1510 16.4 16.4 mg/Kg ☼05/02/23 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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QC Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 180-432587/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432587
RL MDL
1,1,1-Trichloroethane ND 5.00 1.67 ug/Kg 04/18/23 12:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.525.00 ug/Kg 04/18/23 12:06 11,1,2,2-Tetrachloroethane
ND 2.005.00 ug/Kg 04/18/23 12:06 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.9905.00 ug/Kg 04/18/23 12:06 11,1,2-Trichloroethane
ND 1.605.00 ug/Kg 04/18/23 12:06 11,1-Dichloroethane
ND 2.265.00 ug/Kg 04/18/23 12:06 11,1-Dichloroethene
ND 3.235.00 ug/Kg 04/18/23 12:06 11,2-Dibromo-3-Chloropropane
ND 1.685.00 ug/Kg 04/18/23 12:06 11,2-Dichlorobenzene
ND 1.445.00 ug/Kg 04/18/23 12:06 11,2-Dichloroethane
ND 1.335.00 ug/Kg 04/18/23 12:06 11,2-Dichloropropane
ND 2.545.00 ug/Kg 04/18/23 12:06 11,2,4-Trichlorobenzene
ND 3.085.00 ug/Kg 04/18/23 12:06 11,3-Dichlorobenzene
ND 1.505.00 ug/Kg 04/18/23 12:06 11,4-Dichlorobenzene
ND 2.545.00 ug/Kg 04/18/23 12:06 12-Butanone (MEK)
ND 1.575.00 ug/Kg 04/18/23 12:06 12-Hexanone
ND 1.835.00 ug/Kg 04/18/23 12:06 14-Methyl-2-pentanone (MIBK)
ND 3.9020.0 ug/Kg 04/18/23 12:06 1Acetone
ND 1.415.00 ug/Kg 04/18/23 12:06 1Benzene
ND 2.525.00 ug/Kg 04/18/23 12:06 1Bromoform
ND 2.285.00 ug/Kg 04/18/23 12:06 1Bromomethane
ND 4.005.00 ug/Kg 04/18/23 12:06 1Carbon disulfide
ND 2.035.00 ug/Kg 04/18/23 12:06 1Carbon tetrachloride
ND 1.305.00 ug/Kg 04/18/23 12:06 1Chlorobenzene
ND 2.485.00 ug/Kg 04/18/23 12:06 1Chlorodibromomethane
ND 1.615.00 ug/Kg 04/18/23 12:06 1Chloroform
ND 1.985.00 ug/Kg 04/18/23 12:06 1Chloromethane
ND 2.925.00 ug/Kg 04/18/23 12:06 1Chloroethane
ND 1.515.00 ug/Kg 04/18/23 12:06 1cis-1,2-Dichloroethene
ND 2.215.00 ug/Kg 04/18/23 12:06 1cis-1,3-Dichloropropene
ND 2.335.00 ug/Kg 04/18/23 12:06 1Dichlorobromomethane
ND 2.495.00 ug/Kg 04/18/23 12:06 1Dichlorodifluoromethane
ND 1.855.00 ug/Kg 04/18/23 12:06 1Ethylbenzene
ND 1.375.00 ug/Kg 04/18/23 12:06 11,2-Dibromoethane
ND 2.395.00 ug/Kg 04/18/23 12:06 1Cyclohexane
ND 2.605.00 ug/Kg 04/18/23 12:06 1Isopropylbenzene
ND 7.3625.0 ug/Kg 04/18/23 12:06 1Methyl acetate
ND 1.475.00 ug/Kg 04/18/23 12:06 1Methyl tert-butyl ether
ND 2.415.00 ug/Kg 04/18/23 12:06 1Methylcyclohexane
ND 4.515.00 ug/Kg 04/18/23 12:06 1Methylene Chloride
ND 1.505.00 ug/Kg 04/18/23 12:06 1Styrene
ND 2.015.00 ug/Kg 04/18/23 12:06 1Tetrachloroethene
ND 1.445.00 ug/Kg 04/18/23 12:06 1Toluene
ND 1.755.00 ug/Kg 04/18/23 12:06 1trans-1,2-Dichloroethene
ND 2.255.00 ug/Kg 04/18/23 12:06 1trans-1,3-Dichloropropene
ND 1.575.00 ug/Kg 04/18/23 12:06 1Trichloroethene
ND 4.155.00 ug/Kg 04/18/23 12:06 1Trichlorofluoromethane
ND 3.605.00 ug/Kg 04/18/23 12:06 1Vinyl chloride
ND 7.2110.0 ug/Kg 04/18/23 12:06 1Xylenes, Total
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QC Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-432587/9
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432587
1,2-Dichloroethane-d4 (Surr)124 73-135 04/18/23 12:06 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
100 04/18/23 12:06 14-Bromofluorobenzene (Surr)60-124
110 04/18/23 12:06 1Dibromofluoromethane (Surr)69-126
97 04/18/23 12:06 1Toluene-d8 (Surr)67-134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432587/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432587
1,1,1-Trichloroethane 40.0 41.24 ug/Kg 103 72-134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2,2-Tetrachloroethane 40.0 38.46 ug/Kg 96 36-170
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 54.49 *+ug/Kg 136 59-135
1,1,2-Trichloroethane 40.0 33.60 ug/Kg 84 66-128
1,1-Dichloroethane 40.0 36.62 ug/Kg 92 73-124
1,1-Dichloroethene 40.0 51.41 ug/Kg 129 55-136
1,2-Dibromo-3-Chloropropane 40.0 41.60 ug/Kg 104 30-163
1,2-Dichlorobenzene 40.0 33.13 ug/Kg 83 76-120
1,2-Dichloroethane 40.0 44.00 ug/Kg 110 64-140
1,2-Dichloropropane 40.0 33.71 ug/Kg 84 77-119
1,2,4-Trichlorobenzene 40.0 41.21 ug/Kg 103 22-170
1,3-Dichlorobenzene 40.0 34.13 ug/Kg 85 77-121
1,4-Dichlorobenzene 40.0 34.01 ug/Kg 85 79-120
2-Butanone (MEK)40.0 39.06 ug/Kg 98 39-157
2-Hexanone 40.0 36.27 ug/Kg 91 42-152
4-Methyl-2-pentanone (MIBK)40.0 34.19 ug/Kg 85 51-147
Acetone 40.0 54.16 ug/Kg 135 23-170
Benzene 40.0 36.26 ug/Kg 91 77-120
Bromoform 40.0 38.66 ug/Kg 97 37-147
Bromomethane 40.0 41.15 ug/Kg 103 47-149
Carbon disulfide 40.0 62.68 *+ug/Kg 157 40-156
Carbon tetrachloride 40.0 42.65 ug/Kg 107 73-130
Chlorobenzene 40.0 34.53 ug/Kg 86 79-122
Chlorodibromomethane 40.0 37.24 ug/Kg 93 60-134
Chloroform 40.0 37.93 ug/Kg 95 73-126
Chloromethane 40.0 39.21 ug/Kg 98 46-151
Chloroethane 40.0 45.31 ug/Kg 113 37-159
cis-1,2-Dichloroethene 40.0 37.50 ug/Kg 94 77-118
cis-1,3-Dichloropropene 40.0 38.69 ug/Kg 97 73-127
Dichlorobromomethane 40.0 38.21 ug/Kg 96 75-123
Dichlorodifluoromethane 40.0 66.09 *+ug/Kg 165 26-149
Ethylbenzene 40.0 34.21 ug/Kg 86 79-119
1,2-Dibromoethane 40.0 35.68 ug/Kg 89 59-137
Cyclohexane 40.0 37.61 ug/Kg 94 63-143
Isopropylbenzene 40.0 34.66 ug/Kg 87 70-125
Methyl acetate 80.0 157.8 *+ug/Kg 197 20-170
Methyl tert-butyl ether 40.0 40.01 ug/Kg 100 58-132
Methylcyclohexane 40.0 37.70 ug/Kg 94 70-125
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QC Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432587/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432587
Methylene Chloride 40.0 43.32 ug/Kg 108 67-131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
m-Xylene & p-Xylene 40.0 35.84 ug/Kg 90 77-120
o-Xylene 40.0 35.22 ug/Kg 88 78-118
Styrene 40.0 34.75 ug/Kg 87 80-120
Tetrachloroethene 40.0 35.94 ug/Kg 90 71-121
Toluene 40.0 32.68 ug/Kg 82 76-120
trans-1,2-Dichloroethene 40.0 40.19 ug/Kg 100 75-122
trans-1,3-Dichloropropene 40.0 34.00 ug/Kg 85 68-133
Trichloroethene 40.0 39.10 ug/Kg 98 69-118
Trichlorofluoromethane 40.0 39.23 ug/Kg 98 32-149
Vinyl chloride 40.0 41.73 ug/Kg 104 64-134
Xylenes, Total 80.0 71.06 ug/Kg 89 78-118
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
109
LCS LCS
Qualifier Limits%Recovery
1004-Bromofluorobenzene (Surr)60 -124
106Dibromofluoromethane (Surr)69 -126
95Toluene-d8 (Surr)67 -134
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-432293/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
RL MDL
1,1'-Biphenyl ND 330 122 ug/Kg 04/14/23 06:07 04/14/23 13:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 24.767.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,2'-oxybis[1-chloropropane]
ND 116330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4,5-Trichlorophenol
ND 111330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4,6-Trichlorophenol
ND 25.767.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4-Dichlorophenol
ND 112330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4-Dimethylphenol
ND 20703300 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4-Dinitrophenol
ND 199330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,4-Dinitrotoluene
ND 130330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12,6-Dinitrotoluene
ND 15.367.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Chloronaphthalene
ND 123330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Chlorophenol
ND 16.067.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Methylnaphthalene
ND 95.6330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Methylphenol
ND 1521700 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Nitroaniline
ND 123330 ug/Kg 04/14/23 06:07 04/14/23 13:13 12-Nitrophenol
ND 311330 ug/Kg 04/14/23 06:07 04/14/23 13:13 13,3'-Dichlorobenzidine
ND 84.81700 ug/Kg 04/14/23 06:07 04/14/23 13:13 13-Nitroaniline
ND 5751700 ug/Kg 04/14/23 06:07 04/14/23 13:13 14,6-Dinitro-2-methylphenol
ND 142330 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Bromophenyl phenyl ether
ND 117330 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Chloro-3-methylphenol
ND 87.5330 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Chloroaniline
ND 111330 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Chlorophenyl phenyl ether
ND 97.9330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Methylphenol, 3 & 4
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-432293/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
RL MDL
4-Nitroaniline ND 1700 124 ug/Kg 04/14/23 06:07 04/14/23 13:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 2341700 ug/Kg 04/14/23 06:07 04/14/23 13:13 14-Nitrophenol
ND 19.267.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Acenaphthene
ND 14.667.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Acenaphthylene
ND 119670 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Acetophenone
ND 17.367.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Anthracene
ND 146670 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Atrazine
ND 41.4670 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzaldehyde
ND 30.167.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[a]anthracene
ND 28.967.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[a]pyrene
ND 16.467.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[b]fluoranthene
ND 14.467.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[g,h,i]perylene
ND 20.067.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Benzo[k]fluoranthene
ND 122330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Bis(2-chloroethoxy)methane
ND 12.167.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Bis(2-chloroethyl)ether
ND 3553300 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Bis(2-ethylhexyl) phthalate
ND 229330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Butyl benzyl phthalate
ND 2171700 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Caprolactam
ND 15.667.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Carbazole
ND 37.067.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Chrysene
ND 42.767.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Dibenz(a,h)anthracene
ND 123330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Dibenzofuran
ND 117330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Diethyl phthalate
ND 132330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Dimethyl phthalate
ND 146330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Di-n-butyl phthalate
ND 194330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Di-n-octyl phthalate
ND 17.667.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Fluoranthene
ND 13.167.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Fluorene
ND 23.967.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Hexachlorobenzene
ND 19.567.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Hexachlorobutadiene
ND 34.1330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Hexachlorocyclopentadiene
ND 118330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Hexachloroethane
ND 33.267.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Indeno[1,2,3-cd]pyrene
ND 125330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Isophorone
ND 13.067.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Naphthalene
ND 122670 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Nitrobenzene
ND 22.667.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1N-Nitrosodi-n-propylamine
ND 111330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1N-Nitrosodiphenylamine
ND 5361700 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Pentachlorophenol
ND 17.967.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Phenanthrene
ND 101330 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Phenol
ND 15.867.0 ug/Kg 04/14/23 06:07 04/14/23 13:13 1Pyrene
2,4,6-Tribromophenol (Surr)91 34-108 04/14/23 13:13 1
MB MB
Surrogate
04/14/23 06:07
Dil FacPreparedAnalyzedQualifierLimits%Recovery
92 04/14/23 06:07 04/14/23 13:13 12-Fluorobiphenyl 44-105
92 04/14/23 06:07 04/14/23 13:13 12-Fluorophenol (Surr)48-105
90 04/14/23 06:07 04/14/23 13:13 1Nitrobenzene-d5 (Surr)46-105
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-432293/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
Phenol-d5 (Surr)90 46-105 04/14/23 13:13 1
MB MB
Surrogate
04/14/23 06:07
Dil FacPreparedAnalyzedQualifierLimits%Recovery
104 04/14/23 06:07 04/14/23 13:13 1Terphenyl-d14 (Surr)39-105
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432293/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
1,1'-Biphenyl 6670 5434 ug/Kg 82 50-100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,2'-oxybis[1-chloropropane]6670 5341 ug/Kg 80 30-113
2,4,5-Trichlorophenol 6670 5774 ug/Kg 87 50-104
2,4,6-Trichlorophenol 6670 5834 ug/Kg 88 50-105
2,4-Dichlorophenol 6670 5725 ug/Kg 86 53-101
2,4-Dimethylphenol 6670 5410 ug/Kg 81 51-101
2,4-Dinitrophenol 13300 10090 ug/Kg 76 33-101
2,4-Dinitrotoluene 6670 5875 ug/Kg 88 54-104
2,6-Dinitrotoluene 6670 5754 ug/Kg 86 51-106
2-Chloronaphthalene 6670 5279 ug/Kg 79 51-100
2-Chlorophenol 6670 5482 ug/Kg 82 51-100
2-Methylnaphthalene 6670 5427 ug/Kg 81 53-100
2-Methylphenol 6670 5418 ug/Kg 81 50-101
2-Nitroaniline 6670 5903 ug/Kg 89 42-123
2-Nitrophenol 6670 5964 ug/Kg 89 55-107
3,3'-Dichlorobenzidine 6670 4779 ug/Kg 72 43-100
3-Nitroaniline 6670 5989 ug/Kg 90 50-103
4,6-Dinitro-2-methylphenol 13300 9967 ug/Kg 75 51-100
4-Bromophenyl phenyl ether 6670 5413 ug/Kg 81 52-101
4-Chloro-3-methylphenol 6670 5681 ug/Kg 85 49-106
4-Chloroaniline 6670 5318 ug/Kg 80 47-100
4-Chlorophenyl phenyl ether 6670 5579 ug/Kg 84 52-100
Methylphenol, 3 & 4 6670 5699 ug/Kg 85 50-103
4-Nitroaniline 6670 5722 ug/Kg 86 52-103
4-Nitrophenol 13300 12180 ug/Kg 91 30-134
Acenaphthene 6670 5431 ug/Kg 81 50-100
Acenaphthylene 6670 5546 ug/Kg 83 52-100
Acetophenone 6670 5250 ug/Kg 79 48-100
Anthracene 6670 5633 ug/Kg 84 53-100
Atrazine 6670 5182 ug/Kg 78 49-103
Benzaldehyde 6670 3686 ug/Kg 55 23-105
Benzo[a]anthracene 6670 5225 ug/Kg 78 51-100
Benzo[a]pyrene 6670 5504 ug/Kg 83 51-100
Benzo[b]fluoranthene 6670 5286 ug/Kg 79 48-100
Benzo[g,h,i]perylene 6670 5785 ug/Kg 87 48-105
Benzo[k]fluoranthene 6670 5700 ug/Kg 86 19-100
Bis(2-chloroethoxy)methane 6670 5424 ug/Kg 81 49-100
Bis(2-chloroethyl)ether 6670 5375 ug/Kg 81 48-100
Bis(2-ethylhexyl) phthalate 6670 5745 ug/Kg 86 53-107
Butyl benzyl phthalate 6670 5685 ug/Kg 85 52-107
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432293/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 432297 Prep Batch: 432293
Carbazole 6670 5537 ug/Kg 83 53-100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chrysene 6670 5071 ug/Kg 76 50-100
Dibenz(a,h)anthracene 6670 6099 ug/Kg 91 50-107
Dibenzofuran 6670 5485 ug/Kg 82 52-100
Diethyl phthalate 6670 5598 ug/Kg 84 48-104
Dimethyl phthalate 6670 5572 ug/Kg 84 53-100
Di-n-butyl phthalate 6670 5807 ug/Kg 87 57-102
Di-n-octyl phthalate 6670 5855 ug/Kg 88 41-106
Fluoranthene 6670 5649 ug/Kg 85 55-100
Fluorene 6670 5641 ug/Kg 85 52-100
Hexachlorobenzene 6670 5440 ug/Kg 82 49-100
Hexachlorobutadiene 6670 5432 ug/Kg 81 38-107
Hexachlorocyclopentadiene 6670 5272 ug/Kg 79 33-117
Hexachloroethane 6670 5412 ug/Kg 81 47-100
Indeno[1,2,3-cd]pyrene 6670 6098 ug/Kg 91 51-103
Isophorone 6670 5517 ug/Kg 83 48-105
Naphthalene 6670 5417 ug/Kg 81 51-100
Nitrobenzene 6670 5523 ug/Kg 83 44-108
N-Nitrosodi-n-propylamine 6670 5582 ug/Kg 84 45-107
N-Nitrosodiphenylamine 6670 5535 ug/Kg 83 52-100
Pentachlorophenol 13300 12500 ug/Kg 94 42-110
Phenanthrene 6670 5406 ug/Kg 81 53-100
Phenol 6670 5491 ug/Kg 82 49-100
Pyrene 6670 5181 ug/Kg 78 52-100
2,4,6-Tribromophenol (Surr)34 -108
Surrogate
80
LCS LCS
Qualifier Limits%Recovery
752-Fluorobiphenyl 44 -105
782-Fluorophenol (Surr)48 -105
75Nitrobenzene-d5 (Surr)46 -105
76Phenol-d5 (Surr)46 -105
71Terphenyl-d14 (Surr)39 -105
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-366573/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 366575 Prep Batch: 366573
RL MDL
C5-C8 Aliphatics (unadjusted)ND 5.00 1.25 mg/Kg 04/20/23 11:29 04/20/23 12:38 50
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.255.00 mg/Kg 04/20/23 11:29 04/20/23 12:38 50C9-C10 Aromatics
ND 1.255.00 mg/Kg 04/20/23 11:29 04/20/23 12:38 50C9-C12 Aliphatics (unadjusted)
ND 1.255.00 mg/Kg 04/20/23 11:29 04/20/23 12:38 50C9-C12 Aliphatics (adjusted)
ND 1.255.00 mg/Kg 04/20/23 11:29 04/20/23 12:38 50C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)99 70-130 04/20/23 12:38 50
MB MB
Surrogate
04/20/23 11:29
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-366573/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 366575 Prep Batch: 366573
a,a,a-Trifluorotoluene (pid)91 70-130 04/20/23 12:38 50
MB MB
Surrogate
04/20/23 11:29
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-366573/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 366575 Prep Batch: 366573
C5-C8 Aliphatics (unadjusted)7.53 6.868 mg/Kg 91 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 2.51 2.412 J mg/Kg 96 70-130
C9-C12 Aliphatics (unadjusted)7.53 6.511 mg/Kg 87 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
96a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-366573/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 366575 Prep Batch: 366573
C5-C8 Aliphatics (unadjusted)7.53 6.685 mg/Kg 89 70-130 3 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 2.51 2.346 J mg/Kg 94 70-130 3 30
C9-C12 Aliphatics (unadjusted)7.53 6.531 mg/Kg 87 70-130 0 30
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
99
LCSD LCSD
Qualifier Limits%Recovery
93a,a,a-Trifluorotoluene (pid)70 -130
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-364138/1-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371212 Prep Batch: 364138
RL MDL
C19-C36 Aliphatics ND 12.0 12.0 mg/Kg 04/13/23 14:59 05/02/23 18:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 6.006.00 mg/Kg 04/13/23 14:59 05/02/23 18:41 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)43 40-140 05/02/23 18:41 1
MB MB
Surrogate
04/13/23 14:59
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-364138/1-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371207 Prep Batch: 364138
RL MDL
C11-C22 Aromatics (unadjusted)ND 12.0 12.0 mg/Kg 04/13/23 14:59 05/02/23 18:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 12.012.0 mg/Kg 04/13/23 14:59 05/02/23 18:41 1C11-C22 Aromatics (Adjusted)
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
2-Fluorobiphenyl (Surr)75 40-140 05/02/23 18:41 1
MB MB
Surrogate
04/13/23 14:59
Dil FacPreparedAnalyzedQualifierLimits%Recovery
72 04/13/23 14:59 05/02/23 18:41 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-364138/2-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371212 Prep Batch: 364138
C19-C36 Aliphatics 32.1 23.54 mg/Kg 73 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 24.1 18.71 mg/Kg 78 40-140
1-Chlorooctadecane (Surr)40 -140
Surrogate
44
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-364138/2-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371207 Prep Batch: 364138
C11-C22 Aromatics (unadjusted)68.1 47.28 mg/Kg 69 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Fluorobiphenyl (Surr)40 -140
Surrogate
76
LCS LCS
Qualifier Limits%Recovery
70o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-364138/3-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371212 Prep Batch: 364138
C19-C36 Aliphatics 32.1 22.32 mg/Kg 69 40-140 5 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 24.1 17.96 mg/Kg 75 40-140 4 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
51
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-364138/3-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371207 Prep Batch: 364138
C11-C22 Aromatics (unadjusted)68.1 46.86 mg/Kg 69 40-140 1 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)40 -140
Surrogate
77
LCSD LCSD
Qualifier Limits%Recovery
68o- terphenyl (Surr)40 -140
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-154822-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: EB-4 (8-10)Lab Sample ID: 180-154822-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371207 Prep Batch: 364138
C11-C22 Aromatics (unadjusted)ND 101 65.33 mg/Kg 64 40-140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
C19-C36 Aliphatics ND 47.8 31.20 mg/Kg 65 40-140☼
C9-C18 Aliphatics ND 35.9 24.33 mg/Kg 68 40-140☼
1-Chlorooctadecane (Surr)40 -140
Surrogate
52
MS MS
Qualifier Limits%Recovery
822-Fluorobiphenyl (Surr)40 -140
65o- terphenyl (Surr)40 -140
Client Sample ID: EB-4 (8-10)Lab Sample ID: 180-154822-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 371207 Prep Batch: 364138
C11-C22 Aromatics (unadjusted)ND 103 58.95 mg/Kg 57 40-140 10 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
C19-C36 Aliphatics ND 48.5 24.58 mg/Kg 51 40-140 24 50☼
C9-C18 Aliphatics ND 36.4 20.25 mg/Kg 56 40-140 18 50☼
1-Chlorooctadecane (Surr)S1-40 -140
Surrogate
38
MSD MSD
Qualifier Limits%Recovery
822-Fluorobiphenyl (Surr)40 -140
54o- terphenyl (Surr)40 -140
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-154822-1
SDG Number: 640 Rock Lane
Login Number: 154822
Question Answer Comment
Creator: Abernathy, Eric L
List Source: Eurofins Pittsburgh
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-154822-1
SDG Number: 640 Rock Lane
Login Number: 154822
Question Answer Comment
Creator: Cyms, Carolyn M
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 04/10/23 10:46 AMList Number: 2
TrueThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
FalseAppropriate sample containers are used.Did not receive all required containers.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.Not present.
N/AVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
Eurofins Pittsburgh
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ANALYTICAL REPORT
PREPARED FOR
Attn: Mr. Bruce Stainbrook
Altec Industries, Inc
Bruce Stainbrook
810 Franklin Court, Ste A
Marietta, Georgia 30067
Generated 5/5/2023 4:29:59 PM
JOB DESCRIPTION
China Grove NC
SDG NUMBER 640 Rock Lane
JOB NUMBER
180-155027-1
See page two for job notes and contact information.
Pittsburgh PA 15238
RIDC Park
301 Alpha Drive
Eurofins Pittsburgh
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Eurofins Pittsburgh
Eurofins Pittsburgh is a laboratory within Eurofins Environment Testing Northeast LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
PA Lab ID: 02-00416
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Pittsburgh Project Manager.
Authorization
Generated
5/5/2023 4:29:59 PM
Authorized for release by
Shali Brown, Project Manager II
[e-mail]
[phone]
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Case Narrative
Client: Altec Industries, Inc Job ID: 180-155027-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-155027-1
Laboratory: Eurofins Pittsburgh
Narrative
Job Narrative
180-155027-1
Receipt
The samples were received on 4/13/2023 9:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 4.6°C
GC/MS VOA
Method 8260D_LL: The laboratory control sample (LCS) for analytical batch 180-433155 recovered outside control limits for the following
analytes: 1,3-Dichlorobenzene and Chlorobenzene. These analytes were biased high in the LCS and were not detected in the associated
samples; therefore, the data have been reported.
Method 8260D_LL: The following sample was diluted to bring the concentration of target analytes within the calibration range: TMW-1
(180-155027-3). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
Method 625.1_LL_PREC: Received limited quantity, insufficient amount for MSD.(180-155027-C-2 MS)
Method 625.1_LL_PREC: The matrix spike (MS) recoveries for preparation batch 180-432661 and analytical batch 180-432988 were
outside control limits. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery was
within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method MAEPH2.1: The breakthrough for naphthalene and 2-methylnaphthalene in the LCS is <1%. The breakthrough for naphthalene
and 2-methylnaphthalene in the LCSD is 1%. The method requirement for breakthrough is <5%. TMW-1 (180-155027-1), TMW-2
(180-155027-5) and TMW-3 (180-155027-12)
Method MAEPH2.1: 1-Chlorooctadecane (Surr) recovery for the following samples were outside acceptance limits: TMW-1 (180-155027-1)
and TMW-3 (180-155027-12). The samples cannot be re-extracted and re-analyzed within method holding time. The results have been
reported per client request.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Definitions/Glossary
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
E Result exceeded calibration range.
F1 MS and/or MSD recovery exceeds control limits.
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
S1-Surrogate recovery exceeds control limits, low biased.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Pittsburgh
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Accreditation/Certification Summary
Client: Altec Industries, Inc Job ID: 180-155027-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Laboratory: Eurofins Pittsburgh
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 434 05-03-23
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 521 12-31-23
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-1Client Sample ID: TMW-1
Matrix: WaterDate Collected: 04/12/23 10:15
Date Received: 04/13/23 09:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 41.6 41.6 ug/L 04/20/23 21:54 05/01/23 21:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
41.6 41.6 ug/L 04/20/23 21:54 05/01/23 21:55 1NDC11-C22 Aromatics (Adjusted)
52.1 52.1 ug/L 04/20/23 21:54 05/01/23 21:55 1NDC19-C36 Aliphatics
31.2 31.2 ug/L 04/20/23 21:54 05/01/23 21:55 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)20 S1-40-140 04/20/23 21:54 05/01/23 21:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)73 04/20/23 21:54 05/01/23 21:55 140-140
o- terphenyl (Surr)49 04/20/23 21:54 05/01/23 21:55 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 05/03/23 14:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-2Client Sample ID: TMW-1
Matrix: WaterDate Collected: 04/12/23 11:00
Date Received: 04/13/23 09:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.176 0.0602 ug/L 04/18/23 13:20 04/21/23 14:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.176 0.0602 ug/L 04/18/23 13:20 04/21/23 14:55 1NDAcenaphthylene
0.176 0.0454 ug/L 04/18/23 13:20 04/21/23 14:55 1NDAnthracene
0.176 0.0694 ug/L 04/18/23 13:20 04/21/23 14:55 1NDBenzo[a]anthracene
0.176 0.0491 ug/L 04/18/23 13:20 04/21/23 14:55 1NDBenzo[a]pyrene
0.176 0.0898 ug/L 04/18/23 13:20 04/21/23 14:55 1NDBenzo[b]fluoranthene
0.176 0.0639 ug/L 04/18/23 13:20 04/21/23 14:55 1NDBenzo[g,h,i]perylene
0.176 0.0815 ug/L 04/18/23 13:20 04/21/23 14:55 1NDBenzo[k]fluoranthene
0.926 0.141 ug/L 04/18/23 13:20 04/21/23 14:55 1NDBis(2-chloroethoxy)methane
0.176 0.0370 ug/L 04/18/23 13:20 04/21/23 14:55 1NDBis(2-chloroethyl)ether
0.176 0.0537 ug/L 04/18/23 13:20 04/21/23 14:55 1ND2,2'-oxybis[1-chloropropane]
9.26 5.77 ug/L 04/18/23 13:20 04/21/23 14:55 1NDBis(2-ethylhexyl) phthalate
0.926 0.295 ug/L 04/18/23 13:20 04/21/23 14:55 1ND4-Bromophenyl phenyl ether
0.926 0.428 ug/L 04/18/23 13:20 04/21/23 14:55 1NDButyl benzyl phthalate
0.176 0.0546 ug/L 04/18/23 13:20 04/21/23 14:55 1NDF12-Chloronaphthalene
0.926 0.205 ug/L 04/18/23 13:20 04/21/23 14:55 1ND4-Chlorophenyl phenyl ether
0.176 0.0750 ug/L 04/18/23 13:20 04/21/23 14:55 1NDChrysene
0.176 0.0667 ug/L 04/18/23 13:20 04/21/23 14:55 1NDDibenz(a,h)anthracene
0.926 0.540 ug/L 04/18/23 13:20 04/21/23 14:55 1ND3,3'-Dichlorobenzidine
0.926 0.525 ug/L 04/18/23 13:20 04/21/23 14:55 1NDDiethyl phthalate
0.926 0.634 ug/L 04/18/23 13:20 04/21/23 14:55 1NDDi-n-octyl phthalate
0.926 0.181 ug/L 04/18/23 13:20 04/21/23 14:55 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.176 0.0556 ug/L 04/18/23 13:20 04/21/23 14:55 1NDFluoranthene
0.176 0.0639 ug/L 04/18/23 13:20 04/21/23 14:55 1NDF1Fluorene
0.176 0.0519 ug/L 04/18/23 13:20 04/21/23 14:55 1NDHexachlorobenzene
0.176 0.0639 ug/L 04/18/23 13:20 04/21/23 14:55 1NDHexachlorobutadiene
0.926 0.460 ug/L 04/18/23 13:20 04/21/23 14:55 1NDHexachlorocyclopentadiene
0.926 0.123 ug/L 04/18/23 13:20 04/21/23 14:55 1NDHexachloroethane
0.176 0.0787 ug/L 04/18/23 13:20 04/21/23 14:55 1NDIndeno[1,2,3-cd]pyrene
0.926 0.174 ug/L 04/18/23 13:20 04/21/23 14:55 10.294 JIsophorone
0.176 0.0546 ug/L 04/18/23 13:20 04/21/23 14:55 10.0719 JNaphthalene
1.85 0.463 ug/L 04/18/23 13:20 04/21/23 14:55 1NDNitrobenzene
0.926 0.0620 ug/L 04/18/23 13:20 04/21/23 14:55 1NDN-Nitrosodimethylamine
0.176 0.0657 ug/L 04/18/23 13:20 04/21/23 14:55 1NDN-Nitrosodi-n-propylamine
0.176 0.0509 ug/L 04/18/23 13:20 04/21/23 14:55 1NDPhenanthrene
0.176 0.0500 ug/L 04/18/23 13:20 04/21/23 14:55 1NDPyrene
4.63 0.784 ug/L 04/18/23 13:20 04/21/23 14:55 1NDPentachlorophenol
0.926 0.451 ug/L 04/18/23 13:20 04/21/23 14:55 1NDPhenol
0.926 0.121 ug/L 04/18/23 13:20 04/21/23 14:55 1ND1,2,4-Trichlorobenzene
0.176 0.0472 ug/L 04/18/23 13:20 04/21/23 14:55 1ND2,4-Dichlorophenol
9.26 1.42 ug/L 04/18/23 13:20 04/21/23 14:55 1ND2,4-Dinitrophenol
0.926 0.155 ug/L 04/18/23 13:20 04/21/23 14:55 1ND2,4-Dimethylphenol
0.926 0.207 ug/L 04/18/23 13:20 04/21/23 14:55 1ND2,4,6-Trichlorophenol
0.926 0.119 ug/L 04/18/23 13:20 04/21/23 14:55 1ND2-Chlorophenol
0.926 0.179 ug/L 04/18/23 13:20 04/21/23 14:55 1ND2-Nitrophenol
4.63 1.36 ug/L 04/18/23 13:20 04/21/23 14:55 1ND4,6-Dinitro-2-methylphenol
0.926 0.257 ug/L 04/18/23 13:20 04/21/23 14:55 1ND4-Chloro-3-methylphenol
4.63 0.870 ug/L 04/18/23 13:20 04/21/23 14:55 1ND4-Nitrophenol
0.926 0.176 ug/L 04/18/23 13:20 04/21/23 14:55 1NDF1Dibenzofuran
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-2Client Sample ID: TMW-1
Matrix: WaterDate Collected: 04/12/23 11:00
Date Received: 04/13/23 09:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND F1 0.176 0.0574 ug/L 04/18/23 13:20 04/21/23 14:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2-Methylnaphthalene
0.926 0.344 ug/L 04/18/23 13:20 04/21/23 14:55 1ND4-Methylphenol
0.926 0.0917 ug/L 04/18/23 13:20 04/21/23 14:55 1NDF11,3-Dichlorobenzene
0.926 0.278 ug/L 04/18/23 13:20 04/21/23 14:55 1ND2-Methylphenol
0.176 0.0519 ug/L 04/18/23 13:20 04/21/23 14:55 1NDF11-Methylnaphthalene
0.926 0.0880 ug/L 04/18/23 13:20 04/21/23 14:55 1NDF11,2-Dichlorobenzene
0.926 0.348 ug/L 04/18/23 13:20 04/21/23 14:55 1ND4-Chloroaniline
0.926 0.151 ug/L 04/18/23 13:20 04/21/23 14:55 1NDBenzyl alcohol
0.926 0.0565 ug/L 04/18/23 13:20 04/21/23 14:55 1NDF11,4-Dichlorobenzene
2,4,6-Tribromophenol (Surr)46 32-127 04/18/23 13:20 04/21/23 14:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 48 04/18/23 13:20 04/21/23 14:55 147-107
2-Fluorophenol (Surr)50 04/18/23 13:20 04/21/23 14:55 135-109
Nitrobenzene-d5 (Surr)63 04/18/23 13:20 04/21/23 14:55 147-110
Phenol-d5 (Surr)51 04/18/23 13:20 04/21/23 14:55 137-110
Terphenyl-d14 (Surr)54 04/18/23 13:20 04/21/23 14:55 132-115
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-3Client Sample ID: TMW-1
Matrix: WaterDate Collected: 04/12/23 11:45
Date Received: 04/13/23 09:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 04/24/23 18:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 04/24/23 18:18 1ND*+1,3-Dichlorobenzene
1.00 0.544 ug/L 04/24/23 18:18 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 04/24/23 18:18 115.3Benzene
1.00 0.501 ug/L 04/24/23 18:18 1ND*+Chlorobenzene
1.00 0.507 ug/L 04/24/23 18:18 1NDEthylbenzene
1.00 0.457 ug/L 04/24/23 18:18 11.12Toluene
1,2-Dichloroethane-d4 (Surr)88 26-156 04/24/23 18:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)90 04/24/23 18:18 136-124
Dibromofluoromethane (Surr)98 04/24/23 18:18 146-149
Toluene-d8 (Surr)97 04/24/23 18:18 140-146
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS - DL
RL MDL
28.7 4.00 1.62 ug/L 04/24/23 19:22 4
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
o-Xylene
4.00 1.93 ug/L 04/24/23 19:22 4NDm-Xylene & p-Xylene
8.00 3.56 ug/L 04/24/23 19:22 428.7Xylenes, Total
1,2-Dichloroethane-d4 (Surr)84 26-156 04/24/23 19:22 4
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 04/24/23 19:22 436-124
Dibromofluoromethane (Surr)111 04/24/23 19:22 446-149
Toluene-d8 (Surr)102 04/24/23 19:22 440-146
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-4Client Sample ID: TMW-1
Matrix: WaterDate Collected: 04/12/23 11:50
Date Received: 04/13/23 09:30
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
300 100 20.0 ug/L 04/27/23 10:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
191 100 25.0 ug/L 04/24/23 14:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 04/24/23 14:39 124.7 JC9-C10 Aromatics
100 25.0 ug/L 04/24/23 14:39 1109C9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 04/24/23 14:39 148.6 JC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 04/24/23 14:39 1172C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)118 70-130 04/24/23 14:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)107 04/24/23 14:39 170-130
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-5Client Sample ID: TMW-2
Matrix: WaterDate Collected: 04/12/23 13:00
Date Received: 04/13/23 09:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 43.1 43.1 ug/L 04/20/23 21:54 05/01/23 22:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
43.1 43.1 ug/L 04/20/23 21:54 05/01/23 22:18 1NDC11-C22 Aromatics (Adjusted)
53.9 53.9 ug/L 04/20/23 21:54 05/01/23 22:18 1NDC19-C36 Aliphatics
32.3 32.3 ug/L 04/20/23 21:54 05/01/23 22:18 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)55 40-140 04/20/23 21:54 05/01/23 22:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)88 04/20/23 21:54 05/01/23 22:18 140-140
o- terphenyl (Surr)80 04/20/23 21:54 05/01/23 22:18 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 05/03/23 14:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-6Client Sample ID: TMW-2
Matrix: WaterDate Collected: 04/12/23 13:30
Date Received: 04/13/23 09:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.207 0.0707 ug/L 04/18/23 13:20 04/21/23 15:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.207 0.0707 ug/L 04/18/23 13:20 04/21/23 15:39 1NDAcenaphthylene
0.207 0.0533 ug/L 04/18/23 13:20 04/21/23 15:39 1NDAnthracene
0.207 0.0815 ug/L 04/18/23 13:20 04/21/23 15:39 1NDBenzo[a]anthracene
0.207 0.0576 ug/L 04/18/23 13:20 04/21/23 15:39 1NDBenzo[a]pyrene
0.207 0.105 ug/L 04/18/23 13:20 04/21/23 15:39 1NDBenzo[b]fluoranthene
0.207 0.0750 ug/L 04/18/23 13:20 04/21/23 15:39 1NDBenzo[g,h,i]perylene
0.207 0.0957 ug/L 04/18/23 13:20 04/21/23 15:39 1NDBenzo[k]fluoranthene
1.09 0.165 ug/L 04/18/23 13:20 04/21/23 15:39 1NDBis(2-chloroethoxy)methane
0.207 0.0435 ug/L 04/18/23 13:20 04/21/23 15:39 1NDBis(2-chloroethyl)ether
0.207 0.0630 ug/L 04/18/23 13:20 04/21/23 15:39 1ND2,2'-oxybis[1-chloropropane]
10.9 6.77 ug/L 04/18/23 13:20 04/21/23 15:39 1NDBis(2-ethylhexyl) phthalate
1.09 0.347 ug/L 04/18/23 13:20 04/21/23 15:39 1ND4-Bromophenyl phenyl ether
1.09 0.502 ug/L 04/18/23 13:20 04/21/23 15:39 1NDButyl benzyl phthalate
0.207 0.0641 ug/L 04/18/23 13:20 04/21/23 15:39 1ND2-Chloronaphthalene
1.09 0.240 ug/L 04/18/23 13:20 04/21/23 15:39 1ND4-Chlorophenyl phenyl ether
0.207 0.0880 ug/L 04/18/23 13:20 04/21/23 15:39 1NDChrysene
0.207 0.0783 ug/L 04/18/23 13:20 04/21/23 15:39 1NDDibenz(a,h)anthracene
1.09 0.634 ug/L 04/18/23 13:20 04/21/23 15:39 1ND3,3'-Dichlorobenzidine
1.09 0.616 ug/L 04/18/23 13:20 04/21/23 15:39 1NDDiethyl phthalate
1.09 0.745 ug/L 04/18/23 13:20 04/21/23 15:39 1NDDi-n-octyl phthalate
1.09 0.213 ug/L 04/18/23 13:20 04/21/23 15:39 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.207 0.0652 ug/L 04/18/23 13:20 04/21/23 15:39 1NDFluoranthene
0.207 0.0750 ug/L 04/18/23 13:20 04/21/23 15:39 1NDFluorene
0.207 0.0609 ug/L 04/18/23 13:20 04/21/23 15:39 1NDHexachlorobenzene
0.207 0.0750 ug/L 04/18/23 13:20 04/21/23 15:39 1NDHexachlorobutadiene
1.09 0.540 ug/L 04/18/23 13:20 04/21/23 15:39 1NDHexachlorocyclopentadiene
1.09 0.145 ug/L 04/18/23 13:20 04/21/23 15:39 1NDHexachloroethane
0.207 0.0924 ug/L 04/18/23 13:20 04/21/23 15:39 1NDIndeno[1,2,3-cd]pyrene
1.09 0.204 ug/L 04/18/23 13:20 04/21/23 15:39 1NDIsophorone
0.207 0.0641 ug/L 04/18/23 13:20 04/21/23 15:39 1NDNaphthalene
2.17 0.543 ug/L 04/18/23 13:20 04/21/23 15:39 1NDNitrobenzene
1.09 0.0728 ug/L 04/18/23 13:20 04/21/23 15:39 1NDN-Nitrosodimethylamine
0.207 0.0772 ug/L 04/18/23 13:20 04/21/23 15:39 1NDN-Nitrosodi-n-propylamine
0.207 0.0598 ug/L 04/18/23 13:20 04/21/23 15:39 1NDPhenanthrene
0.207 0.0587 ug/L 04/18/23 13:20 04/21/23 15:39 1NDPyrene
5.43 0.921 ug/L 04/18/23 13:20 04/21/23 15:39 1NDPentachlorophenol
1.09 0.529 ug/L 04/18/23 13:20 04/21/23 15:39 1NDPhenol
1.09 0.142 ug/L 04/18/23 13:20 04/21/23 15:39 1ND1,2,4-Trichlorobenzene
0.207 0.0554 ug/L 04/18/23 13:20 04/21/23 15:39 1ND2,4-Dichlorophenol
10.9 1.66 ug/L 04/18/23 13:20 04/21/23 15:39 1ND2,4-Dinitrophenol
1.09 0.182 ug/L 04/18/23 13:20 04/21/23 15:39 1ND2,4-Dimethylphenol
1.09 0.243 ug/L 04/18/23 13:20 04/21/23 15:39 1ND2,4,6-Trichlorophenol
1.09 0.140 ug/L 04/18/23 13:20 04/21/23 15:39 1ND2-Chlorophenol
1.09 0.210 ug/L 04/18/23 13:20 04/21/23 15:39 1ND2-Nitrophenol
5.43 1.60 ug/L 04/18/23 13:20 04/21/23 15:39 1ND4,6-Dinitro-2-methylphenol
1.09 0.302 ug/L 04/18/23 13:20 04/21/23 15:39 1ND4-Chloro-3-methylphenol
5.43 1.02 ug/L 04/18/23 13:20 04/21/23 15:39 1ND4-Nitrophenol
1.09 0.207 ug/L 04/18/23 13:20 04/21/23 15:39 1NDDibenzofuran
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-6Client Sample ID: TMW-2
Matrix: WaterDate Collected: 04/12/23 13:30
Date Received: 04/13/23 09:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.207 0.0674 ug/L 04/18/23 13:20 04/21/23 15:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2-Methylnaphthalene
1.09 0.404 ug/L 04/18/23 13:20 04/21/23 15:39 1ND4-Methylphenol
1.09 0.108 ug/L 04/18/23 13:20 04/21/23 15:39 1ND1,3-Dichlorobenzene
1.09 0.326 ug/L 04/18/23 13:20 04/21/23 15:39 1ND2-Methylphenol
0.207 0.0609 ug/L 04/18/23 13:20 04/21/23 15:39 1ND1-Methylnaphthalene
1.09 0.103 ug/L 04/18/23 13:20 04/21/23 15:39 1ND1,2-Dichlorobenzene
1.09 0.409 ug/L 04/18/23 13:20 04/21/23 15:39 1ND4-Chloroaniline
1.09 0.177 ug/L 04/18/23 13:20 04/21/23 15:39 1NDBenzyl alcohol
1.09 0.0663 ug/L 04/18/23 13:20 04/21/23 15:39 1ND1,4-Dichlorobenzene
2,4,6-Tribromophenol (Surr)59 32-127 04/18/23 13:20 04/21/23 15:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 51 04/18/23 13:20 04/21/23 15:39 147-107
2-Fluorophenol (Surr)66 04/18/23 13:20 04/21/23 15:39 135-109
Nitrobenzene-d5 (Surr)64 04/18/23 13:20 04/21/23 15:39 147-110
Phenol-d5 (Surr)62 04/18/23 13:20 04/21/23 15:39 137-110
Terphenyl-d14 (Surr)56 04/18/23 13:20 04/21/23 15:39 132-115
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-7Client Sample ID: TMW-2
Matrix: WaterDate Collected: 04/12/23 13:45
Date Received: 04/13/23 09:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 04/24/23 18:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 04/24/23 18:39 1ND*+1,3-Dichlorobenzene
1.00 0.544 ug/L 04/24/23 18:39 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 04/24/23 18:39 1NDBenzene
1.00 0.501 ug/L 04/24/23 18:39 1ND*+Chlorobenzene
1.00 0.507 ug/L 04/24/23 18:39 1NDEthylbenzene
1.00 0.457 ug/L 04/24/23 18:39 1NDToluene
1.00 0.406 ug/L 04/24/23 18:39 1NDo-Xylene
1.00 0.482 ug/L 04/24/23 18:39 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 04/24/23 18:39 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)87 26-156 04/24/23 18:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)87 04/24/23 18:39 136-124
Dibromofluoromethane (Surr)114 04/24/23 18:39 146-149
Toluene-d8 (Surr)107 04/24/23 18:39 140-146
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-8Client Sample ID: TMW-2
Matrix: WaterDate Collected: 04/12/23 13:50
Date Received: 04/13/23 09:30
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 20.0 ug/L 04/27/23 10:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 25.0 ug/L 04/24/23 15:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 04/24/23 15:20 1NDC9-C10 Aromatics
100 25.0 ug/L 04/24/23 15:20 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 04/24/23 15:20 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 04/24/23 15:20 1NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)108 70-130 04/24/23 15:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)99 04/24/23 15:20 170-130
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-9Client Sample ID: TMW-3
Matrix: WaterDate Collected: 04/12/23 14:45
Date Received: 04/13/23 09:30
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 20.0 ug/L 04/27/23 10:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 25.0 ug/L 04/24/23 16:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 04/24/23 16:01 1NDC9-C10 Aromatics
100 25.0 ug/L 04/24/23 16:01 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 04/24/23 16:01 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 04/24/23 16:01 1NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)105 70-130 04/24/23 16:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)97 04/24/23 16:01 170-130
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-10Client Sample ID: TMW-3
Matrix: WaterDate Collected: 04/12/23 15:30
Date Received: 04/13/23 09:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 04/24/23 20:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 04/24/23 20:05 1ND*+1,3-Dichlorobenzene
1.00 0.544 ug/L 04/24/23 20:05 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 04/24/23 20:05 1NDBenzene
1.00 0.501 ug/L 04/24/23 20:05 1ND*+Chlorobenzene
1.00 0.507 ug/L 04/24/23 20:05 1NDEthylbenzene
1.00 0.457 ug/L 04/24/23 20:05 1NDToluene
1.00 0.406 ug/L 04/24/23 20:05 1NDo-Xylene
1.00 0.482 ug/L 04/24/23 20:05 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 04/24/23 20:05 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)92 26-156 04/24/23 20:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)87 04/24/23 20:05 136-124
Dibromofluoromethane (Surr)118 04/24/23 20:05 146-149
Toluene-d8 (Surr)104 04/24/23 20:05 140-146
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-11Client Sample ID: TMW-3
Matrix: WaterDate Collected: 04/12/23 15:40
Date Received: 04/13/23 09:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.198 0.0677 ug/L 04/18/23 13:20 04/21/23 16:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.198 0.0677 ug/L 04/18/23 13:20 04/21/23 16:02 1NDAcenaphthylene
0.198 0.0510 ug/L 04/18/23 13:20 04/21/23 16:02 1NDAnthracene
0.198 0.0781 ug/L 04/18/23 13:20 04/21/23 16:02 1NDBenzo[a]anthracene
0.198 0.0552 ug/L 04/18/23 13:20 04/21/23 16:02 1NDBenzo[a]pyrene
0.198 0.101 ug/L 04/18/23 13:20 04/21/23 16:02 1NDBenzo[b]fluoranthene
0.198 0.0719 ug/L 04/18/23 13:20 04/21/23 16:02 1NDBenzo[g,h,i]perylene
0.198 0.0917 ug/L 04/18/23 13:20 04/21/23 16:02 1NDBenzo[k]fluoranthene
1.04 0.158 ug/L 04/18/23 13:20 04/21/23 16:02 1NDBis(2-chloroethoxy)methane
0.198 0.0417 ug/L 04/18/23 13:20 04/21/23 16:02 1NDBis(2-chloroethyl)ether
0.198 0.0604 ug/L 04/18/23 13:20 04/21/23 16:02 1ND2,2'-oxybis[1-chloropropane]
10.4 6.49 ug/L 04/18/23 13:20 04/21/23 16:02 1NDBis(2-ethylhexyl) phthalate
1.04 0.332 ug/L 04/18/23 13:20 04/21/23 16:02 1ND4-Bromophenyl phenyl ether
1.04 0.481 ug/L 04/18/23 13:20 04/21/23 16:02 1NDButyl benzyl phthalate
0.198 0.0615 ug/L 04/18/23 13:20 04/21/23 16:02 1ND2-Chloronaphthalene
1.04 0.230 ug/L 04/18/23 13:20 04/21/23 16:02 1ND4-Chlorophenyl phenyl ether
0.198 0.0844 ug/L 04/18/23 13:20 04/21/23 16:02 1NDChrysene
0.198 0.0750 ug/L 04/18/23 13:20 04/21/23 16:02 1NDDibenz(a,h)anthracene
1.04 0.607 ug/L 04/18/23 13:20 04/21/23 16:02 1ND3,3'-Dichlorobenzidine
1.04 0.591 ug/L 04/18/23 13:20 04/21/23 16:02 1NDDiethyl phthalate
1.04 0.714 ug/L 04/18/23 13:20 04/21/23 16:02 1NDDi-n-octyl phthalate
1.04 0.204 ug/L 04/18/23 13:20 04/21/23 16:02 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.198 0.0625 ug/L 04/18/23 13:20 04/21/23 16:02 1NDFluoranthene
0.198 0.0719 ug/L 04/18/23 13:20 04/21/23 16:02 1NDFluorene
0.198 0.0583 ug/L 04/18/23 13:20 04/21/23 16:02 1NDHexachlorobenzene
0.198 0.0719 ug/L 04/18/23 13:20 04/21/23 16:02 1NDHexachlorobutadiene
1.04 0.518 ug/L 04/18/23 13:20 04/21/23 16:02 1NDHexachlorocyclopentadiene
1.04 0.139 ug/L 04/18/23 13:20 04/21/23 16:02 1NDHexachloroethane
0.198 0.0885 ug/L 04/18/23 13:20 04/21/23 16:02 1NDIndeno[1,2,3-cd]pyrene
1.04 0.196 ug/L 04/18/23 13:20 04/21/23 16:02 1NDIsophorone
0.198 0.0615 ug/L 04/18/23 13:20 04/21/23 16:02 1NDNaphthalene
2.08 0.521 ug/L 04/18/23 13:20 04/21/23 16:02 1NDNitrobenzene
1.04 0.0698 ug/L 04/18/23 13:20 04/21/23 16:02 1NDN-Nitrosodimethylamine
0.198 0.0740 ug/L 04/18/23 13:20 04/21/23 16:02 1NDN-Nitrosodi-n-propylamine
0.198 0.0573 ug/L 04/18/23 13:20 04/21/23 16:02 1NDPhenanthrene
0.198 0.0563 ug/L 04/18/23 13:20 04/21/23 16:02 1NDPyrene
5.21 0.882 ug/L 04/18/23 13:20 04/21/23 16:02 1NDPentachlorophenol
1.04 0.507 ug/L 04/18/23 13:20 04/21/23 16:02 1NDPhenol
1.04 0.136 ug/L 04/18/23 13:20 04/21/23 16:02 1ND1,2,4-Trichlorobenzene
0.198 0.0531 ug/L 04/18/23 13:20 04/21/23 16:02 1ND2,4-Dichlorophenol
10.4 1.59 ug/L 04/18/23 13:20 04/21/23 16:02 1ND2,4-Dinitrophenol
1.04 0.174 ug/L 04/18/23 13:20 04/21/23 16:02 1ND2,4-Dimethylphenol
1.04 0.233 ug/L 04/18/23 13:20 04/21/23 16:02 1ND2,4,6-Trichlorophenol
1.04 0.134 ug/L 04/18/23 13:20 04/21/23 16:02 1ND2-Chlorophenol
1.04 0.201 ug/L 04/18/23 13:20 04/21/23 16:02 1ND2-Nitrophenol
5.21 1.53 ug/L 04/18/23 13:20 04/21/23 16:02 1ND4,6-Dinitro-2-methylphenol
1.04 0.290 ug/L 04/18/23 13:20 04/21/23 16:02 1ND4-Chloro-3-methylphenol
5.21 0.979 ug/L 04/18/23 13:20 04/21/23 16:02 1ND4-Nitrophenol
1.04 0.198 ug/L 04/18/23 13:20 04/21/23 16:02 1NDDibenzofuran
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-11Client Sample ID: TMW-3
Matrix: WaterDate Collected: 04/12/23 15:40
Date Received: 04/13/23 09:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.198 0.0646 ug/L 04/18/23 13:20 04/21/23 16:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2-Methylnaphthalene
1.04 0.388 ug/L 04/18/23 13:20 04/21/23 16:02 1ND4-Methylphenol
1.04 0.103 ug/L 04/18/23 13:20 04/21/23 16:02 1ND1,3-Dichlorobenzene
1.04 0.313 ug/L 04/18/23 13:20 04/21/23 16:02 1ND2-Methylphenol
0.198 0.0583 ug/L 04/18/23 13:20 04/21/23 16:02 1ND1-Methylnaphthalene
1.04 0.0990 ug/L 04/18/23 13:20 04/21/23 16:02 1ND1,2-Dichlorobenzene
1.04 0.392 ug/L 04/18/23 13:20 04/21/23 16:02 1ND4-Chloroaniline
1.04 0.170 ug/L 04/18/23 13:20 04/21/23 16:02 1NDBenzyl alcohol
1.04 0.0635 ug/L 04/18/23 13:20 04/21/23 16:02 1ND1,4-Dichlorobenzene
2,4,6-Tribromophenol (Surr)60 32-127 04/18/23 13:20 04/21/23 16:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 55 04/18/23 13:20 04/21/23 16:02 147-107
2-Fluorophenol (Surr)70 04/18/23 13:20 04/21/23 16:02 135-109
Nitrobenzene-d5 (Surr)65 04/18/23 13:20 04/21/23 16:02 147-110
Phenol-d5 (Surr)65 04/18/23 13:20 04/21/23 16:02 137-110
Terphenyl-d14 (Surr)57 04/18/23 13:20 04/21/23 16:02 132-115
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Client Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-155027-12Client Sample ID: TMW-3
Matrix: WaterDate Collected: 04/12/23 15:10
Date Received: 04/13/23 09:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 42.8 42.8 ug/L 04/20/23 21:54 05/01/23 22:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
42.8 42.8 ug/L 04/20/23 21:54 05/01/23 22:40 1NDC11-C22 Aromatics (Adjusted)
53.5 53.5 ug/L 04/20/23 21:54 05/01/23 22:40 1NDC19-C36 Aliphatics
32.1 32.1 ug/L 04/20/23 21:54 05/01/23 22:40 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)36 S1-40-140 04/20/23 21:54 05/01/23 22:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)74 04/20/23 21:54 05/01/23 22:40 140-140
o- terphenyl (Surr)58 04/20/23 21:54 05/01/23 22:40 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 05/03/23 14:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 180-433155/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433155
RL MDL
1,2-Dichlorobenzene ND 1.00 0.364 ug/L 04/24/23 09:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.5041.00 ug/L 04/24/23 09:21 11,3-Dichlorobenzene
ND 0.5441.00 ug/L 04/24/23 09:21 11,4-Dichlorobenzene
ND 0.5961.00 ug/L 04/24/23 09:21 1Benzene
ND 0.5011.00 ug/L 04/24/23 09:21 1Chlorobenzene
ND 0.5071.00 ug/L 04/24/23 09:21 1Ethylbenzene
ND 0.4571.00 ug/L 04/24/23 09:21 1Toluene
ND 0.4061.00 ug/L 04/24/23 09:21 1o-Xylene
ND 0.4821.00 ug/L 04/24/23 09:21 1m-Xylene & p-Xylene
ND 0.8902.00 ug/L 04/24/23 09:21 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)89 26-156 04/24/23 09:21 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
88 04/24/23 09:21 14-Bromofluorobenzene (Surr)36-124
118 04/24/23 09:21 1Dibromofluoromethane (Surr)46-149
103 04/24/23 09:21 1Toluene-d8 (Surr)40-146
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-433155/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433155
1,2-Dichlorobenzene 10.0 9.355 ug/L 94 64-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,3-Dichlorobenzene 10.0 12.57 *+ug/L 126 63-123
1,4-Dichlorobenzene 10.0 9.766 ug/L 98 67-118
Benzene 10.0 11.67 ug/L 117 68-125
Chlorobenzene 10.0 12.27 *+ug/L 123 68-121
Ethylbenzene 10.0 11.69 ug/L 117 65-126
Toluene 10.0 10.69 ug/L 107 69-124
o-Xylene 10.0 11.71 ug/L 117 64-127
m-Xylene & p-Xylene 10.0 11.50 ug/L 115 66-131
Xylenes, Total 20.0 23.21 ug/L 116 68-124
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
1164-Bromofluorobenzene (Surr)36 -124
122Dibromofluoromethane (Surr)46 -149
118Toluene-d8 (Surr)40 -146
Client Sample ID: Matrix SpikeLab Sample ID: 180-155273-F-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433155
1,2-Dichlorobenzene ND 10.0 9.126 ug/L 91 64-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,3-Dichlorobenzene ND *+10.0 11.71 ug/L 117 63-123
1,4-Dichlorobenzene ND 10.0 8.937 ug/L 89 67-118
Benzene ND 10.0 10.58 ug/L 106 68-125
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-155273-F-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433155
Chlorobenzene ND *+10.0 11.05 ug/L 110 68-121
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Ethylbenzene ND 10.0 10.58 ug/L 106 65-126
Toluene ND 10.0 9.768 ug/L 98 69-124
o-Xylene ND 10.0 10.47 ug/L 105 64-127
m-Xylene & p-Xylene ND 10.0 10.47 ug/L 105 66-131
Xylenes, Total ND 20.0 20.94 ug/L 105 68-124
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
91
MS MS
Qualifier Limits%Recovery
1074-Bromofluorobenzene (Surr)36 -124
111Dibromofluoromethane (Surr)46 -149
110Toluene-d8 (Surr)40 -146
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-155273-G-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433155
1,2-Dichlorobenzene ND 10.0 10.12 ug/L 101 64-120 10 27
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,3-Dichlorobenzene ND *+10.0 11.33 ug/L 113 63-123 3 27
1,4-Dichlorobenzene ND 10.0 8.789 ug/L 88 67-118 2 24
Benzene ND 10.0 10.20 ug/L 102 68-125 4 24
Chlorobenzene ND *+10.0 11.22 ug/L 112 68-121 2 21
Ethylbenzene ND 10.0 10.71 ug/L 107 65-126 1 22
Toluene ND 10.0 9.947 ug/L 99 69-124 2 23
o-Xylene ND 10.0 10.50 ug/L 105 64-127 0 26
m-Xylene & p-Xylene ND 10.0 10.46 ug/L 105 66-131 0 26
Xylenes, Total ND 20.0 20.96 ug/L 105 68-124 0 24
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
92
MSD MSD
Qualifier Limits%Recovery
1044-Bromofluorobenzene (Surr)36 -124
121Dibromofluoromethane (Surr)46 -149
111Toluene-d8 (Surr)40 -146
Client Sample ID: Matrix SpikeLab Sample ID: 180-155359-G-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433155
1,2-Dichlorobenzene ND F1 200 126.0 F1 ug/L 63 64-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,3-Dichlorobenzene ND *+200 216.6 ug/L 108 63-123
1,4-Dichlorobenzene ND 200 185.0 ug/L 93 67-118
Benzene 56.3 200 256.2 ug/L 100 68-125
Chlorobenzene ND *+200 218.1 ug/L 109 68-121
Ethylbenzene 204 200 432.5 E ug/L 114 65-126
Toluene ND 200 195.6 ug/L 98 69-124
o-Xylene ND 200 220.3 ug/L 110 64-127
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-155359-G-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433155
m-Xylene & p-Xylene 62.0 200 277.6 ug/L 108 66-131
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Xylenes, Total 62.0 400 497.9 ug/L 109 68-124
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
90
MS MS
Qualifier Limits%Recovery
1034-Bromofluorobenzene (Surr)36 -124
120Dibromofluoromethane (Surr)46 -149
109Toluene-d8 (Surr)40 -146
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-155359-I-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 433155
1,2-Dichlorobenzene ND F1 200 126.6 F1 ug/L 63 64-120 0 27
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,3-Dichlorobenzene ND *+200 216.7 ug/L 108 63-123 0 27
1,4-Dichlorobenzene ND 200 186.2 ug/L 93 67-118 1 24
Benzene 56.3 200 262.0 ug/L 103 68-125 2 24
Chlorobenzene ND *+200 214.4 ug/L 107 68-121 2 21
Ethylbenzene 204 200 437.9 E ug/L 117 65-126 1 22
Toluene ND 200 192.9 ug/L 96 69-124 1 23
o-Xylene ND 200 215.4 ug/L 108 64-127 2 26
m-Xylene & p-Xylene 62.0 200 268.2 ug/L 103 66-131 3 26
Xylenes, Total 62.0 400 483.6 ug/L 105 68-124 3 24
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
86
MSD MSD
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)36 -124
119Dibromofluoromethane (Surr)46 -149
107Toluene-d8 (Surr)40 -146
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-432661/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432988 Prep Batch: 432661
RL MDL
Acenaphthene ND 0.190 0.0650 ug/L 04/18/23 13:20 04/21/23 11:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.06500.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Acenaphthylene
ND 0.04900.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Anthracene
ND 0.07500.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Benzo[a]anthracene
ND 0.05300.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Benzo[a]pyrene
ND 0.09700.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Benzo[b]fluoranthene
ND 0.06900.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Benzo[g,h,i]perylene
ND 0.08800.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Benzo[k]fluoranthene
ND 0.1521.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Bis(2-chloroethoxy)methane
ND 0.04000.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Bis(2-chloroethyl)ether
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-432661/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432988 Prep Batch: 432661
RL MDL
2,2'-oxybis[1-chloropropane]ND 0.190 0.0580 ug/L 04/18/23 13:20 04/21/23 11:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 6.2310.0 ug/L 04/18/23 13:20 04/21/23 11:34 1Bis(2-ethylhexyl) phthalate
ND 0.3191.00 ug/L 04/18/23 13:20 04/21/23 11:34 14-Bromophenyl phenyl ether
ND 0.4621.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Butyl benzyl phthalate
ND 0.05900.190 ug/L 04/18/23 13:20 04/21/23 11:34 12-Chloronaphthalene
ND 0.2211.00 ug/L 04/18/23 13:20 04/21/23 11:34 14-Chlorophenyl phenyl ether
ND 0.08100.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Chrysene
ND 0.07200.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Dibenz(a,h)anthracene
ND 0.5831.00 ug/L 04/18/23 13:20 04/21/23 11:34 13,3'-Dichlorobenzidine
ND 0.5671.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Diethyl phthalate
ND 0.6851.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Di-n-octyl phthalate
ND 0.1961.00 ug/L 04/18/23 13:20 04/21/23 11:34 11,2-Diphenylhydrazine(as
Azobenzene)
ND 0.06000.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Fluoranthene
ND 0.06900.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Fluorene
ND 0.05600.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Hexachlorobenzene
ND 0.06900.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Hexachlorobutadiene
ND 0.4971.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Hexachlorocyclopentadiene
ND 0.1331.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Hexachloroethane
ND 0.08500.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Indeno[1,2,3-cd]pyrene
ND 0.1881.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Isophorone
ND 0.05900.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Naphthalene
ND 0.5002.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Nitrobenzene
ND 0.06701.00 ug/L 04/18/23 13:20 04/21/23 11:34 1N-Nitrosodimethylamine
ND 0.07100.190 ug/L 04/18/23 13:20 04/21/23 11:34 1N-Nitrosodi-n-propylamine
ND 0.05500.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Phenanthrene
ND 0.05400.190 ug/L 04/18/23 13:20 04/21/23 11:34 1Pyrene
ND 0.8475.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Pentachlorophenol
ND 0.4871.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Phenol
ND 0.1311.00 ug/L 04/18/23 13:20 04/21/23 11:34 11,2,4-Trichlorobenzene
ND 0.05100.190 ug/L 04/18/23 13:20 04/21/23 11:34 12,4-Dichlorophenol
ND 1.5310.0 ug/L 04/18/23 13:20 04/21/23 11:34 12,4-Dinitrophenol
ND 0.1671.00 ug/L 04/18/23 13:20 04/21/23 11:34 12,4-Dimethylphenol
ND 0.2241.00 ug/L 04/18/23 13:20 04/21/23 11:34 12,4,6-Trichlorophenol
ND 0.1291.00 ug/L 04/18/23 13:20 04/21/23 11:34 12-Chlorophenol
ND 0.1931.00 ug/L 04/18/23 13:20 04/21/23 11:34 12-Nitrophenol
ND 1.475.00 ug/L 04/18/23 13:20 04/21/23 11:34 14,6-Dinitro-2-methylphenol
ND 0.2781.00 ug/L 04/18/23 13:20 04/21/23 11:34 14-Chloro-3-methylphenol
ND 0.9405.00 ug/L 04/18/23 13:20 04/21/23 11:34 14-Nitrophenol
ND 0.1901.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Dibenzofuran
ND 0.06200.190 ug/L 04/18/23 13:20 04/21/23 11:34 12-Methylnaphthalene
ND 0.3721.00 ug/L 04/18/23 13:20 04/21/23 11:34 14-Methylphenol
ND 0.09901.00 ug/L 04/18/23 13:20 04/21/23 11:34 11,3-Dichlorobenzene
ND 0.3001.00 ug/L 04/18/23 13:20 04/21/23 11:34 12-Methylphenol
ND 0.05600.190 ug/L 04/18/23 13:20 04/21/23 11:34 11-Methylnaphthalene
ND 0.09501.00 ug/L 04/18/23 13:20 04/21/23 11:34 11,2-Dichlorobenzene
ND 0.3761.00 ug/L 04/18/23 13:20 04/21/23 11:34 14-Chloroaniline
ND 0.1631.00 ug/L 04/18/23 13:20 04/21/23 11:34 1Benzyl alcohol
ND 0.06101.00 ug/L 04/18/23 13:20 04/21/23 11:34 11,4-Dichlorobenzene
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)79 32-127 04/21/23 11:34 1
MB MB
Surrogate
04/18/23 13:20
Dil FacPreparedAnalyzedQualifierLimits%Recovery
86 04/18/23 13:20 04/21/23 11:34 12-Fluorobiphenyl 47-107
108 04/18/23 13:20 04/21/23 11:34 12-Fluorophenol (Surr)35-109
100 04/18/23 13:20 04/21/23 11:34 1Nitrobenzene-d5 (Surr)47-110
104 04/18/23 13:20 04/21/23 11:34 1Phenol-d5 (Surr)37-110
96 04/18/23 13:20 04/21/23 11:34 1Terphenyl-d14 (Surr)32-115
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432661/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432988 Prep Batch: 432661
Acenaphthene 10.0 7.568 ug/L 76 47-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Acenaphthylene 10.0 8.113 ug/L 81 33-145
Anthracene 10.0 7.807 ug/L 78 27-133
Benzo[a]anthracene 10.0 7.962 ug/L 80 33-143
Benzo[a]pyrene 10.0 7.611 ug/L 76 17-150
Benzo[b]fluoranthene 10.0 7.211 ug/L 72 24-150
Benzo[g,h,i]perylene 10.0 7.720 ug/L 77 10-150
Benzo[k]fluoranthene 10.0 7.061 ug/L 71 11-150
Bis(2-chloroethoxy)methane 10.0 8.295 ug/L 83 33-150
Bis(2-chloroethyl)ether 10.0 8.667 ug/L 87 12-150
2,2'-oxybis[1-chloropropane]10.0 9.379 ug/L 94 36-150
Bis(2-ethylhexyl) phthalate 10.0 9.024 J ug/L 90 10-150
4-Bromophenyl phenyl ether 10.0 7.450 ug/L 74 53-127
Butyl benzyl phthalate 10.0 9.266 ug/L 93 10-150
2-Chloronaphthalene 10.0 7.601 ug/L 76 60-120
4-Chlorophenyl phenyl ether 10.0 7.327 ug/L 73 25-150
Chrysene 10.0 7.378 ug/L 74 17-150
Dibenz(a,h)anthracene 10.0 7.619 ug/L 76 10-150
3,3'-Dichlorobenzidine 10.0 7.277 ug/L 73 10-150
Diethyl phthalate 10.0 8.103 ug/L 81 10-120
Di-n-octyl phthalate 10.0 9.673 ug/L 97 10-146
1,2-Diphenylhydrazine(as
Azobenzene)
10.0 9.776 ug/L 98 43-105
Fluoranthene 10.0 7.722 ug/L 77 26-137
Fluorene 10.0 7.675 ug/L 77 59-121
Hexachlorobenzene 10.0 7.315 ug/L 73 10-150
Hexachlorobutadiene 10.0 6.876 ug/L 69 24-120
Hexachlorocyclopentadiene 10.0 6.795 ug/L 68 37-121
Hexachloroethane 10.0 8.203 ug/L 82 40-120
Indeno[1,2,3-cd]pyrene 10.0 7.982 ug/L 80 10-150
Isophorone 10.0 9.281 ug/L 93 21-150
Naphthalene 10.0 7.392 ug/L 74 21-133
Nitrobenzene 10.0 8.773 ug/L 88 35-150
N-Nitrosodimethylamine 10.0 10.21 ug/L 102 33-130
N-Nitrosodi-n-propylamine 10.0 9.906 ug/L 99 10-150
Phenanthrene 10.0 7.383 ug/L 74 54-120
Pyrene 10.0 8.180 ug/L 82 52-120
Pentachlorophenol 20.0 13.12 ug/L 66 14-150
Phenol 10.0 8.990 ug/L 90 10-120
1,2,4-Trichlorobenzene 10.0 7.063 ug/L 71 44-142
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-432661/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432988 Prep Batch: 432661
2,4-Dichlorophenol 10.0 7.955 ug/L 80 39-135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,4-Dinitrophenol 20.0 13.32 ug/L 67 10-150
2,4-Dimethylphenol 10.0 8.445 ug/L 84 32-120
2,4,6-Trichlorophenol 10.0 8.014 ug/L 80 37-144
2-Chlorophenol 10.0 8.682 ug/L 87 23-134
2-Nitrophenol 10.0 8.473 ug/L 85 29-150
4,6-Dinitro-2-methylphenol 20.0 15.00 ug/L 75 10-150
4-Chloro-3-methylphenol 10.0 8.734 ug/L 87 22-147
4-Nitrophenol 20.0 18.61 ug/L 93 10-132
Dibenzofuran 10.0 7.358 ug/L 74 51-100
2-Methylnaphthalene 10.0 7.193 ug/L 72 51-100
4-Methylphenol 10.0 8.874 ug/L 89 47-100
1,3-Dichlorobenzene 10.0 7.693 ug/L 77 51-100
2-Methylphenol 10.0 9.112 ug/L 91 48-100
1-Methylnaphthalene 10.0 7.196 ug/L 72 49-100
1,2-Dichlorobenzene 10.0 7.638 ug/L 76 50-100
4-Chloroaniline 10.0 8.078 ug/L 81 49-100
Benzyl alcohol 10.0 9.058 ug/L 91 30-102
1,4-Dichlorobenzene 10.0 7.751 ug/L 78 51-100
2,4,6-Tribromophenol (Surr)32 -127
Surrogate
81
LCS LCS
Qualifier Limits%Recovery
742-Fluorobiphenyl 47 -107
952-Fluorophenol (Surr)35 -109
90Nitrobenzene-d5 (Surr)47 -110
93Phenol-d5 (Surr)37 -110
78Terphenyl-d14 (Surr)32 -115
Client Sample ID: TMW-1Lab Sample ID: 180-155027-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432988 Prep Batch: 432661
Acenaphthene ND 10.9 5.804 ug/L 53 47-145
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Acenaphthylene ND 10.9 6.274 ug/L 58 35-145
Anthracene ND 10.9 6.557 ug/L 60 27-133
Benzo[a]anthracene ND 10.9 6.960 ug/L 64 33-143
Benzo[a]pyrene ND 10.9 6.667 ug/L 61 17-163
Benzo[b]fluoranthene ND 10.9 6.432 ug/L 59 24-159
Benzo[g,h,i]perylene ND 10.9 7.120 ug/L 66 10-170
Benzo[k]fluoranthene ND 10.9 6.388 ug/L 59 11-162
Bis(2-chloroethoxy)methane ND 10.9 7.212 ug/L 66 33-170
Bis(2-chloroethyl)ether ND 10.9 6.935 ug/L 64 12-158
2,2'-oxybis[1-chloropropane]ND 10.9 7.692 ug/L 71 36-166
Bis(2-ethylhexyl) phthalate ND 10.9 8.868 J ug/L 82 10-158
4-Bromophenyl phenyl ether ND 10.9 6.537 ug/L 60 53-127
Butyl benzyl phthalate ND 10.9 8.535 ug/L 79 10-152
2-Chloronaphthalene ND F1 10.9 6.072 F1 ug/L 56 60-120
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TMW-1Lab Sample ID: 180-155027-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432988 Prep Batch: 432661
4-Chlorophenyl phenyl ether ND 10.9 6.004 ug/L 55 25-158
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Chrysene ND 10.9 6.720 ug/L 62 17-168
Dibenz(a,h)anthracene ND 10.9 6.926 ug/L 64 10-170
3,3'-Dichlorobenzidine ND 10.9 4.935 ug/L 45 10-170
Diethyl phthalate ND 10.9 6.664 ug/L 61 10-120
Di-n-octyl phthalate ND 10.9 8.318 ug/L 77 10-146
1,2-Diphenylhydrazine(as
Azobenzene)
ND 10.9 8.082 ug/L 74 46-103
Fluoranthene ND 10.9 6.894 ug/L 63 26-137
Fluorene ND F1 10.9 6.266 F1 ug/L 58 59-121
Hexachlorobenzene ND 10.9 6.505 ug/L 60 10-152
Hexachlorobutadiene ND 10.9 5.782 ug/L 53 24-120
Hexachlorocyclopentadiene ND 10.9 4.947 ug/L 46 41-106
Hexachloroethane ND 10.9 6.557 ug/L 60 40-120
Indeno[1,2,3-cd]pyrene ND 10.9 7.116 ug/L 65 10-170
Isophorone 0.294 J 10.9 7.909 ug/L 70 21-170
Naphthalene 0.0719 J 10.9 6.146 ug/L 56 21-133
Nitrobenzene ND 10.9 7.496 ug/L 69 35-170
N-Nitrosodimethylamine ND 10.9 7.994 ug/L 74 48-109
N-Nitrosodi-n-propylamine ND 10.9 8.206 ug/L 75 10-170
Phenanthrene ND 10.9 6.561 ug/L 60 54-120
Pyrene ND 10.9 7.278 ug/L 67 52-120
Pentachlorophenol ND 21.7 11.10 ug/L 51 17-170
Phenol ND 10.9 6.533 ug/L 60 10-120
1,2,4-Trichlorobenzene ND 10.9 5.827 ug/L 54 44-142
2,4-Dichlorophenol ND 10.9 6.463 ug/L 59 39-135
2,4-Dinitrophenol ND 21.7 11.71 ug/L 54 10-170
2,4-Dimethylphenol ND 10.9 6.214 ug/L 57 32-120
2,4,6-Trichlorophenol ND 10.9 6.326 ug/L 58 37-144
2-Chlorophenol ND 10.9 6.701 ug/L 62 23-134
2-Nitrophenol ND 10.9 7.299 ug/L 67 29-170
4,6-Dinitro-2-methylphenol ND 21.7 13.17 ug/L 61 10-170
4-Chloro-3-methylphenol ND 10.9 7.324 ug/L 67 22-147
4-Nitrophenol ND 21.7 14.71 ug/L 68 10-132
Dibenzofuran ND F1 10.9 5.974 F1 ug/L 55 57-100
2-Methylnaphthalene ND F1 10.9 6.241 F1 ug/L 57 58-100
4-Methylphenol ND 10.9 6.840 ug/L 63 56-102
1,3-Dichlorobenzene ND F1 10.9 6.197 F1 ug/L 57 60-100
2-Methylphenol ND 10.9 6.692 ug/L 62 55-101
1-Methylnaphthalene ND F1 10.9 6.099 F1 ug/L 56 58-100
1,2-Dichlorobenzene ND F1 10.9 6.064 F1 ug/L 56 60-100
4-Chloroaniline ND 10.9 5.506 ug/L 51 50-100
Benzyl alcohol ND 10.9 7.601 ug/L 70 24-117
1,4-Dichlorobenzene ND F1 10.9 6.090 F1 ug/L 56 60-100
2,4,6-Tribromophenol (Surr)32 -127
Surrogate
64
MS MS
Qualifier Limits%Recovery
642-Fluorobiphenyl 47 -107
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TMW-1Lab Sample ID: 180-155027-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 432988 Prep Batch: 432661
2-Fluorophenol (Surr)35 -109
Surrogate
69
MS MS
Qualifier Limits%Recovery
84Nitrobenzene-d5 (Surr)47 -110
69Phenol-d5 (Surr)37 -110
73Terphenyl-d14 (Surr)32 -115
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-367728/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 367728
RL MDL
C5-C8 Aliphatics (unadjusted)ND 100 25.0 ug/L 04/24/23 12:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10.0100 ug/L 04/24/23 12:30 1C9-C10 Aromatics
ND 25.0100 ug/L 04/24/23 12:30 1C9-C12 Aliphatics (unadjusted)
ND 25.0100 ug/L 04/24/23 12:30 1C9-C12 Aliphatics (adjusted)
ND 25.0100 ug/L 04/24/23 12:30 1C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)106 70-130 04/24/23 12:30 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 04/24/23 12:30 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-367728/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 367728
C5-C8 Aliphatics (unadjusted)151 157.8 ug/L 105 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 50.2 48.49 J ug/L 97 70-130
C9-C12 Aliphatics (unadjusted)151 134.3 ug/L 89 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
109
LCS LCS
Qualifier Limits%Recovery
102a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-367728/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 367728
C5-C8 Aliphatics (unadjusted)151 154.0 ug/L 102 70-130 2 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 50.2 48.08 J ug/L 96 70-130 1 25
C9-C12 Aliphatics (unadjusted)151 139.7 ug/L 93 70-130 4 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
107
LCSD LCSD
Qualifier Limits%Recovery
100a,a,a-Trifluorotoluene (pid)70 -130
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-366862/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 370712 Prep Batch: 366862
RL MDL
C19-C36 Aliphatics ND 50.0 50.0 ug/L 04/20/23 21:54 05/01/23 20:47 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 30.030.0 ug/L 04/20/23 21:54 05/01/23 20:47 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)51 40-140 05/01/23 20:47 1
MB MB
Surrogate
04/20/23 21:54
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-366862/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 370708 Prep Batch: 366862
RL MDL
C11-C22 Aromatics (unadjusted)ND 40.0 40.0 ug/L 04/20/23 21:54 05/01/23 20:47 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 40.040.0 ug/L 04/20/23 21:54 05/01/23 20:47 1C11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)75 40-140 05/01/23 20:47 1
MB MB
Surrogate
04/20/23 21:54
Dil FacPreparedAnalyzedQualifierLimits%Recovery
70 04/20/23 21:54 05/01/23 20:47 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-366862/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 370712 Prep Batch: 366862
C19-C36 Aliphatics 321 213.5 ug/L 66 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 142.0 ug/L 59 40-140
1-Chlorooctadecane (Surr)40 -140
Surrogate
52
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-366862/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 370708 Prep Batch: 366862
C11-C22 Aromatics (unadjusted)681 418.7 ug/L 61 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Fluorobiphenyl (Surr)40 -140
Surrogate
76
LCS LCS
Qualifier Limits%Recovery
65o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-366862/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 370712 Prep Batch: 366862
C19-C36 Aliphatics 321 233.2 ug/L 73 40-140 9 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 241 144.7 ug/L 60 40-140 2 25
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-155027-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-366862/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 370712 Prep Batch: 366862
1-Chlorooctadecane (Surr)40 -140
Surrogate
59
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-366862/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 370708 Prep Batch: 366862
C11-C22 Aromatics (unadjusted)681 438.2 ug/L 64 40-140 5 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)40 -140
Surrogate
78
LCSD LCSD
Qualifier Limits%Recovery
66o- terphenyl (Surr)40 -140
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-155027-1
SDG Number: 640 Rock Lane
Login Number: 155027
Question Answer Comment
Creator: Abernathy, Eric L
List Source: Eurofins Pittsburgh
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-155027-1
SDG Number: 640 Rock Lane
Login Number: 155027
Question Answer Comment
Creator: McCaskey, Jonathan
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 04/15/23 12:38 PMList Number: 2
N/AThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
TrueVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
Eurofins Pittsburgh
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ANALYTICAL REPORT
PREPARED FOR
Attn: Mr. Bruce Stainbrook
Altec Industries, Inc
Bruce Stainbrook
810 Franklin Court, Ste A
Marietta, Georgia 30067
Generated 6/28/2023 3:33:55 PM
JOB DESCRIPTION
China Grove NC
SDG NUMBER 640 Rock Lane
JOB NUMBER
180-157266-1
See page two for job notes and contact information.
Pittsburgh PA 15238
RIDC Park
301 Alpha Drive
Eurofins Pittsburgh
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Eurofins Pittsburgh
Eurofins Pittsburgh is a laboratory within Eurofins Environment Testing Northeast LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
PA Lab ID: 02-00416
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Pittsburgh Project Manager.
Authorization
Generated
6/28/2023 3:33:55 PM
Authorized for release by
Shali Brown, Project Manager II
[e-mail]
[phone]
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Case Narrative
Client: Altec Industries, Inc Job ID: 180-157266-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-157266-1
Laboratory: Eurofins Pittsburgh
Narrative
Job Narrative
180-157266-1
Receipt
The samples were received on 5/31/2023 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 4.8°C
Receipt Exceptions
The following samples were found to be frozen solid upon receipt by the Lancaster laboratory. The samples and containers appeared to
be intact. TMW-1 (180-157266-1), EB-6B (3-5) (180-157266-2), EB-7B (8-10) (180-157266-3), EB-10 (8-10) (180-157266-4), EB-11 (3-5)
(180-157266-5), EB-15 (8-10) (180-157266-6), EB-12 (2-4) (180-157361-1), EB-12 (6-8) (180-157361-2), EB-13 (6-8) (180-157361-3),
EB-14 (8-10) (180-157361-4), EB-16 (2-3) (180-157361-5) and EB-17 (8-10) (180-157361-6)
GC/MS VOA
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-436704 was outside the method criteria for the
following analyte(s): 1,2-Dibromo-3-Chloropropane, 4-Methyl-2-pentanone, Bromoform, Chloroethane and Dichloro-difluoromethane
(LOW). A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As
indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered
estimated.
Method 8260D: The continuing calibration verification (CCV) analyzed in 180-436704 was outside the method criteria for the following
analyte(s): Trichlorofluoromethane and Acetone (HIGH). As indicated in the reference method, sample analysis may proceed; however,
any detection for the affected analyte(s) is considered estimated.
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-436704 was outside the method criteria for the
following analyte(s): Methyl acetate (RF). A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and
found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected
analyte(s) is considered estimated.
Method 8260D_LL: The continuing calibration verification (CCV) analyzed in batch 180-436709 was outside the method criteria for the
following analyte(s): Dichloro-difluoromethane, 4-Methyl-2-pentanone and 1,2-Dibromo-3-Chloropropane.(LOW). A CCV standard at or
below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method,
sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated.
Method 8260D_LL: The continuing calibration verification (CCV) analyzed in 180-436709 was outside the method criteria for the following
analyte(s): 1,1,2-Trichloro-1,2,2-trifluoroethane and Acetone.(HIGH). As indicated in the reference method, sample analysis may proceed;
however, any detection for the affected analyte(s) is considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
Method MAVPH: Surrogate recovery for the following sample was outside control limits: TMW-1 (180-157266-1). Evidence of matrix
interference is confirmed by reanalysis.
Method MAVPH: The method requirement for no headspace was not met. The following volatile sample was analyzed with headspace in
the sample container(s): TMW-1 (180-157266-1).
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Case Narrative
Client: Altec Industries, Inc Job ID: 180-157266-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-157266-1 (Continued)
Laboratory: Eurofins Pittsburgh (Continued)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method MAEPH2.1: The breakthrough for naphthalene is 5% and the breakthrough for 2-methylnaphthalene is 2% in the LCS. The
breakthrough for naphthalene is 4% and the breakthrough for 2-methylnaphthalene is 2% in the LCSD. The method requirement for
breakthrough is 5% or less. TMW-1 (180-157266-1)
Method MAEPH2.1: The breakthrough for naphthalene and 2-methylnaphthalene in the LCS and LCSD is <1%. The method requirement
for breakthrough is <5%. EB-6B (3-5) (180-157266-2), EB-7B (8-10) (180-157266-3), EB-10 (8-10) (180-157266-4), EB-11 (3-5)
(180-157266-5), EB-15 (8-10) (180-157266-6), (180-157266-A-2-C MS) and (180-157266-A-2-D MSD)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Definitions/Glossary
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
F2 MS/MSD RPD exceeds control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
S1+Surrogate recovery exceeds control limits, high biased.
GC Semi VOA
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
S1-Surrogate recovery exceeds control limits, low biased.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Accreditation/Certification Summary
Client: Altec Industries, Inc Job ID: 180-157266-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Laboratory: Eurofins Pittsburgh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 434 12-31-23
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 521 12-31-23
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-1Client Sample ID: TMW-1
Matrix: WaterDate Collected: 05/30/23 15:55
Date Received: 05/31/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 06/01/23 15:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 06/01/23 15:28 1ND1,3-Dichlorobenzene
1.00 0.544 ug/L 06/01/23 15:28 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 06/01/23 15:28 121.4Benzene
1.00 0.501 ug/L 06/01/23 15:28 1NDChlorobenzene
1.00 0.507 ug/L 06/01/23 15:28 1NDEthylbenzene
1.00 0.457 ug/L 06/01/23 15:28 11.36Toluene
1.00 0.406 ug/L 06/01/23 15:28 149.1o-Xylene
1.00 0.482 ug/L 06/01/23 15:28 114.1m-Xylene & p-Xylene
2.00 0.890 ug/L 06/01/23 15:28 163.2Xylenes, Total
1,2-Dichloroethane-d4 (Surr)92 26-156 06/01/23 15:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 06/01/23 15:28 136-124
Dibromofluoromethane (Surr)135 06/01/23 15:28 146-149
Toluene-d8 (Surr)92 06/01/23 15:28 140-146
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND F1 0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 16:48 1NDAcenaphthylene
0.190 0.0490 ug/L 06/05/23 11:58 06/07/23 16:48 1NDAnthracene
1.00 0.0950 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF11,2-Dichlorobenzene
0.190 0.0750 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBenzo[a]anthracene
0.190 0.0530 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBenzo[a]pyrene
1.00 0.0990 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF11,3-Dichlorobenzene
0.190 0.0970 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBenzo[b]fluoranthene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBenzo[g,h,i]perylene
1.00 0.0610 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF11,4-Dichlorobenzene
0.190 0.0880 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBenzo[k]fluoranthene
1.00 0.152 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBis(2-chloroethoxy)methane
0.190 0.0400 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBis(2-chloroethyl)ether
0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 16:48 10.370 F11-Methylnaphthalene
0.190 0.0580 ug/L 06/05/23 11:58 06/07/23 16:48 1ND2,2'-oxybis[1-chloropropane]
10.0 6.23 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBis(2-ethylhexyl) phthalate
1.00 0.319 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF14-Bromophenyl phenyl ether
1.00 0.462 ug/L 06/05/23 11:58 06/07/23 16:48 10.706 JButyl benzyl phthalate
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF12-Chloronaphthalene
1.00 0.221 ug/L 06/05/23 11:58 06/07/23 16:48 1ND4-Chlorophenyl phenyl ether
0.190 0.0810 ug/L 06/05/23 11:58 06/07/23 16:48 1NDChrysene
0.190 0.0720 ug/L 06/05/23 11:58 06/07/23 16:48 1NDDibenz(a,h)anthracene
1.00 0.583 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF13,3'-Dichlorobenzidine
1.00 0.567 ug/L 06/05/23 11:58 06/07/23 16:48 1NDDiethyl phthalate
1.00 0.685 ug/L 06/05/23 11:58 06/07/23 16:48 1NDDi-n-octyl phthalate
1.00 0.196 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF11,2-Diphenylhydrazine(as
Azobenzene)
0.190 0.0620 ug/L 06/05/23 11:58 06/07/23 16:48 10.361 F12-Methylnaphthalene
0.190 0.0600 ug/L 06/05/23 11:58 06/07/23 16:48 1NDFluoranthene
1.00 0.300 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF12-Methylphenol
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF1Fluorene
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-1Client Sample ID: TMW-1
Matrix: WaterDate Collected: 05/30/23 15:55
Date Received: 05/31/23 10:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexachlorobenzene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF1Hexachlorobutadiene
1.00 0.497 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF1Hexachlorocyclopentadiene
1.00 0.133 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF1Hexachloroethane
0.190 0.0850 ug/L 06/05/23 11:58 06/07/23 16:48 1NDIndeno[1,2,3-cd]pyrene
1.00 0.188 ug/L 06/05/23 11:58 06/07/23 16:48 1NDIsophorone
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 16:48 12.15Naphthalene
2.00 0.500 ug/L 06/05/23 11:58 06/07/23 16:48 1NDNitrobenzene
1.00 0.0670 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF1N-Nitrosodimethylamine
0.190 0.0710 ug/L 06/05/23 11:58 06/07/23 16:48 1NDN-Nitrosodi-n-propylamine
1.00 0.376 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF14-Chloroaniline
0.190 0.0550 ug/L 06/05/23 11:58 06/07/23 16:48 10.104 J F1Phenanthrene
0.190 0.0540 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF1Pyrene
1.00 0.372 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF14-Methylphenol
5.00 0.847 ug/L 06/05/23 11:58 06/07/23 16:48 1NDPentachlorophenol
1.00 0.487 ug/L 06/05/23 11:58 06/07/23 16:48 1NDPhenol
1.00 0.131 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF11,2,4-Trichlorobenzene
0.190 0.0510 ug/L 06/05/23 11:58 06/07/23 16:48 1ND2,4-Dichlorophenol
10.0 1.53 ug/L 06/05/23 11:58 06/07/23 16:48 1ND2,4-Dinitrophenol
1.00 0.167 ug/L 06/05/23 11:58 06/07/23 16:48 1ND2,4-Dimethylphenol
1.00 0.224 ug/L 06/05/23 11:58 06/07/23 16:48 1ND2,4,6-Trichlorophenol
1.00 0.129 ug/L 06/05/23 11:58 06/07/23 16:48 1ND2-Chlorophenol
1.00 0.193 ug/L 06/05/23 11:58 06/07/23 16:48 1ND2-Nitrophenol
5.00 1.47 ug/L 06/05/23 11:58 06/07/23 16:48 1ND4,6-Dinitro-2-methylphenol
1.00 0.278 ug/L 06/05/23 11:58 06/07/23 16:48 1ND4-Chloro-3-methylphenol
5.00 0.940 ug/L 06/05/23 11:58 06/07/23 16:48 1ND4-Nitrophenol
5.00 0.923 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBenzoic acid
1.00 0.163 ug/L 06/05/23 11:58 06/07/23 16:48 1NDBenzyl alcohol
1.00 0.190 ug/L 06/05/23 11:58 06/07/23 16:48 1NDF1Dibenzofuran
2,4,6-Tribromophenol (Surr)53 32-127 06/05/23 11:58 06/07/23 16:48 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 64 06/05/23 11:58 06/07/23 16:48 147-107
2-Fluorophenol (Surr)57 06/05/23 11:58 06/07/23 16:48 135-109
Nitrobenzene-d5 (Surr)71 06/05/23 11:58 06/07/23 16:48 147-110
Phenol-d5 (Surr)63 06/05/23 11:58 06/07/23 16:48 137-110
Terphenyl-d14 (Surr)67 06/05/23 11:58 06/07/23 16:48 132-115
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
732 100 20.0 ug/L 06/13/23 12:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
372 100 25.0 ug/L 06/12/23 12:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 06/12/23 12:11 196.7 JC9-C10 Aromatics
100 25.0 ug/L 06/12/23 12:11 1360C9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 06/12/23 12:11 1154C9-C12 Aliphatics (adjusted)
100 25.0 ug/L 06/12/23 12:11 1341C5-C8 Aliphatics (adjusted)
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-1Client Sample ID: TMW-1
Matrix: WaterDate Collected: 05/30/23 15:55
Date Received: 05/31/23 10:30
a,a,a-Trifluorotoluene (fid)163 S1+70-130 06/12/23 12:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)123 06/12/23 12:11 170-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
81.7 42.6 42.6 ug/L 06/09/23 19:11 06/27/23 03:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
42.6 42.6 ug/L 06/09/23 19:11 06/27/23 03:38 165.2C11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)91 40-140 06/09/23 19:11 06/27/23 03:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o- terphenyl (Surr)70 06/09/23 19:11 06/27/23 03:38 140-140
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - RE
RL MDL
ND 53.3 53.3 ug/L 06/09/23 19:11 06/27/23 03:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
32.0 32.0 ug/L 06/09/23 19:11 06/27/23 03:38 152.5C9-C18 Aliphatics
1-Chlorooctadecane (Surr)35 S1-40-140 06/09/23 19:11 06/27/23 03:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
134 100 30.0 ug/L 06/27/23 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-2Client Sample ID: EB-6B (3-5)
Matrix: SolidDate Collected: 05/30/23 15:30
Percent Solids: 72.8Date Received: 05/31/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 6.57 2.19 ug/Kg ☼06/01/23 07:58 06/01/23 19:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
6.57 2.00 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,1,2,2-Tetrachloroethane
6.57 2.63 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
6.57 1.30 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,1,2-Trichloroethane
6.57 2.10 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,1-Dichloroethane
6.57 2.97 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,1-Dichloroethene
6.57 4.24 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,2-Dibromo-3-Chloropropane
6.57 2.21 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,2-Dichlorobenzene
6.57 1.89 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,2-Dichloroethane
6.57 1.75 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,2-Dichloropropane
6.57 3.34 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,2,4-Trichlorobenzene
6.57 4.05 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,3-Dichlorobenzene
6.57 1.97 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,4-Dichlorobenzene
32.9 3.34 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND2-Butanone (MEK)
32.9 2.06 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND2-Hexanone
32.9 2.40 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND4-Methyl-2-pentanone (MIBK)
32.9 5.12 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDAcetone
6.57 1.85 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDBenzene
6.57 3.31 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDBromoform
6.57 3.00 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDBromomethane
6.57 5.26 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDCarbon disulfide
6.57 2.67 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDCarbon tetrachloride
6.57 1.71 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDChlorobenzene
6.57 3.26 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDChlorodibromomethane
6.57 4.40 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDChloroform
6.57 2.60 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDChloromethane
6.57 3.84 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDChloroethane
6.57 1.98 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDcis-1,2-Dichloroethene
6.57 2.90 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDcis-1,3-Dichloropropene
6.57 3.06 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDDichlorobromomethane
6.57 3.27 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDDichlorodifluoromethane
6.57 2.43 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDEthylbenzene
6.57 1.80 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼ND1,2-Dibromoethane
6.57 3.14 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDCyclohexane
6.57 3.42 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDIsopropylbenzene
32.9 9.67 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDMethyl acetate
6.57 1.93 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDMethyl tert-butyl ether
6.57 3.17 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDMethylcyclohexane
6.57 5.93 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDMethylene Chloride
6.57 1.97 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDStyrene
6.57 2.64 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDTetrachloroethene
6.57 1.89 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDToluene
6.57 2.30 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDtrans-1,2-Dichloroethene
6.57 2.96 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDtrans-1,3-Dichloropropene
6.57 2.06 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDTrichloroethene
6.57 5.45 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDTrichlorofluoromethane
6.57 4.73 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDVinyl chloride
13.1 9.47 ug/Kg 06/01/23 07:58 06/01/23 19:23 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-2Client Sample ID: EB-6B (3-5)
Matrix: SolidDate Collected: 05/30/23 15:30
Percent Solids: 72.8Date Received: 05/31/23 10:30
1,2-Dichloroethane-d4 (Surr)100 73-135 06/01/23 07:58 06/01/23 19:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)86 06/01/23 07:58 06/01/23 19:23 160-124
Dibromofluoromethane (Surr)92 06/01/23 07:58 06/01/23 19:23 169-126
Toluene-d8 (Surr)84 06/01/23 07:58 06/01/23 19:23 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 439 162 ug/Kg ☼06/08/23 16:27 06/09/23 16:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
89.1 32.8 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2,2'-oxybis[1-chloropropane]
439 154 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2,4,5-Trichlorophenol
439 148 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2,4,6-Trichlorophenol
89.1 34.2 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2,4-Dichlorophenol
439 149 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2,4-Dimethylphenol
4390 2750 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2,4-Dinitrophenol
439 265 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2,4-Dinitrotoluene
439 173 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2,6-Dinitrotoluene
89.1 20.3 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2-Chloronaphthalene
439 163 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2-Chlorophenol
89.1 21.3 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2-Methylnaphthalene
439 127 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2-Methylphenol
2260 202 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2-Nitroaniline
439 163 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND2-Nitrophenol
439 413 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND3,3'-Dichlorobenzidine
2260 113 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND3-Nitroaniline
2260 764 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND4,6-Dinitro-2-methylphenol
439 189 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND4-Bromophenyl phenyl ether
439 156 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND4-Chloro-3-methylphenol
439 116 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND4-Chloroaniline
439 148 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND4-Chlorophenyl phenyl ether
439 130 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDMethylphenol, 3 & 4
2260 165 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND4-Nitroaniline
2260 311 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼ND4-Nitrophenol
89.1 25.5 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDAcenaphthene
89.1 19.4 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDAcenaphthylene
891 158 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDAcetophenone
89.1 23.0 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDAnthracene
891 194 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDAtrazine
891 55.0 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDBenzaldehyde
89.1 40.0 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDBenzo[a]anthracene
89.1 38.4 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDBenzo[a]pyrene
89.1 21.8 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDBenzo[b]fluoranthene
89.1 19.1 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDBenzo[g,h,i]perylene
89.1 26.6 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDBenzo[k]fluoranthene
439 162 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDBis(2-chloroethoxy)methane
89.1 16.1 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDBis(2-chloroethyl)ether
4390 472 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDBis(2-ethylhexyl) phthalate
439 304 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDButyl benzyl phthalate
2260 288 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDCaprolactam
89.1 20.7 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDCarbazole
89.1 49.2 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDChrysene
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-2Client Sample ID: EB-6B (3-5)
Matrix: SolidDate Collected: 05/30/23 15:30
Percent Solids: 72.8Date Received: 05/31/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 89.1 56.8 ug/Kg ☼06/08/23 16:27 06/09/23 16:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
439 163 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDDibenzofuran
439 156 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDDiethyl phthalate
439 175 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDDimethyl phthalate
439 194 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDDi-n-butyl phthalate
439 258 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDDi-n-octyl phthalate
89.1 23.4 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDFluoranthene
89.1 17.4 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDFluorene
89.1 31.8 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDHexachlorobenzene
89.1 25.9 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDHexachlorobutadiene
439 45.3 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDHexachlorocyclopentadiene
439 157 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDHexachloroethane
89.1 44.1 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDIndeno[1,2,3-cd]pyrene
439 166 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDIsophorone
89.1 17.3 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDNaphthalene
891 162 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDNitrobenzene
89.1 30.0 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDN-Nitrosodi-n-propylamine
439 148 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDN-Nitrosodiphenylamine
2260 712 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDPentachlorophenol
89.1 23.8 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDPhenanthrene
439 134 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDPhenol
89.1 21.0 ug/Kg 06/08/23 16:27 06/09/23 16:20 1☼NDPyrene
2,4,6-Tribromophenol (Surr)62 34-108 06/08/23 16:27 06/09/23 16:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 64 06/08/23 16:27 06/09/23 16:20 144-105
2-Fluorophenol (Surr)65 06/08/23 16:27 06/09/23 16:20 148-105
Nitrobenzene-d5 (Surr)62 06/08/23 16:27 06/09/23 16:20 146-105
Phenol-d5 (Surr)65 06/08/23 16:27 06/09/23 16:20 146-105
Terphenyl-d14 (Surr)76 06/08/23 16:27 06/09/23 16:20 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 6.87 1.72 mg/Kg ☼06/16/23 07:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 26.4 6.59 mg/Kg ☼06/13/23 15:06 06/14/23 17:58 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
26.4 6.59 mg/Kg 06/13/23 15:06 06/14/23 17:58 50☼NDC9-C10 Aromatics
26.4 6.59 mg/Kg 06/13/23 15:06 06/14/23 17:58 50☼NDC9-C12 Aliphatics (unadjusted)
26.4 6.59 mg/Kg 06/13/23 15:06 06/14/23 17:58 50☼NDC9-C12 Aliphatics (adjusted)
26.4 6.59 mg/Kg 06/13/23 15:06 06/14/23 17:58 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)111 70-130 06/13/23 15:06 06/14/23 17:58 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)97 06/13/23 15:06 06/14/23 17:58 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 16.2 16.2 mg/Kg ☼06/06/23 16:31 06/20/23 20:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
16.2 16.2 mg/Kg 06/06/23 16:31 06/20/23 20:45 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-2Client Sample ID: EB-6B (3-5)
Matrix: SolidDate Collected: 05/30/23 15:30
Percent Solids: 72.8Date Received: 05/31/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 16.2 16.2 mg/Kg ☼06/06/23 16:31 06/20/23 20:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.11 8.11 mg/Kg 06/06/23 16:31 06/20/23 20:45 1☼ND F1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)50 40-140 06/06/23 16:31 06/20/23 20:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)71 06/06/23 16:31 06/20/23 20:45 140-140
o- terphenyl (Surr)43 06/06/23 16:31 06/20/23 20:45 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 16.5 16.5 mg/Kg ☼06/27/23 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
27.2 0.1 0.1 %06/05/23 17:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/05/23 17:33 172.8Percent Solids (SM22 2540G)
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-3Client Sample ID: EB-7B (8-10)
Matrix: SolidDate Collected: 05/30/23 15:10
Percent Solids: 65.6Date Received: 05/31/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 6.98 2.33 ug/Kg ☼06/01/23 07:58 06/01/23 19:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
6.98 2.12 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,1,2,2-Tetrachloroethane
6.98 2.79 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
6.98 1.38 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,1,2-Trichloroethane
6.98 2.23 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,1-Dichloroethane
6.98 3.16 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,1-Dichloroethene
6.98 4.51 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,2-Dibromo-3-Chloropropane
6.98 2.35 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,2-Dichlorobenzene
6.98 2.01 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,2-Dichloroethane
6.98 1.86 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,2-Dichloropropane
6.98 3.55 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,2,4-Trichlorobenzene
6.98 4.30 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,3-Dichlorobenzene
6.98 2.09 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,4-Dichlorobenzene
34.9 3.55 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND2-Butanone (MEK)
34.9 2.19 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND2-Hexanone
34.9 2.56 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND4-Methyl-2-pentanone (MIBK)
34.9 5.45 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDAcetone
6.98 1.97 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDBenzene
6.98 3.52 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDBromoform
6.98 3.18 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDBromomethane
6.98 5.59 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDCarbon disulfide
6.98 2.83 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDCarbon tetrachloride
6.98 1.82 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDChlorobenzene
6.98 3.46 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDChlorodibromomethane
6.98 4.68 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDChloroform
6.98 2.76 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDChloromethane
6.98 4.08 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDChloroethane
6.98 2.11 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDcis-1,2-Dichloroethene
6.98 3.09 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDcis-1,3-Dichloropropene
6.98 3.25 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDDichlorobromomethane
6.98 3.48 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDDichlorodifluoromethane
6.98 2.58 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDEthylbenzene
6.98 1.91 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼ND1,2-Dibromoethane
6.98 3.34 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDCyclohexane
6.98 3.63 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDIsopropylbenzene
34.9 10.3 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDMethyl acetate
6.98 2.05 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDMethyl tert-butyl ether
6.98 3.37 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDMethylcyclohexane
6.98 6.30 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDMethylene Chloride
6.98 2.09 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDStyrene
6.98 2.81 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDTetrachloroethene
6.98 2.01 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDToluene
6.98 2.44 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDtrans-1,2-Dichloroethene
6.98 3.14 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDtrans-1,3-Dichloropropene
6.98 2.19 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDTrichloroethene
6.98 5.79 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDTrichlorofluoromethane
6.98 5.03 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDVinyl chloride
14.0 10.1 ug/Kg 06/01/23 07:58 06/01/23 19:46 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-3Client Sample ID: EB-7B (8-10)
Matrix: SolidDate Collected: 05/30/23 15:10
Percent Solids: 65.6Date Received: 05/31/23 10:30
1,2-Dichloroethane-d4 (Surr)98 73-135 06/01/23 07:58 06/01/23 19:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)83 06/01/23 07:58 06/01/23 19:46 160-124
Dibromofluoromethane (Surr)87 06/01/23 07:58 06/01/23 19:46 169-126
Toluene-d8 (Surr)85 06/01/23 07:58 06/01/23 19:46 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 487 180 ug/Kg ☼06/08/23 16:27 06/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
98.9 36.5 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2,2'-oxybis[1-chloropropane]
487 171 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2,4,5-Trichlorophenol
487 164 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2,4,6-Trichlorophenol
98.9 37.9 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2,4-Dichlorophenol
487 165 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2,4-Dimethylphenol
4870 3060 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2,4-Dinitrophenol
487 294 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2,4-Dinitrotoluene
487 192 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2,6-Dinitrotoluene
98.9 22.6 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2-Chloronaphthalene
487 182 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2-Chlorophenol
98.9 23.6 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2-Methylnaphthalene
487 141 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2-Methylphenol
2510 224 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2-Nitroaniline
487 182 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND2-Nitrophenol
487 459 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND3,3'-Dichlorobenzidine
2510 125 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND3-Nitroaniline
2510 849 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND4,6-Dinitro-2-methylphenol
487 210 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND4-Bromophenyl phenyl ether
487 173 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND4-Chloro-3-methylphenol
487 129 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND4-Chloroaniline
487 164 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND4-Chlorophenyl phenyl ether
487 145 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDMethylphenol, 3 & 4
2510 183 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND4-Nitroaniline
2510 345 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼ND4-Nitrophenol
98.9 28.3 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDAcenaphthene
98.9 21.6 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDAcenaphthylene
989 176 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDAcetophenone
98.9 25.5 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDAnthracene
989 216 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDAtrazine
989 61.1 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDBenzaldehyde
98.9 44.4 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDBenzo[a]anthracene
98.9 42.7 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDBenzo[a]pyrene
98.9 24.2 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDBenzo[b]fluoranthene
98.9 21.3 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDBenzo[g,h,i]perylene
98.9 29.5 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDBenzo[k]fluoranthene
487 180 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDBis(2-chloroethoxy)methane
98.9 17.9 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDBis(2-chloroethyl)ether
4870 524 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDBis(2-ethylhexyl) phthalate
487 338 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDButyl benzyl phthalate
2510 320 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDCaprolactam
98.9 23.0 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDCarbazole
98.9 54.6 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDChrysene
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-3Client Sample ID: EB-7B (8-10)
Matrix: SolidDate Collected: 05/30/23 15:10
Percent Solids: 65.6Date Received: 05/31/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 98.9 63.0 ug/Kg ☼06/08/23 16:27 06/12/23 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
487 182 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDDibenzofuran
487 173 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDDiethyl phthalate
487 195 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDDimethyl phthalate
487 216 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDDi-n-butyl phthalate
487 286 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDDi-n-octyl phthalate
98.9 26.0 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDFluoranthene
98.9 19.3 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDFluorene
98.9 35.3 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDHexachlorobenzene
98.9 28.8 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDHexachlorobutadiene
487 50.3 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDHexachlorocyclopentadiene
487 174 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDHexachloroethane
98.9 49.0 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDIndeno[1,2,3-cd]pyrene
487 185 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDIsophorone
98.9 19.2 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDNaphthalene
989 180 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDNitrobenzene
98.9 33.4 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDN-Nitrosodi-n-propylamine
487 164 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDN-Nitrosodiphenylamine
2510 791 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDPentachlorophenol
98.9 26.4 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDPhenanthrene
487 149 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDPhenol
98.9 23.3 ug/Kg 06/08/23 16:27 06/12/23 10:59 1☼NDPyrene
2,4,6-Tribromophenol (Surr)59 34-108 06/08/23 16:27 06/12/23 10:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 74 06/08/23 16:27 06/12/23 10:59 144-105
2-Fluorophenol (Surr)64 06/08/23 16:27 06/12/23 10:59 148-105
Nitrobenzene-d5 (Surr)84 06/08/23 16:27 06/12/23 10:59 146-105
Phenol-d5 (Surr)73 06/08/23 16:27 06/12/23 10:59 146-105
Terphenyl-d14 (Surr)76 06/08/23 16:27 06/12/23 10:59 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.63 1.91 mg/Kg ☼06/16/23 07:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 27.7 6.92 mg/Kg ☼06/13/23 15:06 06/14/23 18:39 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
27.7 6.92 mg/Kg 06/13/23 15:06 06/14/23 18:39 50☼NDC9-C10 Aromatics
27.7 6.92 mg/Kg 06/13/23 15:06 06/14/23 18:39 50☼NDC9-C12 Aliphatics (unadjusted)
27.7 6.92 mg/Kg 06/13/23 15:06 06/14/23 18:39 50☼NDC9-C12 Aliphatics (adjusted)
27.7 6.92 mg/Kg 06/13/23 15:06 06/14/23 18:39 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)116 70-130 06/13/23 15:06 06/14/23 18:39 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)101 06/13/23 15:06 06/14/23 18:39 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.0 18.0 mg/Kg ☼06/06/23 16:31 06/20/23 21:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
18.0 18.0 mg/Kg 06/06/23 16:31 06/20/23 21:52 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-3Client Sample ID: EB-7B (8-10)
Matrix: SolidDate Collected: 05/30/23 15:10
Percent Solids: 65.6Date Received: 05/31/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
25.0 18.0 18.0 mg/Kg ☼06/06/23 16:31 06/20/23 21:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
9.00 9.00 mg/Kg 06/06/23 16:31 06/20/23 21:52 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)61 40-140 06/06/23 16:31 06/20/23 21:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)72 06/06/23 16:31 06/20/23 21:52 140-140
o- terphenyl (Surr)53 06/06/23 16:31 06/20/23 21:52 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
25.0 18.3 18.3 mg/Kg ☼06/27/23 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
34.4 0.1 0.1 %06/05/23 17:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/05/23 17:33 165.6Percent Solids (SM22 2540G)
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-4Client Sample ID: EB-10 (8-10)
Matrix: SolidDate Collected: 05/30/23 13:35
Percent Solids: 62.5Date Received: 05/31/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
5.86 J 7.64 2.55 ug/Kg ☼06/02/23 07:05 06/02/23 14:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.64 2.32 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,1,2,2-Tetrachloroethane
7.64 3.06 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
7.64 1.51 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,1,2-Trichloroethane
7.64 2.44 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,1-Dichloroethane
7.64 3.45 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,1-Dichloroethene
7.64 4.94 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,2-Dibromo-3-Chloropropane
7.64 2.57 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,2-Dichlorobenzene
7.64 2.20 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,2-Dichloroethane
7.64 2.03 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,2-Dichloropropane
7.64 3.88 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,2,4-Trichlorobenzene
7.64 4.71 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,3-Dichlorobenzene
7.64 2.29 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,4-Dichlorobenzene
38.2 3.88 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND2-Butanone (MEK)
38.2 2.40 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND2-Hexanone
38.2 2.80 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND4-Methyl-2-pentanone (MIBK)
38.2 5.96 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDAcetone
7.64 2.15 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDBenzene
7.64 3.85 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDBromoform
7.64 3.48 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDBromomethane
7.64 6.11 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDCarbon disulfide
7.64 3.10 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDCarbon tetrachloride
7.64 1.99 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDChlorobenzene
7.64 3.79 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDChlorodibromomethane
7.64 5.12 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDChloroform
7.64 3.03 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDChloromethane
7.64 4.46 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDChloroethane
7.64 2.31 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDcis-1,2-Dichloroethene
7.64 3.38 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDcis-1,3-Dichloropropene
7.64 3.56 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDDichlorobromomethane
7.64 3.80 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDDichlorodifluoromethane
7.64 2.83 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDEthylbenzene
7.64 2.09 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼ND1,2-Dibromoethane
7.64 3.65 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDCyclohexane
7.64 3.97 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDIsopropylbenzene
38.2 11.2 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDMethyl acetate
7.64 2.25 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDMethyl tert-butyl ether
7.64 3.68 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDMethylcyclohexane
7.64 6.89 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDMethylene Chloride
7.64 2.29 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDStyrene
7.64 3.07 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDTetrachloroethene
7.64 2.20 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDToluene
7.64 2.67 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDtrans-1,2-Dichloroethene
7.64 3.44 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDtrans-1,3-Dichloropropene
7.64 2.40 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDTrichloroethene
7.64 6.34 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDTrichlorofluoromethane
7.64 5.50 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDVinyl chloride
15.3 11.0 ug/Kg 06/02/23 07:05 06/02/23 14:59 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-4Client Sample ID: EB-10 (8-10)
Matrix: SolidDate Collected: 05/30/23 13:35
Percent Solids: 62.5Date Received: 05/31/23 10:30
1,2-Dichloroethane-d4 (Surr)98 73-135 06/02/23 07:05 06/02/23 14:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)91 06/02/23 07:05 06/02/23 14:59 160-124
Dibromofluoromethane (Surr)95 06/02/23 07:05 06/02/23 14:59 169-126
Toluene-d8 (Surr)90 06/02/23 07:05 06/02/23 14:59 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 514 190 ug/Kg ☼06/08/23 16:27 06/09/23 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
104 38.5 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2,2'-oxybis[1-chloropropane]
514 181 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2,4,5-Trichlorophenol
514 173 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2,4,6-Trichlorophenol
104 40.0 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2,4-Dichlorophenol
514 174 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2,4-Dimethylphenol
5140 3220 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2,4-Dinitrophenol
514 310 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2,4-Dinitrotoluene
514 202 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2,6-Dinitrotoluene
104 23.8 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2-Chloronaphthalene
514 192 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2-Chlorophenol
104 24.9 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2-Methylnaphthalene
514 149 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2-Methylphenol
2650 237 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2-Nitroaniline
514 192 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND2-Nitrophenol
514 484 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND3,3'-Dichlorobenzidine
2650 132 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND3-Nitroaniline
2650 896 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND4,6-Dinitro-2-methylphenol
514 221 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND4-Bromophenyl phenyl ether
514 182 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND4-Chloro-3-methylphenol
514 136 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND4-Chloroaniline
514 173 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND4-Chlorophenyl phenyl ether
514 152 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDMethylphenol, 3 & 4
2650 193 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND4-Nitroaniline
2650 364 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼ND4-Nitrophenol
104 29.9 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDAcenaphthene
104 22.7 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDAcenaphthylene
1040 185 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDAcetophenone
104 26.9 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDAnthracene
1040 227 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDAtrazine
1040 64.5 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDBenzaldehyde
104 46.9 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDBenzo[a]anthracene
104 45.0 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDBenzo[a]pyrene
104 25.5 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDBenzo[b]fluoranthene
104 22.4 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDBenzo[g,h,i]perylene
104 31.1 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDBenzo[k]fluoranthene
514 190 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDBis(2-chloroethoxy)methane
104 18.8 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDBis(2-chloroethyl)ether
5140 553 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDBis(2-ethylhexyl) phthalate
514 357 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDButyl benzyl phthalate
2650 338 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDCaprolactam
104 24.3 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDCarbazole
104 57.6 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDChrysene
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-4Client Sample ID: EB-10 (8-10)
Matrix: SolidDate Collected: 05/30/23 13:35
Percent Solids: 62.5Date Received: 05/31/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 104 66.5 ug/Kg ☼06/08/23 16:27 06/09/23 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
514 192 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDDibenzofuran
514 182 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDDiethyl phthalate
514 206 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDDimethyl phthalate
514 227 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDDi-n-butyl phthalate
514 302 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDDi-n-octyl phthalate
104 27.4 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDFluoranthene
104 20.4 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDFluorene
104 37.2 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDHexachlorobenzene
104 30.4 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDHexachlorobutadiene
514 53.1 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDHexachlorocyclopentadiene
514 184 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDHexachloroethane
104 51.7 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDIndeno[1,2,3-cd]pyrene
514 195 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDIsophorone
104 20.2 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDNaphthalene
1040 190 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDNitrobenzene
104 35.2 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDN-Nitrosodi-n-propylamine
514 173 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDN-Nitrosodiphenylamine
2650 835 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDPentachlorophenol
104 27.9 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDPhenanthrene
514 157 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDPhenol
104 24.6 ug/Kg 06/08/23 16:27 06/09/23 17:05 1☼NDPyrene
2,4,6-Tribromophenol (Surr)67 34-108 06/08/23 16:27 06/09/23 17:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 65 06/08/23 16:27 06/09/23 17:05 144-105
2-Fluorophenol (Surr)67 06/08/23 16:27 06/09/23 17:05 148-105
Nitrobenzene-d5 (Surr)65 06/08/23 16:27 06/09/23 17:05 146-105
Phenol-d5 (Surr)63 06/08/23 16:27 06/09/23 17:05 146-105
Terphenyl-d14 (Surr)78 06/08/23 16:27 06/09/23 17:05 139-105
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 19.0 19.0 mg/Kg ☼06/06/23 16:31 06/20/23 22:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
19.0 19.0 mg/Kg 06/06/23 16:31 06/20/23 22:14 1☼NDC11-C22 Aromatics (Adjusted)
19.0 19.0 mg/Kg 06/06/23 16:31 06/20/23 22:14 1☼NDC19-C36 Aliphatics
9.52 9.52 mg/Kg 06/06/23 16:31 06/20/23 22:14 1☼15.1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)59 40-140 06/06/23 16:31 06/20/23 22:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)78 06/06/23 16:31 06/20/23 22:14 140-140
o- terphenyl (Surr)56 06/06/23 16:31 06/20/23 22:14 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 19.2 19.2 mg/Kg ☼06/27/23 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
37.5 0.1 0.1 %06/05/23 17:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/05/23 17:33 162.5Percent Solids (SM22 2540G)
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-5Client Sample ID: EB-11 (3-5)
Matrix: SolidDate Collected: 05/30/23 14:15
Percent Solids: 66.0Date Received: 05/31/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.41 2.47 ug/Kg ☼06/02/23 07:05 06/02/23 15:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.41 2.25 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,1,2,2-Tetrachloroethane
7.41 2.96 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
7.41 1.47 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,1,2-Trichloroethane
7.41 2.37 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,1-Dichloroethane
7.41 3.35 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,1-Dichloroethene
7.41 4.79 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,2-Dibromo-3-Chloropropane
7.41 2.49 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,2-Dichlorobenzene
7.41 2.13 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,2-Dichloroethane
7.41 1.97 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,2-Dichloropropane
7.41 3.76 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,2,4-Trichlorobenzene
7.41 4.56 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,3-Dichlorobenzene
7.41 2.22 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,4-Dichlorobenzene
37.0 3.76 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND2-Butanone (MEK)
37.0 2.33 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND2-Hexanone
37.0 2.71 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND4-Methyl-2-pentanone (MIBK)
37.0 5.78 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDAcetone
7.41 2.09 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDBenzene
7.41 3.73 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDBromoform
7.41 3.38 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDBromomethane
7.41 5.93 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDCarbon disulfide
7.41 3.01 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDCarbon tetrachloride
7.41 1.93 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDChlorobenzene
7.41 3.67 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDChlorodibromomethane
7.41 4.96 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDChloroform
7.41 2.93 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDChloromethane
7.41 4.33 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDChloroethane
7.41 2.24 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDcis-1,2-Dichloroethene
7.41 3.27 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDcis-1,3-Dichloropropene
7.41 3.45 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDDichlorobromomethane
7.41 3.69 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDDichlorodifluoromethane
7.41 2.74 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDEthylbenzene
7.41 2.03 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼ND1,2-Dibromoethane
7.41 3.54 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDCyclohexane
7.41 3.85 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDIsopropylbenzene
37.0 10.9 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDMethyl acetate
7.41 2.18 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDMethyl tert-butyl ether
7.41 3.57 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDMethylcyclohexane
7.41 6.68 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDMethylene Chloride
7.41 2.22 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDStyrene
7.41 2.98 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDTetrachloroethene
7.41 2.13 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDToluene
7.41 2.59 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDtrans-1,2-Dichloroethene
7.41 3.33 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDtrans-1,3-Dichloropropene
7.41 2.33 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDTrichloroethene
7.41 6.15 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDTrichlorofluoromethane
7.41 5.33 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDVinyl chloride
14.8 10.7 ug/Kg 06/02/23 07:05 06/02/23 15:22 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-5Client Sample ID: EB-11 (3-5)
Matrix: SolidDate Collected: 05/30/23 14:15
Percent Solids: 66.0Date Received: 05/31/23 10:30
1,2-Dichloroethane-d4 (Surr)95 73-135 06/02/23 07:05 06/02/23 15:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 06/02/23 07:05 06/02/23 15:22 160-124
Dibromofluoromethane (Surr)98 06/02/23 07:05 06/02/23 15:22 169-126
Toluene-d8 (Surr)95 06/02/23 07:05 06/02/23 15:22 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 497 184 ug/Kg ☼06/08/23 16:27 06/09/23 17:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
101 37.2 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2,2'-oxybis[1-chloropropane]
497 175 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2,4,5-Trichlorophenol
497 167 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2,4,6-Trichlorophenol
101 38.7 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2,4-Dichlorophenol
497 169 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2,4-Dimethylphenol
4970 3120 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2,4-Dinitrophenol
497 300 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2,4-Dinitrotoluene
497 196 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2,6-Dinitrotoluene
101 23.0 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2-Chloronaphthalene
497 185 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2-Chlorophenol
101 24.1 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2-Methylnaphthalene
497 144 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2-Methylphenol
2560 229 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2-Nitroaniline
497 185 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND2-Nitrophenol
497 468 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND3,3'-Dichlorobenzidine
2560 128 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND3-Nitroaniline
2560 866 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND4,6-Dinitro-2-methylphenol
497 214 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND4-Bromophenyl phenyl ether
497 176 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND4-Chloro-3-methylphenol
497 132 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND4-Chloroaniline
497 167 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND4-Chlorophenyl phenyl ether
497 147 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDMethylphenol, 3 & 4
2560 187 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND4-Nitroaniline
2560 352 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼ND4-Nitrophenol
101 28.9 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDAcenaphthene
101 22.0 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDAcenaphthylene
1010 179 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDAcetophenone
101 26.1 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDAnthracene
1010 220 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDAtrazine
1010 62.3 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDBenzaldehyde
101 45.3 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDBenzo[a]anthracene
101 43.5 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDBenzo[a]pyrene
101 24.7 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDBenzo[b]fluoranthene
101 21.7 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDBenzo[g,h,i]perylene
101 30.1 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDBenzo[k]fluoranthene
497 184 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDBis(2-chloroethoxy)methane
101 18.2 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDBis(2-chloroethyl)ether
4970 535 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDBis(2-ethylhexyl) phthalate
497 345 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDButyl benzyl phthalate
2560 327 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDCaprolactam
101 23.5 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDCarbazole
101 55.7 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDChrysene
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-5Client Sample ID: EB-11 (3-5)
Matrix: SolidDate Collected: 05/30/23 14:15
Percent Solids: 66.0Date Received: 05/31/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 101 64.3 ug/Kg ☼06/08/23 16:27 06/09/23 17:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
497 185 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDDibenzofuran
497 176 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDDiethyl phthalate
497 199 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDDimethyl phthalate
497 220 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDDi-n-butyl phthalate
497 292 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDDi-n-octyl phthalate
101 26.5 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDFluoranthene
101 19.7 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDFluorene
101 36.0 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDHexachlorobenzene
101 29.4 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDHexachlorobutadiene
497 51.4 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDHexachlorocyclopentadiene
497 178 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDHexachloroethane
101 50.0 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDIndeno[1,2,3-cd]pyrene
497 188 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDIsophorone
101 19.6 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDNaphthalene
1010 184 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDNitrobenzene
101 34.0 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDN-Nitrosodi-n-propylamine
497 167 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDN-Nitrosodiphenylamine
2560 807 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDPentachlorophenol
101 27.0 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDPhenanthrene
497 152 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDPhenol
101 23.8 ug/Kg 06/08/23 16:27 06/09/23 17:27 1☼NDPyrene
2,4,6-Tribromophenol (Surr)58 34-108 06/08/23 16:27 06/09/23 17:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 62 06/08/23 16:27 06/09/23 17:27 144-105
2-Fluorophenol (Surr)64 06/08/23 16:27 06/09/23 17:27 148-105
Nitrobenzene-d5 (Surr)61 06/08/23 16:27 06/09/23 17:27 146-105
Phenol-d5 (Surr)64 06/08/23 16:27 06/09/23 17:27 146-105
Terphenyl-d14 (Surr)69 06/08/23 16:27 06/09/23 17:27 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.58 1.90 mg/Kg ☼06/16/23 07:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 31.3 7.83 mg/Kg ☼06/13/23 15:06 06/14/23 20:02 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
31.3 7.83 mg/Kg 06/13/23 15:06 06/14/23 20:02 50☼NDC9-C10 Aromatics
31.3 7.83 mg/Kg 06/13/23 15:06 06/14/23 20:02 50☼NDC9-C12 Aliphatics (unadjusted)
31.3 7.83 mg/Kg 06/13/23 15:06 06/14/23 20:02 50☼NDC9-C12 Aliphatics (adjusted)
31.3 7.83 mg/Kg 06/13/23 15:06 06/14/23 20:02 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)119 70-130 06/13/23 15:06 06/14/23 20:02 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)104 06/13/23 15:06 06/14/23 20:02 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.5 17.5 mg/Kg ☼06/06/23 16:31 06/20/23 22:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
17.5 17.5 mg/Kg 06/06/23 16:31 06/20/23 22:36 1☼NDC11-C22 Aromatics (Adjusted)
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-5Client Sample ID: EB-11 (3-5)
Matrix: SolidDate Collected: 05/30/23 14:15
Percent Solids: 66.0Date Received: 05/31/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 17.5 17.5 mg/Kg ☼06/06/23 16:31 06/20/23 22:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.74 8.74 mg/Kg 06/06/23 16:31 06/20/23 22:36 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)62 40-140 06/06/23 16:31 06/20/23 22:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)56 06/06/23 16:31 06/20/23 22:36 140-140
o- terphenyl (Surr)43 06/06/23 16:31 06/20/23 22:36 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.2 18.2 mg/Kg ☼06/27/23 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
34.0 0.1 0.1 %06/05/23 17:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/05/23 17:33 166.0Percent Solids (SM22 2540G)
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-6Client Sample ID: EB-15 (8-10)
Matrix: SolidDate Collected: 05/30/23 16:10
Percent Solids: 70.2Date Received: 05/31/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 6.81 2.27 ug/Kg ☼06/02/23 07:05 06/02/23 15:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
6.81 2.07 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,1,2,2-Tetrachloroethane
6.81 2.72 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
6.81 1.35 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,1,2-Trichloroethane
6.81 2.18 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,1-Dichloroethane
6.81 3.08 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,1-Dichloroethene
6.81 4.40 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,2-Dibromo-3-Chloropropane
6.81 2.29 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,2-Dichlorobenzene
6.81 1.96 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,2-Dichloroethane
6.81 1.81 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,2-Dichloropropane
6.81 3.46 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,2,4-Trichlorobenzene
6.81 4.19 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,3-Dichlorobenzene
6.81 2.04 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,4-Dichlorobenzene
34.0 3.46 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND2-Butanone (MEK)
34.0 2.14 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND2-Hexanone
34.0 2.49 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND4-Methyl-2-pentanone (MIBK)
34.0 5.31 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDAcetone
6.81 1.92 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDBenzene
6.81 3.43 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDBromoform
6.81 3.10 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDBromomethane
6.81 5.44 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDCarbon disulfide
6.81 2.76 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDCarbon tetrachloride
6.81 1.77 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDChlorobenzene
6.81 3.38 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDChlorodibromomethane
6.81 4.56 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDChloroform
6.81 2.70 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDChloromethane
6.81 3.97 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDChloroethane
6.81 2.06 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDcis-1,2-Dichloroethene
6.81 3.01 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDcis-1,3-Dichloropropene
6.81 3.17 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDDichlorobromomethane
6.81 3.39 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDDichlorodifluoromethane
6.81 2.52 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDEthylbenzene
6.81 1.86 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼ND1,2-Dibromoethane
6.81 3.25 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDCyclohexane
6.81 3.54 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDIsopropylbenzene
34.0 10.0 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDMethyl acetate
6.81 2.00 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDMethyl tert-butyl ether
6.81 3.28 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDMethylcyclohexane
6.81 6.14 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDMethylene Chloride
6.81 2.04 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDStyrene
6.81 2.74 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDTetrachloroethene
6.81 1.96 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDToluene
6.81 2.38 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDtrans-1,2-Dichloroethene
6.81 3.06 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDtrans-1,3-Dichloropropene
6.81 2.14 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDTrichloroethene
6.81 5.65 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDTrichlorofluoromethane
6.81 4.90 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDVinyl chloride
13.6 9.81 ug/Kg 06/02/23 07:05 06/02/23 15:44 1☼NDXylenes, Total
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-6Client Sample ID: EB-15 (8-10)
Matrix: SolidDate Collected: 05/30/23 16:10
Percent Solids: 70.2Date Received: 05/31/23 10:30
1,2-Dichloroethane-d4 (Surr)97 73-135 06/02/23 07:05 06/02/23 15:44 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 06/02/23 07:05 06/02/23 15:44 160-124
Dibromofluoromethane (Surr)100 06/02/23 07:05 06/02/23 15:44 169-126
Toluene-d8 (Surr)98 06/02/23 07:05 06/02/23 15:44 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 464 171 ug/Kg ☼06/08/23 16:27 06/09/23 17:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
94.1 34.7 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2,2'-oxybis[1-chloropropane]
464 163 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2,4,5-Trichlorophenol
464 156 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2,4,6-Trichlorophenol
94.1 36.1 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2,4-Dichlorophenol
464 157 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2,4-Dimethylphenol
4640 2910 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2,4-Dinitrophenol
464 280 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2,4-Dinitrotoluene
464 183 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2,6-Dinitrotoluene
94.1 21.5 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2-Chloronaphthalene
464 173 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2-Chlorophenol
94.1 22.5 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2-Methylnaphthalene
464 134 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2-Methylphenol
2390 214 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2-Nitroaniline
464 173 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND2-Nitrophenol
464 437 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND3,3'-Dichlorobenzidine
2390 119 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND3-Nitroaniline
2390 808 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND4,6-Dinitro-2-methylphenol
464 200 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND4-Bromophenyl phenyl ether
464 164 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND4-Chloro-3-methylphenol
464 123 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND4-Chloroaniline
464 156 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND4-Chlorophenyl phenyl ether
464 138 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDMethylphenol, 3 & 4
2390 174 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND4-Nitroaniline
2390 329 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼ND4-Nitrophenol
94.1 27.0 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDAcenaphthene
94.1 20.5 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDAcenaphthylene
941 167 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDAcetophenone
94.1 24.3 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDAnthracene
941 205 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDAtrazine
941 58.2 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDBenzaldehyde
94.1 42.3 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDBenzo[a]anthracene
94.1 40.6 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDBenzo[a]pyrene
94.1 23.0 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDBenzo[b]fluoranthene
94.1 20.2 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDBenzo[g,h,i]perylene
94.1 28.1 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDBenzo[k]fluoranthene
464 171 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDBis(2-chloroethoxy)methane
94.1 17.0 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDBis(2-chloroethyl)ether
4640 499 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDBis(2-ethylhexyl) phthalate
464 322 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDButyl benzyl phthalate
2390 305 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDCaprolactam
94.1 21.9 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDCarbazole
94.1 52.0 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDChrysene
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-6Client Sample ID: EB-15 (8-10)
Matrix: SolidDate Collected: 05/30/23 16:10
Percent Solids: 70.2Date Received: 05/31/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 94.1 60.0 ug/Kg ☼06/08/23 16:27 06/09/23 17:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
464 173 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDDibenzofuran
464 164 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDDiethyl phthalate
464 185 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDDimethyl phthalate
464 205 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDDi-n-butyl phthalate
464 273 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDDi-n-octyl phthalate
94.1 24.7 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDFluoranthene
94.1 18.4 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDFluorene
94.1 33.6 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDHexachlorobenzene
94.1 27.4 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDHexachlorobutadiene
464 47.9 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDHexachlorocyclopentadiene
464 166 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDHexachloroethane
94.1 46.7 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDIndeno[1,2,3-cd]pyrene
464 176 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDIsophorone
94.1 18.3 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDNaphthalene
941 171 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDNitrobenzene
94.1 31.8 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDN-Nitrosodi-n-propylamine
464 156 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDN-Nitrosodiphenylamine
2390 753 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDPentachlorophenol
94.1 25.2 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDPhenanthrene
464 142 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDPhenol
94.1 22.2 ug/Kg 06/08/23 16:27 06/09/23 17:49 1☼NDPyrene
2,4,6-Tribromophenol (Surr)67 34-108 06/08/23 16:27 06/09/23 17:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 74 06/08/23 16:27 06/09/23 17:49 144-105
2-Fluorophenol (Surr)73 06/08/23 16:27 06/09/23 17:49 148-105
Nitrobenzene-d5 (Surr)73 06/08/23 16:27 06/09/23 17:49 146-105
Phenol-d5 (Surr)69 06/08/23 16:27 06/09/23 17:49 146-105
Terphenyl-d14 (Surr)76 06/08/23 16:27 06/09/23 17:49 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.12 1.78 mg/Kg ☼06/16/23 07:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 62.8 15.7 mg/Kg ☼06/13/23 15:06 06/14/23 20:43 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
62.8 15.7 mg/Kg 06/13/23 15:06 06/14/23 20:43 50☼NDC9-C10 Aromatics
62.8 15.7 mg/Kg 06/13/23 15:06 06/14/23 20:43 50☼NDC9-C12 Aliphatics (unadjusted)
62.8 15.7 mg/Kg 06/13/23 15:06 06/14/23 20:43 50☼NDC9-C12 Aliphatics (adjusted)
62.8 15.7 mg/Kg 06/13/23 15:06 06/14/23 20:43 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)149 S1+70-130 06/13/23 15:06 06/14/23 20:43 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)130 06/13/23 15:06 06/14/23 20:43 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 16.8 16.8 mg/Kg ☼06/06/23 16:31 06/20/23 22:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
16.8 16.8 mg/Kg 06/06/23 16:31 06/20/23 22:59 1☼NDC11-C22 Aromatics (Adjusted)
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157266-6Client Sample ID: EB-15 (8-10)
Matrix: SolidDate Collected: 05/30/23 16:10
Percent Solids: 70.2Date Received: 05/31/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 16.8 16.8 mg/Kg ☼06/06/23 16:31 06/20/23 22:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.39 8.39 mg/Kg 06/06/23 16:31 06/20/23 22:59 1☼28.3C9-C18 Aliphatics
1-Chlorooctadecane (Surr)63 40-140 06/06/23 16:31 06/20/23 22:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)65 06/06/23 16:31 06/20/23 22:59 140-140
o- terphenyl (Surr)49 06/06/23 16:31 06/20/23 22:59 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
28.3 17.1 17.1 mg/Kg ☼06/27/23 19:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
29.8 0.1 0.1 %06/05/23 17:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/05/23 17:33 170.2Percent Solids (SM22 2540G)
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 180-436704/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436704
RL MDL
1,1,1-Trichloroethane ND 5.00 1.67 ug/Kg 06/01/23 10:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.525.00 ug/Kg 06/01/23 10:58 11,1,2,2-Tetrachloroethane
ND 2.005.00 ug/Kg 06/01/23 10:58 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.9905.00 ug/Kg 06/01/23 10:58 11,1,2-Trichloroethane
ND 1.605.00 ug/Kg 06/01/23 10:58 11,1-Dichloroethane
ND 2.265.00 ug/Kg 06/01/23 10:58 11,1-Dichloroethene
ND 3.235.00 ug/Kg 06/01/23 10:58 11,2-Dibromo-3-Chloropropane
ND 1.685.00 ug/Kg 06/01/23 10:58 11,2-Dichlorobenzene
ND 1.445.00 ug/Kg 06/01/23 10:58 11,2-Dichloroethane
ND 1.335.00 ug/Kg 06/01/23 10:58 11,2-Dichloropropane
ND 2.545.00 ug/Kg 06/01/23 10:58 11,2,4-Trichlorobenzene
ND 3.085.00 ug/Kg 06/01/23 10:58 11,3-Dichlorobenzene
ND 1.505.00 ug/Kg 06/01/23 10:58 11,4-Dichlorobenzene
ND 2.5425.0 ug/Kg 06/01/23 10:58 12-Butanone (MEK)
ND 1.5725.0 ug/Kg 06/01/23 10:58 12-Hexanone
ND 1.8325.0 ug/Kg 06/01/23 10:58 14-Methyl-2-pentanone (MIBK)
ND 3.9025.0 ug/Kg 06/01/23 10:58 1Acetone
ND 1.415.00 ug/Kg 06/01/23 10:58 1Benzene
ND 2.525.00 ug/Kg 06/01/23 10:58 1Bromoform
ND 2.285.00 ug/Kg 06/01/23 10:58 1Bromomethane
ND 4.005.00 ug/Kg 06/01/23 10:58 1Carbon disulfide
ND 2.035.00 ug/Kg 06/01/23 10:58 1Carbon tetrachloride
ND 1.305.00 ug/Kg 06/01/23 10:58 1Chlorobenzene
ND 2.485.00 ug/Kg 06/01/23 10:58 1Chlorodibromomethane
ND 3.355.00 ug/Kg 06/01/23 10:58 1Chloroform
ND 1.985.00 ug/Kg 06/01/23 10:58 1Chloromethane
ND 2.925.00 ug/Kg 06/01/23 10:58 1Chloroethane
ND 1.515.00 ug/Kg 06/01/23 10:58 1cis-1,2-Dichloroethene
ND 2.215.00 ug/Kg 06/01/23 10:58 1cis-1,3-Dichloropropene
ND 2.335.00 ug/Kg 06/01/23 10:58 1Dichlorobromomethane
ND 2.495.00 ug/Kg 06/01/23 10:58 1Dichlorodifluoromethane
ND 1.855.00 ug/Kg 06/01/23 10:58 1Ethylbenzene
ND 1.375.00 ug/Kg 06/01/23 10:58 11,2-Dibromoethane
ND 2.395.00 ug/Kg 06/01/23 10:58 1Cyclohexane
ND 2.605.00 ug/Kg 06/01/23 10:58 1Isopropylbenzene
ND 7.3625.0 ug/Kg 06/01/23 10:58 1Methyl acetate
ND 1.475.00 ug/Kg 06/01/23 10:58 1Methyl tert-butyl ether
ND 2.415.00 ug/Kg 06/01/23 10:58 1Methylcyclohexane
ND 4.515.00 ug/Kg 06/01/23 10:58 1Methylene Chloride
ND 1.505.00 ug/Kg 06/01/23 10:58 1Styrene
ND 2.015.00 ug/Kg 06/01/23 10:58 1Tetrachloroethene
ND 1.445.00 ug/Kg 06/01/23 10:58 1Toluene
ND 1.755.00 ug/Kg 06/01/23 10:58 1trans-1,2-Dichloroethene
ND 2.255.00 ug/Kg 06/01/23 10:58 1trans-1,3-Dichloropropene
ND 1.575.00 ug/Kg 06/01/23 10:58 1Trichloroethene
ND 4.155.00 ug/Kg 06/01/23 10:58 1Trichlorofluoromethane
ND 3.605.00 ug/Kg 06/01/23 10:58 1Vinyl chloride
ND 7.2110.0 ug/Kg 06/01/23 10:58 1Xylenes, Total
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-436704/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436704
1,2-Dichloroethane-d4 (Surr)120 73-135 06/01/23 10:58 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
101 06/01/23 10:58 14-Bromofluorobenzene (Surr)60-124
108 06/01/23 10:58 1Dibromofluoromethane (Surr)69-126
99 06/01/23 10:58 1Toluene-d8 (Surr)67-134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-436704/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436704
1,1,1-Trichloroethane 40.0 37.45 ug/Kg 94 72-134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2,2-Tetrachloroethane 40.0 38.38 ug/Kg 96 36-170
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 36.88 ug/Kg 92 59-135
1,1,2-Trichloroethane 40.0 38.75 ug/Kg 97 66-128
1,1-Dichloroethane 40.0 38.37 ug/Kg 96 73-124
1,1-Dichloroethene 40.0 38.06 ug/Kg 95 55-136
1,2-Dibromo-3-Chloropropane 40.0 32.51 ug/Kg 81 30-163
1,2-Dichlorobenzene 40.0 38.29 ug/Kg 96 76-120
1,2-Dichloroethane 40.0 38.97 ug/Kg 97 64-140
1,2-Dichloropropane 40.0 38.31 ug/Kg 96 77-119
1,2,4-Trichlorobenzene 40.0 36.24 ug/Kg 91 22-170
1,3-Dichlorobenzene 40.0 38.02 ug/Kg 95 77-121
1,4-Dichlorobenzene 40.0 38.12 ug/Kg 95 79-120
2-Butanone (MEK)40.0 50.95 ug/Kg 127 39-157
2-Hexanone 40.0 44.41 ug/Kg 111 42-152
4-Methyl-2-pentanone (MIBK)40.0 36.32 ug/Kg 91 51-147
Acetone 40.0 56.45 ug/Kg 141 23-170
Benzene 40.0 39.24 ug/Kg 98 77-120
Bromoform 40.0 34.29 ug/Kg 86 37-147
Bromomethane 40.0 38.62 ug/Kg 97 47-149
Carbon disulfide 40.0 34.60 ug/Kg 87 40-156
Carbon tetrachloride 40.0 36.90 ug/Kg 92 73-130
Chlorobenzene 40.0 37.40 ug/Kg 93 79-122
Chlorodibromomethane 40.0 35.16 ug/Kg 88 60-134
Chloroform 40.0 39.50 ug/Kg 99 73-126
Chloromethane 40.0 37.40 ug/Kg 94 46-151
Chloroethane 40.0 30.76 ug/Kg 77 37-159
cis-1,2-Dichloroethene 40.0 39.11 ug/Kg 98 77-118
cis-1,3-Dichloropropene 40.0 39.00 ug/Kg 98 73-127
Dichlorobromomethane 40.0 38.52 ug/Kg 96 75-123
Dichlorodifluoromethane 40.0 28.51 ug/Kg 71 26-149
Ethylbenzene 40.0 37.88 ug/Kg 95 79-119
1,2-Dibromoethane 40.0 39.27 ug/Kg 98 59-137
Cyclohexane 40.0 36.76 ug/Kg 92 63-143
Isopropylbenzene 40.0 37.68 ug/Kg 94 70-125
Methyl acetate 80.0 100.7 ug/Kg 126 20-170
Methyl tert-butyl ether 40.0 37.40 ug/Kg 93 58-132
Methylcyclohexane 40.0 37.52 ug/Kg 94 70-125
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-436704/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436704
Methylene Chloride 40.0 43.75 ug/Kg 109 67-131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
m-Xylene & p-Xylene 40.0 37.49 ug/Kg 94 77-120
o-Xylene 40.0 37.74 ug/Kg 94 78-118
Styrene 40.0 37.96 ug/Kg 95 80-120
Tetrachloroethene 40.0 37.78 ug/Kg 94 71-121
Toluene 40.0 37.38 ug/Kg 93 76-120
trans-1,2-Dichloroethene 40.0 38.90 ug/Kg 97 75-122
trans-1,3-Dichloropropene 40.0 37.12 ug/Kg 93 68-133
Trichloroethene 40.0 38.47 ug/Kg 96 69-118
Trichlorofluoromethane 40.0 47.62 ug/Kg 119 32-149
Vinyl chloride 40.0 42.34 ug/Kg 106 64-134
Xylenes, Total 80.0 75.23 ug/Kg 94 78-118
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)60 -124
97Dibromofluoromethane (Surr)69 -126
98Toluene-d8 (Surr)67 -134
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-436704/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436704
1,1,1-Trichloroethane 40.0 37.54 ug/Kg 94 72-134 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 40.0 34.68 ug/Kg 87 36-170 10 23
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 35.39 ug/Kg 88 59-135 4 28
1,1,2-Trichloroethane 40.0 37.26 ug/Kg 93 66-128 4 21
1,1-Dichloroethane 40.0 38.72 ug/Kg 97 73-124 1 20
1,1-Dichloroethene 40.0 37.82 ug/Kg 95 55-136 1 21
1,2-Dibromo-3-Chloropropane 40.0 29.14 ug/Kg 73 30-163 11 34
1,2-Dichlorobenzene 40.0 38.63 ug/Kg 97 76-120 1 20
1,2-Dichloroethane 40.0 37.60 ug/Kg 94 64-140 4 20
1,2-Dichloropropane 40.0 38.41 ug/Kg 96 77-119 0 20
1,2,4-Trichlorobenzene 40.0 36.95 ug/Kg 92 22-170 2 29
1,3-Dichlorobenzene 40.0 39.10 ug/Kg 98 77-121 3 20
1,4-Dichlorobenzene 40.0 38.28 ug/Kg 96 79-120 0 20
2-Butanone (MEK)40.0 42.81 ug/Kg 107 39-157 17 33
2-Hexanone 40.0 39.52 ug/Kg 99 42-152 12 30
4-Methyl-2-pentanone (MIBK)40.0 33.91 ug/Kg 85 51-147 7 27
Acetone 40.0 52.51 ug/Kg 131 23-170 7 35
Benzene 40.0 39.49 ug/Kg 99 77-120 1 20
Bromoform 40.0 31.86 ug/Kg 80 37-147 7 23
Bromomethane 40.0 40.42 ug/Kg 101 47-149 5 25
Carbon disulfide 40.0 34.98 ug/Kg 87 40-156 1 25
Carbon tetrachloride 40.0 36.87 ug/Kg 92 73-130 0 21
Chlorobenzene 40.0 38.11 ug/Kg 95 79-122 2 20
Chlorodibromomethane 40.0 34.26 ug/Kg 86 60-134 3 40
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-436704/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436704
Chloroform 40.0 40.02 ug/Kg 100 73-126 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloromethane 40.0 37.10 ug/Kg 93 46-151 1 33
Chloroethane 40.0 31.46 ug/Kg 79 37-159 2 25
cis-1,2-Dichloroethene 40.0 39.90 ug/Kg 100 77-118 2 20
cis-1,3-Dichloropropene 40.0 38.58 ug/Kg 96 73-127 1 20
Dichlorobromomethane 40.0 38.44 ug/Kg 96 75-123 0 20
Dichlorodifluoromethane 40.0 26.57 ug/Kg 66 26-149 7 24
Ethylbenzene 40.0 38.46 ug/Kg 96 79-119 2 20
1,2-Dibromoethane 40.0 37.31 ug/Kg 93 59-137 5 20
Cyclohexane 40.0 36.51 ug/Kg 91 63-143 1 25
Isopropylbenzene 40.0 38.55 ug/Kg 96 70-125 2 21
Methyl acetate 80.0 86.16 ug/Kg 108 20-170 16 33
Methyl tert-butyl ether 40.0 35.42 ug/Kg 89 58-132 5 24
Methylcyclohexane 40.0 37.38 ug/Kg 93 70-125 0 22
Methylene Chloride 40.0 44.06 ug/Kg 110 67-131 1 32
m-Xylene & p-Xylene 40.0 38.11 ug/Kg 95 77-120 2 20
o-Xylene 40.0 38.56 ug/Kg 96 78-118 2 20
Styrene 40.0 38.29 ug/Kg 96 80-120 1 20
Tetrachloroethene 40.0 37.76 ug/Kg 94 71-121 0 21
Toluene 40.0 38.45 ug/Kg 96 76-120 3 20
trans-1,2-Dichloroethene 40.0 39.87 ug/Kg 100 75-122 2 20
trans-1,3-Dichloropropene 40.0 36.19 ug/Kg 90 68-133 3 20
Trichloroethene 40.0 39.04 ug/Kg 98 69-118 1 20
Trichlorofluoromethane 40.0 52.48 ug/Kg 131 32-149 10 39
Vinyl chloride 40.0 42.09 ug/Kg 105 64-134 1 23
Xylenes, Total 80.0 76.67 ug/Kg 96 78-118 2 20
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
95
LCSD LCSD
Qualifier Limits%Recovery
974-Bromofluorobenzene (Surr)60 -124
98Dibromofluoromethane (Surr)69 -126
101Toluene-d8 (Surr)67 -134
Client Sample ID: Method BlankLab Sample ID: MB 180-436709/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 436709
RL MDL
1,2-Dichlorobenzene ND 1.00 0.364 ug/L 06/01/23 11:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.5041.00 ug/L 06/01/23 11:27 11,3-Dichlorobenzene
ND 0.5441.00 ug/L 06/01/23 11:27 11,4-Dichlorobenzene
ND 0.5961.00 ug/L 06/01/23 11:27 1Benzene
ND 0.5011.00 ug/L 06/01/23 11:27 1Chlorobenzene
ND 0.5071.00 ug/L 06/01/23 11:27 1Ethylbenzene
ND 0.4571.00 ug/L 06/01/23 11:27 1Toluene
ND 0.4061.00 ug/L 06/01/23 11:27 1o-Xylene
ND 0.4821.00 ug/L 06/01/23 11:27 1m-Xylene & p-Xylene
ND 0.8902.00 ug/L 06/01/23 11:27 1Xylenes, Total
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-436709/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 436709
1,2-Dichloroethane-d4 (Surr)101 26-156 06/01/23 11:27 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
85 06/01/23 11:27 14-Bromofluorobenzene (Surr)36-124
110 06/01/23 11:27 1Dibromofluoromethane (Surr)46-149
99 06/01/23 11:27 1Toluene-d8 (Surr)40-146
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-436709/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 436709
1,2-Dichlorobenzene 10.0 9.423 ug/L 94 64-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,3-Dichlorobenzene 10.0 9.045 ug/L 90 63-123
1,4-Dichlorobenzene 10.0 9.187 ug/L 92 67-118
Benzene 10.0 9.541 ug/L 95 68-125
Chlorobenzene 10.0 9.257 ug/L 93 68-121
Ethylbenzene 10.0 9.254 ug/L 93 65-126
Toluene 10.0 9.723 ug/L 97 69-124
o-Xylene 10.0 9.030 ug/L 90 64-127
m-Xylene & p-Xylene 10.0 9.487 ug/L 95 66-131
Xylenes, Total 20.0 18.52 ug/L 93 68-124
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
1004-Bromofluorobenzene (Surr)36 -124
99Dibromofluoromethane (Surr)46 -149
97Toluene-d8 (Surr)40 -146
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-436709/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 436709
1,2-Dichlorobenzene 10.0 9.275 ug/L 93 64-120 2 27
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,3-Dichlorobenzene 10.0 8.852 ug/L 89 63-123 2 27
1,4-Dichlorobenzene 10.0 9.119 ug/L 91 67-118 1 24
Benzene 10.0 9.079 ug/L 91 68-125 5 24
Chlorobenzene 10.0 9.209 ug/L 92 68-121 1 21
Ethylbenzene 10.0 9.024 ug/L 90 65-126 3 22
Toluene 10.0 9.632 ug/L 96 69-124 1 23
o-Xylene 10.0 8.779 ug/L 88 64-127 3 26
m-Xylene & p-Xylene 10.0 9.362 ug/L 94 66-131 1 26
Xylenes, Total 20.0 18.14 ug/L 91 68-124 2 24
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
94
LCSD LCSD
Qualifier Limits%Recovery
1014-Bromofluorobenzene (Surr)36 -124
96Dibromofluoromethane (Surr)46 -149
95Toluene-d8 (Surr)40 -146
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 180-436827/10
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436827
RL MDL
1,1,1-Trichloroethane ND 5.00 1.67 ug/Kg 06/02/23 11:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.525.00 ug/Kg 06/02/23 11:58 11,1,2,2-Tetrachloroethane
ND 2.005.00 ug/Kg 06/02/23 11:58 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.9905.00 ug/Kg 06/02/23 11:58 11,1,2-Trichloroethane
ND 1.605.00 ug/Kg 06/02/23 11:58 11,1-Dichloroethane
ND 2.265.00 ug/Kg 06/02/23 11:58 11,1-Dichloroethene
ND 3.235.00 ug/Kg 06/02/23 11:58 11,2-Dibromo-3-Chloropropane
ND 1.685.00 ug/Kg 06/02/23 11:58 11,2-Dichlorobenzene
ND 1.445.00 ug/Kg 06/02/23 11:58 11,2-Dichloroethane
ND 1.335.00 ug/Kg 06/02/23 11:58 11,2-Dichloropropane
ND 2.545.00 ug/Kg 06/02/23 11:58 11,2,4-Trichlorobenzene
ND 3.085.00 ug/Kg 06/02/23 11:58 11,3-Dichlorobenzene
ND 1.505.00 ug/Kg 06/02/23 11:58 11,4-Dichlorobenzene
ND 2.5425.0 ug/Kg 06/02/23 11:58 12-Butanone (MEK)
ND 1.5725.0 ug/Kg 06/02/23 11:58 12-Hexanone
ND 1.8325.0 ug/Kg 06/02/23 11:58 14-Methyl-2-pentanone (MIBK)
ND 3.9025.0 ug/Kg 06/02/23 11:58 1Acetone
ND 1.415.00 ug/Kg 06/02/23 11:58 1Benzene
ND 2.525.00 ug/Kg 06/02/23 11:58 1Bromoform
ND 2.285.00 ug/Kg 06/02/23 11:58 1Bromomethane
ND 4.005.00 ug/Kg 06/02/23 11:58 1Carbon disulfide
ND 2.035.00 ug/Kg 06/02/23 11:58 1Carbon tetrachloride
ND 1.305.00 ug/Kg 06/02/23 11:58 1Chlorobenzene
ND 2.485.00 ug/Kg 06/02/23 11:58 1Chlorodibromomethane
ND 3.355.00 ug/Kg 06/02/23 11:58 1Chloroform
ND 1.985.00 ug/Kg 06/02/23 11:58 1Chloromethane
ND 2.925.00 ug/Kg 06/02/23 11:58 1Chloroethane
ND 1.515.00 ug/Kg 06/02/23 11:58 1cis-1,2-Dichloroethene
ND 2.215.00 ug/Kg 06/02/23 11:58 1cis-1,3-Dichloropropene
ND 2.335.00 ug/Kg 06/02/23 11:58 1Dichlorobromomethane
ND 2.495.00 ug/Kg 06/02/23 11:58 1Dichlorodifluoromethane
ND 1.855.00 ug/Kg 06/02/23 11:58 1Ethylbenzene
ND 1.375.00 ug/Kg 06/02/23 11:58 11,2-Dibromoethane
ND 2.395.00 ug/Kg 06/02/23 11:58 1Cyclohexane
ND 2.605.00 ug/Kg 06/02/23 11:58 1Isopropylbenzene
ND 7.3625.0 ug/Kg 06/02/23 11:58 1Methyl acetate
ND 1.475.00 ug/Kg 06/02/23 11:58 1Methyl tert-butyl ether
ND 2.415.00 ug/Kg 06/02/23 11:58 1Methylcyclohexane
ND 4.515.00 ug/Kg 06/02/23 11:58 1Methylene Chloride
ND 1.505.00 ug/Kg 06/02/23 11:58 1Styrene
ND 2.015.00 ug/Kg 06/02/23 11:58 1Tetrachloroethene
ND 1.445.00 ug/Kg 06/02/23 11:58 1Toluene
ND 1.755.00 ug/Kg 06/02/23 11:58 1trans-1,2-Dichloroethene
ND 2.255.00 ug/Kg 06/02/23 11:58 1trans-1,3-Dichloropropene
ND 1.575.00 ug/Kg 06/02/23 11:58 1Trichloroethene
ND 4.155.00 ug/Kg 06/02/23 11:58 1Trichlorofluoromethane
ND 3.605.00 ug/Kg 06/02/23 11:58 1Vinyl chloride
ND 7.2110.0 ug/Kg 06/02/23 11:58 1Xylenes, Total
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-436827/10
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436827
1,2-Dichloroethane-d4 (Surr)121 73-135 06/02/23 11:58 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
100 06/02/23 11:58 14-Bromofluorobenzene (Surr)60-124
109 06/02/23 11:58 1Dibromofluoromethane (Surr)69-126
92 06/02/23 11:58 1Toluene-d8 (Surr)67-134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-436827/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436827
1,1,1-Trichloroethane 40.0 36.74 ug/Kg 92 72-134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2,2-Tetrachloroethane 40.0 35.01 ug/Kg 88 36-170
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 35.41 ug/Kg 89 59-135
1,1,2-Trichloroethane 40.0 37.03 ug/Kg 93 66-128
1,1-Dichloroethane 40.0 38.36 ug/Kg 96 73-124
1,1-Dichloroethene 40.0 37.21 ug/Kg 93 55-136
1,2-Dibromo-3-Chloropropane 40.0 29.97 ug/Kg 75 30-163
1,2-Dichlorobenzene 40.0 37.68 ug/Kg 94 76-120
1,2-Dichloroethane 40.0 37.78 ug/Kg 94 64-140
1,2-Dichloropropane 40.0 38.31 ug/Kg 96 77-119
1,2,4-Trichlorobenzene 40.0 37.15 ug/Kg 93 22-170
1,3-Dichlorobenzene 40.0 37.62 ug/Kg 94 77-121
1,4-Dichlorobenzene 40.0 37.34 ug/Kg 93 79-120
2-Butanone (MEK)40.0 49.46 ug/Kg 124 39-157
2-Hexanone 40.0 43.02 ug/Kg 108 42-152
4-Methyl-2-pentanone (MIBK)40.0 45.12 ug/Kg 113 51-147
Acetone 40.0 43.84 ug/Kg 110 23-170
Benzene 40.0 38.81 ug/Kg 97 77-120
Bromoform 40.0 31.59 ug/Kg 79 37-147
Bromomethane 40.0 39.56 ug/Kg 99 47-149
Carbon disulfide 40.0 34.87 ug/Kg 87 40-156
Carbon tetrachloride 40.0 35.96 ug/Kg 90 73-130
Chlorobenzene 40.0 37.17 ug/Kg 93 79-122
Chlorodibromomethane 40.0 34.13 ug/Kg 85 60-134
Chloroform 40.0 39.29 ug/Kg 98 73-126
Chloromethane 40.0 38.38 ug/Kg 96 46-151
Chloroethane 40.0 30.74 ug/Kg 77 37-159
cis-1,2-Dichloroethene 40.0 38.78 ug/Kg 97 77-118
cis-1,3-Dichloropropene 40.0 37.98 ug/Kg 95 73-127
Dichlorobromomethane 40.0 37.45 ug/Kg 94 75-123
Dichlorodifluoromethane 40.0 28.51 ug/Kg 71 26-149
Ethylbenzene 40.0 37.03 ug/Kg 93 79-119
1,2-Dibromoethane 40.0 37.61 ug/Kg 94 59-137
Cyclohexane 40.0 36.74 ug/Kg 92 63-143
Isopropylbenzene 40.0 37.34 ug/Kg 93 70-125
Methyl acetate 80.0 90.57 ug/Kg 113 20-170
Methyl tert-butyl ether 40.0 36.30 ug/Kg 91 58-132
Methylcyclohexane 40.0 36.83 ug/Kg 92 70-125
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-436827/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436827
Methylene Chloride 40.0 41.68 ug/Kg 104 67-131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
m-Xylene & p-Xylene 40.0 37.70 ug/Kg 94 77-120
o-Xylene 40.0 37.73 ug/Kg 94 78-118
Styrene 40.0 37.55 ug/Kg 94 80-120
Tetrachloroethene 40.0 36.95 ug/Kg 92 71-121
Toluene 40.0 40.55 ug/Kg 101 76-120
trans-1,2-Dichloroethene 40.0 38.10 ug/Kg 95 75-122
trans-1,3-Dichloropropene 40.0 35.95 ug/Kg 90 68-133
Trichloroethene 40.0 38.13 ug/Kg 95 69-118
Trichlorofluoromethane 40.0 50.92 ug/Kg 127 32-149
Vinyl chloride 40.0 43.02 ug/Kg 108 64-134
Xylenes, Total 80.0 75.43 ug/Kg 94 78-118
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
1004-Bromofluorobenzene (Surr)60 -124
102Dibromofluoromethane (Surr)69 -126
103Toluene-d8 (Surr)67 -134
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-436827/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436827
1,1,1-Trichloroethane 40.0 36.47 ug/Kg 91 72-134 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 40.0 32.98 ug/Kg 82 36-170 6 23
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 34.39 ug/Kg 86 59-135 3 28
1,1,2-Trichloroethane 40.0 34.87 ug/Kg 87 66-128 6 21
1,1-Dichloroethane 40.0 37.59 ug/Kg 94 73-124 2 20
1,1-Dichloroethene 40.0 36.76 ug/Kg 92 55-136 1 21
1,2-Dibromo-3-Chloropropane 40.0 30.54 ug/Kg 76 30-163 2 34
1,2-Dichlorobenzene 40.0 36.35 ug/Kg 91 76-120 4 20
1,2-Dichloroethane 40.0 35.93 ug/Kg 90 64-140 5 20
1,2-Dichloropropane 40.0 36.70 ug/Kg 92 77-119 4 20
1,2,4-Trichlorobenzene 40.0 36.21 ug/Kg 91 22-170 3 29
1,3-Dichlorobenzene 40.0 37.12 ug/Kg 93 77-121 1 20
1,4-Dichlorobenzene 40.0 37.07 ug/Kg 93 79-120 1 20
2-Butanone (MEK)40.0 37.56 ug/Kg 94 39-157 27 33
2-Hexanone 40.0 37.26 ug/Kg 93 42-152 14 30
4-Methyl-2-pentanone (MIBK)40.0 44.58 ug/Kg 111 51-147 1 27
Acetone 40.0 31.74 ug/Kg 79 23-170 32 35
Benzene 40.0 38.48 ug/Kg 96 77-120 1 20
Bromoform 40.0 29.61 ug/Kg 74 37-147 6 23
Bromomethane 40.0 37.24 ug/Kg 93 47-149 6 25
Carbon disulfide 40.0 34.78 ug/Kg 87 40-156 0 25
Carbon tetrachloride 40.0 35.92 ug/Kg 90 73-130 0 21
Chlorobenzene 40.0 36.72 ug/Kg 92 79-122 1 20
Chlorodibromomethane 40.0 33.01 ug/Kg 83 60-134 3 40
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-436827/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436827
Chloroform 40.0 38.29 ug/Kg 96 73-126 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloromethane 40.0 36.69 ug/Kg 92 46-151 5 33
Chloroethane 40.0 27.34 ug/Kg 68 37-159 12 25
cis-1,2-Dichloroethene 40.0 37.70 ug/Kg 94 77-118 3 20
cis-1,3-Dichloropropene 40.0 36.57 ug/Kg 91 73-127 4 20
Dichlorobromomethane 40.0 36.29 ug/Kg 91 75-123 3 20
Dichlorodifluoromethane 40.0 28.60 ug/Kg 71 26-149 0 24
Ethylbenzene 40.0 37.74 ug/Kg 94 79-119 2 20
1,2-Dibromoethane 40.0 35.65 ug/Kg 89 59-137 5 20
Cyclohexane 40.0 36.32 ug/Kg 91 63-143 1 25
Isopropylbenzene 40.0 37.75 ug/Kg 94 70-125 1 21
Methyl acetate 80.0 83.31 ug/Kg 104 20-170 8 33
Methyl tert-butyl ether 40.0 33.59 ug/Kg 84 58-132 8 24
Methylcyclohexane 40.0 36.87 ug/Kg 92 70-125 0 22
Methylene Chloride 40.0 40.71 ug/Kg 102 67-131 2 32
m-Xylene & p-Xylene 40.0 37.48 ug/Kg 94 77-120 1 20
o-Xylene 40.0 37.66 ug/Kg 94 78-118 0 20
Styrene 40.0 37.29 ug/Kg 93 80-120 1 20
Tetrachloroethene 40.0 37.91 ug/Kg 95 71-121 3 21
Toluene 40.0 42.67 ug/Kg 107 76-120 5 20
trans-1,2-Dichloroethene 40.0 38.03 ug/Kg 95 75-122 0 20
trans-1,3-Dichloropropene 40.0 34.75 ug/Kg 87 68-133 3 20
Trichloroethene 40.0 38.38 ug/Kg 96 69-118 1 20
Trichlorofluoromethane 40.0 49.98 ug/Kg 125 32-149 2 39
Vinyl chloride 40.0 41.86 ug/Kg 105 64-134 3 23
Xylenes, Total 80.0 75.14 ug/Kg 94 78-118 0 20
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
94
LCSD LCSD
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)60 -124
95Dibromofluoromethane (Surr)69 -126
102Toluene-d8 (Surr)67 -134
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-437005/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
RL MDL
Acenaphthene ND 0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 10:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.06500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Acenaphthylene
ND 0.04900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Anthracene
ND 0.09501.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,2-Dichlorobenzene
ND 0.07500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[a]anthracene
ND 0.05300.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[a]pyrene
ND 0.09901.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,3-Dichlorobenzene
ND 0.09700.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[b]fluoranthene
ND 0.06900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[g,h,i]perylene
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437005/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
RL MDL
1,4-Dichlorobenzene ND 1.00 0.0610 ug/L 06/05/23 11:58 06/07/23 10:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.08800.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[k]fluoranthene
ND 0.1521.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Bis(2-chloroethoxy)methane
ND 0.04000.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Bis(2-chloroethyl)ether
ND 0.05600.190 ug/L 06/05/23 11:58 06/07/23 10:59 11-Methylnaphthalene
ND 0.05800.190 ug/L 06/05/23 11:58 06/07/23 10:59 12,2'-oxybis[1-chloropropane]
ND 6.2310.0 ug/L 06/05/23 11:58 06/07/23 10:59 1Bis(2-ethylhexyl) phthalate
ND 0.3191.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Bromophenyl phenyl ether
ND 0.4621.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Butyl benzyl phthalate
ND 0.05900.190 ug/L 06/05/23 11:58 06/07/23 10:59 12-Chloronaphthalene
ND 0.2211.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Chlorophenyl phenyl ether
ND 0.08100.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Chrysene
ND 0.07200.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Dibenz(a,h)anthracene
ND 0.5831.00 ug/L 06/05/23 11:58 06/07/23 10:59 13,3'-Dichlorobenzidine
ND 0.5671.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Diethyl phthalate
ND 0.6851.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Di-n-octyl phthalate
ND 0.1961.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,2-Diphenylhydrazine(as
Azobenzene)
ND 0.06200.190 ug/L 06/05/23 11:58 06/07/23 10:59 12-Methylnaphthalene
ND 0.06000.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Fluoranthene
ND 0.3001.00 ug/L 06/05/23 11:58 06/07/23 10:59 12-Methylphenol
ND 0.06900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Fluorene
ND 0.05600.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachlorobenzene
ND 0.06900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachlorobutadiene
ND 0.4971.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachlorocyclopentadiene
ND 0.1331.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachloroethane
ND 0.08500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Indeno[1,2,3-cd]pyrene
ND 0.1881.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Isophorone
ND 0.05900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Naphthalene
ND 0.5002.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Nitrobenzene
ND 0.06701.00 ug/L 06/05/23 11:58 06/07/23 10:59 1N-Nitrosodimethylamine
ND 0.07100.190 ug/L 06/05/23 11:58 06/07/23 10:59 1N-Nitrosodi-n-propylamine
ND 0.3761.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Chloroaniline
ND 0.05500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Phenanthrene
ND 0.05400.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Pyrene
ND 0.3721.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Methylphenol
ND 0.8475.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Pentachlorophenol
ND 0.4871.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Phenol
ND 0.1311.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,2,4-Trichlorobenzene
ND 0.05100.190 ug/L 06/05/23 11:58 06/07/23 10:59 12,4-Dichlorophenol
ND 1.5310.0 ug/L 06/05/23 11:58 06/07/23 10:59 12,4-Dinitrophenol
ND 0.1671.00 ug/L 06/05/23 11:58 06/07/23 10:59 12,4-Dimethylphenol
ND 0.2241.00 ug/L 06/05/23 11:58 06/07/23 10:59 12,4,6-Trichlorophenol
ND 0.1291.00 ug/L 06/05/23 11:58 06/07/23 10:59 12-Chlorophenol
ND 0.1931.00 ug/L 06/05/23 11:58 06/07/23 10:59 12-Nitrophenol
ND 1.475.00 ug/L 06/05/23 11:58 06/07/23 10:59 14,6-Dinitro-2-methylphenol
ND 0.2781.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Chloro-3-methylphenol
ND 0.9405.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Nitrophenol
ND 0.9235.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzoic acid
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437005/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
RL MDL
Benzyl alcohol ND 1.00 0.163 ug/L 06/05/23 11:58 06/07/23 10:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1901.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Dibenzofuran
2,4,6-Tribromophenol (Surr)56 32-127 06/07/23 10:59 1
MB MB
Surrogate
06/05/23 11:58
Dil FacPreparedAnalyzedQualifierLimits%Recovery
81 06/05/23 11:58 06/07/23 10:59 12-Fluorobiphenyl 47-107
73 06/05/23 11:58 06/07/23 10:59 12-Fluorophenol (Surr)35-109
74 06/05/23 11:58 06/07/23 10:59 1Nitrobenzene-d5 (Surr)47-110
69 06/05/23 11:58 06/07/23 10:59 1Phenol-d5 (Surr)37-110
90 06/05/23 11:58 06/07/23 10:59 1Terphenyl-d14 (Surr)32-115
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437005/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Acenaphthene 10.0 7.822 ug/L 78 47-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Acenaphthylene 10.0 8.169 ug/L 82 33-145
Anthracene 10.0 7.734 ug/L 77 27-133
1,2-Dichlorobenzene 10.0 7.657 ug/L 77 50-100
Benzo[a]anthracene 10.0 8.044 ug/L 80 33-143
Benzo[a]pyrene 10.0 8.443 ug/L 84 17-150
1,3-Dichlorobenzene 10.0 7.589 ug/L 76 51-100
Benzo[b]fluoranthene 10.0 8.442 ug/L 84 24-150
Benzo[g,h,i]perylene 10.0 7.818 ug/L 78 10-150
1,4-Dichlorobenzene 10.0 7.731 ug/L 77 51-100
Benzo[k]fluoranthene 10.0 8.189 ug/L 82 11-150
Bis(2-chloroethoxy)methane 10.0 6.832 ug/L 68 33-150
Bis(2-chloroethyl)ether 10.0 6.714 ug/L 67 12-150
1-Methylnaphthalene 10.0 8.103 ug/L 81 49-100
2,2'-oxybis[1-chloropropane]10.0 7.946 ug/L 79 36-150
Bis(2-ethylhexyl) phthalate 10.0 8.044 J ug/L 80 10-150
4-Bromophenyl phenyl ether 10.0 7.870 ug/L 79 53-127
Butyl benzyl phthalate 10.0 8.489 ug/L 85 10-150
2-Chloronaphthalene 10.0 7.727 ug/L 77 60-120
4-Chlorophenyl phenyl ether 10.0 8.200 ug/L 82 25-150
Chrysene 10.0 8.096 ug/L 81 17-150
Dibenz(a,h)anthracene 10.0 8.290 ug/L 83 10-150
3,3'-Dichlorobenzidine 10.0 7.939 ug/L 79 10-150
Diethyl phthalate 10.0 7.283 ug/L 73 10-120
Di-n-octyl phthalate 10.0 7.927 ug/L 79 10-146
1,2-Diphenylhydrazine(as
Azobenzene)
10.0 7.019 ug/L 70 43-105
2-Methylnaphthalene 10.0 8.097 ug/L 81 51-100
Fluoranthene 10.0 7.690 ug/L 77 26-137
2-Methylphenol 10.0 7.742 ug/L 77 48-100
Fluorene 10.0 7.496 ug/L 75 59-121
Hexachlorobenzene 10.0 6.900 ug/L 69 10-150
Hexachlorobutadiene 10.0 7.247 ug/L 72 24-120
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437005/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Hexachlorocyclopentadiene 10.0 6.817 ug/L 68 37-121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Hexachloroethane 10.0 7.057 ug/L 71 40-120
Indeno[1,2,3-cd]pyrene 10.0 7.976 ug/L 80 10-150
Isophorone 10.0 7.648 ug/L 76 21-150
Naphthalene 10.0 7.477 ug/L 75 21-133
Nitrobenzene 10.0 7.467 ug/L 75 35-150
N-Nitrosodimethylamine 10.0 8.734 ug/L 87 33-130
N-Nitrosodi-n-propylamine 10.0 8.578 ug/L 86 10-150
4-Chloroaniline 10.0 7.412 ug/L 74 49-100
Phenanthrene 10.0 7.461 ug/L 75 54-120
Pyrene 10.0 9.091 ug/L 91 52-120
4-Methylphenol 10.0 7.899 ug/L 79 47-100
Pentachlorophenol 20.0 13.38 ug/L 67 14-150
Phenol 10.0 6.802 ug/L 68 10-120
1,2,4-Trichlorobenzene 10.0 7.765 ug/L 78 44-142
2,4-Dichlorophenol 10.0 7.630 ug/L 76 39-135
2,4-Dinitrophenol 20.0 13.19 ug/L 66 10-150
2,4-Dimethylphenol 10.0 6.635 ug/L 66 32-120
2,4,6-Trichlorophenol 10.0 8.448 ug/L 84 37-144
2-Chlorophenol 10.0 7.376 ug/L 74 23-134
2-Nitrophenol 10.0 8.119 ug/L 81 29-150
4,6-Dinitro-2-methylphenol 20.0 16.83 ug/L 84 10-150
4-Chloro-3-methylphenol 10.0 8.274 ug/L 83 22-147
4-Nitrophenol 20.0 12.40 ug/L 62 10-132
Benzoic acid 10.0 6.461 ug/L 65 26-127
Benzyl alcohol 10.0 6.997 ug/L 70 30-102
Dibenzofuran 10.0 7.514 ug/L 75 51-100
2,4,6-Tribromophenol (Surr)32 -127
Surrogate
63
LCS LCS
Qualifier Limits%Recovery
782-Fluorobiphenyl 47 -107
712-Fluorophenol (Surr)35 -109
75Nitrobenzene-d5 (Surr)47 -110
69Phenol-d5 (Surr)37 -110
83Terphenyl-d14 (Surr)32 -115
Client Sample ID: TMW-1Lab Sample ID: 180-157266-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Acenaphthene ND F1 10.0 4.111 F1 ug/L 41 47-145
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Acenaphthylene ND 10.0 4.093 ug/L 41 35-145
Anthracene ND 10.0 3.947 ug/L 39 27-133
1,2-Dichlorobenzene ND F1 10.0 1.693 F1 ug/L 17 60-100
Benzo[a]anthracene ND 10.0 4.369 ug/L 44 33-143
Benzo[a]pyrene ND 10.0 4.183 ug/L 42 17-163
1,3-Dichlorobenzene ND F1 10.0 1.594 F1 ug/L 16 60-100
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TMW-1Lab Sample ID: 180-157266-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Benzo[b]fluoranthene ND 10.0 4.204 ug/L 42 24-159
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Benzo[g,h,i]perylene ND 10.0 4.237 ug/L 42 10-170
1,4-Dichlorobenzene ND F1 10.0 1.637 F1 ug/L 16 60-100
Benzo[k]fluoranthene ND 10.0 4.458 ug/L 45 11-162
Bis(2-chloroethoxy)methane ND 10.0 4.101 ug/L 41 33-170
Bis(2-chloroethyl)ether ND 10.0 3.140 ug/L 31 12-158
1-Methylnaphthalene 0.370 F1 10.0 3.781 F1 ug/L 34 58-100
2,2'-oxybis[1-chloropropane]ND 10.0 3.746 ug/L 37 36-166
Bis(2-ethylhexyl) phthalate ND 10.0 6.449 J ug/L 64 10-158
4-Bromophenyl phenyl ether ND F1 10.0 4.395 F1 ug/L 44 53-127
Butyl benzyl phthalate 0.706 J 10.0 5.242 ug/L 45 10-152
2-Chloronaphthalene ND F1 10.0 3.393 F1 ug/L 34 60-120
4-Chlorophenyl phenyl ether ND 10.0 4.414 ug/L 44 25-158
Chrysene ND 10.0 4.537 ug/L 45 17-168
Dibenz(a,h)anthracene ND 10.0 4.485 ug/L 45 10-170
3,3'-Dichlorobenzidine ND F1 10.0 ND F1 ug/L 0 10-170
Diethyl phthalate ND 10.0 4.232 ug/L 42 10-120
Di-n-octyl phthalate ND 10.0 4.196 ug/L 42 10-146
1,2-Diphenylhydrazine(as
Azobenzene)
ND F1 10.0 3.867 F1 ug/L 39 46-103
2-Methylnaphthalene 0.361 F1 10.0 3.778 F1 ug/L 34 58-100
Fluoranthene ND 10.0 4.206 ug/L 42 26-137
2-Methylphenol ND F1 10.0 4.264 F1 ug/L 43 55-101
Fluorene ND F1 10.0 3.985 F1 ug/L 40 59-121
Hexachlorobenzene ND 10.0 3.981 ug/L 40 10-152
Hexachlorobutadiene ND F1 10.0 1.784 F1 ug/L 18 24-120
Hexachlorocyclopentadiene ND F1 10.0 ND F1 ug/L 0 41-106
Hexachloroethane ND F1 10.0 1.440 F1 ug/L 14 40-120
Indeno[1,2,3-cd]pyrene ND 10.0 4.282 ug/L 43 10-170
Isophorone ND 10.0 4.539 ug/L 45 21-170
Naphthalene 2.15 10.0 6.223 ug/L 41 21-133
Nitrobenzene ND 10.0 3.789 ug/L 38 35-170
N-Nitrosodimethylamine ND F1 10.0 4.043 F1 ug/L 40 48-109
N-Nitrosodi-n-propylamine ND 10.0 4.495 ug/L 45 10-170
4-Chloroaniline ND F1 10.0 2.376 F1 ug/L 24 50-100
Phenanthrene 0.104 J F1 10.0 4.313 F1 ug/L 42 54-120
Pyrene ND F1 10.0 4.937 F1 ug/L 49 52-120
4-Methylphenol ND F1 10.0 4.333 F1 ug/L 43 56-102
Pentachlorophenol ND 20.0 7.469 ug/L 37 17-170
Phenol ND 10.0 3.468 ug/L 35 10-120
1,2,4-Trichlorobenzene ND F1 10.0 2.138 F1 ug/L 21 44-142
2,4-Dichlorophenol ND 10.0 4.455 ug/L 45 39-135
2,4-Dinitrophenol ND 20.0 8.690 J ug/L 43 10-170
2,4-Dimethylphenol ND 10.0 3.738 ug/L 37 32-120
2,4,6-Trichlorophenol ND 10.0 4.621 ug/L 46 37-144
2-Chlorophenol ND 10.0 3.721 ug/L 37 23-134
2-Nitrophenol ND 10.0 4.577 ug/L 46 29-170
4,6-Dinitro-2-methylphenol ND 20.0 9.164 ug/L 46 10-170
4-Chloro-3-methylphenol ND 10.0 5.470 ug/L 55 22-147
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TMW-1Lab Sample ID: 180-157266-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
4-Nitrophenol ND 20.0 7.566 ug/L 38 10-132
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Benzoic acid ND 10.0 4.960 J ug/L 50 32-118
Benzyl alcohol ND 10.0 4.020 ug/L 40 24-117
Dibenzofuran ND F1 10.0 3.956 F1 ug/L 40 57-100
2,4,6-Tribromophenol (Surr)32 -127
Surrogate
59
MS MS
Qualifier Limits%Recovery
572-Fluorobiphenyl 47 -107
532-Fluorophenol (Surr)35 -109
69Nitrobenzene-d5 (Surr)47 -110
56Phenol-d5 (Surr)37 -110
65Terphenyl-d14 (Surr)32 -115
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-437429/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
RL MDL
1,1'-Biphenyl ND 330 122 ug/Kg 06/08/23 16:27 06/09/23 09:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 24.767.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,2'-oxybis[1-chloropropane]
ND 116330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4,5-Trichlorophenol
ND 111330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4,6-Trichlorophenol
ND 25.767.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4-Dichlorophenol
ND 112330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4-Dimethylphenol
ND 20703300 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4-Dinitrophenol
ND 199330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4-Dinitrotoluene
ND 130330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,6-Dinitrotoluene
ND 15.367.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Chloronaphthalene
ND 123330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Chlorophenol
ND 16.067.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Methylnaphthalene
ND 95.6330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Methylphenol
ND 1521700 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Nitroaniline
ND 123330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Nitrophenol
ND 311330 ug/Kg 06/08/23 16:27 06/09/23 09:19 13,3'-Dichlorobenzidine
ND 84.81700 ug/Kg 06/08/23 16:27 06/09/23 09:19 13-Nitroaniline
ND 5751700 ug/Kg 06/08/23 16:27 06/09/23 09:19 14,6-Dinitro-2-methylphenol
ND 142330 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Bromophenyl phenyl ether
ND 117330 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Chloro-3-methylphenol
ND 87.5330 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Chloroaniline
ND 111330 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Chlorophenyl phenyl ether
ND 97.9330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Methylphenol, 3 & 4
ND 1241700 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Nitroaniline
ND 2341700 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Nitrophenol
ND 19.267.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Acenaphthene
ND 14.667.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Acenaphthylene
ND 119670 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Acetophenone
ND 17.367.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Anthracene
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437429/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
RL MDL
Atrazine ND 670 146 ug/Kg 06/08/23 16:27 06/09/23 09:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 41.4670 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzaldehyde
ND 30.167.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[a]anthracene
ND 28.967.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[a]pyrene
ND 16.467.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[b]fluoranthene
ND 14.467.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[g,h,i]perylene
ND 20.067.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[k]fluoranthene
ND 122330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Bis(2-chloroethoxy)methane
ND 12.167.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Bis(2-chloroethyl)ether
ND 3553300 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Bis(2-ethylhexyl) phthalate
ND 229330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Butyl benzyl phthalate
ND 2171700 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Caprolactam
ND 15.667.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Carbazole
ND 37.067.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Chrysene
ND 42.767.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Dibenz(a,h)anthracene
ND 123330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Dibenzofuran
ND 117330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Diethyl phthalate
ND 132330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Dimethyl phthalate
ND 146330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Di-n-butyl phthalate
ND 194330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Di-n-octyl phthalate
ND 17.667.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Fluoranthene
ND 13.167.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Fluorene
ND 23.967.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Hexachlorobenzene
ND 19.567.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Hexachlorobutadiene
ND 34.1330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Hexachlorocyclopentadiene
ND 118330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Hexachloroethane
ND 33.267.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Indeno[1,2,3-cd]pyrene
ND 125330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Isophorone
ND 13.067.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Naphthalene
ND 122670 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Nitrobenzene
ND 22.667.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1N-Nitrosodi-n-propylamine
ND 111330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1N-Nitrosodiphenylamine
ND 5361700 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Pentachlorophenol
ND 17.967.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Phenanthrene
ND 101330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Phenol
ND 15.867.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Pyrene
2,4,6-Tribromophenol (Surr)72 34-108 06/09/23 09:19 1
MB MB
Surrogate
06/08/23 16:27
Dil FacPreparedAnalyzedQualifierLimits%Recovery
76 06/08/23 16:27 06/09/23 09:19 12-Fluorobiphenyl 44-105
78 06/08/23 16:27 06/09/23 09:19 12-Fluorophenol (Surr)48-105
74 06/08/23 16:27 06/09/23 09:19 1Nitrobenzene-d5 (Surr)46-105
72 06/08/23 16:27 06/09/23 09:19 1Phenol-d5 (Surr)46-105
84 06/08/23 16:27 06/09/23 09:19 1Terphenyl-d14 (Surr)39-105
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437429/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
1,1'-Biphenyl 6670 4835 ug/Kg 73 50-100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,2'-oxybis[1-chloropropane]6670 4585 ug/Kg 69 30-113
2,4,5-Trichlorophenol 6670 4748 ug/Kg 71 50-104
2,4,6-Trichlorophenol 6670 5087 ug/Kg 76 50-105
2,4-Dichlorophenol 6670 4552 ug/Kg 68 53-101
2,4-Dimethylphenol 6670 4468 ug/Kg 67 51-101
2,4-Dinitrophenol 13300 6128 ug/Kg 46 33-101
2,4-Dinitrotoluene 6670 4942 ug/Kg 74 54-104
2,6-Dinitrotoluene 6670 4926 ug/Kg 74 51-106
2-Chloronaphthalene 6670 4844 ug/Kg 73 51-100
2-Chlorophenol 6670 4798 ug/Kg 72 51-100
2-Methylnaphthalene 6670 4750 ug/Kg 71 53-100
2-Methylphenol 6670 4486 ug/Kg 67 50-101
2-Nitroaniline 6670 4875 ug/Kg 73 42-123
2-Nitrophenol 6670 5316 ug/Kg 80 55-107
3,3'-Dichlorobenzidine 6670 4968 ug/Kg 75 43-100
3-Nitroaniline 6670 4616 ug/Kg 69 50-103
4,6-Dinitro-2-methylphenol 13300 7989 ug/Kg 60 51-100
4-Bromophenyl phenyl ether 6670 5541 ug/Kg 83 52-101
4-Chloro-3-methylphenol 6670 4425 ug/Kg 66 49-106
4-Chloroaniline 6670 4529 ug/Kg 68 47-100
4-Chlorophenyl phenyl ether 6670 4838 ug/Kg 73 52-100
Methylphenol, 3 & 4 6670 4455 ug/Kg 67 50-103
4-Nitroaniline 6670 4270 ug/Kg 64 52-103
4-Nitrophenol 13300 9142 ug/Kg 69 30-134
Acenaphthene 6670 4556 ug/Kg 68 50-100
Acenaphthylene 6670 4722 ug/Kg 71 52-100
Acetophenone 6670 4452 ug/Kg 67 48-100
Anthracene 6670 4827 ug/Kg 72 53-100
Atrazine 6670 4616 ug/Kg 69 49-103
Benzaldehyde 6670 5118 ug/Kg 77 23-105
Benzo[a]anthracene 6670 4778 ug/Kg 72 51-100
Benzo[a]pyrene 6670 4618 ug/Kg 69 51-100
Benzo[b]fluoranthene 6670 4741 ug/Kg 71 48-100
Benzo[g,h,i]perylene 6670 4508 ug/Kg 68 48-105
Benzo[k]fluoranthene 6670 4426 ug/Kg 66 19-100
Bis(2-chloroethoxy)methane 6670 4595 ug/Kg 69 49-100
Bis(2-chloroethyl)ether 6670 4700 ug/Kg 70 48-100
Bis(2-ethylhexyl) phthalate 6670 5592 ug/Kg 84 53-107
Butyl benzyl phthalate 6670 5585 ug/Kg 84 52-107
Carbazole 6670 4234 ug/Kg 64 53-100
Chrysene 6670 4136 ug/Kg 62 50-100
Dibenz(a,h)anthracene 6670 4860 ug/Kg 73 50-107
Dibenzofuran 6670 4792 ug/Kg 72 52-100
Diethyl phthalate 6670 4780 ug/Kg 72 48-104
Dimethyl phthalate 6670 4837 ug/Kg 73 53-100
Di-n-butyl phthalate 6670 4999 ug/Kg 75 57-102
Di-n-octyl phthalate 6670 5783 ug/Kg 87 41-106
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437429/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
Fluoranthene 6670 4581 ug/Kg 69 55-100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Fluorene 6670 4714 ug/Kg 71 52-100
Hexachlorobenzene 6670 5490 ug/Kg 82 49-100
Hexachlorobutadiene 6670 5224 ug/Kg 78 38-107
Hexachlorocyclopentadiene 6670 5231 ug/Kg 78 33-117
Hexachloroethane 6670 4777 ug/Kg 72 47-100
Indeno[1,2,3-cd]pyrene 6670 4739 ug/Kg 71 51-103
Isophorone 6670 4562 ug/Kg 68 48-105
Naphthalene 6670 4688 ug/Kg 70 51-100
Nitrobenzene 6670 4698 ug/Kg 70 44-108
N-Nitrosodi-n-propylamine 6670 4673 ug/Kg 70 45-107
N-Nitrosodiphenylamine 6670 5166 ug/Kg 77 52-100
Pentachlorophenol 13300 10230 ug/Kg 77 42-110
Phenanthrene 6670 4667 ug/Kg 70 53-100
Phenol 6670 4344 ug/Kg 65 49-100
Pyrene 6670 5224 ug/Kg 78 52-100
2,4,6-Tribromophenol (Surr)34 -108
Surrogate
82
LCS LCS
Qualifier Limits%Recovery
692-Fluorobiphenyl 44 -105
692-Fluorophenol (Surr)48 -105
66Nitrobenzene-d5 (Surr)46 -105
67Phenol-d5 (Surr)46 -105
78Terphenyl-d14 (Surr)39 -105
Client Sample ID: Matrix SpikeLab Sample ID: 140-31976-O-1-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
1,1'-Biphenyl ND 6620 5249 ug/Kg 79 50-100
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
2,2'-oxybis[1-chloropropane]ND 6620 4517 ug/Kg 68 30-113
2,4,5-Trichlorophenol ND F1 6620 2954 F1 ug/Kg 45 50-104
2,4,6-Trichlorophenol ND F1 F2 6620 399.5 F1 ug/Kg 6 50-105
2,4-Dichlorophenol ND F1 6620 201.7 F1 ug/Kg 3 53-101
2,4-Dimethylphenol ND F1 6620 208.6 J F1 ug/Kg 3 51-101
2,4-Dinitrophenol ND F1 13200 ND F1 ug/Kg 0 33-101
2,4-Dinitrotoluene ND 6620 3688 ug/Kg 56 54-104
2,6-Dinitrotoluene ND 6620 4527 ug/Kg 68 51-106
2-Chloronaphthalene ND 6620 3707 ug/Kg 56 51-100
2-Chlorophenol ND F1 6620 3270 F1 ug/Kg 49 51-100
2-Methylnaphthalene ND F1 6620 3371 F1 ug/Kg 51 53-100
2-Methylphenol ND F1 6620 1137 F1 ug/Kg 17 50-101
2-Nitroaniline ND 6620 3475 ug/Kg 52 42-123
2-Nitrophenol ND F1 6620 3508 F1 ug/Kg 53 55-107
3,3'-Dichlorobenzidine ND F1 6620 2257 F1 ug/Kg 34 43-100
3-Nitroaniline ND F1 6620 2916 F1 ug/Kg 44 50-103
4,6-Dinitro-2-methylphenol ND F1 F2 13200 2490 F1 ug/Kg 19 51-100
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 140-31976-O-1-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
4-Bromophenyl phenyl ether ND 6620 4914 ug/Kg 74 52-101
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
4-Chloro-3-methylphenol ND F1 6620 2444 F1 ug/Kg 37 49-106
4-Chloroaniline ND F1 6620 1649 F1 ug/Kg 25 47-100
4-Chlorophenyl phenyl ether ND 6620 4411 ug/Kg 67 52-100
Methylphenol, 3 & 4 ND F1 F2 6620 2331 F1 ug/Kg 35 50-103
4-Nitroaniline ND F1 6620 2608 F1 ug/Kg 39 52-103
4-Nitrophenol ND 13200 4997 ug/Kg 38 30-134
Acenaphthene ND 6620 3357 ug/Kg 51 50-100
Acenaphthylene ND 6620 3542 ug/Kg 53 52-100
Acetophenone ND 6620 3897 ug/Kg 59 48-100
Anthracene ND F1 6620 2558 F1 ug/Kg 39 53-100
Atrazine ND F1 6620 626.4 J F1 ug/Kg 9 49-103
Benzaldehyde ND 6620 3087 ug/Kg 47 23-105
Benzo[a]anthracene ND F1 6620 2670 F1 ug/Kg 40 51-100
Benzo[a]pyrene ND F1 6620 2557 F1 ug/Kg 39 51-100
Benzo[b]fluoranthene ND F1 6620 2342 F1 ug/Kg 35 48-100
Benzo[g,h,i]perylene ND 6620 3491 ug/Kg 53 48-105
Benzo[k]fluoranthene ND 6620 1999 ug/Kg 30 19-100
Bis(2-chloroethoxy)methane ND 6620 4377 ug/Kg 66 49-100
Bis(2-chloroethyl)ether 10000 F1 6620 11860 F1 ug/Kg 27 48-100
Bis(2-ethylhexyl) phthalate ND 6620 6571 ug/Kg 99 53-107
Butyl benzyl phthalate ND 6620 5532 ug/Kg 84 52-107
Carbazole ND F1 6620 2165 F1 ug/Kg 33 53-100
Chrysene ND F1 6620 2455 F1 ug/Kg 37 50-100
Dibenz(a,h)anthracene ND 6620 3562 ug/Kg 54 50-107
Dibenzofuran ND F1 6620 3013 F1 ug/Kg 45 52-100
Diethyl phthalate ND 6620 4820 ug/Kg 73 48-104
Dimethyl phthalate ND 6620 4833 ug/Kg 73 53-100
Di-n-butyl phthalate ND 6620 4768 ug/Kg 72 57-102
Di-n-octyl phthalate ND 6620 5108 ug/Kg 77 41-106
Fluoranthene ND F1 6620 2115 F1 ug/Kg 32 55-100
Fluorene ND F1 6620 3000 F1 ug/Kg 45 52-100
Hexachlorobenzene ND 6620 3975 ug/Kg 60 49-100
Hexachlorobutadiene ND 6620 4701 ug/Kg 71 38-107
Hexachlorocyclopentadiene ND F1 6620 1557 F1 ug/Kg 24 33-117
Hexachloroethane ND 6620 4491 ug/Kg 68 47-100
Indeno[1,2,3-cd]pyrene ND 6620 3572 ug/Kg 54 51-103
Isophorone ND 6620 3774 ug/Kg 57 48-105
Naphthalene ND 6620 4066 ug/Kg 61 51-100
Nitrobenzene ND 6620 4721 ug/Kg 71 44-108
N-Nitrosodi-n-propylamine ND 6620 4790 ug/Kg 72 45-107
N-Nitrosodiphenylamine ND 6620 4014 ug/Kg 61 52-100
Pentachlorophenol ND F1 13200 4713 F1 ug/Kg 36 42-110
Phenanthrene ND F1 6620 2800 F1 ug/Kg 42 53-100
Phenol ND F1 6620 2227 F1 ug/Kg 34 49-100
Pyrene ND F1 6620 2836 F1 ug/Kg 43 52-100
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 140-31976-O-1-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
2,4,6-Tribromophenol (Surr)34 -108
Surrogate
49
MS MS
Qualifier Limits%Recovery
602-Fluorobiphenyl 44 -105
552-Fluorophenol (Surr)48 -105
55Nitrobenzene-d5 (Surr)46 -105
50Phenol-d5 (Surr)46 -105
43Terphenyl-d14 (Surr)39 -105
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 140-31976-O-1-B MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
1,1'-Biphenyl ND 6580 5362 ug/Kg 82 50-100 2 19
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
2,2'-oxybis[1-chloropropane]ND 6580 4679 ug/Kg 71 30-113 4 17
2,4,5-Trichlorophenol ND F1 6580 2992 F1 ug/Kg 45 50-104 1 21
2,4,6-Trichlorophenol ND F1 F2 6580 304.2 J F1 F2 ug/Kg 5 50-105 27 21
2,4-Dichlorophenol ND F1 6580 230.0 F1 ug/Kg 3 53-101 13 22
2,4-Dimethylphenol ND F1 6580 182.1 J F1 ug/Kg 3 51-101 14 32
2,4-Dinitrophenol ND F1 13200 ND F1 ug/Kg 0 33-101 NC 20
2,4-Dinitrotoluene ND 6580 3826 ug/Kg 58 54-104 4 20
2,6-Dinitrotoluene ND 6580 4583 ug/Kg 70 51-106 1 20
2-Chloronaphthalene ND 6580 3835 ug/Kg 58 51-100 3 20
2-Chlorophenol ND F1 6580 3441 ug/Kg 52 51-100 5 17
2-Methylnaphthalene ND F1 6580 3470 ug/Kg 53 53-100 3 21
2-Methylphenol ND F1 6580 1264 F1 ug/Kg 19 50-101 11 17
2-Nitroaniline ND 6580 3698 ug/Kg 56 42-123 6 19
2-Nitrophenol ND F1 6580 3647 ug/Kg 55 55-107 4 19
3,3'-Dichlorobenzidine ND F1 6580 2554 F1 ug/Kg 39 43-100 12 19
3-Nitroaniline ND F1 6580 2981 F1 ug/Kg 45 50-103 2 20
4,6-Dinitro-2-methylphenol ND F1 F2 13200 3328 F1 F2 ug/Kg 25 51-100 29 22
4-Bromophenyl phenyl ether ND 6580 5043 ug/Kg 77 52-101 3 20
4-Chloro-3-methylphenol ND F1 6580 2749 F1 ug/Kg 42 49-106 12 20
4-Chloroaniline ND F1 6580 1710 F1 ug/Kg 26 47-100 4 20
4-Chlorophenyl phenyl ether ND 6580 4507 ug/Kg 69 52-100 2 19
Methylphenol, 3 & 4 ND F1 F2 6580 1847 F1 F2 ug/Kg 28 50-103 23 19
4-Nitroaniline ND F1 6580 2678 F1 ug/Kg 41 52-103 3 18
4-Nitrophenol ND 13200 5433 ug/Kg 41 30-134 8 18
Acenaphthene ND 6580 3429 ug/Kg 52 50-100 2 20
Acenaphthylene ND 6580 3668 ug/Kg 56 52-100 3 20
Acetophenone ND 6580 4032 ug/Kg 61 48-100 3 17
Anthracene ND F1 6580 2597 F1 ug/Kg 39 53-100 2 20
Atrazine ND F1 6580 727.3 F1 ug/Kg 11 49-103 15 19
Benzaldehyde ND 6580 3145 ug/Kg 48 23-105 2 31
Benzo[a]anthracene ND F1 6580 2909 F1 ug/Kg 44 51-100 9 21
Benzo[a]pyrene ND F1 6580 2725 F1 ug/Kg 41 51-100 6 20
Benzo[b]fluoranthene ND F1 6580 2512 F1 ug/Kg 38 48-100 7 20
Benzo[g,h,i]perylene ND 6580 3358 ug/Kg 51 48-105 4 19
Benzo[k]fluoranthene ND 6580 2196 ug/Kg 33 19-100 9 20
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 140-31976-O-1-B MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
Bis(2-chloroethoxy)methane ND 6580 4527 ug/Kg 69 49-100 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Bis(2-chloroethyl)ether 10000 F1 6580 11820 F1 ug/Kg 27 48-100 0 18
Bis(2-ethylhexyl) phthalate ND 6580 6423 ug/Kg 98 53-107 2 20
Butyl benzyl phthalate ND 6580 5847 ug/Kg 89 52-107 6 19
Carbazole ND F1 6580 2296 F1 ug/Kg 35 53-100 6 20
Chrysene ND F1 6580 2650 F1 ug/Kg 40 50-100 8 20
Dibenz(a,h)anthracene ND 6580 3710 ug/Kg 56 50-107 4 21
Dibenzofuran ND F1 6580 3141 F1 ug/Kg 48 52-100 4 19
Diethyl phthalate ND 6580 4973 ug/Kg 76 48-104 3 20
Dimethyl phthalate ND 6580 4954 ug/Kg 75 53-100 2 21
Di-n-butyl phthalate ND 6580 4714 ug/Kg 72 57-102 1 20
Di-n-octyl phthalate ND 6580 5225 ug/Kg 79 41-106 2 18
Fluoranthene ND F1 6580 2347 F1 ug/Kg 36 55-100 10 20
Fluorene ND F1 6580 3109 F1 ug/Kg 47 52-100 4 19
Hexachlorobenzene ND 6580 4122 ug/Kg 63 49-100 4 20
Hexachlorobutadiene ND 6580 4913 ug/Kg 75 38-107 4 22
Hexachlorocyclopentadiene ND F1 6580 1654 F1 ug/Kg 25 33-117 6 19
Hexachloroethane ND 6580 4673 ug/Kg 71 47-100 4 17
Indeno[1,2,3-cd]pyrene ND 6580 3537 ug/Kg 54 51-103 1 19
Isophorone ND 6580 3962 ug/Kg 60 48-105 5 20
Naphthalene ND 6580 4261 ug/Kg 65 51-100 5 20
Nitrobenzene ND 6580 4897 ug/Kg 74 44-108 4 21
N-Nitrosodi-n-propylamine ND 6580 4920 ug/Kg 75 45-107 3 18
N-Nitrosodiphenylamine ND 6580 4065 ug/Kg 62 52-100 1 20
Pentachlorophenol ND F1 13200 4770 F1 ug/Kg 36 42-110 1 20
Phenanthrene ND F1 6580 2892 F1 ug/Kg 44 53-100 3 20
Phenol ND F1 6580 2465 F1 ug/Kg 37 49-100 10 16
Pyrene ND F1 6580 3030 F1 ug/Kg 46 52-100 7 20
2,4,6-Tribromophenol (Surr)34 -108
Surrogate
53
MSD MSD
Qualifier Limits%Recovery
632-Fluorobiphenyl 44 -105
582-Fluorophenol (Surr)48 -105
58Nitrobenzene-d5 (Surr)46 -105
53Phenol-d5 (Surr)46 -105
46Terphenyl-d14 (Surr)39 -105
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-385316/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 385316
RL MDL
C5-C8 Aliphatics (unadjusted)ND 100 25.0 ug/L 06/12/23 10:07 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10.0100 ug/L 06/12/23 10:07 1C9-C10 Aromatics
ND 25.0100 ug/L 06/12/23 10:07 1C9-C12 Aliphatics (unadjusted)
ND 25.0100 ug/L 06/12/23 10:07 1C9-C12 Aliphatics (adjusted)
ND 25.0100 ug/L 06/12/23 10:07 1C5-C8 Aliphatics (adjusted)
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
a,a,a-Trifluorotoluene (fid)109 70-130 06/12/23 10:07 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 06/12/23 10:07 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-385316/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 385316
C5-C8 Aliphatics (unadjusted)151 147.6 ug/L 98 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 50.2 45.69 J ug/L 91 70-130
C9-C12 Aliphatics (unadjusted)151 132.4 ug/L 88 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
109
LCS LCS
Qualifier Limits%Recovery
97a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-385316/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 385316
C5-C8 Aliphatics (unadjusted)151 148.0 ug/L 98 70-130 0 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 50.2 45.98 J ug/L 92 70-130 1 25
C9-C12 Aliphatics (unadjusted)151 134.3 ug/L 89 70-130 1 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
109
LCSD LCSD
Qualifier Limits%Recovery
97a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 410-386087/23-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 386298 Prep Batch: 386087
RL MDL
C5-C8 Aliphatics (unadjusted)ND 5.00 1.25 mg/Kg 06/14/23 07:06 06/14/23 09:42 50
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.255.00 mg/Kg 06/14/23 07:06 06/14/23 09:42 50C9-C10 Aromatics
ND 1.255.00 mg/Kg 06/14/23 07:06 06/14/23 09:42 50C9-C12 Aliphatics (unadjusted)
ND 1.255.00 mg/Kg 06/14/23 07:06 06/14/23 09:42 50C9-C12 Aliphatics (adjusted)
ND 1.255.00 mg/Kg 06/14/23 07:06 06/14/23 09:42 50C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)99 70-130 06/14/23 09:42 50
MB MB
Surrogate
06/14/23 07:06
Dil FacPreparedAnalyzedQualifierLimits%Recovery
86 06/14/23 07:06 06/14/23 09:42 50a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-386087/24-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 386298 Prep Batch: 386087
C5-C8 Aliphatics (unadjusted)7.53 6.104 mg/Kg 81 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 2.51 2.198 J mg/Kg 88 70-130
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-386087/24-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 386298 Prep Batch: 386087
C9-C12 Aliphatics (unadjusted)7.53 6.377 mg/Kg 85 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
87a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-386087/25-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 386298 Prep Batch: 386087
C5-C8 Aliphatics (unadjusted)7.53 6.220 mg/Kg 83 70-130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 2.51 2.208 J mg/Kg 88 70-130 0 30
C9-C12 Aliphatics (unadjusted)7.53 6.505 mg/Kg 86 70-130 2 30
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
89a,a,a-Trifluorotoluene (pid)70 -130
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-383574/1-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388785 Prep Batch: 383574
RL MDL
C19-C36 Aliphatics ND 12.0 12.0 mg/Kg 06/06/23 16:31 06/20/23 19:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 6.006.00 mg/Kg 06/06/23 16:31 06/20/23 19:38 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)48 40-140 06/20/23 19:38 1
MB MB
Surrogate
06/06/23 16:31
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-383574/1-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388783 Prep Batch: 383574
RL MDL
C11-C22 Aromatics (unadjusted)ND 12.0 12.0 mg/Kg 06/06/23 16:31 06/20/23 19:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 12.012.0 mg/Kg 06/06/23 16:31 06/20/23 19:38 1C11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)70 40-140 06/20/23 19:38 1
MB MB
Surrogate
06/06/23 16:31
Dil FacPreparedAnalyzedQualifierLimits%Recovery
61 06/06/23 16:31 06/20/23 19:38 1o- terphenyl (Surr)40-140
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-383574/2-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388785 Prep Batch: 383574
C19-C36 Aliphatics 32.1 24.50 mg/Kg 76 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 24.1 19.14 mg/Kg 79 40-140
1-Chlorooctadecane (Surr)40 -140
Surrogate
47
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-383574/2-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388783 Prep Batch: 383574
C11-C22 Aromatics (unadjusted)68.1 42.96 mg/Kg 63 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Fluorobiphenyl (Surr)40 -140
Surrogate
69
LCS LCS
Qualifier Limits%Recovery
59o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-383574/3-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388785 Prep Batch: 383574
C19-C36 Aliphatics 32.1 25.41 mg/Kg 79 40-140 4 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 24.1 19.78 mg/Kg 82 40-140 3 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
61
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-383574/3-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388783 Prep Batch: 383574
C11-C22 Aromatics (unadjusted)68.1 48.00 mg/Kg 70 40-140 11 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)40 -140
Surrogate
75
LCSD LCSD
Qualifier Limits%Recovery
67o- terphenyl (Surr)40 -140
Client Sample ID: EB-6B (3-5)Lab Sample ID: 180-157266-2 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388783 Prep Batch: 383574
C11-C22 Aromatics (unadjusted)ND 92.4 51.48 mg/Kg 56 40-140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
C19-C36 Aliphatics ND 43.6 31.52 mg/Kg 72 40-140☼
C9-C18 Aliphatics ND F1 32.7 47.97 F1 mg/Kg 147 40-140☼
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: EB-6B (3-5)Lab Sample ID: 180-157266-2 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388785 Prep Batch: 383574
1-Chlorooctadecane (Surr)40 -140
Surrogate
50
MS MS
Qualifier Limits%Recovery
692-Fluorobiphenyl (Surr)40 -140
50o- terphenyl (Surr)40 -140
Client Sample ID: EB-6B (3-5)Lab Sample ID: 180-157266-2 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388783 Prep Batch: 383574
C11-C22 Aromatics (unadjusted)ND 92.6 61.91 mg/Kg 67 40-140 18 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
C19-C36 Aliphatics ND 43.7 29.91 mg/Kg 68 40-140 5 50☼
C9-C18 Aliphatics ND F1 32.8 52.57 F1 mg/Kg 160 40-140 9 50☼
1-Chlorooctadecane (Surr)40 -140
Surrogate
55
MSD MSD
Qualifier Limits%Recovery
772-Fluorobiphenyl (Surr)40 -140
60o- terphenyl (Surr)40 -140
Client Sample ID: Method BlankLab Sample ID: MB 410-385076/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
RL MDL
C19-C36 Aliphatics ND 50.0 50.0 ug/L 06/09/23 19:11 06/27/23 02:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 30.030.0 ug/L 06/09/23 19:11 06/27/23 02:30 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)59 40-140 06/27/23 02:30 1
MB MB
Surrogate
06/09/23 19:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-385076/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390845 Prep Batch: 385076
RL MDL
C11-C22 Aromatics (unadjusted)ND 40.0 40.0 ug/L 06/09/23 19:11 06/27/23 02:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 40.040.0 ug/L 06/09/23 19:11 06/27/23 02:30 1C11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)79 40-140 06/27/23 02:30 1
MB MB
Surrogate
06/09/23 19:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
64 06/09/23 19:11 06/27/23 02:30 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-385076/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
C19-C36 Aliphatics 321 191.4 ug/L 60 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 157.7 ug/L 65 40-140
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157266-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
1-Chlorooctadecane (Surr)40 -140
Surrogate
54
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-385076/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390845 Prep Batch: 385076
C11-C22 Aromatics (unadjusted)681 480.1 ug/L 70 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Fluorobiphenyl (Surr)40 -140
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
77o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-385076/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
C19-C36 Aliphatics 321 195.7 ug/L 61 40-140 2 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 241 158.1 ug/L 66 40-140 0 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
60
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-385076/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390845 Prep Batch: 385076
C11-C22 Aromatics (unadjusted)681 448.9 ug/L 66 40-140 7 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)40 -140
Surrogate
83
LCSD LCSD
Qualifier Limits%Recovery
75o- terphenyl (Surr)40 -140
Method: 2540G - SM 2540G
Client Sample ID: EB-15 (8-10)Lab Sample ID: 180-157266-6 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437029
Percent Moisture 29.8 31.5 %6 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 70.2 68.5 %3 10
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-157266-1
SDG Number: 640 Rock Lane
Login Number: 157266
Question Answer Comment
Creator: Abernathy, Eric L
List Source: Eurofins Pittsburgh
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-157266-1
SDG Number: 640 Rock Lane
Login Number: 157266
Question Answer Comment
Creator: McCaskey, Jonathan
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 06/01/23 01:14 PMList Number: 2
N/AThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
FalseThere are no discrepancies between the containers received and the COC.Refer to Job Narrative for details.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
N/AVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-157266-1
SDG Number: 640 Rock Lane
Login Number: 157266
Question Answer Comment
Creator: McBeth, Jessica
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 06/09/23 10:33 AMList Number: 3
N/AThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
FalseCooler Temperature is acceptable (</=6C, not frozen).Refer to Job Narrative for details.
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
FalseCOC is present.Refer to Job Narrative for details.
N/ACOC is filled out in ink and legible.
N/ACOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
N/AIs the Field Sampler's name present on COC?
N/ASample custody seals are intact.
TrueVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
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ANALYTICAL REPORT
PREPARED FOR
Attn: Mr. Bruce Stainbrook
Altec Industries, Inc
Bruce Stainbrook
810 Franklin Court, Ste A
Marietta, Georgia 30067
Generated 6/28/2023 4:14:37 PM
JOB DESCRIPTION
China Grove NC
SDG NUMBER 640 Rock Lane
JOB NUMBER
180-157361-1
See page two for job notes and contact information.
Pittsburgh PA 15238
RIDC Park
301 Alpha Drive
Eurofins Pittsburgh
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Eurofins Pittsburgh
Eurofins Pittsburgh is a laboratory within Eurofins Environment Testing Northeast LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
PA Lab ID: 02-00416
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Pittsburgh Project Manager.
Authorization
Generated
6/28/2023 4:14:37 PM
Authorized for release by
Shali Brown, Project Manager II
[e-mail]
[phone]
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Case Narrative
Client: Altec Industries, Inc Job ID: 180-157361-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-157361-1
Laboratory: Eurofins Pittsburgh
Narrative
Job Narrative
180-157361-1
Receipt
The samples were received on 6/1/2023 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 3.1°C and 5.8°C
Receipt Exceptions
USDA Compliance agreement documentation to be submitted was either missing or incomplete for the following samples: TMW-1
(180-157266-1), EB-6B (3-5) (180-157266-2), EB-7B (8-10) (180-157266-3), EB-10 (8-10) (180-157266-4), EB-11 (3-5) (180-157266-5),
EB-15 (8-10) (180-157266-6), EB-12 (2-4) (180-157361-1), EB-12 (6-8) (180-157361-2), EB-13 (6-8) (180-157361-3), EB-14 (8-10)
(180-157361-4), EB-16 (2-3) (180-157361-5), EB-17 (8-10) (180-157361-6), TMW-2 (180-157361-7), TMW-3 (180-157361-8), TMW-4
(180-157361-9) and TMW-8 (180-157361-10).
The following samples were found to be frozen solid upon receipt by the laboratory. The samples and containers appeared to be intact.
TMW-1 (180-157266-1), EB-6B (3-5) (180-157266-2), EB-7B (8-10) (180-157266-3), EB-10 (8-10) (180-157266-4), EB-11 (3-5)
(180-157266-5), EB-15 (8-10) (180-157266-6), EB-12 (2-4) (180-157361-1), EB-12 (6-8) (180-157361-2), EB-13 (6-8) (180-157361-3),
EB-14 (8-10) (180-157361-4), EB-16 (2-3) (180-157361-5) and EB-17 (8-10) (180-157361-6)
GC/MS VOA
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-436900 was outside the method criteria for the
following analyte(s): Chlorodibromomethane, Dichloro-difluoromethane, Bromoform and 1,2-Dibromo-3-Chloropropane.(LOW). A CCV
standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the
reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated.
Method 8260D: The continuing calibration verification (CCV) analyzed in 180-436900 was outside the method criteria for the following
analyte(s): Trichlorofluoromethane and Methyl acetate.(HIGH). As indicated in the reference method, sample analysis may proceed;
however, any detection for the affected analyte(s) is considered estimated.
Method 8260D: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch 180-436900
recovered outside control limits for the following analytes: Methyl acetate. These analytes were biased high in the LCS and were not
detected in the associated samples; therefore, the data have been reported.
Method 8260D: The laboratory control sample (LCS) for analytical batch 180-437362 recovered outside control limits for the following
analyte: Trichlorofluoromethane. This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the
data have been reported.
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-437362 was outside the method criteria for the
following surrogate: 1,2-Dichloroethane-d4 (LOW). All samples recovered this surrogate within QC criteria.
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-437362 was outside the method criteria for the
following analytes: 1,2-Dibromo-3-Chloropropane, 1,1,2,2-Tetrachloroethane, Bromoform, Chlorodibromomethane, Chloroethane and
Dichloro-difluoromethane. (LOW). A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found
to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s)
is considered estimated.
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-437362 was outside the method criteria for the
following analyte: Methyl acetate. (LOW MINIMUM RRF). A low-level LCS (LLCS), spiked at the reporting limit (RL), was prepared with this
batch. The affected target analyte recovered within acceptance limits; therefore, the LLCS demonstrates the analytical system had
sufficient sensitivity to detect the compound.
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Case Narrative
Client: Altec Industries, Inc Job ID: 180-157361-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-157361-1 (Continued)
Laboratory: Eurofins Pittsburgh (Continued)
Method 8260D_LL: The continuing calibration verification (CCV) analyzed in batch 180-437251 was outside the method criteria for the
following analyte(s): 1,2-Dichloroethane-d4. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples
and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected
analyte(s) is considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
Method 8270E: The continuing calibration verification (CCV) associated with batch 180-437462 recovered above the upper control limit for
Hexachlorocyclopentadiene. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have
been reported. The associated sample is impacted: (CCVIS 180-437462/3).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
Method MAVPH: Surrogate recovery for the following samples were outside the upper control limit: EB-14 (8-10) (180-157361-4) and
EB-17 (8-10) (180-157361-6). This sample did not contain any target analytes; therefore, re-extraction and/or re-analysis was not
performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method MAEPH2.1: The breakthrough for naphthalene is 5% and the breakthrough for 2-methylnaphthalene is 2% in the LCS. The
breakthrough for naphthalene is 4% and the breakthrough for 2-methylnaphthalene is 2% in the LCSD. The method requirement for
breakthrough is 5% or less. TMW-2 (180-157361-7), TMW-3 (180-157361-8), TMW-4 (180-157361-9) and TMW-8 (180-157361-10)
Method MAEPH2.1: Surrogate recovery for the following sample was outside control limits: EB-12 (2-4) (180-157361-1). The matrix of the
sample is clay which is known to cause interference and suppress surrogate recoveries; therefore, re-extraction and/or re-analysis was
not performed.
Method MAEPH2.1: The breakthrough for naphthalene and 2-methylnaphthalene in the LCS and LCSD is <1%. The method requirement
for breakthrough is <5%. EB-12 (2-4) (180-157361-1), EB-12 (6-8) (180-157361-2), EB-13 (6-8) (180-157361-3), EB-14 (8-10)
(180-157361-4), EB-16 (2-3) (180-157361-5) and EB-17 (8-10) (180-157361-6)
Method MAEPH2.1: Surrogate recovery for the following sample was outside control limits: EB-12 (6-8) (180-157361-2). The matrix of the
sample is clay which is known to cause interference and suppress surrogate recoveries; therefore, re-extraction and/or re-analysis was
not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Definitions/Glossary
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
F2 MS/MSD RPD exceeds control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
S1-Surrogate recovery exceeds control limits, low biased.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Accreditation/Certification Summary
Client: Altec Industries, Inc Job ID: 180-157361-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Laboratory: Eurofins Pittsburgh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 434 12-31-23
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 521 12-31-23
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-1Client Sample ID: EB-12 (2-4)
Matrix: SolidDate Collected: 05/31/23 13:00
Percent Solids: 66.8Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
16.6 6.61 2.21 ug/Kg ☼06/02/23 07:05 06/03/23 20:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
6.61 2.01 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,1,2,2-Tetrachloroethane
6.61 2.65 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
6.61 1.31 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,1,2-Trichloroethane
6.61 2.12 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,1-Dichloroethane
6.61 2.99 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,1-Dichloroethene
6.61 4.27 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,2-Dibromo-3-Chloropropane
6.61 2.22 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,2-Dichlorobenzene
6.61 1.90 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,2-Dichloroethane
6.61 1.76 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,2-Dichloropropane
6.61 3.36 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,2,4-Trichlorobenzene
6.61 4.07 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,3-Dichlorobenzene
6.61 1.98 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,4-Dichlorobenzene
33.1 3.36 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND2-Butanone (MEK)
33.1 2.08 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND2-Hexanone
33.1 2.42 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND4-Methyl-2-pentanone (MIBK)
33.1 5.16 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDAcetone
6.61 1.86 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDBenzene
6.61 3.33 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDBromoform
6.61 3.02 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDBromomethane
6.61 5.29 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDCarbon disulfide
6.61 2.68 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDCarbon tetrachloride
6.61 1.72 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDChlorobenzene
6.61 3.28 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDChlorodibromomethane
6.61 4.43 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDChloroform
6.61 2.62 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDChloromethane
6.61 3.86 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDChloroethane
6.61 2.00 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDcis-1,2-Dichloroethene
6.61 2.92 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDcis-1,3-Dichloropropene
6.61 3.08 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDDichlorobromomethane
6.61 3.29 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDDichlorodifluoromethane
6.61 2.45 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDEthylbenzene
6.61 1.81 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND1,2-Dibromoethane
6.61 3.16 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDCyclohexane
6.61 3.44 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDIsopropylbenzene
33.1 9.73 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼ND *+Methyl acetate
6.61 1.94 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDMethyl tert-butyl ether
6.61 3.19 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDMethylcyclohexane
6.61 5.96 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDMethylene Chloride
6.61 1.98 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDStyrene
6.61 2.66 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDTetrachloroethene
6.61 1.90 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDToluene
6.61 2.31 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDtrans-1,2-Dichloroethene
6.61 2.98 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDtrans-1,3-Dichloropropene
6.61 2.08 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDTrichloroethene
6.61 5.49 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDTrichlorofluoromethane
6.61 4.76 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDVinyl chloride
13.2 9.54 ug/Kg 06/02/23 07:05 06/03/23 20:32 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-1Client Sample ID: EB-12 (2-4)
Matrix: SolidDate Collected: 05/31/23 13:00
Percent Solids: 66.8Date Received: 06/01/23 10:30
1,2-Dichloroethane-d4 (Surr)116 73-135 06/02/23 07:05 06/03/23 20:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 06/02/23 07:05 06/03/23 20:32 160-124
Dibromofluoromethane (Surr)110 06/02/23 07:05 06/03/23 20:32 169-126
Toluene-d8 (Surr)95 06/02/23 07:05 06/03/23 20:32 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 487 180 ug/Kg ☼06/08/23 16:27 06/09/23 18:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
99.0 36.5 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2,2'-oxybis[1-chloropropane]
487 171 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2,4,5-Trichlorophenol
487 164 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2,4,6-Trichlorophenol
99.0 38.0 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2,4-Dichlorophenol
487 165 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2,4-Dimethylphenol
4870 3060 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2,4-Dinitrophenol
487 294 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2,4-Dinitrotoluene
487 192 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2,6-Dinitrotoluene
99.0 22.6 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2-Chloronaphthalene
487 182 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2-Chlorophenol
99.0 23.6 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2-Methylnaphthalene
487 141 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2-Methylphenol
2510 225 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2-Nitroaniline
487 182 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND2-Nitrophenol
487 459 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND3,3'-Dichlorobenzidine
2510 125 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND3-Nitroaniline
2510 849 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND4,6-Dinitro-2-methylphenol
487 210 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND4-Bromophenyl phenyl ether
487 173 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND4-Chloro-3-methylphenol
487 129 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND4-Chloroaniline
487 164 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND4-Chlorophenyl phenyl ether
487 145 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDMethylphenol, 3 & 4
2510 183 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND4-Nitroaniline
2510 346 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼ND4-Nitrophenol
99.0 28.4 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDAcenaphthene
99.0 21.6 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDAcenaphthylene
990 176 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDAcetophenone
99.0 25.6 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDAnthracene
990 216 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDAtrazine
990 61.2 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDBenzaldehyde
99.0 44.5 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDBenzo[a]anthracene
99.0 42.7 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDBenzo[a]pyrene
99.0 24.2 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDBenzo[b]fluoranthene
99.0 21.3 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDBenzo[g,h,i]perylene
99.0 29.5 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDBenzo[k]fluoranthene
487 180 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDBis(2-chloroethoxy)methane
99.0 17.9 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDBis(2-chloroethyl)ether
4870 524 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDBis(2-ethylhexyl) phthalate
487 338 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDButyl benzyl phthalate
2510 321 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDCaprolactam
99.0 23.0 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDCarbazole
99.0 54.7 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDChrysene
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-1Client Sample ID: EB-12 (2-4)
Matrix: SolidDate Collected: 05/31/23 13:00
Percent Solids: 66.8Date Received: 06/01/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 99.0 63.1 ug/Kg ☼06/08/23 16:27 06/09/23 18:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
487 182 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDDibenzofuran
487 173 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDDiethyl phthalate
487 195 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDDimethyl phthalate
487 216 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDDi-n-butyl phthalate
487 287 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDDi-n-octyl phthalate
99.0 26.0 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDFluoranthene
99.0 19.4 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDFluorene
99.0 35.3 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDHexachlorobenzene
99.0 28.8 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDHexachlorobutadiene
487 50.4 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDHexachlorocyclopentadiene
487 174 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDHexachloroethane
99.0 49.0 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDIndeno[1,2,3-cd]pyrene
487 185 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDIsophorone
99.0 19.2 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDNaphthalene
990 180 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDNitrobenzene
99.0 33.4 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDN-Nitrosodi-n-propylamine
487 164 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDN-Nitrosodiphenylamine
2510 792 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDPentachlorophenol
99.0 26.4 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDPhenanthrene
487 149 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDPhenol
99.0 23.3 ug/Kg 06/08/23 16:27 06/09/23 18:12 1☼NDPyrene
2,4,6-Tribromophenol (Surr)76 34-108 06/08/23 16:27 06/09/23 18:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 74 06/08/23 16:27 06/09/23 18:12 144-105
2-Fluorophenol (Surr)73 06/08/23 16:27 06/09/23 18:12 148-105
Nitrobenzene-d5 (Surr)70 06/08/23 16:27 06/09/23 18:12 146-105
Phenol-d5 (Surr)69 06/08/23 16:27 06/09/23 18:12 146-105
Terphenyl-d14 (Surr)83 06/08/23 16:27 06/09/23 18:12 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
194 7.48 1.87 mg/Kg ☼06/15/23 08:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
8.19 J 25.6 6.41 mg/Kg ☼06/13/23 15:06 06/14/23 13:50 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
25.6 6.41 mg/Kg 06/13/23 15:06 06/14/23 13:50 50☼61.2C9-C10 Aromatics
25.6 6.41 mg/Kg 06/13/23 15:06 06/14/23 13:50 50☼186C9-C12 Aliphatics (unadjusted)
25.6 6.41 mg/Kg 06/13/23 15:06 06/14/23 13:50 50☼123C9-C12 Aliphatics (adjusted)
25.6 6.41 mg/Kg 06/13/23 15:06 06/14/23 13:50 50☼8.18 JC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)111 70-130 06/13/23 15:06 06/14/23 13:50 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)96 06/13/23 15:06 06/14/23 13:50 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
49.0 17.3 17.3 mg/Kg ☼06/06/23 16:31 06/20/23 23:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
17.3 17.3 mg/Kg 06/06/23 16:31 06/20/23 23:21 1☼43.6C11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-1Client Sample ID: EB-12 (2-4)
Matrix: SolidDate Collected: 05/31/23 13:00
Percent Solids: 66.8Date Received: 06/01/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
39.0 8.65 8.65 mg/Kg ☼06/06/23 16:31 06/20/23 23:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C9-C18 Aliphatics
1-Chlorooctadecane (Surr)33 S1-40-140 06/06/23 16:31 06/20/23 23:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)65 06/06/23 16:31 06/20/23 23:21 140-140
o- terphenyl (Surr)38 S1-06/06/23 16:31 06/20/23 23:21 140-140
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - DL
RL MDL
934 86.5 86.5 mg/Kg ☼06/06/23 16:31 06/21/23 15:05 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
1-Chlorooctadecane (Surr)40 40-140 06/06/23 16:31 06/21/23 15:05 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
1020 18.0 18.0 mg/Kg ☼06/27/23 19:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
33.2 0.1 0.1 %06/06/23 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/06/23 14:44 166.8Percent Solids (SM22 2540G)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-2Client Sample ID: EB-12 (6-8)
Matrix: SolidDate Collected: 05/31/23 13:10
Percent Solids: 71.7Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
18.9 6.27 2.10 ug/Kg ☼06/02/23 07:05 06/03/23 20:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
6.27 1.91 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,1,2,2-Tetrachloroethane
6.27 2.51 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
6.27 1.24 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,1,2-Trichloroethane
6.27 2.01 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,1-Dichloroethane
6.27 2.84 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,1-Dichloroethene
6.27 4.05 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,2-Dibromo-3-Chloropropane
6.27 2.11 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,2-Dichlorobenzene
6.27 1.81 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,2-Dichloroethane
6.27 1.67 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,2-Dichloropropane
6.27 3.19 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,2,4-Trichlorobenzene
6.27 3.86 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,3-Dichlorobenzene
6.27 1.88 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,4-Dichlorobenzene
31.4 3.19 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND2-Butanone (MEK)
31.4 1.97 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND2-Hexanone
31.4 2.30 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND4-Methyl-2-pentanone (MIBK)
31.4 4.89 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDAcetone
6.27 1.77 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDBenzene
6.27 3.16 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDBromoform
6.27 2.86 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDBromomethane
6.27 5.02 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDCarbon disulfide
6.27 2.55 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDCarbon tetrachloride
6.27 1.63 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDChlorobenzene
6.27 3.11 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDChlorodibromomethane
6.27 4.20 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDChloroform
6.27 2.48 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDChloromethane
6.27 3.66 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDChloroethane
6.27 1.89 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDcis-1,2-Dichloroethene
6.27 2.77 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDcis-1,3-Dichloropropene
6.27 2.92 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDDichlorobromomethane
6.27 3.12 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDDichlorodifluoromethane
6.27 2.32 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDEthylbenzene
6.27 1.72 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND1,2-Dibromoethane
6.27 3.00 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDCyclohexane
6.27 3.26 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDIsopropylbenzene
31.4 9.24 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼ND *+Methyl acetate
6.27 1.84 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDMethyl tert-butyl ether
6.27 3.02 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDMethylcyclohexane
6.27 5.66 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDMethylene Chloride
6.27 1.88 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDStyrene
6.27 2.52 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDTetrachloroethene
6.27 1.81 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDToluene
6.27 2.20 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDtrans-1,2-Dichloroethene
6.27 2.82 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDtrans-1,3-Dichloropropene
6.27 1.97 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDTrichloroethene
6.27 5.21 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDTrichlorofluoromethane
6.27 4.52 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDVinyl chloride
12.5 9.05 ug/Kg 06/02/23 07:05 06/03/23 20:55 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-2Client Sample ID: EB-12 (6-8)
Matrix: SolidDate Collected: 05/31/23 13:10
Percent Solids: 71.7Date Received: 06/01/23 10:30
1,2-Dichloroethane-d4 (Surr)128 73-135 06/02/23 07:05 06/03/23 20:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)102 06/02/23 07:05 06/03/23 20:55 160-124
Dibromofluoromethane (Surr)117 06/02/23 07:05 06/03/23 20:55 169-126
Toluene-d8 (Surr)97 06/02/23 07:05 06/03/23 20:55 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 451 167 ug/Kg ☼06/08/23 16:27 06/09/23 18:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
91.6 33.8 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2,2'-oxybis[1-chloropropane]
451 159 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2,4,5-Trichlorophenol
451 152 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2,4,6-Trichlorophenol
91.6 35.1 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2,4-Dichlorophenol
451 153 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2,4-Dimethylphenol
4510 2830 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2,4-Dinitrophenol
451 272 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2,4-Dinitrotoluene
451 178 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2,6-Dinitrotoluene
91.6 20.9 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2-Chloronaphthalene
451 168 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2-Chlorophenol
91.6 21.9 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2-Methylnaphthalene
451 131 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2-Methylphenol
2320 208 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2-Nitroaniline
451 168 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND2-Nitrophenol
451 425 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND3,3'-Dichlorobenzidine
2320 116 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND3-Nitroaniline
2320 786 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND4,6-Dinitro-2-methylphenol
451 194 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND4-Bromophenyl phenyl ether
451 160 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND4-Chloro-3-methylphenol
451 120 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND4-Chloroaniline
451 152 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND4-Chlorophenyl phenyl ether
451 134 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDMethylphenol, 3 & 4
2320 170 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND4-Nitroaniline
2320 320 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼ND4-Nitrophenol
91.6 26.3 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDAcenaphthene
91.6 20.0 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDAcenaphthylene
916 163 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDAcetophenone
91.6 23.7 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼85.3 JAnthracene
916 200 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDAtrazine
916 56.6 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDBenzaldehyde
91.6 41.2 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼99.8Benzo[a]anthracene
91.6 39.5 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDBenzo[a]pyrene
91.6 22.4 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼56.5 JBenzo[b]fluoranthene
91.6 19.7 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDBenzo[g,h,i]perylene
91.6 27.3 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDBenzo[k]fluoranthene
451 167 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDBis(2-chloroethoxy)methane
91.6 16.5 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDBis(2-chloroethyl)ether
4510 485 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDBis(2-ethylhexyl) phthalate
451 313 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDButyl benzyl phthalate
2320 297 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDCaprolactam
91.6 21.3 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDCarbazole
91.6 50.6 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼94.6Chrysene
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-2Client Sample ID: EB-12 (6-8)
Matrix: SolidDate Collected: 05/31/23 13:10
Percent Solids: 71.7Date Received: 06/01/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 91.6 58.4 ug/Kg ☼06/08/23 16:27 06/09/23 18:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
451 168 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDDibenzofuran
451 160 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDDiethyl phthalate
451 180 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDDimethyl phthalate
451 200 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDDi-n-butyl phthalate
451 265 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDDi-n-octyl phthalate
91.6 24.1 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼320Fluoranthene
91.6 17.9 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDFluorene
91.6 32.7 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDHexachlorobenzene
91.6 26.7 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDHexachlorobutadiene
451 46.6 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDHexachlorocyclopentadiene
451 161 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDHexachloroethane
91.6 45.4 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDIndeno[1,2,3-cd]pyrene
451 171 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDIsophorone
91.6 17.8 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDNaphthalene
916 167 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDNitrobenzene
91.6 30.9 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDN-Nitrosodi-n-propylamine
451 152 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDN-Nitrosodiphenylamine
2320 733 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDPentachlorophenol
91.6 24.5 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼291Phenanthrene
451 138 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼NDPhenol
91.6 21.6 ug/Kg 06/08/23 16:27 06/09/23 18:34 1☼342Pyrene
2,4,6-Tribromophenol (Surr)77 34-108 06/08/23 16:27 06/09/23 18:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 77 06/08/23 16:27 06/09/23 18:34 144-105
2-Fluorophenol (Surr)75 06/08/23 16:27 06/09/23 18:34 148-105
Nitrobenzene-d5 (Surr)75 06/08/23 16:27 06/09/23 18:34 146-105
Phenol-d5 (Surr)73 06/08/23 16:27 06/09/23 18:34 146-105
Terphenyl-d14 (Surr)88 06/08/23 16:27 06/09/23 18:34 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
123 6.97 1.74 mg/Kg ☼06/15/23 08:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
8.64 J 24.4 6.09 mg/Kg ☼06/13/23 15:06 06/14/23 14:31 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
24.4 6.09 mg/Kg 06/13/23 15:06 06/14/23 14:31 50☼32.8C9-C10 Aromatics
24.4 6.09 mg/Kg 06/13/23 15:06 06/14/23 14:31 50☼114C9-C12 Aliphatics (unadjusted)
24.4 6.09 mg/Kg 06/13/23 15:06 06/14/23 14:31 50☼80.5C9-C12 Aliphatics (adjusted)
24.4 6.09 mg/Kg 06/13/23 15:06 06/14/23 14:31 50☼8.63 JC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)114 70-130 06/13/23 15:06 06/14/23 14:31 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)98 06/13/23 15:06 06/14/23 14:31 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
27.9 16.4 16.4 mg/Kg ☼06/06/23 16:31 06/20/23 23:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
16.4 16.4 mg/Kg 06/06/23 16:31 06/20/23 23:43 1☼26.1C11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-2Client Sample ID: EB-12 (6-8)
Matrix: SolidDate Collected: 05/31/23 13:10
Percent Solids: 71.7Date Received: 06/01/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
36.5 8.18 8.18 mg/Kg ☼06/06/23 16:31 06/20/23 23:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C9-C18 Aliphatics
1-Chlorooctadecane (Surr)32 S1-40-140 06/06/23 16:31 06/20/23 23:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)69 06/06/23 16:31 06/20/23 23:43 140-140
o- terphenyl (Surr)47 06/06/23 16:31 06/20/23 23:43 140-140
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) - DL
RL MDL
535 32.7 32.7 mg/Kg ☼06/06/23 16:31 06/21/23 15:27 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
1-Chlorooctadecane (Surr)35 S1-40-140 06/06/23 16:31 06/21/23 15:27 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
599 16.7 16.7 mg/Kg ☼06/27/23 19:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
28.3 0.1 0.1 %06/06/23 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/06/23 14:44 171.7Percent Solids (SM22 2540G)
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-3Client Sample ID: EB-13 (6-8)
Matrix: SolidDate Collected: 05/31/23 09:30
Percent Solids: 68.2Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 6.61 2.21 ug/Kg ☼06/02/23 07:05 06/08/23 16:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
6.61 2.01 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,1,2,2-Tetrachloroethane
6.61 2.64 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
6.61 1.31 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,1,2-Trichloroethane
6.61 2.12 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,1-Dichloroethane
6.61 2.99 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,1-Dichloroethene
6.61 4.27 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,2-Dibromo-3-Chloropropane
6.61 2.22 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,2-Dichlorobenzene
6.61 1.90 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,2-Dichloroethane
6.61 1.76 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,2-Dichloropropane
6.61 3.36 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,2,4-Trichlorobenzene
6.61 4.07 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,3-Dichlorobenzene
6.61 1.98 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,4-Dichlorobenzene
33.1 3.36 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND2-Butanone (MEK)
33.1 2.08 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND2-Hexanone
33.1 2.42 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND4-Methyl-2-pentanone (MIBK)
33.1 5.16 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDAcetone
6.61 1.86 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDBenzene
6.61 3.33 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDBromoform
6.61 3.01 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDBromomethane
6.61 5.29 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDCarbon disulfide
6.61 2.68 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDCarbon tetrachloride
6.61 1.72 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDChlorobenzene
6.61 3.28 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDChlorodibromomethane
6.61 4.43 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDChloroform
6.61 2.62 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDChloromethane
6.61 3.86 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDChloroethane
6.61 2.00 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDcis-1,2-Dichloroethene
6.61 2.92 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDcis-1,3-Dichloropropene
6.61 3.08 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDDichlorobromomethane
6.61 3.29 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDDichlorodifluoromethane
6.61 2.45 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDEthylbenzene
6.61 1.81 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND1,2-Dibromoethane
6.61 3.16 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDCyclohexane
6.61 3.44 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDIsopropylbenzene
33.1 9.73 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDMethyl acetate
6.61 1.94 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDMethyl tert-butyl ether
6.61 3.19 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDMethylcyclohexane
6.61 5.96 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDMethylene Chloride
6.61 1.98 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDStyrene
6.61 2.66 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDTetrachloroethene
6.61 1.90 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDToluene
6.61 2.31 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDtrans-1,2-Dichloroethene
6.61 2.98 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDtrans-1,3-Dichloropropene
6.61 2.08 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDTrichloroethene
6.61 5.49 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼ND *+Trichlorofluoromethane
6.61 4.76 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDVinyl chloride
13.2 9.53 ug/Kg 06/02/23 07:05 06/08/23 16:51 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-3Client Sample ID: EB-13 (6-8)
Matrix: SolidDate Collected: 05/31/23 09:30
Percent Solids: 68.2Date Received: 06/01/23 10:30
1,2-Dichloroethane-d4 (Surr)99 73-135 06/02/23 07:05 06/08/23 16:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)104 06/02/23 07:05 06/08/23 16:51 160-124
Dibromofluoromethane (Surr)103 06/02/23 07:05 06/08/23 16:51 169-126
Toluene-d8 (Surr)89 06/02/23 07:05 06/08/23 16:51 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 471 174 ug/Kg ☼06/08/23 16:27 06/09/23 18:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
95.7 35.3 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2,2'-oxybis[1-chloropropane]
471 166 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2,4,5-Trichlorophenol
471 159 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2,4,6-Trichlorophenol
95.7 36.7 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2,4-Dichlorophenol
471 160 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2,4-Dimethylphenol
4710 2960 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2,4-Dinitrophenol
471 284 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2,4-Dinitrotoluene
471 186 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2,6-Dinitrotoluene
95.7 21.8 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2-Chloronaphthalene
471 176 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2-Chlorophenol
95.7 22.8 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2-Methylnaphthalene
471 137 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2-Methylphenol
2430 217 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2-Nitroaniline
471 176 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND2-Nitrophenol
471 444 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND3,3'-Dichlorobenzidine
2430 121 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND3-Nitroaniline
2430 821 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND4,6-Dinitro-2-methylphenol
471 203 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND4-Bromophenyl phenyl ether
471 167 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND4-Chloro-3-methylphenol
471 125 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND4-Chloroaniline
471 159 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND4-Chlorophenyl phenyl ether
471 140 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDMethylphenol, 3 & 4
2430 177 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND4-Nitroaniline
2430 334 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼ND4-Nitrophenol
95.7 27.4 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDAcenaphthene
95.7 20.8 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDAcenaphthylene
957 170 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDAcetophenone
95.7 24.7 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDAnthracene
957 208 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDAtrazine
957 59.1 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDBenzaldehyde
95.7 43.0 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDBenzo[a]anthracene
95.7 41.3 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDBenzo[a]pyrene
95.7 23.4 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDBenzo[b]fluoranthene
95.7 20.6 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDBenzo[g,h,i]perylene
95.7 28.6 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDBenzo[k]fluoranthene
471 174 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDBis(2-chloroethoxy)methane
95.7 17.3 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDBis(2-chloroethyl)ether
4710 507 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDBis(2-ethylhexyl) phthalate
471 327 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDButyl benzyl phthalate
2430 310 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDCaprolactam
95.7 22.3 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDCarbazole
95.7 52.8 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDChrysene
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-3Client Sample ID: EB-13 (6-8)
Matrix: SolidDate Collected: 05/31/23 09:30
Percent Solids: 68.2Date Received: 06/01/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 95.7 61.0 ug/Kg ☼06/08/23 16:27 06/09/23 18:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
471 176 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDDibenzofuran
471 167 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDDiethyl phthalate
471 189 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDDimethyl phthalate
471 208 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDDi-n-butyl phthalate
471 277 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDDi-n-octyl phthalate
95.7 25.1 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDFluoranthene
95.7 18.7 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDFluorene
95.7 34.1 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDHexachlorobenzene
95.7 27.8 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDHexachlorobutadiene
471 48.7 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDHexachlorocyclopentadiene
471 169 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDHexachloroethane
95.7 47.4 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDIndeno[1,2,3-cd]pyrene
471 179 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDIsophorone
95.7 18.6 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDNaphthalene
957 174 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDNitrobenzene
95.7 32.3 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDN-Nitrosodi-n-propylamine
471 159 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDN-Nitrosodiphenylamine
2430 765 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDPentachlorophenol
95.7 25.6 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDPhenanthrene
471 144 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDPhenol
95.7 22.6 ug/Kg 06/08/23 16:27 06/09/23 18:56 1☼NDPyrene
2,4,6-Tribromophenol (Surr)71 34-108 06/08/23 16:27 06/09/23 18:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 71 06/08/23 16:27 06/09/23 18:56 144-105
2-Fluorophenol (Surr)68 06/08/23 16:27 06/09/23 18:56 148-105
Nitrobenzene-d5 (Surr)68 06/08/23 16:27 06/09/23 18:56 146-105
Phenol-d5 (Surr)66 06/08/23 16:27 06/09/23 18:56 146-105
Terphenyl-d14 (Surr)80 06/08/23 16:27 06/09/23 18:56 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.33 1.83 mg/Kg ☼06/15/23 08:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 25.3 6.33 mg/Kg ☼06/13/23 15:06 06/14/23 15:13 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
25.3 6.33 mg/Kg 06/13/23 15:06 06/14/23 15:13 50☼NDC9-C10 Aromatics
25.3 6.33 mg/Kg 06/13/23 15:06 06/14/23 15:13 50☼NDC9-C12 Aliphatics (unadjusted)
25.3 6.33 mg/Kg 06/13/23 15:06 06/14/23 15:13 50☼NDC9-C12 Aliphatics (adjusted)
25.3 6.33 mg/Kg 06/13/23 15:06 06/14/23 15:13 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)111 70-130 06/13/23 15:06 06/14/23 15:13 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)96 06/13/23 15:06 06/14/23 15:13 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.6 17.6 mg/Kg ☼06/06/23 16:31 06/21/23 00:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
17.6 17.6 mg/Kg 06/06/23 16:31 06/21/23 00:06 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-3Client Sample ID: EB-13 (6-8)
Matrix: SolidDate Collected: 05/31/23 09:30
Percent Solids: 68.2Date Received: 06/01/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 17.6 17.6 mg/Kg ☼06/06/23 16:31 06/21/23 00:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.80 8.80 mg/Kg 06/06/23 16:31 06/21/23 00:06 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)51 40-140 06/06/23 16:31 06/21/23 00:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)76 06/06/23 16:31 06/21/23 00:06 140-140
o- terphenyl (Surr)48 06/06/23 16:31 06/21/23 00:06 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.6 17.6 mg/Kg ☼06/27/23 19:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
31.8 0.1 0.1 %06/06/23 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/06/23 14:44 168.2Percent Solids (SM22 2540G)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-4Client Sample ID: EB-14 (8-10)
Matrix: SolidDate Collected: 05/31/23 10:22
Percent Solids: 66.3Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.11 2.37 ug/Kg ☼06/02/23 07:05 06/08/23 17:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.11 2.16 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,1,2,2-Tetrachloroethane
7.11 2.84 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
7.11 1.41 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,1,2-Trichloroethane
7.11 2.28 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,1-Dichloroethane
7.11 3.21 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,1-Dichloroethene
7.11 4.59 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,2-Dibromo-3-Chloropropane
7.11 2.39 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,2-Dichlorobenzene
7.11 2.05 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,2-Dichloroethane
7.11 1.89 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,2-Dichloropropane
7.11 3.61 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,2,4-Trichlorobenzene
7.11 4.38 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,3-Dichlorobenzene
7.11 2.13 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,4-Dichlorobenzene
35.5 3.61 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND2-Butanone (MEK)
35.5 2.23 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND2-Hexanone
35.5 2.60 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND4-Methyl-2-pentanone (MIBK)
35.5 5.55 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDAcetone
7.11 2.00 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDBenzene
7.11 3.58 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDBromoform
7.11 3.24 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDBromomethane
7.11 5.69 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDCarbon disulfide
7.11 2.89 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDCarbon tetrachloride
7.11 1.85 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDChlorobenzene
7.11 3.53 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDChlorodibromomethane
7.11 4.76 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDChloroform
7.11 2.82 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDChloromethane
7.11 4.15 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDChloroethane
7.11 2.15 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDcis-1,2-Dichloroethene
7.11 3.14 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDcis-1,3-Dichloropropene
7.11 3.31 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDDichlorobromomethane
7.11 3.54 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDDichlorodifluoromethane
7.11 2.63 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDEthylbenzene
7.11 1.95 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND1,2-Dibromoethane
7.11 3.40 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDCyclohexane
7.11 3.70 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDIsopropylbenzene
35.5 10.5 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDMethyl acetate
7.11 2.09 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDMethyl tert-butyl ether
7.11 3.43 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDMethylcyclohexane
7.11 6.41 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDMethylene Chloride
7.11 2.13 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDStyrene
7.11 2.86 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDTetrachloroethene
7.11 2.05 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDToluene
7.11 2.49 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDtrans-1,2-Dichloroethene
7.11 3.20 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDtrans-1,3-Dichloropropene
7.11 2.23 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDTrichloroethene
7.11 5.90 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼ND *+Trichlorofluoromethane
7.11 5.12 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDVinyl chloride
14.2 10.3 ug/Kg 06/02/23 07:05 06/08/23 17:13 1☼NDXylenes, Total
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-4Client Sample ID: EB-14 (8-10)
Matrix: SolidDate Collected: 05/31/23 10:22
Percent Solids: 66.3Date Received: 06/01/23 10:30
1,2-Dichloroethane-d4 (Surr)90 73-135 06/02/23 07:05 06/08/23 17:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 06/02/23 07:05 06/08/23 17:13 160-124
Dibromofluoromethane (Surr)94 06/02/23 07:05 06/08/23 17:13 169-126
Toluene-d8 (Surr)82 06/02/23 07:05 06/08/23 17:13 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 482 178 ug/Kg ☼06/08/23 16:27 06/12/23 11:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
97.8 36.1 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2,2'-oxybis[1-chloropropane]
482 169 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2,4,5-Trichlorophenol
482 162 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2,4,6-Trichlorophenol
97.8 37.5 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2,4-Dichlorophenol
482 164 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2,4-Dimethylphenol
4820 3020 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2,4-Dinitrophenol
482 291 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2,4-Dinitrotoluene
482 190 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2,6-Dinitrotoluene
97.8 22.3 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2-Chloronaphthalene
482 180 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2-Chlorophenol
97.8 23.4 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2-Methylnaphthalene
482 140 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2-Methylphenol
2480 222 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2-Nitroaniline
482 180 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND2-Nitrophenol
482 454 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND3,3'-Dichlorobenzidine
2480 124 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND3-Nitroaniline
2480 839 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND4,6-Dinitro-2-methylphenol
482 207 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND4-Bromophenyl phenyl ether
482 171 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND4-Chloro-3-methylphenol
482 128 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND4-Chloroaniline
482 162 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND4-Chlorophenyl phenyl ether
482 143 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDMethylphenol, 3 & 4
2480 181 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND4-Nitroaniline
2480 342 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼ND4-Nitrophenol
97.8 28.0 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDAcenaphthene
97.8 21.3 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDAcenaphthylene
978 174 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDAcetophenone
97.8 25.3 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDAnthracene
978 213 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDAtrazine
978 60.4 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDBenzaldehyde
97.8 43.9 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDBenzo[a]anthracene
97.8 42.2 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDBenzo[a]pyrene
97.8 23.9 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDBenzo[b]fluoranthene
97.8 21.0 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDBenzo[g,h,i]perylene
97.8 29.2 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDBenzo[k]fluoranthene
482 178 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDBis(2-chloroethoxy)methane
97.8 17.7 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDBis(2-chloroethyl)ether
4820 518 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDBis(2-ethylhexyl) phthalate
482 334 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDButyl benzyl phthalate
2480 317 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDCaprolactam
97.8 22.8 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDCarbazole
97.8 54.0 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDChrysene
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-4Client Sample ID: EB-14 (8-10)
Matrix: SolidDate Collected: 05/31/23 10:22
Percent Solids: 66.3Date Received: 06/01/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 97.8 62.3 ug/Kg ☼06/08/23 16:27 06/12/23 11:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
482 180 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDDibenzofuran
482 171 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDDiethyl phthalate
482 193 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDDimethyl phthalate
482 213 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDDi-n-butyl phthalate
482 283 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDDi-n-octyl phthalate
97.8 25.7 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDFluoranthene
97.8 19.1 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDFluorene
97.8 34.9 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDHexachlorobenzene
97.8 28.5 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDHexachlorobutadiene
482 49.8 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDHexachlorocyclopentadiene
482 172 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDHexachloroethane
97.8 48.5 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDIndeno[1,2,3-cd]pyrene
482 182 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDIsophorone
97.8 19.0 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDNaphthalene
978 178 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDNitrobenzene
97.8 33.0 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDN-Nitrosodi-n-propylamine
482 162 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDN-Nitrosodiphenylamine
2480 783 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDPentachlorophenol
97.8 26.1 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDPhenanthrene
482 147 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDPhenol
97.8 23.1 ug/Kg 06/08/23 16:27 06/12/23 11:21 1☼NDPyrene
2,4,6-Tribromophenol (Surr)57 34-108 06/08/23 16:27 06/12/23 11:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 80 06/08/23 16:27 06/12/23 11:21 144-105
2-Fluorophenol (Surr)68 06/08/23 16:27 06/12/23 11:21 148-105
Nitrobenzene-d5 (Surr)88 06/08/23 16:27 06/12/23 11:21 146-105
Phenol-d5 (Surr)76 06/08/23 16:27 06/12/23 11:21 146-105
Terphenyl-d14 (Surr)80 06/08/23 16:27 06/12/23 11:21 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.54 1.89 mg/Kg ☼06/15/23 08:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 28.6 7.16 mg/Kg ☼06/13/23 15:06 06/14/23 15:54 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
28.6 7.16 mg/Kg 06/13/23 15:06 06/14/23 15:54 50☼NDC9-C10 Aromatics
28.6 7.16 mg/Kg 06/13/23 15:06 06/14/23 15:54 50☼NDC9-C12 Aliphatics (unadjusted)
28.6 7.16 mg/Kg 06/13/23 15:06 06/14/23 15:54 50☼NDC9-C12 Aliphatics (adjusted)
28.6 7.16 mg/Kg 06/13/23 15:06 06/14/23 15:54 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)114 70-130 06/13/23 15:06 06/14/23 15:54 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)99 06/13/23 15:06 06/14/23 15:54 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.4 17.4 mg/Kg ☼06/06/23 16:31 06/21/23 00:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
17.4 17.4 mg/Kg 06/06/23 16:31 06/21/23 00:28 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-4Client Sample ID: EB-14 (8-10)
Matrix: SolidDate Collected: 05/31/23 10:22
Percent Solids: 66.3Date Received: 06/01/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 17.4 17.4 mg/Kg ☼06/06/23 16:31 06/21/23 00:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.69 8.69 mg/Kg 06/06/23 16:31 06/21/23 00:28 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)53 40-140 06/06/23 16:31 06/21/23 00:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)65 06/06/23 16:31 06/21/23 00:28 140-140
o- terphenyl (Surr)46 06/06/23 16:31 06/21/23 00:28 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 18.1 18.1 mg/Kg ☼06/27/23 19:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
33.7 0.1 0.1 %06/06/23 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/06/23 14:44 166.3Percent Solids (SM22 2540G)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-5Client Sample ID: EB-16 (2-3)
Matrix: SolidDate Collected: 05/31/23 10:45
Percent Solids: 69.9Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 6.70 2.24 ug/Kg ☼06/02/23 07:05 06/08/23 17:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
6.70 2.04 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,1,2,2-Tetrachloroethane
6.70 2.68 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
6.70 1.33 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,1,2-Trichloroethane
6.70 2.14 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,1-Dichloroethane
6.70 3.03 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,1-Dichloroethene
6.70 4.33 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,2-Dibromo-3-Chloropropane
6.70 2.25 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,2-Dichlorobenzene
6.70 1.93 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,2-Dichloroethane
6.70 1.78 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,2-Dichloropropane
6.70 3.40 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,2,4-Trichlorobenzene
6.70 4.13 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,3-Dichlorobenzene
6.70 2.01 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,4-Dichlorobenzene
33.5 3.40 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND2-Butanone (MEK)
33.5 2.10 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND2-Hexanone
33.5 2.45 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND4-Methyl-2-pentanone (MIBK)
33.5 5.23 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDAcetone
6.70 1.89 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDBenzene
6.70 3.38 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDBromoform
6.70 3.06 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDBromomethane
6.70 5.36 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDCarbon disulfide
6.70 2.72 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDCarbon tetrachloride
6.70 1.74 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDChlorobenzene
6.70 3.32 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDChlorodibromomethane
6.70 4.49 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDChloroform
6.70 2.65 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDChloromethane
6.70 3.91 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDChloroethane
6.70 2.02 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDcis-1,2-Dichloroethene
6.70 2.96 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDcis-1,3-Dichloropropene
6.70 3.12 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDDichlorobromomethane
6.70 3.34 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDDichlorodifluoromethane
6.70 2.48 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDEthylbenzene
6.70 1.84 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND1,2-Dibromoethane
6.70 3.20 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDCyclohexane
6.70 3.48 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDIsopropylbenzene
33.5 9.86 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDMethyl acetate
6.70 1.97 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDMethyl tert-butyl ether
6.70 3.23 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDMethylcyclohexane
6.70 6.04 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDMethylene Chloride
6.70 2.01 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDStyrene
6.70 2.69 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDTetrachloroethene
6.70 1.93 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDToluene
6.70 2.35 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDtrans-1,2-Dichloroethene
6.70 3.02 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDtrans-1,3-Dichloropropene
6.70 2.10 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDTrichloroethene
6.70 5.56 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼ND *+Trichlorofluoromethane
6.70 4.83 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDVinyl chloride
13.4 9.66 ug/Kg 06/02/23 07:05 06/08/23 17:36 1☼NDXylenes, Total
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-5Client Sample ID: EB-16 (2-3)
Matrix: SolidDate Collected: 05/31/23 10:45
Percent Solids: 69.9Date Received: 06/01/23 10:30
1,2-Dichloroethane-d4 (Surr)88 73-135 06/02/23 07:05 06/08/23 17:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 06/02/23 07:05 06/08/23 17:36 160-124
Dibromofluoromethane (Surr)93 06/02/23 07:05 06/08/23 17:36 169-126
Toluene-d8 (Surr)80 06/02/23 07:05 06/08/23 17:36 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 466 172 ug/Kg ☼06/08/23 16:27 06/09/23 19:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
94.6 34.9 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2,2'-oxybis[1-chloropropane]
466 164 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2,4,5-Trichlorophenol
466 157 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2,4,6-Trichlorophenol
94.6 36.3 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2,4-Dichlorophenol
466 158 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2,4-Dimethylphenol
4660 2920 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2,4-Dinitrophenol
466 281 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2,4-Dinitrotoluene
466 184 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2,6-Dinitrotoluene
94.6 21.6 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2-Chloronaphthalene
466 174 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2-Chlorophenol
94.6 22.6 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2-Methylnaphthalene
466 135 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2-Methylphenol
2400 215 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2-Nitroaniline
466 174 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND2-Nitrophenol
466 439 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND3,3'-Dichlorobenzidine
2400 120 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND3-Nitroaniline
2400 812 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND4,6-Dinitro-2-methylphenol
466 201 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND4-Bromophenyl phenyl ether
466 165 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND4-Chloro-3-methylphenol
466 124 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND4-Chloroaniline
466 157 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND4-Chlorophenyl phenyl ether
466 138 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDMethylphenol, 3 & 4
2400 175 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND4-Nitroaniline
2400 330 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼ND4-Nitrophenol
94.6 27.1 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDAcenaphthene
94.6 20.6 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDAcenaphthylene
946 168 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDAcetophenone
94.6 24.4 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDAnthracene
946 206 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDAtrazine
946 58.5 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDBenzaldehyde
94.6 42.5 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDBenzo[a]anthracene
94.6 40.8 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDBenzo[a]pyrene
94.6 23.2 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDBenzo[b]fluoranthene
94.6 20.3 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDBenzo[g,h,i]perylene
94.6 28.2 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDBenzo[k]fluoranthene
466 172 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDBis(2-chloroethoxy)methane
94.6 17.1 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDBis(2-chloroethyl)ether
4660 501 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDBis(2-ethylhexyl) phthalate
466 323 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDButyl benzyl phthalate
2400 306 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDCaprolactam
94.6 22.0 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDCarbazole
94.6 52.2 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDChrysene
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-5Client Sample ID: EB-16 (2-3)
Matrix: SolidDate Collected: 05/31/23 10:45
Percent Solids: 69.9Date Received: 06/01/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 94.6 60.3 ug/Kg ☼06/08/23 16:27 06/09/23 19:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
466 174 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDDibenzofuran
466 165 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDDiethyl phthalate
466 186 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDDimethyl phthalate
466 206 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDDi-n-butyl phthalate
466 274 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDDi-n-octyl phthalate
94.6 24.9 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDFluoranthene
94.6 18.5 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDFluorene
94.6 33.7 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDHexachlorobenzene
94.6 27.5 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDHexachlorobutadiene
466 48.2 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDHexachlorocyclopentadiene
466 167 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDHexachloroethane
94.6 46.9 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDIndeno[1,2,3-cd]pyrene
466 177 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDIsophorone
94.6 18.4 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDNaphthalene
946 172 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDNitrobenzene
94.6 31.9 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDN-Nitrosodi-n-propylamine
466 157 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDN-Nitrosodiphenylamine
2400 757 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDPentachlorophenol
94.6 25.3 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDPhenanthrene
466 143 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDPhenol
94.6 22.3 ug/Kg 06/08/23 16:27 06/09/23 19:02 1☼NDPyrene
2,4,6-Tribromophenol (Surr)48 34-108 06/08/23 16:27 06/09/23 19:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 72 06/08/23 16:27 06/09/23 19:02 144-105
2-Fluorophenol (Surr)58 06/08/23 16:27 06/09/23 19:02 148-105
Nitrobenzene-d5 (Surr)77 06/08/23 16:27 06/09/23 19:02 146-105
Phenol-d5 (Surr)62 06/08/23 16:27 06/09/23 19:02 146-105
Terphenyl-d14 (Surr)75 06/08/23 16:27 06/09/23 19:02 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.15 1.79 mg/Kg ☼06/15/23 08:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 21.2 5.30 mg/Kg ☼06/13/23 15:06 06/14/23 16:35 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
21.2 5.30 mg/Kg 06/13/23 15:06 06/14/23 16:35 50☼NDC9-C10 Aromatics
21.2 5.30 mg/Kg 06/13/23 15:06 06/14/23 16:35 50☼NDC9-C12 Aliphatics (unadjusted)
21.2 5.30 mg/Kg 06/13/23 15:06 06/14/23 16:35 50☼NDC9-C12 Aliphatics (adjusted)
21.2 5.30 mg/Kg 06/13/23 15:06 06/14/23 16:35 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)114 70-130 06/13/23 15:06 06/14/23 16:35 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)98 06/13/23 15:06 06/14/23 16:35 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 16.6 16.6 mg/Kg ☼06/06/23 16:31 06/21/23 00:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
16.6 16.6 mg/Kg 06/06/23 16:31 06/21/23 00:50 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-5Client Sample ID: EB-16 (2-3)
Matrix: SolidDate Collected: 05/31/23 10:45
Percent Solids: 69.9Date Received: 06/01/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 16.6 16.6 mg/Kg ☼06/06/23 16:31 06/21/23 00:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.30 8.30 mg/Kg 06/06/23 16:31 06/21/23 00:50 1☼NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)44 40-140 06/06/23 16:31 06/21/23 00:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)72 06/06/23 16:31 06/21/23 00:50 140-140
o- terphenyl (Surr)44 06/06/23 16:31 06/21/23 00:50 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.2 17.2 mg/Kg ☼06/27/23 19:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
30.1 0.1 0.1 %06/06/23 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/06/23 14:44 169.9Percent Solids (SM22 2540G)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-6Client Sample ID: EB-17 (8-10)
Matrix: SolidDate Collected: 05/31/23 11:50
Percent Solids: 65.4Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 7.55 2.52 ug/Kg ☼06/02/23 07:05 06/08/23 17:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1-Trichloroethane
7.55 2.30 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,1,2,2-Tetrachloroethane
7.55 3.02 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,1,2-Trichloro-1,2,2-trifluoroethane
7.55 1.50 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,1,2-Trichloroethane
7.55 2.42 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,1-Dichloroethane
7.55 3.41 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,1-Dichloroethene
7.55 4.88 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,2-Dibromo-3-Chloropropane
7.55 2.54 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,2-Dichlorobenzene
7.55 2.18 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,2-Dichloroethane
7.55 2.01 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,2-Dichloropropane
7.55 3.84 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,2,4-Trichlorobenzene
7.55 4.65 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,3-Dichlorobenzene
7.55 2.27 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,4-Dichlorobenzene
37.8 3.84 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND2-Butanone (MEK)
37.8 2.37 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND2-Hexanone
37.8 2.76 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND4-Methyl-2-pentanone (MIBK)
37.8 5.89 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDAcetone
7.55 2.13 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDBenzene
7.55 3.81 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDBromoform
7.55 3.44 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDBromomethane
7.55 6.04 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDCarbon disulfide
7.55 3.07 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDCarbon tetrachloride
7.55 1.96 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDChlorobenzene
7.55 3.75 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDChlorodibromomethane
7.55 5.06 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDChloroform
7.55 2.99 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDChloromethane
7.55 4.41 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDChloroethane
7.55 2.28 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDcis-1,2-Dichloroethene
7.55 3.34 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDcis-1,3-Dichloropropene
7.55 3.52 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDDichlorobromomethane
7.55 3.76 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDDichlorodifluoromethane
7.55 2.79 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDEthylbenzene
7.55 2.07 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND1,2-Dibromoethane
7.55 3.61 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDCyclohexane
7.55 3.93 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDIsopropylbenzene
37.8 11.1 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDMethyl acetate
7.55 2.22 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDMethyl tert-butyl ether
7.55 3.64 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDMethylcyclohexane
7.55 6.81 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDMethylene Chloride
7.55 2.27 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDStyrene
7.55 3.04 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDTetrachloroethene
7.55 2.18 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDToluene
7.55 2.64 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDtrans-1,2-Dichloroethene
7.55 3.40 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDtrans-1,3-Dichloropropene
7.55 2.37 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDTrichloroethene
7.55 6.27 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼ND *+Trichlorofluoromethane
7.55 5.44 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDVinyl chloride
15.1 10.9 ug/Kg 06/02/23 07:05 06/08/23 17:59 1☼NDXylenes, Total
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-6Client Sample ID: EB-17 (8-10)
Matrix: SolidDate Collected: 05/31/23 11:50
Percent Solids: 65.4Date Received: 06/01/23 10:30
1,2-Dichloroethane-d4 (Surr)100 73-135 06/02/23 07:05 06/08/23 17:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)99 06/02/23 07:05 06/08/23 17:59 160-124
Dibromofluoromethane (Surr)99 06/02/23 07:05 06/08/23 17:59 169-126
Toluene-d8 (Surr)82 06/02/23 07:05 06/08/23 17:59 167-134
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 498 184 ug/Kg ☼06/08/23 16:27 06/09/23 19:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1'-Biphenyl
101 37.3 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2,2'-oxybis[1-chloropropane]
498 175 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2,4,5-Trichlorophenol
498 168 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2,4,6-Trichlorophenol
101 38.8 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2,4-Dichlorophenol
498 169 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2,4-Dimethylphenol
4980 3120 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2,4-Dinitrophenol
498 300 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2,4-Dinitrotoluene
498 196 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2,6-Dinitrotoluene
101 23.1 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2-Chloronaphthalene
498 186 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2-Chlorophenol
101 24.2 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2-Methylnaphthalene
498 144 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2-Methylphenol
2570 229 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2-Nitroaniline
498 186 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND2-Nitrophenol
498 469 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND3,3'-Dichlorobenzidine
2570 128 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND3-Nitroaniline
2570 868 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND4,6-Dinitro-2-methylphenol
498 214 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND4-Bromophenyl phenyl ether
498 177 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND4-Chloro-3-methylphenol
498 132 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND4-Chloroaniline
498 168 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND4-Chlorophenyl phenyl ether
498 148 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDMethylphenol, 3 & 4
2570 187 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND4-Nitroaniline
2570 353 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼ND4-Nitrophenol
101 29.0 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDAcenaphthene
101 22.0 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDAcenaphthylene
1010 180 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDAcetophenone
101 26.1 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼40.5 JAnthracene
1010 220 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDAtrazine
1010 62.5 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDBenzaldehyde
101 45.4 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDBenzo[a]anthracene
101 43.6 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDBenzo[a]pyrene
101 24.8 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDBenzo[b]fluoranthene
101 21.7 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDBenzo[g,h,i]perylene
101 30.2 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDBenzo[k]fluoranthene
498 184 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDBis(2-chloroethoxy)methane
101 18.3 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDBis(2-chloroethyl)ether
4980 536 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDBis(2-ethylhexyl) phthalate
498 346 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDButyl benzyl phthalate
2570 328 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDCaprolactam
101 23.5 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDCarbazole
101 55.8 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDChrysene
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-6Client Sample ID: EB-17 (8-10)
Matrix: SolidDate Collected: 05/31/23 11:50
Percent Solids: 65.4Date Received: 06/01/23 10:30
Method: SW846 EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 101 64.5 ug/Kg ☼06/08/23 16:27 06/09/23 19:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Dibenz(a,h)anthracene
498 186 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDDibenzofuran
498 177 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDDiethyl phthalate
498 199 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDDimethyl phthalate
498 220 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDDi-n-butyl phthalate
498 293 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDDi-n-octyl phthalate
101 26.6 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼164Fluoranthene
101 19.8 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDFluorene
101 36.1 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDHexachlorobenzene
101 29.4 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDHexachlorobutadiene
498 51.5 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDHexachlorocyclopentadiene
498 178 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDHexachloroethane
101 50.1 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDIndeno[1,2,3-cd]pyrene
498 189 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDIsophorone
101 19.6 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDNaphthalene
1010 184 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDNitrobenzene
101 34.1 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDN-Nitrosodi-n-propylamine
498 168 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDN-Nitrosodiphenylamine
2570 809 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDPentachlorophenol
101 27.0 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼141Phenanthrene
498 152 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼NDPhenol
101 23.8 ug/Kg 06/08/23 16:27 06/09/23 19:24 1☼133Pyrene
2,4,6-Tribromophenol (Surr)52 34-108 06/08/23 16:27 06/09/23 19:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 78 06/08/23 16:27 06/09/23 19:24 144-105
2-Fluorophenol (Surr)64 06/08/23 16:27 06/09/23 19:24 148-105
Nitrobenzene-d5 (Surr)85 06/08/23 16:27 06/09/23 19:24 146-105
Phenol-d5 (Surr)72 06/08/23 16:27 06/09/23 19:24 146-105
Terphenyl-d14 (Surr)76 06/08/23 16:27 06/09/23 19:24 139-105
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 7.65 1.91 mg/Kg ☼06/15/23 08:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 30.1 7.51 mg/Kg ☼06/13/23 15:06 06/14/23 17:17 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
30.1 7.51 mg/Kg 06/13/23 15:06 06/14/23 17:17 50☼NDC9-C10 Aromatics
30.1 7.51 mg/Kg 06/13/23 15:06 06/14/23 17:17 50☼NDC9-C12 Aliphatics (unadjusted)
30.1 7.51 mg/Kg 06/13/23 15:06 06/14/23 17:17 50☼NDC9-C12 Aliphatics (adjusted)
30.1 7.51 mg/Kg 06/13/23 15:06 06/14/23 17:17 50☼NDC5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)117 70-130 06/13/23 15:06 06/14/23 17:17 50
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)102 06/13/23 15:06 06/14/23 17:17 5070-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 17.7 17.7 mg/Kg ☼06/06/23 16:31 06/21/23 01:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
17.7 17.7 mg/Kg 06/06/23 16:31 06/21/23 01:13 1☼NDC11-C22 Aromatics (Adjusted)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-6Client Sample ID: EB-17 (8-10)
Matrix: SolidDate Collected: 05/31/23 11:50
Percent Solids: 65.4Date Received: 06/01/23 10:30
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
RL MDL
ND 17.7 17.7 mg/Kg ☼06/06/23 16:31 06/21/23 01:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C19-C36 Aliphatics
8.83 8.83 mg/Kg 06/06/23 16:31 06/21/23 01:13 1☼47.0C9-C18 Aliphatics
1-Chlorooctadecane (Surr)50 40-140 06/06/23 16:31 06/21/23 01:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)73 06/06/23 16:31 06/21/23 01:13 140-140
o- terphenyl (Surr)51 06/06/23 16:31 06/21/23 01:13 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
47.0 18.4 18.4 mg/Kg ☼06/27/23 19:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
General Chemistry
RL MDL
34.6 0.1 0.1 %06/06/23 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Percent Moisture (SM22 2540G)
0.1 0.1 %06/06/23 14:44 165.4Percent Solids (SM22 2540G)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-7Client Sample ID: TMW-2
Matrix: WaterDate Collected: 05/31/23 13:35
Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 06/07/23 15:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 06/07/23 15:22 1ND1,3-Dichlorobenzene
1.00 0.544 ug/L 06/07/23 15:22 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 06/07/23 15:22 1NDBenzene
1.00 0.501 ug/L 06/07/23 15:22 1NDChlorobenzene
1.00 0.507 ug/L 06/07/23 15:22 1NDEthylbenzene
1.00 0.457 ug/L 06/07/23 15:22 1NDToluene
1.00 0.406 ug/L 06/07/23 15:22 1NDo-Xylene
1.00 0.482 ug/L 06/07/23 15:22 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 06/07/23 15:22 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)83 26-156 06/07/23 15:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)76 06/07/23 15:22 136-124
Dibromofluoromethane (Surr)111 06/07/23 15:22 146-149
Toluene-d8 (Surr)94 06/07/23 15:22 140-146
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.198 0.0677 ug/L 06/05/23 11:58 06/07/23 17:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.198 0.0677 ug/L 06/05/23 11:58 06/07/23 17:32 1NDAcenaphthylene
0.198 0.0510 ug/L 06/05/23 11:58 06/07/23 17:32 1NDAnthracene
1.04 0.0990 ug/L 06/05/23 11:58 06/07/23 17:32 1ND1,2-Dichlorobenzene
0.198 0.0781 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBenzo[a]anthracene
0.198 0.0552 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBenzo[a]pyrene
1.04 0.103 ug/L 06/05/23 11:58 06/07/23 17:32 1ND1,3-Dichlorobenzene
0.198 0.101 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBenzo[b]fluoranthene
0.198 0.0719 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBenzo[g,h,i]perylene
1.04 0.0635 ug/L 06/05/23 11:58 06/07/23 17:32 1ND1,4-Dichlorobenzene
0.198 0.0917 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBenzo[k]fluoranthene
1.04 0.158 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBis(2-chloroethoxy)methane
0.198 0.0417 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBis(2-chloroethyl)ether
0.198 0.0583 ug/L 06/05/23 11:58 06/07/23 17:32 1ND1-Methylnaphthalene
0.198 0.0604 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2,2'-oxybis[1-chloropropane]
10.4 6.49 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBis(2-ethylhexyl) phthalate
1.04 0.332 ug/L 06/05/23 11:58 06/07/23 17:32 1ND4-Bromophenyl phenyl ether
1.04 0.481 ug/L 06/05/23 11:58 06/07/23 17:32 1NDButyl benzyl phthalate
0.198 0.0615 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2-Chloronaphthalene
1.04 0.230 ug/L 06/05/23 11:58 06/07/23 17:32 1ND4-Chlorophenyl phenyl ether
0.198 0.0844 ug/L 06/05/23 11:58 06/07/23 17:32 1NDChrysene
0.198 0.0750 ug/L 06/05/23 11:58 06/07/23 17:32 1NDDibenz(a,h)anthracene
1.04 0.607 ug/L 06/05/23 11:58 06/07/23 17:32 1ND3,3'-Dichlorobenzidine
1.04 0.591 ug/L 06/05/23 11:58 06/07/23 17:32 1NDDiethyl phthalate
1.04 0.714 ug/L 06/05/23 11:58 06/07/23 17:32 1NDDi-n-octyl phthalate
1.04 0.204 ug/L 06/05/23 11:58 06/07/23 17:32 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.198 0.0646 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2-Methylnaphthalene
0.198 0.0625 ug/L 06/05/23 11:58 06/07/23 17:32 1NDFluoranthene
1.04 0.313 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2-Methylphenol
0.198 0.0719 ug/L 06/05/23 11:58 06/07/23 17:32 1NDFluorene
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-7Client Sample ID: TMW-2
Matrix: WaterDate Collected: 05/31/23 13:35
Date Received: 06/01/23 10:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.198 0.0583 ug/L 06/05/23 11:58 06/07/23 17:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexachlorobenzene
0.198 0.0719 ug/L 06/05/23 11:58 06/07/23 17:32 1NDHexachlorobutadiene
1.04 0.518 ug/L 06/05/23 11:58 06/07/23 17:32 1NDHexachlorocyclopentadiene
1.04 0.139 ug/L 06/05/23 11:58 06/07/23 17:32 1NDHexachloroethane
0.198 0.0885 ug/L 06/05/23 11:58 06/07/23 17:32 1NDIndeno[1,2,3-cd]pyrene
1.04 0.196 ug/L 06/05/23 11:58 06/07/23 17:32 1NDIsophorone
0.198 0.0615 ug/L 06/05/23 11:58 06/07/23 17:32 1NDNaphthalene
2.08 0.521 ug/L 06/05/23 11:58 06/07/23 17:32 1NDNitrobenzene
1.04 0.0698 ug/L 06/05/23 11:58 06/07/23 17:32 1NDN-Nitrosodimethylamine
0.198 0.0740 ug/L 06/05/23 11:58 06/07/23 17:32 1NDN-Nitrosodi-n-propylamine
1.04 0.392 ug/L 06/05/23 11:58 06/07/23 17:32 1ND4-Chloroaniline
0.198 0.0573 ug/L 06/05/23 11:58 06/07/23 17:32 1NDPhenanthrene
0.198 0.0563 ug/L 06/05/23 11:58 06/07/23 17:32 1NDPyrene
1.04 0.388 ug/L 06/05/23 11:58 06/07/23 17:32 1ND4-Methylphenol
5.21 0.882 ug/L 06/05/23 11:58 06/07/23 17:32 1NDPentachlorophenol
1.04 0.507 ug/L 06/05/23 11:58 06/07/23 17:32 1NDPhenol
1.04 0.136 ug/L 06/05/23 11:58 06/07/23 17:32 1ND1,2,4-Trichlorobenzene
0.198 0.0531 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2,4-Dichlorophenol
10.4 1.59 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2,4-Dinitrophenol
1.04 0.174 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2,4-Dimethylphenol
1.04 0.233 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2,4,6-Trichlorophenol
1.04 0.134 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2-Chlorophenol
1.04 0.201 ug/L 06/05/23 11:58 06/07/23 17:32 1ND2-Nitrophenol
5.21 1.53 ug/L 06/05/23 11:58 06/07/23 17:32 1ND4,6-Dinitro-2-methylphenol
1.04 0.290 ug/L 06/05/23 11:58 06/07/23 17:32 1ND4-Chloro-3-methylphenol
5.21 0.979 ug/L 06/05/23 11:58 06/07/23 17:32 1ND4-Nitrophenol
5.21 0.961 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBenzoic acid
1.04 0.170 ug/L 06/05/23 11:58 06/07/23 17:32 1NDBenzyl alcohol
1.04 0.198 ug/L 06/05/23 11:58 06/07/23 17:32 1NDDibenzofuran
2,4,6-Tribromophenol (Surr)46 32-127 06/05/23 11:58 06/07/23 17:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 59 06/05/23 11:58 06/07/23 17:32 147-107
2-Fluorophenol (Surr)48 06/05/23 11:58 06/07/23 17:32 135-109
Nitrobenzene-d5 (Surr)56 06/05/23 11:58 06/07/23 17:32 147-110
Phenol-d5 (Surr)51 06/05/23 11:58 06/07/23 17:32 137-110
Terphenyl-d14 (Surr)79 06/05/23 11:58 06/07/23 17:32 132-115
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
29.6 J 100 20.0 ug/L 06/09/23 13:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
29.6 J 100 25.0 ug/L 06/09/23 07:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 06/09/23 07:54 1NDC9-C10 Aromatics
100 25.0 ug/L 06/09/23 07:54 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 06/09/23 07:54 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 06/09/23 07:54 129.2 JC5-C8 Aliphatics (adjusted)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-7Client Sample ID: TMW-2
Matrix: WaterDate Collected: 05/31/23 13:35
Date Received: 06/01/23 10:30
a,a,a-Trifluorotoluene (fid)107 70-130 06/09/23 07:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)98 06/09/23 07:54 170-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 43.1 43.1 ug/L 06/09/23 19:11 06/27/23 04:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
43.1 43.1 ug/L 06/09/23 19:11 06/27/23 04:01 1NDC11-C22 Aromatics (Adjusted)
53.9 53.9 ug/L 06/09/23 19:11 06/27/23 04:01 1NDC19-C36 Aliphatics
32.3 32.3 ug/L 06/09/23 19:11 06/27/23 04:01 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)47 40-140 06/09/23 19:11 06/27/23 04:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)90 06/09/23 19:11 06/27/23 04:01 140-140
o- terphenyl (Surr)77 06/09/23 19:11 06/27/23 04:01 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 06/27/23 19:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
43.1 43.1 ug/L 06/27/23 19:05 1NDC11-C22 Aromatics
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-8Client Sample ID: TMW-3
Matrix: WaterDate Collected: 05/31/23 09:15
Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 06/07/23 18:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 06/07/23 18:16 1ND1,3-Dichlorobenzene
1.00 0.544 ug/L 06/07/23 18:16 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 06/07/23 18:16 12.00Benzene
1.00 0.501 ug/L 06/07/23 18:16 1NDChlorobenzene
1.00 0.507 ug/L 06/07/23 18:16 1NDEthylbenzene
1.00 0.457 ug/L 06/07/23 18:16 1NDToluene
1.00 0.406 ug/L 06/07/23 18:16 14.20o-Xylene
1.00 0.482 ug/L 06/07/23 18:16 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 06/07/23 18:16 14.20Xylenes, Total
1,2-Dichloroethane-d4 (Surr)91 26-156 06/07/23 18:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)86 06/07/23 18:16 136-124
Dibromofluoromethane (Surr)111 06/07/23 18:16 146-149
Toluene-d8 (Surr)93 06/07/23 18:16 140-146
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.183 0.0625 ug/L 06/05/23 11:58 06/07/23 17:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.183 0.0625 ug/L 06/05/23 11:58 06/07/23 17:55 1NDAcenaphthylene
0.183 0.0471 ug/L 06/05/23 11:58 06/07/23 17:55 1NDAnthracene
0.962 0.0913 ug/L 06/05/23 11:58 06/07/23 17:55 1ND1,2-Dichlorobenzene
0.183 0.0721 ug/L 06/05/23 11:58 06/07/23 17:55 1NDBenzo[a]anthracene
0.183 0.0510 ug/L 06/05/23 11:58 06/07/23 17:55 1NDBenzo[a]pyrene
0.962 0.0952 ug/L 06/05/23 11:58 06/07/23 17:55 1ND1,3-Dichlorobenzene
0.183 0.0933 ug/L 06/05/23 11:58 06/07/23 17:55 1NDBenzo[b]fluoranthene
0.183 0.0663 ug/L 06/05/23 11:58 06/07/23 17:55 1NDBenzo[g,h,i]perylene
0.962 0.0587 ug/L 06/05/23 11:58 06/07/23 17:55 1ND1,4-Dichlorobenzene
0.183 0.0846 ug/L 06/05/23 11:58 06/07/23 17:55 1NDBenzo[k]fluoranthene
0.962 0.146 ug/L 06/05/23 11:58 06/07/23 17:55 1NDBis(2-chloroethoxy)methane
0.183 0.0385 ug/L 06/05/23 11:58 06/07/23 17:55 1NDBis(2-chloroethyl)ether
0.183 0.0538 ug/L 06/05/23 11:58 06/07/23 17:55 1ND1-Methylnaphthalene
0.183 0.0558 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2,2'-oxybis[1-chloropropane]
9.62 5.99 ug/L 06/05/23 11:58 06/07/23 17:55 1NDBis(2-ethylhexyl) phthalate
0.962 0.307 ug/L 06/05/23 11:58 06/07/23 17:55 1ND4-Bromophenyl phenyl ether
0.962 0.444 ug/L 06/05/23 11:58 06/07/23 17:55 1NDButyl benzyl phthalate
0.183 0.0567 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2-Chloronaphthalene
0.962 0.213 ug/L 06/05/23 11:58 06/07/23 17:55 1ND4-Chlorophenyl phenyl ether
0.183 0.0779 ug/L 06/05/23 11:58 06/07/23 17:55 1NDChrysene
0.183 0.0692 ug/L 06/05/23 11:58 06/07/23 17:55 1NDDibenz(a,h)anthracene
0.962 0.561 ug/L 06/05/23 11:58 06/07/23 17:55 1ND3,3'-Dichlorobenzidine
0.962 0.545 ug/L 06/05/23 11:58 06/07/23 17:55 1NDDiethyl phthalate
0.962 0.659 ug/L 06/05/23 11:58 06/07/23 17:55 1NDDi-n-octyl phthalate
0.962 0.188 ug/L 06/05/23 11:58 06/07/23 17:55 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.183 0.0596 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2-Methylnaphthalene
0.183 0.0577 ug/L 06/05/23 11:58 06/07/23 17:55 1NDFluoranthene
0.962 0.288 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2-Methylphenol
0.183 0.0663 ug/L 06/05/23 11:58 06/07/23 17:55 1NDFluorene
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-8Client Sample ID: TMW-3
Matrix: WaterDate Collected: 05/31/23 09:15
Date Received: 06/01/23 10:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.183 0.0538 ug/L 06/05/23 11:58 06/07/23 17:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexachlorobenzene
0.183 0.0663 ug/L 06/05/23 11:58 06/07/23 17:55 1NDHexachlorobutadiene
0.962 0.478 ug/L 06/05/23 11:58 06/07/23 17:55 1NDHexachlorocyclopentadiene
0.962 0.128 ug/L 06/05/23 11:58 06/07/23 17:55 1NDHexachloroethane
0.183 0.0817 ug/L 06/05/23 11:58 06/07/23 17:55 1NDIndeno[1,2,3-cd]pyrene
0.962 0.181 ug/L 06/05/23 11:58 06/07/23 17:55 1NDIsophorone
0.183 0.0567 ug/L 06/05/23 11:58 06/07/23 17:55 10.0902 JNaphthalene
1.92 0.481 ug/L 06/05/23 11:58 06/07/23 17:55 1NDNitrobenzene
0.962 0.0644 ug/L 06/05/23 11:58 06/07/23 17:55 1NDN-Nitrosodimethylamine
0.183 0.0683 ug/L 06/05/23 11:58 06/07/23 17:55 1NDN-Nitrosodi-n-propylamine
0.962 0.362 ug/L 06/05/23 11:58 06/07/23 17:55 1ND4-Chloroaniline
0.183 0.0529 ug/L 06/05/23 11:58 06/07/23 17:55 1NDPhenanthrene
0.183 0.0519 ug/L 06/05/23 11:58 06/07/23 17:55 1NDPyrene
0.962 0.358 ug/L 06/05/23 11:58 06/07/23 17:55 1ND4-Methylphenol
4.81 0.814 ug/L 06/05/23 11:58 06/07/23 17:55 1NDPentachlorophenol
0.962 0.468 ug/L 06/05/23 11:58 06/07/23 17:55 1NDPhenol
0.962 0.126 ug/L 06/05/23 11:58 06/07/23 17:55 1ND1,2,4-Trichlorobenzene
0.183 0.0490 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2,4-Dichlorophenol
9.62 1.47 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2,4-Dinitrophenol
0.962 0.161 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2,4-Dimethylphenol
0.962 0.215 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2,4,6-Trichlorophenol
0.962 0.124 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2-Chlorophenol
0.962 0.186 ug/L 06/05/23 11:58 06/07/23 17:55 1ND2-Nitrophenol
4.81 1.41 ug/L 06/05/23 11:58 06/07/23 17:55 1ND4,6-Dinitro-2-methylphenol
0.962 0.267 ug/L 06/05/23 11:58 06/07/23 17:55 1ND4-Chloro-3-methylphenol
4.81 0.904 ug/L 06/05/23 11:58 06/07/23 17:55 1ND4-Nitrophenol
4.81 0.888 ug/L 06/05/23 11:58 06/07/23 17:55 1NDBenzoic acid
0.962 0.157 ug/L 06/05/23 11:58 06/07/23 17:55 10.236 JBenzyl alcohol
0.962 0.183 ug/L 06/05/23 11:58 06/07/23 17:55 1NDDibenzofuran
2,4,6-Tribromophenol (Surr)51 32-127 06/05/23 11:58 06/07/23 17:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 64 06/05/23 11:58 06/07/23 17:55 147-107
2-Fluorophenol (Surr)51 06/05/23 11:58 06/07/23 17:55 135-109
Nitrobenzene-d5 (Surr)60 06/05/23 11:58 06/07/23 17:55 147-110
Phenol-d5 (Surr)56 06/05/23 11:58 06/07/23 17:55 137-110
Terphenyl-d14 (Surr)97 06/05/23 11:58 06/07/23 17:55 132-115
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
64.3 J 100 20.0 ug/L 06/09/23 13:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
64.3 J 100 25.0 ug/L 06/09/23 08:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 06/09/23 08:35 1NDC9-C10 Aromatics
100 25.0 ug/L 06/09/23 08:35 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 06/09/23 08:35 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 06/09/23 08:35 161.9 JC5-C8 Aliphatics (adjusted)
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-8Client Sample ID: TMW-3
Matrix: WaterDate Collected: 05/31/23 09:15
Date Received: 06/01/23 10:30
a,a,a-Trifluorotoluene (fid)113 70-130 06/09/23 08:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)100 06/09/23 08:35 170-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 41.7 41.7 ug/L 06/09/23 19:11 06/27/23 04:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
41.7 41.7 ug/L 06/09/23 19:11 06/27/23 04:24 1NDC11-C22 Aromatics (Adjusted)
52.1 52.1 ug/L 06/09/23 19:11 06/27/23 04:24 1NDC19-C36 Aliphatics
31.3 31.3 ug/L 06/09/23 19:11 06/27/23 04:24 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)37 S1-40-140 06/09/23 19:11 06/27/23 04:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)85 06/09/23 19:11 06/27/23 04:24 140-140
o- terphenyl (Surr)48 06/09/23 19:11 06/27/23 04:24 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 06/27/23 19:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
41.7 41.7 ug/L 06/27/23 19:06 1NDC11-C22 Aromatics
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-9Client Sample ID: TMW-4
Matrix: WaterDate Collected: 05/31/23 15:31
Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 06/07/23 17:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 06/07/23 17:12 1ND1,3-Dichlorobenzene
1.00 0.544 ug/L 06/07/23 17:12 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 06/07/23 17:12 1NDBenzene
1.00 0.501 ug/L 06/07/23 17:12 1NDChlorobenzene
1.00 0.507 ug/L 06/07/23 17:12 1NDEthylbenzene
1.00 0.457 ug/L 06/07/23 17:12 1NDToluene
1.00 0.406 ug/L 06/07/23 17:12 1NDo-Xylene
1.00 0.482 ug/L 06/07/23 17:12 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 06/07/23 17:12 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)83 26-156 06/07/23 17:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)81 06/07/23 17:12 136-124
Dibromofluoromethane (Surr)109 06/07/23 17:12 146-149
Toluene-d8 (Surr)101 06/07/23 17:12 140-146
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 18:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 18:18 1NDAcenaphthylene
0.190 0.0490 ug/L 06/05/23 11:58 06/07/23 18:18 1NDAnthracene
1.00 0.0950 ug/L 06/05/23 11:58 06/07/23 18:18 1ND1,2-Dichlorobenzene
0.190 0.0750 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBenzo[a]anthracene
0.190 0.0530 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBenzo[a]pyrene
1.00 0.0990 ug/L 06/05/23 11:58 06/07/23 18:18 1ND1,3-Dichlorobenzene
0.190 0.0970 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBenzo[b]fluoranthene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBenzo[g,h,i]perylene
1.00 0.0610 ug/L 06/05/23 11:58 06/07/23 18:18 1ND1,4-Dichlorobenzene
0.190 0.0880 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBenzo[k]fluoranthene
1.00 0.152 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBis(2-chloroethoxy)methane
0.190 0.0400 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBis(2-chloroethyl)ether
0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 18:18 1ND1-Methylnaphthalene
0.190 0.0580 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2,2'-oxybis[1-chloropropane]
10.0 6.23 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBis(2-ethylhexyl) phthalate
1.00 0.319 ug/L 06/05/23 11:58 06/07/23 18:18 1ND4-Bromophenyl phenyl ether
1.00 0.462 ug/L 06/05/23 11:58 06/07/23 18:18 1NDButyl benzyl phthalate
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2-Chloronaphthalene
1.00 0.221 ug/L 06/05/23 11:58 06/07/23 18:18 1ND4-Chlorophenyl phenyl ether
0.190 0.0810 ug/L 06/05/23 11:58 06/07/23 18:18 1NDChrysene
0.190 0.0720 ug/L 06/05/23 11:58 06/07/23 18:18 1NDDibenz(a,h)anthracene
1.00 0.583 ug/L 06/05/23 11:58 06/07/23 18:18 1ND3,3'-Dichlorobenzidine
1.00 0.567 ug/L 06/05/23 11:58 06/07/23 18:18 10.678 JDiethyl phthalate
1.00 0.685 ug/L 06/05/23 11:58 06/07/23 18:18 1NDDi-n-octyl phthalate
1.00 0.196 ug/L 06/05/23 11:58 06/07/23 18:18 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.190 0.0620 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2-Methylnaphthalene
0.190 0.0600 ug/L 06/05/23 11:58 06/07/23 18:18 1NDFluoranthene
1.00 0.300 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2-Methylphenol
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 18:18 1NDFluorene
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-9Client Sample ID: TMW-4
Matrix: WaterDate Collected: 05/31/23 15:31
Date Received: 06/01/23 10:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 18:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexachlorobenzene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 18:18 1NDHexachlorobutadiene
1.00 0.497 ug/L 06/05/23 11:58 06/07/23 18:18 1NDHexachlorocyclopentadiene
1.00 0.133 ug/L 06/05/23 11:58 06/07/23 18:18 1NDHexachloroethane
0.190 0.0850 ug/L 06/05/23 11:58 06/07/23 18:18 1NDIndeno[1,2,3-cd]pyrene
1.00 0.188 ug/L 06/05/23 11:58 06/07/23 18:18 1NDIsophorone
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 18:18 10.0958 JNaphthalene
2.00 0.500 ug/L 06/05/23 11:58 06/07/23 18:18 1NDNitrobenzene
1.00 0.0670 ug/L 06/05/23 11:58 06/07/23 18:18 1NDN-Nitrosodimethylamine
0.190 0.0710 ug/L 06/05/23 11:58 06/07/23 18:18 1NDN-Nitrosodi-n-propylamine
1.00 0.376 ug/L 06/05/23 11:58 06/07/23 18:18 1ND4-Chloroaniline
0.190 0.0550 ug/L 06/05/23 11:58 06/07/23 18:18 1NDPhenanthrene
0.190 0.0540 ug/L 06/05/23 11:58 06/07/23 18:18 1NDPyrene
1.00 0.372 ug/L 06/05/23 11:58 06/07/23 18:18 1ND4-Methylphenol
5.00 0.847 ug/L 06/05/23 11:58 06/07/23 18:18 1NDPentachlorophenol
1.00 0.487 ug/L 06/05/23 11:58 06/07/23 18:18 1NDPhenol
1.00 0.131 ug/L 06/05/23 11:58 06/07/23 18:18 1ND1,2,4-Trichlorobenzene
0.190 0.0510 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2,4-Dichlorophenol
10.0 1.53 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2,4-Dinitrophenol
1.00 0.167 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2,4-Dimethylphenol
1.00 0.224 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2,4,6-Trichlorophenol
1.00 0.129 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2-Chlorophenol
1.00 0.193 ug/L 06/05/23 11:58 06/07/23 18:18 1ND2-Nitrophenol
5.00 1.47 ug/L 06/05/23 11:58 06/07/23 18:18 1ND4,6-Dinitro-2-methylphenol
1.00 0.278 ug/L 06/05/23 11:58 06/07/23 18:18 1ND4-Chloro-3-methylphenol
5.00 0.940 ug/L 06/05/23 11:58 06/07/23 18:18 1ND4-Nitrophenol
5.00 0.923 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBenzoic acid
1.00 0.163 ug/L 06/05/23 11:58 06/07/23 18:18 1NDBenzyl alcohol
1.00 0.190 ug/L 06/05/23 11:58 06/07/23 18:18 1NDDibenzofuran
2,4,6-Tribromophenol (Surr)48 32-127 06/05/23 11:58 06/07/23 18:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 62 06/05/23 11:58 06/07/23 18:18 147-107
2-Fluorophenol (Surr)51 06/05/23 11:58 06/07/23 18:18 135-109
Nitrobenzene-d5 (Surr)57 06/05/23 11:58 06/07/23 18:18 147-110
Phenol-d5 (Surr)51 06/05/23 11:58 06/07/23 18:18 137-110
Terphenyl-d14 (Surr)79 06/05/23 11:58 06/07/23 18:18 132-115
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 20.0 ug/L 06/09/23 13:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 25.0 ug/L 06/09/23 09:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 06/09/23 09:16 1NDC9-C10 Aromatics
100 25.0 ug/L 06/09/23 09:16 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 06/09/23 09:16 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 06/09/23 09:16 1NDC5-C8 Aliphatics (adjusted)
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-9Client Sample ID: TMW-4
Matrix: WaterDate Collected: 05/31/23 15:31
Date Received: 06/01/23 10:30
a,a,a-Trifluorotoluene (fid)107 70-130 06/09/23 09:16 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)97 06/09/23 09:16 170-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 44.5 44.5 ug/L 06/09/23 19:11 06/27/23 04:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
44.5 44.5 ug/L 06/09/23 19:11 06/27/23 04:47 1NDC11-C22 Aromatics (Adjusted)
55.6 55.6 ug/L 06/09/23 19:11 06/27/23 04:47 1NDC19-C36 Aliphatics
33.4 33.4 ug/L 06/09/23 19:11 06/27/23 04:47 133.8C9-C18 Aliphatics
1-Chlorooctadecane (Surr)53 40-140 06/09/23 19:11 06/27/23 04:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)90 06/09/23 19:11 06/27/23 04:47 140-140
o- terphenyl (Surr)75 06/09/23 19:11 06/27/23 04:47 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
33.8 J 100 30.0 ug/L 06/27/23 19:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
44.5 44.5 ug/L 06/27/23 19:06 1NDC11-C22 Aromatics
Eurofins Pittsburgh
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-10Client Sample ID: TMW-8
Matrix: WaterDate Collected: 05/31/23 12:30
Date Received: 06/01/23 10:30
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 06/07/23 17:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 06/07/23 17:33 1ND1,3-Dichlorobenzene
1.00 0.544 ug/L 06/07/23 17:33 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 06/07/23 17:33 1NDBenzene
1.00 0.501 ug/L 06/07/23 17:33 1NDChlorobenzene
1.00 0.507 ug/L 06/07/23 17:33 1NDEthylbenzene
1.00 0.457 ug/L 06/07/23 17:33 1NDToluene
1.00 0.406 ug/L 06/07/23 17:33 1NDo-Xylene
1.00 0.482 ug/L 06/07/23 17:33 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 06/07/23 17:33 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)90 26-156 06/07/23 17:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)78 06/07/23 17:33 136-124
Dibromofluoromethane (Surr)111 06/07/23 17:33 146-149
Toluene-d8 (Surr)96 06/07/23 17:33 140-146
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 18:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 18:40 1NDAcenaphthylene
0.190 0.0490 ug/L 06/05/23 11:58 06/07/23 18:40 1NDAnthracene
1.00 0.0950 ug/L 06/05/23 11:58 06/07/23 18:40 1ND1,2-Dichlorobenzene
0.190 0.0750 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBenzo[a]anthracene
0.190 0.0530 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBenzo[a]pyrene
1.00 0.0990 ug/L 06/05/23 11:58 06/07/23 18:40 1ND1,3-Dichlorobenzene
0.190 0.0970 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBenzo[b]fluoranthene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBenzo[g,h,i]perylene
1.00 0.0610 ug/L 06/05/23 11:58 06/07/23 18:40 1ND1,4-Dichlorobenzene
0.190 0.0880 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBenzo[k]fluoranthene
1.00 0.152 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBis(2-chloroethoxy)methane
0.190 0.0400 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBis(2-chloroethyl)ether
0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 18:40 1ND1-Methylnaphthalene
0.190 0.0580 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2,2'-oxybis[1-chloropropane]
10.0 6.23 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBis(2-ethylhexyl) phthalate
1.00 0.319 ug/L 06/05/23 11:58 06/07/23 18:40 1ND4-Bromophenyl phenyl ether
1.00 0.462 ug/L 06/05/23 11:58 06/07/23 18:40 1NDButyl benzyl phthalate
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2-Chloronaphthalene
1.00 0.221 ug/L 06/05/23 11:58 06/07/23 18:40 1ND4-Chlorophenyl phenyl ether
0.190 0.0810 ug/L 06/05/23 11:58 06/07/23 18:40 1NDChrysene
0.190 0.0720 ug/L 06/05/23 11:58 06/07/23 18:40 1NDDibenz(a,h)anthracene
1.00 0.583 ug/L 06/05/23 11:58 06/07/23 18:40 1ND3,3'-Dichlorobenzidine
1.00 0.567 ug/L 06/05/23 11:58 06/07/23 18:40 1NDDiethyl phthalate
1.00 0.685 ug/L 06/05/23 11:58 06/07/23 18:40 1NDDi-n-octyl phthalate
1.00 0.196 ug/L 06/05/23 11:58 06/07/23 18:40 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.190 0.0620 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2-Methylnaphthalene
0.190 0.0600 ug/L 06/05/23 11:58 06/07/23 18:40 1NDFluoranthene
1.00 0.300 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2-Methylphenol
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 18:40 1NDFluorene
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-10Client Sample ID: TMW-8
Matrix: WaterDate Collected: 05/31/23 12:30
Date Received: 06/01/23 10:30
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 18:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexachlorobenzene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 18:40 1NDHexachlorobutadiene
1.00 0.497 ug/L 06/05/23 11:58 06/07/23 18:40 1NDHexachlorocyclopentadiene
1.00 0.133 ug/L 06/05/23 11:58 06/07/23 18:40 1NDHexachloroethane
0.190 0.0850 ug/L 06/05/23 11:58 06/07/23 18:40 1NDIndeno[1,2,3-cd]pyrene
1.00 0.188 ug/L 06/05/23 11:58 06/07/23 18:40 1NDIsophorone
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 18:40 1NDNaphthalene
2.00 0.500 ug/L 06/05/23 11:58 06/07/23 18:40 1NDNitrobenzene
1.00 0.0670 ug/L 06/05/23 11:58 06/07/23 18:40 1NDN-Nitrosodimethylamine
0.190 0.0710 ug/L 06/05/23 11:58 06/07/23 18:40 1NDN-Nitrosodi-n-propylamine
1.00 0.376 ug/L 06/05/23 11:58 06/07/23 18:40 1ND4-Chloroaniline
0.190 0.0550 ug/L 06/05/23 11:58 06/07/23 18:40 1NDPhenanthrene
0.190 0.0540 ug/L 06/05/23 11:58 06/07/23 18:40 1NDPyrene
1.00 0.372 ug/L 06/05/23 11:58 06/07/23 18:40 1ND4-Methylphenol
5.00 0.847 ug/L 06/05/23 11:58 06/07/23 18:40 1NDPentachlorophenol
1.00 0.487 ug/L 06/05/23 11:58 06/07/23 18:40 1NDPhenol
1.00 0.131 ug/L 06/05/23 11:58 06/07/23 18:40 1ND1,2,4-Trichlorobenzene
0.190 0.0510 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2,4-Dichlorophenol
10.0 1.53 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2,4-Dinitrophenol
1.00 0.167 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2,4-Dimethylphenol
1.00 0.224 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2,4,6-Trichlorophenol
1.00 0.129 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2-Chlorophenol
1.00 0.193 ug/L 06/05/23 11:58 06/07/23 18:40 1ND2-Nitrophenol
5.00 1.47 ug/L 06/05/23 11:58 06/07/23 18:40 1ND4,6-Dinitro-2-methylphenol
1.00 0.278 ug/L 06/05/23 11:58 06/07/23 18:40 1ND4-Chloro-3-methylphenol
5.00 0.940 ug/L 06/05/23 11:58 06/07/23 18:40 1ND4-Nitrophenol
5.00 0.923 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBenzoic acid
1.00 0.163 ug/L 06/05/23 11:58 06/07/23 18:40 1NDBenzyl alcohol
1.00 0.190 ug/L 06/05/23 11:58 06/07/23 18:40 1NDDibenzofuran
2,4,6-Tribromophenol (Surr)49 32-127 06/05/23 11:58 06/07/23 18:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 64 06/05/23 11:58 06/07/23 18:40 147-107
2-Fluorophenol (Surr)58 06/05/23 11:58 06/07/23 18:40 135-109
Nitrobenzene-d5 (Surr)60 06/05/23 11:58 06/07/23 18:40 147-110
Phenol-d5 (Surr)56 06/05/23 11:58 06/07/23 18:40 137-110
Terphenyl-d14 (Surr)73 06/05/23 11:58 06/07/23 18:40 132-115
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 20.0 ug/L 06/09/23 13:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 25.0 ug/L 06/09/23 09:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 06/09/23 09:57 1NDC9-C10 Aromatics
100 25.0 ug/L 06/09/23 09:57 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 06/09/23 09:57 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 06/09/23 09:57 1NDC5-C8 Aliphatics (adjusted)
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Client Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157361-10Client Sample ID: TMW-8
Matrix: WaterDate Collected: 05/31/23 12:30
Date Received: 06/01/23 10:30
a,a,a-Trifluorotoluene (fid)108 70-130 06/09/23 09:57 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)98 06/09/23 09:57 170-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 41.5 41.5 ug/L 06/09/23 19:11 06/27/23 05:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
41.5 41.5 ug/L 06/09/23 19:11 06/27/23 05:09 1NDC11-C22 Aromatics (Adjusted)
51.9 51.9 ug/L 06/09/23 19:11 06/27/23 05:09 1NDC19-C36 Aliphatics
31.1 31.1 ug/L 06/09/23 19:11 06/27/23 05:09 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)53 40-140 06/09/23 19:11 06/27/23 05:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)81 06/09/23 19:11 06/27/23 05:09 140-140
o- terphenyl (Surr)66 06/09/23 19:11 06/27/23 05:09 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 06/27/23 19:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
41.5 41.5 ug/L 06/27/23 19:06 1NDC11-C22 Aromatics
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Matrix SpikeLab Sample ID: 180-157381-C-19-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900 Prep Batch: 436877
1,1,1-Trichloroethane ND 38.7 34.26 ug/Kg 89 72-134☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,1,2,2-Tetrachloroethane ND 38.7 33.93 ug/Kg 88 36-170☼
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 38.7 32.43 ug/Kg 84 59-135☼
1,1,2-Trichloroethane ND 38.7 34.40 ug/Kg 89 66-128☼
1,1-Dichloroethane ND 38.7 35.00 ug/Kg 90 73-124☼
1,1-Dichloroethene ND 38.7 34.43 ug/Kg 89 55-136☼
1,2-Dibromo-3-Chloropropane ND 38.7 30.46 ug/Kg 79 30-163☼
1,2-Dichlorobenzene ND 38.7 34.77 ug/Kg 90 76-120☼
1,2-Dichloroethane ND 38.7 34.50 ug/Kg 89 64-140☼
1,2-Dichloropropane ND 38.7 34.36 ug/Kg 89 77-119☼
1,2,4-Trichlorobenzene ND 38.7 32.49 ug/Kg 84 22-170☼
1,3-Dichlorobenzene ND 38.7 34.67 ug/Kg 90 77-121☼
1,4-Dichlorobenzene ND 38.7 34.45 ug/Kg 89 79-120☼
2-Butanone (MEK)ND 38.7 37.01 ug/Kg 96 39-157☼
2-Hexanone ND 38.7 34.24 ug/Kg 88 42-152☼
4-Methyl-2-pentanone (MIBK)ND 38.7 35.59 ug/Kg 92 51-147☼
Acetone ND 38.7 37.80 ug/Kg 98 23-170☼
Benzene ND 38.7 35.52 ug/Kg 92 77-120☼
Bromoform ND 38.7 30.01 ug/Kg 78 37-147☼
Bromomethane ND 38.7 27.70 ug/Kg 72 47-149☼
Carbon disulfide ND 38.7 31.82 ug/Kg 82 40-156☼
Carbon tetrachloride ND 38.7 33.68 ug/Kg 87 73-130☼
Chlorobenzene ND 38.7 34.77 ug/Kg 90 79-122☼
Chlorodibromomethane ND 38.7 32.05 ug/Kg 83 60-134☼
Chloroform ND 38.7 35.52 ug/Kg 92 73-126☼
Chloromethane ND 38.7 33.53 ug/Kg 87 46-151☼
Chloroethane ND 38.7 27.11 ug/Kg 70 37-159☼
cis-1,2-Dichloroethene ND 38.7 35.65 ug/Kg 92 77-118☼
cis-1,3-Dichloropropene ND 38.7 34.54 ug/Kg 89 73-127☼
Dichlorobromomethane ND 38.7 33.85 ug/Kg 87 75-123☼
Dichlorodifluoromethane ND 38.7 26.08 ug/Kg 67 26-149☼
Ethylbenzene ND 38.7 34.59 ug/Kg 89 79-119☼
1,2-Dibromoethane ND 38.7 34.99 ug/Kg 90 59-137☼
Cyclohexane ND 38.7 33.50 ug/Kg 87 63-143☼
Isopropylbenzene ND 38.7 35.30 ug/Kg 91 70-125☼
Methyl acetate ND *+77.4 83.67 ug/Kg 108 20-170☼
Methyl tert-butyl ether ND 38.7 32.92 ug/Kg 85 58-132☼
Methylcyclohexane ND 38.7 34.34 ug/Kg 89 70-125☼
Methylene Chloride ND 38.7 35.06 ug/Kg 91 67-131☼
m-Xylene & p-Xylene ND 38.7 34.64 ug/Kg 89 77-120☼
o-Xylene ND 38.7 34.63 ug/Kg 89 78-118☼
Styrene ND 38.7 34.35 ug/Kg 89 80-120☼
Tetrachloroethene ND 38.7 34.91 ug/Kg 90 71-121☼
Toluene ND 38.7 34.62 ug/Kg 89 76-120☼
trans-1,2-Dichloroethene ND 38.7 35.38 ug/Kg 91 75-122☼
trans-1,3-Dichloropropene ND 38.7 33.52 ug/Kg 87 68-133☼
Trichloroethene ND 38.7 35.22 ug/Kg 91 69-118☼
Trichlorofluoromethane ND 38.7 46.66 ug/Kg 121 32-149☼
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-157381-C-19-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900 Prep Batch: 436877
Vinyl chloride ND 38.7 37.02 ug/Kg 96 64-134☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Xylenes, Total ND 77.4 69.27 ug/Kg 89 78-118☼
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
95
MS MS
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)60 -124
95Dibromofluoromethane (Surr)69 -126
99Toluene-d8 (Surr)67 -134
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-157381-C-19-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900 Prep Batch: 436877
1,1,1-Trichloroethane ND 39.6 34.20 ug/Kg 86 72-134 0 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane ND 39.6 32.66 ug/Kg 82 36-170 4 23☼
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
ND 39.6 33.03 ug/Kg 83 59-135 2 28☼
1,1,2-Trichloroethane ND 39.6 33.28 ug/Kg 84 66-128 3 21☼
1,1-Dichloroethane ND 39.6 35.40 ug/Kg 89 73-124 1 20☼
1,1-Dichloroethene ND 39.6 34.62 ug/Kg 87 55-136 1 21☼
1,2-Dibromo-3-Chloropropane ND 39.6 28.18 ug/Kg 71 30-163 8 34☼
1,2-Dichlorobenzene ND 39.6 34.55 ug/Kg 87 76-120 1 20☼
1,2-Dichloroethane ND 39.6 33.76 ug/Kg 85 64-140 2 20☼
1,2-Dichloropropane ND 39.6 35.08 ug/Kg 89 77-119 2 20☼
1,2,4-Trichlorobenzene ND 39.6 33.55 ug/Kg 85 22-170 3 29☼
1,3-Dichlorobenzene ND 39.6 35.40 ug/Kg 89 77-121 2 20☼
1,4-Dichlorobenzene ND 39.6 34.70 ug/Kg 88 79-120 1 20☼
2-Butanone (MEK)ND 39.6 29.66 ug/Kg 75 39-157 22 33☼
2-Hexanone ND 39.6 28.97 ug/Kg 73 42-152 17 30☼
4-Methyl-2-pentanone (MIBK)ND 39.6 30.04 ug/Kg 76 51-147 17 27☼
Acetone ND 39.6 34.04 ug/Kg 86 23-170 10 35☼
Benzene ND 39.6 35.84 ug/Kg 90 77-120 1 20☼
Bromoform ND 39.6 28.83 ug/Kg 73 37-147 4 23☼
Bromomethane ND 39.6 30.75 ug/Kg 78 47-149 10 25☼
Carbon disulfide ND 39.6 32.52 ug/Kg 82 40-156 2 25☼
Carbon tetrachloride ND 39.6 33.86 ug/Kg 85 73-130 1 21☼
Chlorobenzene ND 39.6 34.84 ug/Kg 88 79-122 0 20☼
Chlorodibromomethane ND 39.6 32.20 ug/Kg 81 60-134 0 40☼
Chloroform ND 39.6 36.46 ug/Kg 92 73-126 3 20☼
Chloromethane ND 39.6 35.10 ug/Kg 89 46-151 5 33☼
Chloroethane ND 39.6 27.77 ug/Kg 70 37-159 2 25☼
cis-1,2-Dichloroethene ND 39.6 35.64 ug/Kg 90 77-118 0 20☼
cis-1,3-Dichloropropene ND 39.6 34.99 ug/Kg 88 73-127 1 20☼
Dichlorobromomethane ND 39.6 34.40 ug/Kg 87 75-123 2 20☼
Dichlorodifluoromethane ND 39.6 26.01 ug/Kg 66 26-149 0 24☼
Ethylbenzene ND 39.6 35.07 ug/Kg 89 79-119 1 20☼
1,2-Dibromoethane ND 39.6 34.09 ug/Kg 86 59-137 3 20☼
Cyclohexane ND 39.6 34.24 ug/Kg 86 63-143 2 25☼
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-157381-C-19-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900 Prep Batch: 436877
Isopropylbenzene ND 39.6 35.41 ug/Kg 89 70-125 0 21☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Methyl acetate ND *+79.2 74.97 ug/Kg 95 20-170 11 33☼
Methyl tert-butyl ether ND 39.6 32.73 ug/Kg 83 58-132 1 24☼
Methylcyclohexane ND 39.6 34.31 ug/Kg 87 70-125 0 22☼
Methylene Chloride ND 39.6 35.75 ug/Kg 90 67-131 2 32☼
m-Xylene & p-Xylene ND 39.6 35.46 ug/Kg 90 77-120 2 20☼
o-Xylene ND 39.6 35.41 ug/Kg 89 78-118 2 20☼
Styrene ND 39.6 35.04 ug/Kg 88 80-120 2 20☼
Tetrachloroethene ND 39.6 34.71 ug/Kg 88 71-121 1 21☼
Toluene ND 39.6 34.96 ug/Kg 88 76-120 1 20☼
trans-1,2-Dichloroethene ND 39.6 35.76 ug/Kg 90 75-122 1 20☼
trans-1,3-Dichloropropene ND 39.6 32.97 ug/Kg 83 68-133 2 20☼
Trichloroethene ND 39.6 35.61 ug/Kg 90 69-118 1 20☼
Trichlorofluoromethane ND 39.6 49.98 ug/Kg 126 32-149 7 39☼
Vinyl chloride ND 39.6 37.00 ug/Kg 93 64-134 0 23☼
Xylenes, Total ND 79.2 70.87 ug/Kg 89 78-118 2 20☼
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
92
MSD MSD
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)60 -124
94Dibromofluoromethane (Surr)69 -126
99Toluene-d8 (Surr)67 -134
Client Sample ID: Method BlankLab Sample ID: MB 180-436900/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900
RL MDL
1,1,1-Trichloroethane ND 5.00 1.67 ug/Kg 06/03/23 12:29 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.525.00 ug/Kg 06/03/23 12:29 11,1,2,2-Tetrachloroethane
ND 2.005.00 ug/Kg 06/03/23 12:29 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.9905.00 ug/Kg 06/03/23 12:29 11,1,2-Trichloroethane
ND 1.605.00 ug/Kg 06/03/23 12:29 11,1-Dichloroethane
ND 2.265.00 ug/Kg 06/03/23 12:29 11,1-Dichloroethene
ND 3.235.00 ug/Kg 06/03/23 12:29 11,2-Dibromo-3-Chloropropane
ND 1.685.00 ug/Kg 06/03/23 12:29 11,2-Dichlorobenzene
ND 1.445.00 ug/Kg 06/03/23 12:29 11,2-Dichloroethane
ND 1.335.00 ug/Kg 06/03/23 12:29 11,2-Dichloropropane
ND 2.545.00 ug/Kg 06/03/23 12:29 11,2,4-Trichlorobenzene
ND 3.085.00 ug/Kg 06/03/23 12:29 11,3-Dichlorobenzene
ND 1.505.00 ug/Kg 06/03/23 12:29 11,4-Dichlorobenzene
ND 2.5425.0 ug/Kg 06/03/23 12:29 12-Butanone (MEK)
ND 1.5725.0 ug/Kg 06/03/23 12:29 12-Hexanone
ND 1.8325.0 ug/Kg 06/03/23 12:29 14-Methyl-2-pentanone (MIBK)
ND 3.9025.0 ug/Kg 06/03/23 12:29 1Acetone
ND 1.415.00 ug/Kg 06/03/23 12:29 1Benzene
ND 2.525.00 ug/Kg 06/03/23 12:29 1Bromoform
ND 2.285.00 ug/Kg 06/03/23 12:29 1Bromomethane
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-436900/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900
RL MDL
Carbon disulfide ND 5.00 4.00 ug/Kg 06/03/23 12:29 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 2.035.00 ug/Kg 06/03/23 12:29 1Carbon tetrachloride
ND 1.305.00 ug/Kg 06/03/23 12:29 1Chlorobenzene
ND 2.485.00 ug/Kg 06/03/23 12:29 1Chlorodibromomethane
ND 3.355.00 ug/Kg 06/03/23 12:29 1Chloroform
ND 1.985.00 ug/Kg 06/03/23 12:29 1Chloromethane
ND 2.925.00 ug/Kg 06/03/23 12:29 1Chloroethane
ND 1.515.00 ug/Kg 06/03/23 12:29 1cis-1,2-Dichloroethene
ND 2.215.00 ug/Kg 06/03/23 12:29 1cis-1,3-Dichloropropene
ND 2.335.00 ug/Kg 06/03/23 12:29 1Dichlorobromomethane
ND 2.495.00 ug/Kg 06/03/23 12:29 1Dichlorodifluoromethane
ND 1.855.00 ug/Kg 06/03/23 12:29 1Ethylbenzene
ND 1.375.00 ug/Kg 06/03/23 12:29 11,2-Dibromoethane
ND 2.395.00 ug/Kg 06/03/23 12:29 1Cyclohexane
ND 2.605.00 ug/Kg 06/03/23 12:29 1Isopropylbenzene
ND 7.3625.0 ug/Kg 06/03/23 12:29 1Methyl acetate
ND 1.475.00 ug/Kg 06/03/23 12:29 1Methyl tert-butyl ether
ND 2.415.00 ug/Kg 06/03/23 12:29 1Methylcyclohexane
ND 4.515.00 ug/Kg 06/03/23 12:29 1Methylene Chloride
ND 1.505.00 ug/Kg 06/03/23 12:29 1Styrene
ND 2.015.00 ug/Kg 06/03/23 12:29 1Tetrachloroethene
ND 1.445.00 ug/Kg 06/03/23 12:29 1Toluene
ND 1.755.00 ug/Kg 06/03/23 12:29 1trans-1,2-Dichloroethene
ND 2.255.00 ug/Kg 06/03/23 12:29 1trans-1,3-Dichloropropene
ND 1.575.00 ug/Kg 06/03/23 12:29 1Trichloroethene
ND 4.155.00 ug/Kg 06/03/23 12:29 1Trichlorofluoromethane
ND 3.605.00 ug/Kg 06/03/23 12:29 1Vinyl chloride
ND 7.2110.0 ug/Kg 06/03/23 12:29 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)112 73-135 06/03/23 12:29 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
98 06/03/23 12:29 14-Bromofluorobenzene (Surr)60-124
104 06/03/23 12:29 1Dibromofluoromethane (Surr)69-126
94 06/03/23 12:29 1Toluene-d8 (Surr)67-134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-436900/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900
1,1,1-Trichloroethane 40.0 38.13 ug/Kg 95 72-134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2,2-Tetrachloroethane 40.0 33.05 ug/Kg 83 36-170
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 35.99 ug/Kg 90 59-135
1,1,2-Trichloroethane 40.0 34.59 ug/Kg 86 66-128
1,1-Dichloroethane 40.0 39.38 ug/Kg 98 73-124
1,1-Dichloroethene 40.0 37.99 ug/Kg 95 55-136
1,2-Dibromo-3-Chloropropane 40.0 27.31 ug/Kg 68 30-163
1,2-Dichlorobenzene 40.0 34.49 ug/Kg 86 76-120
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-436900/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900
1,2-Dichloroethane 40.0 38.20 ug/Kg 95 64-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dichloropropane 40.0 38.05 ug/Kg 95 77-119
1,2,4-Trichlorobenzene 40.0 33.36 ug/Kg 83 22-170
1,3-Dichlorobenzene 40.0 34.98 ug/Kg 87 77-121
1,4-Dichlorobenzene 40.0 34.77 ug/Kg 87 79-120
2-Butanone (MEK)40.0 42.12 ug/Kg 105 39-157
2-Hexanone 40.0 38.07 ug/Kg 95 42-152
4-Methyl-2-pentanone (MIBK)40.0 40.86 ug/Kg 102 51-147
Acetone 40.0 42.82 ug/Kg 107 23-170
Benzene 40.0 39.64 ug/Kg 99 77-120
Bromoform 40.0 29.49 ug/Kg 74 37-147
Bromomethane 40.0 32.36 ug/Kg 81 47-149
Carbon disulfide 40.0 35.27 ug/Kg 88 40-156
Carbon tetrachloride 40.0 37.21 ug/Kg 93 73-130
Chlorobenzene 40.0 34.76 ug/Kg 87 79-122
Chlorodibromomethane 40.0 31.50 ug/Kg 79 60-134
Chloroform 40.0 40.19 ug/Kg 100 73-126
Chloromethane 40.0 36.95 ug/Kg 92 46-151
Chloroethane 40.0 28.04 ug/Kg 70 37-159
cis-1,2-Dichloroethene 40.0 39.37 ug/Kg 98 77-118
cis-1,3-Dichloropropene 40.0 38.55 ug/Kg 96 73-127
Dichlorobromomethane 40.0 38.27 ug/Kg 96 75-123
Dichlorodifluoromethane 40.0 29.08 ug/Kg 73 26-149
Ethylbenzene 40.0 35.28 ug/Kg 88 79-119
1,2-Dibromoethane 40.0 35.26 ug/Kg 88 59-137
Cyclohexane 40.0 37.08 ug/Kg 93 63-143
Isopropylbenzene 40.0 35.36 ug/Kg 88 70-125
Methyl acetate 80.0 197.9 *+ug/Kg 247 20-170
Methyl tert-butyl ether 40.0 36.74 ug/Kg 92 58-132
Methylcyclohexane 40.0 37.65 ug/Kg 94 70-125
Methylene Chloride 40.0 41.17 ug/Kg 103 67-131
m-Xylene & p-Xylene 40.0 35.25 ug/Kg 88 77-120
o-Xylene 40.0 35.11 ug/Kg 88 78-118
Styrene 40.0 35.41 ug/Kg 89 80-120
Tetrachloroethene 40.0 35.28 ug/Kg 88 71-121
Toluene 40.0 35.56 ug/Kg 89 76-120
trans-1,2-Dichloroethene 40.0 39.80 ug/Kg 100 75-122
trans-1,3-Dichloropropene 40.0 33.89 ug/Kg 85 68-133
Trichloroethene 40.0 38.84 ug/Kg 97 69-118
Trichlorofluoromethane 40.0 48.75 ug/Kg 122 32-149
Vinyl chloride 40.0 42.60 ug/Kg 107 64-134
Xylenes, Total 80.0 70.36 ug/Kg 88 78-118
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
974-Bromofluorobenzene (Surr)60 -124
102Dibromofluoromethane (Surr)69 -126
97Toluene-d8 (Surr)67 -134
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-436900/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900
1,1,1-Trichloroethane 40.0 39.55 ug/Kg 99 72-134 4 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 40.0 31.58 ug/Kg 79 36-170 5 23
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 37.39 ug/Kg 93 59-135 4 28
1,1,2-Trichloroethane 40.0 33.55 ug/Kg 84 66-128 3 21
1,1-Dichloroethane 40.0 40.81 ug/Kg 102 73-124 4 20
1,1-Dichloroethene 40.0 40.06 ug/Kg 100 55-136 5 21
1,2-Dibromo-3-Chloropropane 40.0 26.02 ug/Kg 65 30-163 5 34
1,2-Dichlorobenzene 40.0 35.56 ug/Kg 89 76-120 3 20
1,2-Dichloroethane 40.0 36.37 ug/Kg 91 64-140 5 20
1,2-Dichloropropane 40.0 38.87 ug/Kg 97 77-119 2 20
1,2,4-Trichlorobenzene 40.0 33.92 ug/Kg 85 22-170 2 29
1,3-Dichlorobenzene 40.0 36.96 ug/Kg 92 77-121 6 20
1,4-Dichlorobenzene 40.0 36.24 ug/Kg 91 79-120 4 20
2-Butanone (MEK)40.0 41.83 ug/Kg 105 39-157 1 33
2-Hexanone 40.0 39.77 ug/Kg 99 42-152 4 30
4-Methyl-2-pentanone (MIBK)40.0 44.44 ug/Kg 111 51-147 8 27
Acetone 40.0 44.46 ug/Kg 111 23-170 4 35
Benzene 40.0 41.03 ug/Kg 103 77-120 3 20
Bromoform 40.0 28.39 ug/Kg 71 37-147 4 23
Bromomethane 40.0 35.37 ug/Kg 88 47-149 9 25
Carbon disulfide 40.0 37.86 ug/Kg 95 40-156 7 25
Carbon tetrachloride 40.0 39.12 ug/Kg 98 73-130 5 21
Chlorobenzene 40.0 37.16 ug/Kg 93 79-122 7 20
Chlorodibromomethane 40.0 31.21 ug/Kg 78 60-134 1 40
Chloroform 40.0 41.02 ug/Kg 103 73-126 2 20
Chloromethane 40.0 38.43 ug/Kg 96 46-151 4 33
Chloroethane 40.0 32.22 ug/Kg 81 37-159 14 25
cis-1,2-Dichloroethene 40.0 41.18 ug/Kg 103 77-118 4 20
cis-1,3-Dichloropropene 40.0 38.23 ug/Kg 96 73-127 1 20
Dichlorobromomethane 40.0 37.77 ug/Kg 94 75-123 1 20
Dichlorodifluoromethane 40.0 30.64 ug/Kg 77 26-149 5 24
Ethylbenzene 40.0 38.35 ug/Kg 96 79-119 8 20
1,2-Dibromoethane 40.0 33.97 ug/Kg 85 59-137 4 20
Cyclohexane 40.0 39.13 ug/Kg 98 63-143 5 25
Isopropylbenzene 40.0 38.27 ug/Kg 96 70-125 8 21
Methyl acetate 80.0 169.5 *+ug/Kg 212 20-170 15 33
Methyl tert-butyl ether 40.0 34.41 ug/Kg 86 58-132 7 24
Methylcyclohexane 40.0 39.72 ug/Kg 99 70-125 5 22
Methylene Chloride 40.0 41.99 ug/Kg 105 67-131 2 32
m-Xylene & p-Xylene 40.0 38.10 ug/Kg 95 77-120 8 20
o-Xylene 40.0 37.79 ug/Kg 94 78-118 7 20
Styrene 40.0 37.30 ug/Kg 93 80-120 5 20
Tetrachloroethene 40.0 38.55 ug/Kg 96 71-121 9 21
Toluene 40.0 38.18 ug/Kg 95 76-120 7 20
trans-1,2-Dichloroethene 40.0 42.00 ug/Kg 105 75-122 5 20
trans-1,3-Dichloropropene 40.0 33.93 ug/Kg 85 68-133 0 20
Trichloroethene 40.0 41.09 ug/Kg 103 69-118 6 20
Trichlorofluoromethane 40.0 52.21 ug/Kg 131 32-149 7 39
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-436900/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 436900
Vinyl chloride 40.0 42.46 ug/Kg 106 64-134 0 23
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Xylenes, Total 80.0 75.89 ug/Kg 95 78-118 8 20
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
96
LCSD LCSD
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)60 -124
101Dibromofluoromethane (Surr)69 -126
103Toluene-d8 (Surr)67 -134
Client Sample ID: Method BlankLab Sample ID: MB 180-437251/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
RL MDL
1,2-Dichlorobenzene ND 1.00 0.364 ug/L 06/07/23 15:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.5041.00 ug/L 06/07/23 15:00 11,3-Dichlorobenzene
ND 0.5441.00 ug/L 06/07/23 15:00 11,4-Dichlorobenzene
ND 0.5961.00 ug/L 06/07/23 15:00 1Benzene
ND 0.5011.00 ug/L 06/07/23 15:00 1Chlorobenzene
ND 0.5071.00 ug/L 06/07/23 15:00 1Ethylbenzene
ND 0.4571.00 ug/L 06/07/23 15:00 1Toluene
ND 0.4061.00 ug/L 06/07/23 15:00 1o-Xylene
ND 0.4821.00 ug/L 06/07/23 15:00 1m-Xylene & p-Xylene
ND 0.8902.00 ug/L 06/07/23 15:00 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)80 26-156 06/07/23 15:00 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
79 06/07/23 15:00 14-Bromofluorobenzene (Surr)36-124
102 06/07/23 15:00 1Dibromofluoromethane (Surr)46-149
94 06/07/23 15:00 1Toluene-d8 (Surr)40-146
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437251/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
1,2-Dichlorobenzene 10.0 10.38 ug/L 104 64-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,3-Dichlorobenzene 10.0 10.11 ug/L 101 63-123
1,4-Dichlorobenzene 10.0 8.557 ug/L 86 67-118
Benzene 10.0 9.777 ug/L 98 68-125
Chlorobenzene 10.0 10.19 ug/L 102 68-121
Ethylbenzene 10.0 9.729 ug/L 97 65-126
Toluene 10.0 9.190 ug/L 92 69-124
o-Xylene 10.0 9.645 ug/L 96 64-127
m-Xylene & p-Xylene 10.0 9.565 ug/L 96 66-131
Xylenes, Total 20.0 19.21 ug/L 96 68-124
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437251/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
84
LCS LCS
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)36 -124
110Dibromofluoromethane (Surr)46 -149
98Toluene-d8 (Surr)40 -146
Client Sample ID: TMW-2Lab Sample ID: 180-157361-7 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
1,2-Dichlorobenzene ND 10.0 10.24 ug/L 102 64-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,3-Dichlorobenzene ND 10.0 10.02 ug/L 100 63-123
1,4-Dichlorobenzene ND 10.0 8.439 ug/L 84 67-118
Benzene ND 10.0 9.414 ug/L 94 68-125
Chlorobenzene ND 10.0 10.24 ug/L 102 68-121
Ethylbenzene ND 10.0 9.743 ug/L 97 65-126
Toluene ND 10.0 8.942 ug/L 89 69-124
o-Xylene ND 10.0 9.551 ug/L 96 64-127
m-Xylene & p-Xylene ND 10.0 9.565 ug/L 96 66-131
Xylenes, Total ND 20.0 19.12 ug/L 96 68-124
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
87
MS MS
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)36 -124
112Dibromofluoromethane (Surr)46 -149
95Toluene-d8 (Surr)40 -146
Client Sample ID: TMW-2Lab Sample ID: 180-157361-7 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
1,2-Dichlorobenzene ND 10.0 10.33 ug/L 103 64-120 1 27
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,3-Dichlorobenzene ND 10.0 10.41 ug/L 104 63-123 4 27
1,4-Dichlorobenzene ND 10.0 8.687 ug/L 87 67-118 3 24
Benzene ND 10.0 9.925 ug/L 99 68-125 5 24
Chlorobenzene ND 10.0 10.60 ug/L 106 68-121 3 21
Ethylbenzene ND 10.0 9.728 ug/L 97 65-126 0 22
Toluene ND 10.0 9.190 ug/L 92 69-124 3 23
o-Xylene ND 10.0 9.811 ug/L 98 64-127 3 26
m-Xylene & p-Xylene ND 10.0 9.660 ug/L 97 66-131 1 26
Xylenes, Total ND 20.0 19.47 ug/L 97 68-124 2 24
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
92
MSD MSD
Qualifier Limits%Recovery
1074-Bromofluorobenzene (Surr)36 -124
117Dibromofluoromethane (Surr)46 -149
94Toluene-d8 (Surr)40 -146
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 180-437362/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437362
RL MDL
1,1,1-Trichloroethane ND 5.00 1.67 ug/Kg 06/08/23 11:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.525.00 ug/Kg 06/08/23 11:10 11,1,2,2-Tetrachloroethane
ND 2.005.00 ug/Kg 06/08/23 11:10 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.9905.00 ug/Kg 06/08/23 11:10 11,1,2-Trichloroethane
ND 1.605.00 ug/Kg 06/08/23 11:10 11,1-Dichloroethane
ND 2.265.00 ug/Kg 06/08/23 11:10 11,1-Dichloroethene
ND 3.235.00 ug/Kg 06/08/23 11:10 11,2-Dibromo-3-Chloropropane
ND 1.685.00 ug/Kg 06/08/23 11:10 11,2-Dichlorobenzene
ND 1.445.00 ug/Kg 06/08/23 11:10 11,2-Dichloroethane
ND 1.335.00 ug/Kg 06/08/23 11:10 11,2-Dichloropropane
ND 2.545.00 ug/Kg 06/08/23 11:10 11,2,4-Trichlorobenzene
ND 3.085.00 ug/Kg 06/08/23 11:10 11,3-Dichlorobenzene
ND 1.505.00 ug/Kg 06/08/23 11:10 11,4-Dichlorobenzene
ND 2.5425.0 ug/Kg 06/08/23 11:10 12-Butanone (MEK)
ND 1.5725.0 ug/Kg 06/08/23 11:10 12-Hexanone
ND 1.8325.0 ug/Kg 06/08/23 11:10 14-Methyl-2-pentanone (MIBK)
ND 3.9025.0 ug/Kg 06/08/23 11:10 1Acetone
ND 1.415.00 ug/Kg 06/08/23 11:10 1Benzene
ND 2.525.00 ug/Kg 06/08/23 11:10 1Bromoform
ND 2.285.00 ug/Kg 06/08/23 11:10 1Bromomethane
ND 4.005.00 ug/Kg 06/08/23 11:10 1Carbon disulfide
ND 2.035.00 ug/Kg 06/08/23 11:10 1Carbon tetrachloride
ND 1.305.00 ug/Kg 06/08/23 11:10 1Chlorobenzene
ND 2.485.00 ug/Kg 06/08/23 11:10 1Chlorodibromomethane
ND 3.355.00 ug/Kg 06/08/23 11:10 1Chloroform
ND 1.985.00 ug/Kg 06/08/23 11:10 1Chloromethane
ND 2.925.00 ug/Kg 06/08/23 11:10 1Chloroethane
ND 1.515.00 ug/Kg 06/08/23 11:10 1cis-1,2-Dichloroethene
ND 2.215.00 ug/Kg 06/08/23 11:10 1cis-1,3-Dichloropropene
ND 2.335.00 ug/Kg 06/08/23 11:10 1Dichlorobromomethane
ND 2.495.00 ug/Kg 06/08/23 11:10 1Dichlorodifluoromethane
ND 1.855.00 ug/Kg 06/08/23 11:10 1Ethylbenzene
ND 1.375.00 ug/Kg 06/08/23 11:10 11,2-Dibromoethane
ND 2.395.00 ug/Kg 06/08/23 11:10 1Cyclohexane
ND 2.605.00 ug/Kg 06/08/23 11:10 1Isopropylbenzene
ND 7.3625.0 ug/Kg 06/08/23 11:10 1Methyl acetate
ND 1.475.00 ug/Kg 06/08/23 11:10 1Methyl tert-butyl ether
ND 2.415.00 ug/Kg 06/08/23 11:10 1Methylcyclohexane
ND 4.515.00 ug/Kg 06/08/23 11:10 1Methylene Chloride
ND 1.505.00 ug/Kg 06/08/23 11:10 1Styrene
ND 2.015.00 ug/Kg 06/08/23 11:10 1Tetrachloroethene
ND 1.445.00 ug/Kg 06/08/23 11:10 1Toluene
ND 1.755.00 ug/Kg 06/08/23 11:10 1trans-1,2-Dichloroethene
ND 2.255.00 ug/Kg 06/08/23 11:10 1trans-1,3-Dichloropropene
ND 1.575.00 ug/Kg 06/08/23 11:10 1Trichloroethene
ND 4.155.00 ug/Kg 06/08/23 11:10 1Trichlorofluoromethane
ND 3.605.00 ug/Kg 06/08/23 11:10 1Vinyl chloride
ND 7.2110.0 ug/Kg 06/08/23 11:10 1Xylenes, Total
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437362/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437362
1,2-Dichloroethane-d4 (Surr)128 73-135 06/08/23 11:10 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
107 06/08/23 11:10 14-Bromofluorobenzene (Surr)60-124
115 06/08/23 11:10 1Dibromofluoromethane (Surr)69-126
99 06/08/23 11:10 1Toluene-d8 (Surr)67-134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437362/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437362
1,1,1-Trichloroethane 40.0 38.46 ug/Kg 96 72-134
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,2,2-Tetrachloroethane 40.0 33.94 ug/Kg 85 36-170
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 35.12 ug/Kg 88 59-135
1,1,2-Trichloroethane 40.0 35.59 ug/Kg 89 66-128
1,1-Dichloroethane 40.0 39.63 ug/Kg 99 73-124
1,1-Dichloroethene 40.0 38.20 ug/Kg 95 55-136
1,2-Dibromo-3-Chloropropane 40.0 30.62 ug/Kg 77 30-163
1,2-Dichlorobenzene 40.0 37.46 ug/Kg 94 76-120
1,2-Dichloroethane 40.0 36.23 ug/Kg 91 64-140
1,2-Dichloropropane 40.0 38.72 ug/Kg 97 77-119
1,2,4-Trichlorobenzene 40.0 37.01 ug/Kg 93 22-170
1,3-Dichlorobenzene 40.0 38.85 ug/Kg 97 77-121
1,4-Dichlorobenzene 40.0 38.02 ug/Kg 95 79-120
2-Butanone (MEK)40.0 42.16 ug/Kg 105 39-157
2-Hexanone 40.0 37.12 ug/Kg 93 42-152
4-Methyl-2-pentanone (MIBK)40.0 42.10 ug/Kg 105 51-147
Acetone 40.0 42.39 ug/Kg 106 23-170
Benzene 40.0 39.97 ug/Kg 100 77-120
Bromoform 40.0 31.22 ug/Kg 78 37-147
Bromomethane 40.0 34.58 ug/Kg 86 47-149
Carbon disulfide 40.0 35.78 ug/Kg 89 40-156
Carbon tetrachloride 40.0 37.49 ug/Kg 94 73-130
Chlorobenzene 40.0 37.82 ug/Kg 95 79-122
Chlorodibromomethane 40.0 34.01 ug/Kg 85 60-134
Chloroform 40.0 40.02 ug/Kg 100 73-126
Chloromethane 40.0 35.99 ug/Kg 90 46-151
Chloroethane 40.0 26.60 ug/Kg 66 37-159
cis-1,2-Dichloroethene 40.0 39.41 ug/Kg 99 77-118
cis-1,3-Dichloropropene 40.0 38.65 ug/Kg 97 73-127
Dichlorobromomethane 40.0 37.91 ug/Kg 95 75-123
Dichlorodifluoromethane 40.0 26.89 ug/Kg 67 26-149
Ethylbenzene 40.0 39.25 ug/Kg 98 79-119
1,2-Dibromoethane 40.0 36.07 ug/Kg 90 59-137
Cyclohexane 40.0 37.93 ug/Kg 95 63-143
Isopropylbenzene 40.0 39.83 ug/Kg 100 70-125
Methyl acetate 80.0 73.94 ug/Kg 92 20-170
Methyl tert-butyl ether 40.0 34.91 ug/Kg 87 58-132
Methylcyclohexane 40.0 38.96 ug/Kg 97 70-125
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437362/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437362
Methylene Chloride 40.0 41.09 ug/Kg 103 67-131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
m-Xylene & p-Xylene 40.0 39.05 ug/Kg 98 77-120
o-Xylene 40.0 39.04 ug/Kg 98 78-118
Styrene 40.0 38.46 ug/Kg 96 80-120
Tetrachloroethene 40.0 38.54 ug/Kg 96 71-121
Toluene 40.0 39.00 ug/Kg 97 76-120
trans-1,2-Dichloroethene 40.0 39.96 ug/Kg 100 75-122
trans-1,3-Dichloropropene 40.0 36.82 ug/Kg 92 68-133
Trichloroethene 40.0 39.51 ug/Kg 99 69-118
Trichlorofluoromethane 40.0 64.92 *+ug/Kg 162 32-149
Vinyl chloride 40.0 41.16 ug/Kg 103 64-134
Xylenes, Total 80.0 78.09 ug/Kg 98 78-118
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
81
LCS LCS
Qualifier Limits%Recovery
974-Bromofluorobenzene (Surr)60 -124
90Dibromofluoromethane (Surr)69 -126
87Toluene-d8 (Surr)67 -134
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-437362/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437362
1,1,1-Trichloroethane 40.0 37.39 ug/Kg 93 72-134 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
1,1,2,2-Tetrachloroethane 40.0 33.06 ug/Kg 83 36-170 3 23
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
40.0 34.49 ug/Kg 86 59-135 2 28
1,1,2-Trichloroethane 40.0 34.76 ug/Kg 87 66-128 2 21
1,1-Dichloroethane 40.0 38.33 ug/Kg 96 73-124 3 20
1,1-Dichloroethene 40.0 36.69 ug/Kg 92 55-136 4 21
1,2-Dibromo-3-Chloropropane 40.0 30.02 ug/Kg 75 30-163 2 34
1,2-Dichlorobenzene 40.0 36.44 ug/Kg 91 76-120 3 20
1,2-Dichloroethane 40.0 35.27 ug/Kg 88 64-140 3 20
1,2-Dichloropropane 40.0 37.21 ug/Kg 93 77-119 4 20
1,2,4-Trichlorobenzene 40.0 36.93 ug/Kg 92 22-170 0 29
1,3-Dichlorobenzene 40.0 37.32 ug/Kg 93 77-121 4 20
1,4-Dichlorobenzene 40.0 36.76 ug/Kg 92 79-120 3 20
2-Butanone (MEK)40.0 35.68 ug/Kg 89 39-157 17 33
2-Hexanone 40.0 37.02 ug/Kg 93 42-152 0 30
4-Methyl-2-pentanone (MIBK)40.0 46.41 ug/Kg 116 51-147 10 27
Acetone 40.0 31.03 ug/Kg 78 23-170 31 35
Benzene 40.0 38.13 ug/Kg 95 77-120 5 20
Bromoform 40.0 29.57 ug/Kg 74 37-147 5 23
Bromomethane 40.0 32.80 ug/Kg 82 47-149 5 25
Carbon disulfide 40.0 34.49 ug/Kg 86 40-156 4 25
Carbon tetrachloride 40.0 36.03 ug/Kg 90 73-130 4 21
Chlorobenzene 40.0 36.46 ug/Kg 91 79-122 4 20
Chlorodibromomethane 40.0 32.51 ug/Kg 81 60-134 4 40
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 180-437362/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437362
Chloroform 40.0 38.66 ug/Kg 97 73-126 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloromethane 40.0 34.67 ug/Kg 87 46-151 4 33
Chloroethane 40.0 25.73 ug/Kg 64 37-159 3 25
cis-1,2-Dichloroethene 40.0 38.96 ug/Kg 97 77-118 1 20
cis-1,3-Dichloropropene 40.0 37.59 ug/Kg 94 73-127 3 20
Dichlorobromomethane 40.0 36.57 ug/Kg 91 75-123 4 20
Dichlorodifluoromethane 40.0 25.30 ug/Kg 63 26-149 6 24
Ethylbenzene 40.0 37.49 ug/Kg 94 79-119 5 20
1,2-Dibromoethane 40.0 35.35 ug/Kg 88 59-137 2 20
Cyclohexane 40.0 36.90 ug/Kg 92 63-143 3 25
Isopropylbenzene 40.0 37.88 ug/Kg 95 70-125 5 21
Methyl acetate 80.0 75.79 ug/Kg 95 20-170 2 33
Methyl tert-butyl ether 40.0 34.54 ug/Kg 86 58-132 1 24
Methylcyclohexane 40.0 37.95 ug/Kg 95 70-125 3 22
Methylene Chloride 40.0 40.02 ug/Kg 100 67-131 3 32
m-Xylene & p-Xylene 40.0 37.49 ug/Kg 94 77-120 4 20
o-Xylene 40.0 37.30 ug/Kg 93 78-118 5 20
Styrene 40.0 36.61 ug/Kg 92 80-120 5 20
Tetrachloroethene 40.0 36.74 ug/Kg 92 71-121 5 21
Toluene 40.0 37.59 ug/Kg 94 76-120 4 20
trans-1,2-Dichloroethene 40.0 38.52 ug/Kg 96 75-122 4 20
trans-1,3-Dichloropropene 40.0 35.49 ug/Kg 89 68-133 4 20
Trichloroethene 40.0 38.33 ug/Kg 96 69-118 3 20
Trichlorofluoromethane 40.0 58.27 ug/Kg 146 32-149 11 39
Vinyl chloride 40.0 40.23 ug/Kg 101 64-134 2 23
Xylenes, Total 80.0 74.79 ug/Kg 93 78-118 4 20
1,2-Dichloroethane-d4 (Surr)73 -135
Surrogate
81
LCSD LCSD
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr)60 -124
89Dibromofluoromethane (Surr)69 -126
85Toluene-d8 (Surr)67 -134
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-437005/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
RL MDL
Acenaphthene ND 0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 10:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.06500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Acenaphthylene
ND 0.04900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Anthracene
ND 0.09501.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,2-Dichlorobenzene
ND 0.07500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[a]anthracene
ND 0.05300.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[a]pyrene
ND 0.09901.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,3-Dichlorobenzene
ND 0.09700.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[b]fluoranthene
ND 0.06900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[g,h,i]perylene
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437005/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
RL MDL
1,4-Dichlorobenzene ND 1.00 0.0610 ug/L 06/05/23 11:58 06/07/23 10:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.08800.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[k]fluoranthene
ND 0.1521.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Bis(2-chloroethoxy)methane
ND 0.04000.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Bis(2-chloroethyl)ether
ND 0.05600.190 ug/L 06/05/23 11:58 06/07/23 10:59 11-Methylnaphthalene
ND 0.05800.190 ug/L 06/05/23 11:58 06/07/23 10:59 12,2'-oxybis[1-chloropropane]
ND 6.2310.0 ug/L 06/05/23 11:58 06/07/23 10:59 1Bis(2-ethylhexyl) phthalate
ND 0.3191.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Bromophenyl phenyl ether
ND 0.4621.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Butyl benzyl phthalate
ND 0.05900.190 ug/L 06/05/23 11:58 06/07/23 10:59 12-Chloronaphthalene
ND 0.2211.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Chlorophenyl phenyl ether
ND 0.08100.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Chrysene
ND 0.07200.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Dibenz(a,h)anthracene
ND 0.5831.00 ug/L 06/05/23 11:58 06/07/23 10:59 13,3'-Dichlorobenzidine
ND 0.5671.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Diethyl phthalate
ND 0.6851.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Di-n-octyl phthalate
ND 0.1961.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,2-Diphenylhydrazine(as
Azobenzene)
ND 0.06200.190 ug/L 06/05/23 11:58 06/07/23 10:59 12-Methylnaphthalene
ND 0.06000.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Fluoranthene
ND 0.3001.00 ug/L 06/05/23 11:58 06/07/23 10:59 12-Methylphenol
ND 0.06900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Fluorene
ND 0.05600.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachlorobenzene
ND 0.06900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachlorobutadiene
ND 0.4971.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachlorocyclopentadiene
ND 0.1331.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachloroethane
ND 0.08500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Indeno[1,2,3-cd]pyrene
ND 0.1881.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Isophorone
ND 0.05900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Naphthalene
ND 0.5002.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Nitrobenzene
ND 0.06701.00 ug/L 06/05/23 11:58 06/07/23 10:59 1N-Nitrosodimethylamine
ND 0.07100.190 ug/L 06/05/23 11:58 06/07/23 10:59 1N-Nitrosodi-n-propylamine
ND 0.3761.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Chloroaniline
ND 0.05500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Phenanthrene
ND 0.05400.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Pyrene
ND 0.3721.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Methylphenol
ND 0.8475.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Pentachlorophenol
ND 0.4871.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Phenol
ND 0.1311.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,2,4-Trichlorobenzene
ND 0.05100.190 ug/L 06/05/23 11:58 06/07/23 10:59 12,4-Dichlorophenol
ND 1.5310.0 ug/L 06/05/23 11:58 06/07/23 10:59 12,4-Dinitrophenol
ND 0.1671.00 ug/L 06/05/23 11:58 06/07/23 10:59 12,4-Dimethylphenol
ND 0.2241.00 ug/L 06/05/23 11:58 06/07/23 10:59 12,4,6-Trichlorophenol
ND 0.1291.00 ug/L 06/05/23 11:58 06/07/23 10:59 12-Chlorophenol
ND 0.1931.00 ug/L 06/05/23 11:58 06/07/23 10:59 12-Nitrophenol
ND 1.475.00 ug/L 06/05/23 11:58 06/07/23 10:59 14,6-Dinitro-2-methylphenol
ND 0.2781.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Chloro-3-methylphenol
ND 0.9405.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Nitrophenol
ND 0.9235.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzoic acid
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437005/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
RL MDL
Benzyl alcohol ND 1.00 0.163 ug/L 06/05/23 11:58 06/07/23 10:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.1901.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Dibenzofuran
2,4,6-Tribromophenol (Surr)56 32-127 06/07/23 10:59 1
MB MB
Surrogate
06/05/23 11:58
Dil FacPreparedAnalyzedQualifierLimits%Recovery
81 06/05/23 11:58 06/07/23 10:59 12-Fluorobiphenyl 47-107
73 06/05/23 11:58 06/07/23 10:59 12-Fluorophenol (Surr)35-109
74 06/05/23 11:58 06/07/23 10:59 1Nitrobenzene-d5 (Surr)47-110
69 06/05/23 11:58 06/07/23 10:59 1Phenol-d5 (Surr)37-110
90 06/05/23 11:58 06/07/23 10:59 1Terphenyl-d14 (Surr)32-115
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437005/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Acenaphthene 10.0 7.822 ug/L 78 47-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Acenaphthylene 10.0 8.169 ug/L 82 33-145
Anthracene 10.0 7.734 ug/L 77 27-133
1,2-Dichlorobenzene 10.0 7.657 ug/L 77 50-100
Benzo[a]anthracene 10.0 8.044 ug/L 80 33-143
Benzo[a]pyrene 10.0 8.443 ug/L 84 17-150
1,3-Dichlorobenzene 10.0 7.589 ug/L 76 51-100
Benzo[b]fluoranthene 10.0 8.442 ug/L 84 24-150
Benzo[g,h,i]perylene 10.0 7.818 ug/L 78 10-150
1,4-Dichlorobenzene 10.0 7.731 ug/L 77 51-100
Benzo[k]fluoranthene 10.0 8.189 ug/L 82 11-150
Bis(2-chloroethoxy)methane 10.0 6.832 ug/L 68 33-150
Bis(2-chloroethyl)ether 10.0 6.714 ug/L 67 12-150
1-Methylnaphthalene 10.0 8.103 ug/L 81 49-100
2,2'-oxybis[1-chloropropane]10.0 7.946 ug/L 79 36-150
Bis(2-ethylhexyl) phthalate 10.0 8.044 J ug/L 80 10-150
4-Bromophenyl phenyl ether 10.0 7.870 ug/L 79 53-127
Butyl benzyl phthalate 10.0 8.489 ug/L 85 10-150
2-Chloronaphthalene 10.0 7.727 ug/L 77 60-120
4-Chlorophenyl phenyl ether 10.0 8.200 ug/L 82 25-150
Chrysene 10.0 8.096 ug/L 81 17-150
Dibenz(a,h)anthracene 10.0 8.290 ug/L 83 10-150
3,3'-Dichlorobenzidine 10.0 7.939 ug/L 79 10-150
Diethyl phthalate 10.0 7.283 ug/L 73 10-120
Di-n-octyl phthalate 10.0 7.927 ug/L 79 10-146
1,2-Diphenylhydrazine(as
Azobenzene)
10.0 7.019 ug/L 70 43-105
2-Methylnaphthalene 10.0 8.097 ug/L 81 51-100
Fluoranthene 10.0 7.690 ug/L 77 26-137
2-Methylphenol 10.0 7.742 ug/L 77 48-100
Fluorene 10.0 7.496 ug/L 75 59-121
Hexachlorobenzene 10.0 6.900 ug/L 69 10-150
Hexachlorobutadiene 10.0 7.247 ug/L 72 24-120
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437005/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Hexachlorocyclopentadiene 10.0 6.817 ug/L 68 37-121
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Hexachloroethane 10.0 7.057 ug/L 71 40-120
Indeno[1,2,3-cd]pyrene 10.0 7.976 ug/L 80 10-150
Isophorone 10.0 7.648 ug/L 76 21-150
Naphthalene 10.0 7.477 ug/L 75 21-133
Nitrobenzene 10.0 7.467 ug/L 75 35-150
N-Nitrosodimethylamine 10.0 8.734 ug/L 87 33-130
N-Nitrosodi-n-propylamine 10.0 8.578 ug/L 86 10-150
4-Chloroaniline 10.0 7.412 ug/L 74 49-100
Phenanthrene 10.0 7.461 ug/L 75 54-120
Pyrene 10.0 9.091 ug/L 91 52-120
4-Methylphenol 10.0 7.899 ug/L 79 47-100
Pentachlorophenol 20.0 13.38 ug/L 67 14-150
Phenol 10.0 6.802 ug/L 68 10-120
1,2,4-Trichlorobenzene 10.0 7.765 ug/L 78 44-142
2,4-Dichlorophenol 10.0 7.630 ug/L 76 39-135
2,4-Dinitrophenol 20.0 13.19 ug/L 66 10-150
2,4-Dimethylphenol 10.0 6.635 ug/L 66 32-120
2,4,6-Trichlorophenol 10.0 8.448 ug/L 84 37-144
2-Chlorophenol 10.0 7.376 ug/L 74 23-134
2-Nitrophenol 10.0 8.119 ug/L 81 29-150
4,6-Dinitro-2-methylphenol 20.0 16.83 ug/L 84 10-150
4-Chloro-3-methylphenol 10.0 8.274 ug/L 83 22-147
4-Nitrophenol 20.0 12.40 ug/L 62 10-132
Benzoic acid 10.0 6.461 ug/L 65 26-127
Benzyl alcohol 10.0 6.997 ug/L 70 30-102
Dibenzofuran 10.0 7.514 ug/L 75 51-100
2,4,6-Tribromophenol (Surr)32 -127
Surrogate
63
LCS LCS
Qualifier Limits%Recovery
782-Fluorobiphenyl 47 -107
712-Fluorophenol (Surr)35 -109
75Nitrobenzene-d5 (Surr)47 -110
69Phenol-d5 (Surr)37 -110
83Terphenyl-d14 (Surr)32 -115
Client Sample ID: Matrix SpikeLab Sample ID: 180-157266-D-1-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Acenaphthene ND F1 10.0 4.111 F1 ug/L 41 47-145
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Acenaphthylene ND 10.0 4.093 ug/L 41 35-145
Anthracene ND 10.0 3.947 ug/L 39 27-133
1,2-Dichlorobenzene ND F1 10.0 1.693 F1 ug/L 17 60-100
Benzo[a]anthracene ND 10.0 4.369 ug/L 44 33-143
Benzo[a]pyrene ND 10.0 4.183 ug/L 42 17-163
1,3-Dichlorobenzene ND F1 10.0 1.594 F1 ug/L 16 60-100
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-157266-D-1-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Benzo[b]fluoranthene ND 10.0 4.204 ug/L 42 24-159
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Benzo[g,h,i]perylene ND 10.0 4.237 ug/L 42 10-170
1,4-Dichlorobenzene ND F1 10.0 1.637 F1 ug/L 16 60-100
Benzo[k]fluoranthene ND 10.0 4.458 ug/L 45 11-162
Bis(2-chloroethoxy)methane ND 10.0 4.101 ug/L 41 33-170
Bis(2-chloroethyl)ether ND 10.0 3.140 ug/L 31 12-158
1-Methylnaphthalene 0.370 F1 10.0 3.781 F1 ug/L 34 58-100
2,2'-oxybis[1-chloropropane]ND 10.0 3.746 ug/L 37 36-166
Bis(2-ethylhexyl) phthalate ND 10.0 6.449 J ug/L 64 10-158
4-Bromophenyl phenyl ether ND F1 10.0 4.395 F1 ug/L 44 53-127
Butyl benzyl phthalate 0.706 J 10.0 5.242 ug/L 45 10-152
2-Chloronaphthalene ND F1 10.0 3.393 F1 ug/L 34 60-120
4-Chlorophenyl phenyl ether ND 10.0 4.414 ug/L 44 25-158
Chrysene ND 10.0 4.537 ug/L 45 17-168
Dibenz(a,h)anthracene ND 10.0 4.485 ug/L 45 10-170
3,3'-Dichlorobenzidine ND F1 10.0 ND F1 ug/L 0 10-170
Diethyl phthalate ND 10.0 4.232 ug/L 42 10-120
Di-n-octyl phthalate ND 10.0 4.196 ug/L 42 10-146
1,2-Diphenylhydrazine(as
Azobenzene)
ND F1 10.0 3.867 F1 ug/L 39 46-103
2-Methylnaphthalene 0.361 F1 10.0 3.778 F1 ug/L 34 58-100
Fluoranthene ND 10.0 4.206 ug/L 42 26-137
2-Methylphenol ND F1 10.0 4.264 F1 ug/L 43 55-101
Fluorene ND F1 10.0 3.985 F1 ug/L 40 59-121
Hexachlorobenzene ND 10.0 3.981 ug/L 40 10-152
Hexachlorobutadiene ND F1 10.0 1.784 F1 ug/L 18 24-120
Hexachlorocyclopentadiene ND F1 10.0 ND F1 ug/L 0 41-106
Hexachloroethane ND F1 10.0 1.440 F1 ug/L 14 40-120
Indeno[1,2,3-cd]pyrene ND 10.0 4.282 ug/L 43 10-170
Isophorone ND 10.0 4.539 ug/L 45 21-170
Naphthalene 2.15 10.0 6.223 ug/L 41 21-133
Nitrobenzene ND 10.0 3.789 ug/L 38 35-170
N-Nitrosodimethylamine ND F1 10.0 4.043 F1 ug/L 40 48-109
N-Nitrosodi-n-propylamine ND 10.0 4.495 ug/L 45 10-170
4-Chloroaniline ND F1 10.0 2.376 F1 ug/L 24 50-100
Phenanthrene 0.104 J F1 10.0 4.313 F1 ug/L 42 54-120
Pyrene ND F1 10.0 4.937 F1 ug/L 49 52-120
4-Methylphenol ND F1 10.0 4.333 F1 ug/L 43 56-102
Pentachlorophenol ND 20.0 7.469 ug/L 37 17-170
Phenol ND 10.0 3.468 ug/L 35 10-120
1,2,4-Trichlorobenzene ND F1 10.0 2.138 F1 ug/L 21 44-142
2,4-Dichlorophenol ND 10.0 4.455 ug/L 45 39-135
2,4-Dinitrophenol ND 20.0 8.690 J ug/L 43 10-170
2,4-Dimethylphenol ND 10.0 3.738 ug/L 37 32-120
2,4,6-Trichlorophenol ND 10.0 4.621 ug/L 46 37-144
2-Chlorophenol ND 10.0 3.721 ug/L 37 23-134
2-Nitrophenol ND 10.0 4.577 ug/L 46 29-170
4,6-Dinitro-2-methylphenol ND 20.0 9.164 ug/L 46 10-170
4-Chloro-3-methylphenol ND 10.0 5.470 ug/L 55 22-147
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-157266-D-1-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
4-Nitrophenol ND 20.0 7.566 ug/L 38 10-132
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Benzoic acid ND 10.0 4.960 J ug/L 50 32-118
Benzyl alcohol ND 10.0 4.020 ug/L 40 24-117
Dibenzofuran ND F1 10.0 3.956 F1 ug/L 40 57-100
2,4,6-Tribromophenol (Surr)32 -127
Surrogate
59
MS MS
Qualifier Limits%Recovery
572-Fluorobiphenyl 47 -107
532-Fluorophenol (Surr)35 -109
69Nitrobenzene-d5 (Surr)47 -110
56Phenol-d5 (Surr)37 -110
65Terphenyl-d14 (Surr)32 -115
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-437429/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
RL MDL
1,1'-Biphenyl ND 330 122 ug/Kg 06/08/23 16:27 06/09/23 09:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 24.767.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,2'-oxybis[1-chloropropane]
ND 116330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4,5-Trichlorophenol
ND 111330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4,6-Trichlorophenol
ND 25.767.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4-Dichlorophenol
ND 112330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4-Dimethylphenol
ND 20703300 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4-Dinitrophenol
ND 199330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,4-Dinitrotoluene
ND 130330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12,6-Dinitrotoluene
ND 15.367.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Chloronaphthalene
ND 123330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Chlorophenol
ND 16.067.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Methylnaphthalene
ND 95.6330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Methylphenol
ND 1521700 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Nitroaniline
ND 123330 ug/Kg 06/08/23 16:27 06/09/23 09:19 12-Nitrophenol
ND 311330 ug/Kg 06/08/23 16:27 06/09/23 09:19 13,3'-Dichlorobenzidine
ND 84.81700 ug/Kg 06/08/23 16:27 06/09/23 09:19 13-Nitroaniline
ND 5751700 ug/Kg 06/08/23 16:27 06/09/23 09:19 14,6-Dinitro-2-methylphenol
ND 142330 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Bromophenyl phenyl ether
ND 117330 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Chloro-3-methylphenol
ND 87.5330 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Chloroaniline
ND 111330 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Chlorophenyl phenyl ether
ND 97.9330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Methylphenol, 3 & 4
ND 1241700 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Nitroaniline
ND 2341700 ug/Kg 06/08/23 16:27 06/09/23 09:19 14-Nitrophenol
ND 19.267.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Acenaphthene
ND 14.667.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Acenaphthylene
ND 119670 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Acetophenone
ND 17.367.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Anthracene
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437429/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
RL MDL
Atrazine ND 670 146 ug/Kg 06/08/23 16:27 06/09/23 09:19 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 41.4670 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzaldehyde
ND 30.167.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[a]anthracene
ND 28.967.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[a]pyrene
ND 16.467.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[b]fluoranthene
ND 14.467.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[g,h,i]perylene
ND 20.067.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Benzo[k]fluoranthene
ND 122330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Bis(2-chloroethoxy)methane
ND 12.167.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Bis(2-chloroethyl)ether
ND 3553300 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Bis(2-ethylhexyl) phthalate
ND 229330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Butyl benzyl phthalate
ND 2171700 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Caprolactam
ND 15.667.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Carbazole
ND 37.067.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Chrysene
ND 42.767.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Dibenz(a,h)anthracene
ND 123330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Dibenzofuran
ND 117330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Diethyl phthalate
ND 132330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Dimethyl phthalate
ND 146330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Di-n-butyl phthalate
ND 194330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Di-n-octyl phthalate
ND 17.667.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Fluoranthene
ND 13.167.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Fluorene
ND 23.967.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Hexachlorobenzene
ND 19.567.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Hexachlorobutadiene
ND 34.1330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Hexachlorocyclopentadiene
ND 118330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Hexachloroethane
ND 33.267.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Indeno[1,2,3-cd]pyrene
ND 125330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Isophorone
ND 13.067.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Naphthalene
ND 122670 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Nitrobenzene
ND 22.667.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1N-Nitrosodi-n-propylamine
ND 111330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1N-Nitrosodiphenylamine
ND 5361700 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Pentachlorophenol
ND 17.967.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Phenanthrene
ND 101330 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Phenol
ND 15.867.0 ug/Kg 06/08/23 16:27 06/09/23 09:19 1Pyrene
2,4,6-Tribromophenol (Surr)72 34-108 06/09/23 09:19 1
MB MB
Surrogate
06/08/23 16:27
Dil FacPreparedAnalyzedQualifierLimits%Recovery
76 06/08/23 16:27 06/09/23 09:19 12-Fluorobiphenyl 44-105
78 06/08/23 16:27 06/09/23 09:19 12-Fluorophenol (Surr)48-105
74 06/08/23 16:27 06/09/23 09:19 1Nitrobenzene-d5 (Surr)46-105
72 06/08/23 16:27 06/09/23 09:19 1Phenol-d5 (Surr)46-105
84 06/08/23 16:27 06/09/23 09:19 1Terphenyl-d14 (Surr)39-105
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437429/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
1,1'-Biphenyl 6670 4835 ug/Kg 73 50-100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2,2'-oxybis[1-chloropropane]6670 4585 ug/Kg 69 30-113
2,4,5-Trichlorophenol 6670 4748 ug/Kg 71 50-104
2,4,6-Trichlorophenol 6670 5087 ug/Kg 76 50-105
2,4-Dichlorophenol 6670 4552 ug/Kg 68 53-101
2,4-Dimethylphenol 6670 4468 ug/Kg 67 51-101
2,4-Dinitrophenol 13300 6128 ug/Kg 46 33-101
2,4-Dinitrotoluene 6670 4942 ug/Kg 74 54-104
2,6-Dinitrotoluene 6670 4926 ug/Kg 74 51-106
2-Chloronaphthalene 6670 4844 ug/Kg 73 51-100
2-Chlorophenol 6670 4798 ug/Kg 72 51-100
2-Methylnaphthalene 6670 4750 ug/Kg 71 53-100
2-Methylphenol 6670 4486 ug/Kg 67 50-101
2-Nitroaniline 6670 4875 ug/Kg 73 42-123
2-Nitrophenol 6670 5316 ug/Kg 80 55-107
3,3'-Dichlorobenzidine 6670 4968 ug/Kg 75 43-100
3-Nitroaniline 6670 4616 ug/Kg 69 50-103
4,6-Dinitro-2-methylphenol 13300 7989 ug/Kg 60 51-100
4-Bromophenyl phenyl ether 6670 5541 ug/Kg 83 52-101
4-Chloro-3-methylphenol 6670 4425 ug/Kg 66 49-106
4-Chloroaniline 6670 4529 ug/Kg 68 47-100
4-Chlorophenyl phenyl ether 6670 4838 ug/Kg 73 52-100
Methylphenol, 3 & 4 6670 4455 ug/Kg 67 50-103
4-Nitroaniline 6670 4270 ug/Kg 64 52-103
4-Nitrophenol 13300 9142 ug/Kg 69 30-134
Acenaphthene 6670 4556 ug/Kg 68 50-100
Acenaphthylene 6670 4722 ug/Kg 71 52-100
Acetophenone 6670 4452 ug/Kg 67 48-100
Anthracene 6670 4827 ug/Kg 72 53-100
Atrazine 6670 4616 ug/Kg 69 49-103
Benzaldehyde 6670 5118 ug/Kg 77 23-105
Benzo[a]anthracene 6670 4778 ug/Kg 72 51-100
Benzo[a]pyrene 6670 4618 ug/Kg 69 51-100
Benzo[b]fluoranthene 6670 4741 ug/Kg 71 48-100
Benzo[g,h,i]perylene 6670 4508 ug/Kg 68 48-105
Benzo[k]fluoranthene 6670 4426 ug/Kg 66 19-100
Bis(2-chloroethoxy)methane 6670 4595 ug/Kg 69 49-100
Bis(2-chloroethyl)ether 6670 4700 ug/Kg 70 48-100
Bis(2-ethylhexyl) phthalate 6670 5592 ug/Kg 84 53-107
Butyl benzyl phthalate 6670 5585 ug/Kg 84 52-107
Carbazole 6670 4234 ug/Kg 64 53-100
Chrysene 6670 4136 ug/Kg 62 50-100
Dibenz(a,h)anthracene 6670 4860 ug/Kg 73 50-107
Dibenzofuran 6670 4792 ug/Kg 72 52-100
Diethyl phthalate 6670 4780 ug/Kg 72 48-104
Dimethyl phthalate 6670 4837 ug/Kg 73 53-100
Di-n-butyl phthalate 6670 4999 ug/Kg 75 57-102
Di-n-octyl phthalate 6670 5783 ug/Kg 87 41-106
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437429/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
Fluoranthene 6670 4581 ug/Kg 69 55-100
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Fluorene 6670 4714 ug/Kg 71 52-100
Hexachlorobenzene 6670 5490 ug/Kg 82 49-100
Hexachlorobutadiene 6670 5224 ug/Kg 78 38-107
Hexachlorocyclopentadiene 6670 5231 ug/Kg 78 33-117
Hexachloroethane 6670 4777 ug/Kg 72 47-100
Indeno[1,2,3-cd]pyrene 6670 4739 ug/Kg 71 51-103
Isophorone 6670 4562 ug/Kg 68 48-105
Naphthalene 6670 4688 ug/Kg 70 51-100
Nitrobenzene 6670 4698 ug/Kg 70 44-108
N-Nitrosodi-n-propylamine 6670 4673 ug/Kg 70 45-107
N-Nitrosodiphenylamine 6670 5166 ug/Kg 77 52-100
Pentachlorophenol 13300 10230 ug/Kg 77 42-110
Phenanthrene 6670 4667 ug/Kg 70 53-100
Phenol 6670 4344 ug/Kg 65 49-100
Pyrene 6670 5224 ug/Kg 78 52-100
2,4,6-Tribromophenol (Surr)34 -108
Surrogate
82
LCS LCS
Qualifier Limits%Recovery
692-Fluorobiphenyl 44 -105
692-Fluorophenol (Surr)48 -105
66Nitrobenzene-d5 (Surr)46 -105
67Phenol-d5 (Surr)46 -105
78Terphenyl-d14 (Surr)39 -105
Client Sample ID: Matrix SpikeLab Sample ID: 140-31976-O-1-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
1,1'-Biphenyl ND 6620 5249 ug/Kg 79 50-100
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
2,2'-oxybis[1-chloropropane]ND 6620 4517 ug/Kg 68 30-113
2,4,5-Trichlorophenol ND F1 6620 2954 F1 ug/Kg 45 50-104
2,4,6-Trichlorophenol ND F1 F2 6620 399.5 F1 ug/Kg 6 50-105
2,4-Dichlorophenol ND F1 6620 201.7 F1 ug/Kg 3 53-101
2,4-Dimethylphenol ND F1 6620 208.6 J F1 ug/Kg 3 51-101
2,4-Dinitrophenol ND F1 13200 ND F1 ug/Kg 0 33-101
2,4-Dinitrotoluene ND 6620 3688 ug/Kg 56 54-104
2,6-Dinitrotoluene ND 6620 4527 ug/Kg 68 51-106
2-Chloronaphthalene ND 6620 3707 ug/Kg 56 51-100
2-Chlorophenol ND F1 6620 3270 F1 ug/Kg 49 51-100
2-Methylnaphthalene ND F1 6620 3371 F1 ug/Kg 51 53-100
2-Methylphenol ND F1 6620 1137 F1 ug/Kg 17 50-101
2-Nitroaniline ND 6620 3475 ug/Kg 52 42-123
2-Nitrophenol ND F1 6620 3508 F1 ug/Kg 53 55-107
3,3'-Dichlorobenzidine ND F1 6620 2257 F1 ug/Kg 34 43-100
3-Nitroaniline ND F1 6620 2916 F1 ug/Kg 44 50-103
4,6-Dinitro-2-methylphenol ND F1 F2 13200 2490 F1 ug/Kg 19 51-100
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 140-31976-O-1-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
4-Bromophenyl phenyl ether ND 6620 4914 ug/Kg 74 52-101
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
4-Chloro-3-methylphenol ND F1 6620 2444 F1 ug/Kg 37 49-106
4-Chloroaniline ND F1 6620 1649 F1 ug/Kg 25 47-100
4-Chlorophenyl phenyl ether ND 6620 4411 ug/Kg 67 52-100
Methylphenol, 3 & 4 ND F1 F2 6620 2331 F1 ug/Kg 35 50-103
4-Nitroaniline ND F1 6620 2608 F1 ug/Kg 39 52-103
4-Nitrophenol ND 13200 4997 ug/Kg 38 30-134
Acenaphthene ND 6620 3357 ug/Kg 51 50-100
Acenaphthylene ND 6620 3542 ug/Kg 53 52-100
Acetophenone ND 6620 3897 ug/Kg 59 48-100
Anthracene ND F1 6620 2558 F1 ug/Kg 39 53-100
Atrazine ND F1 6620 626.4 J F1 ug/Kg 9 49-103
Benzaldehyde ND 6620 3087 ug/Kg 47 23-105
Benzo[a]anthracene ND F1 6620 2670 F1 ug/Kg 40 51-100
Benzo[a]pyrene ND F1 6620 2557 F1 ug/Kg 39 51-100
Benzo[b]fluoranthene ND F1 6620 2342 F1 ug/Kg 35 48-100
Benzo[g,h,i]perylene ND 6620 3491 ug/Kg 53 48-105
Benzo[k]fluoranthene ND 6620 1999 ug/Kg 30 19-100
Bis(2-chloroethoxy)methane ND 6620 4377 ug/Kg 66 49-100
Bis(2-chloroethyl)ether 10000 F1 6620 11860 F1 ug/Kg 27 48-100
Bis(2-ethylhexyl) phthalate ND 6620 6571 ug/Kg 99 53-107
Butyl benzyl phthalate ND 6620 5532 ug/Kg 84 52-107
Carbazole ND F1 6620 2165 F1 ug/Kg 33 53-100
Chrysene ND F1 6620 2455 F1 ug/Kg 37 50-100
Dibenz(a,h)anthracene ND 6620 3562 ug/Kg 54 50-107
Dibenzofuran ND F1 6620 3013 F1 ug/Kg 45 52-100
Diethyl phthalate ND 6620 4820 ug/Kg 73 48-104
Dimethyl phthalate ND 6620 4833 ug/Kg 73 53-100
Di-n-butyl phthalate ND 6620 4768 ug/Kg 72 57-102
Di-n-octyl phthalate ND 6620 5108 ug/Kg 77 41-106
Fluoranthene ND F1 6620 2115 F1 ug/Kg 32 55-100
Fluorene ND F1 6620 3000 F1 ug/Kg 45 52-100
Hexachlorobenzene ND 6620 3975 ug/Kg 60 49-100
Hexachlorobutadiene ND 6620 4701 ug/Kg 71 38-107
Hexachlorocyclopentadiene ND F1 6620 1557 F1 ug/Kg 24 33-117
Hexachloroethane ND 6620 4491 ug/Kg 68 47-100
Indeno[1,2,3-cd]pyrene ND 6620 3572 ug/Kg 54 51-103
Isophorone ND 6620 3774 ug/Kg 57 48-105
Naphthalene ND 6620 4066 ug/Kg 61 51-100
Nitrobenzene ND 6620 4721 ug/Kg 71 44-108
N-Nitrosodi-n-propylamine ND 6620 4790 ug/Kg 72 45-107
N-Nitrosodiphenylamine ND 6620 4014 ug/Kg 61 52-100
Pentachlorophenol ND F1 13200 4713 F1 ug/Kg 36 42-110
Phenanthrene ND F1 6620 2800 F1 ug/Kg 42 53-100
Phenol ND F1 6620 2227 F1 ug/Kg 34 49-100
Pyrene ND F1 6620 2836 F1 ug/Kg 43 52-100
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 140-31976-O-1-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
2,4,6-Tribromophenol (Surr)34 -108
Surrogate
49
MS MS
Qualifier Limits%Recovery
602-Fluorobiphenyl 44 -105
552-Fluorophenol (Surr)48 -105
55Nitrobenzene-d5 (Surr)46 -105
50Phenol-d5 (Surr)46 -105
43Terphenyl-d14 (Surr)39 -105
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 140-31976-O-1-B MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
1,1'-Biphenyl ND 6580 5362 ug/Kg 82 50-100 2 19
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
2,2'-oxybis[1-chloropropane]ND 6580 4679 ug/Kg 71 30-113 4 17
2,4,5-Trichlorophenol ND F1 6580 2992 F1 ug/Kg 45 50-104 1 21
2,4,6-Trichlorophenol ND F1 F2 6580 304.2 J F1 F2 ug/Kg 5 50-105 27 21
2,4-Dichlorophenol ND F1 6580 230.0 F1 ug/Kg 3 53-101 13 22
2,4-Dimethylphenol ND F1 6580 182.1 J F1 ug/Kg 3 51-101 14 32
2,4-Dinitrophenol ND F1 13200 ND F1 ug/Kg 0 33-101 NC 20
2,4-Dinitrotoluene ND 6580 3826 ug/Kg 58 54-104 4 20
2,6-Dinitrotoluene ND 6580 4583 ug/Kg 70 51-106 1 20
2-Chloronaphthalene ND 6580 3835 ug/Kg 58 51-100 3 20
2-Chlorophenol ND F1 6580 3441 ug/Kg 52 51-100 5 17
2-Methylnaphthalene ND F1 6580 3470 ug/Kg 53 53-100 3 21
2-Methylphenol ND F1 6580 1264 F1 ug/Kg 19 50-101 11 17
2-Nitroaniline ND 6580 3698 ug/Kg 56 42-123 6 19
2-Nitrophenol ND F1 6580 3647 ug/Kg 55 55-107 4 19
3,3'-Dichlorobenzidine ND F1 6580 2554 F1 ug/Kg 39 43-100 12 19
3-Nitroaniline ND F1 6580 2981 F1 ug/Kg 45 50-103 2 20
4,6-Dinitro-2-methylphenol ND F1 F2 13200 3328 F1 F2 ug/Kg 25 51-100 29 22
4-Bromophenyl phenyl ether ND 6580 5043 ug/Kg 77 52-101 3 20
4-Chloro-3-methylphenol ND F1 6580 2749 F1 ug/Kg 42 49-106 12 20
4-Chloroaniline ND F1 6580 1710 F1 ug/Kg 26 47-100 4 20
4-Chlorophenyl phenyl ether ND 6580 4507 ug/Kg 69 52-100 2 19
Methylphenol, 3 & 4 ND F1 F2 6580 1847 F1 F2 ug/Kg 28 50-103 23 19
4-Nitroaniline ND F1 6580 2678 F1 ug/Kg 41 52-103 3 18
4-Nitrophenol ND 13200 5433 ug/Kg 41 30-134 8 18
Acenaphthene ND 6580 3429 ug/Kg 52 50-100 2 20
Acenaphthylene ND 6580 3668 ug/Kg 56 52-100 3 20
Acetophenone ND 6580 4032 ug/Kg 61 48-100 3 17
Anthracene ND F1 6580 2597 F1 ug/Kg 39 53-100 2 20
Atrazine ND F1 6580 727.3 F1 ug/Kg 11 49-103 15 19
Benzaldehyde ND 6580 3145 ug/Kg 48 23-105 2 31
Benzo[a]anthracene ND F1 6580 2909 F1 ug/Kg 44 51-100 9 21
Benzo[a]pyrene ND F1 6580 2725 F1 ug/Kg 41 51-100 6 20
Benzo[b]fluoranthene ND F1 6580 2512 F1 ug/Kg 38 48-100 7 20
Benzo[g,h,i]perylene ND 6580 3358 ug/Kg 51 48-105 4 19
Benzo[k]fluoranthene ND 6580 2196 ug/Kg 33 19-100 9 20
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 140-31976-O-1-B MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437462 Prep Batch: 437429
Bis(2-chloroethoxy)methane ND 6580 4527 ug/Kg 69 49-100 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Bis(2-chloroethyl)ether 10000 F1 6580 11820 F1 ug/Kg 27 48-100 0 18
Bis(2-ethylhexyl) phthalate ND 6580 6423 ug/Kg 98 53-107 2 20
Butyl benzyl phthalate ND 6580 5847 ug/Kg 89 52-107 6 19
Carbazole ND F1 6580 2296 F1 ug/Kg 35 53-100 6 20
Chrysene ND F1 6580 2650 F1 ug/Kg 40 50-100 8 20
Dibenz(a,h)anthracene ND 6580 3710 ug/Kg 56 50-107 4 21
Dibenzofuran ND F1 6580 3141 F1 ug/Kg 48 52-100 4 19
Diethyl phthalate ND 6580 4973 ug/Kg 76 48-104 3 20
Dimethyl phthalate ND 6580 4954 ug/Kg 75 53-100 2 21
Di-n-butyl phthalate ND 6580 4714 ug/Kg 72 57-102 1 20
Di-n-octyl phthalate ND 6580 5225 ug/Kg 79 41-106 2 18
Fluoranthene ND F1 6580 2347 F1 ug/Kg 36 55-100 10 20
Fluorene ND F1 6580 3109 F1 ug/Kg 47 52-100 4 19
Hexachlorobenzene ND 6580 4122 ug/Kg 63 49-100 4 20
Hexachlorobutadiene ND 6580 4913 ug/Kg 75 38-107 4 22
Hexachlorocyclopentadiene ND F1 6580 1654 F1 ug/Kg 25 33-117 6 19
Hexachloroethane ND 6580 4673 ug/Kg 71 47-100 4 17
Indeno[1,2,3-cd]pyrene ND 6580 3537 ug/Kg 54 51-103 1 19
Isophorone ND 6580 3962 ug/Kg 60 48-105 5 20
Naphthalene ND 6580 4261 ug/Kg 65 51-100 5 20
Nitrobenzene ND 6580 4897 ug/Kg 74 44-108 4 21
N-Nitrosodi-n-propylamine ND 6580 4920 ug/Kg 75 45-107 3 18
N-Nitrosodiphenylamine ND 6580 4065 ug/Kg 62 52-100 1 20
Pentachlorophenol ND F1 13200 4770 F1 ug/Kg 36 42-110 1 20
Phenanthrene ND F1 6580 2892 F1 ug/Kg 44 53-100 3 20
Phenol ND F1 6580 2465 F1 ug/Kg 37 49-100 10 16
Pyrene ND F1 6580 3030 F1 ug/Kg 46 52-100 7 20
2,4,6-Tribromophenol (Surr)34 -108
Surrogate
53
MSD MSD
Qualifier Limits%Recovery
632-Fluorobiphenyl 44 -105
582-Fluorophenol (Surr)48 -105
58Nitrobenzene-d5 (Surr)46 -105
53Phenol-d5 (Surr)46 -105
46Terphenyl-d14 (Surr)39 -105
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-384264/20
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384264
RL MDL
C5-C8 Aliphatics (unadjusted)ND 100 25.0 ug/L 06/08/23 21:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10.0100 ug/L 06/08/23 21:39 1C9-C10 Aromatics
ND 25.0100 ug/L 06/08/23 21:39 1C9-C12 Aliphatics (unadjusted)
ND 25.0100 ug/L 06/08/23 21:39 1C9-C12 Aliphatics (adjusted)
ND 25.0100 ug/L 06/08/23 21:39 1C5-C8 Aliphatics (adjusted)
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
a,a,a-Trifluorotoluene (fid)108 70-130 06/08/23 21:39 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 06/08/23 21:39 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-384264/21
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384264
C5-C8 Aliphatics (unadjusted)151 150.8 ug/L 100 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 50.2 47.04 J ug/L 94 70-130
C9-C12 Aliphatics (unadjusted)151 133.8 ug/L 89 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
108
LCS LCS
Qualifier Limits%Recovery
98a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-384264/22
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384264
C5-C8 Aliphatics (unadjusted)151 147.4 ug/L 98 70-130 2 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 50.2 46.31 J ug/L 92 70-130 2 25
C9-C12 Aliphatics (unadjusted)151 133.1 ug/L 88 70-130 1 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
108
LCSD LCSD
Qualifier Limits%Recovery
97a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 410-386087/23-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 386298 Prep Batch: 386087
RL MDL
C5-C8 Aliphatics (unadjusted)ND 5.00 1.25 mg/Kg 06/14/23 07:06 06/14/23 09:42 50
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.255.00 mg/Kg 06/14/23 07:06 06/14/23 09:42 50C9-C10 Aromatics
ND 1.255.00 mg/Kg 06/14/23 07:06 06/14/23 09:42 50C9-C12 Aliphatics (unadjusted)
ND 1.255.00 mg/Kg 06/14/23 07:06 06/14/23 09:42 50C9-C12 Aliphatics (adjusted)
ND 1.255.00 mg/Kg 06/14/23 07:06 06/14/23 09:42 50C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)99 70-130 06/14/23 09:42 50
MB MB
Surrogate
06/14/23 07:06
Dil FacPreparedAnalyzedQualifierLimits%Recovery
86 06/14/23 07:06 06/14/23 09:42 50a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-386087/24-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 386298 Prep Batch: 386087
C5-C8 Aliphatics (unadjusted)7.53 6.104 mg/Kg 81 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 2.51 2.198 J mg/Kg 88 70-130
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-386087/24-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 386298 Prep Batch: 386087
C9-C12 Aliphatics (unadjusted)7.53 6.377 mg/Kg 85 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
87a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-386087/25-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 386298 Prep Batch: 386087
C5-C8 Aliphatics (unadjusted)7.53 6.220 mg/Kg 83 70-130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 2.51 2.208 J mg/Kg 88 70-130 0 30
C9-C12 Aliphatics (unadjusted)7.53 6.505 mg/Kg 86 70-130 2 30
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
89a,a,a-Trifluorotoluene (pid)70 -130
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-383574/1-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388785 Prep Batch: 383574
RL MDL
C19-C36 Aliphatics ND 12.0 12.0 mg/Kg 06/06/23 16:31 06/20/23 19:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 6.006.00 mg/Kg 06/06/23 16:31 06/20/23 19:38 1C9-C18 Aliphatics
1-Chlorooctadecane (Surr)48 40-140 06/20/23 19:38 1
MB MB
Surrogate
06/06/23 16:31
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-383574/1-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388783 Prep Batch: 383574
RL MDL
C11-C22 Aromatics (unadjusted)ND 12.0 12.0 mg/Kg 06/06/23 16:31 06/20/23 19:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 12.012.0 mg/Kg 06/06/23 16:31 06/20/23 19:38 1C11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)70 40-140 06/20/23 19:38 1
MB MB
Surrogate
06/06/23 16:31
Dil FacPreparedAnalyzedQualifierLimits%Recovery
61 06/06/23 16:31 06/20/23 19:38 1o- terphenyl (Surr)40-140
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-383574/2-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388785 Prep Batch: 383574
C19-C36 Aliphatics 32.1 24.50 mg/Kg 76 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 24.1 19.14 mg/Kg 79 40-140
1-Chlorooctadecane (Surr)40 -140
Surrogate
47
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-383574/2-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388783 Prep Batch: 383574
C11-C22 Aromatics (unadjusted)68.1 42.96 mg/Kg 63 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Fluorobiphenyl (Surr)40 -140
Surrogate
69
LCS LCS
Qualifier Limits%Recovery
59o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-383574/3-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388785 Prep Batch: 383574
C19-C36 Aliphatics 32.1 25.41 mg/Kg 79 40-140 4 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 24.1 19.78 mg/Kg 82 40-140 3 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
61
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-383574/3-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 388783 Prep Batch: 383574
C11-C22 Aromatics (unadjusted)68.1 48.00 mg/Kg 70 40-140 11 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)40 -140
Surrogate
75
LCSD LCSD
Qualifier Limits%Recovery
67o- terphenyl (Surr)40 -140
Client Sample ID: Method BlankLab Sample ID: MB 410-385076/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
RL MDL
C19-C36 Aliphatics ND 50.0 50.0 ug/L 06/09/23 19:11 06/27/23 02:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 30.030.0 ug/L 06/09/23 19:11 06/27/23 02:30 1C9-C18 Aliphatics
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-385076/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
1-Chlorooctadecane (Surr)59 40-140 06/27/23 02:30 1
MB MB
Surrogate
06/09/23 19:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-385076/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390845 Prep Batch: 385076
RL MDL
C11-C22 Aromatics (unadjusted)ND 40.0 40.0 ug/L 06/09/23 19:11 06/27/23 02:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 40.040.0 ug/L 06/09/23 19:11 06/27/23 02:30 1C11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)79 40-140 06/27/23 02:30 1
MB MB
Surrogate
06/09/23 19:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
64 06/09/23 19:11 06/27/23 02:30 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-385076/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
C19-C36 Aliphatics 321 191.4 ug/L 60 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 157.7 ug/L 65 40-140
1-Chlorooctadecane (Surr)40 -140
Surrogate
54
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-385076/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390845 Prep Batch: 385076
C11-C22 Aromatics (unadjusted)681 480.1 ug/L 70 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Fluorobiphenyl (Surr)40 -140
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
77o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-385076/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
C19-C36 Aliphatics 321 195.7 ug/L 61 40-140 2 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 241 158.1 ug/L 66 40-140 0 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
60
LCSD LCSD
Qualifier Limits%Recovery
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157361-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-385076/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390845 Prep Batch: 385076
C11-C22 Aromatics (unadjusted)681 448.9 ug/L 66 40-140 7 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)40 -140
Surrogate
83
LCSD LCSD
Qualifier Limits%Recovery
75o- terphenyl (Surr)40 -140
Method: 2540G - SM 2540G
Client Sample ID: EB-12 (2-4)Lab Sample ID: 180-157361-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 437141
Percent Moisture 33.2 33.1 %0.4 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 66.8 66.9 %0.2 10
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-157361-1
SDG Number: 640 Rock Lane
Login Number: 157361
Question Answer Comment
Creator: Abernathy, Eric L
List Source: Eurofins Pittsburgh
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-157361-1
SDG Number: 640 Rock Lane
Login Number: 157361
Question Answer Comment
Creator: McCaskey, Jonathan
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 06/03/23 11:20 AMList Number: 2
N/AThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
TrueVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-157361-1
SDG Number: 640 Rock Lane
Login Number: 157361
Question Answer Comment
Creator: McBeth, Jessica
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 06/09/23 10:32 AMList Number: 3
N/AThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
FalseCooler Temperature is acceptable (</=6C, not frozen).samples frozen
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
N/AVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
Eurofins Pittsburgh
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ANALYTICAL REPORT
PREPARED FOR
Attn: Mr. Bruce Stainbrook
Altec Industries, Inc
Bruce Stainbrook
810 Franklin Court, Ste A
Marietta, Georgia 30067
Generated 6/29/2023 4:45:39 PM
JOB DESCRIPTION
China Grove NC
SDG NUMBER 640 Rock Lane
JOB NUMBER
180-157472-1
See page two for job notes and contact information.
Pittsburgh PA 15238
RIDC Park
301 Alpha Drive
Eurofins Pittsburgh
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Eurofins Pittsburgh
Eurofins Pittsburgh is a laboratory within Eurofins Environment Testing Northeast LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
PA Lab ID: 02-00416
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Pittsburgh Project Manager.
Authorization
Generated
6/29/2023 4:45:39 PM
Authorized for release by
Shali Brown, Project Manager II
[e-mail]
[phone]
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Case Narrative
Client: Altec Industries, Inc Job ID: 180-157472-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Job ID: 180-157472-1
Laboratory: Eurofins Pittsburgh
Narrative
Job Narrative
180-157472-1
Receipt
The samples were received on 6/3/2023 9:20 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 2.7°C
GC/MS VOA
Method 8260D_LL: The continuing calibration verification (CCV) analyzed in batch 180-437251 was outside the method criteria for the
following analyte(s): 1,2-Dichloroethane-d4. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples
and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected
analyte(s) is considered estimated.
Method 8260D_LL: The continuing calibration verification (CCV) analyzed in 180-437390 was outside the method criteria for the following
analyte(s): Dibromofluoromethane. As indicated in the reference method, sample analysis may proceed; however, any detection for the
affected analyte(s) is considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
Method 625.1_LL_PREC: An incorrect volume of surrogate spiking solution was inadvertently added the following samples: TMW-5
(180-157472-1), TMW-7 (180-157472-2), TMW-9 (180-157472-3) and TMW-10 (180-157472-4). Percent recoveries are based on the
amount spiked.
Method 625.1_LL_PREC: The matrix spike (MS) recoveries for preparation batch 180-437005 and analytical batch 180-437193 were
outside control limits. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery was
within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Hydrocarbons
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method MAEPH2.1: The breakthrough for naphthalene is 5% and the breakthrough for 2-methylnaphthalene is 2% in the LCS. The
breakthrough for naphthalene is 4% and the breakthrough for 2-methylnaphthalene is 2% in the LCSD. The method requirement for
breakthrough is 5% or less. TMW-5 (180-157472-1), TMW-7 (180-157472-2), TMW-9 (180-157472-3) and TMW-10 (180-157472-4)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Definitions/Glossary
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Qualifiers
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Accreditation/Certification Summary
Client: Altec Industries, Inc Job ID: 180-157472-1
Project/Site: China Grove NC SDG: 640 Rock Lane
Laboratory: Eurofins Pittsburgh
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 434 12-31-23
Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 521 12-31-23
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-1Client Sample ID: TMW-5
Matrix: WaterDate Collected: 05/31/23 16:57
Date Received: 06/03/23 09:20
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 06/07/23 18:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 06/07/23 18:38 1ND1,3-Dichlorobenzene
1.00 0.544 ug/L 06/07/23 18:38 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 06/07/23 18:38 1NDBenzene
1.00 0.501 ug/L 06/07/23 18:38 1NDChlorobenzene
1.00 0.507 ug/L 06/07/23 18:38 1NDEthylbenzene
1.00 0.457 ug/L 06/07/23 18:38 1NDToluene
1.00 0.406 ug/L 06/07/23 18:38 1NDo-Xylene
1.00 0.482 ug/L 06/07/23 18:38 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 06/07/23 18:38 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)83 26-156 06/07/23 18:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)75 06/07/23 18:38 136-124
Dibromofluoromethane (Surr)100 06/07/23 18:38 146-149
Toluene-d8 (Surr)90 06/07/23 18:38 140-146
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 15:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 15:26 1NDAcenaphthylene
0.190 0.0490 ug/L 06/05/23 11:58 06/07/23 15:26 1NDAnthracene
1.00 0.0950 ug/L 06/05/23 11:58 06/07/23 15:26 1ND1,2-Dichlorobenzene
0.190 0.0750 ug/L 06/05/23 11:58 06/07/23 15:26 1NDBenzo[a]anthracene
0.190 0.0530 ug/L 06/05/23 11:58 06/07/23 15:26 1NDBenzo[a]pyrene
1.00 0.0990 ug/L 06/05/23 11:58 06/07/23 15:26 1ND1,3-Dichlorobenzene
0.190 0.0970 ug/L 06/05/23 11:58 06/07/23 15:26 1NDBenzo[b]fluoranthene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 15:26 1NDBenzo[g,h,i]perylene
1.00 0.0610 ug/L 06/05/23 11:58 06/07/23 15:26 1ND1,4-Dichlorobenzene
0.190 0.0880 ug/L 06/05/23 11:58 06/07/23 15:26 1NDBenzo[k]fluoranthene
1.00 0.152 ug/L 06/05/23 11:58 06/07/23 15:26 1NDBis(2-chloroethoxy)methane
0.190 0.0400 ug/L 06/05/23 11:58 06/07/23 15:26 1NDBis(2-chloroethyl)ether
0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 15:26 1ND1-Methylnaphthalene
0.190 0.0580 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2,2'-oxybis[1-chloropropane]
10.0 6.23 ug/L 06/05/23 11:58 06/07/23 15:26 1NDBis(2-ethylhexyl) phthalate
1.00 0.319 ug/L 06/05/23 11:58 06/07/23 15:26 1ND4-Bromophenyl phenyl ether
1.00 0.462 ug/L 06/05/23 11:58 06/07/23 15:26 10.796 JButyl benzyl phthalate
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2-Chloronaphthalene
1.00 0.221 ug/L 06/05/23 11:58 06/07/23 15:26 1ND4-Chlorophenyl phenyl ether
0.190 0.0810 ug/L 06/05/23 11:58 06/07/23 15:26 1NDChrysene
0.190 0.0720 ug/L 06/05/23 11:58 06/07/23 15:26 1NDDibenz(a,h)anthracene
1.00 0.583 ug/L 06/05/23 11:58 06/07/23 15:26 1ND3,3'-Dichlorobenzidine
1.00 0.567 ug/L 06/05/23 11:58 06/07/23 15:26 10.672 JDiethyl phthalate
1.00 0.685 ug/L 06/05/23 11:58 06/07/23 15:26 1NDDi-n-octyl phthalate
1.00 0.196 ug/L 06/05/23 11:58 06/07/23 15:26 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.190 0.0620 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2-Methylnaphthalene
0.190 0.0600 ug/L 06/05/23 11:58 06/07/23 15:26 1NDFluoranthene
1.00 0.300 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2-Methylphenol
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 15:26 1NDFluorene
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-1Client Sample ID: TMW-5
Matrix: WaterDate Collected: 05/31/23 16:57
Date Received: 06/03/23 09:20
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 15:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexachlorobenzene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 15:26 1NDHexachlorobutadiene
1.00 0.497 ug/L 06/05/23 11:58 06/07/23 15:26 1NDHexachlorocyclopentadiene
1.00 0.133 ug/L 06/05/23 11:58 06/07/23 15:26 1NDHexachloroethane
0.190 0.0850 ug/L 06/05/23 11:58 06/07/23 15:26 1NDIndeno[1,2,3-cd]pyrene
1.00 0.188 ug/L 06/05/23 11:58 06/07/23 15:26 1NDIsophorone
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 15:26 1NDNaphthalene
2.00 0.500 ug/L 06/05/23 11:58 06/07/23 15:26 1NDNitrobenzene
1.00 0.0670 ug/L 06/05/23 11:58 06/07/23 15:26 1NDN-Nitrosodimethylamine
0.190 0.0710 ug/L 06/05/23 11:58 06/07/23 15:26 1NDN-Nitrosodi-n-propylamine
1.00 0.376 ug/L 06/05/23 11:58 06/07/23 15:26 1ND4-Chloroaniline
0.190 0.0550 ug/L 06/05/23 11:58 06/07/23 15:26 10.0920 JPhenanthrene
0.190 0.0540 ug/L 06/05/23 11:58 06/07/23 15:26 1NDPyrene
1.00 0.372 ug/L 06/05/23 11:58 06/07/23 15:26 1ND4-Methylphenol
5.00 0.847 ug/L 06/05/23 11:58 06/07/23 15:26 1NDPentachlorophenol
1.00 0.487 ug/L 06/05/23 11:58 06/07/23 15:26 1NDPhenol
1.00 0.131 ug/L 06/05/23 11:58 06/07/23 15:26 1ND1,2,4-Trichlorobenzene
0.190 0.0510 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2,4-Dichlorophenol
10.0 1.53 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2,4-Dinitrophenol
1.00 0.167 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2,4-Dimethylphenol
1.00 0.224 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2,4,6-Trichlorophenol
1.00 0.129 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2-Chlorophenol
1.00 0.193 ug/L 06/05/23 11:58 06/07/23 15:26 1ND2-Nitrophenol
5.00 1.47 ug/L 06/05/23 11:58 06/07/23 15:26 1ND4,6-Dinitro-2-methylphenol
1.00 0.278 ug/L 06/05/23 11:58 06/07/23 15:26 1ND4-Chloro-3-methylphenol
5.00 0.940 ug/L 06/05/23 11:58 06/07/23 15:26 1ND4-Nitrophenol
5.00 0.923 ug/L 06/05/23 11:58 06/07/23 15:26 11.20 JBenzoic acid
1.00 0.163 ug/L 06/05/23 11:58 06/07/23 15:26 10.217 JBenzyl alcohol
1.00 0.190 ug/L 06/05/23 11:58 06/07/23 15:26 1NDDibenzofuran
2,4,6-Tribromophenol (Surr)76 32-127 06/05/23 11:58 06/07/23 15:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 70 06/05/23 11:58 06/07/23 15:26 147-107
2-Fluorophenol (Surr)73 06/05/23 11:58 06/07/23 15:26 135-109
Nitrobenzene-d5 (Surr)74 06/05/23 11:58 06/07/23 15:26 147-110
Phenol-d5 (Surr)75 06/05/23 11:58 06/07/23 15:26 137-110
Terphenyl-d14 (Surr)81 06/05/23 11:58 06/07/23 15:26 132-115
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 20.0 ug/L 06/09/23 13:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 25.0 ug/L 06/09/23 07:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 06/09/23 07:13 1NDC9-C10 Aromatics
100 25.0 ug/L 06/09/23 07:13 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 06/09/23 07:13 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 06/09/23 07:13 1NDC5-C8 Aliphatics (adjusted)
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-1Client Sample ID: TMW-5
Matrix: WaterDate Collected: 05/31/23 16:57
Date Received: 06/03/23 09:20
a,a,a-Trifluorotoluene (fid)107 70-130 06/09/23 07:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)97 06/09/23 07:13 170-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 41.3 41.3 ug/L 06/09/23 19:11 06/27/23 05:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
41.3 41.3 ug/L 06/09/23 19:11 06/27/23 05:32 1NDC11-C22 Aromatics (Adjusted)
51.6 51.6 ug/L 06/09/23 19:11 06/27/23 05:32 1NDC19-C36 Aliphatics
31.0 31.0 ug/L 06/09/23 19:11 06/27/23 05:32 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)48 40-140 06/09/23 19:11 06/27/23 05:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)85 06/09/23 19:11 06/27/23 05:32 140-140
o- terphenyl (Surr)69 06/09/23 19:11 06/27/23 05:32 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 06/28/23 14:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-2Client Sample ID: TMW-7
Matrix: WaterDate Collected: 06/01/23 10:15
Date Received: 06/03/23 09:20
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 06/07/23 18:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 06/07/23 18:59 1ND1,3-Dichlorobenzene
1.00 0.544 ug/L 06/07/23 18:59 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 06/07/23 18:59 1NDBenzene
1.00 0.501 ug/L 06/07/23 18:59 1NDChlorobenzene
1.00 0.507 ug/L 06/07/23 18:59 1NDEthylbenzene
1.00 0.457 ug/L 06/07/23 18:59 1NDToluene
1.00 0.406 ug/L 06/07/23 18:59 1NDo-Xylene
1.00 0.482 ug/L 06/07/23 18:59 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 06/07/23 18:59 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)91 26-156 06/07/23 18:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)73 06/07/23 18:59 136-124
Dibromofluoromethane (Surr)116 06/07/23 18:59 146-149
Toluene-d8 (Surr)89 06/07/23 18:59 140-146
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 15:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 15:48 1NDAcenaphthylene
0.190 0.0490 ug/L 06/05/23 11:58 06/07/23 15:48 1NDAnthracene
1.00 0.0950 ug/L 06/05/23 11:58 06/07/23 15:48 1ND1,2-Dichlorobenzene
0.190 0.0750 ug/L 06/05/23 11:58 06/07/23 15:48 1NDBenzo[a]anthracene
0.190 0.0530 ug/L 06/05/23 11:58 06/07/23 15:48 1NDBenzo[a]pyrene
1.00 0.0990 ug/L 06/05/23 11:58 06/07/23 15:48 1ND1,3-Dichlorobenzene
0.190 0.0970 ug/L 06/05/23 11:58 06/07/23 15:48 1NDBenzo[b]fluoranthene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 15:48 1NDBenzo[g,h,i]perylene
1.00 0.0610 ug/L 06/05/23 11:58 06/07/23 15:48 1ND1,4-Dichlorobenzene
0.190 0.0880 ug/L 06/05/23 11:58 06/07/23 15:48 1NDBenzo[k]fluoranthene
1.00 0.152 ug/L 06/05/23 11:58 06/07/23 15:48 1NDBis(2-chloroethoxy)methane
0.190 0.0400 ug/L 06/05/23 11:58 06/07/23 15:48 1NDBis(2-chloroethyl)ether
0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 15:48 1ND1-Methylnaphthalene
0.190 0.0580 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2,2'-oxybis[1-chloropropane]
10.0 6.23 ug/L 06/05/23 11:58 06/07/23 15:48 1NDBis(2-ethylhexyl) phthalate
1.00 0.319 ug/L 06/05/23 11:58 06/07/23 15:48 1ND4-Bromophenyl phenyl ether
1.00 0.462 ug/L 06/05/23 11:58 06/07/23 15:48 10.875 JButyl benzyl phthalate
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2-Chloronaphthalene
1.00 0.221 ug/L 06/05/23 11:58 06/07/23 15:48 1ND4-Chlorophenyl phenyl ether
0.190 0.0810 ug/L 06/05/23 11:58 06/07/23 15:48 1NDChrysene
0.190 0.0720 ug/L 06/05/23 11:58 06/07/23 15:48 1NDDibenz(a,h)anthracene
1.00 0.583 ug/L 06/05/23 11:58 06/07/23 15:48 1ND3,3'-Dichlorobenzidine
1.00 0.567 ug/L 06/05/23 11:58 06/07/23 15:48 1NDDiethyl phthalate
1.00 0.685 ug/L 06/05/23 11:58 06/07/23 15:48 1NDDi-n-octyl phthalate
1.00 0.196 ug/L 06/05/23 11:58 06/07/23 15:48 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.190 0.0620 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2-Methylnaphthalene
0.190 0.0600 ug/L 06/05/23 11:58 06/07/23 15:48 10.0611 JFluoranthene
1.00 0.300 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2-Methylphenol
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 15:48 1NDFluorene
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-2Client Sample ID: TMW-7
Matrix: WaterDate Collected: 06/01/23 10:15
Date Received: 06/03/23 09:20
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.190 0.0560 ug/L 06/05/23 11:58 06/07/23 15:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexachlorobenzene
0.190 0.0690 ug/L 06/05/23 11:58 06/07/23 15:48 1NDHexachlorobutadiene
1.00 0.497 ug/L 06/05/23 11:58 06/07/23 15:48 1NDHexachlorocyclopentadiene
1.00 0.133 ug/L 06/05/23 11:58 06/07/23 15:48 1NDHexachloroethane
0.190 0.0850 ug/L 06/05/23 11:58 06/07/23 15:48 1NDIndeno[1,2,3-cd]pyrene
1.00 0.188 ug/L 06/05/23 11:58 06/07/23 15:48 1NDIsophorone
0.190 0.0590 ug/L 06/05/23 11:58 06/07/23 15:48 1NDNaphthalene
2.00 0.500 ug/L 06/05/23 11:58 06/07/23 15:48 1NDNitrobenzene
1.00 0.0670 ug/L 06/05/23 11:58 06/07/23 15:48 1NDN-Nitrosodimethylamine
0.190 0.0710 ug/L 06/05/23 11:58 06/07/23 15:48 1NDN-Nitrosodi-n-propylamine
1.00 0.376 ug/L 06/05/23 11:58 06/07/23 15:48 1ND4-Chloroaniline
0.190 0.0550 ug/L 06/05/23 11:58 06/07/23 15:48 10.136 JPhenanthrene
0.190 0.0540 ug/L 06/05/23 11:58 06/07/23 15:48 1NDPyrene
1.00 0.372 ug/L 06/05/23 11:58 06/07/23 15:48 1ND4-Methylphenol
5.00 0.847 ug/L 06/05/23 11:58 06/07/23 15:48 1NDPentachlorophenol
1.00 0.487 ug/L 06/05/23 11:58 06/07/23 15:48 1NDPhenol
1.00 0.131 ug/L 06/05/23 11:58 06/07/23 15:48 1ND1,2,4-Trichlorobenzene
0.190 0.0510 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2,4-Dichlorophenol
10.0 1.53 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2,4-Dinitrophenol
1.00 0.167 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2,4-Dimethylphenol
1.00 0.224 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2,4,6-Trichlorophenol
1.00 0.129 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2-Chlorophenol
1.00 0.193 ug/L 06/05/23 11:58 06/07/23 15:48 1ND2-Nitrophenol
5.00 1.47 ug/L 06/05/23 11:58 06/07/23 15:48 1ND4,6-Dinitro-2-methylphenol
1.00 0.278 ug/L 06/05/23 11:58 06/07/23 15:48 1ND4-Chloro-3-methylphenol
5.00 0.940 ug/L 06/05/23 11:58 06/07/23 15:48 1ND4-Nitrophenol
5.00 0.923 ug/L 06/05/23 11:58 06/07/23 15:48 11.08 JBenzoic acid
1.00 0.163 ug/L 06/05/23 11:58 06/07/23 15:48 1NDBenzyl alcohol
1.00 0.190 ug/L 06/05/23 11:58 06/07/23 15:48 1NDDibenzofuran
2,4,6-Tribromophenol (Surr)57 32-127 06/05/23 11:58 06/07/23 15:48 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 58 06/05/23 11:58 06/07/23 15:48 147-107
2-Fluorophenol (Surr)59 06/05/23 11:58 06/07/23 15:48 135-109
Nitrobenzene-d5 (Surr)60 06/05/23 11:58 06/07/23 15:48 147-110
Phenol-d5 (Surr)58 06/05/23 11:58 06/07/23 15:48 137-110
Terphenyl-d14 (Surr)62 06/05/23 11:58 06/07/23 15:48 132-115
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
57.7 J 100 20.0 ug/L 06/13/23 12:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
57.7 J 100 25.0 ug/L 06/12/23 12:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 06/12/23 12:52 1NDC9-C10 Aromatics
100 25.0 ug/L 06/12/23 12:52 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 06/12/23 12:52 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 06/12/23 12:52 157.4 JC5-C8 Aliphatics (adjusted)
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-2Client Sample ID: TMW-7
Matrix: WaterDate Collected: 06/01/23 10:15
Date Received: 06/03/23 09:20
a,a,a-Trifluorotoluene (fid)110 70-130 06/12/23 12:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)96 06/12/23 12:52 170-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 42.8 42.8 ug/L 06/09/23 19:11 06/27/23 05:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
42.8 42.8 ug/L 06/09/23 19:11 06/27/23 05:55 1NDC11-C22 Aromatics (Adjusted)
53.5 53.5 ug/L 06/09/23 19:11 06/27/23 05:55 1NDC19-C36 Aliphatics
32.1 32.1 ug/L 06/09/23 19:11 06/27/23 05:55 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)47 40-140 06/09/23 19:11 06/27/23 05:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)83 06/09/23 19:11 06/27/23 05:55 140-140
o- terphenyl (Surr)63 06/09/23 19:11 06/27/23 05:55 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 06/28/23 14:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-3Client Sample ID: TMW-9
Matrix: WaterDate Collected: 06/01/23 09:05
Date Received: 06/03/23 09:20
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 06/07/23 19:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 06/07/23 19:21 1ND1,3-Dichlorobenzene
1.00 0.544 ug/L 06/07/23 19:21 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 06/07/23 19:21 1NDBenzene
1.00 0.501 ug/L 06/07/23 19:21 1NDChlorobenzene
1.00 0.507 ug/L 06/07/23 19:21 1NDEthylbenzene
1.00 0.457 ug/L 06/07/23 19:21 1NDToluene
1.00 0.406 ug/L 06/07/23 19:21 1NDo-Xylene
1.00 0.482 ug/L 06/07/23 19:21 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 06/07/23 19:21 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)88 26-156 06/07/23 19:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)66 06/07/23 19:21 136-124
Dibromofluoromethane (Surr)106 06/07/23 19:21 146-149
Toluene-d8 (Surr)84 06/07/23 19:21 140-146
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.207 0.0707 ug/L 06/05/23 11:58 06/07/23 16:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.207 0.0707 ug/L 06/05/23 11:58 06/07/23 16:11 1NDAcenaphthylene
0.207 0.0533 ug/L 06/05/23 11:58 06/07/23 16:11 1NDAnthracene
1.09 0.103 ug/L 06/05/23 11:58 06/07/23 16:11 1ND1,2-Dichlorobenzene
0.207 0.0815 ug/L 06/05/23 11:58 06/07/23 16:11 1NDBenzo[a]anthracene
0.207 0.0576 ug/L 06/05/23 11:58 06/07/23 16:11 1NDBenzo[a]pyrene
1.09 0.108 ug/L 06/05/23 11:58 06/07/23 16:11 1ND1,3-Dichlorobenzene
0.207 0.105 ug/L 06/05/23 11:58 06/07/23 16:11 1NDBenzo[b]fluoranthene
0.207 0.0750 ug/L 06/05/23 11:58 06/07/23 16:11 1NDBenzo[g,h,i]perylene
1.09 0.0663 ug/L 06/05/23 11:58 06/07/23 16:11 1ND1,4-Dichlorobenzene
0.207 0.0957 ug/L 06/05/23 11:58 06/07/23 16:11 1NDBenzo[k]fluoranthene
1.09 0.165 ug/L 06/05/23 11:58 06/07/23 16:11 1NDBis(2-chloroethoxy)methane
0.207 0.0435 ug/L 06/05/23 11:58 06/07/23 16:11 1NDBis(2-chloroethyl)ether
0.207 0.0609 ug/L 06/05/23 11:58 06/07/23 16:11 1ND1-Methylnaphthalene
0.207 0.0630 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2,2'-oxybis[1-chloropropane]
10.9 6.77 ug/L 06/05/23 11:58 06/07/23 16:11 1NDBis(2-ethylhexyl) phthalate
1.09 0.347 ug/L 06/05/23 11:58 06/07/23 16:11 1ND4-Bromophenyl phenyl ether
1.09 0.502 ug/L 06/05/23 11:58 06/07/23 16:11 10.938 JButyl benzyl phthalate
0.207 0.0641 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2-Chloronaphthalene
1.09 0.240 ug/L 06/05/23 11:58 06/07/23 16:11 1ND4-Chlorophenyl phenyl ether
0.207 0.0880 ug/L 06/05/23 11:58 06/07/23 16:11 1NDChrysene
0.207 0.0783 ug/L 06/05/23 11:58 06/07/23 16:11 1NDDibenz(a,h)anthracene
1.09 0.634 ug/L 06/05/23 11:58 06/07/23 16:11 1ND3,3'-Dichlorobenzidine
1.09 0.616 ug/L 06/05/23 11:58 06/07/23 16:11 1NDDiethyl phthalate
1.09 0.745 ug/L 06/05/23 11:58 06/07/23 16:11 1NDDi-n-octyl phthalate
1.09 0.213 ug/L 06/05/23 11:58 06/07/23 16:11 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.207 0.0674 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2-Methylnaphthalene
0.207 0.0652 ug/L 06/05/23 11:58 06/07/23 16:11 1NDFluoranthene
1.09 0.326 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2-Methylphenol
0.207 0.0750 ug/L 06/05/23 11:58 06/07/23 16:11 1NDFluorene
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-3Client Sample ID: TMW-9
Matrix: WaterDate Collected: 06/01/23 09:05
Date Received: 06/03/23 09:20
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.207 0.0609 ug/L 06/05/23 11:58 06/07/23 16:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexachlorobenzene
0.207 0.0750 ug/L 06/05/23 11:58 06/07/23 16:11 1NDHexachlorobutadiene
1.09 0.540 ug/L 06/05/23 11:58 06/07/23 16:11 1NDHexachlorocyclopentadiene
1.09 0.145 ug/L 06/05/23 11:58 06/07/23 16:11 1NDHexachloroethane
0.207 0.0924 ug/L 06/05/23 11:58 06/07/23 16:11 1NDIndeno[1,2,3-cd]pyrene
1.09 0.204 ug/L 06/05/23 11:58 06/07/23 16:11 1NDIsophorone
0.207 0.0641 ug/L 06/05/23 11:58 06/07/23 16:11 1NDNaphthalene
2.17 0.543 ug/L 06/05/23 11:58 06/07/23 16:11 1NDNitrobenzene
1.09 0.0728 ug/L 06/05/23 11:58 06/07/23 16:11 1NDN-Nitrosodimethylamine
0.207 0.0772 ug/L 06/05/23 11:58 06/07/23 16:11 1NDN-Nitrosodi-n-propylamine
1.09 0.409 ug/L 06/05/23 11:58 06/07/23 16:11 1ND4-Chloroaniline
0.207 0.0598 ug/L 06/05/23 11:58 06/07/23 16:11 10.0984 JPhenanthrene
0.207 0.0587 ug/L 06/05/23 11:58 06/07/23 16:11 1NDPyrene
1.09 0.404 ug/L 06/05/23 11:58 06/07/23 16:11 1ND4-Methylphenol
5.43 0.921 ug/L 06/05/23 11:58 06/07/23 16:11 1NDPentachlorophenol
1.09 0.529 ug/L 06/05/23 11:58 06/07/23 16:11 1NDPhenol
1.09 0.142 ug/L 06/05/23 11:58 06/07/23 16:11 1ND1,2,4-Trichlorobenzene
0.207 0.0554 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2,4-Dichlorophenol
10.9 1.66 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2,4-Dinitrophenol
1.09 0.182 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2,4-Dimethylphenol
1.09 0.243 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2,4,6-Trichlorophenol
1.09 0.140 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2-Chlorophenol
1.09 0.210 ug/L 06/05/23 11:58 06/07/23 16:11 1ND2-Nitrophenol
5.43 1.60 ug/L 06/05/23 11:58 06/07/23 16:11 1ND4,6-Dinitro-2-methylphenol
1.09 0.302 ug/L 06/05/23 11:58 06/07/23 16:11 1ND4-Chloro-3-methylphenol
5.43 1.02 ug/L 06/05/23 11:58 06/07/23 16:11 1ND4-Nitrophenol
5.43 1.00 ug/L 06/05/23 11:58 06/07/23 16:11 11.27 JBenzoic acid
1.09 0.177 ug/L 06/05/23 11:58 06/07/23 16:11 10.258 JBenzyl alcohol
1.09 0.207 ug/L 06/05/23 11:58 06/07/23 16:11 1NDDibenzofuran
2,4,6-Tribromophenol (Surr)65 32-127 06/05/23 11:58 06/07/23 16:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 61 06/05/23 11:58 06/07/23 16:11 147-107
2-Fluorophenol (Surr)64 06/05/23 11:58 06/07/23 16:11 135-109
Nitrobenzene-d5 (Surr)65 06/05/23 11:58 06/07/23 16:11 147-110
Phenol-d5 (Surr)65 06/05/23 11:58 06/07/23 16:11 137-110
Terphenyl-d14 (Surr)61 06/05/23 11:58 06/07/23 16:11 132-115
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 20.0 ug/L 06/13/23 12:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 25.0 ug/L 06/12/23 13:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 06/12/23 13:33 1NDC9-C10 Aromatics
100 25.0 ug/L 06/12/23 13:33 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 06/12/23 13:33 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 06/12/23 13:33 1NDC5-C8 Aliphatics (adjusted)
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-3Client Sample ID: TMW-9
Matrix: WaterDate Collected: 06/01/23 09:05
Date Received: 06/03/23 09:20
a,a,a-Trifluorotoluene (fid)108 70-130 06/12/23 13:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)93 06/12/23 13:33 170-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 42.0 42.0 ug/L 06/09/23 19:11 06/27/23 06:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
42.0 42.0 ug/L 06/09/23 19:11 06/27/23 06:17 1NDC11-C22 Aromatics (Adjusted)
52.5 52.5 ug/L 06/09/23 19:11 06/27/23 06:17 1NDC19-C36 Aliphatics
31.5 31.5 ug/L 06/09/23 19:11 06/27/23 06:17 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)55 40-140 06/09/23 19:11 06/27/23 06:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)87 06/09/23 19:11 06/27/23 06:17 140-140
o- terphenyl (Surr)75 06/09/23 19:11 06/27/23 06:17 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 06/28/23 14:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-4Client Sample ID: TMW-10
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 06/03/23 09:20
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
RL MDL
ND 1.00 0.364 ug/L 06/08/23 14:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichlorobenzene
1.00 0.504 ug/L 06/08/23 14:18 1ND1,3-Dichlorobenzene
1.00 0.544 ug/L 06/08/23 14:18 1ND1,4-Dichlorobenzene
1.00 0.596 ug/L 06/08/23 14:18 1NDBenzene
1.00 0.501 ug/L 06/08/23 14:18 1NDChlorobenzene
1.00 0.507 ug/L 06/08/23 14:18 1NDEthylbenzene
1.00 0.457 ug/L 06/08/23 14:18 1NDToluene
1.00 0.406 ug/L 06/08/23 14:18 1NDo-Xylene
1.00 0.482 ug/L 06/08/23 14:18 1NDm-Xylene & p-Xylene
2.00 0.890 ug/L 06/08/23 14:18 1NDXylenes, Total
1,2-Dichloroethane-d4 (Surr)80 26-156 06/08/23 14:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)70 06/08/23 14:18 136-124
Dibromofluoromethane (Surr)96 06/08/23 14:18 146-149
Toluene-d8 (Surr)74 06/08/23 14:18 140-146
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
RL MDL
ND 0.198 0.0677 ug/L 06/05/23 11:58 06/07/23 16:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Acenaphthene
0.198 0.0677 ug/L 06/05/23 11:58 06/07/23 16:33 1NDAcenaphthylene
0.198 0.0510 ug/L 06/05/23 11:58 06/07/23 16:33 1NDAnthracene
1.04 0.0990 ug/L 06/05/23 11:58 06/07/23 16:33 1ND1,2-Dichlorobenzene
0.198 0.0781 ug/L 06/05/23 11:58 06/07/23 16:33 1NDBenzo[a]anthracene
0.198 0.0552 ug/L 06/05/23 11:58 06/07/23 16:33 1NDBenzo[a]pyrene
1.04 0.103 ug/L 06/05/23 11:58 06/07/23 16:33 1ND1,3-Dichlorobenzene
0.198 0.101 ug/L 06/05/23 11:58 06/07/23 16:33 1NDBenzo[b]fluoranthene
0.198 0.0719 ug/L 06/05/23 11:58 06/07/23 16:33 1NDBenzo[g,h,i]perylene
1.04 0.0635 ug/L 06/05/23 11:58 06/07/23 16:33 1ND1,4-Dichlorobenzene
0.198 0.0917 ug/L 06/05/23 11:58 06/07/23 16:33 1NDBenzo[k]fluoranthene
1.04 0.158 ug/L 06/05/23 11:58 06/07/23 16:33 1NDBis(2-chloroethoxy)methane
0.198 0.0417 ug/L 06/05/23 11:58 06/07/23 16:33 1NDBis(2-chloroethyl)ether
0.198 0.0583 ug/L 06/05/23 11:58 06/07/23 16:33 1ND1-Methylnaphthalene
0.198 0.0604 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2,2'-oxybis[1-chloropropane]
10.4 6.49 ug/L 06/05/23 11:58 06/07/23 16:33 1NDBis(2-ethylhexyl) phthalate
1.04 0.332 ug/L 06/05/23 11:58 06/07/23 16:33 1ND4-Bromophenyl phenyl ether
1.04 0.481 ug/L 06/05/23 11:58 06/07/23 16:33 11.02 JButyl benzyl phthalate
0.198 0.0615 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2-Chloronaphthalene
1.04 0.230 ug/L 06/05/23 11:58 06/07/23 16:33 1ND4-Chlorophenyl phenyl ether
0.198 0.0844 ug/L 06/05/23 11:58 06/07/23 16:33 1NDChrysene
0.198 0.0750 ug/L 06/05/23 11:58 06/07/23 16:33 1NDDibenz(a,h)anthracene
1.04 0.607 ug/L 06/05/23 11:58 06/07/23 16:33 1ND3,3'-Dichlorobenzidine
1.04 0.591 ug/L 06/05/23 11:58 06/07/23 16:33 1NDDiethyl phthalate
1.04 0.714 ug/L 06/05/23 11:58 06/07/23 16:33 1NDDi-n-octyl phthalate
1.04 0.204 ug/L 06/05/23 11:58 06/07/23 16:33 1ND1,2-Diphenylhydrazine(as
Azobenzene)
0.198 0.0646 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2-Methylnaphthalene
0.198 0.0625 ug/L 06/05/23 11:58 06/07/23 16:33 1NDFluoranthene
1.04 0.313 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2-Methylphenol
0.198 0.0719 ug/L 06/05/23 11:58 06/07/23 16:33 1NDFluorene
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-4Client Sample ID: TMW-10
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 06/03/23 09:20
Method: 40 CFR 761 EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
ND 0.198 0.0583 ug/L 06/05/23 11:58 06/07/23 16:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Hexachlorobenzene
0.198 0.0719 ug/L 06/05/23 11:58 06/07/23 16:33 1NDHexachlorobutadiene
1.04 0.518 ug/L 06/05/23 11:58 06/07/23 16:33 1NDHexachlorocyclopentadiene
1.04 0.139 ug/L 06/05/23 11:58 06/07/23 16:33 1NDHexachloroethane
0.198 0.0885 ug/L 06/05/23 11:58 06/07/23 16:33 1NDIndeno[1,2,3-cd]pyrene
1.04 0.196 ug/L 06/05/23 11:58 06/07/23 16:33 1NDIsophorone
0.198 0.0615 ug/L 06/05/23 11:58 06/07/23 16:33 1NDNaphthalene
2.08 0.521 ug/L 06/05/23 11:58 06/07/23 16:33 1NDNitrobenzene
1.04 0.0698 ug/L 06/05/23 11:58 06/07/23 16:33 1NDN-Nitrosodimethylamine
0.198 0.0740 ug/L 06/05/23 11:58 06/07/23 16:33 1NDN-Nitrosodi-n-propylamine
1.04 0.392 ug/L 06/05/23 11:58 06/07/23 16:33 1ND4-Chloroaniline
0.198 0.0573 ug/L 06/05/23 11:58 06/07/23 16:33 10.131 JPhenanthrene
0.198 0.0563 ug/L 06/05/23 11:58 06/07/23 16:33 1NDPyrene
1.04 0.388 ug/L 06/05/23 11:58 06/07/23 16:33 1ND4-Methylphenol
5.21 0.882 ug/L 06/05/23 11:58 06/07/23 16:33 1NDPentachlorophenol
1.04 0.507 ug/L 06/05/23 11:58 06/07/23 16:33 1NDPhenol
1.04 0.136 ug/L 06/05/23 11:58 06/07/23 16:33 1ND1,2,4-Trichlorobenzene
0.198 0.0531 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2,4-Dichlorophenol
10.4 1.59 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2,4-Dinitrophenol
1.04 0.174 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2,4-Dimethylphenol
1.04 0.233 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2,4,6-Trichlorophenol
1.04 0.134 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2-Chlorophenol
1.04 0.201 ug/L 06/05/23 11:58 06/07/23 16:33 1ND2-Nitrophenol
5.21 1.53 ug/L 06/05/23 11:58 06/07/23 16:33 1ND4,6-Dinitro-2-methylphenol
1.04 0.290 ug/L 06/05/23 11:58 06/07/23 16:33 1ND4-Chloro-3-methylphenol
5.21 0.979 ug/L 06/05/23 11:58 06/07/23 16:33 1ND4-Nitrophenol
5.21 0.961 ug/L 06/05/23 11:58 06/07/23 16:33 11.48 JBenzoic acid
1.04 0.170 ug/L 06/05/23 11:58 06/07/23 16:33 1NDBenzyl alcohol
1.04 0.198 ug/L 06/05/23 11:58 06/07/23 16:33 1NDDibenzofuran
2,4,6-Tribromophenol (Surr)74 32-127 06/05/23 11:58 06/07/23 16:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl 66 06/05/23 11:58 06/07/23 16:33 147-107
2-Fluorophenol (Surr)70 06/05/23 11:58 06/07/23 16:33 135-109
Nitrobenzene-d5 (Surr)69 06/05/23 11:58 06/07/23 16:33 147-110
Phenol-d5 (Surr)72 06/05/23 11:58 06/07/23 16:33 137-110
Terphenyl-d14 (Surr)66 06/05/23 11:58 06/07/23 16:33 132-115
Method: MA DEP MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 20.0 ug/L 06/13/23 12:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total VPH
Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
ND 100 25.0 ug/L 06/12/23 14:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C5-C8 Aliphatics (unadjusted)
100 10.0 ug/L 06/12/23 14:14 1NDC9-C10 Aromatics
100 25.0 ug/L 06/12/23 14:14 1NDC9-C12 Aliphatics (unadjusted)
100 25.0 ug/L 06/12/23 14:14 1NDC9-C12 Aliphatics (adjusted)
100 25.0 ug/L 06/12/23 14:14 1NDC5-C8 Aliphatics (adjusted)
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Client Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Lab Sample ID: 180-157472-4Client Sample ID: TMW-10
Matrix: WaterDate Collected: 06/01/23 11:45
Date Received: 06/03/23 09:20
a,a,a-Trifluorotoluene (fid)109 70-130 06/12/23 14:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
a,a,a-Trifluorotoluene (pid)95 06/12/23 14:14 170-130
Method: MA DEP MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 41.6 41.6 ug/L 06/09/23 19:11 06/27/23 06:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
C11-C22 Aromatics (unadjusted)
41.6 41.6 ug/L 06/09/23 19:11 06/27/23 06:40 1NDC11-C22 Aromatics (Adjusted)
52.0 52.0 ug/L 06/09/23 19:11 06/27/23 06:40 1NDC19-C36 Aliphatics
31.2 31.2 ug/L 06/09/23 19:11 06/27/23 06:40 1NDC9-C18 Aliphatics
1-Chlorooctadecane (Surr)52 40-140 06/09/23 19:11 06/27/23 06:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)87 06/09/23 19:11 06/27/23 06:40 140-140
o- terphenyl (Surr)74 06/09/23 19:11 06/27/23 06:40 140-140
Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
ND 100 30.0 ug/L 06/28/23 14:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Total EPH
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 180-437251/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
RL MDL
1,2-Dichlorobenzene ND 1.00 0.364 ug/L 06/07/23 15:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.5041.00 ug/L 06/07/23 15:00 11,3-Dichlorobenzene
ND 0.5441.00 ug/L 06/07/23 15:00 11,4-Dichlorobenzene
ND 0.5961.00 ug/L 06/07/23 15:00 1Benzene
ND 0.5011.00 ug/L 06/07/23 15:00 1Chlorobenzene
ND 0.5071.00 ug/L 06/07/23 15:00 1Ethylbenzene
ND 0.4571.00 ug/L 06/07/23 15:00 1Toluene
ND 0.4061.00 ug/L 06/07/23 15:00 1o-Xylene
ND 0.4821.00 ug/L 06/07/23 15:00 1m-Xylene & p-Xylene
ND 0.8902.00 ug/L 06/07/23 15:00 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)80 26-156 06/07/23 15:00 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
79 06/07/23 15:00 14-Bromofluorobenzene (Surr)36-124
102 06/07/23 15:00 1Dibromofluoromethane (Surr)46-149
94 06/07/23 15:00 1Toluene-d8 (Surr)40-146
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437251/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
1,2-Dichlorobenzene 10.0 10.38 ug/L 104 64-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,3-Dichlorobenzene 10.0 10.11 ug/L 101 63-123
1,4-Dichlorobenzene 10.0 8.557 ug/L 86 67-118
Benzene 10.0 9.777 ug/L 98 68-125
Chlorobenzene 10.0 10.19 ug/L 102 68-121
Ethylbenzene 10.0 9.729 ug/L 97 65-126
Toluene 10.0 9.190 ug/L 92 69-124
o-Xylene 10.0 9.645 ug/L 96 64-127
m-Xylene & p-Xylene 10.0 9.565 ug/L 96 66-131
Xylenes, Total 20.0 19.21 ug/L 96 68-124
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
84
LCS LCS
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)36 -124
110Dibromofluoromethane (Surr)46 -149
98Toluene-d8 (Surr)40 -146
Client Sample ID: Matrix SpikeLab Sample ID: 180-157361-F-7 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
1,2-Dichlorobenzene ND 10.0 10.24 ug/L 102 64-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,3-Dichlorobenzene ND 10.0 10.02 ug/L 100 63-123
1,4-Dichlorobenzene ND 10.0 8.439 ug/L 84 67-118
Benzene ND 10.0 9.414 ug/L 94 68-125
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-157361-F-7 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
Chlorobenzene ND 10.0 10.24 ug/L 102 68-121
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Ethylbenzene ND 10.0 9.743 ug/L 97 65-126
Toluene ND 10.0 8.942 ug/L 89 69-124
o-Xylene ND 10.0 9.551 ug/L 96 64-127
m-Xylene & p-Xylene ND 10.0 9.565 ug/L 96 66-131
Xylenes, Total ND 20.0 19.12 ug/L 96 68-124
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
87
MS MS
Qualifier Limits%Recovery
934-Bromofluorobenzene (Surr)36 -124
112Dibromofluoromethane (Surr)46 -149
95Toluene-d8 (Surr)40 -146
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-157361-H-7 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437251
1,2-Dichlorobenzene ND 10.0 10.33 ug/L 103 64-120 1 27
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,3-Dichlorobenzene ND 10.0 10.41 ug/L 104 63-123 4 27
1,4-Dichlorobenzene ND 10.0 8.687 ug/L 87 67-118 3 24
Benzene ND 10.0 9.925 ug/L 99 68-125 5 24
Chlorobenzene ND 10.0 10.60 ug/L 106 68-121 3 21
Ethylbenzene ND 10.0 9.728 ug/L 97 65-126 0 22
Toluene ND 10.0 9.190 ug/L 92 69-124 3 23
o-Xylene ND 10.0 9.811 ug/L 98 64-127 3 26
m-Xylene & p-Xylene ND 10.0 9.660 ug/L 97 66-131 1 26
Xylenes, Total ND 20.0 19.47 ug/L 97 68-124 2 24
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
92
MSD MSD
Qualifier Limits%Recovery
1074-Bromofluorobenzene (Surr)36 -124
117Dibromofluoromethane (Surr)46 -149
94Toluene-d8 (Surr)40 -146
Client Sample ID: Method BlankLab Sample ID: MB 180-437390/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437390
RL MDL
1,2-Dichlorobenzene ND 1.00 0.364 ug/L 06/08/23 12:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.5041.00 ug/L 06/08/23 12:52 11,3-Dichlorobenzene
ND 0.5441.00 ug/L 06/08/23 12:52 11,4-Dichlorobenzene
ND 0.5961.00 ug/L 06/08/23 12:52 1Benzene
ND 0.5011.00 ug/L 06/08/23 12:52 1Chlorobenzene
ND 0.5071.00 ug/L 06/08/23 12:52 1Ethylbenzene
ND 0.4571.00 ug/L 06/08/23 12:52 1Toluene
ND 0.4061.00 ug/L 06/08/23 12:52 1o-Xylene
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437390/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437390
RL MDL
m-Xylene & p-Xylene ND 1.00 0.482 ug/L 06/08/23 12:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.8902.00 ug/L 06/08/23 12:52 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)75 26-156 06/08/23 12:52 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
71 06/08/23 12:52 14-Bromofluorobenzene (Surr)36-124
93 06/08/23 12:52 1Dibromofluoromethane (Surr)46-149
77 06/08/23 12:52 1Toluene-d8 (Surr)40-146
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437390/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437390
1,2-Dichlorobenzene 10.0 10.59 ug/L 106 64-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,3-Dichlorobenzene 10.0 10.32 ug/L 103 63-123
1,4-Dichlorobenzene 10.0 8.802 ug/L 88 67-118
Benzene 10.0 10.39 ug/L 104 68-125
Chlorobenzene 10.0 11.16 ug/L 112 68-121
Ethylbenzene 10.0 10.59 ug/L 106 65-126
Toluene 10.0 9.683 ug/L 97 69-124
o-Xylene 10.0 10.56 ug/L 106 64-127
m-Xylene & p-Xylene 10.0 10.53 ug/L 105 66-131
Xylenes, Total 20.0 21.09 ug/L 105 68-124
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
106
LCS LCS
Qualifier Limits%Recovery
1034-Bromofluorobenzene (Surr)36 -124
127Dibromofluoromethane (Surr)46 -149
100Toluene-d8 (Surr)40 -146
Client Sample ID: Matrix SpikeLab Sample ID: 180-157615-H-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437390
1,2-Dichlorobenzene ND 10.0 9.867 ug/L 99 64-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,3-Dichlorobenzene ND 10.0 9.301 ug/L 93 63-123
1,4-Dichlorobenzene ND 10.0 8.108 ug/L 81 67-118
Benzene ND 10.0 9.668 ug/L 97 68-125
Chlorobenzene ND 10.0 10.68 ug/L 107 68-121
Ethylbenzene ND 10.0 9.791 ug/L 98 65-126
Toluene ND 10.0 9.018 ug/L 90 69-124
o-Xylene ND 10.0 9.767 ug/L 98 64-127
m-Xylene & p-Xylene ND 10.0 9.821 ug/L 98 66-131
Xylenes, Total ND 20.0 19.59 ug/L 98 68-124
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-157615-H-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437390
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
84
MS MS
Qualifier Limits%Recovery
944-Bromofluorobenzene (Surr)36 -124
101Dibromofluoromethane (Surr)46 -149
76Toluene-d8 (Surr)40 -146
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 180-157615-I-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437390
1,2-Dichlorobenzene ND 10.0 9.705 ug/L 97 64-120 2 27
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,3-Dichlorobenzene ND 10.0 9.508 ug/L 95 63-123 2 27
1,4-Dichlorobenzene ND 10.0 8.122 ug/L 81 67-118 0 24
Benzene ND 10.0 9.219 ug/L 92 68-125 5 24
Chlorobenzene ND 10.0 10.61 ug/L 106 68-121 1 21
Ethylbenzene ND 10.0 9.972 ug/L 100 65-126 2 22
Toluene ND 10.0 9.116 ug/L 91 69-124 1 23
o-Xylene ND 10.0 9.858 ug/L 99 64-127 1 26
m-Xylene & p-Xylene ND 10.0 9.960 ug/L 100 66-131 1 26
Xylenes, Total ND 20.0 19.82 ug/L 99 68-124 1 24
1,2-Dichloroethane-d4 (Surr)26 -156
Surrogate
80
MSD MSD
Qualifier Limits%Recovery
1004-Bromofluorobenzene (Surr)36 -124
106Dibromofluoromethane (Surr)46 -149
83Toluene-d8 (Surr)40 -146
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 180-437005/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
RL MDL
Acenaphthene ND 0.190 0.0650 ug/L 06/05/23 11:58 06/07/23 10:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.06500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Acenaphthylene
ND 0.04900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Anthracene
ND 0.09501.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,2-Dichlorobenzene
ND 0.07500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[a]anthracene
ND 0.05300.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[a]pyrene
ND 0.09901.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,3-Dichlorobenzene
ND 0.09700.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[b]fluoranthene
ND 0.06900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[g,h,i]perylene
ND 0.06101.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,4-Dichlorobenzene
ND 0.08800.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzo[k]fluoranthene
ND 0.1521.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Bis(2-chloroethoxy)methane
ND 0.04000.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Bis(2-chloroethyl)ether
ND 0.05600.190 ug/L 06/05/23 11:58 06/07/23 10:59 11-Methylnaphthalene
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437005/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
RL MDL
2,2'-oxybis[1-chloropropane]ND 0.190 0.0580 ug/L 06/05/23 11:58 06/07/23 10:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 6.2310.0 ug/L 06/05/23 11:58 06/07/23 10:59 1Bis(2-ethylhexyl) phthalate
ND 0.3191.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Bromophenyl phenyl ether
ND 0.4621.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Butyl benzyl phthalate
ND 0.05900.190 ug/L 06/05/23 11:58 06/07/23 10:59 12-Chloronaphthalene
ND 0.2211.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Chlorophenyl phenyl ether
ND 0.08100.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Chrysene
ND 0.07200.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Dibenz(a,h)anthracene
ND 0.5831.00 ug/L 06/05/23 11:58 06/07/23 10:59 13,3'-Dichlorobenzidine
ND 0.5671.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Diethyl phthalate
ND 0.6851.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Di-n-octyl phthalate
ND 0.1961.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,2-Diphenylhydrazine(as
Azobenzene)
ND 0.06200.190 ug/L 06/05/23 11:58 06/07/23 10:59 12-Methylnaphthalene
ND 0.06000.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Fluoranthene
ND 0.3001.00 ug/L 06/05/23 11:58 06/07/23 10:59 12-Methylphenol
ND 0.06900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Fluorene
ND 0.05600.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachlorobenzene
ND 0.06900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachlorobutadiene
ND 0.4971.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachlorocyclopentadiene
ND 0.1331.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Hexachloroethane
ND 0.08500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Indeno[1,2,3-cd]pyrene
ND 0.1881.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Isophorone
ND 0.05900.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Naphthalene
ND 0.5002.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Nitrobenzene
ND 0.06701.00 ug/L 06/05/23 11:58 06/07/23 10:59 1N-Nitrosodimethylamine
ND 0.07100.190 ug/L 06/05/23 11:58 06/07/23 10:59 1N-Nitrosodi-n-propylamine
ND 0.3761.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Chloroaniline
ND 0.05500.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Phenanthrene
ND 0.05400.190 ug/L 06/05/23 11:58 06/07/23 10:59 1Pyrene
ND 0.3721.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Methylphenol
ND 0.8475.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Pentachlorophenol
ND 0.4871.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Phenol
ND 0.1311.00 ug/L 06/05/23 11:58 06/07/23 10:59 11,2,4-Trichlorobenzene
ND 0.05100.190 ug/L 06/05/23 11:58 06/07/23 10:59 12,4-Dichlorophenol
ND 1.5310.0 ug/L 06/05/23 11:58 06/07/23 10:59 12,4-Dinitrophenol
ND 0.1671.00 ug/L 06/05/23 11:58 06/07/23 10:59 12,4-Dimethylphenol
ND 0.2241.00 ug/L 06/05/23 11:58 06/07/23 10:59 12,4,6-Trichlorophenol
ND 0.1291.00 ug/L 06/05/23 11:58 06/07/23 10:59 12-Chlorophenol
ND 0.1931.00 ug/L 06/05/23 11:58 06/07/23 10:59 12-Nitrophenol
ND 1.475.00 ug/L 06/05/23 11:58 06/07/23 10:59 14,6-Dinitro-2-methylphenol
ND 0.2781.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Chloro-3-methylphenol
ND 0.9405.00 ug/L 06/05/23 11:58 06/07/23 10:59 14-Nitrophenol
ND 0.9235.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzoic acid
ND 0.1631.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Benzyl alcohol
ND 0.1901.00 ug/L 06/05/23 11:58 06/07/23 10:59 1Dibenzofuran
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 180-437005/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
2,4,6-Tribromophenol (Surr)56 32-127 06/07/23 10:59 1
MB MB
Surrogate
06/05/23 11:58
Dil FacPreparedAnalyzedQualifierLimits%Recovery
81 06/05/23 11:58 06/07/23 10:59 12-Fluorobiphenyl 47-107
73 06/05/23 11:58 06/07/23 10:59 12-Fluorophenol (Surr)35-109
74 06/05/23 11:58 06/07/23 10:59 1Nitrobenzene-d5 (Surr)47-110
69 06/05/23 11:58 06/07/23 10:59 1Phenol-d5 (Surr)37-110
90 06/05/23 11:58 06/07/23 10:59 1Terphenyl-d14 (Surr)32-115
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437005/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Acenaphthene 10.0 7.822 ug/L 78 47-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Acenaphthylene 10.0 8.169 ug/L 82 33-145
Anthracene 10.0 7.734 ug/L 77 27-133
1,2-Dichlorobenzene 10.0 7.657 ug/L 77 50-100
Benzo[a]anthracene 10.0 8.044 ug/L 80 33-143
Benzo[a]pyrene 10.0 8.443 ug/L 84 17-150
1,3-Dichlorobenzene 10.0 7.589 ug/L 76 51-100
Benzo[b]fluoranthene 10.0 8.442 ug/L 84 24-150
Benzo[g,h,i]perylene 10.0 7.818 ug/L 78 10-150
1,4-Dichlorobenzene 10.0 7.731 ug/L 77 51-100
Benzo[k]fluoranthene 10.0 8.189 ug/L 82 11-150
Bis(2-chloroethoxy)methane 10.0 6.832 ug/L 68 33-150
Bis(2-chloroethyl)ether 10.0 6.714 ug/L 67 12-150
1-Methylnaphthalene 10.0 8.103 ug/L 81 49-100
2,2'-oxybis[1-chloropropane]10.0 7.946 ug/L 79 36-150
Bis(2-ethylhexyl) phthalate 10.0 8.044 J ug/L 80 10-150
4-Bromophenyl phenyl ether 10.0 7.870 ug/L 79 53-127
Butyl benzyl phthalate 10.0 8.489 ug/L 85 10-150
2-Chloronaphthalene 10.0 7.727 ug/L 77 60-120
4-Chlorophenyl phenyl ether 10.0 8.200 ug/L 82 25-150
Chrysene 10.0 8.096 ug/L 81 17-150
Dibenz(a,h)anthracene 10.0 8.290 ug/L 83 10-150
3,3'-Dichlorobenzidine 10.0 7.939 ug/L 79 10-150
Diethyl phthalate 10.0 7.283 ug/L 73 10-120
Di-n-octyl phthalate 10.0 7.927 ug/L 79 10-146
1,2-Diphenylhydrazine(as
Azobenzene)
10.0 7.019 ug/L 70 43-105
2-Methylnaphthalene 10.0 8.097 ug/L 81 51-100
Fluoranthene 10.0 7.690 ug/L 77 26-137
2-Methylphenol 10.0 7.742 ug/L 77 48-100
Fluorene 10.0 7.496 ug/L 75 59-121
Hexachlorobenzene 10.0 6.900 ug/L 69 10-150
Hexachlorobutadiene 10.0 7.247 ug/L 72 24-120
Hexachlorocyclopentadiene 10.0 6.817 ug/L 68 37-121
Hexachloroethane 10.0 7.057 ug/L 71 40-120
Indeno[1,2,3-cd]pyrene 10.0 7.976 ug/L 80 10-150
Isophorone 10.0 7.648 ug/L 76 21-150
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437005/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Naphthalene 10.0 7.477 ug/L 75 21-133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Nitrobenzene 10.0 7.467 ug/L 75 35-150
N-Nitrosodimethylamine 10.0 8.734 ug/L 87 33-130
N-Nitrosodi-n-propylamine 10.0 8.578 ug/L 86 10-150
4-Chloroaniline 10.0 7.412 ug/L 74 49-100
Phenanthrene 10.0 7.461 ug/L 75 54-120
Pyrene 10.0 9.091 ug/L 91 52-120
4-Methylphenol 10.0 7.899 ug/L 79 47-100
Pentachlorophenol 20.0 13.38 ug/L 67 14-150
Phenol 10.0 6.802 ug/L 68 10-120
1,2,4-Trichlorobenzene 10.0 7.765 ug/L 78 44-142
2,4-Dichlorophenol 10.0 7.630 ug/L 76 39-135
2,4-Dinitrophenol 20.0 13.19 ug/L 66 10-150
2,4-Dimethylphenol 10.0 6.635 ug/L 66 32-120
2,4,6-Trichlorophenol 10.0 8.448 ug/L 84 37-144
2-Chlorophenol 10.0 7.376 ug/L 74 23-134
2-Nitrophenol 10.0 8.119 ug/L 81 29-150
4,6-Dinitro-2-methylphenol 20.0 16.83 ug/L 84 10-150
4-Chloro-3-methylphenol 10.0 8.274 ug/L 83 22-147
4-Nitrophenol 20.0 12.40 ug/L 62 10-132
Benzoic acid 10.0 6.461 ug/L 65 26-127
Benzyl alcohol 10.0 6.997 ug/L 70 30-102
Dibenzofuran 10.0 7.514 ug/L 75 51-100
2,4,6-Tribromophenol (Surr)32 -127
Surrogate
63
LCS LCS
Qualifier Limits%Recovery
782-Fluorobiphenyl 47 -107
712-Fluorophenol (Surr)35 -109
75Nitrobenzene-d5 (Surr)47 -110
69Phenol-d5 (Surr)37 -110
83Terphenyl-d14 (Surr)32 -115
Client Sample ID: Matrix SpikeLab Sample ID: 180-157266-D-1-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Acenaphthene ND F1 10.0 4.111 F1 ug/L 41 47-145
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Acenaphthylene ND 10.0 4.093 ug/L 41 35-145
Anthracene ND 10.0 3.947 ug/L 39 27-133
1,2-Dichlorobenzene ND F1 10.0 1.693 F1 ug/L 17 60-100
Benzo[a]anthracene ND 10.0 4.369 ug/L 44 33-143
Benzo[a]pyrene ND 10.0 4.183 ug/L 42 17-163
1,3-Dichlorobenzene ND F1 10.0 1.594 F1 ug/L 16 60-100
Benzo[b]fluoranthene ND 10.0 4.204 ug/L 42 24-159
Benzo[g,h,i]perylene ND 10.0 4.237 ug/L 42 10-170
1,4-Dichlorobenzene ND F1 10.0 1.637 F1 ug/L 16 60-100
Benzo[k]fluoranthene ND 10.0 4.458 ug/L 45 11-162
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 180-157266-D-1-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 437193 Prep Batch: 437005
Bis(2-chloroethoxy)methane ND 10.0 4.101 ug/L 41 33-170
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Bis(2-chloroethyl)ether ND 10.0 3.140 ug/L 31 12-158
1-Methylnaphthalene 0.370 F1 10.0 3.781 F1 ug/L 34 58-100
2,2'-oxybis[1-chloropropane]ND 10.0 3.746 ug/L 37 36-166
Bis(2-ethylhexyl) phthalate ND 10.0 6.449 J ug/L 64 10-158
4-Bromophenyl phenyl ether ND F1 10.0 4.395 F1 ug/L 44 53-127
Butyl benzyl phthalate 0.706 J 10.0 5.242 ug/L 45 10-152
2-Chloronaphthalene ND F1 10.0 3.393 F1 ug/L 34 60-120
4-Chlorophenyl phenyl ether ND 10.0 4.414 ug/L 44 25-158
Chrysene ND 10.0 4.537 ug/L 45 17-168
Dibenz(a,h)anthracene ND 10.0 4.485 ug/L 45 10-170
3,3'-Dichlorobenzidine ND F1 10.0 ND F1 ug/L 0 10-170
Diethyl phthalate ND 10.0 4.232 ug/L 42 10-120
Di-n-octyl phthalate ND 10.0 4.196 ug/L 42 10-146
1,2-Diphenylhydrazine(as
Azobenzene)
ND F1 10.0 3.867 F1 ug/L 39 46-103
2-Methylnaphthalene 0.361 F1 10.0 3.778 F1 ug/L 34 58-100
Fluoranthene ND 10.0 4.206 ug/L 42 26-137
2-Methylphenol ND F1 10.0 4.264 F1 ug/L 43 55-101
Fluorene ND F1 10.0 3.985 F1 ug/L 40 59-121
Hexachlorobenzene ND 10.0 3.981 ug/L 40 10-152
Hexachlorobutadiene ND F1 10.0 1.784 F1 ug/L 18 24-120
Hexachlorocyclopentadiene ND F1 10.0 ND F1 ug/L 0 41-106
Hexachloroethane ND F1 10.0 1.440 F1 ug/L 14 40-120
Indeno[1,2,3-cd]pyrene ND 10.0 4.282 ug/L 43 10-170
Isophorone ND 10.0 4.539 ug/L 45 21-170
Naphthalene 2.15 10.0 6.223 ug/L 41 21-133
Nitrobenzene ND 10.0 3.789 ug/L 38 35-170
N-Nitrosodimethylamine ND F1 10.0 4.043 F1 ug/L 40 48-109
N-Nitrosodi-n-propylamine ND 10.0 4.495 ug/L 45 10-170
4-Chloroaniline ND F1 10.0 2.376 F1 ug/L 24 50-100
Phenanthrene 0.104 J F1 10.0 4.313 F1 ug/L 42 54-120
Pyrene ND F1 10.0 4.937 F1 ug/L 49 52-120
4-Methylphenol ND F1 10.0 4.333 F1 ug/L 43 56-102
Pentachlorophenol ND 20.0 7.469 ug/L 37 17-170
Phenol ND 10.0 3.468 ug/L 35 10-120
1,2,4-Trichlorobenzene ND F1 10.0 2.138 F1 ug/L 21 44-142
2,4-Dichlorophenol ND 10.0 4.455 ug/L 45 39-135
2,4-Dinitrophenol ND 20.0 8.690 J ug/L 43 10-170
2,4-Dimethylphenol ND 10.0 3.738 ug/L 37 32-120
2,4,6-Trichlorophenol ND 10.0 4.621 ug/L 46 37-144
2-Chlorophenol ND 10.0 3.721 ug/L 37 23-134
2-Nitrophenol ND 10.0 4.577 ug/L 46 29-170
4,6-Dinitro-2-methylphenol ND 20.0 9.164 ug/L 46 10-170
4-Chloro-3-methylphenol ND 10.0 5.470 ug/L 55 22-147
4-Nitrophenol ND 20.0 7.566 ug/L 38 10-132
Benzoic acid ND 10.0 4.960 J ug/L 50 32-118
Benzyl alcohol ND 10.0 4.020 ug/L 40 24-117
Dibenzofuran ND F1 10.0 3.956 F1 ug/L 40 57-100
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: EPA 625.1 - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)32 -127
Surrogate
59
MS MS
Qualifier Limits%Recovery
572-Fluorobiphenyl 47 -107
532-Fluorophenol (Surr)35 -109
69Nitrobenzene-d5 (Surr)47 -110
56Phenol-d5 (Surr)37 -110
65Terphenyl-d14 (Surr)32 -115
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-384264/20
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384264
RL MDL
C5-C8 Aliphatics (unadjusted)ND 100 25.0 ug/L 06/08/23 21:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10.0100 ug/L 06/08/23 21:39 1C9-C10 Aromatics
ND 25.0100 ug/L 06/08/23 21:39 1C9-C12 Aliphatics (unadjusted)
ND 25.0100 ug/L 06/08/23 21:39 1C9-C12 Aliphatics (adjusted)
ND 25.0100 ug/L 06/08/23 21:39 1C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)108 70-130 06/08/23 21:39 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 06/08/23 21:39 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-384264/21
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384264
C5-C8 Aliphatics (unadjusted)151 150.8 ug/L 100 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 50.2 47.04 J ug/L 94 70-130
C9-C12 Aliphatics (unadjusted)151 133.8 ug/L 89 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
108
LCS LCS
Qualifier Limits%Recovery
98a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-384264/22
Matrix: Water Prep Type: Total/NA
Analysis Batch: 384264
C5-C8 Aliphatics (unadjusted)151 147.4 ug/L 98 70-130 2 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 50.2 46.31 J ug/L 92 70-130 2 25
C9-C12 Aliphatics (unadjusted)151 133.1 ug/L 88 70-130 1 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
108
LCSD LCSD
Qualifier Limits%Recovery
97a,a,a-Trifluorotoluene (pid)70 -130
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-385316/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 385316
RL MDL
C5-C8 Aliphatics (unadjusted)ND 100 25.0 ug/L 06/12/23 10:07 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10.0100 ug/L 06/12/23 10:07 1C9-C10 Aromatics
ND 25.0100 ug/L 06/12/23 10:07 1C9-C12 Aliphatics (unadjusted)
ND 25.0100 ug/L 06/12/23 10:07 1C9-C12 Aliphatics (adjusted)
ND 25.0100 ug/L 06/12/23 10:07 1C5-C8 Aliphatics (adjusted)
a,a,a-Trifluorotoluene (fid)109 70-130 06/12/23 10:07 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 06/12/23 10:07 1a,a,a-Trifluorotoluene (pid)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-385316/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 385316
C5-C8 Aliphatics (unadjusted)151 147.6 ug/L 98 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C10 Aromatics 50.2 45.69 J ug/L 91 70-130
C9-C12 Aliphatics (unadjusted)151 132.4 ug/L 88 70-130
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
109
LCS LCS
Qualifier Limits%Recovery
97a,a,a-Trifluorotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-385316/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 385316
C5-C8 Aliphatics (unadjusted)151 148.0 ug/L 98 70-130 0 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C10 Aromatics 50.2 45.98 J ug/L 92 70-130 1 25
C9-C12 Aliphatics (unadjusted)151 134.3 ug/L 89 70-130 1 25
a,a,a-Trifluorotoluene (fid)70 -130
Surrogate
109
LCSD LCSD
Qualifier Limits%Recovery
97a,a,a-Trifluorotoluene (pid)70 -130
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-385076/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
RL MDL
C19-C36 Aliphatics ND 50.0 50.0 ug/L 06/09/23 19:11 06/27/23 02:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 30.030.0 ug/L 06/09/23 19:11 06/27/23 02:30 1C9-C18 Aliphatics
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 410-385076/1-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
1-Chlorooctadecane (Surr)59 40-140 06/27/23 02:30 1
MB MB
Surrogate
06/09/23 19:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 410-385076/1-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390845 Prep Batch: 385076
RL MDL
C11-C22 Aromatics (unadjusted)ND 40.0 40.0 ug/L 06/09/23 19:11 06/27/23 02:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 40.040.0 ug/L 06/09/23 19:11 06/27/23 02:30 1C11-C22 Aromatics (Adjusted)
2-Fluorobiphenyl (Surr)79 40-140 06/27/23 02:30 1
MB MB
Surrogate
06/09/23 19:11
Dil FacPreparedAnalyzedQualifierLimits%Recovery
64 06/09/23 19:11 06/27/23 02:30 1o- terphenyl (Surr)40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-385076/2-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
C19-C36 Aliphatics 321 191.4 ug/L 60 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
C9-C18 Aliphatics 241 157.7 ug/L 65 40-140
1-Chlorooctadecane (Surr)40 -140
Surrogate
54
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-385076/2-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390845 Prep Batch: 385076
C11-C22 Aromatics (unadjusted)681 480.1 ug/L 70 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Fluorobiphenyl (Surr)40 -140
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
77o- terphenyl (Surr)40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-385076/3-B
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390861 Prep Batch: 385076
C19-C36 Aliphatics 321 195.7 ug/L 61 40-140 2 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
C9-C18 Aliphatics 241 158.1 ug/L 66 40-140 0 25
1-Chlorooctadecane (Surr)40 -140
Surrogate
60
LCSD LCSD
Qualifier Limits%Recovery
Eurofins Pittsburgh
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QC Sample Results
Job ID: 180-157472-1Client: Altec Industries, Inc
SDG: 640 Rock LaneProject/Site: China Grove NC
Method: MAEPH2.1 - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-385076/3-C
Matrix: Water Prep Type: Total/NA
Analysis Batch: 390845 Prep Batch: 385076
C11-C22 Aromatics (unadjusted)681 448.9 ug/L 66 40-140 7 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Fluorobiphenyl (Surr)40 -140
Surrogate
83
LCSD LCSD
Qualifier Limits%Recovery
75o- terphenyl (Surr)40 -140
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-157472-1
SDG Number: 640 Rock Lane
Login Number: 157472
Question Answer Comment
Creator: Watson, Debbie
List Source: Eurofins Pittsburgh
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Pittsburgh
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Login Sample Receipt Checklist
Client: Altec Industries, Inc Job Number: 180-157472-1
SDG Number: 640 Rock Lane
Login Number: 157472
Question Answer Comment
Creator: McCaskey, Jonathan
List Source: Eurofins Lancaster Laboratories Environment Testing, LLC
List Creation: 06/06/23 12:05 PMList Number: 2
N/AThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
TrueVOA sample vials do not have headspace >6mm in diameter (none, if from
WV)?
Eurofins Pittsburgh
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