MO-30136_49192_CA_IAR_20230831

INITIAL ABATEMENT ACTION REPORT

416 Winecoff Street
Troutman, NC 28166

SUMMIT PROJECT NO. 2944.E0003

Prepared For:
North Carolina Department of Environmental Quality
UST Section
Mooresville Regional Office

Prepared By:
SUMMIT Engineering, Laboratory & Testing, Inc.
10121 Pineville Distribution Street
Pineville, NC 28134
[phone]

August 31, 2023

I, Michael D. Zavislak, NRCC-EAC, CHMM, CIH, PE, a Professional
Engineer for SUMMIT, do certify that the information contained in
this report is correct and accurate to the best of my knowledge.
Michael D. Zavislak, NRCC-EAC, CHMM, CIH, PE
SUMMIT Engineering, Laboratory & Testing, Inc. SUMMIT Engineering, Laboratory & Testing, Inc. is licensed to practice engineering in the State
of North Carolina.

The certification number of SUMMIT Engineering, Laboratory & Testing, Inc. is C-4361.
UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

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TABLE OF CONTENTS
1.0 TANK CLOSURE REPORT .................................................................................................... 1
A. SITE INFORMATION ...................................................................................................................... 1
A.1. Site Identification .............................................................................................................. 1
A.2. Contact Information .......................................................................................................... 1
A.3. Release Information .......................................................................................................... 2
A.4. Certification ...................................................................................................................... 2
B. SITE HISTORY AND CHARACTERIZATION .............................................................................. 2
B.1. UST Owner and Information ............................................................................................ 2
B.2. UST Information ............................................................................................................... 2
B.3. Non-UST Information ...................................................................................................... 3
B.4. Release Information .......................................................................................................... 3
B.5. Site Characteristics ........................................................................................................... 4
C. SITE CHECK ..................................................................................................................................... 4
D. CHANGE IN SERVICE .................................................................................................................... 4
E. FREE PRODUCT INVESTIGATION .............................................................................................. 4
F. GROUNDWATER AND SURFACE WATER INVESTIGATION .................................................. 4
G. INITIAL RESPONSE AND ABATEMENT ACTION ..................................................................... 4
G.1. Notification ....................................................................................................................... 4
H. EXCAVATION OF CONTAMINATED SOIL .................................................................................. 5
H.1. Initial Investigation ........................................................................................................... 5
H.2. Excavation ........................................................................................................................ 5
H.3. Post Excavation Sampling ................................................................................................ 6
H.4 Soil Investigation .............................................................................................................. 7
H.5. Disposal............................................................................................................................. 8
H.6. Conclusions and Recommendations ................................................................................. 8
I. CONCLUSIONS................................................................................................................................ 8
UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

ii

APPENDICES
FIGURES
Figure 1.0 Topographic Map
Figure 2.0 Site Map
Figure 3.0 Sampling Map
Figure 3.1 Cross Sectional Sampling Map
Figure 4.0 Aerial Photograph
NRCS Soil Survey
Site Photographs

TABLES
Table B-1
Table B-2
Table B-3
Table B-4
APPENDIX C: UST-61 24-Hour Notice of Release
APPENDIX E: Certificate of UST Disposal
APPENDIX H: Waste Manifests/Weight Tickets
APPENDIX I: Chain of Custody
APPENDIX J: Analytical Results

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

1
1.0 TANK CLOSURE REPORT

A. SITE INFORMATION

A.1. Site Identification

Date of Report: August 31, 2023
Facility ID: N/A
Incident Number: Unknown
Site Rank: N/A
Site Name: Winecoff Village
Site Street Address: 416 Winecoff Street
Troutman, NC 28166
Geographic Data Point: Tank Basin
Location Method: GPS
Latitude: 35°42’14.75” N
Longitude: -80°52’53.96” W

A.2. Contact Information

Property Owner: Winecoff Development Partners, LLC
236 Raceway Drive
Mooresville, NC 28117

Property Occupant: Vacant

Consultant: SUMMIT Engineering, Laboratory & Testing, Inc.
10121 Pineville Distribution Street
Pineville, NC 28134
[phone]
North Carolina Professional Engineer’s License Number: C-4361

Laboratory: Waypoint Analytical, LLC
449 Springbok Road
Charlotte, NC 28217
UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

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[phone]
State of North Carolina Certification Number: 402

A.3. Release Information

Date Discovered: April 26, 2023
Estimated Release: Unknown
Cause of Release: Unknown
Source of Release: UST
Size and Contents: 3.5’ x 5’ x 2.25’ – Fuel Oil

A.4. Certification

See Cover Page.

B. SITE HISTORY AND CHARACTERIZATION

B.1. UST Owner and Information
Table B-2: Site History - Owner and Operator Information

ID Number UST-1 Facility ID Number N/A
Name of Owner

Dates of Operation
(mm/dd/yy to mm/dd/yy)
Winecoff Development Partners, LLC Unknown
Street Address
PO Box 3965
City State Zip Telephone Number
Mooresville NC 28117
Name of Operator Dates of Operation
(mm/dd/yy to mm/dd/yy)
N/A Unknown
Street Address

City State Zip Telephone Number

B.2. UST Information
Table B-1: Site History – System Information
UST ID
Number
Current
/Last
Contents
Previous
Contents
Capacity
(in
gallons)
Construction
Details
Tank
Dimensions
Description
of
Associated
Piping and
Pumps
Date Tank
Installed
Status
of
UST
Was
release
associated
with the
UST
System?
UST-1 Fuel
Oil/Water
N/A ~275 Steel 3.5’ x 5’ x
2.25’
unknown unknown removed Yes

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

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B.3. Non-UST Information

There are no other USTs, ASTs, piping and/or dispensers located on the site. There are no historical
compliance issues.

B.4. Release Information

SUMMIT was retained by the property owner to direct the removal of an onsite UST.

On April 26, 2023, initial removal and abatement actions began for an onsite Fuel Oil UST. The
tank was discovered following demolition activities and during site preparation activities for new
construction. The removal contractor, Landcrafters USA, indicated that an unknown amount of
liquids had been removed / pumped from the UST prior to the initiation of tank closure.

On May 1, 2023, the UST removal continued with the contractor, Landcrafters USA. The
contractor removed the UST and excavated soils were stockpiled on a plastic liner adjacent to the
UST excavation. During excavation, soils beneath the UST exhibited soil staining, odors, and
positive detections of field screening equipment (IAQRAE Indoor Air Quality Monitor w/VOC
measurement). Following these activities, the excavation measured approximately 7’ x 5’ x 8’
(LxWxD).

Due to exceedances reported in laboratory results, on May 10, 2023, SUMMIT arrived onsite for
the continuation of the excavation of contaminated soils. Previously stockpiled soils and newly
excavated soils continued to be stockpiled onsite on plastic lining. An additional 1 foot was
excavated from the north, east, and south sidewalls and approximately 2 feet was excavated from
the bottom.

Due to continued exceedances reported in laboratory results, on June 12, 2023, SUMMIT arrived
onsite for the continuation of the excavation of contaminated soils. Previously stockpiled soils and
newly excavated soils continued to be stockpiled onsite on plastic lining. An additional 1 foot was
excavated from the east sidewall and approximately 1 foot was excavated from the bottom.
Contractor then backfilled and compacted with clean fill to grade. The final excavation measured
approximately 7’ x 9’ x 11’ (LxWxD).

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

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Contractor then backfilled and compacted with clean fill to grade. The final excavation measured
approximately 7’ x 9’ x 11’ (LxWxD). Approximately 57 tons of contaminated soils were
stockpiled onsite on poly. The contaminated soils were transported to the EVO Corporation facility
in Winston Salem, NC on August 25, 2023.

B.5. Site Characteristics

The United States Geological Survey (USGS) “Troutman, North Carolina, United States”
topographic quadrangle map was reviewed. According to the contour lines on the topographic
maps, the elevation of the subject site is approximately 885 feet above Mean Sea Level (MSL). The
inferred groundwater flow direction based on topography appears to be to the east towards an
unnamed creek.

This site contains the soil types:

CgC—Cecil-Urban land complex, 2 to 10 percent slopes

The surface cover of the UST basin was soil.

C. SITE CHECK

Not Applicable.

D. CHANGE IN SERVICE

Not Applicable.

E. FREE PRODUCT INVESTIGATION

Not applicable.

F. GROUNDWATER AND SURFACE WATER INVESTIGATION

Not applicable.

G. INITIAL RESPONSE AND ABATEMENT ACTION

G.1. Notification

SUMMIT was retained by the property owner to direct the removal of an onsite UST.

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023
5
On April 26, 2023, initial removal and abatement actions began for an onsite Fuel Oil UST. The
tank was discovered following demolition activities and during site preparation activities for new
construction. The removal contractor, Landcrafters USA, indicated that an unknown amount of
liquids had been removed / pumped from the UST prior to the initiation of tank closure.
H.EXCAVATION OF CONTAMINATED SOIL
H.1. Initial Investigation
SUMMIT was retained by the property owner to direct the removal of an onsite UST.
On April 26, 2023, initial removal and abatement actions began for an onsite Fuel Oil UST. The
tank was discovered following demolition activities and during site preparation activities for new
construction. The removal contractor, Landcrafters USA, indicated that an unknown amount of
liquids had been removed / pumped from the UST prior to the initiation of tank closure.
H.2. Excavation
On April 26, 2023, initial removal and abatement actions began for an onsite Fuel Oil UST.
The tank was discovered following demolition activities and during site preparation activities for
new construction. The removal contractor, Landcrafters USA, indicated that an unknown amount of
liquids had been removed / pumped from the UST prior to the initiation of tank closure.
On May 1, 2023, the UST removal continued with the contractor, Landcrafters USA. The
contractor removed the UST and excavated soils were stockpiled on a plastic liner adjacent to the
UST excavation. During excavation, soils beneath the UST exhibited soil staining, odors, and
positive detections of field screening equipment (IAQRAE Indoor Air Quality Monitor w/VOC
measurement). Following these activities, the excavation measured approximately 7’ x 5’ x 8’
(LxWxD).
Due to exceedances reported in laboratory results, on May 10, 2023, SUMMIT arrived onsite for
the continuation of the excavation of contaminated soils. Previously stockpiled soils and newly
excavated soils continued to be stockpiled onsite on plastic lining. An additional 1 foot was
excavated from the north, east, and south sidewalls and approximately 2 feet was excavated from
the bottom.
UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

6
Due to continued exceedances reported in laboratory results, on June 12, 2023, SUMMIT arrived
onsite for the continuation of the excavation of contaminated soils. Previously stockpiled soils and
newly excavated soils continued to be stockpiled onsite on plastic lining. An additional 1 foot was
excavated from the east sidewall and approximately 1 foot was excavated from the bottom.
Contractor then backfilled and compacted with clean fill to grade. The final excavation measured
approximately 7’ x 9’ x 11’ (LxWxD).

H.3. Post Excavation Sampling

Following the initial excavation, on May 1, 2023, SUMMIT collected one (1) soil sample from the
bottom of the existing excavation (designated Bottom), four (4) soil samples from the sidewalls of
the tank basin (SW-1 to SW-4), and one (1) from the stockpiled soils (Tank). The sidewall samples
were collected at approximately four (4) feet from the top of the excavation. The bottom sample
was collected approximately eight (8) feet from the top of the excavation at the center of the tank
basin excavation. Samples were submitted for VOC, SVOC and EPH/DPH analysis in accordance
with DEQ guidance. Sample results indicated elevated EPH in the base area of the excavation and
on the sidewalls.

On May 10, 2023, SUMMIT collected one (1) soil sample from the north sidewall (SW-1-A) of the
tank basin excavation and one (1) soil sample from the base of the excavation (Bottom-A). The
sidewall sample was collected at approximately five (5) feet from the top of the excavation. The
bottom sample was collected approximately ten (10) feet from the top of the excavation at the center
of the tank basin excavation. Samples were submitted for EPH to reevaluate EPH exceedances
following additional excavation.

On June 12, 2023, SUMMIT collected one (1) soil sample from the east sidewall (SW-2-A) of the
tank basin excavation and one (1) soil sample from the base of the excavation (Bottom-B). The
sidewall sample was collected at approximately six (6) feet from the top of the excavation. The
bottom sample was collected approximately eleven (10) feet from the top of the excavation at the
center of the tank basin excavation. Samples were submitted for EPH to reevaluate EPH
exceedances following additional excavation. Figures 3A and 3B document the location of the
samples collected.

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

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Table B-4: Summary of Soil Sampling Results
Analytical Method (e.g., VOC by EPA 8260) 8260 8270 EPH VPH
Contaminant of Concern

Sample ID Date
Collected
(mm/dd/yy)

Source Area
(eg. Tank
pt 1)

Sample
Depth
(ft BGS)

Incident
Phase
(Closure,
20Day,
LSA, etc.)

SW-1 5/1/2023 sidewall 4 Closure BRL BRL Exceed BRL
SW-2 5/1/2023 sidewall 4 Closure BRL BRL Exceed BRL
SW-3 5/1/2023 sidewall 4 Closure BRL BRL BRL BRL
SW-4 5/1/2023 sidewall 4 Closure BRL BRL BRL BRL
Bottom 5/1/2023 bottom 8 Closure BRL BRL Exceed BRL
SW-1-A 5/10/2023 sidewall 5 Closure BRL BRL BRL BRL
Bottom-A 5/10/2023 bottom 10 Closure BRL BRL Exceed BRL
SW-2-A 6/12/2023 sidewall 6 Closure BRL BRL BRL BRL
Bottom-B 6/12/2023 bottom 11 Closure BRL BRL BRL BRL
Soil to groundwater MSCC (mg/kg)

BRL BRL BRL BRL
Residential MSCC (mg/kg)

BRL BRL BRL BRL
Industrial/Commercial MSCC (mg/kg)

BRL BRL BRL BRL

Indicate method detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
Results must be reported in ug/l
ug/l =micrograms per liter
GCL = gross contamination level

H.4 Soil Investigation

New, clean disposable latex gloves were used for the collection of each soil or groundwater sample.
Samples collected for laboratory analyses were placed in laboratory-supplied containers with the
sampler’s name, time and date the sample was collected, and laboratory analyses to be performed.
The samples were packed on ice and taken to Waypoint Analytical in Charlotte, North Carolina. For
a drawing detailing the locations of the soil samples, please refer to Figure 3.0 in the appendices.
Groundwater was not encountered in the excavation. The samples were grab samples. Standard
chain-of-custody procedures were followed.

Field screening was based on visual and olfactory observations. In addition, soil samples were
taken from the excavation and were analyzed onsite using an IAQRAE Indoor Air Quality Monitor
w/ VOC Measurement. Prior to each analysis, the IAQRAE was allowed to equilibrate to the area
temperature and ambient air conditions.
UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

8
H.5. Disposal

Approximately 57 tons of contaminated soils were stockpiled onsite on poly. The contaminated
soils were transported to the EVO Corporation facility in Winston Salem, NC on August 25, 2023.
Manifests and weigh tickets are presented in Appendix H.

H.6. Conclusions and Recommendations

After the contaminated soils were excavated, the soil contamination levels were not above the
regulatory levels for Soil to Groundwater MSCC.

No free product was encountered. Groundwater was not encountered.

I. Conclusions

Based on the concentrations of the analytical results reported in the soil samples collected, no
further assessment is recommended.
UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

18

FIGURES
D:\!Michael!\!SUMMIT!\2944 - Nest Communities\2944.E0003 - Winecoff\Phase I ESA\Report Files\Ph I - Figure 1 - Topo.doc

SUMMIT ELT, Inc.

Project: 2944.E0003

Figure 1

USGS Topographic Map

Winecoff Village

Troutman, NC
Subject Property N
D:\!Michael!\!SUMMIT!\2944 - Nest Communities\2944.E0003 - Winecoff\Phase I ESA\Report Files\Ph I - Figure 3 - Site Map.doc

SUMMIT ELT, Inc.

Project: 2944.E0003

Figure 2

Site Map

Winecoff Village

Troutman, NC
N
D:\!Michael!\!SUMMIT!\2944 - Nest Communities\2944.E0003 - Winecoff\Phase I ESA\Report Files\Ph I - Figure 2 - Aerial Map.doc

SUMMIT ELT, Inc.

Project: 2944.E0003

Figure 4

Aerial Photograph

Winecoff Village

Troutman, NC
Subject Property
N
M
ed
416 Winecoff St
Sampling Location Plan
Figure 3A
Site Plan
SW-2A
SW-1A
SW-2SW-4
N
UST
(3.5x5x2.25)
0'5'2'
Bottom
SW-3A
Final Limits of
Excavation
(7x9x11)
Initial Limit of
Excavation (5x7x8)
SW-3
SW-1
To Winecoff St
M
ed
6'5'4'3'2'1'0'
0'
0.5'
1'
2'
3'
4'
5'
6'
7'
8'
9'
10'
11"
Figure 3B
Cross-Section
416 Winecoff St
Cross-Section Plan
Bottom
SW-2
0'2.5'1'
SW-4SW-1
Final Limits of
Excavation
Initial Limit of
Excavation
West End of
UST -
3.5'x5'x2.25'
Ground Surface
Bottom-A
Bottom-B
D:\!Michael!\!SUMMIT!\2944 - Nest Communities\2944.E0003 - Winecoff\Phase I ESA\Report Files\Ph I - Figure 2 - Aerial Map.doc

SUMMIT ELT, Inc.

Project: 2944.E0003

Figure 4

Aerial Photograph

Winecoff Village

Troutman, NC
Subject Property
N
Soil Map—Iredell County, North Carolina
Natural Resources
Conservation Service
Web Soil Survey
National Cooperative Soil Survey
7/23/2021
Page 1 of 3
39
5
1
0
0
0
39
5
1
0
8
0
39
5
1
1
6
0
39
5
1
2
4
0
39
5
1
3
2
0
39
5
1
4
0
0
39
5
1
4
8
0
39
5
1
0
0
0
39
5
1
0
8
0
39
5
1
1
6
0
39
5
1
2
4
0
39
5
1
3
2
0
39
5
1
4
0
0
39
5
1
4
8
0
510550 510630 510710 510790 510870 510950 511030 511110 511190 511270
510550 510630 510710 510790 510870 510950 511030 511110 511190 511270
35° 42' 25'' N
80
°

5
3
'

0
'
'

W
35° 42' 25'' N
80
°

5
2
'

3
0
'
'

W
35° 42' 9'' N
80
°

5
3
'

0
'
'

W
35° 42' 9'' N
80
°

5
2
'

3
0
'
'

W
N
Map projection: Web Mercator Corner coordinates: WGS84 Edge tics: UTM Zone 17N WGS84
0 150 300 600 900Feet
0 50 100 200 300Meters
Map Scale: 1:3,470 if printed on A landscape (11" x 8.5") sheet.
Soil Map may not be valid at this scale.
MAP LEGEND MAP INFORMATION
Area of Interest (AOI)
Area of Interest (AOI)
Soils
Soil Map Unit Polygons
Soil Map Unit Lines
Soil Map Unit Points
Special Point Features
Blowout
Borrow Pit
Clay Spot
Closed Depression
Gravel Pit
Gravelly Spot
Landfill
Lava Flow
Marsh or swamp
Mine or Quarry
Miscellaneous Water
Perennial Water
Rock Outcrop
Saline Spot
Sandy Spot
Severely Eroded Spot
Sinkhole
Slide or Slip
Sodic Spot
Spoil Area
Stony Spot
Very Stony Spot
Wet Spot
Other
Special Line Features
Water Features
Streams and Canals
Transportation
Rails
Interstate Highways
US Routes
Major Roads
Local Roads
Background
Aerial Photography
The soil surveys that comprise your AOI were mapped at
1:12,000.
Warning: Soil Map may not be valid at this scale.
Enlargement of maps beyond the scale of mapping can cause
misunderstanding of the detail of mapping and accuracy of soil
line placement. The maps do not show the small areas of
contrasting soils that could have been shown at a more detailed
scale.
Please rely on the bar scale on each map sheet for map
measurements.
Source of Map: Natural Resources Conservation Service
Web Soil Survey URL:
Coordinate System: Web Mercator (EPSG:3857)
Maps from the Web Soil Survey are based on the Web Mercator
projection, which preserves direction and shape but distorts
distance and area. A projection that preserves area, such as the
Albers equal-area conic projection, should be used if more
accurate calculations of distance or area are required.
This product is generated from the USDA-NRCS certified data as
of the version date(s) listed below.
Soil Survey Area: Iredell County, North Carolina
Survey Area Data: Version 25, Jun 4, 2020
Soil map units are labeled (as space allows) for map scales
1:50,000 or larger.
Date(s) aerial images were photographed: Nov 17, 2019—Dec
18, 2019
The orthophoto or other base map on which the soil lines were
compiled and digitized probably differs from the background
imagery displayed on these maps. As a result, some minor
shifting of map unit boundaries may be evident.
Soil Map—Iredell County, North Carolina
Natural Resources
Conservation Service
Web Soil Survey
National Cooperative Soil Survey
7/23/2021
Page 2 of 3
Map Unit Legend
Map Unit Symbol Map Unit Name Acres in AOI Percent of AOI
CeB2 Cecil sandy clay loam, 2 to 6
percent slopes, moderately
eroded
2.6 6.7%
CeC2 Cecil sandy clay loam, 6 to 10
percent slopes, moderately
eroded
6.1 15.9%
CgC Cecil-Urban land complex, 2 to
10 percent slopes
5.6 14.6%
CgE Cecil-Urban land complex, 10
to 25 percent slopes
1.6 4.1%
ChA Chewacla loam, 0 to 2 percent
slopes, frequently flooded
1.0 2.6%
PaF Pacolet sandy loam, 25 to 45
percent slopes
4.8 12.7%
PcC2 Pacolet sandy clay loam, 6 to
10 percent slopes,
moderately eroded
3.1 8.0%
PcD2 Pacolet sandy clay loam, 10 to
15 percent slopes,
moderately eroded
10.5 27.4%
ScD Spartanburg-Cecil-Bethlehem
complex, 8 to 15 percent
slopes, stony
2.4 6.3%
WaA Warne loam, 0 to 2 percent
slopes, occasionally flooded
0.7 1.7%
Totals for Area of Interest 38.2 100.0%
Soil Map—Iredell County, North Carolina
Natural Resources
Conservation Service
Web Soil Survey
National Cooperative Soil Survey
7/23/2021
Page 3 of 3
UST Initial Abatement Action Report – 416 Winecoff St SUMMIT Project No. 2944.E0003
Troutman, North Carolina August 31, 2023

1
SITE PHOTOGRAPHS
View of excavation – 5/1/23.

View of excavation – 5/10/23.
UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, NC August 31, 2023

TABLES

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, NC August 31, 2023

Table B-1: Site History – System Information

AST ID
Number
Current
/Last
Contents
Previous
Contents
Capacity
(in
gallons)
Construction
Details
Tank
Dimensions
Description
of
Associated
Piping and
Pumps
Date
Tank
Installed
Status of
UST
Was
release
associated
with the
UST
System?
UST-1 Fuel
Oil/Water
N/A ~275 Steel 3.5’ x 5’ x
2.25’
unknown unknown removed Yes

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, NC August 31, 2023

Table B-2: Site History - Owner and Operator Information

ID Number UST-1 Facility ID Number N/A
Name of Owner

Dates of Operation
(mm/dd/yy to mm/dd/yy)
Winecoff Development Partners, LLC Unknown to Unknown
Street Address
PO Box 3965
City State Zip Telephone Number
Mooresville NC 283117
Name of Operator Dates of Operation
(mm/dd/yy to mm/dd/yy)
N/A Unknown to Unknown
Street Address

City State Zip Telephone Number

Page 1 of 2
Date:8/31/2023 Winecoff St, Troutman (2944.E0003)
8260 8260 8260 8260 8260 8270 8270 8270 8270 8270 8270 8270
Sample ID Date Source
Depth
('bgs)
Incident
Phase
SW-1 5/1/2023 N. Wall 4 0.059 <0.0008 <0.0006 NT <0.0007 <0.186 <0.180 <0.191 <0.190 <0.177 <0.178 <0.184
SW-2 5/1/2023 E. Wall 4 0.025 <0.0008 <0.0006 NT <0.0007 <0.186 <0.180 <0.191 <0.190 <0.177 <0.178 <0.184
SW-3 5/1/2023 S. Wall 4 0.007 <0.0008 <0.0006 NT <0.0007 <0.186 <0.180 <0.191 <0.190 <0.177 <0.178 <0.184
SW-4 5/1/2023 W. Wall 4 0.012 <0.0008 <0.0006 NT <0.0007 <0.186 <0.180 <0.191 <0.190 <0.177 <0.178 <0.184
Bottom 5/1/2023 Base Center 8 0.02 J 0.001 J 0.001 J NT 0.006 J <0.186 <0.180 <0.191 <0.190 <0.177 <0.178 <0.184
SW-1-A 5/10/2023 N. Wall 5 NT NT NT NT NT NT NT NT NT NT NT NT
Bottom-A 5/10/2023 Base Center 10 NT NT NT NT NT NT NT NT NT NT NT NT
SW-2-A 6/12/2023 E. Wall 6 NT NT NT NT NT NT NT NT NT NT NT NT
SW-3-A 6/12/2023 S. Wall 6 NT NT NT NT NT NT NT NT NT NT NT NT
Bottom-B 6/12/2023 Base Center 11 NT NT NT NT NT NT NT NT NT NT NT NT
0.003 0.0008 0.0006 0.002 0.0007 0.186 0.180 0.191 0.190 0.177 0.178 0.184
24 8 1.3 NA 6 640 0.17 0.058 0.6 7600 5.8 18
14000 60.3 1560 NA 3120 4600 6.6 0.66 6.6 469 66 663
210000 297 2330 NA 46700 70000 32 3.2 32 7000 327 3270
<# = Below Method Detection Limit
BOLD = Concentration Above Reference Values
J = Estimated Concentration
Q = Surrogate Failure
NT = Not Tested
Table B-3 Summary of Soil Sample Results
Industrial/Commercial MSCC (mg/kg)
Be
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Be
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Residential MSCC (mg/kg)
Soil to Groundwater MSCC (mg/kg)
Minimum Reporting Limit (mg/kg)
Ac
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(
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All Values in mg/kg
Incident Number and Name:Facility ID:#:Not Assigned
IAA Tank
Closure
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Page 1 Table B-3 SUMMIT - Skibo Rd (8470.E0001)
Page 2 of 2
Date:8/31/2023 Winecoff St, Troutman (2944.E0003)
8270 8270 8270 8270 8270 8270 8270 8270 VPH/EPH VPH/EPH VPH/EPH VPH/EPH
Sample ID Date Source
Depth
('bgs)
Incident
Phase
SW-1 5/1/2023 N. Wall 4 <0.160 <0.166 <0.233 <0.130 <0.187 <0.270 3.31 NT <1.69 3750 1320 2790
SW-2 5/1/2023 E. Wall 4 <0.160 <0.166 <0.233 <0.130 <0.187 <0.270 <0.186 NT <1.69 83.5 52.8 77.8
SW-3 5/1/2023 S. Wall 4 <0.160 <0.166 <0.233 <0.130 <0.187 <0.270 <0.186 NT <1.69 42.9 21.3 24
SW-4 5/1/2023 W. Wall 4 <0.160 <0.166 <0.233 <0.130 <0.187 <0.270 <0.186 NT <1.66 <11.8 <15.7 <18.3
Bottom 5/1/2023 Base Center 8 <0.160 <0.166 <0.233 <0.130 <0.187 <0.270 0.324 J NT 1.71 J 3410 970 J 2970
SW-1-A 5/10/2023 N. Wall 5 NT NT NT NT NT NT NT NT NT <9.92 <13.2 <15.3
Bottom-A 5/10/2023 Base Center 10 NT NT NT NT NT NT NT NT NT 294 98.3 J 214
SW-2-A 6/12/2023 E. Wall 6 NT NT NT NT NT NT NT NT NT <10.9 <14.5 <16.9
SW-3-A 6/12/2023 S. Wall 6 NT NT NT NT NT NT NT NT NT <12.3 <16.3 <19.0
Bottom-B 6/12/2023 Base Center 11 NT NT NT NT NT NT NT NT NT <11.7 <15.6 <18.1
0.160 0.166 0.233 0.130 0.187 0.270 0.186 0.063 1.66 9.92 13.2 15.3
330 55 1.9 1.5 1.5 0.22 210 NA 68 540 NA 31
625 625 6.63 62.5 62.5 4690 469 NA 939 1500 31000 469
9340 9340 32.7 934 934 70000 7000 NA 24528 40000 810000 12264
<# = Below Method Detection Limit
BOLD = Concentration Above Reference Values
J = Estimated Concentration
Q = Surrogate Failure
NT = Not Tested
Soil to Groundwater MSCC (mg/kg)
Table B-3 Summary of Soil Sample Results
Flu
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Industrial/Commercial MSCC (mg/kg)
All Values in mg/kg
Not Assigned Facility ID:#:Incident Number and Name:
C5
-
C
8

A
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a
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C9
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C
1
8

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9
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6

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Minimum Reporting Limit (mg/kg)
IAA Tank
Closure
Residential MSCC (mg/kg)
1,1
-
B
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l
Page 2 Table B-3 SUMMIT - Skibo Rd (8470.E0001)
UST Closure Report SUMMIT Project No. 8470.E0001
1931 Skibo Road, Fayetteville, NC July 26, 2021

Table B-4: Summary of Soil Sampling Results
Analytical Method (e.g., VOC by EPA 8260) 8260 8270 EPH VPH
Contaminant of Concern

Sample ID Date
Collected
(mm/dd/yy)

Source
Area
(eg. Tank
pt 1)

Sample
Depth
(ft
BGS)

Incident
Phase
(Closure,
20Day,
LSA, etc.)

SW-1 5/1/2023 sidewall 4 Closure BRL BRL Exceed BRL
SW-2 5/1/2023 sidewall 4 Closure BRL BRL Exceed BRL
SW-3 5/1/2023 sidewall 4 Closure BRL BRL BRL BRL
SW-4 5/1/2023 sidewall 4 Closure BRL BRL BRL BRL
Bottom 5/1/2023 bottom 8 Closure BRL BRL Exceed BRL
SW-1-A 5/10/2023 sidewall 5 Closure BRL BRL BRL BRL
Bottom-A 5/10/2023 bottom 10 Closure BRL BRL Exceed BRL
SW-2-A 6/12/2023 sidewall 6 Closure BRL BRL BRL BRL
Bottom-B 6/12/2023 bottom 11 Closure BRL BRL BRL BRL
Soil to groundwater MSCC (mg/kg)

BRL BRL BRL BRL
Residential MSCC (mg/kg)

BRL BRL BRL BRL
Industrial/Commercial MSCC (mg/kg)

BRL BRL BRL BRL

Indicate method detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
GCL = gross contamination level
BRL = Below Regulatory Limit
UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

APPENDIX C
UST-61

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

APPENDIX E
DISPOSAL CERTIFICATE

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2023

APPENDIX H
DISPOSAL MANIFESTS

UST Closure Report SUMMIT Project No. 2944.E0003
416 Winecoff St, Troutman, North Carolina August 31, 2021

APPENDIX I & J
CHAIN OF CUSTODY
And ANALYTICAL RESULTS

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/8/2023
Summit Engineering (Charlotte) Matt Hoffman
2520 Whitehall Park Dr Suite 250
Charlotte, NC, 28273
Ref: Analytical Testing Lab Report Number: 23-121-0017
Client Project Description: Winecoff Village
Dear Matt Hoffman:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/1/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 87
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-121-0017
Page 2 of 87
Report Number:
Sample Summary Table
Client Project Description:
23-121-0017
Winecoff Village
Lab No Client Sample ID Matrix Date Collected Date Received
05/01/2023 12:20Solids 95187 Tank 05/01/2023 15:07
05/01/2023 12:45Solids 95188 Bottom 05/01/2023 15:07
05/01/2023 12:55Solids 95189 SW-1 05/01/2023 15:07
05/01/2023 13:05Solids 95190 SW-2 05/01/2023 15:07
05/01/2023 13:15Solids 95191 SW-3 05/01/2023 15:07
05/01/2023 13:30Solids 95192 SW-4 05/01/2023 15:07
Page 3 of 87
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-121-0017
Report Limit
Project:Winecoff Village
V 95187Tank
10900 05/04/2023 15:548015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 1220
359 05/02/2023 16:438015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 27.1
0.787 05/02/2023 17:318260Dn-Butylbenzene mg/Kg - dry 0.016
0.771 05/02/2023 17:318260Dsec-Butyl benzene mg/Kg - dry 0.018
0.690 05/02/2023 17:318260DEthylbenzenemg/Kg - dry 0.019
0.412 05/02/2023 17:318260DIsopropylbenzenemg/Kg - dry 0.015
0.555 05/02/2023 17:318260D4-Isopropyl toluene mg/Kg - dry 0.042
J0.061 05/02/2023 17:318260DMethylene Chloride mg/Kg - dry 0.048
3.51 05/02/2023 17:318260DNaphthalenemg/Kg - dry 0.032
0.766 05/02/2023 17:318260Dn-Propylbenzene mg/Kg - dry 0.017
1.51 05/02/2023 17:318260D1,3,5-Trimethylbenzene mg/Kg - dry 0.017
0.685 05/02/2023 17:318260Do-Xylene mg/Kg - dry 0.016
1.61 05/02/2023 17:318260Dm,p-Xylene mg/Kg - dry 0.041
2.29 05/02/2023 17:318260DXylene (Total)mg/Kg - dry 0.016
15.1 05/05/2023 00:188270E1-Methylnaphthalene mg/Kg - dry 0.555
23.7 05/05/2023 00:188270E2-Methylnaphthalene mg/Kg - dry 0.524
6.68 05/05/2023 00:188270ENaphthalenemg/Kg - dry 0.754
4.65 05/05/2023 00:188270EPhenanthrenemg/Kg - dry 1.09
J1.25 05/05/2023 00:188270EPyrenemg/Kg - dry 0.702
5070 05/05/2023 14:39MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 304
J103005/05/2023 14:39MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 402
3600 05/05/2023 14:39MADEP-EPH Aromatic C11-C22 mg/Kg - dry 469
37.9 05/02/2023 21:51MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 1.60
370 05/02/2023 21:51MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 5.98
366 05/02/2023 21:51MADEP-VPH Aromatic C9-C10 mg/Kg - dry 0.817
23.7 05/03/2023 10:50SW-DRYWT Moisture %
V 95188Bottom
J0.020 05/02/2023 13:278260DAcetonemg/Kg - dry 0.003
J0.002 05/02/2023 13:278260Dsec-Butyl benzene mg/Kg - dry 0.0007
J0.001 05/02/2023 13:278260DEthylbenzenemg/Kg - dry 0.0008
J0.001 05/02/2023 13:278260DIsopropylbenzenemg/Kg - dry 0.0006
J0.001 05/02/2023 13:278260Dn-Propylbenzene mg/Kg - dry 0.0007
0.008 05/02/2023 13:278260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.003 05/02/2023 13:278260Do-Xylene mg/Kg - dry 0.0007
J0.003 05/02/2023 13:278260Dm,p-Xylene mg/Kg - dry 0.001
J0.006 05/02/2023 13:278260DXylene (Total)mg/Kg - dry 0.0007
Page 4 of 87
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-121-0017
Report Limit
Project:Winecoff Village
V 95188Bottom
J0.324 05/04/2023 23:118270EPyrenemg/Kg - dry 0.174
3410 05/05/2023 19:31MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 240
J97005/05/2023 19:31MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 318
2970 05/05/2023 19:31MADEP-EPH Aromatic C11-C22 mg/Kg - dry 368
J1.71 05/02/2023 19:53MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 1.59
174 05/02/2023 19:53MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 5.94
139 05/02/2023 19:53MADEP-VPH Aromatic C9-C10 mg/Kg - dry 0.812
23.2 05/03/2023 10:50SW-DRYWT Moisture %
V 95189SW-1
0.059 05/02/2023 13:548260DAcetonemg/Kg - dry 0.003
J3.31 05/05/2023 00:418270EPyrenemg/Kg - dry 0.693
3750 05/05/2023 20:07MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 238
1320 05/05/2023 20:07MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 316
2790 05/05/2023 20:07MADEP-EPH Aromatic C11-C22 mg/Kg - dry 367
238 05/02/2023 21:04MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 5.90
228 05/02/2023 21:04MADEP-VPH Aromatic C9-C10 mg/Kg - dry 0.807
22.7 05/03/2023 10:50SW-DRYWT Moisture %
V 95190SW-2
J0.025 05/02/2023 14:218260DAcetonemg/Kg - dry 0.003
83.5 05/05/2023 17:42MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 12.8
J52.8 05/05/2023 17:42MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 16.9
77.8 05/05/2023 17:42MADEP-EPH Aromatic C11-C22 mg/Kg - dry 19.7
28.0 05/03/2023 10:50SW-DRYWT Moisture %
V 95191SW-3
J0.007 05/02/2023 14:488260DAcetonemg/Kg - dry 0.003
J42.9 05/05/2023 18:18MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 12.2
J21.3 05/05/2023 18:18MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 16.2
J24.0 05/05/2023 18:18MADEP-EPH Aromatic C11-C22 mg/Kg - dry 18.8
24.5 05/03/2023 10:50SW-DRYWT Moisture %
V 95192SW-4
J0.012 05/02/2023 15:158260DAcetonemg/Kg - dry 0.003
22.3 05/03/2023 10:50SW-DRYWT Moisture %
Page 5 of 87

Client: Summit Engineering (Charlotte) CASE NARRATIVE
Project: Winecoff Village Lab Report Number: 23-121-0017
Date: 5/8/2023
Massachusetts EPH Method MADEP-EPH Sample 95187 (Tank) QC Batch No: V32862
Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Sample 95188 (Bottom) QC Batch No: V32862
Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Sample 95189 (SW-1) Analyte: Chlorooctadecane
QC Batch No: V32862/V32729 Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution
factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO Sample 95187 (Tank) Analyte: o-Terphenyl
QC Batch No: V32744/V32678 Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution
factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: 2-Butanone QC Batch No: V32695/V32696
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 2-Butanone QC Batch No: V32697/V32696 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: 2-Hexanone QC Batch No: V32695/V32696
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: 2-Hexanone QC Batch No: V32697/V32696 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 6 of 87

Analyte: Trichloroethene
QC Batch No: V32695/V32696 CCV result is above control limits but within method parameters. Results are reported but considered estimated.
Semivolatile Organic Compounds - GC/MS Method 8270E Sample 95187 (Tank) QC Batch No: V32895/V32769
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 95189 (SW-1) QC Batch No: V32895/V32769
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.

Page 7 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.7 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 8 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V32678 05/02/23 09:40
10900 mg/Kg - dry 1220 2620Diesel Range Organics (C10-C28)200 05/04/23 15:54 V32744TJW
8015C DROSurrogate: OTP Surrogate 0 *Limits: 31-123%05/04/23 15:54200 TJW
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V32698 05/02/23 08:00
359 mg/Kg - dry 27.1 65.5Gasoline Range Organics (C6-C10)500 05/02/23 16:43 V32699TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 96.4 Limits: 50-137%05/02/23 16:43500 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32696 05/02/23 08:00
<0.078 mg/Kg - dry 0.078 0.655Acetone 50 05/02/23 17:31 V32697TBL
<0.039 mg/Kg - dry 0.039 0.655Acrolein 50 05/02/23 17:31 V32697TBL
<0.024 mg/Kg - dry 0.024 0.655Acrylonitrile 50 05/02/23 17:31 V32697TBL
<0.019 mg/Kg - dry 0.019 0.163Benzene 50 05/02/23 17:31 V32697TBL
<0.016 mg/Kg - dry 0.016 0.163Bromobenzene 50 05/02/23 17:31 V32697TBL
<0.026 mg/Kg - dry 0.026 0.163Bromochloromethane 50 05/02/23 17:31 V32697TBL
<0.039 mg/Kg - dry 0.039 0.163Bromodichloromethane 50 05/02/23 17:31 V32697TBL
<0.033 mg/Kg - dry 0.033 0.163Bromoform 50 05/02/23 17:31 V32697TBL
<0.059 mg/Kg - dry 0.059 0.327Bromomethane 50 05/02/23 17:31 V32697TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 9 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32696 05/02/23 08:00
0.787 mg/Kg - dry 0.016 0.163n-Butylbenzene 50 05/02/23 17:31 V32697TBL
0.771 mg/Kg - dry 0.018 0.163sec-Butyl benzene 50 05/02/23 17:31 V32697TBL
<0.016 mg/Kg - dry 0.016 0.163tert-Butyl benzene 50 05/02/23 17:31 V32697TBL
<0.020 mg/Kg - dry 0.020 0.163Carbon Disulfide 50 05/02/23 17:31 V32697TBL
<0.051 mg/Kg - dry 0.051 0.163Carbon Tetrachloride 50 05/02/23 17:31 V32697TBL
<0.022 mg/Kg - dry 0.022 0.163Chlorobenzene 50 05/02/23 17:31 V32697TBL
<0.029 mg/Kg - dry 0.029 0.163Chlorodibromomethane 50 05/02/23 17:31 V32697TBL
<0.029 mg/Kg - dry 0.029 0.327Chloroethane 50 05/02/23 17:31 V32697TBL
<0.034 mg/Kg - dry 0.034 0.163Chloroform 50 05/02/23 17:31 V32697TBL
<0.020 mg/Kg - dry 0.020 0.327Chloromethane 50 05/02/23 17:31 V32697TBL
<0.016 mg/Kg - dry 0.016 0.1632-Chlorotoluene 50 05/02/23 17:31 V32697TBL
<0.012 mg/Kg - dry 0.012 0.1634-Chlorotoluene 50 05/02/23 17:31 V32697TBL
<0.023 mg/Kg - dry 0.023 0.163Di-Isopropyl Ether (DIPE)50 05/02/23 17:31 V32697TBL
<0.014 mg/Kg - dry 0.014 0.3271,2-Dibromo-3-Chloropropane 50 05/02/23 17:31 V32697TBL
<0.019 mg/Kg - dry 0.019 0.1631,2-Dibromoethane 50 05/02/23 17:31 V32697TBL
<0.032 mg/Kg - dry 0.032 0.163Dibromomethane 50 05/02/23 17:31 V32697TBL
<0.010 mg/Kg - dry 0.010 0.1631,2-Dichlorobenzene 50 05/02/23 17:31 V32697TBL
<0.012 mg/Kg - dry 0.012 0.1631,3-Dichlorobenzene 50 05/02/23 17:31 V32697TBL
<0.019 mg/Kg - dry 0.019 0.1631,4-Dichlorobenzene 50 05/02/23 17:31 V32697TBL
<0.043 mg/Kg - dry 0.043 0.327Dichlorodifluoromethane 50 05/02/23 17:31 V32697TBL
<0.026 mg/Kg - dry 0.026 0.1631,1-Dichloroethane 50 05/02/23 17:31 V32697TBL
<0.045 mg/Kg - dry 0.045 0.1631,2-Dichloroethane 50 05/02/23 17:31 V32697TBL
<0.023 mg/Kg - dry 0.023 0.1631,1-Dichloroethene 50 05/02/23 17:31 V32697TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 10 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32696 05/02/23 08:00
<0.025 mg/Kg - dry 0.025 0.163cis-1,2-Dichloroethene 50 05/02/23 17:31 V32697TBL
<0.034 mg/Kg - dry 0.034 0.163trans-1,2-Dichloroethene 50 05/02/23 17:31 V32697TBL
<0.014 mg/Kg - dry 0.014 0.1631,2-Dichloropropane 50 05/02/23 17:31 V32697TBL
<0.018 mg/Kg - dry 0.018 0.1631,3-Dichloropropane 50 05/02/23 17:31 V32697TBL
<0.041 mg/Kg - dry 0.041 0.1632,2-Dichloropropane 50 05/02/23 17:31 V32697TBL
<0.024 mg/Kg - dry 0.024 0.1631,1-Dichloropropene 50 05/02/23 17:31 V32697TBL
<0.017 mg/Kg - dry 0.017 0.163cis-1,3-Dichloropropene 50 05/02/23 17:31 V32697TBL
<0.026 mg/Kg - dry 0.026 0.163trans-1,3-Dichloropropene 50 05/02/23 17:31 V32697TBL
0.690 mg/Kg - dry 0.019 0.163Ethylbenzene 50 05/02/23 17:31 V32697TBL
<0.027 mg/Kg - dry 0.027 3.28Ethyl Tertiary Butyl Ether (ETBE)50 05/02/23 17:31 V32697TBL
<0.025 mg/Kg - dry 0.025 0.327Hexachlorobutadiene 50 05/02/23 17:31 V32697TBL
<0.021 mg/Kg - dry 0.021 0.327n-Hexane 50 05/02/23 17:31 V32697TBL
<0.020 mg/Kg - dry 0.020 0.6552-Hexanone 50 05/02/23 17:31 V32697TBL
0.412 mg/Kg - dry 0.015 0.163Isopropylbenzene 50 05/02/23 17:31 V32697TBL
0.555 mg/Kg - dry 0.042 0.1634-Isopropyl toluene 50 05/02/23 17:31 V32697TBL
<0.021 mg/Kg - dry 0.021 0.655Methyl Ethyl Ketone (MEK)50 05/02/23 17:31 V32697TBL
<0.020 mg/Kg - dry 0.020 0.163Methyl tert-butyl ether (MTBE)50 05/02/23 17:31 V32697TBL
<0.491 mg/Kg - dry 0.491 0.6554-Methyl-2-Pentanone 50 05/02/23 17:31 V32697TBL
0.061 J mg/Kg - dry 0.048 0.163Methylene Chloride 50 05/02/23 17:31 V32697TBL
3.51 mg/Kg - dry 0.032 0.327Naphthalene 50 05/02/23 17:31 V32697TBL
0.766 mg/Kg - dry 0.017 0.163n-Propylbenzene 50 05/02/23 17:31 V32697TBL
<0.046 mg/Kg - dry 0.046 0.163Styrene 50 05/02/23 17:31 V32697TBL
<0.034 mg/Kg - dry 0.034 0.1631,1,1,2-Tetrachloroethane 50 05/02/23 17:31 V32697TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 11 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32696 05/02/23 08:00
<0.010 mg/Kg - dry 0.010 0.1631,1,2,2-Tetrachloroethane 50 05/02/23 17:31 V32697TBL
<0.029 mg/Kg - dry 0.029 0.163Tetrachloroethene 50 05/02/23 17:31 V32697TBL
<0.021 mg/Kg - dry 0.021 0.163Toluene 50 05/02/23 17:31 V32697TBL
<0.017 mg/Kg - dry 0.017 0.3271,2,3-Trichlorobenzene 50 05/02/23 17:31 V32697TBL
<0.020 mg/Kg - dry 0.020 0.3271,2,4-Trichlorobenzene 50 05/02/23 17:31 V32697TBL
<0.047 mg/Kg - dry 0.047 0.1631,1,1-Trichloroethane 50 05/02/23 17:31 V32697TBL
<0.015 mg/Kg - dry 0.015 0.1631,1,2-Trichloroethane 50 05/02/23 17:31 V32697TBL
<0.030 mg/Kg - dry 0.030 0.163Trichloroethene 50 05/02/23 17:31 V32697TBL
<0.068 mg/Kg - dry 0.068 0.327Trichlorofluoromethane 50 05/02/23 17:31 V32697TBL
<0.023 mg/Kg - dry 0.023 0.1631,2,3-Trichloropropane 50 05/02/23 17:31 V32697TBL
1.51 mg/Kg - dry 0.017 0.1631,3,5-Trimethylbenzene 50 05/02/23 17:31 V32697TBL
<0.015 mg/Kg - dry 0.015 0.327Vinyl Acetate 50 05/02/23 17:31 V32697TBL
<0.015 mg/Kg - dry 0.015 0.327Vinyl Chloride 50 05/02/23 17:31 V32697TBL
0.685 mg/Kg - dry 0.016 0.163o-Xylene 50 05/02/23 17:31 V32697TBL
1.61 mg/Kg - dry 0.041 0.327m,p-Xylene 50 05/02/23 17:31 V32697TBL
2.29 mg/Kg - dry 0.016 0.163Xylene (Total)50 05/02/23 17:31 V32697
Surrogate: 4-Bromofluorobenzene 82.4 Limits: 70-130%05/02/23 17:3150 TBL V32697
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%05/02/23 17:3150 TBL V32697
Surrogate: Toluene-d8 91.4 Limits: 76-129%05/02/23 17:3150 TBL V32697
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 12 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.608 mg/Kg - dry 0.608 3.46Acenaphthene 4 05/05/23 00:18 V32895ANG
<0.550 mg/Kg - dry 0.550 3.46Acenaphthylene 4 05/05/23 00:18 V32895ANG
<0.796 mg/Kg - dry 0.796 3.46Aniline 4 05/05/23 00:18 V32895ANG
<0.749 mg/Kg - dry 0.749 3.46Anthracene 4 05/05/23 00:18 V32895ANG
<0.728 mg/Kg - dry 0.728 3.46Benzo(a)anthracene 4 05/05/23 00:18 V32895ANG
<0.770 mg/Kg - dry 0.770 3.46Benzo(a)pyrene 4 05/05/23 00:18 V32895ANG
<0.765 mg/Kg - dry 0.765 3.46Benzo(b)fluoranthene 4 05/05/23 00:18 V32895ANG
<0.712 mg/Kg - dry 0.712 3.46Benzo(g,h,i)perylene 4 05/05/23 00:18 V32895ANG
<0.718 mg/Kg - dry 0.718 3.46Benzo(k)fluoranthene 4 05/05/23 00:18 V32895ANG
<3.04 mg/Kg - dry 3.04 10.5Benzoic Acid 4 05/05/23 00:18 V32895ANG
<0.550 mg/Kg - dry 0.550 3.46Benzyl alcohol 4 05/05/23 00:18 V32895ANG
<0.618 mg/Kg - dry 0.618 3.46Bis(2-Chloroethoxy)methane 4 05/05/23 00:18 V32895ANG
<0.560 mg/Kg - dry 0.560 3.46Bis(2-Chloroethyl)ether 4 05/05/23 00:18 V32895ANG
<0.712 mg/Kg - dry 0.712 1.73Bis(2-Chloroisopropyl)ether 4 05/05/23 00:18 V32895ANG
<0.629 mg/Kg - dry 0.629 3.46Bis(2-ethylhexyl)phthalate 4 05/05/23 00:18 V32895ANG
<0.571 mg/Kg - dry 0.571 3.464-Bromophenyl phenyl ether 4 05/05/23 00:18 V32895ANG
<0.592 mg/Kg - dry 0.592 1.73Butyl benzyl phthalate 4 05/05/23 00:18 V32895ANG
<0.484 mg/Kg - dry 0.484 3.464-Chloro-3-methylphenol 4 05/05/23 00:18 V32895ANG
<0.587 mg/Kg - dry 0.587 1.734-Chloroaniline 4 05/05/23 00:18 V32895ANG
<0.608 mg/Kg - dry 0.608 3.462-Chloronaphthalene 4 05/05/23 00:18 V32895ANG
<0.515 mg/Kg - dry 0.515 3.462-Chlorophenol 4 05/05/23 00:18 V32895ANG
<0.660 mg/Kg - dry 0.660 5.244-Chlorophenyl phenyl ether 4 05/05/23 00:18 V32895ANG
<0.744 mg/Kg - dry 0.744 3.46Chrysene 4 05/05/23 00:18 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 13 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<1.21 mg/Kg - dry 1.21 3.46Dibenz(a,h)anthracene 4 05/05/23 00:18 V32895ANG
<0.623 mg/Kg - dry 0.623 3.46Dibenzofuran 4 05/05/23 00:18 V32895ANG
<0.495 mg/Kg - dry 0.495 3.461,2-Dichlorobenzene 4 05/05/23 00:18 V32895ANG
<0.509 mg/Kg - dry 0.509 3.461,3-Dichlorobenzene 4 05/05/23 00:18 V32895ANG
<0.511 mg/Kg - dry 0.511 1.731,4-Dichlorobenzene 4 05/05/23 00:18 V32895ANG
<0.770 mg/Kg - dry 0.770 3.463,3'-Dichlorobenzidine 4 05/05/23 00:18 V32895ANG
<0.501 mg/Kg - dry 0.501 3.462,4-Dichlorophenol 4 05/05/23 00:18 V32895ANG
<0.943 mg/Kg - dry 0.943 3.46Diethyl phthalate 4 05/05/23 00:18 V32895ANG
<0.912 mg/Kg - dry 0.912 3.46Dimethyl phthalate 4 05/05/23 00:18 V32895ANG
<0.566 mg/Kg - dry 0.566 1.732,4-Dimethylphenol 4 05/05/23 00:18 V32895ANG
<0.560 mg/Kg - dry 0.560 3.46Di-n-butyl phthalate 4 05/05/23 00:18 V32895ANG
<1.26 mg/Kg - dry 1.26 7.884,6-Dinitro-2-methylphenol 4 05/05/23 00:18 V32895ANG
<2.73 mg/Kg - dry 2.73 7.882,4-Dinitrophenol 4 05/05/23 00:18 V32895ANG
<0.505 mg/Kg - dry 0.505 3.462,4-Dinitrotoluene 4 05/05/23 00:18 V32895ANG
<0.566 mg/Kg - dry 0.566 3.462,6-Dinitrotoluene 4 05/05/23 00:18 V32895ANG
<0.749 mg/Kg - dry 0.749 1.73Di-n-Octyl Phthalate 4 05/05/23 00:18 V32895ANG
<0.644 mg/Kg - dry 0.644 3.46Fluoranthene 4 05/05/23 00:18 V32895ANG
<0.671 mg/Kg - dry 0.671 3.46Fluorene 4 05/05/23 00:18 V32895ANG
<0.555 mg/Kg - dry 0.555 3.46Hexachlorobenzene 4 05/05/23 00:18 V32895ANG
<0.511 mg/Kg - dry 0.511 3.46Hexachlorobutadiene 4 05/05/23 00:18 V32895ANG
<0.823 mg/Kg - dry 0.823 3.46Hexachlorocyclopentadiene 4 05/05/23 00:18 V32895ANG
<0.415 mg/Kg - dry 0.415 3.46Hexachloroethane 4 05/05/23 00:18 V32895ANG
<0.938 mg/Kg - dry 0.938 3.46Indeno(1,2,3-cd)pyrene 4 05/05/23 00:18 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 14 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<1.00 mg/Kg - dry 1.00 3.46Isophorone 4 05/05/23 00:18 V32895ANG
15.1 mg/Kg - dry 0.555 3.461-Methylnaphthalene 4 05/05/23 00:18 V32895ANG
23.7 mg/Kg - dry 0.524 3.462-Methylnaphthalene 4 05/05/23 00:18 V32895ANG
<0.508 mg/Kg - dry 0.508 3.462-Methylphenol 4 05/05/23 00:18 V32895ANG
<0.445 mg/Kg - dry 0.445 3.463&4 Methylphenol 4 05/05/23 00:18 V32895ANG
6.68 mg/Kg - dry 0.754 3.46Naphthalene 4 05/05/23 00:18 V32895ANG
<0.507 mg/Kg - dry 0.507 3.462-Nitroaniline 4 05/05/23 00:18 V32895ANG
<0.629 mg/Kg - dry 0.629 3.463-Nitroaniline 4 05/05/23 00:18 V32895ANG
<0.488 mg/Kg - dry 0.488 1.734-Nitroaniline 4 05/05/23 00:18 V32895ANG
<0.608 mg/Kg - dry 0.608 1.73Nitrobenzene 4 05/05/23 00:18 V32895ANG
<0.465 mg/Kg - dry 0.465 3.462-Nitrophenol 4 05/05/23 00:18 V32895ANG
<0.613 mg/Kg - dry 0.613 3.464-Nitrophenol 4 05/05/23 00:18 V32895ANG
<1.38 mg/Kg - dry 1.38 3.46N-Nitrosodimethylamine 4 05/05/23 00:18 V32895ANG
<0.948 mg/Kg - dry 0.948 3.46N-Nitrosodiphenylamine 4 05/05/23 00:18 V32895ANG
<0.618 mg/Kg - dry 0.618 3.46N-Nitroso-di-n-propylamine 4 05/05/23 00:18 V32895ANG
<1.82 mg/Kg - dry 1.82 5.24Pentachlorophenol 4 05/05/23 00:18 V32895ANG
4.65 mg/Kg - dry 1.09 3.46Phenanthrene 4 05/05/23 00:18 V32895ANG
<0.587 mg/Kg - dry 0.587 3.46Phenol 4 05/05/23 00:18 V32895ANG
1.25 J mg/Kg - dry 0.702 3.46Pyrene 4 05/05/23 00:18 V32895ANG
<0.415 mg/Kg - dry 0.415 1.73Pyridine 4 05/05/23 00:18 V32895ANG
<0.560 mg/Kg - dry 0.560 3.461,2,4-Trichlorobenzene 4 05/05/23 00:18 V32895ANG
<0.504 mg/Kg - dry 0.504 3.462,4,5-Trichlorophenol 4 05/05/23 00:18 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 15 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.505 mg/Kg - dry 0.505 3.462,4,6-Trichlorophenol 4 05/05/23 00:18 V32895ANG
8270ESurrogate: Phenol-d5 49.1 Limits: 34-121%05/05/23 00:184 ANG
Surrogate: 2-Fluorobiphenyl 68.3 Limits: 44-115%05/05/23 00:184 ANG V32895
Surrogate: 2-Fluorophenol 52.1 Limits: 35-115%05/05/23 00:184 ANG V32895
Surrogate: Nitrobenzene-d5 57.2 Limits: 37-122%05/05/23 00:184 ANG V32895
Surrogate: 4-Terphenyl-d14 73.7 Limits: 54-127%05/05/23 00:184 ANG V32895
Surrogate: 2,4,6-Tribromophenol 64.4 Limits: 39-132%05/05/23 00:184 ANG V32895
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 16 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Tank
95187 Matrix:
5/1/2023 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V32729 05/03/23 10:15
5070 mg/Kg - dry 304 1650Aliphatic C9-C18 25 05/05/23 14:39 V32862AMP
1030 J mg/Kg - dry 402 1650Aliphatic C19-C36 25 05/05/23 14:39 V32862AMP
3600 mg/Kg - dry 469 1650Aromatic C11-C22 25 05/05/23 14:39 V32862AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 180 *Limits: 40-140%05/05/23 14:3925 AMP
MADEP-EPHSurrogate: Chlorooctadecane 123 Limits: 40-140%05/05/23 14:3925 AMP
MADEP-EPHSurrogate: OTP Surrogate 59.1 Limits: 40-140%05/05/23 14:3925 AMP
Surrogate: 2-Fluorobiphenyl 92.3 Limits: 40-140%05/05/23 14:3925 AMP V32862
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
37.9 mg/Kg - dry 1.60 10.5Aliphatic C5-C8 100 05/02/23 21:51 V32693TBL
370 mg/Kg - dry 5.98 10.5Aliphatic C9-C12 100 05/02/23 21:51 V32693TBL
366 mg/Kg - dry 0.817 10.5Aromatic C9-C10 100 05/02/23 21:51 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)86.4 Limits: 70-130%05/02/23 21:51100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)80.6 Limits: 70-130%05/02/23 21:51100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 17 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Bottom
95188 Matrix:
5/1/2023 12:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.2 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 18 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Bottom
95188 Matrix:
5/1/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
0.020 J mg/Kg - dry 0.003 0.026Acetone 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/02/23 13:27 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/02/23 13:27 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 05/02/23 13:27 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/02/23 13:27 V32695TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/02/23 13:27 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/02/23 13:27 V32695TBL
0.002 J mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/02/23 13:27 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 05/02/23 13:27 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/02/23 13:27 V32695TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/02/23 13:27 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/02/23 13:27 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/02/23 13:27 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/02/23 13:27 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/02/23 13:27 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/02/23 13:27 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/02/23 13:27 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 19 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Bottom
95188 Matrix:
5/1/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/02/23 13:27 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 05/02/23 13:27 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/02/23 13:27 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/02/23 13:27 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/02/23 13:27 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/02/23 13:27 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/02/23 13:27 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/02/23 13:27 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/02/23 13:27 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/02/23 13:27 V32695TBL
0.001 J mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/02/23 13:27 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/02/23 13:27 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/02/23 13:27 V32695TBL
0.001 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/02/23 13:27 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 20 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Bottom
95188 Matrix:
5/1/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/02/23 13:27 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.026Methyl Ethyl Ketone (MEK)1 05/02/23 13:27 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/02/23 13:27 V32695TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/02/23 13:27 V32695TBL
0.001 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/02/23 13:27 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/02/23 13:27 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/02/23 13:27 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/02/23 13:27 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/02/23 13:27 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/02/23 13:27 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/02/23 13:27 V32695TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/02/23 13:27 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/02/23 13:27 V32695TBL
0.008 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/02/23 13:27 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/02/23 13:27 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 05/02/23 13:27 V32695TBL
0.003 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/02/23 13:27 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 21 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Bottom
95188 Matrix:
5/1/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
0.003 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/02/23 13:27 V32695TBL
0.006 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/02/23 13:27 V32695
Surrogate: 4-Bromofluorobenzene 96.3 Limits: 70-130%05/02/23 13:271 TBL V32695
Surrogate: Dibromofluoromethane 104 Limits: 84-123%05/02/23 13:271 TBL V32695
Surrogate: Toluene-d8 88.1 Limits: 76-129%05/02/23 13:271 TBL V32695
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.151 mg/Kg - dry 0.151 0.859Acenaphthene 1 05/04/23 23:11 V32895ANG
<0.136 mg/Kg - dry 0.136 0.859Acenaphthylene 1 05/04/23 23:11 V32895ANG
<0.197 mg/Kg - dry 0.197 0.859Aniline 1 05/04/23 23:11 V32895ANG
<0.186 mg/Kg - dry 0.186 0.859Anthracene 1 05/04/23 23:11 V32895ANG
<0.180 mg/Kg - dry 0.180 0.859Benzo(a)anthracene 1 05/04/23 23:11 V32895ANG
<0.191 mg/Kg - dry 0.191 0.859Benzo(a)pyrene 1 05/04/23 23:11 V32895ANG
<0.190 mg/Kg - dry 0.190 0.859Benzo(b)fluoranthene 1 05/04/23 23:11 V32895ANG
<0.177 mg/Kg - dry 0.177 0.859Benzo(g,h,i)perylene 1 05/04/23 23:11 V32895ANG
<0.178 mg/Kg - dry 0.178 0.859Benzo(k)fluoranthene 1 05/04/23 23:11 V32895ANG
<0.755 mg/Kg - dry 0.755 2.60Benzoic Acid 1 05/04/23 23:11 V32895ANG
<0.136 mg/Kg - dry 0.136 0.859Benzyl alcohol 1 05/04/23 23:11 V32895ANG
<0.153 mg/Kg - dry 0.153 0.859Bis(2-Chloroethoxy)methane 1 05/04/23 23:11 V32895ANG
<0.139 mg/Kg - dry 0.139 0.859Bis(2-Chloroethyl)ether 1 05/04/23 23:11 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 22 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Bottom
95188 Matrix:
5/1/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.177 mg/Kg - dry 0.177 0.429Bis(2-Chloroisopropyl)ether 1 05/04/23 23:11 V32895ANG
<0.156 mg/Kg - dry 0.156 0.859Bis(2-ethylhexyl)phthalate 1 05/04/23 23:11 V32895ANG
<0.141 mg/Kg - dry 0.141 0.8594-Bromophenyl phenyl ether 1 05/04/23 23:11 V32895ANG
<0.147 mg/Kg - dry 0.147 0.429Butyl benzyl phthalate 1 05/04/23 23:11 V32895ANG
<0.120 mg/Kg - dry 0.120 0.8594-Chloro-3-methylphenol 1 05/04/23 23:11 V32895ANG
<0.145 mg/Kg - dry 0.145 0.4294-Chloroaniline 1 05/04/23 23:11 V32895ANG
<0.151 mg/Kg - dry 0.151 0.8592-Chloronaphthalene 1 05/04/23 23:11 V32895ANG
<0.127 mg/Kg - dry 0.127 0.8592-Chlorophenol 1 05/04/23 23:11 V32895ANG
<0.164 mg/Kg - dry 0.164 1.304-Chlorophenyl phenyl ether 1 05/04/23 23:11 V32895ANG
<0.184 mg/Kg - dry 0.184 0.859Chrysene 1 05/04/23 23:11 V32895ANG
<0.299 mg/Kg - dry 0.299 0.859Dibenz(a,h)anthracene 1 05/04/23 23:11 V32895ANG
<0.154 mg/Kg - dry 0.154 0.859Dibenzofuran 1 05/04/23 23:11 V32895ANG
<0.122 mg/Kg - dry 0.122 0.8591,2-Dichlorobenzene 1 05/04/23 23:11 V32895ANG
<0.126 mg/Kg - dry 0.126 0.8591,3-Dichlorobenzene 1 05/04/23 23:11 V32895ANG
<0.126 mg/Kg - dry 0.126 0.4291,4-Dichlorobenzene 1 05/04/23 23:11 V32895ANG
<0.191 mg/Kg - dry 0.191 0.8593,3'-Dichlorobenzidine 1 05/04/23 23:11 V32895ANG
<0.124 mg/Kg - dry 0.124 0.8592,4-Dichlorophenol 1 05/04/23 23:11 V32895ANG
<0.234 mg/Kg - dry 0.234 0.859Diethyl phthalate 1 05/04/23 23:11 V32895ANG
<0.226 mg/Kg - dry 0.226 0.859Dimethyl phthalate 1 05/04/23 23:11 V32895ANG
<0.140 mg/Kg - dry 0.140 0.4292,4-Dimethylphenol 1 05/04/23 23:11 V32895ANG
<0.139 mg/Kg - dry 0.139 0.859Di-n-butyl phthalate 1 05/04/23 23:11 V32895ANG
<0.312 mg/Kg - dry 0.312 1.954,6-Dinitro-2-methylphenol 1 05/04/23 23:11 V32895ANG
<0.677 mg/Kg - dry 0.677 1.952,4-Dinitrophenol 1 05/04/23 23:11 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 23 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Bottom
95188 Matrix:
5/1/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.125 mg/Kg - dry 0.125 0.8592,4-Dinitrotoluene 1 05/04/23 23:11 V32895ANG
<0.140 mg/Kg - dry 0.140 0.8592,6-Dinitrotoluene 1 05/04/23 23:11 V32895ANG
<0.186 mg/Kg - dry 0.186 0.429Di-n-Octyl Phthalate 1 05/04/23 23:11 V32895ANG
<0.160 mg/Kg - dry 0.160 0.859Fluoranthene 1 05/04/23 23:11 V32895ANG
<0.166 mg/Kg - dry 0.166 0.859Fluorene 1 05/04/23 23:11 V32895ANG
<0.138 mg/Kg - dry 0.138 0.859Hexachlorobenzene 1 05/04/23 23:11 V32895ANG
<0.127 mg/Kg - dry 0.127 0.859Hexachlorobutadiene 1 05/04/23 23:11 V32895ANG
<0.204 mg/Kg - dry 0.204 0.859Hexachlorocyclopentadiene 1 05/04/23 23:11 V32895ANG
<0.103 mg/Kg - dry 0.103 0.859Hexachloroethane 1 05/04/23 23:11 V32895ANG
<0.233 mg/Kg - dry 0.233 0.859Indeno(1,2,3-cd)pyrene 1 05/04/23 23:11 V32895ANG
<0.248 mg/Kg - dry 0.248 0.859Isophorone 1 05/04/23 23:11 V32895ANG
<0.138 mg/Kg - dry 0.138 0.8591-Methylnaphthalene 1 05/04/23 23:11 V32895ANG
<0.130 mg/Kg - dry 0.130 0.8592-Methylnaphthalene 1 05/04/23 23:11 V32895ANG
<0.126 mg/Kg - dry 0.126 0.8592-Methylphenol 1 05/04/23 23:11 V32895ANG
<0.110 mg/Kg - dry 0.110 0.8593&4 Methylphenol 1 05/04/23 23:11 V32895ANG
<0.187 mg/Kg - dry 0.187 0.859Naphthalene 1 05/04/23 23:11 V32895ANG
<0.125 mg/Kg - dry 0.125 0.8592-Nitroaniline 1 05/04/23 23:11 V32895ANG
<0.156 mg/Kg - dry 0.156 0.8593-Nitroaniline 1 05/04/23 23:11 V32895ANG
<0.121 mg/Kg - dry 0.121 0.4294-Nitroaniline 1 05/04/23 23:11 V32895ANG
<0.151 mg/Kg - dry 0.151 0.429Nitrobenzene 1 05/04/23 23:11 V32895ANG
<0.115 mg/Kg - dry 0.115 0.8592-Nitrophenol 1 05/04/23 23:11 V32895ANG
<0.152 mg/Kg - dry 0.152 0.8594-Nitrophenol 1 05/04/23 23:11 V32895ANG
<0.342 mg/Kg - dry 0.342 0.859N-Nitrosodimethylamine 1 05/04/23 23:11 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 24 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Bottom
95188 Matrix:
5/1/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.235 mg/Kg - dry 0.235 0.859N-Nitrosodiphenylamine 1 05/04/23 23:11 V32895ANG
<0.153 mg/Kg - dry 0.153 0.859N-Nitroso-di-n-propylamine 1 05/04/23 23:11 V32895ANG
<0.451 mg/Kg - dry 0.451 1.30Pentachlorophenol 1 05/04/23 23:11 V32895ANG
<0.270 mg/Kg - dry 0.270 0.859Phenanthrene 1 05/04/23 23:11 V32895ANG
<0.145 mg/Kg - dry 0.145 0.859Phenol 1 05/04/23 23:11 V32895ANG
0.324 J mg/Kg - dry 0.174 0.859Pyrene 1 05/04/23 23:11 V32895ANG
<0.103 mg/Kg - dry 0.103 0.429Pyridine 1 05/04/23 23:11 V32895ANG
<0.139 mg/Kg - dry 0.139 0.8591,2,4-Trichlorobenzene 1 05/04/23 23:11 V32895ANG
<0.125 mg/Kg - dry 0.125 0.8592,4,5-Trichlorophenol 1 05/04/23 23:11 V32895ANG
<0.125 mg/Kg - dry 0.125 0.8592,4,6-Trichlorophenol 1 05/04/23 23:11 V32895ANG
8270ESurrogate: Phenol-d5 66.1 Limits: 34-121%05/04/23 23:111 ANG
Surrogate: 2-Fluorobiphenyl 74.3 Limits: 44-115%05/04/23 23:111 ANG V32895
Surrogate: 2-Fluorophenol 69.7 Limits: 35-115%05/04/23 23:111 ANG V32895
Surrogate: Nitrobenzene-d5 67.7 Limits: 37-122%05/04/23 23:111 ANG V32895
Surrogate: 4-Terphenyl-d14 82.0 Limits: 54-127%05/04/23 23:111 ANG V32895
Surrogate: 2,4,6-Tribromophenol 80.5 Limits: 39-132%05/04/23 23:111 ANG V32895
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 25 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:Bottom
95188 Matrix:
5/1/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V32729 05/03/23 10:15
3410 mg/Kg - dry 240 1300Aliphatic C9-C18 20 05/05/23 19:31 V32862AMP
970 J mg/Kg - dry 318 1300Aliphatic C19-C36 20 05/05/23 19:31 V32862AMP
2970 mg/Kg - dry 368 1300Aromatic C11-C22 20 05/05/23 19:31 V32862AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 168 *Limits: 40-140%05/05/23 19:3120 AMP
MADEP-EPHSurrogate: Chlorooctadecane I *Limits: 40-140%05/05/23 19:3120 AMP
MADEP-EPHSurrogate: OTP Surrogate 58.3 Limits: 40-140%05/05/23 19:3120 AMP
Surrogate: 2-Fluorobiphenyl 85.7 Limits: 40-140%05/05/23 19:3120 AMP V32862
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
1.71 J mg/Kg - dry 1.59 10.4Aliphatic C5-C8 100 05/02/23 19:53 V32693TBL
174 mg/Kg - dry 5.94 10.4Aliphatic C9-C12 100 05/02/23 19:53 V32693TBL
139 mg/Kg - dry 0.812 10.4Aromatic C9-C10 100 05/02/23 19:53 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)88.0 Limits: 70-130%05/02/23 19:53100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)103 Limits: 70-130%05/02/23 19:53100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 26 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-1
95189 Matrix:
5/1/2023 12:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.7 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 27 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-1
95189 Matrix:
5/1/2023 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
0.059 mg/Kg - dry 0.003 0.025Acetone 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 05/02/23 13:54 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 05/02/23 13:54 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/02/23 13:54 V32695TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/02/23 13:54 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 05/02/23 13:54 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/02/23 13:54 V32695TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/02/23 13:54 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/02/23 13:54 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/02/23 13:54 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/02/23 13:54 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/02/23 13:54 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 05/02/23 13:54 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 28 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-1
95189 Matrix:
5/1/2023 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/02/23 13:54 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 05/02/23 13:54 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/02/23 13:54 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/02/23 13:54 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/02/23 13:54 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/02/23 13:54 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/02/23 13:54 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/02/23 13:54 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/02/23 13:54 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 05/02/23 13:54 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 05/02/23 13:54 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/02/23 13:54 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 29 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-1
95189 Matrix:
5/1/2023 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/02/23 13:54 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 05/02/23 13:54 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/02/23 13:54 V32695TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/02/23 13:54 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/02/23 13:54 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/02/23 13:54 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/02/23 13:54 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/02/23 13:54 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/02/23 13:54 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/02/23 13:54 V32695TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/02/23 13:54 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/02/23 13:54 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/02/23 13:54 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 30 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-1
95189 Matrix:
5/1/2023 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/02/23 13:54 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/02/23 13:54 V32695
Surrogate: 4-Bromofluorobenzene 97.9 Limits: 70-130%05/02/23 13:541 TBL V32695
Surrogate: Dibromofluoromethane 100 Limits: 84-123%05/02/23 13:541 TBL V32695
Surrogate: Toluene-d8 88.2 Limits: 76-129%05/02/23 13:541 TBL V32695
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.600 mg/Kg - dry 0.600 3.42Acenaphthene 4 05/05/23 00:41 V32895ANG
<0.543 mg/Kg - dry 0.543 3.42Acenaphthylene 4 05/05/23 00:41 V32895ANG
<0.786 mg/Kg - dry 0.786 3.42Aniline 4 05/05/23 00:41 V32895ANG
<0.739 mg/Kg - dry 0.739 3.42Anthracene 4 05/05/23 00:41 V32895ANG
<0.719 mg/Kg - dry 0.719 3.42Benzo(a)anthracene 4 05/05/23 00:41 V32895ANG
<0.760 mg/Kg - dry 0.760 3.42Benzo(a)pyrene 4 05/05/23 00:41 V32895ANG
<0.755 mg/Kg - dry 0.755 3.42Benzo(b)fluoranthene 4 05/05/23 00:41 V32895ANG
<0.703 mg/Kg - dry 0.703 3.42Benzo(g,h,i)perylene 4 05/05/23 00:41 V32895ANG
<0.708 mg/Kg - dry 0.708 3.42Benzo(k)fluoranthene 4 05/05/23 00:41 V32895ANG
<3.00 mg/Kg - dry 3.00 10.4Benzoic Acid 4 05/05/23 00:41 V32895ANG
<0.543 mg/Kg - dry 0.543 3.42Benzyl alcohol 4 05/05/23 00:41 V32895ANG
<0.610 mg/Kg - dry 0.610 3.42Bis(2-Chloroethoxy)methane 4 05/05/23 00:41 V32895ANG
<0.553 mg/Kg - dry 0.553 3.42Bis(2-Chloroethyl)ether 4 05/05/23 00:41 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 31 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-1
95189 Matrix:
5/1/2023 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.703 mg/Kg - dry 0.703 1.71Bis(2-Chloroisopropyl)ether 4 05/05/23 00:41 V32895ANG
<0.620 mg/Kg - dry 0.620 3.42Bis(2-ethylhexyl)phthalate 4 05/05/23 00:41 V32895ANG
<0.564 mg/Kg - dry 0.564 3.424-Bromophenyl phenyl ether 4 05/05/23 00:41 V32895ANG
<0.584 mg/Kg - dry 0.584 1.71Butyl benzyl phthalate 4 05/05/23 00:41 V32895ANG
<0.478 mg/Kg - dry 0.478 3.424-Chloro-3-methylphenol 4 05/05/23 00:41 V32895ANG
<0.579 mg/Kg - dry 0.579 1.714-Chloroaniline 4 05/05/23 00:41 V32895ANG
<0.600 mg/Kg - dry 0.600 3.422-Chloronaphthalene 4 05/05/23 00:41 V32895ANG
<0.508 mg/Kg - dry 0.508 3.422-Chlorophenol 4 05/05/23 00:41 V32895ANG
<0.653 mg/Kg - dry 0.653 5.194-Chlorophenyl phenyl ether 4 05/05/23 00:41 V32895ANG
<0.734 mg/Kg - dry 0.734 3.42Chrysene 4 05/05/23 00:41 V32895ANG
<1.19 mg/Kg - dry 1.19 3.42Dibenz(a,h)anthracene 4 05/05/23 00:41 V32895ANG
<0.615 mg/Kg - dry 0.615 3.42Dibenzofuran 4 05/05/23 00:41 V32895ANG
<0.489 mg/Kg - dry 0.489 3.421,2-Dichlorobenzene 4 05/05/23 00:41 V32895ANG
<0.503 mg/Kg - dry 0.503 3.421,3-Dichlorobenzene 4 05/05/23 00:41 V32895ANG
<0.504 mg/Kg - dry 0.504 1.711,4-Dichlorobenzene 4 05/05/23 00:41 V32895ANG
<0.760 mg/Kg - dry 0.760 3.423,3'-Dichlorobenzidine 4 05/05/23 00:41 V32895ANG
<0.495 mg/Kg - dry 0.495 3.422,4-Dichlorophenol 4 05/05/23 00:41 V32895ANG
<0.931 mg/Kg - dry 0.931 3.42Diethyl phthalate 4 05/05/23 00:41 V32895ANG
<0.900 mg/Kg - dry 0.900 3.42Dimethyl phthalate 4 05/05/23 00:41 V32895ANG
<0.558 mg/Kg - dry 0.558 1.712,4-Dimethylphenol 4 05/05/23 00:41 V32895ANG
<0.553 mg/Kg - dry 0.553 3.42Di-n-butyl phthalate 4 05/05/23 00:41 V32895ANG
<1.24 mg/Kg - dry 1.24 7.774,6-Dinitro-2-methylphenol 4 05/05/23 00:41 V32895ANG
<2.69 mg/Kg - dry 2.69 7.772,4-Dinitrophenol 4 05/05/23 00:41 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 32 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-1
95189 Matrix:
5/1/2023 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.499 mg/Kg - dry 0.499 3.422,4-Dinitrotoluene 4 05/05/23 00:41 V32895ANG
<0.558 mg/Kg - dry 0.558 3.422,6-Dinitrotoluene 4 05/05/23 00:41 V32895ANG
<0.739 mg/Kg - dry 0.739 1.71Di-n-Octyl Phthalate 4 05/05/23 00:41 V32895ANG
<0.636 mg/Kg - dry 0.636 3.42Fluoranthene 4 05/05/23 00:41 V32895ANG
<0.662 mg/Kg - dry 0.662 3.42Fluorene 4 05/05/23 00:41 V32895ANG
<0.548 mg/Kg - dry 0.548 3.42Hexachlorobenzene 4 05/05/23 00:41 V32895ANG
<0.504 mg/Kg - dry 0.504 3.42Hexachlorobutadiene 4 05/05/23 00:41 V32895ANG
<0.812 mg/Kg - dry 0.812 3.42Hexachlorocyclopentadiene 4 05/05/23 00:41 V32895ANG
<0.410 mg/Kg - dry 0.410 3.42Hexachloroethane 4 05/05/23 00:41 V32895ANG
<0.926 mg/Kg - dry 0.926 3.42Indeno(1,2,3-cd)pyrene 4 05/05/23 00:41 V32895ANG
<0.988 mg/Kg - dry 0.988 3.42Isophorone 4 05/05/23 00:41 V32895ANG
<0.548 mg/Kg - dry 0.548 3.421-Methylnaphthalene 4 05/05/23 00:41 V32895ANG
<0.517 mg/Kg - dry 0.517 3.422-Methylnaphthalene 4 05/05/23 00:41 V32895ANG
<0.501 mg/Kg - dry 0.501 3.422-Methylphenol 4 05/05/23 00:41 V32895ANG
<0.439 mg/Kg - dry 0.439 3.423&4 Methylphenol 4 05/05/23 00:41 V32895ANG
<0.745 mg/Kg - dry 0.745 3.42Naphthalene 4 05/05/23 00:41 V32895ANG
<0.500 mg/Kg - dry 0.500 3.422-Nitroaniline 4 05/05/23 00:41 V32895ANG
<0.620 mg/Kg - dry 0.620 3.423-Nitroaniline 4 05/05/23 00:41 V32895ANG
<0.482 mg/Kg - dry 0.482 1.714-Nitroaniline 4 05/05/23 00:41 V32895ANG
<0.600 mg/Kg - dry 0.600 1.71Nitrobenzene 4 05/05/23 00:41 V32895ANG
<0.459 mg/Kg - dry 0.459 3.422-Nitrophenol 4 05/05/23 00:41 V32895ANG
<0.605 mg/Kg - dry 0.605 3.424-Nitrophenol 4 05/05/23 00:41 V32895ANG
<1.36 mg/Kg - dry 1.36 3.42N-Nitrosodimethylamine 4 05/05/23 00:41 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 33 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-1
95189 Matrix:
5/1/2023 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.936 mg/Kg - dry 0.936 3.42N-Nitrosodiphenylamine 4 05/05/23 00:41 V32895ANG
<0.610 mg/Kg - dry 0.610 3.42N-Nitroso-di-n-propylamine 4 05/05/23 00:41 V32895ANG
<1.80 mg/Kg - dry 1.80 5.19Pentachlorophenol 4 05/05/23 00:41 V32895ANG
<1.08 mg/Kg - dry 1.08 3.42Phenanthrene 4 05/05/23 00:41 V32895ANG
<0.579 mg/Kg - dry 0.579 3.42Phenol 4 05/05/23 00:41 V32895ANG
3.31 J mg/Kg - dry 0.693 3.42Pyrene 4 05/05/23 00:41 V32895ANG
<0.410 mg/Kg - dry 0.410 1.71Pyridine 4 05/05/23 00:41 V32895ANG
<0.553 mg/Kg - dry 0.553 3.421,2,4-Trichlorobenzene 4 05/05/23 00:41 V32895ANG
<0.498 mg/Kg - dry 0.498 3.422,4,5-Trichlorophenol 4 05/05/23 00:41 V32895ANG
<0.499 mg/Kg - dry 0.499 3.422,4,6-Trichlorophenol 4 05/05/23 00:41 V32895ANG
8270ESurrogate: Phenol-d5 59.0 Limits: 34-121%05/05/23 00:414 ANG
Surrogate: 2-Fluorobiphenyl 70.1 Limits: 44-115%05/05/23 00:414 ANG V32895
Surrogate: 2-Fluorophenol 60.5 Limits: 35-115%05/05/23 00:414 ANG V32895
Surrogate: Nitrobenzene-d5 55.4 Limits: 37-122%05/05/23 00:414 ANG V32895
Surrogate: 4-Terphenyl-d14 79.0 Limits: 54-127%05/05/23 00:414 ANG V32895
Surrogate: 2,4,6-Tribromophenol 75.1 Limits: 39-132%05/05/23 00:414 ANG V32895
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 34 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-1
95189 Matrix:
5/1/2023 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V32729 05/03/23 10:15
3750 mg/Kg - dry 238 1290Aliphatic C9-C18 20 05/05/23 20:07 V32862AMP
1320 mg/Kg - dry 316 1290Aliphatic C19-C36 20 05/05/23 20:07 V32862AMP
2790 mg/Kg - dry 367 1290Aromatic C11-C22 20 05/05/23 20:07 V32862AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 126 Limits: 40-140%05/05/23 20:0720 AMP
MADEP-EPHSurrogate: Chlorooctadecane I *Limits: 40-140%05/05/23 20:0720 AMP
MADEP-EPHSurrogate: OTP Surrogate 63.0 Limits: 40-140%05/05/23 20:0720 AMP
Surrogate: 2-Fluorobiphenyl 130 Limits: 40-140%05/05/23 20:0720 AMP V32862
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
<1.58 mg/Kg - dry 1.58 10.3Aliphatic C5-C8 100 05/02/23 21:04 V32693TBL
238 mg/Kg - dry 5.90 10.3Aliphatic C9-C12 100 05/02/23 21:04 V32693TBL
228 mg/Kg - dry 0.807 10.3Aromatic C9-C10 100 05/02/23 21:04 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)98.9 Limits: 70-130%05/02/23 21:04100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)79.0 Limits: 70-130%05/02/23 21:04100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 35 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-2
95190 Matrix:
5/1/2023 13:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.0 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 36 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-2
95190 Matrix:
5/1/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
0.025 J mg/Kg - dry 0.003 0.027Acetone 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 05/02/23 14:21 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/02/23 14:21 V32695TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/02/23 14:21 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 05/02/23 14:21 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 05/02/23 14:21 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 05/02/23 14:21 V32695TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/02/23 14:21 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/02/23 14:21 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 05/02/23 14:21 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/02/23 14:21 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 05/02/23 14:21 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/02/23 14:21 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 37 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-2
95190 Matrix:
5/1/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 05/02/23 14:21 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/02/23 14:21 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/02/23 14:21 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006cis-1,3-Dichloropropene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/02/23 14:21 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/02/23 14:21 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 05/02/23 14:21 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/02/23 14:21 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 38 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-2
95190 Matrix:
5/1/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/02/23 14:21 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 05/02/23 14:21 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 05/02/23 14:21 V32695TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 05/02/23 14:21 V32695TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006n-Propylbenzene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/02/23 14:21 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/02/23 14:21 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,3-Trichlorobenzene 1 05/02/23 14:21 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 05/02/23 14:21 V32695TBL
<0.002 mg/Kg - dry 0.002 0.0061,1,1-Trichloroethane 1 05/02/23 14:21 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/02/23 14:21 V32695TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/02/23 14:21 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,2,3-Trichloropropane 1 05/02/23 14:21 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 05/02/23 14:21 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/02/23 14:21 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 05/02/23 14:21 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 05/02/23 14:21 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 39 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-2
95190 Matrix:
5/1/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/02/23 14:21 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/02/23 14:21 V32695
Surrogate: 4-Bromofluorobenzene 86.8 Limits: 70-130%05/02/23 14:211 TBL V32695
Surrogate: Dibromofluoromethane 105 Limits: 84-123%05/02/23 14:211 TBL V32695
Surrogate: Toluene-d8 88.9 Limits: 76-129%05/02/23 14:211 TBL V32695
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.161 mg/Kg - dry 0.161 0.916Acenaphthene 1 05/04/23 23:56 V32895ANG
<0.145 mg/Kg - dry 0.145 0.916Acenaphthylene 1 05/04/23 23:56 V32895ANG
<0.211 mg/Kg - dry 0.211 0.916Aniline 1 05/04/23 23:56 V32895ANG
<0.198 mg/Kg - dry 0.198 0.916Anthracene 1 05/04/23 23:56 V32895ANG
<0.193 mg/Kg - dry 0.193 0.916Benzo(a)anthracene 1 05/04/23 23:56 V32895ANG
<0.204 mg/Kg - dry 0.204 0.916Benzo(a)pyrene 1 05/04/23 23:56 V32895ANG
<0.202 mg/Kg - dry 0.202 0.916Benzo(b)fluoranthene 1 05/04/23 23:56 V32895ANG
<0.188 mg/Kg - dry 0.188 0.916Benzo(g,h,i)perylene 1 05/04/23 23:56 V32895ANG
<0.190 mg/Kg - dry 0.190 0.916Benzo(k)fluoranthene 1 05/04/23 23:56 V32895ANG
<0.805 mg/Kg - dry 0.805 2.78Benzoic Acid 1 05/04/23 23:56 V32895ANG
<0.145 mg/Kg - dry 0.145 0.916Benzyl alcohol 1 05/04/23 23:56 V32895ANG
<0.163 mg/Kg - dry 0.163 0.916Bis(2-Chloroethoxy)methane 1 05/04/23 23:56 V32895ANG
<0.148 mg/Kg - dry 0.148 0.916Bis(2-Chloroethyl)ether 1 05/04/23 23:56 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 40 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-2
95190 Matrix:
5/1/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.188 mg/Kg - dry 0.188 0.458Bis(2-Chloroisopropyl)ether 1 05/04/23 23:56 V32895ANG
<0.166 mg/Kg - dry 0.166 0.916Bis(2-ethylhexyl)phthalate 1 05/04/23 23:56 V32895ANG
<0.151 mg/Kg - dry 0.151 0.9164-Bromophenyl phenyl ether 1 05/04/23 23:56 V32895ANG
<0.156 mg/Kg - dry 0.156 0.458Butyl benzyl phthalate 1 05/04/23 23:56 V32895ANG
<0.128 mg/Kg - dry 0.128 0.9164-Chloro-3-methylphenol 1 05/04/23 23:56 V32895ANG
<0.155 mg/Kg - dry 0.155 0.4584-Chloroaniline 1 05/04/23 23:56 V32895ANG
<0.161 mg/Kg - dry 0.161 0.9162-Chloronaphthalene 1 05/04/23 23:56 V32895ANG
<0.136 mg/Kg - dry 0.136 0.9162-Chlorophenol 1 05/04/23 23:56 V32895ANG
<0.175 mg/Kg - dry 0.175 1.394-Chlorophenyl phenyl ether 1 05/04/23 23:56 V32895ANG
<0.197 mg/Kg - dry 0.197 0.916Chrysene 1 05/04/23 23:56 V32895ANG
<0.319 mg/Kg - dry 0.319 0.916Dibenz(a,h)anthracene 1 05/04/23 23:56 V32895ANG
<0.165 mg/Kg - dry 0.165 0.916Dibenzofuran 1 05/04/23 23:56 V32895ANG
<0.131 mg/Kg - dry 0.131 0.9161,2-Dichlorobenzene 1 05/04/23 23:56 V32895ANG
<0.135 mg/Kg - dry 0.135 0.9161,3-Dichlorobenzene 1 05/04/23 23:56 V32895ANG
<0.135 mg/Kg - dry 0.135 0.4581,4-Dichlorobenzene 1 05/04/23 23:56 V32895ANG
<0.204 mg/Kg - dry 0.204 0.9163,3'-Dichlorobenzidine 1 05/04/23 23:56 V32895ANG
<0.133 mg/Kg - dry 0.133 0.9162,4-Dichlorophenol 1 05/04/23 23:56 V32895ANG
<0.250 mg/Kg - dry 0.250 0.916Diethyl phthalate 1 05/04/23 23:56 V32895ANG
<0.241 mg/Kg - dry 0.241 0.916Dimethyl phthalate 1 05/04/23 23:56 V32895ANG
<0.150 mg/Kg - dry 0.150 0.4582,4-Dimethylphenol 1 05/04/23 23:56 V32895ANG
<0.148 mg/Kg - dry 0.148 0.916Di-n-butyl phthalate 1 05/04/23 23:56 V32895ANG
<0.333 mg/Kg - dry 0.333 2.084,6-Dinitro-2-methylphenol 1 05/04/23 23:56 V32895ANG
<0.722 mg/Kg - dry 0.722 2.082,4-Dinitrophenol 1 05/04/23 23:56 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 41 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-2
95190 Matrix:
5/1/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.134 mg/Kg - dry 0.134 0.9162,4-Dinitrotoluene 1 05/04/23 23:56 V32895ANG
<0.150 mg/Kg - dry 0.150 0.9162,6-Dinitrotoluene 1 05/04/23 23:56 V32895ANG
<0.198 mg/Kg - dry 0.198 0.458Di-n-Octyl Phthalate 1 05/04/23 23:56 V32895ANG
<0.170 mg/Kg - dry 0.170 0.916Fluoranthene 1 05/04/23 23:56 V32895ANG
<0.177 mg/Kg - dry 0.177 0.916Fluorene 1 05/04/23 23:56 V32895ANG
<0.147 mg/Kg - dry 0.147 0.916Hexachlorobenzene 1 05/04/23 23:56 V32895ANG
<0.135 mg/Kg - dry 0.135 0.916Hexachlorobutadiene 1 05/04/23 23:56 V32895ANG
<0.218 mg/Kg - dry 0.218 0.916Hexachlorocyclopentadiene 1 05/04/23 23:56 V32895ANG
<0.110 mg/Kg - dry 0.110 0.916Hexachloroethane 1 05/04/23 23:56 V32895ANG
<0.248 mg/Kg - dry 0.248 0.916Indeno(1,2,3-cd)pyrene 1 05/04/23 23:56 V32895ANG
<0.265 mg/Kg - dry 0.265 0.916Isophorone 1 05/04/23 23:56 V32895ANG
<0.147 mg/Kg - dry 0.147 0.9161-Methylnaphthalene 1 05/04/23 23:56 V32895ANG
<0.138 mg/Kg - dry 0.138 0.9162-Methylnaphthalene 1 05/04/23 23:56 V32895ANG
<0.134 mg/Kg - dry 0.134 0.9162-Methylphenol 1 05/04/23 23:56 V32895ANG
<0.117 mg/Kg - dry 0.117 0.9163&4 Methylphenol 1 05/04/23 23:56 V32895ANG
<0.200 mg/Kg - dry 0.200 0.916Naphthalene 1 05/04/23 23:56 V32895ANG
<0.134 mg/Kg - dry 0.134 0.9162-Nitroaniline 1 05/04/23 23:56 V32895ANG
<0.166 mg/Kg - dry 0.166 0.9163-Nitroaniline 1 05/04/23 23:56 V32895ANG
<0.129 mg/Kg - dry 0.129 0.4584-Nitroaniline 1 05/04/23 23:56 V32895ANG
<0.161 mg/Kg - dry 0.161 0.458Nitrobenzene 1 05/04/23 23:56 V32895ANG
<0.123 mg/Kg - dry 0.123 0.9162-Nitrophenol 1 05/04/23 23:56 V32895ANG
<0.162 mg/Kg - dry 0.162 0.9164-Nitrophenol 1 05/04/23 23:56 V32895ANG
<0.365 mg/Kg - dry 0.365 0.916N-Nitrosodimethylamine 1 05/04/23 23:56 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 42 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-2
95190 Matrix:
5/1/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.251 mg/Kg - dry 0.251 0.916N-Nitrosodiphenylamine 1 05/04/23 23:56 V32895ANG
<0.163 mg/Kg - dry 0.163 0.916N-Nitroso-di-n-propylamine 1 05/04/23 23:56 V32895ANG
<0.481 mg/Kg - dry 0.481 1.39Pentachlorophenol 1 05/04/23 23:56 V32895ANG
<0.288 mg/Kg - dry 0.288 0.916Phenanthrene 1 05/04/23 23:56 V32895ANG
<0.155 mg/Kg - dry 0.155 0.916Phenol 1 05/04/23 23:56 V32895ANG
<0.186 mg/Kg - dry 0.186 0.916Pyrene 1 05/04/23 23:56 V32895ANG
<0.110 mg/Kg - dry 0.110 0.458Pyridine 1 05/04/23 23:56 V32895ANG
<0.148 mg/Kg - dry 0.148 0.9161,2,4-Trichlorobenzene 1 05/04/23 23:56 V32895ANG
<0.133 mg/Kg - dry 0.133 0.9162,4,5-Trichlorophenol 1 05/04/23 23:56 V32895ANG
<0.134 mg/Kg - dry 0.134 0.9162,4,6-Trichlorophenol 1 05/04/23 23:56 V32895ANG
8270ESurrogate: Phenol-d5 64.3 Limits: 34-121%05/04/23 23:561 ANG
Surrogate: 2-Fluorobiphenyl 68.3 Limits: 44-115%05/04/23 23:561 ANG V32895
Surrogate: 2-Fluorophenol 69.1 Limits: 35-115%05/04/23 23:561 ANG V32895
Surrogate: Nitrobenzene-d5 65.9 Limits: 37-122%05/04/23 23:561 ANG V32895
Surrogate: 4-Terphenyl-d14 70.1 Limits: 54-127%05/04/23 23:561 ANG V32895
Surrogate: 2,4,6-Tribromophenol 67.9 Limits: 39-132%05/04/23 23:561 ANG V32895
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 43 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-2
95190 Matrix:
5/1/2023 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V32729 05/03/23 10:15
83.5 mg/Kg - dry 12.8 69.3Aliphatic C9-C18 1 05/05/23 17:42 V32862AMP
52.8 J mg/Kg - dry 16.9 69.3Aliphatic C19-C36 1 05/05/23 17:42 V32862AMP
77.8 mg/Kg - dry 19.7 69.3Aromatic C11-C22 1 05/05/23 17:42 V32862AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 101 Limits: 40-140%05/05/23 17:421 AMP
MADEP-EPHSurrogate: Chlorooctadecane 69.3 Limits: 40-140%05/05/23 17:421 AMP
MADEP-EPHSurrogate: OTP Surrogate 76.4 Limits: 40-140%05/05/23 17:421 AMP
Surrogate: 2-Fluorobiphenyl 100 Limits: 40-140%05/05/23 17:421 AMP V32862
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
<1.69 mg/Kg - dry 1.69 11.1Aliphatic C5-C8 100 05/02/23 18:42 V32693TBL
<6.33 mg/Kg - dry 6.33 11.1Aliphatic C9-C12 100 05/02/23 18:42 V32693TBL
<0.866 mg/Kg - dry 0.866 11.1Aromatic C9-C10 100 05/02/23 18:42 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)88.5 Limits: 70-130%05/02/23 18:42100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)111 Limits: 70-130%05/02/23 18:42100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 44 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-3
95191 Matrix:
5/1/2023 13:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.5 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 45 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-3
95191 Matrix:
5/1/2023 13:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
0.007 J mg/Kg - dry 0.003 0.026Acetone 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/02/23 14:48 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/02/23 14:48 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/02/23 14:48 V32695TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/02/23 14:48 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 05/02/23 14:48 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/02/23 14:48 V32695TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/02/23 14:48 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/02/23 14:48 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/02/23 14:48 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/02/23 14:48 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/02/23 14:48 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/02/23 14:48 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 46 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-3
95191 Matrix:
5/1/2023 13:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 05/02/23 14:48 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/02/23 14:48 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/02/23 14:48 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/02/23 14:48 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/02/23 14:48 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/02/23 14:48 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/02/23 14:48 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/02/23 14:48 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/02/23 14:48 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/02/23 14:48 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 47 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-3
95191 Matrix:
5/1/2023 13:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/02/23 14:48 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/02/23 14:48 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/02/23 14:48 V32695TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/02/23 14:48 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/02/23 14:48 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/02/23 14:48 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/02/23 14:48 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/02/23 14:48 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/02/23 14:48 V32695TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/02/23 14:48 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/02/23 14:48 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/02/23 14:48 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 05/02/23 14:48 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 48 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-3
95191 Matrix:
5/1/2023 13:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/02/23 14:48 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/02/23 14:48 V32695
Surrogate: 4-Bromofluorobenzene 87.7 Limits: 70-130%05/02/23 14:481 TBL V32695
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/02/23 14:481 TBL V32695
Surrogate: Toluene-d8 88.1 Limits: 76-129%05/02/23 14:481 TBL V32695
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.153 mg/Kg - dry 0.153 0.874Acenaphthene 1 05/04/23 22:26 V32895ANG
<0.139 mg/Kg - dry 0.139 0.874Acenaphthylene 1 05/04/23 22:26 V32895ANG
<0.201 mg/Kg - dry 0.201 0.874Aniline 1 05/04/23 22:26 V32895ANG
<0.189 mg/Kg - dry 0.189 0.874Anthracene 1 05/04/23 22:26 V32895ANG
<0.184 mg/Kg - dry 0.184 0.874Benzo(a)anthracene 1 05/04/23 22:26 V32895ANG
<0.194 mg/Kg - dry 0.194 0.874Benzo(a)pyrene 1 05/04/23 22:26 V32895ANG
<0.193 mg/Kg - dry 0.193 0.874Benzo(b)fluoranthene 1 05/04/23 22:26 V32895ANG
<0.180 mg/Kg - dry 0.180 0.874Benzo(g,h,i)perylene 1 05/04/23 22:26 V32895ANG
<0.181 mg/Kg - dry 0.181 0.874Benzo(k)fluoranthene 1 05/04/23 22:26 V32895ANG
<0.768 mg/Kg - dry 0.768 2.65Benzoic Acid 1 05/04/23 22:26 V32895ANG
<0.139 mg/Kg - dry 0.139 0.874Benzyl alcohol 1 05/04/23 22:26 V32895ANG
<0.156 mg/Kg - dry 0.156 0.874Bis(2-Chloroethoxy)methane 1 05/04/23 22:26 V32895ANG
<0.141 mg/Kg - dry 0.141 0.874Bis(2-Chloroethyl)ether 1 05/04/23 22:26 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 49 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-3
95191 Matrix:
5/1/2023 13:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.180 mg/Kg - dry 0.180 0.437Bis(2-Chloroisopropyl)ether 1 05/04/23 22:26 V32895ANG
<0.158 mg/Kg - dry 0.158 0.874Bis(2-ethylhexyl)phthalate 1 05/04/23 22:26 V32895ANG
<0.144 mg/Kg - dry 0.144 0.8744-Bromophenyl phenyl ether 1 05/04/23 22:26 V32895ANG
<0.149 mg/Kg - dry 0.149 0.437Butyl benzyl phthalate 1 05/04/23 22:26 V32895ANG
<0.122 mg/Kg - dry 0.122 0.8744-Chloro-3-methylphenol 1 05/04/23 22:26 V32895ANG
<0.148 mg/Kg - dry 0.148 0.4374-Chloroaniline 1 05/04/23 22:26 V32895ANG
<0.153 mg/Kg - dry 0.153 0.8742-Chloronaphthalene 1 05/04/23 22:26 V32895ANG
<0.130 mg/Kg - dry 0.130 0.8742-Chlorophenol 1 05/04/23 22:26 V32895ANG
<0.166 mg/Kg - dry 0.166 1.324-Chlorophenyl phenyl ether 1 05/04/23 22:26 V32895ANG
<0.188 mg/Kg - dry 0.188 0.874Chrysene 1 05/04/23 22:26 V32895ANG
<0.304 mg/Kg - dry 0.304 0.874Dibenz(a,h)anthracene 1 05/04/23 22:26 V32895ANG
<0.157 mg/Kg - dry 0.157 0.874Dibenzofuran 1 05/04/23 22:26 V32895ANG
<0.125 mg/Kg - dry 0.125 0.8741,2-Dichlorobenzene 1 05/04/23 22:26 V32895ANG
<0.128 mg/Kg - dry 0.128 0.8741,3-Dichlorobenzene 1 05/04/23 22:26 V32895ANG
<0.129 mg/Kg - dry 0.129 0.4371,4-Dichlorobenzene 1 05/04/23 22:26 V32895ANG
<0.194 mg/Kg - dry 0.194 0.8743,3'-Dichlorobenzidine 1 05/04/23 22:26 V32895ANG
<0.126 mg/Kg - dry 0.126 0.8742,4-Dichlorophenol 1 05/04/23 22:26 V32895ANG
<0.238 mg/Kg - dry 0.238 0.874Diethyl phthalate 1 05/04/23 22:26 V32895ANG
<0.230 mg/Kg - dry 0.230 0.874Dimethyl phthalate 1 05/04/23 22:26 V32895ANG
<0.143 mg/Kg - dry 0.143 0.4372,4-Dimethylphenol 1 05/04/23 22:26 V32895ANG
<0.141 mg/Kg - dry 0.141 0.874Di-n-butyl phthalate 1 05/04/23 22:26 V32895ANG
<0.317 mg/Kg - dry 0.317 1.994,6-Dinitro-2-methylphenol 1 05/04/23 22:26 V32895ANG
<0.688 mg/Kg - dry 0.688 1.992,4-Dinitrophenol 1 05/04/23 22:26 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 50 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-3
95191 Matrix:
5/1/2023 13:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.127 mg/Kg - dry 0.127 0.8742,4-Dinitrotoluene 1 05/04/23 22:26 V32895ANG
<0.143 mg/Kg - dry 0.143 0.8742,6-Dinitrotoluene 1 05/04/23 22:26 V32895ANG
<0.189 mg/Kg - dry 0.189 0.437Di-n-Octyl Phthalate 1 05/04/23 22:26 V32895ANG
<0.162 mg/Kg - dry 0.162 0.874Fluoranthene 1 05/04/23 22:26 V32895ANG
<0.169 mg/Kg - dry 0.169 0.874Fluorene 1 05/04/23 22:26 V32895ANG
<0.140 mg/Kg - dry 0.140 0.874Hexachlorobenzene 1 05/04/23 22:26 V32895ANG
<0.129 mg/Kg - dry 0.129 0.874Hexachlorobutadiene 1 05/04/23 22:26 V32895ANG
<0.207 mg/Kg - dry 0.207 0.874Hexachlorocyclopentadiene 1 05/04/23 22:26 V32895ANG
<0.104 mg/Kg - dry 0.104 0.874Hexachloroethane 1 05/04/23 22:26 V32895ANG
<0.237 mg/Kg - dry 0.237 0.874Indeno(1,2,3-cd)pyrene 1 05/04/23 22:26 V32895ANG
<0.252 mg/Kg - dry 0.252 0.874Isophorone 1 05/04/23 22:26 V32895ANG
<0.140 mg/Kg - dry 0.140 0.8741-Methylnaphthalene 1 05/04/23 22:26 V32895ANG
<0.132 mg/Kg - dry 0.132 0.8742-Methylnaphthalene 1 05/04/23 22:26 V32895ANG
<0.128 mg/Kg - dry 0.128 0.8742-Methylphenol 1 05/04/23 22:26 V32895ANG
<0.112 mg/Kg - dry 0.112 0.8743&4 Methylphenol 1 05/04/23 22:26 V32895ANG
<0.190 mg/Kg - dry 0.190 0.874Naphthalene 1 05/04/23 22:26 V32895ANG
<0.128 mg/Kg - dry 0.128 0.8742-Nitroaniline 1 05/04/23 22:26 V32895ANG
<0.158 mg/Kg - dry 0.158 0.8743-Nitroaniline 1 05/04/23 22:26 V32895ANG
<0.123 mg/Kg - dry 0.123 0.4374-Nitroaniline 1 05/04/23 22:26 V32895ANG
<0.153 mg/Kg - dry 0.153 0.437Nitrobenzene 1 05/04/23 22:26 V32895ANG
<0.117 mg/Kg - dry 0.117 0.8742-Nitrophenol 1 05/04/23 22:26 V32895ANG
<0.154 mg/Kg - dry 0.154 0.8744-Nitrophenol 1 05/04/23 22:26 V32895ANG
<0.348 mg/Kg - dry 0.348 0.874N-Nitrosodimethylamine 1 05/04/23 22:26 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 51 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-3
95191 Matrix:
5/1/2023 13:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.239 mg/Kg - dry 0.239 0.874N-Nitrosodiphenylamine 1 05/04/23 22:26 V32895ANG
<0.156 mg/Kg - dry 0.156 0.874N-Nitroso-di-n-propylamine 1 05/04/23 22:26 V32895ANG
<0.459 mg/Kg - dry 0.459 1.32Pentachlorophenol 1 05/04/23 22:26 V32895ANG
<0.275 mg/Kg - dry 0.275 0.874Phenanthrene 1 05/04/23 22:26 V32895ANG
<0.148 mg/Kg - dry 0.148 0.874Phenol 1 05/04/23 22:26 V32895ANG
<0.177 mg/Kg - dry 0.177 0.874Pyrene 1 05/04/23 22:26 V32895ANG
<0.104 mg/Kg - dry 0.104 0.437Pyridine 1 05/04/23 22:26 V32895ANG
<0.141 mg/Kg - dry 0.141 0.8741,2,4-Trichlorobenzene 1 05/04/23 22:26 V32895ANG
<0.127 mg/Kg - dry 0.127 0.8742,4,5-Trichlorophenol 1 05/04/23 22:26 V32895ANG
<0.127 mg/Kg - dry 0.127 0.8742,4,6-Trichlorophenol 1 05/04/23 22:26 V32895ANG
8270ESurrogate: Phenol-d5 64.0 Limits: 34-121%05/04/23 22:261 ANG
Surrogate: 2-Fluorobiphenyl 72.5 Limits: 44-115%05/04/23 22:261 ANG V32895
Surrogate: 2-Fluorophenol 66.7 Limits: 35-115%05/04/23 22:261 ANG V32895
Surrogate: Nitrobenzene-d5 64.7 Limits: 37-122%05/04/23 22:261 ANG V32895
Surrogate: 4-Terphenyl-d14 78.4 Limits: 54-127%05/04/23 22:261 ANG V32895
Surrogate: 2,4,6-Tribromophenol 73.6 Limits: 39-132%05/04/23 22:261 ANG V32895
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 52 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-3
95191 Matrix:
5/1/2023 13:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V32729 05/03/23 10:15
42.9 J mg/Kg - dry 12.2 66.1Aliphatic C9-C18 1 05/05/23 18:18 V32862AMP
21.3 J mg/Kg - dry 16.2 66.1Aliphatic C19-C36 1 05/05/23 18:18 V32862AMP
24.0 J mg/Kg - dry 18.8 66.1Aromatic C11-C22 1 05/05/23 18:18 V32862AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 100 Limits: 40-140%05/05/23 18:181 AMP
MADEP-EPHSurrogate: Chlorooctadecane 75.3 Limits: 40-140%05/05/23 18:181 AMP
MADEP-EPHSurrogate: OTP Surrogate 82.7 Limits: 40-140%05/05/23 18:181 AMP
Surrogate: 2-Fluorobiphenyl 97.7 Limits: 40-140%05/05/23 18:181 AMP V32862
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
<1.97 mg/Kg - dry 1.97 13.0Aliphatic C5-C8 100 05/02/23 19:05 V32693TBL
<7.42 mg/Kg - dry 7.42 13.0Aliphatic C9-C12 100 05/02/23 19:05 V32693TBL
<1.02 mg/Kg - dry 1.02 13.0Aromatic C9-C10 100 05/02/23 19:05 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)84.5 Limits: 70-130%05/02/23 19:05100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)116 Limits: 70-130%05/02/23 19:05100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 53 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-4
95192 Matrix:
5/1/2023 13:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.3 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 54 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-4
95192 Matrix:
5/1/2023 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
0.012 J mg/Kg - dry 0.003 0.025Acetone 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 05/02/23 15:15 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/02/23 15:15 V32695TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 05/02/23 15:15 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/02/23 15:15 V32695TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/02/23 15:15 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/02/23 15:15 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/02/23 15:15 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/02/23 15:15 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 05/02/23 15:15 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 55 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-4
95192 Matrix:
5/1/2023 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 05/02/23 15:15 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/02/23 15:15 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/02/23 15:15 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/02/23 15:15 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/02/23 15:15 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 05/02/23 15:15 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 05/02/23 15:15 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/02/23 15:15 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 56 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-4
95192 Matrix:
5/1/2023 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/02/23 15:15 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 05/02/23 15:15 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/02/23 15:15 V32695TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/02/23 15:15 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/02/23 15:15 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/02/23 15:15 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/02/23 15:15 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/02/23 15:15 V32695TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/02/23 15:15 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/02/23 15:15 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/02/23 15:15 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 57 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-4
95192 Matrix:
5/1/2023 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/02/23 15:15 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/02/23 15:15 V32695
Surrogate: 4-Bromofluorobenzene 114 Limits: 70-130%05/02/23 15:151 TBL V32695
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/02/23 15:151 TBL V32695
Surrogate: Toluene-d8 86.9 Limits: 76-129%05/02/23 15:151 TBL V32695
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.149 mg/Kg - dry 0.149 0.849Acenaphthene 1 05/04/23 22:48 V32895ANG
<0.135 mg/Kg - dry 0.135 0.849Acenaphthylene 1 05/04/23 22:48 V32895ANG
<0.195 mg/Kg - dry 0.195 0.849Aniline 1 05/04/23 22:48 V32895ANG
<0.184 mg/Kg - dry 0.184 0.849Anthracene 1 05/04/23 22:48 V32895ANG
<0.178 mg/Kg - dry 0.178 0.849Benzo(a)anthracene 1 05/04/23 22:48 V32895ANG
<0.189 mg/Kg - dry 0.189 0.849Benzo(a)pyrene 1 05/04/23 22:48 V32895ANG
<0.187 mg/Kg - dry 0.187 0.849Benzo(b)fluoranthene 1 05/04/23 22:48 V32895ANG
<0.175 mg/Kg - dry 0.175 0.849Benzo(g,h,i)perylene 1 05/04/23 22:48 V32895ANG
<0.176 mg/Kg - dry 0.176 0.849Benzo(k)fluoranthene 1 05/04/23 22:48 V32895ANG
<0.746 mg/Kg - dry 0.746 2.57Benzoic Acid 1 05/04/23 22:48 V32895ANG
<0.135 mg/Kg - dry 0.135 0.849Benzyl alcohol 1 05/04/23 22:48 V32895ANG
<0.151 mg/Kg - dry 0.151 0.849Bis(2-Chloroethoxy)methane 1 05/04/23 22:48 V32895ANG
<0.137 mg/Kg - dry 0.137 0.849Bis(2-Chloroethyl)ether 1 05/04/23 22:48 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 58 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-4
95192 Matrix:
5/1/2023 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.175 mg/Kg - dry 0.175 0.424Bis(2-Chloroisopropyl)ether 1 05/04/23 22:48 V32895ANG
<0.154 mg/Kg - dry 0.154 0.849Bis(2-ethylhexyl)phthalate 1 05/04/23 22:48 V32895ANG
<0.140 mg/Kg - dry 0.140 0.8494-Bromophenyl phenyl ether 1 05/04/23 22:48 V32895ANG
<0.145 mg/Kg - dry 0.145 0.424Butyl benzyl phthalate 1 05/04/23 22:48 V32895ANG
<0.118 mg/Kg - dry 0.118 0.8494-Chloro-3-methylphenol 1 05/04/23 22:48 V32895ANG
<0.144 mg/Kg - dry 0.144 0.4244-Chloroaniline 1 05/04/23 22:48 V32895ANG
<0.149 mg/Kg - dry 0.149 0.8492-Chloronaphthalene 1 05/04/23 22:48 V32895ANG
<0.126 mg/Kg - dry 0.126 0.8492-Chlorophenol 1 05/04/23 22:48 V32895ANG
<0.162 mg/Kg - dry 0.162 1.294-Chlorophenyl phenyl ether 1 05/04/23 22:48 V32895ANG
<0.182 mg/Kg - dry 0.182 0.849Chrysene 1 05/04/23 22:48 V32895ANG
<0.296 mg/Kg - dry 0.296 0.849Dibenz(a,h)anthracene 1 05/04/23 22:48 V32895ANG
<0.153 mg/Kg - dry 0.153 0.849Dibenzofuran 1 05/04/23 22:48 V32895ANG
<0.121 mg/Kg - dry 0.121 0.8491,2-Dichlorobenzene 1 05/04/23 22:48 V32895ANG
<0.125 mg/Kg - dry 0.125 0.8491,3-Dichlorobenzene 1 05/04/23 22:48 V32895ANG
<0.125 mg/Kg - dry 0.125 0.4241,4-Dichlorobenzene 1 05/04/23 22:48 V32895ANG
<0.189 mg/Kg - dry 0.189 0.8493,3'-Dichlorobenzidine 1 05/04/23 22:48 V32895ANG
<0.123 mg/Kg - dry 0.123 0.8492,4-Dichlorophenol 1 05/04/23 22:48 V32895ANG
<0.231 mg/Kg - dry 0.231 0.849Diethyl phthalate 1 05/04/23 22:48 V32895ANG
<0.223 mg/Kg - dry 0.223 0.849Dimethyl phthalate 1 05/04/23 22:48 V32895ANG
<0.138 mg/Kg - dry 0.138 0.4242,4-Dimethylphenol 1 05/04/23 22:48 V32895ANG
<0.137 mg/Kg - dry 0.137 0.849Di-n-butyl phthalate 1 05/04/23 22:48 V32895ANG
<0.308 mg/Kg - dry 0.308 1.934,6-Dinitro-2-methylphenol 1 05/04/23 22:48 V32895ANG
<0.669 mg/Kg - dry 0.669 1.932,4-Dinitrophenol 1 05/04/23 22:48 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 59 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-4
95192 Matrix:
5/1/2023 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.124 mg/Kg - dry 0.124 0.8492,4-Dinitrotoluene 1 05/04/23 22:48 V32895ANG
<0.138 mg/Kg - dry 0.138 0.8492,6-Dinitrotoluene 1 05/04/23 22:48 V32895ANG
<0.184 mg/Kg - dry 0.184 0.424Di-n-Octyl Phthalate 1 05/04/23 22:48 V32895ANG
<0.158 mg/Kg - dry 0.158 0.849Fluoranthene 1 05/04/23 22:48 V32895ANG
<0.164 mg/Kg - dry 0.164 0.849Fluorene 1 05/04/23 22:48 V32895ANG
<0.136 mg/Kg - dry 0.136 0.849Hexachlorobenzene 1 05/04/23 22:48 V32895ANG
<0.125 mg/Kg - dry 0.125 0.849Hexachlorobutadiene 1 05/04/23 22:48 V32895ANG
<0.202 mg/Kg - dry 0.202 0.849Hexachlorocyclopentadiene 1 05/04/23 22:48 V32895ANG
<0.101 mg/Kg - dry 0.101 0.849Hexachloroethane 1 05/04/23 22:48 V32895ANG
<0.230 mg/Kg - dry 0.230 0.849Indeno(1,2,3-cd)pyrene 1 05/04/23 22:48 V32895ANG
<0.245 mg/Kg - dry 0.245 0.849Isophorone 1 05/04/23 22:48 V32895ANG
<0.136 mg/Kg - dry 0.136 0.8491-Methylnaphthalene 1 05/04/23 22:48 V32895ANG
<0.128 mg/Kg - dry 0.128 0.8492-Methylnaphthalene 1 05/04/23 22:48 V32895ANG
<0.124 mg/Kg - dry 0.124 0.8492-Methylphenol 1 05/04/23 22:48 V32895ANG
<0.109 mg/Kg - dry 0.109 0.8493&4 Methylphenol 1 05/04/23 22:48 V32895ANG
<0.185 mg/Kg - dry 0.185 0.849Naphthalene 1 05/04/23 22:48 V32895ANG
<0.124 mg/Kg - dry 0.124 0.8492-Nitroaniline 1 05/04/23 22:48 V32895ANG
<0.154 mg/Kg - dry 0.154 0.8493-Nitroaniline 1 05/04/23 22:48 V32895ANG
<0.120 mg/Kg - dry 0.120 0.4244-Nitroaniline 1 05/04/23 22:48 V32895ANG
<0.149 mg/Kg - dry 0.149 0.424Nitrobenzene 1 05/04/23 22:48 V32895ANG
<0.114 mg/Kg - dry 0.114 0.8492-Nitrophenol 1 05/04/23 22:48 V32895ANG
<0.150 mg/Kg - dry 0.150 0.8494-Nitrophenol 1 05/04/23 22:48 V32895ANG
<0.338 mg/Kg - dry 0.338 0.849N-Nitrosodimethylamine 1 05/04/23 22:48 V32895ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 60 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-4
95192 Matrix:
5/1/2023 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32769 05/04/23 09:50
<0.232 mg/Kg - dry 0.232 0.849N-Nitrosodiphenylamine 1 05/04/23 22:48 V32895ANG
<0.151 mg/Kg - dry 0.151 0.849N-Nitroso-di-n-propylamine 1 05/04/23 22:48 V32895ANG
<0.446 mg/Kg - dry 0.446 1.29Pentachlorophenol 1 05/04/23 22:48 V32895ANG
<0.267 mg/Kg - dry 0.267 0.849Phenanthrene 1 05/04/23 22:48 V32895ANG
<0.144 mg/Kg - dry 0.144 0.849Phenol 1 05/04/23 22:48 V32895ANG
<0.172 mg/Kg - dry 0.172 0.849Pyrene 1 05/04/23 22:48 V32895ANG
<0.101 mg/Kg - dry 0.101 0.424Pyridine 1 05/04/23 22:48 V32895ANG
<0.137 mg/Kg - dry 0.137 0.8491,2,4-Trichlorobenzene 1 05/04/23 22:48 V32895ANG
<0.123 mg/Kg - dry 0.123 0.8492,4,5-Trichlorophenol 1 05/04/23 22:48 V32895ANG
<0.124 mg/Kg - dry 0.124 0.8492,4,6-Trichlorophenol 1 05/04/23 22:48 V32895ANG
8270ESurrogate: Phenol-d5 66.1 Limits: 34-121%05/04/23 22:481 ANG
Surrogate: 2-Fluorobiphenyl 73.7 Limits: 44-115%05/04/23 22:481 ANG V32895
Surrogate: 2-Fluorophenol 70.9 Limits: 35-115%05/04/23 22:481 ANG V32895
Surrogate: Nitrobenzene-d5 67.7 Limits: 37-122%05/04/23 22:481 ANG V32895
Surrogate: 4-Terphenyl-d14 77.8 Limits: 54-127%05/04/23 22:481 ANG V32895
Surrogate: 2,4,6-Tribromophenol 73.6 Limits: 39-132%05/04/23 22:481 ANG V32895
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 61 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-121-0017
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 05/01/2023
Winecoff Village
Report Date : 05/08/2023
Sample ID :
Lab No :
Sampled:SW-4
95192 Matrix:
5/1/2023 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V32729 05/03/23 10:15
<11.8 mg/Kg - dry 11.8 64.2Aliphatic C9-C18 1 05/05/23 18:55 V32862AMP
<15.7 mg/Kg - dry 15.7 64.2Aliphatic C19-C36 1 05/05/23 18:55 V32862AMP
<18.3 mg/Kg - dry 18.3 64.2Aromatic C11-C22 1 05/05/23 18:55 V32862AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 112 Limits: 40-140%05/05/23 18:551 AMP
MADEP-EPHSurrogate: Chlorooctadecane 69.2 Limits: 40-140%05/05/23 18:551 AMP
MADEP-EPHSurrogate: OTP Surrogate 89.6 Limits: 40-140%05/05/23 18:551 AMP
Surrogate: 2-Fluorobiphenyl 112 Limits: 40-140%05/05/23 18:551 AMP V32862
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
<1.66 mg/Kg - dry 1.66 11.0Aliphatic C5-C8 100 05/02/23 19:29 V32693TBL
<6.24 mg/Kg - dry 6.24 11.0Aliphatic C9-C12 100 05/02/23 19:29 V32693TBL
<0.854 mg/Kg - dry 0.854 11.0Aromatic C9-C10 100 05/02/23 19:29 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)90.6 Limits: 70-130%05/02/23 19:29100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)91.8 Limits: 70-130%05/02/23 19:29100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJRecovery out of rangeI
Method Quantitation LimitMQL
Page 62 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V32744QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32678
Associated Lab Samples: 95187
LRB-V32678 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/04/23 09:3010.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
05/04/23 09:30OTP Surrogate (S)86.4 31-123
LCS-V32678 LCSD-V32678Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
74.8 11210469.566.7mg/KgDiesel Range Organics (C10-C28)46-126 7.3 20
96.291.7OTP Surrogate (S)31-123
Page 1 of 23Date:05/08/2023 03:34 PM
Page 63 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V32699QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V32698
Associated Lab Samples: 95187
LRB-V32698 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 16:145.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
05/02/23 16:14a,a,a-Trifluorotoluene (S)110 50-137
LCS-V32698 LCSD-V32698Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
59.7 11911155.450.0mg/KgGasoline Range Organics (C6-C10)41-138 7.4 20
107116a,a,a-Trifluorotoluene (S)50-137
Page 2 of 23Date:05/08/2023 03:34 PM
Page 64 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
Associated Lab Samples: 95188, 95189, 95190, 95191, 95192
LRB-V32694 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 11:110.0200.002<0.002mg/KgAcetone
05/02/23 11:110.0200.001<0.001mg/KgAcrolein
05/02/23 11:110.0200.0008<0.0008mg/KgAcrylonitrile
05/02/23 11:110.0050.0006<0.0006mg/KgBenzene
05/02/23 11:110.0050.0005<0.0005mg/KgBromobenzene
05/02/23 11:110.0050.0008<0.0008mg/KgBromochloromethane
05/02/23 11:110.0050.001<0.001mg/KgBromodichloromethane
05/02/23 11:110.0050.001<0.001mg/KgBromoform
05/02/23 11:110.0100.001<0.001mg/KgBromomethane
05/02/23 11:110.0050.0005<0.0005mg/Kgn-Butylbenzene
05/02/23 11:110.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/02/23 11:110.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/02/23 11:110.0050.0006<0.0006mg/KgCarbon Disulfide
05/02/23 11:110.0050.001<0.001mg/KgCarbon Tetrachloride
05/02/23 11:110.0050.0007<0.0007mg/KgChlorobenzene
05/02/23 11:110.0050.0009<0.0009mg/KgChlorodibromomethane
05/02/23 11:110.0100.0009<0.0009mg/KgChloroethane
05/02/23 11:110.0050.001<0.001mg/KgChloroform
05/02/23 11:110.0100.0006<0.0006mg/KgChloromethane
05/02/23 11:110.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/02/23 11:110.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/02/23 11:110.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/02/23 11:110.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/02/23 11:110.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/02/23 11:110.0050.0006<0.0006mg/KgDibromomethane
05/02/23 11:110.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/02/23 11:110.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 3 of 23Date:05/08/2023 03:34 PM
Page 65 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
Associated Lab Samples: 95188, 95189, 95190, 95191, 95192
LRB-V32694 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 11:110.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/02/23 11:110.0100.001<0.001mg/KgDichlorodifluoromethane
05/02/23 11:110.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/02/23 11:110.0050.001<0.001mg/Kg1,2-Dichloroethane
05/02/23 11:110.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/02/23 11:110.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/02/23 11:110.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/02/23 11:110.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/02/23 11:110.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/02/23 11:110.0050.001<0.001mg/Kg2,2-Dichloropropane
05/02/23 11:110.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/02/23 11:110.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/02/23 11:110.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/02/23 11:110.0050.0006<0.0006mg/KgEthylbenzene
05/02/23 11:110.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/02/23 11:110.0100.0008<0.0008mg/KgHexachlorobutadiene
05/02/23 11:110.0100.0007<0.0007mg/Kgn-Hexane
05/02/23 11:110.0200.0006<0.0006mg/Kg2-Hexanone
05/02/23 11:110.0050.0005<0.0005mg/KgIsopropylbenzene
05/02/23 11:110.0050.001<0.001mg/Kg4-Isopropyl toluene
05/02/23 11:110.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/02/23 11:110.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/02/23 11:110.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/02/23 11:110.0100.001<0.001mg/KgMethylene Chloride
05/02/23 11:110.0100.0010<0.0010mg/KgNaphthalene
05/02/23 11:110.0050.0005<0.0005mg/Kgn-Propylbenzene
05/02/23 11:110.0050.001<0.001mg/KgStyrene
Page 4 of 23Date:05/08/2023 03:34 PM
Page 66 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
Associated Lab Samples: 95188, 95189, 95190, 95191, 95192
LRB-V32694 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 11:110.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/02/23 11:110.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/02/23 11:110.0050.0009<0.0009mg/KgTetrachloroethene
05/02/23 11:110.0050.0007<0.0007mg/KgToluene
05/02/23 11:110.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/02/23 11:110.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/02/23 11:110.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/02/23 11:110.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/02/23 11:110.0050.0009<0.0009mg/KgTrichloroethene
05/02/23 11:110.0100.002<0.002mg/KgTrichlorofluoromethane
05/02/23 11:110.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/02/23 11:110.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/02/23 11:110.0100.0005<0.0005mg/KgVinyl Acetate
05/02/23 11:110.0100.0005<0.0005mg/KgVinyl Chloride
05/02/23 11:110.0050.0005<0.0005mg/Kgo-Xylene
05/02/23 11:110.0100.001<0.001mg/Kgm,p-Xylene
05/02/23 11:114-Bromofluorobenzene (S)97.8 70-130
05/02/23 11:11Dibromofluoromethane (S)96.6 84-123
05/02/23 11:11Toluene-d8 (S)90.2 76-129
LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.105 1051200.1200.100mg/KgAcetone 29-198 13.3 20
0.088 88.090.30.0900.100mg/KgAcrolein 70-130 2.5 20
0.101 10197.20.0970.100mg/KgAcrylonitrile 65-134 3.8 20
Page 5 of 23Date:05/08/2023 03:34 PM
Page 67 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.055 1101110.0550.050mg/KgBenzene 74-127 0.7 20
0.044 88.692.80.0460.050mg/KgBromobenzene 73-125 4.6 20
0.059 1201190.0590.050mg/KgBromochloromethane 72-134 1.0 20
0.057 1161160.0580.050mg/KgBromodichloromethane 75-122 0.5 20
0.052 1051060.0530.050mg/KgBromoform 66-135 1.5 20
0.056 11395.00.0470.050mg/KgBromomethane 20-180 17.1 20
0.045 90.695.20.0470.050mg/Kgn-Butylbenzene 65-135 4.9 20
0.044 89.493.40.0460.050mg/Kgsec-Butyl benzene 66-131 4.3 20
0.044 89.293.00.0460.050mg/Kgtert-Butyl benzene 67-132 4.1 20
0.052 1061110.0550.050mg/KgCarbon Disulfide 61-129 4.7 20
0.058 1161180.0590.050mg/KgCarbon Tetrachloride 64-143 1.8 20
0.050 1021040.0520.050mg/KgChlorobenzene 74-118 2.5 20
0.051 1041040.0520.050mg/KgChlorodibromomethane 73-122 0.5 20
0.049 99.81080.0540.050mg/KgChloroethane 33-149 8.2 20
0.056 1141170.0580.050mg/KgChloroform 73-127 2.9 20
0.052 1041040.0520.050mg/KgChloromethane 45-143 0.3 20
0.044 89.893.20.0460.050mg/Kg2-Chlorotoluene 67-124 3.7 20
0.044 89.893.20.0460.050mg/Kg4-Chlorotoluene 71-126 3.7 20
0.054 1091100.0540.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.7 20
0.050 1011020.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.1 20
0.054 1081050.0520.050mg/Kg1,2-Dibromoethane 70-132 2.6 20
0.055 1111170.0580.050mg/KgDibromomethane 74-133 4.5 20
0.046 92.497.40.0480.050mg/Kg1,2-Dichlorobenzene 72-123 5.2 20
0.046 93.495.80.0470.050mg/Kg1,3-Dichlorobenzene 71-120 2.5 20
0.045 91.095.00.0470.050mg/Kg1,4-Dichlorobenzene 71-123 4.3 20
0.050 1001040.0510.050mg/KgDichlorodifluoromethane 26-146 3.5 20
Page 6 of 23Date:05/08/2023 03:34 PM
Page 68 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.053 1071130.0560.050mg/Kg1,1-Dichloroethane 74-127 4.7 20
0.053 1061080.0530.050mg/Kg1,2-Dichloroethane 68-128 1.1 20
0.052 1061120.0550.050mg/Kg1,1-Dichloroethene 67-149 5.5 20
0.054 1081090.0540.050mg/Kgcis-1,2-Dichloroethene 76-134 0.9 20
0.052 1061110.0550.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.6 20
0.053 1071130.0560.050mg/Kg1,2-Dichloropropane 73-130 5.2 20
0.051 1021030.0510.050mg/Kg1,3-Dichloropropane 75-124 0.3 20
0.055 1101140.0570.050mg/Kg2,2-Dichloropropane 50-142 3.3 20
0.055 1101160.0580.050mg/Kg1,1-Dichloropropene 71-130 5.4 20
0.057 1151150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 0.3 20
0.059 1181190.0590.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.5 20
0.048 96.898.60.0490.050mg/KgEthylbenzene 74-128 1.8 20
0.107 1071080.1080.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.047 94.81010.0500.050mg/KgHexachlorobutadiene 64-125 6.1 20
0.055 1111250.0620.050mg/Kgn-Hexane 70-130 11.6 20
0.049 98.41220.0610.050mg/Kg2-Hexanone 61-157 21.4*20
0.045 90.494.80.0470.050mg/KgIsopropylbenzene 68-126 4.7 20
0.045 90.695.40.0470.050mg/Kg4-Isopropyl toluene 68-129 5.1 20
0.040 80.499.80.0490.050mg/KgMethyl Ethyl Ketone (MEK)63-149 21.5*20
0.055 1101100.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.3 20
0.058 1161200.0600.050mg/Kg4-Methyl-2-Pentanone 57-162 3.2 20
0.045 91.892.00.0460.050mg/KgMethylene Chloride 74-129 0.2 20
0.046 93.499.20.0490.050mg/KgNaphthalene 57-157 6.0 20
0.044 89.492.40.0460.050mg/Kgn-Propylbenzene 67-130 3.3 20
0.051 1031040.0520.050mg/KgStyrene 77-121 1.3 20
0.050 1011010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.0 20
Page 7 of 23* QC Fail Date:05/08/2023 03:34 PM
Page 69 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.093.00.0460.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.2 20
0.056 1121160.0570.050mg/KgTetrachloroethene 68-130 3.3 20
0.053 1081080.0540.050mg/KgToluene 71-129 0.7 20
0.047 95.01050.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 10.1 20
0.049 99.41060.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 6.0 20
0.055 1101140.0560.050mg/Kg1,1,1-Trichloroethane 67-131 2.8 20
0.051 1031050.0520.050mg/Kg1,1,2-Trichloroethane 70-133 1.7 20
0.055 1121160.0580.050mg/KgTrichloroethene 75-133 4.2 20
0.042 85.482.00.0410.050mg/KgTrichlorofluoromethane 44-146 4.0 20
0.048 97.694.00.0470.050mg/Kg1,2,3-Trichloropropane 60-137 3.7 20
0.044 88.493.60.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.7 20
0.058 11897.80.0480.050mg/KgVinyl Acetate 60-140 18.5 20
0.051 1021060.0530.050mg/KgVinyl Chloride 48-147 4.0 20
0.048 96.499.20.0490.050mg/Kgo-Xylene 74-126 2.8 20
0.099 99.31020.1020.100mg/Kgm,p-Xylene 75-124 2.6 20
97.81014-Bromofluorobenzene (S)70-130
10196.2Dibromofluoromethane (S)84-123
90.289.6Toluene-d8 (S)76-129
Page 8 of 23Date:05/08/2023 03:34 PM
Page 70 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32696
Associated Lab Samples: 95187
LRB-V32696 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 11:110.0200.002<0.002mg/KgAcetone
05/02/23 11:110.0200.001<0.001mg/KgAcrolein
05/02/23 11:110.0200.0008<0.0008mg/KgAcrylonitrile
05/02/23 11:110.0050.0006<0.0006mg/KgBenzene
05/02/23 11:110.0050.0005<0.0005mg/KgBromobenzene
05/02/23 11:110.0050.0008<0.0008mg/KgBromochloromethane
05/02/23 11:110.0050.001<0.001mg/KgBromodichloromethane
05/02/23 11:110.0050.001<0.001mg/KgBromoform
05/02/23 11:110.0100.001<0.001mg/KgBromomethane
05/02/23 11:110.0050.0005<0.0005mg/Kgn-Butylbenzene
05/02/23 11:110.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/02/23 11:110.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/02/23 11:110.0050.0006<0.0006mg/KgCarbon Disulfide
05/02/23 11:110.0050.001<0.001mg/KgCarbon Tetrachloride
05/02/23 11:110.0050.0007<0.0007mg/KgChlorobenzene
05/02/23 11:110.0050.0009<0.0009mg/KgChlorodibromomethane
05/02/23 11:110.0100.0009<0.0009mg/KgChloroethane
05/02/23 11:110.0050.001<0.001mg/KgChloroform
05/02/23 11:110.0100.0006<0.0006mg/KgChloromethane
05/02/23 11:110.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/02/23 11:110.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/02/23 11:110.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/02/23 11:110.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/02/23 11:110.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/02/23 11:110.0050.0010<0.0010mg/KgDibromomethane
05/02/23 11:110.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/02/23 11:110.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 9 of 23Date:05/08/2023 03:34 PM
Page 71 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32696
Associated Lab Samples: 95187
LRB-V32696 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 11:110.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/02/23 11:110.0100.001<0.001mg/KgDichlorodifluoromethane
05/02/23 11:110.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/02/23 11:110.0050.001<0.001mg/Kg1,2-Dichloroethane
05/02/23 11:110.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/02/23 11:110.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/02/23 11:110.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/02/23 11:110.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/02/23 11:110.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/02/23 11:110.0050.001<0.001mg/Kg2,2-Dichloropropane
05/02/23 11:110.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/02/23 11:110.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/02/23 11:110.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/02/23 11:110.0050.0006<0.0006mg/KgEthylbenzene
05/02/23 11:110.1000.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/02/23 11:110.0100.0008<0.0008mg/KgHexachlorobutadiene
05/02/23 11:110.0100.0007<0.0007mg/Kgn-Hexane
05/02/23 11:110.0200.0006<0.0006mg/Kg2-Hexanone
05/02/23 11:110.0050.0005<0.0005mg/KgIsopropylbenzene
05/02/23 11:110.0050.001<0.001mg/Kg4-Isopropyl toluene
05/02/23 11:110.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/02/23 11:110.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/02/23 11:110.0050.001<0.001mg/KgMethylene Chloride
05/02/23 11:110.0100.0010<0.0010mg/KgNaphthalene
05/02/23 11:110.0050.0005<0.0005mg/Kgn-Propylbenzene
05/02/23 11:110.0050.001<0.001mg/KgStyrene
05/02/23 11:110.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
Page 10 of 23Date:05/08/2023 03:34 PM
Page 72 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32696
Associated Lab Samples: 95187
LRB-V32696 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 11:110.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/02/23 11:110.0050.0009<0.0009mg/KgTetrachloroethene
05/02/23 11:110.0050.0007<0.0007mg/KgToluene
05/02/23 11:110.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/02/23 11:110.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/02/23 11:110.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/02/23 11:110.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/02/23 11:110.0050.0009<0.0009mg/KgTrichloroethene
05/02/23 11:110.0100.002<0.002mg/KgTrichlorofluoromethane
05/02/23 11:110.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/02/23 11:110.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/02/23 11:110.0100.0005<0.0005mg/KgVinyl Acetate
05/02/23 11:110.0100.0005<0.0005mg/KgVinyl Chloride
05/02/23 11:110.0050.0005<0.0005mg/Kgo-Xylene
05/02/23 11:110.0100.001<0.001mg/Kgm,p-Xylene
05/02/23 11:114-Bromofluorobenzene (S)97.8 70-130
05/02/23 11:11Dibromofluoromethane (S)96.6 70-130
05/02/23 11:11Toluene-d8 (S)90.2 76-129
LCS-V32696 LCSD-V32696Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.105 1051200.1200.100mg/KgAcetone 29-198 13.3 20
0.088 88.090.30.0900.100mg/KgAcrolein 70-130 2.5 20
0.101 10197.20.0970.100mg/KgAcrylonitrile 65-134 3.8 20
0.055 1101110.0550.050mg/KgBenzene 74-127 0.7 20
Page 11 of 23Date:05/08/2023 03:34 PM
Page 73 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32696
LCS-V32696 LCSD-V32696Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 88.692.80.0460.050mg/KgBromobenzene 73-125 4.6 20
0.059 1201190.0590.050mg/KgBromochloromethane 72-134 1.0 20
0.057 1161160.0580.050mg/KgBromodichloromethane 75-122 0.5 20
0.052 1051060.0530.050mg/KgBromoform 66-135 1.5 20
0.056 11395.00.0470.050mg/KgBromomethane 20-180 17.1 20
0.045 90.695.20.0470.050mg/Kgn-Butylbenzene 65-135 4.9 20
0.044 89.493.40.0460.050mg/Kgsec-Butyl benzene 66-131 4.3 20
0.044 89.293.00.0460.050mg/Kgtert-Butyl benzene 67-132 4.1 20
0.052 1061110.0550.050mg/KgCarbon Disulfide 61-129 4.7 20
0.058 1161180.0590.050mg/KgCarbon Tetrachloride 64-143 1.8 20
0.050 1021040.0520.050mg/KgChlorobenzene 74-118 2.5 20
0.051 1041040.0520.050mg/KgChlorodibromomethane 73-122 0.5 20
0.049 99.81080.0540.050mg/KgChloroethane 33-149 8.2 20
0.056 1141170.0580.050mg/KgChloroform 73-127 2.9 20
0.052 1041040.0520.050mg/KgChloromethane 45-143 0.3 20
0.044 89.893.20.0460.050mg/Kg2-Chlorotoluene 67-124 3.7 20
0.044 89.893.20.0460.050mg/Kg4-Chlorotoluene 71-126 3.7 20
0.054 1091100.0540.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.7 20
0.050 1011020.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.1 20
0.054 1081050.0520.050mg/Kg1,2-Dibromoethane 70-132 2.6 20
0.055 1111170.0580.050mg/KgDibromomethane 74-133 4.5 20
0.046 92.497.40.0480.050mg/Kg1,2-Dichlorobenzene 72-123 5.2 20
0.046 93.495.80.0470.050mg/Kg1,3-Dichlorobenzene 71-120 2.5 20
0.045 91.095.00.0470.050mg/Kg1,4-Dichlorobenzene 71-123 4.3 20
0.050 1001040.0510.050mg/KgDichlorodifluoromethane 26-146 3.5 20
0.053 1071130.0560.050mg/Kg1,1-Dichloroethane 74-127 4.7 20
Page 12 of 23Date:05/08/2023 03:34 PM
Page 74 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32696
LCS-V32696 LCSD-V32696Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.053 1061080.0530.050mg/Kg1,2-Dichloroethane 68-128 1.1 20
0.052 1061120.0550.050mg/Kg1,1-Dichloroethene 67-149 5.5 20
0.054 1081090.0540.050mg/Kgcis-1,2-Dichloroethene 76-134 0.9 20
0.052 1061110.0550.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.6 20
0.053 1071130.0560.050mg/Kg1,2-Dichloropropane 73-130 5.2 20
0.051 1021030.0510.050mg/Kg1,3-Dichloropropane 75-124 0.3 20
0.055 1101140.0570.050mg/Kg2,2-Dichloropropane 50-142 3.3 20
0.055 1101160.0580.050mg/Kg1,1-Dichloropropene 71-130 5.4 20
0.057 1151150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 0.3 20
0.059 1181190.0590.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.5 20
0.048 96.898.60.0490.050mg/KgEthylbenzene 74-128 1.8 20
0.107 1071080.1080.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.047 94.81010.0500.050mg/KgHexachlorobutadiene 64-125 6.1 20
0.055 1111250.0620.050mg/Kgn-Hexane 70-130 11.6 20
0.049 98.41220.0610.050mg/Kg2-Hexanone 61-157 21.4*20
0.045 90.494.80.0470.050mg/KgIsopropylbenzene 68-126 4.7 20
0.045 90.695.40.0470.050mg/Kg4-Isopropyl toluene 68-129 5.1 20
0.040 80.499.80.0490.050mg/KgMethyl Ethyl Ketone (MEK)63-149 21.5*20
0.055 1101100.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.3 20
0.045 91.892.00.0460.050mg/KgMethylene Chloride 74-129 0.2 20
0.046 93.499.20.0490.050mg/KgNaphthalene 57-157 6.0 20
0.044 89.492.40.0460.050mg/Kgn-Propylbenzene 67-130 3.3 20
0.051 1031040.0520.050mg/KgStyrene 77-121 1.3 20
0.050 1011010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.0 20
0.045 90.093.00.0460.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.2 20
0.056 1121160.0570.050mg/KgTetrachloroethene 68-130 3.3 20
Page 13 of 23* QC Fail Date:05/08/2023 03:34 PM
Page 75 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32697QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32696
LCS-V32696 LCSD-V32696Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.053 1081080.0540.050mg/KgToluene 71-129 0.7 20
0.047 95.01050.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 10.1 20
0.049 99.41060.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 6.0 20
0.055 1101140.0560.050mg/Kg1,1,1-Trichloroethane 67-131 2.8 20
0.051 1031050.0520.050mg/Kg1,1,2-Trichloroethane 70-133 1.7 20
0.055 1121160.0580.050mg/KgTrichloroethene 75-133 4.2 20
0.042 85.482.00.0410.050mg/KgTrichlorofluoromethane 44-146 4.0 20
0.048 97.694.00.0470.050mg/Kg1,2,3-Trichloropropane 60-137 3.7 20
0.044 88.493.60.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.7 20
0.058 11897.80.0480.050mg/KgVinyl Acetate 60-140 18.5 20
0.051 1021060.0530.050mg/KgVinyl Chloride 48-147 4.0 20
0.048 96.499.20.0490.050mg/Kgo-Xylene 74-126 2.8 20
0.099 99.31020.1020.100mg/Kgm,p-Xylene 75-124 2.6 20
97.81014-Bromofluorobenzene (S)70-130
10196.2Dibromofluoromethane (S)70-130
90.289.6Toluene-d8 (S)76-129
Page 14 of 23Date:05/08/2023 03:34 PM
Page 76 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32895QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32769
Associated Lab Samples: 95187, 95188, 95189, 95190, 95191, 95192
LRB-V32769 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/04/23 17:560.6600.116<0.116mg/KgAcenaphthene
05/04/23 17:560.6600.105<0.105mg/KgAcenaphthylene
05/04/23 17:560.6600.152<0.152mg/KgAniline
05/04/23 17:560.6600.143<0.143mg/KgAnthracene
05/04/23 17:560.6600.139<0.139mg/KgBenzo(a)anthracene
05/04/23 17:560.6600.147<0.147mg/KgBenzo(a)pyrene
05/04/23 17:560.6600.146<0.146mg/KgBenzo(b)fluoranthene
05/04/23 17:560.6600.136<0.136mg/KgBenzo(g,h,i)perylene
05/04/23 17:560.6600.137<0.137mg/KgBenzo(k)fluoranthene
05/04/23 17:562.000.580<0.580mg/KgBenzoic Acid
05/04/23 17:560.6600.105<0.105mg/KgBenzyl alcohol
05/04/23 17:560.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
05/04/23 17:560.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
05/04/23 17:560.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
05/04/23 17:560.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
05/04/23 17:560.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
05/04/23 17:560.3300.113<0.113mg/KgButyl benzyl phthalate
05/04/23 17:560.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
05/04/23 17:560.3300.112<0.112mg/Kg4-Chloroaniline
05/04/23 17:560.6600.116<0.116mg/Kg2-Chloronaphthalene
05/04/23 17:560.6600.098<0.098mg/Kg2-Chlorophenol
05/04/23 17:561.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
05/04/23 17:560.6600.142<0.142mg/KgChrysene
05/04/23 17:560.6600.230<0.230mg/KgDibenz(a,h)anthracene
05/04/23 17:560.6600.119<0.119mg/KgDibenzofuran
05/04/23 17:560.6600.094<0.094mg/Kg1,2-Dichlorobenzene
05/04/23 17:560.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 15 of 23Date:05/08/2023 03:34 PM
Page 77 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32895QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32769
Associated Lab Samples: 95187, 95188, 95189, 95190, 95191, 95192
LRB-V32769 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/04/23 17:560.3300.097<0.097mg/Kg1,4-Dichlorobenzene
05/04/23 17:560.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
05/04/23 17:560.6600.095<0.095mg/Kg2,4-Dichlorophenol
05/04/23 17:560.6600.180<0.180mg/KgDiethyl phthalate
05/04/23 17:560.6600.174<0.174mg/KgDimethyl phthalate
05/04/23 17:560.3300.108<0.108mg/Kg2,4-Dimethylphenol
05/04/23 17:560.6600.107<0.107mg/KgDi-n-butyl phthalate
05/04/23 17:561.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
05/04/23 17:561.500.520<0.520mg/Kg2,4-Dinitrophenol
05/04/23 17:560.6600.096<0.096mg/Kg2,4-Dinitrotoluene
05/04/23 17:560.6600.108<0.108mg/Kg2,6-Dinitrotoluene
05/04/23 17:560.3300.143<0.143mg/KgDi-n-Octyl Phthalate
05/04/23 17:560.6600.123<0.123mg/KgFluoranthene
05/04/23 17:560.6600.128<0.128mg/KgFluorene
05/04/23 17:560.6600.106<0.106mg/KgHexachlorobenzene
05/04/23 17:560.6600.097<0.097mg/KgHexachlorobutadiene
05/04/23 17:560.6600.157<0.157mg/KgHexachlorocyclopentadiene
05/04/23 17:560.6600.079<0.079mg/KgHexachloroethane
05/04/23 17:560.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
05/04/23 17:560.6600.191<0.191mg/KgIsophorone
05/04/23 17:560.6600.106<0.106mg/Kg1-Methylnaphthalene
05/04/23 17:560.6600.100<0.100mg/Kg2-Methylnaphthalene
05/04/23 17:560.6600.097<0.097mg/Kg2-Methylphenol
05/04/23 17:560.6600.084<0.084mg/Kg3&4 Methylphenol
05/04/23 17:560.6600.144<0.144mg/KgNaphthalene
05/04/23 17:560.6600.096<0.096mg/Kg2-Nitroaniline
05/04/23 17:560.6600.120<0.120mg/Kg3-Nitroaniline
Page 16 of 23Date:05/08/2023 03:34 PM
Page 78 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32895QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32769
Associated Lab Samples: 95187, 95188, 95189, 95190, 95191, 95192
LRB-V32769 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/04/23 17:560.3300.093<0.093mg/Kg4-Nitroaniline
05/04/23 17:560.3300.116<0.116mg/KgNitrobenzene
05/04/23 17:560.6600.088<0.088mg/Kg2-Nitrophenol
05/04/23 17:560.6600.117<0.117mg/Kg4-Nitrophenol
05/04/23 17:560.6600.263<0.263mg/KgN-Nitrosodimethylamine
05/04/23 17:560.6600.181<0.181mg/KgN-Nitrosodiphenylamine
05/04/23 17:560.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
05/04/23 17:561.000.347<0.347mg/KgPentachlorophenol
05/04/23 17:560.6600.208<0.208mg/KgPhenanthrene
05/04/23 17:560.6600.112<0.112mg/KgPhenol
05/04/23 17:560.6600.134<0.134mg/KgPyrene
05/04/23 17:560.3300.079<0.079mg/KgPyridine
05/04/23 17:560.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
05/04/23 17:560.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
05/04/23 17:560.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
05/04/23 17:562-Fluorobiphenyl (S)69.4 44-115
05/04/23 17:562-Fluorophenol (S)59.4 35-115
05/04/23 17:56Nitrobenzene-d5 (S)64.6 37-122
05/04/23 17:564-Terphenyl-d14 (S)79.0 54-127
05/04/23 17:562,4,6-Tribromophenol (S)58.2 39-132
05/04/23 17:56Phenol-d5 (S)57.0 34-121
LCS-V32769 LCSD-V32769Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.20 71.867.01.121.67mg/KgAcenaphthene 40-123 6.8 20
Page 17 of 23Date:05/08/2023 03:34 PM
Page 79 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32895QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32769
LCS-V32769 LCSD-V32769Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.21 72.468.81.151.67mg/KgAcenaphthylene 32-132 5.0 20
1.67 1001071.781.67mg/KgAniline 12-197 6.3 20
1.37 82.074.21.241.67mg/KgAnthracene 47-123 9.9 20
1.37 82.076.01.271.67mg/KgBenzo(a)anthracene 49-126 7.5 20
1.48 88.684.41.411.67mg/KgBenzo(a)pyrene 45-129 4.8 20
1.69 10197.01.621.67mg/KgBenzo(b)fluoranthene 45-132 4.2 20
1.37 82.073.01.221.67mg/KgBenzo(g,h,i)perylene 43-134 11.5 20
1.54 92.289.21.491.67mg/KgBenzo(k)fluoranthene 47-132 3.3 20
1.07 64.065.21.091.67mg/KgBenzoic Acid 10-83 1.8 20
1.29 77.269.41.161.67mg/KgBenzyl alcohol 29-122 10.6 20
1.22 73.065.81.101.67mg/KgBis(2-Chloroethoxy)methane 36-121 10.3 20
1.10 65.857.50.9611.67mg/KgBis(2-Chloroethyl)ether 31-120 13.4 20
1.22 73.069.41.161.67mg/KgBis(2-Chloroisopropyl)ether 33-131 5.0 20
1.48 88.686.21.441.67mg/KgBis(2-ethylhexyl)phthalate 51-133 2.7 20
1.33 79.672.41.211.67mg/Kg4-Bromophenyl phenyl ether 46-124 9.4 20
1.37 82.084.41.411.67mg/KgButyl benzyl phthalate 48-132 2.8 20
1.32 79.065.81.101.67mg/Kg4-Chloro-3-methylphenol 45-122 18.1 20
1.12 67.061.01.021.67mg/Kg4-Chloroaniline 17-106 9.3 20
1.18 70.668.81.151.67mg/Kg2-Chloronaphthalene 41-114 2.5 20
1.20 71.868.81.151.67mg/Kg2-Chlorophenol 34-121 4.2 20
1.33 79.672.41.211.67mg/Kg4-Chlorophenyl phenyl ether 45-121 9.4 20
1.27 76.071.21.191.67mg/KgChrysene 50-124 6.5 20
1.34 80.274.21.241.67mg/KgDibenz(a,h)anthracene 45-134 7.7 20
1.22 73.068.21.141.67mg/KgDibenzofuran 44-120 6.7 20
1.07 64.060.41.011.67mg/Kg1,2-Dichlorobenzene 33-117 5.7 20
1.03 61.658.20.9721.67mg/Kg1,3-Dichlorobenzene 30-115 5.7 20
Page 18 of 23Date:05/08/2023 03:34 PM
Page 80 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32895QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32769
LCS-V32769 LCSD-V32769Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.02 61.058.20.9721.67mg/Kg1,4-Dichlorobenzene 31-115 4.8 20
1.26 75.473.01.221.67mg/Kg3,3'-Dichlorobenzidine 22-121 3.2 20
1.27 76.066.41.111.67mg/Kg2,4-Dichlorophenol 40-122 13.4 20
1.33 79.676.01.271.67mg/KgDiethyl phthalate 50-124 4.6 20
1.29 77.274.21.241.67mg/KgDimethyl phthalate 48-124 3.9 20
1.44 86.276.01.271.67mg/Kg2,4-Dimethylphenol 30-127 12.5 20
1.47 88.085.61.431.67mg/KgDi-n-butyl phthalate 51-128 2.7 20
1.21 72.470.61.181.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 2.5 20
1.43 85.684.41.411.67mg/Kg2,4-Dinitrophenol 27-129 1.4 20
1.43 85.679.61.331.67mg/Kg2,4-Dinitrotoluene 48-126 7.2 20
1.35 80.875.41.261.67mg/Kg2,6-Dinitrotoluene 46-124 6.8 20
2.18 1311292.161.67mg/KgDi-n-Octyl Phthalate 45-140 0.9 20
1.29 77.271.81.201.67mg/KgFluoranthene 50-127 7.2 20
1.27 76.071.21.191.67mg/KgFluorene 43-125 6.5 20
1.27 76.070.61.181.67mg/KgHexachlorobenzene 45-122 7.3 20
1.14 68.259.60.9961.67mg/KgHexachlorobutadiene 32-123 13.4 20
1.05 62.862.21.041.67mg/KgHexachlorocyclopentadiene 32-117 0.9 20
1.03 61.658.30.9751.67mg/KgHexachloroethane 28-117 5.4 20
1.43 85.677.81.301.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 9.5 20
1.08 64.657.10.9541.67mg/KgIsophorone 30-122 12.3 20
1.15 68.859.30.9911.67mg/Kg1-Methylnaphthalene 40-119 14.8 20
1.15 68.859.40.9931.67mg/Kg2-Methylnaphthalene 38-122 14.6 20
1.26 75.470.01.171.67mg/Kg2-Methylphenol 32-122 7.4 20
1.15 68.864.61.081.67mg/Kg3&4 Methylphenol 34-119 6.2 20
1.09 65.258.30.9751.67mg/KgNaphthalene 35-123 11.1 20
1.36 81.481.41.361.67mg/Kg2-Nitroaniline 44-127 0.0 20
Page 19 of 23Date:05/08/2023 03:34 PM
Page 81 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32895QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32769
LCS-V32769 LCSD-V32769Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.24 74.274.81.251.67mg/Kg3-Nitroaniline 33-119 0.8 20
1.32 79.074.81.251.67mg/Kg4-Nitroaniline 63-147 5.4 20
1.07 64.057.50.9611.67mg/KgNitrobenzene 34-122 10.7 20
1.20 71.864.61.081.67mg/Kg2-Nitrophenol 36-123 10.5 20
1.29 77.278.41.311.67mg/Kg4-Nitrophenol 30-132 1.5 20
1.00 59.852.00.8691.67mg/KgN-Nitrosodimethylamine 10-146 14.0 20
1.52 91.088.01.471.67mg/KgN-Nitrosodiphenylamine 38-127 3.3 20
1.22 73.067.61.131.67mg/KgN-Nitroso-di-n-propylamine 36-120 7.6 20
1.24 74.276.61.281.67mg/KgPentachlorophenol 25-133 3.1 20
1.27 76.071.21.191.67mg/KgPhenanthrene 50-121 6.5 20
1.16 69.465.81.101.67mg/KgPhenol 34-121 5.3 20
1.24 74.268.81.151.67mg/KgPyrene 47-127 7.5 20
0.658 39.437.20.6221.67mg/KgPyridine 10-80 5.6 20
1.07 64.057.40.9591.67mg/Kg1,2,4-Trichlorobenzene 34-118 10.9 20
1.25 74.871.21.191.67mg/Kg2,4,5-Trichlorophenol 41-124 4.9 20
1.25 74.871.81.201.67mg/Kg2,4,6-Trichlorophenol 39-126 4.0 20
71.269.42-Fluorobiphenyl (S)44-115
65.163.02-Fluorophenol (S)35-115
65.859.8Nitrobenzene-d5 (S)37-122
79.674.84-Terphenyl-d14 (S)54-127
70.266.32,4,6-Tribromophenol (S)39-132
62.460.0Phenol-d5 (S)34-121
Page 20 of 23Date:05/08/2023 03:34 PM
Page 82 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V32862QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V32729
Associated Lab Samples: 95187, 95188, 95189, 95190, 95191, 95192
LRB-V32729 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/05/23 10:5950.09.20<9.20mg/KgAliphatic C9-C18
05/05/23 10:5950.012.2<12.2mg/KgAliphatic C19-C36
05/05/23 10:5950.014.2<14.2mg/KgAromatic C11-C22
05/05/23 10:592-Fluorobiphenyl (S)101 40-140
05/05/23 10:592-Bromonaphthalene (S)99.0 40-140
05/05/23 10:59Chlorooctadecane (S)64.6 40-140
05/05/23 10:59OTP Surrogate (S)78.7 40-140
LCS-V32729 LCSD-V32729Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.8 66.365.539.360.0mg/KgAliphatic C9-C18 40-140 1.2 50
68.2 85.278.262.680.0mg/KgAliphatic C19-C36 40-140 8.5 50
199 117108184170mg/KgAromatic C11-C22 40-140 7.8 50
1151132-Fluorobiphenyl (S)40-140
1141112-Bromonaphthalene (S)40-140
76.669.8Chlorooctadecane (S)40-140
96.893.0OTP Surrogate (S)40-140
Page 21 of 23Date:05/08/2023 03:34 PM
Page 83 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V32693QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V32692
Associated Lab Samples: 95187, 95188, 95189, 95190, 95191, 95192
LRB-V32692 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 16:208.001.22<1.22mg/KgAliphatic C5-C8
05/02/23 16:208.004.56<4.56mg/KgAliphatic C9-C12
05/02/23 16:208.000.624<0.624mg/KgAromatic C9-C10
05/02/23 16:202,5-Dibromotoluene (FID) (S)80.8 70-130
05/02/23 16:202,5-Dibromotoluene (PID) (S)112 70-130
LCS-V32692 LCSD-V32692Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.1 10097.531.232.0mg/KgAliphatic C5-C8 70-130 2.8 50
35.9 11211035.132.0mg/KgAliphatic C9-C12 70-130 2.2 50
13.1 12212313.210.7mg/KgAromatic C9-C10 70-130 0.7 50
81.677.02,5-Dibromotoluene (FID) (S)70-130
1121122,5-Dibromotoluene (PID) (S)70-130
Page 22 of 23Date:05/08/2023 03:34 PM
Page 84 of 87
Quality Control Data
23-121-0017Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff Village
Dry Weight Determination
SW-DRYWT
V32710QC Analytical Batch:
Analysis Method:
Analysis Description:
V 95156-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/03/23 10:501.519.319.6%Moisture
V 95200-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/03/23 10:500.921.521.7%Moisture
Page 23 of 23Date:05/08/2023 03:34 PM
Page 85 of 87
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-121-0017
Summit Engineering (Charlotte)
01197
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:05/01/2023 15:21:51
Special precautions or instructions included?
Comments:
Page 86 of 87
Page 87 of 87

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/16/2023
Summit Engineering (Charlotte) Matt Hoffman
2520 Whitehall Park Dr Suite 250
Charlotte, NC, 28273
Ref: Analytical Testing Lab Report Number: 23-130-0032
Client Project Description: Analytical Testing
Dear Matt Hoffman:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/10/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 12
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-130-0032
Page 2 of 12
Report Number:
Sample Summary Table
Client Project Description:
23-130-0032
Analytical Testing
Lab No Client Sample ID Matrix Date Collected Date Received
05/10/2023 11:20Solids 95848 Bottom-A 05/10/2023 14:42
05/10/2023 11:30Solids 95849 SW-1-A 05/10/2023 14:42
Page 3 of 12
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-130-0032
Report Limit
Project:Analytical Testing
V 95848Bottom-A
294 05/15/2023 15:42MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 22.0
J98.3 05/15/2023 15:42MADEP-EPH Aliphatic C19-C36 mg/Kg - dry 29.2
214 05/15/2023 15:42MADEP-EPH Aromatic C11-C22 mg/Kg - dry 34.0
16.7 05/12/2023 13:50SW-DRYWT Moisture %
V 95849SW-1-A
7.68 05/12/2023 13:50SW-DRYWT Moisture %
Page 4 of 12
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-130-0032
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Bottom-A
95848 Matrix:
5/10/2023 11:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.7 %Moisture 1 05/12/23 13:50 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 5 of 12
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-130-0032
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Bottom-A
95848 Matrix:
5/10/2023 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):05/11/23 10:30
294 mg/Kg - dry 22.0 119Aliphatic C9-C18 2 05/15/23 15:42 V33187AMP
98.3 J mg/Kg - dry 29.2 119Aliphatic C19-C36 2 05/15/23 15:42 V33187AMP
214 mg/Kg - dry 34.0 119Aromatic C11-C22 2 05/15/23 15:42 V33187AMP
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 12
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-130-0032
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
SW-1-A
95849 Matrix:
5/10/2023 11:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
7.68 %Moisture 1 05/12/23 13:50 SW-DRYWTCNC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 12
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-130-0032
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
SW-1-A
95849 Matrix:
5/10/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):05/11/23 10:30
<9.92 mg/Kg - dry 9.92 53.9Aliphatic C9-C18 1 05/15/23 13:06 V33187AMP
<13.2 mg/Kg - dry 13.2 53.9Aliphatic C19-C36 1 05/15/23 13:06 V33187AMP
<15.3 mg/Kg - dry 15.3 53.9Aromatic C11-C22 1 05/15/23 13:06 V33187AMP
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 12
Quality Control Data
23-130-0032Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Analytical Testing
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V33187QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V33065
Associated Lab Samples: 95848, 95849
Lab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/15/23 10:4150.09.20<9.20mg/KgAliphatic C9-C18
05/15/23 10:4150.012.2<12.2mg/KgAliphatic C19-C36
05/15/23 10:4150.014.2<14.2mg/KgAromatic C11-C22
05/15/23 10:412-Fluorobiphenyl (S)94.2 40-140
05/15/23 10:412-Bromonaphthalene (S)90.2 40-140
05/15/23 10:41Chlorooctadecane (S)67.3 40-140
05/15/23 10:41OTP Surrogate (S)76.8 40-140
LCS-V33065 LCSD-V33065Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.8 61.362.537.560.0mg/KgAliphatic C9-C18 40-140 1.8 50
54.1 67.668.755.080.0mg/KgAliphatic C19-C36 40-140 1.6 50
143 84.182.9141170mg/KgAromatic C11-C22 40-140 1.4 50
10597.22-Fluorobiphenyl (S)40-140
10293.72-Bromonaphthalene (S)40-140
74.273.8Chlorooctadecane (S)40-140
84.183.8OTP Surrogate (S)40-140
Page 1 of 2Date:05/16/2023 03:22 PM
Page 9 of 12
Quality Control Data
23-130-0032Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Analytical Testing
Dry Weight Determination
SW-DRYWT
V33095QC Analytical Batch:
Analysis Method:
Analysis Description:
V 95848-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/12/23 13:503.616.116.7%Moisture
V 95866-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/12/23 13:503.327.126.2%Moisture
Page 2 of 2Date:05/16/2023 03:22 PM
Page 10 of 12
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-130-0032
Summit Engineering (Charlotte)
01197
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.4C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:05/10/2023 15:46:44
Special precautions or instructions included?
Comments:
Page 11 of 12
Page 12 of 12

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

6/21/2023
Summit Engineering (Charlotte) Matt Hoffman
2520 Whitehall Park Dr Suite 250
Charlotte, NC, 28273
Ref: Analytical Testing Lab Report Number: 23-163-0021
Client Project Description: Winecoff
Dear Matt Hoffman:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/12/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 14
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-163-0021
Page 2 of 14
Report Number:
Sample Summary Table
Client Project Description:
23-163-0021
Winecoff
Lab No Client Sample ID Matrix Date Collected Date Received
06/12/2023 11:00Solids 98177 SW-2A 06/12/2023 16:36
06/12/2023 11:10Solids 98178 SW-3A 06/12/2023 16:36
06/12/2023 11:20Solids 98179 Bottom B 06/12/2023 16:36
Page 3 of 14
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-163-0021
Report Limit
Project:Winecoff
V 98177SW-2A
15.8 06/13/2023 16:32SW-DRYWT Moisture %
V 98178SW-3A
25.1 06/13/2023 16:32SW-DRYWT Moisture %
V 98179Bottom B
21.6 06/13/2023 16:32SW-DRYWT Moisture %
Page 4 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-163-0021
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 06/12/2023
Winecoff
Report Date : 06/21/2023
Sample ID :
Lab No :
Sampled:SW-2A
98177 Matrix:
6/12/2023 11:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.8 %Moisture 1 06/13/23 16:32 SW-DRYWTCNC
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 5 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-163-0021
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 06/12/2023
Winecoff
Report Date : 06/21/2023
Sample ID :
Lab No :
Sampled:SW-2A
98177 Matrix:
6/12/2023 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):06/14/23 12:00
<10.9 mg/Kg - dry 10.9 59.3Aliphatic C9-C18 1 06/20/23 22:00 V34450AMP
<14.5 mg/Kg - dry 14.5 59.3Aliphatic C19-C36 1 06/20/23 22:00 V34450AMP
<16.9 mg/Kg - dry 16.9 59.3Aromatic C11-C22 1 06/20/23 22:00 V34450AMP
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 6 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-163-0021
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 06/12/2023
Winecoff
Report Date : 06/21/2023
Sample ID :
Lab No :
Sampled:SW-3A
98178 Matrix:
6/12/2023 11:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.1 %Moisture 1 06/13/23 16:32 SW-DRYWTCNC
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 7 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-163-0021
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 06/12/2023
Winecoff
Report Date : 06/21/2023
Sample ID :
Lab No :
Sampled:SW-3A
98178 Matrix:
6/12/2023 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):06/14/23 12:00
<12.3 mg/Kg - dry 12.3 66.8Aliphatic C9-C18 1 06/20/23 22:36 V34450AMP
<16.3 mg/Kg - dry 16.3 66.8Aliphatic C19-C36 1 06/20/23 22:36 V34450AMP
<19.0 mg/Kg - dry 19.0 66.8Aromatic C11-C22 1 06/20/23 22:36 V34450AMP
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 8 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-163-0021
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 06/12/2023
Winecoff
Report Date : 06/21/2023
Sample ID :
Lab No :
Sampled:Bottom B
98179 Matrix:
6/12/2023 11:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.6 %Moisture 1 06/13/23 16:32 SW-DRYWTCNC
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 9 of 14
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28273
23-163-0021
01197
Suite 250
Summit Engineering (Charlotte)
2520 Whitehall Park Dr
Matt Hoffman
Charlotte
Danyale Love
Project Manager
Received : 06/12/2023
Winecoff
Report Date : 06/21/2023
Sample ID :
Lab No :
Sampled:Bottom B
98179 Matrix:
6/12/2023 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):06/14/23 12:00
<11.7 mg/Kg - dry 11.7 63.6Aliphatic C9-C18 1 06/20/23 23:12 V34450AMP
<15.6 mg/Kg - dry 15.6 63.6Aliphatic C19-C36 1 06/20/23 23:12 V34450AMP
<18.1 mg/Kg - dry 18.1 63.6Aromatic C11-C22 1 06/20/23 23:12 V34450AMP
Surrogate: 2-Bromonaphthalene
Surrogate: Chlorooctadecane
Surrogate: OTP Surrogate
Surrogate: 2-Fluorobiphenyl
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 10 of 14
Quality Control Data
23-163-0021Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V34450QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V34328
Associated Lab Samples: 98177, 98178, 98179
LRB-V34328 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
06/20/23 18:2150.09.20<9.20mg/KgAliphatic C9-C18
06/20/23 18:2150.012.2<12.2mg/KgAliphatic C19-C36
06/20/23 18:2150.014.2<14.2mg/KgAromatic C11-C22
06/20/23 18:212-Fluorobiphenyl (S)98.5 40-140
06/20/23 18:212-Bromonaphthalene (S)91.7 40-140
06/20/23 18:21Chlorooctadecane (S)66.0 40-140
06/20/23 18:21OTP Surrogate (S)88.7 40-140
LCS-V34328 LCSD-V34328Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
44.1 73.571.542.960.0mg/KgAliphatic C9-C18 40-140 2.7 50
68.4 85.592.073.680.0mg/KgAliphatic C19-C36 40-140 7.3 50
185 109102174170mg/KgAromatic C11-C22 40-140 6.1 50
98.093.02-Fluorobiphenyl (S)40-140
95.089.72-Bromonaphthalene (S)40-140
65.767.8Chlorooctadecane (S)40-140
83.780.3OTP Surrogate (S)40-140
Page 1 of 2Date:06/21/2023 02:54 PM
Page 11 of 14
Quality Control Data
23-163-0021Report No:
Project Description:
Client ID:Summit Engineering (Charlotte)
Winecoff
Dry Weight Determination
SW-DRYWT
V34290QC Analytical Batch:
Analysis Method:
Analysis Description:
V 98068-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 06/13/23 16:321.531.131.6%Moisture
V 98178-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 06/13/23 16:320.325.025.1%Moisture
Page 2 of 2Date:06/21/2023 02:54 PM
Page 12 of 14
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-163-0021
Summit Engineering (Charlotte)
01197
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 4.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:06/12/2023 18:19:57
Special precautions or instructions included?
Comments:
Page 13 of 14
Page 14 of 14