MO-30102_49169_CA_SAR_20230825

ANALYTICAL REPORT
August 16, 2023
EHC, Inc.
Sample Delivery Group:L1642492
Samples Received:08/03/2023
Project Number:
Description:Statesville
Report To:Mr. Thomas Ammons
PO Box 902
Red Springs, NC 28377
Entire Report Reviewed By:
August 16, 2023
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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August 16, 2023
Heather J Wagner
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
SS-1 L1642492-01 5
SS-1 L1642492-02 8
Qc: Quality Control Summary 10
Total Solids by Method 2540 G-2011 10
Mercury by Method 7470A 11
Metals (ICP) by Method 6010D 12
Volatile Organic Compounds (GC/MS) by Method 8260D 13
Chlorinated Acid Herbicides (GC) by Method 8151A 21
Pesticides (GC) by Method 8081B 22
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 23
Gl: Glossary of Terms 30
Al: Accreditations & Locations 31
Sc: Sample Chain of Custody 32
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SS-1 L1642492-01 Solid Aric Clark 08/02/23 14:05 08/03/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG2108300 1 08/05/23 18:07 08/05/23 18:22 CMK Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2110246 1 08/02/23 14:05 08/09/23 01:20 JBE Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2110345 1 08/09/23 09:28 08/10/23 07:12 JDJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2110345 20 08/09/23 09:28 08/12/23 06:48 JCH Mt. Juliet, TN
Collected by Collected date/time Received date/time
SS-1 L1642492-02 Waste Aric Clark 08/02/23 14:05 08/03/23 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Preparation by Method 1311 WG2108018 1 08/06/23 09:41 08/06/23 09:41 NAH Mt. Juliet, TN
Preparation by Method 1311 WG2108027 1 08/06/23 12:24 08/06/23 12:24 JTM Mt. Juliet, TN
Mercury by Method 7470A WG2108984 1 08/07/23 11:16 08/07/23 16:39 AKB Mt. Juliet, TN
Metals (ICP) by Method 6010D WG2109177 1 08/07/23 12:37 08/08/23 12:22 ZSA Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG2109635 1 08/09/23 19:47 08/09/23 19:47 JHH Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A WG2109557 1 08/09/23 14:11 08/10/23 06:31 HMH Mt. Juliet, TN
Pesticides (GC) by Method 8081B WG2109521 1 08/08/23 06:40 08/08/23 16:51 DLH Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG2110330 1 08/09/23 07:53 08/10/23 04:08 MBE Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Heather J Wagner
Project Manager
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SAMPLE RESULTS - 01
L1642492
SS-1
Collected date/time: 08/02/23 14:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 97.8 1 08/05/2023 18:22 WG2108300
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND C3 0.0532 1 08/09/2023 01:20 WG2110246
Acrylonitrile ND 0.0133 1 08/09/2023 01:20 WG2110246
Benzene 0.00118 0.00106 1 08/09/2023 01:20 WG2110246
Bromobenzene ND 0.0133 1 08/09/2023 01:20 WG2110246
Bromodichloromethane ND 0.00266 1 08/09/2023 01:20 WG2110246
Bromoform ND 0.0266 1 08/09/2023 01:20 WG2110246
Bromomethane ND 0.0133 1 08/09/2023 01:20 WG2110246
n-Butylbenzene ND 0.0133 1 08/09/2023 01:20 WG2110246
sec-Butylbenzene 0.0369 0.0133 1 08/09/2023 01:20 WG2110246
tert-Butylbenzene ND C3 0.00532 1 08/09/2023 01:20 WG2110246
Carbon tetrachloride ND 0.00532 1 08/09/2023 01:20 WG2110246
Chlorobenzene ND 0.00266 1 08/09/2023 01:20 WG2110246
Chlorodibromomethane ND 0.00266 1 08/09/2023 01:20 WG2110246
Chloroethane ND 0.00532 1 08/09/2023 01:20 WG2110246
Chloroform ND 0.00266 1 08/09/2023 01:20 WG2110246
Chloromethane ND J3 J4 0.0133 1 08/09/2023 01:20 WG2110246
2-Chlorotoluene ND 0.00266 1 08/09/2023 01:20 WG2110246
4-Chlorotoluene ND 0.00532 1 08/09/2023 01:20 WG2110246
1,2-Dibromo-3-Chloropropane ND 0.0266 1 08/09/2023 01:20 WG2110246
1,2-Dibromoethane ND 0.00266 1 08/09/2023 01:20 WG2110246
Dibromomethane ND 0.00532 1 08/09/2023 01:20 WG2110246
1,2-Dichlorobenzene ND 0.00532 1 08/09/2023 01:20 WG2110246
1,3-Dichlorobenzene ND 0.00532 1 08/09/2023 01:20 WG2110246
1,4-Dichlorobenzene ND 0.00532 1 08/09/2023 01:20 WG2110246
Dichlorodifluoromethane ND 0.00266 1 08/09/2023 01:20 WG2110246
1,1-Dichloroethane ND 0.00266 1 08/09/2023 01:20 WG2110246
1,2-Dichloroethane ND 0.00266 1 08/09/2023 01:20 WG2110246
1,1-Dichloroethene ND 0.00266 1 08/09/2023 01:20 WG2110246
cis-1,2-Dichloroethene ND 0.00266 1 08/09/2023 01:20 WG2110246
trans-1,2-Dichloroethene ND 0.00532 1 08/09/2023 01:20 WG2110246
1,2-Dichloropropane ND 0.00532 1 08/09/2023 01:20 WG2110246
1,1-Dichloropropene ND 0.00266 1 08/09/2023 01:20 WG2110246
1,3-Dichloropropane ND 0.00532 1 08/09/2023 01:20 WG2110246
cis-1,3-Dichloropropene ND 0.00266 1 08/09/2023 01:20 WG2110246
trans-1,3-Dichloropropene ND 0.00532 1 08/09/2023 01:20 WG2110246
2,2-Dichloropropane ND 0.00266 1 08/09/2023 01:20 WG2110246
Di-isopropyl ether ND 0.00106 1 08/09/2023 01:20 WG2110246
Ethylbenzene 0.00973 0.00266 1 08/09/2023 01:20 WG2110246
Hexachloro-1,3-butadiene ND 0.0266 1 08/09/2023 01:20 WG2110246
Isopropylbenzene ND 0.00266 1 08/09/2023 01:20 WG2110246
p-Isopropyltoluene 0.216 C3 0.00532 1 08/09/2023 01:20 WG2110246
2-Butanone (MEK)ND 0.106 1 08/09/2023 01:20 WG2110246
Methylene Chloride ND 0.0266 1 08/09/2023 01:20 WG2110246
4-Methyl-2-pentanone (MIBK)ND 0.0266 1 08/09/2023 01:20 WG2110246
Methyl tert-butyl ether ND 0.00106 1 08/09/2023 01:20 WG2110246
Naphthalene 0.201 C3 0.0133 1 08/09/2023 01:20 WG2110246
n-Propylbenzene ND 0.00532 1 08/09/2023 01:20 WG2110246
Styrene ND 0.0133 1 08/09/2023 01:20 WG2110246
1,1,1,2-Tetrachloroethane ND 0.00266 1 08/09/2023 01:20 WG2110246
1,1,2,2-Tetrachloroethane ND 0.00266 1 08/09/2023 01:20 WG2110246
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1642492
SS-1
Collected date/time: 08/02/23 14:05
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane ND 0.00266 1 08/09/2023 01:20 WG2110246
Tetrachloroethene ND 0.00266 1 08/09/2023 01:20 WG2110246
Toluene 0.0149 0.00532 1 08/09/2023 01:20 WG2110246
1,2,3-Trichlorobenzene ND C3 0.0133 1 08/09/2023 01:20 WG2110246
1,2,4-Trichlorobenzene ND C3 0.0133 1 08/09/2023 01:20 WG2110246
1,1,1-Trichloroethane ND 0.00266 1 08/09/2023 01:20 WG2110246
1,1,2-Trichloroethane ND 0.00266 1 08/09/2023 01:20 WG2110246
Trichloroethene ND 0.00106 1 08/09/2023 01:20 WG2110246
Trichlorofluoromethane ND 0.00266 1 08/09/2023 01:20 WG2110246
1,2,3-Trichloropropane ND 0.0133 1 08/09/2023 01:20 WG2110246
1,2,4-Trimethylbenzene 0.456 C3 0.00532 1 08/09/2023 01:20 WG2110246
1,2,3-Trimethylbenzene 0.967 C3 0.00532 1 08/09/2023 01:20 WG2110246
1,3,5-Trimethylbenzene 0.565 0.00532 1 08/09/2023 01:20 WG2110246
Vinyl chloride ND J4 0.00266 1 08/09/2023 01:20 WG2110246
Xylenes, Total 0.299 0.00692 1 08/09/2023 01:20 WG2110246
(S) Toluene-d8 108 75.0-131 08/09/2023 01:20 WG2110246
(S) 4-Bromofluorobenzene 120 67.0-138 08/09/2023 01:20 WG2110246
(S) 1,2-Dichloroethane-d4 91.4 70.0-130 08/09/2023 01:20 WG2110246
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.681 20 08/12/2023 06:48 WG2110345
Acenaphthylene ND 0.681 20 08/12/2023 06:48 WG2110345
Anthracene ND 0.681 20 08/12/2023 06:48 WG2110345
Benzidine ND 34.2 20 08/12/2023 06:48 WG2110345
Benzo(a)anthracene ND 0.681 20 08/12/2023 06:48 WG2110345
Benzo(b)fluoranthene ND 0.681 20 08/12/2023 06:48 WG2110345
Benzo(k)fluoranthene ND 0.681 20 08/12/2023 06:48 WG2110345
Benzo(g,h,i)perylene ND 0.681 20 08/12/2023 06:48 WG2110345
Benzo(a)pyrene ND 0.681 20 08/12/2023 06:48 WG2110345
Bis(2-chlorethoxy)methane ND 0.341 1 08/10/2023 07:12 WG2110345
Bis(2-chloroethyl)ether ND 0.341 1 08/10/2023 07:12 WG2110345
2,2-Oxybis(1-Chloropropane)ND 0.341 1 08/10/2023 07:12 WG2110345
4-Bromophenyl-phenylether ND 6.81 20 08/12/2023 06:48 WG2110345
2-Chloronaphthalene ND 0.681 20 08/12/2023 06:48 WG2110345
4-Chlorophenyl-phenylether ND 6.81 20 08/12/2023 06:48 WG2110345
Chrysene ND 0.681 20 08/12/2023 06:48 WG2110345
Dibenz(a,h)anthracene ND 0.681 20 08/12/2023 06:48 WG2110345
3,3-Dichlorobenzidine ND 6.81 20 08/12/2023 06:48 WG2110345
2,4-Dinitrotoluene ND 6.81 20 08/12/2023 06:48 WG2110345
2,6-Dinitrotoluene ND 6.81 20 08/12/2023 06:48 WG2110345
Fluoranthene ND 0.681 20 08/12/2023 06:48 WG2110345
Fluorene ND 0.681 20 08/12/2023 06:48 WG2110345
Hexachlorobenzene ND 6.81 20 08/12/2023 06:48 WG2110345
Hexachloro-1,3-butadiene ND 0.341 1 08/10/2023 07:12 WG2110345
Hexachlorocyclopentadiene ND C3 6.81 20 08/12/2023 06:48 WG2110345
Hexachloroethane ND 0.341 1 08/10/2023 07:12 WG2110345
Indeno(1,2,3-cd)pyrene ND J4 0.681 20 08/12/2023 06:48 WG2110345
Isophorone ND 0.341 1 08/10/2023 07:12 WG2110345
Naphthalene ND 0.0341 1 08/10/2023 07:12 WG2110345
Nitrobenzene ND 0.341 1 08/10/2023 07:12 WG2110345
n-Nitrosodimethylamine ND 0.341 1 08/10/2023 07:12 WG2110345
n-Nitrosodiphenylamine ND 6.81 20 08/12/2023 06:48 WG2110345
n-Nitrosodi-n-propylamine ND 0.341 1 08/10/2023 07:12 WG2110345
Phenanthrene ND 0.681 20 08/12/2023 06:48 WG2110345
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1642492
SS-1
Collected date/time: 08/02/23 14:05
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Benzylbutyl phthalate ND 6.81 20 08/12/2023 06:48 WG2110345
Bis(2-ethylhexyl)phthalate ND 6.81 20 08/12/2023 06:48 WG2110345
Di-n-butyl phthalate ND 6.81 20 08/12/2023 06:48 WG2110345
Diethyl phthalate ND 6.81 20 08/12/2023 06:48 WG2110345
Dimethyl phthalate ND 6.81 20 08/12/2023 06:48 WG2110345
Di-n-octyl phthalate ND 6.81 20 08/12/2023 06:48 WG2110345
Pyrene ND 0.681 20 08/12/2023 06:48 WG2110345
1,2,4-Trichlorobenzene ND 0.341 1 08/10/2023 07:12 WG2110345
4-Chloro-3-methylphenol ND 0.341 1 08/10/2023 07:12 WG2110345
2-Chlorophenol ND 0.341 1 08/10/2023 07:12 WG2110345
2,4-Dichlorophenol ND 0.341 1 08/10/2023 07:12 WG2110345
2,4-Dimethylphenol ND 0.341 1 08/10/2023 07:12 WG2110345
4,6-Dinitro-2-methylphenol ND 6.81 20 08/12/2023 06:48 WG2110345
2,4-Dinitrophenol ND 6.81 20 08/12/2023 06:48 WG2110345
2-Nitrophenol ND 0.341 1 08/10/2023 07:12 WG2110345
4-Nitrophenol ND 6.81 20 08/12/2023 06:48 WG2110345
Pentachlorophenol ND 6.81 20 08/12/2023 06:48 WG2110345
Phenol ND 0.341 1 08/10/2023 07:12 WG2110345
2,4,6-Trichlorophenol ND 6.81 20 08/12/2023 06:48 WG2110345
(S) 2-Fluorophenol 40.2 12.0-120 08/10/2023 07:12 WG2110345
(S) 2-Fluorophenol 63.9 J7 12.0-120 08/12/2023 06:48 WG2110345
(S) Phenol-d5 42.1 10.0-120 08/10/2023 07:12 WG2110345
(S) Phenol-d5 57.4 J7 10.0-120 08/12/2023 06:48 WG2110345
(S) Nitrobenzene-d5 0.000 J2 10.0-122 08/10/2023 07:12 WG2110345
(S) Nitrobenzene-d5 0.000 J7 10.0-122 08/12/2023 06:48 WG2110345
(S) 2-Fluorobiphenyl 59.1 J7 15.0-120 08/12/2023 06:48 WG2110345
(S) 2-Fluorobiphenyl 41.2 15.0-120 08/10/2023 07:12 WG2110345
(S) 2,4,6-Tribromophenol 64.5 10.0-127 08/10/2023 07:12 WG2110345
(S) 2,4,6-Tribromophenol 62.6 J7 10.0-127 08/12/2023 06:48 WG2110345
(S) p-Terphenyl-d14 56.4 10.0-120 08/10/2023 07:12 WG2110345
(S) p-Terphenyl-d14 69.1 J7 10.0-120 08/12/2023 06:48 WG2110345
Sample Narrative:
L1642492-01 WG2110345: Dilution and surrogate failure due to matrix interference.
L1642492-01 WG2110345: Surrogate failure due to matrix interference.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1642492
SS-1
Collected date/time: 08/02/23 14:05
Preparation by Method 1311
Result Qualifier Prep Batch
Analyte date / time
TCLP Extraction -8/6/2023 9:41:54 AM WG2108018
TCLP ZHE Extraction -8/6/2023 12:24:28 PM WG2108027
Initial pH 8.71 8/6/2023 9:41:54 AM WG2108018
Final pH 5.01 8/6/2023 9:41:54 AM WG2108018
Mercury by Method 7470A
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Mercury ND 0.0100 0.20 1 08/07/2023 16:39 WG2108984
Metals (ICP) by Method 6010D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Arsenic ND 0.100 5 1 08/08/2023 12:22 WG2109177
Barium 0.712 0.100 100 1 08/08/2023 12:22 WG2109177
Cadmium ND 0.100 1 1 08/08/2023 12:22 WG2109177
Chromium ND 0.100 5 1 08/08/2023 12:22 WG2109177
Lead ND 0.100 5 1 08/08/2023 12:22 WG2109177
Selenium ND 0.100 1 1 08/08/2023 12:22 WG2109177
Silver ND 0.100 5 1 08/08/2023 12:22 WG2109177
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Benzene ND 0.0500 0.50 1 08/09/2023 19:47 WG2109635
Carbon tetrachloride ND 0.0500 0.50 1 08/09/2023 19:47 WG2109635
Chlorobenzene ND 0.0500 100 1 08/09/2023 19:47 WG2109635
Chloroform ND 0.250 6 1 08/09/2023 19:47 WG2109635
1,2-Dichloroethane ND 0.0500 0.50 1 08/09/2023 19:47 WG2109635
1,1-Dichloroethene ND 0.0500 0.70 1 08/09/2023 19:47 WG2109635
2-Butanone (MEK)ND 0.500 200 1 08/09/2023 19:47 WG2109635
Tetrachloroethene ND 0.0500 0.70 1 08/09/2023 19:47 WG2109635
Trichloroethene ND 0.0500 0.50 1 08/09/2023 19:47 WG2109635
Vinyl chloride ND 0.0500 0.20 1 08/09/2023 19:47 WG2109635
(S) Toluene-d8 107 80.0-120 08/09/2023 19:47 WG2109635
(S) 4-Bromofluorobenzene 94.9 77.0-126 08/09/2023 19:47 WG2109635
(S) 1,2-Dichloroethane-d4 104 70.0-130 08/09/2023 19:47 WG2109635
Chlorinated Acid Herbicides (GC) by Method 8151A
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
2,4,5-TP (Silvex)ND 0.00200 1 08/10/2023 06:31 WG2109557
2,4-D ND 0.00200 1 08/10/2023 06:31 WG2109557
(S) 2,4-Dichlorophenyl Acetic Acid 126 14.0-158 08/10/2023 06:31 WG2109557
Pesticides (GC) by Method 8081B
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Chlordane ND 0.00500 0.03 1 08/08/2023 16:51 WG2109521
Endrin ND 0.00500 0.02 1 08/08/2023 16:51 WG2109521
Heptachlor ND 0.00500 0.0080 1 08/08/2023 16:51 WG2109521
Lindane ND 0.00500 0.40 1 08/08/2023 16:51 WG2109521
Methoxychlor ND 0.00500 10 1 08/08/2023 16:51 WG2109521
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1642492
SS-1
Collected date/time: 08/02/23 14:05
Pesticides (GC) by Method 8081B
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
Toxaphene ND 0.0100 0.50 1 08/08/2023 16:51 WG2109521
(S) Decachlorobiphenyl 70.2 10.0-128 08/08/2023 16:51 WG2109521
(S) Tetrachloro-m-xylene 69.4 10.0-127 08/08/2023 16:51 WG2109521
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/l mg/l mg/l date / time
1,4-Dichlorobenzene ND 0.100 7.50 1 08/10/2023 04:08 WG2110330
2,4-Dinitrotoluene ND 0.100 0.13 1 08/10/2023 04:08 WG2110330
Hexachlorobenzene ND 0.100 0.13 1 08/10/2023 04:08 WG2110330
Hexachloro-1,3-butadiene ND 0.100 0.50 1 08/10/2023 04:08 WG2110330
Hexachloroethane ND 0.100 3 1 08/10/2023 04:08 WG2110330
Nitrobenzene ND 0.100 2 1 08/10/2023 04:08 WG2110330
Pyridine ND 0.100 5 1 08/10/2023 04:08 WG2110330
3&4-Methyl Phenol ND 0.100 400 1 08/10/2023 04:08 WG2110330
2-Methylphenol ND 0.100 200 1 08/10/2023 04:08 WG2110330
Pentachlorophenol ND 0.100 100 1 08/10/2023 04:08 WG2110330
2,4,5-Trichlorophenol ND 0.100 400 1 08/10/2023 04:08 WG2110330
2,4,6-Trichlorophenol ND 0.100 2 1 08/10/2023 04:08 WG2110330
(S) 2-Fluorophenol 16.0 10.0-120 08/10/2023 04:08 WG2110330
(S) Phenol-d5 10.0 10.0-120 08/10/2023 04:08 WG2110330
(S) Nitrobenzene-d5 46.4 10.0-127 08/10/2023 04:08 WG2110330
(S) 2-Fluorobiphenyl 46.7 10.0-130 08/10/2023 04:08 WG2110330
(S) 2,4,6-Tribromophenol 52.0 10.0-155 08/10/2023 04:08 WG2110330
(S) p-Terphenyl-d14 65.4 10.0-128 08/10/2023 04:08 WG2110330
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2108300
Total Solids by Method 2540 G-2011 L1642492-01
Method Blank (MB)
(MB) R3957465-1 08/05/23 18:22
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1642336-10 Original Sample (OS) • Duplicate (DUP)
(OS) L1642336-10 08/05/23 18:22 • (DUP) R3957465-3 08/05/23 18:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 88.1 84.8 1 3.85 10
Laboratory Control Sample (LCS)
(LCS) R3957465-2 08/05/23 18:22
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2108984
Mercury by Method 7470A L1642492-02
Method Blank (MB)
(MB) R3957752-1 08/07/23 16:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Mercury U 0.00330 0.0100
Laboratory Control Sample (LCS)
(LCS) R3957752-2 08/07/23 16:25
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Mercury 0.0300 0.0345 115 80.0-120
L1642479-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1642479-02 08/07/23 16:27 • (MS) R3957752-3 08/07/23 16:30 • (MSD) R3957752-5 08/07/23 16:32
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Mercury 0.0300 ND 0.0351 0.0347 117 116 1 75.0-125 1.10 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2109177
Metals (ICP) by Method 6010D L1642492-02
Method Blank (MB)
(MB) R3958082-1 08/08/23 11:36
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Arsenic U 0.0333 0.100
Barium U 0.0333 0.100
Cadmium U 0.0333 0.100
Chromium U 0.0333 0.100
Lead U 0.0333 0.100
Selenium U 0.0333 0.100
Silver U 0.0333 0.100
Laboratory Control Sample (LCS)
(LCS) R3958082-2 08/08/23 11:38
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Arsenic 10.0 10.3 103 80.0-120
Barium 10.0 9.91 99.1 80.0-120
Cadmium 10.0 9.73 97.3 80.0-120
Chromium 10.0 9.70 97.0 80.0-120
Lead 10.0 10.1 101 80.0-120
Selenium 10.0 9.51 95.1 80.0-120
Silver 2.00 1.92 96.2 80.0-120
L1641772-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1641772-05 08/08/23 11:41 • (MS) R3958082-4 08/08/23 11:46 • (MSD) R3958082-5 08/08/23 11:49
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Arsenic 10.0 ND 10.7 10.9 107 109 1 75.0-125 1.58 20
Barium 10.0 0.441 10.6 10.7 101 103 1 75.0-125 1.58 20
Cadmium 10.0 ND 10.1 10.2 101 102 1 75.0-125 0.919 20
Chromium 10.0 ND 9.97 9.94 99.7 99.4 1 75.0-125 0.244 20
Lead 10.0 ND 10.5 10.6 105 106 1 75.0-125 1.01 20
Selenium 10.0 ND 9.72 9.83 97.2 98.3 1 75.0-125 1.08 20
Silver 2.00 ND 2.00 2.01 100 100 1 75.0-125 0.275 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2109635
Volatile Organic Compounds (GC/MS) by Method 8260D L1642492-02
Method Blank (MB)
(MB) R3958810-2 08/09/23 15:01
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Benzene U 0.0167 0.0500
Carbon tetrachloride U 0.0167 0.0500
Chlorobenzene U 0.0167 0.0500
Chloroform U 0.0833 0.250
1,2-Dichloroethane U 0.0167 0.0500
1,1-Dichloroethene U 0.0167 0.0500
2-Butanone (MEK)U 0.167 0.500
Tetrachloroethene U 0.0167 0.0500
Trichloroethene U 0.0167 0.0500
Vinyl chloride U 0.0167 0.0500
(S) Toluene-d8 106 80.0-120
(S) 4-Bromofluorobenzene 99.4 77.0-126
(S) 1,2-Dichloroethane-d4 105 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3958810-1 08/09/23 12:15 • (LCSD) R3958810-5 08/09/23 21:03
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Benzene 0.250 0.240 0.252 96.0 101 70.0-123 4.88 20
Carbon tetrachloride 0.250 0.218 0.246 87.2 98.4 68.0-126 12.1 20
Chlorobenzene 0.250 0.243 0.255 97.2 102 80.0-121 4.82 20
Chloroform 0.250 0.216 0.236 86.4 94.4 73.0-120 8.85 20
1,2-Dichloroethane 0.250 0.229 0.244 91.6 97.6 70.0-128 6.34 20
1,1-Dichloroethene 0.250 0.209 0.233 83.6 93.2 71.0-124 10.9 20
2-Butanone (MEK)1.25 1.25 1.25 100 100 44.0-160 0.000 20
Tetrachloroethene 0.250 0.244 0.251 97.6 100 72.0-132 2.83 20
Trichloroethene 0.250 0.230 0.255 92.0 102 78.0-124 10.3 20
Vinyl chloride 0.250 0.234 0.244 93.6 97.6 67.0-131 4.18 20
(S) Toluene-d8 110 107 80.0-120
(S) 4-Bromofluorobenzene 92.8 96.2 77.0-126
(S) 1,2-Dichloroethane-d4 101 103 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2109635
Volatile Organic Compounds (GC/MS) by Method 8260D L1642492-02
L1642101-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1642101-11 08/09/23 18:50 • (MS) R3958810-3 08/09/23 20:06 • (MSD) R3958810-4 08/09/23 20:25
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Benzene 0.250 ND 0.167 0.193 66.8 77.2 1 17.0-158 14.4 27
Carbon tetrachloride 0.250 ND 0.153 0.177 61.2 70.8 1 23.0-159 14.5 28
Chlorobenzene 0.250 ND 0.172 0.206 68.8 82.4 1 33.0-152 18.0 27
Chloroform 0.250 ND ND ND 61.6 74.0 1 29.0-154 18.3 28
1,2-Dichloroethane 0.250 ND 0.174 0.201 69.6 80.4 1 29.0-151 14.4 27
1,1-Dichloroethene 0.250 ND 0.145 0.169 58.0 67.6 1 11.0-160 15.3 29
2-Butanone (MEK)1.25 ND 0.881 1.09 70.5 87.2 1 10.0-160 21.2 32
Tetrachloroethene 0.250 ND 0.161 0.186 64.4 74.4 1 10.0-160 14.4 27
Trichloroethene 0.250 ND 0.149 0.178 59.6 71.2 1 10.0-160 17.7 25
Vinyl chloride 0.250 ND 0.151 0.184 60.4 73.6 1 10.0-160 19.7 27
(S) Toluene-d8 111 110 80.0-120
(S) 4-Bromofluorobenzene 96.6 95.5 77.0-126
(S) 1,2-Dichloroethane-d4 103 102 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110246
Volatile Organic Compounds (GC/MS) by Method 8260D L1642492-01
Method Blank (MB)
(MB) R3960913-3 08/08/23 19:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane 0.00523 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110246
Volatile Organic Compounds (GC/MS) by Method 8260D L1642492-01
Method Blank (MB)
(MB) R3960913-3 08/08/23 19:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)U 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Methyl tert-butyl ether 0.000650 J 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 117 75.0-131
(S) 4-Bromofluorobenzene 85.6 67.0-138
(S) 1,2-Dichloroethane-d4 93.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3960913-1 08/08/23 18:14 • (LCSD) R3960913-2 08/08/23 18:34
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.465 0.501 74.4 80.2 10.0-160 7.45 31
Acrylonitrile 0.625 0.575 0.633 92.0 101 45.0-153 9.60 22
Benzene 0.125 0.109 0.112 87.2 89.6 70.0-123 2.71 20
Bromobenzene 0.125 0.121 0.127 96.8 102 73.0-121 4.84 20
Bromodichloromethane 0.125 0.106 0.114 84.8 91.2 73.0-121 7.27 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110246
Volatile Organic Compounds (GC/MS) by Method 8260D L1642492-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3960913-1 08/08/23 18:14 • (LCSD) R3960913-2 08/08/23 18:34
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.126 0.128 101 102 64.0-132 1.57 20
Bromomethane 0.125 0.175 0.176 140 141 56.0-147 0.570 20
n-Butylbenzene 0.125 0.105 0.117 84.0 93.6 68.0-135 10.8 20
sec-Butylbenzene 0.125 0.101 0.110 80.8 88.0 74.0-130 8.53 20
tert-Butylbenzene 0.125 0.0956 0.102 76.5 81.6 75.0-127 6.48 20
Carbon tetrachloride 0.125 0.138 0.145 110 116 66.0-128 4.95 20
Chlorobenzene 0.125 0.120 0.124 96.0 99.2 76.0-128 3.28 20
Chlorodibromomethane 0.125 0.129 0.134 103 107 74.0-127 3.80 20
Chloroethane 0.125 0.151 0.155 121 124 61.0-134 2.61 20
Chloroform 0.125 0.115 0.120 92.0 96.0 72.0-123 4.26 20
Chloromethane 0.125 0.150 0.208 120 166 51.0-138 J3 J4 32.4 20
2-Chlorotoluene 0.125 0.121 0.131 96.8 105 75.0-124 7.94 20
4-Chlorotoluene 0.125 0.101 0.102 80.8 81.6 75.0-124 0.985 20
1,2-Dibromo-3-Chloropropane 0.125 0.113 0.112 90.4 89.6 59.0-130 0.889 20
1,2-Dibromoethane 0.125 0.115 0.117 92.0 93.6 74.0-128 1.72 20
Dibromomethane 0.125 0.107 0.117 85.6 93.6 75.0-122 8.93 20
1,2-Dichlorobenzene 0.125 0.110 0.121 88.0 96.8 76.0-124 9.52 20
1,3-Dichlorobenzene 0.125 0.111 0.119 88.8 95.2 76.0-125 6.96 20
1,4-Dichlorobenzene 0.125 0.115 0.122 92.0 97.6 77.0-121 5.91 20
Dichlorodifluoromethane 0.125 0.144 0.160 115 128 43.0-156 10.5 20
1,1-Dichloroethane 0.125 0.118 0.119 94.4 95.2 70.0-127 0.844 20
1,2-Dichloroethane 0.125 0.108 0.116 86.4 92.8 65.0-131 7.14 20
1,1-Dichloroethene 0.125 0.135 0.141 108 113 65.0-131 4.35 20
cis-1,2-Dichloroethene 0.125 0.115 0.115 92.0 92.0 73.0-125 0.000 20
trans-1,2-Dichloroethene 0.125 0.121 0.124 96.8 99.2 71.0-125 2.45 20
1,2-Dichloropropane 0.125 0.109 0.111 87.2 88.8 74.0-125 1.82 20
1,1-Dichloropropene 0.125 0.122 0.134 97.6 107 73.0-125 9.38 20
1,3-Dichloropropane 0.125 0.120 0.125 96.0 100 80.0-125 4.08 20
cis-1,3-Dichloropropene 0.125 0.102 0.105 81.6 84.0 76.0-127 2.90 20
trans-1,3-Dichloropropene 0.125 0.117 0.124 93.6 99.2 73.0-127 5.81 20
2,2-Dichloropropane 0.125 0.133 0.131 106 105 59.0-135 1.52 20
Di-isopropyl ether 0.125 0.110 0.110 88.0 88.0 60.0-136 0.000 20
Ethylbenzene 0.125 0.123 0.119 98.4 95.2 74.0-126 3.31 20
Hexachloro-1,3-butadiene 0.125 0.113 0.133 90.4 106 57.0-150 16.3 20
Isopropylbenzene 0.125 0.111 0.115 88.8 92.0 72.0-127 3.54 20
p-Isopropyltoluene 0.125 0.0991 0.108 79.3 86.4 72.0-133 8.59 20
2-Butanone (MEK)0.625 0.605 0.660 96.8 106 30.0-160 8.70 24
Methylene Chloride 0.125 0.106 0.112 84.8 89.6 68.0-123 5.50 20
4-Methyl-2-pentanone (MIBK)0.625 0.665 0.679 106 109 56.0-143 2.08 20
Methyl tert-butyl ether 0.125 0.116 0.120 92.8 96.0 66.0-132 3.39 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110246
Volatile Organic Compounds (GC/MS) by Method 8260D L1642492-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3960913-1 08/08/23 18:14 • (LCSD) R3960913-2 08/08/23 18:34
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.0832 0.0899 66.6 71.9 59.0-130 7.74 20
n-Propylbenzene 0.125 0.105 0.115 84.0 92.0 74.0-126 9.09 20
Styrene 0.125 0.107 0.115 85.6 92.0 72.0-127 7.21 20
1,1,1,2-Tetrachloroethane 0.125 0.138 0.143 110 114 74.0-129 3.56 20
1,1,2,2-Tetrachloroethane 0.125 0.122 0.126 97.6 101 68.0-128 3.23 20
1,1,2-Trichlorotrifluoroethane 0.125 0.119 0.126 95.2 101 61.0-139 5.71 20
Tetrachloroethene 0.125 0.142 0.148 114 118 70.0-136 4.14 20
Toluene 0.125 0.122 0.128 97.6 102 75.0-121 4.80 20
1,2,3-Trichlorobenzene 0.125 0.0938 0.110 75.0 88.0 59.0-139 15.9 20
1,2,4-Trichlorobenzene 0.125 0.0954 0.107 76.3 85.6 62.0-137 11.5 20
1,1,1-Trichloroethane 0.125 0.124 0.128 99.2 102 69.0-126 3.17 20
1,1,2-Trichloroethane 0.125 0.119 0.123 95.2 98.4 78.0-123 3.31 20
Trichloroethene 0.125 0.120 0.131 96.0 105 76.0-126 8.76 20
Trichlorofluoromethane 0.125 0.141 0.153 113 122 61.0-142 8.16 20
1,2,3-Trichloropropane 0.125 0.125 0.132 100 106 67.0-129 5.45 20
1,2,4-Trimethylbenzene 0.125 0.0966 0.101 77.3 80.8 70.0-126 4.45 20
1,2,3-Trimethylbenzene 0.125 0.0965 0.103 77.2 82.4 74.0-124 6.52 20
1,3,5-Trimethylbenzene 0.125 0.101 0.107 80.8 85.6 73.0-127 5.77 20
Vinyl chloride 0.125 0.163 0.178 130 142 63.0-134 J4 8.80 20
Xylenes, Total 0.375 0.341 0.357 90.9 95.2 72.0-127 4.58 20
(S) Toluene-d8 112 112 75.0-131
(S) 4-Bromofluorobenzene 89.5 87.5 67.0-138
(S) 1,2-Dichloroethane-d4 103 104 70.0-130
L1641201-17 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1641201-17 08/09/23 04:36 • (MS) R3960913-4 08/09/23 05:15 • (MSD) R3960913-5 08/09/23 05:35
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 16.4 ND 11.7 12.7 71.5 77.4 20 10.0-160 7.85 40
Acrylonitrile 16.4 ND 14.2 16.1 86.4 98.3 20 10.0-160 12.8 40
Benzene 3.27 ND 2.18 2.68 66.8 82.1 20 10.0-149 20.6 37
Bromobenzene 3.27 ND 2.67 3.50 81.7 107 20 10.0-156 27.0 38
Bromodichloromethane 3.27 ND 2.40 2.86 73.6 87.7 20 10.0-143 17.4 37
Bromoform 3.27 ND 3.22 3.81 98.7 117 20 10.0-146 16.6 36
Bromomethane 3.27 ND 2.95 3.95 90.2 121 20 10.0-149 29.0 38
n-Butylbenzene 3.27 ND 3.96 4.88 121 149 20 10.0-160 20.8 40
sec-Butylbenzene 3.27 ND 2.29 3.28 70.2 100 20 10.0-159 35.4 39
tert-Butylbenzene 3.27 ND 2.25 3.06 68.9 93.6 20 10.0-156 30.4 39
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110246
Volatile Organic Compounds (GC/MS) by Method 8260D L1642492-01
L1641201-17 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1641201-17 08/09/23 04:36 • (MS) R3960913-4 08/09/23 05:15 • (MSD) R3960913-5 08/09/23 05:35
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 3.27 ND 2.49 3.39 76.2 104 20 10.0-145 30.7 37
Chlorobenzene 3.27 ND 2.61 3.29 80.0 101 20 10.0-152 23.1 39
Chlorodibromomethane 3.27 ND 2.92 3.81 89.4 117 20 10.0-146 26.4 37
Chloroethane 3.27 ND 2.61 3.57 80.0 109 20 10.0-146 31.0 40
Chloroform 3.27 ND 2.43 3.06 74.5 93.6 20 10.0-146 22.8 37
Chloromethane 3.27 ND 3.07 3.95 94.0 121 20 10.0-159 25.0 37
2-Chlorotoluene 3.27 ND 2.60 3.36 79.6 103 20 10.0-159 25.6 38
4-Chlorotoluene 3.27 ND 2.21 2.97 67.7 91.1 20 10.0-155 29.5 39
1,2-Dibromo-3-Chloropropane 3.27 ND 3.04 3.67 93.2 112 20 10.0-151 18.6 39
1,2-Dibromoethane 3.27 ND 2.84 3.27 86.8 100 20 10.0-148 14.1 34
Dibromomethane 3.27 ND 2.61 2.99 80.0 91.5 20 10.0-147 13.4 35
1,2-Dichlorobenzene 3.27 ND 2.60 3.35 79.6 103 20 10.0-155 25.2 37
1,3-Dichlorobenzene 3.27 ND 2.52 3.38 77.0 103 20 10.0-153 29.2 38
1,4-Dichlorobenzene 3.27 ND 2.45 3.32 74.9 102 20 10.0-151 30.4 38
Dichlorodifluoromethane 3.27 ND 2.60 3.54 79.6 109 20 10.0-160 30.8 35
1,1-Dichloroethane 3.27 ND 2.32 2.93 71.1 89.8 20 10.0-147 23.3 37
1,2-Dichloroethane 3.27 ND 2.52 2.89 77.0 88.5 20 10.0-148 13.9 35
1,1-Dichloroethene 3.27 ND 2.29 3.16 70.2 96.6 20 10.0-155 31.6 37
cis-1,2-Dichloroethene 3.27 ND 2.24 2.91 68.5 88.9 20 10.0-149 25.9 37
trans-1,2-Dichloroethene 3.27 ND 2.25 2.92 68.9 89.4 20 10.0-150 25.8 37
1,2-Dichloropropane 3.27 ND 2.31 2.84 70.6 86.8 20 10.0-148 20.5 37
1,1-Dichloropropene 3.27 ND 2.24 3.09 68.5 94.5 20 10.0-153 31.9 35
1,3-Dichloropropane 3.27 ND 2.75 3.29 84.3 101 20 10.0-154 17.9 35
cis-1,3-Dichloropropene 3.27 ND 2.36 2.67 72.3 81.7 20 10.0-151 12.2 37
trans-1,3-Dichloropropene 3.27 ND 2.79 3.36 85.5 103 20 10.0-148 18.5 37
2,2-Dichloropropane 3.27 ND 2.61 3.57 80.0 109 20 10.0-138 31.0 36
Di-isopropyl ether 3.27 ND 2.49 2.95 76.2 90.2 20 10.0-147 16.9 36
Ethylbenzene 3.27 ND 2.52 3.20 75.6 96.4 20 10.0-160 23.8 38
Hexachloro-1,3-butadiene 3.27 ND 2.79 3.88 85.5 119 20 10.0-160 32.5 40
Isopropylbenzene 3.27 ND 2.65 3.49 79.2 105 20 10.0-155 27.1 38
p-Isopropyltoluene 3.27 ND 2.46 3.46 75.3 106 20 10.0-160 33.8 40
2-Butanone (MEK)16.4 ND 15.2 16.8 92.4 103 20 10.0-160 10.4 40
Methylene Chloride 3.27 ND 2.04 2.57 62.6 78.7 20 10.0-141 22.9 37
4-Methyl-2-pentanone (MIBK)16.4 ND 16.1 18.6 98.3 114 20 10.0-160 14.4 35
Methyl tert-butyl ether 3.27 ND 2.81 3.35 86.0 103 20 11.0-147 17.6 35
Naphthalene 3.27 0.500 2.67 3.35 66.4 87.2 20 10.0-160 22.6 36
n-Propylbenzene 3.27 ND 2.18 3.04 65.5 91.9 20 10.0-158 33.0 38
Styrene 3.27 ND 2.61 3.41 80.0 104 20 10.0-160 26.3 40
1,1,1,2-Tetrachloroethane 3.27 ND 3.13 3.95 95.7 121 20 10.0-149 23.2 39
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110246
Volatile Organic Compounds (GC/MS) by Method 8260D L1642492-01
L1641201-17 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1641201-17 08/09/23 04:36 • (MS) R3960913-4 08/09/23 05:15 • (MSD) R3960913-5 08/09/23 05:35
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,2,2-Tetrachloroethane 3.27 ND 3.16 3.56 96.6 109 20 10.0-160 12.0 35
1,1,2-Trichlorotrifluoroethane 3.27 ND 2.08 2.85 63.8 87.2 20 10.0-160 31.0 36
Tetrachloroethene 3.27 ND 2.60 3.74 79.6 114 20 10.0-156 36.0 39
Toluene 3.27 ND 2.49 3.21 73.3 95.5 20 10.0-156 25.4 38
1,2,3-Trichlorobenzene 3.27 ND 2.42 3.29 74.0 101 20 10.0-160 30.7 40
1,2,4-Trichlorobenzene 3.27 ND 2.54 3.57 77.9 109 20 10.0-160 33.6 40
1,1,1-Trichloroethane 3.27 ND 2.36 3.14 72.3 96.2 20 10.0-144 28.3 35
1,1,2-Trichloroethane 3.27 ND 2.93 3.39 89.8 104 20 10.0-160 14.5 35
Trichloroethene 3.27 ND 2.28 3.04 69.8 93.2 20 10.0-156 28.7 38
Trichlorofluoromethane 3.27 ND 2.57 3.42 78.7 105 20 10.0-160 28.3 40
1,2,3-Trichloropropane 3.27 ND 2.93 3.46 89.8 106 20 10.0-156 16.5 35
1,2,4-Trimethylbenzene 3.27 0.841 2.54 3.13 52.1 70.0 20 10.0-160 20.6 36
1,2,3-Trimethylbenzene 3.27 0.247 2.28 2.95 62.2 82.6 20 10.0-160 25.5 36
1,3,5-Trimethylbenzene 3.27 0.282 2.31 3.04 62.0 84.6 20 10.0-160 27.5 38
Vinyl chloride 3.27 ND 2.64 3.57 80.9 109 20 10.0-160 30.0 37
Xylenes, Total 9.80 0.671 7.63 10.1 71.0 96.4 20 10.0-160 28.0 38
(S) Toluene-d8 112 115 75.0-131
(S) 4-Bromofluorobenzene 94.9 95.1 67.0-138
(S) 1,2-Dichloroethane-d4 101 96.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2109557
Chlorinated Acid Herbicides (GC) by Method 8151A L1642492-02
Method Blank (MB)
(MB) R3959198-1 08/10/23 04:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
2,4,5-TP (Silvex)U 0.000667 0.00200
2,4-D U 0.000667 0.00200
(S) 2,4-Dichlorophenyl Acetic
Acid 122 14.0-158
Laboratory Control Sample (LCS)
(LCS) R3959198-2 08/10/23 04:51
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
2,4,5-TP (Silvex)0.0500 0.0530 106 50.0-125 E
2,4-D 0.0500 0.0519 104 50.0-120 E
(S) 2,4-Dichlorophenyl Acetic
Acid 122 14.0-158
L1641368-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1641368-02 08/10/23 07:38 • (MS) R3959198-3 08/10/23 07:49 • (MSD) R3959198-4 08/10/23 08:00
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
2,4,5-TP (Silvex)0.0500 ND 0.0552 0.0511 110 102 1 50.0-125 E E 7.71 20
2,4-D 0.0500 ND 0.0525 0.0486 105 97.2 1 50.0-120 E 7.72 20
(S) 2,4-Dichlorophenyl Acetic
Acid 132 126 14.0-158
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2109521
Pesticides (GC) by Method 8081B L1642492-02
Method Blank (MB)
(MB) R3958404-1 08/08/23 15:15
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Chlordane U 0.00167 0.00500
Endrin U 0.00167 0.00500
Heptachlor U 0.00167 0.00500
Lindane U 0.00167 0.00500
Methoxychlor U 0.00167 0.00500
Toxaphene U 0.00333 0.0100
(S) Decachlorobiphenyl 83.5 10.0-128
(S) Tetrachloro-m-xylene 86.8 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3958404-2 08/08/23 15:25
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Endrin 0.0100 0.00969 96.9 57.0-134
Heptachlor 0.0100 0.00947 94.7 27.0-132
Lindane 0.0100 0.00911 91.1 55.0-129
Methoxychlor 0.0100 0.00992 99.2 54.0-155
(S) Decachlorobiphenyl 84.7 10.0-128
(S) Tetrachloro-m-xylene 78.2 10.0-127
L1639522-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1639522-04 08/08/23 15:34 • (MS) R3958404-3 08/08/23 15:44 • (MSD) R3958404-4 08/08/23 15:53
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Endrin 0.0100 ND ND 0.00537 37.0 53.7 1 10.0-160 36.8 39
Heptachlor 0.0100 ND ND ND 30.5 41.0 1 16.0-136 P 29.4 40
Lindane 0.0100 ND 0.00587 0.00701 58.7 70.1 1 14.0-141 17.7 40
Methoxychlor 0.0100 ND ND ND 28.3 45.0 1 10.0-160 J3 45.6 34
(S) Decachlorobiphenyl 10.4 21.5 10.0-128
(S) Tetrachloro-m-xylene 32.8 46.2 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110330
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1642492-02
Method Blank (MB)
(MB) R3958826-2 08/09/23 23:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
1,4-Dichlorobenzene U 0.0333 0.100
2,4-Dinitrotoluene U 0.0333 0.100
Hexachlorobenzene U 0.0333 0.100
Hexachloro-1,3-butadiene U 0.0333 0.100
Hexachloroethane U 0.0333 0.100
Nitrobenzene U 0.0333 0.100
Pyridine U 0.0333 0.100
3&4-Methyl Phenol U 0.0333 0.100
2-Methylphenol U 0.0333 0.100
Pentachlorophenol U 0.0333 0.100
2,4,5-Trichlorophenol U 0.0333 0.100
2,4,6-Trichlorophenol U 0.0333 0.100
(S) 2-Fluorophenol 26.6 10.0-120
(S) Phenol-d5 15.7 10.0-120
(S) Nitrobenzene-d5 58.1 10.0-127
(S) 2-Fluorobiphenyl 62.3 10.0-130
(S) 2,4,6-Tribromophenol 53.0 10.0-155
(S) p-Terphenyl-d14 71.6 10.0-128
Laboratory Control Sample (LCS)
(LCS) R3958826-1 08/09/23 22:46
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
1,4-Dichlorobenzene 0.500 0.347 69.4 18.0-120
2,4-Dinitrotoluene 0.500 0.487 97.4 49.0-124
Hexachlorobenzene 0.500 0.397 79.4 44.0-120
Hexachloro-1,3-butadiene 0.500 0.369 73.8 19.0-120
Hexachloroethane 0.500 0.347 69.4 15.0-120
Nitrobenzene 0.500 0.355 71.0 27.0-120
Pyridine 0.500 0.119 23.8 10.0-120
3&4-Methyl Phenol 0.500 0.294 58.8 31.0-120
2-Methylphenol 0.500 0.289 57.8 28.0-120
Pentachlorophenol 0.500 0.406 81.2 23.0-120
2,4,5-Trichlorophenol 0.500 0.463 92.6 44.0-120
2,4,6-Trichlorophenol 0.500 0.446 89.2 42.0-120
(S) 2-Fluorophenol 37.7 10.0-120
(S) Phenol-d5 26.9 10.0-120
(S) Nitrobenzene-d5 74.7 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110330
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1642492-02
Laboratory Control Sample (LCS)
(LCS) R3958826-1 08/09/23 22:46
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
(S) 2-Fluorobiphenyl 78.0 10.0-130
(S) 2,4,6-Tribromophenol 83.5 10.0-155
(S) p-Terphenyl-d14 91.5 10.0-128
L1641733-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1641733-07 08/10/23 00:12 • (MS) R3958826-3 08/10/23 00:33 • (MSD) R3958826-4 08/10/23 00:55
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
1,4-Dichlorobenzene 0.500 ND 0.215 0.240 43.0 48.0 1 17.0-120 11.0 40
2,4-Dinitrotoluene 0.500 ND 0.315 0.349 63.0 69.8 1 39.0-125 10.2 25
Hexachlorobenzene 0.500 ND 0.255 0.271 51.0 54.2 1 35.0-122 6.08 24
Hexachloro-1,3-butadiene 0.500 ND 0.244 0.252 48.8 50.4 1 12.0-120 3.23 34
Hexachloroethane 0.500 ND 0.217 0.241 43.4 48.2 1 10.0-120 10.5 40
Nitrobenzene 0.500 ND 0.236 0.258 47.2 51.6 1 12.0-120 8.91 30
Pyridine 0.500 ND ND ND 12.8 12.4 1 10.0-120 3.17 37
3&4-Methyl Phenol 0.500 ND 0.182 0.185 36.4 37.0 1 10.0-120 1.63 36
2-Methylphenol 0.500 ND 0.181 0.183 36.2 36.6 1 10.0-120 1.10 30
Pentachlorophenol 0.500 ND 0.268 0.281 53.6 56.2 1 10.0-128 4.74 37
2,4,5-Trichlorophenol 0.500 ND 0.296 0.314 59.2 62.8 1 33.0-120 5.90 31
2,4,6-Trichlorophenol 0.500 ND 0.289 0.304 57.8 60.8 1 26.0-120 5.06 31
(S) 2-Fluorophenol 25.1 25.9 10.0-120
(S) Phenol-d5 15.3 16.5 10.0-120
(S) Nitrobenzene-d5 45.1 49.9 10.0-127
(S) 2-Fluorobiphenyl 51.3 53.4 10.0-130
(S) 2,4,6-Tribromophenol 53.0 57.0 10.0-155
(S) p-Terphenyl-d14 56.6 63.5 10.0-128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110345
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1642492-01
Method Blank (MB)
(MB) R3959596-2 08/10/23 01:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-Oxybis(1-Chloropropane)U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110345
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1642492-01
Method Blank (MB)
(MB) R3959596-2 08/10/23 01:02
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) 2-Fluorophenol 54.2 12.0-120
(S) Phenol-d5 54.5 10.0-120
(S) Nitrobenzene-d5 55.9 10.0-122
(S) 2-Fluorobiphenyl 40.8 15.0-120
(S) 2,4,6-Tribromophenol 39.6 10.0-127
(S) p-Terphenyl-d14 52.6 10.0-120
Laboratory Control Sample (LCS)
(LCS) R3959596-1 08/10/23 00:41
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.314 47.1 38.0-120
Acenaphthylene 0.666 0.285 42.8 40.0-120
Anthracene 0.666 0.332 49.8 42.0-120
Benzidine 1.33 0.229 17.2 10.0-120
Benzo(a)anthracene 0.666 0.357 53.6 44.0-120
Benzo(b)fluoranthene 0.666 0.346 52.0 43.0-120
Benzo(k)fluoranthene 0.666 0.346 52.0 44.0-120
Benzo(g,h,i)perylene 0.666 0.321 48.2 43.0-120
Benzo(a)pyrene 0.666 0.368 55.3 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.299 44.9 20.0-120
Bis(2-chloroethyl)ether 0.666 0.355 53.3 16.0-120
2,2-Oxybis(1-Chloropropane)0.666 0.309 46.4 23.0-120
4-Bromophenyl-phenylether 0.666 0.297 44.6 40.0-120
2-Chloronaphthalene 0.666 0.282 42.3 35.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110345
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1642492-01
Laboratory Control Sample (LCS)
(LCS) R3959596-1 08/10/23 00:41
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.285 42.8 40.0-120
Chrysene 0.666 0.343 51.5 43.0-120
Dibenz(a,h)anthracene 0.666 0.300 45.0 44.0-120
3,3-Dichlorobenzidine 1.33 0.575 43.2 28.0-120
2,4-Dinitrotoluene 0.666 0.366 55.0 45.0-120
2,6-Dinitrotoluene 0.666 0.321 48.2 42.0-120
Fluoranthene 0.666 0.336 50.5 44.0-120
Fluorene 0.666 0.300 45.0 41.0-120
Hexachlorobenzene 0.666 0.267 40.1 39.0-120
Hexachloro-1,3-butadiene 0.666 0.218 32.7 15.0-120
Hexachlorocyclopentadiene 0.666 0.177 26.6 15.0-120
Hexachloroethane 0.666 0.307 46.1 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.290 43.5 45.0-120 J4
Isophorone 0.666 0.298 44.7 23.0-120
Naphthalene 0.666 0.249 37.4 18.0-120
Nitrobenzene 0.666 0.328 49.2 17.0-120
n-Nitrosodimethylamine 0.666 0.478 71.8 10.0-125
n-Nitrosodiphenylamine 0.666 0.324 48.6 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.380 57.1 26.0-120
Phenanthrene 0.666 0.329 49.4 42.0-120
Benzylbutyl phthalate 0.666 0.362 54.4 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.374 56.2 41.0-120
Di-n-butyl phthalate 0.666 0.350 52.6 43.0-120
Diethyl phthalate 0.666 0.309 46.4 43.0-120
Dimethyl phthalate 0.666 0.312 46.8 43.0-120
Di-n-octyl phthalate 0.666 0.343 51.5 40.0-120
Pyrene 0.666 0.345 51.8 41.0-120
1,2,4-Trichlorobenzene 0.666 0.224 33.6 17.0-120
4-Chloro-3-methylphenol 0.666 0.271 40.7 28.0-120
2-Chlorophenol 0.666 0.303 45.5 28.0-120
2,4-Dichlorophenol 0.666 0.248 37.2 25.0-120
2,4-Dimethylphenol 0.666 0.320 48.0 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.372 55.9 16.0-120
2,4-Dinitrophenol 0.666 0.255 38.3 10.0-120
2-Nitrophenol 0.666 0.282 42.3 20.0-120
4-Nitrophenol 0.666 0.304 45.6 27.0-120
Pentachlorophenol 0.666 0.276 41.4 29.0-120
Phenol 0.666 0.365 54.8 28.0-120
2,4,6-Trichlorophenol 0.666 0.257 38.6 37.0-120
(S) 2-Fluorophenol 52.9 12.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110345
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1642492-01
Laboratory Control Sample (LCS)
(LCS) R3959596-1 08/10/23 00:41
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) Phenol-d5 53.0 10.0-120
(S) Nitrobenzene-d5 46.5 10.0-122
(S) 2-Fluorobiphenyl 40.2 15.0-120
(S) 2,4,6-Tribromophenol 44.3 10.0-127
(S) p-Terphenyl-d14 47.7 10.0-120
L1642776-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1642776-10 08/10/23 02:24 • (MS) R3959596-3 08/10/23 02:44 • (MSD) R3959596-4 08/10/23 03:04
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.697 ND 0.302 0.343 43.3 49.8 1 18.0-120 12.8 32
Acenaphthylene 0.697 ND 0.270 0.315 38.8 45.8 1 25.0-120 15.2 32
Anthracene 0.697 ND 0.323 0.385 46.4 56.0 1 22.0-120 17.4 29
Benzidine 1.40 ND ND ND 22.2 22.1 1 10.0-120 2.11 40
Benzo(a)anthracene 0.697 ND 0.334 0.387 48.0 56.3 1 25.0-120 14.7 29
Benzo(b)fluoranthene 0.697 ND 0.309 0.370 44.4 53.8 1 19.0-122 17.8 31
Benzo(k)fluoranthene 0.697 ND 0.308 0.373 44.3 54.2 1 23.0-120 19.0 30
Benzo(g,h,i)perylene 0.697 ND 0.286 0.343 41.0 49.8 1 10.0-120 18.2 33
Benzo(a)pyrene 0.697 ND 0.334 0.398 48.0 57.9 1 24.0-120 17.4 30
Bis(2-chlorethoxy)methane 0.697 ND ND ND 40.2 47.0 1 10.0-120 14.3 34
Bis(2-chloroethyl)ether 0.697 ND ND 0.405 47.4 58.8 1 10.0-120 20.3 40
2,2-Oxybis(1-Chloropropane)0.697 ND ND ND 40.5 50.8 1 10.0-120 21.2 40
4-Bromophenyl-phenylether 0.697 ND ND ND 40.2 50.0 1 27.0-120 20.5 30
2-Chloronaphthalene 0.697 ND 0.268 0.312 38.5 45.3 1 20.0-120 14.9 32
4-Chlorophenyl-phenylether 0.697 ND ND ND 38.0 46.2 1 24.0-120 18.2 29
Chrysene 0.697 ND 0.330 0.376 47.4 54.7 1 21.0-120 13.2 29
Dibenz(a,h)anthracene 0.697 ND 0.282 0.328 40.5 47.6 1 10.0-120 14.9 32
3,3-Dichlorobenzidine 1.40 ND 0.569 0.650 40.8 47.3 1 10.0-120 13.3 34
2,4-Dinitrotoluene 0.697 ND ND 0.412 50.2 59.9 1 30.0-120 16.5 31
2,6-Dinitrotoluene 0.697 ND ND 0.362 44.7 52.7 1 25.0-120 15.1 31
Fluoranthene 0.697 ND 0.326 0.396 46.7 57.5 1 18.0-126 19.5 32
Fluorene 0.697 ND 0.285 0.339 40.8 49.2 1 25.0-120 17.4 30
Hexachlorobenzene 0.697 ND ND ND 36.0 44.0 1 27.0-120 18.8 28
Hexachloro-1,3-butadiene 0.697 ND ND ND 29.0 34.4 1 10.0-120 15.8 38
Hexachlorocyclopentadiene 0.697 ND ND ND 19.3 24.5 1 10.0-120 22.9 40
Hexachloroethane 0.697 ND ND ND 40.7 50.2 1 10.0-120 19.6 40
Indeno(1,2,3-cd)pyrene 0.697 ND 0.272 0.318 39.0 46.2 1 10.0-120 15.8 32
Isophorone 0.697 ND ND ND 41.8 47.3 1 13.0-120 11.2 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG2110345
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1642492-01
L1642776-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1642776-10 08/10/23 02:24 • (MS) R3959596-3 08/10/23 02:44 • (MSD) R3959596-4 08/10/23 03:04
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.697 ND 0.236 0.272 33.9 39.5 1 10.0-120 14.1 35
Nitrobenzene 0.697 ND ND ND 43.0 51.7 1 10.0-120 17.2 36
n-Nitrosodimethylamine 0.697 ND 0.444 0.518 63.7 75.3 1 10.0-127 15.5 40
n-Nitrosodiphenylamine 0.697 ND ND 0.364 44.9 52.8 1 17.0-120 15.0 29
n-Nitrosodi-n-propylamine 0.697 ND ND 0.433 50.6 62.9 1 10.0-120 20.4 37
Phenanthrene 0.697 ND 0.312 0.373 44.7 54.2 1 17.0-120 18.0 31
Benzylbutyl phthalate 0.697 ND ND 0.409 49.8 59.4 1 23.0-120 16.3 30
Bis(2-ethylhexyl)phthalate 0.697 ND 0.360 0.414 51.7 60.2 1 17.0-126 14.0 30
Di-n-butyl phthalate 0.697 ND ND 0.410 48.0 59.6 1 30.0-120 20.3 29
Diethyl phthalate 0.697 ND ND ND 42.9 48.7 1 26.0-120 11.6 28
Dimethyl phthalate 0.697 ND ND ND 43.6 50.9 1 25.0-120 14.2 29
Di-n-octyl phthalate 0.697 ND ND 0.389 47.2 56.6 1 21.0-123 16.9 29
Pyrene 0.697 ND 0.333 0.386 47.8 56.1 1 16.0-121 14.7 32
1,2,4-Trichlorobenzene 0.697 ND ND ND 29.8 35.1 1 12.0-120 14.9 37
4-Chloro-3-methylphenol 0.697 ND ND ND 37.9 43.6 1 15.0-120 12.7 30
2-Chlorophenol 0.697 ND ND ND 40.2 49.2 1 15.0-120 18.9 37
2,4-Dichlorophenol 0.697 ND ND ND 34.0 38.4 1 20.0-120 10.8 31
2,4-Dimethylphenol 0.697 ND ND ND 42.2 47.3 1 10.0-120 10.1 33
4,6-Dinitro-2-methylphenol 0.697 ND 0.373 0.467 53.6 67.9 1 10.0-120 22.4 39
2,4-Dinitrophenol 0.697 ND ND 0.415 48.3 60.4 1 10.0-121 21.0 40
2-Nitrophenol 0.697 ND ND ND 38.7 44.2 1 12.0-120 12.1 39
4-Nitrophenol 0.697 ND ND 0.367 45.3 53.3 1 10.0-137 14.9 32
Pentachlorophenol 0.697 ND ND ND 39.8 48.7 1 10.0-160 19.1 31
Phenol 0.697 ND ND 0.399 48.4 58.0 1 12.0-120 16.7 38
2,4,6-Trichlorophenol 0.697 ND ND ND 36.2 41.8 1 19.0-120 13.2 32
(S) 2-Fluorophenol 46.1 55.3 12.0-120
(S) Phenol-d5 49.2 58.2 10.0-120
(S) Nitrobenzene-d5 42.2 48.4 10.0-122
(S) 2-Fluorobiphenyl 36.6 43.1 15.0-120
(S) 2,4,6-Tribromophenol 40.1 46.2 10.0-127
(S) p-Terphenyl-d14 42.2 49.7 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
P RPD between the primary and confirmatory analysis exceeded 40%.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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