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HomeMy WebLinkAboutMO-29997_49079_C_O_20230620
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Limited Phase II Subsurface
Investigation Report
REPORT DATE: June 20, 2023
SITE INFORMATION
Sunbelt Rentals - Statesville, NC
625 Sullivan Road
PROJECT INFORMATION AEI Project No. 479067
Development, LLC, its successors,
70 East Long Lake Road
Bloomfield Hills, Michigan 48304
PREPARED BY
4255 Wade Green Rd, Suite 510
Kennesaw, Georgia 30144
(678) 279-2820
AEI Consultants, North Carolina, PLLC
4255 Wade Green Rd, Suite 510
Kennesaw, Georgia 30144
June 20, 2023
Drew Fogel
Agree Limited Partnership, Agree Development, LLC, its successors, assigns and mortgagees
70 East Long Lake Road
Bloomfield Hills, Michigan 48304
Subject: Limited Phase II Subsurface Investigation
Sunbelt Rentals - Statesville, NC
625 Sullivan Road
Statesville, North Carolina 28677
AEI Project No. 479067
Dear Mr. Fogel,
This report presents the results of the Limited Phase II Subsurface Investigation (Phase II) performed by
AEI Consultants-North Carolina, PLLC (AEI-NC, PLLC; AEI) at 625 Sullivan Road, Statesville, North Carolina
(“the Site”). This investigation was completed to assess the recognized environmental condition (REC)
identified in the Phase I Environmental Site Assessment (ESA) report prepared by Hart & Hickman PC,
dated June 16, 2022. The investigation was in general accordance with the scope of services outlined in our proposal dated May 17, 2023 (AEI Proposal Number 90812), which was authorized on the same day.
Information regarding the site description, background, scope of work, findings, conclusions, and
recommendations are provided in the following sections.
Sincerely,
David Witt
Executive Vice President AEI Consultants-North Carolina, PLLC
(214) 393-5810
dwitt@aeiconsultants.com
AEI Consultants-NC PLLC
Project No.479067
June 20, 2023 Page 3
TABLE OF CONTENTS
1.0 SITE DESCRIPTION ............................................................................................... 4
2.0 BACKGROUND ..................................................................................................... 5
3.0 INVESTIGATION EFFORTS ....................................................................................... 6
3.1 Health and Safety Plan ........................................................................................... 6 3.2 Permitting and Utility Clearance ............................................................................... 6
3.3 Geophysical Survey ............................................................................................... 6
3.4 Drilling and Soil Sample Collection ............................................................................. 7
3.4.1 Soil Sample Collection ............................................................................... 7
3.4.2 Headspace Testing and Field Screening........................................................... 8 3.5 Groundwater Sample Collection ................................................................................ 8
3.6 Boring Destruction ................................................................................................ 8
3.7 Decontamination Procedures and Investigation-Derived Waste ............................................ 8
3.8 Laboratory Analysis ............................................................................................... 9
4.0 FINDINGS ..........................................................................................................10
4.1 Subsurface Conditions and Field Screening ................................................................... 10
4.2 Analytical Results ................................................................................................ 10
4.2.1 Soil Sample Analytical Results ......................................................................... 10 4.2.2 Groundwater Sample Analytical Results ......................................................... 11
5.0 SUMMARY AND CONCLUSIONS .................................................................................12
6.0 REFERENCES .....................................................................................................13
7.0 REPORT LIMITATIONS AND RELIANCE ........................................................................14
8.0 SIGNATURES .....................................................................................................15
FIGURES
Figure 1 Site Detail Map
TABLES
Table 1 Soil Sample Data Summary
Table 2 Groundwater Sample Data Summary
Table 3 TCLP Sample Data Summary
APPENDICES
Appendix A Geophysical Survey Report
Appendix B Boring Logs
Appendix C Laboratory Analytical Report
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067 June 20, 2023
Page 4
1.0 SITE DESCRIPTION
The Site is located on the west side of Sullivan Road and east side of Brookdale Drive (with no
vehicular access to Brookdale Drive) in Statesville, North Carolina. The Site consists of
approximately 1.93 acres of land that is improved with one single-story building which totals
10,688 square feet. The Site is occupied by Sunbelt Rentals and utilized for equipment and tool rentals. The remaining of the Site consists of asphalt-paved parking areas and associated
landscaping. The Site currently receives drinking water from the City of Statesville and no water
supply wells are located at the Site. The location of the Site is shown on Figure 1.
The ground surface at the Site and nearby properties consists of rolling hills, with a topographic
gradient toward the northwest and is situated at an elevation approximately 800 feet above
mean sea level. According to the information obtained from a subsurface investigation on a
nearby property obtained from the North Carolina Department of Environmental Quality,
groundwater was expected to be encountered from a depth of approximately nine to 12 feet
below ground surface (bgs) and groundwater flow direction beneath the Site is inferred to
follow the topographic gradient, and flow to the northwest.
Refer to Section 4.1 below for additional information on the Site subsurface conditions.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 5
2.0 BACKGROUND
According to the June 16, 2022 Phase I ESA report, the following REC was identified:
• The Site was utilized for automotive repair purposes from approximately 1973 until
2021. During Site reconnaissance, H&H observed evidence of four in-ground hydraulic
lifts and two floor drains within the former automotive service garage. Additionally, H&H observed at least one concrete patch in the former automotive service garage that
may be indicative of a previously removed in-ground lift. Additional inground lifts and
floor drains may be present within the facility that were not able to be observed due to
the presence of stored materials within the former service garage. The existing Site
owner indicated that the lifts have not been used since her purchase of the Site in 2016.
H&H was unable to obtain inspection/maintenance records pertaining to the lifts, and
there is no documentation of prior environmental assessment conducted in the vicinity
of the lifts or floor drains. The Site contact indicated that the floor drains are connected
to the municipal sanitary sewer system and was not aware of an oil/water separator (OWS) located at the Site. However, it is possible that an OWS was historically utilized
at the Site by a prior owner. H&H considers historical automotive repair operations
conducted at the Site and the associated in-ground hydraulic lifts, floor drains, and
potential OWS to be a REC.
AEI NC was also provided with an invoice from Omega Construction for the pumping out of eight
hydraulic lift tanks from the Site in February 2023. During this investigation, AEI NC was notified
by the Site owner that the eight lifts were recently pumped out and filled with gravel and the
floor surface had been completed with new concrete patches; however, AEI was not provided with a report which documented these activities.
According to the EDR Geocheck report included in the Phase I ESA, no public water supply
systems or wells on the state database are located within one mile of the Site. One USGS well
is listed on the federal well database to the east, approximately 750 feet and up gradient from
the Site.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 6
3.0 INVESTIGATION EFFORTS
AEI was contracted to perform a Limited Phase II Subsurface Investigation in order to evaluate
if the subsurface at the Site has been adversely impacted by REC in the June 16, 2022 Phase I
ESA report referenced above. Investigation efforts included the advancement of 12 exploratory
soil borings, and two temporary monitoring wells at the Site to collect soil and groundwater
samples.
The boring locations are shown on Figure 1. The completed Site activities are summarized
below.
3.1 Health and Safety Plan
A site-specific health and safety plan was prepared, reviewed by on-site personnel, and kept
on the Site for the duration of the fieldwork.
3.2 Permitting and Utility Clearance
Drilling permits were not required for this investigation.
The public underground utility locator North Carolina 811 was notified who, in turn, notified
subscribing utility companies of the planned investigation work for underground utility locations
to be marked along the ground surface around the Site boundaries and proposed boring
locations, where accessible. Private utility locating was conducted by Integrated Scanning
Solutions (ISS) of Huntersville, North Carolina under subcontract to AEI to further identify and
locate underground utilities on the Site, and to shift boring locations, as appropriate.
3.3 Geophysical Survey
On May 30, 2023, in addition to the utility locating activities, a geophysical survey was
conducted by ISS. The geophysical survey was conducted in the interior and immediate exterior
areas of the Site. The purpose of the survey was to evaluate the potential presence of
underground structures, underground storage tanks (USTs), oil/water separators, associated
piping, disturbed soils, and/or cavities at the Site. The geophysical survey was conducted using ground-penetrating radar (GPR), magnetometer, and other utility locating equipment.
The geophysical survey identified a possible former oil/water separator in the southwest
portion of the building which the Site owner indicated was previously abandoned. The survey
also identified an area of disturbed soil at the southwest exterior corner of the building which
likely is associated with the removed UST. The UST received regulatory closure and was not
further assessed during this investigation. The geophysical survey report is included in Appendix
A.
The Client should be aware of the inherent limitations of geophysical surveying methods and
that above and underground utilities and other man-made or natural features (i.e. automobiles,
debris piles, tree roots, reinforced concrete, certain soil conditions, etc.), if in the area of the
survey, may decrease the effectiveness of the survey. The Client should be aware that the lack
of a detection of a feature from a geophysical survey does not mean that the feature does not
exist only that it was not detected.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 7
3.4 Drilling and Soil Sample Collection
On May 30, 2023, 12 exploratory soil borings (AB-1 through AB-12) were advanced at the Site at
the locations shown on Figure 1. The borings were advanced by Mid South Environmental of
Gold Hill, North Carolina using a direct push (DP) tractor-mounted drill rig to collect soil and groundwater samples. The locations of the borings are listed below:
• Borings AB-1, AB-2, AB-4, and AB-6 through AB-9 were advanced to the total depths of
15 feet bgs with the DP drilling method throughout the interior of the building near the
former hydraulic lifts. Boring AB-1 was also advanced near the abandoned oil/water
separator.
• Boring AB-3 was advanced to a total depth of 20 feet bgs with the DP drilling method adjacent to a former hydraulic lift.
• Boring AB-5 was advanced to a total depth of 18 feet bgs in a downgradient location on
the north exterior of the on-site building with the DP drilling method.
• Borings AB-10 and AB-11 were advanced to the total depths of five feet bgs with the DP
drilling method near the former floor drains.
• Boring AB-12 was advanced to a total depth of 7.5 feet bgs with a hand auger in the
western undeveloped area of the Site to collect background soil samples.
The locations of the borings were chosen in part based on existing and former Site structures,
results of the utility clearance, and anticipated groundwater flow direction.
3.4.1 Soil Sample Collection
The soil borings were evaluated throughout their entire depths for the purposes of lithologic
logging, field screening (headspace testing), and laboratory analyses. The soil samples from
borings were obtained using a single-walled coring system with approximately 2.25 inches and 4 feet in length containing plastic liners. The coring system was connected to 1-inch diameter,
flush-jointed drill rod that was hydraulically driven (pushed) by the rig to each target sample
depth. Upon retrieval from each sample depth interval, the coring system was opened, and the
liners were removed and cut for visual inspection and lithologic logging purposes. Recovered
soil samples were examined for soil classification and described on detailed boring log in
general conformance with the Unified Soil Classification System. The boring logs are presented
in Appendix B.
Select soil samples were collected from the plastic liners or plastic baggies and placed into
clean laboratory-supplied jars. A measured amount of the selected sample was placed into
laboratory provided bottle ware for the intended analyses. After sealing, each sample was
labeled with the project name, project number, boring number, sample depth, and sampling
date/time of sampling, and each sample was entered onto chain-of-custody documentation for
transportation to a State of Texas-certified laboratory for analysis, and was placed into an
insulated, chilled ice chest containing ice.
Samples from the borings near the hydraulic lifts were collected from eight to nine feet bgs, with the exception of boring AB-4 in which the sample was collected from six to seven feet bgs,
the interval with the highest PID reading. A sample was also collected from boring AB-1 at 12
to 13 feet bgs to assess impacts from the former oil/water separator. Samples from borings AB-
10, AB-11, and AB-12 were collected from four to five feet bgs.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 8
The chain-of-custody documentation and analytical laboratory report is included in Appendix
C.
3.4.2 Headspace Testing and Field Screening
Headspace screening was performed with a PID equipped with an electrodeless 10.6 eV ultraviolet lamp or equivalent for detecting the presence of organic vapors in the soil samples
collected. The PID was calibrated by the rental company before use. To initiate the headspace
testing procedure, soil samples were placed into labeled, plastic bags, and sealed prior to
conducting the tests.
After approximately 20-30 minutes had elapsed for organic vapor build-up inside the bags, each
bag was punctured with the probe tip of the PID to allow for measurement of the organic vapors
or headspace gases. Measurements of the organic vapors were reported in parts per million
(ppm). The resulting PID measurements were then recorded in the boring logs that are
presented in Appendix B.
3.5 Groundwater Sample Collection
On May 30, 2023, after reaching the maximum depth of 20 feet bgs in boring AB-3 and 18 feet
bgs in boring AB-5, a temporary groundwater monitoring well was installed in each of the boring
locations to facilitate collection of a groundwater sample. The temporary well materials
consisted of one-inch diameter polyvinyl chloride 0.010-slotted screen that was installed into
the borehole to facilitate groundwater infiltration and groundwater sample collection from the
borings. The temporary well materials remained in-place for at least 30 minutes to allow for
groundwater infiltration for sample collection. During this timeframe, sufficient amount of groundwater did infiltrate in each of the temporary wells to allow for groundwater sample
collection.
Prior to the collection of groundwater sample from borings AB-3 and AB-5, due to low flow
conditions, AEI was not able to purge the wells prior to sample collection. The groundwater
samples were collected utilizing a peristaltic pump with dedicated tubing. Groundwater
samples were collected in laboratory-supplied bottles. The collected sample containers were
sealed, labeled with a unique identifier, and placed in an ice chilled cooler. Chain-of-custody
documentation was prepared and accompanied the groundwater sample to the analytical
laboratory, a copy of which is included in Appendix C.
3.6 Boring Destruction
Following completion of field activities, removal of well/probe construction material, and
tooling, the boring locations were backfilled with borehole drilling cuttings and hydrated
bentonite chips and completed at the surface to match the surrounding conditions.
3.7 Decontamination Procedures and Investigation-Derived Waste
AEI personnel wore disposable Nitrile gloves during sample collection and changed gloves prior
to and between each sample collection. Down-hole equipment including sampling tubes,
samplers, and hand tools were decontaminated prior to drilling each boring and/or were
dedicated to a single boring.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 9
No investigation-derived waste requiring disposal or characterization was generated during the
field activities.
3.8 Laboratory Analysis
Soil and groundwater samples were labeled and placed into coolers with ice following sampling
and transferred under appropriate chain-of-custody documentation to Analytical Environmental
Services, Inc. of Atlanta, Georgia.
The following is a summary of the soil analyses performed:
• Samples AB-1:8-9, AB-2:8-9, AB-3:8-9, AB-4:6-7, AB-6:8-9, AB-7:8-9, AB-8:8-9, and AB-
9:8-9 were analyzed for total petroleum hydrocarbons diesel range organics (TPH-DRO)
by US EPA Testing Method 8015C and polychlorinated biphenyls (PCBs) by US EPA Testing
Method 8081.
• Samples AB-1:12-13, AB-10:4-5, and AB-11:4-5 were analyzed for volatile organic
compounds (VOCs) by US EPA Testing Method 8260B, polycyclic aromatic hydrocarbons (PAHs) by US EPA Testing Method 8270 and lead and chromium by US EPA Testing Method
6020.
• Sample AB-12:4-5 was analyzed for lead and chromium using the same method as above.
The following is a summary of the groundwater analyses performed:
• Samples AB-3 and AB-5 were analyzed for VOCs and PAHs using the same methods as
above.
Due to elevated concentrations of TPH-DRO above the NCDEQ Action Level in samples AB-1:8-9
and AB-4:6-7, additional analysis was completed for polycyclic aromatic hydrocarbons (PAHs) on these two soil samples.
Based on elevated concentrations of certain PAHs in soil samples AB-1:8-9, AB-1:12-13, and AB-
4:6-7, these samples were also analyzed using the Toxic Characteristic Leaching Procedure
(TCLP) for the compounds 1-Methylnaphthalene, 2-methylnaphthalene, and naphthalene.
Sample AB-1:12-13 was also analyzed for TCLP VOCs for the compounds 1,4-Dichlorobenzene,
chlorobenzene, and Benzene.
No further sample analyses were conducted as part of this investigation. Chain-of-custody
documentations and the certified analytical reports are provided in Appendix C.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 10
4.0 FINDINGS
The findings of this investigation are summarized below.
4.1 Subsurface Conditions and Field Screening
Subsurface conditions observed during the drilling activities of borings AB-1 through AB-12 indicated that soils underlaying the Site consisted primarily of clays and silts to a depth of 20
feet, a total depth of this investigation. DP refusal was encountered in boring AB-4 at 12 feet
bgs, AB-5 at 18 feet bgs, and AB-12 at 7.5 feet bgs. Groundwater was encountered during drilling
of borings AB-3 and AB-5 at approximately 14 to 16 feet bgs.
There was no visual or olfactory evidence (i.e., soil discoloration, odor) of potentially impacted
soils observed in soils that were recovered during drilling activities with the exception of
petroleum odors and elevated PID readings in borings AB-1 and AB-4. The maximum PID reading
was 135 ppm in boring B-4 between approximately 6 to 7 feet bgs.
4.2 Analytical Results
For the purpose of providing context to the data obtained during this Phase II investigation,
analytical results were compared to available regulatory standards and screening levels. The
NCDEQ has the responsibility for overseeing soil and groundwater cleanups which are managed
under a variety of different regulatory programs. The soil results of this investigation were
reviewed along with the Underground Storage Tank Division’s Maximum Contaminant
Concentration Levels (MSCCs) for soil-to-water and industrial/commercial sites. The soil results
were also compared to the Inactive Hazardous Site Branch’s Preliminary Soil Remediation Goals
(PSRG) for Unrestricted (Residential), Industrial/Commercial, and Protection of Groundwater for PCB results. The TPH-DRO soil results were also compared to the NCDEQ UST Section’s Action
Level for TPH-DRO. The groundwater results of this investigation were reviewed along with the
UST divisions groundwater quality standards (GWQS) and gross contaminant levels (GCLs). The
TCLP results were also compared to the GCLs.
4.2.1 Soil Sample Analytical Results
Table 1 presents a summary of the soil sample analytical results. The analytical results can be
summarized as follows:
• TPH-DRO was detected in sample AB-1:8-9 at 6,100 milligrams per kilogram (mg/kg) and in
sample AB-4:6-7 at 2,600 mg/kg. These concentrations are above the TPH-DRO Action Level
of 100 mg/kg. TPH-DRO was not detected above the laboratory method detection limits
(MDLs) in any other soil samples.
• PCBs, Aroclor 1242 and Aroclor 1254, were detected at low concentrations in sample AB-
1:8-9, below their respective PSRGs.
• Chlorobenzene, 1,4-dichlorobenzene, benzene, and 1-methylnaphthalene were detected in
sample AB-1:12-13 at concentrations which exceed their respective soil-to-water MSCCs.
but below their respective Residential and Industrial/Commercial MSCCs.
• 1-Methylnaphthalene and naphthalene were detected in sample AB-1:8-9 at concentrations
which exceed their respective soil-to-water MSCCs but below their respective Residential
and Industrial/Commercial MSCCs.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 11
• 1-Methylnaphthalene and 2-methylnaphthalene were detected in sample AB-4:6-7 at
concentrations which exceed their respective soil-to-water MSCCs but below their
respective Residential and Industrial/Commercial MSCCs.
• Naphthalene was detected in sample AB-4:6-7 at a concentration which exceeds its
respective soil-to-water MSCC but is below its residential and Industrial/Commercial MSCCs.
• No other compounds were detected were detected above their respective MSCCs.
4.2.2 Groundwater Sample Analytical Results
Table 2 presents a summary of the groundwater sample results. The analytical results can be
summarized as follows:
• Two VOCs were detected in the groundwater samples, including toluene in sample AB-3 and
chloroform in sample AB-5. Both compounds were detected at concentrations below their
respective NCDEQ GWQS and GCL values.
• One PAHs, Naphthalene, was detected in both groundwater samples, below it respective
NCDEQ GWQS and GCL values.
• No other compounds were detected in the groundwater samples above the laboratory MDLs.
4.2.3 TCLP Sample Analytical Results
Table 3 presents a summary of the TCLP sample results. The analytical results can be
summarized as follows:
• No compounds analyzed using the TCLP analysis exceeded their respective NCDEQ GCLs.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 12
5.0 SUMMARY AND CONCLUSIONS
AEI completed a Limited Phase II Subsurface Investigation at the Site to evaluate if the
subsurface at the Site has been adversely impacted by the former auto repair operations, which
included eight inground hydraulic lifts, floor drains, and oil/water separator, identified as a
REC. Investigation efforts included the advancement of 12 exploratory soil borings and two
temporary monitoring wells to collect soil and groundwater samples. The investigation results
can be summarized as follows:
• AEI noted petroleum odors and elevated PID readings in the soil samples from AB-1 and
AB-4.
• TPH-DRO was detected in sample AB-1:8-9 at 6,100 mg/kg and in sample AB-4:6-7 at
2,600 mg/kg. These concentrations are above the TPH-DRO Action Level of 100 mg/kg.
Therefore, these samples were analyzed for PAHs.
• A few VOCs and two PAHs were detected in two soil samples from AB-1 at concentrations
which exceed their respective soil-to-water MSCCs.
• A couple PAHs were detected in soil sample from AB-4 at concentrations which exceed their respective soil-to-water MSCCs.
• One PAH, naphthalene, was detected in soil sample from AB-4 at a concentration which
exceeds its respective soil-to-water MSCC.
• No compounds were detected in the groundwater samples above their respective NCDEQ
GCLs.
• N0 PCBs were detected above their respective PSRGs.
• No TCLP results for the elevated compounds above their respective NCDEQ GCLs.
In AEI’s opinion, the presence of these petroleum constituents with exceedances of NCDEQ’s
MSCCs and TPH-DRO action levels suggest that a release has occurred in the areas of borings
AB-1 and AB-4. Upon discovery of a release, the property owner is required to report this
release within 24 hours to the NCDEQ’s Underground Storage Tank Section in accordance with
non-UST petroleum releases per 15A NCAC 02L.0504(1). Based on the low level of
concentrations detected, groundwater results from the Site, results of the additional TCLP
analysis, and lack of groundwater use in the area of the Site, AEI believes this release represents
a low risk. Therefore, AEI recommends submitting the release notification to the NCDEQ UST
Division in order to request and obtain a No Further Action. Additionally, if soils are disturbed as part of future site re-development plans, then it should be appropriately managed under a
Soil Management Plan, and/or appropriately characterized if transported and disposed off-site.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067 June 20, 2023
Page 13
6.0 REFERENCES
Hart & Hickman, PC, 2022, Phase I Environmental Site Assessment, Iredell COAST Resale Shop
and Community Food Bank, 625 Sullivan Road, Statesville, North Carolina, dated June 16.
NCDEQ, 2022. North Carolina Department of Environmental Quality Preliminary Soil
Remediation Goals (PSRGs), July.
NCDEQ, 2022, 15A NCAC 02L .0202 Groundwater Standards, Effective April 1, 2022.
NCDEQ, 2016. Guidelines for North Carolina Action Limits for Total Petroleum Hydrocarbons
(TPH), July 26.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 14
7.0 REPORT LIMITATIONS AND RELIANCE
This report presents a summary of work completed by AEI Consultants-North Carolina (NC),
PLLC. The completed work includes observations and descriptions of site conditions encountered. Where appropriate, it includes analytical results for samples taken during the
course of the work. The number and location of samples are chosen to provide the requested
information, subject to scope of work for which AEI-NC, PLLC was retained and limitations
inherent in this type of work, but it cannot be assumed that they are representative of areas
not sampled. This report should not be regarded as a guarantee that no further contamination
beyond that which could have been detected within the scope of this investigation is present
beneath the Site. Undocumented, unauthorized releases of hazardous material, the remains
of which are not readily identifiable by visual inspection and are of different chemical
constituents, are difficult and often impossible to detect within the scope of a chemical specific
investigation.
Any conclusions and/or recommendations are based on these analyses and observations, and
the governing regulations. Conclusions beyond those stated and reported herein should not be
inferred from this document. These services were performed in accordance with generally
accepted practices, in the environmental engineering and construction field, which existed at
the time and location of the work. No other warranty, either expressed or implied, has been
made.
This investigation was prepared for the sole use and benefit of Agree Limited Partnership, Agree
Development, LLC, its successors, assigns and mortgagees. Both verbal and written, whether
in draft or final, are for the benefit of Agree Limited Partnership, Agree Development, LLC, its
successors, assigns and mortgagees. This report has no other purpose and may not be relied upon by any other person or entity without the written consent of AEI-NC, PLLC. Either verbally
or in writing, third parties may come into possession of this report or all or part of the
information generated as a result of this work. In the absence of a written agreement with AEI-
NC, PLLC granting such rights, no third parties shall have rights of recourse or recovery whatsoever under any course of action against AEI, its officers, employees, vendors, successors
or assigns. Reliance is provided in accordance with AEI-NC, PLLC’s Proposal and Standard Terms
& Conditions executed by Agree Realty. The limitation of liability defined in the Terms and
Conditions is the aggregate limit of AEI-NC, PLLC’s liability to the client and all relying parties.
Limited Phase II Subsurface Investigation
625 Sullivan Road, Statesville, North Carolina 28677
Project No.479067
June 20, 2023 Page 15
8.0 SIGNATURES
This document was prepared by, or under the direction of, the undersigned.
Daniel Bakos Ben Friedman
Project Geologist I Project Scientist II
Michael Meares, PG 2445
Senior Geologist I
FIGURES
LEGEND SITE MAP
FIGURE 1
Proposal No. 479067
625 Sullivan Road
Statesville, NC
Approximate Site Boundary
Soil Boring/Temp Well Location
Soil Boring Location
Approximate locations of former drains
02040
SCALE: 1” = 40’
Temporary Well Point
Monitoring Well
Soil Boring
SB-1
Proposed Soil Gas Sample Location
Hydraulic Lift
Oil/Water Separator
Floor Drain
UST
Estimated Groundwater Flow Direction
SU
L
L
I
V
AN
R
O
A
D
BR
O
O
K
D
A
L
E
D
R
I
V
E
AB-4
AB-2
AB-12
AB-11
AB-10
AB-6
AB-7
AB-8
AB-9
AB-1
AB-3
AB-5
Inferred Groundwater Flow Direction
Location of former clarifier
Location of historical UST
TABLES
Sample ID AB-1:8-9 AB-1:12-13 AB-2:8-9 AB-3:8-9 AB-4:6-7 AB-6:8-9 AB-7:8-9 AB-8:8-9 AB-9:8-9 AB-10:4-5 AB-11:4-5 AB-12:4-5 NCDEQ NCDEQ NCDEQ NCDEQ NCDEQ NCDEQ NCDEQDate5/30/2023 5/30/2023 5/30/2023 5/30/2023 5/30/2023 5/30/2023 5/30/2023 5/30/2023 5/30/2023 5/30/2023 5/30/2023 5/30/2023 Soil-to-Ind/com Protection of Soil-to-Water Residential Ind/Com TPH ActionDepth8-9 12-13 8-9 8-9 6-7 8-9 8-9 8-9 8-9 4-5 4-5 4-5 Health Health Based Groundwater MSCCs MSCCs MSCCs Action Level(feet bgs)(feet bgs)(feet bgs)(feet bgs)(feet bgs)(feet bgs)(feet bgs)(feet bgs)(feet bgs)(feet bgs)(feet bgs)(feet bgs)PSRGs PSRGs PSRGs
1,2-Dichlorobenzene mg/kg --0.08 --------------<MDL <MDL --380 200 0.39 0.23 1,400 36,000 NS1,4-Dichlorobenzene mg/kg --1.3 --------------<MDL <MDL --3 12 0.12 0.099 110 1,000 NSBenzenemg/kg --0.16 --------------<MDL <MDL --1.2 5.4 0.01 0.0056 18 164 NSToluenemg/kg --0.0058 J --------------<MDL <MDL --990 9,700 8.3 4.3 1,200 32,000 NSEthylbenzenemg/kg --0.017 --------------<MDL <MDL --6.1 2.7 13 4.9 1,560 40,000 NSAcetonemg/kg --0.040 J --------------<MDL <MDL --14,000 210,000 25 24 14,000 360,000 NSCarbon disulfide mg/kg --0.0047 J --------------<MDL <MDL --160 740 4.1 4.3 1,564 40,880 NSChlorobenzenemg/kg --29 --------------<MDL 0.0038 J --58 280 0.68 0.44 312 8,176 NSIsopropylbenzenemg/kg --0.013 --------------<MDL <MDL --410 2,100 2.3 1.7 1,564 40,880 NSMethylene Chloride mg/kg --0.0042 J --------------<MDL <MDL --58 650 0.025 0.02 85 763 NSMethylcyclohexanemg/kg --0.015 --------------<MDL <MDL --NS NS NS NS NS NS NSo-Xylene mg/kg --0.025 --------------<MDL <MDL --140 590 9.8 4.6 3,129 81,760 NSRemaining VOCs mg/kg --<MDL --------------<MDL <MDL --Various Various Various Various Various Various NS
Benzo(a)anthracene mg/kg 0.048 0.019 ----0.024 --------<MDL 0.0042 --1.1 21 0.35 0.35 0.88 8 NSBenzo(a)pyrene mg/kg 0.063 0.015 ----0.002 J --------<MDL 0.0034 --0.11 2.1 0.12 0.096 0.088 0.78 NSBenzo(b)fluoranthene mg/kg 0.095 0.02 ----0.0029 J --------<MDL 0.0054 --1.1 21 1 1.2 0.88 8 NSBenzo(g,h,i)perylene mg/kg 0.023 0.01 ----0.0024 J --------<MDL 0.0027 J --NS NS NS 6,400 469 12,264 NSBenzo(k)fluoranthene mg/kg <MDL 0.0054 ----<MDL --------<MDL 0.0021 J --11 210 12 12 9 78 NSChrysenemg/kg 0.075 0.02 ----0.049 --------<MDL 0.0029 --110 2,100 36 39 88 780 NSDibenz(a,h)anthracene mg/kg <MDL 0.0036 J ----<MDL --------<MDL 0.0023 J --0.11 2.1 0.38 0.17 0.088 0.78 NSFluoranthenemg/kg 0.18 0.057 ----<MDL --------<MDL 0.0043 --480 6,000 670 290 620 16,400 NSFluorenemg/kg 0.37 0.13 ----2 --------<MDL <MDL --480 6,000 110 47 620 16,400 NSIndeno(1,2,3-cd)pyrene mg/kg 0.016 0.0078 ----<MDL --------<MDL 0.0031 --1.1 21 3.9 3.4 0.88 8 NS1-Methylnaphthalene mg/kg 6.4 1.3 ----10 --------<MDL <MDL --18 73 0.11 0.004 20 100 NS2-Methylnaphthalene mg/kg 1.2 0.4 ----16 --------<MDL <MDL --48 600 3.1 3.6 63 1,635 NSAcenaphthenemg/kg <MDL 0.037 ----<MDL --------<MDL <MDL --720 9,000 16 8.2 940 24,000 NSAnthracenemg/kg 0.084 0.025 ----0.41 --------<MDL 0.0016 J --3,600 45,000 1,300 940 4,600 122,000 NSNaphthalenemg/kg 2 0.058 ----3.5 --------<MDL <MDL --2.1 8.8 0.39 0.16 313 8,176 NSPhenanthrenemg/kg 0.77 0.18 ----4.5 --------<MDL 0.0023 --NS NS NS 56 469 12,264 NSPyrenemg/kg 0.17 0.061 ----0.92 --------<MDL 0.0078 --360 4,500 440 270 469 12,264 NSRemaining PAHs mg/kg <MDL <MDL ----<MDL --------<MDL <MDL --Various Various Various Various Various Various NS
Aroclor 1242 mg/kg 0.014 J --<MDL <MDL <MDL <MDL <MDL <MDL <MDL ------0.23 0.95 0.055 NS NS NS NSAroclor 1254 mg/kg 0.015 J --<MDL <MDL <MDL <MDL <MDL <MDL <MDL ------0.23 0.97 0.091 NS NS NS NSAll Other PCBs mg/kg <MDL --<MDL <MDL <MDL <MDL <MDL <MDL <MDL ------Various Various Various NS NS NS NS
Chromium mg/kg --52.6 --------------59.4 67.6 93.9 23,000*350,000*360,000*4,200 23,460 613,200 NSLeadmg/kg --10.9 --------------11.7 13.3 40 400 800 270 270 400 400 NS
TPH-DRO mg/kg 6,100 --<MDL <MDL 2,600 <MDL <MDL <MDL <MDL ------NS NS NS NS NS NS 100Notes:mg/kg Milligrams per kilogram--Not analyzedft bgs Feet below ground surface<MDL Not detected above the laboratory method detection limit (MDL)PQL Practical Quantitation Limit*PSRG listed for Chromium(III), Insoluble SaltsUS EPA United States Environmental Protection AgencyNCDEQNorth Carolina Department of Environmental QualityInd/Com Industrial/CommercialPSRGsPreliminary Soil Remediation Goals, July 2022MSCCsNCDEQ Maximum Soil Contaminant Concentration LevelsNSJThe reported value is an estimate between the MDL and the PQLBold
Bold Bold blue entries indicate that the detection exceeds the Protection of Groundwater PSRGhighlighted entries indicate that a detected concentration exceeds the soil-to-water-MSCCs
TABLE 1: SOIL SAMPLE DATA SUMMARY625 Sullivan Road, Statesville, North Carolina 28677
Comparison Value(s):AEI NC Project No. 479067
Bold red entries indicate that the detected concentration exceeds the TPH Action Level
An analyte for which a Comparison Value has not been established
Total Petroleum Hydrocarbons - Diesel Range Organics (TPH-DRO) by US EPA Method 8015
Lead and Chromium by US EPA Method 6010
Polychlorinated Biphenyls (PCBs) by US EPA Method 8082
Polycyclic Aromatic Hydrocarbons (PAHs) by US EPA Method 8270
Volatile Organic Compounds (VOCs) by US EPA Method 8260
Page 1 of 3
Sample ID AB-3 AB-5 NCDEQ NCDEQ
Date 5/30/2023 5/30/2023 GWQS GCLs
(µg/L)(µg/L)
VOCs by US EPA Method
8260B
Toluene µg/L 0.53 J <MDL 600 260,000Chloroformµg/L <MDL 1.1 70 70,000
Remaining VOCs µg/L <MDL <MDL Varies Varies
PAHs via US EPA Method
Naphthalene µg/L 0.067 J 0.053 J 6 6,000Remaining PAHs µg/L <MDL <MDL Varies Varies
Notes:µg/L<MDL Not detected above the laboratory method detection limit (MDL)
PQL Laboratory practical quantitation limit
J Concentration is an estimated value between the MDL and the PQL
US EPANCDEQ North Carolina Department of Environmental Quality
GWQS NCDEQ Groundwater Quality Standards
GCLs
VOCs
PAHs Polycyclic Aromatic Hydrocarbons
Micrograms per liter
United States Environmental Protection Agency
NCDEQ Gross Contaminant Levels
Volatile Organic Compounds
Page 2 of 3
Comparison Value(s):
Sample ID AB-1:8-9 AB-1:12-13 AB-4:6-7 NCDEQ
Date 5/30/2023 5/30/2023 5/30/2023 GCLs
(µg/L)
TCLP VOCs by US EPA
Method SW1311/8260D
1,4-Dichlorobenzene µg/L NA 19 NA 6,000Chlorobenzeneµg/L NA 0.21 NA 50,000
Benzene µg/L NA <MDL NA 5,000
TCLP PAHs via US EPA
1-Methylnaphthalene µg/L 16 32 140 1,0002-Methylnaphthalene µg/L <MDL 27 200 12,500
Naphthalene µg/L 16 14 81 6,000Notes:
µg/L<MDL Not detected above the laboratory method detection limit (MDL)
PQL Laboratory practical quantitation limit
J Concentration is an estimated value between the MDL and the PQL
NA Not analyzed
TCLP Toxic Characteristic Leaching Procedure
US EPANCDEQ North Carolina Department of Environmental Quality
GCLs
VOCs
PAHs Polycyclic Aromatic Hydrocarbons
Volatile Organic Compounds
Micrograms per liter
NCDEQ Gross Contaminant Levels
United States Environmental Protection Agency
Page 3 of 3
APPENDIX A
GEOPHYSICAL
SURVEY
REPORT
Utility Locate Report
11330 Vanstory Dr Ste 115D
Huntersville NC 28078
(877) 337-2267, (704) 728-5555
Invoice@intscan.com
DATE 05/30/2023 -
TECH(S)Joseph Whitehill
JOB #1020164261
PO #
CUSTOMER
AEI Consultants
Ben Friedman
200 South Park Road, Suite 400
Hollywood, FL, 33021
(862) 703-6329
bfriedman@aeiconsultants.com
SERVICE LOCATION
AEI Consultants
625 Sullivan Road
Statesville, NC, 28677
(862) 703-6329
bfriedman@aeiconsultants.com
JOB DETAILS 12 borings
Borings will mostly be close together inside an auto repair around in-ground lifts and floor drains. Check if
the drains discharge to an oil/water separator or not.
COMPLETION NOTES Cleared interior areas prior to soil bores. Objects detected marked with blue crayon and tape. Also cleared
several areas outside and detected area where UST was removed. GPR detected disturbed soil consistent
with excavated soil.
ADDITIONAL INFORMATION COLLECTED AT JOB SITE
Any relevant and collected data in the form of images and GPS will be attached in the email corresponding with this document.
Links to the collected data are also included at the end of this report.
11330 Vanstory Dr Ste 115D
Huntersville NC 28078
(877) 337-2267, (704) 728-5555
Invoice@intscan.com
DATE 05/30/2023 -
TECH(S)Joseph Whitehill
JOB #1020164261
PO #
CUSTOMER AEI Consultants
SERVICE LOCATION
ADDITIONAL DOCUMENTS
Documents Attached To This Job:
90812 site map.pdf
5.30.23.kmz
5.30.23.pdf
The standard reports we do include a PDF & a Google Earth file. The links are in
the space above. They are also included as attachments to the email corresponding
with this document. The Google Earth file can be opened on a phone with the
Google Earth app installed. If you open it on a computer it will include photos as
well.
The linked folder contains a folder with photos from the site. If you need an ESRI
or geodatabase file for import into an existing GIS system please do not hesitate to
ask.
Interior areas investigated. Objects marked with either blue crayon or blue
tape.
Probable area of former UST outlined in pink based on detected soil
disturbance,
PICTURES
Back area cleared for soil boring marked in white
CUSTOMER MESSAGE
Ground Penetrating Radar & 3D Laser Scanning are technologies designed to gather data for interpretation. These technologies
are limited in their ability by the conditions of any given project. Any information collected by these technologies should be
verified by other available means.
No liability is accepted by iSS.
For more information on -
Concrete scanning: https://goo.gl/XAsv4E
Utility Locating: https://goo.gl/QbEuWM
This is not an invoice. Invoice will be sent per your company's invoice guidelines.
APPENDIX B
BORING LOGS
0.5
1.0
8.0
13.0
15.0
Concrete
(GW) Gravel
(CL) LP Clay, dark red, moist
(CL) LP Clay, dark greenish grey, moist, petroleum odor
(CL) LP clay, orange, moist
Bottom of borehole at 15.0 feet.
AB-1:8-9
AB-1:12-13
0
0
0
23.0
5
34.4
11.2
NOTES Adjacent to former lift and clarifier
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
T
H
(f
t
)
0
5
10
15
MATERIAL DESCRIPTION COMPLETION
SA
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PAGE 1 OF 1
BORING NUMBER AB-1
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
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AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
1.0
6.0
12.0
15.0
Concrete
(GW) Gravel
(CH) HP Clay, dark red
(CH) HP Clay, red
(CH) HP Clay, light red, moist
Bottom of borehole at 15.0 feet.
AB-2:8-9
0
0
0
0
0
0
0
NOTES Adjacent to former lift
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
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(f
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0
5
10
15
MATERIAL DESCRIPTION COMPLETION
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PAGE 1 OF 1
BORING NUMBER AB-2
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
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AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
1.0
8.0
12.0
20.0
Concrete
(GW) Gravel
(CH) HP Clay, dark red to red
(CH) HP Clay to silt, light red
No core - SP-22 groundwater sampling rod push to 20 feet bgs,replaced with pvc temp well
Bottom of borehole at 20.0 feet.
10 foot screen
AB-3:8-9
0
0
0
0
0
0
NOTES Adjacent to former lift
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING 16.00 ft
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
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DE
P
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(f
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)
0
5
10
15
20
MATERIAL DESCRIPTION COMPLETION
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PAGE 1 OF 1
BORING NUMBER AB-3
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
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B
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AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
1.0
4.0
10.0
12.0
Concrete
(GW) Gravel
(CH) HP Clay, dark red, petroleum odor
(CH) HP Clay, brown, petroleum odor
(ML) Silt, saprolite, pale brown - refusal on rock
Refusal at 12.0 feet.Bottom of borehole at 12.0 feet.
AB-4:6-7
9
20.4
110.8
111.7
135
67
60
122.2
NOTES Adjacent to former lift
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
T
H
(f
t
)
0
5
10
MATERIAL DESCRIPTION COMPLETION
SA
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PAGE 1 OF 1
BORING NUMBER AB-4
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
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B
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AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
6.0
12.0
18.0
Asphalt
(CH) HP Clay, dark red, moist
(CH) HP Clay, brown, moist
Groundwater sampling rod, replaced with PVC temp well due tolow flow conditions
Bottom of borehole at 18.0 feet.
10-foot screen
AB-5:10-11
0
0
0
0
0
0
NOTES Downgradient of lifts and drains
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING 16.00 ft
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
T
H
(f
t
)
0
5
10
15
MATERIAL DESCRIPTION COMPLETION
SA
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PAGE 1 OF 1
BORING NUMBER AB-5
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
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B
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G
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AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
1.0
7.0
15.0
Concrete
(GW) Gravel
(CH) HP Clay, dark red
(ML) Silt, brown
Bottom of borehole at 15.0 feet.
AB-6:8-9
0
0
0
0
0
0
0
NOTES Adjacent to former lift
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
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LO
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DE
P
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(f
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)
0
5
10
15
MATERIAL DESCRIPTION COMPLETION
SA
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(
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)
PAGE 1 OF 1
BORING NUMBER AB-6
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
I
B
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N
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P
J
AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
1.0
7.0
15.0
Concrete
(GW) Gravel
(CH) HP Clay, dark red
(ML) Silt, brown
Bottom of borehole at 15.0 feet.
AB-7:8-9
0
0
0
0
0
0
0
NOTES Adjacent to former lift
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
T
H
(f
t
)
0
5
10
15
MATERIAL DESCRIPTION COMPLETION
SA
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(
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PAGE 1 OF 1
BORING NUMBER AB-7
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
I
B
O
R
I
N
G
-
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I
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.
G
P
J
AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
1.0
4.0
8.0
15.0
Concrete
(GW) Gravel
(CH) HP Clay, dark red
(SM) Silty sand, dark brown
(ML) Silt, light brown with white clay nodes, moist
Bottom of borehole at 15.0 feet.
AB-8:8-9
0
0
0
0
0
0
0
NOTES Adjacent to former lift
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
T
H
(f
t
)
0
5
10
15
MATERIAL DESCRIPTION COMPLETION
SA
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P
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NU
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BL
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(
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PAGE 1 OF 1
BORING NUMBER AB-8
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
I
B
O
R
I
N
G
-
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AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
1.0
4.0
8.0
10.0
15.0
Concrete
(GW) Gravel
(CH) HP Clay, dark red
(CL) LP Clay, brown
(ML) Silt, brown
(ML) Silt, saprolite, brown
Bottom of borehole at 15.0 feet.
AB-9:8-9
0
0
0
0
0
0
0
NOTES Adjacent to former lift
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
T
H
(f
t
)
0
5
10
15
MATERIAL DESCRIPTION COMPLETION
SA
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P
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(
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PAGE 1 OF 1
BORING NUMBER AB-9
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
I
B
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I
N
G
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AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
1.0
5.0
Concrete
(GW) Gravel
(CH) HP Clay, dark red with micas
Bottom of borehole at 5.0 feet.
AB-10:4-5
0
0
0
0
NOTES Adjacent to former drains
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
T
H
(f
t
)
0
5
MATERIAL DESCRIPTION COMPLETION
SA
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P
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(
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PAGE 1 OF 1
BORING NUMBER AB-10
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
I
B
O
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I
N
G
-
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S
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G
P
J
AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
1.0
5.0
Concrete
(GW) Gravel
(CH) HP Clay, dark red
Bottom of borehole at 5.0 feet.
AB-11:4-5
0
0
0
0
NOTES Adjacent to former drains
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Direct Push
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
T
H
(f
t
)
0
5
MATERIAL DESCRIPTION COMPLETION
SA
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P
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P
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NU
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B
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BL
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(
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PAGE 1 OF 1
BORING NUMBER AB-11
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
I
B
O
R
I
N
G
-
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J
AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
0.5
7.5
Topsoil
(CL) Clay, dark red to brown, moist
Bottom of borehole at 7.5 feet.
AB-12:4-5
0
0
0
0
0
0
0
NOTES Background metal sample
GROUND ELEVATION
LOGGED BY Daniel Bakos
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR Mid-South Enviormental GROUND WATER LEVELS:
CHECKED BY Michael Meares
DATE STARTED 5/30/23 COMPLETED 5/30/23
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 2.25 inches
GR
A
P
H
I
C
LO
G
DE
P
T
H
(f
t
)
0
5
MATERIAL DESCRIPTION COMPLETION
SA
M
P
L
E
T
Y
P
E
NU
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B
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BL
O
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CO
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D
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A
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(
p
p
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)
PAGE 1 OF 1
BORING NUMBER AB-12
CLIENT Agree
PROJECT NUMBER 479067
PROJECT NAME Sunbelt Rentals
PROJECT LOCATION 625 Sullivan Road
AE
I
B
O
R
I
N
G
-
G
I
N
T
S
T
D
U
S
L
A
B
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4
7
9
0
6
7
B
O
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I
N
G
L
O
G
S
.
G
P
J
AEI Consultants
2500 Camino Diablo
Walnut creek, CA 94596
Telephone: 925-746-6000
Fax: 925-746-6099
APPENDIX C
LABORATORY
ANALYTICAL REPORTS
June 14, 2023
Analytical Environmental Services, Inc. received samples on
for the analyses presented in following report.
14
“No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in
the report or QC Summary. Additionally, all results for the associated Quality Control samples were within
EPA and/or AES established limits.
AES’s accreditations are as follows:
-NELAP/State of Florida Laboratory ID E87582 for analysis of Non-Potable Water, Solid & Chemical
Materials, Air & Emissions Volatile Organics, and Drinking Water Microbiology & Metals, effective
07/01/22-06/30/23.
State of Georgia, Department of Natural Resources ID #800 for analysis of Drinking Water Metals, effective
through 06/30/23 and Total Coliforms/ E. coli, effective 04/25/23-04/24/24.
-AIHA LAP, LLC Laboratory ID: 100671 for Industrial Hygiene samples (Metals and PCM Asbestos),
Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct
Examination, effective until 11/01/23.
These results relate only to the items tested as received. This report may only be reproduced in full.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Project Manager
230534A
Daniel Bakos
AEI Consultants
4225 Wade Green Rd
Kennesaw GA 30144
Sunbelt
Shawn Boyd
May 31, 2023 4:31 pm
Daniel Bakos:
Page 1 of 57
Page 2 of 57
Page 3 of 57
Analytical Environmental Services, Inc Date:14-Jun-23
Analyses Dilution
FactorBatchIDUnitsQualReporting
LimitResultMDL
SUMMARY OF ANALYTES DETECTED
230534A-001
Soil5/30/2023 8:35:00 AM
AB-1:8-9
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
1-Methylnaphthalene 6.4 2.3 mg/Kg-dry 357654 1000.082
2-Methylnaphthalene 1.2 0.23 mg/Kg-dry 357654 1000.095
Anthracene 0.084 0.0023 mg/Kg-dry 357654 10.00099
Benz(a)anthracene 0.048 0.0023 mg/Kg-dry 357654 10.0017
Benzo(a)pyrene 0.063 0.0023 mg/Kg-dry 357654 10.0012
Benzo(b)fluoranthene 0.095 0.0045 mg/Kg-dry 357654 10.0016
Benzo(g,h,i)perylene 0.023 0.0045 mg/Kg-dry 357654 10.0013
Chrysene 0.075 0.0023 mg/Kg-dry 357654 10.00099
Fluoranthene 0.18 0.0045 mg/Kg-dry 357654 10.0012
Fluorene 0.37 0.0045 mg/Kg-dry 357654 10.00095
Indeno(1,2,3-cd)pyrene 0.016 0.0023 mg/Kg-dry 357654 10.0016
Naphthalene 2.0 0.23 mg/Kg-dry 357654 1000.068
Phenanthrene 0.77 0.23 mg/Kg-dry 357654 1000.088
Pyrene 0.17 0.0023 mg/Kg-dry 357654 10.0015
(SW3546)POLYCHLORINATED BIPHENYLS SW8082A
Aroclor 1242 0.014 0.046J mg/Kg-dry 357304 10.013
Aroclor 1254 0.015 0.046J mg/Kg-dry 357304 10.013
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)6100 920 mg/Kg-dry 357230 100460
PERCENT MOISTURE D2216
Percent Moisture 26.9 0 wt%R517885 10
230534A-002
Soil5/30/2023 8:40:00 AM
AB-1:12-13
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW5035)TCL VOLATILE ORGANICS SW8260D
1,2-Dichlorobenzene 0.080 0.0071 mg/Kg-dry 357337 10.0016
1,3-Dichlorobenzene 0.071 0.0071 mg/Kg-dry 357337 10.0023
1,4-Dichlorobenzene 1.3 0.76 mg/Kg-dry 357431 5001.2
Acetone 0.040 0.14J mg/Kg-dry 357337 10.034
Benzene 0.16 0.0071 mg/Kg-dry 357337 10.0013
Carbon disulfide 0.0047 0.014J mg/Kg-dry 357337 10.0031
Chlorobenzene 29 3.8 mg/Kg-dry 357431 5000.71
Ethylbenzene 0.017 0.0071 mg/Kg-dry 357337 10.0014
Isopropylbenzene 0.013 0.0071 mg/Kg-dry 357337 10.0016
Methylcyclohexane 0.015 0.0071 mg/Kg-dry 357337 10.0026
Methylene chloride 0.0042 0.028J mg/Kg-dry 357337 10.0034
o-Xylene 0.025 0.0071 mg/Kg-dry 357337 10.0019
Toluene 0.0058 0.0071J mg/Kg-dry 357337 10.0017
Xylenes, Total 0.025 0.0071 mg/Kg-dry 357337 10.0069
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
1-Methylnaphthalene 1.3 0.23 mg/Kg-dry 357345 100.0080
2-Methylnaphthalene 0.40 0.023 mg/Kg-dry 357345 10.00093
Acenaphthene 0.037 0.023 mg/Kg-dry 357345 10.0012
Anthracene 0.025 0.0023 mg/Kg-dry 357345 10.00096
Benz(a)anthracene 0.019 0.0023 mg/Kg-dry 357345 10.0016
Benzo(a)pyrene 0.015 0.0023 mg/Kg-dry 357345 10.0012 Page 4 of 57
Analytical Environmental Services, Inc Date:14-Jun-23
Analyses Dilution
FactorBatchIDUnitsQualReporting
LimitResultMDL
SUMMARY OF ANALYTES DETECTED
230534A-002
Soil5/30/2023 8:40:00 AM
AB-1:12-13
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Benzo(b)fluoranthene 0.020 0.0044 mg/Kg-dry 357345 10.0015
Benzo(g,h,i)perylene 0.010 0.0044 mg/Kg-dry 357345 10.0013
Benzo(k)fluoranthene 0.0054 0.0023 mg/Kg-dry 357345 10.0011
Chrysene 0.020 0.0023 mg/Kg-dry 357345 10.00096
Dibenz(a,h)anthracene 0.0036 0.0044J mg/Kg-dry 357345 10.0015
Fluoranthene 0.057 0.0044 mg/Kg-dry 357345 10.0012
Fluorene 0.13 0.0044 mg/Kg-dry 357345 10.00093
Indeno(1,2,3-cd)pyrene 0.0078 0.0023 mg/Kg-dry 357345 10.0016
Naphthalene 0.058 0.023 mg/Kg-dry 357345 10.00066
Phenanthrene 0.18 0.0023 mg/Kg-dry 357345 10.00086
Pyrene 0.061 0.0023 mg/Kg-dry 357345 10.0015
(SW3050B)Metals by ICP/MS SW6020B
Chromium 52.6 0.97 mg/Kg-dry 357293 50.321
Lead 10.9 0.48 mg/Kg-dry 357293 50.0347
PERCENT MOISTURE D2216
Percent Moisture 24.9 0 wt%R517885 10
230534A-003
Soil5/30/2023 9:00:00 AM
AB-2:8-9
Matrix:Collection Date:
Client Sample ID:Lab ID:
PERCENT MOISTURE D2216
Percent Moisture 32.5 0 wt%R517885 10
230534A-004
Soil5/30/2023 9:40:00 AM
AB-3:8-9
Matrix:Collection Date:
Client Sample ID:Lab ID:
PERCENT MOISTURE D2216
Percent Moisture 31.7 0 wt%R517885 10
230534A-005
Soil5/30/2023 10:00:00 AM
AB-4:6-7
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
1-Methylnaphthalene 10 2.2 mg/Kg-dry 357654 1000.078
2-Methylnaphthalene 16 2.2 mg/Kg-dry 357654 1000.090
Anthracene 0.41 0.22 mg/Kg-dry 357654 1000.093
Benz(a)anthracene 0.024 0.0022 mg/Kg-dry 357654 10.0016
Benzo(a)pyrene 0.0020 0.0022J mg/Kg-dry 357654 10.0011
Benzo(b)fluoranthene 0.0029 0.0042J mg/Kg-dry 357654 10.0015
Benzo(g,h,i)perylene 0.0024 0.0042J mg/Kg-dry 357654 10.0012
Chrysene 0.049 0.0022 mg/Kg-dry 357654 10.00093
Fluorene 2.0 0.42 mg/Kg-dry 357654 1000.090
Naphthalene 3.5 2.2 mg/Kg-dry 357654 1000.064
Phenanthrene 4.5 0.22 mg/Kg-dry 357654 1000.083
Pyrene 0.92 0.22 mg/Kg-dry 357654 1000.15
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)2600 86 mg/Kg-dry 357230 1044
PERCENT MOISTURE D2216
Percent Moisture 22.2 0 wt%R517885 10
Page 5 of 57
Analytical Environmental Services, Inc Date:14-Jun-23
Analyses Dilution
FactorBatchIDUnitsQualReporting
LimitResultMDL
SUMMARY OF ANALYTES DETECTED
230534A-008
Soil5/30/2023 12:40:00 PM
AB-6:8-9
Matrix:Collection Date:
Client Sample ID:Lab ID:
PERCENT MOISTURE D2216
Percent Moisture 28.1 0 wt%R517885 10
230534A-009
Soil5/30/2023 12:20:00 PM
AB-7:8-9
Matrix:Collection Date:
Client Sample ID:Lab ID:
PERCENT MOISTURE D2216
Percent Moisture 31.8 0 wt%R517885 10
230534A-010
Soil5/30/2023 12:05:00 PM
AB-8:8-9
Matrix:Collection Date:
Client Sample ID:Lab ID:
PERCENT MOISTURE D2216
Percent Moisture 27.3 0 wt%R517885 10
230534A-011
Soil5/30/2023 11:25:00 AM
AB-9:8-9
Matrix:Collection Date:
Client Sample ID:Lab ID:
PERCENT MOISTURE D2216
Percent Moisture 23.2 0 wt%R517885 10
230534A-012
Soil5/30/2023 9:25:00 AM
AB-10:4-5
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW3050B)Metals by ICP/MS SW6020B
Chromium 59.4 0.81 mg/Kg-dry 357293 50.269
Lead 11.7 0.40 mg/Kg-dry 357293 50.0290
PERCENT MOISTURE D2216
Percent Moisture 19.6 0 wt%R517885 10
230534A-013
Soil5/30/2023 11:50:00 AM
AB-11:4-5
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW5035)TCL VOLATILE ORGANICS SW8260D
Chlorobenzene 0.0038 0.0083J mg/Kg-dry 357337 10.0016
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Anthracene 0.0016 0.0022J mg/Kg-dry 357345 10.00092
Benz(a)anthracene 0.0042 0.0022 mg/Kg-dry 357345 10.0016
Benzo(a)pyrene 0.0034 0.0022 mg/Kg-dry 357345 10.0011
Benzo(b)fluoranthene 0.0054 0.0042 mg/Kg-dry 357345 10.0015
Benzo(g,h,i)perylene 0.0027 0.0042J mg/Kg-dry 357345 10.0012
Benzo(k)fluoranthene 0.0021 0.0022J mg/Kg-dry 357345 10.0011
Chrysene 0.0029 0.0022 mg/Kg-dry 357345 10.00092
Dibenz(a,h)anthracene 0.0023 0.0042J mg/Kg-dry 357345 10.0014
Fluoranthene 0.0043 0.0042 mg/Kg-dry 357345 10.0011
Indeno(1,2,3-cd)pyrene 0.0031 0.0022 mg/Kg-dry 357345 10.0015
Phenanthrene 0.0029 0.0022 mg/Kg-dry 357345 10.00082
Pyrene 0.0078 0.0022 mg/Kg-dry 357345 10.0014
(SW3050B)Metals by ICP/MS SW6020B
Chromium 67.6 0.94 mg/Kg-dry 357293 50.314
Lead 13.3 0.47 mg/Kg-dry 357293 50.0339
PERCENT MOISTURE D2216
Percent Moisture 21.6 0 wt%R517885 10
230534A-014AB-12:4-5Client Sample ID:Lab ID:Page 6 of 57
Analytical Environmental Services, Inc Date:14-Jun-23
Analyses Dilution
FactorBatchIDUnitsQualReporting
LimitResultMDL
SUMMARY OF ANALYTES DETECTED
Soil5/30/2023 1:15:00 PM Matrix:Collection Date:
(SW3050B)Metals by ICP/MS SW6020B
Chromium 93.9 0.78 mg/Kg-dry 357293 50.259
Lead 40.0 0.39 mg/Kg-dry 357293 50.0279
PERCENT MOISTURE D2216
Percent Moisture 24.4 0 wt%R517885 10
230534A-016
Groundwater5/30/2023 12:00:00 PM
AB-3
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW5030B)Volatile Organic Compounds by GC/MS SW8260D
Toluene 0.53 1.0J ug/L 357462 10.33
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 0.067 0.50J ug/L 357258 10.015
230534A-017
Groundwater5/30/2023 2:00:00 PM
AB-5
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW5030B)Volatile Organic Compounds by GC/MS SW8260D
Chloroform 1.1 1.0 ug/L 357462 10.28
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 0.053 0.50J ug/L 357258 10.015
H Holding times for preparation or analysis exceeded
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit Page 7 of 57
230534A-001
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 8:35:00 AM
AB-1:8-9
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
1-Methylnaphthalene 6.4 2.3 mg/Kg-dry 357654 100 06/08/2023 15:05 YH0.082
2-Methylnaphthalene 1.2 0.23 mg/Kg-dry 357654 100 06/08/2023 15:05 YH0.095
Acenaphthene BRL 0.023 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0012
Acenaphthylene BRL 0.045 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0012
Anthracene 0.084 0.0023 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.00099
Benz(a)anthracene 0.048 0.0023 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0017
Benzo(a)pyrene 0.063 0.0023 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0012
Benzo(b)fluoranthene 0.095 0.0045 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0016
Benzo(g,h,i)perylene 0.023 0.0045 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0013
Benzo(k)fluoranthene BRL 0.0023 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0011
Chrysene 0.075 0.0023 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.00099
Dibenz(a,h)anthracene BRL 0.0045 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0015
Fluoranthene 0.18 0.0045 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0012
Fluorene 0.37 0.0045 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.00095
Indeno(1,2,3-cd)pyrene 0.016 0.0023 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0016
Naphthalene 2.0 0.23 mg/Kg-dry 357654 100 06/08/2023 15:05 YH0.068
Phenanthrene 0.77 0.23 mg/Kg-dry 357654 100 06/08/2023 15:05 YH0.088
Pyrene 0.17 0.0023 mg/Kg-dry 357654 1 06/08/2023 12:51 YH0.0015
Surr: 4-Terphenyl-d14 46.5 58.4-135S %REC 357654 1 06/08/2023 12:51 YH0
(SW3546)POLYCHLORINATED BIPHENYLS SW8082A
Aroclor 1016 BRL 0.046 mg/Kg-dry 357304 1 06/02/2023 22:56 ST0.013
Aroclor 1221 BRL 0.046 mg/Kg-dry 357304 1 06/02/2023 22:56 ST0.013
Aroclor 1232 BRL 0.046 mg/Kg-dry 357304 1 06/02/2023 22:56 ST0.013
Aroclor 1242 0.014 0.046J mg/Kg-dry 357304 1 06/02/2023 22:56 ST0.013
Aroclor 1248 BRL 0.046 mg/Kg-dry 357304 1 06/02/2023 22:56 ST0.013
Aroclor 1254 0.015 0.046J mg/Kg-dry 357304 1 06/02/2023 22:56 ST0.013
Aroclor 1260 BRL 0.046 mg/Kg-dry 357304 1 06/02/2023 22:56 ST0.013
Aroclor 1262 BRL 0.046 mg/Kg-dry 357304 1 06/02/2023 22:56 ST0.013
Aroclor 1268 BRL 0.046 mg/Kg-dry 357304 1 06/02/2023 22:56 ST0.013
Surr: Decachlorobiphenyl 76.4 45-130 %REC 357304 1 06/02/2023 22:56 ST0
Surr: Tetrachloro-m-xylene 76.9 49-131 %REC 357304 1 06/02/2023 22:56 ST0
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)6100 920 mg/Kg-dry 357230 100 06/02/2023 17:22 BH460
Surr: Dioctylphthalate 262 50-120S %REC 357230 100 06/02/2023 17:22 BH0
PERCENT MOISTURE D2216
Percent Moisture 26.9 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 8 of 57
230534A-002
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 8:40:00 AM
AB-1:12-13
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5035)TCL VOLATILE ORGANICS SW8260D
1,1,1-Trichloroethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0015
1,1,2,2-Tetrachloroethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0013
1,1,2-Trichloroethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0016
1,1-Dichloroethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0019
1,1-Dichloroethene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0016
1,2,4-Trichlorobenzene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0027
1,2-Dibromo-3-chloropropane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0027
1,2-Dibromoethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0012
1,2-Dichlorobenzene 0.080 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0016
1,2-Dichloroethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0020
1,2-Dichloropropane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0015
1,3-Dichlorobenzene 0.071 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0023
1,4-Dichlorobenzene 1.3 0.76 mg/Kg-dry 357431 500 06/02/2023 14:28 AV1.2
2-Butanone BRL 0.071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0032
2-Hexanone BRL 0.014 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0058
4-Methyl-2-pentanone BRL 0.014 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0036
Acetone 0.040 0.14J mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.034
Benzene 0.16 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0013
Bromodichloromethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0017
Bromoform BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0016
Bromomethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0023
Carbon disulfide 0.0047 0.014J mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0031
Carbon tetrachloride BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0015
Chlorobenzene 29 3.8 mg/Kg-dry 357431 500 06/02/2023 14:28 AV0.71
Chloroethane BRL 0.014 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0024
Chloroform BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0017
Chloromethane BRL 0.014 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0015
cis-1,2-Dichloroethene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0017
cis-1,3-Dichloropropene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0014
Cyclohexane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0028
Dibromochloromethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0013
Dichlorodifluoromethane BRL 0.014 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0028
Ethylbenzene 0.017 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0014
Freon-113 BRL 0.014 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0022
Isopropylbenzene 0.013 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0016
m,p-Xylene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0035
Methyl acetate BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0023
Methyl tert-butyl ether BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0020
Methylcyclohexane 0.015 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0026
Methylene chloride 0.0042 0.028J mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0034
o-Xylene 0.025 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0019
Styrene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0041
Tetrachloroethene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0016
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 9 of 57
230534A-002
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 8:40:00 AM
AB-1:12-13
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5035)TCL VOLATILE ORGANICS SW8260D
Toluene 0.0058 0.0071J mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0017
trans-1,2-Dichloroethene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0015
trans-1,3-Dichloropropene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0013
Trichloroethene BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0016
Trichlorofluoromethane BRL 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0020
Vinyl chloride BRL 0.014 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0019
1,2-Dichloroethene, Total BRL 0.014 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0036
Xylenes, Total 0.025 0.0071 mg/Kg-dry 357337 1 06/01/2023 17:22 RC0.0069
Surr: 4-Bromofluorobenzene 148 63-123S %REC 357337 1 06/01/2023 17:22 RC0
Surr: 4-Bromofluorobenzene 93.9 63-123 %REC 357431 500 06/02/2023 14:28 AV0
Surr: Dibromofluoromethane 100 72-132 %REC 357337 1 06/01/2023 17:22 RC0
Surr: Dibromofluoromethane 85.1 72-132 %REC 357431 500 06/02/2023 14:28 AV0
Surr: Toluene-d8 94.3 70-128 %REC 357337 1 06/01/2023 17:22 RC0
Surr: Toluene-d8 96.8 70-128 %REC 357431 500 06/02/2023 14:28 AV0
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
1-Methylnaphthalene 1.3 0.23 mg/Kg-dry 357345 10 06/05/2023 15:02 YH0.0080
2-Methylnaphthalene 0.40 0.023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.00093
Acenaphthene 0.037 0.023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0012
Acenaphthylene BRL 0.044 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0012
Anthracene 0.025 0.0023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.00096
Benz(a)anthracene 0.019 0.0023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0016
Benzo(a)pyrene 0.015 0.0023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0012
Benzo(b)fluoranthene 0.020 0.0044 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0015
Benzo(g,h,i)perylene 0.010 0.0044 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0013
Benzo(k)fluoranthene 0.0054 0.0023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0011
Chrysene 0.020 0.0023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.00096
Dibenz(a,h)anthracene 0.0036 0.0044J mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0015
Fluoranthene 0.057 0.0044 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0012
Fluorene 0.13 0.0044 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.00093
Indeno(1,2,3-cd)pyrene 0.0078 0.0023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0016
Naphthalene 0.058 0.023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.00066
Phenanthrene 0.18 0.0023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.00086
Pyrene 0.061 0.0023 mg/Kg-dry 357345 1 06/03/2023 01:28 YH0.0015
Surr: 4-Terphenyl-d14 98.2 58.4-135 %REC 357345 1 06/03/2023 01:28 YH0
(SW3050B)Metals by ICP/MS SW6020B
Chromium 52.6 0.97 mg/Kg-dry 357293 5 06/02/2023 03:45 IF0.321
Lead 10.9 0.48 mg/Kg-dry 357293 5 06/02/2023 03:45 IF0.0347
PERCENT MOISTURE D2216
Percent Moisture 24.9 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 10 of 57
230534A-003
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 9:00:00 AM
AB-2:8-9
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3546)POLYCHLORINATED BIPHENYLS SW8082A
Aroclor 1016 BRL 0.049 mg/Kg-dry 357304 1 06/02/2023 22:19 ST0.014
Aroclor 1221 BRL 0.049 mg/Kg-dry 357304 1 06/02/2023 22:19 ST0.014
Aroclor 1232 BRL 0.049 mg/Kg-dry 357304 1 06/02/2023 22:19 ST0.014
Aroclor 1242 BRL 0.049 mg/Kg-dry 357304 1 06/02/2023 22:19 ST0.014
Aroclor 1248 BRL 0.049 mg/Kg-dry 357304 1 06/02/2023 22:19 ST0.014
Aroclor 1254 BRL 0.049 mg/Kg-dry 357304 1 06/02/2023 22:19 ST0.014
Aroclor 1260 BRL 0.049 mg/Kg-dry 357304 1 06/02/2023 22:19 ST0.014
Aroclor 1262 BRL 0.049 mg/Kg-dry 357304 1 06/02/2023 22:19 ST0.014
Aroclor 1268 BRL 0.049 mg/Kg-dry 357304 1 06/02/2023 22:19 ST0.014
Surr: Decachlorobiphenyl 88.7 45-130 %REC 357304 1 06/02/2023 22:19 ST0
Surr: Tetrachloro-m-xylene 81.9 49-131 %REC 357304 1 06/02/2023 22:19 ST0
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)BRL 9.9 mg/Kg-dry 357230 1 06/02/2023 13:22 BH5.0
Surr: Dioctylphthalate 70.6 50-120 %REC 357230 1 06/02/2023 13:22 BH0
PERCENT MOISTURE D2216
Percent Moisture 32.5 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 11 of 57
230534A-004
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 9:40:00 AM
AB-3:8-9
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3546)POLYCHLORINATED BIPHENYLS SW8082A
Aroclor 1016 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 11:42 ST0.014
Aroclor 1221 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 11:42 ST0.014
Aroclor 1232 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 11:42 ST0.014
Aroclor 1242 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 11:42 ST0.014
Aroclor 1248 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 11:42 ST0.014
Aroclor 1254 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 11:42 ST0.014
Aroclor 1260 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 11:42 ST0.014
Aroclor 1262 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 11:42 ST0.014
Aroclor 1268 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 11:42 ST0.014
Surr: Decachlorobiphenyl 94.7 45-130 %REC 357304 1 06/05/2023 11:42 ST0
Surr: Tetrachloro-m-xylene 88.5 49-131 %REC 357304 1 06/05/2023 11:42 ST0
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)BRL 9.8 mg/Kg-dry 357230 1 06/02/2023 13:52 BH5.0
Surr: Dioctylphthalate 68.3 50-120 %REC 357230 1 06/02/2023 13:52 BH0
PERCENT MOISTURE D2216
Percent Moisture 31.7 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 12 of 57
230534A-005
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 10:00:00 AM
AB-4:6-7
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
1-Methylnaphthalene 10 2.2 mg/Kg-dry 357654 100 06/08/2023 15:34 YH0.078
2-Methylnaphthalene 16 2.2 mg/Kg-dry 357654 100 06/08/2023 15:34 YH0.090
Acenaphthene BRL 0.022 mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0012
Acenaphthylene BRL 0.042 mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0011
Anthracene 0.41 0.22 mg/Kg-dry 357654 100 06/08/2023 15:34 YH0.093
Benz(a)anthracene 0.024 0.0022 mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0016
Benzo(a)pyrene 0.0020 0.0022J mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0011
Benzo(b)fluoranthene 0.0029 0.0042J mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0015
Benzo(g,h,i)perylene 0.0024 0.0042J mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0012
Benzo(k)fluoranthene BRL 0.0022 mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0011
Chrysene 0.049 0.0022 mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.00093
Dibenz(a,h)anthracene BRL 0.0042 mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0014
Fluoranthene BRL 0.0042 mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0011
Fluorene 2.0 0.42 mg/Kg-dry 357654 100 06/08/2023 15:34 YH0.090
Indeno(1,2,3-cd)pyrene BRL 0.0022 mg/Kg-dry 357654 1 06/08/2023 13:17 YH0.0015
Naphthalene 3.5 2.2 mg/Kg-dry 357654 100 06/08/2023 15:34 YH0.064
Phenanthrene 4.5 0.22 mg/Kg-dry 357654 100 06/08/2023 15:34 YH0.083
Pyrene 0.92 0.22 mg/Kg-dry 357654 100 06/08/2023 15:34 YH0.15
Surr: 4-Terphenyl-d14 103 58.4-135 %REC 357654 1 06/08/2023 13:17 YH0
(SW3546)POLYCHLORINATED BIPHENYLS SW8082A
Aroclor 1016 BRL 0.043 mg/Kg-dry 357304 1 06/02/2023 23:20 ST0.012
Aroclor 1221 BRL 0.043 mg/Kg-dry 357304 1 06/02/2023 23:20 ST0.012
Aroclor 1232 BRL 0.043 mg/Kg-dry 357304 1 06/02/2023 23:20 ST0.012
Aroclor 1242 BRL 0.043 mg/Kg-dry 357304 1 06/02/2023 23:20 ST0.012
Aroclor 1248 BRL 0.043 mg/Kg-dry 357304 1 06/02/2023 23:20 ST0.012
Aroclor 1254 BRL 0.043 mg/Kg-dry 357304 1 06/02/2023 23:20 ST0.012
Aroclor 1260 BRL 0.043 mg/Kg-dry 357304 1 06/02/2023 23:20 ST0.012
Aroclor 1262 BRL 0.043 mg/Kg-dry 357304 1 06/02/2023 23:20 ST0.012
Aroclor 1268 BRL 0.043 mg/Kg-dry 357304 1 06/02/2023 23:20 ST0.012
Surr: Decachlorobiphenyl 82.4 45-130 %REC 357304 1 06/02/2023 23:20 ST0
Surr: Tetrachloro-m-xylene 72.6 49-131 %REC 357304 1 06/02/2023 23:20 ST0
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)2600 86 mg/Kg-dry 357230 10 06/02/2023 17:53 BH44
Surr: Dioctylphthalate 72.4 50-120 %REC 357230 1 06/02/2023 14:22 BH0
PERCENT MOISTURE D2216
Percent Moisture 22.2 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 13 of 57
230534A-008
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 12:40:00 PM
AB-6:8-9
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3546)POLYCHLORINATED BIPHENYLS SW8082A
Aroclor 1016 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 11:54 ST0.013
Aroclor 1221 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 11:54 ST0.013
Aroclor 1232 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 11:54 ST0.013
Aroclor 1242 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 11:54 ST0.013
Aroclor 1248 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 11:54 ST0.013
Aroclor 1254 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 11:54 ST0.013
Aroclor 1260 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 11:54 ST0.013
Aroclor 1262 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 11:54 ST0.013
Aroclor 1268 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 11:54 ST0.013
Surr: Decachlorobiphenyl 84.3 45-130 %REC 357304 1 06/05/2023 11:54 ST0
Surr: Tetrachloro-m-xylene 79.5 49-131 %REC 357304 1 06/05/2023 11:54 ST0
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)BRL 9.3 mg/Kg-dry 357230 1 06/02/2023 14:51 BH4.7
Surr: Dioctylphthalate 67.1 50-120 %REC 357230 1 06/02/2023 14:51 BH0
PERCENT MOISTURE D2216
Percent Moisture 28.1 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 14 of 57
230534A-009
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 12:20:00 PM
AB-7:8-9
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3546)POLYCHLORINATED BIPHENYLS SW8082A
Aroclor 1016 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 12:06 ST0.014
Aroclor 1221 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 12:06 ST0.014
Aroclor 1232 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 12:06 ST0.014
Aroclor 1242 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 12:06 ST0.014
Aroclor 1248 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 12:06 ST0.014
Aroclor 1254 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 12:06 ST0.014
Aroclor 1260 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 12:06 ST0.014
Aroclor 1262 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 12:06 ST0.014
Aroclor 1268 BRL 0.049 mg/Kg-dry 357304 1 06/05/2023 12:06 ST0.014
Surr: Decachlorobiphenyl 82.3 45-130 %REC 357304 1 06/05/2023 12:06 ST0
Surr: Tetrachloro-m-xylene 77.6 49-131 %REC 357304 1 06/05/2023 12:06 ST0
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)BRL 9.8 mg/Kg-dry 357230 1 06/02/2023 15:21 BH5.0
Surr: Dioctylphthalate 76.2 50-120 %REC 357230 1 06/02/2023 15:21 BH0
PERCENT MOISTURE D2216
Percent Moisture 31.8 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 15 of 57
230534A-010
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 12:05:00 PM
AB-8:8-9
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3546)POLYCHLORINATED BIPHENYLS SW8082A
Aroclor 1016 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 12:19 ST0.013
Aroclor 1221 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 12:19 ST0.013
Aroclor 1232 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 12:19 ST0.013
Aroclor 1242 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 12:19 ST0.013
Aroclor 1248 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 12:19 ST0.013
Aroclor 1254 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 12:19 ST0.013
Aroclor 1260 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 12:19 ST0.013
Aroclor 1262 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 12:19 ST0.013
Aroclor 1268 BRL 0.046 mg/Kg-dry 357304 1 06/05/2023 12:19 ST0.013
Surr: Decachlorobiphenyl 81.4 45-130 %REC 357304 1 06/05/2023 12:19 ST0
Surr: Tetrachloro-m-xylene 76.4 49-131 %REC 357304 1 06/05/2023 12:19 ST0
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)BRL 9.2 mg/Kg-dry 357230 1 06/02/2023 15:51 BH4.7
Surr: Dioctylphthalate 62.8 50-120 %REC 357230 1 06/02/2023 15:51 BH0
PERCENT MOISTURE D2216
Percent Moisture 27.3 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 16 of 57
230534A-011
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 11:25:00 AM
AB-9:8-9
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3546)POLYCHLORINATED BIPHENYLS SW8082A
Aroclor 1016 BRL 0.043 mg/Kg-dry 357304 1 06/05/2023 12:31 ST0.012
Aroclor 1221 BRL 0.043 mg/Kg-dry 357304 1 06/05/2023 12:31 ST0.012
Aroclor 1232 BRL 0.043 mg/Kg-dry 357304 1 06/05/2023 12:31 ST0.012
Aroclor 1242 BRL 0.043 mg/Kg-dry 357304 1 06/05/2023 12:31 ST0.012
Aroclor 1248 BRL 0.043 mg/Kg-dry 357304 1 06/05/2023 12:31 ST0.012
Aroclor 1254 BRL 0.043 mg/Kg-dry 357304 1 06/05/2023 12:31 ST0.012
Aroclor 1260 BRL 0.043 mg/Kg-dry 357304 1 06/05/2023 12:31 ST0.012
Aroclor 1262 BRL 0.043 mg/Kg-dry 357304 1 06/05/2023 12:31 ST0.012
Aroclor 1268 BRL 0.043 mg/Kg-dry 357304 1 06/05/2023 12:31 ST0.012
Surr: Decachlorobiphenyl 86.5 45-130 %REC 357304 1 06/05/2023 12:31 ST0
Surr: Tetrachloro-m-xylene 80.9 49-131 %REC 357304 1 06/05/2023 12:31 ST0
(SW3550C)DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)BRL 8.7 mg/Kg-dry 357230 1 06/02/2023 16:21 BH4.4
Surr: Dioctylphthalate 66.5 50-120 %REC 357230 1 06/02/2023 16:21 BH0
PERCENT MOISTURE D2216
Percent Moisture 23.2 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 17 of 57
230534A-012
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 9:25:00 AM
AB-10:4-5
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5035)TCL VOLATILE ORGANICS SW8260D
1,1,1-Trichloroethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0019
1,1,2,2-Tetrachloroethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0016
1,1,2-Trichloroethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0020
1,1-Dichloroethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0023
1,1-Dichloroethene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0020
1,2,4-Trichlorobenzene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0034
1,2-Dibromo-3-chloropropane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0034
1,2-Dibromoethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0015
1,2-Dichlorobenzene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0020
1,2-Dichloroethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0025
1,2-Dichloropropane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0019
1,3-Dichlorobenzene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0029
1,4-Dichlorobenzene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0027
2-Butanone BRL 0.089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0040
2-Hexanone BRL 0.018 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0072
4-Methyl-2-pentanone BRL 0.018 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0045
Acetone BRL 0.18 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.043
Benzene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0017
Bromodichloromethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0021
Bromoform BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0019
Bromomethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0028
Carbon disulfide BRL 0.018 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0039
Carbon tetrachloride BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0019
Chlorobenzene BRL 0.0089 mg/Kg-dry 357337 1 06/02/2023 13:03 RC0.0017
Chloroethane BRL 0.018 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0030
Chloroform BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0021
Chloromethane BRL 0.018 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0018
cis-1,2-Dichloroethene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0021
cis-1,3-Dichloropropene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0017
Cyclohexane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0035
Dibromochloromethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0016
Dichlorodifluoromethane BRL 0.018 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0035
Ethylbenzene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0018
Freon-113 BRL 0.018 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0027
Isopropylbenzene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0020
m,p-Xylene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0044
Methyl acetate BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0029
Methyl tert-butyl ether BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0025
Methylcyclohexane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0032
Methylene chloride BRL 0.035 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0043
o-Xylene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0024
Styrene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0051
Tetrachloroethene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0019
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 18 of 57
230534A-012
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 9:25:00 AM
AB-10:4-5
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5035)TCL VOLATILE ORGANICS SW8260D
Toluene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0021
trans-1,2-Dichloroethene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0018
trans-1,3-Dichloropropene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0016
Trichloroethene BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0020
Trichlorofluoromethane BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0025
Vinyl chloride BRL 0.018 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0024
1,2-Dichloroethene, Total BRL 0.018 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0045
Xylenes, Total BRL 0.0089 mg/Kg-dry 357337 1 06/01/2023 17:46 RC0.0086
Surr: 4-Bromofluorobenzene 100 63-123 %REC 357337 1 06/02/2023 13:03 RC0
Surr: 4-Bromofluorobenzene 100 63-123 %REC 357337 1 06/01/2023 17:46 RC0
Surr: Dibromofluoromethane 96.3 72-132 %REC 357337 1 06/01/2023 17:46 RC0
Surr: Dibromofluoromethane 97.1 72-132 %REC 357337 1 06/02/2023 13:03 RC0
Surr: Toluene-d8 96.2 70-128 %REC 357337 1 06/01/2023 17:46 RC0
Surr: Toluene-d8 99.2 70-128 %REC 357337 1 06/02/2023 13:03 RC0
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
1-Methylnaphthalene BRL 0.021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.00075
2-Methylnaphthalene BRL 0.021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.00087
Acenaphthene BRL 0.021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0011
Acenaphthylene BRL 0.041 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0011
Anthracene BRL 0.0021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.00090
Benz(a)anthracene BRL 0.0021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0015
Benzo(a)pyrene BRL 0.0021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0011
Benzo(b)fluoranthene BRL 0.0041 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0014
Benzo(g,h,i)perylene BRL 0.0041 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0012
Benzo(k)fluoranthene BRL 0.0021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0010
Chrysene BRL 0.0021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.00090
Dibenz(a,h)anthracene BRL 0.0041 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0014
Fluoranthene BRL 0.0041 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0011
Fluorene BRL 0.0041 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.00087
Indeno(1,2,3-cd)pyrene BRL 0.0021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0015
Naphthalene BRL 0.021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.00062
Phenanthrene BRL 0.0021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.00080
Pyrene BRL 0.0021 mg/Kg-dry 357345 1 06/03/2023 01:55 YH0.0014
Surr: 4-Terphenyl-d14 102 58.4-135 %REC 357345 1 06/03/2023 01:55 YH0
(SW3050B)Metals by ICP/MS SW6020B
Chromium 59.4 0.81 mg/Kg-dry 357293 5 06/02/2023 21:29 IF0.269
Lead 11.7 0.40 mg/Kg-dry 357293 5 06/02/2023 04:24 IF0.0290
PERCENT MOISTURE D2216
Percent Moisture 19.6 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 19 of 57
230534A-013
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 11:50:00 AM
AB-11:4-5
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5035)TCL VOLATILE ORGANICS SW8260D
1,1,1-Trichloroethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0018
1,1,2,2-Tetrachloroethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0015
1,1,2-Trichloroethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0019
1,1-Dichloroethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0022
1,1-Dichloroethene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0019
1,2,4-Trichlorobenzene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0031
1,2-Dibromo-3-chloropropane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0031
1,2-Dibromoethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0014
1,2-Dichlorobenzene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0019
1,2-Dichloroethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0023
1,2-Dichloropropane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0018
1,3-Dichlorobenzene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0027
1,4-Dichlorobenzene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0026
2-Butanone BRL 0.083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0037
2-Hexanone BRL 0.017 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0068
4-Methyl-2-pentanone BRL 0.017 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0042
Acetone BRL 0.17 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.040
Benzene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0016
Bromodichloromethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0020
Bromoform BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0018
Bromomethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0026
Carbon disulfide BRL 0.017 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0037
Carbon tetrachloride BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0018
Chlorobenzene 0.0038 0.0083J mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0016
Chloroethane BRL 0.017 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0028
Chloroform BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0020
Chloromethane BRL 0.017 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0017
cis-1,2-Dichloroethene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0019
cis-1,3-Dichloropropene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0016
Cyclohexane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0032
Dibromochloromethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0015
Dichlorodifluoromethane BRL 0.017 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0032
Ethylbenzene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0017
Freon-113 BRL 0.017 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0026
Isopropylbenzene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0019
m,p-Xylene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0041
Methyl acetate BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0027
Methyl tert-butyl ether BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0023
Methylcyclohexane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0030
Methylene chloride BRL 0.033 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0040
o-Xylene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0022
Styrene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0047
Tetrachloroethene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0018
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 20 of 57
230534A-013
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 11:50:00 AM
AB-11:4-5
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5035)TCL VOLATILE ORGANICS SW8260D
Toluene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0019
trans-1,2-Dichloroethene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0017
trans-1,3-Dichloropropene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0015
Trichloroethene BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0019
Trichlorofluoromethane BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0023
Vinyl chloride BRL 0.017 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0023
1,2-Dichloroethene, Total BRL 0.017 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0042
Xylenes, Total BRL 0.0083 mg/Kg-dry 357337 1 06/01/2023 18:10 RC0.0080
Surr: 4-Bromofluorobenzene 102 63-123 %REC 357337 1 06/01/2023 18:10 RC0
Surr: Dibromofluoromethane 96.8 72-132 %REC 357337 1 06/01/2023 18:10 RC0
Surr: Toluene-d8 98 70-128 %REC 357337 1 06/01/2023 18:10 RC0
(SW3550C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
1-Methylnaphthalene BRL 0.022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.00077
2-Methylnaphthalene BRL 0.022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.00089
Acenaphthene BRL 0.022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0011
Acenaphthylene BRL 0.042 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0011
Anthracene 0.0016 0.0022J mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.00092
Benz(a)anthracene 0.0042 0.0022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0016
Benzo(a)pyrene 0.0034 0.0022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0011
Benzo(b)fluoranthene 0.0054 0.0042 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0015
Benzo(g,h,i)perylene 0.0027 0.0042J mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0012
Benzo(k)fluoranthene 0.0021 0.0022J mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0011
Chrysene 0.0029 0.0022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.00092
Dibenz(a,h)anthracene 0.0023 0.0042J mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0014
Fluoranthene 0.0043 0.0042 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0011
Fluorene BRL 0.0042 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.00089
Indeno(1,2,3-cd)pyrene 0.0031 0.0022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0015
Naphthalene BRL 0.022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.00064
Phenanthrene 0.0029 0.0022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.00082
Pyrene 0.0078 0.0022 mg/Kg-dry 357345 1 06/03/2023 02:20 YH0.0014
Surr: 4-Terphenyl-d14 108 58.4-135 %REC 357345 1 06/03/2023 02:20 YH0
(SW3050B)Metals by ICP/MS SW6020B
Chromium 67.6 0.94 mg/Kg-dry 357293 5 06/02/2023 21:32 IF0.314
Lead 13.3 0.47 mg/Kg-dry 357293 5 06/02/2023 04:28 IF0.0339
PERCENT MOISTURE D2216
Percent Moisture 21.6 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 21 of 57
230534A-014
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 1:15:00 PM
AB-12:4-5
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3050B)Metals by ICP/MS SW6020B
Chromium 93.9 0.78 mg/Kg-dry 357293 5 06/02/2023 21:36 IF0.259
Lead 40.0 0.39 mg/Kg-dry 357293 5 06/02/2023 04:31 IF0.0279
PERCENT MOISTURE D2216
Percent Moisture 24.4 0 wt%R517885 1 06/04/2023 00:00 JW0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 22 of 57
230534A-016
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Groundwater
5/30/2023 12:00:00 PM
AB-3
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5030B)Volatile Organic Compounds by GC/MS SW8260D
1,1,1-Trichloroethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.26
1,1,2,2-Tetrachloroethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.21
1,1,2-Trichloroethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.25
1,1-Dichloroethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.28
1,1-Dichloroethene BRL 2.0 ug/L 357462 1 06/02/2023 19:07 OM0.31
1,2,4-Trichlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.33
1,2-Dibromo-3-chloropropane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.62
1,2-Dibromoethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.20
1,2-Dichlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.47
1,2-Dichloroethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.29
1,2-Dichloropropane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.73
1,3-Dichlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.34
1,4-Dichlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.55
2-Butanone BRL 10 ug/L 357462 1 06/02/2023 19:07 OM6.7
2-Hexanone BRL 10 ug/L 357462 1 06/02/2023 19:07 OM2.1
4-Methyl-2-pentanone BRL 10 ug/L 357462 1 06/02/2023 19:07 OM2.2
Acetone BRL 20 ug/L 357462 1 06/02/2023 19:07 OM5.8
Benzene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.26
Bromodichloromethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.28
Bromoform BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.62
Bromomethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.52
Carbon disulfide BRL 5.0 ug/L 357462 1 06/02/2023 19:07 OM0.65
Carbon tetrachloride BRL 2.0 ug/L 357462 1 06/02/2023 19:07 OM0.45
Chlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.29
Chloroethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.36
Chloroform BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.28
Chloromethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.31
cis-1,2-Dichloroethene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.29
cis-1,3-Dichloropropene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.26
Cyclohexane BRL 2.0 ug/L 357462 1 06/02/2023 19:07 OM0.66
Dibromochloromethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.26
Dichlorodifluoromethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.29
Ethylbenzene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.24
Freon-113 BRL 5.0 ug/L 357462 1 06/02/2023 19:07 OM0.28
Isopropylbenzene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.29
m,p-Xylene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.49
Methyl acetate BRL 2.0 ug/L 357462 1 06/02/2023 19:07 OM0.88
Methyl tert-butyl ether BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.23
Methylcyclohexane BRL 2.0 ug/L 357462 1 06/02/2023 19:07 OM0.27
Methylene chloride BRL 5.0 ug/L 357462 1 06/02/2023 19:07 OM2.4
o-Xylene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.27
Styrene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.32
Tetrachloroethene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.29
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 23 of 57
230534A-016
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Groundwater
5/30/2023 12:00:00 PM
AB-3
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5030B)Volatile Organic Compounds by GC/MS SW8260D
Toluene 0.53 1.0J ug/L 357462 1 06/02/2023 19:07 OM0.33
trans-1,2-Dichloroethene BRL 2.0 ug/L 357462 1 06/02/2023 19:07 OM0.31
trans-1,3-Dichloropropene BRL 2.0 ug/L 357462 1 06/02/2023 19:07 OM0.29
Trichloroethene BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.26
Trichlorofluoromethane BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.24
Vinyl chloride BRL 1.0 ug/L 357462 1 06/02/2023 19:07 OM0.33
Surr: 4-Bromofluorobenzene 103 70-126 %REC 357462 1 06/02/2023 19:07 OM0
Surr: Dibromofluoromethane 104 77-121 %REC 357462 1 06/02/2023 19:07 OM0
Surr: Toluene-d8 98 78.6-119 %REC 357462 1 06/02/2023 19:07 OM0
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 0.067 0.50J ug/L 357258 1 06/02/2023 18:56 YH0.015
1-Methylnaphthalene BRL 0.50 ug/L 357258 1 06/02/2023 18:56 YH0.023
2-Methylnaphthalene BRL 0.50 ug/L 357258 1 06/02/2023 18:56 YH0.019
Acenaphthylene BRL 1.0 ug/L 357258 1 06/02/2023 18:56 YH0.021
Acenaphthene BRL 0.50 ug/L 357258 1 06/02/2023 18:56 YH0.057
Fluorene BRL 0.10 ug/L 357258 1 06/02/2023 18:56 YH0.018
Phenanthrene BRL 0.050 ug/L 357258 1 06/02/2023 18:56 YH0.020
Anthracene BRL 0.050 ug/L 357258 1 06/02/2023 18:56 YH0.017
Fluoranthene BRL 0.10 ug/L 357258 1 06/02/2023 18:56 YH0.068
Pyrene BRL 0.050 ug/L 357258 1 06/02/2023 18:56 YH0.028
Benz(a)anthracene BRL 0.050 ug/L 357258 1 06/02/2023 18:56 YH0.027
Chrysene BRL 0.050 ug/L 357258 1 06/02/2023 18:56 YH0.023
Benzo(b)fluoranthene BRL 0.10 ug/L 357258 1 06/02/2023 18:56 YH0.026
Benzo(k)fluoranthene BRL 0.050 ug/L 357258 1 06/02/2023 18:56 YH0.023
Benzo(a)pyrene BRL 0.050 ug/L 357258 1 06/02/2023 18:56 YH0.022
Indeno(1,2,3-cd)pyrene BRL 0.050 ug/L 357258 1 06/02/2023 18:56 YH0.026
Dibenz(a,h)anthracene BRL 0.10 ug/L 357258 1 06/02/2023 18:56 YH0.070
Benzo(g,h,i)perylene BRL 0.10 ug/L 357258 1 06/02/2023 18:56 YH0.054
Surr: 4-Terphenyl-d14 120 64.1-136 %REC 357258 1 06/02/2023 18:56 YH0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 24 of 57
230534A-017
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Groundwater
5/30/2023 2:00:00 PM
AB-5
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5030B)Volatile Organic Compounds by GC/MS SW8260D
1,1,1-Trichloroethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.26
1,1,2,2-Tetrachloroethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.21
1,1,2-Trichloroethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.25
1,1-Dichloroethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.28
1,1-Dichloroethene BRL 2.0 ug/L 357462 1 06/02/2023 18:43 OM0.31
1,2,4-Trichlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.33
1,2-Dibromo-3-chloropropane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.62
1,2-Dibromoethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.20
1,2-Dichlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.47
1,2-Dichloroethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.29
1,2-Dichloropropane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.73
1,3-Dichlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.34
1,4-Dichlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.55
2-Butanone BRL 10 ug/L 357462 1 06/02/2023 18:43 OM6.7
2-Hexanone BRL 10 ug/L 357462 1 06/02/2023 18:43 OM2.1
4-Methyl-2-pentanone BRL 10 ug/L 357462 1 06/02/2023 18:43 OM2.2
Acetone BRL 20 ug/L 357462 1 06/02/2023 18:43 OM5.8
Benzene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.26
Bromodichloromethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.28
Bromoform BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.62
Bromomethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.52
Carbon disulfide BRL 5.0 ug/L 357462 1 06/02/2023 18:43 OM0.65
Carbon tetrachloride BRL 2.0 ug/L 357462 1 06/02/2023 18:43 OM0.45
Chlorobenzene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.29
Chloroethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.36
Chloroform 1.1 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.28
Chloromethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.31
cis-1,2-Dichloroethene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.29
cis-1,3-Dichloropropene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.26
Cyclohexane BRL 2.0 ug/L 357462 1 06/02/2023 18:43 OM0.66
Dibromochloromethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.26
Dichlorodifluoromethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.29
Ethylbenzene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.24
Freon-113 BRL 5.0 ug/L 357462 1 06/02/2023 18:43 OM0.28
Isopropylbenzene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.29
m,p-Xylene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.49
Methyl acetate BRL 2.0 ug/L 357462 1 06/02/2023 18:43 OM0.88
Methyl tert-butyl ether BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.23
Methylcyclohexane BRL 2.0 ug/L 357462 1 06/02/2023 18:43 OM0.27
Methylene chloride BRL 5.0 ug/L 357462 1 06/02/2023 18:43 OM2.4
o-Xylene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.27
Styrene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.32
Tetrachloroethene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.29
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 25 of 57
230534A-017
14-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Groundwater
5/30/2023 2:00:00 PM
AB-5
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5030B)Volatile Organic Compounds by GC/MS SW8260D
Toluene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.33
trans-1,2-Dichloroethene BRL 2.0 ug/L 357462 1 06/02/2023 18:43 OM0.31
trans-1,3-Dichloropropene BRL 2.0 ug/L 357462 1 06/02/2023 18:43 OM0.29
Trichloroethene BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.26
Trichlorofluoromethane BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.24
Vinyl chloride BRL 1.0 ug/L 357462 1 06/02/2023 18:43 OM0.33
Surr: 4-Bromofluorobenzene 102 70-126 %REC 357462 1 06/02/2023 18:43 OM0
Surr: Dibromofluoromethane 104 77-121 %REC 357462 1 06/02/2023 18:43 OM0
Surr: Toluene-d8 98.2 78.6-119 %REC 357462 1 06/02/2023 18:43 OM0
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 0.053 0.50J ug/L 357258 1 06/02/2023 20:15 YH0.015
1-Methylnaphthalene BRL 0.50 ug/L 357258 1 06/02/2023 20:15 YH0.023
2-Methylnaphthalene BRL 0.50 ug/L 357258 1 06/02/2023 20:15 YH0.019
Acenaphthylene BRL 1.0 ug/L 357258 1 06/02/2023 20:15 YH0.021
Acenaphthene BRL 0.50 ug/L 357258 1 06/02/2023 20:15 YH0.057
Fluorene BRL 0.10 ug/L 357258 1 06/02/2023 20:15 YH0.018
Phenanthrene BRL 0.050 ug/L 357258 1 06/02/2023 20:15 YH0.020
Anthracene BRL 0.050 ug/L 357258 1 06/02/2023 20:15 YH0.017
Fluoranthene BRL 0.10 ug/L 357258 1 06/02/2023 20:15 YH0.068
Pyrene BRL 0.050 ug/L 357258 1 06/02/2023 20:15 YH0.028
Benz(a)anthracene BRL 0.050 ug/L 357258 1 06/02/2023 20:15 YH0.027
Chrysene BRL 0.050 ug/L 357258 1 06/02/2023 20:15 YH0.023
Benzo(b)fluoranthene BRL 0.10 ug/L 357258 1 06/02/2023 20:15 YH0.026
Benzo(k)fluoranthene BRL 0.050 ug/L 357258 1 06/02/2023 20:15 YH0.023
Benzo(a)pyrene BRL 0.050 ug/L 357258 1 06/02/2023 20:15 YH0.022
Indeno(1,2,3-cd)pyrene BRL 0.050 ug/L 357258 1 06/02/2023 20:15 YH0.026
Dibenz(a,h)anthracene BRL 0.10 ug/L 357258 1 06/02/2023 20:15 YH0.070
Benzo(g,h,i)perylene BRL 0.10 ug/L 357258 1 06/02/2023 20:15 YH0.054
Surr: 4-Terphenyl-d14 82.4 64.1-136 %REC 357258 1 06/02/2023 20:15 YH0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 26 of 57
SAMPLE/COOLERRECEIPTCHECKLIS
1. ClientName:AESWorkOrderNumber:
2.Carrier:FedExUPSUSPSClientCourierOthe
Yes No N/A Details Comments
3.Shippingcontainer/coolerreceivedingoodcondition?damagedleakingother
4.Custodysealspresentonshippingcontainer?
5.Custodysealsintactonshippingcontainer?
6.Temperatureblankspresent?
7.Coolertemperature(s)withinlimitsof0Ͳ6϶C?[Seeitem13 and 14for
temperature recordings.]
Coolinginitiatedforrecentlycollectedsamples/ice
present
8.ChainofCustody(COC)present?
9.ChainofCustodysigned,dated,andtimedwhenrelinquishedandreceived?
10.Samplernameand/orsignatureonCOC?
11.Wereallsamplesreceivedwithinholdingtime?
12.TATmarkedontheCOC?IfnoTATindicated,proceededwithstandardTATperTerms&Conditions.
13.Cooler1Temperature϶CCooler2Temperature϶CCooler3Temperature϶CCooler4Temperature϶C
Cooler5Temperature϶CCooler6Temperature϶CCooler7Temperature϶CCooler8Temperature϶C
15.Comments:
IcertifythatIhavecompletedsections1Ͳ1ϱ(datedinitials).
Yes No N/A Details Comments
16.Weresamplecontainersintactuponreceipt?
17.Custodysealspresentonsamplecontainers?
18.Custodysealsintactonsamplecontainers?
19.DosamplecontainerlabelsmatchtheCOC?incompleteinfoillegible
nolabelother
20.AreanalysesrequestedindicatedontheCOC?
21. WereallofthesampleslistedontheCOCreceived?samplesreceivedbutnotlistedonCOC
sampleslistedonCOCnotreceived
22.Wasthesamplecollectiondate/timenoted?
23.Didwereceivesufficientsamplevolumeforindicatedanalyses?
24.Weresamplesreceivedinappropriatecontainers?
25.WereVOAsamplesreceivedwithoutheadspace(<1/4"bubble)?
26.Weretripblankssubmitted?listedonCOCnotlistedonCOC
27.Comments:
IcertifythatIhavecompletedsections1ϲͲ27(datedinitials).
Yes No N/A Details Comments
28.Havecontainersneedingchemicalpreservationbeenchecked? *
29.Containersmeetpreservationguidelines?
30.WaspHadjusted at Sample Receipt?
IcertifythatIhavecompletedsections28Ͳ30(datedinitials).
Clear Save as
AEI Consultants 230534A
■
2.4 2.1
14.
DG 6/1/23
■
This section only applies to samples where pH can be
checked at Sample Receipt.
DG 6/1/23
* Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
This also excludes metals by EPA 200.7, 200.8 and 245.1 which will be verified between 16 and 24 hours after preservation.DG 6/1/23
LockedChecklist 7.9.20 Rev 3
Page 27 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357230
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357230MBLK 06/03/2023DIESEL RANGE ORGANICS SW8015C
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 06/01/2023 517919MB-357230
12224654
TPH (Diesel Range Organics)6.7BRL
Surr: Dioctylphthalate 02.402 3.300 72.8 70 130
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357230LCS 06/05/2023DIESEL RANGE ORGANICS SW8015C
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 06/01/2023 517971LCS-357230
12226049
TPH (Diesel Range Organics)6.727.02 33.30 81.1 70 130
Surr: Dioctylphthalate 02.518 3.330 75.6 70 130
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357230MS 06/05/2023DIESEL RANGE ORGANICS SW8015C
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/01/2023 5179712305U58-002BMS
12226050
TPH (Diesel Range Organics)1038.54 50.34 76.5 40.6 121
Surr: Dioctylphthalate 03.303 5.034 65.6 50 120
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357230MSD 06/05/2023DIESEL RANGE ORGANICS SW8015C
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/01/2023 5179712305U58-002BMSD
12226051
TPH (Diesel Range Organics)1042.47 35.650.34 84.4 40.6 121 38.54 9.72
Surr: Dioctylphthalate 03.640 05.034 72.3 50 120 3.303 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 28 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357258
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357258MBLK 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/01/2023 517914MB-357258
12224628
1-Methylnaphthalene 0.50BRL
2-Methylnaphthalene 0.50BRL
Acenaphthene 0.50BRL
Acenaphthylene 1.0BRL
Anthracene 0.050BRL
Benz(a)anthracene 0.050BRL
Benzo(a)pyrene 0.050BRL
Benzo(b)fluoranthene 0.10BRL
Benzo(g,h,i)perylene 0.10BRL
Benzo(k)fluoranthene 0.050BRL
Chrysene 0.050BRL
Dibenz(a,h)anthracene 0.10BRL
Fluoranthene 0.10BRL
Fluorene 0.10BRL
Indeno(1,2,3-cd)pyrene 0.050BRL
Naphthalene 0.50BRL
Phenanthrene 0.050BRL
Pyrene 0.050BRL
Surr: 4-Terphenyl-d14 02.138 2.000 107 64.1 136
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357258LCS 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/01/2023 517914LCS-357258
12224629
1-Methylnaphthalene 0.502.234 2.000 112 67 126
2-Methylnaphthalene 0.502.179 2.000 109 67.7 121
Acenaphthene 0.502.172 2.000 109 70.3 118
Acenaphthylene 1.02.205 2.000 110 70 118
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 29 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357258
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357258LCS 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/01/2023 517914LCS-357258
12224629
Anthracene 0.0502.124 2.000 106 69.4 126
Benz(a)anthracene 0.0502.396 2.000 120 65.9 126
Benzo(a)pyrene 0.0502.168 2.000 108 70.8 125
Benzo(b)fluoranthene 0.102.231 2.000 112 70.4 125
Benzo(g,h,i)perylene 0.102.306 2.000 115 69.8 128
Benzo(k)fluoranthene 0.0502.391 2.000 120 70 131
Chrysene 0.0502.352 2.000 118 70 131
Dibenz(a,h)anthracene 0.102.285 2.000 114 65.4 132
Fluoranthene 0.102.225 2.000 111 69.7 128
Fluorene 0.102.220 2.000 111 70 123
Indeno(1,2,3-cd)pyrene 0.0501.517 2.000 75.9 70.1 130
Naphthalene 0.502.168 2.000 108 69.9 121
Phenanthrene 0.0502.246 2.000 112 69.5 123
Pyrene 0.0502.260 2.000 113 71.2 132
Surr: 4-Terphenyl-d14 02.382 2.000 119 64.1 136
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357258MS 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
AB-3 Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/01/2023 517914230534A-016BMS
12224631
1-Methylnaphthalene 0.502.111 2.000 106 60.2 120
2-Methylnaphthalene 0.502.079 2.000 104 61.3 120
Acenaphthene 0.502.021 2.000 101 51.7 120
Acenaphthylene 1.02.060 2.000 103 50.3 120
Anthracene 0.0501.959 2.000 97.9 54.8 119
Benz(a)anthracene 0.0502.151 2.000 108 57.1 118
Benzo(a)pyrene 0.0501.964 2.000 98.2 53.1 121
Benzo(b)fluoranthene 0.102.037 2.000 102 50.2 117
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 30 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357258
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357258MS 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
AB-3 Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/01/2023 517914230534A-016BMS
12224631
Benzo(g,h,i)perylene 0.102.028 2.000 101 48 122
Benzo(k)fluoranthene 0.0502.235 2.000 112 53 126
Chrysene 0.0502.086 2.000 104 60.2 125
Dibenz(a,h)anthracene 0.101.969 2.000 98.5 47.1 130
Fluoranthene 0.102.084 2.000 104 63 121
Fluorene 0.102.059 2.000 103 61.4 120
Indeno(1,2,3-cd)pyrene 0.0501.935 2.000 96.8 51.1 124
Naphthalene 0.502.093 2.000 0.06742 101 57.3 120
Phenanthrene 0.0502.099 2.000 105 58.3 118
Pyrene 0.0502.096 2.000 105 53.5 124
Surr: 4-Terphenyl-d14 02.312 2.000 116 64.1 136
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357258MSD 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
AB-3 Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/01/2023 517914230534A-016BMSD
12224632
1-Methylnaphthalene 0.502.180 17.52.000 109 60.2 120 2.111 3.22
2-Methylnaphthalene 0.502.141 202.000 107 61.3 120 2.079 2.93
Acenaphthene 0.502.090 18.82.000 105 51.7 120 2.021 3.36
Acenaphthylene 1.02.126 17.82.000 106 50.3 120 2.060 3.16
Anthracene 0.0502.031 41.32.000 102 54.8 119 1.959 3.61
Benz(a)anthracene 0.0502.303 26.82.000 115 57.1 118 2.151 6.84
Benzo(a)pyrene 0.0502.072 19.82.000 104 53.1 121 1.964 5.38
Benzo(b)fluoranthene 0.102.164 24.52.000 108 50.2 117 2.037 6.01
Benzo(g,h,i)perylene 0.102.196 39.72.000 110 48 122 2.028 7.99
Benzo(k)fluoranthene 0.0502.430 30.62.000 122 53 126 2.235 8.35
Chrysene 0.0502.244 20.52.000 112 60.2 125 2.086 7.27
Dibenz(a,h)anthracene 0.102.184 26.52.000 109 47.1 130 1.969 10.3
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 31 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357258
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357258MSD 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
AB-3 Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/01/2023 517914230534A-016BMSD
12224632
Fluoranthene 0.102.131 202.000 107 63 121 2.084 2.21
Fluorene 0.102.149 202.000 107 61.4 120 2.059 4.26
Indeno(1,2,3-cd)pyrene 0.0501.994 33.12.000 99.7 51.1 124 1.935 2.97
Naphthalene 0.502.160 17.62.000 0.06742 105 57.3 120 2.093 3.18
Phenanthrene 0.0502.152 202.000 108 58.3 118 2.099 2.45
Pyrene 0.0502.179 282.000 109 53.5 124 2.096 3.88
Surr: 4-Terphenyl-d14 02.328 02.000 116 64.1 136 2.312 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 32 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357293
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357293MBLK 06/02/2023Metals by ICP/MS SW6020B
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/01/2023 517811MB-357293
12221318
Chromium 1000BRL
Lead 500BRL
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357293LCS 06/02/2023Metals by ICP/MS SW6020B
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/01/2023 517811LCS-357293
12221319
Chromium 10008827 10000 88.3 80 120
Lead 50011100 10000 111 80 120
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357293MS 06/02/2023Metals by ICP/MS SW6020B
AB-1:12-13 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/01/2023 517811230534A-002CMS
12221321
Chromium 0.9754.88 9.675 52.62 23.3 75 125 S
Lead 0.4819.94 9.675 10.88 93.6 75 125
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357293MSD 06/02/2023Metals by ICP/MS SW6020B
AB-1:12-13 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/01/2023 517811230534A-002CMSD
12221324
Chromium 0.9757.78 209.672 52.62 53.4 75 125 54.88 S5.16
Lead 0.4820.37 209.672 10.88 98.1 75 125 19.94 2.13
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 33 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357304
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357304MBLK 06/02/2023POLYCHLORINATED BIPHENYLS SW8082A
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/02/2023 517857MB-357304
12224286
Aroclor 1016 33BRL
Aroclor 1221 33BRL
Aroclor 1232 33BRL
Aroclor 1242 33BRL
Aroclor 1248 33BRL
Aroclor 1254 33BRL
Aroclor 1260 33BRL
Aroclor 1262 33BRL
Aroclor 1268 33BRL
Surr: Decachlorobiphenyl 017.42 16.67 105 45 130
Surr: Tetrachloro-m-xylene 015.02 16.67 90.1 49 131
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357304LCS 06/02/2023POLYCHLORINATED BIPHENYLS SW8082A
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/02/2023 517857LCS-357304
12224287
Aroclor 1016 33147.1 166.7 88.3 60.3 130
Aroclor 1260 33150.8 166.7 90.5 60.7 130
Surr: Decachlorobiphenyl 018.65 16.67 112 45 130
Surr: Tetrachloro-m-xylene 016.83 16.67 101 49 131
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357304MS 06/02/2023POLYCHLORINATED BIPHENYLS SW8082A
AB-2:8-9 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 517857230534A-003AMS
12224289
Aroclor 1016 0.0490.1760 0.2470 71.2 51.4 133
Aroclor 1260 0.0490.1879 0.2470 76.1 51.2 130
Surr: Decachlorobiphenyl 00.02274 0.0247 92.0 45 130
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 34 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357304
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357304MS 06/02/2023POLYCHLORINATED BIPHENYLS SW8082A
AB-2:8-9 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 517857230534A-003AMS
12224289
Surr: Tetrachloro-m-xylene 00.02090 0.0247 84.6 49 131
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357304MSD 06/02/2023POLYCHLORINATED BIPHENYLS SW8082A
AB-2:8-9 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 517857230534A-003AMSD
12224290
Aroclor 1016 0.0490.1896 20.30.2470 76.8 51.4 133 0.1760 7.46
Aroclor 1260 0.0490.1963 21.20.2470 79.4 51.2 130 0.1879 4.36
Surr: Decachlorobiphenyl 00.02274 00.0247 92.0 45 130 0.02274 0
Surr: Tetrachloro-m-xylene 00.02199 00.0247 89.0 49 131 0.02090 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 35 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357337
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357337MBLK 06/01/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/01/2023 517787MB-357337
12220695
1,1,1-Trichloroethane 5.0BRL
1,1,2,2-Tetrachloroethane 5.0BRL
1,1,2-Trichloroethane 5.0BRL
1,1-Dichloroethane 5.0BRL
1,1-Dichloroethene 5.0BRL
1,2,4-Trichlorobenzene 5.0BRL
1,2-Dibromo-3-chloropropane 5.0BRL
1,2-Dibromoethane 5.0BRL
1,2-Dichlorobenzene 5.0BRL
1,2-Dichloroethane 5.0BRL
1,2-Dichloroethene, Total 10BRL
1,2-Dichloropropane 5.0BRL
1,3-Dichlorobenzene 5.0BRL
1,4-Dichlorobenzene 5.0BRL
2-Butanone 50BRL
2-Hexanone 10BRL
4-Methyl-2-pentanone 10BRL
Acetone 100BRL
Benzene 5.0BRL
Bromodichloromethane 5.0BRL
Bromoform 5.0BRL
Bromomethane 5.0BRL
Carbon disulfide 10BRL
Carbon tetrachloride 5.0BRL
Chlorobenzene 5.0BRL
Chloroethane 10BRL
Chloroform 5.0BRL
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 36 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357337
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357337MBLK 06/01/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/01/2023 517787MB-357337
12220695
Chloromethane 10BRL
cis-1,2-Dichloroethene 5.0BRL
cis-1,3-Dichloropropene 5.0BRL
Cyclohexane 5.0BRL
Dibromochloromethane 5.0BRL
Dichlorodifluoromethane 10BRL
Ethylbenzene 5.0BRL
Freon-113 10BRL
Isopropylbenzene 5.0BRL
m,p-Xylene 5.0BRL
Methyl acetate 5.0BRL
Methyl tert-butyl ether 5.0BRL
Methylcyclohexane 5.0BRL
Methylene chloride 20BRL
o-Xylene 5.0BRL
Styrene 5.0BRL
Tetrachloroethene 5.0BRL
Toluene 5.0BRL
trans-1,2-Dichloroethene 5.0BRL
trans-1,3-Dichloropropene 5.0BRL
Trichloroethene 5.0BRL
Trichlorofluoromethane 5.0BRL
Vinyl chloride 10BRL
Xylenes, Total 5.0BRL
Surr: 4-Bromofluorobenzene 049.57 50.00 99.1 63 123
Surr: Dibromofluoromethane 050.19 50.00 100 72 132
Surr: Toluene-d8 050.07 50.00 100 70 128
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 37 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357337
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357337LCS 06/01/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/01/2023 517787LCS-357337
12220696
1,1-Dichloroethene 5.055.04 50.00 110 70 130
Benzene 5.051.10 50.00 102 70 130
Chlorobenzene 5.050.54 50.00 101 70 130
Toluene 5.052.44 50.00 105 70 130
Trichloroethene 5.052.09 50.00 104 70 130
Surr: 4-Bromofluorobenzene 052.05 50.00 104 63 123
Surr: Dibromofluoromethane 050.90 50.00 102 72 132
Surr: Toluene-d8 050.80 50.00 102 70 128
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357337MS 06/02/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/01/2023 5177872305X14-009AMS
12222463
1,1-Dichloroethene 0.00840.08311 0.0842 98.7 55.6 135
Benzene 0.00840.08060 0.0842 95.7 55.2 133
Chlorobenzene 0.00840.07947 0.0842 94.3 60.2 127
Toluene 0.00840.08144 0.0842 96.7 60.2 132
Trichloroethene 0.00840.08185 0.0842 97.2 60 132
Surr: 4-Bromofluorobenzene 00.08399 0.0842 99.7 63 123
Surr: Dibromofluoromethane 00.08311 0.0842 98.7 72 132
Surr: Toluene-d8 00.08557 0.0842 102 70 128
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357337DUP 06/02/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/01/2023 5177872305X14-010ADUP
12222464
1,1,1-Trichloroethane 0.0078BRL 2000
1,1,2,2-Tetrachloroethane 0.0078BRL 2000
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 38 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357337
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357337DUP 06/02/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/01/2023 5177872305X14-010ADUP
12222464
1,1,2-Trichloroethane 0.0078BRL 2000
1,1-Dichloroethane 0.0078BRL 2000
1,1-Dichloroethene 0.0078BRL 2000
1,2,4-Trichlorobenzene 0.0078BRL 2000
1,2-Dibromo-3-chloropropane 0.0078BRL 2000
1,2-Dibromoethane 0.0078BRL 2000
1,2-Dichlorobenzene 0.0078BRL 2000
1,2-Dichloroethane 0.0078BRL 2000
1,2-Dichloroethene, Total 0.016BRL 000
1,2-Dichloropropane 0.0078BRL 2000
1,3-Dichlorobenzene 0.0078BRL 2000
1,4-Dichlorobenzene 0.0078BRL 2000
2-Butanone 0.078BRL 2000
2-Hexanone 0.016BRL 2000
4-Methyl-2-pentanone 0.016BRL 2000
Acetone 0.16BRL 2000
Benzene 0.0078BRL 2000
Bromodichloromethane 0.0078BRL 2000
Bromoform 0.0078BRL 2000
Bromomethane 0.0078BRL 2000
Carbon disulfide 0.016BRL 2000
Carbon tetrachloride 0.0078BRL 2000
Chlorobenzene 0.0078BRL 2000
Chloroethane 0.016BRL 2000
Chloroform 0.0078BRL 2000
Chloromethane 0.016BRL 2000
cis-1,2-Dichloroethene 0.0078BRL 2000
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 39 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357337
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357337DUP 06/02/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/01/2023 5177872305X14-010ADUP
12222464
cis-1,3-Dichloropropene 0.0078BRL 2000
Cyclohexane 0.0078BRL 2000
Dibromochloromethane 0.0078BRL 2000
Dichlorodifluoromethane 0.016BRL 2000
Ethylbenzene 0.0078BRL 2000
Freon-113 0.016BRL 2000
Isopropylbenzene 0.0078BRL 2000
m,p-Xylene 0.0078BRL 2000
Methyl acetate 0.0078BRL 2000
Methyl tert-butyl ether 0.0078BRL 2000
Methylcyclohexane 0.0078BRL 2000
Methylene chloride 0.031BRL 2000
o-Xylene 0.0078BRL 2000
Styrene 0.0078BRL 2000
Tetrachloroethene 0.0078BRL 2000
Toluene 0.0078BRL 2000
trans-1,2-Dichloroethene 0.0078BRL 2000
trans-1,3-Dichloropropene 0.0078BRL 2000
Trichloroethene 0.0078BRL 2000
Trichlorofluoromethane 0.0078BRL 2000
Vinyl chloride 0.016BRL 2000
Xylenes, Total 0.0078BRL 000
Surr: 4-Bromofluorobenzene 00.07676 00.0783 98.0 63 123 0.07607 0
Surr: Dibromofluoromethane 00.07574 00.0783 96.7 72 132 0.07654 0
Surr: Toluene-d8 00.07725 00.0783 98.6 70 128 0.07688 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 40 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357345
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357345MBLK 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/02/2023 517915MB-357345
12224671
1-Methylnaphthalene 17BRL
2-Methylnaphthalene 17BRL
Acenaphthene 17BRL
Acenaphthylene 33BRL
Anthracene 1.7BRL
Benz(a)anthracene 1.7BRL
Benzo(a)pyrene 1.7BRL
Benzo(b)fluoranthene 3.3BRL
Benzo(g,h,i)perylene 3.3BRL
Benzo(k)fluoranthene 1.7BRL
Chrysene 1.7BRL
Dibenz(a,h)anthracene 3.3BRL
Fluoranthene 3.3BRL
Fluorene 3.3BRL
Indeno(1,2,3-cd)pyrene 1.7BRL
Naphthalene 17BRL
Phenanthrene 1.7BRL
Pyrene 1.7BRL
Surr: 4-Terphenyl-d14 076.52 66.70 115 58.4 135
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357345LCS 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/02/2023 517915LCS-357345
12224672
1-Methylnaphthalene 1751.00 66.70 76.5 63 118
2-Methylnaphthalene 1749.95 66.70 74.9 67.4 120
Acenaphthene 1751.26 66.70 76.9 64.9 120
Acenaphthylene 3351.15 66.70 76.7 63.8 120
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 41 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357345
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357345LCS 06/02/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/02/2023 517915LCS-357345
12224672
Anthracene 1.749.78 66.70 74.6 66 120
Benz(a)anthracene 1.755.53 66.70 83.2 63 123
Benzo(a)pyrene 1.750.15 66.70 75.2 65.9 123
Benzo(b)fluoranthene 3.350.05 66.70 75.0 62 126
Benzo(g,h,i)perylene 3.350.66 66.70 76.0 66.3 123
Benzo(k)fluoranthene 1.759.20 66.70 88.8 64.5 129
Chrysene 1.754.58 66.70 81.8 65.9 128
Dibenz(a,h)anthracene 3.348.51 66.70 72.7 68.7 131
Fluoranthene 3.353.89 66.70 80.8 65.7 130
Fluorene 3.352.44 66.70 78.6 65 120
Indeno(1,2,3-cd)pyrene 1.748.75 66.70 73.1 66.3 128
Naphthalene 1749.41 66.70 74.1 63.5 120
Phenanthrene 1.754.58 66.70 81.8 63.4 121
Pyrene 1.756.56 66.70 84.8 65.3 123
Surr: 4-Terphenyl-d14 067.85 66.70 102 58.4 135
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357345MS 06/03/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 5179152305Z64-003BMS
12224674
1-Methylnaphthalene 0.0220.08536 0.0855 99.8 55.3 122
2-Methylnaphthalene 0.0220.08301 0.0855 97.1 53.2 121
Acenaphthene 0.0220.08410 0.0855 98.4 52.5 121
Acenaphthylene 0.0420.08467 0.0855 0.001379 97.4 50.4 121
Anthracene 0.00220.08548 0.0855 0.003772 95.5 56.5 124
Benz(a)anthracene 0.00220.1047 0.0855 0.01221 108 54.3 129
Benzo(a)pyrene 0.00220.09369 0.0855 0.01185 95.7 53.8 127
Benzo(b)fluoranthene 0.00420.09941 0.0855 0.01633 97.2 51.9 126
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 42 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357345
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357345MS 06/03/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 5179152305Z64-003BMS
12224674
Benzo(g,h,i)perylene 0.00420.09973 0.0855 0.01157 103 53 125
Benzo(k)fluoranthene 0.00220.06537 0.0855 0.007244 68.0 52.7 128
Chrysene 0.00220.09972 0.0855 0.01488 99.2 57.5 130
Dibenz(a,h)anthracene 0.00420.08424 0.0855 0.003785 94.1 53.4 128
Fluoranthene 0.00420.1178 0.0855 0.02386 110 60.3 131
Fluorene 0.00420.08703 0.0855 0.002234 99.2 55.7 124
Indeno(1,2,3-cd)pyrene 0.00220.08896 0.0855 0.008943 93.6 54.1 127
Naphthalene 0.0220.08283 0.0855 0.002417 94.0 53.2 120
Phenanthrene 0.00220.1054 0.0855 0.01486 106 54.9 126
Pyrene 0.00220.1149 0.0855 0.02203 109 55.6 129
Surr: 4-Terphenyl-d14 00.09880 0.0855 116 58.4 135
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357345MSD 06/03/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 5179152305Z64-003BMSD
12224675
1-Methylnaphthalene 0.0220.08795 26.80.0855 103 55.3 122 0.08536 2.98
2-Methylnaphthalene 0.0220.08640 31.10.0855 101 53.2 121 0.08301 4.00
Acenaphthene 0.0220.08727 25.80.0855 102 52.5 121 0.08410 3.70
Acenaphthylene 0.0420.08929 31.60.0855 0.001379 103 50.4 121 0.08467 5.31
Anthracene 0.00220.09806 270.0855 0.003772 110 56.5 124 0.08548 13.7
Benz(a)anthracene 0.00220.1254 21.30.0855 0.01221 132 54.3 129 0.1047 S18.0
Benzo(a)pyrene 0.00220.1123 26.40.0855 0.01185 117 53.8 127 0.09369 18.0
Benzo(b)fluoranthene 0.00420.1214 29.40.0855 0.01633 123 51.9 126 0.09941 19.9
Benzo(g,h,i)perylene 0.00420.1263 25.80.0855 0.01157 134 53 125 0.09973 S23.5
Benzo(k)fluoranthene 0.00220.07825 320.0855 0.007244 83.0 52.7 128 0.06537 17.9
Chrysene 0.00220.1184 23.70.0855 0.01488 121 57.5 130 0.09972 17.1
Dibenz(a,h)anthracene 0.00420.1043 28.30.0855 0.003785 118 53.4 128 0.08424 21.3
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 43 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357345
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357345MSD 06/03/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 5179152305Z64-003BMSD
12224675
Fluoranthene 0.00420.1424 27.20.0855 0.02386 139 60.3 131 0.1178 S18.9
Fluorene 0.00420.09380 25.60.0855 0.002234 107 55.7 124 0.08703 7.48
Indeno(1,2,3-cd)pyrene 0.00220.1141 25.40.0855 0.008943 123 54.1 127 0.08896 24.8
Naphthalene 0.0220.08739 290.0855 0.002417 99.4 53.2 120 0.08283 5.36
Phenanthrene 0.00220.1256 26.80.0855 0.01486 130 54.9 126 0.1054 S17.5
Pyrene 0.00220.1376 24.40.0855 0.02203 135 55.6 129 0.1149 S18.0
Surr: 4-Terphenyl-d14 00.1041 00.0855 122 58.4 135 0.09880 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 44 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357431
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357431MBLK 06/02/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/02/2023 517887MB-357431
12223846
1,1,1-Trichloroethane 250BRL
1,1,2,2-Tetrachloroethane 250BRL
1,1,2-Trichloroethane 250BRL
1,1-Dichloroethane 250BRL
1,1-Dichloroethene 250BRL
1,2,4-Trichlorobenzene 250BRL
1,2-Dibromo-3-chloropropane 250BRL
1,2-Dibromoethane 250BRL
1,2-Dichlorobenzene 250BRL
1,2-Dichloroethane 250BRL
1,2-Dichloroethene, Total 500BRL
1,2-Dichloropropane 250BRL
1,3-Dichlorobenzene 250BRL
1,4-Dichlorobenzene 250BRL
2-Butanone 2500BRL
2-Hexanone 500BRL
4-Methyl-2-pentanone 500BRL
Acetone 5000BRL
Benzene 250BRL
Bromodichloromethane 250BRL
Bromoform 250BRL
Bromomethane 250BRL
Carbon disulfide 500BRL
Carbon tetrachloride 250BRL
Chlorobenzene 250BRL
Chloroethane 500BRL
Chloroform 250BRL
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 45 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357431
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357431MBLK 06/02/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/02/2023 517887MB-357431
12223846
Chloromethane 500BRL
cis-1,2-Dichloroethene 250BRL
cis-1,3-Dichloropropene 250BRL
Cyclohexane 250BRL
Dibromochloromethane 250BRL
Dichlorodifluoromethane 500BRL
Ethylbenzene 250BRL
Freon-113 500BRL
Isopropylbenzene 250BRL
m,p-Xylene 250BRL
Methyl acetate 250BRL
Methyl tert-butyl ether 250BRL
Methylcyclohexane 250BRL
Methylene chloride 1000BRL
o-Xylene 250BRL
Styrene 250BRL
Tetrachloroethene 250BRL
Toluene 250BRL
trans-1,2-Dichloroethene 250BRL
trans-1,3-Dichloropropene 250BRL
Trichloroethene 250BRL
Trichlorofluoromethane 250BRL
Vinyl chloride 500BRL
Xylenes, Total 250BRL
Surr: 4-Bromofluorobenzene 02334 2500 93.4 63 123
Surr: Dibromofluoromethane 02266 2500 90.6 72 132
Surr: Toluene-d8 02437 2500 97.5 70 128
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 46 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357431
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357431LCS 06/02/2023TCL VOLATILE ORGANICS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/02/2023 517887LCS-357431
12223847
1,1-Dichloroethene 2502448 2500 97.9 70 130
Benzene 2502608 2500 104 70 130
Chlorobenzene 2502514 2500 101 70 130
Toluene 2502601 2500 104 70 130
Trichloroethene 2502610 2500 104 70 130
Surr: 4-Bromofluorobenzene 02468 2500 98.7 63 123
Surr: Dibromofluoromethane 02448 2500 97.9 72 132
Surr: Toluene-d8 02501 2500 100 70 128
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357431MS 06/02/2023TCL VOLATILE ORGANICS SW8260D
AB-1:12-13 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 517887230534A-002AMS
12223850
1,1-Dichloroethene 3.834.08 37.99 89.7 55.6 135
Benzene 3.837.06 37.99 97.5 55.2 133
Chlorobenzene 3.882.70 37.99 218 60.2 127 S
Toluene 3.835.14 37.99 92.5 60.2 132
Trichloroethene 3.835.92 37.99 94.5 60 132
Surr: 4-Bromofluorobenzene 037.93 37.99 99.8 63 123
Surr: Dibromofluoromethane 039.10 37.99 103 72 132
Surr: Toluene-d8 036.63 37.99 96.4 70 128
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357431MSD 06/02/2023TCL VOLATILE ORGANICS SW8260D
AB-1:12-13 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 517887230534A-002AMSD
12223851
1,1-Dichloroethene 3.828.91 23.737.99 76.1 55.6 135 34.08 16.4
Benzene 3.832.56 17.337.99 85.7 55.2 133 37.06 12.9
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 47 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357431
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357431MSD 06/02/2023TCL VOLATILE ORGANICS SW8260D
AB-1:12-13 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/02/2023 517887230534A-002AMSD
12223851
Chlorobenzene 3.878.35 2037.99 206 60.2 127 82.70 S5.41
Toluene 3.834.61 2037.99 91.1 60.2 132 35.14 1.53
Trichloroethene 3.832.43 2037.99 85.4 60 132 35.92 10.2
Surr: 4-Bromofluorobenzene 036.88 037.99 97.1 63 123 37.93 0
Surr: Dibromofluoromethane 033.57 037.99 88.4 72 132 39.10 0
Surr: Toluene-d8 038.24 037.99 101 70 128 36.63 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 48 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357462
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357462MBLK 06/02/2023Volatile Organic Compounds by GC/MS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/02/2023 517929MB-357462
12225244
1,1,1-Trichloroethane 1.0BRL
1,1,2,2-Tetrachloroethane 1.0BRL
1,1,2-Trichloroethane 1.0BRL
1,1-Dichloroethane 1.0BRL
1,1-Dichloroethene 2.0BRL
1,2,4-Trichlorobenzene 1.0BRL
1,2-Dibromo-3-chloropropane 1.0BRL
1,2-Dibromoethane 1.0BRL
1,2-Dichlorobenzene 1.0BRL
1,2-Dichloroethane 1.0BRL
1,2-Dichloropropane 1.0BRL
1,3-Dichlorobenzene 1.0BRL
1,4-Dichlorobenzene 1.0BRL
2-Butanone 10BRL
2-Hexanone 10BRL
4-Methyl-2-pentanone 10BRL
Acetone 20BRL
Benzene 1.0BRL
Bromodichloromethane 1.0BRL
Bromoform 1.0BRL
Bromomethane 1.0BRL
Carbon disulfide 5.0BRL
Carbon tetrachloride 2.0BRL
Chlorobenzene 1.0BRL
Chloroethane 1.0BRL
Chloroform 1.0BRL
Chloromethane 1.0BRL
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 49 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357462
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357462MBLK 06/02/2023Volatile Organic Compounds by GC/MS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/02/2023 517929MB-357462
12225244
cis-1,2-Dichloroethene 1.0BRL
cis-1,3-Dichloropropene 1.0BRL
Cyclohexane 2.0BRL
Dibromochloromethane 1.0BRL
Dichlorodifluoromethane 1.0BRL
Ethylbenzene 1.0BRL
Freon-113 5.0BRL
Isopropylbenzene 1.0BRL
m,p-Xylene 1.0BRL
Methyl acetate 2.0BRL
Methyl tert-butyl ether 1.0BRL
Methylcyclohexane 2.0BRL
Methylene chloride 5.0BRL
o-Xylene 1.0BRL
Styrene 1.0BRL
Tetrachloroethene 1.0BRL
Toluene 1.0BRL
trans-1,2-Dichloroethene 2.0BRL
trans-1,3-Dichloropropene 2.0BRL
Trichloroethene 1.0BRL
Trichlorofluoromethane 1.0BRL
Vinyl chloride 1.0BRL
Surr: 4-Bromofluorobenzene 051.41 50.00 103 70 126
Surr: Dibromofluoromethane 052.41 50.00 105 77 121
Surr: Toluene-d8 048.65 50.00 97.3 78.6 119
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 50 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357462
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357462LCS 06/02/2023Volatile Organic Compounds by GC/MS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/02/2023 517929LCS-357462
12225246
1,1-Dichloroethene 2.020.32 20.00 102 71 130
Benzene 1.020.08 20.00 100 78.8 120
Chlorobenzene 1.020.34 20.00 102 80 118
Toluene 1.020.22 20.00 101 76.6 125
Trichloroethene 1.022.20 20.00 111 75.3 127
Surr: 4-Bromofluorobenzene 051.65 50.00 103 70 126
Surr: Dibromofluoromethane 052.00 50.00 104 77 121
Surr: Toluene-d8 049.59 50.00 99.2 78.6 119
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357462MS 06/05/2023Volatile Organic Compounds by GC/MS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/02/2023 518035230552A-002AMS
12227920
1,1-Dichloroethene 2.020.11 20.00 101 69 142
Benzene 1.020.41 20.00 102 71.4 135
Chlorobenzene 1.021.54 20.00 108 77.7 129
Toluene 1.021.65 20.00 108 70.3 136
Trichloroethene 1.023.34 20.00 117 77 134
Surr: 4-Bromofluorobenzene 047.88 50.00 95.8 70 126
Surr: Dibromofluoromethane 051.51 50.00 103 77 121
Surr: Toluene-d8 048.80 50.00 97.6 78.6 119
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357462MSD 06/05/2023Volatile Organic Compounds by GC/MS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/02/2023 518035230552A-002AMSD
12227923
1,1-Dichloroethene 2.018.77 39.220.00 93.8 69 142 20.11 6.89
Benzene 1.019.47 31.620.00 97.4 71.4 135 20.41 4.71
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 51 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357462
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357462MSD 06/05/2023Volatile Organic Compounds by GC/MS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/02/2023 518035230552A-002AMSD
12227923
Chlorobenzene 1.020.61 34.320.00 103 77.7 129 21.54 4.41
Toluene 1.020.51 3220.00 103 70.3 136 21.65 5.41
Trichloroethene 1.022.02 35.320.00 110 77 134 23.34 5.82
Surr: 4-Bromofluorobenzene 047.82 050.00 95.6 70 126 47.88 0
Surr: Dibromofluoromethane 051.91 050.00 104 77 121 51.51 0
Surr: Toluene-d8 049.07 050.00 98.1 78.6 119 48.80 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 52 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357654
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357654MBLK 06/08/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/08/2023 518309MB-357654
12236367
1-Methylnaphthalene 17BRL
2-Methylnaphthalene 17BRL
Acenaphthene 17BRL
Acenaphthylene 33BRL
Anthracene 1.7BRL
Benz(a)anthracene 1.7BRL
Benzo(a)pyrene 1.7BRL
Benzo(b)fluoranthene 3.3BRL
Benzo(g,h,i)perylene 3.3BRL
Benzo(k)fluoranthene 1.7BRL
Chrysene 1.7BRL
Dibenz(a,h)anthracene 3.3BRL
Fluoranthene 3.3BRL
Fluorene 3.3BRL
Indeno(1,2,3-cd)pyrene 1.7BRL
Naphthalene 17BRL
Phenanthrene 1.7BRL
Pyrene 1.7BRL
Surr: 4-Terphenyl-d14 080.67 66.70 121 58.4 135
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357654LCS 06/08/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/08/2023 518309LCS-357654
12236368
1-Methylnaphthalene 1768.28 66.70 102 63 118
2-Methylnaphthalene 1766.14 66.70 99.2 67.4 120
Acenaphthene 1767.85 66.70 102 64.9 120
Acenaphthylene 3367.49 66.70 101 63.8 120
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 53 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357654
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357654LCS 06/08/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 06/08/2023 518309LCS-357654
12236368
Anthracene 1.768.13 66.70 102 66 120
Benz(a)anthracene 1.774.65 66.70 112 63 123
Benzo(a)pyrene 1.768.28 66.70 102 65.9 123
Benzo(b)fluoranthene 3.363.25 66.70 94.8 62 126
Benzo(g,h,i)perylene 3.366.32 66.70 99.4 66.3 123
Benzo(k)fluoranthene 1.781.23 66.70 122 64.5 129
Chrysene 1.774.91 66.70 112 65.9 128
Dibenz(a,h)anthracene 3.364.42 66.70 96.6 68.7 131
Fluoranthene 3.372.18 66.70 108 65.7 130
Fluorene 3.370.75 66.70 106 65 120
Indeno(1,2,3-cd)pyrene 1.757.68 66.70 86.5 66.3 128
Naphthalene 1766.37 66.70 99.5 63.5 120
Phenanthrene 1.773.23 66.70 110 63.4 121
Pyrene 1.771.93 66.70 108 65.3 123
Surr: 4-Terphenyl-d14 070.48 66.70 106 58.4 135
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357654MS 06/08/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/08/2023 5183092306590-003BMS
12236372
1-Methylnaphthalene 0.0190.06260 0.0738 84.8 55.3 122
2-Methylnaphthalene 0.0190.06084 0.0738 82.5 53.2 121
Acenaphthene 0.0190.06342 0.0738 86.0 52.5 121
Acenaphthylene 0.0370.06465 0.0738 87.6 50.4 121
Anthracene 0.00190.06534 0.0738 88.6 56.5 124
Benz(a)anthracene 0.00190.07629 0.0738 103 54.3 129
Benzo(a)pyrene 0.00190.06745 0.0738 0.001505 89.4 53.8 127
Benzo(b)fluoranthene 0.00370.06691 0.0738 0.002463 87.3 51.9 126
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 54 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357654
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357654MS 06/08/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/08/2023 5183092306590-003BMS
12236372
Benzo(g,h,i)perylene 0.00370.06690 0.0738 90.7 53 125
Benzo(k)fluoranthene 0.00190.04823 0.0738 65.4 52.7 128
Chrysene 0.00190.07004 0.0738 0.001673 92.7 57.5 130
Dibenz(a,h)anthracene 0.00370.06411 0.0738 86.9 53.4 128
Fluoranthene 0.00370.07040 0.0738 0.001716 93.1 60.3 131
Fluorene 0.00370.06717 0.0738 91.0 55.7 124
Indeno(1,2,3-cd)pyrene 0.00190.06364 0.0738 0.001417 84.3 54.1 127
Naphthalene 0.0190.05840 0.0738 79.2 53.2 120
Phenanthrene 0.00190.06773 0.0738 91.8 54.9 126
Pyrene 0.00190.06881 0.0738 0.001784 90.9 55.6 129
Surr: 4-Terphenyl-d14 00.06698 0.0738 90.8 58.4 135
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357654MSD 06/08/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/08/2023 5183092306590-003BMSD
12242195
1-Methylnaphthalene 0.0190.07152 26.80.0738 96.9 55.3 122 0.06260 13.3
2-Methylnaphthalene 0.0190.06964 31.10.0738 94.4 53.2 121 0.06084 13.5
Acenaphthene 0.0190.06996 25.80.0738 94.8 52.5 121 0.06342 9.80
Acenaphthylene 0.0370.07161 31.60.0738 97.1 50.4 121 0.06465 10.2
Anthracene 0.00190.07110 270.0738 96.4 56.5 124 0.06534 8.45
Benz(a)anthracene 0.00190.08051 21.30.0738 109 54.3 129 0.07629 5.39
Benzo(a)pyrene 0.00190.07123 26.40.0738 0.001505 94.5 53.8 127 0.06745 5.45
Benzo(b)fluoranthene 0.00370.07213 29.40.0738 0.002463 94.4 51.9 126 0.06691 7.52
Benzo(g,h,i)perylene 0.00370.07299 25.80.0738 98.9 53 125 0.06690 8.70
Benzo(k)fluoranthene 0.00190.05083 320.0738 68.9 52.7 128 0.04823 5.25
Chrysene 0.00190.07490 23.70.0738 0.001673 99.3 57.5 130 0.07004 6.71
Dibenz(a,h)anthracene 0.00370.07076 28.30.0738 95.9 53.4 128 0.06411 9.87
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 55 of 57
14-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
230534A
AEI Consultants
357654
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:357654MSD 06/08/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg-dry 06/08/2023 5183092306590-003BMSD
12242195
Fluoranthene 0.00370.07587 27.20.0738 0.001716 101 60.3 131 0.07040 7.48
Fluorene 0.00370.07310 25.60.0738 99.1 55.7 124 0.06717 8.46
Indeno(1,2,3-cd)pyrene 0.00190.06909 25.40.0738 0.001417 91.7 54.1 127 0.06364 8.21
Naphthalene 0.0190.06825 290.0738 92.5 53.2 120 0.05840 15.6
Phenanthrene 0.00190.07359 26.80.0738 99.7 54.9 126 0.06773 8.30
Pyrene 0.00190.07383 24.40.0738 0.001784 97.7 55.6 129 0.06881 7.03
Surr: 4-Terphenyl-d14 00.07252 00.0738 98.3 58.4 135 0.06698 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 56 of 57
End of Report
Page 57 of 57
June 19, 2023
Analytical Environmental Services, Inc. received samples on
for the analyses presented in following report.
3
“No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in
the report or QC Summary. Additionally, all results for the associated Quality Control samples were within
EPA and/or AES established limits.
AES’ certifications are as follows:
-NELAP/Florida State Laboratory ID E87582 for analysis of Non-Potable Water, Solid & Chemical Materials,
Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/22-06/30/23.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until
12/31/23.
-South Carolina Environmental Laboratory Certification number 98016003 effective until 6/30/23.
These results relate only to the items tested as received. This report may only be reproduced in full and with
written permission from the laboratory.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Project Manager
2306H83
Michael Meares
AEI Consultants
4225 Wade Green Rd
Kennesaw GA 30144
Sunbelt
Shawn Boyd
June 15, 2023 12:00 am
Michael Meares:
Page 1 of 16
Page 2 of 16
Page 3 of 16
19-Jun-23Date:Analytical Environmental Services, Inc
Client:
Case NarrativeSunbelt
AEI Consultants
Lab ID:
Project:
2306H83
Sample Analyses:
Sample 2306H83-002 was analyzed for TCLP Volatiles and all samples for PAH on laboratory created leachate per client request
via email 6/15/23.
Samples were analyzed out of hold per client request via phone 6/15/23 11:04 AM.
Page 4 of 16
Analytical Environmental Services, Inc Date:19-Jun-23
Analyses Dilution
FactorBatchIDUnitsQualReporting
LimitResultMDL
SUMMARY OF ANALYTES DETECTED
2306H83-001
Soil5/30/2023 8:35:00 AM
AB-1:8-9
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 16 5.0H ug/L 358167 10.15
1-Methylnaphthalene 16 5.0H ug/L 358167 10.23
2306H83-002
Soil5/30/2023 8:40:00 AM
AB-1:12-13
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW5030B)VOLATILES, TCLP SW1311/8260D
Chlorobenzene 0.21 0.10H mg/L 358187 200.0058
(SW5030B)Volatile Organic Compounds by GC/MS SW8260D
1,4-Dichlorobenzene 19 100JH ug/L 358187 2011
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 14 5.0H ug/L 358167 10.15
1-Methylnaphthalene 32 5.0H ug/L 358167 10.23
2-Methylnaphthalene 27 5.0H ug/L 358167 10.19
2306H83-003
Soil5/30/2023 10:00:00 AM
AB-4:6-7
Matrix:Collection Date:
Client Sample ID:Lab ID:
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 81 5.0H ug/L 358167 10.15
1-Methylnaphthalene 140 50 ug/L 358167 102.3
2-Methylnaphthalene 200 50 ug/L 358167 101.9
H Holding times for preparation or analysis exceeded
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit Page 5 of 16
2306H83-001
19-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 8:35:00 AM
AB-1:8-9
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 16 5.0H ug/L 358167 1 06/16/2023 17:14 YH0.15
1-Methylnaphthalene 16 5.0H ug/L 358167 1 06/16/2023 17:14 YH0.23
2-Methylnaphthalene BRL 5.0H ug/L 358167 1 06/16/2023 17:14 YH0.19
Surr: 4-Terphenyl-d14 98.7 64.1-136H %REC 358167 1 06/16/2023 17:14 YH0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 6 of 16
2306H83-002
19-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 8:40:00 AM
AB-1:12-13
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW5030B)VOLATILES, TCLP SW1311/8260D
Benzene BRL 0.10H mg/L 358187 20 06/16/2023 13:30 AG0.0053
Chlorobenzene 0.21 0.10H mg/L 358187 20 06/16/2023 13:30 AG0.0058
Surr: 4-Bromofluorobenzene 94.2 78-117H %REC 358187 20 06/16/2023 13:30 AG0
Surr: Dibromofluoromethane 94.5 77.2-124H %REC 358187 20 06/16/2023 13:30 AG0
Surr: Toluene-d8 100 80-120H %REC 358187 20 06/16/2023 13:30 AG0
(SW5030B)Volatile Organic Compounds by GC/MS SW8260D
1,4-Dichlorobenzene 19 100JH ug/L 358187 20 06/16/2023 13:30 AG11
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 14 5.0H ug/L 358167 1 06/16/2023 17:39 YH0.15
1-Methylnaphthalene 32 5.0H ug/L 358167 1 06/16/2023 17:39 YH0.23
2-Methylnaphthalene 27 5.0H ug/L 358167 1 06/16/2023 17:39 YH0.19
Surr: 4-Terphenyl-d14 86.7 64.1-136H %REC 358167 1 06/16/2023 17:39 YH0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 7 of 16
2306H83-003
19-Jun-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Soil
5/30/2023 10:00:00 AM
AB-4:6-7
Matrix:
Collection Date:
Client Sample ID:
Sunbelt
AEI Consultants
Lab ID:
Project Name:
AnalystMDL
(SW3510C)SIM Polynuclear Aromatic Hydrocarbons SW8270E
Naphthalene 81 5.0H ug/L 358167 1 06/16/2023 18:06 YH0.15
1-Methylnaphthalene 140 50 ug/L 358167 10 06/19/2023 16:01 YH2.3
2-Methylnaphthalene 200 50 ug/L 358167 10 06/19/2023 16:01 YH1.9
Surr: 4-Terphenyl-d14 84.9 64.1-136H %REC 358167 1 06/16/2023 18:06 YH0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
F Analyzed in the lab which is a deviation from the method Narr See case narrative Page 8 of 16
SAMPLE/COOLERRECEIPTCHECKLIS
1. ClientName:AESWorkOrderNumber:
2.Carrier:FedExUPSUSPSClientCourierOthe
Yes No N/A Details Comments
3.Shippingcontainer/coolerreceivedingoodcondition?damagedleakingother
4.Custodysealspresentonshippingcontainer?
5.Custodysealsintactonshippingcontainer?
6.Temperatureblankspresent?
7.Coolertemperature(s)withinlimitsof0Ͳ6϶C?[Seeitem13 and 14for
temperature recordings.]
Coolinginitiatedforrecentlycollectedsamples/ice
present
8.ChainofCustody(COC)present?
9.ChainofCustodysigned,dated,andtimedwhenrelinquishedandreceived?
10.Samplernameand/orsignatureonCOC?
11.Wereallsamplesreceivedwithinholdingtime?
12.TATmarkedontheCOC?IfnoTATindicated,proceededwithstandardTATperTerms&Conditions.
13.Cooler1Temperature϶CCooler2Temperature϶CCooler3Temperature϶CCooler4Temperature϶C
Cooler5Temperature϶CCooler6Temperature϶CCooler7Temperature϶CCooler8Temperature϶C
15.Comments:
IcertifythatIhavecompletedsections1Ͳ1ϱ(datedinitials).
Yes No N/A Details Comments
16.Weresamplecontainersintactuponreceipt?
17.Custodysealspresentonsamplecontainers?
18.Custodysealsintactonsamplecontainers?
19.DosamplecontainerlabelsmatchtheCOC?incompleteinfoillegible
nolabelother
20.AreanalysesrequestedindicatedontheCOC?
21. WereallofthesampleslistedontheCOCreceived?samplesreceivedbutnotlistedonCOC
sampleslistedonCOCnotreceived
22.Wasthesamplecollectiondate/timenoted?
23.Didwereceivesufficientsamplevolumeforindicatedanalyses?
24.Weresamplesreceivedinappropriatecontainers?
25.WereVOAsamplesreceivedwithoutheadspace(<1/4"bubble)?
26.Weretripblankssubmitted?listedonCOCnotlistedonCOC
27.Comments:
IcertifythatIhavecompletedsections1ϲͲ27(datedinitials).
Yes No N/A Details Comments
28.Havecontainersneedingchemicalpreservationbeenchecked? *
29.Containersmeetpreservationguidelines?
30.WaspHadjusted at Sample Receipt?
IcertifythatIhavecompletedsections28Ͳ30(datedinitials).
Clear Save as
AEI Consultants 2306H83
2.4
14.
DG 06/01/23
This section only applies to samples where pH can be
checked at Sample Receipt.
CD 06/15/23
* Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
This also excludes metals by EPA 200.7, 200.8 and 245.1 which will be verified between 16 and 24 hours after preservation.CD 06/15/23
LockedChecklist 7.9.20 Rev 3
Page 9 of 16
19-Jun-23Date:Analytical Environmental Services, Inc
Client:
Dates ReportLab Order:
Project Name:
Lab Sample ID Client Sample ID Test NameCollection Date Matrix TCLP Date Prep Date Analysis Date
2306H83
Sunbelt
AEI Consultants
2306H83-001A AB-1:8-9 5/30/2023 8:35:00AM Soil Polynuclear Aromatic Hydrocarbons 6/16/2023 11:45:18 AM 06/16/2023
2306H83-002A AB-1:12-13 5/30/2023 8:40:00AM Soil VOLATILES, TCLP Leached 06/15/2023 6/16/2023 10:45:00 AM 06/16/2023
2306H83-002A AB-1:12-13 5/30/2023 8:40:00AM Soil Volatile Organic Compounds by GC/MS 6/16/2023 10:45:00 AM 06/16/2023
2306H83-002B AB-1:12-13 5/30/2023 8:40:00AM Soil Polynuclear Aromatic Hydrocarbons 6/16/2023 11:45:18 AM 06/16/2023
2306H83-003A AB-4:6-7 5/30/2023 10:00:00AM Soil Polynuclear Aromatic Hydrocarbons 06/19/2023
2306H83-003A AB-4:6-7 5/30/2023 10:00:00AM Soil Polynuclear Aromatic Hydrocarbons 6/16/2023 11:45:18 AM 06/16/2023
2306H83-003A AB-4:6-7 5/30/2023 10:00:00AM Soil Polynuclear Aromatic Hydrocarbons 6/16/2023 11:45:18 AM 06/19/2023
Page 10 of 16
19-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
2306H83
AEI Consultants
358187
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358187MBLK 06/16/2023VOLATILES, TCLP SW1311/8260D
Units:Prep Date:Sample ID:Client ID:Run No:mg/L 06/16/2023 519028MB-358187
12257414
Benzene 0.10BRL
Chlorobenzene 0.10BRL
Surr: 4-Bromofluorobenzene 00.9828 1.000 98.3 78 117
Surr: Dibromofluoromethane 01.012 1.000 101 77.2 124
Surr: Toluene-d8 00.9682 1.000 96.8 80 120
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358187MBLK 06/16/2023Volatile Organic Compounds by GC/MS SW8260D
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/16/2023 519028MB-358187
12257417
1,4-Dichlorobenzene 100BRL
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358187LCS 06/16/2023VOLATILES, TCLP SW1311/8260D
Units:Prep Date:Sample ID:Client ID:Run No:mg/L 06/16/2023 519028LCS-358187
12257138
Benzene 0.100.8150 1.000 81.5 76.4 118
Chlorobenzene 0.100.8766 1.000 87.7 79.4 117
Surr: 4-Bromofluorobenzene 01.005 1.000 100 78 117
Surr: Dibromofluoromethane 00.9118 1.000 91.2 77.2 124
Surr: Toluene-d8 01.048 1.000 105 80 120
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358187MS 06/17/2023VOLATILES, TCLP SW1311/8260D
Units:Prep Date:Sample ID:Client ID:Run No:mg/L 06/16/2023 5190282306F21-001AMS
12259792
Benzene 0.100.9462 1.000 94.6 78.9 124
Chlorobenzene 0.100.9384 1.000 93.8 81.5 122
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 11 of 16
19-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
2306H83
AEI Consultants
358187
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358187MS 06/17/2023VOLATILES, TCLP SW1311/8260D
Units:Prep Date:Sample ID:Client ID:Run No:mg/L 06/16/2023 5190282306F21-001AMS
12259792
Surr: 4-Bromofluorobenzene 00.9980 1.000 99.8 78 117
Surr: Dibromofluoromethane 01.003 1.000 100 77.2 124
Surr: Toluene-d8 00.9392 1.000 93.9 80 120
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358187DUP 06/17/2023VOLATILES, TCLP SW1311/8260D
Units:Prep Date:Sample ID:Client ID:Run No:mg/L 06/16/2023 5190282306F21-001ADUP
12259785
Benzene 0.10BRL 3000
Chlorobenzene 0.10BRL 3000
Surr: 4-Bromofluorobenzene 01.000 01.000 100 78 117 0.9214 0
Surr: Dibromofluoromethane 00.9978 01.000 99.8 77.2 124 0.9392 0
Surr: Toluene-d8 01.019 01.000 102 80 120 0.9998 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 12 of 16
19-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
2306H83
AEI Consultants
358167
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358167MBLK 06/16/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/16/2023 519073MB-358167
12259699
1-Methylnaphthalene 0.50BRL
2-Methylnaphthalene 0.50BRL
Acenaphthene 0.50BRL
Acenaphthylene 1.0BRL
Anthracene 0.050BRL
Benz(a)anthracene 0.050BRL
Benzo(a)pyrene 0.050BRL
Benzo(b)fluoranthene 0.10BRL
Benzo(g,h,i)perylene 0.10BRL
Benzo(k)fluoranthene 0.050BRL
Chrysene 0.050BRL
Dibenz(a,h)anthracene 0.10BRL
Fluoranthene 0.10BRL
Fluorene 0.10BRL
Indeno(1,2,3-cd)pyrene 0.050BRL
Naphthalene 0.50BRL
Phenanthrene 0.050BRL
Pyrene 0.050BRL
Surr: 4-Terphenyl-d14 02.090 2.000 104 64.1 136
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358167LCS 06/16/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/16/2023 519073LCS-358167
12259700
1-Methylnaphthalene 0.502.194 2.000 110 67 126
2-Methylnaphthalene 0.502.098 2.000 105 67.7 121
Acenaphthene 0.502.010 2.000 101 70.3 118
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 13 of 16
19-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
2306H83
AEI Consultants
358167
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358167LCS 06/16/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/16/2023 519073LCS-358167
12259700
Acenaphthylene 1.02.038 2.000 102 70 118
Anthracene 0.0502.054 2.000 103 69.4 126
Benz(a)anthracene 0.0502.280 2.000 114 65.9 126
Benzo(a)pyrene 0.0502.055 2.000 103 70.8 125
Benzo(b)fluoranthene 0.102.012 2.000 101 70.4 125
Benzo(g,h,i)perylene 0.102.369 2.000 118 69.8 128
Benzo(k)fluoranthene 0.0502.301 2.000 115 70 131
Chrysene 0.0502.228 2.000 111 70 131
Dibenz(a,h)anthracene 0.102.024 2.000 101 65.4 132
Fluoranthene 0.102.122 2.000 106 69.7 128
Fluorene 0.102.102 2.000 105 70 123
Indeno(1,2,3-cd)pyrene 0.0502.014 2.000 101 70.1 130
Naphthalene 0.502.073 2.000 104 69.9 121
Phenanthrene 0.0502.150 2.000 108 69.5 123
Pyrene 0.0502.236 2.000 112 71.2 132
Surr: 4-Terphenyl-d14 02.252 2.000 113 64.1 136
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358167MS 06/16/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
AB-4:6-7 Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/16/2023 5190732306H83-003AMS
12259701
Acenaphthene 0.502.797 2.000 8.749 -298 51.7 120 SH
Acenaphthylene 1.02.082 2.000 1.377 35.3 50.3 120 SH
Anthracene 0.0502.042 2.000 102 54.8 119 H
Benz(a)anthracene 0.0502.216 2.000 111 57.1 118 H
Benzo(a)pyrene 0.0502.011 2.000 101 53.1 121 H
Benzo(b)fluoranthene 0.101.963 2.000 98.2 50.2 117 H
Benzo(g,h,i)perylene 0.102.326 2.000 116 48 122 H
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 14 of 16
19-Jun-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORTSunbelt
2306H83
AEI Consultants
358167
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:358167MS 06/16/2023SIM Polynuclear Aromatic Hydrocarbons SW8270E
AB-4:6-7 Units:Prep Date:Sample ID:Client ID:Run No:ug/L 06/16/2023 5190732306H83-003AMS
12259701
Benzo(k)fluoranthene 0.0502.274 2.000 114 53 126 H
Chrysene 0.0502.156 2.000 108 60.2 125 H
Dibenz(a,h)anthracene 0.101.934 2.000 96.7 47.1 130 H
Fluoranthene 0.102.100 2.000 105 63 121 H
Fluorene 0.103.171 2.000 11.18 -401 61.4 120 SH
Indeno(1,2,3-cd)pyrene 0.0501.977 2.000 98.8 51.1 124 H
Phenanthrene 0.0503.546 2.000 14.89 -567 58.3 118 SH
Pyrene 0.0502.251 2.000 0.6111 82.0 53.5 124 H
Surr: 4-Terphenyl-d14 02.113 2.000 106 64.1 136 H
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 15 of 16
End of Report
Page 16 of 16