MO-29963_49049_CA_TCR_20231009_Murphy Oil Tank Closure

Groundwater & Environmental Services, Inc.
104 Corporate Boulevard, Suite 411
West Columbia, SC 29169
T. 866.765.4851

GESonline.com
September 18, 2023
Ron Taraban
NCDEQ – DWM – UST Section – MRO
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115

Re: Murphy Oil 7214
UST Closure Report
721 Leonard Avenue
Albemarle, Stanly County
UST Facility 00-0-0000036740
Dear Mr. Taraban:
Groundwater & Environmental Services, Inc., on behalf of Murphy Oil USA, Inc., is providing the
enclosed UST Closure Report for the referenced site for your review and approval. Should you
have any questions, please do not hesitate to contact the undersigned by phone at (866) 765-
4851 x4523 or by email at [e-mail].

Sincerely,
Groundwater & Environmental Services, Inc.

Daniel Dabkowski
Senior Project Manager

Cc: Ryan Pederson, Murphy Oil USA, Inc. (electronic)
Enclosure
Murphy O il USA, Inc.
UST Closure Report
Murphy USA # 7214
721 Leonard Avenue
Albemarle, N orth Carolina 28001
NCDEQ Facility #00-0-0000036740
September 18, 2023
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001
UST Closure Report
Murphy USA # 7214
721 Leonard Avenue
Albemarle, North Carolina 28001
Prepared for: Murphy Oil USA, Inc.
200 E. Peach Street El Dorado, AR 71731
Prepared by: Groundwater & Environmental Services, Inc. 104 Corporate Boulevard - Suite 411 West Columbia, SC 29169 TEL: [phone] www.gesonline.com
GES Project: 2702015
Date: September 18, 2023
Daniel Dabkowski Senior Project Manager Groundwater & Environmental Services, Inc.
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001
1 Executive Summary
The site is currently inactive, but did operate as Murphy USA #7214, a convenience store and
fueling station with unbranded petroleum fuel. The site is utilized for commercial purposes with
adjoining properties in all cardinal directions also utilized for commercial purposes.
On August 16, 2023, the two (2) underground storage tanks (USTs) and their associated piping
and dispensers were removed from Murphy USA - Store Number 7214 during site construction
activities. A total of twenty-nine (29) soil samples were collected from underneath all product lines,
dispensers, and USTs.
Laboratory analytical results dated August 16, 2023 indicated that the soil sample collected from
underneath piping labeled “Line 6-2” exceeded the Soil-to-Water Maximum Soil Contaminant
Concentration Level (MSCC) of 100 mg/kg for TPH-DRO with a concentration of 243 mg/kg. Soil
collected from piping labeled “Line 4” exceeded the Soil-to-Water MSCC of 0.023 mg/kg for
methylene chloride with a concentration of 0.027 mg/kg. Soil collected from underneath the
southernmost gasoline dispenser on site labeled “Sump 1” exceeded the Soil-to-Water MSCC of
0.12 mg/kg for p-Isopropyltoluene with a concentration of 0.843 mg/kg. No soil samples exceeded
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

Residential MSCCs or Industrial/Commercial MSCCs. A summary of the soil analytical results are
provided in Table 4.

During UST removal perched groundwater was found in the UST pit and a sample was collected.
The perched groundwater sample “GW-1” exhibited an exceedance in the NC 2L standard of 1
ug/L for benzene with a concentration 3.2 ug/L. A summary of the groundwater analytical results
are provided in Table 5.

UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

2 Site Information
2.1 Site Identification
• Date of Report: September 15, 2023
• Facility I.D.: UST Facility ID: 00-0-0000036740
• NCDEQ Incident Number(s): 49049
• Site Name: Murphy USA - Store Number 7412
• Risk Classification: Pending
• Land Use Classification: Commercial
• Address: 721 Leonard Avenue
• Site Location: Albemarle
• State: North Carolina
• County: Stanly
• Latitude: 35.398947° (For Official Use Only)
• Longitude: -81.340375° (For Official Use Only)
2.2 Contact Information Associated with the Release
• Property Owner:
Murphy Oil USA, Inc.
200 E. Peach Street
El Dorado, AR 71731
[phone]
• Mailing Address:
Murphy Oil USA, Inc.
PO Box 7300
El Dorado, AR 71731
[phone]
• Property Occupant:
Murphy Oil USA, Inc.
Store Number 6540
3050 North Main Street
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

Hope Mills, North Carolina
[phone]
• Consultant/Contractor:
Groundwater & Environmental Services, Inc.
104 Corporate Boulevard - Suite 411
West Columbia, SC 29169
[phone]

UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001
2.3 Certification
I, Mike McKeague, P.G., a Professional Geologist of Groundwater & Environmental Services,
Inc., do certify that the information contained in this report is correct and accurate to the best
of my knowledge.
____________________________ Mike McKeague, P.G
P.G. License #2554
Groundwater & Environmental Services of North Carolina, Inc. is licensed to practice geology in
North Carolina. The certification number of the corporation is C-353.
9/18/2023
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

3 Site History and Characterization
Murphy USA - Store Number 7214 is located on a 0.77-acre parcel of land owned by Murphy Oil
USA, Inc. (Murphy) at 721 Leonard Avenue in Albemarle, NC (site). A site location map is provided
as Figure 1. A site map illustrating the site layout with tank and dispenser locations is provided
as Figure 2.
3.1 UST Owner/Operator Information
At the time of closure, the former UST system was owned by Murphy and has reportedly
been owned and operated by Murphy since June 2005. Available UST owner/operator
information is summarized in Table 1.
3.2 UST System Information
Two 20,000-gallon USTs were present at the site, one of which was compartmentalized
into two compartments, with one 12,000-gallon gasoline compartment, and one 8,000-
gallon diesel compartment. The two USTs were located within a common tank hold
generally oriented east-west and located near the northern central perimeter of the site
property. The dimensions of the tank hold were approximately 40-feet by 30-feet. Available
UST system information is summarized in Table 2.
Four (4) dispenser islands are located beneath a dispenser canopy trending northeast to
southwest, with two (2) islands on either side of a centrally located convenience store
building. Double-sided gasoline dispensers are present at each dispenser island along
with a diesel dispenser at the northernmost island. Additionally, a fifth dispenser island
with both gasoline and diesel dispensers is located south of the canopy (uncovered) near
the southern-central portion of the property. Product piping exited the tank hold from the
eastern side and approached the northern dispenser before angling south towards the
remaining dispensers.
3.3 Past Releases
On December 15, 2022, a release of petroleum product occurred during a fuel delivery to
the site UST system. Reportedly, the tanker truck operated by Petroleum Transport
Company (PTC) was in the process of delivering diesel fuel when an overfill occurred
causing a spill of diesel fuel from the tanker truck delivery hose. Diesel fuel was observed
flowing outward from the hose connection to the fill port, overflowing the spill bucket,
contacting concrete ground surface around the spill bucket, and flowing over paved
ground surfaces towards the east. Estimates reported the release to be approximately
300-gallons.
Another release was reported on June 1, 2023, when groundwater analytical data
collected from tank pit observation wells (OW-1 and OW-2) on May 15, 2023 reported
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001
concentrations above 2L Standards for 1,2, Dichloroethane, C9-C18 Aliphatics, and C9-
C22 Aromatics. The reported release was assigned incident #49049 on June 9, 2023.
3.4 Current Facility Status
At the time of assessment, the site facility was inactive and undergoing construction for
raise and rebuild activities to be used as a retail petroleum service station and
a convenience store. An upgraded UST system is planned to be installed at the site.
3.5 Subject Site and surrounding Property Use
The site is located along a primarily commercial corridor of Leonard Avenue and NC State
Highway 24/27. At the time of this assessment, the site was being utilized for commercial
purposes with adjacent properties to the north, south, east, and west also utilized as
commercial properties. Properties outside the immediate vicinity of the site were also
observed to be utilized for commercial uses.
3.6 Regional Geology and Site Hydrogeology
The site is located within the Piedmont Physiographic Province. According to the 1985
“Geologic Map of North Carolina”, the site is underlain by metamorphic rocks of the Floyd
Church Formation described as thin to thick bedded; bedding plane and axial-planar
cleavage common; interbedded with metasandstone, metaconglomerate, and
metavolcanic rock.
Soils encountered during excavation activities consisted primarily of stiff to hard sandy
clay with varying amounts of silt and rock fragments from grade to a depth of
approximately 15-feet below ground surface (BGS), the maximum depth of the excavation.
Perched groundwater was encountered during excavation activities in the UST pit, but it
had no recharge, therefore groundwater is estimated to be located greater than 15-feet
BGS.
Site topography is relatively flat resting at an elevation of approximately 555-feet above
sea level. Regional surface drainage appears to trend towards the west. Surface runoff at
the site flows to the east towards a common centralized storm water detention basin which
is shared with the entire shopping center. Surface runoff from the site and nearby
businesses is routed to the detention basin via sheet flow at which point it enters the basin
via a number of concrete flumes. Water accumulates within the detention basin near the
northwest corner, flows through a berm of gravel (south & east, upgradient sides) and rip
rap (north and west, downgradient sides), and enters a grated concrete outlet box
connected to an underground storm drain system.
During a Geotechnical Exploration performed by United Consulting in October of 2022, a
silty to clayey sand or stiff clay with stiff to hard sandy clay with varying amounts of silt
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

and rock fragments, and clayey elastic silt were encountered to the limit of drilling at 17-ft
BGS. Groundwater was not encountered.
3.7 Receptor Survey
Receptor information is summarized in Table 3. Reportedly, no water supply wells were
identified within a 500-foot radius of the site and properties in the immediate vicinity of the
site are serviced by municipal water. Although a man-made detention basin is located
approximately 400-feet north-northwest of the site, the nearest identified natural surface
water body is Poplin Creek located approximately 1,350-feet west of the site.
During a vehicular reconnaissance windshield survey performed by GES as part of the
UST closure assessment activities, no suspect water supply wells or subsurface structures
(i.e. basements) were observed within a 500-foot radius of the site. GES also performed
a desktop survey by accessing the NCDEQ Source Water Assessment Program mapping
application. According to the application, there are no water supply wells present within
1,500-feet of the site.
Municipal water supplies the site and adjacent properties by the City of Albemarle (PWS
ID NC0184010). The source of municipal water in this area is reported to be surface water
intake from two (2) reservoirs (Narrows/Badin Lake and Tuckertown) located
approximately 6-miles northeast of the site.
4 UST Closure Procedures
In conducting UST removal and assessment activities at the site, the most recent revision of the
NCDEQ “Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
Releases” was utilized for guidance. The following offers further details and provides required
information pertaining to the UST removal activities conducted at the subject facility.
On August 16, 2023, personnel from GES (Mary Arnold) arrived onsite to provide oversight for
the removal, backfill and resurfacing of two 20,000-gallon underground storage tanks, seven
dispenser sumps and the associated UST system piping.
4.1 Preparations for Closure
A “Notice of Intent: UST Permanent Closure or Change-In-Service” form (UST-3) was
completed and submitted to the NCDEQ (refer to Attachment A for a copy of the UST-3
Form). The local municipality (Albemarle) fire marshal was contacted by the UST removal
contractor.
4.2 UST Cleaning and Residual Fluids Disposal
On August 15, 2023, the product lines were blown back to the USTs after removal of the
dispensers. The USTs were evacuated of residual product, cleaned, and rendered inert
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

by A&D Environmental Services of Archdale, NC utilizing a pressure washer and vacuum
truck in tandem. A total of approximately 576-gallons of a product/water mixture,
consisting primarily of rinsate, was removed from the USTs. Refer to Attachment B for
a copy of the disposal manifest. Subsequent to cleaning and prior to removal, the
atmosphere within the USTs was verified inert through the use of an explosive limit meter
under supervision of Robert Wilhoit, the Albemarle Fire Marshal.
4.3 UST System Removal and Disposal
On August 16, 2023 the product piping was exposed for visual assessment. The piping
was observed to be in good condition. Product piping was constructed of fiberglass
reinforced plastic (FRP) with secondary containment of corrugated plastic pipe. Following
inspection, the product piping was removed from the ground. Dispenser sumps were
present, constructed of FRP, and inspected to be in good condition. Dispenser sumps
were removed from the ground with the piping on August 16, 2023.
Between August 16 and August 17, 2023, the cleaned, evacuated, and inert FRP USTs
were removed from the excavation, crushed on-site, loaded, and transported off-site by
Republic Services for disposal. After removal from the ground but prior to destruction, the
tanks were visually inspected and determined to be in good condition. Manifest of tank
disposal is included in Attachment B.
Photographic documentation of the activities is included in Attachment C.
4.4 Excavation Activities
The ground surface above the UST tank hold consisted of concrete. Upon removal of the
concrete, the UST system backfill material was observed to be pea gravel. The
overburden pea gravel material was removed from the tank pit, stockpiled on site, and
screened with a photo-ionization detector (PID). The PID did not indicate elevated
readings (>50,000-parts per billion [ppb]) from the pea gravel material, and the material
was ultimately reused as site backfill. Overburden concrete was loaded, transported, and
disposed of off-site.
The top of the USTs were encountered at approximately 4 to 5-feet BGS and the base of
the USTs were approximately 12 to 13-feet BGS. Depth of the product lines varied
between 2 to 3-feet BGS. Only the amount of material necessary for surgical extraction of
the UST system was excavated. Since the UST system fill material was pea gravel,
minimal soils were generated during system removal.
No significant soil staining or free product was observed within the excavated area. The
final dimensions of the UST excavation were approximately 45-feet by 35-feet. Bedrock
was not encountered during UST system removal activities, and no over-excavation was
performed. The UST void was backfilled with the original pea gravel and material that was
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

excavated from the UST pit and mechanically compacted to no specific compaction
standard.
Murphy USA is awaiting the permit for the new USTs that will be installed on site. Once
the permit has been received, the UST pit will be excavated again to install the new USTs.
Clean fill and pea gravel will used to backfill the void.
5 Site Investigation
GES referred to the most recent revision of the NCDEQ “Guidelines for Site Checks, Tank
Closure, and Initial Response and Abatement for UST Releases” for guidance in completing the
UST closure assessment activities. The following offers further details and provides required
information pertaining to the UST closure assessment activities conducted at the subject facility.
A “Site Investigation Report for Permanent Closure or Change-in-Service of Registered UST”
form (UST-2A) is included as required in Attachment D.
5.1 Soil Sampling Locations and Collection Procedures
All soil samples were collected in accordance with procedures outlined in the NCDEQ
Guidelines for Sampling and GES Standard Operating Procedure (SOP): FM-9.6 Soil
Sampling in Test Pits and Trenches. A copy of this SOP is provided in Attachment E.
Soil samples were collected as required from directly beneath the former UST system
components concurrent with removal. The number of soil samples collected was based
on the specific dimensions of the UST system, as applicable. Soil sample collection was
conducted as follows:
• One sample per 10-linear feet under each UST (8 samples);
• One sample beneath each dispenser (7 samples);
• One sample per 10-linear feet under product lines and at joints (14 samples).
• Two samples were collected for waste profiling purposes from material that was
excavated from the UST pit.
Soil samples were collected no greater than 2-feet into native soil beneath the bottom of
the UST system components. The locations of soil samples collected from the site is
illustrated on Figure 4. Soil samples collected for laboratory analysis were preserved and
packed into laboratory provided sample containers pre-filled with appropriate
preservatives, immediately placed onto wet ice in a cooler maintained at approximately 4-
degrees Celsius, and submitted to Pace Analytical Services, LLC, a North Carolina
certified laboratory, located in Huntersville, NC.
Soil samples collected from the UST pit were taken directly from the bucket of excavating
equipment. Soil samples from beneath the dispensers and product lines were collected
using a new TerraCore sampling kit at each sampling location. All of the soil samples
collected from along the piping and dispensers were collected approximately 4-feet BGS
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

and 5-feet BGS, respectively. The primary soil type encountered was stiff to hard sandy
clay with varying amounts of silt and rock fragments.
On August 16, 2023, soil samples were collected from the bottom of the UST Pit at
approximately 15 feet bgs. The two USTs were removed and a total of eight soil samples
were collected, four samples were collected from along the bottom of each of the former
UST locations.
A portion of each soil sample was placed into a sealable air tight bag with the required
volume for laboratory analysis being placed in laboratory provided bottle-ware. The
bagged sample was allowed time to volatilize and equilibrate at an ambient temperature
of at least 68-degrees Fahrenheit at which point the head-space was screened for the
presence of volatile organic vapors using a photoionization detector (PID). Sample dates,
depths, locations, and the results of the PID screening are included on Table 4.
5.2 Groundwater and Surface Water Sampling Procedures
Perched groundwater was encountered in the excavation pit around the base of the USTs
and a groundwater sample was collected for waste profiling purposes. No natural surface
water bodies were observed within 500-feet of the site; therefore, no surface water
samples were collected during UST closure activities conducted as part of this
assessment. The perched groundwater sample (GW-1) that was collected from the UST
pit was analyzed for VOCs via EPA Method 8260D and TCLP metals by EPA Method
6010.
5.3 Quality Control Measures
Sample handling procedures consisted of placing soil samples into sterilized, laboratory-
provided containers. Each sample was labeled with a unique specific identification number
using indelible ink, including at a minimum the collection date and time and then
transported to the laboratory for analysis under chain-of-custody protocol.
As previously discussed, the stainless-steel hand auger was decontaminated between
sampling locations using a non-phosphate detergent solution followed by a potable water
rinse. For soil samples collected directly from the bucket of heavy excavation equipment,
care was taken to collect samples which were not in direct contact with the excavator
bucket. To reduce the potential of cross contamination, new disposable nitrile gloves were
worn during all phases of sample handling.
As part of GES standard operating procedures, field screening equipment is calibrated
according to the manufacturer’s specification prior to each use. The PID unit was
calibrated to a 100-ppb isobutylene standard along with a fresh air calibration prior to each
day’s use.
Soil samples were collected on August 16, 2023, and were logged into the laboratory on
August 17, 2023. All samples were received by the laboratory within method specified
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

holding times and temperatures (<6°C). No duplicates or trip blanks were utilized for this
assessment. A copy of the chain-of-custody form(s) is located in Attachment F.
5.4 Analytical Methods Used
Soil samples collected beneath the former UST system were laboratory analyzed for Total
Petroleum Hydrocarbons – Gasoline Range Organics (TPH-GRO) and Total Petroleum
Hydrocarbons – Diesel Range Organics (TPH-DRO) by United States Environmental
Protection Agency (EPA) Method 8015, as well as benzene, toluene, ethylbenzene,
xylenes, and naphthalene by EPA Method 8260D. These analytical methods are in
compliance with the previously mentioned NCDEQ guidance.
5.5 Soil Analytical Results
After review of the laboratory analytical report, the following samples were reported with
detections in excess of the NCDEQ Action Levels for TPH-DRO (100 mg/kg), methylene
chloride (0.023 mg/kg), and p-Isopropyltoluene (0.12 mg/kg):
• LINE 6-1 at 243 mg/kg TPH-DRO.
• LINE 4 at 0.027 mg/kg methylene chloride.
• SUMP 1 at 0.843 mg/kg p-Isopropyltoluene.
Soil analytical results for all the other sample locations reported concentrations that were
either below action levels or below laboratory detection limits. A summary of the analytical
data is provided in Table 4 with soil analytical results illustrated on Figure 4. A copy of
the laboratory analytical report is included as Attachment F.
5.6 Groundwater Analytical Results
Laboratory analytical results for the perched groundwater sample (GW-1) collected from
the tank pit reported benzene concentrations at 3.2 ug/L which exceeds the 2L standard
of 1.0 ug/L. There was a detection of ethylbenzene at a concentration of 0.46 J ug/L, which
is below the regulatory limit. All other contaminants of concern were reported to be below
laboratory detection limits. A summary of the groundwater analytical data is provided in
Table 5. A copy of the laboratory analytical report is included as Attachment F.
6 Conclusion
No significant soil staining, free product, or bedrock was encountered during the investigation or
excavation. Laboratory analysis of the soil revealed only small exceedances of NCDEQ action
levels in three of the twenty-nine soil samples collected. GES recommends filing a Notice of
Residual Petroleum for the site followed by public notice.
If you have any questions, please do not hesitate to call Daniel Dabkowski at [phone]
ext. 4523 or via email at [e-mail].
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

Sincerely,
Groundwater and Environmental Services, Inc.

Daniel Dabkowski
Senior Project Manager
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

References

UST Section, Division of Waste Management, Department of Environment and Natural
Resources, May 17, 2021. Guidelines for Site Checks, Tank Closure, and Initial Response and
Abatement. State of North Carolina

UST Section, Division of Waste Management, Department of Environment and Natural
Resources, July 15, 2008 Version, Change 3, Effective December 1, 2013. Guidelines for
Sampling. State of North Carolina

United Consulting (May 10, 2023). Soil and Groundwater Management Plan. Norcross, GA.

Stanly County, (n.d.). Stanly County GIS Data Viewer. Retrieved August 25, 2023 from
https://stanlycounty.maps.arcgis.com/apps/webappviewer/index.html?id=195ae28fc5454875a5c
c60eb8b28bbf6

NCDEQ (n.d.). SWAP Info 2.0. Retrieved September 1, 2023 from
https://ncdenr.maps.arcgis.com/apps/webappviewer/index.html?id=26f4e2b3140f4e58825e487
81ccebf5e

NCDEQ (n.d.). Classifications. Retrieved September 1, 2023 from
https://deq.nc.gov/about/divisions/water-resources/planning/classification-
standards/classifications

North Carolina Geological Survey, 1985, Geologic Map of North Carolina: Raleigh, North
Carolina Department of Natural Resources and Community Development, Geological Survey
Section, scale 1:500,000, in color.
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

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&<Approximate Groundwater Sample
ED Approximate Soil Sample
Storm Sewer Features
Drawn
0 20
Scale In Feet (Approximate)
9/12/23
Soil and GroundwaterAnalytical Results Map
Murphy USA
7214
721 Leonard Avenue
Albemarle, North Carolina
Designed
Approved
Figure
3
DMC
DMC
Date
AW
TPH-GRO = Total Petroleum Hydrocarbons-Gasoline Range Organics
TPH-DRO = Total Petroleum Hydrocarbons-Diesel Range Organics
ND = Analyte was not detected above the reporting limit
NM = Not Measured
All results in mg/kg unless otherwise noted.
LINE 1-1
8/16/2023
2
ND
ND
LINE 1-2
8/16/2023
2
ND
ND
LINE 2
8/16/2023
2
1.9 J
ND
LINE 3
8/16/2023
2
ND
13.4
LINE 5
8/16/2023
2
ND
ND
LINE 6-1
8/16/2023
2
ND
ND
LINE 6-3
8/16/2023
2
ND
23.7
LINE 7-1
8/16/2023
2
ND
4.8 J LINE 7-2
8/16/2023
2
ND
ND
LINE 7-3
8/16/2023
2
ND
NDLINE 8
8/16/2023
2
ND
4.3 J
SUMP 2
8/16/2023
2
ND
17.2
SUMP 3
8/16/2023
2
ND
ND
SUMP 4
8/16/2023
2
ND
ND
SUMP-5
8/16/2023
2
ND
ND
SUMP 6
8/16/2023
2
ND
ND
SUMP 7
8/16/2023
2
ND
ND
UST-1
8/16/2023
NM
ND
ND
UST-2
8/16/2023
NM
ND
ND
UST-3
8/16/2023
NM
ND
ND
UST-4
8/16/2023
NM
ND
ND
UST-5
8/16/2023
NM
ND
ND
UST-6
8/16/2023
NM
ND
ND
UST-7
8/16/2023
NM
ND
ND
UST-8
8/16/2023
NM
ND
ND
NEW BUILD
8/16/2023
2
ND
ND
LINE 6-2
8/16/2023
2
ND
243
Soil Chemical of Concern →TPH-GRO TPH-DRO
p-Isopropyltoluene
(p-cymene)
Methylene
Chloride
Action Level 50 100 --------
Soil-to-Water MSCCs --------0.12 0.023
Residential MSCCs --------1,560 93.8
Industrial/Commercial MSCCs --------23,300 1,400
Location
Date
Depth (ft BGS)
TPH-GRO
TPH-DRO
p-Isopropyltoluene
(p-cymene)
Methylene Chloride
2L
Standard GCL
1 5,000 µg/l 3.2
Date 8/16/2023
Benzene
Sample ID GW-1
Location SUMP 1
Date 8/16/2023
Depth (ft BGS)2
TPH-GRO 3.2 J
TPH-DRO ND
p-Isopropyltoluene
(p-cymene)0.843
Methylene Chloride ND
Location LINE 4
Date 8/16/2023
Depth (ft BGS)2
TPH-GRO ND
TPH-DRO ND
p-Isopropyltoluene
(p-cymene)ND
Methylene Chloride 0.0270
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

Tables

UST Closure Report
Murphy USA #7214
721 Leonard Avenue, Albemarle, NC
UST ID Number 1, 2A, 2B Facility ID Number 00-0-0000036740
City State Zip Telephone Number
City State Zip Telephone Number
Incident Number None Date Incident Occurred N/A
Date Incident Report N/A
Date Incident Closed N/A
City State Zip Telephone Number
N/A N/A N/A N/A
*Regulatory and owner installation dates differ; the earlier date is shown (regulatory).
Street Address
Name of Operator
N/A
Street Address
Name of Other Responsible Party
N/A
Other Incidents Onsite or Commingled/In Close Proximity
Dates of Operation* (MM/DD/YY to MM/DD/YY)
Murphy Oil USA, Inc.06/02/2005 to Present
Street Address
TABLE 1
SITE HISTORY - UST OWNER / OPERATOR & OTHER RESPONSIBLE PARTY INFORMATION
Name of Owner Dates of Operation* (MM/DD/YY to MM/DD/YY)
Murphy Oil USA, Inc.06/02/2005 to 05/2023
Privileged and Confidential Page 1 of 5
UST Closure Report
Murphy USA #7214
721 Leonard Avenue, Albemarle, NC
UST ID Number
Current/Last
Contents Previous Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
(feet)
Description of
Pumps
Date Tank
Installed*
Status of
UST
Was Release
Associated with
the UST System?
1 Gasoline (Regular)N/A 20,000 DW FRP Unknown DW UPP/Pressure 06/02/2005 Active No
2A Gasoline N/A 12,000 DW FRP Unknown DW UPP/Pressure 06/02/2005 Active No
2B Diesel N/A 8,000 DW FRP Unknown DW UPP/Pressure 06/02/2005 Active Yes
AST ID Number
Current/Last
Contents Previous Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions Pumps
Date Tank
Installed
Status of
AST
Associated with
the AST System?
Number Material Released Date of Release
49049 Diesel 6/1/2023
Notes:
SW = Single Wall
FRP = Fiberglass Reinforced Plastic
*Regulatory and owner installation dates differ; the earlier date is shown (regulatory).
Descrtiption of Release
Groundwater samples collected from tank pit observation wells (OW-1 and OW-2) on 05/15/23 reported
concentrations above 2L Standards for 1,2, Dichloroethane, C9-C18 Aliphatics, and C9-C22 Aromatics.
Privileged and Confidential Page 2 of 5
UST Closure Report
Murphy USA #7214
721 Leonard Ave, Albemarle, NC
Lat / Lon
(decimal degrees)Distance (ft)Direction
35.342022
-80.176519
35.342075
-80.180786
Total Depth Casing Depth Screen Interval
(ft BGS)(ft BGS)(ft BGS)
WSW = Water Supply Well SWB = Surface Water Body BGS = Below Ground Surface
Table 3
Receptor Information
Receptor
Type Contact / Phone / Email Receptor Location Receptor Description & Location Details Up or Down
Gradient
Detention
Basin Unknown North-Northwest 400 North-Northwest Unknown
SWB Unknown West 1,350 West Unknown
Public Water Supply Status Current Use Status Access Drilling Method /
Well Type
N/A
Privileged and Confidential Page 3 of 5
LSA Report
Murphy Express #8572
1670 N Howe St, Southport, NC 28461
ID Date
PID
(ppm)(ft BGS)
LINE 1-1 8/16/2023 0.0 2 ND ND ND ND 0.005 ND ND ND ND 0.0033 J ND 0.0048 ND ND ND ND ND ND ND ND 0.0218 0.0088 0.0105
LINE 1-2 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
LINE 2 8/16/2023 0.0 2 1.9 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
LINE 3 8/16/2023 0.0 2 ND 13.4 ND ND ND ND ND ND ND 0.0022 J ND ND ND ND ND ND ND ND ND 0.0037 J ND ND ND
LINE 4 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.0270 ND ND ND ND ND ND ND ND ND
LINE 5 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
LINE 6-1 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.0185 ND ND ND ND ND ND ND ND ND
LINE 6-2 8/16/2023 0.0 2 ND 243 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
LINE 6-3 8/16/2023 0.0 2 ND 23.7 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
LINE 7-1 8/16/2023 0.0 2 ND 4.8 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
LINE 7-2 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.0136 J ND ND ND ND ND ND ND ND ND
LINE 7-3 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
LINE 8 8/16/2023 0.0 2 ND 4.3 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
SUMP 1 8/16/2023 0.0 2 3.2 J ND ND ND 0.587 ND 0.0687 ND ND ND ND 0.843 ND ND 0.627 ND ND 0.220 ND ND 5.740 2.350 0.0189
SUMP 2 8/16/2023 0.0 2 ND 17.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
SUMP 3 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
SUMP 4 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
SUMP-5 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
SUMP 6 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
SUMP 7 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
UST-1 8/16/2023 0.2 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
UST-2 8/16/2023 0.0 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
UST-3 8/16/2023 0.4 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
UST-4 8/16/2023 0.3 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
UST-5 8/16/2023 0.3 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
UST-6 8/16/2023 0.5 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
UST-7 8/16/2023 0.7 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.0025 J ND
UST-8 8/16/2023 0.4 15 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
WASTE 1 8/16/2023 0.2 NM ND ND NA ND NA NA NA ND NA ND NA NA NA NA NA NA NA NA NA ND NA NA ND
WASTE 2 8/16/2023 0.4 NM ND ND NA ND NA NA NA ND NA ND NA NA NA NA NA NA NA NA NA ND NA NA ND
NEW BUILD 8/16/2023 0.0 2 ND ND ND ND ND ND ND ND ND 0.0017 J ND ND ND ND ND ND ND ND ND 0.0028 ND ND 0.0019 J
NOTES:
Units are milligrams per kilogram (mg/kg = ppm) unless otherwise noted
Bold typeface indicates concentration is greater than action level
MSCCs = Maximum Soil Contaminant Concentration Levels
BGS = Below Ground Surface
TPH-GRO = Total Petroleum Hydrocarbons-Gasoline Range Organics
TPH-DRO = Total Petroleum Hydrocarbons-Diesel Range Organics
ND = Analyte was not detected above the reporting limit
NM = Not Measured
NA = Not Analyzed
J = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
Analytes not shown were below laboratory reporting limits in all samples; refer to the laboratory report for additional information
Table 4
Summary of Soil Analytical Results
Analytical Method →EPA 8015C EPA 8260D
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Chemical of Concern →
TP
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Privileged and Confidential Page 4 of 5
Murphy Express #7214
721 Leonard Avenue, Albemarle, NC 28001
504.1 6010 625.1
Sample ID Date
OW-1 5/15/2023 <50 U 1810 5280 <86 U <1.2 U <0.27 U <0.20 U 0.54 <0.28 U <0.13 U <0.080 U 0.26 0.10 U <0.29 U 0.45 <0.16 U 7.3 J
OW-2 5/15/2023 <50 U 1940 5490 <86 U <1.2 U <0.27 U <0.20 U <0.12 U <0.28 U <0.13 U <0.080 U <0.068 U 0.10 U <0.29 U <0.17 U <0.16 U <3.7
GW-1 8/16/2023 NA NA NA NA NA 3.2 0.46J NA NA NA NA NA NA <0.48 NA <0.34 NA <21
NOTES:
Units are micrograms per liter (ug/L = parts per billion) unless otherwise noted
Italic typface indicates the analyte was not detected, but the detection limit exceeds the regulatory limit.
GCL = Gross Contaminant Level
J = Estimated value between the method detection limit and laboratory reporting limit.
U = Not detected
COC = Contaminant of Concern
C9-C18 Aliphatics is the sum of C9-C12 VPH and C9-C18 EPH.
C9-C22 Aromatics in the sum of C9-C10 VPH and C11-C22 EPH.
Analytes not shown were below detection limits; refer to the laboratory report for additional information.
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GCL
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Table 5
Summary of Water Analytical Results
Analytical Method →MADEP VPH/EPH Rev 2.1 Standard Methods 6200
COC →
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Privileged and Confidential Page 5 of 5
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

Attachment A – Notice of Intent: UST Permanent Closure or Change-In-Service (Form UST-3)

UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

Attachment B – Disposal Manifests / Certificates of Disposal

UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

Attachment C – Photographic Documentation

Attachment C – Photographic Documentation MUSA #7214 – UST Closure Report

Date: 08/16/2023
Location: MUSA #7214
721 Leonard Avenue
Albemarle, NC 28001
northwest from the site
entrance along Leonard
Ave. View of the UST
excavation area while the
remainder of the concrete
pad is being removed.

Photograph 2
721 Leonard Avenue
Albemarle, NC 28001
of the site facing north,
taken from site entrance
along the south that
borders the Wal-Mart
parking lot.

Attachment C – Photographic Documentation MUSA #7214 – UST Closure Report

Photograph 3
721 Leonard Avenue
Albemarle, NC 28001
southernmost dispenser
sumps. The sump
pictured on the left was
for gasoline, and the one
on the right was for
diesel.

Photograph 4
721 Leonard Avenue
Albemarle, NC 28001
gasoline dispenser sump.

Attachment C – Photographic Documentation MUSA #7214 – UST Closure Report

Photograph 5
721 Leonard Avenue
Albemarle, NC 28001
remainder of concrete
pad being removed from
UST pit. Also pictured,
the three northernmost
dispenser sumps before
removal.

Photograph 6
721 Leonard Avenue
Albemarle, NC 28001
northwest, dispenser
sumps and associated
piping after removal. Test
pits were excavated out
to a maximum depth of 2
ft into native soils.

Attachment C – Photographic Documentation MUSA #7214 – UST Closure Report

Photograph 7
721 Leonard Avenue
Albemarle, NC 28001
groundwater uncovered
during UST
excavation/removal
activities. A sample was
collected (GW-1) for
waste profiling purposes.

Photograph 8
721 Leonard Avenue
Albemarle, NC 28001
view of the tops of the
USTs after being
uncovered at
approximately 4.5-feet
bgs.

Attachment C – Photographic Documentation MUSA #7214 – UST Closure Report

Photograph 9
721 Leonard Avenue
Albemarle, NC 28001
southeast, view of the
southernmost UST being
removed.

Photograph 10
721 Leonard Avenue
Albemarle, NC 28001
southeast, view of the
bottom of the first UST
that was removed.

Attachment C – Photographic Documentation MUSA #7214 – UST Closure Report

Photograph 11
721 Leonard Avenue
Albemarle, NC 28001
southwest, view of the of
the second UST that was
removed.

Photograph 12
721 Leonard Avenue
Albemarle, NC 28001
view UST pit after both
USTs were removed.

UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

Attachment D – Site Investigation Report for Permanent Closure or Change-in-Service of
Registered UST (Form UST-2A)

UST-2A Site Investigation Report for Permanent Closure or Change-in
Service of
NC DEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING
phone [phone] fax [phone] http://www.wastenotnc.org/
STATE USE ONLY:
INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where a UST system will be converted from storing a regulated substance to a non-III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator mu
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-2B
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS

III. CONTACT PERSONNEL

IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
UNREGISTERED USTs use Form UST-2B V. EXCAVATION CONDITION

VI. CERTIFICATION

Murphy Oil USA, Inc.
200 Peach Street, PO Box 7300
El Dorado Union
AR 71731
870-875-6411
Murphy USA #7214
00-0-0000036740
721 Leonard Avenue
Albemarle 28001Stanly
704-984-6236
Ryan Pederson Environmental Risk Ma 303-817-9262
homas Chmura Groundwater & Environmental Services, Inc.104 Corporate Blvd., Sui 866-765-4851 x4520
1 20,000 Gasoline (REMOVED 08/16/2023 ■■■
2A 12,000 Gasoline 08/16/2023 ■■■
2B 8,000 Diesel 08/16/2023 ■■■
REMOVED
REMOVED
Print name and official title of owner or owner’s authorized representative
Mike McKeague, PG# 2554 (NC)/Sr. Hydrogeologist
9/18/2023
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001
Attachment E – GES Standard Operating Procedure (SOP): FM-9.6 Soil Sampling in Test Pits and Trenches
Standard Operating Procedure Section: FM-9.6
Revision #: 003
Date: 09/01/2016
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 1 of 8
Title: Soil Sampling in Test Pits and Trenches
1. Purpose/Scope
This guideline describes the method for logging and sampling of test pits and trenches to
determine subsurface soil and rock conditions and recover small-volume or bulk samples.
The methods apply only to data collection and not to the construction of excavations.
The guideline is applicable to the collection of bulk and small-volume samples of subsurface
soils for laboratory testing at sites where exposure to hazardous substances may occur.
Nobody is permitted to enter an excavation greater than four feet in depth or an excavation
that contains standing water without an approved work and health and safety plan and
required permitting.
2. References
GES SOP FM 9.1: Soil Sampling for Analysis
GES SOP FM 13.2: Sample Preservation
GES SOP FM 13.3: Sample Identification
GES SOP FM 13.4: Chain-of-Custody
GES SOP FM 13.5: Sample Packaging and Shipping
GES SOP HS 1.11: Excavation and Trenching
Occupational Safety and Health Administration, 1979:29 CFR 1926.650-653.
3. Equipment/Materials
The following equipment is needed for taking samples for chemical or geotechnical analysis
from test pits and trenches:
x A site-specific health and safety plan and excavation plan.
x Backhoe or other excavating machinery
x Shovels, picks and hand augers, stainless steel trowels
Standard Operating Procedure Section: FM-9.6
Revision #: 003
Date: 09/01/2016
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 2 of 8
x Sample container (bucket with locking lid for large samples and glass bottles for chemical
or geotechnical analysis samples.
x Polyethylene bags for enclosing sample; buckets
x Remote sampler consisting of 10-foot sections of steel conduit (1-inch diameter), hose
clamps and right angle adapter for conduit (See Attachment B).
x Field notebook
x Photoionization detector (PID)
x Combustible gas meter
x Camera
4. Procedure
A private utility mark-out company should be contracted prior to performing subsurface
activities so that the approximate location of any potential subsurface utility line is identified
near the areas to be excavated. This is in addition to the state required one-call notice. Site
features may warrant a site walk prior to identify potential subsurface hazards. For any utility
line which is identified, a “soft-dig” contractor should be utilized to verify the location and
depth of the lines as well as the size and type of line.
Also, prior to excavation, the site-specific health and safety plan will need reviewed. The
plan should address known and/or potential excavation and trench hazards, air monitoring
requirements, potential flash fire hazards (high concentrations of volatiles and sparking via
equipment or rock ripping) and mitigating actions.
4.1 Data Collection and Sampling
4.1.1 General
Test pits and trenches are usually logged as they are excavated. Records of each test
pit/trench will be made on prepared forms or in a field notebook. These records include plan
and profile sketches of the test pit/trench showing materials encountered, their depth and
distribution in the pit/trench, and sample locations. These records will also include sample
screening information.
General test pit/trench log forms are shown in Attachments A-1 and A-2. This suggested
format is useful because it provides all necessary sampling, monitoring and subsurface
records for each pit or trench in a concise and uniform manner. This format also provides a
cross-check with chain-of-custody records and sample labels. In completing a record of the
trench profile (Attachment A-2), sketch the profile of each wall on the same form (or use
Standard Operating Procedure Section: FM-9.6
Revision #: 003
Date: 09/01/2016
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 3 of 8
two forms) when there are significant differences in the two trench walls. Requirements for
sampling should be determined by the scope of work and work order. Field personnel should
have sufficient tools and equipment to sample each pit. The tools and equipment must be
properly decontaminated prior to use.
Entry of test pits by personnel is extremely dangerous and should be avoided unless
absolutely necessary. Pits more than four feet deep must be shored prior to entry, the
“buddy” system must be used, and all applicable H&S and OSHA requirements should be
followed (see Section 5.1.3).
The final depth and type of samples obtained from each test pit will be determined at the
time the test pit is excavated. Sufficient samples are usually obtained and analyzed to
quantify contaminant distribution as a function of depth for each test pit. Additional samples
of each waste phase and any fluids encountered in each test pit may be collected.
In some cases, samples of soil may be extracted from the test pit for reasons other than
waste sampling and chemical analysis, such as to obtain geotechnical information.
4.2 Sampling Methods
The methods discussed in this section refer to test pit sampling from grade level. If test pit
entry is required, see Section 5.1.3.
1. Excavate trench or pit in several depth increments. After each increment the operator
will wait while the sampler inspects the test pit from grade level to decide if conditions
are appropriate for sampling. Monitoring of background air with a PID may be necessary.
Practical depth increments range from 2 to 4 feet.
2. The backhoe operator, who will have the best view of the test pit, will immediately cease
digging if:
x Any fluid phase or groundwater seepage is encountered in the test pit,
x Any drums, other potential waste containers, obstructions or un-marked utility lines are
encountered, or
x Distinct changes of material are encountered.
This action is necessary to permit proper sampling of the test pit and to prevent a breach
of safety protocol. Depending upon the conditions encountered, it may be necessary to
excavate more slowly and carefully with the backhoe.
3. Remove loose material to the greatest extent possible with backhoe.
4. Secure walls of pit if necessary (refer to SOP HS-1.11). There is seldom any need to
enter a pit or trench which would justify the expense of shoring the walls. All observations
and samples can generally be taken from the ground surface.
Standard Operating Procedure Section: FM-9.6
Revision #: 003
Date: 09/01/2016
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 4 of 8
5. Samples can be obtained from the backhoe bucket. The sampler or Field Operations
Leader directs the backhoe operator to remove material from the selected depth or
location within the test pit/trench. The bucket is brought to the surface and moved away
from the pit. The sampler and/or HSO then approaches the bucket and monitors its
contents with a PID or organic vapor meter (OVM) meter. If granular or loose soils and/or
uniform materials are encountered, the sample can be obtained directly from the bucket.
The sample is collected from the center of the bucket and placed in sample jars using a
clean stainless steel trowel or spatula.
If a composite sample is desired, several depths or locations within the pit/trench are
selected and a bucket is filled from each area. It is preferable to send individual sample
bottles filled from each bucket to the laboratory for compositing under more controlled
laboratory conditions. However, if compositing in the field is required, each sample bottle
should be emptied into a mixing container (e.g., a stainless steel bucket) and thoroughly
stirred prior to being placed into the sample jars. Composite sampling is not appropriate
for samples which will undergo analysis for volatile organic compounds.
6. Using the remote sampler shown in Attachment B, samples can be taken at the desired
depth from the side wall or bottom of the pit. The face of the pit/trench should first be
scraped (using a long-handled shovel or hoe) to remove the smeared zone that has
contacted the backhoe bucket. The sample is then collected directly into the sample jar
by scraping with the jar edge, eliminating the need to utilize samplers and minimizing the
likelihood of cross-contamination. The sample jar can be capped, removed from the
assembly, and packaged for shipment.
7. Prepare shipping papers, labels, and chain-of-custody records in accordance with SOPs
FM-13.1, and FM-13.3–13.5. Preserve samples as described in SOP FM-13.2.
4.2.1 In-Pit Sampling
Samples can also be obtained by personnel entering the test pit/trench. This is necessary
when soil conditions preclude obtaining suitable samples from the backhoe bucket (e.g.,
excessive mixing of soils or wastes within the test pit/trench) or when samples from relatively
small discrete zones within the test pit are required. This approach may also be necessary
to sample any seepage occurring at discrete levels or zones in the test pit that are not
accessible with remote samplers.
In general, personnel should sample and log pits and trenches from the ground surface,
except as provided for by the following criteria:
x The project will benefit significantly from the improved quality of the logging and sampling
data obtained if personnel enter a pit or trench rather than conduct such operations from
the ground surface.
Standard Operating Procedure Section: FM-9.6
Revision #: 003
Date: 09/01/2016
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 5 of 8
x There is no practical alternative means of obtaining such data.
x The Site Health & Safety Officer determines that such action can be accomplished
without breaching site safety protocol. This determination will be based on actual
monitoring of the pit/trench after it is dug (including, at a minimum, measurements of
volatile organics, explosive gases and available oxygen).
x An experienced geotechnical professional determines that the pit/trench is stable or is
made stable prior to entrance of any personnel (by grading the sidewalls or using
shoring). OSHA requirements must be strictly implemented.
If these conditions are satisfied, one person will enter the pit/trench. On potentially
hazardous waste sites, this individual will be dressed in safety gear as required by the
conditions in the pit. He will be affixed to a safety rope and continuously monitored while in
the pit. Procedures described in SOPs HS-1.9 and HS-1.11 must be followed, as
appropriate.
A second individual will be fully dressed in protective clothing, including a self-contained
breathing device, and on standby during all pit entry operations. The individual entering the
pit will remain therein for as brief a period as practical, commensurate with performance of
his work. After removing the smeared zone, samples are obtained with a clean trowel or
spoon.
As an added precaution, it is advisable to keep the backhoe bucket in the test pit when
personnel are working below grade. Such personnel can either stand in or near the bucket
while performing sampling operations. In the event of a cave-in they can either be lifted clear
in the bucket, or at least climb up on the backhoe arm to reach safety.
4.2.2 Geotechnical Sampling
In addition to the equipment described in Section 4.0, the following equipment is needed for
geotechnical sampling:
x Soil sampling equipment, similar to that used in shallow drilled borings (i.e., open tube
samplers), which can be pushed or driven into the floor of the test pit.
x Suitable driving (e.g., a sledge hammer) or pushing (e.g., the backhoe bucket)
equipment which is used to advance the sampler into the soil.
x Knives, spatulas, and other suitable devices for trimming hand-carved samples.
x Suitable containers (bags, jars, tubes, boxes, etc.), labels, wax, etc. for holding and
safely transporting collected soil samples.
x Geotechnical equipment (pocket penetrometer, torvane, etc.) for field testing collected
soil samples for classification and strength properties.
Standard Operating Procedure Section: FM-9.6
Revision #: 003
Date: 09/01/2016
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 6 of 8
Disturbed grab or bulk geotechnical soil samples may be collected for most soils in the same
manner as comparable soil samples for chemical analysis (see Sections 5.1.2 and 5.1.3).
These collected samples may be stored in jars or plastic-lined sacks (larger samples), which
will preserve their moisture content. Smaller samples of this type are usually tested for their
index properties, to aid in soil identification and classification, while larger bulk samples are
usually required to perform compaction tests.
Relatively undisturbed samples are usually extracted in cohesive soils using open tube
samplers, and such samples are then tested in a geotechnical laboratory for their strength,
permeability and/or compressibility. The techniques for extracting and preserving such
samples are similar to those used in performing Shelby tube sampling in borings (see SOP
FM-9.1), except the sampler is advanced by hand or backhoe, rather than a drill rig. Also,
the sampler may be extracted from the test pit by excavation around the sampler when it is
difficult to pull it out of the ground. If this excavation requires entry of the test pit, the
requirements described in Section 5.1.3 must be followed. The open tube sampler should
be pushed or driven vertically at a steady rate into the floor or steps excavated in the test pit
at the desired sampling elevations. Extracting tube samples horizontally from the walls of
the test pit is not appropriate, because the sample will not have the correct orientation.
A backhoe may be used to drive or push the sampler or tube into the ground. Place a piece
of wood over the top of the sampler or sampling tube to prevent damage during
driving/pushing of the sample. Pushing the sampler with a constant thrust is always
preferable to driving it with repeated blows, to minimize disturbance to the sample. If the
sample cannot be extracted by rotating it at least two revolutions (to shear off the sample at
the bottom), hand excavation to remove the soil from around the sides of the sampler and
slice off the sample at its bottom may be required. Again, if this requires entry of the test pit,
the requirements in Section 5.1.3 must be followed. Prepare, label, pack and transport the
sample in the required manner, as described in SOP FM-13.5.
Hand-carved block samples are extracted in a similar manner to open tube samples, except
that the sampling container (usually a large tube or box with no top or bottom) is not used to
cut the sample. Instead, the surrounding sections of the test pit floor are carved away by
hand to leave a sample slightly smaller in plan dimensions than the container, with the
sample remaining connected to the test pit floor at its bottom. The container is slipped over
the sample, and the annular space and top of the sample is covered with melted wax. The
bottom of the sample is then sliced away from the test pit floor, the container is inverted,
about 1/2 inch of soil removed, and the space filled with melted wax. Caps are then installed,
taped, and dipped in hot wax for each end of the container, and the block sample is labeled
and shipped in the same manner as a tube sample.
Because the above method requires entering the test pit, it will be necessary to adhere to all
appropriate Health and Safety procedures for doing so.
Standard Operating Procedure Section: FM-9.6
Revision #: 003
Date: 09/01/2016
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 7 of 8
5. Records
The following information is to be recorded on the test pit/trench log form and in the field
notebook:
x Name, work assignment number and location of job
x Date of digging or trenching
x Surface elevation
x Depth, surface area and orientation of pit or trench
x Sample numbers
x Method of taking samples, type and size of samples
x Approximate water levels after stabilization (if below the water table), and location and
depth of any seeps
x Description of soil
x Other pertinent information, such as PID readings, weather conditions, etc.
x List of photographs
x Name of contractor, backhoe (or other equipment) operator and sampler
x Date and type of backfill
Standard Operating Procedure Section: FM-9.6
Revision #: 003
Date: 09/01/2016
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 8 of 8
Attachments
Attachment A-1 – Test Pit Record
Attachment A-2 – Test Pit/Trench Profile
Attachment B – Remote Sampling/Sample Holder for Test Pit/Trench
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 1 of 2
Attachment A-1 – Test Pit Record
Test Pit Date
Time Start Time End
Coordinates Grid Element
Sketch map of test pit site, showing surface monitoring
results Crew Members
1
2
3
4
5
6
Monitor Equipment
PID
Explosive Gas
Available Oxygen
OVM
Camera
Other
Record winds
N
Scale 1” = ________ feet
Notes
Site
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Pits and Trenches Page 2 of 2
Attachment A-2 – Test Pit/Trench Profile
TEST PIT RECORD: PROFILE ALONG TEST PIT
Site
Depth (ft) Scale 1” = feet
SAMPLES OBTAINED
Notes No.Depth (ft)Init. Ser. No.HD SP VOA
(ppm)
S-1
S-2
S-3
S-4
S-5
S-6
S-7
S-8
Reference: Field Book, P.G.
Signature Attachments
STANDARD OPERATING PROCEDURE:Soil Sampling in Test Puts and Trenches Page 1 of 1
Attachment B – Remote Sampling/Sample Holder for Test Pit/Trench
Figure 1 – Remote Sample Holder for Test Pit/Trench Sampling
UST Closure Report Murphy USA # 7214 721 Leonard Avenue
Albemarle, North Carolina 28001

Attachment F – Laboratory Analytical Report & Chain-of-Custody Documentation

#=CL#
August 22, 2023
LIMS USE: FR - DANIEL DABKOWSKI
LIMS OBJECT ID: 92683348
92683348
Project:
Pace Project No.:
RE:
Mr. Daniel Dabkowski
Groundwater & Environmental Services, Inc.
104 Corporate Blvd.
Suite 411
West Columbia, SC 29169
MUSA #7214 ALBEMARLE, NC
Dear Mr. Dabkowski:
Enclosed are the analytical results for sample(s) received by the laboratory on August 17, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
cc:SouthwestPR, GES-SC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 104
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 104
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Lab ID Sample ID Matrix Date Collected Date Received
92683348001 SUMP 1 Solid 08/16/23 10:00 08/17/23 13:50
92683348002 LINE 1-1 Solid 08/16/23 10:15 08/17/23 13:50
92683348003 LINE 1-2 Solid 08/16/23 10:30 08/17/23 13:50
92683348004 SUMP 3 Solid 08/16/23 11:00 08/17/23 13:50
92683348005 LINE 2 Solid 08/16/23 12:15 08/17/23 13:50
92683348006 SUMP 4 Solid 08/16/23 12:45 08/17/23 13:50
92683348007 NEW BUILD Solid 08/16/23 13:40 08/17/23 13:50
92683348008 LINE 3 Solid 08/16/23 14:20 08/17/23 13:50
92683348009 UST-1 Solid 08/16/23 14:30 08/17/23 13:50
92683348010 UST-2 Solid 08/16/23 14:35 08/17/23 13:50
92683348011 UST-3 Solid 08/16/23 14:40 08/17/23 13:50
92683348012 UST-4 Solid 08/16/23 14:45 08/17/23 13:50
92683348013 UST-5 Solid 08/16/23 15:25 08/17/23 13:50
92683348014 UST-6 Solid 08/16/23 15:30 08/17/23 13:50
92683348015 UST-7 Solid 08/16/23 15:40 08/17/23 13:50
92683348016 UST-8 Solid 08/16/23 15:45 08/17/23 13:50
92683348017 SUMP 5 Solid 08/16/23 16:00 08/17/23 13:50
92683348018 SUMP 2 Solid 08/16/23 16:30 08/17/23 13:50
92683348019 LINE 4 Solid 08/16/23 17:00 08/17/23 13:50
92683348020 SUMP 6 Solid 08/16/23 17:15 08/17/23 13:50
92683348021 SUMP 7 Solid 08/16/23 17:30 08/17/23 13:50
92683348022 LINE 5 Solid 08/16/23 17:45 08/17/23 13:50
92683348023 LINE 6-1 Solid 08/16/23 18:15 08/17/23 13:50
92683348024 LINE 6-2 Solid 08/16/23 18:30 08/17/23 13:50
92683348025 LINE 7-1 Solid 08/16/23 18:40 08/17/23 13:50
92683348026 LINE 7-2 Solid 08/16/23 18:55 08/17/23 13:50
92683348027 LINE 7-3 Solid 08/16/23 19:05 08/17/23 13:50
92683348028 LINE 8 Solid 08/16/23 19:20 08/17/23 13:50
92683348029 LINE 6-3 Solid 08/16/23 19:50 08/17/23 13:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 104
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92683348001 SUMP 1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348002 LINE 1-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348003 LINE 1-2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348004 SUMP 3 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348005 LINE 2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348006 SUMP 4 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348007 NEW BUILD EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348008 LINE 3 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348009 UST-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348010 UST-2 EPA 8015C 2 PASI-CHH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 104
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348011 UST-3 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348012 UST-4 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348013 UST-5 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348014 UST-6 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348015 UST-7 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348016 UST-8 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348017 SUMP 5 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348018 SUMP 2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348019 LINE 4 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 104
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348020 SUMP 6 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348021 SUMP 7 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348022 LINE 5 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348023 LINE 6-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348024 LINE 6-2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348025 LINE 7-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348026 LINE 7-2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348027 LINE 7-3 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92683348028 LINE 8 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 104
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SW-846 1 PASI-CKDF
92683348029 LINE 6-3 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 1 Lab ID:92683348001 Collected:08/16/23 10:00 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 12:1608/18/23 14:226.3 4.5 1
Surrogates
n-Pentacosane (S)86 %08/21/23 12:16 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)3.2J mg/kg 08/18/23 20:2308/18/23 14:554.5 1.2 1
Surrogates
4-Bromofluorobenzene (S)108 %08/18/23 20:23 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 15:36 67-64-1 v208/18/23 08:1596.7 31.0 1
Benzene ND ug/kg 08/18/23 15:36 71-43-208/18/23 08:154.8 1.9 1
Bromobenzene ND ug/kg 08/18/23 15:36 108-86-108/18/23 08:154.8 1.6 1
Bromochloromethane ND ug/kg 08/18/23 15:36 74-97-508/18/23 08:154.8 1.4 1
Bromodichloromethane ND ug/kg 08/18/23 15:36 75-27-408/18/23 08:154.8 1.9 1
Bromoform ND ug/kg 08/18/23 15:36 75-25-208/18/23 08:154.8 1.7 1
Bromomethane ND ug/kg 08/18/23 15:36 74-83-9 v208/18/23 08:1519.3 15.0 1
2-Butanone (MEK)627 ug/kg 08/18/23 15:36 78-93-308/18/23 08:1596.7 23.2 1
n-Butylbenzene 587 ug/kg 08/18/23 15:36 104-51-808/18/23 08:154.8 3.0 1
sec-Butylbenzene ND ug/kg 08/18/23 15:36 135-98-808/18/23 08:154.8 2.1 1
tert-Butylbenzene ND ug/kg 08/18/23 15:36 98-06-608/18/23 08:154.8 1.7 1
Carbon tetrachloride ND ug/kg 08/18/23 15:36 56-23-508/18/23 08:154.8 1.8 1
Chlorobenzene 68.7 ug/kg 08/18/23 15:36 108-90-708/18/23 08:154.8 2.8 1
Chloroethane ND ug/kg 08/18/23 15:36 75-00-308/18/23 08:159.7 3.7 1
Chloroform ND ug/kg 08/18/23 15:36 67-66-308/18/23 08:154.8 4.0 1
Chloromethane ND ug/kg 08/18/23 15:36 74-87-308/18/23 08:159.7 4.1 1
2-Chlorotoluene ND ug/kg 08/18/23 15:36 95-49-808/18/23 08:154.8 1.7 1
4-Chlorotoluene ND ug/kg 08/18/23 15:36 106-43-408/18/23 08:154.8 2.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 15:36 96-12-808/18/23 08:154.8 1.9 1
Dibromochloromethane ND ug/kg 08/18/23 15:36 124-48-108/18/23 08:154.8 2.7 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 15:36 106-93-408/18/23 08:154.8 2.1 1
Dibromomethane ND ug/kg 08/18/23 15:36 74-95-308/18/23 08:154.8 1.0 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 15:36 95-50-108/18/23 08:154.8 1.7 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 15:36 541-73-108/18/23 08:154.8 1.5 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 15:36 106-46-708/18/23 08:154.8 1.3 1
Dichlorodifluoromethane ND ug/kg 08/18/23 15:36 75-71-808/18/23 08:159.7 4.9 1
1,1-Dichloroethane ND ug/kg 08/18/23 15:36 75-34-308/18/23 08:154.8 2.0 1
1,2-Dichloroethane ND ug/kg 08/18/23 15:36 107-06-208/18/23 08:154.8 3.2 1
1,1-Dichloroethene ND ug/kg 08/18/23 15:36 75-35-408/18/23 08:154.8 2.0 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 15:36 156-59-208/18/23 08:154.8 1.7 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 15:36 156-60-508/18/23 08:154.8 4.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 1 Lab ID:92683348001 Collected:08/16/23 10:00 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 15:36 78-87-508/18/23 08:154.8 1.5 1
1,3-Dichloropropane ND ug/kg 08/18/23 15:36 142-28-908/18/23 08:154.8 1.5 1
2,2-Dichloropropane ND ug/kg 08/18/23 15:36 594-20-708/18/23 08:154.8 3.7 1
1,1-Dichloropropene ND ug/kg 08/18/23 15:36 563-58-608/18/23 08:154.8 2.3 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 15:36 10061-01-508/18/23 08:154.8 1.3 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 15:36 10061-02-608/18/23 08:154.8 1.7 1
Diisopropyl ether ND ug/kg 08/18/23 15:36 108-20-308/18/23 08:154.8 1.3 1
Ethylbenzene ND ug/kg 08/18/23 15:36 100-41-408/18/23 08:154.8 2.3 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 15:36 87-68-308/18/23 08:159.7 7.9 1
2-Hexanone ND ug/kg 08/18/23 15:36 591-78-608/18/23 08:1548.3 4.7 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 15:36 98-82-808/18/23 08:154.8 1.6 1
p-Isopropyltoluene 843 ug/kg 08/18/23 15:36 99-87-608/18/23 08:154.8 2.4 1
Methylene Chloride ND ug/kg 08/18/23 15:36 75-09-208/18/23 08:1519.3 13.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 15:36 108-10-108/18/23 08:1548.3 4.7 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 15:36 1634-04-408/18/23 08:154.8 1.8 1
Naphthalene ND ug/kg 08/18/23 15:36 91-20-308/18/23 08:154.8 2.5 1
n-Propylbenzene 220 ug/kg 08/18/23 15:36 103-65-108/18/23 08:154.8 1.7 1
Styrene ND ug/kg 08/18/23 15:36 100-42-508/18/23 08:154.8 1.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 15:36 630-20-608/18/23 08:154.8 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 15:36 79-34-508/18/23 08:154.8 1.3 1
Tetrachloroethene ND ug/kg 08/18/23 15:36 127-18-408/18/23 08:154.8 1.5 1
Toluene ND ug/kg 08/18/23 15:36 108-88-308/18/23 08:154.8 3.3 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 15:36 87-61-608/18/23 08:154.8 3.9 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 15:36 120-82-108/18/23 08:154.8 4.1 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 15:36 71-55-608/18/23 08:154.8 2.5 1
1,1,2-Trichloroethane 448 ug/kg 08/18/23 15:36 79-00-508/18/23 08:154.8 1.6 1
Trichloroethene 13.8 ug/kg 08/18/23 15:36 79-01-608/18/23 08:154.8 3.9 1
Trichlorofluoromethane ND ug/kg 08/18/23 15:36 75-69-408/18/23 08:154.8 2.7 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 15:36 96-18-408/18/23 08:154.8 2.4 1
1,2,4-Trimethylbenzene 5740 ug/kg 08/21/23 11:25 95-63-608/18/23 08:159.7 5.7 2
1,3,5-Trimethylbenzene 2350 ug/kg 08/18/23 15:36 108-67-808/18/23 08:154.8 1.6 1
Vinyl acetate ND ug/kg 08/18/23 15:36 108-05-408/18/23 08:1548.3 9.9 1
Vinyl chloride ND ug/kg 08/18/23 15:36 75-01-408/18/23 08:159.7 2.5 1
Xylene (Total)189 ug/kg 08/18/23 15:36 1330-20-708/18/23 08:159.7 2.8 1
m&p-Xylene 174 ug/kg 08/18/23 15:36 179601-23-108/18/23 08:159.7 3.3 1
o-Xylene 15.3 ug/kg 08/18/23 15:36 95-47-608/18/23 08:154.8 2.1 1
Surrogates
Toluene-d8 (S)90 %08/18/23 15:36 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)105 %08/18/23 15:36 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)96 %08/18/23 15:36 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.4 %08/17/23 17:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 1-1 Lab ID:92683348002 Collected:08/16/23 10:15 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 12:1608/18/23 14:226.1 4.3 1
Surrogates
n-Pentacosane (S)83 %08/21/23 12:16 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/18/23 20:4908/18/23 14:554.6 1.3 1
Surrogates
4-Bromofluorobenzene (S)105 %08/18/23 20:49 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 16:13 67-64-1 v208/18/23 08:1581.9 26.3 1
Benzene ND ug/kg 08/18/23 16:13 71-43-208/18/23 08:154.1 1.6 1
Bromobenzene ND ug/kg 08/18/23 16:13 108-86-108/18/23 08:154.1 1.3 1
Bromochloromethane ND ug/kg 08/18/23 16:13 74-97-508/18/23 08:154.1 1.2 1
Bromodichloromethane ND ug/kg 08/18/23 16:13 75-27-408/18/23 08:154.1 1.6 1
Bromoform ND ug/kg 08/18/23 16:13 75-25-208/18/23 08:154.1 1.4 1
Bromomethane ND ug/kg 08/18/23 16:13 74-83-9 v208/18/23 08:1516.4 12.7 1
2-Butanone (MEK)ND ug/kg 08/18/23 16:13 78-93-308/18/23 08:1581.9 19.6 1
n-Butylbenzene 5.0 ug/kg 08/18/23 16:13 104-51-808/18/23 08:154.1 2.6 1
sec-Butylbenzene ND ug/kg 08/18/23 16:13 135-98-808/18/23 08:154.1 1.8 1
tert-Butylbenzene ND ug/kg 08/18/23 16:13 98-06-608/18/23 08:154.1 1.5 1
Carbon tetrachloride ND ug/kg 08/18/23 16:13 56-23-508/18/23 08:154.1 1.5 1
Chlorobenzene ND ug/kg 08/18/23 16:13 108-90-708/18/23 08:154.1 2.3 1
Chloroethane ND ug/kg 08/18/23 16:13 75-00-308/18/23 08:158.2 3.2 1
Chloroform ND ug/kg 08/18/23 16:13 67-66-308/18/23 08:154.1 3.4 1
Chloromethane ND ug/kg 08/18/23 16:13 74-87-308/18/23 08:158.2 3.4 1
2-Chlorotoluene ND ug/kg 08/18/23 16:13 95-49-808/18/23 08:154.1 1.4 1
4-Chlorotoluene ND ug/kg 08/18/23 16:13 106-43-408/18/23 08:154.1 2.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 16:13 96-12-808/18/23 08:154.1 1.6 1
Dibromochloromethane ND ug/kg 08/18/23 16:13 124-48-108/18/23 08:154.1 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 16:13 106-93-408/18/23 08:154.1 1.8 1
Dibromomethane ND ug/kg 08/18/23 16:13 74-95-308/18/23 08:154.1 0.88 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 16:13 95-50-108/18/23 08:154.1 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 16:13 541-73-108/18/23 08:154.1 1.3 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 16:13 106-46-708/18/23 08:154.1 1.1 1
Dichlorodifluoromethane ND ug/kg 08/18/23 16:13 75-71-808/18/23 08:158.2 4.2 1
1,1-Dichloroethane ND ug/kg 08/18/23 16:13 75-34-308/18/23 08:154.1 1.7 1
1,2-Dichloroethane ND ug/kg 08/18/23 16:13 107-06-208/18/23 08:154.1 2.7 1
1,1-Dichloroethene ND ug/kg 08/18/23 16:13 75-35-408/18/23 08:154.1 1.7 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 16:13 156-59-208/18/23 08:154.1 1.4 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 16:13 156-60-508/18/23 08:154.1 3.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 1-1 Lab ID:92683348002 Collected:08/16/23 10:15 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 16:13 78-87-508/18/23 08:154.1 1.2 1
1,3-Dichloropropane ND ug/kg 08/18/23 16:13 142-28-908/18/23 08:154.1 1.3 1
2,2-Dichloropropane ND ug/kg 08/18/23 16:13 594-20-708/18/23 08:154.1 3.1 1
1,1-Dichloropropene ND ug/kg 08/18/23 16:13 563-58-608/18/23 08:154.1 2.0 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 16:13 10061-01-508/18/23 08:154.1 1.1 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 16:13 10061-02-608/18/23 08:154.1 1.4 1
Diisopropyl ether ND ug/kg 08/18/23 16:13 108-20-308/18/23 08:154.1 1.1 1
Ethylbenzene 3.3J ug/kg 08/18/23 16:13 100-41-408/18/23 08:154.1 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 16:13 87-68-308/18/23 08:158.2 6.7 1
2-Hexanone ND ug/kg 08/18/23 16:13 591-78-608/18/23 08:1540.9 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 16:13 98-82-808/18/23 08:154.1 1.4 1
p-Isopropyltoluene 4.8 ug/kg 08/18/23 16:13 99-87-608/18/23 08:154.1 2.0 1
Methylene Chloride ND ug/kg 08/18/23 16:13 75-09-208/18/23 08:1516.4 11.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 16:13 108-10-108/18/23 08:1540.9 3.9 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 16:13 1634-04-408/18/23 08:154.1 1.5 1
Naphthalene ND ug/kg 08/18/23 16:13 91-20-308/18/23 08:154.1 2.2 1
n-Propylbenzene ND ug/kg 08/18/23 16:13 103-65-108/18/23 08:154.1 1.5 1
Styrene ND ug/kg 08/18/23 16:13 100-42-508/18/23 08:154.1 1.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 16:13 630-20-608/18/23 08:154.1 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 16:13 79-34-508/18/23 08:154.1 1.1 1
Tetrachloroethene ND ug/kg 08/18/23 16:13 127-18-408/18/23 08:154.1 1.3 1
Toluene ND ug/kg 08/18/23 16:13 108-88-308/18/23 08:154.1 2.8 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 16:13 87-61-608/18/23 08:154.1 3.3 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 16:13 120-82-108/18/23 08:154.1 3.4 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 16:13 71-55-608/18/23 08:154.1 2.1 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 16:13 79-00-508/18/23 08:154.1 1.4 1
Trichloroethene ND ug/kg 08/18/23 16:13 79-01-608/18/23 08:154.1 3.3 1
Trichlorofluoromethane ND ug/kg 08/18/23 16:13 75-69-408/18/23 08:154.1 2.3 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 16:13 96-18-408/18/23 08:154.1 2.1 1
1,2,4-Trimethylbenzene 21.8 ug/kg 08/18/23 16:13 95-63-608/18/23 08:154.1 2.4 1
1,3,5-Trimethylbenzene 8.8 ug/kg 08/18/23 16:13 108-67-808/18/23 08:154.1 1.4 1
Vinyl acetate ND ug/kg 08/18/23 16:13 108-05-408/18/23 08:1540.9 8.4 1
Vinyl chloride ND ug/kg 08/18/23 16:13 75-01-408/18/23 08:158.2 2.1 1
Xylene (Total)10.5 ug/kg 08/18/23 16:13 1330-20-708/18/23 08:158.2 2.3 1
m&p-Xylene 7.0J ug/kg 08/18/23 16:13 179601-23-108/18/23 08:158.2 2.8 1
o-Xylene 3.6J ug/kg 08/18/23 16:13 95-47-608/18/23 08:154.1 1.8 1
Surrogates
Toluene-d8 (S)97 %08/18/23 16:13 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)98 %08/18/23 16:13 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)89 %08/18/23 16:13 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.5 %08/17/23 17:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 1-2 Lab ID:92683348003 Collected:08/16/23 10:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 12:3408/18/23 14:226.2 4.4 1
Surrogates
n-Pentacosane (S)79 %08/21/23 12:34 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/18/23 21:1508/18/23 14:554.4 1.2 1
Surrogates
4-Bromofluorobenzene (S)104 %08/18/23 21:15 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 16:32 67-64-1 v208/18/23 08:1583.0 26.6 1
Benzene ND ug/kg 08/18/23 16:32 71-43-208/18/23 08:154.1 1.7 1
Bromobenzene ND ug/kg 08/18/23 16:32 108-86-108/18/23 08:154.1 1.4 1
Bromochloromethane ND ug/kg 08/18/23 16:32 74-97-508/18/23 08:154.1 1.2 1
Bromodichloromethane ND ug/kg 08/18/23 16:32 75-27-408/18/23 08:154.1 1.6 1
Bromoform ND ug/kg 08/18/23 16:32 75-25-208/18/23 08:154.1 1.5 1
Bromomethane ND ug/kg 08/18/23 16:32 74-83-9 v208/18/23 08:1516.6 12.9 1
2-Butanone (MEK)ND ug/kg 08/18/23 16:32 78-93-308/18/23 08:1583.0 19.9 1
n-Butylbenzene ND ug/kg 08/18/23 16:32 104-51-808/18/23 08:154.1 2.6 1
sec-Butylbenzene ND ug/kg 08/18/23 16:32 135-98-808/18/23 08:154.1 1.8 1
tert-Butylbenzene ND ug/kg 08/18/23 16:32 98-06-608/18/23 08:154.1 1.5 1
Carbon tetrachloride ND ug/kg 08/18/23 16:32 56-23-508/18/23 08:154.1 1.6 1
Chlorobenzene ND ug/kg 08/18/23 16:32 108-90-708/18/23 08:154.1 2.4 1
Chloroethane ND ug/kg 08/18/23 16:32 75-00-308/18/23 08:158.3 3.2 1
Chloroform ND ug/kg 08/18/23 16:32 67-66-308/18/23 08:154.1 3.5 1
Chloromethane ND ug/kg 08/18/23 16:32 74-87-308/18/23 08:158.3 3.5 1
2-Chlorotoluene ND ug/kg 08/18/23 16:32 95-49-808/18/23 08:154.1 1.5 1
4-Chlorotoluene ND ug/kg 08/18/23 16:32 106-43-408/18/23 08:154.1 2.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 16:32 96-12-808/18/23 08:154.1 1.6 1
Dibromochloromethane ND ug/kg 08/18/23 16:32 124-48-108/18/23 08:154.1 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 16:32 106-93-408/18/23 08:154.1 1.8 1
Dibromomethane ND ug/kg 08/18/23 16:32 74-95-308/18/23 08:154.1 0.89 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 16:32 95-50-108/18/23 08:154.1 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 16:32 541-73-108/18/23 08:154.1 1.3 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 16:32 106-46-708/18/23 08:154.1 1.1 1
Dichlorodifluoromethane ND ug/kg 08/18/23 16:32 75-71-808/18/23 08:158.3 4.2 1
1,1-Dichloroethane ND ug/kg 08/18/23 16:32 75-34-308/18/23 08:154.1 1.7 1
1,2-Dichloroethane ND ug/kg 08/18/23 16:32 107-06-208/18/23 08:154.1 2.7 1
1,1-Dichloroethene ND ug/kg 08/18/23 16:32 75-35-408/18/23 08:154.1 1.7 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 16:32 156-59-208/18/23 08:154.1 1.4 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 16:32 156-60-508/18/23 08:154.1 3.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 1-2 Lab ID:92683348003 Collected:08/16/23 10:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 16:32 78-87-508/18/23 08:154.1 1.2 1
1,3-Dichloropropane ND ug/kg 08/18/23 16:32 142-28-908/18/23 08:154.1 1.3 1
2,2-Dichloropropane ND ug/kg 08/18/23 16:32 594-20-708/18/23 08:154.1 3.1 1
1,1-Dichloropropene ND ug/kg 08/18/23 16:32 563-58-608/18/23 08:154.1 2.0 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 16:32 10061-01-508/18/23 08:154.1 1.1 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 16:32 10061-02-608/18/23 08:154.1 1.4 1
Diisopropyl ether ND ug/kg 08/18/23 16:32 108-20-308/18/23 08:154.1 1.1 1
Ethylbenzene ND ug/kg 08/18/23 16:32 100-41-408/18/23 08:154.1 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 16:32 87-68-308/18/23 08:158.3 6.8 1
2-Hexanone ND ug/kg 08/18/23 16:32 591-78-608/18/23 08:1541.5 4.0 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 16:32 98-82-808/18/23 08:154.1 1.4 1
p-Isopropyltoluene ND ug/kg 08/18/23 16:32 99-87-608/18/23 08:154.1 2.0 1
Methylene Chloride ND ug/kg 08/18/23 16:32 75-09-208/18/23 08:1516.6 11.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 16:32 108-10-108/18/23 08:1541.5 4.0 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 16:32 1634-04-408/18/23 08:154.1 1.6 1
Naphthalene ND ug/kg 08/18/23 16:32 91-20-308/18/23 08:154.1 2.2 1
n-Propylbenzene ND ug/kg 08/18/23 16:32 103-65-108/18/23 08:154.1 1.5 1
Styrene ND ug/kg 08/18/23 16:32 100-42-508/18/23 08:154.1 1.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 16:32 630-20-608/18/23 08:154.1 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 16:32 79-34-508/18/23 08:154.1 1.1 1
Tetrachloroethene ND ug/kg 08/18/23 16:32 127-18-408/18/23 08:154.1 1.3 1
Toluene ND ug/kg 08/18/23 16:32 108-88-308/18/23 08:154.1 2.9 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 16:32 87-61-608/18/23 08:154.1 3.4 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 16:32 120-82-108/18/23 08:154.1 3.5 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 16:32 71-55-608/18/23 08:154.1 2.2 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 16:32 79-00-508/18/23 08:154.1 1.4 1
Trichloroethene ND ug/kg 08/18/23 16:32 79-01-608/18/23 08:154.1 3.3 1
Trichlorofluoromethane ND ug/kg 08/18/23 16:32 75-69-408/18/23 08:154.1 2.3 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 16:32 96-18-408/18/23 08:154.1 2.1 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 16:32 95-63-608/18/23 08:154.1 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 16:32 108-67-808/18/23 08:154.1 1.4 1
Vinyl acetate ND ug/kg 08/18/23 16:32 108-05-408/18/23 08:1541.5 8.5 1
Vinyl chloride ND ug/kg 08/18/23 16:32 75-01-408/18/23 08:158.3 2.1 1
Xylene (Total)ND ug/kg 08/18/23 16:32 1330-20-708/18/23 08:158.3 2.4 1
m&p-Xylene ND ug/kg 08/18/23 16:32 179601-23-108/18/23 08:158.3 2.8 1
o-Xylene ND ug/kg 08/18/23 16:32 95-47-608/18/23 08:154.1 1.8 1
Surrogates
Toluene-d8 (S)96 %08/18/23 16:32 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)98 %08/18/23 16:32 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)90 %08/18/23 16:32 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.3 %08/17/23 17:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 3 Lab ID:92683348004 Collected:08/16/23 11:00 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 12:3408/18/23 14:226.2 4.4 1
Surrogates
n-Pentacosane (S)83 %08/21/23 12:34 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/18/23 21:4108/18/23 14:555.1 1.4 1
Surrogates
4-Bromofluorobenzene (S)106 %08/18/23 21:41 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 16:50 67-64-1 v208/18/23 08:1569.1 22.2 1
Benzene ND ug/kg 08/18/23 16:50 71-43-208/18/23 08:153.5 1.4 1
Bromobenzene ND ug/kg 08/18/23 16:50 108-86-108/18/23 08:153.5 1.1 1
Bromochloromethane ND ug/kg 08/18/23 16:50 74-97-508/18/23 08:153.5 1.0 1
Bromodichloromethane ND ug/kg 08/18/23 16:50 75-27-408/18/23 08:153.5 1.3 1
Bromoform ND ug/kg 08/18/23 16:50 75-25-208/18/23 08:153.5 1.2 1
Bromomethane ND ug/kg 08/18/23 16:50 74-83-9 v208/18/23 08:1513.8 10.7 1
2-Butanone (MEK)ND ug/kg 08/18/23 16:50 78-93-308/18/23 08:1569.1 16.6 1
n-Butylbenzene ND ug/kg 08/18/23 16:50 104-51-808/18/23 08:153.5 2.2 1
sec-Butylbenzene ND ug/kg 08/18/23 16:50 135-98-808/18/23 08:153.5 1.5 1
tert-Butylbenzene ND ug/kg 08/18/23 16:50 98-06-608/18/23 08:153.5 1.2 1
Carbon tetrachloride ND ug/kg 08/18/23 16:50 56-23-508/18/23 08:153.5 1.3 1
Chlorobenzene ND ug/kg 08/18/23 16:50 108-90-708/18/23 08:153.5 2.0 1
Chloroethane ND ug/kg 08/18/23 16:50 75-00-308/18/23 08:156.9 2.7 1
Chloroform ND ug/kg 08/18/23 16:50 67-66-308/18/23 08:153.5 2.9 1
Chloromethane ND ug/kg 08/18/23 16:50 74-87-308/18/23 08:156.9 2.9 1
2-Chlorotoluene ND ug/kg 08/18/23 16:50 95-49-808/18/23 08:153.5 1.2 1
4-Chlorotoluene ND ug/kg 08/18/23 16:50 106-43-408/18/23 08:153.5 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 16:50 96-12-808/18/23 08:153.5 1.3 1
Dibromochloromethane ND ug/kg 08/18/23 16:50 124-48-108/18/23 08:153.5 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 16:50 106-93-408/18/23 08:153.5 1.5 1
Dibromomethane ND ug/kg 08/18/23 16:50 74-95-308/18/23 08:153.5 0.74 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 16:50 95-50-108/18/23 08:153.5 1.2 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 16:50 541-73-108/18/23 08:153.5 1.1 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 16:50 106-46-708/18/23 08:153.5 0.90 1
Dichlorodifluoromethane ND ug/kg 08/18/23 16:50 75-71-808/18/23 08:156.9 3.5 1
1,1-Dichloroethane ND ug/kg 08/18/23 16:50 75-34-308/18/23 08:153.5 1.4 1
1,2-Dichloroethane ND ug/kg 08/18/23 16:50 107-06-208/18/23 08:153.5 2.3 1
1,1-Dichloroethene ND ug/kg 08/18/23 16:50 75-35-408/18/23 08:153.5 1.4 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 16:50 156-59-208/18/23 08:153.5 1.2 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 16:50 156-60-508/18/23 08:153.5 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 3 Lab ID:92683348004 Collected:08/16/23 11:00 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 16:50 78-87-508/18/23 08:153.5 1.0 1
1,3-Dichloropropane ND ug/kg 08/18/23 16:50 142-28-908/18/23 08:153.5 1.1 1
2,2-Dichloropropane ND ug/kg 08/18/23 16:50 594-20-708/18/23 08:153.5 2.6 1
1,1-Dichloropropene ND ug/kg 08/18/23 16:50 563-58-608/18/23 08:153.5 1.7 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 16:50 10061-01-508/18/23 08:153.5 0.94 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 16:50 10061-02-608/18/23 08:153.5 1.2 1
Diisopropyl ether ND ug/kg 08/18/23 16:50 108-20-308/18/23 08:153.5 0.93 1
Ethylbenzene ND ug/kg 08/18/23 16:50 100-41-408/18/23 08:153.5 1.6 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 16:50 87-68-308/18/23 08:156.9 5.6 1
2-Hexanone ND ug/kg 08/18/23 16:50 591-78-608/18/23 08:1534.5 3.3 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 16:50 98-82-808/18/23 08:153.5 1.2 1
p-Isopropyltoluene ND ug/kg 08/18/23 16:50 99-87-608/18/23 08:153.5 1.7 1
Methylene Chloride ND ug/kg 08/18/23 16:50 75-09-208/18/23 08:1513.8 9.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 16:50 108-10-108/18/23 08:1534.5 3.3 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 16:50 1634-04-408/18/23 08:153.5 1.3 1
Naphthalene ND ug/kg 08/18/23 16:50 91-20-308/18/23 08:153.5 1.8 1
n-Propylbenzene ND ug/kg 08/18/23 16:50 103-65-108/18/23 08:153.5 1.2 1
Styrene ND ug/kg 08/18/23 16:50 100-42-508/18/23 08:153.5 0.91 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 16:50 630-20-608/18/23 08:153.5 1.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 16:50 79-34-508/18/23 08:153.5 0.91 1
Tetrachloroethene ND ug/kg 08/18/23 16:50 127-18-408/18/23 08:153.5 1.1 1
Toluene ND ug/kg 08/18/23 16:50 108-88-308/18/23 08:153.5 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 16:50 87-61-608/18/23 08:153.5 2.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 16:50 120-82-108/18/23 08:153.5 2.9 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 16:50 71-55-608/18/23 08:153.5 1.8 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 16:50 79-00-508/18/23 08:153.5 1.1 1
Trichloroethene ND ug/kg 08/18/23 16:50 79-01-608/18/23 08:153.5 2.8 1
Trichlorofluoromethane ND ug/kg 08/18/23 16:50 75-69-408/18/23 08:153.5 1.9 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 16:50 96-18-408/18/23 08:153.5 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 16:50 95-63-608/18/23 08:153.5 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 16:50 108-67-808/18/23 08:153.5 1.2 1
Vinyl acetate ND ug/kg 08/18/23 16:50 108-05-408/18/23 08:1534.5 7.1 1
Vinyl chloride ND ug/kg 08/18/23 16:50 75-01-408/18/23 08:156.9 1.8 1
Xylene (Total)ND ug/kg 08/18/23 16:50 1330-20-708/18/23 08:156.9 2.0 1
m&p-Xylene ND ug/kg 08/18/23 16:50 179601-23-108/18/23 08:156.9 2.4 1
o-Xylene ND ug/kg 08/18/23 16:50 95-47-608/18/23 08:153.5 1.5 1
Surrogates
Toluene-d8 (S)98 %08/18/23 16:50 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)99 %08/18/23 16:50 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)92 %08/18/23 16:50 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.2 %08/17/23 17:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 2 Lab ID:92683348005 Collected:08/16/23 12:15 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 12:5208/18/23 14:226.0 4.3 1
Surrogates
n-Pentacosane (S)84 %08/21/23 12:52 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1.9J mg/kg 08/18/23 22:0708/18/23 14:554.4 1.2 1
Surrogates
4-Bromofluorobenzene (S)106 %08/18/23 22:07 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 17:09 67-64-1 v208/18/23 08:1597.7 31.4 1
Benzene ND ug/kg 08/18/23 17:09 71-43-208/18/23 08:154.9 1.9 1
Bromobenzene ND ug/kg 08/18/23 17:09 108-86-108/18/23 08:154.9 1.6 1
Bromochloromethane ND ug/kg 08/18/23 17:09 74-97-508/18/23 08:154.9 1.4 1
Bromodichloromethane ND ug/kg 08/18/23 17:09 75-27-408/18/23 08:154.9 1.9 1
Bromoform ND ug/kg 08/18/23 17:09 75-25-208/18/23 08:154.9 1.7 1
Bromomethane ND ug/kg 08/18/23 17:09 74-83-9 v208/18/23 08:1519.5 15.1 1
2-Butanone (MEK)ND ug/kg 08/18/23 17:09 78-93-308/18/23 08:1597.7 23.5 1
n-Butylbenzene ND ug/kg 08/18/23 17:09 104-51-808/18/23 08:154.9 3.1 1
sec-Butylbenzene ND ug/kg 08/18/23 17:09 135-98-808/18/23 08:154.9 2.1 1
tert-Butylbenzene ND ug/kg 08/18/23 17:09 98-06-608/18/23 08:154.9 1.7 1
Carbon tetrachloride ND ug/kg 08/18/23 17:09 56-23-508/18/23 08:154.9 1.8 1
Chlorobenzene ND ug/kg 08/18/23 17:09 108-90-708/18/23 08:154.9 2.8 1
Chloroethane ND ug/kg 08/18/23 17:09 75-00-308/18/23 08:159.8 3.8 1
Chloroform ND ug/kg 08/18/23 17:09 67-66-308/18/23 08:154.9 4.1 1
Chloromethane ND ug/kg 08/18/23 17:09 74-87-308/18/23 08:159.8 4.1 1
2-Chlorotoluene ND ug/kg 08/18/23 17:09 95-49-808/18/23 08:154.9 1.7 1
4-Chlorotoluene ND ug/kg 08/18/23 17:09 106-43-408/18/23 08:154.9 2.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 17:09 96-12-808/18/23 08:154.9 1.9 1
Dibromochloromethane ND ug/kg 08/18/23 17:09 124-48-108/18/23 08:154.9 2.7 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 17:09 106-93-408/18/23 08:154.9 2.1 1
Dibromomethane ND ug/kg 08/18/23 17:09 74-95-308/18/23 08:154.9 1.0 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 17:09 95-50-108/18/23 08:154.9 1.8 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 17:09 541-73-108/18/23 08:154.9 1.5 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 17:09 106-46-708/18/23 08:154.9 1.3 1
Dichlorodifluoromethane ND ug/kg 08/18/23 17:09 75-71-808/18/23 08:159.8 5.0 1
1,1-Dichloroethane ND ug/kg 08/18/23 17:09 75-34-308/18/23 08:154.9 2.0 1
1,2-Dichloroethane ND ug/kg 08/18/23 17:09 107-06-208/18/23 08:154.9 3.2 1
1,1-Dichloroethene ND ug/kg 08/18/23 17:09 75-35-408/18/23 08:154.9 2.0 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 17:09 156-59-208/18/23 08:154.9 1.7 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 17:09 156-60-508/18/23 08:154.9 4.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 2 Lab ID:92683348005 Collected:08/16/23 12:15 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 17:09 78-87-508/18/23 08:154.9 1.5 1
1,3-Dichloropropane ND ug/kg 08/18/23 17:09 142-28-908/18/23 08:154.9 1.5 1
2,2-Dichloropropane ND ug/kg 08/18/23 17:09 594-20-708/18/23 08:154.9 3.7 1
1,1-Dichloropropene ND ug/kg 08/18/23 17:09 563-58-608/18/23 08:154.9 2.3 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 17:09 10061-01-508/18/23 08:154.9 1.3 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 17:09 10061-02-608/18/23 08:154.9 1.7 1
Diisopropyl ether ND ug/kg 08/18/23 17:09 108-20-308/18/23 08:154.9 1.3 1
Ethylbenzene ND ug/kg 08/18/23 17:09 100-41-408/18/23 08:154.9 2.3 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 17:09 87-68-308/18/23 08:159.8 8.0 1
2-Hexanone ND ug/kg 08/18/23 17:09 591-78-608/18/23 08:1548.9 4.7 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 17:09 98-82-808/18/23 08:154.9 1.7 1
p-Isopropyltoluene ND ug/kg 08/18/23 17:09 99-87-608/18/23 08:154.9 2.4 1
Methylene Chloride ND ug/kg 08/18/23 17:09 75-09-208/18/23 08:1519.5 13.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 17:09 108-10-108/18/23 08:1548.9 4.7 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 17:09 1634-04-408/18/23 08:154.9 1.8 1
Naphthalene ND ug/kg 08/18/23 17:09 91-20-308/18/23 08:154.9 2.6 1
n-Propylbenzene ND ug/kg 08/18/23 17:09 103-65-108/18/23 08:154.9 1.7 1
Styrene 9.8 ug/kg 08/18/23 17:09 100-42-508/18/23 08:154.9 1.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 17:09 630-20-608/18/23 08:154.9 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 17:09 79-34-508/18/23 08:154.9 1.3 1
Tetrachloroethene ND ug/kg 08/18/23 17:09 127-18-408/18/23 08:154.9 1.5 1
Toluene ND ug/kg 08/18/23 17:09 108-88-308/18/23 08:154.9 3.4 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 17:09 87-61-608/18/23 08:154.9 3.9 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 17:09 120-82-108/18/23 08:154.9 4.1 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 17:09 71-55-608/18/23 08:154.9 2.5 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 17:09 79-00-508/18/23 08:154.9 1.6 1
Trichloroethene ND ug/kg 08/18/23 17:09 79-01-608/18/23 08:154.9 3.9 1
Trichlorofluoromethane ND ug/kg 08/18/23 17:09 75-69-408/18/23 08:154.9 2.7 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 17:09 96-18-408/18/23 08:154.9 2.5 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 17:09 95-63-608/18/23 08:154.9 2.9 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 17:09 108-67-808/18/23 08:154.9 1.6 1
Vinyl acetate ND ug/kg 08/18/23 17:09 108-05-408/18/23 08:1548.9 10.1 1
Vinyl chloride ND ug/kg 08/18/23 17:09 75-01-408/18/23 08:159.8 2.5 1
Xylene (Total)ND ug/kg 08/18/23 17:09 1330-20-708/18/23 08:159.8 2.8 1
m&p-Xylene ND ug/kg 08/18/23 17:09 179601-23-108/18/23 08:159.8 3.3 1
o-Xylene ND ug/kg 08/18/23 17:09 95-47-608/18/23 08:154.9 2.2 1
Surrogates
Toluene-d8 (S)97 %08/18/23 17:09 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)97 %08/18/23 17:09 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)90 %08/18/23 17:09 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.4 %08/17/23 17:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 4 Lab ID:92683348006 Collected:08/16/23 12:45 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 12:5208/18/23 14:226.3 4.5 1
Surrogates
n-Pentacosane (S)82 %08/21/23 12:52 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/18/23 22:3308/18/23 14:559.4 2.6 1
Surrogates
4-Bromofluorobenzene (S)106 %08/18/23 22:33 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 17:28 67-64-1 v208/18/23 08:1583.0 26.6 1
Benzene ND ug/kg 08/18/23 17:28 71-43-208/18/23 08:154.1 1.7 1
Bromobenzene ND ug/kg 08/18/23 17:28 108-86-108/18/23 08:154.1 1.4 1
Bromochloromethane ND ug/kg 08/18/23 17:28 74-97-508/18/23 08:154.1 1.2 1
Bromodichloromethane ND ug/kg 08/18/23 17:28 75-27-408/18/23 08:154.1 1.6 1
Bromoform ND ug/kg 08/18/23 17:28 75-25-208/18/23 08:154.1 1.5 1
Bromomethane ND ug/kg 08/18/23 17:28 74-83-9 v208/18/23 08:1516.6 12.9 1
2-Butanone (MEK)ND ug/kg 08/18/23 17:28 78-93-308/18/23 08:1583.0 19.9 1
n-Butylbenzene ND ug/kg 08/18/23 17:28 104-51-808/18/23 08:154.1 2.6 1
sec-Butylbenzene ND ug/kg 08/18/23 17:28 135-98-808/18/23 08:154.1 1.8 1
tert-Butylbenzene ND ug/kg 08/18/23 17:28 98-06-608/18/23 08:154.1 1.5 1
Carbon tetrachloride ND ug/kg 08/18/23 17:28 56-23-508/18/23 08:154.1 1.6 1
Chlorobenzene ND ug/kg 08/18/23 17:28 108-90-708/18/23 08:154.1 2.4 1
Chloroethane ND ug/kg 08/18/23 17:28 75-00-308/18/23 08:158.3 3.2 1
Chloroform ND ug/kg 08/18/23 17:28 67-66-308/18/23 08:154.1 3.5 1
Chloromethane ND ug/kg 08/18/23 17:28 74-87-308/18/23 08:158.3 3.5 1
2-Chlorotoluene ND ug/kg 08/18/23 17:28 95-49-808/18/23 08:154.1 1.5 1
4-Chlorotoluene ND ug/kg 08/18/23 17:28 106-43-408/18/23 08:154.1 2.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 17:28 96-12-808/18/23 08:154.1 1.6 1
Dibromochloromethane ND ug/kg 08/18/23 17:28 124-48-108/18/23 08:154.1 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 17:28 106-93-408/18/23 08:154.1 1.8 1
Dibromomethane ND ug/kg 08/18/23 17:28 74-95-308/18/23 08:154.1 0.89 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 17:28 95-50-108/18/23 08:154.1 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 17:28 541-73-108/18/23 08:154.1 1.3 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 17:28 106-46-708/18/23 08:154.1 1.1 1
Dichlorodifluoromethane ND ug/kg 08/18/23 17:28 75-71-808/18/23 08:158.3 4.2 1
1,1-Dichloroethane ND ug/kg 08/18/23 17:28 75-34-308/18/23 08:154.1 1.7 1
1,2-Dichloroethane ND ug/kg 08/18/23 17:28 107-06-208/18/23 08:154.1 2.7 1
1,1-Dichloroethene ND ug/kg 08/18/23 17:28 75-35-408/18/23 08:154.1 1.7 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 17:28 156-59-208/18/23 08:154.1 1.4 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 17:28 156-60-508/18/23 08:154.1 3.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 4 Lab ID:92683348006 Collected:08/16/23 12:45 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 17:28 78-87-508/18/23 08:154.1 1.2 1
1,3-Dichloropropane ND ug/kg 08/18/23 17:28 142-28-908/18/23 08:154.1 1.3 1
2,2-Dichloropropane ND ug/kg 08/18/23 17:28 594-20-708/18/23 08:154.1 3.1 1
1,1-Dichloropropene ND ug/kg 08/18/23 17:28 563-58-608/18/23 08:154.1 2.0 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 17:28 10061-01-508/18/23 08:154.1 1.1 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 17:28 10061-02-608/18/23 08:154.1 1.4 1
Diisopropyl ether ND ug/kg 08/18/23 17:28 108-20-308/18/23 08:154.1 1.1 1
Ethylbenzene ND ug/kg 08/18/23 17:28 100-41-408/18/23 08:154.1 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 17:28 87-68-308/18/23 08:158.3 6.8 1
2-Hexanone ND ug/kg 08/18/23 17:28 591-78-608/18/23 08:1541.5 4.0 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 17:28 98-82-808/18/23 08:154.1 1.4 1
p-Isopropyltoluene ND ug/kg 08/18/23 17:28 99-87-608/18/23 08:154.1 2.0 1
Methylene Chloride ND ug/kg 08/18/23 17:28 75-09-208/18/23 08:1516.6 11.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 17:28 108-10-108/18/23 08:1541.5 4.0 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 17:28 1634-04-408/18/23 08:154.1 1.6 1
Naphthalene ND ug/kg 08/18/23 17:28 91-20-308/18/23 08:154.1 2.2 1
n-Propylbenzene ND ug/kg 08/18/23 17:28 103-65-108/18/23 08:154.1 1.5 1
Styrene 3.0J ug/kg 08/18/23 17:28 100-42-508/18/23 08:154.1 1.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 17:28 630-20-608/18/23 08:154.1 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 17:28 79-34-508/18/23 08:154.1 1.1 1
Tetrachloroethene ND ug/kg 08/18/23 17:28 127-18-408/18/23 08:154.1 1.3 1
Toluene ND ug/kg 08/18/23 17:28 108-88-308/18/23 08:154.1 2.9 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 17:28 87-61-608/18/23 08:154.1 3.4 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 17:28 120-82-108/18/23 08:154.1 3.5 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 17:28 71-55-608/18/23 08:154.1 2.2 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 17:28 79-00-508/18/23 08:154.1 1.4 1
Trichloroethene ND ug/kg 08/18/23 17:28 79-01-608/18/23 08:154.1 3.3 1
Trichlorofluoromethane ND ug/kg 08/18/23 17:28 75-69-408/18/23 08:154.1 2.3 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 17:28 96-18-408/18/23 08:154.1 2.1 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 17:28 95-63-608/18/23 08:154.1 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 17:28 108-67-808/18/23 08:154.1 1.4 1
Vinyl acetate ND ug/kg 08/18/23 17:28 108-05-408/18/23 08:1541.5 8.5 1
Vinyl chloride ND ug/kg 08/18/23 17:28 75-01-408/18/23 08:158.3 2.1 1
Xylene (Total)ND ug/kg 08/18/23 17:28 1330-20-708/18/23 08:158.3 2.4 1
m&p-Xylene ND ug/kg 08/18/23 17:28 179601-23-108/18/23 08:158.3 2.8 1
o-Xylene ND ug/kg 08/18/23 17:28 95-47-608/18/23 08:154.1 1.8 1
Surrogates
Toluene-d8 (S)97 %08/18/23 17:28 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)97 %08/18/23 17:28 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)93 %08/18/23 17:28 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.2 %08/17/23 17:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:NEW BUILD Lab ID:92683348007 Collected:08/16/23 13:40 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 13:1008/18/23 14:225.6 4.0 1
Surrogates
n-Pentacosane (S)84 %08/21/23 13:10 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/18/23 22:5808/18/23 14:553.2 0.89 1
Surrogates
4-Bromofluorobenzene (S)107 %08/18/23 22:58 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 17:46 67-64-1 v208/18/23 08:1555.5 17.8 1
Benzene ND ug/kg 08/18/23 17:46 71-43-208/18/23 08:152.8 1.1 1
Bromobenzene ND ug/kg 08/18/23 17:46 108-86-108/18/23 08:152.8 0.91 1
Bromochloromethane ND ug/kg 08/18/23 17:46 74-97-508/18/23 08:152.8 0.82 1
Bromodichloromethane ND ug/kg 08/18/23 17:46 75-27-408/18/23 08:152.8 1.1 1
Bromoform ND ug/kg 08/18/23 17:46 75-25-208/18/23 08:152.8 0.98 1
Bromomethane ND ug/kg 08/18/23 17:46 74-83-9 v208/18/23 08:1511.1 8.6 1
2-Butanone (MEK)ND ug/kg 08/18/23 17:46 78-93-308/18/23 08:1555.5 13.3 1
n-Butylbenzene ND ug/kg 08/18/23 17:46 104-51-808/18/23 08:152.8 1.7 1
sec-Butylbenzene ND ug/kg 08/18/23 17:46 135-98-808/18/23 08:152.8 1.2 1
tert-Butylbenzene ND ug/kg 08/18/23 17:46 98-06-608/18/23 08:152.8 0.99 1
Carbon tetrachloride ND ug/kg 08/18/23 17:46 56-23-508/18/23 08:152.8 1.0 1
Chlorobenzene ND ug/kg 08/18/23 17:46 108-90-708/18/23 08:152.8 1.6 1
Chloroethane ND ug/kg 08/18/23 17:46 75-00-308/18/23 08:155.6 2.1 1
Chloroform ND ug/kg 08/18/23 17:46 67-66-308/18/23 08:152.8 2.3 1
Chloromethane ND ug/kg 08/18/23 17:46 74-87-308/18/23 08:155.6 2.3 1
2-Chlorotoluene ND ug/kg 08/18/23 17:46 95-49-808/18/23 08:152.8 0.98 1
4-Chlorotoluene ND ug/kg 08/18/23 17:46 106-43-408/18/23 08:152.8 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 17:46 96-12-808/18/23 08:152.8 1.1 1
Dibromochloromethane ND ug/kg 08/18/23 17:46 124-48-108/18/23 08:152.8 1.6 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 17:46 106-93-408/18/23 08:152.8 1.2 1
Dibromomethane ND ug/kg 08/18/23 17:46 74-95-308/18/23 08:152.8 0.59 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 17:46 95-50-108/18/23 08:152.8 1.0 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 17:46 541-73-108/18/23 08:152.8 0.86 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 17:46 106-46-708/18/23 08:152.8 0.72 1
Dichlorodifluoromethane ND ug/kg 08/18/23 17:46 75-71-808/18/23 08:155.6 2.8 1
1,1-Dichloroethane ND ug/kg 08/18/23 17:46 75-34-308/18/23 08:152.8 1.1 1
1,2-Dichloroethane ND ug/kg 08/18/23 17:46 107-06-208/18/23 08:152.8 1.8 1
1,1-Dichloroethene ND ug/kg 08/18/23 17:46 75-35-408/18/23 08:152.8 1.1 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 17:46 156-59-208/18/23 08:152.8 0.95 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 17:46 156-60-508/18/23 08:152.8 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:NEW BUILD Lab ID:92683348007 Collected:08/16/23 13:40 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 17:46 78-87-508/18/23 08:152.8 0.83 1
1,3-Dichloropropane ND ug/kg 08/18/23 17:46 142-28-908/18/23 08:152.8 0.87 1
2,2-Dichloropropane ND ug/kg 08/18/23 17:46 594-20-708/18/23 08:152.8 2.1 1
1,1-Dichloropropene ND ug/kg 08/18/23 17:46 563-58-608/18/23 08:152.8 1.3 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 17:46 10061-01-508/18/23 08:152.8 0.76 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 17:46 10061-02-608/18/23 08:152.8 0.96 1
Diisopropyl ether ND ug/kg 08/18/23 17:46 108-20-308/18/23 08:152.8 0.75 1
Ethylbenzene 1.7J ug/kg 08/18/23 17:46 100-41-408/18/23 08:152.8 1.3 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 17:46 87-68-308/18/23 08:155.6 4.5 1
2-Hexanone ND ug/kg 08/18/23 17:46 591-78-608/18/23 08:1527.8 2.7 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 17:46 98-82-808/18/23 08:152.8 0.94 1
p-Isopropyltoluene ND ug/kg 08/18/23 17:46 99-87-608/18/23 08:152.8 1.4 1
Methylene Chloride ND ug/kg 08/18/23 17:46 75-09-208/18/23 08:1511.1 7.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 17:46 108-10-108/18/23 08:1527.8 2.7 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 17:46 1634-04-408/18/23 08:152.8 1.0 1
Naphthalene ND ug/kg 08/18/23 17:46 91-20-308/18/23 08:152.8 1.5 1
n-Propylbenzene ND ug/kg 08/18/23 17:46 103-65-108/18/23 08:152.8 0.99 1
Styrene 3.8 ug/kg 08/18/23 17:46 100-42-508/18/23 08:152.8 0.73 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 17:46 630-20-608/18/23 08:152.8 1.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 17:46 79-34-508/18/23 08:152.8 0.73 1
Tetrachloroethene ND ug/kg 08/18/23 17:46 127-18-408/18/23 08:152.8 0.88 1
Toluene 2.8 ug/kg 08/18/23 17:46 108-88-308/18/23 08:152.8 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 17:46 87-61-608/18/23 08:152.8 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 17:46 120-82-108/18/23 08:152.8 2.3 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 17:46 71-55-608/18/23 08:152.8 1.4 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 17:46 79-00-508/18/23 08:152.8 0.92 1
Trichloroethene ND ug/kg 08/18/23 17:46 79-01-608/18/23 08:152.8 2.2 1
Trichlorofluoromethane ND ug/kg 08/18/23 17:46 75-69-408/18/23 08:152.8 1.5 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 17:46 96-18-408/18/23 08:152.8 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 17:46 95-63-608/18/23 08:152.8 1.6 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 17:46 108-67-808/18/23 08:152.8 0.93 1
Vinyl acetate ND ug/kg 08/18/23 17:46 108-05-408/18/23 08:1527.8 5.7 1
Vinyl chloride ND ug/kg 08/18/23 17:46 75-01-408/18/23 08:155.6 1.4 1
Xylene (Total)1.9J ug/kg 08/18/23 17:46 1330-20-708/18/23 08:155.6 1.6 1
m&p-Xylene 1.9J ug/kg 08/18/23 17:46 179601-23-108/18/23 08:155.6 1.9 1
o-Xylene ND ug/kg 08/18/23 17:46 95-47-608/18/23 08:152.8 1.2 1
Surrogates
Toluene-d8 (S)99 %08/18/23 17:46 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)98 %08/18/23 17:46 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)95 %08/18/23 17:46 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.7 %08/17/23 17:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 3 Lab ID:92683348008 Collected:08/16/23 14:20 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)13.4 mg/kg 08/21/23 13:1008/18/23 14:226.1 4.3 1
Surrogates
n-Pentacosane (S)67 %08/21/23 13:10 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/18/23 23:2408/18/23 14:555.6 1.6 1
Surrogates
4-Bromofluorobenzene (S)107 %08/18/23 23:24 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 18:05 67-64-1 v208/18/23 08:1575.8 24.3 1
Benzene ND ug/kg 08/18/23 18:05 71-43-208/18/23 08:153.8 1.5 1
Bromobenzene ND ug/kg 08/18/23 18:05 108-86-108/18/23 08:153.8 1.2 1
Bromochloromethane ND ug/kg 08/18/23 18:05 74-97-508/18/23 08:153.8 1.1 1
Bromodichloromethane ND ug/kg 08/18/23 18:05 75-27-408/18/23 08:153.8 1.5 1
Bromoform ND ug/kg 08/18/23 18:05 75-25-208/18/23 08:153.8 1.3 1
Bromomethane ND ug/kg 08/18/23 18:05 74-83-9 v208/18/23 08:1515.2 11.7 1
2-Butanone (MEK)ND ug/kg 08/18/23 18:05 78-93-308/18/23 08:1575.8 18.2 1
n-Butylbenzene ND ug/kg 08/18/23 18:05 104-51-808/18/23 08:153.8 2.4 1
sec-Butylbenzene ND ug/kg 08/18/23 18:05 135-98-808/18/23 08:153.8 1.7 1
tert-Butylbenzene ND ug/kg 08/18/23 18:05 98-06-608/18/23 08:153.8 1.3 1
Carbon tetrachloride ND ug/kg 08/18/23 18:05 56-23-508/18/23 08:153.8 1.4 1
Chlorobenzene ND ug/kg 08/18/23 18:05 108-90-708/18/23 08:153.8 2.2 1
Chloroethane ND ug/kg 08/18/23 18:05 75-00-308/18/23 08:157.6 2.9 1
Chloroform ND ug/kg 08/18/23 18:05 67-66-308/18/23 08:153.8 3.2 1
Chloromethane ND ug/kg 08/18/23 18:05 74-87-308/18/23 08:157.6 3.2 1
2-Chlorotoluene ND ug/kg 08/18/23 18:05 95-49-808/18/23 08:153.8 1.3 1
4-Chlorotoluene ND ug/kg 08/18/23 18:05 106-43-408/18/23 08:153.8 2.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 18:05 96-12-808/18/23 08:153.8 1.5 1
Dibromochloromethane ND ug/kg 08/18/23 18:05 124-48-108/18/23 08:153.8 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 18:05 106-93-408/18/23 08:153.8 1.7 1
Dibromomethane ND ug/kg 08/18/23 18:05 74-95-308/18/23 08:153.8 0.81 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 18:05 95-50-108/18/23 08:153.8 1.4 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 18:05 541-73-108/18/23 08:153.8 1.2 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 18:05 106-46-708/18/23 08:153.8 0.99 1
Dichlorodifluoromethane ND ug/kg 08/18/23 18:05 75-71-808/18/23 08:157.6 3.9 1
1,1-Dichloroethane ND ug/kg 08/18/23 18:05 75-34-308/18/23 08:153.8 1.6 1
1,2-Dichloroethane ND ug/kg 08/18/23 18:05 107-06-208/18/23 08:153.8 2.5 1
1,1-Dichloroethene ND ug/kg 08/18/23 18:05 75-35-408/18/23 08:153.8 1.6 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 18:05 156-59-208/18/23 08:153.8 1.3 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 18:05 156-60-508/18/23 08:153.8 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 3 Lab ID:92683348008 Collected:08/16/23 14:20 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 18:05 78-87-508/18/23 08:153.8 1.1 1
1,3-Dichloropropane ND ug/kg 08/18/23 18:05 142-28-908/18/23 08:153.8 1.2 1
2,2-Dichloropropane ND ug/kg 08/18/23 18:05 594-20-708/18/23 08:153.8 2.9 1
1,1-Dichloropropene ND ug/kg 08/18/23 18:05 563-58-608/18/23 08:153.8 1.8 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 18:05 10061-01-508/18/23 08:153.8 1.0 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 18:05 10061-02-608/18/23 08:153.8 1.3 1
Diisopropyl ether ND ug/kg 08/18/23 18:05 108-20-308/18/23 08:153.8 1.0 1
Ethylbenzene 2.2J ug/kg 08/18/23 18:05 100-41-408/18/23 08:153.8 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 18:05 87-68-308/18/23 08:157.6 6.2 1
2-Hexanone ND ug/kg 08/18/23 18:05 591-78-608/18/23 08:1537.9 3.7 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 18:05 98-82-808/18/23 08:153.8 1.3 1
p-Isopropyltoluene ND ug/kg 08/18/23 18:05 99-87-608/18/23 08:153.8 1.9 1
Methylene Chloride ND ug/kg 08/18/23 18:05 75-09-208/18/23 08:1515.2 10.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 18:05 108-10-108/18/23 08:1537.9 3.7 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 18:05 1634-04-408/18/23 08:153.8 1.4 1
Naphthalene ND ug/kg 08/18/23 18:05 91-20-308/18/23 08:153.8 2.0 1
n-Propylbenzene ND ug/kg 08/18/23 18:05 103-65-108/18/23 08:153.8 1.3 1
Styrene 15.2 ug/kg 08/18/23 18:05 100-42-508/18/23 08:153.8 1.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 18:05 630-20-608/18/23 08:153.8 1.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 18:05 79-34-508/18/23 08:153.8 1.0 1
Tetrachloroethene ND ug/kg 08/18/23 18:05 127-18-408/18/23 08:153.8 1.2 1
Toluene 3.7J ug/kg 08/18/23 18:05 108-88-308/18/23 08:153.8 2.6 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 18:05 87-61-608/18/23 08:153.8 3.1 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 18:05 120-82-108/18/23 08:153.8 3.2 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 18:05 71-55-608/18/23 08:153.8 2.0 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 18:05 79-00-508/18/23 08:153.8 1.3 1
Trichloroethene ND ug/kg 08/18/23 18:05 79-01-608/18/23 08:153.8 3.1 1
Trichlorofluoromethane ND ug/kg 08/18/23 18:05 75-69-408/18/23 08:153.8 2.1 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 18:05 96-18-408/18/23 08:153.8 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 18:05 95-63-608/18/23 08:153.8 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 18:05 108-67-808/18/23 08:153.8 1.3 1
Vinyl acetate ND ug/kg 08/18/23 18:05 108-05-408/18/23 08:1537.9 7.8 1
Vinyl chloride ND ug/kg 08/18/23 18:05 75-01-408/18/23 08:157.6 1.9 1
Xylene (Total)ND ug/kg 08/18/23 18:05 1330-20-708/18/23 08:157.6 2.2 1
m&p-Xylene ND ug/kg 08/18/23 18:05 179601-23-108/18/23 08:157.6 2.6 1
o-Xylene ND ug/kg 08/18/23 18:05 95-47-608/18/23 08:153.8 1.7 1
Surrogates
Toluene-d8 (S)98 %08/18/23 18:05 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)98 %08/18/23 18:05 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)96 %08/18/23 18:05 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.7 %08/17/23 17:00 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-1 Lab ID:92683348009 Collected:08/16/23 14:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 13:2808/18/23 14:225.9 4.2 1
Surrogates
n-Pentacosane (S)86 %08/21/23 13:28 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/18/23 23:5008/18/23 14:554.4 1.2 1
Surrogates
4-Bromofluorobenzene (S)106 %08/18/23 23:50 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 18:24 67-64-1 v208/18/23 08:1589.3 28.7 1
Benzene ND ug/kg 08/18/23 18:24 71-43-208/18/23 08:154.5 1.8 1
Bromobenzene ND ug/kg 08/18/23 18:24 108-86-108/18/23 08:154.5 1.5 1
Bromochloromethane ND ug/kg 08/18/23 18:24 74-97-508/18/23 08:154.5 1.3 1
Bromodichloromethane ND ug/kg 08/18/23 18:24 75-27-408/18/23 08:154.5 1.7 1
Bromoform ND ug/kg 08/18/23 18:24 75-25-208/18/23 08:154.5 1.6 1
Bromomethane ND ug/kg 08/18/23 18:24 74-83-9 v208/18/23 08:1517.9 13.8 1
2-Butanone (MEK)ND ug/kg 08/18/23 18:24 78-93-308/18/23 08:1589.3 21.4 1
n-Butylbenzene ND ug/kg 08/18/23 18:24 104-51-808/18/23 08:154.5 2.8 1
sec-Butylbenzene ND ug/kg 08/18/23 18:24 135-98-808/18/23 08:154.5 2.0 1
tert-Butylbenzene ND ug/kg 08/18/23 18:24 98-06-608/18/23 08:154.5 1.6 1
Carbon tetrachloride ND ug/kg 08/18/23 18:24 56-23-508/18/23 08:154.5 1.7 1
Chlorobenzene ND ug/kg 08/18/23 18:24 108-90-708/18/23 08:154.5 2.6 1
Chloroethane ND ug/kg 08/18/23 18:24 75-00-308/18/23 08:158.9 3.4 1
Chloroform ND ug/kg 08/18/23 18:24 67-66-308/18/23 08:154.5 3.7 1
Chloromethane ND ug/kg 08/18/23 18:24 74-87-308/18/23 08:158.9 3.8 1
2-Chlorotoluene ND ug/kg 08/18/23 18:24 95-49-808/18/23 08:154.5 1.6 1
4-Chlorotoluene ND ug/kg 08/18/23 18:24 106-43-408/18/23 08:154.5 2.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 18:24 96-12-808/18/23 08:154.5 1.7 1
Dibromochloromethane ND ug/kg 08/18/23 18:24 124-48-108/18/23 08:154.5 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 18:24 106-93-408/18/23 08:154.5 2.0 1
Dibromomethane ND ug/kg 08/18/23 18:24 74-95-308/18/23 08:154.5 0.96 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 18:24 95-50-108/18/23 08:154.5 1.6 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 18:24 541-73-108/18/23 08:154.5 1.4 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 18:24 106-46-708/18/23 08:154.5 1.2 1
Dichlorodifluoromethane ND ug/kg 08/18/23 18:24 75-71-808/18/23 08:158.9 4.5 1
1,1-Dichloroethane ND ug/kg 08/18/23 18:24 75-34-308/18/23 08:154.5 1.8 1
1,2-Dichloroethane ND ug/kg 08/18/23 18:24 107-06-208/18/23 08:154.5 3.0 1
1,1-Dichloroethene ND ug/kg 08/18/23 18:24 75-35-408/18/23 08:154.5 1.8 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 18:24 156-59-208/18/23 08:154.5 1.5 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 18:24 156-60-508/18/23 08:154.5 3.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-1 Lab ID:92683348009 Collected:08/16/23 14:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 18:24 78-87-508/18/23 08:154.5 1.3 1
1,3-Dichloropropane ND ug/kg 08/18/23 18:24 142-28-908/18/23 08:154.5 1.4 1
2,2-Dichloropropane ND ug/kg 08/18/23 18:24 594-20-708/18/23 08:154.5 3.4 1
1,1-Dichloropropene ND ug/kg 08/18/23 18:24 563-58-608/18/23 08:154.5 2.1 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 18:24 10061-01-508/18/23 08:154.5 1.2 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 18:24 10061-02-608/18/23 08:154.5 1.5 1
Diisopropyl ether ND ug/kg 08/18/23 18:24 108-20-308/18/23 08:154.5 1.2 1
Ethylbenzene ND ug/kg 08/18/23 18:24 100-41-408/18/23 08:154.5 2.1 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 18:24 87-68-308/18/23 08:158.9 7.3 1
2-Hexanone ND ug/kg 08/18/23 18:24 591-78-608/18/23 08:1544.7 4.3 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 18:24 98-82-808/18/23 08:154.5 1.5 1
p-Isopropyltoluene ND ug/kg 08/18/23 18:24 99-87-608/18/23 08:154.5 2.2 1
Methylene Chloride ND ug/kg 08/18/23 18:24 75-09-208/18/23 08:1517.9 12.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 18:24 108-10-108/18/23 08:1544.7 4.3 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 18:24 1634-04-408/18/23 08:154.5 1.7 1
Naphthalene ND ug/kg 08/18/23 18:24 91-20-308/18/23 08:154.5 2.3 1
n-Propylbenzene ND ug/kg 08/18/23 18:24 103-65-108/18/23 08:154.5 1.6 1
Styrene ND ug/kg 08/18/23 18:24 100-42-508/18/23 08:154.5 1.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 18:24 630-20-608/18/23 08:154.5 1.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 18:24 79-34-508/18/23 08:154.5 1.2 1
Tetrachloroethene ND ug/kg 08/18/23 18:24 127-18-408/18/23 08:154.5 1.4 1
Toluene ND ug/kg 08/18/23 18:24 108-88-308/18/23 08:154.5 3.1 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 18:24 87-61-608/18/23 08:154.5 3.6 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 18:24 120-82-108/18/23 08:154.5 3.8 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 18:24 71-55-608/18/23 08:154.5 2.3 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 18:24 79-00-508/18/23 08:154.5 1.5 1
Trichloroethene ND ug/kg 08/18/23 18:24 79-01-608/18/23 08:154.5 3.6 1
Trichlorofluoromethane ND ug/kg 08/18/23 18:24 75-69-408/18/23 08:154.5 2.5 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 18:24 96-18-408/18/23 08:154.5 2.3 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 18:24 95-63-608/18/23 08:154.5 2.7 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 18:24 108-67-808/18/23 08:154.5 1.5 1
Vinyl acetate ND ug/kg 08/18/23 18:24 108-05-408/18/23 08:1544.7 9.2 1
Vinyl chloride ND ug/kg 08/18/23 18:24 75-01-408/18/23 08:158.9 2.3 1
Xylene (Total)ND ug/kg 08/18/23 18:24 1330-20-708/18/23 08:158.9 2.5 1
m&p-Xylene ND ug/kg 08/18/23 18:24 179601-23-108/18/23 08:158.9 3.1 1
o-Xylene ND ug/kg 08/18/23 18:24 95-47-608/18/23 08:154.5 2.0 1
Surrogates
Toluene-d8 (S)98 %08/18/23 18:24 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)97 %08/18/23 18:24 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)93 %08/18/23 18:24 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.4 %08/17/23 17:01 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-2 Lab ID:92683348010 Collected:08/16/23 14:35 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 13:2808/18/23 14:225.8 4.1 1
Surrogates
n-Pentacosane (S)83 %08/21/23 13:28 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 00:1608/18/23 14:554.9 1.4 1
Surrogates
4-Bromofluorobenzene (S)106 %08/19/23 00:16 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 18:42 67-64-1 v208/18/23 08:1572.2 23.2 1
Benzene ND ug/kg 08/18/23 18:42 71-43-208/18/23 08:153.6 1.4 1
Bromobenzene ND ug/kg 08/18/23 18:42 108-86-108/18/23 08:153.6 1.2 1
Bromochloromethane ND ug/kg 08/18/23 18:42 74-97-508/18/23 08:153.6 1.1 1
Bromodichloromethane ND ug/kg 08/18/23 18:42 75-27-408/18/23 08:153.6 1.4 1
Bromoform ND ug/kg 08/18/23 18:42 75-25-208/18/23 08:153.6 1.3 1
Bromomethane ND ug/kg 08/18/23 18:42 74-83-9 v208/18/23 08:1514.4 11.2 1
2-Butanone (MEK)ND ug/kg 08/18/23 18:42 78-93-308/18/23 08:1572.2 17.3 1
n-Butylbenzene ND ug/kg 08/18/23 18:42 104-51-808/18/23 08:153.6 2.3 1
sec-Butylbenzene ND ug/kg 08/18/23 18:42 135-98-808/18/23 08:153.6 1.6 1
tert-Butylbenzene ND ug/kg 08/18/23 18:42 98-06-608/18/23 08:153.6 1.3 1
Carbon tetrachloride ND ug/kg 08/18/23 18:42 56-23-508/18/23 08:153.6 1.4 1
Chlorobenzene ND ug/kg 08/18/23 18:42 108-90-708/18/23 08:153.6 2.1 1
Chloroethane ND ug/kg 08/18/23 18:42 75-00-308/18/23 08:157.2 2.8 1
Chloroform ND ug/kg 08/18/23 18:42 67-66-308/18/23 08:153.6 3.0 1
Chloromethane ND ug/kg 08/18/23 18:42 74-87-308/18/23 08:157.2 3.0 1
2-Chlorotoluene ND ug/kg 08/18/23 18:42 95-49-808/18/23 08:153.6 1.3 1
4-Chlorotoluene ND ug/kg 08/18/23 18:42 106-43-408/18/23 08:153.6 2.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 18:42 96-12-808/18/23 08:153.6 1.4 1
Dibromochloromethane ND ug/kg 08/18/23 18:42 124-48-108/18/23 08:153.6 2.0 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 18:42 106-93-408/18/23 08:153.6 1.6 1
Dibromomethane ND ug/kg 08/18/23 18:42 74-95-308/18/23 08:153.6 0.77 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 18:42 95-50-108/18/23 08:153.6 1.3 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 18:42 541-73-108/18/23 08:153.6 1.1 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 18:42 106-46-708/18/23 08:153.6 0.94 1
Dichlorodifluoromethane ND ug/kg 08/18/23 18:42 75-71-808/18/23 08:157.2 3.7 1
1,1-Dichloroethane ND ug/kg 08/18/23 18:42 75-34-308/18/23 08:153.6 1.5 1
1,2-Dichloroethane ND ug/kg 08/18/23 18:42 107-06-208/18/23 08:153.6 2.4 1
1,1-Dichloroethene ND ug/kg 08/18/23 18:42 75-35-408/18/23 08:153.6 1.5 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 18:42 156-59-208/18/23 08:153.6 1.2 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 18:42 156-60-508/18/23 08:153.6 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-2 Lab ID:92683348010 Collected:08/16/23 14:35 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 18:42 78-87-508/18/23 08:153.6 1.1 1
1,3-Dichloropropane ND ug/kg 08/18/23 18:42 142-28-908/18/23 08:153.6 1.1 1
2,2-Dichloropropane ND ug/kg 08/18/23 18:42 594-20-708/18/23 08:153.6 2.7 1
1,1-Dichloropropene ND ug/kg 08/18/23 18:42 563-58-608/18/23 08:153.6 1.7 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 18:42 10061-01-508/18/23 08:153.6 0.98 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 18:42 10061-02-608/18/23 08:153.6 1.2 1
Diisopropyl ether ND ug/kg 08/18/23 18:42 108-20-308/18/23 08:153.6 0.97 1
Ethylbenzene ND ug/kg 08/18/23 18:42 100-41-408/18/23 08:153.6 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 18:42 87-68-308/18/23 08:157.2 5.9 1
2-Hexanone ND ug/kg 08/18/23 18:42 591-78-608/18/23 08:1536.1 3.5 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 18:42 98-82-808/18/23 08:153.6 1.2 1
p-Isopropyltoluene ND ug/kg 08/18/23 18:42 99-87-608/18/23 08:153.6 1.8 1
Methylene Chloride ND ug/kg 08/18/23 18:42 75-09-208/18/23 08:1514.4 9.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 18:42 108-10-108/18/23 08:1536.1 3.5 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 18:42 1634-04-408/18/23 08:153.6 1.4 1
Naphthalene ND ug/kg 08/18/23 18:42 91-20-308/18/23 08:153.6 1.9 1
n-Propylbenzene ND ug/kg 08/18/23 18:42 103-65-108/18/23 08:153.6 1.3 1
Styrene ND ug/kg 08/18/23 18:42 100-42-508/18/23 08:153.6 0.95 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 18:42 630-20-608/18/23 08:153.6 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 18:42 79-34-508/18/23 08:153.6 0.95 1
Tetrachloroethene ND ug/kg 08/18/23 18:42 127-18-408/18/23 08:153.6 1.1 1
Toluene ND ug/kg 08/18/23 18:42 108-88-308/18/23 08:153.6 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 18:42 87-61-608/18/23 08:153.6 2.9 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 18:42 120-82-108/18/23 08:153.6 3.0 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 18:42 71-55-608/18/23 08:153.6 1.9 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 18:42 79-00-508/18/23 08:153.6 1.2 1
Trichloroethene ND ug/kg 08/18/23 18:42 79-01-608/18/23 08:153.6 2.9 1
Trichlorofluoromethane ND ug/kg 08/18/23 18:42 75-69-408/18/23 08:153.6 2.0 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 18:42 96-18-408/18/23 08:153.6 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 18:42 95-63-608/18/23 08:153.6 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 18:42 108-67-808/18/23 08:153.6 1.2 1
Vinyl acetate ND ug/kg 08/18/23 18:42 108-05-408/18/23 08:1536.1 7.4 1
Vinyl chloride ND ug/kg 08/18/23 18:42 75-01-408/18/23 08:157.2 1.8 1
Xylene (Total)ND ug/kg 08/18/23 18:42 1330-20-708/18/23 08:157.2 2.1 1
m&p-Xylene ND ug/kg 08/18/23 18:42 179601-23-108/18/23 08:157.2 2.5 1
o-Xylene ND ug/kg 08/18/23 18:42 95-47-608/18/23 08:153.6 1.6 1
Surrogates
Toluene-d8 (S)98 %08/18/23 18:42 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)97 %08/18/23 18:42 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)93 %08/18/23 18:42 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.9 %08/17/23 17:01 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-3 Lab ID:92683348011 Collected:08/16/23 14:40 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 13:4608/18/23 14:225.8 4.2 1
Surrogates
n-Pentacosane (S)84 %08/21/23 13:46 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 00:4208/18/23 14:553.7 1.0 1
Surrogates
4-Bromofluorobenzene (S)107 %08/19/23 00:42 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 19:01 67-64-1 v208/18/23 08:1565.8 21.1 1
Benzene ND ug/kg 08/18/23 19:01 71-43-208/18/23 08:153.3 1.3 1
Bromobenzene ND ug/kg 08/18/23 19:01 108-86-108/18/23 08:153.3 1.1 1
Bromochloromethane ND ug/kg 08/18/23 19:01 74-97-508/18/23 08:153.3 0.97 1
Bromodichloromethane ND ug/kg 08/18/23 19:01 75-27-408/18/23 08:153.3 1.3 1
Bromoform ND ug/kg 08/18/23 19:01 75-25-208/18/23 08:153.3 1.2 1
Bromomethane ND ug/kg 08/18/23 19:01 74-83-9 v208/18/23 08:1513.2 10.2 1
2-Butanone (MEK)ND ug/kg 08/18/23 19:01 78-93-308/18/23 08:1565.8 15.8 1
n-Butylbenzene ND ug/kg 08/18/23 19:01 104-51-808/18/23 08:153.3 2.1 1
sec-Butylbenzene ND ug/kg 08/18/23 19:01 135-98-808/18/23 08:153.3 1.4 1
tert-Butylbenzene ND ug/kg 08/18/23 19:01 98-06-608/18/23 08:153.3 1.2 1
Carbon tetrachloride ND ug/kg 08/18/23 19:01 56-23-508/18/23 08:153.3 1.2 1
Chlorobenzene ND ug/kg 08/18/23 19:01 108-90-708/18/23 08:153.3 1.9 1
Chloroethane ND ug/kg 08/18/23 19:01 75-00-308/18/23 08:156.6 2.5 1
Chloroform ND ug/kg 08/18/23 19:01 67-66-308/18/23 08:153.3 2.8 1
Chloromethane ND ug/kg 08/18/23 19:01 74-87-308/18/23 08:156.6 2.8 1
2-Chlorotoluene ND ug/kg 08/18/23 19:01 95-49-808/18/23 08:153.3 1.2 1
4-Chlorotoluene ND ug/kg 08/18/23 19:01 106-43-408/18/23 08:153.3 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 19:01 96-12-808/18/23 08:153.3 1.3 1
Dibromochloromethane ND ug/kg 08/18/23 19:01 124-48-108/18/23 08:153.3 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 19:01 106-93-408/18/23 08:153.3 1.4 1
Dibromomethane ND ug/kg 08/18/23 19:01 74-95-308/18/23 08:153.3 0.70 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 19:01 95-50-108/18/23 08:153.3 1.2 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 19:01 541-73-108/18/23 08:153.3 1.0 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 19:01 106-46-708/18/23 08:153.3 0.86 1
Dichlorodifluoromethane ND ug/kg 08/18/23 19:01 75-71-808/18/23 08:156.6 3.4 1
1,1-Dichloroethane ND ug/kg 08/18/23 19:01 75-34-308/18/23 08:153.3 1.4 1
1,2-Dichloroethane ND ug/kg 08/18/23 19:01 107-06-208/18/23 08:153.3 2.2 1
1,1-Dichloroethene ND ug/kg 08/18/23 19:01 75-35-408/18/23 08:153.3 1.4 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 19:01 156-59-208/18/23 08:153.3 1.1 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 19:01 156-60-508/18/23 08:153.3 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-3 Lab ID:92683348011 Collected:08/16/23 14:40 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 19:01 78-87-508/18/23 08:153.3 0.99 1
1,3-Dichloropropane ND ug/kg 08/18/23 19:01 142-28-908/18/23 08:153.3 1.0 1
2,2-Dichloropropane ND ug/kg 08/18/23 19:01 594-20-708/18/23 08:153.3 2.5 1
1,1-Dichloropropene ND ug/kg 08/18/23 19:01 563-58-608/18/23 08:153.3 1.6 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 19:01 10061-01-508/18/23 08:153.3 0.90 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 19:01 10061-02-608/18/23 08:153.3 1.1 1
Diisopropyl ether ND ug/kg 08/18/23 19:01 108-20-308/18/23 08:153.3 0.89 1
Ethylbenzene ND ug/kg 08/18/23 19:01 100-41-408/18/23 08:153.3 1.5 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 19:01 87-68-308/18/23 08:156.6 5.4 1
2-Hexanone ND ug/kg 08/18/23 19:01 591-78-608/18/23 08:1532.9 3.2 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 19:01 98-82-808/18/23 08:153.3 1.1 1
p-Isopropyltoluene ND ug/kg 08/18/23 19:01 99-87-608/18/23 08:153.3 1.6 1
Methylene Chloride ND ug/kg 08/18/23 19:01 75-09-208/18/23 08:1513.2 9.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 19:01 108-10-108/18/23 08:1532.9 3.2 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 19:01 1634-04-408/18/23 08:153.3 1.2 1
Naphthalene ND ug/kg 08/18/23 19:01 91-20-308/18/23 08:153.3 1.7 1
n-Propylbenzene ND ug/kg 08/18/23 19:01 103-65-108/18/23 08:153.3 1.2 1
Styrene ND ug/kg 08/18/23 19:01 100-42-508/18/23 08:153.3 0.87 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 19:01 630-20-608/18/23 08:153.3 1.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 19:01 79-34-508/18/23 08:153.3 0.87 1
Tetrachloroethene ND ug/kg 08/18/23 19:01 127-18-408/18/23 08:153.3 1.0 1
Toluene ND ug/kg 08/18/23 19:01 108-88-308/18/23 08:153.3 2.3 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 19:01 87-61-608/18/23 08:153.3 2.7 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 19:01 120-82-108/18/23 08:153.3 2.8 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 19:01 71-55-608/18/23 08:153.3 1.7 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 19:01 79-00-508/18/23 08:153.3 1.1 1
Trichloroethene ND ug/kg 08/18/23 19:01 79-01-608/18/23 08:153.3 2.7 1
Trichlorofluoromethane ND ug/kg 08/18/23 19:01 75-69-408/18/23 08:153.3 1.8 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 19:01 96-18-408/18/23 08:153.3 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 19:01 95-63-608/18/23 08:153.3 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 19:01 108-67-808/18/23 08:153.3 1.1 1
Vinyl acetate ND ug/kg 08/18/23 19:01 108-05-408/18/23 08:1532.9 6.8 1
Vinyl chloride ND ug/kg 08/18/23 19:01 75-01-408/18/23 08:156.6 1.7 1
Xylene (Total)ND ug/kg 08/18/23 19:01 1330-20-708/18/23 08:156.6 1.9 1
m&p-Xylene ND ug/kg 08/18/23 19:01 179601-23-108/18/23 08:156.6 2.3 1
o-Xylene ND ug/kg 08/18/23 19:01 95-47-608/18/23 08:153.3 1.5 1
Surrogates
Toluene-d8 (S)98 %08/18/23 19:01 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)98 %08/18/23 19:01 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)93 %08/18/23 19:01 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.3 %08/17/23 17:01 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-4 Lab ID:92683348012 Collected:08/16/23 14:45 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 13:4608/18/23 14:226.0 4.3 1
Surrogates
n-Pentacosane (S)87 %08/21/23 13:46 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 01:0708/18/23 14:554.2 1.2 1
Surrogates
4-Bromofluorobenzene (S)106 %08/19/23 01:07 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 19:20 67-64-1 v208/18/23 08:1513643.6 1
Benzene ND ug/kg 08/18/23 19:20 71-43-208/18/23 08:156.8 2.7 1
Bromobenzene ND ug/kg 08/18/23 19:20 108-86-108/18/23 08:156.8 2.2 1
Bromochloromethane ND ug/kg 08/18/23 19:20 74-97-508/18/23 08:156.8 2.0 1
Bromodichloromethane ND ug/kg 08/18/23 19:20 75-27-408/18/23 08:156.8 2.6 1
Bromoform ND ug/kg 08/18/23 19:20 75-25-208/18/23 08:156.8 2.4 1
Bromomethane ND ug/kg 08/18/23 19:20 74-83-9 v208/18/23 08:1527.2 21.0 1
2-Butanone (MEK)ND ug/kg 08/18/23 19:20 78-93-308/18/23 08:1513632.6 1
n-Butylbenzene ND ug/kg 08/18/23 19:20 104-51-808/18/23 08:156.8 4.3 1
sec-Butylbenzene ND ug/kg 08/18/23 19:20 135-98-808/18/23 08:156.8 3.0 1
tert-Butylbenzene ND ug/kg 08/18/23 19:20 98-06-608/18/23 08:156.8 2.4 1
Carbon tetrachloride ND ug/kg 08/18/23 19:20 56-23-508/18/23 08:156.8 2.5 1
Chlorobenzene ND ug/kg 08/18/23 19:20 108-90-708/18/23 08:156.8 3.9 1
Chloroethane ND ug/kg 08/18/23 19:20 75-00-308/18/23 08:1513.6 5.2 1
Chloroform ND ug/kg 08/18/23 19:20 67-66-308/18/23 08:156.8 5.7 1
Chloromethane ND ug/kg 08/18/23 19:20 74-87-308/18/23 08:1513.6 5.7 1
2-Chlorotoluene ND ug/kg 08/18/23 19:20 95-49-808/18/23 08:156.8 2.4 1
4-Chlorotoluene ND ug/kg 08/18/23 19:20 106-43-408/18/23 08:156.8 3.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 19:20 96-12-808/18/23 08:156.8 2.6 1
Dibromochloromethane ND ug/kg 08/18/23 19:20 124-48-108/18/23 08:156.8 3.8 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 19:20 106-93-408/18/23 08:156.8 3.0 1
Dibromomethane ND ug/kg 08/18/23 19:20 74-95-308/18/23 08:156.8 1.5 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 19:20 95-50-108/18/23 08:156.8 2.4 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 19:20 541-73-108/18/23 08:156.8 2.1 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 19:20 106-46-708/18/23 08:156.8 1.8 1
Dichlorodifluoromethane ND ug/kg 08/18/23 19:20 75-71-808/18/23 08:1513.6 6.9 1
1,1-Dichloroethane ND ug/kg 08/18/23 19:20 75-34-308/18/23 08:156.8 2.8 1
1,2-Dichloroethane ND ug/kg 08/18/23 19:20 107-06-208/18/23 08:156.8 4.5 1
1,1-Dichloroethene ND ug/kg 08/18/23 19:20 75-35-408/18/23 08:156.8 2.8 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 19:20 156-59-208/18/23 08:156.8 2.3 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 19:20 156-60-508/18/23 08:156.8 5.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-4 Lab ID:92683348012 Collected:08/16/23 14:45 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 19:20 78-87-508/18/23 08:156.8 2.0 1
1,3-Dichloropropane ND ug/kg 08/18/23 19:20 142-28-908/18/23 08:156.8 2.1 1
2,2-Dichloropropane ND ug/kg 08/18/23 19:20 594-20-708/18/23 08:156.8 5.1 1
1,1-Dichloropropene ND ug/kg 08/18/23 19:20 563-58-608/18/23 08:156.8 3.3 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 19:20 10061-01-508/18/23 08:156.8 1.8 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 19:20 10061-02-608/18/23 08:156.8 2.3 1
Diisopropyl ether ND ug/kg 08/18/23 19:20 108-20-308/18/23 08:156.8 1.8 1
Ethylbenzene ND ug/kg 08/18/23 19:20 100-41-408/18/23 08:156.8 3.2 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 19:20 87-68-308/18/23 08:1513.6 11.1 1
2-Hexanone ND ug/kg 08/18/23 19:20 591-78-608/18/23 08:1567.9 6.5 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 19:20 98-82-808/18/23 08:156.8 2.3 1
p-Isopropyltoluene ND ug/kg 08/18/23 19:20 99-87-608/18/23 08:156.8 3.3 1
Methylene Chloride ND ug/kg 08/18/23 19:20 75-09-208/18/23 08:1527.2 18.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 19:20 108-10-108/18/23 08:1567.9 6.5 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 19:20 1634-04-408/18/23 08:156.8 2.5 1
Naphthalene ND ug/kg 08/18/23 19:20 91-20-308/18/23 08:156.8 3.6 1
n-Propylbenzene ND ug/kg 08/18/23 19:20 103-65-108/18/23 08:156.8 2.4 1
Styrene ND ug/kg 08/18/23 19:20 100-42-508/18/23 08:156.8 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 19:20 630-20-608/18/23 08:156.8 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 19:20 79-34-508/18/23 08:156.8 1.8 1
Tetrachloroethene ND ug/kg 08/18/23 19:20 127-18-408/18/23 08:156.8 2.1 1
Toluene ND ug/kg 08/18/23 19:20 108-88-308/18/23 08:156.8 4.7 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 19:20 87-61-608/18/23 08:156.8 5.5 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 19:20 120-82-108/18/23 08:156.8 5.7 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 19:20 71-55-608/18/23 08:156.8 3.5 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 19:20 79-00-508/18/23 08:156.8 2.3 1
Trichloroethene ND ug/kg 08/18/23 19:20 79-01-608/18/23 08:156.8 5.5 1
Trichlorofluoromethane ND ug/kg 08/18/23 19:20 75-69-408/18/23 08:156.8 3.7 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 19:20 96-18-408/18/23 08:156.8 3.4 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 19:20 95-63-608/18/23 08:156.8 4.0 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 19:20 108-67-808/18/23 08:156.8 2.3 1
Vinyl acetate ND ug/kg 08/18/23 19:20 108-05-408/18/23 08:1567.9 14.0 1
Vinyl chloride ND ug/kg 08/18/23 19:20 75-01-408/18/23 08:1513.6 3.4 1
Xylene (Total)6.0J ug/kg 08/18/23 19:20 1330-20-708/18/23 08:1513.6 3.9 1
m&p-Xylene 6.0J ug/kg 08/18/23 19:20 179601-23-108/18/23 08:1513.6 4.6 1
o-Xylene ND ug/kg 08/18/23 19:20 95-47-608/18/23 08:156.8 3.0 1
Surrogates
Toluene-d8 (S)98 %08/18/23 19:20 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)96 %08/18/23 19:20 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)95 %08/18/23 19:20 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.4 %08/17/23 17:25 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-5 Lab ID:92683348013 Collected:08/16/23 15:25 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 14:0408/18/23 14:226.1 4.3 1
Surrogates
n-Pentacosane (S)74 %08/21/23 14:04 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 01:3308/18/23 14:556.1 1.7 1
Surrogates
4-Bromofluorobenzene (S)107 %08/19/23 01:33 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 19:38 67-64-1 v208/18/23 08:1576.4 24.5 1
Benzene ND ug/kg 08/18/23 19:38 71-43-208/18/23 08:153.8 1.5 1
Bromobenzene ND ug/kg 08/18/23 19:38 108-86-108/18/23 08:153.8 1.2 1
Bromochloromethane ND ug/kg 08/18/23 19:38 74-97-508/18/23 08:153.8 1.1 1
Bromodichloromethane ND ug/kg 08/18/23 19:38 75-27-408/18/23 08:153.8 1.5 1
Bromoform ND ug/kg 08/18/23 19:38 75-25-208/18/23 08:153.8 1.3 1
Bromomethane ND ug/kg 08/18/23 19:38 74-83-9 v208/18/23 08:1515.3 11.8 1
2-Butanone (MEK)ND ug/kg 08/18/23 19:38 78-93-308/18/23 08:1576.4 18.3 1
n-Butylbenzene ND ug/kg 08/18/23 19:38 104-51-808/18/23 08:153.8 2.4 1
sec-Butylbenzene ND ug/kg 08/18/23 19:38 135-98-808/18/23 08:153.8 1.7 1
tert-Butylbenzene ND ug/kg 08/18/23 19:38 98-06-608/18/23 08:153.8 1.4 1
Carbon tetrachloride ND ug/kg 08/18/23 19:38 56-23-508/18/23 08:153.8 1.4 1
Chlorobenzene ND ug/kg 08/18/23 19:38 108-90-708/18/23 08:153.8 2.2 1
Chloroethane ND ug/kg 08/18/23 19:38 75-00-308/18/23 08:157.6 2.9 1
Chloroform ND ug/kg 08/18/23 19:38 67-66-308/18/23 08:153.8 3.2 1
Chloromethane ND ug/kg 08/18/23 19:38 74-87-308/18/23 08:157.6 3.2 1
2-Chlorotoluene ND ug/kg 08/18/23 19:38 95-49-808/18/23 08:153.8 1.4 1
4-Chlorotoluene ND ug/kg 08/18/23 19:38 106-43-408/18/23 08:153.8 2.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 19:38 96-12-808/18/23 08:153.8 1.5 1
Dibromochloromethane ND ug/kg 08/18/23 19:38 124-48-108/18/23 08:153.8 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 19:38 106-93-408/18/23 08:153.8 1.7 1
Dibromomethane ND ug/kg 08/18/23 19:38 74-95-308/18/23 08:153.8 0.82 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 19:38 95-50-108/18/23 08:153.8 1.4 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 19:38 541-73-108/18/23 08:153.8 1.2 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 19:38 106-46-708/18/23 08:153.8 0.99 1
Dichlorodifluoromethane ND ug/kg 08/18/23 19:38 75-71-808/18/23 08:157.6 3.9 1
1,1-Dichloroethane ND ug/kg 08/18/23 19:38 75-34-308/18/23 08:153.8 1.6 1
1,2-Dichloroethane ND ug/kg 08/18/23 19:38 107-06-208/18/23 08:153.8 2.5 1
1,1-Dichloroethene ND ug/kg 08/18/23 19:38 75-35-408/18/23 08:153.8 1.6 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 19:38 156-59-208/18/23 08:153.8 1.3 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 19:38 156-60-508/18/23 08:153.8 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-5 Lab ID:92683348013 Collected:08/16/23 15:25 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 19:38 78-87-508/18/23 08:153.8 1.1 1
1,3-Dichloropropane ND ug/kg 08/18/23 19:38 142-28-908/18/23 08:153.8 1.2 1
2,2-Dichloropropane ND ug/kg 08/18/23 19:38 594-20-708/18/23 08:153.8 2.9 1
1,1-Dichloropropene ND ug/kg 08/18/23 19:38 563-58-608/18/23 08:153.8 1.8 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 19:38 10061-01-508/18/23 08:153.8 1.0 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 19:38 10061-02-608/18/23 08:153.8 1.3 1
Diisopropyl ether ND ug/kg 08/18/23 19:38 108-20-308/18/23 08:153.8 1.0 1
Ethylbenzene ND ug/kg 08/18/23 19:38 100-41-408/18/23 08:153.8 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 19:38 87-68-308/18/23 08:157.6 6.2 1
2-Hexanone ND ug/kg 08/18/23 19:38 591-78-608/18/23 08:1538.2 3.7 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 19:38 98-82-808/18/23 08:153.8 1.3 1
p-Isopropyltoluene ND ug/kg 08/18/23 19:38 99-87-608/18/23 08:153.8 1.9 1
Methylene Chloride ND ug/kg 08/18/23 19:38 75-09-208/18/23 08:1515.3 10.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 19:38 108-10-108/18/23 08:1538.2 3.7 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 19:38 1634-04-408/18/23 08:153.8 1.4 1
Naphthalene ND ug/kg 08/18/23 19:38 91-20-308/18/23 08:153.8 2.0 1
n-Propylbenzene ND ug/kg 08/18/23 19:38 103-65-108/18/23 08:153.8 1.4 1
Styrene ND ug/kg 08/18/23 19:38 100-42-508/18/23 08:153.8 1.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 19:38 630-20-608/18/23 08:153.8 1.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 19:38 79-34-508/18/23 08:153.8 1.0 1
Tetrachloroethene ND ug/kg 08/18/23 19:38 127-18-408/18/23 08:153.8 1.2 1
Toluene ND ug/kg 08/18/23 19:38 108-88-308/18/23 08:153.8 2.6 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 19:38 87-61-608/18/23 08:153.8 3.1 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 19:38 120-82-108/18/23 08:153.8 3.2 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 19:38 71-55-608/18/23 08:153.8 2.0 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 19:38 79-00-508/18/23 08:153.8 1.3 1
Trichloroethene ND ug/kg 08/18/23 19:38 79-01-608/18/23 08:153.8 3.1 1
Trichlorofluoromethane ND ug/kg 08/18/23 19:38 75-69-408/18/23 08:153.8 2.1 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 19:38 96-18-408/18/23 08:153.8 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 19:38 95-63-608/18/23 08:153.8 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 19:38 108-67-808/18/23 08:153.8 1.3 1
Vinyl acetate ND ug/kg 08/18/23 19:38 108-05-408/18/23 08:1538.2 7.9 1
Vinyl chloride ND ug/kg 08/18/23 19:38 75-01-408/18/23 08:157.6 1.9 1
Xylene (Total)ND ug/kg 08/18/23 19:38 1330-20-708/18/23 08:157.6 2.2 1
m&p-Xylene ND ug/kg 08/18/23 19:38 179601-23-108/18/23 08:157.6 2.6 1
o-Xylene ND ug/kg 08/18/23 19:38 95-47-608/18/23 08:153.8 1.7 1
Surrogates
Toluene-d8 (S)98 %08/18/23 19:38 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)97 %08/18/23 19:38 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)98 %08/18/23 19:38 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.3 %08/17/23 17:25 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-6 Lab ID:92683348014 Collected:08/16/23 15:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 14:0408/18/23 14:226.1 4.3 1
Surrogates
n-Pentacosane (S)87 %08/21/23 14:04 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 01:5908/18/23 14:555.6 1.6 1
Surrogates
4-Bromofluorobenzene (S)107 %08/19/23 01:59 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 19:57 67-64-1 v208/18/23 08:1512941.5 1
Benzene ND ug/kg 08/18/23 19:57 71-43-208/18/23 08:156.5 2.6 1
Bromobenzene ND ug/kg 08/18/23 19:57 108-86-108/18/23 08:156.5 2.1 1
Bromochloromethane ND ug/kg 08/18/23 19:57 74-97-508/18/23 08:156.5 1.9 1
Bromodichloromethane ND ug/kg 08/18/23 19:57 75-27-408/18/23 08:156.5 2.5 1
Bromoform ND ug/kg 08/18/23 19:57 75-25-208/18/23 08:156.5 2.3 1
Bromomethane ND ug/kg 08/18/23 19:57 74-83-9 v208/18/23 08:1525.9 20.1 1
2-Butanone (MEK)ND ug/kg 08/18/23 19:57 78-93-308/18/23 08:1512931.0 1
n-Butylbenzene ND ug/kg 08/18/23 19:57 104-51-808/18/23 08:156.5 4.1 1
sec-Butylbenzene ND ug/kg 08/18/23 19:57 135-98-808/18/23 08:156.5 2.8 1
tert-Butylbenzene ND ug/kg 08/18/23 19:57 98-06-608/18/23 08:156.5 2.3 1
Carbon tetrachloride ND ug/kg 08/18/23 19:57 56-23-508/18/23 08:156.5 2.4 1
Chlorobenzene ND ug/kg 08/18/23 19:57 108-90-708/18/23 08:156.5 3.7 1
Chloroethane ND ug/kg 08/18/23 19:57 75-00-308/18/23 08:1512.9 5.0 1
Chloroform ND ug/kg 08/18/23 19:57 67-66-308/18/23 08:156.5 5.4 1
Chloromethane ND ug/kg 08/18/23 19:57 74-87-308/18/23 08:1512.9 5.4 1
2-Chlorotoluene ND ug/kg 08/18/23 19:57 95-49-808/18/23 08:156.5 2.3 1
4-Chlorotoluene ND ug/kg 08/18/23 19:57 106-43-408/18/23 08:156.5 3.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 19:57 96-12-808/18/23 08:156.5 2.5 1
Dibromochloromethane ND ug/kg 08/18/23 19:57 124-48-108/18/23 08:156.5 3.6 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 19:57 106-93-408/18/23 08:156.5 2.8 1
Dibromomethane ND ug/kg 08/18/23 19:57 74-95-308/18/23 08:156.5 1.4 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 19:57 95-50-108/18/23 08:156.5 2.3 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 19:57 541-73-108/18/23 08:156.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 19:57 106-46-708/18/23 08:156.5 1.7 1
Dichlorodifluoromethane ND ug/kg 08/18/23 19:57 75-71-808/18/23 08:1512.9 6.6 1
1,1-Dichloroethane ND ug/kg 08/18/23 19:57 75-34-308/18/23 08:156.5 2.7 1
1,2-Dichloroethane ND ug/kg 08/18/23 19:57 107-06-208/18/23 08:156.5 4.3 1
1,1-Dichloroethene ND ug/kg 08/18/23 19:57 75-35-408/18/23 08:156.5 2.7 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 19:57 156-59-208/18/23 08:156.5 2.2 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 19:57 156-60-508/18/23 08:156.5 5.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-6 Lab ID:92683348014 Collected:08/16/23 15:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 19:57 78-87-508/18/23 08:156.5 1.9 1
1,3-Dichloropropane ND ug/kg 08/18/23 19:57 142-28-908/18/23 08:156.5 2.0 1
2,2-Dichloropropane ND ug/kg 08/18/23 19:57 594-20-708/18/23 08:156.5 4.9 1
1,1-Dichloropropene ND ug/kg 08/18/23 19:57 563-58-608/18/23 08:156.5 3.1 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 19:57 10061-01-508/18/23 08:156.5 1.8 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 19:57 10061-02-608/18/23 08:156.5 2.2 1
Diisopropyl ether ND ug/kg 08/18/23 19:57 108-20-308/18/23 08:156.5 1.7 1
Ethylbenzene ND ug/kg 08/18/23 19:57 100-41-408/18/23 08:156.5 3.0 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 19:57 87-68-308/18/23 08:1512.9 10.6 1
2-Hexanone ND ug/kg 08/18/23 19:57 591-78-608/18/23 08:1564.7 6.2 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 19:57 98-82-808/18/23 08:156.5 2.2 1
p-Isopropyltoluene ND ug/kg 08/18/23 19:57 99-87-608/18/23 08:156.5 3.2 1
Methylene Chloride ND ug/kg 08/18/23 19:57 75-09-208/18/23 08:1525.9 17.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 19:57 108-10-108/18/23 08:1564.7 6.2 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 19:57 1634-04-408/18/23 08:156.5 2.4 1
Naphthalene ND ug/kg 08/18/23 19:57 91-20-308/18/23 08:156.5 3.4 1
n-Propylbenzene ND ug/kg 08/18/23 19:57 103-65-108/18/23 08:156.5 2.3 1
Styrene ND ug/kg 08/18/23 19:57 100-42-508/18/23 08:156.5 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 19:57 630-20-608/18/23 08:156.5 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 19:57 79-34-508/18/23 08:156.5 1.7 1
Tetrachloroethene ND ug/kg 08/18/23 19:57 127-18-408/18/23 08:156.5 2.0 1
Toluene ND ug/kg 08/18/23 19:57 108-88-308/18/23 08:156.5 4.5 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 19:57 87-61-608/18/23 08:156.5 5.2 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 19:57 120-82-108/18/23 08:156.5 5.4 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 19:57 71-55-608/18/23 08:156.5 3.4 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 19:57 79-00-508/18/23 08:156.5 2.1 1
Trichloroethene ND ug/kg 08/18/23 19:57 79-01-608/18/23 08:156.5 5.2 1
Trichlorofluoromethane ND ug/kg 08/18/23 19:57 75-69-408/18/23 08:156.5 3.6 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 19:57 96-18-408/18/23 08:156.5 3.3 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 19:57 95-63-608/18/23 08:156.5 3.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 19:57 108-67-808/18/23 08:156.5 2.2 1
Vinyl acetate ND ug/kg 08/18/23 19:57 108-05-408/18/23 08:1564.7 13.3 1
Vinyl chloride ND ug/kg 08/18/23 19:57 75-01-408/18/23 08:1512.9 3.3 1
Xylene (Total)ND ug/kg 08/18/23 19:57 1330-20-708/18/23 08:1512.9 3.7 1
m&p-Xylene ND ug/kg 08/18/23 19:57 179601-23-108/18/23 08:1512.9 4.4 1
o-Xylene ND ug/kg 08/18/23 19:57 95-47-608/18/23 08:156.5 2.9 1
Surrogates
Toluene-d8 (S)99 %08/18/23 19:57 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)98 %08/18/23 19:57 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)96 %08/18/23 19:57 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.1 %08/17/23 17:25 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-7 Lab ID:92683348015 Collected:08/16/23 15:40 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 14:2208/18/23 14:226.3 4.5 1
Surrogates
n-Pentacosane (S)81 %08/21/23 14:22 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 02:2508/18/23 14:556.3 1.7 1
Surrogates
4-Bromofluorobenzene (S)108 %08/19/23 02:25 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 20:16 67-64-1 v208/18/23 08:1597.8 31.4 1
Benzene ND ug/kg 08/18/23 20:16 71-43-208/18/23 08:154.9 1.9 1
Bromobenzene ND ug/kg 08/18/23 20:16 108-86-108/18/23 08:154.9 1.6 1
Bromochloromethane ND ug/kg 08/18/23 20:16 74-97-508/18/23 08:154.9 1.4 1
Bromodichloromethane ND ug/kg 08/18/23 20:16 75-27-408/18/23 08:154.9 1.9 1
Bromoform ND ug/kg 08/18/23 20:16 75-25-208/18/23 08:154.9 1.7 1
Bromomethane ND ug/kg 08/18/23 20:16 74-83-9 v208/18/23 08:1519.6 15.2 1
2-Butanone (MEK)ND ug/kg 08/18/23 20:16 78-93-308/18/23 08:1597.8 23.5 1
n-Butylbenzene ND ug/kg 08/18/23 20:16 104-51-808/18/23 08:154.9 3.1 1
sec-Butylbenzene ND ug/kg 08/18/23 20:16 135-98-808/18/23 08:154.9 2.2 1
tert-Butylbenzene ND ug/kg 08/18/23 20:16 98-06-608/18/23 08:154.9 1.7 1
Carbon tetrachloride ND ug/kg 08/18/23 20:16 56-23-508/18/23 08:154.9 1.8 1
Chlorobenzene ND ug/kg 08/18/23 20:16 108-90-708/18/23 08:154.9 2.8 1
Chloroethane ND ug/kg 08/18/23 20:16 75-00-308/18/23 08:159.8 3.8 1
Chloroform ND ug/kg 08/18/23 20:16 67-66-308/18/23 08:154.9 4.1 1
Chloromethane ND ug/kg 08/18/23 20:16 74-87-308/18/23 08:159.8 4.1 1
2-Chlorotoluene ND ug/kg 08/18/23 20:16 95-49-808/18/23 08:154.9 1.7 1
4-Chlorotoluene ND ug/kg 08/18/23 20:16 106-43-408/18/23 08:154.9 2.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 20:16 96-12-808/18/23 08:154.9 1.9 1
Dibromochloromethane ND ug/kg 08/18/23 20:16 124-48-108/18/23 08:154.9 2.7 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 20:16 106-93-408/18/23 08:154.9 2.2 1
Dibromomethane ND ug/kg 08/18/23 20:16 74-95-308/18/23 08:154.9 1.0 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 20:16 95-50-108/18/23 08:154.9 1.8 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 20:16 541-73-108/18/23 08:154.9 1.5 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 20:16 106-46-708/18/23 08:154.9 1.3 1
Dichlorodifluoromethane ND ug/kg 08/18/23 20:16 75-71-808/18/23 08:159.8 5.0 1
1,1-Dichloroethane ND ug/kg 08/18/23 20:16 75-34-308/18/23 08:154.9 2.0 1
1,2-Dichloroethane ND ug/kg 08/18/23 20:16 107-06-208/18/23 08:154.9 3.2 1
1,1-Dichloroethene ND ug/kg 08/18/23 20:16 75-35-408/18/23 08:154.9 2.0 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 20:16 156-59-208/18/23 08:154.9 1.7 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 20:16 156-60-508/18/23 08:154.9 4.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-7 Lab ID:92683348015 Collected:08/16/23 15:40 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 20:16 78-87-508/18/23 08:154.9 1.5 1
1,3-Dichloropropane ND ug/kg 08/18/23 20:16 142-28-908/18/23 08:154.9 1.5 1
2,2-Dichloropropane ND ug/kg 08/18/23 20:16 594-20-708/18/23 08:154.9 3.7 1
1,1-Dichloropropene ND ug/kg 08/18/23 20:16 563-58-608/18/23 08:154.9 2.3 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 20:16 10061-01-508/18/23 08:154.9 1.3 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 20:16 10061-02-608/18/23 08:154.9 1.7 1
Diisopropyl ether ND ug/kg 08/18/23 20:16 108-20-308/18/23 08:154.9 1.3 1
Ethylbenzene ND ug/kg 08/18/23 20:16 100-41-408/18/23 08:154.9 2.3 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 20:16 87-68-308/18/23 08:159.8 8.0 1
2-Hexanone ND ug/kg 08/18/23 20:16 591-78-608/18/23 08:1548.9 4.7 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 20:16 98-82-808/18/23 08:154.9 1.7 1
p-Isopropyltoluene ND ug/kg 08/18/23 20:16 99-87-608/18/23 08:154.9 2.4 1
Methylene Chloride ND ug/kg 08/18/23 20:16 75-09-208/18/23 08:1519.6 13.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 20:16 108-10-108/18/23 08:1548.9 4.7 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 20:16 1634-04-408/18/23 08:154.9 1.8 1
Naphthalene ND ug/kg 08/18/23 20:16 91-20-308/18/23 08:154.9 2.6 1
n-Propylbenzene ND ug/kg 08/18/23 20:16 103-65-108/18/23 08:154.9 1.7 1
Styrene 5.3 ug/kg 08/18/23 20:16 100-42-508/18/23 08:154.9 1.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 20:16 630-20-608/18/23 08:154.9 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 20:16 79-34-508/18/23 08:154.9 1.3 1
Tetrachloroethene ND ug/kg 08/18/23 20:16 127-18-408/18/23 08:154.9 1.5 1
Toluene ND ug/kg 08/18/23 20:16 108-88-308/18/23 08:154.9 3.4 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 20:16 87-61-608/18/23 08:154.9 4.0 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 20:16 120-82-108/18/23 08:154.9 4.1 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 20:16 71-55-608/18/23 08:154.9 2.5 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 20:16 79-00-508/18/23 08:154.9 1.6 1
Trichloroethene ND ug/kg 08/18/23 20:16 79-01-608/18/23 08:154.9 3.9 1
Trichlorofluoromethane ND ug/kg 08/18/23 20:16 75-69-408/18/23 08:154.9 2.7 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 20:16 96-18-408/18/23 08:154.9 2.5 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 20:16 95-63-608/18/23 08:154.9 2.9 1
1,3,5-Trimethylbenzene 2.5J ug/kg 08/18/23 20:16 108-67-808/18/23 08:154.9 1.6 1
Vinyl acetate ND ug/kg 08/18/23 20:16 108-05-408/18/23 08:1548.9 10.1 1
Vinyl chloride ND ug/kg 08/18/23 20:16 75-01-408/18/23 08:159.8 2.5 1
Xylene (Total)ND ug/kg 08/18/23 20:16 1330-20-708/18/23 08:159.8 2.8 1
m&p-Xylene ND ug/kg 08/18/23 20:16 179601-23-108/18/23 08:159.8 3.3 1
o-Xylene ND ug/kg 08/18/23 20:16 95-47-608/18/23 08:154.9 2.2 1
Surrogates
Toluene-d8 (S)98 %08/18/23 20:16 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)99 %08/18/23 20:16 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)94 %08/18/23 20:16 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.9 %08/17/23 17:25 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-8 Lab ID:92683348016 Collected:08/16/23 15:45 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 22:4508/18/23 17:196.1 4.3 1
Surrogates
n-Pentacosane (S)72 %08/21/23 22:45 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 02:5108/18/23 14:555.3 1.5 1
Surrogates
4-Bromofluorobenzene (S)108 %08/19/23 02:51 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/18/23 20:34 67-64-1 v208/18/23 08:1512239.2 1
Benzene ND ug/kg 08/18/23 20:34 71-43-208/18/23 08:156.1 2.4 1
Bromobenzene ND ug/kg 08/18/23 20:34 108-86-108/18/23 08:156.1 2.0 1
Bromochloromethane ND ug/kg 08/18/23 20:34 74-97-508/18/23 08:156.1 1.8 1
Bromodichloromethane ND ug/kg 08/18/23 20:34 75-27-408/18/23 08:156.1 2.4 1
Bromoform ND ug/kg 08/18/23 20:34 75-25-208/18/23 08:156.1 2.2 1
Bromomethane ND ug/kg 08/18/23 20:34 74-83-9 v208/18/23 08:1524.4 18.9 1
2-Butanone (MEK)ND ug/kg 08/18/23 20:34 78-93-308/18/23 08:1512229.3 1
n-Butylbenzene ND ug/kg 08/18/23 20:34 104-51-808/18/23 08:156.1 3.8 1
sec-Butylbenzene ND ug/kg 08/18/23 20:34 135-98-808/18/23 08:156.1 2.7 1
tert-Butylbenzene ND ug/kg 08/18/23 20:34 98-06-608/18/23 08:156.1 2.2 1
Carbon tetrachloride ND ug/kg 08/18/23 20:34 56-23-508/18/23 08:156.1 2.3 1
Chlorobenzene ND ug/kg 08/18/23 20:34 108-90-708/18/23 08:156.1 3.5 1
Chloroethane ND ug/kg 08/18/23 20:34 75-00-308/18/23 08:1512.2 4.7 1
Chloroform ND ug/kg 08/18/23 20:34 67-66-308/18/23 08:156.1 5.1 1
Chloromethane ND ug/kg 08/18/23 20:34 74-87-308/18/23 08:1512.2 5.1 1
2-Chlorotoluene ND ug/kg 08/18/23 20:34 95-49-808/18/23 08:156.1 2.2 1
4-Chlorotoluene ND ug/kg 08/18/23 20:34 106-43-408/18/23 08:156.1 3.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/18/23 20:34 96-12-808/18/23 08:156.1 2.4 1
Dibromochloromethane ND ug/kg 08/18/23 20:34 124-48-108/18/23 08:156.1 3.4 1
1,2-Dibromoethane (EDB)ND ug/kg 08/18/23 20:34 106-93-408/18/23 08:156.1 2.7 1
Dibromomethane ND ug/kg 08/18/23 20:34 74-95-308/18/23 08:156.1 1.3 1
1,2-Dichlorobenzene ND ug/kg 08/18/23 20:34 95-50-108/18/23 08:156.1 2.2 1
1,3-Dichlorobenzene ND ug/kg 08/18/23 20:34 541-73-108/18/23 08:156.1 1.9 1
1,4-Dichlorobenzene ND ug/kg 08/18/23 20:34 106-46-708/18/23 08:156.1 1.6 1
Dichlorodifluoromethane ND ug/kg 08/18/23 20:34 75-71-808/18/23 08:1512.2 6.2 1
1,1-Dichloroethane ND ug/kg 08/18/23 20:34 75-34-308/18/23 08:156.1 2.5 1
1,2-Dichloroethane ND ug/kg 08/18/23 20:34 107-06-208/18/23 08:156.1 4.0 1
1,1-Dichloroethene ND ug/kg 08/18/23 20:34 75-35-408/18/23 08:156.1 2.5 1
cis-1,2-Dichloroethene ND ug/kg 08/18/23 20:34 156-59-208/18/23 08:156.1 2.1 1
trans-1,2-Dichloroethene ND ug/kg 08/18/23 20:34 156-60-508/18/23 08:156.1 5.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:UST-8 Lab ID:92683348016 Collected:08/16/23 15:45 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/18/23 20:34 78-87-508/18/23 08:156.1 1.8 1
1,3-Dichloropropane ND ug/kg 08/18/23 20:34 142-28-908/18/23 08:156.1 1.9 1
2,2-Dichloropropane ND ug/kg 08/18/23 20:34 594-20-708/18/23 08:156.1 4.6 1
1,1-Dichloropropene ND ug/kg 08/18/23 20:34 563-58-608/18/23 08:156.1 2.9 1
cis-1,3-Dichloropropene ND ug/kg 08/18/23 20:34 10061-01-508/18/23 08:156.1 1.7 1
trans-1,3-Dichloropropene ND ug/kg 08/18/23 20:34 10061-02-608/18/23 08:156.1 2.1 1
Diisopropyl ether ND ug/kg 08/18/23 20:34 108-20-308/18/23 08:156.1 1.6 1
Ethylbenzene ND ug/kg 08/18/23 20:34 100-41-408/18/23 08:156.1 2.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/18/23 20:34 87-68-308/18/23 08:1512.2 10 1
2-Hexanone ND ug/kg 08/18/23 20:34 591-78-608/18/23 08:1561.1 5.9 1
Isopropylbenzene (Cumene)ND ug/kg 08/18/23 20:34 98-82-808/18/23 08:156.1 2.1 1
p-Isopropyltoluene ND ug/kg 08/18/23 20:34 99-87-608/18/23 08:156.1 3.0 1
Methylene Chloride ND ug/kg 08/18/23 20:34 75-09-208/18/23 08:1524.4 16.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/18/23 20:34 108-10-108/18/23 08:1561.1 5.9 1
Methyl-tert-butyl ether ND ug/kg 08/18/23 20:34 1634-04-408/18/23 08:156.1 2.3 1
Naphthalene ND ug/kg 08/18/23 20:34 91-20-308/18/23 08:156.1 3.2 1
n-Propylbenzene ND ug/kg 08/18/23 20:34 103-65-108/18/23 08:156.1 2.2 1
Styrene ND ug/kg 08/18/23 20:34 100-42-508/18/23 08:156.1 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/18/23 20:34 630-20-608/18/23 08:156.1 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/18/23 20:34 79-34-508/18/23 08:156.1 1.6 1
Tetrachloroethene ND ug/kg 08/18/23 20:34 127-18-408/18/23 08:156.1 1.9 1
Toluene ND ug/kg 08/18/23 20:34 108-88-308/18/23 08:156.1 4.2 1
1,2,3-Trichlorobenzene ND ug/kg 08/18/23 20:34 87-61-608/18/23 08:156.1 4.9 1
1,2,4-Trichlorobenzene ND ug/kg 08/18/23 20:34 120-82-108/18/23 08:156.1 5.1 1
1,1,1-Trichloroethane ND ug/kg 08/18/23 20:34 71-55-608/18/23 08:156.1 3.2 1
1,1,2-Trichloroethane ND ug/kg 08/18/23 20:34 79-00-508/18/23 08:156.1 2.0 1
Trichloroethene ND ug/kg 08/18/23 20:34 79-01-608/18/23 08:156.1 4.9 1
Trichlorofluoromethane ND ug/kg 08/18/23 20:34 75-69-408/18/23 08:156.1 3.4 1
1,2,3-Trichloropropane ND ug/kg 08/18/23 20:34 96-18-408/18/23 08:156.1 3.1 1
1,2,4-Trimethylbenzene ND ug/kg 08/18/23 20:34 95-63-608/18/23 08:156.1 3.6 1
1,3,5-Trimethylbenzene ND ug/kg 08/18/23 20:34 108-67-808/18/23 08:156.1 2.1 1
Vinyl acetate ND ug/kg 08/18/23 20:34 108-05-408/18/23 08:1561.1 12.6 1
Vinyl chloride ND ug/kg 08/18/23 20:34 75-01-408/18/23 08:1512.2 3.1 1
Xylene (Total)ND ug/kg 08/18/23 20:34 1330-20-708/18/23 08:1512.2 3.5 1
m&p-Xylene ND ug/kg 08/18/23 20:34 179601-23-108/18/23 08:1512.2 4.2 1
o-Xylene ND ug/kg 08/18/23 20:34 95-47-608/18/23 08:156.1 2.7 1
Surrogates
Toluene-d8 (S)99 %08/18/23 20:34 2037-26-508/18/23 08:1570-130 1
4-Bromofluorobenzene (S)98 %08/18/23 20:34 460-00-408/18/23 08:1570-130 1
1,2-Dichloroethane-d4 (S)96 %08/18/23 20:34 17060-07-008/18/23 08:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.0 %08/17/23 17:25 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 5 Lab ID:92683348017 Collected:08/16/23 16:00 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 23:0208/18/23 17:196.1 4.3 1
Surrogates
n-Pentacosane (S)91 %08/21/23 23:02 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 03:1608/18/23 14:555.3 1.5 1
Surrogates
4-Bromofluorobenzene (S)108 %08/19/23 03:16 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 17:01 67-64-108/18/23 15:0785.4 27.4 1
Benzene ND ug/kg 08/21/23 17:01 71-43-208/18/23 15:074.3 1.7 1
Bromobenzene ND ug/kg 08/21/23 17:01 108-86-108/18/23 15:074.3 1.4 1
Bromochloromethane ND ug/kg 08/21/23 17:01 74-97-508/18/23 15:074.3 1.3 1
Bromodichloromethane ND ug/kg 08/21/23 17:01 75-27-408/18/23 15:074.3 1.6 1
Bromoform ND ug/kg 08/21/23 17:01 75-25-208/18/23 15:074.3 1.5 1
Bromomethane ND ug/kg 08/21/23 17:01 74-83-908/18/23 15:0717.1 13.2 1
2-Butanone (MEK)ND ug/kg 08/21/23 17:01 78-93-308/18/23 15:0785.4 20.5 1
n-Butylbenzene ND ug/kg 08/21/23 17:01 104-51-808/18/23 15:074.3 2.7 1
sec-Butylbenzene ND ug/kg 08/21/23 17:01 135-98-808/18/23 15:074.3 1.9 1
tert-Butylbenzene ND ug/kg 08/21/23 17:01 98-06-608/18/23 15:074.3 1.5 1
Carbon tetrachloride ND ug/kg 08/21/23 17:01 56-23-508/18/23 15:074.3 1.6 1
Chlorobenzene ND ug/kg 08/21/23 17:01 108-90-708/18/23 15:074.3 2.5 1
Chloroethane ND ug/kg 08/21/23 17:01 75-00-308/18/23 15:078.5 3.3 1
Chloroform ND ug/kg 08/21/23 17:01 67-66-308/18/23 15:074.3 3.6 1
Chloromethane ND ug/kg 08/21/23 17:01 74-87-308/18/23 15:078.5 3.6 1
2-Chlorotoluene ND ug/kg 08/21/23 17:01 95-49-808/18/23 15:074.3 1.5 1
4-Chlorotoluene ND ug/kg 08/21/23 17:01 106-43-408/18/23 15:074.3 2.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 17:01 96-12-808/18/23 15:074.3 1.7 1
Dibromochloromethane ND ug/kg 08/21/23 17:01 124-48-108/18/23 15:074.3 2.4 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 17:01 106-93-408/18/23 15:074.3 1.9 1
Dibromomethane ND ug/kg 08/21/23 17:01 74-95-308/18/23 15:074.3 0.91 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 17:01 95-50-108/18/23 15:074.3 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 17:01 541-73-108/18/23 15:074.3 1.3 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 17:01 106-46-708/18/23 15:074.3 1.1 1
Dichlorodifluoromethane ND ug/kg 08/21/23 17:01 75-71-808/18/23 15:078.5 4.3 1
1,1-Dichloroethane ND ug/kg 08/21/23 17:01 75-34-308/18/23 15:074.3 1.8 1
1,2-Dichloroethane ND ug/kg 08/21/23 17:01 107-06-208/18/23 15:074.3 2.8 1
1,1-Dichloroethene ND ug/kg 08/21/23 17:01 75-35-408/18/23 15:074.3 1.8 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 17:01 156-59-208/18/23 15:074.3 1.5 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 17:01 156-60-508/18/23 15:074.3 3.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 5 Lab ID:92683348017 Collected:08/16/23 16:00 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 17:01 78-87-508/18/23 15:074.3 1.3 1
1,3-Dichloropropane ND ug/kg 08/21/23 17:01 142-28-908/18/23 15:074.3 1.3 1
2,2-Dichloropropane ND ug/kg 08/21/23 17:01 594-20-708/18/23 15:074.3 3.2 1
1,1-Dichloropropene ND ug/kg 08/21/23 17:01 563-58-608/18/23 15:074.3 2.0 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 17:01 10061-01-508/18/23 15:074.3 1.2 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 17:01 10061-02-608/18/23 15:074.3 1.5 1
Diisopropyl ether ND ug/kg 08/21/23 17:01 108-20-308/18/23 15:074.3 1.2 1
Ethylbenzene ND ug/kg 08/21/23 17:01 100-41-408/18/23 15:074.3 2.0 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 17:01 87-68-308/18/23 15:078.5 7.0 1
2-Hexanone ND ug/kg 08/21/23 17:01 591-78-608/18/23 15:0742.7 4.1 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 17:01 98-82-808/18/23 15:074.3 1.5 1
p-Isopropyltoluene ND ug/kg 08/21/23 17:01 99-87-608/18/23 15:074.3 2.1 1
Methylene Chloride ND ug/kg 08/21/23 17:01 75-09-208/18/23 15:0717.1 11.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 17:01 108-10-108/18/23 15:0742.7 4.1 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 17:01 1634-04-408/18/23 15:074.3 1.6 1
Naphthalene ND ug/kg 08/21/23 17:01 91-20-308/18/23 15:074.3 2.2 1
n-Propylbenzene ND ug/kg 08/21/23 17:01 103-65-108/18/23 15:074.3 1.5 1
Styrene ND ug/kg 08/21/23 17:01 100-42-508/18/23 15:074.3 1.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 17:01 630-20-608/18/23 15:074.3 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 17:01 79-34-508/18/23 15:074.3 1.1 1
Tetrachloroethene ND ug/kg 08/21/23 17:01 127-18-408/18/23 15:074.3 1.3 1
Toluene ND ug/kg 08/21/23 17:01 108-88-308/18/23 15:074.3 2.9 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 17:01 87-61-608/18/23 15:074.3 3.5 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 17:01 120-82-108/18/23 15:074.3 3.6 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 17:01 71-55-608/18/23 15:074.3 2.2 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 17:01 79-00-508/18/23 15:074.3 1.4 1
Trichloroethene ND ug/kg 08/21/23 17:01 79-01-608/18/23 15:074.3 3.4 1
Trichlorofluoromethane ND ug/kg 08/21/23 17:01 75-69-408/18/23 15:074.3 2.3 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 17:01 96-18-408/18/23 15:074.3 2.2 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 17:01 95-63-608/18/23 15:074.3 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 17:01 108-67-808/18/23 15:074.3 1.4 1
Vinyl acetate ND ug/kg 08/21/23 17:01 108-05-408/18/23 15:0742.7 8.8 1
Vinyl chloride ND ug/kg 08/21/23 17:01 75-01-408/18/23 15:078.5 2.2 1
Xylene (Total)ND ug/kg 08/21/23 17:01 1330-20-708/18/23 15:078.5 2.4 1
m&p-Xylene ND ug/kg 08/21/23 17:01 179601-23-108/18/23 15:078.5 2.9 1
o-Xylene ND ug/kg 08/21/23 17:01 95-47-608/18/23 15:074.3 1.9 1
Surrogates
Toluene-d8 (S)100 %08/21/23 17:01 2037-26-508/18/23 15:0770-130 1
4-Bromofluorobenzene (S)97 %08/21/23 17:01 460-00-408/18/23 15:0770-130 1
1,2-Dichloroethane-d4 (S)102 %08/21/23 17:01 17060-07-008/18/23 15:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.0 %08/17/23 17:25 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 2 Lab ID:92683348018 Collected:08/16/23 16:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)17.2 mg/kg 08/21/23 23:2008/18/23 17:196.6 4.7 1
Surrogates
n-Pentacosane (S)80 %08/21/23 23:20 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 03:4208/18/23 14:555.9 1.6 1
Surrogates
4-Bromofluorobenzene (S)107 %08/19/23 03:42 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 17:20 67-64-108/18/23 15:0711637.2 1
Benzene ND ug/kg 08/21/23 17:20 71-43-208/18/23 15:075.8 2.3 1
Bromobenzene ND ug/kg 08/21/23 17:20 108-86-108/18/23 15:075.8 1.9 1
Bromochloromethane ND ug/kg 08/21/23 17:20 74-97-508/18/23 15:075.8 1.7 1
Bromodichloromethane ND ug/kg 08/21/23 17:20 75-27-408/18/23 15:075.8 2.2 1
Bromoform ND ug/kg 08/21/23 17:20 75-25-208/18/23 15:075.8 2.0 1
Bromomethane ND ug/kg 08/21/23 17:20 74-83-908/18/23 15:0723.2 18.0 1
2-Butanone (MEK)ND ug/kg 08/21/23 17:20 78-93-308/18/23 15:0711627.8 1
n-Butylbenzene ND ug/kg 08/21/23 17:20 104-51-808/18/23 15:075.8 3.6 1
sec-Butylbenzene ND ug/kg 08/21/23 17:20 135-98-808/18/23 15:075.8 2.5 1
tert-Butylbenzene ND ug/kg 08/21/23 17:20 98-06-608/18/23 15:075.8 2.1 1
Carbon tetrachloride ND ug/kg 08/21/23 17:20 56-23-508/18/23 15:075.8 2.2 1
Chlorobenzene ND ug/kg 08/21/23 17:20 108-90-708/18/23 15:075.8 3.3 1
Chloroethane ND ug/kg 08/21/23 17:20 75-00-308/18/23 15:0711.6 4.5 1
Chloroform ND ug/kg 08/21/23 17:20 67-66-308/18/23 15:075.8 4.8 1
Chloromethane ND ug/kg 08/21/23 17:20 74-87-308/18/23 15:0711.6 4.9 1
2-Chlorotoluene ND ug/kg 08/21/23 17:20 95-49-808/18/23 15:075.8 2.0 1
4-Chlorotoluene ND ug/kg 08/21/23 17:20 106-43-408/18/23 15:075.8 3.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 17:20 96-12-808/18/23 15:075.8 2.2 1
Dibromochloromethane ND ug/kg 08/21/23 17:20 124-48-108/18/23 15:075.8 3.3 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 17:20 106-93-408/18/23 15:075.8 2.5 1
Dibromomethane ND ug/kg 08/21/23 17:20 74-95-308/18/23 15:075.8 1.2 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 17:20 95-50-108/18/23 15:075.8 2.1 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 17:20 541-73-108/18/23 15:075.8 1.8 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 17:20 106-46-708/18/23 15:075.8 1.5 1
Dichlorodifluoromethane ND ug/kg 08/21/23 17:20 75-71-808/18/23 15:0711.6 5.9 1
1,1-Dichloroethane ND ug/kg 08/21/23 17:20 75-34-308/18/23 15:075.8 2.4 1
1,2-Dichloroethane ND ug/kg 08/21/23 17:20 107-06-208/18/23 15:075.8 3.8 1
1,1-Dichloroethene ND ug/kg 08/21/23 17:20 75-35-408/18/23 15:075.8 2.4 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 17:20 156-59-208/18/23 15:075.8 2.0 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 17:20 156-60-508/18/23 15:075.8 4.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 2 Lab ID:92683348018 Collected:08/16/23 16:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 17:20 78-87-508/18/23 15:075.8 1.7 1
1,3-Dichloropropane ND ug/kg 08/21/23 17:20 142-28-908/18/23 15:075.8 1.8 1
2,2-Dichloropropane ND ug/kg 08/21/23 17:20 594-20-708/18/23 15:075.8 4.4 1
1,1-Dichloropropene ND ug/kg 08/21/23 17:20 563-58-608/18/23 15:075.8 2.8 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 17:20 10061-01-508/18/23 15:075.8 1.6 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 17:20 10061-02-608/18/23 15:075.8 2.0 1
Diisopropyl ether ND ug/kg 08/21/23 17:20 108-20-308/18/23 15:075.8 1.6 1
Ethylbenzene ND ug/kg 08/21/23 17:20 100-41-408/18/23 15:075.8 2.7 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 17:20 87-68-308/18/23 15:0711.6 9.5 1
2-Hexanone ND ug/kg 08/21/23 17:20 591-78-608/18/23 15:0757.9 5.6 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 17:20 98-82-808/18/23 15:075.8 2.0 1
p-Isopropyltoluene ND ug/kg 08/21/23 17:20 99-87-608/18/23 15:075.8 2.8 1
Methylene Chloride ND ug/kg 08/21/23 17:20 75-09-208/18/23 15:0723.2 15.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 17:20 108-10-108/18/23 15:0757.9 5.6 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 17:20 1634-04-408/18/23 15:075.8 2.2 1
Naphthalene ND ug/kg 08/21/23 17:20 91-20-308/18/23 15:075.8 3.0 1
n-Propylbenzene ND ug/kg 08/21/23 17:20 103-65-108/18/23 15:075.8 2.1 1
Styrene ND ug/kg 08/21/23 17:20 100-42-508/18/23 15:075.8 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 17:20 630-20-608/18/23 15:075.8 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 17:20 79-34-508/18/23 15:075.8 1.5 1
Tetrachloroethene ND ug/kg 08/21/23 17:20 127-18-408/18/23 15:075.8 1.8 1
Toluene ND ug/kg 08/21/23 17:20 108-88-308/18/23 15:075.8 4.0 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 17:20 87-61-608/18/23 15:075.8 4.7 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 17:20 120-82-108/18/23 15:075.8 4.9 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 17:20 71-55-608/18/23 15:075.8 3.0 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 17:20 79-00-508/18/23 15:075.8 1.9 1
Trichloroethene ND ug/kg 08/21/23 17:20 79-01-608/18/23 15:075.8 4.7 1
Trichlorofluoromethane ND ug/kg 08/21/23 17:20 75-69-408/18/23 15:075.8 3.2 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 17:20 96-18-408/18/23 15:075.8 2.9 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 17:20 95-63-608/18/23 15:075.8 3.4 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 17:20 108-67-808/18/23 15:075.8 1.9 1
Vinyl acetate ND ug/kg 08/21/23 17:20 108-05-408/18/23 15:0757.9 11.9 1
Vinyl chloride ND ug/kg 08/21/23 17:20 75-01-408/18/23 15:0711.6 2.9 1
Xylene (Total)ND ug/kg 08/21/23 17:20 1330-20-708/18/23 15:0711.6 3.3 1
m&p-Xylene ND ug/kg 08/21/23 17:20 179601-23-108/18/23 15:0711.6 4.0 1
o-Xylene ND ug/kg 08/21/23 17:20 95-47-608/18/23 15:075.8 2.6 1
Surrogates
Toluene-d8 (S)97 %08/21/23 17:20 2037-26-508/18/23 15:0770-130 1
4-Bromofluorobenzene (S)97 %08/21/23 17:20 460-00-408/18/23 15:0770-130 1
1,2-Dichloroethane-d4 (S)95 %08/21/23 17:20 17060-07-008/18/23 15:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.7 %08/17/23 17:25 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 4 Lab ID:92683348019 Collected:08/16/23 17:00 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 15:3408/18/23 17:195.9 4.2 1
Surrogates
n-Pentacosane (S)63 %08/21/23 15:34 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 07:0808/18/23 15:034.2 1.2 1
Surrogates
4-Bromofluorobenzene (S)108 %08/19/23 07:08 460-00-408/18/23 15:0366-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 17:57 67-64-108/18/23 15:0777.3 24.8 1
Benzene ND ug/kg 08/21/23 17:57 71-43-208/18/23 15:073.9 1.5 1
Bromobenzene ND ug/kg 08/21/23 17:57 108-86-108/18/23 15:073.9 1.3 1
Bromochloromethane ND ug/kg 08/21/23 17:57 74-97-508/18/23 15:073.9 1.1 1
Bromodichloromethane ND ug/kg 08/21/23 17:57 75-27-408/18/23 15:073.9 1.5 1
Bromoform ND ug/kg 08/21/23 17:57 75-25-208/18/23 15:073.9 1.4 1
Bromomethane ND ug/kg 08/21/23 17:57 74-83-908/18/23 15:0715.5 12.0 1
2-Butanone (MEK)ND ug/kg 08/21/23 17:57 78-93-308/18/23 15:0777.3 18.5 1
n-Butylbenzene ND ug/kg 08/21/23 17:57 104-51-808/18/23 15:073.9 2.4 1
sec-Butylbenzene ND ug/kg 08/21/23 17:57 135-98-808/18/23 15:073.9 1.7 1
tert-Butylbenzene ND ug/kg 08/21/23 17:57 98-06-608/18/23 15:073.9 1.4 1
Carbon tetrachloride ND ug/kg 08/21/23 17:57 56-23-508/18/23 15:073.9 1.4 1
Chlorobenzene ND ug/kg 08/21/23 17:57 108-90-708/18/23 15:073.9 2.2 1
Chloroethane ND ug/kg 08/21/23 17:57 75-00-308/18/23 15:077.7 3.0 1
Chloroform ND ug/kg 08/21/23 17:57 67-66-308/18/23 15:073.9 3.2 1
Chloromethane ND ug/kg 08/21/23 17:57 74-87-308/18/23 15:077.7 3.2 1
2-Chlorotoluene ND ug/kg 08/21/23 17:57 95-49-808/18/23 15:073.9 1.4 1
4-Chlorotoluene ND ug/kg 08/21/23 17:57 106-43-408/18/23 15:073.9 2.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 17:57 96-12-808/18/23 15:073.9 1.5 1
Dibromochloromethane ND ug/kg 08/21/23 17:57 124-48-108/18/23 15:073.9 2.2 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 17:57 106-93-408/18/23 15:073.9 1.7 1
Dibromomethane ND ug/kg 08/21/23 17:57 74-95-308/18/23 15:073.9 0.83 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 17:57 95-50-108/18/23 15:073.9 1.4 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 17:57 541-73-108/18/23 15:073.9 1.2 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 17:57 106-46-708/18/23 15:073.9 1.0 1
Dichlorodifluoromethane ND ug/kg 08/21/23 17:57 75-71-808/18/23 15:077.7 3.9 1
1,1-Dichloroethane ND ug/kg 08/21/23 17:57 75-34-308/18/23 15:073.9 1.6 1
1,2-Dichloroethane ND ug/kg 08/21/23 17:57 107-06-208/18/23 15:073.9 2.6 1
1,1-Dichloroethene ND ug/kg 08/21/23 17:57 75-35-408/18/23 15:073.9 1.6 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 17:57 156-59-208/18/23 15:073.9 1.3 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 17:57 156-60-508/18/23 15:073.9 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 4 Lab ID:92683348019 Collected:08/16/23 17:00 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 17:57 78-87-508/18/23 15:073.9 1.2 1
1,3-Dichloropropane ND ug/kg 08/21/23 17:57 142-28-908/18/23 15:073.9 1.2 1
2,2-Dichloropropane ND ug/kg 08/21/23 17:57 594-20-708/18/23 15:073.9 2.9 1
1,1-Dichloropropene ND ug/kg 08/21/23 17:57 563-58-608/18/23 15:073.9 1.9 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 17:57 10061-01-508/18/23 15:073.9 1.1 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 17:57 10061-02-608/18/23 15:073.9 1.3 1
Diisopropyl ether ND ug/kg 08/21/23 17:57 108-20-308/18/23 15:073.9 1.0 1
Ethylbenzene ND ug/kg 08/21/23 17:57 100-41-408/18/23 15:073.9 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 17:57 87-68-308/18/23 15:077.7 6.3 1
2-Hexanone ND ug/kg 08/21/23 17:57 591-78-608/18/23 15:0738.6 3.7 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 17:57 98-82-808/18/23 15:073.9 1.3 1
p-Isopropyltoluene ND ug/kg 08/21/23 17:57 99-87-608/18/23 15:073.9 1.9 1
Methylene Chloride 27.0 ug/kg 08/21/23 17:57 75-09-2 C908/18/23 15:0715.5 10.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 17:57 108-10-108/18/23 15:0738.6 3.7 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 17:57 1634-04-408/18/23 15:073.9 1.4 1
Naphthalene ND ug/kg 08/21/23 17:57 91-20-308/18/23 15:073.9 2.0 1
n-Propylbenzene ND ug/kg 08/21/23 17:57 103-65-108/18/23 15:073.9 1.4 1
Styrene ND ug/kg 08/21/23 17:57 100-42-508/18/23 15:073.9 1.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 17:57 630-20-608/18/23 15:073.9 1.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 17:57 79-34-508/18/23 15:073.9 1.0 1
Tetrachloroethene ND ug/kg 08/21/23 17:57 127-18-408/18/23 15:073.9 1.2 1
Toluene ND ug/kg 08/21/23 17:57 108-88-308/18/23 15:073.9 2.7 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 17:57 87-61-608/18/23 15:073.9 3.1 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 17:57 120-82-108/18/23 15:073.9 3.2 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 17:57 71-55-608/18/23 15:073.9 2.0 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 17:57 79-00-508/18/23 15:073.9 1.3 1
Trichloroethene ND ug/kg 08/21/23 17:57 79-01-608/18/23 15:073.9 3.1 1
Trichlorofluoromethane ND ug/kg 08/21/23 17:57 75-69-408/18/23 15:073.9 2.1 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 17:57 96-18-408/18/23 15:073.9 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 17:57 95-63-608/18/23 15:073.9 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 17:57 108-67-808/18/23 15:073.9 1.3 1
Vinyl acetate ND ug/kg 08/21/23 17:57 108-05-408/18/23 15:0738.6 8.0 1
Vinyl chloride ND ug/kg 08/21/23 17:57 75-01-408/18/23 15:077.7 2.0 1
Xylene (Total)ND ug/kg 08/21/23 17:57 1330-20-708/18/23 15:077.7 2.2 1
m&p-Xylene ND ug/kg 08/21/23 17:57 179601-23-108/18/23 15:077.7 2.6 1
o-Xylene ND ug/kg 08/21/23 17:57 95-47-608/18/23 15:073.9 1.7 1
Surrogates
Toluene-d8 (S)100 %08/21/23 17:57 2037-26-508/18/23 15:0770-130 1
4-Bromofluorobenzene (S)99 %08/21/23 17:57 460-00-408/18/23 15:0770-130 1
1,2-Dichloroethane-d4 (S)102 %08/21/23 17:57 17060-07-008/18/23 15:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.5 %08/17/23 17:25 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 6 Lab ID:92683348020 Collected:08/16/23 17:15 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 23:2008/18/23 17:196.1 4.3 1
Surrogates
n-Pentacosane (S)83 %08/21/23 23:20 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 07:3408/18/23 15:033.8 1.1 1
Surrogates
4-Bromofluorobenzene (S)108 %08/19/23 07:34 460-00-408/18/23 15:0366-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 18:16 67-64-108/18/23 15:0786.9 27.9 1
Benzene ND ug/kg 08/21/23 18:16 71-43-208/18/23 15:074.3 1.7 1
Bromobenzene ND ug/kg 08/21/23 18:16 108-86-108/18/23 15:074.3 1.4 1
Bromochloromethane ND ug/kg 08/21/23 18:16 74-97-508/18/23 15:074.3 1.3 1
Bromodichloromethane ND ug/kg 08/21/23 18:16 75-27-408/18/23 15:074.3 1.7 1
Bromoform ND ug/kg 08/21/23 18:16 75-25-208/18/23 15:074.3 1.5 1
Bromomethane ND ug/kg 08/21/23 18:16 74-83-908/18/23 15:0717.4 13.5 1
2-Butanone (MEK)ND ug/kg 08/21/23 18:16 78-93-308/18/23 15:0786.9 20.9 1
n-Butylbenzene ND ug/kg 08/21/23 18:16 104-51-808/18/23 15:074.3 2.7 1
sec-Butylbenzene ND ug/kg 08/21/23 18:16 135-98-808/18/23 15:074.3 1.9 1
tert-Butylbenzene ND ug/kg 08/21/23 18:16 98-06-608/18/23 15:074.3 1.5 1
Carbon tetrachloride ND ug/kg 08/21/23 18:16 56-23-508/18/23 15:074.3 1.6 1
Chlorobenzene ND ug/kg 08/21/23 18:16 108-90-708/18/23 15:074.3 2.5 1
Chloroethane ND ug/kg 08/21/23 18:16 75-00-308/18/23 15:078.7 3.4 1
Chloroform ND ug/kg 08/21/23 18:16 67-66-308/18/23 15:074.3 3.6 1
Chloromethane ND ug/kg 08/21/23 18:16 74-87-308/18/23 15:078.7 3.6 1
2-Chlorotoluene ND ug/kg 08/21/23 18:16 95-49-808/18/23 15:074.3 1.5 1
4-Chlorotoluene ND ug/kg 08/21/23 18:16 106-43-408/18/23 15:074.3 2.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 18:16 96-12-808/18/23 15:074.3 1.7 1
Dibromochloromethane ND ug/kg 08/21/23 18:16 124-48-108/18/23 15:074.3 2.4 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 18:16 106-93-408/18/23 15:074.3 1.9 1
Dibromomethane ND ug/kg 08/21/23 18:16 74-95-308/18/23 15:074.3 0.93 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 18:16 95-50-108/18/23 15:074.3 1.6 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 18:16 541-73-108/18/23 15:074.3 1.3 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 18:16 106-46-708/18/23 15:074.3 1.1 1
Dichlorodifluoromethane ND ug/kg 08/21/23 18:16 75-71-808/18/23 15:078.7 4.4 1
1,1-Dichloroethane ND ug/kg 08/21/23 18:16 75-34-308/18/23 15:074.3 1.8 1
1,2-Dichloroethane ND ug/kg 08/21/23 18:16 107-06-208/18/23 15:074.3 2.9 1
1,1-Dichloroethene ND ug/kg 08/21/23 18:16 75-35-408/18/23 15:074.3 1.8 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 18:16 156-59-208/18/23 15:074.3 1.5 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 18:16 156-60-508/18/23 15:074.3 3.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 6 Lab ID:92683348020 Collected:08/16/23 17:15 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 18:16 78-87-508/18/23 15:074.3 1.3 1
1,3-Dichloropropane ND ug/kg 08/21/23 18:16 142-28-908/18/23 15:074.3 1.4 1
2,2-Dichloropropane ND ug/kg 08/21/23 18:16 594-20-708/18/23 15:074.3 3.3 1
1,1-Dichloropropene ND ug/kg 08/21/23 18:16 563-58-608/18/23 15:074.3 2.1 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 18:16 10061-01-508/18/23 15:074.3 1.2 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 18:16 10061-02-608/18/23 15:074.3 1.5 1
Diisopropyl ether ND ug/kg 08/21/23 18:16 108-20-308/18/23 15:074.3 1.2 1
Ethylbenzene ND ug/kg 08/21/23 18:16 100-41-408/18/23 15:074.3 2.0 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 18:16 87-68-308/18/23 15:078.7 7.1 1
2-Hexanone ND ug/kg 08/21/23 18:16 591-78-608/18/23 15:0743.4 4.2 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 18:16 98-82-808/18/23 15:074.3 1.5 1
p-Isopropyltoluene ND ug/kg 08/21/23 18:16 99-87-608/18/23 15:074.3 2.1 1
Methylene Chloride ND ug/kg 08/21/23 18:16 75-09-208/18/23 15:0717.4 11.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 18:16 108-10-108/18/23 15:0743.4 4.2 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 18:16 1634-04-408/18/23 15:074.3 1.6 1
Naphthalene ND ug/kg 08/21/23 18:16 91-20-308/18/23 15:074.3 2.3 1
n-Propylbenzene ND ug/kg 08/21/23 18:16 103-65-108/18/23 15:074.3 1.5 1
Styrene ND ug/kg 08/21/23 18:16 100-42-508/18/23 15:074.3 1.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 18:16 630-20-608/18/23 15:074.3 1.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 18:16 79-34-508/18/23 15:074.3 1.1 1
Tetrachloroethene ND ug/kg 08/21/23 18:16 127-18-408/18/23 15:074.3 1.4 1
Toluene ND ug/kg 08/21/23 18:16 108-88-308/18/23 15:074.3 3.0 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 18:16 87-61-608/18/23 15:074.3 3.5 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 18:16 120-82-108/18/23 15:074.3 3.6 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 18:16 71-55-608/18/23 15:074.3 2.3 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 18:16 79-00-508/18/23 15:074.3 1.4 1
Trichloroethene ND ug/kg 08/21/23 18:16 79-01-608/18/23 15:074.3 3.5 1
Trichlorofluoromethane ND ug/kg 08/21/23 18:16 75-69-408/18/23 15:074.3 2.4 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 18:16 96-18-408/18/23 15:074.3 2.2 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 18:16 95-63-608/18/23 15:074.3 2.6 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 18:16 108-67-808/18/23 15:074.3 1.5 1
Vinyl acetate ND ug/kg 08/21/23 18:16 108-05-408/18/23 15:0743.4 8.9 1
Vinyl chloride ND ug/kg 08/21/23 18:16 75-01-408/18/23 15:078.7 2.2 1
Xylene (Total)ND ug/kg 08/21/23 18:16 1330-20-708/18/23 15:078.7 2.5 1
m&p-Xylene ND ug/kg 08/21/23 18:16 179601-23-108/18/23 15:078.7 3.0 1
o-Xylene ND ug/kg 08/21/23 18:16 95-47-608/18/23 15:074.3 1.9 1
Surrogates
Toluene-d8 (S)99 %08/21/23 18:16 2037-26-508/18/23 15:0770-130 1
4-Bromofluorobenzene (S)97 %08/21/23 18:16 460-00-408/18/23 15:0770-130 1
1,2-Dichloroethane-d4 (S)103 %08/21/23 18:16 17060-07-008/18/23 15:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.7 %08/17/23 17:25 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 7 Lab ID:92683348021 Collected:08/16/23 17:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 23:3708/18/23 17:196.2 4.4 1
Surrogates
n-Pentacosane (S)83 %08/21/23 23:37 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 07:5908/18/23 15:035.4 1.5 1
Surrogates
4-Bromofluorobenzene (S)106 %08/19/23 07:59 460-00-408/18/23 15:0366-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 18:35 67-64-108/18/23 15:0789.2 28.6 1
Benzene ND ug/kg 08/21/23 18:35 71-43-208/18/23 15:074.5 1.8 1
Bromobenzene ND ug/kg 08/21/23 18:35 108-86-108/18/23 15:074.5 1.5 1
Bromochloromethane ND ug/kg 08/21/23 18:35 74-97-508/18/23 15:074.5 1.3 1
Bromodichloromethane ND ug/kg 08/21/23 18:35 75-27-408/18/23 15:074.5 1.7 1
Bromoform ND ug/kg 08/21/23 18:35 75-25-208/18/23 15:074.5 1.6 1
Bromomethane ND ug/kg 08/21/23 18:35 74-83-908/18/23 15:0717.8 13.8 1
2-Butanone (MEK)ND ug/kg 08/21/23 18:35 78-93-308/18/23 15:0789.2 21.4 1
n-Butylbenzene ND ug/kg 08/21/23 18:35 104-51-808/18/23 15:074.5 2.8 1
sec-Butylbenzene ND ug/kg 08/21/23 18:35 135-98-808/18/23 15:074.5 2.0 1
tert-Butylbenzene ND ug/kg 08/21/23 18:35 98-06-608/18/23 15:074.5 1.6 1
Carbon tetrachloride ND ug/kg 08/21/23 18:35 56-23-508/18/23 15:074.5 1.7 1
Chlorobenzene ND ug/kg 08/21/23 18:35 108-90-708/18/23 15:074.5 2.6 1
Chloroethane ND ug/kg 08/21/23 18:35 75-00-308/18/23 15:078.9 3.4 1
Chloroform ND ug/kg 08/21/23 18:35 67-66-308/18/23 15:074.5 3.7 1
Chloromethane ND ug/kg 08/21/23 18:35 74-87-308/18/23 15:078.9 3.7 1
2-Chlorotoluene ND ug/kg 08/21/23 18:35 95-49-808/18/23 15:074.5 1.6 1
4-Chlorotoluene ND ug/kg 08/21/23 18:35 106-43-408/18/23 15:074.5 2.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 18:35 96-12-808/18/23 15:074.5 1.7 1
Dibromochloromethane ND ug/kg 08/21/23 18:35 124-48-108/18/23 15:074.5 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 18:35 106-93-408/18/23 15:074.5 2.0 1
Dibromomethane ND ug/kg 08/21/23 18:35 74-95-308/18/23 15:074.5 0.95 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 18:35 95-50-108/18/23 15:074.5 1.6 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 18:35 541-73-108/18/23 15:074.5 1.4 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 18:35 106-46-708/18/23 15:074.5 1.2 1
Dichlorodifluoromethane ND ug/kg 08/21/23 18:35 75-71-808/18/23 15:078.9 4.5 1
1,1-Dichloroethane ND ug/kg 08/21/23 18:35 75-34-308/18/23 15:074.5 1.8 1
1,2-Dichloroethane ND ug/kg 08/21/23 18:35 107-06-208/18/23 15:074.5 3.0 1
1,1-Dichloroethene ND ug/kg 08/21/23 18:35 75-35-408/18/23 15:074.5 1.8 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 18:35 156-59-208/18/23 15:074.5 1.5 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 18:35 156-60-508/18/23 15:074.5 3.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:SUMP 7 Lab ID:92683348021 Collected:08/16/23 17:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 18:35 78-87-508/18/23 15:074.5 1.3 1
1,3-Dichloropropane ND ug/kg 08/21/23 18:35 142-28-908/18/23 15:074.5 1.4 1
2,2-Dichloropropane ND ug/kg 08/21/23 18:35 594-20-708/18/23 15:074.5 3.4 1
1,1-Dichloropropene ND ug/kg 08/21/23 18:35 563-58-608/18/23 15:074.5 2.1 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 18:35 10061-01-508/18/23 15:074.5 1.2 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 18:35 10061-02-608/18/23 15:074.5 1.5 1
Diisopropyl ether ND ug/kg 08/21/23 18:35 108-20-308/18/23 15:074.5 1.2 1
Ethylbenzene ND ug/kg 08/21/23 18:35 100-41-408/18/23 15:074.5 2.1 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 18:35 87-68-308/18/23 15:078.9 7.3 1
2-Hexanone ND ug/kg 08/21/23 18:35 591-78-608/18/23 15:0744.6 4.3 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 18:35 98-82-808/18/23 15:074.5 1.5 1
p-Isopropyltoluene ND ug/kg 08/21/23 18:35 99-87-608/18/23 15:074.5 2.2 1
Methylene Chloride ND ug/kg 08/21/23 18:35 75-09-208/18/23 15:0717.8 12.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 18:35 108-10-108/18/23 15:0744.6 4.3 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 18:35 1634-04-408/18/23 15:074.5 1.7 1
Naphthalene ND ug/kg 08/21/23 18:35 91-20-308/18/23 15:074.5 2.3 1
n-Propylbenzene ND ug/kg 08/21/23 18:35 103-65-108/18/23 15:074.5 1.6 1
Styrene ND ug/kg 08/21/23 18:35 100-42-508/18/23 15:074.5 1.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 18:35 630-20-608/18/23 15:074.5 1.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 18:35 79-34-508/18/23 15:074.5 1.2 1
Tetrachloroethene ND ug/kg 08/21/23 18:35 127-18-408/18/23 15:074.5 1.4 1
Toluene ND ug/kg 08/21/23 18:35 108-88-308/18/23 15:074.5 3.1 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 18:35 87-61-608/18/23 15:074.5 3.6 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 18:35 120-82-108/18/23 15:074.5 3.7 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 18:35 71-55-608/18/23 15:074.5 2.3 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 18:35 79-00-508/18/23 15:074.5 1.5 1
Trichloroethene ND ug/kg 08/21/23 18:35 79-01-608/18/23 15:074.5 3.6 1
Trichlorofluoromethane ND ug/kg 08/21/23 18:35 75-69-408/18/23 15:074.5 2.5 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 18:35 96-18-408/18/23 15:074.5 2.3 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 18:35 95-63-608/18/23 15:074.5 2.6 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 18:35 108-67-808/18/23 15:074.5 1.5 1
Vinyl acetate ND ug/kg 08/21/23 18:35 108-05-408/18/23 15:0744.6 9.2 1
Vinyl chloride ND ug/kg 08/21/23 18:35 75-01-408/18/23 15:078.9 2.3 1
Xylene (Total)ND ug/kg 08/21/23 18:35 1330-20-708/18/23 15:078.9 2.5 1
m&p-Xylene ND ug/kg 08/21/23 18:35 179601-23-108/18/23 15:078.9 3.1 1
o-Xylene ND ug/kg 08/21/23 18:35 95-47-608/18/23 15:074.5 2.0 1
Surrogates
Toluene-d8 (S)97 %08/21/23 18:35 2037-26-508/18/23 15:0770-130 1
4-Bromofluorobenzene (S)93 %08/21/23 18:35 460-00-408/18/23 15:0770-130 1
1,2-Dichloroethane-d4 (S)85 %08/21/23 18:35 17060-07-008/18/23 15:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.2 %08/17/23 17:26 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 5 Lab ID:92683348022 Collected:08/16/23 17:45 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 16:1508/18/23 17:196.3 4.5 1
Surrogates
n-Pentacosane (S)83 %08/21/23 16:15 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 08:2508/18/23 15:035.6 1.5 1
Surrogates
4-Bromofluorobenzene (S)109 %08/19/23 08:25 460-00-408/18/23 15:0366-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 18:53 67-64-108/18/23 15:0780.0 25.7 1
Benzene ND ug/kg 08/21/23 18:53 71-43-208/18/23 15:074.0 1.6 1
Bromobenzene ND ug/kg 08/21/23 18:53 108-86-108/18/23 15:074.0 1.3 1
Bromochloromethane ND ug/kg 08/21/23 18:53 74-97-508/18/23 15:074.0 1.2 1
Bromodichloromethane ND ug/kg 08/21/23 18:53 75-27-408/18/23 15:074.0 1.5 1
Bromoform ND ug/kg 08/21/23 18:53 75-25-208/18/23 15:074.0 1.4 1
Bromomethane ND ug/kg 08/21/23 18:53 74-83-908/18/23 15:0716.0 12.4 1
2-Butanone (MEK)ND ug/kg 08/21/23 18:53 78-93-308/18/23 15:0780.0 19.2 1
n-Butylbenzene ND ug/kg 08/21/23 18:53 104-51-808/18/23 15:074.0 2.5 1
sec-Butylbenzene ND ug/kg 08/21/23 18:53 135-98-808/18/23 15:074.0 1.8 1
tert-Butylbenzene ND ug/kg 08/21/23 18:53 98-06-608/18/23 15:074.0 1.4 1
Carbon tetrachloride ND ug/kg 08/21/23 18:53 56-23-508/18/23 15:074.0 1.5 1
Chlorobenzene ND ug/kg 08/21/23 18:53 108-90-708/18/23 15:074.0 2.3 1
Chloroethane ND ug/kg 08/21/23 18:53 75-00-308/18/23 15:078.0 3.1 1
Chloroform ND ug/kg 08/21/23 18:53 67-66-308/18/23 15:074.0 3.3 1
Chloromethane ND ug/kg 08/21/23 18:53 74-87-308/18/23 15:078.0 3.4 1
2-Chlorotoluene ND ug/kg 08/21/23 18:53 95-49-808/18/23 15:074.0 1.4 1
4-Chlorotoluene ND ug/kg 08/21/23 18:53 106-43-408/18/23 15:074.0 2.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 18:53 96-12-808/18/23 15:074.0 1.6 1
Dibromochloromethane ND ug/kg 08/21/23 18:53 124-48-108/18/23 15:074.0 2.2 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 18:53 106-93-408/18/23 15:074.0 1.8 1
Dibromomethane ND ug/kg 08/21/23 18:53 74-95-308/18/23 15:074.0 0.86 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 18:53 95-50-108/18/23 15:074.0 1.4 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 18:53 541-73-108/18/23 15:074.0 1.2 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 18:53 106-46-708/18/23 15:074.0 1.0 1
Dichlorodifluoromethane ND ug/kg 08/21/23 18:53 75-71-808/18/23 15:078.0 4.1 1
1,1-Dichloroethane ND ug/kg 08/21/23 18:53 75-34-308/18/23 15:074.0 1.6 1
1,2-Dichloroethane ND ug/kg 08/21/23 18:53 107-06-208/18/23 15:074.0 2.6 1
1,1-Dichloroethene ND ug/kg 08/21/23 18:53 75-35-408/18/23 15:074.0 1.6 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 18:53 156-59-208/18/23 15:074.0 1.4 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 18:53 156-60-508/18/23 15:074.0 3.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 5 Lab ID:92683348022 Collected:08/16/23 17:45 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 18:53 78-87-508/18/23 15:074.0 1.2 1
1,3-Dichloropropane ND ug/kg 08/21/23 18:53 142-28-908/18/23 15:074.0 1.2 1
2,2-Dichloropropane ND ug/kg 08/21/23 18:53 594-20-708/18/23 15:074.0 3.0 1
1,1-Dichloropropene ND ug/kg 08/21/23 18:53 563-58-608/18/23 15:074.0 1.9 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 18:53 10061-01-508/18/23 15:074.0 1.1 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 18:53 10061-02-608/18/23 15:074.0 1.4 1
Diisopropyl ether ND ug/kg 08/21/23 18:53 108-20-308/18/23 15:074.0 1.1 1
Ethylbenzene ND ug/kg 08/21/23 18:53 100-41-408/18/23 15:074.0 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 18:53 87-68-308/18/23 15:078.0 6.5 1
2-Hexanone ND ug/kg 08/21/23 18:53 591-78-608/18/23 15:0740.0 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 18:53 98-82-808/18/23 15:074.0 1.4 1
p-Isopropyltoluene ND ug/kg 08/21/23 18:53 99-87-608/18/23 15:074.0 2.0 1
Methylene Chloride ND ug/kg 08/21/23 18:53 75-09-208/18/23 15:0716.0 11.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 18:53 108-10-108/18/23 15:0740.0 3.9 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 18:53 1634-04-408/18/23 15:074.0 1.5 1
Naphthalene ND ug/kg 08/21/23 18:53 91-20-308/18/23 15:074.0 2.1 1
n-Propylbenzene ND ug/kg 08/21/23 18:53 103-65-108/18/23 15:074.0 1.4 1
Styrene ND ug/kg 08/21/23 18:53 100-42-508/18/23 15:074.0 1.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 18:53 630-20-608/18/23 15:074.0 1.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 18:53 79-34-508/18/23 15:074.0 1.1 1
Tetrachloroethene ND ug/kg 08/21/23 18:53 127-18-408/18/23 15:074.0 1.3 1
Toluene ND ug/kg 08/21/23 18:53 108-88-308/18/23 15:074.0 2.8 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 18:53 87-61-608/18/23 15:074.0 3.2 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 18:53 120-82-108/18/23 15:074.0 3.4 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 18:53 71-55-608/18/23 15:074.0 2.1 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 18:53 79-00-508/18/23 15:074.0 1.3 1
Trichloroethene ND ug/kg 08/21/23 18:53 79-01-608/18/23 15:074.0 3.2 1
Trichlorofluoromethane ND ug/kg 08/21/23 18:53 75-69-408/18/23 15:074.0 2.2 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 18:53 96-18-408/18/23 15:074.0 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 18:53 95-63-608/18/23 15:074.0 2.4 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 18:53 108-67-808/18/23 15:074.0 1.3 1
Vinyl acetate ND ug/kg 08/21/23 18:53 108-05-408/18/23 15:0740.0 8.2 1
Vinyl chloride ND ug/kg 08/21/23 18:53 75-01-408/18/23 15:078.0 2.0 1
Xylene (Total)ND ug/kg 08/21/23 18:53 1330-20-708/18/23 15:078.0 2.3 1
m&p-Xylene ND ug/kg 08/21/23 18:53 179601-23-108/18/23 15:078.0 2.7 1
o-Xylene ND ug/kg 08/21/23 18:53 95-47-608/18/23 15:074.0 1.8 1
Surrogates
Toluene-d8 (S)97 %08/21/23 18:53 2037-26-508/18/23 15:0770-130 1
4-Bromofluorobenzene (S)95 %08/21/23 18:53 460-00-408/18/23 15:0770-130 1
1,2-Dichloroethane-d4 (S)85 %08/21/23 18:53 17060-07-008/18/23 15:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.3 %08/17/23 17:26 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 6-1 Lab ID:92683348023 Collected:08/16/23 18:15 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 16:1508/18/23 17:196.2 4.4 1
Surrogates
n-Pentacosane (S)82 %08/21/23 16:15 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 08:5108/18/23 15:034.7 1.3 1
Surrogates
4-Bromofluorobenzene (S)108 %08/19/23 08:51 460-00-408/18/23 15:0366-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 19:12 67-64-108/18/23 15:0785.2 27.4 1
Benzene ND ug/kg 08/21/23 19:12 71-43-208/18/23 15:074.3 1.7 1
Bromobenzene ND ug/kg 08/21/23 19:12 108-86-108/18/23 15:074.3 1.4 1
Bromochloromethane ND ug/kg 08/21/23 19:12 74-97-508/18/23 15:074.3 1.3 1
Bromodichloromethane ND ug/kg 08/21/23 19:12 75-27-408/18/23 15:074.3 1.6 1
Bromoform ND ug/kg 08/21/23 19:12 75-25-208/18/23 15:074.3 1.5 1
Bromomethane ND ug/kg 08/21/23 19:12 74-83-908/18/23 15:0717.0 13.2 1
2-Butanone (MEK)ND ug/kg 08/21/23 19:12 78-93-308/18/23 15:0785.2 20.5 1
n-Butylbenzene ND ug/kg 08/21/23 19:12 104-51-808/18/23 15:074.3 2.7 1
sec-Butylbenzene ND ug/kg 08/21/23 19:12 135-98-808/18/23 15:074.3 1.9 1
tert-Butylbenzene ND ug/kg 08/21/23 19:12 98-06-608/18/23 15:074.3 1.5 1
Carbon tetrachloride ND ug/kg 08/21/23 19:12 56-23-508/18/23 15:074.3 1.6 1
Chlorobenzene ND ug/kg 08/21/23 19:12 108-90-708/18/23 15:074.3 2.4 1
Chloroethane ND ug/kg 08/21/23 19:12 75-00-308/18/23 15:078.5 3.3 1
Chloroform ND ug/kg 08/21/23 19:12 67-66-308/18/23 15:074.3 3.6 1
Chloromethane ND ug/kg 08/21/23 19:12 74-87-308/18/23 15:078.5 3.6 1
2-Chlorotoluene ND ug/kg 08/21/23 19:12 95-49-808/18/23 15:074.3 1.5 1
4-Chlorotoluene ND ug/kg 08/21/23 19:12 106-43-408/18/23 15:074.3 2.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 19:12 96-12-808/18/23 15:074.3 1.7 1
Dibromochloromethane ND ug/kg 08/21/23 19:12 124-48-108/18/23 15:074.3 2.4 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 19:12 106-93-408/18/23 15:074.3 1.9 1
Dibromomethane ND ug/kg 08/21/23 19:12 74-95-308/18/23 15:074.3 0.91 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 19:12 95-50-108/18/23 15:074.3 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 19:12 541-73-108/18/23 15:074.3 1.3 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 19:12 106-46-708/18/23 15:074.3 1.1 1
Dichlorodifluoromethane ND ug/kg 08/21/23 19:12 75-71-808/18/23 15:078.5 4.3 1
1,1-Dichloroethane ND ug/kg 08/21/23 19:12 75-34-308/18/23 15:074.3 1.8 1
1,2-Dichloroethane ND ug/kg 08/21/23 19:12 107-06-208/18/23 15:074.3 2.8 1
1,1-Dichloroethene ND ug/kg 08/21/23 19:12 75-35-408/18/23 15:074.3 1.8 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 19:12 156-59-208/18/23 15:074.3 1.5 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 19:12 156-60-508/18/23 15:074.3 3.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 6-1 Lab ID:92683348023 Collected:08/16/23 18:15 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 19:12 78-87-508/18/23 15:074.3 1.3 1
1,3-Dichloropropane ND ug/kg 08/21/23 19:12 142-28-908/18/23 15:074.3 1.3 1
2,2-Dichloropropane ND ug/kg 08/21/23 19:12 594-20-708/18/23 15:074.3 3.2 1
1,1-Dichloropropene ND ug/kg 08/21/23 19:12 563-58-608/18/23 15:074.3 2.0 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 19:12 10061-01-508/18/23 15:074.3 1.2 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 19:12 10061-02-608/18/23 15:074.3 1.5 1
Diisopropyl ether ND ug/kg 08/21/23 19:12 108-20-308/18/23 15:074.3 1.2 1
Ethylbenzene ND ug/kg 08/21/23 19:12 100-41-408/18/23 15:074.3 2.0 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 19:12 87-68-308/18/23 15:078.5 7.0 1
2-Hexanone ND ug/kg 08/21/23 19:12 591-78-608/18/23 15:0742.6 4.1 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 19:12 98-82-808/18/23 15:074.3 1.4 1
p-Isopropyltoluene ND ug/kg 08/21/23 19:12 99-87-608/18/23 15:074.3 2.1 1
Methylene Chloride 18.5 ug/kg 08/21/23 19:12 75-09-2 C908/18/23 15:0717.0 11.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 19:12 108-10-108/18/23 15:0742.6 4.1 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 19:12 1634-04-408/18/23 15:074.3 1.6 1
Naphthalene ND ug/kg 08/21/23 19:12 91-20-308/18/23 15:074.3 2.2 1
n-Propylbenzene ND ug/kg 08/21/23 19:12 103-65-108/18/23 15:074.3 1.5 1
Styrene ND ug/kg 08/21/23 19:12 100-42-508/18/23 15:074.3 1.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 19:12 630-20-608/18/23 15:074.3 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 19:12 79-34-508/18/23 15:074.3 1.1 1
Tetrachloroethene ND ug/kg 08/21/23 19:12 127-18-408/18/23 15:074.3 1.3 1
Toluene ND ug/kg 08/21/23 19:12 108-88-308/18/23 15:074.3 2.9 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 19:12 87-61-608/18/23 15:074.3 3.4 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 19:12 120-82-108/18/23 15:074.3 3.6 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 19:12 71-55-608/18/23 15:074.3 2.2 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 19:12 79-00-508/18/23 15:074.3 1.4 1
Trichloroethene ND ug/kg 08/21/23 19:12 79-01-608/18/23 15:074.3 3.4 1
Trichlorofluoromethane ND ug/kg 08/21/23 19:12 75-69-408/18/23 15:074.3 2.3 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 19:12 96-18-408/18/23 15:074.3 2.2 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 19:12 95-63-608/18/23 15:074.3 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 19:12 108-67-808/18/23 15:074.3 1.4 1
Vinyl acetate ND ug/kg 08/21/23 19:12 108-05-408/18/23 15:0742.6 8.8 1
Vinyl chloride ND ug/kg 08/21/23 19:12 75-01-408/18/23 15:078.5 2.2 1
Xylene (Total)ND ug/kg 08/21/23 19:12 1330-20-708/18/23 15:078.5 2.4 1
m&p-Xylene ND ug/kg 08/21/23 19:12 179601-23-108/18/23 15:078.5 2.9 1
o-Xylene ND ug/kg 08/21/23 19:12 95-47-608/18/23 15:074.3 1.9 1
Surrogates
Toluene-d8 (S)97 %08/21/23 19:12 2037-26-508/18/23 15:0770-130 1
4-Bromofluorobenzene (S)94 %08/21/23 19:12 460-00-408/18/23 15:0770-130 1
1,2-Dichloroethane-d4 (S)86 %08/21/23 19:12 17060-07-008/18/23 15:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.6 %08/17/23 17:26 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 6-2 Lab ID:92683348024 Collected:08/16/23 18:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)243 mg/kg 08/21/23 16:3308/18/23 17:196.2 4.4 1
Surrogates
n-Pentacosane (S)111 %08/21/23 16:33 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 09:1708/18/23 15:035.9 1.6 1
Surrogates
4-Bromofluorobenzene (S)108 %08/19/23 09:17 460-00-408/18/23 15:0366-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 19:31 67-64-108/18/23 15:0795.6 30.7 1
Benzene ND ug/kg 08/21/23 19:31 71-43-208/18/23 15:074.8 1.9 1
Bromobenzene ND ug/kg 08/21/23 19:31 108-86-108/18/23 15:074.8 1.6 1
Bromochloromethane ND ug/kg 08/21/23 19:31 74-97-508/18/23 15:074.8 1.4 1
Bromodichloromethane ND ug/kg 08/21/23 19:31 75-27-408/18/23 15:074.8 1.8 1
Bromoform ND ug/kg 08/21/23 19:31 75-25-208/18/23 15:074.8 1.7 1
Bromomethane ND ug/kg 08/21/23 19:31 74-83-908/18/23 15:0719.1 14.8 1
2-Butanone (MEK)ND ug/kg 08/21/23 19:31 78-93-308/18/23 15:0795.6 22.9 1
n-Butylbenzene ND ug/kg 08/21/23 19:31 104-51-808/18/23 15:074.8 3.0 1
sec-Butylbenzene ND ug/kg 08/21/23 19:31 135-98-808/18/23 15:074.8 2.1 1
tert-Butylbenzene ND ug/kg 08/21/23 19:31 98-06-608/18/23 15:074.8 1.7 1
Carbon tetrachloride ND ug/kg 08/21/23 19:31 56-23-508/18/23 15:074.8 1.8 1
Chlorobenzene ND ug/kg 08/21/23 19:31 108-90-708/18/23 15:074.8 2.7 1
Chloroethane ND ug/kg 08/21/23 19:31 75-00-308/18/23 15:079.6 3.7 1
Chloroform ND ug/kg 08/21/23 19:31 67-66-308/18/23 15:074.8 4.0 1
Chloromethane ND ug/kg 08/21/23 19:31 74-87-308/18/23 15:079.6 4.0 1
2-Chlorotoluene ND ug/kg 08/21/23 19:31 95-49-808/18/23 15:074.8 1.7 1
4-Chlorotoluene ND ug/kg 08/21/23 19:31 106-43-408/18/23 15:074.8 2.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 19:31 96-12-808/18/23 15:074.8 1.9 1
Dibromochloromethane ND ug/kg 08/21/23 19:31 124-48-108/18/23 15:074.8 2.7 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 19:31 106-93-408/18/23 15:074.8 2.1 1
Dibromomethane ND ug/kg 08/21/23 19:31 74-95-308/18/23 15:074.8 1.0 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 19:31 95-50-108/18/23 15:074.8 1.7 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 19:31 541-73-108/18/23 15:074.8 1.5 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 19:31 106-46-708/18/23 15:074.8 1.2 1
Dichlorodifluoromethane ND ug/kg 08/21/23 19:31 75-71-808/18/23 15:079.6 4.9 1
1,1-Dichloroethane ND ug/kg 08/21/23 19:31 75-34-308/18/23 15:074.8 2.0 1
1,2-Dichloroethane ND ug/kg 08/21/23 19:31 107-06-208/18/23 15:074.8 3.2 1
1,1-Dichloroethene ND ug/kg 08/21/23 19:31 75-35-408/18/23 15:074.8 2.0 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 19:31 156-59-208/18/23 15:074.8 1.6 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 19:31 156-60-508/18/23 15:074.8 4.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 6-2 Lab ID:92683348024 Collected:08/16/23 18:30 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 19:31 78-87-508/18/23 15:074.8 1.4 1
1,3-Dichloropropane ND ug/kg 08/21/23 19:31 142-28-908/18/23 15:074.8 1.5 1
2,2-Dichloropropane ND ug/kg 08/21/23 19:31 594-20-708/18/23 15:074.8 3.6 1
1,1-Dichloropropene ND ug/kg 08/21/23 19:31 563-58-608/18/23 15:074.8 2.3 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 19:31 10061-01-508/18/23 15:074.8 1.3 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 19:31 10061-02-608/18/23 15:074.8 1.6 1
Diisopropyl ether ND ug/kg 08/21/23 19:31 108-20-308/18/23 15:074.8 1.3 1
Ethylbenzene ND ug/kg 08/21/23 19:31 100-41-408/18/23 15:074.8 2.2 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 19:31 87-68-308/18/23 15:079.6 7.8 1
2-Hexanone ND ug/kg 08/21/23 19:31 591-78-608/18/23 15:0747.8 4.6 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 19:31 98-82-808/18/23 15:074.8 1.6 1
p-Isopropyltoluene ND ug/kg 08/21/23 19:31 99-87-608/18/23 15:074.8 2.4 1
Methylene Chloride ND ug/kg 08/21/23 19:31 75-09-208/18/23 15:0719.1 13.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 19:31 108-10-108/18/23 15:0747.8 4.6 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 19:31 1634-04-408/18/23 15:074.8 1.8 1
Naphthalene ND ug/kg 08/21/23 19:31 91-20-308/18/23 15:074.8 2.5 1
n-Propylbenzene ND ug/kg 08/21/23 19:31 103-65-108/18/23 15:074.8 1.7 1
Styrene ND ug/kg 08/21/23 19:31 100-42-508/18/23 15:074.8 1.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 19:31 630-20-608/18/23 15:074.8 1.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 19:31 79-34-508/18/23 15:074.8 1.3 1
Tetrachloroethene ND ug/kg 08/21/23 19:31 127-18-408/18/23 15:074.8 1.5 1
Toluene ND ug/kg 08/21/23 19:31 108-88-308/18/23 15:074.8 3.3 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 19:31 87-61-608/18/23 15:074.8 3.9 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 19:31 120-82-108/18/23 15:074.8 4.0 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 19:31 71-55-608/18/23 15:074.8 2.5 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 19:31 79-00-508/18/23 15:074.8 1.6 1
Trichloroethene ND ug/kg 08/21/23 19:31 79-01-608/18/23 15:074.8 3.9 1
Trichlorofluoromethane ND ug/kg 08/21/23 19:31 75-69-408/18/23 15:074.8 2.6 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 19:31 96-18-408/18/23 15:074.8 2.4 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 19:31 95-63-608/18/23 15:074.8 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 19:31 108-67-808/18/23 15:074.8 1.6 1
Vinyl acetate ND ug/kg 08/21/23 19:31 108-05-408/18/23 15:0747.8 9.8 1
Vinyl chloride ND ug/kg 08/21/23 19:31 75-01-408/18/23 15:079.6 2.4 1
Xylene (Total)ND ug/kg 08/21/23 19:31 1330-20-708/18/23 15:079.6 2.7 1
m&p-Xylene ND ug/kg 08/21/23 19:31 179601-23-108/18/23 15:079.6 3.3 1
o-Xylene ND ug/kg 08/21/23 19:31 95-47-608/18/23 15:074.8 2.1 1
Surrogates
Toluene-d8 (S)97 %08/21/23 19:31 2037-26-508/18/23 15:0770-130 1
4-Bromofluorobenzene (S)94 %08/21/23 19:31 460-00-408/18/23 15:0770-130 1
1,2-Dichloroethane-d4 (S)84 %08/21/23 19:31 17060-07-008/18/23 15:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.3 %08/17/23 17:26 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 7-1 Lab ID:92683348025 Collected:08/16/23 18:40 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)4.8J mg/kg 08/21/23 16:3308/18/23 17:196.6 4.7 1
Surrogates
n-Pentacosane (S)88 %08/21/23 16:33 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/23 09:4308/18/23 15:036.4 1.8 1
Surrogates
4-Bromofluorobenzene (S)113 %08/19/23 09:43 460-00-408/18/23 15:0366-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 19:49 67-64-108/18/23 15:0794.7 30.4 1
Benzene ND ug/kg 08/21/23 19:49 71-43-208/18/23 15:074.7 1.9 1
Bromobenzene ND ug/kg 08/21/23 19:49 108-86-108/18/23 15:074.7 1.5 1
Bromochloromethane ND ug/kg 08/21/23 19:49 74-97-508/18/23 15:074.7 1.4 1
Bromodichloromethane ND ug/kg 08/21/23 19:49 75-27-408/18/23 15:074.7 1.8 1
Bromoform ND ug/kg 08/21/23 19:49 75-25-208/18/23 15:074.7 1.7 1
Bromomethane ND ug/kg 08/21/23 19:49 74-83-908/18/23 15:0718.9 14.7 1
2-Butanone (MEK)ND ug/kg 08/21/23 19:49 78-93-308/18/23 15:0794.7 22.7 1
n-Butylbenzene ND ug/kg 08/21/23 19:49 104-51-808/18/23 15:074.7 3.0 1
sec-Butylbenzene ND ug/kg 08/21/23 19:49 135-98-808/18/23 15:074.7 2.1 1
tert-Butylbenzene ND ug/kg 08/21/23 19:49 98-06-608/18/23 15:074.7 1.7 1
Carbon tetrachloride ND ug/kg 08/21/23 19:49 56-23-508/18/23 15:074.7 1.8 1
Chlorobenzene ND ug/kg 08/21/23 19:49 108-90-708/18/23 15:074.7 2.7 1
Chloroethane ND ug/kg 08/21/23 19:49 75-00-308/18/23 15:079.5 3.7 1
Chloroform ND ug/kg 08/21/23 19:49 67-66-308/18/23 15:074.7 4.0 1
Chloromethane ND ug/kg 08/21/23 19:49 74-87-308/18/23 15:079.5 4.0 1
2-Chlorotoluene ND ug/kg 08/21/23 19:49 95-49-808/18/23 15:074.7 1.7 1
4-Chlorotoluene ND ug/kg 08/21/23 19:49 106-43-408/18/23 15:074.7 2.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 19:49 96-12-808/18/23 15:074.7 1.8 1
Dibromochloromethane ND ug/kg 08/21/23 19:49 124-48-108/18/23 15:074.7 2.7 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 19:49 106-93-408/18/23 15:074.7 2.1 1
Dibromomethane ND ug/kg 08/21/23 19:49 74-95-308/18/23 15:074.7 1.0 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 19:49 95-50-108/18/23 15:074.7 1.7 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 19:49 541-73-108/18/23 15:074.7 1.5 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 19:49 106-46-708/18/23 15:074.7 1.2 1
Dichlorodifluoromethane ND ug/kg 08/21/23 19:49 75-71-808/18/23 15:079.5 4.8 1
1,1-Dichloroethane ND ug/kg 08/21/23 19:49 75-34-308/18/23 15:074.7 2.0 1
1,2-Dichloroethane ND ug/kg 08/21/23 19:49 107-06-208/18/23 15:074.7 3.1 1
1,1-Dichloroethene ND ug/kg 08/21/23 19:49 75-35-408/18/23 15:074.7 2.0 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 19:49 156-59-208/18/23 15:074.7 1.6 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 19:49 156-60-508/18/23 15:074.7 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 7-1 Lab ID:92683348025 Collected:08/16/23 18:40 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 19:49 78-87-508/18/23 15:074.7 1.4 1
1,3-Dichloropropane ND ug/kg 08/21/23 19:49 142-28-908/18/23 15:074.7 1.5 1
2,2-Dichloropropane ND ug/kg 08/21/23 19:49 594-20-708/18/23 15:074.7 3.6 1
1,1-Dichloropropene ND ug/kg 08/21/23 19:49 563-58-608/18/23 15:074.7 2.3 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 19:49 10061-01-508/18/23 15:074.7 1.3 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 19:49 10061-02-608/18/23 15:074.7 1.6 1
Diisopropyl ether ND ug/kg 08/21/23 19:49 108-20-308/18/23 15:074.7 1.3 1
Ethylbenzene ND ug/kg 08/21/23 19:49 100-41-408/18/23 15:074.7 2.2 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 19:49 87-68-308/18/23 15:079.5 7.7 1
2-Hexanone ND ug/kg 08/21/23 19:49 591-78-608/18/23 15:0747.4 4.6 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 19:49 98-82-808/18/23 15:074.7 1.6 1
p-Isopropyltoluene ND ug/kg 08/21/23 19:49 99-87-608/18/23 15:074.7 2.3 1
Methylene Chloride ND ug/kg 08/21/23 19:49 75-09-208/18/23 15:0718.9 13.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 19:49 108-10-108/18/23 15:0747.4 4.6 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 19:49 1634-04-408/18/23 15:074.7 1.8 1
Naphthalene ND ug/kg 08/21/23 19:49 91-20-308/18/23 15:074.7 2.5 1
n-Propylbenzene ND ug/kg 08/21/23 19:49 103-65-108/18/23 15:074.7 1.7 1
Styrene ND ug/kg 08/21/23 19:49 100-42-508/18/23 15:074.7 1.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 19:49 630-20-608/18/23 15:074.7 1.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 19:49 79-34-508/18/23 15:074.7 1.3 1
Tetrachloroethene ND ug/kg 08/21/23 19:49 127-18-408/18/23 15:074.7 1.5 1
Toluene ND ug/kg 08/21/23 19:49 108-88-308/18/23 15:074.7 3.3 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 19:49 87-61-608/18/23 15:074.7 3.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 19:49 120-82-108/18/23 15:074.7 4.0 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 19:49 71-55-608/18/23 15:074.7 2.5 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 19:49 79-00-508/18/23 15:074.7 1.6 1
Trichloroethene ND ug/kg 08/21/23 19:49 79-01-608/18/23 15:074.7 3.8 1
Trichlorofluoromethane ND ug/kg 08/21/23 19:49 75-69-408/18/23 15:074.7 2.6 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 19:49 96-18-408/18/23 15:074.7 2.4 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 19:49 95-63-608/18/23 15:074.7 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 19:49 108-67-808/18/23 15:074.7 1.6 1
Vinyl acetate ND ug/kg 08/21/23 19:49 108-05-408/18/23 15:0747.4 9.7 1
Vinyl chloride ND ug/kg 08/21/23 19:49 75-01-408/18/23 15:079.5 2.4 1
Xylene (Total)ND ug/kg 08/21/23 19:49 1330-20-708/18/23 15:079.5 2.7 1
m&p-Xylene ND ug/kg 08/21/23 19:49 179601-23-108/18/23 15:079.5 3.2 1
o-Xylene ND ug/kg 08/21/23 19:49 95-47-608/18/23 15:074.7 2.1 1
Surrogates
Toluene-d8 (S)97 %08/21/23 19:49 2037-26-508/18/23 15:0770-130 1
4-Bromofluorobenzene (S)97 %08/21/23 19:49 460-00-408/18/23 15:0770-130 1
1,2-Dichloroethane-d4 (S)84 %08/21/23 19:49 17060-07-008/18/23 15:0770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.6 %08/17/23 17:26 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 7-2 Lab ID:92683348026 Collected:08/16/23 18:55 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 16:5108/18/23 17:196.1 4.4 1
Surrogates
n-Pentacosane (S)83 %08/21/23 16:51 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/21/23 15:5208/21/23 12:024.9 1.4 1
Surrogates
4-Bromofluorobenzene (S)110 %08/21/23 15:52 460-00-408/21/23 12:0266-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 13:17 67-64-108/18/23 17:2273.0 23.4 1
Benzene ND ug/kg 08/21/23 13:17 71-43-208/18/23 17:223.6 1.5 1
Bromobenzene ND ug/kg 08/21/23 13:17 108-86-108/18/23 17:223.6 1.2 1
Bromochloromethane ND ug/kg 08/21/23 13:17 74-97-508/18/23 17:223.6 1.1 1
Bromodichloromethane ND ug/kg 08/21/23 13:17 75-27-408/18/23 17:223.6 1.4 1
Bromoform ND ug/kg 08/21/23 13:17 75-25-208/18/23 17:223.6 1.3 1
Bromomethane ND ug/kg 08/21/23 13:17 74-83-908/18/23 17:2214.6 11.3 1
2-Butanone (MEK)ND ug/kg 08/21/23 13:17 78-93-308/18/23 17:2273.0 17.5 1
n-Butylbenzene ND ug/kg 08/21/23 13:17 104-51-808/18/23 17:223.6 2.3 1
sec-Butylbenzene ND ug/kg 08/21/23 13:17 135-98-808/18/23 17:223.6 1.6 1
tert-Butylbenzene ND ug/kg 08/21/23 13:17 98-06-608/18/23 17:223.6 1.3 1
Carbon tetrachloride ND ug/kg 08/21/23 13:17 56-23-508/18/23 17:223.6 1.4 1
Chlorobenzene ND ug/kg 08/21/23 13:17 108-90-708/18/23 17:223.6 2.1 1
Chloroethane ND ug/kg 08/21/23 13:17 75-00-308/18/23 17:227.3 2.8 1
Chloroform ND ug/kg 08/21/23 13:17 67-66-308/18/23 17:223.6 3.1 1
Chloromethane ND ug/kg 08/21/23 13:17 74-87-308/18/23 17:227.3 3.1 1
2-Chlorotoluene ND ug/kg 08/21/23 13:17 95-49-808/18/23 17:223.6 1.3 1
4-Chlorotoluene ND ug/kg 08/21/23 13:17 106-43-408/18/23 17:223.6 2.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 13:17 96-12-808/18/23 17:223.6 1.4 1
Dibromochloromethane ND ug/kg 08/21/23 13:17 124-48-108/18/23 17:223.6 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 13:17 106-93-408/18/23 17:223.6 1.6 1
Dibromomethane ND ug/kg 08/21/23 13:17 74-95-308/18/23 17:223.6 0.78 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 13:17 95-50-108/18/23 17:223.6 1.3 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 13:17 541-73-108/18/23 17:223.6 1.1 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 13:17 106-46-708/18/23 17:223.6 0.95 1
Dichlorodifluoromethane ND ug/kg 08/21/23 13:17 75-71-808/18/23 17:227.3 3.7 1
1,1-Dichloroethane ND ug/kg 08/21/23 13:17 75-34-308/18/23 17:223.6 1.5 1
1,2-Dichloroethane ND ug/kg 08/21/23 13:17 107-06-208/18/23 17:223.6 2.4 1
1,1-Dichloroethene ND ug/kg 08/21/23 13:17 75-35-408/18/23 17:223.6 1.5 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 13:17 156-59-208/18/23 17:223.6 1.2 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 13:17 156-60-508/18/23 17:223.6 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 7-2 Lab ID:92683348026 Collected:08/16/23 18:55 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 13:17 78-87-508/18/23 17:223.6 1.1 1
1,3-Dichloropropane ND ug/kg 08/21/23 13:17 142-28-908/18/23 17:223.6 1.1 1
2,2-Dichloropropane ND ug/kg 08/21/23 13:17 594-20-708/18/23 17:223.6 2.8 1
1,1-Dichloropropene ND ug/kg 08/21/23 13:17 563-58-608/18/23 17:223.6 1.8 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 13:17 10061-01-508/18/23 17:223.6 0.99 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 13:17 10061-02-608/18/23 17:223.6 1.3 1
Diisopropyl ether ND ug/kg 08/21/23 13:17 108-20-308/18/23 17:223.6 0.99 1
Ethylbenzene ND ug/kg 08/21/23 13:17 100-41-408/18/23 17:223.6 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 13:17 87-68-308/18/23 17:227.3 6.0 1
2-Hexanone ND ug/kg 08/21/23 13:17 591-78-608/18/23 17:2236.5 3.5 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 13:17 98-82-808/18/23 17:223.6 1.2 1
p-Isopropyltoluene ND ug/kg 08/21/23 13:17 99-87-608/18/23 17:223.6 1.8 1
Methylene Chloride 13.6J ug/kg 08/21/23 13:17 75-09-2 C908/18/23 17:2214.6 10.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 13:17 108-10-108/18/23 17:2236.5 3.5 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 13:17 1634-04-408/18/23 17:223.6 1.4 1
Naphthalene ND ug/kg 08/21/23 13:17 91-20-308/18/23 17:223.6 1.9 1
n-Propylbenzene ND ug/kg 08/21/23 13:17 103-65-108/18/23 17:223.6 1.3 1
Styrene ND ug/kg 08/21/23 13:17 100-42-508/18/23 17:223.6 0.96 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 13:17 630-20-608/18/23 17:223.6 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 13:17 79-34-508/18/23 17:223.6 0.96 1
Tetrachloroethene ND ug/kg 08/21/23 13:17 127-18-408/18/23 17:223.6 1.2 1
Toluene ND ug/kg 08/21/23 13:17 108-88-308/18/23 17:223.6 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 13:17 87-61-608/18/23 17:223.6 2.9 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 13:17 120-82-108/18/23 17:223.6 3.1 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 13:17 71-55-608/18/23 17:223.6 1.9 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 13:17 79-00-508/18/23 17:223.6 1.2 1
Trichloroethene ND ug/kg 08/21/23 13:17 79-01-608/18/23 17:223.6 2.9 1
Trichlorofluoromethane ND ug/kg 08/21/23 13:17 75-69-408/18/23 17:223.6 2.0 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 13:17 96-18-408/18/23 17:223.6 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 13:17 95-63-608/18/23 17:223.6 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 13:17 108-67-808/18/23 17:223.6 1.2 1
Vinyl acetate ND ug/kg 08/21/23 13:17 108-05-408/18/23 17:2236.5 7.5 1
Vinyl chloride ND ug/kg 08/21/23 13:17 75-01-408/18/23 17:227.3 1.9 1
Xylene (Total)3.0J ug/kg 08/21/23 13:17 1330-20-708/18/23 17:227.3 2.1 1
m&p-Xylene 3.0J ug/kg 08/21/23 13:17 179601-23-108/18/23 17:227.3 2.5 1
o-Xylene ND ug/kg 08/21/23 13:17 95-47-608/18/23 17:223.6 1.6 1
Surrogates
Toluene-d8 (S)98 %08/21/23 13:17 2037-26-508/18/23 17:2270-130 1
4-Bromofluorobenzene (S)98 %08/21/23 13:17 460-00-408/18/23 17:2270-130 1
1,2-Dichloroethane-d4 (S)100 %08/21/23 13:17 17060-07-008/18/23 17:2270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.4 %08/17/23 17:26 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 7-3 Lab ID:92683348027 Collected:08/16/23 19:05 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 16:5108/18/23 17:196.4 4.6 1
Surrogates
n-Pentacosane (S)82 %08/21/23 16:51 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/21/23 16:44 M108/21/23 12:025.4 1.5 1
Surrogates
4-Bromofluorobenzene (S)111 %08/21/23 16:44 460-00-408/21/23 12:0266-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 13:36 67-64-108/18/23 17:2210333.1 1
Benzene ND ug/kg 08/21/23 13:36 71-43-208/18/23 17:225.2 2.1 1
Bromobenzene ND ug/kg 08/21/23 13:36 108-86-108/18/23 17:225.2 1.7 1
Bromochloromethane ND ug/kg 08/21/23 13:36 74-97-508/18/23 17:225.2 1.5 1
Bromodichloromethane ND ug/kg 08/21/23 13:36 75-27-408/18/23 17:225.2 2.0 1
Bromoform ND ug/kg 08/21/23 13:36 75-25-208/18/23 17:225.2 1.8 1
Bromomethane ND ug/kg 08/21/23 13:36 74-83-908/18/23 17:2220.6 16.0 1
2-Butanone (MEK)ND ug/kg 08/21/23 13:36 78-93-308/18/23 17:2210324.7 1
n-Butylbenzene ND ug/kg 08/21/23 13:36 104-51-808/18/23 17:225.2 3.2 1
sec-Butylbenzene ND ug/kg 08/21/23 13:36 135-98-808/18/23 17:225.2 2.3 1
tert-Butylbenzene ND ug/kg 08/21/23 13:36 98-06-608/18/23 17:225.2 1.8 1
Carbon tetrachloride ND ug/kg 08/21/23 13:36 56-23-508/18/23 17:225.2 1.9 1
Chlorobenzene ND ug/kg 08/21/23 13:36 108-90-708/18/23 17:225.2 3.0 1
Chloroethane ND ug/kg 08/21/23 13:36 75-00-308/18/23 17:2210.3 4.0 1
Chloroform ND ug/kg 08/21/23 13:36 67-66-308/18/23 17:225.2 4.3 1
Chloromethane ND ug/kg 08/21/23 13:36 74-87-308/18/23 17:2210.3 4.3 1
2-Chlorotoluene ND ug/kg 08/21/23 13:36 95-49-808/18/23 17:225.2 1.8 1
4-Chlorotoluene ND ug/kg 08/21/23 13:36 106-43-408/18/23 17:225.2 2.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 13:36 96-12-808/18/23 17:225.2 2.0 1
Dibromochloromethane ND ug/kg 08/21/23 13:36 124-48-108/18/23 17:225.2 2.9 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 13:36 106-93-408/18/23 17:225.2 2.3 1
Dibromomethane ND ug/kg 08/21/23 13:36 74-95-308/18/23 17:225.2 1.1 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 13:36 95-50-108/18/23 17:225.2 1.9 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 13:36 541-73-108/18/23 17:225.2 1.6 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 13:36 106-46-708/18/23 17:225.2 1.3 1
Dichlorodifluoromethane ND ug/kg 08/21/23 13:36 75-71-808/18/23 17:2210.3 5.2 1
1,1-Dichloroethane ND ug/kg 08/21/23 13:36 75-34-308/18/23 17:225.2 2.1 1
1,2-Dichloroethane ND ug/kg 08/21/23 13:36 107-06-208/18/23 17:225.2 3.4 1
1,1-Dichloroethene ND ug/kg 08/21/23 13:36 75-35-408/18/23 17:225.2 2.1 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 13:36 156-59-208/18/23 17:225.2 1.8 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 13:36 156-60-508/18/23 17:225.2 4.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 7-3 Lab ID:92683348027 Collected:08/16/23 19:05 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 13:36 78-87-508/18/23 17:225.2 1.5 1
1,3-Dichloropropane ND ug/kg 08/21/23 13:36 142-28-908/18/23 17:225.2 1.6 1
2,2-Dichloropropane ND ug/kg 08/21/23 13:36 594-20-708/18/23 17:225.2 3.9 1
1,1-Dichloropropene ND ug/kg 08/21/23 13:36 563-58-608/18/23 17:225.2 2.5 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 13:36 10061-01-508/18/23 17:225.2 1.4 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 13:36 10061-02-608/18/23 17:225.2 1.8 1
Diisopropyl ether ND ug/kg 08/21/23 13:36 108-20-308/18/23 17:225.2 1.4 1
Ethylbenzene ND ug/kg 08/21/23 13:36 100-41-408/18/23 17:225.2 2.4 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 13:36 87-68-308/18/23 17:2210.3 8.4 1
2-Hexanone ND ug/kg 08/21/23 13:36 591-78-608/18/23 17:2251.5 5.0 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 13:36 98-82-808/18/23 17:225.2 1.8 1
p-Isopropyltoluene ND ug/kg 08/21/23 13:36 99-87-608/18/23 17:225.2 2.5 1
Methylene Chloride ND ug/kg 08/21/23 13:36 75-09-208/18/23 17:2220.6 14.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 13:36 108-10-108/18/23 17:2251.5 5.0 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 13:36 1634-04-408/18/23 17:225.2 1.9 1
Naphthalene ND ug/kg 08/21/23 13:36 91-20-308/18/23 17:225.2 2.7 1
n-Propylbenzene ND ug/kg 08/21/23 13:36 103-65-108/18/23 17:225.2 1.8 1
Styrene ND ug/kg 08/21/23 13:36 100-42-508/18/23 17:225.2 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 13:36 630-20-608/18/23 17:225.2 2.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 13:36 79-34-508/18/23 17:225.2 1.4 1
Tetrachloroethene ND ug/kg 08/21/23 13:36 127-18-408/18/23 17:225.2 1.6 1
Toluene ND ug/kg 08/21/23 13:36 108-88-308/18/23 17:225.2 3.6 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 13:36 87-61-608/18/23 17:225.2 4.2 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 13:36 120-82-108/18/23 17:225.2 4.3 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 13:36 71-55-608/18/23 17:225.2 2.7 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 13:36 79-00-508/18/23 17:225.2 1.7 1
Trichloroethene ND ug/kg 08/21/23 13:36 79-01-608/18/23 17:225.2 4.2 1
Trichlorofluoromethane ND ug/kg 08/21/23 13:36 75-69-408/18/23 17:225.2 2.8 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 13:36 96-18-408/18/23 17:225.2 2.6 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 13:36 95-63-608/18/23 17:225.2 3.1 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 13:36 108-67-808/18/23 17:225.2 1.7 1
Vinyl acetate ND ug/kg 08/21/23 13:36 108-05-408/18/23 17:2251.5 10.6 1
Vinyl chloride ND ug/kg 08/21/23 13:36 75-01-408/18/23 17:2210.3 2.6 1
Xylene (Total)ND ug/kg 08/21/23 13:36 1330-20-708/18/23 17:2210.3 2.9 1
m&p-Xylene ND ug/kg 08/21/23 13:36 179601-23-108/18/23 17:2210.3 3.5 1
o-Xylene ND ug/kg 08/21/23 13:36 95-47-608/18/23 17:225.2 2.3 1
Surrogates
Toluene-d8 (S)99 %08/21/23 13:36 2037-26-508/18/23 17:2270-130 1
4-Bromofluorobenzene (S)98 %08/21/23 13:36 460-00-408/18/23 17:2270-130 1
1,2-Dichloroethane-d4 (S)99 %08/21/23 13:36 17060-07-008/18/23 17:2270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.5 %08/17/23 17:26 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 8 Lab ID:92683348028 Collected:08/16/23 19:20 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)4.3J mg/kg 08/21/23 17:0908/18/23 17:196.0 4.3 1
Surrogates
n-Pentacosane (S)65 %08/21/23 17:09 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/21/23 17:1008/21/23 12:024.3 1.2 1
Surrogates
4-Bromofluorobenzene (S)111 %08/21/23 17:10 460-00-408/21/23 12:0266-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 14:13 67-64-108/18/23 17:2282.5 26.5 1
Benzene ND ug/kg 08/21/23 14:13 71-43-208/18/23 17:224.1 1.6 1
Bromobenzene ND ug/kg 08/21/23 14:13 108-86-108/18/23 17:224.1 1.3 1
Bromochloromethane ND ug/kg 08/21/23 14:13 74-97-508/18/23 17:224.1 1.2 1
Bromodichloromethane ND ug/kg 08/21/23 14:13 75-27-408/18/23 17:224.1 1.6 1
Bromoform ND ug/kg 08/21/23 14:13 75-25-208/18/23 17:224.1 1.5 1
Bromomethane ND ug/kg 08/21/23 14:13 74-83-908/18/23 17:2216.5 12.8 1
2-Butanone (MEK)ND ug/kg 08/21/23 14:13 78-93-308/18/23 17:2282.5 19.8 1
n-Butylbenzene ND ug/kg 08/21/23 14:13 104-51-808/18/23 17:224.1 2.6 1
sec-Butylbenzene ND ug/kg 08/21/23 14:13 135-98-808/18/23 17:224.1 1.8 1
tert-Butylbenzene ND ug/kg 08/21/23 14:13 98-06-608/18/23 17:224.1 1.5 1
Carbon tetrachloride ND ug/kg 08/21/23 14:13 56-23-508/18/23 17:224.1 1.5 1
Chlorobenzene ND ug/kg 08/21/23 14:13 108-90-708/18/23 17:224.1 2.4 1
Chloroethane ND ug/kg 08/21/23 14:13 75-00-308/18/23 17:228.2 3.2 1
Chloroform ND ug/kg 08/21/23 14:13 67-66-308/18/23 17:224.1 3.4 1
Chloromethane ND ug/kg 08/21/23 14:13 74-87-308/18/23 17:228.2 3.5 1
2-Chlorotoluene ND ug/kg 08/21/23 14:13 95-49-808/18/23 17:224.1 1.5 1
4-Chlorotoluene ND ug/kg 08/21/23 14:13 106-43-408/18/23 17:224.1 2.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 14:13 96-12-808/18/23 17:224.1 1.6 1
Dibromochloromethane ND ug/kg 08/21/23 14:13 124-48-108/18/23 17:224.1 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 14:13 106-93-408/18/23 17:224.1 1.8 1
Dibromomethane ND ug/kg 08/21/23 14:13 74-95-308/18/23 17:224.1 0.88 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 14:13 95-50-108/18/23 17:224.1 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 14:13 541-73-108/18/23 17:224.1 1.3 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 14:13 106-46-708/18/23 17:224.1 1.1 1
Dichlorodifluoromethane ND ug/kg 08/21/23 14:13 75-71-808/18/23 17:228.2 4.2 1
1,1-Dichloroethane ND ug/kg 08/21/23 14:13 75-34-308/18/23 17:224.1 1.7 1
1,2-Dichloroethane ND ug/kg 08/21/23 14:13 107-06-208/18/23 17:224.1 2.7 1
1,1-Dichloroethene ND ug/kg 08/21/23 14:13 75-35-408/18/23 17:224.1 1.7 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 14:13 156-59-208/18/23 17:224.1 1.4 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 14:13 156-60-508/18/23 17:224.1 3.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 8 Lab ID:92683348028 Collected:08/16/23 19:20 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 14:13 78-87-508/18/23 17:224.1 1.2 1
1,3-Dichloropropane ND ug/kg 08/21/23 14:13 142-28-908/18/23 17:224.1 1.3 1
2,2-Dichloropropane ND ug/kg 08/21/23 14:13 594-20-708/18/23 17:224.1 3.1 1
1,1-Dichloropropene ND ug/kg 08/21/23 14:13 563-58-608/18/23 17:224.1 2.0 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 14:13 10061-01-508/18/23 17:224.1 1.1 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 14:13 10061-02-608/18/23 17:224.1 1.4 1
Diisopropyl ether ND ug/kg 08/21/23 14:13 108-20-308/18/23 17:224.1 1.1 1
Ethylbenzene ND ug/kg 08/21/23 14:13 100-41-408/18/23 17:224.1 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 14:13 87-68-308/18/23 17:228.2 6.7 1
2-Hexanone ND ug/kg 08/21/23 14:13 591-78-608/18/23 17:2241.2 4.0 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 14:13 98-82-808/18/23 17:224.1 1.4 1
p-Isopropyltoluene ND ug/kg 08/21/23 14:13 99-87-608/18/23 17:224.1 2.0 1
Methylene Chloride ND ug/kg 08/21/23 14:13 75-09-208/18/23 17:2216.5 11.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 14:13 108-10-108/18/23 17:2241.2 4.0 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 14:13 1634-04-408/18/23 17:224.1 1.5 1
Naphthalene ND ug/kg 08/21/23 14:13 91-20-308/18/23 17:224.1 2.2 1
n-Propylbenzene ND ug/kg 08/21/23 14:13 103-65-108/18/23 17:224.1 1.5 1
Styrene ND ug/kg 08/21/23 14:13 100-42-508/18/23 17:224.1 1.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 14:13 630-20-608/18/23 17:224.1 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 14:13 79-34-508/18/23 17:224.1 1.1 1
Tetrachloroethene ND ug/kg 08/21/23 14:13 127-18-408/18/23 17:224.1 1.3 1
Toluene ND ug/kg 08/21/23 14:13 108-88-308/18/23 17:224.1 2.8 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 14:13 87-61-608/18/23 17:224.1 3.3 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 14:13 120-82-108/18/23 17:224.1 3.5 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 14:13 71-55-608/18/23 17:224.1 2.1 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 14:13 79-00-508/18/23 17:224.1 1.4 1
Trichloroethene ND ug/kg 08/21/23 14:13 79-01-608/18/23 17:224.1 3.3 1
Trichlorofluoromethane ND ug/kg 08/21/23 14:13 75-69-408/18/23 17:224.1 2.3 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 14:13 96-18-408/18/23 17:224.1 2.1 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 14:13 95-63-608/18/23 17:224.1 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 14:13 108-67-808/18/23 17:224.1 1.4 1
Vinyl acetate ND ug/kg 08/21/23 14:13 108-05-408/18/23 17:2241.2 8.5 1
Vinyl chloride ND ug/kg 08/21/23 14:13 75-01-408/18/23 17:228.2 2.1 1
Xylene (Total)ND ug/kg 08/21/23 14:13 1330-20-708/18/23 17:228.2 2.4 1
m&p-Xylene ND ug/kg 08/21/23 14:13 179601-23-108/18/23 17:228.2 2.8 1
o-Xylene ND ug/kg 08/21/23 14:13 95-47-608/18/23 17:224.1 1.8 1
Surrogates
Toluene-d8 (S)100 %08/21/23 14:13 2037-26-508/18/23 17:2270-130 1
4-Bromofluorobenzene (S)99 %08/21/23 14:13 460-00-408/18/23 17:2270-130 1
1,2-Dichloroethane-d4 (S)99 %08/21/23 14:13 17060-07-008/18/23 17:2270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.6 %08/17/23 17:26 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 6-3 Lab ID:92683348029 Collected:08/16/23 19:50 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)23.7 mg/kg 08/21/23 17:0908/18/23 17:196.4 4.6 1
Surrogates
n-Pentacosane (S)69 %08/21/23 17:09 629-99-208/18/23 17:1910-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/21/23 17:3508/21/23 12:025.4 1.5 1
Surrogates
4-Bromofluorobenzene (S)110 %08/21/23 17:35 460-00-408/21/23 12:0266-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/21/23 14:32 67-64-108/18/23 17:2292.9 29.8 1
Benzene ND ug/kg 08/21/23 14:32 71-43-208/18/23 17:224.6 1.8 1
Bromobenzene ND ug/kg 08/21/23 14:32 108-86-108/18/23 17:224.6 1.5 1
Bromochloromethane ND ug/kg 08/21/23 14:32 74-97-508/18/23 17:224.6 1.4 1
Bromodichloromethane ND ug/kg 08/21/23 14:32 75-27-408/18/23 17:224.6 1.8 1
Bromoform ND ug/kg 08/21/23 14:32 75-25-208/18/23 17:224.6 1.6 1
Bromomethane ND ug/kg 08/21/23 14:32 74-83-908/18/23 17:2218.6 14.4 1
2-Butanone (MEK)ND ug/kg 08/21/23 14:32 78-93-308/18/23 17:2292.9 22.3 1
n-Butylbenzene ND ug/kg 08/21/23 14:32 104-51-808/18/23 17:224.6 2.9 1
sec-Butylbenzene ND ug/kg 08/21/23 14:32 135-98-808/18/23 17:224.6 2.0 1
tert-Butylbenzene ND ug/kg 08/21/23 14:32 98-06-608/18/23 17:224.6 1.7 1
Carbon tetrachloride ND ug/kg 08/21/23 14:32 56-23-508/18/23 17:224.6 1.7 1
Chlorobenzene ND ug/kg 08/21/23 14:32 108-90-708/18/23 17:224.6 2.7 1
Chloroethane ND ug/kg 08/21/23 14:32 75-00-308/18/23 17:229.3 3.6 1
Chloroform ND ug/kg 08/21/23 14:32 67-66-308/18/23 17:224.6 3.9 1
Chloromethane ND ug/kg 08/21/23 14:32 74-87-308/18/23 17:229.3 3.9 1
2-Chlorotoluene ND ug/kg 08/21/23 14:32 95-49-808/18/23 17:224.6 1.6 1
4-Chlorotoluene ND ug/kg 08/21/23 14:32 106-43-408/18/23 17:224.6 2.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/21/23 14:32 96-12-808/18/23 17:224.6 1.8 1
Dibromochloromethane ND ug/kg 08/21/23 14:32 124-48-108/18/23 17:224.6 2.6 1
1,2-Dibromoethane (EDB)ND ug/kg 08/21/23 14:32 106-93-408/18/23 17:224.6 2.0 1
Dibromomethane ND ug/kg 08/21/23 14:32 74-95-308/18/23 17:224.6 0.99 1
1,2-Dichlorobenzene ND ug/kg 08/21/23 14:32 95-50-108/18/23 17:224.6 1.7 1
1,3-Dichlorobenzene ND ug/kg 08/21/23 14:32 541-73-108/18/23 17:224.6 1.4 1
1,4-Dichlorobenzene ND ug/kg 08/21/23 14:32 106-46-708/18/23 17:224.6 1.2 1
Dichlorodifluoromethane ND ug/kg 08/21/23 14:32 75-71-808/18/23 17:229.3 4.7 1
1,1-Dichloroethane ND ug/kg 08/21/23 14:32 75-34-308/18/23 17:224.6 1.9 1
1,2-Dichloroethane ND ug/kg 08/21/23 14:32 107-06-208/18/23 17:224.6 3.1 1
1,1-Dichloroethene ND ug/kg 08/21/23 14:32 75-35-408/18/23 17:224.6 1.9 1
cis-1,2-Dichloroethene ND ug/kg 08/21/23 14:32 156-59-208/18/23 17:224.6 1.6 1
trans-1,2-Dichloroethene ND ug/kg 08/21/23 14:32 156-60-508/18/23 17:224.6 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 104
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Sample:LINE 6-3 Lab ID:92683348029 Collected:08/16/23 19:50 Received:08/17/23 13:50 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 08/21/23 14:32 78-87-508/18/23 17:224.6 1.4 1
1,3-Dichloropropane ND ug/kg 08/21/23 14:32 142-28-908/18/23 17:224.6 1.4 1
2,2-Dichloropropane ND ug/kg 08/21/23 14:32 594-20-708/18/23 17:224.6 3.5 1
1,1-Dichloropropene ND ug/kg 08/21/23 14:32 563-58-608/18/23 17:224.6 2.2 1
cis-1,3-Dichloropropene ND ug/kg 08/21/23 14:32 10061-01-508/18/23 17:224.6 1.3 1
trans-1,3-Dichloropropene ND ug/kg 08/21/23 14:32 10061-02-608/18/23 17:224.6 1.6 1
Diisopropyl ether ND ug/kg 08/21/23 14:32 108-20-308/18/23 17:224.6 1.3 1
Ethylbenzene ND ug/kg 08/21/23 14:32 100-41-408/18/23 17:224.6 2.2 1
Hexachloro-1,3-butadiene ND ug/kg 08/21/23 14:32 87-68-308/18/23 17:229.3 7.6 1
2-Hexanone ND ug/kg 08/21/23 14:32 591-78-608/18/23 17:2246.5 4.5 1
Isopropylbenzene (Cumene)ND ug/kg 08/21/23 14:32 98-82-808/18/23 17:224.6 1.6 1
p-Isopropyltoluene ND ug/kg 08/21/23 14:32 99-87-608/18/23 17:224.6 2.3 1
Methylene Chloride ND ug/kg 08/21/23 14:32 75-09-208/18/23 17:2218.6 12.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/21/23 14:32 108-10-108/18/23 17:2246.5 4.5 1
Methyl-tert-butyl ether ND ug/kg 08/21/23 14:32 1634-04-408/18/23 17:224.6 1.7 1
Naphthalene ND ug/kg 08/21/23 14:32 91-20-308/18/23 17:224.6 2.4 1
n-Propylbenzene ND ug/kg 08/21/23 14:32 103-65-108/18/23 17:224.6 1.7 1
Styrene ND ug/kg 08/21/23 14:32 100-42-508/18/23 17:224.6 1.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/21/23 14:32 630-20-608/18/23 17:224.6 1.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/21/23 14:32 79-34-508/18/23 17:224.6 1.2 1
Tetrachloroethene ND ug/kg 08/21/23 14:32 127-18-408/18/23 17:224.6 1.5 1
Toluene ND ug/kg 08/21/23 14:32 108-88-308/18/23 17:224.6 3.2 1
1,2,3-Trichlorobenzene ND ug/kg 08/21/23 14:32 87-61-608/18/23 17:224.6 3.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/21/23 14:32 120-82-108/18/23 17:224.6 3.9 1
1,1,1-Trichloroethane ND ug/kg 08/21/23 14:32 71-55-608/18/23 17:224.6 2.4 1
1,1,2-Trichloroethane ND ug/kg 08/21/23 14:32 79-00-508/18/23 17:224.6 1.5 1
Trichloroethene ND ug/kg 08/21/23 14:32 79-01-608/18/23 17:224.6 3.7 1
Trichlorofluoromethane ND ug/kg 08/21/23 14:32 75-69-408/18/23 17:224.6 2.6 1
1,2,3-Trichloropropane ND ug/kg 08/21/23 14:32 96-18-408/18/23 17:224.6 2.4 1
1,2,4-Trimethylbenzene ND ug/kg 08/21/23 14:32 95-63-608/18/23 17:224.6 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/21/23 14:32 108-67-808/18/23 17:224.6 1.6 1
Vinyl acetate ND ug/kg 08/21/23 14:32 108-05-408/18/23 17:2246.5 9.6 1
Vinyl chloride ND ug/kg 08/21/23 14:32 75-01-408/18/23 17:229.3 2.4 1
Xylene (Total)ND ug/kg 08/21/23 14:32 1330-20-708/18/23 17:229.3 2.6 1
m&p-Xylene ND ug/kg 08/21/23 14:32 179601-23-108/18/23 17:229.3 3.2 1
o-Xylene ND ug/kg 08/21/23 14:32 95-47-608/18/23 17:224.6 2.1 1
Surrogates
Toluene-d8 (S)99 %08/21/23 14:32 2037-26-508/18/23 17:2270-130 1
4-Bromofluorobenzene (S)98 %08/21/23 14:32 460-00-408/18/23 17:2270-130 1
1,2-Dichloroethane-d4 (S)101 %08/21/23 14:32 17060-07-008/18/23 17:2270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.2 %08/17/23 17:26 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794602
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348001, 92683348002, 92683348003, 92683348004, 92683348005, 92683348006, 92683348007,
92683348008, 92683348009, 92683348010, 92683348011, 92683348012, 92683348013, 92683348014,
92683348015, 92683348016, 92683348017, 92683348018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4117317
Associated Lab Samples:92683348001, 92683348002, 92683348003, 92683348004, 92683348005, 92683348006, 92683348007,
92683348008, 92683348009, 92683348010, 92683348011, 92683348012, 92683348013, 92683348014,
92683348015, 92683348016, 92683348017, 92683348018
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/18/23 18:141.7
4-Bromofluorobenzene (S)%104 66-130 08/18/23 18:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117318LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 49.450.4 98 70-130
4-Bromofluorobenzene (S)%107 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4117320MATRIX SPIKE SAMPLE:
MSSpike
Result
92683264002
Gas Range Organics (C6-C10)mg/kg 36.341.5 87 57-154ND
4-Bromofluorobenzene (S)%110 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683264001
4117319SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%105105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794605
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348019, 92683348020, 92683348021, 92683348022, 92683348023, 92683348024, 92683348025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4117338
Associated Lab Samples:92683348019, 92683348020, 92683348021, 92683348022, 92683348023, 92683348024, 92683348025
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/18/23 18:401.7
4-Bromofluorobenzene (S)%105 66-130 08/18/23 18:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117339LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 47.750.4 95 70-130
4-Bromofluorobenzene (S)%106 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4117341MATRIX SPIKE SAMPLE:
MSSpike
Result
92683084001
Gas Range Organics (C6-C10)mg/kg 54.264.4 83 57-154ND
4-Bromofluorobenzene (S)%110 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683014004
4117340SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30<2.9
4-Bromofluorobenzene (S)%108109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794919
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348026, 92683348027, 92683348028, 92683348029
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4118888
Associated Lab Samples:92683348026, 92683348027, 92683348028, 92683348029
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/21/23 15:001.7
4-Bromofluorobenzene (S)%110 66-130 08/21/23 15:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4118889LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 47.749.8 96 70-130
4-Bromofluorobenzene (S)%111 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4118891MATRIX SPIKE SAMPLE:
MSSpike
Result
92683348027
Gas Range Organics (C6-C10)mg/kg 23.8 M145.2 52 57-154ND
4-Bromofluorobenzene (S)%96 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683348026
4118890SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%109110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794570
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348001, 92683348002, 92683348003, 92683348004, 92683348005, 92683348006, 92683348007,
92683348008, 92683348009, 92683348010, 92683348011, 92683348012, 92683348013, 92683348014,
92683348015, 92683348016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4117121
Associated Lab Samples:92683348001, 92683348002, 92683348003, 92683348004, 92683348005, 92683348006, 92683348007,
92683348008, 92683348009, 92683348010, 92683348011, 92683348012, 92683348013, 92683348014,
92683348015, 92683348016
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/18/23 12:111.9
1,1,1-Trichloroethane ug/kg ND 5.0 08/18/23 12:112.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/18/23 12:111.3
1,1,2-Trichloroethane ug/kg ND 5.0 08/18/23 12:111.7
1,1-Dichloroethane ug/kg ND 5.0 08/18/23 12:112.1
1,1-Dichloroethene ug/kg ND 5.0 08/18/23 12:112.1
1,1-Dichloropropene ug/kg ND 5.0 08/18/23 12:112.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/18/23 12:114.0
1,2,3-Trichloropropane ug/kg ND 5.0 08/18/23 12:112.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/18/23 12:114.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/18/23 12:113.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/18/23 12:111.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/18/23 12:112.2
1,2-Dichlorobenzene ug/kg ND 5.0 08/18/23 12:111.8
1,2-Dichloroethane ug/kg ND 5.0 08/18/23 12:113.3
1,2-Dichloropropane ug/kg ND 5.0 08/18/23 12:111.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/18/23 12:111.7
1,3-Dichlorobenzene ug/kg ND 5.0 08/18/23 12:111.6
1,3-Dichloropropane ug/kg ND 5.0 08/18/23 12:111.6
1,4-Dichlorobenzene ug/kg ND 5.0 08/18/23 12:111.3
2,2-Dichloropropane ug/kg ND 5.0 08/18/23 12:113.8
2-Butanone (MEK)ug/kg ND 100 08/18/23 12:1124.0
2-Chlorotoluene ug/kg ND 5.0 08/18/23 12:111.8
2-Hexanone ug/kg ND 50.0 08/18/23 12:114.8
4-Chlorotoluene ug/kg ND 5.0 08/18/23 12:112.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/18/23 12:114.8
Acetone ug/kg ND 100 v208/18/23 12:1132.1
Benzene ug/kg ND 5.0 08/18/23 12:112.0
Bromobenzene ug/kg ND 5.0 08/18/23 12:111.6
Bromochloromethane ug/kg ND 5.0 08/18/23 12:111.5
Bromodichloromethane ug/kg ND 5.0 08/18/23 12:111.9
Bromoform ug/kg ND 5.0 08/18/23 12:111.8
Bromomethane ug/kg ND 20.0 v208/18/23 12:1115.5
Carbon tetrachloride ug/kg ND 5.0 08/18/23 12:111.9
Chlorobenzene ug/kg ND 5.0 08/18/23 12:112.9
Chloroethane ug/kg ND 10.0 08/18/23 12:113.9
Chloroform ug/kg ND 5.0 08/18/23 12:114.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4117121
Associated Lab Samples:92683348001, 92683348002, 92683348003, 92683348004, 92683348005, 92683348006, 92683348007,
92683348008, 92683348009, 92683348010, 92683348011, 92683348012, 92683348013, 92683348014,
92683348015, 92683348016
Matrix:Solid
AnalyzedMDL
Chloromethane ug/kg ND 10.0 08/18/23 12:114.2
cis-1,2-Dichloroethene ug/kg ND 5.0 08/18/23 12:111.7
cis-1,3-Dichloropropene ug/kg ND 5.0 08/18/23 12:111.4
Dibromochloromethane ug/kg ND 5.0 08/18/23 12:112.8
Dibromomethane ug/kg ND 5.0 08/18/23 12:111.1
Dichlorodifluoromethane ug/kg ND 10.0 08/18/23 12:115.1
Diisopropyl ether ug/kg ND 5.0 08/18/23 12:111.4
Ethylbenzene ug/kg ND 5.0 08/18/23 12:112.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 08/18/23 12:118.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/18/23 12:111.7
m&p-Xylene ug/kg ND 10.0 08/18/23 12:113.4
Methyl-tert-butyl ether ug/kg ND 5.0 08/18/23 12:111.9
Methylene Chloride ug/kg ND 20.0 08/18/23 12:1113.7
n-Butylbenzene ug/kg ND 5.0 08/18/23 12:113.2
n-Propylbenzene ug/kg ND 5.0 08/18/23 12:111.8
Naphthalene ug/kg ND 5.0 08/18/23 12:112.6
o-Xylene ug/kg ND 5.0 08/18/23 12:112.2
p-Isopropyltoluene ug/kg ND 5.0 08/18/23 12:112.5
sec-Butylbenzene ug/kg ND 5.0 08/18/23 12:112.2
Styrene ug/kg ND 5.0 08/18/23 12:111.3
tert-Butylbenzene ug/kg ND 5.0 08/18/23 12:111.8
Tetrachloroethene ug/kg ND 5.0 08/18/23 12:111.6
Toluene ug/kg ND 5.0 08/18/23 12:113.4
trans-1,2-Dichloroethene ug/kg ND 5.0 08/18/23 12:114.2
trans-1,3-Dichloropropene ug/kg ND 5.0 08/18/23 12:111.7
Trichloroethene ug/kg ND 5.0 08/18/23 12:114.0
Trichlorofluoromethane ug/kg ND 5.0 08/18/23 12:112.8
Vinyl acetate ug/kg ND 50.0 08/18/23 12:1110.3
Vinyl chloride ug/kg ND 10.0 08/18/23 12:112.5
Xylene (Total)ug/kg ND 10.0 08/18/23 12:112.8
1,2-Dichloroethane-d4 (S)%93 70-130 08/18/23 12:11
4-Bromofluorobenzene (S)%98 70-130 08/18/23 12:11
Toluene-d8 (S)%98 70-130 08/18/23 12:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117122LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 532500 106 70-130
1,1,1-Trichloroethane ug/kg 468500 94 70-130
1,1,2,2-Tetrachloroethane ug/kg 515500 103 70-130
1,1,2-Trichloroethane ug/kg 492500 98 70-130
1,1-Dichloroethane ug/kg 457500 91 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117122LABORATORY CONTROL SAMPLE:
LCSSpike
1,1-Dichloroethene ug/kg 471500 94 70-132
1,1-Dichloropropene ug/kg 496500 99 70-130
1,2,3-Trichlorobenzene ug/kg 531500 106 62-136
1,2,3-Trichloropropane ug/kg 472500 94 70-130
1,2,4-Trichlorobenzene ug/kg 551500 110 70-130
1,2,4-Trimethylbenzene ug/kg 538500 108 70-130
1,2-Dibromo-3-chloropropane ug/kg 494500 99 65-130
1,2-Dibromoethane (EDB)ug/kg 517500 103 70-130
1,2-Dichlorobenzene ug/kg 535500 107 70-130
1,2-Dichloroethane ug/kg 422500 84 70-130
1,2-Dichloropropane ug/kg 473500 95 70-130
1,3,5-Trimethylbenzene ug/kg 550500 110 70-130
1,3-Dichlorobenzene ug/kg 543500 109 70-130
1,3-Dichloropropane ug/kg 490500 98 70-130
1,4-Dichlorobenzene ug/kg 534500 107 70-130
2,2-Dichloropropane ug/kg 450500 90 60-130
2-Butanone (MEK)ug/kg 8561000 86 66-130
2-Chlorotoluene ug/kg 520500 104 70-130
2-Hexanone ug/kg 9521000 95 68-130
4-Chlorotoluene ug/kg 534500 107 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 9111000 91 70-130
Acetone ug/kg 781 v310007860-130
Benzene ug/kg 489500 98 70-130
Bromobenzene ug/kg 573500 115 70-130
Bromochloromethane ug/kg 519500 104 70-130
Bromodichloromethane ug/kg 468500 94 70-130
Bromoform ug/kg 570500 114 70-130
Bromomethane ug/kg 413 v35008343-175
Carbon tetrachloride ug/kg 548500 110 70-130
Chlorobenzene ug/kg 542500 108 70-130
Chloroethane ug/kg 426500 85 70-145
Chloroform ug/kg 467500 93 70-130
Chloromethane ug/kg 453500 91 66-146
cis-1,2-Dichloroethene ug/kg 456500 91 70-130
cis-1,3-Dichloropropene ug/kg 469500 94 70-130
Dibromochloromethane ug/kg 539500 108 70-130
Dibromomethane ug/kg 554500 111 70-130
Dichlorodifluoromethane ug/kg 783500 157 42-197
Diisopropyl ether ug/kg 423500 85 68-130
Ethylbenzene ug/kg 482500 96 70-130
Hexachloro-1,3-butadiene ug/kg 617500 123 70-130
Isopropylbenzene (Cumene)ug/kg 543500 109 70-130
m&p-Xylene ug/kg 10501000 105 70-130
Methyl-tert-butyl ether ug/kg 428500 86 70-130
Methylene Chloride ug/kg 424500 85 65-130
n-Butylbenzene ug/kg 547500 109 70-130
n-Propylbenzene ug/kg 530500 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117122LABORATORY CONTROL SAMPLE:
LCSSpike
Naphthalene ug/kg 554500 111 65-135
o-Xylene ug/kg 541500 108 70-130
p-Isopropyltoluene ug/kg 565500 113 70-130
sec-Butylbenzene ug/kg 528500 106 70-130
Styrene ug/kg 558500 112 70-130
tert-Butylbenzene ug/kg 420500 84 70-130
Tetrachloroethene ug/kg 541500 108 70-130
Toluene ug/kg 495500 99 70-130
trans-1,2-Dichloroethene ug/kg 456500 91 70-130
trans-1,3-Dichloropropene ug/kg 457500 91 70-130
Trichloroethene ug/kg 549500 110 70-130
Trichlorofluoromethane ug/kg 508500 102 62-140
Vinyl acetate ug/kg 9091000 91 70-140
Vinyl chloride ug/kg 430500 86 70-152
Xylene (Total)ug/kg 15901500 106 70-130
1,2-Dichloroethane-d4 (S)%81 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4117124MATRIX SPIKE SAMPLE:
MSSpike
Result
92683348002
1,1,1,2-Tetrachloroethane ug/kg 438410 107 22-166ND
1,1,1-Trichloroethane ug/kg 430410 105 23-172ND
1,1,2,2-Tetrachloroethane ug/kg 409410 100 21-158ND
1,1,2-Trichloroethane ug/kg 407410 99 25-160ND
1,1-Dichloroethane ug/kg 418410 102 22-166ND
1,1-Dichloroethene ug/kg 471410 115 18-183ND
1,1-Dichloropropene ug/kg 459410 112 20-181ND
1,2,3-Trichlorobenzene ug/kg 398410 97 10-161ND
1,2,3-Trichloropropane ug/kg 372410 91 21-147ND
1,2,4-Trichlorobenzene ug/kg 433410 106 10-159ND
1,2,4-Trimethylbenzene ug/kg 447410 104 17-17021.8
1,2-Dibromo-3-chloropropane ug/kg 349410 85 10-135ND
1,2-Dibromoethane (EDB)ug/kg 415410 101 30-154ND
1,2-Dichlorobenzene ug/kg 434410 106 26-162ND
1,2-Dichloroethane ug/kg 380410 93 23-161ND
1,2-Dichloropropane ug/kg 426410 104 29-165ND
1,3,5-Trimethylbenzene ug/kg 455410 109 20-1728.8
1,3-Dichlorobenzene ug/kg 447410 109 22-164ND
1,3-Dichloropropane ug/kg 412410 101 27-156ND
1,4-Dichlorobenzene ug/kg 423410 103 20-161ND
2,2-Dichloropropane ug/kg 353410 86 10-159ND
2-Butanone (MEK)ug/kg 719819 88 13-143ND
2-Chlorotoluene ug/kg 432410 106 21-166ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4117124MATRIX SPIKE SAMPLE:
MSSpike
Result
92683348002
2-Hexanone ug/kg 718819 88 19-145ND
4-Chlorotoluene ug/kg 440410 108 19-163ND
4-Methyl-2-pentanone (MIBK)ug/kg 729819 89 21-151ND
Acetone ug/kg 508 v38196210-133ND
Benzene ug/kg 431410 105 29-156ND
Bromobenzene ug/kg 457410 112 25-161ND
Bromochloromethane ug/kg 440410 107 27-158ND
Bromodichloromethane ug/kg 393410 96 23-158ND
Bromoform ug/kg 431410 105 19-152ND
Bromomethane ug/kg 162 v34104010-152ND
Carbon tetrachloride ug/kg 420410 103 18-172ND
Chlorobenzene ug/kg 446410 109 26-166ND
Chloroethane ug/kg 158410 39 10-130ND
Chloroform ug/kg 422410 103 25-161ND
Chloromethane ug/kg 497410 121 27-197ND
cis-1,2-Dichloroethene ug/kg 420410 103 28-165ND
cis-1,3-Dichloropropene ug/kg 387410 94 23-159ND
Dibromochloromethane ug/kg 425410 104 21-151ND
Dibromomethane ug/kg 442410 108 38-158ND
Dichlorodifluoromethane ug/kg 782410 191 10-200ND
Diisopropyl ether ug/kg 386410 94 23-160ND
Ethylbenzene ug/kg 412410 100 22-1633.3J
Hexachloro-1,3-butadiene ug/kg 500410 122 10-192ND
Isopropylbenzene (Cumene)ug/kg 462410 113 24-173ND
m&p-Xylene ug/kg 892819 108 22-1717.0J
Methyl-tert-butyl ether ug/kg 368410 90 25-153ND
Methylene Chloride ug/kg 399410 97 10-165ND
n-Butylbenzene ug/kg 454410 110 10-1865.0
n-Propylbenzene ug/kg 443410 108 16-171ND
Naphthalene ug/kg 404410 99 10-159ND
o-Xylene ug/kg 452410 110 23-1713.6J
p-Isopropyltoluene ug/kg 464410 112 13-1844.8
sec-Butylbenzene ug/kg 452410 110 16-182ND
Styrene ug/kg 453410 111 25-169ND
tert-Butylbenzene ug/kg 348410 85 20-174ND
Tetrachloroethene ug/kg 444410 109 14-171ND
Toluene ug/kg 428410 104 24-166ND
trans-1,2-Dichloroethene ug/kg 427410 104 24-170ND
trans-1,3-Dichloropropene ug/kg 383410 94 22-157ND
Trichloroethene ug/kg 465410 113 23-176ND
Trichlorofluoromethane ug/kg 252410 62 10-138ND
Vinyl acetate ug/kg 723819 88 11-166ND
Vinyl chloride ug/kg 413410 101 21-200ND
Xylene (Total)ug/kg 13401220 109 23-17010.5
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683348001
4117123SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg 464 3 30448
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg 5670 1 305740
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg 2510 7 302350
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30627
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 3068.7
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg 55.0 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683348001
4117123SAMPLE DUPLICATE:
m&p-Xylene ug/kg 174 0 30174
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30587
n-Propylbenzene ug/kg ND 30220
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg 15.8 4 3015.3
p-Isopropyltoluene ug/kg 855 1 30843
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 3013.8
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg 190 0 30189
1,2-Dichloroethane-d4 (S)%8596
4-Bromofluorobenzene (S)%101105
Toluene-d8 (S)%9490
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794627
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348017, 92683348018, 92683348019, 92683348020, 92683348021, 92683348022, 92683348023,
92683348024, 92683348025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4117554
Associated Lab Samples:92683348017, 92683348018, 92683348019, 92683348020, 92683348021, 92683348022, 92683348023,
92683348024, 92683348025
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/21/23 12:401.9
1,1,1-Trichloroethane ug/kg ND 5.0 08/21/23 12:402.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/21/23 12:401.3
1,1,2-Trichloroethane ug/kg ND 5.0 08/21/23 12:401.7
1,1-Dichloroethane ug/kg ND 5.0 08/21/23 12:402.1
1,1-Dichloroethene ug/kg ND 5.0 08/21/23 12:402.1
1,1-Dichloropropene ug/kg ND 5.0 08/21/23 12:402.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/21/23 12:404.0
1,2,3-Trichloropropane ug/kg ND 5.0 08/21/23 12:402.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/21/23 12:404.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/21/23 12:403.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/21/23 12:401.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/21/23 12:402.2
1,2-Dichlorobenzene ug/kg ND 5.0 08/21/23 12:401.8
1,2-Dichloroethane ug/kg ND 5.0 08/21/23 12:403.3
1,2-Dichloropropane ug/kg ND 5.0 08/21/23 12:401.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/21/23 12:401.7
1,3-Dichlorobenzene ug/kg ND 5.0 08/21/23 12:401.6
1,3-Dichloropropane ug/kg ND 5.0 08/21/23 12:401.6
1,4-Dichlorobenzene ug/kg ND 5.0 08/21/23 12:401.3
2,2-Dichloropropane ug/kg ND 5.0 08/21/23 12:403.8
2-Butanone (MEK)ug/kg ND 100 08/21/23 12:4024.0
2-Chlorotoluene ug/kg ND 5.0 08/21/23 12:401.8
2-Hexanone ug/kg ND 50.0 08/21/23 12:404.8
4-Chlorotoluene ug/kg ND 5.0 08/21/23 12:402.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/21/23 12:404.8
Acetone ug/kg ND 100 08/21/23 12:4032.1
Benzene ug/kg ND 5.0 08/21/23 12:402.0
Bromobenzene ug/kg ND 5.0 08/21/23 12:401.6
Bromochloromethane ug/kg ND 5.0 08/21/23 12:401.5
Bromodichloromethane ug/kg ND 5.0 08/21/23 12:401.9
Bromoform ug/kg ND 5.0 08/21/23 12:401.8
Bromomethane ug/kg ND 20.0 08/21/23 12:4015.5
Carbon tetrachloride ug/kg ND 5.0 08/21/23 12:401.9
Chlorobenzene ug/kg ND 5.0 08/21/23 12:402.9
Chloroethane ug/kg ND 10.0 08/21/23 12:403.9
Chloroform ug/kg ND 5.0 08/21/23 12:404.2
Chloromethane ug/kg ND 10.0 08/21/23 12:404.2
cis-1,2-Dichloroethene ug/kg ND 5.0 08/21/23 12:401.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4117554
Associated Lab Samples:92683348017, 92683348018, 92683348019, 92683348020, 92683348021, 92683348022, 92683348023,
92683348024, 92683348025
Matrix:Solid
AnalyzedMDL
cis-1,3-Dichloropropene ug/kg ND 5.0 08/21/23 12:401.4
Dibromochloromethane ug/kg ND 5.0 08/21/23 12:402.8
Dibromomethane ug/kg ND 5.0 08/21/23 12:401.1
Dichlorodifluoromethane ug/kg ND 10.0 08/21/23 12:405.1
Diisopropyl ether ug/kg ND 5.0 08/21/23 12:401.4
Ethylbenzene ug/kg ND 5.0 08/21/23 12:402.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 08/21/23 12:408.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/21/23 12:401.7
m&p-Xylene ug/kg ND 10.0 08/21/23 12:403.4
Methyl-tert-butyl ether ug/kg ND 5.0 08/21/23 12:401.9
Methylene Chloride ug/kg ND 20.0 08/21/23 12:4013.7
n-Butylbenzene ug/kg ND 5.0 08/21/23 12:403.2
n-Propylbenzene ug/kg ND 5.0 08/21/23 12:401.8
Naphthalene ug/kg ND 5.0 08/21/23 12:402.6
o-Xylene ug/kg ND 5.0 08/21/23 12:402.2
p-Isopropyltoluene ug/kg ND 5.0 08/21/23 12:402.5
sec-Butylbenzene ug/kg ND 5.0 08/21/23 12:402.2
Styrene ug/kg ND 5.0 08/21/23 12:401.3
tert-Butylbenzene ug/kg ND 5.0 08/21/23 12:401.8
Tetrachloroethene ug/kg ND 5.0 08/21/23 12:401.6
Toluene ug/kg ND 5.0 08/21/23 12:403.4
trans-1,2-Dichloroethene ug/kg ND 5.0 08/21/23 12:404.2
trans-1,3-Dichloropropene ug/kg ND 5.0 08/21/23 12:401.7
Trichloroethene ug/kg ND 5.0 08/21/23 12:404.0
Trichlorofluoromethane ug/kg ND 5.0 08/21/23 12:402.8
Vinyl acetate ug/kg ND 50.0 08/21/23 12:4010.3
Vinyl chloride ug/kg ND 10.0 08/21/23 12:402.5
Xylene (Total)ug/kg ND 10.0 08/21/23 12:402.8
1,2-Dichloroethane-d4 (S)%88 70-130 08/21/23 12:40
4-Bromofluorobenzene (S)%96 70-130 08/21/23 12:40
Toluene-d8 (S)%97 70-130 08/21/23 12:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117555LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 509500 102 70-130
1,1,1-Trichloroethane ug/kg 457500 91 70-130
1,1,2,2-Tetrachloroethane ug/kg 515500 103 70-130
1,1,2-Trichloroethane ug/kg 484500 97 70-130
1,1-Dichloroethane ug/kg 454500 91 70-130
1,1-Dichloroethene ug/kg 476500 95 70-132
1,1-Dichloropropene ug/kg 482500 96 70-130
1,2,3-Trichlorobenzene ug/kg 501500 100 62-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117555LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,3-Trichloropropane ug/kg 475500 95 70-130
1,2,4-Trichlorobenzene ug/kg 514500 103 70-130
1,2,4-Trimethylbenzene ug/kg 523500 105 70-130
1,2-Dibromo-3-chloropropane ug/kg 471500 94 65-130
1,2-Dibromoethane (EDB)ug/kg 502500 100 70-130
1,2-Dichlorobenzene ug/kg 512500 102 70-130
1,2-Dichloroethane ug/kg 438500 88 70-130
1,2-Dichloropropane ug/kg 469500 94 70-130
1,3,5-Trimethylbenzene ug/kg 522500 104 70-130
1,3-Dichlorobenzene ug/kg 520500 104 70-130
1,3-Dichloropropane ug/kg 479500 96 70-130
1,4-Dichlorobenzene ug/kg 516500 103 70-130
2,2-Dichloropropane ug/kg 443500 89 60-130
2-Butanone (MEK)ug/kg 9051000 91 66-130
2-Chlorotoluene ug/kg 503500 101 70-130
2-Hexanone ug/kg 9791000 98 68-130
4-Chlorotoluene ug/kg 519500 104 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 9441000 94 70-130
Acetone ug/kg 9001000 90 60-130
Benzene ug/kg 472500 94 70-130
Bromobenzene ug/kg 539500 108 70-130
Bromochloromethane ug/kg 502500 100 70-130
Bromodichloromethane ug/kg 464500 93 70-130
Bromoform ug/kg 539500 108 70-130
Bromomethane ug/kg 468500 94 43-175
Carbon tetrachloride ug/kg 519500 104 70-130
Chlorobenzene ug/kg 505500 101 70-130
Chloroethane ug/kg 464500 93 70-145
Chloroform ug/kg 458500 92 70-130
Chloromethane ug/kg 486500 97 66-146
cis-1,2-Dichloroethene ug/kg 461500 92 70-130
cis-1,3-Dichloropropene ug/kg 454500 91 70-130
Dibromochloromethane ug/kg 511500 102 70-130
Dibromomethane ug/kg 512500 102 70-130
Dichlorodifluoromethane ug/kg 760500 152 42-197
Diisopropyl ether ug/kg 437500 87 68-130
Ethylbenzene ug/kg 462500 92 70-130
Hexachloro-1,3-butadiene ug/kg 540500 108 70-130
Isopropylbenzene (Cumene)ug/kg 509500 102 70-130
m&p-Xylene ug/kg 10101000 101 70-130
Methyl-tert-butyl ether ug/kg 426500 85 70-130
Methylene Chloride ug/kg 451500 90 65-130
n-Butylbenzene ug/kg 526500 105 70-130
n-Propylbenzene ug/kg 514500 103 70-130
Naphthalene ug/kg 527500 105 65-135
o-Xylene ug/kg 516500 103 70-130
p-Isopropyltoluene ug/kg 531500 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117555LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene ug/kg 509500 102 70-130
Styrene ug/kg 525500 105 70-130
tert-Butylbenzene ug/kg 396500 79 70-130
Tetrachloroethene ug/kg 497500 99 70-130
Toluene ug/kg 475500 95 70-130
trans-1,2-Dichloroethene ug/kg 467500 93 70-130
trans-1,3-Dichloropropene ug/kg 455500 91 70-130
Trichloroethene ug/kg 506500 101 70-130
Trichlorofluoromethane ug/kg 507500 101 62-140
Vinyl acetate ug/kg 9221000 92 70-140
Vinyl chloride ug/kg 461500 92 70-152
Xylene (Total)ug/kg 15201500 102 70-130
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4117556MATRIX SPIKE SAMPLE:
MSSpike
Result
92683348017
1,1,1,2-Tetrachloroethane ug/kg 455428 107 22-166ND
1,1,1-Trichloroethane ug/kg 418428 98 23-172ND
1,1,2,2-Tetrachloroethane ug/kg 407428 95 21-158ND
1,1,2-Trichloroethane ug/kg 414428 97 25-160ND
1,1-Dichloroethane ug/kg 394428 92 22-166ND
1,1-Dichloroethene ug/kg 404428 95 18-183ND
1,1-Dichloropropene ug/kg 411428 96 20-181ND
1,2,3-Trichlorobenzene ug/kg 424428 99 10-161ND
1,2,3-Trichloropropane ug/kg 334428 78 21-147ND
1,2,4-Trichlorobenzene ug/kg 432428 101 10-159ND
1,2,4-Trimethylbenzene ug/kg 421428 99 17-170ND
1,2-Dibromo-3-chloropropane ug/kg 389428 91 10-135ND
1,2-Dibromoethane (EDB)ug/kg 423428 99 30-154ND
1,2-Dichlorobenzene ug/kg 447428 105 26-162ND
1,2-Dichloroethane ug/kg 333428 78 23-161ND
1,2-Dichloropropane ug/kg 410428 96 29-165ND
1,3,5-Trimethylbenzene ug/kg 432428 101 20-172ND
1,3-Dichlorobenzene ug/kg 449428 105 22-164ND
1,3-Dichloropropane ug/kg 401428 94 27-156ND
1,4-Dichlorobenzene ug/kg 412428 96 20-161ND
2,2-Dichloropropane ug/kg 160428 38 10-159ND
2-Butanone (MEK)ug/kg 675854 79 13-143ND
2-Chlorotoluene ug/kg 406428 95 21-166ND
2-Hexanone ug/kg 685854 80 19-145ND
4-Chlorotoluene ug/kg 407428 95 19-163ND
4-Methyl-2-pentanone (MIBK)ug/kg 682854 80 21-151ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4117556MATRIX SPIKE SAMPLE:
MSSpike
Result
92683348017
Acetone ug/kg 524854 61 10-133ND
Benzene ug/kg 429428 100 29-156ND
Bromobenzene ug/kg 474428 111 25-161ND
Bromochloromethane ug/kg 457428 107 27-158ND
Bromodichloromethane ug/kg 382428 90 23-158ND
Bromoform ug/kg 466428 109 19-152ND
Bromomethane ug/kg 144428 34 10-152ND
Carbon tetrachloride ug/kg 414428 97 18-172ND
Chlorobenzene ug/kg 450428 106 26-166ND
Chloroethane ug/kg 137428 32 10-130ND
Chloroform ug/kg 400428 94 25-161ND
Chloromethane ug/kg 456428 107 27-197ND
cis-1,2-Dichloroethene ug/kg 386428 90 28-165ND
cis-1,3-Dichloropropene ug/kg 330428 77 23-159ND
Dibromochloromethane ug/kg 442428 103 21-151ND
Dibromomethane ug/kg 491428 115 38-158ND
Dichlorodifluoromethane ug/kg 647428 152 10-200ND
Diisopropyl ether ug/kg 356428 83 23-160ND
Ethylbenzene ug/kg 401428 94 22-163ND
Hexachloro-1,3-butadiene ug/kg 473428 111 10-192ND
Isopropylbenzene (Cumene)ug/kg 459428 107 24-173ND
m&p-Xylene ug/kg 858854 100 22-171ND
Methyl-tert-butyl ether ug/kg 353428 83 25-153ND
Methylene Chloride ug/kg 377428 88 10-165ND
n-Butylbenzene ug/kg 370428 87 10-186ND
n-Propylbenzene ug/kg 410428 96 16-171ND
Naphthalene ug/kg 421428 99 10-159ND
o-Xylene ug/kg 455428 106 23-171ND
p-Isopropyltoluene ug/kg 433428 102 13-184ND
sec-Butylbenzene ug/kg 421428 99 16-182ND
Styrene ug/kg 454428 106 25-169ND
tert-Butylbenzene ug/kg 340428 80 20-174ND
Tetrachloroethene ug/kg 456428 107 14-171ND
Toluene ug/kg 431428 101 24-166ND
trans-1,2-Dichloroethene ug/kg 374428 87 24-170ND
trans-1,3-Dichloropropene ug/kg 315428 74 22-157ND
Trichloroethene ug/kg 481428 113 23-176ND
Trichlorofluoromethane ug/kg 190428 44 10-138ND
Vinyl acetate ug/kg 521854 61 11-166ND
Vinyl chloride ug/kg 371428 87 21-200ND
Xylene (Total)ug/kg 13101280 102 23-170ND
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%93 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683348018
4117557SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683348018
4117557SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%10195
4-Bromofluorobenzene (S)%9897
Toluene-d8 (S)%9997
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794665
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348026, 92683348027, 92683348028, 92683348029
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4118031
Associated Lab Samples:92683348026, 92683348027, 92683348028, 92683348029
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/21/23 12:591.9
1,1,1-Trichloroethane ug/kg ND 5.0 08/21/23 12:592.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/21/23 12:591.3
1,1,2-Trichloroethane ug/kg ND 5.0 08/21/23 12:591.7
1,1-Dichloroethane ug/kg ND 5.0 08/21/23 12:592.1
1,1-Dichloroethene ug/kg ND 5.0 08/21/23 12:592.1
1,1-Dichloropropene ug/kg ND 5.0 08/21/23 12:592.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/21/23 12:594.0
1,2,3-Trichloropropane ug/kg ND 5.0 08/21/23 12:592.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/21/23 12:594.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/21/23 12:593.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/21/23 12:591.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/21/23 12:592.2
1,2-Dichlorobenzene ug/kg ND 5.0 08/21/23 12:591.8
1,2-Dichloroethane ug/kg ND 5.0 08/21/23 12:593.3
1,2-Dichloropropane ug/kg ND 5.0 08/21/23 12:591.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/21/23 12:591.7
1,3-Dichlorobenzene ug/kg ND 5.0 08/21/23 12:591.6
1,3-Dichloropropane ug/kg ND 5.0 08/21/23 12:591.6
1,4-Dichlorobenzene ug/kg ND 5.0 08/21/23 12:591.3
2,2-Dichloropropane ug/kg ND 5.0 08/21/23 12:593.8
2-Butanone (MEK)ug/kg ND 100 08/21/23 12:5924.0
2-Chlorotoluene ug/kg ND 5.0 08/21/23 12:591.8
2-Hexanone ug/kg ND 50.0 08/21/23 12:594.8
4-Chlorotoluene ug/kg ND 5.0 08/21/23 12:592.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/21/23 12:594.8
Acetone ug/kg ND 100 08/21/23 12:5932.1
Benzene ug/kg ND 5.0 08/21/23 12:592.0
Bromobenzene ug/kg ND 5.0 08/21/23 12:591.6
Bromochloromethane ug/kg ND 5.0 08/21/23 12:591.5
Bromodichloromethane ug/kg ND 5.0 08/21/23 12:591.9
Bromoform ug/kg ND 5.0 08/21/23 12:591.8
Bromomethane ug/kg ND 20.0 08/21/23 12:5915.5
Carbon tetrachloride ug/kg ND 5.0 08/21/23 12:591.9
Chlorobenzene ug/kg ND 5.0 08/21/23 12:592.9
Chloroethane ug/kg ND 10.0 08/21/23 12:593.9
Chloroform ug/kg ND 5.0 08/21/23 12:594.2
Chloromethane ug/kg ND 10.0 08/21/23 12:594.2
cis-1,2-Dichloroethene ug/kg ND 5.0 08/21/23 12:591.7
cis-1,3-Dichloropropene ug/kg ND 5.0 08/21/23 12:591.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4118031
Associated Lab Samples:92683348026, 92683348027, 92683348028, 92683348029
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 08/21/23 12:592.8
Dibromomethane ug/kg ND 5.0 08/21/23 12:591.1
Dichlorodifluoromethane ug/kg ND 10.0 08/21/23 12:595.1
Diisopropyl ether ug/kg ND 5.0 08/21/23 12:591.4
Ethylbenzene ug/kg ND 5.0 08/21/23 12:592.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 08/21/23 12:598.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/21/23 12:591.7
m&p-Xylene ug/kg ND 10.0 08/21/23 12:593.4
Methyl-tert-butyl ether ug/kg ND 5.0 08/21/23 12:591.9
Methylene Chloride ug/kg ND 20.0 08/21/23 12:5913.7
n-Butylbenzene ug/kg ND 5.0 08/21/23 12:593.2
n-Propylbenzene ug/kg ND 5.0 08/21/23 12:591.8
Naphthalene ug/kg ND 5.0 08/21/23 12:592.6
o-Xylene ug/kg ND 5.0 08/21/23 12:592.2
p-Isopropyltoluene ug/kg ND 5.0 08/21/23 12:592.5
sec-Butylbenzene ug/kg ND 5.0 08/21/23 12:592.2
Styrene ug/kg ND 5.0 08/21/23 12:591.3
tert-Butylbenzene ug/kg ND 5.0 08/21/23 12:591.8
Tetrachloroethene ug/kg ND 5.0 08/21/23 12:591.6
Toluene ug/kg ND 5.0 08/21/23 12:593.4
trans-1,2-Dichloroethene ug/kg ND 5.0 08/21/23 12:594.2
trans-1,3-Dichloropropene ug/kg ND 5.0 08/21/23 12:591.7
Trichloroethene ug/kg ND 5.0 08/21/23 12:594.0
Trichlorofluoromethane ug/kg ND 5.0 08/21/23 12:592.8
Vinyl acetate ug/kg ND 50.0 08/21/23 12:5910.3
Vinyl chloride ug/kg ND 10.0 08/21/23 12:592.5
Xylene (Total)ug/kg ND 10.0 08/21/23 12:592.8
1,2-Dichloroethane-d4 (S)%95 70-130 08/21/23 12:59
4-Bromofluorobenzene (S)%95 70-130 08/21/23 12:59
Toluene-d8 (S)%98 70-130 08/21/23 12:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4118032LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 495500 99 70-130
1,1,1-Trichloroethane ug/kg 444500 89 70-130
1,1,2,2-Tetrachloroethane ug/kg 496500 99 70-130
1,1,2-Trichloroethane ug/kg 462500 92 70-130
1,1-Dichloroethane ug/kg 442500 88 70-130
1,1-Dichloroethene ug/kg 458500 92 70-132
1,1-Dichloropropene ug/kg 467500 93 70-130
1,2,3-Trichlorobenzene ug/kg 468500 94 62-136
1,2,3-Trichloropropane ug/kg 455500 91 70-130
1,2,4-Trichlorobenzene ug/kg 484500 97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4118032LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 507500 101 70-130
1,2-Dibromo-3-chloropropane ug/kg 440500 88 65-130
1,2-Dibromoethane (EDB)ug/kg 484500 97 70-130
1,2-Dichlorobenzene ug/kg 489500 98 70-130
1,2-Dichloroethane ug/kg 424500 85 70-130
1,2-Dichloropropane ug/kg 459500 92 70-130
1,3,5-Trimethylbenzene ug/kg 501500 100 70-130
1,3-Dichlorobenzene ug/kg 501500 100 70-130
1,3-Dichloropropane ug/kg 465500 93 70-130
1,4-Dichlorobenzene ug/kg 481500 96 70-130
2,2-Dichloropropane ug/kg 428500 86 60-130
2-Butanone (MEK)ug/kg 8431000 84 66-130
2-Chlorotoluene ug/kg 482500 96 70-130
2-Hexanone ug/kg 9201000 92 68-130
4-Chlorotoluene ug/kg 495500 99 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 8911000 89 70-130
Acetone ug/kg 8361000 84 60-130
Benzene ug/kg 458500 92 70-130
Bromobenzene ug/kg 516500 103 70-130
Bromochloromethane ug/kg 467500 93 70-130
Bromodichloromethane ug/kg 453500 91 70-130
Bromoform ug/kg 518500 104 70-130
Bromomethane ug/kg 442500 88 43-175
Carbon tetrachloride ug/kg 502500 100 70-130
Chlorobenzene ug/kg 494500 99 70-130
Chloroethane ug/kg 428500 86 70-145
Chloroform ug/kg 445500 89 70-130
Chloromethane ug/kg 468500 94 66-146
cis-1,2-Dichloroethene ug/kg 445500 89 70-130
cis-1,3-Dichloropropene ug/kg 437500 87 70-130
Dibromochloromethane ug/kg 501500 100 70-130
Dibromomethane ug/kg 486500 97 70-130
Dichlorodifluoromethane ug/kg 752500 150 42-197
Diisopropyl ether ug/kg 422500 84 68-130
Ethylbenzene ug/kg 449500 90 70-130
Hexachloro-1,3-butadiene ug/kg 525500 105 70-130
Isopropylbenzene (Cumene)ug/kg 498500 100 70-130
m&p-Xylene ug/kg 9791000 98 70-130
Methyl-tert-butyl ether ug/kg 415500 83 70-130
Methylene Chloride ug/kg 433500 87 65-130
n-Butylbenzene ug/kg 507500 101 70-130
n-Propylbenzene ug/kg 496500 99 70-130
Naphthalene ug/kg 498500 100 65-135
o-Xylene ug/kg 501500 100 70-130
p-Isopropyltoluene ug/kg 510500 102 70-130
sec-Butylbenzene ug/kg 485500 97 70-130
Styrene ug/kg 521500 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4118032LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 391500 78 70-130
Tetrachloroethene ug/kg 481500 96 70-130
Toluene ug/kg 460500 92 70-130
trans-1,2-Dichloroethene ug/kg 451500 90 70-130
trans-1,3-Dichloropropene ug/kg 439500 88 70-130
Trichloroethene ug/kg 479500 96 70-130
Trichlorofluoromethane ug/kg 479500 96 62-140
Vinyl acetate ug/kg 8921000 89 70-140
Vinyl chloride ug/kg 443500 89 70-152
Xylene (Total)ug/kg 14801500 99 70-130
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4118033MATRIX SPIKE SAMPLE:
MSSpike
Result
92683348026
1,1,1,2-Tetrachloroethane ug/kg 387365 106 22-166ND
1,1,1-Trichloroethane ug/kg 353365 97 23-172ND
1,1,2,2-Tetrachloroethane ug/kg 352365 97 21-158ND
1,1,2-Trichloroethane ug/kg 360365 99 25-160ND
1,1-Dichloroethane ug/kg 334365 92 22-166ND
1,1-Dichloroethene ug/kg 338365 93 18-183ND
1,1-Dichloropropene ug/kg 347365 95 20-181ND
1,2,3-Trichlorobenzene ug/kg 367365 101 10-161ND
1,2,3-Trichloropropane ug/kg 288365 79 21-147ND
1,2,4-Trichlorobenzene ug/kg 375365 103 10-159ND
1,2,4-Trimethylbenzene ug/kg 345365 94 17-170ND
1,2-Dibromo-3-chloropropane ug/kg 340365 93 10-135ND
1,2-Dibromoethane (EDB)ug/kg 361365 99 30-154ND
1,2-Dichlorobenzene ug/kg 382365 105 26-162ND
1,2-Dichloroethane ug/kg 282365 77 23-161ND
1,2-Dichloropropane ug/kg 362365 99 29-165ND
1,3,5-Trimethylbenzene ug/kg 365365 100 20-172ND
1,3-Dichlorobenzene ug/kg 362365 99 22-164ND
1,3-Dichloropropane ug/kg 346365 95 27-156ND
1,4-Dichlorobenzene ug/kg 353365 97 20-161ND
2,2-Dichloropropane ug/kg 134365 37 10-159ND
2-Butanone (MEK)ug/kg 589730 81 13-143ND
2-Chlorotoluene ug/kg 340365 93 21-166ND
2-Hexanone ug/kg 610730 84 19-145ND
4-Chlorotoluene ug/kg 339365 93 19-163ND
4-Methyl-2-pentanone (MIBK)ug/kg 601730 82 21-151ND
Acetone ug/kg 469730 64 10-133ND
Benzene ug/kg 370365 101 29-156ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4118033MATRIX SPIKE SAMPLE:
MSSpike
Result
92683348026
Bromobenzene ug/kg 396365 109 25-161ND
Bromochloromethane ug/kg 382365 105 27-158ND
Bromodichloromethane ug/kg 331365 91 23-158ND
Bromoform ug/kg 401365 110 19-152ND
Bromomethane ug/kg 117365 32 10-152ND
Carbon tetrachloride ug/kg 372365 102 18-172ND
Chlorobenzene ug/kg 383365 105 26-166ND
Chloroethane ug/kg 123365 34 10-130ND
Chloroform ug/kg 340365 93 25-161ND
Chloromethane ug/kg 379365 104 27-197ND
cis-1,2-Dichloroethene ug/kg 331365 91 28-165ND
cis-1,3-Dichloropropene ug/kg 287365 79 23-159ND
Dibromochloromethane ug/kg 384365 105 21-151ND
Dibromomethane ug/kg 417365 114 38-158ND
Dichlorodifluoromethane ug/kg 539365 148 10-200ND
Diisopropyl ether ug/kg 305365 84 23-160ND
Ethylbenzene ug/kg 342365 94 22-163ND
Hexachloro-1,3-butadiene ug/kg 409365 112 10-192ND
Isopropylbenzene (Cumene)ug/kg 390365 107 24-173ND
m&p-Xylene ug/kg 727730 99 22-1713.0J
Methyl-tert-butyl ether ug/kg 294365 81 25-153ND
Methylene Chloride ug/kg 311365 82 10-16513.6J
n-Butylbenzene ug/kg 323365 89 10-186ND
n-Propylbenzene ug/kg 345365 94 16-171ND
Naphthalene ug/kg 375365 103 10-159ND
o-Xylene ug/kg 386365 106 23-171ND
p-Isopropyltoluene ug/kg 366365 100 13-184ND
sec-Butylbenzene ug/kg 354365 97 16-182ND
Styrene ug/kg 382365 105 25-169ND
tert-Butylbenzene ug/kg 291365 80 20-174ND
Tetrachloroethene ug/kg 389365 107 14-171ND
Toluene ug/kg 368365 100 24-166ND
trans-1,2-Dichloroethene ug/kg 310365 85 24-170ND
trans-1,3-Dichloropropene ug/kg 270365 74 22-157ND
Trichloroethene ug/kg 411365 113 23-176ND
Trichlorofluoromethane ug/kg 171365 47 10-138ND
Vinyl acetate ug/kg 451730 62 11-166ND
Vinyl chloride ug/kg 309365 85 21-200ND
Xylene (Total)ug/kg 11101100 101 23-1703.0J
1,2-Dichloroethane-d4 (S)%81 70-130
4-Bromofluorobenzene (S)%93 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683348027
4118034SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683348027
4118034SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9999
4-Bromofluorobenzene (S)%9998
Toluene-d8 (S)%9999
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794551
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348001, 92683348002, 92683348003, 92683348004, 92683348005, 92683348006, 92683348007,
92683348008, 92683348009, 92683348010, 92683348011, 92683348012, 92683348013, 92683348014,
92683348015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4116987
Associated Lab Samples:92683348001, 92683348002, 92683348003, 92683348004, 92683348005, 92683348006, 92683348007,
92683348008, 92683348009, 92683348010, 92683348011, 92683348012, 92683348013, 92683348014,
92683348015
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 4.9 08/21/23 11:053.5
n-Pentacosane (S)%74 10-133 08/21/23 11:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4116988LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 57.066 86 43-130
n-Pentacosane (S)%91 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4116989MATRIX SPIKE SAMPLE:
MSSpike
Result
92683264001
Diesel Range Organics(C10-C28)mg/kg 57.284.5 67 15-130ND
n-Pentacosane (S)%70 10-133
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683264002
4116990SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg ND 30ND
n-Pentacosane (S)%9385
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794607
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348016, 92683348017, 92683348018, 92683348019, 92683348020, 92683348021, 92683348022,
92683348023, 92683348024, 92683348025, 92683348026, 92683348027, 92683348028, 92683348029
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4117367
Associated Lab Samples:92683348016, 92683348017, 92683348018, 92683348019, 92683348020, 92683348021, 92683348022,
92683348023, 92683348024, 92683348025, 92683348026, 92683348027, 92683348028, 92683348029
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 5.0 08/21/23 22:283.6
n-Pentacosane (S)%85 10-133 08/21/23 22:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117368LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 54.767.3 81 43-130
n-Pentacosane (S)%90 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4117369MATRIX SPIKE SAMPLE:
MSSpike
Result
92683348016
Diesel Range Organics(C10-C28)mg/kg 73.981 90 15-130ND
n-Pentacosane (S)%92 10-133
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683371001
4117370SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg ND 30ND
n-Pentacosane (S)%7368
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794375
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348001, 92683348002, 92683348003, 92683348004, 92683348005, 92683348006, 92683348007,
92683348008, 92683348009, 92683348010, 92683348011
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683348001
4116315SAMPLE DUPLICATE:
Percent Moisture %19.9 N282521.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683294012
4116316SAMPLE DUPLICATE:
Percent Moisture %25.1 N212525.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 104
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794379
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683348012, 92683348013, 92683348014, 92683348015, 92683348016, 92683348017, 92683348018,
92683348019, 92683348020, 92683348021, 92683348022, 92683348023, 92683348024, 92683348025,
92683348026, 92683348027, 92683348028, 92683348029
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683348012
4116351SAMPLE DUPLICATE:
Percent Moisture %16.6 N212516.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683371002
4116352SAMPLE DUPLICATE:
Percent Moisture %21.4 N212521.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 104
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 104
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92683348001 794551 794845SUMP 1 EPA 3546 EPA 8015C
92683348002 794551 794845LINE 1-1 EPA 3546 EPA 8015C
92683348003 794551 794845LINE 1-2 EPA 3546 EPA 8015C
92683348004 794551 794845SUMP 3 EPA 3546 EPA 8015C
92683348005 794551 794845LINE 2 EPA 3546 EPA 8015C
92683348006 794551 794845SUMP 4 EPA 3546 EPA 8015C
92683348007 794551 794845NEW BUILD EPA 3546 EPA 8015C
92683348008 794551 794845LINE 3 EPA 3546 EPA 8015C
92683348009 794551 794845UST-1 EPA 3546 EPA 8015C
92683348010 794551 794845UST-2 EPA 3546 EPA 8015C
92683348011 794551 794845UST-3 EPA 3546 EPA 8015C
92683348012 794551 794845UST-4 EPA 3546 EPA 8015C
92683348013 794551 794845UST-5 EPA 3546 EPA 8015C
92683348014 794551 794845UST-6 EPA 3546 EPA 8015C
92683348015 794551 794845UST-7 EPA 3546 EPA 8015C
92683348016 794607 794846UST-8 EPA 3546 EPA 8015C
92683348017 794607 794846SUMP 5 EPA 3546 EPA 8015C
92683348018 794607 794846SUMP 2 EPA 3546 EPA 8015C
92683348019 794607 794846LINE 4 EPA 3546 EPA 8015C
92683348020 794607 794846SUMP 6 EPA 3546 EPA 8015C
92683348021 794607 794846SUMP 7 EPA 3546 EPA 8015C
92683348022 794607 794846LINE 5 EPA 3546 EPA 8015C
92683348023 794607 794846LINE 6-1 EPA 3546 EPA 8015C
92683348024 794607 794846LINE 6-2 EPA 3546 EPA 8015C
92683348025 794607 794846LINE 7-1 EPA 3546 EPA 8015C
92683348026 794607 794846LINE 7-2 EPA 3546 EPA 8015C
92683348027 794607 794846LINE 7-3 EPA 3546 EPA 8015C
92683348028 794607 794846LINE 8 EPA 3546 EPA 8015C
92683348029 794607 794846LINE 6-3 EPA 3546 EPA 8015C
92683348001 794602 794652SUMP 1 EPA 5030B EPA 8015C
92683348002 794602 794652LINE 1-1 EPA 5030B EPA 8015C
92683348003 794602 794652LINE 1-2 EPA 5030B EPA 8015C
92683348004 794602 794652SUMP 3 EPA 5030B EPA 8015C
92683348005 794602 794652LINE 2 EPA 5030B EPA 8015C
92683348006 794602 794652SUMP 4 EPA 5030B EPA 8015C
92683348007 794602 794652NEW BUILD EPA 5030B EPA 8015C
92683348008 794602 794652LINE 3 EPA 5030B EPA 8015C
92683348009 794602 794652UST-1 EPA 5030B EPA 8015C
92683348010 794602 794652UST-2 EPA 5030B EPA 8015C
92683348011 794602 794652UST-3 EPA 5030B EPA 8015C
92683348012 794602 794652UST-4 EPA 5030B EPA 8015C
92683348013 794602 794652UST-5 EPA 5030B EPA 8015C
92683348014 794602 794652UST-6 EPA 5030B EPA 8015C
92683348015 794602 794652UST-7 EPA 5030B EPA 8015C
92683348016 794602 794652UST-8 EPA 5030B EPA 8015C
92683348017 794602 794652SUMP 5 EPA 5030B EPA 8015C
92683348018 794602 794652SUMP 2 EPA 5030B EPA 8015C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 104
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92683348019 794605 794651LINE 4 EPA 5030B EPA 8015C
92683348020 794605 794651SUMP 6 EPA 5030B EPA 8015C
92683348021 794605 794651SUMP 7 EPA 5030B EPA 8015C
92683348022 794605 794651LINE 5 EPA 5030B EPA 8015C
92683348023 794605 794651LINE 6-1 EPA 5030B EPA 8015C
92683348024 794605 794651LINE 6-2 EPA 5030B EPA 8015C
92683348025 794605 794651LINE 7-1 EPA 5030B EPA 8015C
92683348026 794919 794967LINE 7-2 EPA 5030B EPA 8015C
92683348027 794919 794967LINE 7-3 EPA 5030B EPA 8015C
92683348028 794919 794967LINE 8 EPA 5030B EPA 8015C
92683348029 794919 794967LINE 6-3 EPA 5030B EPA 8015C
92683348001 794570 794593SUMP 1 EPA 5035A/5030B EPA 8260D
92683348002 794570 794593LINE 1-1 EPA 5035A/5030B EPA 8260D
92683348003 794570 794593LINE 1-2 EPA 5035A/5030B EPA 8260D
92683348004 794570 794593SUMP 3 EPA 5035A/5030B EPA 8260D
92683348005 794570 794593LINE 2 EPA 5035A/5030B EPA 8260D
92683348006 794570 794593SUMP 4 EPA 5035A/5030B EPA 8260D
92683348007 794570 794593NEW BUILD EPA 5035A/5030B EPA 8260D
92683348008 794570 794593LINE 3 EPA 5035A/5030B EPA 8260D
92683348009 794570 794593UST-1 EPA 5035A/5030B EPA 8260D
92683348010 794570 794593UST-2 EPA 5035A/5030B EPA 8260D
92683348011 794570 794593UST-3 EPA 5035A/5030B EPA 8260D
92683348012 794570 794593UST-4 EPA 5035A/5030B EPA 8260D
92683348013 794570 794593UST-5 EPA 5035A/5030B EPA 8260D
92683348014 794570 794593UST-6 EPA 5035A/5030B EPA 8260D
92683348015 794570 794593UST-7 EPA 5035A/5030B EPA 8260D
92683348016 794570 794593UST-8 EPA 5035A/5030B EPA 8260D
92683348017 794627 794817SUMP 5 EPA 5035A/5030B EPA 8260D
92683348018 794627 794817SUMP 2 EPA 5035A/5030B EPA 8260D
92683348019 794627 794817LINE 4 EPA 5035A/5030B EPA 8260D
92683348020 794627 794817SUMP 6 EPA 5035A/5030B EPA 8260D
92683348021 794627 794817SUMP 7 EPA 5035A/5030B EPA 8260D
92683348022 794627 794817LINE 5 EPA 5035A/5030B EPA 8260D
92683348023 794627 794817LINE 6-1 EPA 5035A/5030B EPA 8260D
92683348024 794627 794817LINE 6-2 EPA 5035A/5030B EPA 8260D
92683348025 794627 794817LINE 7-1 EPA 5035A/5030B EPA 8260D
92683348026 794665 794816LINE 7-2 EPA 5035A/5030B EPA 8260D
92683348027 794665 794816LINE 7-3 EPA 5035A/5030B EPA 8260D
92683348028 794665 794816LINE 8 EPA 5035A/5030B EPA 8260D
92683348029 794665 794816LINE 6-3 EPA 5035A/5030B EPA 8260D
92683348001 794375SUMP 1 SW-846
92683348002 794375LINE 1-1 SW-846
92683348003 794375LINE 1-2 SW-846
92683348004 794375SUMP 3 SW-846
92683348005 794375LINE 2 SW-846
92683348006 794375SUMP 4 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 104
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92683348
MUSA #7214 ALBEMARLE, NC
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92683348007 794375NEW BUILD SW-846
92683348008 794375LINE 3 SW-846
92683348009 794375UST-1 SW-846
92683348010 794375UST-2 SW-846
92683348011 794375UST-3 SW-846
92683348012 794379UST-4 SW-846
92683348013 794379UST-5 SW-846
92683348014 794379UST-6 SW-846
92683348015 794379UST-7 SW-846
92683348016 794379UST-8 SW-846
92683348017 794379SUMP 5 SW-846
92683348018 794379SUMP 2 SW-846
92683348019 794379LINE 4 SW-846
92683348020 794379SUMP 6 SW-846
92683348021 794379SUMP 7 SW-846
92683348022 794379LINE 5 SW-846
92683348023 794379LINE 6-1 SW-846
92683348024 794379LINE 6-2 SW-846
92683348025 794379LINE 7-1 SW-846
92683348026 794379LINE 7-2 SW-846
92683348027 794379LINE 7-3 SW-846
92683348028 794379LINE 8 SW-846
92683348029 794379LINE 6-3 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/22/2023 02:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 104
Page 98 of 104
Page 99 of 104
Page 100 of 104
Page 101 of 104
Page 102 of 104
Page 103 of 104
Page 104 of 104
#=CL#
August 23, 2023
LIMS USE: FR - DANIEL DABKOWSKI
LIMS OBJECT ID: 92683264
92683264
Project:
Pace Project No.:
RE:
Mr. Daniel Dabkowski
Groundwater & Environmental Services, Inc.
104 Corporate Blvd.
Suite 411
West Columbia, SC 29169
MUSA 7214 ALBEMARLE, NC SOIL
Dear Mr. Dabkowski:
Enclosed are the analytical results for sample(s) received by the laboratory on August 17, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
cc:SouthwestPR, GES-SC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 18
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 18
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Lab ID Sample ID Matrix Date Collected Date Received
92683264001 WASTE-1 Solid 08/16/23 18:00 08/17/23 10:00
92683264002 WASTE-2 Solid 08/16/23 18:05 08/17/23 10:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 18
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92683264001 WASTE-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 6010 1 PASI-OAME
EPA 6010 1 PASI-OTMA
EPA 8260D 9 PASI-CSAS
SW-846 1 PASI-CKDF
92683264002 WASTE-2 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CTEG
EPA 6010 1 PASI-OAAM1
EPA 6010 1 PASI-OTMA
EPA 8260D 9 PASI-CSAS
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Sample:WASTE-1 Lab ID:92683264001 Collected:08/16/23 18:00 Received:08/17/23 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 11:2208/18/23 14:226.4 4.6 1
Surrogates
n-Pentacosane (S)84 %08/21/23 11:22 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/18/23 19:0608/18/23 14:555.5 1.5 1
Surrogates
4-Bromofluorobenzene (S)105 %08/18/23 19:06 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
6010 MET ICP
Lead 14.4 mg/kg 08/22/23 03:14 7439-92-108/21/23 08:020.76 0.38 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/21/23 11:57
Pace Analytical Services - Ormond Beach
6010 MET ICP, TCLP
Lead ND mg/L 08/22/23 20:04 7439-92-108/22/23 11:170.10 0.021 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B SC Volatiles
Benzene ND ug/kg 08/17/23 18:12 71-43-208/17/23 10:175.6 2.2 1
Ethylbenzene ND ug/kg 08/17/23 18:12 100-41-408/17/23 10:175.6 2.6 1
Toluene ND ug/kg 08/17/23 18:12 108-88-308/17/23 10:175.6 3.8 1
Xylene (Total)ND ug/kg 08/17/23 18:12 1330-20-708/17/23 10:1711.2 3.2 1
m&p-Xylene ND ug/kg 08/17/23 18:12 179601-23-108/17/23 10:1711.2 3.8 1
o-Xylene ND ug/kg 08/17/23 18:12 95-47-608/17/23 10:175.6 2.5 1
Surrogates
Toluene-d8 (S)97 %08/17/23 18:12 2037-26-508/17/23 10:1770-130 1
4-Bromofluorobenzene (S)99 %08/17/23 18:12 460-00-408/17/23 10:1770-130 1
1,2-Dichloroethane-d4 (S)92 %08/17/23 18:12 17060-07-008/17/23 10:1770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.9 %08/17/23 15:36 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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9800 Kincey Ave. Suite 100
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Page 5 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Sample:WASTE-2 Lab ID:92683264002 Collected:08/16/23 18:05 Received:08/17/23 10:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 08/21/23 11:4008/18/23 14:226.4 4.5 1
Surrogates
n-Pentacosane (S)85 %08/21/23 11:40 629-99-208/18/23 14:2210-133 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/18/23 19:5708/18/23 14:555.0 1.4 1
Surrogates
4-Bromofluorobenzene (S)106 %08/18/23 19:57 460-00-408/18/23 14:5566-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
6010 MET ICP
Lead 18.3 mg/kg 08/22/23 14:24 7439-92-108/21/23 08:023.8 1.9 5
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/21/23 11:57
Pace Analytical Services - Ormond Beach
6010 MET ICP, TCLP
Lead ND mg/L 08/22/23 20:07 7439-92-108/22/23 11:170.10 0.021 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B SC Volatiles
Benzene ND ug/kg 08/17/23 18:49 71-43-208/17/23 10:175.1 2.0 1
Ethylbenzene ND ug/kg 08/17/23 18:49 100-41-408/17/23 10:175.1 2.4 1
Toluene ND ug/kg 08/17/23 18:49 108-88-308/17/23 10:175.1 3.5 1
Xylene (Total)ND ug/kg 08/17/23 18:49 1330-20-708/17/23 10:1710.2 2.9 1
m&p-Xylene ND ug/kg 08/17/23 18:49 179601-23-108/17/23 10:1710.2 3.5 1
o-Xylene ND ug/kg 08/17/23 18:49 95-47-608/17/23 10:175.1 2.3 1
Surrogates
Toluene-d8 (S)98 %08/17/23 18:49 2037-26-508/17/23 10:1770-130 1
4-Bromofluorobenzene (S)99 %08/17/23 18:49 460-00-408/17/23 10:1770-130 1
1,2-Dichloroethane-d4 (S)93 %08/17/23 18:49 17060-07-008/17/23 10:1770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.7 %08/17/23 15:36 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 6 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794602
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683264001, 92683264002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4117317
Associated Lab Samples:92683264001, 92683264002
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/18/23 18:141.7
4-Bromofluorobenzene (S)%104 66-130 08/18/23 18:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117318LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 49.450.4 98 70-130
4-Bromofluorobenzene (S)%107 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4117320MATRIX SPIKE SAMPLE:
MSSpike
Result
92683264002
Gas Range Organics (C6-C10)mg/kg 36.341.5 87 57-154ND
4-Bromofluorobenzene (S)%110 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683264001
4117319SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%105105
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
943750
EPA 3050
EPA 6010
6010 MET Solid
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92683264001, 92683264002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5187582
Associated Lab Samples:92683264001, 92683264002
Matrix:Solid
AnalyzedMDL
Lead mg/kg ND 0.56 08/22/23 02:140.28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5187583LABORATORY CONTROL SAMPLE:
LCSSpike
Lead mg/kg 14.114.1 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5187584MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35817123079
5187585
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead mg/kg M115.7 69 75-12573 1 2014.525.0 35.9 35.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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[phone]
Page 8 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
944159
EPA 3010
EPA 6010
6010 MET TCLP
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92683264001, 92683264002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5187593
Associated Lab Samples:92683264001, 92683264002
Matrix:Water
AnalyzedMDL
Lead mg/L ND 0.010 08/22/23 19:440.0021
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5189263LABORATORY CONTROL SAMPLE:
LCSSpike
Lead mg/L 0.260.25 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5189264MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35820562001
5189265
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead mg/L 2.5 106 75-125107 1 202.50.021U 2.7 2.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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Huntersville, NC 28078
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Page 9 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794341
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B SC
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683264001, 92683264002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4116121
Associated Lab Samples:92683264001, 92683264002
Matrix:Solid
AnalyzedMDL
Benzene ug/kg ND 5.0 08/17/23 16:382.0
Ethylbenzene ug/kg ND 5.0 08/17/23 16:382.3
m&p-Xylene ug/kg ND 10.0 08/17/23 16:383.4
o-Xylene ug/kg ND 5.0 08/17/23 16:382.2
Toluene ug/kg ND 5.0 08/17/23 16:383.4
Xylene (Total)ug/kg ND 10.0 08/17/23 16:382.8
1,2-Dichloroethane-d4 (S)%87 70-130 08/17/23 16:38
4-Bromofluorobenzene (S)%95 70-130 08/17/23 16:38
Toluene-d8 (S)%97 70-130 08/17/23 16:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4116122LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/kg 434500 87 70-130
Ethylbenzene ug/kg 424500 85 70-130
m&p-Xylene ug/kg 9201000 92 70-130
o-Xylene ug/kg 474500 95 70-130
Toluene ug/kg 434500 87 70-130
Xylene (Total)ug/kg 13901500 93 70-130
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4116124MATRIX SPIKE SAMPLE:
MSSpike
Result
92683264002
Benzene ug/kg 544511 106 29-156ND
Ethylbenzene ug/kg 521511 102 22-163ND
m&p-Xylene ug/kg 11201020 110 22-171ND
o-Xylene ug/kg 579511 113 23-171ND
Toluene ug/kg 548511 107 24-166ND
Xylene (Total)ug/kg 17001540 111 23-170ND
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683264001
4116123SAMPLE DUPLICATE:
Benzene ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
Toluene ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9092
4-Bromofluorobenzene (S)%9899
Toluene-d8 (S)%9797
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 11 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794551
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683264001, 92683264002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4116987
Associated Lab Samples:92683264001, 92683264002
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 4.9 08/21/23 11:053.5
n-Pentacosane (S)%74 10-133 08/21/23 11:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4116988LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 57.066 86 43-130
n-Pentacosane (S)%91 10-133
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4116989MATRIX SPIKE SAMPLE:
MSSpike
Result
92683264001
Diesel Range Organics(C10-C28)mg/kg 57.284.5 67 15-130ND
n-Pentacosane (S)%70 10-133
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683264002
4116990SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg ND 30ND
n-Pentacosane (S)%9385
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794336
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683264001, 92683264002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683101001
4116014SAMPLE DUPLICATE:
Percent Moisture %47.9 N292552.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92683300005
4116015SAMPLE DUPLICATE:
Percent Moisture %16.3 N222516.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 13 of 18
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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Page 14 of 18
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92683264
MUSA 7214 ALBEMARLE, NC SOIL
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92683264001 794551 794845WASTE-1 EPA 3546 EPA 8015C
92683264002 794551 794845WASTE-2 EPA 3546 EPA 8015C
92683264001 794602 794652WASTE-1 EPA 5030B EPA 8015C
92683264002 794602 794652WASTE-2 EPA 5030B EPA 8015C
92683264001 943750 943892WASTE-1 EPA 3050 EPA 6010
92683264002 943750 943892WASTE-2 EPA 3050 EPA 6010
92683264001 944159 944243WASTE-1 EPA 3010 EPA 6010
92683264002 944159 944243WASTE-2 EPA 3010 EPA 6010
92683264001 794341 794354WASTE-1 EPA 5035A/5030B EPA 8260D
92683264002 794341 794354WASTE-2 EPA 5035A/5030B EPA 8260D
92683264001 794336WASTE-1 SW-846
92683264002 794336WASTE-2 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 12:30 PM
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[phone]
Page 15 of 18
Page 16 of 18
Page 17 of 18
Page 18 of 18
#=CL#
August 23, 2023
LIMS USE: FR - DANIEL DABKOWSKI
LIMS OBJECT ID: 92683368
92683368
Project:
Pace Project No.:
RE:
Mr. Daniel Dabkowski
Groundwater & Environmental Services, Inc.
104 Corporate Blvd.
Suite 411
West Columbia, SC 29169
MUSA 7214 ALBEMARLE NC WATER
Dear Mr. Dabkowski:
Enclosed are the analytical results for sample(s) received by the laboratory on August 17, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
cc:SouthwestPR, GES-SC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 23
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Lab ID Sample ID Matrix Date Collected Date Received
92683368001 GW-1 Water 08/16/23 15:15 08/17/23 13:50
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92683368001 GW-1 EPA 6010 7 PASI-OAME
EPA 7470 1 PASI-OJNK
EPA 8260D 9 PASI-CJJK
EPA 1010B 1 PASI-ASMS
EPA 9040C 1 PASI-ASMS
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Sample:GW-1 Lab ID:92683368001 Collected:08/16/23 15:15 Received:08/17/23 13:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/21/23 14:09
Pace Analytical Services - Ormond Beach
6010 MET ICP, TCLP
Arsenic ND mg/L 08/23/23 11:44 7440-38-208/22/23 15:030.10 0.034 1
Barium 0.013J mg/L 08/23/23 11:44 7440-39-308/22/23 15:030.10 0.0084 1
Cadmium ND mg/L 08/23/23 11:44 7440-43-908/22/23 15:030.010 0.0033 1
Chromium ND mg/L 08/23/23 11:44 7440-47-308/22/23 15:030.050 0.017 1
Lead ND mg/L 08/23/23 11:44 7439-92-108/22/23 15:030.10 0.021 1
Selenium ND mg/L 08/23/23 11:44 7782-49-208/22/23 15:030.15 0.039 1
Silver ND mg/L 08/23/23 11:44 7440-22-408/22/23 15:030.050 0.010 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 08/21/23 14:09
Pace Analytical Services - Ormond Beach
7470 Mercury, TCLP
Mercury ND mg/L 08/22/23 14:55 7439-97-608/22/23 10:080.0020 0.00090 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260 MSV Low Level SC
Benzene 3.2 ug/L 08/19/23 01:17 71-43-21.0 0.34 1
Ethylbenzene 0.46J ug/L 08/19/23 01:17 100-41-41.0 0.30 1
Toluene ND ug/L 08/19/23 01:17 108-88-31.0 0.48 1
Xylene (Total)ND ug/L 08/19/23 01:17 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 08/19/23 01:17 179601-23-12.0 0.71 1
o-Xylene ND ug/L 08/19/23 01:17 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %08/19/23 01:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %08/19/23 01:17 17060-07-070-130 1
Toluene-d8 (S)100 %08/19/23 01:17 2037-26-570-130 1
Analytical Method: EPA 1010B
Pace Analytical Services - Asheville
1010 Flashpoint,Closed Cup
Flashpoint >200 deg F 08/19/23 12:0570.0 1
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
9040 pH
pH at 25 Degrees C 7.4 Std. Units 08/18/23 16:39 H30.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 02:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
944107
EPA 7470
EPA 7470
7470 Mercury TCLP
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92683368001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5187594
Associated Lab Samples:92683368001
Matrix:Water
AnalyzedMDL
Mercury mg/L ND 0.00020 08/22/23 14:460.000090
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5189027LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/L 0.00180.002 88 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5189028MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683368001
5189029
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/L 0.02 88 75-12590 3 200.02ND 0.018 0.018
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 02:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
944244
EPA 3010
EPA 6010
6010 MET TCLP
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples:92683368001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:5187594
Associated Lab Samples:92683368001
Matrix:Water
AnalyzedMDL
Arsenic mg/L ND 0.010 08/23/23 11:370.0034
Barium mg/L ND 0.010 08/23/23 11:370.00084
Cadmium mg/L ND 0.0010 08/23/23 11:370.00033
Chromium mg/L ND 0.0050 08/23/23 11:370.0017
Lead mg/L ND 0.010 08/23/23 11:370.0021
Selenium mg/L ND 0.015 08/23/23 11:370.0039
Silver mg/L ND 0.0050 08/23/23 11:370.0010
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
5189828LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 0.240.25 95 80-120
Barium mg/L 0.260.25 106 80-120
Cadmium mg/L 0.0250.025 100 80-120
Chromium mg/L 0.260.25 102 80-120
Lead mg/L 0.260.25 103 80-120
Selenium mg/L 0.250.25 98 80-120
Silver mg/L 0.0260.025 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
5189829MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92683368001
5189830
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/L 2.5 95 75-12595 0 202.5ND 2.4 2.4
Barium mg/L 2.5 104 75-125104 0 202.50.013J 2.6 2.6
Cadmium mg/L 0.25 99 75-125100 0 200.25ND 0.25 0.25
Chromium mg/L 2.5 100 75-125101 0 202.5ND 2.5 2.5
Lead mg/L 2.5 103 75-125103 0 202.5ND 2.6 2.6
Selenium mg/L 2.5 98 75-12598 0 202.5ND 2.5 2.4
Silver mg/L 0.25 104 75-125110 5 200.25ND 0.26 0.28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 02:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794649
EPA 8260D
EPA 8260D
8260 MSV Low Level SC
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92683368001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4117881
Associated Lab Samples:92683368001
Matrix:Water
AnalyzedMDL
Benzene ug/L ND 1.0 08/18/23 17:430.34
Ethylbenzene ug/L ND 1.0 08/18/23 17:430.30
m&p-Xylene ug/L ND 2.0 08/18/23 17:430.71
o-Xylene ug/L ND 1.0 08/18/23 17:430.34
Toluene ug/L ND 1.0 08/18/23 17:430.48
Xylene (Total)ug/L ND 1.0 08/18/23 17:430.34
1,2-Dichloroethane-d4 (S)%109 70-130 08/18/23 17:43
4-Bromofluorobenzene (S)%98 70-130 08/18/23 17:43
Toluene-d8 (S)%100 70-130 08/18/23 17:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4117882LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/L 20.220 101 70-130
Ethylbenzene ug/L 20.420 102 70-130
m&p-Xylene ug/L 41.540 104 70-130
o-Xylene ug/L 20.620 103 70-130
Toluene ug/L 20.320 101 70-130
Xylene (Total)ug/L 62.160 104 70-130
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4117884MATRIX SPIKE SAMPLE:
MSSpike
Result
92682803001
Benzene ug/L 24.720 123 70-151ND
Ethylbenzene ug/L 25.320 127 66-153ND
m&p-Xylene ug/L 50.940 127 69-152ND
o-Xylene ug/L 25.020 125 70-148ND
Toluene ug/L 24.620 123 59-148ND
Xylene (Total)ug/L 75.960 127 63-158ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 02:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92682776005
4117883SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
o-Xylene ug/L ND 30ND
Toluene ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%111111
4-Bromofluorobenzene (S)%9798
Toluene-d8 (S)%99101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 02:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794768
EPA 1010B
EPA 1010B
1010 Flash Point, Closed Cup
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92683368001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92682494001
4118353SAMPLE DUPLICATE:
Flashpoint deg F >200>200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 02:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
794370
EPA 9040C
EPA 9040C
9040 pH
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92683368001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92682308002
4116283SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 7.9 H10107.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92682333001
4116284SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 7.0 H31107.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 02:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Sample was received or analysis requested beyond the recognized method holding time.H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 02:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92683368
MUSA 7214 ALBEMARLE NC WATER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92683368001 944244 944318GW-1 EPA 3010 EPA 6010
92683368001 944107 944168GW-1 EPA 7470 EPA 7470
92683368001 794649GW-1 EPA 8260D
92683368001 794768GW-1 EPA 1010B
92683368001 794370GW-1 EPA 9040C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2023 02:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
Page 14 of 23
Page 15 of 23
Page 16 of 23
August 22, 2023
Analytical Environmental Services, Inc. received samples on
for the analyses presented in following report.
1
“No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in
the report or QC Summary. Additionally, all results for the associated Quality Control samples were within
EPA and/or AES established limits.
AES’ certifications are as follows:
-South Carolina Certification number 98016003 for Clean Water Act and for Solid and Hazardous Waste,
effective until 6/30/24.
These results relate only to the items tested as received. This report may only be reproduced in full.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Project Manager
2308N45
Taylor Cannon
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville NC 28078-8400
92683368
Shawn Boyd
August 18, 2023 7:55 am
Taylor Cannon:
Page 1 of 7Page 17 of 23
Page 2 of 7Page 18 of 23
2308N45-001
22-Aug-23Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQualReporting
LimitResult
Client:
Aqueous
8/16/2023 3:15:00 PM
GW-1
Matrix:
Collection Date:
Client Sample ID:
92683368
Pace Analytical Services, Inc.
Lab ID:
Project Name:
Analyst
(SW7.3.4.2)Sulfide, Reactive SW846-7.3
Sulfide, Reactive 144 100 mg/Kg 361781 1 08/22/2023 13:52 AA
(SW7.3.3.2)Cyanide, Reactive SW846-7.3
Cyanide, Reactive BRL 0.962 mg/Kg 361795 1 08/22/2023 14:48 AA
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit Page 3 of 7Page 19 of 23
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Page 20 of 23
22-Aug-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORT92683368
2308N45
Pace Analytical Services, Inc.
361781
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:361781MBLK 08/22/2023Sulfide, Reactive SW846-7.3
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 08/22/2023 524287MB-361781
12410493
Sulfide, Reactive 100BRL
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:361781LCS 08/22/2023Sulfide, Reactive SW846-7.3
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 08/22/2023 524287LCS-361781
12410494
Sulfide, Reactive 100472.0 472.0 100 65.5 125
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:361781MS 08/22/2023Sulfide, Reactive SW846-7.3
GW-1 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 08/22/2023 5242872308N45-001AMS
12410496
Sulfide, Reactive 100454.2 472.0 144.0 65.7 56.5 128
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:361781MSD 08/22/2023Sulfide, Reactive SW846-7.3
GW-1 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 08/22/2023 5242872308N45-001AMSD
12410497
Sulfide, Reactive 100438.2 19.6472.0 144.0 62.3 56.5 128 454.2 3.57
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 5 of 7Page 21 of 23
22-Aug-23Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORT92683368
2308N45
Pace Analytical Services, Inc.
361795
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:361795MBLK 08/22/2023Cyanide, Reactive SW846-7.3
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 08/22/2023 524294MB-361795
12410651
Cyanide, Reactive 1.00BRL
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:361795LCS 08/22/2023Cyanide, Reactive SW846-7.3
Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 08/22/2023 524294LCS-361795
12410652
Cyanide, Reactive 1.009.600 12.50 76.8 50.9 125
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:361795MS 08/22/2023Cyanide, Reactive SW846-7.3
GW-1 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 08/22/2023 5242942308N45-001AMS
12410654
Cyanide, Reactive 0.95213.76 11.90 116 33.8 127
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:361795MSD 08/22/2023Cyanide, Reactive SW846-7.3
GW-1 Units:Prep Date:Sample ID:Client ID:Run No:mg/Kg 08/22/2023 5242942308N45-001AMSD
12410655
Cyanide, Reactive 0.95212.24 31.511.90 103 33.8 127 13.76 11.7
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit Page 6 of 7Page 22 of 23

End of Report
Page 7 of 7Page 23 of 23