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HomeMy WebLinkAboutMO-29916_49005_CA_IAR_20230914_280 Ervin Woods Waste Oil Tank 100 East Ruffin Street · Mebane, North Carolina 27302 Telephone (919) 563-9091 · Facsimile (919) 563-9095 www.terraquestpc.com INITIAL ABATEMENT ACTION REPORT WASTE OIL UST Details of the UST Removal and Contaminated Soil Excavation FORMER BCA PROPERTY MGMT., LLC 280 ERVIN WOODS DR. KANNAPOLIS, ROWAN COUNTY, NC Latitude: 35.50798o N Longitude: -80.66742o W Release Information Date Discovered: March 31, 2023 (Lab Confirmed) Estimated Release Quantity: Unknown Release Cause/Source: Waste Oil UST UST Capacity: (1) 6,600-gallon steel UST Facility ID: Not Registered NCDWM-UST Incident No.: 49005 Property Owner: UST System Owner: B&S Management, LLC BCA Property Mgmt., LLC 28015 Villa Walk Ln. 117 Harbour Dr. Fort Mill, SC 29707 Hubert, NC 28539 Terraquest Project No. 08423 September 14, 2023 Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 i Kannapolis, NC CERTIFICATION FOR THE SUBMITTAL OF AN ENVIRONMENTAL / GEOLOGICAL ASSESSMENT Attached is the Initial Abatement Action Report-Waste Oil UST for: Property Owner: B&S Management, LLC n Address: 28015 Villa Walk Ln. City: Fort Mill State: SC Zip Code: 29707 Site Name: Former BCA Property Mgmt., LLC Address: 280 Ervin Woods Dr. City: Kannapolis State: NC Zip Code: 27260 UST Owner: BCA Property Mgmt., LLC Address: 117 Harbour Dr. City: Hubert State: NC Zip Code: 28539 I, Jonathan R. Grubbs, a Licensed Geologist in the State of North Carolina for TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. do hereby certify that I am familiar with and have reviewed all material including figures within this report and that to the best of my knowledge the data, site assessment, figures, and other associated materials are correct and accurate. All work was performed under my direct supervision. My seal and signature are affixed below. Terraquest Environmental Consultants, P.C. is licensed to practice geology in North Carolina. The certification number of the corporation is C-291. TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. Jonathan R. Grubbs, P.G. Michael J. Brown Vice President President Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 ii Kannapolis, NC TABLE OF CONTENTS 1.0 INTRODUCTION ................................................................................................................... 1 2.0 SITE HISTORY ....................................................................................................................... 1 3.0 RELEASE INCIDENT DISCOVERY ........................................................................................... 2 4.0 UST REMOVAL AND SOIL EXCAVATION .............................................................................. 3 4.0 FIELD AND LABORATORY ANALYSES ................................................................................... 4 4.1 Soil Sampling Methodology and Results – UST Closure & Soil Excavation ..................... 4 4.2 Groundwater Sampling Methodology and Results – Soil Excavation ............................. 5 5.0 FREE PRODUCT .................................................................................................................... 6 6.0 POTENTIAL SOURCES OF PETROLEUM HYDROCARBONS ................................................... 6 7.0 NATURE AND ESTIMATED QUANTITY OF RELEASE ............................................................. 6 8.0 SITE AND VICINITY DESCRIPTION ........................................................................................ 6 9.0 CONCLUSIONS/RECOMENDATIONS .................................................................................... 7 10.0 LIMITATIONS ....................................................................................................................... 7 REFERENCES .................................................................................................................................... 9 TABLES: 1. Site History (UST System Information) 2. Summary of Soil Sampling Results: Phase II ESA 3. Summary of Soil Sampling Results: Waste Oil UST Closure Soil Excavation FIGURES: 1. Site Location Map 2. Site Layout Map 3. Limits of Excavation Soil Sample Location Map APPENDICES: A. Environmental Acronyms and Technical Methods/Standard Procedures B. Residual Liquid and Soil Waste Manifests C. Photographs D. Analytical Reports Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 1 Kannapolis, NC 1.0 INTRODUCTION On behalf of BCA Property Mgmt., LLC (BCA), the UST owner and former property owner, Terraquest Environmental Consultants, P.C. (Terraquest) has prepared this Initial Abatement Action Report for the former BCA property located at 280 Ervin Woods Dr. in Kannapolis in Rowan County, North Carolina (herein referred to as the subject property). The release incident is associated with a 6,600-gallon steel non-registered, commercial, regulated waste oil underground storage tank (UST) that was formerly located on the subject property south of the mobile office building. This report documents the UST removal and soil excavation activities conducted in July and August 2023. The location of the subject property is depicted in Figure 1. The site layout is depicted in Figure 2. Environmental acronyms used in this report are detailed in Appendix A along with Terraquest’s technical methods and standard procedures. 2.0 SITE HISTORY According to the Rowan County Tax Records, the garage structure on the subject property was built in 1988. The 6,600-gallon waste oil UST was installed during the construction of the garage building. A 280-gallon heating oil UST was also installed off the west side of the garage building and was removed during the removal of the waste oil UST. The product type, capacity, date installed, date closed, and release detection information for the USTs are listed in Table 1. The locations of the USTs are depicted in Figure 2. The subject property is located outside the city limits of Kannapolis, NC. Historically the subject property has been woods and a residence. Surrounding properties have historically been cultivated farmland and woods with a gradual development of residences and light industrial buildings to the north, east, and west and a sand rock pit to the south. A water supply well is Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 2 Kannapolis, NC connected to the subject property’s buildings. Each building has its own septic system that are located on the adjacent properties to the east and west. 3.0 RELEASE INCIDENT DISCOVERY On March 30, 2023, Terraquest personnel located the UST basin based upon the presence of the fill port of the south side of the mobile office building. Terraquest advanced three soil borings, SB3, SB4, and SB5, along the south and east sides of the UST. The SB3 and SB5 borings were advanced to a depth of 10 feet below ground level (BGL) where refusal was encountered. The SB4 boring was advanced to a depth of 4 feet BGL where refusal was encountered. In the SB3 and SB5 soil borings, soils from the sample intervals (3-5, 5-7, and 8-10 feet BGL) were placed in sealable plastic bags and screened for volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs) utilizing a Photoionization Detector (PID). No soil sample was submitted from the SB4 soil boring given its shallow depth. The soil lithology encountered during the soil borings was a yellowish-orange, med. stiff Lean Clay (CL) from 0.5 feet to 10 feet BGL. The soil samples collected for analysis were placed in the proper laboratory-prepared sampling containers, labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples were immediately placed on ice and analyzed before the expiration of an analytical method’s prescribed holding time. The soil samples were analyzed for total petroleum hydrocarbons (TPH) for low boiling point petroleum hydrocarbons (GRO) and medium to high boiling point petroleum hydrocarbons (DRO) by UVF Trilogy technology. The North Carolina Department of Environmental Quality Division of Waste Management – UST Section (NCDEQ DWM-UST) Action Limits of 100 milligrams per kilogram (mg/kg) for TPH DRO and 50 mg/kg for TPH GRO were exceeded in the SB3 (8-10). The attached Table 2 summarizes the sample depth and detected concentrations of the SB3 and SB5 soil samples. The locations of the SB3, SB4, and SB5 soil borings are depicted in the attached Figure 3. Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 3 Kannapolis, NC The release incident was reported to the NCDEQ on May 9, 2023. 4.0 UST REMOVAL AND SOIL EXCAVATION On July 31, 2023, Terraquest supervised the removal of approximately 1,050 gallons of water and waste oil by Clean Green of Durham, NC. The 6,660-gallon waste oil tank was buried approximately 7 feet below ground level (BGL) and was excavated and taken offsite for environmentally-sound disposal at Foil’s, Inc. metal recycling in Concord, NC. An additional 388 gallons of residual liquid were removed on August 1, 2023 once the UST was removed. The dimensions of the UST were 90 inches wide by 240 inches long. Following the UST removal, Terraquest inspected the UST and noted no holes in the USTs. The tank’s former location is shown in Figure 2. Copies of the liquid waste manifests are included in Appendix B. Three confirmation soil samples were collected immediately beneath the UST from a depth of 17 feet BGL at evenly spaced intervals, W.O. CS1(17), W.O. CS2(17), and W.O. CS3(17) on July 31, 2023. Excavation of Contaminated Soil On July 31 and August 1, 2023, Terraquest supervised the excavation of impacted soils from above and surrounding the middle and eastern end of the waste oil UST based upon the SB3 soil sample results. The soil excavation continued until the odor and/or staining dissipated. Soils in the sidewalls and base of the excavation were screened with a PID. Terraquest personnel identified the soil lithologies in the UST basin to be a sandy lean clay from the ground surface to approximately 8 to 10 feet BGL, a sandy silt from 8-10 feet BGL to 12 feet BGL, and a silty sand from 12 to 17 feet BGL. The final limits of the excavation measured 12 feet at the widest section, 27 feet at the longest section, and 17 feet in depth. Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 4 Kannapolis, NC A total of 18.12 tons of contaminated soil were excavated from around the waste oil UST and hauled offsite for disposal at the Environmental Soils, Inc. soil disposal facility in Lattimore, NC. A copy of the soil disposal waste manifest is included in Appendix B. Confirmation soil samples were collected at the final limits of the soil excavation in the eastern portion of the UST to determine in-situ soil quality along the sidewalls {W.O. SW1(12), W.O. SW2(12), and W.O. SW3(12)}. No base of the excavation soil samples were collected given the absence of contaminant concentrations above the regulatory limits in the confirmation soil samples collected beneath the UST {W.O. CS1(17), W.O. CS2(17), and W.O. CS3(17)}. The excavation was backfilled with clean fill dirt from a nearby soil pit. Table 3 lists the sample depths and analytical results of the final limit of excavation soil samples. The locations of the closure and limit of excavation soil samples are depicted in Figure 3. The methods and standard procedures followed during the soil sampling are detailed in Section 4.0. Pictures of the soil excavation are included in Appendix C. 4.0 FIELD AND LABORATORY ANALYSES 4.1 Soil Sampling Methodology and Results – UST Closure & Soil Excavation Three confirmation soil samples were collected immediately beneath the UST from a depth of 17 feet BGL at evenly spaced intervals, W.O. CS1(17), W.O. CS2(17), and W.O. CS3(17), using a track excavator bucket on July 31, 2023. The soil samples collected for analysis were placed in the proper laboratory-prepared sampling containers, labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples were immediately placed on ice and analyzed before the expiration of an analytical method’s prescribed holding time. The soil samples were analyzed for TPH for GRO and DRO by UVF Trilogy technology, EPA Methods for Polyaromatic Hydrocarbons (PAHs), and Total Metals for Chromium and Lead. Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 5 Kannapolis, NC The analytical results revealed no contaminant concentrations above the NCDEQ DWM-UST Action Limits for the TPH analysis or the Soil-to-Groundwater Maximum Soil Contaminant Concentrations (S-t-G MSCCs) for the PAH and metal analyses. After the soil excavation was completed on July 31 and August 1, 2023, soil samples were collected at the limits of the final excavation {W.O. SW1(12), W.O. SW2(12), and W.O. SW3(12)} on August 1, 2023. All of the UST confirmation soil samples were collected following the proper soil sampling protocol in accordance with the NCDEQ DWM-UST guidelines. The final limits of the soil excavation soil samples were collected using a track excavator bucket. A grab sample from each sample location was collected, placed in the appropriate laboratory-prepared containers, and labeled with the sample identification, sample analytical method, and sample time. Since the 6,600-gallon UST formerly contained waste oil, the final sidewall of the excavation samples were analyzed by EPA Methods 8270 Base Neutrals and Acid Extractables (BNA) and Massachusetts Department of Environmental Protection (MADEP) Extractable Petroleum Hydrocarbons (EPH) targeting semi-volatile organics and EPA 8260 + methyl tert-butyl ether (MTBE) + di-isopropyl ether (IPE) and MADEP Volatile Petroleum Hydrocarbons (VPH) targeting volatile organics. Chain-of-custody documentation was maintained for the soil samples. The analytical results of the W.O. SW1(12), W.O. SW2(12), and W.O. SW3(12) soil sample revealed no concentrations greater than the S-t-G MSCCs. The analytical results of the confirmation and limit of the excavation soil samples are detailed in Table 3. Figure 3 depicts the locations of the CS and SW soil samples. The analytical reports for the W.O. CS and W.O. SW are contained in Appendix D. 4.2 Groundwater Sampling Methodology and Results – Soil Excavation Groundwater was not encountered during either soil excavation. Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 6 Kannapolis, NC 5.0 FREE PRODUCT No free product in the form of waste oil was observed in the bottom of the initial or final excavations. 6.0 POTENTIAL SOURCES OF PETROLEUM HYDROCARBONS The primary source of petroleum hydrocarbons in the site vicinity is the former 6,600-gallon waste oil UST. As previously mentioned, a 280-gallon heating oil UST was located along the western side of the garage building. A release incident was also discovered during its removal. Approximately 74.35 tons of contaminated soil were removed from beneath the heating oil UST. Given the distance between the two USTs and the removal of the contaminated soil surrounding the waste oil UST, the two contaminant plumes have not comingled. 7.0 NATURE AND ESTIMATED QUANTITY OF RELEASE The nature of the release is waste oil from the former UST. The amount of the release is currently unknown. 8.0 SITE AND VICINITY DESCRIPTION Land use in the immediate vicinity of the subject property is commercial with the subject property being a landscaping company office and maintenance yard. The subject and surrounding properties derive their drinking water from water supply wells. The garage and mobile office building’s water supply well is located 245 feet to the northeast. The adjacent property to the west at 272 Ervin Woods Dr. has a water supply well that is located 183 feet to the west. The locations of the water supply wells are depicted in Figure 2. Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 7 Kannapolis, NC According to the Geologic Map of North Carolina (Brown, et al, 1985), the site is located in the Charlotte Belt of the Piedmont Physiographic Region of North Carolina and is underlain by megacrystic to equigranular granitic rocks. The nearest surface water body is a pond located approximately 450 feet to the east. 9.0 CONCLUSIONS/RECOMENDATIONS Terraquest personnel supervised the excavation of contaminated soil surrounding the former waste oil UST located off the south side of the mobile office building. From assessment and remedial activities to date, the following conclusions/recommendations can be drawn. • The 6,600-gallon steel waste oil UST was removed on July 31, 2023. • The analytical results of soil samples collected from native soils beneath the former waste oil UST location during a Phase II ESA confirms a release from the UST. • 18.12 tons of waste oil-contaminated soil were excavated surrounding the 6,600-gallon waste oil UST and were hauled offsite for disposal at the Environmental Soils soil disposal facility in Lattimore, NC. • Groundwater was not encountered in the soil excavation. • Confirmation soil samples were collected from beneath the UST and sidewalls of the soil excavation. Analytical results of the collected soil samples revealed no waste oil-type contaminant concentrations exceeding the NCDEQ DWM-UST Action Limits or S-t-G MSCCs. • With the removal of the contaminated soil with concentrations above the NCDEQ DWM- UST Action Limits and S-t-G MSCCs, the release incident is eligible for closure and the issuance of a no further action letter. 10.0 LIMITATIONS This report is limited to the investigation of petroleum hydrocarbons in soil and does not imply that other unforeseen adverse impacts to the environment are not present at or around the Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 8 Kannapolis, NC Former BCA Property Mgmt., LLC property. In addition, subsurface heterogeneities not identified during the current study may influence the migration of groundwater or contaminants in unpredicted ways. The limited amount of sampling and testing conducted during this study cannot practically reveal all subsurface heterogeneities. Furthermore, the subsurface conditions, particularly groundwater flow elevations, and water quality may vary over time. The opinions and conclusions determined in this report are in accordance with industry-accepted geologic and hydrogeologic practices at this time and location. No warranty is implied or intended. Initial Abatement Action Report – Waste Oil UST Former BCA Property Mgmt., LLC Terraquest Environmental Consultants, P.C. 280 Ervin Woods Dr. Prepared on: September 14, 2023 9 Kannapolis, NC REFERENCES Brown, et al., 1985, Geologic Map of North Carolina, North Carolina Department of Natural Resources and Community Development, 1:500,000 scale. North Carolina Administrative Code, Title 15A, Chapter 2, Subchapter 2N, Section .0700, January 1, 1991, "Criteria and Standards Applicable to Underground Storage Tanks". North Carolina Department of Environmental Quality, Division of Waste Management UST Section, UST Section Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement – STIRA, May 17, 2021. USGS 7.5-Minute Quadrangle Topographic Maps, Kannapolis and Enochville, 2022. TABLES Table 1 Date: 8/29/23 Facility ID No: N/A Capacity UST Product (Gallons)Dimensions Release Discovered T1 Waste Oil 6,600 90" x 20'1988 7/31/23 Yes T2 Heating Oil 280 36' X 96"1988 7/31/23 Yes Notes: 1. T = UST 2. UST was of single walled steel construction. SITE HISTORY (UST SYSTEM INFORMATION) Incident Name: 280 Ervin Woods Rd., Kannapolis, NC Incident No. 49005 Date Installed Date Closed Table 2 4/5/2023 UV F T R I L O G Y UV F T R I L O G Y Date Collected Sample Depth (feet BGL) 320 370 8.38 Bold SUMMARY OF SOIL SAMPLING RESULTS: PHASE II ESA Incident Name: 280 Ervin Woods Rd., Kannapolis, NC Incident No. 49005 Analytical Method Sample ID TP H D R O TP H G R O Table 3 Date: 8/29/23 35 5 0 / D R O 50 3 0 / G R O 82 6 0 B 82 6 0 B 82 6 0 B 82 6 0 B 82 6 0 B 82 6 0 B 82 7 0 C 82 7 0 C 82 7 0 C 82 7 0 C 82 7 0 C 82 7 0 C 82 7 0 C 82 7 0 C MA D E P V P H MA D E P V P H / E P H MA D E P E P H MA D E P V P H / E P H Sample ID Date Collected Sample Depth (feet) 0.86 2.22 0.00171 J 0.00198 J 0.00175 J 12.8 18 0.76 1.96 0.0014 0.00178 0.0015 10.4 16.3 0.64 3.74 0.00132 0.00203 0.00133 11.8 19.5 --0.00156 0.0466 13.3 20.1 --0.0024 0.00198 0.0449 0.0907 9.38 18.5 --<0.000664 0.00193 <0.000604 <0.00188 0.0719 <0.0733 <0.0402 <0.0572 <0.120 <0.0402 <0.0803 <0.0402 8.56 16.2 <3.33 <1.95 - -0.0056 4.3 4.9 4.6 24 16 0.35 0.096 1.2 290 NE 56 4,200 270 68 540 ##31 - -18 1,200 1,560 3,129 14,000 7000 0.88 0.088 0.88 620 NE 469 23,460 400 939 1,500 31,000 469 - -164 32,000 40,000 81,760 360,000 200,000 8 0.78 8 16,400 NE 12,264 613,200 400 #40,000 810,000 12,264 100 50 Bold Italics C9 - C 1 8 A l i p h a t i c s C5 - C 8 A l i p h a t i c s C9 - C 2 2 A r o m a t i c s Soil-to-groundwater MSCCs (mg/kg) Residential MSCCs (mg/kg) TP H l o w f r a c t i o n TP H h i g h f r a c t i o n Be n z e n e To l u e n e Et h y l b e n z e n e Industrial/Commercial MSCCs (mg/kg) TPH Action Limit Violation Be n z o [ a ] a n t h r a c e n e Be n z o [ a ] p y r e n e Be n z o [ b ] f l u o r a n t h e n e C1 9 - C 3 6 A l i p h a t i c s Ph e n a n t h r e n e Ch r o m i u m Le a d To t a l X y l e n e s Ac e t o n e Et h a n o l Fl u o r a n t h e n e In d e n o [ 1 , 2 , 3 - c d ] p y r e n e Contaminant of Concern Analytical Method SUMMARY OF SOIL SAMPLING RESULTS: WASTE OIL UST CLOSURE SOIL EXCAVATION Incident Name: 280 Ervin Woods Rd., Kannapolis, NC Incident No. 49005 Facility ID No. NA FIGURES ONSULTANTS, P.C.CENVIRONMENTAL EN V I R O N M E N T A L C O N S U L T A N T S , P . C . EN V I R O N M E N T A L C O N S U L T A N T S , P . C . APPENDIX A MB’s\\MICHAEL-PC\Project Files\Templates\ENVIRONMENTAL ACRONYMS.doc ENVIRONMENTAL ACRONYMS 2L Standard Groundwater Standards under Title 15A NCAC 2L 0.0202(g) 2B Standard Surface Water Standards under Title 15A NCAC 2B AFVR Aggressive Fluid-Vapor Recovery AST Aboveground Storage Tank BGL Below Ground Level BNA Base Neutral and Acid Extractables C&D Construction and Demolition CAP Corrective Action Plan CSA Comprehensive Site Assessment EPA Environmental Protection Agency EPH Extractable Petroleum Hydrocarbons ESA Environmental Site Assessment GCL Gross Contamination Level LEL Lower Explosive Limit LSA Limited Site Assessment IPE di-Isopropyl Ether MADEP Massachusetts Department of Environmental Protection mg/kg Milligrams per kilogram MMPE Mobile Multi Phase Extraction MSCC Maximum Soil Contaminant Concentration MSW Municipal Solid Waste MTBE Methyl tertiary-Butyl Ether NC North Carolina NCAC NC Administrative Code NCDENR NC Department of Environment and Natural Resources NCDOT NC Department of Transportation NCDWM-SW NC Division of Waste Management’s Solid Waste Section NCDWM-UST NC Division of Waste Management’s UST Section NCDWQ NC Division of Water Quality NORR Notice of Regulatory Requirements NORP Notice of Residual Petroleum NOV Notice of Violation NPDES National Pollutant Discharge Elimination System OVM Organic Vapor Meter PID Photo Ionization Detector PLC Programmable Logic Controller POE Point of Entry (water treatment system) POTW Publicly Owned Treatment Works RBCA Risk Based Corrective Action SVE Soil Vapor Extraction stg Soil to Groundwater (MSCC) TA Task Authorization TCC Target Cleanup Concentrations Terraquest Terraquest Environmental Consultants, P.C. TPH Total Petroleum Hydrocarbon UST Underground Storage Tank VOA Volatile Organic Analysis VOC Volatile Organic Compound VPH Volatile Petroleum Hydrocarbons MNA Monitored Natural Attenuation TECHNICAL METHODS/STANDARD PROCEDURES Equipment Decontamination All soil sampling equipment utilized during site assessment activities is decontaminated according to standard and accepted protocol. Cleaning solutions range from clean potable water to acidic solutions or organic solvents depending on the contaminants present at the site. Equipment utilized at sites, such as hand augers, contaminated with petroleum hydrocarbons, is generally decontaminated with a low-sudsing detergent such as Luiquinox® and triple rinsed with distilled water. Larger equipment, such as drill rigs and associated tools, is steam cleaned. All decontamination procedures are completed within an established decontamination area which is located away from the active study area. Frequency of equipment decontamination depends on the nature of work being performed, but in no case is decontamination performed less frequently than once per test (i.e., soil boring, well installation, sample collection, etc.). Equipment blanks are collected as a quality control measure when required by job specifications. Soil Boring Installation Soil borings are completed using hand-operated sampling tools, truck-mounted drills, or Geoprobe® drilling rigs depending on the depth of sample collection and other site-specific conditions. Hand operated stainless-steel bucket augers are utilized to collect soil samples at regular intervals to determine site stratigraphy and to test for the presence of volatile organic compounds. Samples retrieved from the hand auger are necessarily disturbed during the augering process, but can provide accurate information on soil type and contaminant concentrations when properly interpreted. Soil samples from hand augered borings are generally retrieved at one to two foot intervals. Truck-mounted or Geoprobe® drilling equipment is often utilized when sample retrieval depths exceed twenty feet or subsurface conditions prevent utilization of hand augers (i.e., buried rocks, wood, bricks or other materials occur in the subsurface). Truck-mounted drilling rigs usually retrieve soil via a hollow-stem auger/split spoon collection method. Geoprobe® rigs usually employ a Macro-Core® tube retrieval system. Hollow stem augers provide relatively undisturbed 2-foot cores of soil samples. Soil samples are generally collected at five foot intervals utilizing standard penetration test procedures as defined by the American Society for Testing and Materials (ASTM) or are pushed to the desired depth using the head of the drill rig. The standard penetration test involves driving a 2" outside diameter by 1- 3/8" inside diameter split-spoon sampler a minimum distance of one foot with a 340-lb. slide hammer falling a distance of 30 inches. A Geoprobe® rig is a hydraulically-powered soil probing machine. The probe utilizes static force and percussion to advance a small diameter sampling device into the subsurface. The sampling apparatus provides relatively undisturbed 5-foot cores of soil samples. Soil samples are collected continuously. The Macro-Core® tube contains an inserted poly-vinyl chloride (PVC) liner which retains the soil sample as the tube is driven into the ground. The Macro-Core® tube is decontaminated between each 5-foot sample interval in a soil boring using a Liquinox and tap- water mixture. A new PVC liner is used to collect soil from each sample interval in a soil boring. Soil samples retrieved from the hollow-stem augers or Geoprobe are then carefully described according to the Unified Soil Classification System. Soil descriptions are recorded on a soil boring log. Soil Sampling Soils to be analyzed by a North Carolina-certified laboratory are prepared according to the specified analytical method. Initially, soil samples are removed from the ground using either a hand auger, backhoe bucket, spilt spoon auger, or a Macro-Core® sampling tube. During the removal, care is taken to keep the disturbance of the soil structure to a minimum to reduce the loss of contaminants. Once removed, the samples are placed in the proper sample container for the specified analytical method. For samples collected for the MADEP VPH and 8260 method, a TerraCore® sampler is used to collect three 5-gram allotments of soil. All three allotments are placed in methanol-preserved 40 mL vials. Also, two 5-gram allotments of soil are placed into sodium bisulfate-preserved 40 mL vials (5-gram each vial) for the 8260 low concentration method. A 250-mL glass jar of the sampled soil is also collected to provide moisture content information. Soils sampled for MADEP EPH, EPA Methods 8270 and TPH 5030 and 3550 are placed in a 250-mL glass jar. TPH 5030 samples are preserved in methanol similar to the 8260 analysis. Field personnel wear new, disposable latex gloves during the collection of each sample. The soil samples are labeled with the sample location, sample identification, date and time of collection, and the analytical method. The samples are placed on ice, sent to a laboratory, and analyzed before the expiration of an analytical method’s prescribed holding time. Chain-of-custody documentation is maintained for each sample collected in the field. If the soil is being sampled for volatile or semi-volatile compounds, a portion of the collected soil is placed in a sealable bag and screened for volatile organic vapors. Head screening procedures are described in the following paragraph. Headspace Screening Collected soil samples are routinely tested for the presence of volatile organic compounds (VOCs). After retrieval from the ground, a portion of a soil sample is placed in a sealable plastic bag. The soil samples are then set aside for approximately five minutes so that volatile constituents present in the sample can reach equilibrium concentrations with headspace gases in the bag. Once a suitable time period has passed, the probe of the sampling instrument, typically an Organic Vapor Monitor (OVM) or a Photo Ionization Detector (PID) meter, is inserted into the bag and the relative concentration of total VOCs is measured and permanently recorded in a field note book. VOC concentrations are measured using either a Thermo Electron Corp. Innova Series catalytic OVM or an Ion Science PhoCheck PID. Both the OVM and PID instrumentation are periodically calibrated according to the manufacturer’s recommended procedures. The OVM and PID are qualitative tools employed to detect and estimate the concentration of organic or hydrocarbon vapors. A thin probe is inserted through a small break in the seal of a bagged soil sample. For the OVM, an air sample from the headspace of the bag is drawn through the probe into an internal chamber where the vapors are catalyzed. The concentration of the VOCs is registered on a digital scale in parts per million (ppm). For the PID, an air sample from the headspace of the bag is drawn across the face of a lamp causing the sample to emit photons, the presence of which are converted into a VOC ppm reading that is displayed. Oxygen levels are field calibrated prior to each use. VOC calibration occurs periodically depending upon use by using a span gas of known concentration in a process recommended by the manufacturer. Well Installation/Construction Monitoring wells are installed using hand-operated sampling tools, a truck-mounted drill rig, or a Geoprobe drilling rig depending on the depth of well and other site-specific conditions. All monitoring wells are installed according to the requirements of 15A NCAC 2C-Well Construction Standards. Specifically, individual monitoring wells are constructed of 2-inch diameter, schedule 40 PVC casing riser and screen. The screen interval is generally 10 to 15 feet of machine slotted PVC with a slot size of 0.010". Only flush threaded joints are used. The annulus space around the screen is filled with washed filter pack No. 2 sand. The filter pack extends one to two feet above the top of the screen. A one to two foot-thick bentonite pellet seal is then placed above the filter pack. The remainder of the well annulus is completely filled with a Portland (Type I/II) cement grout mixture. A protective outer steel manhole, locking cap, and concrete pad is installed for each well. Type II Monitoring Well Construction Single-cased monitoring wells are generally used in delineation of groundwater quality within the surficial aquifer. The wells are constructed of 2-inch diameter, schedule 40 PVC casing and screen. The screen interval is generally 10 to 15 feet of machine slotted PVC with a slot size of 0.010". Only flush threaded joints are used. The annulus space around the screen is filled with washed filter pack No. 2 sand. The filter pack extends one to two feet above the top of the screen. A one foot- thick bentonite pellet seal is then placed above the filter pack. The remainder of the well annulus is completely filled with a Portland (Type I/II) cement grout mixture. A protective outer steel manhole, locking cap, and concrete pad are installed for each well. Type III Monitoring Well Construction Double-cased monitoring wells are used in the delineation of groundwater quality within a deeper portion of the surficial aquifer or an additional aquifer (e.g. aquitard, bedrock). A four to six-inch outer casing is installed through the surficial aquifer until a sufficient depth or until the deeper aquifer is encountered. The casing is secured with a Portland-grout collar that is tremmied into the annular spaced from the bottom of the bore hole to the surface. Once the grout has sufficiently cured, the bore hole is continued through the bottom of the outer casing to a depth approximately 15 - 20 feet beneath the outer casing. The inner casing is constructed of 2-inch diameter, schedule 40 PVC casing riser and screen. The screen interval is generally 5 to 10 feet of machine slotted PVC with a slot size of 0.010". Only flush threaded joints are used. The annulus space around the screen is filled with washed filter pack No. 2 sand. The filter pack extends one to two feet above the top of the screen. A one to two foot-thick bentonite pellet seal is then placed above the filter pack. The remainder of the well annulus is completely filled with the same Portland grout mixture used in the outer casing. A protective outer steel manhole, locking cap, and concrete pad are installed for each well. Well Development Following installation of each well, surging and pumping or bailing techniques will be used to remove fines from the screened interval. Groundwater is removed from each well until clear water is retrieved or a noticeable reduction in the amount of silt is achieved. Purged groundwater is disposed of in an environmentally safe manner. Other Methods of Groundwater Sampling Geoprobe Screen Point 15/16 Groundwater Samplers The Screen Point 15/16 Groundwater Samplers are used to collect groundwater samples from unconsolidated materials at depths ranging from near ground surface to over 100 feet below grade. The depth that can be reached with the SP15/16 samplers is a function of the equipment and methods being used to advance the sampler (manual, static vehicle weight, or percussion probing), the formation being penetrated, and operator experience. These protected screen samplers have only five parts, including the grout plug, plus a few O-rings. Using either of these tools with O-rings on the rod fittings enables you to collect representative groundwater samples from a discrete interval using a bailer, bladder pump, or tubing and stainless steel check valve. The length of the stainless steel screen exposed to the formation can be set from just a few inches to as much as 41-inches to let you select the sampling zone. The stainless steel screen is a v-wire screen and has a 1.0 in. OD. The screen bore is 0.65 in. The stainless steel screen is wire-wound with a 0.004-in slot width. Groundwater Sampling Petroleum Sites Groundwater samples are collected from temporary or permanent monitoring wells according to established sampling protocol. When multiple monitoring wells or sampling points are sampled, sampling is completed beginning with the least contaminated well to the most contaminated well, if it is known. When permanent monitoring wells for petroleum sites are sampled, the well is purged of a minimum of three well-bore volumes prior to sample collection in order to assure that sampled water is representative of aquifer conditions. In temporary wells, the first water which migrates into the open borehole is sampled. Samples from both temporary and permanent monitoring wells are collected using individually wrapped disposable polyethylene bailers by field personnel wearing disposable nitrile gloves. Only one well is sampled with a given bailer in order to prevent sample cross-contamination. During both well purging and sampling, proper protective clothing and equipment is used and is dependent upon the type and level of contaminants present. Also, field personnel change gloves between different samples to reduce the chance of cross- contamination. Water samples are transferred from the bailer to laboratory-prepared sampling containers using slow emptying devices to reduce the chance of contamination loss through volatilization. Preservatives, such as acids, are added to samples directly after they are collected if in-field preservation is necessary. The samples are labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples are placed on ice, sent to a certified laboratory, and analyzed before the expiration of an analytical method’s prescribed holding time. Chain-of-custody documentation is maintained for each sample collected in the field. Non-Petroleum Groundwater Sampling Protocols When required by state or federal regulations, low-flow groundwater sampling procedures are instituted. Groundwater samples collected in low-flow situations are collected using a peristaltic pump. A peristaltic pump is a type of positive displacement pump. The fluid is contained within a flexible tube fitted inside a circular pump casing. A rotor with a number of rollers attached to the external circumference compresses the flexible tube. As the rotor turns, the part of tube under compression closes thus forcing the fluid to be pumped to move through the tube. Groundwater parameters such as water level drawdown, pH, conductivity, dissolved oxygen (DO) and turbidity. Pumping rate, drawdown, and the time or volume required to obtain stabilization of parameter readings can be used as a future guide to purge the well. Measurements are collected at a pre- pumping established interval (typically five to ten minutes). Once all or a majority of the parameters have stabilized for three successive readings, stabilization has been achieved. In lieu of measuring all five parameters, a minimum subset would include pH, conductivity, and turbidity or DO. Three successive readings should be within ± 0.1 for pH, ± 3% for conductivity, and ± 10% for turbidity and DO. Upon parameter stabilization, sampling is initiated. Sampling flow rate is maintained at the estab- lished purge rate or is adjusted slightly to minimize aeration, bubble formation, turbulent filling of sample bottles, or loss of volatiles due to extended residence time in tubing. The same device used for purging is used to collect the groundwater sample. Generally, volatile parameters are sampled first. The sequence in which samples for inorganic parameters are collected is not determined unless filtered (dissolved) samples are collected. Preservatives, such as acids, are added to samples directly after they are collected if in-field preservation is necessary. The samples are labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples are placed on ice, sent to a certified laboratory, and analyzed before the expiration of an analytical method’s prescribed holding time. Chain-of-custody documentation is maintained for each sample collected in the field. During both well purging and sampling, proper protective clothing and equipment is used and is dependent upon the type and level of contaminants present. Also, field personnel change gloves between different monitoring wells or sampling points to reduce the chance of cross- contamination. When multiple monitoring wells or sampling points are sampled, sampling is completed beginning with the least contaminated well to the most contaminated well, if it is known. Stockpile Sampling The number of composite samples collected from a stockpile or a total quantity of excavated soil is based upon the cubic yardage. One composite sample is collected for every 100 cubic yards of contaminated soil excavated. The volume of a stockpile or total quantity of excavated soil is calculated by approximating the general geometry of a stockpile or estimating the capacity of the dump trucks used for hauling. If a stockpile is sampled, a grid pattern is laid out on the stockpile, dividing the stockpile into segments of approximately 200 cubic yards. Two soil borings are advanced within a grid and three soil samples are collected from each soil boring at various depths. The six soil samples are mixed into a composite sample by a trained TerraQuest technician. If truck loads are sampled, an aliquot sample is collected from the hauling trucks at a frequency based upon the capacity of the hauling trucks. Aliquots are gently mixed into a composite sample by a trained TerraQuest technician. Every effort is made to minimize the loss of contaminants through volatilization. The composited soil samples are jarred in the appropriate laboratory-prepared containers, labeled with the sample location, sample identification, date of collection, time of collection, the analytical method, and the preservative. The samples are placed on ice, sent to a laboratory, and analyzed before the expiration of an analytical method’s prescribed holding time. Chain-of-custody documentation is maintained for each sample collected in the field. Surface Water Sampling Surface water samples, specifically samples from creeks or streams, are collected from a moving/flowing portion of the creek or stream to ensure that stagnant water is not collected. Field personnel are careful to collect samples from flowing areas that are not so turbulent as to cause a loss of volatile contaminants which might have been contained in the creek’s/stream’s water. Samples are collected by field personnel wearing disposable latex gloves. Field personnel change gloves between different locations to reduce the chance of cross-contamination. Samples are collected directly from the appropriate creek or stream location and placed into the appropriate laboratory-prepared containers. Preservatives, such as acids, are added to samples directly after they are collected if preservation is necessary. The samples are labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples are cooled on ice to approximately four degrees centigrade, sent to a certified laboratory, and analyzed before the expiration of an analytical method’s prescribed holding time. Chain-of- custody documentation is maintained for each sample collected in the field. Water Supply Well Sampling Groundwater samples from water supply wells are collected from sampling points, typically spigots, located in the closest proximity to the water supply well pump house as possible. Prior to sample collection, the water is run for a sufficient amount of time to purge the bladder tank and assure that sampled water is representative of aquifer conditions. Once purged, the flow rate is reduced and samples are placed in the appropriate laboratory prepared containers and the appropriate acid preservatives are added if preservation of the sample is necessary. The samples are labeled with the project name, project number, sample identification, required analysis, and date and time of collection. The samples are placed on ice, sent to a laboratory, and analyzed before the expiration of an analytical method’s prescribed holding time. Chain-of-custody documentation is maintained for each sample collected in the field. Public Water Supply Line Sampling Groundwater samples from public water supply lines are collected from sampling points, typically spigots. To sample the spigot, the flow rate is reduced and samples are placed in the appropriate laboratory prepared containers. The samples are labeled with the sample location, sample identification, date of collection, time of collection, and required analytical method. The samples are placed on ice, sent to a laboratory, and analyzed before the expiration of an analytical method’s prescribed holding time. Chain-of-custody documentation is maintained for each sample collected in the field. Air Sampling Air samples are collected with the aide of a manually operated MityVac® pump manufactured by Pristech, Inc. The air sampling process begins by connecting a length of rubber hose from the MityVac® pump to the port to be sampled, or by hanging the hose inside of an emissions stack in such a manner as to ensure no outside air causes dilution. Another length of hose is fixed to the outlet port of the pump and is connected to a new Tedlar bag. Once the pump is hooked up, a valve on the Tedlar collection bag is opened and air is manually forced into the bag by the pumping action of sampling personnel. Field Measurements Field measurements taken to determine the pH, conductivity, temperature, and dissolved oxygen concentration of a particular groundwater sample are taken directly after a particular monitoring well has been adequately purged. This ensures that the groundwater parameter data collected is representative of the aquifer conditions at a given location. Once purging of the monitoring well is complete, the decontaminated probe head and cord of the appropriate unit is lowered into the required monitoring well. If the depth to water in a specific monitoring well is greater than the length of cord for a particular unit, a new, disposable bailer is slowly lowered into the appropriate monitoring well and a representative groundwater sample is retrieved. A slow pouring device is fitted onto the end of the disposable bailer and the sample is slowly poured into a new, disposable plastic cup. Groundwater parameter data are then collected from the groundwater in the cup using the required unit. For pH, conductivity, and temperature, a Hanna Instruments Model 991300 portable meter is utilized. This unit is periodically calibrated and maintained in accordance with the unit’s operations manual by field personnel. Prior to data collection, the unit is properly decontaminated to prevent cross-contamination. The unit is decontaminated between each sample. The procedure used for sample measurement involves lowering the meter’s probe into the new, disposable cup containing the groundwater sample to be measured and slowly stirring the probe to force groundwater across the probe’s membrane. The measurements displayed by the meter are then recorded. For dissolved oxygen concentration measurements, a YSI® Model 55 Handheld Dissolved Oxygen System is utilized. This unit is periodically calibrated and maintained in accordance with the unit’s operations manual by field personnel. Prior to data collection, the unit is properly decontaminated to prevent cross-contamination. The unit is decontaminated between each sample. The procedure used for sample measurement involves adjusting the unit for the correct altitude where the sampling will take place and adjusting the reported units desired. Once this is done, the unit’s probe is inserted into the groundwater sample to be measured and the probe is slowly stirred to force the groundwater across the probe’s membrane. The measurements displayed by the unit are then recorded. For turbidity measurements, a Hach 2100P Portable Turbidity meter or equal equivalent is utilized. The unit is calibrated prior to use in accordance with the unit’s operations manual by field personnel. Groundwater samples are collected in glass containers for measurement by the instrument. The glass containers are washed with bottled-water between each measurement collection. Once the sample is collected and inserted into the instrument, the measurements displayed by the instrument are then recorded. APPENDIX B APPENDIX C 280 Ervin Woods Dr., Kannapolis, NC Picture 1: Excavated Waste Oil UST Picture 2: Limits of waste oil UST soil excavation Picture 3: Backfilled waste oil UST soil excavation APPENDIX D UVF TRILOGY ANALYTICAL REPORT Project Name: 280 Ervin Wood Dr Kannapolis Project Number: 08423 Date: 8/1/23 Standard Technical Procedures The UVF TRILOGY instrument is a fixed-wavelength fluorometer but uses deep UV LEDS to detect monoaromatic and polyaromatic hydrocarbons. SITELAB’s CAL-025 GRO Module is used to detect volatile petroleum hydrocarbons in the C6 to C10 range. This test matches well to EPA Methods for GRO, BTEX, BPH or VOC’s using GC/FID instrumentation. SITELAB’s CAL-042 EDRO Module is used to detect petroleum hydrocarbons in the C10 to C36 diesel and oil range. This test matches well to EPA methods for TPH, EPH, DRO, and others using GC-FID instrumentation. Prior to field usage, the UVF TRILOGY is calibrated with five calibration standard solutions per targeted analyte. Soil samples are weighed to the nearest gram (i.e. 5.0 g) and added to a 1-ounce HDPE Nalgene bottle with a measured amount of laboratory grade methanol to the nearest mL (i.e. 10 mL) to create a sample extract. After addition of both the soil and methanol, the bottle is agitated for several minutes. Next, the sample rests for several minutes allowing for the soil and methanol extract to separate. After ample resting time, the methanol extract is collected with a syringe. A filter is connected to the end of the syringe and dispensed into a clean sample test tube. The test tube is labeled with sample ID and extract dilution factor (i.e. 2X). Known amounts of extract are pipetted into a second test tube and diluted with methanol. The sample ID and dilution factor are labeled on the test tube (i.e. 100X). Samples are placed into a clean cuvette and carefully inserted into the selected UV Module. Prior to analyzing the sample, the stored calibration that matches the UV Module being used, is selected. The UVF TRILOGY produces a result that when multiplied to the dilution factor equals the true TPH value. Quenching occurs when the detector is swamped by too many or certain type of hydrocarbons, producing low or negative concentrations. The sample is tested at multiple dilutions to confirm the results are linear and accurate. Solvent blank samples are periodically analyzed to confirm the solvent is clean and the calibration of the machine is maintained. UVF Analytical Report Project Name 280 Ervin Wood Dr Kannapolis Project Number 08423 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units H.O. BE1 15'15' 7/31/2023 DRO 100 589 10 mg/kg H.O. BE1 15'15' 7/31/2023 GRO 100 884 50 mg/kg Wednesday, August 9, 2023 Page 1 of 9 Project Name 280 Ervin Wood Dr Kannapolis Project Number 08423 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units CS1 17'17' 7/31/2023 DRO 2 0.86 0.2 mg/kg CS1 17'17' 7/31/2023 GRO 2 2.22 1 mg/kg Wednesday, August 9, 2023 Page 2 of 9 Project Name 280 Ervin Wood Dr Kannapolis Project Number 08423 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units CS2 17'17' 7/31/2023 DRO 2 0.76 0.2 mg/kg CS2 17'17' 7/31/2023 GRO 2 1.96 1 mg/kg Wednesday, August 9, 2023 Page 3 of 9 Project Name 280 Ervin Wood Dr Kannapolis Project Number 08423 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units CS3 17'17' 7/31/2023 DRO 2 0.64 0.02 mg/kg CS3 17'17' 7/31/2023 GRO 2 3.74 1 mg/kg Wednesday, August 9, 2023 Page 4 of 9 Project Name 280 Ervin Wood Dr Kannapolis Project Number 08423 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units H.O.SW1 7-8'7-8' 7/31/2023 DRO 2 0.74 0.2 mg/kg H.O.SW1 7-8'7-8' 7/31/2023 GRO 2 2.64 1 mg/kg Wednesday, August 9, 2023 Page 5 of 9 Project Name 280 Ervin Wood Dr Kannapolis Project Number 08423 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units H.O.SW2 7-8'7-8' 7/31/2023 DRO 2 0.64 0.2 mg/kg H.O.SW2 7-8'7-8' 7/31/2023 GRO 2 3.8 1 mg/kg Wednesday, August 9, 2023 Page 6 of 9 Project Name 280 Ervin Wood Dr Kannapolis Project Number 08423 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units H.O.SW3 7-8'7-8' 7/31/2023 DRO 2 0.38 0.2 mg/kg H.O.SW3 7-8'7-8' 7/31/2023 GRO 2 3.5 1 mg/kg Wednesday, August 9, 2023 Page 7 of 9 Project Name 280 Ervin Wood Dr Kannapolis Project Number 08423 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units H.O.SW4 7-8'7-8' 7/31/2023 DRO 2 0.96 0.2 mg/kg H.O.SW4 7-8'7-8' 7/31/2023 GRO 2 3.38 1 mg/kg Wednesday, August 9, 2023 Page 8 of 9 Project Name 280 Ervin Wood Dr Kannapolis Project Number 08423 Method UVF Trilogy Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units H.O. BE1 (17)17' 8/1/2023 GRO 100 1,138 50 mg/kg H.O. BE1 (17)7' 8/1/2023 DRO 100 946 10 mg/kg Wednesday, August 9, 2023 Page 9 of 9 ANALYTICAL REPORT PREPARED FOR Attn: Jonathan Grubs Terraquest Environmental Consultants, PC 100 E. Ruffin Street Mebane, North Carolina 27302 Generated 8/29/2023 4:37:46 PM Revision 1 JOB DESCRIPTION 280 Ervin Woods Dr., Kannapolis, NC JOB NUMBER 400-241823-1 See page two for job notes and contact information. Pensacola FL 32514 3355 McLemore Drive Eurofins Pensacola Page 1 of 67 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Eurofins Pensacola Eurofins Pensacola is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 8/29/2023 4:37:46 PM Revision 1 Authorized for release by Chad Bechtold, Project Manager Chad.Bechtold@et.eurofinsus.com (813)690-3563 Page 2 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Table of Contents Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Laboratory Job ID: 400-241823-1 Page 3 of 67 Eurofins Pensacola8/29/2023 (Rev. 1) Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .56 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .64 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Job ID: 400-241823-1 Laboratory: Eurofins Pensacola Narrative Job Narrative 400-241823-1 Report Revision Per the client the sample listed as W.O. BE1 (17) on the Chain-of-Custody was changed to H.O. BE2 (17). Receipt The samples were received on 8/10/2023 9:49 AM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 1.1°C GC/MS VOA Method 8260D: The following sample was diluted due to the nature of the sample matrix: W.O. BE1 (17) (400-241823-7). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. GC/MS Semi VOA Method 8270E: The following sample was diluted due to the nature of the sample matrix: H.O. BE1 (17) (400-241823-8). Elevated reporting limits (RLs) are provided. Method 8270E: Six surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance criteria without performing re-extraction/re-analysis. The following sample contained an allowable number of surrogate compounds outside limits: H.O. BE1 (17) (400-241823-8). These results have been reported and qualified. Method 8270E_SIM: The method blank for preparation batch 400-636852 and analytical batch 400-637317 contained Indeno[1,2,3-cd]pyrene, 2-Methylnaphthalene, Phenanthrene, Benzo[b]fluoranthene and Benzo[a]pyrene above the method detection limit. These target analyte concentrations in the method blank were less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed. Method 8270E_SIM: Three surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance criteria without performing re-extraction/re-analysis. The following samples contained an allowable number of surrogate compounds outside limits: W.O. CS1 (17) (400-241823-1), (LCS 400-636852/18-A) and (MB 400-636852/1-A). These results have been reported and qualified. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons Method MAVPH: The following samples were diluted because the base dilution for VPH soil analysis is 1:50: W.O. SW1 (12) (400-241823-4), W.O. SW2 (12) (400-241823-5), W.O. SW3 (12) (400-241823-6) and H.O. BE1 (17) (400-241823-8). Method MAVPH: The following sample was diluted to bring the concentration of target analytes within the calibration range: W.O. BE1 (17) (400-241823-7). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Hydrocarbons Method MAEPH: Surrogate recovery for the following sample was outside control limits: H.O. BE1 (17) (400-241823-8). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed. Method MAEPH: The following sample was diluted to bring the concentration of target analytes within the calibration range: H.O. BE1 (17) (400-241823-8). Elevated reporting limits (RLs) are provided. Method MAEPH: Surrogate recovery for the following sample was outside control limits: H.O. BE1 (17) (400-241823-8). Evidence of matrix Eurofins PensacolaPage 4 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Job ID: 400-241823-1 (Continued) Laboratory: Eurofins Pensacola (Continued) interference is present; therefore, re-extraction and/or re-analysis was not performed. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Metals No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. General Chemistry No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins PensacolaPage 5 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: W.O. CS1 (17)Lab Sample ID: 400-241823-1 ☼Benzo[a]anthracene RL 0.00771 mg/Kg MDL 0.00117 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1J0.00171 8270E SIM ☼Benzo[a]pyrene 0.00771 mg/Kg0.00117 Total/NA10.00198 J B 8270E SIM ☼Benzo[b]fluoranthene 0.00771 mg/Kg0.00117 Total/NA10.00175 J B 8270E SIM ☼Indeno[1,2,3-cd]pyrene 0.00771 mg/Kg0.00234 Total/NA10.00299 J B 8270E SIM ☼Phenanthrene 0.00771 mg/Kg0.00117 Total/NA10.00134 J B 8270E SIM ☼Chromium 1.13 mg/Kg0.349 Total/NA112.8 6010D ☼Lead 1.13 mg/Kg0.248 Total/NA118.0 6010D Client Sample ID: W.O. CS2 (17)Lab Sample ID: 400-241823-2 ☼Benzo[a]anthracene RL 0.00760 mg/Kg MDL 0.00115 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1J0.00140 8270E SIM ☼Benzo[a]pyrene 0.00760 mg/Kg0.00115 Total/NA10.00178 J B 8270E SIM ☼Benzo[b]fluoranthene 0.00760 mg/Kg0.00115 Total/NA10.00150 J B 8270E SIM ☼Fluoranthene 0.00760 mg/Kg0.00115 Total/NA10.00261 J 8270E SIM ☼Indeno[1,2,3-cd]pyrene 0.00760 mg/Kg0.00230 Total/NA10.00298 J B 8270E SIM ☼Phenanthrene 0.00760 mg/Kg0.00115 Total/NA10.00140 J B 8270E SIM ☼Chromium 1.06 mg/Kg0.327 Total/NA110.4 6010D ☼Lead 1.06 mg/Kg0.232 Total/NA116.3 6010D Client Sample ID: W.O. CS3 (17)Lab Sample ID: 400-241823-3 ☼Benzo[a]anthracene RL 0.00806 mg/Kg MDL 0.00122 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1J0.00132 8270E SIM ☼Benzo[a]pyrene 0.00806 mg/Kg0.00122 Total/NA10.00203 J B 8270E SIM ☼Benzo[b]fluoranthene 0.00806 mg/Kg0.00122 Total/NA10.00133 J B 8270E SIM ☼Indeno[1,2,3-cd]pyrene 0.00806 mg/Kg0.00244 Total/NA10.00292 J B 8270E SIM ☼Phenanthrene 0.00806 mg/Kg0.00122 Total/NA10.00153 J B 8270E SIM ☼Chromium 1.12 mg/Kg0.347 Total/NA111.8 6010D ☼Lead 1.12 mg/Kg0.246 Total/NA119.5 6010D Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 ☼Acetone RL 0.0238 mg/Kg MDL 0.0114 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA10.0466 8260D ☼Toluene 0.00476 mg/Kg0.000951 Total/NA10.00156 J 8260D ☼Chromium 1.20 mg/Kg0.372 Total/NA113.3 6010D ☼Lead 1.20 mg/Kg0.264 Total/NA120.1 6010D Client Sample ID: W.O. SW2 (12)Lab Sample ID: 400-241823-5 ☼Acetone RL 0.0253 mg/Kg MDL 0.0122 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA10.0449 8260D ☼Ethanol 0.101 mg/Kg0.0750 Total/NA10.0907 J 8260D ☼Toluene 0.00507 mg/Kg0.00101 Total/NA10.00240 J 8260D ☼Xylenes, Total 0.0101 mg/Kg0.00193 Total/NA10.00198 J 8260D ☼Chromium 1.17 mg/Kg0.364 Total/NA19.38 6010D ☼Lead 1.17 mg/Kg0.258 Total/NA118.5 6010D Client Sample ID: W.O. SW3 (12)Lab Sample ID: 400-241823-6 ☼Acetone RL 0.0248 mg/Kg MDL 0.0119 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA10.0719 8260D Eurofins Pensacola This Detection Summary does not include radiochemical test results. Page 6 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: W.O. SW3 (12) (Continued)Lab Sample ID: 400-241823-6 ☼Toluene RL 0.00495 mg/Kg MDL 0.000991 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1J0.00193 8260D ☼Chromium 1.14 mg/Kg0.353 Total/NA18.56 6010D ☼Lead 1.14 mg/Kg0.250 Total/NA116.2 6010D Client Sample ID: H.O. BE2 (17)Lab Sample ID: 400-241823-7 ☼1,3,5-Trimethylbenzene RL 0.279 mg/Kg MDL 0.0463 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA50J0.0787 8260D ☼C9-C12 Aliphatics 62.5 mg/Kg62.5 Total/NA200086.0 MAVPH ☼C9-C10 Aromatics 33.5 mg/Kg33.5 Total/NA2000277MAVPH ☼Chromium 1.15 mg/Kg0.356 Total/NA17.50 6010D ☼Lead 1.15 mg/Kg0.252 Total/NA115.5 6010D Client Sample ID: H.O. BE1 (17)Lab Sample ID: 400-241823-8 ☼Acetone RL 0.0228 mg/Kg MDL 0.0109 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA10.0320 8260D ☼Ethanol 0.0910 mg/Kg0.0673 Total/NA10.0860 J 8260D ☼Toluene 0.00455 mg/Kg0.000910 Total/NA10.00188 J 8260D ☼Fluoranthene 1.86 mg/Kg0.186 Total/NA50.198 J 8270E ☼N-Nitrosodiphenylamine 1.86 mg/Kg0.186 Total/NA52.68 8270E ☼Pyrene 1.86 mg/Kg0.439 Total/NA51.14 J 8270E ☼C9-C18 Aliphatics 36.8 mg/Kg36.8 Total/NA203450MA-EPH ☼C19-C36 Aliphatics 36.8 mg/Kg36.8 Total/NA201610MA-EPH ☼C11-C22 Aromatics 3.45 mg/Kg3.45 Total/NA11550MA-EPH ☼Chromium 1.15 mg/Kg0.358 Total/NA14.27 6010D ☼Lead 1.15 mg/Kg0.254 Total/NA19.91 6010D Eurofins Pensacola This Detection Summary does not include radiochemical test results. Page 7 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Sample Summary Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID Client Sample ID Matrix Collected Received 400-241823-1 W.O. CS1 (17)Solid 07/31/23 12:00 08/10/23 09:49 400-241823-2 W.O. CS2 (17)Solid 07/31/23 12:04 08/10/23 09:49 400-241823-3 W.O. CS3 (17)Solid 07/31/23 12:07 08/10/23 09:49 400-241823-4 W.O. SW1 (12)Solid 08/01/23 12:21 08/10/23 09:49 400-241823-5 W.O. SW2 (12)Solid 08/01/23 12:30 08/10/23 09:49 400-241823-6 W.O. SW3 (12)Solid 08/01/23 12:33 08/10/23 09:49 400-241823-7 H.O. BE2 (17)Solid 08/01/23 12:38 08/10/23 09:49 400-241823-8 H.O. BE1 (17)Solid 08/01/23 13:50 08/10/23 09:49 Eurofins PensacolaPage 8 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-1Client Sample ID: W.O. CS1 (17) Matrix: SolidDate Collected: 07/31/23 12:00 Percent Solids: 82.1Date Received: 08/10/23 09:49 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL 0.00117 U 0.00771 0.00117 mg/Kg ☼08/14/23 08:30 08/16/23 20:01 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 UAcenaphthylene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 UAnthracene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00171 JBenzo[a]anthracene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00198 J BBenzo[a]pyrene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00175 J BBenzo[b]fluoranthene 0.00771 0.00234 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00234 UBenzo[g,h,i]perylene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 UBenzo[k]fluoranthene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 UChrysene 0.00771 0.00234 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00234 UDibenz(a,h)anthracene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 UFluoranthene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 UFluorene 0.00771 0.00234 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00299 J BIndeno[1,2,3-cd]pyrene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 UNaphthalene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00134 J BPhenanthrene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 UPyrene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 U1-Methylnaphthalene 0.00771 0.00117 mg/Kg 08/14/23 08:30 08/16/23 20:01 1☼0.00117 U2-Methylnaphthalene 2-Fluorobiphenyl 119 27-127 08/14/23 08:30 08/16/23 20:01 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 103 08/14/23 08:30 08/16/23 20:01 115-136 Terphenyl-d14 166 S1+08/14/23 08:30 08/16/23 20:01 124-146 Method: SW846 6010D - Metals (ICP) RL MDL 12.8 1.13 0.349 mg/Kg ☼08/16/23 15:09 08/17/23 03:29 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.13 0.248 mg/Kg 08/16/23 15:09 08/17/23 03:29 1☼18.0Lead General Chemistry RL MDL 82.1 0.01 0.01 %08/15/23 17:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %08/15/23 17:12 117.9Percent Moisture (EPA Moisture) Eurofins Pensacola Page 9 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-2Client Sample ID: W.O. CS2 (17) Matrix: SolidDate Collected: 07/31/23 12:04 Percent Solids: 85.9Date Received: 08/10/23 09:49 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL 0.00115 U 0.00760 0.00115 mg/Kg ☼08/14/23 08:30 08/16/23 20:22 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00115 UAcenaphthylene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00115 UAnthracene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00140 JBenzo[a]anthracene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00178 J BBenzo[a]pyrene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00150 J BBenzo[b]fluoranthene 0.00760 0.00230 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00230 UBenzo[g,h,i]perylene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00115 UBenzo[k]fluoranthene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00115 UChrysene 0.00760 0.00230 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00230 UDibenz(a,h)anthracene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00261 JFluoranthene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00115 UFluorene 0.00760 0.00230 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00298 J BIndeno[1,2,3-cd]pyrene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00115 UNaphthalene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00140 J BPhenanthrene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00115 UPyrene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00115 U1-Methylnaphthalene 0.00760 0.00115 mg/Kg 08/14/23 08:30 08/16/23 20:22 1☼0.00115 U2-Methylnaphthalene 2-Fluorobiphenyl 105 27-127 08/14/23 08:30 08/16/23 20:22 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 84 08/14/23 08:30 08/16/23 20:22 115-136 Terphenyl-d14 146 08/14/23 08:30 08/16/23 20:22 124-146 Method: SW846 6010D - Metals (ICP) RL MDL 10.4 1.06 0.327 mg/Kg ☼08/16/23 15:09 08/17/23 03:32 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.06 0.232 mg/Kg 08/16/23 15:09 08/17/23 03:32 1☼16.3Lead General Chemistry RL MDL 85.9 0.01 0.01 %08/15/23 17:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %08/15/23 17:12 114.1Percent Moisture (EPA Moisture) Eurofins Pensacola Page 10 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-3Client Sample ID: W.O. CS3 (17) Matrix: SolidDate Collected: 07/31/23 12:07 Percent Solids: 81.0Date Received: 08/10/23 09:49 Method: SW846 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) RL MDL 0.00122 U 0.00806 0.00122 mg/Kg ☼08/14/23 08:30 08/16/23 20:42 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Acenaphthene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 UAcenaphthylene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 UAnthracene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00132 JBenzo[a]anthracene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00203 J BBenzo[a]pyrene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00133 J BBenzo[b]fluoranthene 0.00806 0.00244 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00244 UBenzo[g,h,i]perylene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 UBenzo[k]fluoranthene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 UChrysene 0.00806 0.00244 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00244 UDibenz(a,h)anthracene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 UFluoranthene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 UFluorene 0.00806 0.00244 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00292 J BIndeno[1,2,3-cd]pyrene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 UNaphthalene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00153 J BPhenanthrene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 UPyrene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 U1-Methylnaphthalene 0.00806 0.00122 mg/Kg 08/14/23 08:30 08/16/23 20:42 1☼0.00122 U2-Methylnaphthalene 2-Fluorobiphenyl 97 27-127 08/14/23 08:30 08/16/23 20:42 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Nitrobenzene-d5 82 08/14/23 08:30 08/16/23 20:42 115-136 Terphenyl-d14 134 08/14/23 08:30 08/16/23 20:42 124-146 Method: SW846 6010D - Metals (ICP) RL MDL 11.8 1.12 0.347 mg/Kg ☼08/16/23 15:09 08/17/23 03:35 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.12 0.246 mg/Kg 08/16/23 15:09 08/17/23 03:35 1☼19.5Lead General Chemistry RL MDL 81.0 0.01 0.01 %08/15/23 17:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %08/15/23 17:12 119.0Percent Moisture (EPA Moisture) Eurofins Pensacola Page 11 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-4Client Sample ID: W.O. SW1 (12) Matrix: SolidDate Collected: 08/01/23 12:21 Percent Solids: 82.7Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL 0.00105 U 0.00476 0.00105 mg/Kg ☼08/15/23 09:46 08/15/23 17:00 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00476 0.00105 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00105 U1,1,1-Trichloroethane 0.00476 0.000780 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000780 U1,1,2,2-Tetrachloroethane 0.00476 0.000742 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000742 U1,1,2-Trichloroethane 0.00476 0.000790 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000790 U1,1-Dichloroethane 0.00476 0.000809 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000809 U1,1-Dichloroethene 0.00476 0.000790 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000790 U1,1-Dichloropropene 0.00476 0.00105 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00105 U1,2,3-Trichlorobenzene 0.00476 0.000761 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000761 U1,2,3-Trichloropropane 0.00476 0.000875 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000875 U1,2,4-Trichlorobenzene 0.00476 0.000951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000951 U1,2,4-Trimethylbenzene 0.00476 0.000951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000951 U1,2-Dibromoethane 0.00476 0.000675 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000675 U1,2-Dichlorobenzene 0.00476 0.000780 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000780 U1,2-Dichloroethane 0.00476 0.000723 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000723 U1,2-Dichloropropane 0.00476 0.000790 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000790 U1,3,5-Trimethylbenzene 0.00476 0.000904 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000904 U1,3-Dichlorobenzene 0.00476 0.000951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000951 U1,3-Dichloropropane 0.00476 0.000818 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000818 U1,4-Dichlorobenzene 0.00476 0.00105 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00105 U2,2-Dichloropropane 0.0238 0.00571 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00571 U2-Butanone (MEK) 0.00476 0.000771 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000771 U2-Chlorotoluene 0.0238 0.00476 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00476 U2-Hexanone 0.00476 0.000932 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000932 U4-Chlorotoluene 0.00476 0.000951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000951 U4-Isopropyltoluene 0.0238 0.00476 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00476 U4-Methyl-2-pentanone (MIBK) 0.0238 0.0114 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.0466Acetone 0.00476 0.000637 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000637 UBenzene 0.00476 0.00124 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00124 UBromobenzene 0.00476 0.000771 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000771 UBromochloromethane 0.00476 0.000875 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000875 UBromodichloromethane 0.00476 0.00124 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00124 UBromoform 0.00476 0.00238 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00238 UBromomethane 0.00476 0.00162 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00162 UCarbon tetrachloride 0.00476 0.000495 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000495 UChlorobenzene 0.00476 0.00114 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00114 UChloroethane 0.00476 0.00476 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00476 UChloroform 0.00476 0.000951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000951 UChloromethane 0.00476 0.000723 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000723 Ucis-1,2-Dichloroethene 0.00476 0.00114 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00114 Ucis-1,3-Dichloropropene 0.00476 0.00114 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00114 UDibromochloromethane 0.00476 0.00124 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00124 UDichlorodifluoromethane 0.0951 0.0704 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.0704 UEthanol 0.00476 0.000580 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000580 UEthylbenzene 0.00476 0.000523 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000523 UIsopropyl ether 0.00476 0.000647 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000647 UIsopropylbenzene 0.00476 0.000951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000951 UMethyl tert-butyl ether 0.0143 0.00951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00951 UMethylene Chloride 0.00476 0.00285 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00285 UNaphthalene Eurofins Pensacola Page 12 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-4Client Sample ID: W.O. SW1 (12) Matrix: SolidDate Collected: 08/01/23 12:21 Percent Solids: 82.7Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL 0.000913 U 0.00476 0.000913 mg/Kg ☼08/15/23 09:46 08/15/23 17:00 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00476 0.000856 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000856 UN-Propylbenzene 0.00476 0.000904 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000904 Usec-Butylbenzene 0.00476 0.000951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000951 UStyrene 0.00476 0.00105 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00105 Utert-Butylbenzene 0.00476 0.00285 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00285 UTetrachloroethene 0.00476 0.000951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00156 JToluene 0.00476 0.000913 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000913 Utrans-1,2-Dichloroethene 0.00476 0.00105 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00105 Utrans-1,3-Dichloropropene 0.00476 0.000951 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000951 UTrichloroethene 0.00476 0.000818 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000818 UTrichlorofluoromethane 0.0238 0.00181 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00181 UVinyl acetate 0.00476 0.000761 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.000761 UVinyl chloride 0.00951 0.00181 mg/Kg 08/15/23 09:46 08/15/23 17:00 1☼0.00181 UXylenes, Total 4-Bromofluorobenzene 103 67-130 08/15/23 09:46 08/15/23 17:00 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 99 08/15/23 09:46 08/15/23 17:00 177-127 Toluene-d8 (Surr)105 08/15/23 09:46 08/15/23 17:00 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL 0.0382 U 0.382 0.0382 mg/Kg ☼08/14/23 08:30 08/15/23 18:45 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1-Methylnaphthalene 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U2,4,5-Trichlorophenol 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U2,4,6-Trichlorophenol 0.382 0.0811 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0811 U2,4-Dichlorophenol 0.382 0.109 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.109 U2,4-Dimethylphenol 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U2,4-Dinitrotoluene 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U2,6-Dinitrotoluene 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U2-Chloronaphthalene 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U2-Chlorophenol 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U2-Methylnaphthalene 0.382 0.0927 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0927 U2-Methylphenol 0.382 0.0811 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0811 U2-Nitroaniline 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U2-Nitrophenol 0.764 0.0892 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0892 U3 & 4 Methylphenol 0.382 0.0903 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0903 U3-Nitroaniline 0.382 0.278 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.278 U4,6-Dinitro-2-methylphenol 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U4-Bromophenyl phenyl ether 0.382 0.0938 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0938 U4-Chloro-3-methylphenol 0.382 0.0938 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0938 U4-Chloroaniline 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 U4-Chlorophenyl phenyl ether 0.382 0.131 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.131 U4-Nitroaniline 0.382 0.347 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.347 U4-Nitrophenol 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UAcenaphthene 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UAcenaphthylene 0.382 0.114 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.114 UAniline 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UAnthracene 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UBenzo[a]anthracene 0.382 0.0544 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0544 UBenzo[a]pyrene Eurofins Pensacola Page 13 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-4Client Sample ID: W.O. SW1 (12) Matrix: SolidDate Collected: 08/01/23 12:21 Percent Solids: 82.7Date Received: 08/10/23 09:49 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 0.115 U 0.382 0.115 mg/Kg ☼08/14/23 08:30 08/15/23 18:45 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzo[b]fluoranthene 0.382 0.127 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.127 UBenzo[g,h,i]perylene 0.382 0.0903 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0903 UBenzo[k]fluoranthene 1.15 0.405 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.405 UBenzoic acid 0.382 0.146 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.146 Ubis (2-chloroisopropyl) ether 0.382 0.0846 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0846 UBis(2-chloroethoxy)methane 0.382 0.0533 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0533 UBis(2-chloroethyl)ether 0.382 0.0938 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0938 UBis(2-ethylhexyl) phthalate 0.382 0.0822 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0822 UButyl benzyl phthalate 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UChrysene 0.382 0.0660 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0660 UDibenz(a,h)anthracene 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UDibenzofuran 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UDiethyl phthalate 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UDimethyl phthalate 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UDi-n-butyl phthalate 0.382 0.139 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.139 UDi-n-octyl phthalate 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UFluoranthene 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UFluorene 0.382 0.116 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.116 UHexachlorobenzene 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UHexachlorobutadiene 0.382 0.0764 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0764 UHexachlorocyclopentadiene 0.382 0.0811 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0811 UHexachloroethane 0.382 0.0764 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0764 UIndeno[1,2,3-cd]pyrene 0.382 0.0776 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0776 UIsophorone 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UNitrobenzene 0.382 0.122 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.122 UN-Nitrosodi-n-propylamine 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UN-Nitrosodiphenylamine 0.764 0.185 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.185 UPentachlorophenol 0.382 0.0382 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0382 UPhenanthrene 0.382 0.103 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.103 UPhenol 0.382 0.0903 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.0903 UPyrene 0.382 0.174 mg/Kg 08/14/23 08:30 08/15/23 18:45 1☼0.174 UPyridine 2,4,6-Tribromophenol (Surr)89 10-150 08/14/23 08:30 08/15/23 18:45 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 70 08/14/23 08:30 08/15/23 18:45 127-127 2-Fluorophenol (Surr)76 08/14/23 08:30 08/15/23 18:45 125-128 Nitrobenzene-d5 (Surr)63 08/14/23 08:30 08/15/23 18:45 115-136 Phenol-d5 (Surr)69 08/14/23 08:30 08/15/23 18:45 129-130 Terphenyl-d14 (Surr)88 08/14/23 08:30 08/15/23 18:45 124-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL 3.56 U 3.56 3.56 mg/Kg ☼08/14/23 09:50 08/14/23 13:06 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.85 1.85 mg/Kg 08/14/23 09:50 08/14/23 13:06 50☼1.85 UC9-C12 Aliphatics 0.990 0.990 mg/Kg 08/14/23 09:50 08/14/23 13:06 50☼0.990 UC9-C10 Aromatics a,a,a-Trifluorotoluene (fid)110 70-130 08/14/23 09:50 08/14/23 13:06 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)108 08/14/23 09:50 08/14/23 13:06 5070-130 Eurofins Pensacola Page 14 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-4Client Sample ID: W.O. SW1 (12) Matrix: SolidDate Collected: 08/01/23 12:21 Percent Solids: 82.7Date Received: 08/10/23 09:49 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL 1.92 U F1 1.92 1.92 mg/Kg ☼08/14/23 13:55 08/17/23 20:16 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.92 1.92 mg/Kg 08/14/23 13:55 08/17/23 20:16 1☼1.92 UC19-C36 Aliphatics 3.60 3.60 mg/Kg 08/14/23 13:55 08/18/23 03:55 1☼3.60 UC11-C22 Aromatics 1-Chlorooctadecane 45 40-140 08/14/23 13:55 08/17/23 20:16 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 40 08/14/23 13:55 08/18/23 03:55 140-140 2-Fluorobiphenyl 80 08/14/23 13:55 08/18/23 03:55 140-140 2-Bromonaphthalene 75 08/14/23 13:55 08/18/23 03:55 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 13.3 1.20 0.372 mg/Kg ☼08/16/23 15:09 08/17/23 03:39 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.20 0.264 mg/Kg 08/16/23 15:09 08/17/23 03:39 1☼20.1Lead General Chemistry RL MDL 82.7 0.01 0.01 %08/15/23 17:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %08/15/23 17:12 117.3Percent Moisture (EPA Moisture) Eurofins Pensacola Page 15 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-5Client Sample ID: W.O. SW2 (12) Matrix: SolidDate Collected: 08/01/23 12:30 Percent Solids: 84.8Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL 0.00112 U 0.00507 0.00112 mg/Kg ☼08/14/23 08:59 08/14/23 18:59 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00507 0.00112 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00112 U1,1,1-Trichloroethane 0.00507 0.000831 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000831 U1,1,2,2-Tetrachloroethane 0.00507 0.000791 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000791 U1,1,2-Trichloroethane 0.00507 0.000842 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000842 U1,1-Dichloroethane 0.00507 0.000862 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000862 U1,1-Dichloroethene 0.00507 0.000842 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000842 U1,1-Dichloropropene 0.00507 0.00112 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00112 U1,2,3-Trichlorobenzene 0.00507 0.000811 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000811 U1,2,3-Trichloropropane 0.00507 0.000933 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000933 U1,2,4-Trichlorobenzene 0.00507 0.00101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00101 U1,2,4-Trimethylbenzene 0.00507 0.00101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00101 U1,2-Dibromoethane 0.00507 0.000720 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000720 U1,2-Dichlorobenzene 0.00507 0.000831 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000831 U1,2-Dichloroethane 0.00507 0.000771 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000771 U1,2-Dichloropropane 0.00507 0.000842 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000842 U1,3,5-Trimethylbenzene 0.00507 0.000963 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000963 U1,3-Dichlorobenzene 0.00507 0.00101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00101 U1,3-Dichloropropane 0.00507 0.000872 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000872 U1,4-Dichlorobenzene 0.00507 0.00112 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00112 U2,2-Dichloropropane 0.0253 0.00608 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00608 U2-Butanone (MEK) 0.00507 0.000821 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000821 U2-Chlorotoluene 0.0253 0.00507 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00507 U2-Hexanone 0.00507 0.000994 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000994 U4-Chlorotoluene 0.00507 0.00101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00101 U4-Isopropyltoluene 0.0253 0.00507 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00507 U4-Methyl-2-pentanone (MIBK) 0.0253 0.0122 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.0449Acetone 0.00507 0.000679 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000679 UBenzene 0.00507 0.00132 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00132 UBromobenzene 0.00507 0.000821 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000821 UBromochloromethane 0.00507 0.000933 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000933 UBromodichloromethane 0.00507 0.00132 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00132 UBromoform 0.00507 0.00253 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00253 UBromomethane 0.00507 0.00172 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00172 UCarbon tetrachloride 0.00507 0.000527 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000527 UChlorobenzene 0.00507 0.00122 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00122 UChloroethane 0.00507 0.00507 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00507 UChloroform 0.00507 0.00101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00101 UChloromethane 0.00507 0.000771 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000771 Ucis-1,2-Dichloroethene 0.00507 0.00122 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00122 Ucis-1,3-Dichloropropene 0.00507 0.00122 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00122 UDibromochloromethane 0.00507 0.00132 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00132 UDichlorodifluoromethane 0.101 0.0750 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.0907 JEthanol 0.00507 0.000619 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000619 UEthylbenzene 0.00507 0.000558 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000558 UIsopropyl ether 0.00507 0.000689 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000689 UIsopropylbenzene 0.00507 0.00101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00101 UMethyl tert-butyl ether 0.0152 0.0101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.0101 UMethylene Chloride 0.00507 0.00304 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00304 UNaphthalene Eurofins Pensacola Page 16 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-5Client Sample ID: W.O. SW2 (12) Matrix: SolidDate Collected: 08/01/23 12:30 Percent Solids: 84.8Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL 0.000973 U 0.00507 0.000973 mg/Kg ☼08/14/23 08:59 08/14/23 18:59 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00507 0.000913 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000913 UN-Propylbenzene 0.00507 0.000963 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000963 Usec-Butylbenzene 0.00507 0.00101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00101 UStyrene 0.00507 0.00112 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00112 Utert-Butylbenzene 0.00507 0.00304 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00304 UTetrachloroethene 0.00507 0.00101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00240 JToluene 0.00507 0.000973 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000973 Utrans-1,2-Dichloroethene 0.00507 0.00112 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00112 Utrans-1,3-Dichloropropene 0.00507 0.00101 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00101 UTrichloroethene 0.00507 0.000872 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000872 UTrichlorofluoromethane 0.0253 0.00193 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00193 UVinyl acetate 0.00507 0.000811 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.000811 UVinyl chloride 0.0101 0.00193 mg/Kg 08/14/23 08:59 08/14/23 18:59 1☼0.00198 JXylenes, Total 4-Bromofluorobenzene 108 67-130 08/14/23 08:59 08/14/23 18:59 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 103 08/14/23 08:59 08/14/23 18:59 177-127 Toluene-d8 (Surr)101 08/14/23 08:59 08/14/23 18:59 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL 0.0367 U 0.367 0.0367 mg/Kg ☼08/14/23 08:30 08/15/23 19:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1-Methylnaphthalene 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U2,4,5-Trichlorophenol 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U2,4,6-Trichlorophenol 0.367 0.0779 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0779 U2,4-Dichlorophenol 0.367 0.105 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.105 U2,4-Dimethylphenol 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U2,4-Dinitrotoluene 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U2,6-Dinitrotoluene 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U2-Chloronaphthalene 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U2-Chlorophenol 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U2-Methylnaphthalene 0.367 0.0890 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0890 U2-Methylphenol 0.367 0.0779 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0779 U2-Nitroaniline 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U2-Nitrophenol 0.734 0.0857 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0857 U3 & 4 Methylphenol 0.367 0.0868 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0868 U3-Nitroaniline 0.367 0.267 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.267 U4,6-Dinitro-2-methylphenol 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U4-Bromophenyl phenyl ether 0.367 0.0901 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0901 U4-Chloro-3-methylphenol 0.367 0.0901 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0901 U4-Chloroaniline 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 U4-Chlorophenyl phenyl ether 0.367 0.126 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.126 U4-Nitroaniline 0.367 0.334 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.334 U4-Nitrophenol 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UAcenaphthene 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UAcenaphthylene 0.367 0.109 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.109 UAniline 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UAnthracene 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UBenzo[a]anthracene 0.367 0.0523 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0523 UBenzo[a]pyrene Eurofins Pensacola Page 17 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-5Client Sample ID: W.O. SW2 (12) Matrix: SolidDate Collected: 08/01/23 12:30 Percent Solids: 84.8Date Received: 08/10/23 09:49 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 0.110 U 0.367 0.110 mg/Kg ☼08/14/23 08:30 08/15/23 19:08 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzo[b]fluoranthene 0.367 0.122 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.122 UBenzo[g,h,i]perylene 0.367 0.0868 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0868 UBenzo[k]fluoranthene 1.10 0.389 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.389 UBenzoic acid 0.367 0.140 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.140 Ubis (2-chloroisopropyl) ether 0.367 0.0812 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0812 UBis(2-chloroethoxy)methane 0.367 0.0512 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0512 UBis(2-chloroethyl)ether 0.367 0.0901 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0901 UBis(2-ethylhexyl) phthalate 0.367 0.0790 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0790 UButyl benzyl phthalate 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UChrysene 0.367 0.0634 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0634 UDibenz(a,h)anthracene 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UDibenzofuran 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UDiethyl phthalate 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UDimethyl phthalate 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UDi-n-butyl phthalate 0.367 0.133 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.133 UDi-n-octyl phthalate 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UFluoranthene 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UFluorene 0.367 0.111 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.111 UHexachlorobenzene 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UHexachlorobutadiene 0.367 0.0734 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0734 UHexachlorocyclopentadiene 0.367 0.0779 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0779 UHexachloroethane 0.367 0.0734 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0734 UIndeno[1,2,3-cd]pyrene 0.367 0.0745 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0745 UIsophorone 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UNitrobenzene 0.367 0.117 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.117 UN-Nitrosodi-n-propylamine 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UN-Nitrosodiphenylamine 0.734 0.178 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.178 UPentachlorophenol 0.367 0.0367 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0367 UPhenanthrene 0.367 0.0990 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0990 UPhenol 0.367 0.0868 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.0868 UPyrene 0.367 0.167 mg/Kg 08/14/23 08:30 08/15/23 19:08 1☼0.167 UPyridine 2,4,6-Tribromophenol (Surr)85 10-150 08/14/23 08:30 08/15/23 19:08 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 68 08/14/23 08:30 08/15/23 19:08 127-127 2-Fluorophenol (Surr)72 08/14/23 08:30 08/15/23 19:08 125-128 Nitrobenzene-d5 (Surr)63 08/14/23 08:30 08/15/23 19:08 115-136 Phenol-d5 (Surr)66 08/14/23 08:30 08/15/23 19:08 129-130 Terphenyl-d14 (Surr)92 08/14/23 08:30 08/15/23 19:08 124-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL 3.04 U 3.04 3.04 mg/Kg ☼08/14/23 09:50 08/14/23 13:44 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.58 1.58 mg/Kg 08/14/23 09:50 08/14/23 13:44 50☼1.58 UC9-C12 Aliphatics 0.845 0.845 mg/Kg 08/14/23 09:50 08/14/23 13:44 50☼0.845 UC9-C10 Aromatics a,a,a-Trifluorotoluene (fid)110 70-130 08/14/23 09:50 08/14/23 13:44 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)108 08/14/23 09:50 08/14/23 13:44 5070-130 Eurofins Pensacola Page 18 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-5Client Sample ID: W.O. SW2 (12) Matrix: SolidDate Collected: 08/01/23 12:30 Percent Solids: 84.8Date Received: 08/10/23 09:49 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL 1.84 U 1.84 1.84 mg/Kg ☼08/14/23 13:55 08/17/23 20:33 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.84 1.84 mg/Kg 08/14/23 13:55 08/17/23 20:33 1☼1.84 UC19-C36 Aliphatics 3.44 3.44 mg/Kg 08/14/23 13:55 08/18/23 04:12 1☼3.44 UC11-C22 Aromatics 1-Chlorooctadecane 54 40-140 08/14/23 13:55 08/17/23 20:33 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 42 08/14/23 13:55 08/18/23 04:12 140-140 2-Fluorobiphenyl 72 08/14/23 13:55 08/18/23 04:12 140-140 2-Bromonaphthalene 68 08/14/23 13:55 08/18/23 04:12 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 9.38 1.17 0.364 mg/Kg ☼08/16/23 15:09 08/17/23 03:42 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.17 0.258 mg/Kg 08/16/23 15:09 08/17/23 03:42 1☼18.5Lead General Chemistry RL MDL 84.8 0.01 0.01 %08/15/23 17:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %08/15/23 17:12 115.2Percent Moisture (EPA Moisture) Eurofins Pensacola Page 19 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-6Client Sample ID: W.O. SW3 (12) Matrix: SolidDate Collected: 08/01/23 12:33 Percent Solids: 81.4Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL 0.00109 U 0.00495 0.00109 mg/Kg ☼08/14/23 08:59 08/14/23 19:26 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00495 0.00109 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00109 U1,1,1-Trichloroethane 0.00495 0.000813 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000813 U1,1,2,2-Tetrachloroethane 0.00495 0.000773 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000773 U1,1,2-Trichloroethane 0.00495 0.000822 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000822 U1,1-Dichloroethane 0.00495 0.000842 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000842 U1,1-Dichloroethene 0.00495 0.000822 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000822 U1,1-Dichloropropene 0.00495 0.00109 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00109 U1,2,3-Trichlorobenzene 0.00495 0.000793 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000793 U1,2,3-Trichloropropane 0.00495 0.000912 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000912 U1,2,4-Trichlorobenzene 0.00495 0.000991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000991 U1,2,4-Trimethylbenzene 0.00495 0.000991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000991 U1,2-Dibromoethane 0.00495 0.000704 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000704 U1,2-Dichlorobenzene 0.00495 0.000813 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000813 U1,2-Dichloroethane 0.00495 0.000753 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000753 U1,2-Dichloropropane 0.00495 0.000822 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000822 U1,3,5-Trimethylbenzene 0.00495 0.000941 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000941 U1,3-Dichlorobenzene 0.00495 0.000991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000991 U1,3-Dichloropropane 0.00495 0.000852 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000852 U1,4-Dichlorobenzene 0.00495 0.00109 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00109 U2,2-Dichloropropane 0.0248 0.00595 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00595 U2-Butanone (MEK) 0.00495 0.000803 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000803 U2-Chlorotoluene 0.0248 0.00495 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00495 U2-Hexanone 0.00495 0.000971 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000971 U4-Chlorotoluene 0.00495 0.000991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000991 U4-Isopropyltoluene 0.0248 0.00495 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00495 U4-Methyl-2-pentanone (MIBK) 0.0248 0.0119 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.0719Acetone 0.00495 0.000664 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000664 UBenzene 0.00495 0.00129 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00129 UBromobenzene 0.00495 0.000803 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000803 UBromochloromethane 0.00495 0.000912 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000912 UBromodichloromethane 0.00495 0.00129 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00129 UBromoform 0.00495 0.00248 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00248 UBromomethane 0.00495 0.00168 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00168 UCarbon tetrachloride 0.00495 0.000515 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000515 UChlorobenzene 0.00495 0.00119 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00119 UChloroethane 0.00495 0.00495 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00495 UChloroform 0.00495 0.000991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000991 UChloromethane 0.00495 0.000753 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000753 Ucis-1,2-Dichloroethene 0.00495 0.00119 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00119 Ucis-1,3-Dichloropropene 0.00495 0.00119 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00119 UDibromochloromethane 0.00495 0.00129 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00129 UDichlorodifluoromethane 0.0991 0.0733 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.0733 UEthanol 0.00495 0.000604 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000604 UEthylbenzene 0.00495 0.000545 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000545 UIsopropyl ether 0.00495 0.000674 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000674 UIsopropylbenzene 0.00495 0.000991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000991 UMethyl tert-butyl ether 0.0149 0.00991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00991 UMethylene Chloride 0.00495 0.00297 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00297 UNaphthalene Eurofins Pensacola Page 20 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-6Client Sample ID: W.O. SW3 (12) Matrix: SolidDate Collected: 08/01/23 12:33 Percent Solids: 81.4Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL 0.000951 U 0.00495 0.000951 mg/Kg ☼08/14/23 08:59 08/14/23 19:26 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00495 0.000892 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000892 UN-Propylbenzene 0.00495 0.000941 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000941 Usec-Butylbenzene 0.00495 0.000991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000991 UStyrene 0.00495 0.00109 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00109 Utert-Butylbenzene 0.00495 0.00297 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00297 UTetrachloroethene 0.00495 0.000991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00193 JToluene 0.00495 0.000951 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000951 Utrans-1,2-Dichloroethene 0.00495 0.00109 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00109 Utrans-1,3-Dichloropropene 0.00495 0.000991 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000991 UTrichloroethene 0.00495 0.000852 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000852 UTrichlorofluoromethane 0.0248 0.00188 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00188 UVinyl acetate 0.00495 0.000793 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.000793 UVinyl chloride 0.00991 0.00188 mg/Kg 08/14/23 08:59 08/14/23 19:26 1☼0.00188 UXylenes, Total 4-Bromofluorobenzene 109 67-130 08/14/23 08:59 08/14/23 19:26 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 104 08/14/23 08:59 08/14/23 19:26 177-127 Toluene-d8 (Surr)101 08/14/23 08:59 08/14/23 19:26 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL 0.0402 U 0.402 0.0402 mg/Kg ☼08/14/23 08:30 08/15/23 19:30 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1-Methylnaphthalene 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U2,4,5-Trichlorophenol 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U2,4,6-Trichlorophenol 0.402 0.0852 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0852 U2,4-Dichlorophenol 0.402 0.114 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.114 U2,4-Dimethylphenol 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U2,4-Dinitrotoluene 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U2,6-Dinitrotoluene 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U2-Chloronaphthalene 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U2-Chlorophenol 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U2-Methylnaphthalene 0.402 0.0974 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0974 U2-Methylphenol 0.402 0.0852 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0852 U2-Nitroaniline 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U2-Nitrophenol 0.803 0.0937 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0937 U3 & 4 Methylphenol 0.402 0.0949 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0949 U3-Nitroaniline 0.402 0.292 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.292 U4,6-Dinitro-2-methylphenol 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U4-Bromophenyl phenyl ether 0.402 0.0986 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0986 U4-Chloro-3-methylphenol 0.402 0.0986 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0986 U4-Chloroaniline 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 U4-Chlorophenyl phenyl ether 0.402 0.138 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.138 U4-Nitroaniline 0.402 0.365 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.365 U4-Nitrophenol 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UAcenaphthene 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UAcenaphthylene 0.402 0.119 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.119 UAniline 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UAnthracene 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UBenzo[a]anthracene 0.402 0.0572 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0572 UBenzo[a]pyrene Eurofins Pensacola Page 21 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-6Client Sample ID: W.O. SW3 (12) Matrix: SolidDate Collected: 08/01/23 12:33 Percent Solids: 81.4Date Received: 08/10/23 09:49 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 0.120 U 0.402 0.120 mg/Kg ☼08/14/23 08:30 08/15/23 19:30 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzo[b]fluoranthene 0.402 0.134 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.134 UBenzo[g,h,i]perylene 0.402 0.0949 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0949 UBenzo[k]fluoranthene 1.20 0.426 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.426 UBenzoic acid 0.402 0.153 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.153 Ubis (2-chloroisopropyl) ether 0.402 0.0889 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0889 UBis(2-chloroethoxy)methane 0.402 0.0560 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0560 UBis(2-chloroethyl)ether 0.402 0.0986 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0986 UBis(2-ethylhexyl) phthalate 0.402 0.0864 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0864 UButyl benzyl phthalate 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UChrysene 0.402 0.0694 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0694 UDibenz(a,h)anthracene 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UDibenzofuran 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UDiethyl phthalate 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UDimethyl phthalate 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UDi-n-butyl phthalate 0.402 0.146 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.146 UDi-n-octyl phthalate 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UFluoranthene 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UFluorene 0.402 0.122 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.122 UHexachlorobenzene 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UHexachlorobutadiene 0.402 0.0803 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0803 UHexachlorocyclopentadiene 0.402 0.0852 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0852 UHexachloroethane 0.402 0.0803 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0803 UIndeno[1,2,3-cd]pyrene 0.402 0.0815 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0815 UIsophorone 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UNitrobenzene 0.402 0.128 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.128 UN-Nitrosodi-n-propylamine 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UN-Nitrosodiphenylamine 0.803 0.195 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.195 UPentachlorophenol 0.402 0.0402 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0402 UPhenanthrene 0.402 0.108 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.108 UPhenol 0.402 0.0949 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.0949 UPyrene 0.402 0.183 mg/Kg 08/14/23 08:30 08/15/23 19:30 1☼0.183 UPyridine 2,4,6-Tribromophenol (Surr)86 10-150 08/14/23 08:30 08/15/23 19:30 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 66 08/14/23 08:30 08/15/23 19:30 127-127 2-Fluorophenol (Surr)72 08/14/23 08:30 08/15/23 19:30 125-128 Nitrobenzene-d5 (Surr)60 08/14/23 08:30 08/15/23 19:30 115-136 Phenol-d5 (Surr)65 08/14/23 08:30 08/15/23 19:30 129-130 Terphenyl-d14 (Surr)87 08/14/23 08:30 08/15/23 19:30 124-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL 3.33 U 3.33 3.33 mg/Kg ☼08/14/23 09:50 08/14/23 14:35 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.72 1.72 mg/Kg 08/14/23 09:50 08/14/23 14:35 50☼1.72 UC9-C12 Aliphatics 0.924 0.924 mg/Kg 08/14/23 09:50 08/14/23 14:35 50☼0.924 UC9-C10 Aromatics a,a,a-Trifluorotoluene (fid)109 70-130 08/14/23 09:50 08/14/23 14:35 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)107 08/14/23 09:50 08/14/23 14:35 5070-130 Eurofins Pensacola Page 22 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-6Client Sample ID: W.O. SW3 (12) Matrix: SolidDate Collected: 08/01/23 12:33 Percent Solids: 81.4Date Received: 08/10/23 09:49 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL 1.95 U 1.95 1.95 mg/Kg ☼08/14/23 13:55 08/17/23 20:50 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.95 1.95 mg/Kg 08/14/23 13:55 08/17/23 20:50 1☼1.95 UC19-C36 Aliphatics 3.65 3.65 mg/Kg 08/14/23 13:55 08/18/23 04:29 1☼3.65 UC11-C22 Aromatics 1-Chlorooctadecane 72 40-140 08/14/23 13:55 08/17/23 20:50 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 67 08/14/23 13:55 08/18/23 04:29 140-140 2-Fluorobiphenyl 88 08/14/23 13:55 08/18/23 04:29 140-140 2-Bromonaphthalene 84 08/14/23 13:55 08/18/23 04:29 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 8.56 1.14 0.353 mg/Kg ☼08/16/23 15:09 08/17/23 03:46 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.14 0.250 mg/Kg 08/16/23 15:09 08/17/23 03:46 1☼16.2Lead General Chemistry RL MDL 81.4 0.01 0.01 %08/15/23 17:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %08/15/23 17:12 118.6Percent Moisture (EPA Moisture) Eurofins Pensacola Page 23 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-7Client Sample ID: H.O. BE2 (17) Matrix: SolidDate Collected: 08/01/23 12:38 Percent Solids: 83.3Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL 0.0614 U 0.279 0.0614 mg/Kg ☼08/14/23 08:59 08/14/23 20:47 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.279 0.0614 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0614 U1,1,1-Trichloroethane 0.279 0.0458 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0458 U1,1,2,2-Tetrachloroethane 0.279 0.0435 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0435 U1,1,2-Trichloroethane 0.279 0.0463 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0463 U1,1-Dichloroethane 0.279 0.0474 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0474 U1,1-Dichloroethene 0.279 0.0463 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0463 U1,1-Dichloropropene 0.279 0.0614 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0614 U1,2,3-Trichlorobenzene 0.279 0.0446 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0446 U1,2,3-Trichloropropane 0.279 0.0396 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0396 U1,2-Dichlorobenzene 0.279 0.0458 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0458 U1,2-Dichloroethane 0.279 0.0424 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0424 U1,2-Dichloropropane 0.279 0.0463 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0787 J1,3,5-Trimethylbenzene 0.279 0.0530 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0530 U1,3-Dichlorobenzene 0.279 0.0558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0558 U1,3-Dichloropropane 0.279 0.0480 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0480 U1,4-Dichlorobenzene 0.279 0.0614 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0614 U2,2-Dichloropropane 0.279 0.0452 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0452 U2-Chlorotoluene 1.39 0.279 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.279 U2-Hexanone 0.279 0.0547 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0547 U4-Chlorotoluene 1.39 0.670 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.670 UAcetone 0.279 0.0374 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0374 UBenzene 0.279 0.0725 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0725 UBromobenzene 0.279 0.0725 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0725 UBromoform 0.279 0.139 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.139 UBromomethane 0.279 0.0949 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0949 UCarbon tetrachloride 0.279 0.0290 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0290 UChlorobenzene 0.279 0.0452 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0452 UBromochloromethane 0.279 0.0670 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0670 UDibromochloromethane 0.279 0.0670 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0670 UChloroethane 0.279 0.279 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.279 UChloroform 0.279 0.0558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0558 UChloromethane 0.279 0.0424 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0424 Ucis-1,2-Dichloroethene 0.279 0.0670 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0670 Ucis-1,3-Dichloropropene 0.279 0.0513 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0513 UBromodichloromethane 0.279 0.0725 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0725 UDichlorodifluoromethane 0.279 0.0340 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0340 UEthylbenzene 0.279 0.0558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0558 U1,2-Dibromoethane 0.279 0.0307 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0307 UIsopropyl ether 0.279 0.0379 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0379 UIsopropylbenzene 0.279 0.0558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0558 UMethyl tert-butyl ether 0.837 0.558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.558 UMethylene Chloride 1.39 0.335 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.335 U2-Butanone (MEK) 1.39 0.279 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.279 U4-Methyl-2-pentanone (MIBK) 0.279 0.0536 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0536 Un-Butylbenzene 0.279 0.0502 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0502 UN-Propylbenzene 0.279 0.167 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.167 UNaphthalene 0.279 0.0530 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0530 Usec-Butylbenzene 0.279 0.0558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0558 UStyrene Eurofins Pensacola Page 24 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-7Client Sample ID: H.O. BE2 (17) Matrix: SolidDate Collected: 08/01/23 12:38 Percent Solids: 83.3Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL 0.0614 U 0.279 0.0614 mg/Kg ☼08/14/23 08:59 08/14/23 20:47 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier tert-Butylbenzene 0.279 0.167 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.167 UTetrachloroethene 0.279 0.0558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0558 UToluene 0.279 0.0536 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0536 Utrans-1,2-Dichloroethene 0.279 0.0614 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0614 Utrans-1,3-Dichloropropene 0.279 0.0558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0558 UTrichloroethene 0.279 0.0480 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0480 UTrichlorofluoromethane 1.39 0.106 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.106 UVinyl acetate 0.279 0.0446 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0446 UVinyl chloride 0.558 0.106 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.106 UXylenes, Total 0.279 0.0558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0558 U4-Isopropyltoluene 5.58 4.13 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼4.13 UEthanol 0.279 0.0558 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0558 U1,2,4-Trimethylbenzene 0.279 0.0513 mg/Kg 08/14/23 08:59 08/14/23 20:47 50☼0.0513 U1,2,4-Trichlorobenzene 4-Bromofluorobenzene 107 67-130 08/14/23 08:59 08/14/23 20:47 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 99 08/14/23 08:59 08/14/23 20:47 5077-127 Toluene-d8 (Surr)100 08/14/23 08:59 08/14/23 20:47 5076-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL 0.0378 U 0.378 0.0378 mg/Kg ☼08/14/23 08:30 08/15/23 19:52 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1-Methylnaphthalene 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U2,4,5-Trichlorophenol 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U2,4,6-Trichlorophenol 0.378 0.0802 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0802 U2,4-Dichlorophenol 0.378 0.108 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.108 U2,4-Dimethylphenol 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U2,4-Dinitrotoluene 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U2,6-Dinitrotoluene 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U2-Chloronaphthalene 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U2-Chlorophenol 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U2-Methylnaphthalene 0.378 0.0916 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0916 U2-Methylphenol 0.378 0.0802 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0802 U2-Nitroaniline 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U2-Nitrophenol 0.756 0.0882 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0882 U3 & 4 Methylphenol 0.378 0.0893 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0893 U3-Nitroaniline 0.378 0.275 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.275 U4,6-Dinitro-2-methylphenol 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U4-Bromophenyl phenyl ether 0.378 0.0928 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0928 U4-Chloro-3-methylphenol 0.378 0.0928 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0928 U4-Chloroaniline 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 U4-Chlorophenyl phenyl ether 0.378 0.129 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.129 U4-Nitroaniline 0.378 0.344 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.344 U4-Nitrophenol 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UAcenaphthene 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UAcenaphthylene 0.378 0.112 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.112 UAniline 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UAnthracene 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UBenzo[a]anthracene 0.378 0.0538 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0538 UBenzo[a]pyrene Eurofins Pensacola Page 25 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-7Client Sample ID: H.O. BE2 (17) Matrix: SolidDate Collected: 08/01/23 12:38 Percent Solids: 83.3Date Received: 08/10/23 09:49 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 0.113 U 0.378 0.113 mg/Kg ☼08/14/23 08:30 08/15/23 19:52 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzo[b]fluoranthene 0.378 0.126 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.126 UBenzo[g,h,i]perylene 0.378 0.0893 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0893 UBenzo[k]fluoranthene 1.13 0.401 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.401 UBenzoic acid 0.378 0.144 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.144 Ubis (2-chloroisopropyl) ether 0.378 0.0836 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0836 UBis(2-chloroethoxy)methane 0.378 0.0527 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0527 UBis(2-chloroethyl)ether 0.378 0.0928 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0928 UBis(2-ethylhexyl) phthalate 0.378 0.0813 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0813 UButyl benzyl phthalate 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UChrysene 0.378 0.0653 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0653 UDibenz(a,h)anthracene 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UDibenzofuran 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UDiethyl phthalate 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UDimethyl phthalate 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UDi-n-butyl phthalate 0.378 0.137 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.137 UDi-n-octyl phthalate 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UFluoranthene 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UFluorene 0.378 0.115 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.115 UHexachlorobenzene 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UHexachlorobutadiene 0.378 0.0756 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0756 UHexachlorocyclopentadiene 0.378 0.0802 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0802 UHexachloroethane 0.378 0.0756 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0756 UIndeno[1,2,3-cd]pyrene 0.378 0.0767 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0767 UIsophorone 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UNitrobenzene 0.378 0.120 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.120 UN-Nitrosodi-n-propylamine 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UN-Nitrosodiphenylamine 0.756 0.183 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.183 UPentachlorophenol 0.378 0.0378 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0378 UPhenanthrene 0.378 0.102 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.102 UPhenol 0.378 0.0893 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.0893 UPyrene 0.378 0.172 mg/Kg 08/14/23 08:30 08/15/23 19:52 1☼0.172 UPyridine 2,4,6-Tribromophenol (Surr)86 10-150 08/14/23 08:30 08/15/23 19:52 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 70 08/14/23 08:30 08/15/23 19:52 127-127 2-Fluorophenol (Surr)68 08/14/23 08:30 08/15/23 19:52 125-128 Nitrobenzene-d5 (Surr)62 08/14/23 08:30 08/15/23 19:52 115-136 Phenol-d5 (Surr)68 08/14/23 08:30 08/15/23 19:52 129-130 Terphenyl-d14 (Surr)93 08/14/23 08:30 08/15/23 19:52 124-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL 121 U 121 121 mg/Kg ☼08/14/23 09:50 08/14/23 20:24 2000 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 62.5 62.5 mg/Kg 08/14/23 09:50 08/14/23 20:24 2000☼86.0C9-C12 Aliphatics 33.5 33.5 mg/Kg 08/14/23 09:50 08/14/23 20:24 2000☼277C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)112 70-130 08/14/23 09:50 08/14/23 20:24 2000 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)111 08/14/23 09:50 08/14/23 20:24 200070-130 Eurofins Pensacola Page 26 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-7Client Sample ID: H.O. BE2 (17) Matrix: SolidDate Collected: 08/01/23 12:38 Percent Solids: 83.3Date Received: 08/10/23 09:49 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL 1.86 U 1.86 1.86 mg/Kg ☼08/14/23 13:55 08/17/23 21:06 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 1.86 1.86 mg/Kg 08/14/23 13:55 08/17/23 21:06 1☼1.86 UC19-C36 Aliphatics 3.49 3.49 mg/Kg 08/14/23 13:55 08/18/23 04:46 1☼3.49 UC11-C22 Aromatics 1-Chlorooctadecane 75 40-140 08/14/23 13:55 08/17/23 21:06 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 60 08/14/23 13:55 08/18/23 04:46 140-140 2-Fluorobiphenyl 85 08/14/23 13:55 08/18/23 04:46 140-140 2-Bromonaphthalene 80 08/14/23 13:55 08/18/23 04:46 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 7.50 1.15 0.356 mg/Kg ☼08/16/23 15:09 08/17/23 03:56 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.15 0.252 mg/Kg 08/16/23 15:09 08/17/23 03:56 1☼15.5Lead General Chemistry RL MDL 83.3 0.01 0.01 %08/15/23 17:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %08/15/23 17:12 116.7Percent Moisture (EPA Moisture) Eurofins Pensacola Page 27 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-8Client Sample ID: H.O. BE1 (17) Matrix: SolidDate Collected: 08/01/23 13:50 Percent Solids: 85.4Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS RL MDL 0.00100 U 0.00455 0.00100 mg/Kg ☼08/14/23 08:59 08/14/23 19:53 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1,1,1,2-Tetrachloroethane 0.00455 0.00100 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00100 U1,1,1-Trichloroethane 0.00455 0.000746 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000746 U1,1,2,2-Tetrachloroethane 0.00455 0.000710 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000710 U1,1,2-Trichloroethane 0.00455 0.000755 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000755 U1,1-Dichloroethane 0.00455 0.000774 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000774 U1,1-Dichloroethene 0.00455 0.000755 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000755 U1,1-Dichloropropene 0.00455 0.00100 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00100 U1,2,3-Trichlorobenzene 0.00455 0.000728 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000728 U1,2,3-Trichloropropane 0.00455 0.000837 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000837 U1,2,4-Trichlorobenzene 0.00455 0.000910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000910 U1,2,4-Trimethylbenzene 0.00455 0.000910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000910 U1,2-Dibromoethane 0.00455 0.000646 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000646 U1,2-Dichlorobenzene 0.00455 0.000746 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000746 U1,2-Dichloroethane 0.00455 0.000692 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000692 U1,2-Dichloropropane 0.00455 0.000755 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000755 U1,3,5-Trimethylbenzene 0.00455 0.000865 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000865 U1,3-Dichlorobenzene 0.00455 0.000910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000910 U1,3-Dichloropropane 0.00455 0.000783 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000783 U1,4-Dichlorobenzene 0.00455 0.00100 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00100 U2,2-Dichloropropane 0.0228 0.00546 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00546 U2-Butanone (MEK) 0.00455 0.000737 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000737 U2-Chlorotoluene 0.0228 0.00455 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00455 U2-Hexanone 0.00455 0.000892 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000892 U4-Chlorotoluene 0.00455 0.000910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000910 U4-Isopropyltoluene 0.0228 0.00455 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00455 U4-Methyl-2-pentanone (MIBK) 0.0228 0.0109 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.0320Acetone 0.00455 0.000610 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000610 UBenzene 0.00455 0.00118 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00118 UBromobenzene 0.00455 0.000737 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000737 UBromochloromethane 0.00455 0.000837 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000837 UBromodichloromethane 0.00455 0.00118 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00118 UBromoform 0.00455 0.00228 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00228 UBromomethane 0.00455 0.00155 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00155 UCarbon tetrachloride 0.00455 0.000473 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000473 UChlorobenzene 0.00455 0.00109 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00109 UChloroethane 0.00455 0.00455 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00455 UChloroform 0.00455 0.000910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000910 UChloromethane 0.00455 0.000692 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000692 Ucis-1,2-Dichloroethene 0.00455 0.00109 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00109 Ucis-1,3-Dichloropropene 0.00455 0.00109 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00109 UDibromochloromethane 0.00455 0.00118 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00118 UDichlorodifluoromethane 0.0910 0.0673 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.0860 JEthanol 0.00455 0.000555 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000555 UEthylbenzene 0.00455 0.000501 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000501 UIsopropyl ether 0.00455 0.000619 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000619 UIsopropylbenzene 0.00455 0.000910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000910 UMethyl tert-butyl ether 0.0137 0.00910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00910 UMethylene Chloride 0.00455 0.00273 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00273 UNaphthalene Eurofins Pensacola Page 28 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-8Client Sample ID: H.O. BE1 (17) Matrix: SolidDate Collected: 08/01/23 13:50 Percent Solids: 85.4Date Received: 08/10/23 09:49 Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued) RL MDL 0.000874 U 0.00455 0.000874 mg/Kg ☼08/14/23 08:59 08/14/23 19:53 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier n-Butylbenzene 0.00455 0.000819 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000819 UN-Propylbenzene 0.00455 0.000865 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000865 Usec-Butylbenzene 0.00455 0.000910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000910 UStyrene 0.00455 0.00100 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00100 Utert-Butylbenzene 0.00455 0.00273 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00273 UTetrachloroethene 0.00455 0.000910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00188 JToluene 0.00455 0.000874 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000874 Utrans-1,2-Dichloroethene 0.00455 0.00100 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00100 Utrans-1,3-Dichloropropene 0.00455 0.000910 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000910 UTrichloroethene 0.00455 0.000783 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000783 UTrichlorofluoromethane 0.0228 0.00173 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00173 UVinyl acetate 0.00455 0.000728 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.000728 UVinyl chloride 0.00910 0.00173 mg/Kg 08/14/23 08:59 08/14/23 19:53 1☼0.00173 UXylenes, Total 4-Bromofluorobenzene 108 67-130 08/14/23 08:59 08/14/23 19:53 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane 102 08/14/23 08:59 08/14/23 19:53 177-127 Toluene-d8 (Surr)101 08/14/23 08:59 08/14/23 19:53 176-127 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) RL MDL 0.186 U 1.86 0.186 mg/Kg ☼08/14/23 08:30 08/16/23 22:12 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 1-Methylnaphthalene 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U2,4,5-Trichlorophenol 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U2,4,6-Trichlorophenol 1.86 0.394 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.394 U2,4-Dichlorophenol 1.86 0.530 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.530 U2,4-Dimethylphenol 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U2,4-Dinitrotoluene 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U2,6-Dinitrotoluene 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U2-Chloronaphthalene 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U2-Chlorophenol 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U2-Methylnaphthalene 1.86 0.451 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.451 U2-Methylphenol 1.86 0.394 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.394 U2-Nitroaniline 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U2-Nitrophenol 3.72 0.434 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.434 U3 & 4 Methylphenol 1.86 0.439 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.439 U3-Nitroaniline 1.86 1.35 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼1.35 U4,6-Dinitro-2-methylphenol 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U4-Bromophenyl phenyl ether 1.86 0.456 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.456 U4-Chloro-3-methylphenol 1.86 0.456 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.456 U4-Chloroaniline 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 U4-Chlorophenyl phenyl ether 1.86 0.637 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.637 U4-Nitroaniline 1.86 1.69 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼1.69 U4-Nitrophenol 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UAcenaphthene 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UAcenaphthylene 1.86 0.552 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.552 UAniline 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UAnthracene 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UBenzo[a]anthracene 1.86 0.265 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.265 UBenzo[a]pyrene Eurofins Pensacola Page 29 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-8Client Sample ID: H.O. BE1 (17) Matrix: SolidDate Collected: 08/01/23 13:50 Percent Solids: 85.4Date Received: 08/10/23 09:49 Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL 0.558 U 1.86 0.558 mg/Kg ☼08/14/23 08:30 08/16/23 22:12 5 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzo[b]fluoranthene 1.86 0.620 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.620 UBenzo[g,h,i]perylene 1.86 0.439 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.439 UBenzo[k]fluoranthene 5.58 1.97 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼1.97 UBenzoic acid 1.86 0.710 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.710 Ubis (2-chloroisopropyl) ether 1.86 0.411 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.411 UBis(2-chloroethoxy)methane 1.86 0.259 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.259 UBis(2-chloroethyl)ether 1.86 0.456 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.456 UBis(2-ethylhexyl) phthalate 1.86 0.400 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.400 UButyl benzyl phthalate 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UChrysene 1.86 0.321 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.321 UDibenz(a,h)anthracene 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UDibenzofuran 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UDiethyl phthalate 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UDimethyl phthalate 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UDi-n-butyl phthalate 1.86 0.676 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.676 UDi-n-octyl phthalate 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.198 JFluoranthene 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UFluorene 1.86 0.563 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.563 UHexachlorobenzene 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UHexachlorobutadiene 1.86 0.372 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.372 UHexachlorocyclopentadiene 1.86 0.394 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.394 UHexachloroethane 1.86 0.372 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.372 UIndeno[1,2,3-cd]pyrene 1.86 0.377 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.377 UIsophorone 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UNitrobenzene 1.86 0.591 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.591 UN-Nitrosodi-n-propylamine 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼2.68N-Nitrosodiphenylamine 3.72 0.901 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.901 UPentachlorophenol 1.86 0.186 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.186 UPhenanthrene 1.86 0.501 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.501 UPhenol 1.86 0.439 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼1.14 JPyrene 1.86 0.845 mg/Kg 08/14/23 08:30 08/16/23 22:12 5☼0.845 UPyridine 2,4,6-Tribromophenol (Surr)218 S1+10-150 08/14/23 08:30 08/16/23 22:12 5 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorobiphenyl 81 08/14/23 08:30 08/16/23 22:12 527-127 2-Fluorophenol (Surr)43 08/14/23 08:30 08/16/23 22:12 525-128 Nitrobenzene-d5 (Surr)43 08/14/23 08:30 08/16/23 22:12 515-136 Phenol-d5 (Surr)63 08/14/23 08:30 08/16/23 22:12 529-130 Terphenyl-d14 (Surr)108 08/14/23 08:30 08/16/23 22:12 524-146 Method: MA DEP MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) RL MDL 3.06 U 3.06 3.06 mg/Kg ☼08/14/23 09:50 08/14/23 16:32 50 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C5-C8 Aliphatics 1.59 1.59 mg/Kg 08/14/23 09:50 08/14/23 16:32 50☼1.59 UC9-C12 Aliphatics 0.850 0.850 mg/Kg 08/14/23 09:50 08/14/23 16:32 50☼0.850 UC9-C10 Aromatics a,a,a-Trifluorotoluene (fid)110 70-130 08/14/23 09:50 08/14/23 16:32 50 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery a,a,a-Trifluorotoluene (pid)109 08/14/23 09:50 08/14/23 16:32 5070-130 Eurofins Pensacola Page 30 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Lab Sample ID: 400-241823-8Client Sample ID: H.O. BE1 (17) Matrix: SolidDate Collected: 08/01/23 13:50 Percent Solids: 85.4Date Received: 08/10/23 09:49 Method: MA DEP MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) RL MDL 3450 36.8 36.8 mg/Kg ☼08/14/23 13:55 08/24/23 23:41 20 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier C9-C18 Aliphatics 36.8 36.8 mg/Kg 08/14/23 13:55 08/24/23 23:41 20☼1610C19-C36 Aliphatics 3.45 3.45 mg/Kg 08/14/23 13:55 08/18/23 05:03 1☼1550C11-C22 Aromatics 1-Chlorooctadecane 278 S1+40-140 08/14/23 13:55 08/24/23 23:41 20 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery o-Terphenyl 68 08/14/23 13:55 08/18/23 05:03 140-140 2-Fluorobiphenyl 222 S1+08/14/23 13:55 08/18/23 05:03 140-140 2-Bromonaphthalene 74 08/14/23 13:55 08/18/23 05:03 140-140 Method: SW846 6010D - Metals (ICP) RL MDL 4.27 1.15 0.358 mg/Kg ☼08/16/23 15:09 08/17/23 03:59 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Chromium 1.15 0.254 mg/Kg 08/16/23 15:09 08/17/23 03:59 1☼9.91Lead General Chemistry RL MDL 85.4 0.01 0.01 %08/15/23 17:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Percent Solids (EPA Moisture) 0.01 0.01 %08/15/23 17:12 114.6Percent Moisture (EPA Moisture) Eurofins Pensacola Page 31 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Qualifiers GC/MS VOA Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Qualifier U Indicates the analyte was analyzed for but not detected. GC/MS Semi VOA Qualifier Description B Compound was found in the blank and sample. Qualifier J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. S1+Surrogate recovery exceeds control limits, high biased. U Indicates the analyte was analyzed for but not detected. GC VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier GC Semi VOA Qualifier Description F1 MS and/or MSD recovery exceeds control limits. Qualifier S1+Surrogate recovery exceeds control limits, high biased. U Indicates the analyte was analyzed for but not detected. Metals Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) Eurofins Pensacola Page 32 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Glossary (Continued) These commonly used abbreviations may or may not be present in this report. RPD Relative Percent Difference, a measure of the relative difference between two points Abbreviation TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Pensacola Page 33 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8260D - Volatile Organic Compounds by GC/MS Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (67-130)(77-127)(76-127) BFB DBFM TOL 103 99 105400-241823-4 Percent Surrogate Recovery (Acceptance Limits) W.O. SW1 (12) 108 103 101400-241823-5 W.O. SW2 (12) 109 104 101400-241823-6 W.O. SW3 (12) 107 99 100400-241823-7 H.O. BE2 (17) 108 102 101400-241823-8 H.O. BE1 (17) 108 102 103LCS 400-636938/1-A Lab Control Sample 98 98 103LCS 400-637089/1-A Lab Control Sample 105 104 101MB 400-636938/2-A Method Blank 101 101 105MB 400-637089/2-A Method Blank Surrogate Legend BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane TOL = Toluene-d8 (Surr) Method: 8270E - Semivolatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (10-150)(27-127)(25-128)(15-136)(29-130)(24-146) TBP FBP 2FP NBZ PHL TPHL 89 70 76 63 69 88400-241823-4 Percent Surrogate Recovery (Acceptance Limits) W.O. SW1 (12) 85 68 72 6663 92400-241823-5 W.O. SW2 (12) 86 66 72 6560 87400-241823-6 W.O. SW3 (12) 86 70 68 6862 93400-241823-7 H.O. BE2 (17) 218 S1+81 43 6343 108400-241823-8 H.O. BE1 (17) 104 73 67 7282 81LCS 400-636852/2-A Lab Control Sample 71 80 84 7271 98MB 400-636852/1-A Method Blank Surrogate Legend TBP = 2,4,6-Tribromophenol (Surr) FBP = 2-Fluorobiphenyl 2FP = 2-Fluorophenol (Surr) NBZ = Nitrobenzene-d5 (Surr) PHL = Phenol-d5 (Surr) TPHL = Terphenyl-d14 (Surr) Method: 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (27-127)(15-136)(24-146) FBP NBZ TPHL 119 103 166 S1+400-241823-1 Percent Surrogate Recovery (Acceptance Limits) W.O. CS1 (17) 105 84 146400-241823-2 W.O. CS2 (17) 97 82 134400-241823-3 W.O. CS3 (17) 111 83 148 S1+LCS 400-636852/18-A Lab Control Sample 103 82 141LCSD 400-636852/19-A Lab Control Sample Dup 119 89 174 S1+MB 400-636852/1-A Method Blank Surrogate Legend FBP = 2-Fluorobiphenyl Eurofins Pensacola Page 34 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC NBZ = Nitrobenzene-d5 TPHL = Terphenyl-d14 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (70-130)(70-130) TFT-F1 TFT-P1 110 108400-241823-4 Percent Surrogate Recovery (Acceptance Limits) W.O. SW1 (12) 110 108400-241823-4 MS W.O. SW1 (12) 110 108400-241823-4 MSD W.O. SW1 (12) 110 108400-241823-5 W.O. SW2 (12) 109 107400-241823-6 W.O. SW3 (12) 112 111400-241823-7 H.O. BE2 (17) 110 109400-241823-8 H.O. BE1 (17) 110 108LCS 400-636903/2-A Lab Control Sample 110 108LCSD 400-636903/3-A Lab Control Sample Dup 108 106MB 400-636903/1-A Method Blank Surrogate Legend TFT-F = a,a,a-Trifluorotoluene (fid) TFT-P = a,a,a-Trifluorotoluene (pid) Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (40-140) 1COD1 45400-241823-4 Percent Surrogate Recovery (Acceptance Limits) W.O. SW1 (12) 51400-241823-4 MS W.O. SW1 (12) 54400-241823-4 MSD W.O. SW1 (12) 54400-241823-5 W.O. SW2 (12) 72400-241823-6 W.O. SW3 (12) 75400-241823-7 H.O. BE2 (17) 278 S1+400-241823-8 H.O. BE1 (17) 68LCS 400-636944/2-A Lab Control Sample 63LCSD 400-636944/11-A Lab Control Sample Dup 54MB 400-636944/1-A Method Blank Surrogate Legend 1COD = 1-Chlorooctadecane Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (40-140)(40-140)(40-140) OTPH1 FBP1 2BN1 40 80 75400-241823-4 Percent Surrogate Recovery (Acceptance Limits) W.O. SW1 (12) 41 79 50400-241823-4 MS W.O. SW1 (12) 44 80 53400-241823-4 MSD W.O. SW1 (12) 42 72 68400-241823-5 W.O. SW2 (12) 67 88 84400-241823-6 W.O. SW3 (12) 60 85 80400-241823-7 H.O. BE2 (17) 68 222 S1+74400-241823-8 H.O. BE1 (17) 54 80 53LCS 400-636944/2-A Lab Control Sample Eurofins Pensacola Page 35 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Prep Type: Total/NAMatrix: Solid Lab Sample ID Client Sample ID (40-140)(40-140)(40-140) OTPH1 FBP1 2BN1 52 85 55LCSD 400-636944/11-A Percent Surrogate Recovery (Acceptance Limits) Lab Control Sample Dup 43 82 75MB 400-636944/1-A Method Blank Surrogate Legend OTPH = o-Terphenyl FBP = 2-Fluorobiphenyl 2BN = 2-Bromonaphthalene Eurofins Pensacola Page 36 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC GC/MS VOA Analysis Batch: 636861 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260D 636938400-241823-5 W.O. SW2 (12)Total/NA Solid 8260D 636938400-241823-6 W.O. SW3 (12)Total/NA Solid 8260D 636938400-241823-7 H.O. BE2 (17)Total/NA Solid 8260D 636938400-241823-8 H.O. BE1 (17)Total/NA Solid 8260D 636938MB 400-636938/2-A Method Blank Total/NA Solid 8260D 636938LCS 400-636938/1-A Lab Control Sample Total/NA Prep Batch: 636938 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-241823-5 W.O. SW2 (12)Total/NA Solid 5035400-241823-6 W.O. SW3 (12)Total/NA Solid 5035400-241823-7 H.O. BE2 (17)Total/NA Solid 5035400-241823-8 H.O. BE1 (17)Total/NA Solid 5035MB 400-636938/2-A Method Blank Total/NA Solid 5035LCS 400-636938/1-A Lab Control Sample Total/NA Prep Batch: 637089 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-241823-4 W.O. SW1 (12)Total/NA Solid 5035MB 400-637089/2-A Method Blank Total/NA Solid 5035LCS 400-637089/1-A Lab Control Sample Total/NA Analysis Batch: 637090 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260D 637089400-241823-4 W.O. SW1 (12)Total/NA Solid 8260D 637089MB 400-637089/2-A Method Blank Total/NA Solid 8260D 637089LCS 400-637089/1-A Lab Control Sample Total/NA GC/MS Semi VOA Prep Batch: 636852 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-241823-1 W.O. CS1 (17)Total/NA Solid 3546400-241823-2 W.O. CS2 (17)Total/NA Solid 3546400-241823-3 W.O. CS3 (17)Total/NA Solid 3546400-241823-4 W.O. SW1 (12)Total/NA Solid 3546400-241823-5 W.O. SW2 (12)Total/NA Solid 3546400-241823-6 W.O. SW3 (12)Total/NA Solid 3546400-241823-7 H.O. BE2 (17)Total/NA Solid 3546400-241823-8 H.O. BE1 (17)Total/NA Solid 3546MB 400-636852/1-A Method Blank Total/NA Solid 3546LCS 400-636852/18-A Lab Control Sample Total/NA Solid 3546LCS 400-636852/2-A Lab Control Sample Total/NA Solid 3546LCSD 400-636852/19-A Lab Control Sample Dup Total/NA Analysis Batch: 637034 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 636852400-241823-4 W.O. SW1 (12)Total/NA Solid 8270E 636852400-241823-5 W.O. SW2 (12)Total/NA Solid 8270E 636852400-241823-6 W.O. SW3 (12)Total/NA Solid 8270E 636852400-241823-7 H.O. BE2 (17)Total/NA Eurofins Pensacola Page 37 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC GC/MS Semi VOA (Continued) Analysis Batch: 637034 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 636852MB 400-636852/1-A Method Blank Total/NA Solid 8270E 636852LCS 400-636852/2-A Lab Control Sample Total/NA Analysis Batch: 637166 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E 636852400-241823-8 H.O. BE1 (17)Total/NA Analysis Batch: 637317 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270E SIM 636852400-241823-1 W.O. CS1 (17)Total/NA Solid 8270E SIM 636852400-241823-2 W.O. CS2 (17)Total/NA Solid 8270E SIM 636852400-241823-3 W.O. CS3 (17)Total/NA Solid 8270E SIM 636852MB 400-636852/1-A Method Blank Total/NA Solid 8270E SIM 636852LCS 400-636852/18-A Lab Control Sample Total/NA Solid 8270E SIM 636852LCSD 400-636852/19-A Lab Control Sample Dup Total/NA GC VOA Analysis Batch: 636880 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MAVPH 636903400-241823-4 W.O. SW1 (12)Total/NA Solid MAVPH 636903400-241823-5 W.O. SW2 (12)Total/NA Solid MAVPH 636903400-241823-6 W.O. SW3 (12)Total/NA Solid MAVPH 636903400-241823-7 H.O. BE2 (17)Total/NA Solid MAVPH 636903400-241823-8 H.O. BE1 (17)Total/NA Solid MAVPH 636903MB 400-636903/1-A Method Blank Total/NA Solid MAVPH 636903LCS 400-636903/2-A Lab Control Sample Total/NA Solid MAVPH 636903LCSD 400-636903/3-A Lab Control Sample Dup Total/NA Solid MAVPH 636903400-241823-4 MS W.O. SW1 (12)Total/NA Solid MAVPH 636903400-241823-4 MSD W.O. SW1 (12)Total/NA Prep Batch: 636903 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035400-241823-4 W.O. SW1 (12)Total/NA Solid 5035400-241823-5 W.O. SW2 (12)Total/NA Solid 5035400-241823-6 W.O. SW3 (12)Total/NA Solid 5035400-241823-7 H.O. BE2 (17)Total/NA Solid 5035400-241823-8 H.O. BE1 (17)Total/NA Solid 5035MB 400-636903/1-A Method Blank Total/NA Solid 5035LCS 400-636903/2-A Lab Control Sample Total/NA Solid 5035LCSD 400-636903/3-A Lab Control Sample Dup Total/NA Solid 5035400-241823-4 MS W.O. SW1 (12)Total/NA Solid 5035400-241823-4 MSD W.O. SW1 (12)Total/NA GC Semi VOA Prep Batch: 636944 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-241823-4 W.O. SW1 (12)Total/NA Solid 3546400-241823-5 W.O. SW2 (12)Total/NA Solid 3546400-241823-6 W.O. SW3 (12)Total/NA Solid 3546400-241823-7 H.O. BE2 (17)Total/NA Eurofins Pensacola Page 38 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC GC Semi VOA (Continued) Prep Batch: 636944 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3546400-241823-8 H.O. BE1 (17)Total/NA Solid 3546MB 400-636944/1-A Method Blank Total/NA Solid 3546LCS 400-636944/2-A Lab Control Sample Total/NA Solid 3546LCSD 400-636944/11-A Lab Control Sample Dup Total/NA Solid 3546400-241823-4 MS W.O. SW1 (12)Total/NA Solid 3546400-241823-4 MSD W.O. SW1 (12)Total/NA Analysis Batch: 637448 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 636944400-241823-4 W.O. SW1 (12)Total/NA Solid MA-EPH 636944400-241823-5 W.O. SW2 (12)Total/NA Solid MA-EPH 636944400-241823-6 W.O. SW3 (12)Total/NA Solid MA-EPH 636944400-241823-7 H.O. BE2 (17)Total/NA Solid MA-EPH 636944MB 400-636944/1-A Method Blank Total/NA Solid MA-EPH 636944LCS 400-636944/2-A Lab Control Sample Total/NA Solid MA-EPH 636944LCSD 400-636944/11-A Lab Control Sample Dup Total/NA Solid MA-EPH 636944400-241823-4 MS W.O. SW1 (12)Total/NA Solid MA-EPH 636944400-241823-4 MSD W.O. SW1 (12)Total/NA Analysis Batch: 637452 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 636944400-241823-4 W.O. SW1 (12)Total/NA Solid MA-EPH 636944400-241823-5 W.O. SW2 (12)Total/NA Solid MA-EPH 636944400-241823-6 W.O. SW3 (12)Total/NA Solid MA-EPH 636944400-241823-7 H.O. BE2 (17)Total/NA Solid MA-EPH 636944400-241823-8 H.O. BE1 (17)Total/NA Solid MA-EPH 636944MB 400-636944/1-A Method Blank Total/NA Solid MA-EPH 636944LCS 400-636944/2-A Lab Control Sample Total/NA Solid MA-EPH 636944LCSD 400-636944/11-A Lab Control Sample Dup Total/NA Solid MA-EPH 636944400-241823-4 MS W.O. SW1 (12)Total/NA Solid MA-EPH 636944400-241823-4 MSD W.O. SW1 (12)Total/NA Analysis Batch: 638211 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid MA-EPH 636944400-241823-8 H.O. BE1 (17)Total/NA Metals Prep Batch: 637246 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3050B400-241823-1 W.O. CS1 (17)Total/NA Solid 3050B400-241823-2 W.O. CS2 (17)Total/NA Solid 3050B400-241823-3 W.O. CS3 (17)Total/NA Solid 3050B400-241823-4 W.O. SW1 (12)Total/NA Solid 3050B400-241823-5 W.O. SW2 (12)Total/NA Solid 3050B400-241823-6 W.O. SW3 (12)Total/NA Solid 3050B400-241823-7 H.O. BE2 (17)Total/NA Solid 3050B400-241823-8 H.O. BE1 (17)Total/NA Solid 3050BMB 400-637246/1-A Method Blank Total/NA Solid 3050BLCS 400-637246/2-A Lab Control Sample Total/NA Eurofins Pensacola Page 39 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Metals Analysis Batch: 637311 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010D 637246400-241823-1 W.O. CS1 (17)Total/NA Solid 6010D 637246400-241823-2 W.O. CS2 (17)Total/NA Solid 6010D 637246400-241823-3 W.O. CS3 (17)Total/NA Solid 6010D 637246400-241823-4 W.O. SW1 (12)Total/NA Solid 6010D 637246400-241823-5 W.O. SW2 (12)Total/NA Solid 6010D 637246400-241823-6 W.O. SW3 (12)Total/NA Solid 6010D 637246400-241823-7 H.O. BE2 (17)Total/NA Solid 6010D 637246400-241823-8 H.O. BE1 (17)Total/NA Solid 6010D 637246MB 400-637246/1-A Method Blank Total/NA Solid 6010D 637246LCS 400-637246/2-A Lab Control Sample Total/NA General Chemistry Analysis Batch: 637224 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture400-241823-1 W.O. CS1 (17)Total/NA Solid Moisture400-241823-2 W.O. CS2 (17)Total/NA Solid Moisture400-241823-3 W.O. CS3 (17)Total/NA Solid Moisture400-241823-4 W.O. SW1 (12)Total/NA Solid Moisture400-241823-5 W.O. SW2 (12)Total/NA Solid Moisture400-241823-6 W.O. SW3 (12)Total/NA Solid Moisture400-241823-7 H.O. BE2 (17)Total/NA Solid Moisture400-241823-8 H.O. BE1 (17)Total/NA Solid Moisture400-241823-2 DU W.O. CS2 (17)Total/NA Eurofins Pensacola Page 40 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8260D - Volatile Organic Compounds by GC/MS Client Sample ID: Method BlankLab Sample ID: MB 400-636938/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 636861 Prep Batch: 636938 RL MDL 1,1,1,2-Tetrachloroethane 0.00110 U 0.00500 0.00110 mg/Kg 08/14/23 08:59 08/14/23 11:47 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 0.00110 U 0.001100.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,1,1-Trichloroethane 0.000820 U 0.0008200.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,1,2,2-Tetrachloroethane 0.000780 U 0.0007800.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,1,2-Trichloroethane 0.000830 U 0.0008300.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,1-Dichloroethane 0.000850 U 0.0008500.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,1-Dichloroethene 0.000830 U 0.0008300.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,1-Dichloropropene 0.00110 U 0.001100.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,2,3-Trichlorobenzene 0.000800 U 0.0008000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,2,3-Trichloropropane 0.000710 U 0.0007100.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,2-Dichlorobenzene 0.000820 U 0.0008200.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,2-Dichloroethane 0.000760 U 0.0007600.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,2-Dichloropropane 0.000830 U 0.0008300.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,3,5-Trimethylbenzene 0.000950 U 0.0009500.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,3-Dichlorobenzene 0.00100 U 0.001000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,3-Dichloropropane 0.000860 U 0.0008600.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,4-Dichlorobenzene 0.00110 U 0.001100.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 12,2-Dichloropropane 0.000810 U 0.0008100.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 12-Chlorotoluene 0.00500 U 0.005000.0250 mg/Kg 08/14/23 08:59 08/14/23 11:47 12-Hexanone 0.000980 U 0.0009800.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 14-Chlorotoluene 0.0120 U 0.01200.0250 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Acetone 0.000670 U 0.0006700.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Benzene 0.00130 U 0.001300.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Bromobenzene 0.000810 U 0.0008100.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Bromochloromethane 0.00130 U 0.001300.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Bromoform 0.00250 U 0.002500.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Bromomethane 0.00170 U 0.001700.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Carbon tetrachloride 0.000520 U 0.0005200.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Chlorobenzene 0.000920 U 0.0009200.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Bromodichloromethane 0.00120 U 0.001200.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Chloroethane 0.00500 U 0.005000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Chloroform 0.00100 U 0.001000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Chloromethane 0.00100 U 0.001000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,2-Dibromoethane 0.000760 U 0.0007600.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1cis-1,2-Dichloroethene 0.00120 U 0.001200.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1cis-1,3-Dichloropropene 0.00120 U 0.001200.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Dibromochloromethane 0.00130 U 0.001300.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Dichlorodifluoromethane 0.00600 U 0.006000.0250 mg/Kg 08/14/23 08:59 08/14/23 11:47 12-Butanone (MEK) 0.00500 U 0.005000.0250 mg/Kg 08/14/23 08:59 08/14/23 11:47 14-Methyl-2-pentanone (MIBK) 0.000610 U 0.0006100.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Ethylbenzene 0.000550 U 0.0005500.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Isopropyl ether 0.000680 U 0.0006800.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Isopropylbenzene 0.00100 U 0.001000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Methyl tert-butyl ether 0.0100 U 0.01000.0150 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Methylene Chloride 0.00300 U 0.003000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Naphthalene 0.000960 U 0.0009600.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1n-Butylbenzene 0.000900 U 0.0009000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1N-Propylbenzene 0.000950 U 0.0009500.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1sec-Butylbenzene Eurofins Pensacola Page 41 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-636938/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 636861 Prep Batch: 636938 RL MDL Styrene 0.00100 U 0.00500 0.00100 mg/Kg 08/14/23 08:59 08/14/23 11:47 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 0.00110 U 0.001100.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1tert-Butylbenzene 0.00300 U 0.003000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Tetrachloroethene 0.00100 U 0.001000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Toluene 0.000960 U 0.0009600.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1trans-1,2-Dichloroethene 0.00110 U 0.001100.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1trans-1,3-Dichloropropene 0.00100 U 0.001000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Trichloroethene 0.00100 U 0.001000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 14-Isopropyltoluene 0.000860 U 0.0008600.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Trichlorofluoromethane 0.0740 U 0.07400.100 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Ethanol 0.00190 U 0.001900.0250 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Vinyl acetate 0.00100 U 0.001000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,2,4-Trimethylbenzene 0.000800 U 0.0008000.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Vinyl chloride 0.000920 U 0.0009200.00500 mg/Kg 08/14/23 08:59 08/14/23 11:47 11,2,4-Trichlorobenzene 0.00190 U 0.001900.0100 mg/Kg 08/14/23 08:59 08/14/23 11:47 1Xylenes, Total 4-Bromofluorobenzene 105 67-130 08/14/23 11:47 1 MB MB Surrogate 08/14/23 08:59 Dil FacPreparedAnalyzedQualifierLimits%Recovery 104 08/14/23 08:59 08/14/23 11:47 1Dibromofluoromethane77-127 101 08/14/23 08:59 08/14/23 11:47 1Toluene-d8 (Surr)76-127 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-636938/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 636861 Prep Batch: 636938 1,1,1,2-Tetrachloroethane 0.0500 0.05314 mg/Kg 106 65-130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,1,1-Trichloroethane 0.0500 0.05585 mg/Kg 112 63-130 1,1,2,2-Tetrachloroethane 0.0500 0.05488 mg/Kg 110 60-131 1,1,2-Trichloroethane 0.0500 0.05573 mg/Kg 111 65-130 1,1-Dichloroethane 0.0500 0.05948 mg/Kg 119 59-130 1,1-Dichloroethene 0.0500 0.04063 mg/Kg 81 55-137 1,1-Dichloropropene 0.0500 0.05692 mg/Kg 114 65-130 1,2,3-Trichlorobenzene 0.0500 0.05160 mg/Kg 103 58-135 1,2,3-Trichloropropane 0.0500 0.05529 mg/Kg 111 60-130 1,2-Dichlorobenzene 0.0500 0.05072 mg/Kg 101 64-130 1,2-Dichloroethane 0.0500 0.05852 mg/Kg 117 62-130 1,2-Dichloropropane 0.0500 0.05784 mg/Kg 116 64-130 1,3,5-Trimethylbenzene 0.0500 0.05261 mg/Kg 105 67-130 1,3-Dichlorobenzene 0.0500 0.05213 mg/Kg 104 66-130 1,3-Dichloropropane 0.0500 0.05691 mg/Kg 114 67-130 1,4-Dichlorobenzene 0.0500 0.05138 mg/Kg 103 65-130 2,2-Dichloropropane 0.0500 0.05860 mg/Kg 117 51-132 2-Chlorotoluene 0.0500 0.05312 mg/Kg 106 67-130 2-Hexanone 0.200 0.2578 mg/Kg 129 57-131 4-Chlorotoluene 0.0500 0.05514 mg/Kg 110 66-130 Acetone 0.200 0.1862 mg/Kg 93 48-160 Benzene 0.0500 0.05491 mg/Kg 110 65-130 Eurofins Pensacola Page 42 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-636938/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 636861 Prep Batch: 636938 Bromobenzene 0.0500 0.05246 mg/Kg 105 65-130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Bromochloromethane 0.0500 0.05039 mg/Kg 101 65-130 Bromoform 0.0500 0.05274 mg/Kg 105 52-136 Bromomethane 0.0500 0.02655 mg/Kg 53 12-160 Carbon tetrachloride 0.0500 0.05522 mg/Kg 110 60-130 Chlorobenzene 0.0500 0.05320 mg/Kg 106 70-130 Bromodichloromethane 0.0500 0.05525 mg/Kg 111 61-130 Chloroethane 0.0500 0.04732 mg/Kg 95 55-134 Chloroform 0.0500 0.05601 mg/Kg 112 62-130 Chloromethane 0.0500 0.04739 mg/Kg 95 49-136 1,2-Dibromoethane 0.0500 0.05460 mg/Kg 109 67-130 cis-1,2-Dichloroethene 0.0500 0.06081 mg/Kg 122 53-135 cis-1,3-Dichloropropene 0.0500 0.05511 mg/Kg 110 61-130 Dibromochloromethane 0.0500 0.05258 mg/Kg 105 58-132 Dichlorodifluoromethane 0.0500 0.04050 mg/Kg 81 34-143 2-Butanone (MEK)0.200 0.2245 mg/Kg 112 55-130 4-Methyl-2-pentanone (MIBK)0.200 0.2434 mg/Kg 122 58-130 Ethylbenzene 0.0500 0.05470 mg/Kg 109 70-130 Isopropyl ether 0.0500 0.05714 mg/Kg 114 62-130 Isopropylbenzene 0.0500 0.05296 mg/Kg 106 70-130 Methyl tert-butyl ether 0.0500 0.05329 mg/Kg 107 63-130 Methylene Chloride 0.0500 0.06054 mg/Kg 121 57-132 m-Xylene & p-Xylene 0.0500 0.05434 mg/Kg 109 70-130 Naphthalene 0.0500 0.05350 mg/Kg 107 45-144 n-Butylbenzene 0.0500 0.05297 mg/Kg 106 66-130 N-Propylbenzene 0.0500 0.05378 mg/Kg 108 67-130 o-Xylene 0.0500 0.05315 mg/Kg 106 70-130 sec-Butylbenzene 0.0500 0.05447 mg/Kg 109 67-130 Styrene 0.0500 0.05137 mg/Kg 103 68-130 tert-Butylbenzene 0.0500 0.05448 mg/Kg 109 67-130 Tetrachloroethene 0.0500 0.05651 mg/Kg 113 67-130 Toluene 0.0500 0.05499 mg/Kg 110 70-130 trans-1,2-Dichloroethene 0.0500 0.05515 mg/Kg 110 58-134 trans-1,3-Dichloropropene 0.0500 0.05769 mg/Kg 115 60-130 Trichloroethene 0.0500 0.05331 mg/Kg 107 65-130 4-Isopropyltoluene 0.0500 0.05350 mg/Kg 107 68-130 Trichlorofluoromethane 0.0500 0.04361 mg/Kg 87 61-136 Ethanol 2.00 1.684 mg/Kg 84 29-160 Vinyl acetate 0.100 0.1119 mg/Kg 112 24-160 1,2,4-Trimethylbenzene 0.0500 0.05354 mg/Kg 107 66-130 Vinyl chloride 0.0500 0.05014 mg/Kg 100 52-132 1,2,4-Trichlorobenzene 0.0500 0.05150 mg/Kg 103 56-138 Xylenes, Total 0.100 0.1075 mg/Kg 107 70-130 4-Bromofluorobenzene 67 -130 Surrogate 108 LCS LCS Qualifier Limits%Recovery 102Dibromofluoromethane 77 -127 103Toluene-d8 (Surr)76 -127 Eurofins Pensacola Page 43 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-637089/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637090 Prep Batch: 637089 RL MDL 1,1,1,2-Tetrachloroethane 0.00110 U 0.00500 0.00110 mg/Kg 08/15/23 09:46 08/15/23 11:33 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 0.00110 U 0.001100.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,1,1-Trichloroethane 0.000820 U 0.0008200.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,1,2,2-Tetrachloroethane 0.000780 U 0.0007800.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,1,2-Trichloroethane 0.000830 U 0.0008300.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,1-Dichloroethane 0.000850 U 0.0008500.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,1-Dichloroethene 0.000830 U 0.0008300.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,1-Dichloropropene 0.00110 U 0.001100.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,2,3-Trichlorobenzene 0.000800 U 0.0008000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,2,3-Trichloropropane 0.000710 U 0.0007100.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,2-Dichlorobenzene 0.000820 U 0.0008200.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,2-Dichloroethane 0.000760 U 0.0007600.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,2-Dichloropropane 0.000830 U 0.0008300.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,3,5-Trimethylbenzene 0.000950 U 0.0009500.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,3-Dichlorobenzene 0.00100 U 0.001000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,3-Dichloropropane 0.000860 U 0.0008600.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,4-Dichlorobenzene 0.00110 U 0.001100.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 12,2-Dichloropropane 0.000810 U 0.0008100.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 12-Chlorotoluene 0.00500 U 0.005000.0250 mg/Kg 08/15/23 09:46 08/15/23 11:33 12-Hexanone 0.000980 U 0.0009800.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 14-Chlorotoluene 0.0120 U 0.01200.0250 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Acetone 0.000670 U 0.0006700.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Benzene 0.00130 U 0.001300.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Bromobenzene 0.000810 U 0.0008100.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Bromochloromethane 0.00130 U 0.001300.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Bromoform 0.00250 U 0.002500.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Bromomethane 0.00170 U 0.001700.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Carbon tetrachloride 0.000520 U 0.0005200.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Chlorobenzene 0.000920 U 0.0009200.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Bromodichloromethane 0.00120 U 0.001200.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Chloroethane 0.00500 U 0.005000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Chloroform 0.00100 U 0.001000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Chloromethane 0.00100 U 0.001000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,2-Dibromoethane 0.000760 U 0.0007600.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1cis-1,2-Dichloroethene 0.00120 U 0.001200.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1cis-1,3-Dichloropropene 0.00120 U 0.001200.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Dibromochloromethane 0.00130 U 0.001300.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Dichlorodifluoromethane 0.00600 U 0.006000.0250 mg/Kg 08/15/23 09:46 08/15/23 11:33 12-Butanone (MEK) 0.00500 U 0.005000.0250 mg/Kg 08/15/23 09:46 08/15/23 11:33 14-Methyl-2-pentanone (MIBK) 0.000610 U 0.0006100.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Ethylbenzene 0.000550 U 0.0005500.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Isopropyl ether 0.000680 U 0.0006800.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Isopropylbenzene 0.00100 U 0.001000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Methyl tert-butyl ether 0.0100 U 0.01000.0150 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Methylene Chloride 0.00300 U 0.003000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Naphthalene 0.000960 U 0.0009600.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1n-Butylbenzene 0.000900 U 0.0009000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1N-Propylbenzene 0.000950 U 0.0009500.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1sec-Butylbenzene Eurofins Pensacola Page 44 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-637089/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637090 Prep Batch: 637089 RL MDL Styrene 0.00100 U 0.00500 0.00100 mg/Kg 08/15/23 09:46 08/15/23 11:33 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 0.00110 U 0.001100.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1tert-Butylbenzene 0.00300 U 0.003000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Tetrachloroethene 0.00100 U 0.001000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Toluene 0.000960 U 0.0009600.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1trans-1,2-Dichloroethene 0.00110 U 0.001100.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1trans-1,3-Dichloropropene 0.00100 U 0.001000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Trichloroethene 0.00100 U 0.001000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 14-Isopropyltoluene 0.000860 U 0.0008600.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Trichlorofluoromethane 0.0740 U 0.07400.100 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Ethanol 0.00190 U 0.001900.0250 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Vinyl acetate 0.00100 U 0.001000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,2,4-Trimethylbenzene 0.000800 U 0.0008000.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Vinyl chloride 0.000920 U 0.0009200.00500 mg/Kg 08/15/23 09:46 08/15/23 11:33 11,2,4-Trichlorobenzene 0.00190 U 0.001900.0100 mg/Kg 08/15/23 09:46 08/15/23 11:33 1Xylenes, Total 4-Bromofluorobenzene 101 67-130 08/15/23 11:33 1 MB MB Surrogate 08/15/23 09:46 Dil FacPreparedAnalyzedQualifierLimits%Recovery 101 08/15/23 09:46 08/15/23 11:33 1Dibromofluoromethane77-127 105 08/15/23 09:46 08/15/23 11:33 1Toluene-d8 (Surr)76-127 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-637089/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637090 Prep Batch: 637089 1,1,1,2-Tetrachloroethane 0.0500 0.04726 mg/Kg 95 65-130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 1,1,1-Trichloroethane 0.0500 0.04639 mg/Kg 93 63-130 1,1,2,2-Tetrachloroethane 0.0500 0.03557 mg/Kg 71 60-131 1,1,2-Trichloroethane 0.0500 0.04905 mg/Kg 98 65-130 1,1-Dichloroethane 0.0500 0.04641 mg/Kg 93 59-130 1,1-Dichloroethene 0.0500 0.04344 mg/Kg 87 55-137 1,1-Dichloropropene 0.0500 0.04794 mg/Kg 96 65-130 1,2,3-Trichlorobenzene 0.0500 0.04665 mg/Kg 93 58-135 1,2,3-Trichloropropane 0.0500 0.04902 mg/Kg 98 60-130 1,2-Dichlorobenzene 0.0500 0.04527 mg/Kg 91 64-130 1,2-Dichloroethane 0.0500 0.04998 mg/Kg 100 62-130 1,2-Dichloropropane 0.0500 0.04931 mg/Kg 99 64-130 1,3,5-Trimethylbenzene 0.0500 0.04702 mg/Kg 94 67-130 1,3-Dichlorobenzene 0.0500 0.04550 mg/Kg 91 66-130 1,3-Dichloropropane 0.0500 0.04924 mg/Kg 98 67-130 1,4-Dichlorobenzene 0.0500 0.04556 mg/Kg 91 65-130 2,2-Dichloropropane 0.0500 0.04360 mg/Kg 87 51-132 2-Chlorotoluene 0.0500 0.04774 mg/Kg 95 67-130 2-Hexanone 0.200 0.2190 mg/Kg 110 57-131 4-Chlorotoluene 0.0500 0.04811 mg/Kg 96 66-130 Acetone 0.200 0.2307 mg/Kg 115 48-160 Benzene 0.0500 0.04681 mg/Kg 94 65-130 Eurofins Pensacola Page 45 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8260D - Volatile Organic Compounds by GC/MS (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-637089/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637090 Prep Batch: 637089 Bromobenzene 0.0500 0.04281 mg/Kg 86 65-130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Bromochloromethane 0.0500 0.03905 mg/Kg 78 65-130 Bromoform 0.0500 0.04350 mg/Kg 87 52-136 Bromomethane 0.0500 0.05051 mg/Kg 101 12-160 Carbon tetrachloride 0.0500 0.04694 mg/Kg 94 60-130 Chlorobenzene 0.0500 0.04737 mg/Kg 95 70-130 Bromodichloromethane 0.0500 0.04996 mg/Kg 100 61-130 Chloroethane 0.0500 0.04644 mg/Kg 93 55-134 Chloroform 0.0500 0.04698 mg/Kg 94 62-130 Chloromethane 0.0500 0.04254 mg/Kg 85 49-136 1,2-Dibromoethane 0.0500 0.04804 mg/Kg 96 67-130 cis-1,2-Dichloroethene 0.0500 0.04765 mg/Kg 95 53-135 cis-1,3-Dichloropropene 0.0500 0.04641 mg/Kg 93 61-130 Dibromochloromethane 0.0500 0.04857 mg/Kg 97 58-132 Dichlorodifluoromethane 0.0500 0.03491 mg/Kg 70 34-143 2-Butanone (MEK)0.200 0.2180 mg/Kg 109 55-130 4-Methyl-2-pentanone (MIBK)0.200 0.2246 mg/Kg 112 58-130 Ethylbenzene 0.0500 0.04916 mg/Kg 98 70-130 Isopropyl ether 0.0500 0.04820 mg/Kg 96 62-130 Isopropylbenzene 0.0500 0.05110 mg/Kg 102 70-130 Methyl tert-butyl ether 0.0500 0.04558 mg/Kg 91 63-130 Methylene Chloride 0.0500 0.04394 mg/Kg 88 57-132 m-Xylene & p-Xylene 0.0500 0.04850 mg/Kg 97 70-130 Naphthalene 0.0500 0.05253 mg/Kg 105 45-144 n-Butylbenzene 0.0500 0.05174 mg/Kg 103 66-130 N-Propylbenzene 0.0500 0.04806 mg/Kg 96 67-130 o-Xylene 0.0500 0.04719 mg/Kg 94 70-130 sec-Butylbenzene 0.0500 0.04928 mg/Kg 99 67-130 Styrene 0.0500 0.04591 mg/Kg 92 68-130 tert-Butylbenzene 0.0500 0.04788 mg/Kg 96 67-130 Tetrachloroethene 0.0500 0.06451 mg/Kg 129 67-130 Toluene 0.0500 0.04710 mg/Kg 94 70-130 trans-1,2-Dichloroethene 0.0500 0.04267 mg/Kg 85 58-134 trans-1,3-Dichloropropene 0.0500 0.04739 mg/Kg 95 60-130 Trichloroethene 0.0500 0.05548 mg/Kg 111 65-130 4-Isopropyltoluene 0.0500 0.04817 mg/Kg 96 68-130 Trichlorofluoromethane 0.0500 0.04203 mg/Kg 84 61-136 Ethanol 2.00 1.024 mg/Kg 51 29-160 Vinyl acetate 0.100 0.09916 mg/Kg 99 24-160 1,2,4-Trimethylbenzene 0.0500 0.04659 mg/Kg 93 66-130 Vinyl chloride 0.0500 0.04567 mg/Kg 91 52-132 1,2,4-Trichlorobenzene 0.0500 0.04730 mg/Kg 95 56-138 Xylenes, Total 0.100 0.09569 mg/Kg 96 70-130 4-Bromofluorobenzene 67 -130 Surrogate 98 LCS LCS Qualifier Limits%Recovery 98Dibromofluoromethane 77 -127 103Toluene-d8 (Surr)76 -127 Eurofins Pensacola Page 46 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8270E - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 400-636852/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637034 Prep Batch: 636852 RL MDL 1-Methylnaphthalene 0.0330 U 0.330 0.0330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12,4,5-Trichlorophenol 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12,4,6-Trichlorophenol 0.0700 U 0.07000.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12,4-Dichlorophenol 0.0940 U 0.09400.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12,4-Dimethylphenol 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12,4-Dinitrotoluene 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12,6-Dinitrotoluene 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12-Chloronaphthalene 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12-Chlorophenol 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12-Methylnaphthalene 0.0800 U 0.08000.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12-Methylphenol 0.0700 U 0.07000.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12-Nitroaniline 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 12-Nitrophenol 0.0770 U 0.07700.660 mg/Kg 08/14/23 08:30 08/15/23 16:30 13 & 4 Methylphenol 0.0780 U 0.07800.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 13-Nitroaniline 0.240 U 0.2400.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 14,6-Dinitro-2-methylphenol 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 14-Bromophenyl phenyl ether 0.0810 U 0.08100.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 14-Chloro-3-methylphenol 0.0810 U 0.08100.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 14-Chloroaniline 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 14-Chlorophenyl phenyl ether 0.113 U 0.1130.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 14-Nitroaniline 0.300 U 0.3000.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 14-Nitrophenol 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Acenaphthene 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Acenaphthylene 0.0980 U 0.09800.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Aniline 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Anthracene 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Benzo[a]anthracene 0.0470 U 0.04700.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Benzo[a]pyrene 0.0990 U 0.09900.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Benzo[b]fluoranthene 0.110 U 0.1100.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Benzo[g,h,i]perylene 0.0780 U 0.07800.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Benzo[k]fluoranthene 0.350 U 0.3500.990 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Benzoic acid 0.126 U 0.1260.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1bis (2-chloroisopropyl) ether 0.0730 U 0.07300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Bis(2-chloroethoxy)methane 0.0460 U 0.04600.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Bis(2-chloroethyl)ether 0.0810 U 0.08100.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Bis(2-ethylhexyl) phthalate 0.0710 U 0.07100.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Butyl benzyl phthalate 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Chrysene 0.0570 U 0.05700.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Dibenz(a,h)anthracene 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Dibenzofuran 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Diethyl phthalate 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Dimethyl phthalate 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Di-n-butyl phthalate 0.120 U 0.1200.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Di-n-octyl phthalate 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Fluoranthene 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Fluorene 0.100 U 0.1000.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Hexachlorobenzene 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Hexachlorobutadiene Eurofins Pensacola Page 47 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 400-636852/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637034 Prep Batch: 636852 RL MDL Hexachlorocyclopentadiene 0.0660 U 0.330 0.0660 mg/Kg 08/14/23 08:30 08/15/23 16:30 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 0.0700 U 0.07000.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Hexachloroethane 0.0660 U 0.06600.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Indeno[1,2,3-cd]pyrene 0.0670 U 0.06700.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Isophorone 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Nitrobenzene 0.105 U 0.1050.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1N-Nitrosodi-n-propylamine 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1N-Nitrosodiphenylamine 0.160 U 0.1600.660 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Pentachlorophenol 0.0330 U 0.03300.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Phenanthrene 0.0890 U 0.08900.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Phenol 0.0780 U 0.07800.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Pyrene 0.150 U 0.1500.330 mg/Kg 08/14/23 08:30 08/15/23 16:30 1Pyridine 2,4,6-Tribromophenol (Surr)71 10-150 08/15/23 16:30 1 MB MB Surrogate 08/14/23 08:30 Dil FacPreparedAnalyzedQualifierLimits%Recovery 80 08/14/23 08:30 08/15/23 16:30 12-Fluorobiphenyl 27-127 84 08/14/23 08:30 08/15/23 16:30 12-Fluorophenol (Surr)25-128 71 08/14/23 08:30 08/15/23 16:30 1Nitrobenzene-d5 (Surr)15-136 72 08/14/23 08:30 08/15/23 16:30 1Phenol-d5 (Surr)29-130 98 08/14/23 08:30 08/15/23 16:30 1Terphenyl-d14 (Surr)24-146 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-636852/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637034 Prep Batch: 636852 1-Methylnaphthalene 2.00 1.668 mg/Kg 83 40-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits 2,4,5-Trichlorophenol 2.00 1.674 mg/Kg 84 53-133 2,4,6-Trichlorophenol 2.00 1.645 mg/Kg 82 51-125 2,4-Dichlorophenol 2.00 1.610 mg/Kg 81 56-120 2,4-Dimethylphenol 2.00 1.720 mg/Kg 86 54-120 2,4-Dinitrotoluene 2.00 1.764 mg/Kg 88 59-133 2,6-Dinitrotoluene 2.00 1.728 mg/Kg 86 57-123 2-Chloronaphthalene 2.00 1.603 mg/Kg 80 55-120 2-Chlorophenol 2.00 1.485 mg/Kg 74 52-120 2-Methylnaphthalene 2.00 1.636 mg/Kg 82 40-120 2-Methylphenol 2.00 1.622 mg/Kg 81 51-123 2-Nitroaniline 2.00 1.589 mg/Kg 79 55-129 2-Nitrophenol 2.00 1.622 mg/Kg 81 53-120 3 & 4 Methylphenol 2.00 1.660 mg/Kg 83 47-123 3-Nitroaniline 2.00 1.652 mg/Kg 83 45-120 4,6-Dinitro-2-methylphenol 4.00 2.554 mg/Kg 64 35-135 4-Bromophenyl phenyl ether 2.00 1.728 mg/Kg 86 51-120 4-Chloro-3-methylphenol 2.00 1.594 mg/Kg 80 57-124 4-Chloroaniline 2.00 1.556 mg/Kg 78 34-120 4-Chlorophenyl phenyl ether 2.00 1.873 mg/Kg 94 56-120 4-Nitroaniline 2.00 1.666 mg/Kg 83 52-126 4-Nitrophenol 4.00 3.635 mg/Kg 91 38-133 Eurofins Pensacola Page 48 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-636852/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637034 Prep Batch: 636852 Acenaphthene 2.00 1.748 mg/Kg 87 50-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Acenaphthylene 2.00 1.643 mg/Kg 82 50-120 Aniline 2.00 1.238 mg/Kg 62 36-120 Anthracene 2.00 1.699 mg/Kg 85 52-120 Benzo[a]anthracene 2.00 1.652 mg/Kg 83 55-120 Benzo[a]pyrene 2.00 1.658 mg/Kg 83 54-120 Benzo[b]fluoranthene 2.00 1.646 mg/Kg 82 55-120 Benzo[g,h,i]perylene 2.00 1.808 mg/Kg 90 45-120 Benzo[k]fluoranthene 2.00 1.658 mg/Kg 83 52-120 Benzoic acid 8.69 4.040 mg/Kg 46 10-139 bis (2-chloroisopropyl) ether 2.00 1.319 mg/Kg 66 34-120 Bis(2-chloroethoxy)methane 2.00 1.533 mg/Kg 77 52-120 Bis(2-chloroethyl)ether 2.00 1.403 mg/Kg 70 28-120 Bis(2-ethylhexyl) phthalate 2.00 1.472 mg/Kg 74 58-158 Butyl benzyl phthalate 2.00 1.582 mg/Kg 79 58-126 Chrysene 2.00 1.638 mg/Kg 82 54-120 Dibenz(a,h)anthracene 2.00 1.832 mg/Kg 92 49-120 Dibenzofuran 2.00 1.784 mg/Kg 89 58-120 Diethyl phthalate 2.00 1.990 mg/Kg 99 56-128 Dimethyl phthalate 2.00 1.816 mg/Kg 91 58-120 Di-n-butyl phthalate 2.00 1.755 mg/Kg 88 64-122 Di-n-octyl phthalate 2.00 1.477 mg/Kg 74 57-137 Fluoranthene 2.00 1.858 mg/Kg 93 49-120 Fluorene 2.00 1.793 mg/Kg 90 47-120 Hexachlorobenzene 2.00 1.999 mg/Kg 100 49-127 Hexachlorobutadiene 2.00 1.892 mg/Kg 95 43-120 Hexachlorocyclopentadiene 2.00 1.184 mg/Kg 59 10-140 Hexachloroethane 2.00 1.426 mg/Kg 71 45-120 Indeno[1,2,3-cd]pyrene 2.00 1.827 mg/Kg 91 47-120 Isophorone 2.00 1.555 mg/Kg 78 50-120 Nitrobenzene 2.00 1.535 mg/Kg 77 50-120 N-Nitrosodi-n-propylamine 2.00 1.476 mg/Kg 74 48-120 N-Nitrosodiphenylamine 1.98 1.535 mg/Kg 77 54-120 Pentachlorophenol 4.00 2.683 mg/Kg 67 32-131 Phenanthrene 2.00 1.727 mg/Kg 86 50-120 Phenol 2.00 1.257 mg/Kg 63 51-120 Pyrene 2.00 1.691 mg/Kg 85 54-120 Pyridine 4.00 1.812 mg/Kg 45 29-120 2,4,6-Tribromophenol (Surr)10 -150 Surrogate 104 LCS LCS Qualifier Limits%Recovery 732-Fluorobiphenyl 27 -127 672-Fluorophenol (Surr)25 -128 82Nitrobenzene-d5 (Surr)15 -136 72Phenol-d5 (Surr)29 -130 81Terphenyl-d14 (Surr)24 -146 Eurofins Pensacola Page 49 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) Client Sample ID: Method BlankLab Sample ID: MB 400-636852/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637317 Prep Batch: 636852 RL MDL Acenaphthene 0.00100 U 0.00660 0.00100 mg/Kg 08/14/23 08:30 08/16/23 18:59 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Acenaphthylene 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Anthracene 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Benzo[a]anthracene 0.002174 J 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Benzo[a]pyrene 0.001830 J 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Benzo[b]fluoranthene 0.00200 U 0.002000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Benzo[g,h,i]perylene 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Benzo[k]fluoranthene 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Chrysene 0.00200 U 0.002000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Dibenz(a,h)anthracene 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Fluoranthene 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Fluorene 0.002940 J 0.002000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Indeno[1,2,3-cd]pyrene 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Naphthalene 0.001478 J 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Phenanthrene 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 1Pyrene 0.00100 U 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 11-Methylnaphthalene 0.001262 J 0.001000.00660 mg/Kg 08/14/23 08:30 08/16/23 18:59 12-Methylnaphthalene 2-Fluorobiphenyl 119 27-127 08/16/23 18:59 1 MB MB Surrogate 08/14/23 08:30 Dil FacPreparedAnalyzedQualifierLimits%Recovery 89 08/14/23 08:30 08/16/23 18:59 1Nitrobenzene-d5 15-136 174 S1+08/14/23 08:30 08/16/23 18:59 1Terphenyl-d14 24-146 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-636852/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637317 Prep Batch: 636852 Acenaphthene 0.0333 0.02793 mg/Kg 84 50-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Acenaphthylene 0.0333 0.02625 mg/Kg 79 50-120 Anthracene 0.0333 0.02569 mg/Kg 77 52-120 Benzo[a]anthracene 0.0333 0.03115 mg/Kg 93 55-120 Benzo[a]pyrene 0.0333 0.02454 mg/Kg 74 54-120 Benzo[b]fluoranthene 0.0333 0.02668 mg/Kg 80 55-120 Benzo[g,h,i]perylene 0.0333 0.02765 mg/Kg 83 45-120 Benzo[k]fluoranthene 0.0333 0.03034 mg/Kg 91 52-120 Chrysene 0.0333 0.02773 mg/Kg 83 54-120 Dibenz(a,h)anthracene 0.0333 0.02878 mg/Kg 86 49-120 Fluoranthene 0.0333 0.02716 mg/Kg 81 49-120 Fluorene 0.0333 0.02804 mg/Kg 84 47-120 Indeno[1,2,3-cd]pyrene 0.0333 0.02514 mg/Kg 75 47-120 Naphthalene 0.0333 0.02763 mg/Kg 83 41-120 Phenanthrene 0.0333 0.02814 mg/Kg 84 50-120 Pyrene 0.0333 0.02961 mg/Kg 89 54-120 1-Methylnaphthalene 0.0333 0.02669 mg/Kg 80 40-120 2-Methylnaphthalene 0.0333 0.02889 mg/Kg 87 40-120 Eurofins Pensacola Page 50 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: 8270E SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-636852/18-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637317 Prep Batch: 636852 2-Fluorobiphenyl 27 -127 Surrogate 111 LCS LCS Qualifier Limits%Recovery 83Nitrobenzene-d5 15 -136 148 S1+Terphenyl-d14 24 -146 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-636852/19-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637317 Prep Batch: 636852 Acenaphthene 0.0333 0.02840 mg/Kg 85 50-120 2 30 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Acenaphthylene 0.0333 0.02679 mg/Kg 80 50-120 2 30 Anthracene 0.0333 0.02584 mg/Kg 78 52-120 1 30 Benzo[a]anthracene 0.0333 0.03210 mg/Kg 96 55-120 3 30 Benzo[a]pyrene 0.0333 0.02481 mg/Kg 74 54-120 1 30 Benzo[b]fluoranthene 0.0333 0.02742 mg/Kg 82 55-120 3 30 Benzo[g,h,i]perylene 0.0333 0.02976 mg/Kg 89 45-120 7 30 Benzo[k]fluoranthene 0.0333 0.03161 mg/Kg 95 52-120 4 30 Chrysene 0.0333 0.02865 mg/Kg 86 54-120 3 30 Dibenz(a,h)anthracene 0.0333 0.03176 mg/Kg 95 49-120 10 30 Fluoranthene 0.0333 0.02702 mg/Kg 81 49-120 1 30 Fluorene 0.0333 0.02899 mg/Kg 87 47-120 3 30 Indeno[1,2,3-cd]pyrene 0.0333 0.02790 mg/Kg 84 47-120 10 30 Naphthalene 0.0333 0.02941 mg/Kg 88 41-120 6 30 Phenanthrene 0.0333 0.02742 mg/Kg 82 50-120 3 30 Pyrene 0.0333 0.02987 mg/Kg 90 54-120 1 30 1-Methylnaphthalene 0.0333 0.02942 mg/Kg 88 40-120 10 30 2-Methylnaphthalene 0.0333 0.03188 mg/Kg 96 40-120 10 30 2-Fluorobiphenyl 27 -127 Surrogate 103 LCSD LCSD Qualifier Limits%Recovery 82Nitrobenzene-d5 15 -136 141Terphenyl-d14 24 -146 Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-636903/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 636880 Prep Batch: 636903 RL MDL C5-C8 Aliphatics 2.70 U 2.70 2.70 mg/Kg 08/14/23 09:50 08/14/23 11:10 50 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 1.40 U 1.401.40 mg/Kg 08/14/23 09:50 08/14/23 11:10 50C9-C12 Aliphatics 0.750 U 0.7500.750 mg/Kg 08/14/23 09:50 08/14/23 11:10 50C9-C10 Aromatics a,a,a-Trifluorotoluene (fid)108 70-130 08/14/23 11:10 50 MB MB Surrogate 08/14/23 09:50 Dil FacPreparedAnalyzedQualifierLimits%Recovery 106 08/14/23 09:50 08/14/23 11:10 50a,a,a-Trifluorotoluene (pid)70-130 Eurofins Pensacola Page 51 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-636903/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 636880 Prep Batch: 636903 C5-C8 Aliphatics 15.0 16.14 mg/Kg 108 70-130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C9-C12 Aliphatics 17.5 19.17 mg/Kg 110 70-130 C9-C10 Aromatics 2.50 2.539 mg/Kg 102 70-130 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 110 LCS LCS Qualifier Limits%Recovery 108a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-636903/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 636880 Prep Batch: 636903 C5-C8 Aliphatics 15.0 15.46 mg/Kg 103 70-130 4 25 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD C9-C12 Aliphatics 17.5 18.15 mg/Kg 104 70-130 5 25 C9-C10 Aromatics 2.50 2.423 mg/Kg 97 70-130 5 25 a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 110 LCSD LCSD Qualifier Limits%Recovery 108a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 636880 Prep Batch: 636903 C5-C8 Aliphatics 3.56 U 19.8 19.56 mg/Kg 99 70-130☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits C9-C12 Aliphatics 1.85 U 23.1 23.80 mg/Kg 103 70-130☼ C9-C10 Aromatics 0.990 U 3.30 3.696 mg/Kg 112 70-130☼ a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 110 MS MS Qualifier Limits%Recovery 108a,a,a-Trifluorotoluene (pid)70 -130 Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 636880 Prep Batch: 636903 C5-C8 Aliphatics 3.56 U 19.8 19.97 mg/Kg 101 70-130 2 25☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD C9-C12 Aliphatics 1.85 U 23.1 24.37 mg/Kg 105 70-130 2 25☼ C9-C10 Aromatics 0.990 U 3.30 3.865 mg/Kg 117 70-130 4 25☼ a,a,a-Trifluorotoluene (fid)70 -130 Surrogate 110 MSD MSD Qualifier Limits%Recovery 108a,a,a-Trifluorotoluene (pid)70 -130 Eurofins Pensacola Page 52 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) Client Sample ID: Method BlankLab Sample ID: MB 400-636944/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637448 Prep Batch: 636944 RL MDL C9-C18 Aliphatics 1.60 U 1.60 1.60 mg/Kg 08/14/23 13:55 08/17/23 18:51 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 1.60 U 1.601.60 mg/Kg 08/14/23 13:55 08/17/23 18:51 1C19-C36 Aliphatics 1-Chlorooctadecane 54 40-140 08/17/23 18:51 1 MB MB Surrogate 08/14/23 13:55 Dil FacPreparedAnalyzedQualifierLimits%Recovery Client Sample ID: Method BlankLab Sample ID: MB 400-636944/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637452 Prep Batch: 636944 RL MDL C11-C22 Aromatics 3.00 U 3.00 3.00 mg/Kg 08/14/23 13:55 08/18/23 02:13 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier o-Terphenyl 43 40-140 08/18/23 02:13 1 MB MB Surrogate 08/14/23 13:55 Dil FacPreparedAnalyzedQualifierLimits%Recovery 82 08/14/23 13:55 08/18/23 02:13 12-Fluorobiphenyl 40-140 75 08/14/23 13:55 08/18/23 02:13 12-Bromonaphthalene 40-140 Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-636944/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637448 Prep Batch: 636944 C9-C18 Aliphatics 20.0 9.376 mg/Kg 47 40-140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits C19-C36 Aliphatics 26.7 24.34 mg/Kg 91 40-140 1-Chlorooctadecane 40 -140 Surrogate 68 LCS LCS Qualifier Limits%Recovery Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-636944/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637452 Prep Batch: 636944 C11-C22 Aromatics 56.7 40.68 mg/Kg 72 40-140 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits o-Terphenyl 40 -140 Surrogate 54 LCS LCS Qualifier Limits%Recovery 802-Fluorobiphenyl 40 -140 532-Bromonaphthalene 40 -140 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-636944/11-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637448 Prep Batch: 636944 C9-C18 Aliphatics 20.0 9.534 mg/Kg 48 40-140 2 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Eurofins Pensacola Page 53 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-636944/11-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637448 Prep Batch: 636944 C19-C36 Aliphatics 26.7 20.02 mg/Kg 75 40-140 19 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD 1-Chlorooctadecane 40 -140 Surrogate 63 LCSD LCSD Qualifier Limits%Recovery Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-636944/11-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637452 Prep Batch: 636944 C11-C22 Aromatics 56.7 41.71 mg/Kg 74 40-140 3 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD o-Terphenyl 40 -140 Surrogate 52 LCSD LCSD Qualifier Limits%Recovery 852-Fluorobiphenyl 40 -140 552-Bromonaphthalene 40 -140 Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 637448 Prep Batch: 636944 C9-C18 Aliphatics 1.92 U F1 24.0 9.044 F1 mg/Kg 38 40-140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits C19-C36 Aliphatics 1.92 U 32.0 19.94 mg/Kg 62 40-140☼ 1-Chlorooctadecane 40 -140 Surrogate 51 MS MS Qualifier Limits%Recovery Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 637452 Prep Batch: 636944 C11-C22 Aromatics 3.60 U 68.1 39.76 mg/Kg 58 40-140☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits o-Terphenyl 40 -140 Surrogate 41 MS MS Qualifier Limits%Recovery 792-Fluorobiphenyl 40 -140 502-Bromonaphthalene 40 -140 Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 637448 Prep Batch: 636944 C9-C18 Aliphatics 1.92 U F1 23.9 9.571 mg/Kg 40 40-140 6 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD C19-C36 Aliphatics 1.92 U 31.9 22.27 mg/Kg 70 40-140 11 50☼ Eurofins Pensacola Page 54 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued) Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 637448 Prep Batch: 636944 1-Chlorooctadecane 40 -140 Surrogate 54 MSD MSD Qualifier Limits%Recovery Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 637452 Prep Batch: 636944 C11-C22 Aromatics 3.60 U 67.8 47.24 mg/Kg 70 40-140 7 50☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec Limits LimitRPD RPD o-Terphenyl 40 -140 Surrogate 44 MSD MSD Qualifier Limits%Recovery 802-Fluorobiphenyl 40 -140 532-Bromonaphthalene 40 -140 Method: 6010D - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 400-637246/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637311 Prep Batch: 637246 RL MDL Chromium 0.309 U 0.998 0.309 mg/Kg 08/16/23 15:09 08/17/23 02:34 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier 0.220 U 0.2200.998 mg/Kg 08/16/23 15:09 08/17/23 02:34 1Lead Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-637246/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 637311 Prep Batch: 637246 Chromium 99.8 98.64 mg/Kg 99 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Lead 99.8 96.84 mg/Kg 97 80-120 Method: Moisture - Percent Moisture Client Sample ID: W.O. CS2 (17)Lab Sample ID: 400-241823-2 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 637224 Percent Solids 85.9 86.9 %1 10 Analyte DU DU DUnitResultQualifier Sample Result Sample Qualifier LimitRPD RPD Percent Moisture 14.1 13.1 %7 Eurofins Pensacola Page 55 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: W.O. CS1 (17)Lab Sample ID: 400-241823-1 Matrix: SolidDate Collected: 07/31/23 12:00 Date Received: 08/10/23 09:49 Analysis Moisture TMP08/15/23 17:121 EET PEN637224 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: W.O. CS1 (17)Lab Sample ID: 400-241823-1 Matrix: SolidDate Collected: 07/31/23 12:00 Percent Solids: 82.1Date Received: 08/10/23 09:49 Prep 3546 LH08/14/23 08:30 EET PEN636852 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.64 g 1 mL Analysis 8270E SIM 1 637317 08/16/23 20:01 KJA EET PENTotal/NA 0.4 mL 0.4 mL Prep 3050B 637246 08/16/23 15:09 KWN EET PENTotal/NA 0.541 g 50 mL Completed:08/16/23 18:33 ¹ Analysis 6010D 1 637311 08/17/23 03:29 LSS EET PENTotal/NA Client Sample ID: W.O. CS2 (17)Lab Sample ID: 400-241823-2 Matrix: SolidDate Collected: 07/31/23 12:04 Date Received: 08/10/23 09:49 Analysis Moisture TMP08/15/23 17:121 EET PEN637224 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: W.O. CS2 (17)Lab Sample ID: 400-241823-2 Matrix: SolidDate Collected: 07/31/23 12:04 Percent Solids: 85.9Date Received: 08/10/23 09:49 Prep 3546 LH08/14/23 08:30 EET PEN636852 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.17 g 1 mL Analysis 8270E SIM 1 637317 08/16/23 20:22 KJA EET PENTotal/NA 0.4 mL 0.4 mL Prep 3050B 637246 08/16/23 15:09 KWN EET PENTotal/NA 0.551 g 50 mL Completed:08/16/23 18:33 ¹ Analysis 6010D 1 637311 08/17/23 03:32 LSS EET PENTotal/NA Client Sample ID: W.O. CS3 (17)Lab Sample ID: 400-241823-3 Matrix: SolidDate Collected: 07/31/23 12:07 Date Received: 08/10/23 09:49 Analysis Moisture TMP08/15/23 17:121 EET PEN637224 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: W.O. CS3 (17)Lab Sample ID: 400-241823-3 Matrix: SolidDate Collected: 07/31/23 12:07 Percent Solids: 81.0Date Received: 08/10/23 09:49 Prep 3546 LH08/14/23 08:30 EET PEN636852 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.17 g 1 mL Analysis 8270E SIM 1 637317 08/16/23 20:42 KJA EET PENTotal/NA 0.4 mL 0.4 mL Eurofins Pensacola Page 56 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: W.O. CS3 (17)Lab Sample ID: 400-241823-3 Matrix: SolidDate Collected: 07/31/23 12:07 Percent Solids: 81.0Date Received: 08/10/23 09:49 Prep 3050B KWN08/16/23 15:09 EET PEN637246 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 0.552 g 50 mL Analysis 6010D 1 637311 08/17/23 03:35 LSS EET PENTotal/NA Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 Matrix: SolidDate Collected: 08/01/23 12:21 Date Received: 08/10/23 09:49 Analysis Moisture TMP08/15/23 17:121 EET PEN637224 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 Matrix: SolidDate Collected: 08/01/23 12:21 Percent Solids: 82.7Date Received: 08/10/23 09:49 Prep 5035 BPO08/15/23 09:46 EET PEN637089 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.355 g 5.00 g Analysis 8260D 1 637090 08/15/23 17:00 BPO EET PENTotal/NA 5 mL 5 mL Prep 3546 636852 08/14/23 08:30 LH EET PENTotal/NA 15.66 g 1 mL Analysis 8270E 1 637034 08/15/23 18:45 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 636903 08/14/23 09:50 PD EET PENTotal/NA 5.443 g 5.00 g Analysis MAVPH 50 636880 08/14/23 13:06 SAB EET PENTotal/NA 5 mL 5 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.10 g 2 mL Analysis MA-EPH 1 637448 08/17/23 20:16 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.10 g 2 mL Analysis MA-EPH 1 637452 08/18/23 03:55 MP EET PENTotal/NA 1 mL 1 mL Prep 3050B 637246 08/16/23 15:09 KWN EET PENTotal/NA 0.504 g 50 mL Completed:08/16/23 18:33 ¹ Analysis 6010D 1 637311 08/17/23 03:39 LSS EET PENTotal/NA Client Sample ID: W.O. SW2 (12)Lab Sample ID: 400-241823-5 Matrix: SolidDate Collected: 08/01/23 12:30 Date Received: 08/10/23 09:49 Analysis Moisture TMP08/15/23 17:121 EET PEN637224 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: W.O. SW2 (12)Lab Sample ID: 400-241823-5 Matrix: SolidDate Collected: 08/01/23 12:30 Percent Solids: 84.8Date Received: 08/10/23 09:49 Prep 5035 BPO08/14/23 08:59 EET PEN636938 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.815 g 5.00 g Analysis 8260D 1 636861 08/14/23 18:59 BPO EET PENTotal/NA 5 mL 5 mL Prep 3546 636852 08/14/23 08:30 LH EET PENTotal/NA 15.90 g 1 mL Analysis 8270E 1 637034 08/15/23 19:08 S1B EET PENTotal/NA 0.4 mL 0.4 mL Eurofins Pensacola Page 57 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: W.O. SW2 (12)Lab Sample ID: 400-241823-5 Matrix: SolidDate Collected: 08/01/23 12:30 Percent Solids: 84.8Date Received: 08/10/23 09:49 Prep 5035 PD08/14/23 09:50 EET PEN636903 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.225 g 5.00 g Analysis MAVPH 50 636880 08/14/23 13:44 SAB EET PENTotal/NA 5 mL 5 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.41 g 2 mL Analysis MA-EPH 1 637448 08/17/23 20:33 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.41 g 2 mL Analysis MA-EPH 1 637452 08/18/23 04:12 MP EET PENTotal/NA 1 mL 1 mL Prep 3050B 637246 08/16/23 15:09 KWN EET PENTotal/NA 0.502 g 50 mL Completed:08/16/23 18:33 ¹ Analysis 6010D 1 637311 08/17/23 03:42 LSS EET PENTotal/NA Client Sample ID: W.O. SW3 (12)Lab Sample ID: 400-241823-6 Matrix: SolidDate Collected: 08/01/23 12:33 Date Received: 08/10/23 09:49 Analysis Moisture TMP08/15/23 17:121 EET PEN637224 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: W.O. SW3 (12)Lab Sample ID: 400-241823-6 Matrix: SolidDate Collected: 08/01/23 12:33 Percent Solids: 81.4Date Received: 08/10/23 09:49 Prep 5035 BPO08/14/23 08:59 EET PEN636938 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.199 g 5.00 g Analysis 8260D 1 636861 08/14/23 19:26 BPO EET PENTotal/NA 5 mL 5 mL Prep 3546 636852 08/14/23 08:30 LH EET PENTotal/NA 15.14 g 1 mL Analysis 8270E 1 637034 08/15/23 19:30 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 636903 08/14/23 09:50 PD EET PENTotal/NA 6.121 g 5.00 g Analysis MAVPH 50 636880 08/14/23 14:35 SAB EET PENTotal/NA 5 mL 5 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.15 g 2 mL Analysis MA-EPH 1 637448 08/17/23 20:50 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.15 g 2 mL Analysis MA-EPH 1 637452 08/18/23 04:29 MP EET PENTotal/NA 1 mL 1 mL Prep 3050B 637246 08/16/23 15:09 KWN EET PENTotal/NA 0.540 g 50 mL Completed:08/16/23 18:33 ¹ Analysis 6010D 1 637311 08/17/23 03:46 LSS EET PENTotal/NA Client Sample ID: H.O. BE2 (17)Lab Sample ID: 400-241823-7 Matrix: SolidDate Collected: 08/01/23 12:38 Date Received: 08/10/23 09:49 Analysis Moisture TMP08/15/23 17:121 EET PEN637224 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Eurofins Pensacola Page 58 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: H.O. BE2 (17)Lab Sample ID: 400-241823-7 Matrix: SolidDate Collected: 08/01/23 12:38 Percent Solids: 83.3Date Received: 08/10/23 09:49 Prep 5035 BPO08/14/23 08:59 EET PEN636938 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.557 g 5.00 g Analysis 8260D 50 636861 08/14/23 20:47 BPO EET PENTotal/NA 5 mL 5 mL Prep 3546 636852 08/14/23 08:30 LH EET PENTotal/NA 15.72 g 1 mL Analysis 8270E 1 637034 08/15/23 19:52 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 636903 08/14/23 09:50 PD EET PENTotal/NA 6.557 g 5.00 g Analysis MAVPH 2000 636880 08/14/23 20:24 SAB EET PENTotal/NA 5 mL 5 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.49 g 2 mL Analysis MA-EPH 1 637448 08/17/23 21:06 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.49 g 2 mL Analysis MA-EPH 1 637452 08/18/23 04:46 MP EET PENTotal/NA 1 mL 1 mL Prep 3050B 637246 08/16/23 15:09 KWN EET PENTotal/NA 0.523 g 50 mL Completed:08/16/23 18:33 ¹ Analysis 6010D 1 637311 08/17/23 03:56 LSS EET PENTotal/NA Client Sample ID: H.O. BE1 (17)Lab Sample ID: 400-241823-8 Matrix: SolidDate Collected: 08/01/23 13:50 Date Received: 08/10/23 09:49 Analysis Moisture TMP08/15/23 17:121 EET PEN637224 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA Client Sample ID: H.O. BE1 (17)Lab Sample ID: 400-241823-8 Matrix: SolidDate Collected: 08/01/23 13:50 Percent Solids: 85.4Date Received: 08/10/23 09:49 Prep 5035 BPO08/14/23 08:59 EET PEN636938 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 6.433 g 5.00 g Analysis 8260D 1 636861 08/14/23 19:53 BPO EET PENTotal/NA 5 mL 5 mL Prep 3546 636852 08/14/23 08:30 LH EET PENTotal/NA 15.59 g 1 mL Analysis 8270E 5 637166 08/16/23 22:12 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 5035 636903 08/14/23 09:50 PD EET PENTotal/NA 6.087 g 5.00 g Analysis MAVPH 50 636880 08/14/23 16:32 SAB EET PENTotal/NA 5 mL 5 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.28 g 2 mL Analysis MA-EPH 1 637452 08/18/23 05:03 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.28 g 2 mL Analysis MA-EPH 20 638211 08/24/23 23:41 MP EET PENTotal/NA 1 mL 1 mL Prep 3050B 637246 08/16/23 15:09 KWN EET PENTotal/NA 0.507 g 50 mL Completed:08/16/23 18:33 ¹ Analysis 6010D 1 637311 08/17/23 03:59 LSS EET PENTotal/NA Eurofins Pensacola Page 59 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: Method Blank Lab Sample ID: MB 400-636852/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH08/14/23 08:30 EET PEN636852 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 637034 08/15/23 16:30 S1B EET PENTotal/NA 0.4 mL 0.4 mL Prep 3546 636852 08/14/23 08:30 LH EET PENTotal/NA 15.00 g 1 mL Analysis 8270E SIM 1 637317 08/16/23 18:59 KJA EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-636903/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 PD08/14/23 09:50 EET PEN636903 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis MAVPH 50 636880 08/14/23 11:10 SAB EET PENTotal/NA 5 mL 5 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-636938/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 BPO08/14/23 08:59 EET PEN636938 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 636861 08/14/23 11:47 BPO EET PENTotal/NA 5 mL 5 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-636944/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH08/14/23 13:55 EET PEN636944 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 637448 08/17/23 18:51 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 637452 08/18/23 02:13 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: Method Blank Lab Sample ID: MB 400-637089/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 BPO08/15/23 09:46 EET PEN637089 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 637090 08/15/23 11:33 BPO EET PENTotal/NA 5 mL 5 mL Eurofins Pensacola Page 60 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: Method Blank Lab Sample ID: MB 400-637246/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3050B KWN08/16/23 15:09 EET PEN637246 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 0.501 g 50 mL Completed:08/16/23 18:33 ¹ Analysis 6010D 1 637311 08/17/23 02:34 LSS EET PENTotal/NA Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-636852/18-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH08/14/23 08:32 EET PEN636852 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E SIM 1 637317 08/16/23 19:19 KJA EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-636852/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH08/14/23 08:30 EET PEN636852 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E 1 637034 08/15/23 16:53 S1B EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-636903/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 PD08/14/23 09:50 EET PEN636903 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis MAVPH 50 636880 08/14/23 11:48 SAB EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-636938/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 BPO08/14/23 08:59 EET PEN636938 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 636861 08/14/23 10:41 BPO EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-636944/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH08/14/23 13:55 EET PEN636944 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 637448 08/17/23 19:08 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 637452 08/18/23 02:47 MP EET PENTotal/NA 1 mL 1 mL Eurofins Pensacola Page 61 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-637089/1-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 BPO08/15/23 09:46 EET PEN637089 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis 8260D 1 637090 08/15/23 10:25 BPO EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-637246/2-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3050B KWN08/16/23 15:09 EET PEN637246 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 0.501 g 50 mL Completed:08/16/23 18:33 ¹ Analysis 6010D 1 637311 08/17/23 02:37 LSS EET PENTotal/NA Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-636852/19-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH08/14/23 08:32 EET PEN636852 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 1 mL Analysis 8270E SIM 1 637317 08/16/23 19:40 KJA EET PENTotal/NA 0.4 mL 0.4 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-636903/3-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 5035 PD08/14/23 09:50 EET PEN636903 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.00 g 5.00 g Analysis MAVPH 50 636880 08/14/23 12:27 SAB EET PENTotal/NA 5 mL 5 mL Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-636944/11-A Matrix: SolidDate Collected: N/A Date Received: N/A Prep 3546 LH08/14/23 13:55 EET PEN636944 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.00 g 2 mL Analysis MA-EPH 1 637448 08/17/23 19:25 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.00 g 2 mL Analysis MA-EPH 1 637452 08/18/23 03:04 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MS Matrix: SolidDate Collected: 08/01/23 12:21 Percent Solids: 82.7Date Received: 08/10/23 09:49 Prep 5035 PD08/14/23 09:50 EET PEN636903 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.443 g 5.00 g Analysis MAVPH 50 636880 08/14/23 15:14 SAB EET PENTotal/NA 5 mL 5 mL Eurofins Pensacola Page 62 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MS Matrix: SolidDate Collected: 08/01/23 12:21 Percent Solids: 82.7Date Received: 08/10/23 09:49 Prep 3546 LH08/14/23 13:55 EET PEN636944 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 15.10 g 2 mL Analysis MA-EPH 1 637448 08/17/23 19:42 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.10 g 2 mL Analysis MA-EPH 1 637452 08/18/23 03:21 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: W.O. SW1 (12)Lab Sample ID: 400-241823-4 MSD Matrix: SolidDate Collected: 08/01/23 12:21 Percent Solids: 82.7Date Received: 08/10/23 09:49 Prep 5035 PD08/14/23 09:50 EET PEN636903 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA 5.443 g 5.00 g Analysis MAVPH 50 636880 08/14/23 15:53 SAB EET PENTotal/NA 5 mL 5 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.15 g 2 mL Analysis MA-EPH 1 637448 08/17/23 19:59 MP EET PENTotal/NA 1 mL 1 mL Prep 3546 636944 08/14/23 13:55 LH EET PENTotal/NA 15.15 g 2 mL Analysis MA-EPH 1 637452 08/18/23 03:38 MP EET PENTotal/NA 1 mL 1 mL Client Sample ID: W.O. CS2 (17)Lab Sample ID: 400-241823-2 DU Matrix: SolidDate Collected: 07/31/23 12:04 Date Received: 08/10/23 09:49 Analysis Moisture TMP08/15/23 17:121 EET PEN637224 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil Total/NA ¹ This procedure uses a method stipulated length of time for the process. Both start and end times are displayed. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 63 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Method Summary Job ID: 400-241823-1Client: Terraquest Environmental Consultants, PC Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Method Method Description LaboratoryProtocol SW8468260DVolatile Organic Compounds by GC/MS EET PEN SW8468270ESemivolatile Organic Compounds (GC/MS)EET PEN SW8468270E SIM Semivolatile Organic Compounds (GC/MS SIM)EET PEN MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)EET PEN MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)EET PEN SW8466010DMetals (ICP)EET PEN EPAMoisturePercent Moisture EET PEN SW8463050BPreparation, Metals EET PEN SW8463546Microwave Extraction EET PEN SW8465035Closed System Purge and Trap EET PEN Protocol References: EPA = US Environmental Protection Agency MA DEP = Massachusetts Department Of Environmental Protection SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 Eurofins Pensacola Page 64 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Accreditation/Certification Summary Client: Terraquest Environmental Consultants, PC Job ID: 400-241823-1 Project/Site: 280 Ervin Woods Dr., Kannapolis, NC Laboratory: Eurofins Pensacola Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 314 12-31-23 Eurofins Pensacola Page 65 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Pa g e 6 6 o f 6 7 8/ 2 9 / 2 0 2 3 ( R e v . 1 ) 123456789101112131415 Login Sample Receipt Checklist Client: Terraquest Environmental Consultants, PC Job Number: 400-241823-1 Login Number: 241823 Question Answer Comment Creator: Roberts, Alexis J List Source: Eurofins Pensacola List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. N/AThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded.1.1°C IR8 TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. Eurofins Pensacola Page 67 of 67 8/29/2023 (Rev. 1) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15