MO-29901_48992_CA_LSA_20230731

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

July 31, 2023

Mr. Ryan Mills
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: High-Risk Limited Site Assessment Report
Handy Corner
2076 Startown Road
Lincolnton, Lincoln County
North Carolina
Facility ID Number: 0-014377
Incident Number: 48992
GRI Project Number: 6389

Dear Mr. Mills,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Joanna Alley at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Johanna Moats
AP/AR Coordinator

Enclosure

Cc: Mr. Jimmy White, Nisbet Oil Company, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
High-Risk Limited Site Assessment Report
Handy Corner
2076 Startown Road
Lincolnton, Lincoln County
North Carolina
Facility ID Number: 0-014377
Incident Number: 48992
GRI Project Number: 6389

Prepared for:

Jimmy White
Nisbet Oil Company
1818 Baxter Street
Charlotte, North Carolina 28204

July 31, 2023

Joanna Alley, P.E.
Project Manager

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
i
EXECUTIVE SUMMARY
The Handy Corner site is located at 2076 Startown Road in Lincolnton, Lincoln County, North Carolina.
The property operates as a petroleum retail facility and convenience store. The site is covered by asphalt,
concrete, and grass. There are one 10,000-gallon and two 6,000-gallon gasoline USTs and one 10,000-
gallon and one 2,000-gallon diesel USTs currently in use at the site with five associated gasoline, one
kerosene, and two diesel dispensers. The surrounding properties are residential.

On January 4, 2023, a site check was conducted at the subject site due to a non-passing spill bucket for
the 10,000-gallon RUL gasoline UST. The concentration of GRO exceeded the RAL; therefore, an LSA was
required.

A receptor survey was conducted on April 26, 2023. Nineteen water supply wells were identified within a
1,500-foot radius of the site, of which eleven are potable and located within 1,000 feet of the source area.
Three of those water supply wells were identified within a 250-foot radius of the site. Public water is
available along Startown Road but is not available along Clarks Creek Road or Carlos Road. No surface
water bodies were identified within a 500-foot radius of the site.

On April 26, 2023, one Type II monitoring well was installed at the UST basin. Soil samples were collected
at 10-foot intervals during the installation of MW-1. All of the reported contaminant concentrations were
below the soil-to-water MCCs.

On April 26, 2023, a ground water sample was collected from MW-1. The concentrations of benzene,
bromodichloromethane, lead, and C9-C10 aromatics reported in the ground water sample collected from
MW-1 exceeded the MACs. Please note that bromodichloromethane is not a petroleum constituent.
Based on the reported ground water contaminant concentrations and the presence of water supply wells
within a 250-foot radius of the site and potable water supply wells within a 1,000-foot radius of the site,
a Phase II LSA was required to be completed at the site.

On July 5, 2023, three additional Type II monitoring wells were installed at the site in order to determine
the ground water flow direction. A ground water sample was collected from each well following
installation. The concentrations of benzene, toluene, xylenes, naphthalene, TAA, TBA, 1,2,4-
trimethylbenzene, lead, C5-C8 aliphatics, C9-C12 aliphatics, and/or C9-C10 aromatics reported in the
ground water samples collected from MW-2, MW-3, and MW-4 exceeded the MACs. All of the reported
concentrations were below the GCLs. No free product was observed at the site.

Based on the presence of water supply well within 250 feet of the site, the presence of potable water
supply wells within 1,000 feet of the site, and the reported contaminant concentrations exceeding the
MACs, the site risk should be classified as high and a CSA should be conducted at the site. Based on the
relatively limited contamination at the site, it is recommended to resample all wells prior to conducting
the CSA to confirm the results of the April and July 2023 sampling events. The water supply wells located

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
ii
within 250 feet of the site should also be sampled.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
iii
SITE INFORMATION
1. Site Identification
 Handy Corner (Facility ID 0-014377)
 Incident Number 48992 – High Risk
 Location of Source Area: 2076 Startown Road
Lincolnton, NC 28092
Lincoln County (Figure 1)
35.512600°N, 81.262114°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System
UST Owner
Nisbet Oil Company (Table 1)
1818 Baxter Street
Charlotte, NC 28204
[e-mail]
704-332-7755

UST Operator
Handy Corner
2076 Startown Road
Lincolnton, NC 28092
Email: Unknown
704-732-6050

Property Owner
Rhodes & Beal Oil Co., Inc.
1404 E Main St.
Lincolnton, NC 28092
Email Unknown
704-735-2508

Property Occupant
Handy Corner
2076 Startown Road
Lincolnton, NC 28092
Email: Unknown
704-732-6050

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical
449 Springbrook Road
Charlotte, NC 28217
State Certification Nos. 37735 & 402
704-529-6364
3. Information about Release
 Release was discovered on January 4, 2023
 An unknown amount of product was released from the leaking UST System via a non-passing spill bucket
 One (1) 10,000-gallon gasoline UST, two (2) 6,000-gallon gasoline USTs, one (1) 10,000-gallon diesel UST,
and one (1) 2,000-gallon diesel UST are in use at the site (Table 2)

Certification:

I, Eric M. Eubanks, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the corporation are C-127 and C-2727, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
iv
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
RUL: Regular Unleaded
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWAP: Source Water Assessment and
Protection
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
TABLE OF CONTENTS

EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ........................................................................................................................... iii
ACRONYMS ....................................................................................................................................... iv
1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................4
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................5
4. SITE INVESTIGATION .............................................................................................................6
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................8
6. LIMITATIONS ........................................................................................................................9

FIGURES
Figure 1: Site Location Map
Figure 2A: Site Vicinity Map
Figure 2B: Zoning Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Soil Quality Map
Figure 6: Ground Water Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Land Use Information
Table 4: Receptor Information
Table 5: Adjacent Property Owner Information
Table 6: Well Construction and Gauging Information
Table 7: Summary of Soil Sample Analytical Results
Table 8: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Water Use Questionnaires
Appendix B: Lincoln County Property Cards
Appendix C: Well Permit, Well Construction Records and Subsurface Logs
Appendix D: State Correspondence
Appendix E: Laboratory Analytical Reports

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? YES

Eleven potable water supply wells are located within 1,000 feet of the source area. A Site Vicinity
Map is included as Figure 2A.

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
YES

Three water supply wells (WSW-1, WSW-11, and WSW-12) are located within 250 feet of the
source area.

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

Public water is available along Startown Road but is not available along Clarks Creek Road or Carlos
Road.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? NO

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? N/A

8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
2
9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? NO

10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? N/A
If YES, describe.
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? NO

All of the reported concentrations were below the GCLs.

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store and petroleum retail facility.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:

The property is easily accessible to pedestrian and vehicular traffic.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
3
6. Do pavement, buildings, or other structures cap the contaminated soil? YES
Explain:
The site is currently covered with concrete, asphalt, and grass.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?
The site is expected to remain in operation as an active convenience store and petroleum retail
facility for the foreseeable future.
7. What is the zoning status of the property?
According to the Lincoln County Zoning Map, the site is zoned B-N (Neighborhood Business).

8. Is the use of the property likely to change in the next 20 years? NO
Explain:

The subject property is currently an active convenience store and petroleum retail facility and
likely remain a convenience store for the foreseeable future.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is 2065 Startown Road located approximately 145 feet west-
southwest of the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

No places of public assembly are located within 1,500 feet of the source area at the site.

11. What is the zoning status of properties in the surrounding area?

According to the Lincoln County Official Zoning Map, the surrounding areas are zoned Residential
(R-25, R-S, R-SF, R-T and PRD).

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is residential. Land use information is included in Table 3. A zoning
map is included as Figure 2B.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
4
2. RECEPTOR INFORMATION
1. Water Supply Wells:
A receptor survey was conducted on April 26, 2023. Nineteen water supply wells were identified
within a 1,500-foot radius of the site, of which eleven (WSW-1 through WSW-5, WSW-9, and
WSW-11 through WSW-15) are potable and located within 1,000 feet of the source area. Three
water supply wells (WSW-1, WSW-11, and WSW-12) are located within a 250-foot radius of the
site. Receptor information is provided in Table 4. Returned water use questionnaires are included
as Appendix A.

2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and along Startown Road but is not available along Clarks
Creek Road or Carlos Road.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
No surface water bodies were identified within a 500-foot radius of the site. An unnamed stream
and a pond are located approximately 1,020 feet southeast and 1,280 feet west of the site,
respectively.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On July 12, 2023, GRI personnel accessed the NCDEQ SWAP Program’s website to identify
wellhead protection areas in the vicinity of the subject site. The site is not located within a
wellhead protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is not located in the Coastal Plain Physiographic Region.

6. Subsurface Structures:
A house with a basement was observed at 814 Clarks Creek Road. The water main and other
underground utilities run along Startown Road, and several underground utility lines were
observed on the property.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
5. Property boundaries are shown on Figure 2A. Property cards for the adjacent property owners

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
5
are attached as Appendix B.
3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is located in the Inner Piedmont Belt. The
bedrock is generally described as an amphibolite and biotite gneiss interlayered with minor layers and
lenses of hornblende gneiss, metagabbro, mica schist, and granite. The soil samples collected during well
installation activities were red to brown silts and fine sands. The depth to ground water during the July 5,
2023 gauging event ranged from 25.26 to 28.15 feet below the top of well casing. A copy of the well
permit, well construction records and subsurface logs are included as Appendix C. A Site Map is included
as Figure 3. Well construction and gauging information is included in Table 6. Photographs of the newly
installed monitoring wells are shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
6
4. SITE INVESTIGATION
On January 4, 2023, a site check was conducted at the subject site due to a non-passing spill bucket for
the 10,000-gallon RUL gasoline UST. The concentration of GRO exceeded the RAL; therefore, an LSA was
required.

One Type II monitoring well (MW-1) was installed at the UST basin by a North Carolina licensed well
contractor on April 26, 2023 to assess the identified release at the site. MW-1 was installed to a total
depth of 35 feet BGS with a 15-foot screened interval set to bracket the water table at the time of
installation.

Based on the ground water contaminant concentrations in the ground water sample collected from MW-
1, the presence of water supply wells within a 250-foot radius of the site, and potable water supply wells
within a 1,000-foot radius of the site, three additional Type II monitoring wells were required to be
installed at the site in order to determine the ground water flow direction. Monitoring wells MW-2
through MW-4 were installed at the site on July 5, 2023 to a total depth of 35 feet BGS each with a
screened interval of 15 feet. A copy of the NCDEQ agreement to proceed to a High Risk LSA is included in
Appendix D.

Monitoring wells MW-1 through MW-4 were gauged on July 5, 2023. The depth to ground water ranged
from 25.26 to 28.15 feet below TOC. The ground water elevation ranged from 73.54 to 76.36 during the
July 2023 ground water gauging event. Ground water flow was generally towards the southeast with a
horizontal gradient of approximately 0.03 feet per foot. A Water Table Surface Map is included as Figure
4. Gauging data from the July 2023 gauging event is included in Table 6. A summary of the current gauging
data is shown below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Groundwater
Elevation
(ft.)
MW-1 20 - 35 35 100.00 25.79 74.21
MW-2 20 - 35 35 102.49 26.13 76.36
MW-3 20 - 35 35 98.80 25.26 73.54
MW-4 20 - 35 35 102.50 28.15 74.35

1. Soil Sampling:
Soil sample (CS-2) was collected on January 4, 2023 during Site Check activities and submitted for
laboratory analysis of GRO by EPA Method 8015D. The concentration of GRO reported in the soil
samples collected from CS-2 exceeded the RAL. No free product was noted at the site.

On April 26, 2023, four soil samples (MW-1-5’, MW-1-10’, MW-1-15’, and MW-1-20’) were collected
at 5-foot intervals during the installation of monitoring well MW-1. The soil samples were submitted
for analysis of VPH by the MADEP Method. Soil samples MW-1-5’ and MW-1-20’ were also submitted
for analysis of VOCs by EPA Method 8260B.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
7
All of the reported contaminant concentrations were below the soil-to-water MCCs. A Soil Quality
Map has been included as Figure 5. A summary of the soil sample analytical results is presented in
Table 7. A copy of the laboratory analytical report from the April 2023 soil sampling event has been
included in Appendix E. A copy of the current soil sampling data collected during the LSA activities is
shown below:

Sa
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(f
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MT
B
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Soil to Water MCC (mg/kg) 0.0072 5.4 8 6 0.085 0.2
Residential SCLs (mg/kg) 12 1,250 60.3 3,120 156 5.5
MW-1-5' 5 <0.0007 <0.0008 <0.0007 <0.0006 0.0009 J <0.001
MW-1-10' 10 NR NR NR NR NR NR
MW-1-15' 15 NR NR NR NR NR NR
MW-1-20' 20 <0.0008 0.0009 J <0.0008 0.005 J 0.002 J <0.001

2. Ground Water Sampling:
On April 26, 2023, MW-1 was gauged, purged, and sampled in accordance with NCDEQ guidelines.
The ground water sample was submitted for analysis of VOCs by EPA Method 6200B, EDB by EPA
Method 504.1, total lead by EPA Method 6010, and VPH by the MADEP Method. The concentrations
of benzene, bromodichloromethane, lead, and C9-C10 aromatics reported in the ground water sample
collected from MW-1 exceeded the MACs. Please note that bromodichloromethane is not a
petroleum constituent. All of the reported contaminant concentrations were below the GCLs.

On July 5, 2023, monitoring wells MW-2 through MW-4 were gauged, purged, and sampled in
accordance with NCDEQ guidelines. The ground water samples were submitted for analysis of VOCs,
EDB, total lead and VPH. The concentrations of benzene, toluene, xylenes, naphthalene, TAA, TBA,
1,2,4-trimethylbenzene, lead, C5-C8 aliphatics, C9-C12 aliphatics and/or C9-C10 aromatics reported
in the ground water samples collected from MW-2, MW-3, and MW-4. All of the reported
concentrations were below the GCLs. No free product was observed at the site. A Ground Water
Quality Map is included as Figure 6. A summary of the ground water analytical data is included in
Table 8. Copies of the laboratory analytical reports are included in Appendix E. A summary of the
current ground water sampling data is shown below:

Contaminant of
Concern

Be
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e

To
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e

Et
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Xy
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s

MT
B
E

Na
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t
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a
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e

Well
ID
MAC (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 38.7 135 41.6 377 0.969 J <0.470

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
8
Contaminant of
Concern

Be
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e

To
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e

Et
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MT
B
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Na
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a
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Well
ID
MAC (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-2 <0.180 <0.220 <0.170 0.674 J <0.140 <0.470
MW-3 325 788 310 3,970 17.6 35.2
MW-4 0.451 J 1.84 0.765 6.09 <0.140 <0.470

3. Quality Control:
The soil and ground water samples were immediately placed in laboratory-supplied containers after
collection, which were then placed in iced coolers. New disposable bailers were used to sample the
monitoring well and new nitrile gloves were worn during soil and ground water sampling. Samples
were logged using proper chain-of-custody procedures. The samples were transported to a North
Carolina certified laboratory for analysis. A laboratory supplied trip blank was included in the sample
cooler. No detectable concentrations of requested method constituents were reported in the trip
blank.

5. CONCLUSIONS AND RECOMMENDATIONS
 The site is an active convenience store and petroleum retail facility. Land use in the area consists
of residential properties.
 A receptor survey was conducted on April 26, 2023. Nineteen water supply wells were identified
within a 1,500-foot radius of the site, of which eleven are potable and located within 1,000 feet
of the source area. Three of those water supply wells were identified within a 250-foot radius of
the site. Public water is available along Startown Road but is not available along Clarks Creek Road
or Carlos Road.
 No surface water bodies were identified within a 500-foot radius of the site.
 On April 26, 2023, one Type II monitoring well was installed at the UST basin. Soil samples were
collected at 5-foot intervals during the installation of MW-1. All of the reported contaminant
concentrations were below the soil-to-water MCCs.
 On April 26, 2023, a ground water sample was collected from MW-1. The concentrations of
benzene, bromodichloromethane, lead, and C9-C10 aromatics reported in the ground water
sample collected from MW-1 exceeded the MACs. Please note that bromodichloromethane is not
a petroleum constituent.
 On July 5, 2023, three additional Type II monitoring wells were installed at the site in order to
determine the ground water flow direction. A ground water sample was collected from each well
following installation. The concentrations of benzene, toluene, xylenes, naphthalene, TAA, TBA,
1,2,4-trimethylbenzene, lead, C5-C8 aliphatics, C9-C12 aliphatics and/or C9-C10 aromatics
reported in the ground water samples collected from MW-2, MW-3, and MW-4 exceeded the

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report
Prepared on: July 31, 2023 Handy Corner
Project Manager: Joanna Alley, P.E. GRI Project No. 6389
9
MACs. All of the reported concentrations were below the GCLs. No free product was observed at
the site.
 Based on the presence of water supply wells within 250 feet of the site, the presence of potable
water supply wells within 1,000 feet of the site, and the reported contaminant concentrations
exceeding the MACs, the site risk should be classified as high and a CSA should be conducted at
the site. Based on the relatively limited contamination at the site, it is recommended to resample
all wells prior to conducting the CSA to confirm the results of the April and July 2023 sampling
events. The water supply wells located within 250 feet of the site should also be sampled.

6. LIMITATIONS
This report has been prepared for the exclusive use of Nisbet Oil Company for specific application to the
referenced site in Lincoln County, North Carolina. The assessment was conducted based on the scope of
work and level of effort specified by NCDEQ and with resources adequate only for that scope of work. Our
findings have been developed in accordance with generally accepted standards of geology and
hydrogeology practices in the State of North Carolina, available information and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATION
Figure 1
Site Location Map
Handy Corner
2076 Startown Road
Lincolnton, North Carolina
Lincoln County
Incident No. 48992
GRI Project No. 6389500 M
2000 FT
Date: 05/03/2023 Location: 35.512600° N -81.262114° W
D
a
d

TABLES
UST ID Number 1 - 5 Facility ID Number
Owner or Operator?
Owner
UST ID Number 1 - 5 Facility ID Number
Owner or Operator?
Owner
UST ID Number 1 - 5 Facility ID Number
Owner or Operator?
Owner
Address Telephone Number
Unknown Unknown
0-014377
Name of Owner or Operator Dates of Ownership / Operation
Unknown 6/6/1979 - 6/6/1989
0-014377
TABLE 1
UST OWNER/OPERATOR INFORMATION
HANDY CORNER (INCIDENT NO. 48992)
1818 Baxter Street, Charlotte NC 28235 704-332-7755
Name of Owner or Operator Dates of Ownership / Operation
Nisbet Oil Company 7/1/2005 - Present
Address Telephone Number
Address Telephone Number
1404 E. Main Street, Lincolnton, NC 28092 704-735-2508
0-014377
Name of Owner or Operator Dates of Ownership / Operation
Rhodes & Beal Oil Co. 6/6/1989 - 7/1/2005
Page 1 of 1
Date: 07/11/23
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 10,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current Yes
2 Gasoline Gasoline 6,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current Yes
3 Gasoline Gasoline 6,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current Yes
4 Diesel Diesel 10,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current No
5 Diesel Diesel 2,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current No
Notes:
*Piping material information was provided in the UST-10B Form
TABLE 2
UST SYSTEM INFORMATION
HANDY CORNER (INCIDENT NO. 48992)
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
Facility ID #: 0-014377
Page 1 of 1
Date: 07/11/23 Facility ID # : 00-0-0000014377
Map ID No. Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
n/a B-N Neighborhood Business N/A N/A
n/a R-S Residential N/A N/A
n/a R-SF Residential Single-
Family N/A N/A
n/a R-T Transitional Residential N/A N/A
n/a R-25 Residential N/A N/A
n/a R-O Residential N/A N/A
n/a PRD Planned Residential
District (City Zoning)N/A N/A
Note:
• Properties are keyed to Figure 2B.
TABLE 3
LAND USE INFORMATION
HANDY CORNER (INCIDENT NO. 48992)
Page 1 of 1
Facility ID # : 0-014377
Well ID. Tax Parcel I.D. Well Owner Mailing Address Well Address Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municipal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Distance
from source
area of
release
(ft.)
WSW-1 59078 Bradley C. and Jennifer S. Keneda 2098 Startown Rd,
Lincolnton, NC 28092
2098 Startown Rd,
Lincolnton, NC 28092 Active Potable Yes No ~240
WSW-2 59077 Sandi E. Alvarado 2110 Startown Rd,
Lincolnton, NC 28092
2110 Startown Rd,
Lincolnton, NC 28092 Active Potable Yes No ~485
WSW-3 59076 Ruth B. Johnson Estate of the High
Judy Johnson As Executrix
1643 Startown Rd,
Lincolnton, NC 28092
2126 Startown Rd,
Lincolnton, NC 28092 Active Potable Yes No ~610
WSW-4 59075 Brett J. and Connie G. Silvia Life
Estate
2138 Startown Rd,
Lincolnton, NC 28092
2138 Startown Rd,
Lincolnton, NC 28092 Active Potable Yes No ~765
WSW-5 73256 James K. Payseur (Delores)2146 Startown Rd,
Lincolnton, NC 28092
2146 Startown Rd*,
Lincolnton, NC 28092 Active Potable Yes No ~845
WSW-6 19155 John D. and Dawn M. Harrison 1146 Carlos Rd,
Lincolnton, NC 28092
1146 Carlos Rd,
Lincolnton, NC 28092 Active Potable No No ~1,310
WSW-7 19527 Jaden and Chelsea Angle 1132 Carlos Rd,
Lincolnton, NC 28092
1132 Carlos Rd,
Lincolnton, NC 28092 Active Potable No No ~1,410
WSW-8 19544 Stoney G. and Jennifer R. Haynes 1127 Carlos Rd,
Lincolnton, NC 28092
1127 Carlos Rd,
Lincolnton, NC 28092 Active Potable No No ~1,190
WSW-9 19057 Michael T. and Bethanna W.
Macomson
2121 Startown Rd,
Lincolnton, NC 28092
2133 Startown Rd,
Lincolnton, NC 28092 Active Potable Yes No ~730
WSW-10 22826 Steven H. Bennett 3594 Maple Ridge Rd,
Maiden, NC 28650
2151 Startown Rd,
Lincolnton, NC 28092 Active Non-Potable Yes Yes ~860
WSW-11 2085 Startown Rd,
Lincolnton, NC 28092 Active Potable Yes No ~240
WSW-12 2065 Startown Rd,
Lincolnton, NC 28092 Active Potable Yes No ~220
WSW-13 18052 Luther Barker 862 Clarks Creek Rd,
Lincolnton, NC 28092
862 Clarks Creek Rd,
Lincolnton, NC 28092 Active Potable No No ~535
WSW-14 16614 Donald and Kay Lawing 852 Clarks Creek Rd,
Lincolnton, NC 28092
852 Clarks Creek Rd,
Lincolnton, NC 28092 Active Potable No No ~460
WSW-15 16707 J. Stephen High, Inc.1620 Startown Rd,
Lincolnton, NC 28092
814 Clarks Creek Rd,
Lincolnton, NC 28092 Active Potable No No ~900
WSW-16 19541 Heirs of John T. and Amy M. Carter 792 Clarks Creek Rd,
Lincolnton, NC 28092
792 Clarks Creek Rd,
Lincolnton, NC 28092 Active Potable No No ~1,015
WSW-17 16138 Glenda M. Rose 760 Clarks Creek Rd,
Lincolnton, NC 28092
760 Clarks Creek Rd,
Lincolnton, NC 28092 Active Potable No No ~1,365
WSW-18 19266 Melanie B. Givens 780 Clarks Creek Rd,
Lincolnton, NC 28092
780 Clarks Creek Rd,
Lincolnton, NC 28092 Active Potable No No ~1,190
WSW-19 19238 Robert L. and Deborah Goins 790 Clarks Creek Rd,
Lincolnton, NC 28092
790 Clarks Creek Rd,
Lincolnton, NC 28092 Active Potable No No ~1,020
William C. and Dianne P. Painter Life
Estate16181 2085 Startown Rd,
Lincolnton, NC 28092
Well Depth: 500 feet
Well Depth: 50 feet
Well Depth: 90 feet
Well Depth: 40 feet
TABLE 4
RECEPTOR INFORMATION
HANDY CORNER (INCIDENT NO. 48992)
Date: 07/26/23
Well Construction Details
(Depth, Screened Interval, Type of
Well, ect.)
Page 1 of 2
Receptor
ID
Latitude/
Longitude of Any
Significant Points
Up or Down-
Gradient
Distance
from
the source
area
of release
(ft.)
n/a n/a Up ~1,280
n/a n/a Down ~1,020
Notes:
• Receptors are shown on Figure 2A.
• n/a: not applicable.
• *: WSW-5 is located on an adjacent parcel to 2146 Startown Road that does not have an address; however, WSW-5 services 2146 Startown Road.
Pond West of the site Unknown Unknown
Unnamed Stream Southeast of the site Unknown Unknown
Description Location Contact/Phone Number Usage
Page 2 of 2
Date: 05/05/23 Facility ID #: 0-014377
Tax Parcel I.D. Property Owner Name Property Owner Address
52985 (site) Rhodes & Beal Oil Co., Inc.1404 E Main St.
Lincolnton, NC 28092
90391 Nisbet Oil Company 1818 Baxter St.
Charlotte NC 28204
18052 Luther Barker 862 Clarks Creek Rd.
Lincolnton, NC 28092
16614 Donald and Kay Lawing 852 Clark Creek Rd.
Lincolnton, NC 28092
15415 BBC Clark Creek, LLC 7224 Jameson Way
Stanley, NC 28164
16181 William C. and Dianne P. Painter Life
Estate
2085 Startown Rd.
Lincolnton, NC 28092
Note:
• Properties are keyed to Figure 2A.
TABLE 5
ADJACENT PROPERTY OWNER INFORMATION
HANDY CORNER (INCIDENT NO. 48992)
Page 1 of 1

APPENDICES

APPENDIX A
Water Use Questionnaires

APPENDIX B
Lincoln County Property Cards
7/12/23, 8:36 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=52985 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 52985 Owner RHODES & BEAL OIL CO INC
Map 3624 Mailing DBA HANDY CORNER
1404 E MAIN ST
Account 0061681 Address LINCOLNTON, NC 28092
Deed 854 227 Last Transaction Date 01/04/1994 Sale Price $105,000
Plat Subdivision Lot
Land Value $116,090 Improvement Value $199,222 Total Value $315,312
Previous Parcel
-----All values for Tax Year 2023 -----
Description LAND & SERVICE STA.Deed Acres 2.284
Address 2076 STARTOWN RD Tax Acres 1.888
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement CONVIENCE STORE Value $140,924
Main Sq Feet 2700 Stories 1 Year Built 1978
Zoning District Calc Acres
B-N 1.89
Voting Precinct Calc Acres
ST36 1.89
Watershed
1.89
Sewer District
1.89
Census County Tract Block
109 070800 3039 1.4
109 070800 3040 0.49
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.89
7/12/23, 8:36 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=90391 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 90391 Owner NISBET OIL COMPANY
Map 3624 Mailing 1818 BAXTER STREET
Account 0235711 Address CHARLOTTE, NC 28204
Deed 2274 179 Last Transaction Date 10/14/2011 Sale Price $12,000
Plat G 74 Subdivision LANDON HEIGHTS Lot PT 5
Land Value $2,448 Improvement Value $0 Total Value $2,448
Previous Parcel 18052
-----All values for Tax Year 2023 -----
Description PT5 LANDON HEIGHTS Deed Acres 0.39
Address STARTOWN RD Tax Acres 0.34
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement Value
Main Sq Feet Stories Year Built
Zoning District Calc Acres
R-SF 0.34
Voting Precinct Calc Acres
ST36 0.34
Watershed
0.34
Sewer District
0.34
Census County Tract Block
109 070800 3040 0.34
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 0.34
7/12/23, 8:37 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=18052 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 18052 Owner BARKER LUTHER
Map 3624 Mailing 862 CLARKS CREEK RD
Account 0220551 Address LINCOLNTON, NC 28092-7342
Deed 3051 899 Last Transaction Date 06/15/2021 Sale Price $180,000
Plat G 74 Subdivision LANDON HEIGHTS Lot PT 5 & PT 8
Land Value $29,802 Improvement Value $183,773 Total Value $213,575
Previous Parcel
-----All values for Tax Year 2023 -----
Description PT#5 & PT#8 LANDON HGHTS Deed Acres 1.959
Address 862 CLARKS CREEK RD Tax Acres 1.982
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement CONVENTIONAL (PRE WWII)Value $172,998
Main Sq Feet 1887 Stories 1 Year Built 1906
Zoning District Calc Acres
R-SF 1.98
Voting Precinct Calc Acres
ST36 1.98
Watershed
1.98
Sewer District
1.98
Census County Tract Block
109 070800 3039 1.71
109 070800 3040 0.27
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.98
7/12/23, 8:35 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16614 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for landconveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 16614 Owner LAWING DONALDLAWING KAY
Map 3624 Mailing 852 CLARK CREEK RD
Account 09941 Address LINCOLNTON, NC 280920000
Deed 643 575 Last Transaction Date 01/01/1992 Sale Price $0
Plat Subdivision Lot
Land Value $33,924 Improvement Value $291,450 Total Value $325,374
Previous Parcel
-----All values for Tax Year 2023 -----
Description REEP - RD 1282 Deed Acres 1.73
Address 852 CLARKS CREEK RD Tax Acres 1.545
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement CAPE COD Value $277,639
Main Sq Feet 2080 Stories 1 Year Built 1986
Zoning District Calc Acres
R-SF 1.54
Voting Precinct Calc Acres
ST36 1.54
Watershed
1.54
Sewer District
1.54
Census County Tract Block
109 070800 3039 1.54
109 070800 3040 0.01
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.54
7/12/23, 8:37 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=15415 1/2
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 15415 Owner BBC CLARK CREEK LLC
Map 3624 Mailing 7224 JAMESON WAY
Account 0291545 Address STANLEY, NC 28164
Deed 3180 688 Last Transaction Date 07/14/2022 Sale Price $0
Plat Subdivision Lot
Land Value $724,736 Improvement Value $0 Total Value $724,736
Previous Parcel
-----All values for Tax Year 2023 -----
Description STARTOWN RD INTERSECTION Deed Acres 86.906
Address CLARKS CREEK RD Tax Acres 84.654
Township LINCOLNTON Tax/Fire District LINCOLNTON
Main Improvement Value
Main Sq Feet Stories Year Built
Zoning District Calc Acres
PRD 84.65
Voting Precinct Calc Acres
ST36 84.65
Watershed
84.65
Sewer District
84.65
Census County Tract Block
109 070800 4007 81.92
109 070800 4008 2.73
Flood Zone Description Panel
X NO FLOOD HAZARD 3710363400 4.93
X NO FLOOD HAZARD 3710362400 67.68
7/12/23, 8:37 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=15415 2/2
SHAX 3710363400 0.76
AEFW FLOODWAY AREA - 100 YEAR FLOOD HAZARD 3710362400 0.82
SHAX 3710362400 0.57
AE SPECIAL FLOOD HAZARD AREA BASE ELEVATIONDETERMINED - 100 YEAR 3710362400 3.33
AE SPECIAL FLOOD HAZARD AREA BASE ELEVATIONDETERMINED - 100 YEAR 3710363400 3.05
AEFW FLOODWAY AREA - 100 YEAR FLOOD HAZARD 3710363400 3.51
7/12/23, 8:37 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16181 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 16181 Owner PAINTER WILLIAM CLINTON LIFESTPAINTER DIANNE P LIFE ESTATE
Map 3624 Mailing 2085 STARTOWN ROAD
Account 0266573 Address LINCOLNTON, NC 28092
Deed 2729 100 Last Transaction Date 03/13/2018 Sale Price $0
Plat Subdivision Lot
Land Value $431,617 Improvement Value $305,247 Total Value $736,864
Previous Parcel
-----All values for Tax Year 2023 -----
Description SMITH LAND - RD 1005 Deed Acres 0
Address 2085 STARTOWN RD Tax Acres 30.752
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $133,245
Main Sq Feet 1200 Stories 1 Year Built 1948
Zoning District Calc Acres
R-25 27.48
R-SF 3.27
Voting Precinct Calc Acres
ST36 30.75
Watershed
25.97
4.78
Sewer District
30.75
Census County Tract Block
109 070800 4012 30.75
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 30.75
7/12/23, 8:38 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=59078 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 59078 Owner KENEDA BRADLEY CHRISTOPHERKENEDA JENNIFER STATON
Map 3624 Mailing 2098 STARTOWN ROAD
Account 0108314 Address LINCOLNTON, NC 28092-9698
Deed 910 61 Last Transaction Date 07/27/1995 Sale Price $85,500
Plat G 74 Subdivision LANDON HEIGHTS Lot 4
Land Value $33,836 Improvement Value $220,773 Total Value $254,609
Previous Parcel
-----All values for Tax Year 2023 -----
Description #4 LANDON HEIGHTS Deed Acres 1.047
Address 2098 STARTOWN RD Tax Acres 0.966
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $206,121
Main Sq Feet 1400 Stories 1 Year Built 1995
Zoning District Calc Acres
R-SF 0.97
Voting Precinct Calc Acres
ST36 0.97
Watershed
0.04
0.93
Sewer District
0.97
Census County Tract Block
109 070800 3040 0.97
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 0.97
7/12/23, 8:38 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=59077 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 59077 Owner SANDI ELADIO ALVARADO
Map 3624 Mailing 2110 STARTOWN ROAD
Account 0273282 Address LINCOLNTON, NC 28092
Deed 2827 200 Last Transaction Date 06/27/2019 Sale Price $210,000
Plat G 74 Subdivision LANDON HEIGHTS Lot 3
Land Value $34,381 Improvement Value $232,684 Total Value $267,065
Previous Parcel
-----All values for Tax Year 2023 -----
Description #3 LANDON HEIGHTS Deed Acres 1.156
Address 2110 STARTOWN RD Tax Acres 1.053
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $226,299
Main Sq Feet 1570 Stories 1 Year Built 1995
Zoning District Calc Acres
R-SF 1.05
Voting Precinct Calc Acres
ST36 1.05
Watershed
0.35
0.7
Sewer District
1.05
Census County Tract Block
109 070800 3040 1.05
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.05
7/12/23, 8:39 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=59076 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 59076 Owner JOHNSON RUTH B ESTATE OF THEHIGH JUDY JOHNSON AS EXECUTRIX
Map 3624 Mailing 1643 STARTOWN RD
Account 0277493 Address LINCOLNTON, NC 28092
Deed 2907 540 Last Transaction Date 05/12/2020 Sale Price $173,500
Plat G 74 Subdivision LANDON HEIGHTS Lot 2
Land Value $34,115 Improvement Value $243,847 Total Value $277,962
Previous Parcel
-----All values for Tax Year 2023 -----
Description #2 LANDON HEIGHTS Deed Acres 1.128
Address 2126 STARTOWN RD Tax Acres 1.016
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $243,847
Main Sq Feet 1680 Stories 1 Year Built 1994
Zoning District Calc Acres
R-SF 1.02
Voting Precinct Calc Acres
ST36 1.02
Watershed
0.82
0.2
Sewer District
1.02
Census County Tract Block
109 070800 3039 0.22
109 070800 3040 0.8
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.02
7/12/23, 8:39 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=59075 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 59075 Owner SILVA BRETT J LIFE ESTATESILVA CONNIE G LIFE ESTATE
Map 3624 Mailing 2138 STARTOWN ROAD
Account 0268098 Address LINCOLNTON, NC 28092
Deed 2753 736 Last Transaction Date 06/29/2018 Sale Price $0
Plat G 74 Subdivision LANDON HEIGHTS Lot 1
Land Value $33,928 Improvement Value $277,771 Total Value $311,699
Previous Parcel
-----All values for Tax Year 2023 -----
Description #1 LANDON HEIGHTS Deed Acres 1.1
Address 2138 STARTOWN RD Tax Acres 0.985
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement CAPE COD Value $264,304
Main Sq Feet 2100 Stories 1.5 Year Built 1993
Zoning District Calc Acres
R-SF 0.99
Voting Precinct Calc Acres
ST36 0.99
Watershed
0.99
Sewer District
0.99
Census County Tract Block
109 070800 3039 0.99
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 0.99
7/12/23, 8:39 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=73256 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 73256 Owner PAYSEUR JAMES KEITH (DELORES)
Map 3624 Mailing 2146 STARTOWN RD
Account 11277 Address LINCOLNTON, NC 28092
Deed 1018 623 Last Transaction Date 12/04/1997 Sale Price $0
Plat G 74 Subdivision LANDON HEIGHTS Lot 7A
Land Value $3,639 Improvement Value $0 Total Value $3,639
Previous Parcel 59080
-----All values for Tax Year 2023 -----
Description #7A LANDON HEIGHTS Deed Acres 0.682
Address CARLOS RD Tax Acres 0.674
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement Value
Main Sq Feet Stories Year Built
Zoning District Calc Acres
R-SF 0.67
Voting Precinct Calc Acres
ST36 0.67
Watershed
0.67
Sewer District
0.67
Census County Tract Block
109 070800 3039 0.67
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 0.67
7/12/23, 8:45 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19155 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 19155 Owner HARRISON JOHN DAVIDHARRISON DAWN M
Map 3625 Mailing 1146 CARLOS RD
Account 0130069 Address LINCOLNTON, NC 28092-9508
Deed 1053 76 Last Transaction Date 06/24/1998 Sale Price $129,500
Plat Subdivision LINCOLN PARK Lot PT LTS 76 84 85
Land Value $30,158 Improvement Value $352,031 Total Value $382,189
Previous Parcel
-----All values for Tax Year 2023 -----
Description PT76 84 85 LIN PK Deed Acres 0
Address 1146 CARLOS RD Tax Acres 0.817
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement SPLIT LEVEL Value $337,568
Main Sq Feet 2385 Stories 1 Year Built 1972
Zoning District Calc Acres
R-SF 0.82
Voting Precinct Calc Acres
ST36 0.82
Watershed
0.68
0.14
Sewer District
0.82
Census County Tract Block
109 070800 3039 0.82
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362500 0.82
7/12/23, 8:45 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19527 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 19527 Owner ANGLE JADENANGLE CHELSEA
Map 3625 Mailing 1132 CARLOS ROAD
Account 0279225 Address LINCOLNTON, NC 28092
Deed 2925 708 Last Transaction Date 07/08/2020 Sale Price $290,000
Plat Subdivision LINCOLN PARK Lot PT 75 & 76
Land Value $28,000 Improvement Value $360,422 Total Value $388,422
Previous Parcel
-----All values for Tax Year 2023 -----
Description LIN PK 75&76 STARTOW Deed Acres 0
Address 1132 CARLOS RD Tax Acres 0.713
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $230,008
Main Sq Feet 1624 Stories 1 Year Built 1972
Zoning District Calc Acres
R-SF 0.71
Voting Precinct Calc Acres
ST36 0.71
Watershed
0.17
0.55
Sewer District
0.71
Census County Tract Block
109 070800 3039 0.71
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362500 0.71
7/12/23, 8:44 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19544 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 19544 Owner HAYNES STONEY GHAYNES JENNIFER R
Map 3625 Mailing 1127 CARLOS RD
Account 0257691 Address LINCOLNTON, NC 28092
Deed 2567 863 Last Transaction Date 02/05/2016 Sale Price $235,000
Plat Subdivision Lot
Land Value $91,925 Improvement Value $364,092 Total Value $456,017
Previous Parcel
-----All values for Tax Year 2023 -----
Description CROWELL RD 1005 Deed Acres 5.958
Address 1127 CARLOS RD Tax Acres 5.513
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $353,759
Main Sq Feet 2335 Stories 1 Year Built 1967
Zoning District Calc Acres
R-SF 5.51
Voting Precinct Calc Acres
ST36 5.51
Watershed
5.08
0.43
Sewer District
5.51
Census County Tract Block
109 070800 3039 5.51
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.38
X NO FLOOD HAZARD 3710362500 4.13
7/12/23, 8:42 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19057 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 19057 Owner MACOMSON MICHAEL TALBOTTMACOMSON BETHANNA W
Map 3624 Mailing 2121 STARTOWN RD
Account 0127797 Address LINCOLNTON, NC 28092
Deed 1033 476 Last Transaction Date 03/13/1998 Sale Price $275,000
Plat Subdivision Lot
Land Value $35,353 Improvement Value $317,984 Total Value $353,337
Previous Parcel
-----All values for Tax Year 2023 -----
Description SMITH LAND & HOME RD 1005 Deed Acres 0
Address 2133 STARTOWN RD Tax Acres 1.188
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $315,716
Main Sq Feet 2624 Stories 1 Year Built 1968
Zoning District Calc Acres
R-SF 1.19
Voting Precinct Calc Acres
ST36 1.19
Watershed
1.19
Sewer District
1.19
Census County Tract Block
109 070800 4012 1.19
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.19
7/12/23, 8:42 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=22826 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 22826 Owner BENNETT STEVEN H
Map 3624 Mailing 3594 MAPLE RIDGE LANE
Account 0271978 Address MAIDEN, NC 28650
Deed 2803 794 Last Transaction Date 03/19/2019 Sale Price $26,000
Plat Subdivision Lot
Land Value $33,256 Improvement Value $199,263 Total Value $232,519
Previous Parcel
-----All values for Tax Year 2023 -----
Description HEEDICK LD RD 1005 Deed Acres 1
Address 2151 STARTOWN RD Tax Acres 0.845
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $198,163
Main Sq Feet 1458 Stories 1 Year Built 1953
Zoning District Calc Acres
R-SF 0.85
Voting Precinct Calc Acres
ST36 0.85
Watershed
0.85
Sewer District
0.85
Census County Tract Block
109 070800 4012 0.85
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 0.85
7/12/23, 8:40 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16181 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 16181 Owner PAINTER WILLIAM CLINTON LIFESTPAINTER DIANNE P LIFE ESTATE
Map 3624 Mailing 2085 STARTOWN ROAD
Account 0266573 Address LINCOLNTON, NC 28092
Deed 2729 100 Last Transaction Date 03/13/2018 Sale Price $0
Plat Subdivision Lot
Land Value $431,617 Improvement Value $305,247 Total Value $736,864
Previous Parcel
-----All values for Tax Year 2023 -----
Description SMITH LAND - RD 1005 Deed Acres 0
Address 2085 STARTOWN RD Tax Acres 30.752
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $133,245
Main Sq Feet 1200 Stories 1 Year Built 1948
Zoning District Calc Acres
R-25 27.48
R-SF 3.27
Voting Precinct Calc Acres
ST36 30.75
Watershed
25.97
4.78
Sewer District
30.75
Census County Tract Block
109 070800 4012 30.75
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 30.75
7/12/23, 8:37 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=18052 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 18052 Owner BARKER LUTHER
Map 3624 Mailing 862 CLARKS CREEK RD
Account 0220551 Address LINCOLNTON, NC 28092-7342
Deed 3051 899 Last Transaction Date 06/15/2021 Sale Price $180,000
Plat G 74 Subdivision LANDON HEIGHTS Lot PT 5 & PT 8
Land Value $29,802 Improvement Value $183,773 Total Value $213,575
Previous Parcel
-----All values for Tax Year 2023 -----
Description PT#5 & PT#8 LANDON HGHTS Deed Acres 1.959
Address 862 CLARKS CREEK RD Tax Acres 1.982
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement CONVENTIONAL (PRE WWII)Value $172,998
Main Sq Feet 1887 Stories 1 Year Built 1906
Zoning District Calc Acres
R-SF 1.98
Voting Precinct Calc Acres
ST36 1.98
Watershed
1.98
Sewer District
1.98
Census County Tract Block
109 070800 3039 1.71
109 070800 3040 0.27
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.98
7/12/23, 8:35 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16614 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for landconveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 16614 Owner LAWING DONALDLAWING KAY
Map 3624 Mailing 852 CLARK CREEK RD
Account 09941 Address LINCOLNTON, NC 280920000
Deed 643 575 Last Transaction Date 01/01/1992 Sale Price $0
Plat Subdivision Lot
Land Value $33,924 Improvement Value $291,450 Total Value $325,374
Previous Parcel
-----All values for Tax Year 2023 -----
Description REEP - RD 1282 Deed Acres 1.73
Address 852 CLARKS CREEK RD Tax Acres 1.545
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement CAPE COD Value $277,639
Main Sq Feet 2080 Stories 1 Year Built 1986
Zoning District Calc Acres
R-SF 1.54
Voting Precinct Calc Acres
ST36 1.54
Watershed
1.54
Sewer District
1.54
Census County Tract Block
109 070800 3039 1.54
109 070800 3040 0.01
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.54
7/12/23, 8:42 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16707 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 16707 Owner J STEPHEN HIGH INC
Map 3624 Mailing 1620 STARTOWN RD
Account 0157151 Address LINCOLNTON, NC 28092-8041
Deed 2508 801 Last Transaction Date 07/14/2022 Sale Price $0
Plat Subdivision Lot
Land Value $38,136 Improvement Value $186,926 Total Value $225,062
Previous Parcel
-----All values for Tax Year 2023 -----
Description SMITH LD RD 1282 Deed Acres 2.75
Address 814 CLARKS CREEK RD Tax Acres 2.13
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $186,926
Main Sq Feet 1681 Stories 1 Year Built 1965
Zoning District Calc Acres
R-SF 2.13
Voting Precinct Calc Acres
ST36 2.13
Watershed
2.13
Sewer District
2.13
Census County Tract Block
109 070800 3039 2.13
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 2.13
7/12/23, 8:43 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19541 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 19541 Owner CARTER JOHN T HEIRS OFCARTER AMY M HEIRS OF AKA
MORRISON AMY HEIRS OF
Map 3624 Mailing 792 CLARKS CREEK
Account 0295479 Address LINCOLNTON, NC 28092
Deed LC110 102 Last Transaction Date 02/18/2023 Sale Price $0
Plat Subdivision Lot
Land Value $27,998 Improvement Value $136,742 Total Value $164,740
Previous Parcel
-----All values for Tax Year 2023 -----
Description SMITH-REEP LD- HMSIT Deed Acres 0.6
Address 792 CLARKS CREEK RD Tax Acres 0.545
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement RANCH Value $136,467
Main Sq Feet 1446 Stories 1 Year Built 1966
Zoning District Calc Acres
R-SF 0.55
Voting Precinct Calc Acres
ST36 0.55
Watershed
0.55
Sewer District
0.55
Census County Tract Block
109 070800 3039 0.55
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 0.55
7/12/23, 8:44 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16138 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 16138 Owner ROSE GLENDA MORGAN
Map 3624 Mailing 760 CLARK CREEK RD
Account 0089843 Address LINCOLNTON, NC 28092
Deed 18E 279 Last Transaction Date 04/24/2018 Sale Price $0
Plat Subdivision Lot
Land Value $51,081 Improvement Value $106,089 Total Value $157,170
Previous Parcel
-----All values for Tax Year 2023 -----
Description HOMESITE RD 1282 Deed Acres 3.86
Address 760 CLARKS CREEK RD Tax Acres 3.928
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement BUNGALOW Value $103,914
Main Sq Feet 1426 Stories 1 Year Built 1940
Zoning District Calc Acres
R-SF 3.93
Voting Precinct Calc Acres
ST36 3.93
Watershed
3.93
Sewer District
3.93
Census County Tract Block
109 070800 3039 3.93
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 3
X NO FLOOD HAZARD 3710362500 0.93
7/12/23, 8:43 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19266 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 19266 Owner GIVENS MELANIE BREWER
Map 3624 Mailing 780 CLARK CREEK RD
Account 0248454 Address LINCOLNTON, NC 28092-7341
Deed 2510 857 Last Transaction Date 07/14/2022 Sale Price $0
Plat Subdivision Lot
Land Value $38,172 Improvement Value $91,737 Total Value $129,909
Previous Parcel
-----All values for Tax Year 2023 -----
Description SMITH LD & D/W R1282 Deed Acres 0
Address 780 CLARKS CREEK RD Tax Acres 2.135
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement MANUFACTURED HOME Value $88,383
Main Sq Feet 1680 Stories 1 Year Built 1986
Zoning District Calc Acres
R-SF 2.13
Voting Precinct Calc Acres
ST36 2.13
Watershed
2.13
Sewer District
2.13
Census County Tract Block
109 070800 3039 2.13
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 2.1
X NO FLOOD HAZARD 3710362500 0.04
7/12/23, 8:43 AM Map with Parcel Information
https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19238 1/1
Lincoln County, NC
Office of the Tax Administrator, GIS Mapping Division
Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land
conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023
Parcel ID 19238 Owner GOINS ROBERT LGOINS DEBORAH
Map 3624 Mailing 790 CLARK CREEK RD
Account 07094 Address LINCOLNTON, NC 280920000
Deed 2477 165 Last Transaction Date 07/14/2022 Sale Price $0
Plat Subdivision Lot
Land Value $29,199 Improvement Value $88,806 Total Value $118,005
Previous Parcel
-----All values for Tax Year 2023 -----
Description HOMESITE W/DW RD1282 Deed Acres 1.29
Address 790 CLARKS CREEK RD Tax Acres 1.216
Township LINCOLNTON Tax/Fire District NORTH 321
Main Improvement MANUFACTURED HOME Value $81,071
Main Sq Feet 1456 Stories 1 Year Built 1986
Zoning District Calc Acres
R-SF 1.22
Voting Precinct Calc Acres
ST36 1.22
Watershed
1.22
Sewer District
1.22
Census County Tract Block
109 070800 3039 1.22
Flood Zone Description Panel
X NO FLOOD HAZARD 3710362400 1.22

APPENDIX C
Well Permit, Well Construction Records, and Subsurface Logs

North Carolina Department of Environmental Quality | Division of Water Resources
Mooresville Regional Office | 601 East Center Avenue, Suite 301 | Mooresville, NC 28115
704.663.1699
March 27, 2023

Mr. Jim White (via email)
Nisbet Oil Company
1818 Baxter Street
Charlotte, NC 28204
RE: Monitoring Well Construction Permit
Permit # WM0301269
2076 Startown Road, Lincolnton
Lincoln County

Dear Mr. White,

In accordance with your completed application received on March 27, 2023, we are forwarding
herewith Monitoring Well Construction Permit Numbered WM0301269 and issued for the
construction of four (4) monitoring wells located near the subject site in Lincolnton, Lincoln County.

This Permit will be effective for one year from the date of issuance and shall be subject to the
conditions and limitations as specified therein.

Should you have any questions, please contact Edward Watson at [phone], or by
email at [e-mail].

Sincerely,

Andrew H. Pitner, P.G., Assistant Regional Supervisor
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources

CC: WQROS, Central Office (via Laserfiche)
Joanna Alley, Geological Resources, Inc. (via email)
Geological Resources, Inc. (via email)
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES
PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL
In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws,
Rules and Regulations.
PERMISSION IS HEREBY GRANTED TO
Nisbet Oil Company (Geological Resources, Inc. as Agent)

FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of four (4) monitoring wells owned by Nisbet Oil
Company, at the subject site located at 2076 Startown Road, in Lincolnton, Lincoln County. This Permit is issued in
accordance with the application received on March 27, 2023, in conformity with specifications and supporting data, all of
which are filed with the Department of Environmental Quality and are considered integral parts of this Permit.
This Permit is for well construction only, and does not waive any provision or requirement of any other applicable law or
regulation. Construction of any well under this Permit shall be in strict compliance with the North Carolina Well Construction
Regulations and Standards (15A NCAC 02C .0100), and other State and Local Laws and regulations pertaining to well
construction.

If any requirements or limitations specified in this Permit are unacceptable, you have a right to an adjudicatory hearing upon
written request within 30 days of receipt of this Permit. The request must be in the form of a written petition conforming to
Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service
Center, Raleigh, North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding.
This Permit will be effective for one year from the date of its issuance and shall be subject to other specified conditions,
limitations, or exceptions as follows:

1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these wells are being installed as
part of an investigation for contamination from an underground storage tank or dry cleaner incident.
2. Issuance of this Permit does not supersede any other agreement, permit, or requirement issued by another agency.
3. The well(s) shall be located and constructed as shown on the attachments submitted as part of the Permit application.
4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC 02C .0108(o).
5. Well construction records (GW-1) for each well shall be submitted to the Division of Water Resources’ Information
Processing Unit within 30 days of the well completion.
6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A NCAC 02C .0113 and a
well abandonment record (GW-30) shall be submitted to the Division of Water Resources’ Information Processing
Unit within 30 days of the well abandonment.
7. If the well penetrates any water-bearing zone that contains contaminated waters, the upper three feet of the well
shall be grouted within one day after the casing is set or the well abandoned.
8. Temporary wells must be permanently abandoned or converted to a permanent well within seven days (168 hours)
of completion of drilling the borehole.

Permit issued the 27th day of March 2023

FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION

_______________________________________________
Andrew H. Pitner, P.G., Assistant Regional Supervisor
Division of Water Resources
By Authority of the Environmental Management Commission
Permit No. # WM0301269
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Handy Corner
6389
4/26/23
Jase Bowers
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-1
6"
35'
Well installed at completion
0 0.5 Asphalt
0.5 9.5 MW-1-5'Silt Red Dry
9.5 10 MW-1-10'Weathered rock
10 35 MW-1-15'Silt Brown Moist
MW-1-20'

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM -MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Handy Corner
6389
4/26/23
Jase Bowers
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-1
6"
100.00
26.23
18 35
16 18
0 16
0 0 0
0 20 2
20 35 2
16
18
35
20
35
WELL CONSTRUCTION RECORD
This form canbe usedforsingle or multiple wells
FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013
1.Well Contractor Information:
Well ContractorName
NC WellContractor Certification Number
CompanyName
2.Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3.Well Use (check well use):
Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)□Irrigation
Non-Water Supply Well:□Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks)
4.Date Well(s)Completed:____________Well ID#______________________
5a.Well Location:
Facility/Owner Name Facility ID#(if applicable)

Physical Address,City,and Zip
County Parcel Identification No.(PIN)
5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient)
N W
6.Is (are)the well(s):□Permanent or □Temporary
7.Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
9.Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below topof casing: (ft.)If water level is above casing, use “+”
11.Borehole diameter: (in.)
12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.)
FOR WATER SUPPLY WELLS ONLY:
13a.Yield (gpm) Method oftest:
13b.Disinfection type: Amount:
14.WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16.INNER CASING OR TUBING(geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS
22.Certification:
Signatureof Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617
24b.For Injection Wells ONLY:In addition to sending the form to the address in
24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636
24c.For Water Supply &Injection Wells:
Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed.
For Internal UseONLY:
_______________
Sam Bowers
3220-A
Geological Resources, Inc.
WM0301269
4/26/23 MW-1
Handy Corner 00-0-0000014377
2076 Startown Rd, Lincolnton, 28092
Lincoln 52985
35.51237333 81.26185667
35
26.23
6"
Solid Stem Auger
26.23 35 Brown Silt
0 0 0
0 20 2 Sch 40 PVC
20 35 2 0.010 Sch 40 PVC
0 16 grout pour
16 18 bentonite pour
18 35 #2 Sand Pour
0 0.5 Asphalt
0.5 9.5 Silt
9.5 10 Weathered rock
10 35 Silt
4/26/23
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Handy Corner
6389
7/5/23
Jase Bowers
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-2
6"
35'
Well installed at completion
0 6 Silt Brown Dry
6 11 Silt Red Dry
11 26 Silt Brown Dry
26 28 Silt Brown Moist
28 35 Fine Sand Brown Wet

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM -MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Handy Corner
6389
7/5/23
Jase Bowers
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-2
6"
102.49
26.13
18 35
16 18
0 16
0 20 2
20 35 2
16
18
35
20
35
WELL CONSTRUCTION RECORD
This form canbe usedforsingle or multiple wells
FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013
1.Well Contractor Information:
Well ContractorName
NC WellContractor Certification Number
CompanyName
2.Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3.Well Use (check well use):
Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)□Irrigation
Non-Water Supply Well:□Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks)
4.Date Well(s)Completed:____________Well ID#______________________
5a.Well Location:
Facility/Owner Name Facility ID#(if applicable)

Physical Address,City,and Zip
County Parcel Identification No.(PIN)
5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient)
N W
6.Is (are)the well(s):□Permanent or □Temporary
7.Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
9.Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below topof casing: (ft.)If water level is above casing, use “+”
11.Borehole diameter: (in.)
12.Well construction method:(i.e.auger,rotary,cable,direct push,etc.)
FOR WATER SUPPLY WELLS ONLY:
13a.Yield (gpm) Method oftest:
13b.Disinfection type: Amount:
14.WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16.INNER CASING OR TUBING(geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS
22.Certification:
Signatureof Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617
24b.For Injection Wells ONLY:In addition to sending the form to the address in
24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636
24c.For Water Supply &Injection Wells:
Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed.
For Internal UseONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
WM0301269
7/5/23 MW-2
Handy Corner 00-0-0000014377
2076 Startown Rd, Lincolnton, 28092
Lincoln 52985
35.51246718 81.26197593
1
35
26.13
6"
Solid Stem Auger
26.13 28 Silt
28 35 Fine Sand
0 20 2 Sch 40 PVC
20 35 2 0.010 Sch 40 PVC
0 16 grout pour
16 18 bentonite pour
18 35 #2 Sand Pour
0 6 Silt
6 11 Silt
11 26 Silt
26 28 Silt
28 35 Fine Sand
7/5/23
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Handy Corner
6389
7/5/23
Jase Bowers
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-3
6"
35'
Well installed at completion
0 0.4 Asphalt
0.4 12 Silt Red Dry
12 26 Silt Brown Dry
26 28 Silt Brown Moist
28 35 Fine Sand Brown Wet

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM -MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Handy Corner
6389
7/5/23
Jase Bowers
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-3
6"
98.80
25.26
18 35
16 18
0 16
0 20 2
20 35 2
16
18
35
20
35
WELL CONSTRUCTION RECORD
This form canbe usedforsingle or multiple wells
FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013
1.Well Contractor Information:
Well ContractorName
NC WellContractor Certification Number
CompanyName
2.Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3.Well Use (check well use):
Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)□Irrigation
Non-Water Supply Well:□Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks)
4.Date Well(s)Completed:____________Well ID#______________________
5a.Well Location:
Facility/Owner Name Facility ID#(if applicable)

Physical Address,City,and Zip
County Parcel Identification No.(PIN)
5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient)
N W
6.Is (are)the well(s):□Permanent or □Temporary
7.Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
9.Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below topof casing: (ft.)If water level is above casing, use “+”
11.Borehole diameter: (in.)
12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.)
FOR WATER SUPPLY WELLS ONLY:
13a.Yield (gpm) Method oftest:
13b.Disinfection type: Amount:
14.WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16.INNER CASING OR TUBING(geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS
22.Certification:
Signatureof Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617
24b.For Injection Wells ONLY:In addition to sending the form to the address in
24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636
24c.For Water Supply &Injection Wells:
Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed.
For Internal UseONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
WM0301269
7/5/23 MW-3
Handy Corner 00-0-0000014377
2076 Startown Rd, Lincolnton, 28092
Lincoln 52985
35.51237493 81.26171790
1
35
25.26
6"
Solid Stem Auger
25.26 28 Silt
28 35 Fine Sand
0 20 2 Sch 40 PVC
20 35 2 0.010 Sch 40 PVC
0 16 grout pour
16 18 bentonite pour
18 35 #2 Sand Pour
0 0.4 Asphalt
0.4 12 Silt
12 26 Silt
26 28 Silt
28 35 Fine Sand
7/5/23
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Handy Corner
6389
7/5/23
Jase Bowers
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-4
6"
35'
Well installed at completion
0 7 Silt Brown Dry
7 12 Silt Red Dry
12 27 Silt Brown Dry
27 29 Silt Brown Moist
29 35 Fine Sand Brown Wet

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM -MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Handy Corner
6389
7/5/23
Jase Bowers
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-4
6"
102.50
28.15
18 35
16 18
0 16
0 20 2
20 35 2
16
18
35
20
35
WELL CONSTRUCTION RECORD
This form canbe usedforsingle or multiple wells
FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013
1.Well Contractor Information:
Well ContractorName
NC WellContractor Certification Number
CompanyName
2.Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3.Well Use (check well use):
Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)□Irrigation
Non-Water Supply Well:□Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks)
4.Date Well(s)Completed:____________Well ID#______________________
5a.Well Location:
Facility/Owner Name Facility ID#(if applicable)

Physical Address,City,and Zip
County Parcel Identification No.(PIN)
5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient)
N W
6.Is (are)the well(s):□Permanent or □Temporary
7.Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
9.Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below topof casing: (ft.)If water level is above casing, use “+”
11.Borehole diameter: (in.)
12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.)
FOR WATER SUPPLY WELLS ONLY:
13a.Yield (gpm) Method oftest:
13b.Disinfection type:Amount:
14.WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16.INNER CASING OR TUBING(geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS
22.Certification:
Signatureof Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617
24b.For Injection Wells ONLY:In addition to sending the form to the address in
24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636
24c.For Water Supply &Injection Wells:
Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed.
For Internal UseONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
WM0301269
7/5/23 MW-4
Handy Corner 00-0-0000014377
2076 Startown Rd, Lincolnton, 28092
Lincoln 52985
35.51230351 81.26193415
1
35
28.15
6"
Solid Stem Auger
28.15 29 Silt
29 35 Fine Sand
0 20 2 Sch 40 PVC
20 35 2 0.010 Sch 40 PVC
0 16 grout pour
16 18 bentonite pour
18 35 #2 Sand Pour
0 7 Silt
7 12 Silt
12 27 Silt
27 29 Silt
29 35 Fine Sand
7/5/23

APPENDIX D
State Correspondence
1
Joanna Alley
From:Mills, Ryan <[e-mail]>
Sent:Monday, May 15, 2023 9:23 PM
To:Joanna Alley
Subject:RE: [External] Handy Corner
I’m not sure if I answered this or not, but yes please go ahead with the High risk LSA work.

Ryan Mills
Environmental Program Consultant, Division of Waste Management
UST Section – Corrective Action Branch
North Carolina Department of Environmental Quality
704.235.2175 (Office)
[e-mail]

From: Joanna Alley <[e-mail]>
Sent: Thursday, May 11, 2023 9:50 AM
To: Mills, Ryan <[e-mail]>
Cc: Taraban, Ron <[e-mail]>
Subject: RE: [External] Handy Corner

CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message
button located on your Outlook menu bar on the Home tab.

A Site Check was submi ed by a previous consultant and we submi ed the UST-61 form to Ron in March. I a ached the
email we sent to Ron that includes the Site Check and the UST-61 form.

This site does not have a prior release so we do not need a TA, but to go to the High Risk LSA, we do have you get your
agreement that the site meets the criteria (High Risk AND exceeds the applicable standards by a factor of 10). There
were a lot of potable wells within 1,000 feet and the contaminant concentra ons were above 10x 2L.

Best Regards,
Joanna Alley, P.E.
Project Manager
Geological Resources, Inc.
2021 Winner of the Union County Chamber Excellence In Business Award
3502 Hayes Road | Monroe, NC 28110 | website | facebook |
704-845-4010-office | 704-698-1244-direct | 704-845-4012-fax

2
From: Mills, Ryan <[e-mail]>
Sent: Thursday, May 11, 2023 9:43 AM
To: Joanna Alley <[e-mail]>
Cc: Taraban, Ron <[e-mail]>
Subject: RE: [External] Handy Corner

Where is this located?

Was a UST-61 turned in or a Site Check?

Ryan Mills
Environmental Program Consultant, Division of Waste Management
UST Section – Corrective Action Branch
North Carolina Department of Environmental Quality
704.235.2175 (Office)
[e-mail]

From: Joanna Alley <[e-mail]>
Sent: Thursday, May 11, 2023 8:42 AM
To: Mills, Ryan <[e-mail]>
Cc: Taraban, Ron <[e-mail]>
Subject: [External] Handy Corner

CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message
button located on your Outlook menu bar on the Home tab.

Good Morning Ryan,

I believe this site will be yours since is it Lincoln County. We performed a LSA and determined this site will be high risk. I
also just received the analy cal results and we have hit over 10x 2L, so this needs to go to a High Risk LSA. Do we have
your agreement on this?

Best Regards,
Joanna Alley, P.E.
Project Manager
Geological Resources, Inc.
2021 Winner of the Union County Chamber Excellence In Business Award
3502 Hayes Road | Monroe, NC 28110 | website | facebook |
704-845-4010-office | 704-698-1244-direct | 704-845-4012-fax

APPENDIX E
Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/10/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-121-0003 Client Project Description: Handy Corner
GRI #6389
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/1/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 51
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-121-0003
Page 2 of 51
Report Number:
Sample Summary Table
Client Project Description:
23-121-0003
Handy Corner
GRI #6389
Lab No Client Sample ID Matrix Date Collected Date Received
04/26/2023 14:14Aqueous 95155 MW-1 05/01/2023 16:51
04/26/2023 09:56Solids 95156 MW-1-5'05/01/2023 16:51
04/26/2023 10:08Solids 95157 MW-1-10'05/01/2023 16:51
04/26/2023 10:12Solids 95158 MW-1-15'05/01/2023 16:51
04/26/2023 10:19Solids 95159 MW-1-20'05/01/2023 16:51
04/26/2023 08:30Aqueous 95160 TB 05/01/2023 16:51
Page 3 of 51
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-121-0003
Report Limit
Project:Handy Corner
V 95155MW-1
0.414 05/04/2023 15:296010DLeadmg/L 0.120
38.7 05/07/2023 23:486200BBenzeneµg/L 0.180
0.929 05/07/2023 23:486200BBromodichloromethaneµg/L 0.160
J0.211 05/07/2023 23:486200Bn-Butylbenzene µg/L 0.180
J0.450 05/07/2023 23:486200Bsec-Butyl benzene µg/L 0.200
30.5 05/07/2023 23:486200BChloroformµg/L 0.220
1.61 05/07/2023 23:486200BDi-Isopropyl Ether (DIPE)µg/L 0.500
41.6 05/07/2023 23:486200BEthylbenzeneµg/L 0.170
20.0 05/07/2023 23:486200B2-Hexanone µg/L 0.380
3.07 05/07/2023 23:486200BIsopropylbenzeneµg/L 0.180
J0.241 05/07/2023 23:486200B4-Isopropyl toluene µg/L 0.089
7.98 05/07/2023 23:486200BMethyl Ethyl Ketone (MEK)µg/L 0.710
J0.969 05/07/2023 23:486200BMethyl tert-butyl ether (MTBE)µg/L 0.140
25.7 05/07/2023 23:486200B4-Methyl-2-Pentanone µg/L 0.078
J0.416 05/07/2023 23:486200BMethylene Chloride µg/L 0.330
4.91 05/07/2023 23:486200Bn-Propylbenzene µg/L 0.190
135 05/08/2023 20:366200BTolueneµg/L 2.20
48.4 05/07/2023 23:486200B1,2,4-Trimethylbenzene µg/L 0.190
26.9 05/07/2023 23:486200B1,3,5-Trimethylbenzene µg/L 0.180
131 05/08/2023 20:366200Bo-Xylene µg/L 2.10
246 05/08/2023 20:366200Bm,p-Xylene µg/L 4.20
377 05/08/2023 20:366200BXylene (Total)µg/L 2.10
235 05/01/2023 14:22CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 11.5
241 05/01/2023 14:22CALCULATIONAromatic C9-C10 (Adjusted)µg/L 4.02
409 05/01/2023 14:22MADEP-VPH Aliphatic C5-C8 µg/L 11.5
665 05/01/2023 14:22MADEP-VPH Aliphatic C9-C12 µg/L 25.8
241 05/01/2023 14:22MADEP-VPH Aromatic C9-C10 µg/L 4.02
V 95156MW-1-5'
J0.013 05/02/2023 12:328260DAcetonemg/Kg - dry 0.002
J0.0009 05/02/2023 12:328260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
19.6 05/03/2023 10:50SW-DRYWT Moisture %
V 95159MW-1-20'
0.098 05/02/2023 12:598260DAcetonemg/Kg - dry 0.003
0.032 05/02/2023 12:598260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.002 05/02/2023 12:598260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.0009 05/02/2023 12:598260DToluenemg/Kg - dry 0.0009
Page 4 of 51
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-121-0003
Report Limit
Project:Handy Corner
V 95159MW-1-20'
J0.001 05/02/2023 12:598260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0007 05/02/2023 12:598260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.002 05/02/2023 12:598260Do-Xylene mg/Kg - dry 0.0007
J0.002 05/02/2023 12:598260Dm,p-Xylene mg/Kg - dry 0.001
J0.005 05/02/2023 12:598260DXylene (Total)mg/Kg - dry 0.0007
23.5 05/03/2023 10:50SW-DRYWT Moisture %
Page 5 of 51

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Handy Corner Lab Report Number: 23-121-0003
Date: 5/10/2023
EDB and DBCP by Microextraction GC/ECD Method EPA-504.1 Analyte: 1,2-Dibromoethane QC Batch No: V32736/V32711
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Massachusetts VPH Method MADEP-VPH Sample 95156 (MW-1-5')
QC Batch No: V32693 No VPH vials received. Sample prepared from bulk container.
Sample 95159 (MW-1-20')
QC Batch No: V32693 No VPH vials received. Sample prepared from bulk container.
Sample 95156 (MW-1-5')
Analyte: 2,5-Dibromotoluene (PID) QC Batch No: V32693/V32692
Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 95159 (MW-1-20') Analyte: 2,5-Dibromotoluene (PID)
QC Batch No: V32693/V32692 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits. Metals Analysis Method 6010D Sample 95155 (MW-1) QC Batch No: V32792/V32658
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 94887 Analyte: Lead QC Batch No: V32755/V32658 LLC failed high. Sample concentration BRL. Result not affected.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: 2-Butanone QC Batch No: V32695/V32694 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 6 of 51

Analyte: 2-Hexanone
QC Batch No: V32695/V32694 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Trichloroethene
QC Batch No: V32695/V32694 CCV result is above control limits but within method parameters. Results are reported but considered estimated.

Page 7 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1
95155 Matrix:
4/26/2023 14:14
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
0.414 mg/L 0.120 0.300Lead 50 05/04/23 15:29 6010DJKC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1
95155 Matrix:
4/26/2023 14:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32933 05/07/23 09:00 V32972 05/08/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 05/07/23 23:48 V32934MSA
38.7 µg/L 0.180 0.500Benzene 1 05/07/23 23:48 V32934MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/07/23 23:48 V32934MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/07/23 23:48 V32934MSA
0.929 µg/L 0.160 0.500Bromodichloromethane 1 05/07/23 23:48 V32934MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/07/23 23:48 V32934MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/07/23 23:48 V32934MSA
0.211 J µg/L 0.180 0.500n-Butylbenzene 1 05/07/23 23:48 V32934MSA
0.450 J µg/L 0.200 0.500sec-Butyl benzene 1 05/07/23 23:48 V32934MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/07/23 23:48 V32934MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/07/23 23:48 V32934MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/07/23 23:48 V32934MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/07/23 23:48 V32934MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/07/23 23:48 V32934MSA
30.5 µg/L 0.220 0.500Chloroform 1 05/07/23 23:48 V32934MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 05/07/23 23:48 V32934MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/07/23 23:48 V32934MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/07/23 23:48 V32934MSA
1.61 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 05/07/23 23:48 V32934MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/07/23 23:48 V32934MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 05/07/23 23:48 V32934MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/07/23 23:48 V32934MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1
95155 Matrix:
4/26/2023 14:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32933 05/07/23 09:00 V32972 05/08/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/07/23 23:48 V32934MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/07/23 23:48 V32934MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/07/23 23:48 V32934MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/07/23 23:48 V32934MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/07/23 23:48 V32934MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/07/23 23:48 V32934MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/07/23 23:48 V32934MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/07/23 23:48 V32934MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/07/23 23:48 V32934MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/07/23 23:48 V32934MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/07/23 23:48 V32934MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/07/23 23:48 V32934MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/07/23 23:48 V32934MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/07/23 23:48 V32934MSA
<42.0 µg/L 42.0 200Ethanol 1 05/07/23 23:48 V32934MSA
41.6 µg/L 0.170 0.500Ethylbenzene 1 05/07/23 23:48 V32934MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 05/07/23 23:48 V32934MSA
20.0 µg/L 0.380 1.002-Hexanone 1 05/07/23 23:48 V32934MSA
3.07 µg/L 0.180 0.500Isopropylbenzene 1 05/07/23 23:48 V32934MSA
0.241 J µg/L 0.089 0.5004-Isopropyl toluene 1 05/07/23 23:48 V32934MSA
7.98 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/07/23 23:48 V32934MSA
0.969 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 05/07/23 23:48 V32934MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1
95155 Matrix:
4/26/2023 14:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32933 05/07/23 09:00 V32972 05/08/23 09:00
25.7 µg/L 0.078 1.004-Methyl-2-Pentanone 1 05/07/23 23:48 V32934MSA
0.416 J µg/L 0.330 2.00Methylene Chloride 1 05/07/23 23:48 V32934MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/07/23 23:48 V32934MSA
4.91 µg/L 0.190 0.500n-Propylbenzene 1 05/07/23 23:48 V32934MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/07/23 23:48 V32934MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/07/23 23:48 V32934MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/07/23 23:48 V32934MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 05/07/23 23:48 V32934MSA
135 µg/L 2.20 5.00Toluene 10 05/08/23 20:36 V32973MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 05/07/23 23:48 V32934MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 05/07/23 23:48 V32934MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/07/23 23:48 V32934MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/07/23 23:48 V32934MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 05/07/23 23:48 V32934MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/07/23 23:48 V32934MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 05/07/23 23:48 V32934MSA
48.4 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 05/07/23 23:48 V32934MSA
26.9 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/07/23 23:48 V32934MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 05/07/23 23:48 V32934MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/07/23 23:48 V32934MSA
131 µg/L 2.10 5.00o-Xylene 10 05/08/23 20:36 V32973MSA
246 µg/L 4.20 10.0m,p-Xylene 10 05/08/23 20:36 V32973MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1
95155 Matrix:
4/26/2023 14:14
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32933 05/07/23 09:00 V32972 05/08/23 09:00
377 µg/L 2.10 5.00Xylene (Total)10 05/08/23 20:36 V32973
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%05/07/23 23:481 MSA V32934
Surrogate: Dibromofluoromethane 103 Limits: 70-130%05/07/23 23:481 MSA V32934
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%05/07/23 23:481 MSA V32934
Surrogate: Toluene-d8 99.4 Limits: 70-130%05/07/23 23:481 MSA V32934
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/08/23 20:3610 MSA V32973
Surrogate: Dibromofluoromethane 106 Limits: 70-130%05/08/23 20:3610 MSA V32973
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%05/08/23 20:3610 MSA V32973
Surrogate: Toluene-d8 97.2 Limits: 70-130%05/08/23 20:3610 MSA V32973
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V32711 05/03/23 10:20
<0.00338 µg/L 0.00338 0.02051,2-Dibromoethane 1 05/03/23 13:55 V32736TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1
95155 Matrix:
4/26/2023 14:14
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
235 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 05/01/23 14:22
<25.8 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 05/01/23 14:22
241 µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 05/01/23 14:22
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32650 05/01/23 08:00
409 µg/L 11.5 50.0Aliphatic C5-C8 1 05/01/23 14:22 V32651TBL
665 µg/L 25.8 50.0Aliphatic C9-C12 1 05/01/23 14:22 V32651TBL
241 µg/L 4.02 50.0Aromatic C9-C10 1 05/01/23 14:22 V32651TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)88.1 Limits: 70-130%05/01/23 14:221 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)100 Limits: 70-130%05/01/23 14:221 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-5'
95156 Matrix:
4/26/2023 9:56
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.6 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-5'
95156 Matrix:
4/26/2023 9:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
0.013 J mg/Kg - dry 0.002 0.024Acetone 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 05/02/23 12:32 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 05/02/23 12:32 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/02/23 12:32 V32695TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 05/02/23 12:32 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 05/02/23 12:32 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/02/23 12:32 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/02/23 12:32 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/02/23 12:32 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/02/23 12:32 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-5'
95156 Matrix:
4/26/2023 9:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 05/02/23 12:32 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/02/23 12:32 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/02/23 12:32 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 05/02/23 12:32 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/02/23 12:32 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/02/23 12:32 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/02/23 12:32 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 12:32 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 05/02/23 12:32 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 05/02/23 12:32 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-5'
95156 Matrix:
4/26/2023 9:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/02/23 12:32 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 05/02/23 12:32 V32695TBL
0.0009 J mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/02/23 12:32 V32695TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/02/23 12:32 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/02/23 12:32 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 05/02/23 12:32 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/02/23 12:32 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/02/23 12:32 V32695TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/02/23 12:32 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/02/23 12:32 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-5'
95156 Matrix:
4/26/2023 9:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/02/23 12:32 V32695TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/02/23 12:32 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/02/23 12:32 V32695
Surrogate: 4-Bromofluorobenzene 85.1 Limits: 70-130%05/02/23 12:321 TBL V32695
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/02/23 12:321 TBL V32695
Surrogate: Toluene-d8 88.5 Limits: 76-129%05/02/23 12:321 TBL V32695
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-5'
95156 Matrix:
4/26/2023 9:56
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.52 mg/Kg - dry 1.52 9.95Aliphatic C5-C8 (Adjusted)1 05/02/23 12:32
<5.67 mg/Kg - dry 5.67 9.95Aliphatics C9-C12 (Adjusted)1 05/02/23 12:32
<0.776 mg/Kg - dry 0.776 9.95Aromatic C9-C10 (Adjusted)100 05/02/23 17:08
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
<1.52 mg/Kg - dry 1.52 9.95Aliphatic C5-C8 100 05/02/23 17:08 V32693TBL
<5.67 mg/Kg - dry 5.67 9.95Aliphatic C9-C12 100 05/02/23 17:08 V32693TBL
<0.776 mg/Kg - dry 0.776 9.95Aromatic C9-C10 100 05/02/23 17:08 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)94.4 Limits: 70-130%05/02/23 17:08100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)145 *Limits: 70-130%05/02/23 17:08100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-10'
95157 Matrix:
4/26/2023 10:08
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
<1.22 mg/Kg 1.22 8.00Aliphatic C5-C8 100 05/02/23 17:31 V32693TBL
<4.56 mg/Kg 4.56 8.00Aliphatic C9-C12 100 05/02/23 17:31 V32693TBL
<0.624 mg/Kg 0.624 8.00Aromatic C9-C10 100 05/02/23 17:31 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)91.2 Limits: 70-130%05/02/23 17:31100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)92.2 Limits: 70-130%05/02/23 17:31100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-15'
95158 Matrix:
4/26/2023 10:12
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
<1.22 mg/Kg 1.22 8.00Aliphatic C5-C8 100 05/02/23 17:55 V32693TBL
<4.56 mg/Kg 4.56 8.00Aliphatic C9-C12 100 05/02/23 17:55 V32693TBL
<0.624 mg/Kg 0.624 8.00Aromatic C9-C10 100 05/02/23 17:55 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)98.1 Limits: 70-130%05/02/23 17:55100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)100 Limits: 70-130%05/02/23 17:55100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-20'
95159 Matrix:
4/26/2023 10:19
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.5 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-20'
95159 Matrix:
4/26/2023 10:19
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
0.098 mg/Kg - dry 0.003 0.026Acetone 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/02/23 12:59 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/02/23 12:59 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 05/02/23 12:59 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/02/23 12:59 V32695TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/02/23 12:59 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/02/23 12:59 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/02/23 12:59 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 05/02/23 12:59 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/02/23 12:59 V32695TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/02/23 12:59 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/02/23 12:59 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/02/23 12:59 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/02/23 12:59 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/02/23 12:59 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/02/23 12:59 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-20'
95159 Matrix:
4/26/2023 10:19
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/02/23 12:59 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/02/23 12:59 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 05/02/23 12:59 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/02/23 12:59 V32695TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/02/23 12:59 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/02/23 12:59 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/02/23 12:59 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/02/23 12:59 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/02/23 12:59 V32695TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/02/23 12:59 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/02/23 12:59 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/02/23 12:59 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/02/23 12:59 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-20'
95159 Matrix:
4/26/2023 10:19
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/02/23 12:59 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/02/23 12:59 V32695TBL
0.032 mg/Kg - dry 0.0008 0.026Methyl Ethyl Ketone (MEK)1 05/02/23 12:59 V32695TBL
0.002 J mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/02/23 12:59 V32695TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/02/23 12:59 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/02/23 12:59 V32695TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/02/23 12:59 V32695TBL
0.0009 J mg/Kg - dry 0.0009 0.006Toluene 1 05/02/23 12:59 V32695TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/02/23 12:59 V32695TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/02/23 12:59 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/02/23 12:59 V32695TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/02/23 12:59 V32695TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/02/23 12:59 V32695TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/02/23 12:59 V32695TBL
0.001 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/02/23 12:59 V32695TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-20'
95159 Matrix:
4/26/2023 10:19
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32694 05/02/23 08:00
0.0007 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/02/23 12:59 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/02/23 12:59 V32695TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 05/02/23 12:59 V32695TBL
0.002 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/02/23 12:59 V32695TBL
0.002 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/02/23 12:59 V32695TBL
0.005 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/02/23 12:59 V32695KCC
Surrogate: 4-Bromofluorobenzene 96.5 Limits: 70-130%05/02/23 12:591 TBL V32695
Surrogate: Dibromofluoromethane 100 Limits: 84-123%05/02/23 12:591 TBL V32695
Surrogate: Toluene-d8 87.8 Limits: 76-129%05/02/23 12:591 TBL V32695
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:MW-1-20'
95159 Matrix:
4/26/2023 10:19
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.59 mg/Kg - dry 1.59 10.5Aliphatic C5-C8 (Adjusted)100 05/02/23 18:18
<5.96 mg/Kg - dry 5.96 10.5Aliphatics C9-C12 (Adjusted)100 05/02/23 18:18
<0.815 mg/Kg - dry 0.815 10.5Aromatic C9-C10 (Adjusted)100 05/02/23 18:18
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00
<1.59 mg/Kg - dry 1.59 10.5Aliphatic C5-C8 100 05/02/23 18:18 V32693TBL
<5.96 mg/Kg - dry 5.96 10.5Aliphatic C9-C12 100 05/02/23 18:18 V32693TBL
<0.815 mg/Kg - dry 0.815 10.5Aromatic C9-C10 100 05/02/23 18:18 V32693TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)95.3 Limits: 70-130%05/02/23 18:18100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)134 *Limits: 70-130%05/02/23 18:18100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:TB
95160 Matrix:
4/26/2023 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32933 05/07/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 05/07/23 20:37 V32934MSA
<0.180 µg/L 0.180 0.500Benzene 1 05/07/23 20:37 V32934MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/07/23 20:37 V32934MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/07/23 20:37 V32934MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/07/23 20:37 V32934MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/07/23 20:37 V32934MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/07/23 20:37 V32934MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 05/07/23 20:37 V32934MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 05/07/23 20:37 V32934MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/07/23 20:37 V32934MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/07/23 20:37 V32934MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/07/23 20:37 V32934MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/07/23 20:37 V32934MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/07/23 20:37 V32934MSA
<0.220 µg/L 0.220 0.500Chloroform 1 05/07/23 20:37 V32934MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 05/07/23 20:37 V32934MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/07/23 20:37 V32934MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/07/23 20:37 V32934MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 05/07/23 20:37 V32934MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/07/23 20:37 V32934MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/07/23 20:37 V32934MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 05/07/23 20:37 V32934MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:TB
95160 Matrix:
4/26/2023 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32933 05/07/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/07/23 20:37 V32934MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/07/23 20:37 V32934MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/07/23 20:37 V32934MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/07/23 20:37 V32934MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/07/23 20:37 V32934MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/07/23 20:37 V32934MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/07/23 20:37 V32934MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/07/23 20:37 V32934MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/07/23 20:37 V32934MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/07/23 20:37 V32934MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/07/23 20:37 V32934MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/07/23 20:37 V32934MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/07/23 20:37 V32934MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/07/23 20:37 V32934MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/07/23 20:37 V32934MSA
<42.0 µg/L 42.0 200Ethanol 1 05/07/23 20:37 V32934MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 05/07/23 20:37 V32934MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 05/07/23 20:37 V32934MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 05/07/23 20:37 V32934MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 05/07/23 20:37 V32934MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/07/23 20:37 V32934MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/07/23 20:37 V32934MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:TB
95160 Matrix:
4/26/2023 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32933 05/07/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 05/07/23 20:37 V32934MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 05/07/23 20:37 V32934MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 05/07/23 20:37 V32934MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/07/23 20:37 V32934MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/07/23 20:37 V32934MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/07/23 20:37 V32934MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/07/23 20:37 V32934MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/07/23 20:37 V32934MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 05/07/23 20:37 V32934MSA
<0.220 µg/L 0.220 0.500Toluene 1 05/07/23 20:37 V32934MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 05/07/23 20:37 V32934MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 05/07/23 20:37 V32934MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/07/23 20:37 V32934MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/07/23 20:37 V32934MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 05/07/23 20:37 V32934MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/07/23 20:37 V32934MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 05/07/23 20:37 V32934MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 05/07/23 20:37 V32934MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/07/23 20:37 V32934MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 05/07/23 20:37 V32934MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/07/23 20:37 V32934MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 05/07/23 20:37 V32934MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 51
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-121-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 05/01/2023
Handy Corner
Report Date : 05/10/2023
Sample ID :
Lab No :
Sampled:TB
95160 Matrix:
4/26/2023 8:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V32933 05/07/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 05/07/23 20:37 V32934MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 05/07/23 20:37 V32934
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/07/23 20:371 MSA V32934
Surrogate: Dibromofluoromethane 103 Limits: 70-130%05/07/23 20:371 MSA V32934
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%05/07/23 20:371 MSA V32934
Surrogate: Toluene-d8 96.8 Limits: 70-130%05/07/23 20:371 MSA V32934
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Metals Analysis
6010D
V32755QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V32658
Associated Lab Samples: 95155
LRB-V32658 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/03/23 14:160.0060.002<0.002mg/LLead
LCS-V32658Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1050.1050.100mg/LLead 80-120
V 94887-MS-V32658 V 94887-MSD-V32658Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.103 1030.1080.1000.100< 0.002mg/LLead 108 75-125 4.7 20.0
V 94887-PDS-V32658Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/03/23 16:441010.252mg/LLead
Page 1 of 18Date:05/10/2023 04:30 PM
Page 32 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32934QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32933
Associated Lab Samples: 95155, 95160
LRB-V32933 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/07/23 19:4310.01.80<1.80µg/LAcetone
05/07/23 19:430.5000.180<0.180µg/LBenzene
05/07/23 19:430.5000.210<0.210µg/LBromobenzene
05/07/23 19:431.000.420<0.420µg/LBromochloromethane
05/07/23 19:430.5000.160<0.160µg/LBromodichloromethane
05/07/23 19:435.001.50<1.50µg/LBromoform
05/07/23 19:431.000.280<0.280µg/LBromomethane
05/07/23 19:430.5000.180<0.180µg/Ln-Butylbenzene
05/07/23 19:430.5000.200<0.200µg/Lsec-Butyl benzene
05/07/23 19:432.000.920<0.920µg/Ltert-Butyl benzene
05/07/23 19:430.5000.180<0.180µg/LCarbon Tetrachloride
05/07/23 19:430.5000.190<0.190µg/LChlorobenzene
05/07/23 19:430.5000.190<0.190µg/LChlorodibromomethane
05/07/23 19:431.000.430<0.430µg/LChloroethane
05/07/23 19:430.5000.220<0.220µg/LChloroform
05/07/23 19:430.5000.220<0.220µg/LChloromethane
05/07/23 19:430.5000.200<0.200µg/L2-Chlorotoluene
05/07/23 19:430.5000.200<0.200µg/L4-Chlorotoluene
05/07/23 19:430.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
05/07/23 19:432.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
05/07/23 19:430.5000.200<0.200µg/L1,2-Dibromoethane
05/07/23 19:430.5000.230<0.230µg/LDibromomethane
05/07/23 19:430.5000.220<0.220µg/L1,2-Dichlorobenzene
05/07/23 19:430.5000.190<0.190µg/L1,3-Dichlorobenzene
05/07/23 19:430.5000.210<0.210µg/L1,4-Dichlorobenzene
05/07/23 19:435.001.20<1.20µg/LDichlorodifluoromethane
05/07/23 19:430.5000.240<0.240µg/L1,1-Dichloroethane
Page 2 of 18Date:05/10/2023 04:30 PM
Page 33 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32934QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32933
Associated Lab Samples: 95155, 95160
LRB-V32933 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/07/23 19:430.5000.150<0.150µg/L1,2-Dichloroethane
05/07/23 19:430.5000.150<0.150µg/L1,1-Dichloroethene
05/07/23 19:430.5000.200<0.200µg/Lcis-1,2-Dichloroethene
05/07/23 19:430.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
05/07/23 19:430.5000.190<0.190µg/L1,2-Dichloropropane
05/07/23 19:430.5000.130<0.130µg/L1,3-Dichloropropane
05/07/23 19:432.000.210<0.210µg/L2,2-Dichloropropane
05/07/23 19:430.5000.200<0.200µg/L1,1-Dichloropropene
05/07/23 19:430.5000.210<0.210µg/Lcis-1,3-Dichloropropene
05/07/23 19:430.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
05/07/23 19:4320042.0<42.0µg/LEthanol
05/07/23 19:430.5000.170<0.170µg/LEthylbenzene
05/07/23 19:433.000.350<0.350µg/LHexachlorobutadiene
05/07/23 19:431.000.380<0.380µg/L2-Hexanone
05/07/23 19:430.5000.180<0.180µg/LIsopropylbenzene
05/07/23 19:430.5000.089<0.089µg/L4-Isopropyl toluene
05/07/23 19:435.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
05/07/23 19:431.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
05/07/23 19:431.000.078<0.078µg/L4-Methyl-2-Pentanone
05/07/23 19:432.000.330<0.330µg/LMethylene Chloride
05/07/23 19:431.000.470<0.470µg/LNaphthalene
05/07/23 19:430.5000.190<0.190µg/Ln-Propylbenzene
05/07/23 19:430.5000.220<0.220µg/LStyrene
05/07/23 19:430.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
05/07/23 19:430.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
05/07/23 19:430.5000.220<0.220µg/LTetrachloroethene
05/07/23 19:430.5000.220<0.220µg/LToluene
Page 3 of 18Date:05/10/2023 04:30 PM
Page 34 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32934QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32933
Associated Lab Samples: 95155, 95160
LRB-V32933 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/07/23 19:430.5000.380<0.380µg/L1,2,3-Trichlorobenzene
05/07/23 19:430.5000.310<0.310µg/L1,2,4-Trichlorobenzene
05/07/23 19:430.5000.160<0.160µg/L1,1,1-Trichloroethane
05/07/23 19:430.5000.096<0.096µg/L1,1,2-Trichloroethane
05/07/23 19:430.5000.180<0.180µg/LTrichloroethene
05/07/23 19:430.5000.180<0.180µg/LTrichlorofluoromethane
05/07/23 19:430.5000.270<0.270µg/L1,2,3-Trichloropropane
05/07/23 19:430.5000.190<0.190µg/L1,2,4-Trimethylbenzene
05/07/23 19:430.5000.180<0.180µg/L1,3,5-Trimethylbenzene
05/07/23 19:435.001.00<1.00µg/LVinyl Acetate
05/07/23 19:430.5000.170<0.170µg/LVinyl Chloride
05/07/23 19:430.5000.210<0.210µg/Lo-Xylene
05/07/23 19:431.000.420<0.420µg/Lm,p-Xylene
05/07/23 19:434-Bromofluorobenzene (S)101 70-130
05/07/23 19:43Dibromofluoromethane (S)102 70-130
05/07/23 19:431,2-Dichloroethane - d4 (S)105 70-130
05/07/23 19:43Toluene-d8 (S)97.0 70-130
LCS-V32933 LCSD-V32933Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.1 90.295.538.240.0µg/LAcetone 40-160 5.6 20.0
19.4 97.010320.620.0µg/LBenzene 70-130 6.0 20.0
19.9 99.510320.620.0µg/LBromobenzene 70-130 3.4 20.0
20.7 10410721.420.0µg/LBromochloromethane 70-130 3.3 20.0
20.9 10511021.920.0µg/LBromodichloromethane 70-130 4.6 20.0
Page 4 of 18Date:05/10/2023 04:30 PM
Page 35 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32934QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32933
LCS-V32933 LCSD-V32933Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.6 10310520.920.0µg/LBromoform 70-130 1.4 20.0
19.2 96.098.019.620.0µg/LBromomethane 60-140 2.0 20.0
18.3 91.597.519.520.0µg/Ln-Butylbenzene 70-130 6.3 20.0
19.0 95.010020.020.0µg/Lsec-Butyl benzene 70-130 5.1 20.0
19.6 98.010320.520.0µg/Ltert-Butyl benzene 70-130 4.4 20.0
22.1 11111623.220.0µg/LCarbon Tetrachloride 70-130 4.8 20.0
19.4 97.010721.320.0µg/LChlorobenzene 70-130 9.3 20.0
21.6 10811322.620.0µg/LChlorodibromomethane 70-130 4.5 20.0
20.7 10411021.920.0µg/LChloroethane 60-140 5.6 20.0
21.3 10711222.420.0µg/LChloroform 70-130 5.0 20.0
18.4 92.097.019.420.0µg/LChloromethane 60-140 5.2 20.0
19.1 95.510220.320.0µg/L2-Chlorotoluene 70-130 6.0 20.0
19.6 98.010420.720.0µg/L4-Chlorotoluene 70-130 5.4 20.0
19.3 96.599.019.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 2.5 20.0
20.4 10210420.820.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.9 20.0
20.9 10510320.520.0µg/L1,2-Dibromoethane 70-130 1.9 20.0
20.3 10210020.020.0µg/LDibromomethane 70-130 1.4 20.0
19.7 98.510220.420.0µg/L1,2-Dichlorobenzene 70-130 3.4 20.0
20.2 10110320.520.0µg/L1,3-Dichlorobenzene 70-130 1.4 20.0
19.4 97.010220.420.0µg/L1,4-Dichlorobenzene 70-130 5.0 20.0
21.5 10810921.720.0µg/LDichlorodifluoromethane 60-140 0.9 20.0
20.2 10110821.620.0µg/L1,1-Dichloroethane 70-130 6.6 20.0
20.6 10311022.020.0µg/L1,2-Dichloroethane 70-130 6.5 20.0
20.6 10311021.920.0µg/L1,1-Dichloroethene 70-130 6.1 20.0
19.7 98.510721.420.0µg/Lcis-1,2-Dichloroethene 70-130 8.2 20.0
21.3 10711322.620.0µg/Ltrans-1,2-Dichloroethene 70-130 5.9 20.0
Page 5 of 18Date:05/10/2023 04:30 PM
Page 36 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32934QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32933
LCS-V32933 LCSD-V32933Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.1 95.510621.120.0µg/L1,2-Dichloropropane 70-130 9.9 20.0
19.3 96.598.019.620.0µg/L1,3-Dichloropropane 70-130 1.5 20.0
22.4 11211322.520.0µg/L2,2-Dichloropropane 70-130 0.4 20.0
21.1 10611723.420.0µg/L1,1-Dichloropropene 70-130 10.3 20.0
19.8 99.010721.320.0µg/Lcis-1,3-Dichloropropene 70-130 7.2 20.0
20.8 10410821.620.0µg/Ltrans-1,3-Dichloropropene 70-130 3.7 20.0
543 10993.2466500µg/LEthanol 60-140 15.2 20.0
19.7 98.510320.620.0µg/LEthylbenzene 70-130 4.4 20.0
20.8 10410821.520.0µg/LHexachlorobutadiene 70-130 3.3 20.0
17.6 88.091.018.220.0µg/L2-Hexanone 60-140 3.3 20.0
20.2 10110521.020.0µg/LIsopropylbenzene 70-130 3.8 20.0
20.1 10110520.920.0µg/L4-Isopropyl toluene 70-130 3.9 20.0
17.1 85.574.014.820.0µg/LMethyl Ethyl Ketone (MEK)60-140 14.4 20.0
20.1 10110721.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 6.2 20.0
17.4 87.090.018.020.0µg/L4-Methyl-2-Pentanone 60-140 3.3 20.0
20.5 10310320.620.0µg/LMethylene Chloride 70-130 0.4 20.0
15.8 79.079.515.920.0µg/LNaphthalene 70-130 0.6 20.0
19.1 95.597.519.520.0µg/Ln-Propylbenzene 70-130 2.0 20.0
20.4 10210220.420.0µg/LStyrene 70-130 0.0 20.0
20.9 10511222.320.0µg/L1,1,1,2-Tetrachloroethane 70-130 6.4 20.0
18.6 93.094.518.920.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.6 20.0
20.8 10410721.420.0µg/LTetrachloroethene 70-130 2.8 20.0
20.1 10110420.820.0µg/LToluene 70-130 3.4 20.0
21.4 10710220.320.0µg/L1,2,3-Trichlorobenzene 70-130 5.2 20.0
19.0 95.097.019.420.0µg/L1,2,4-Trichlorobenzene 70-130 2.0 20.0
22.0 11011322.620.0µg/L1,1,1-Trichloroethane 70-130 2.6 20.0
Page 6 of 18Date:05/10/2023 04:30 PM
Page 37 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32934QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32933
LCS-V32933 LCSD-V32933Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.1 10110320.520.0µg/L1,1,2-Trichloroethane 70-130 1.9 20.0
21.6 10811021.920.0µg/LTrichloroethene 70-130 1.3 20.0
22.1 11111322.620.0µg/LTrichlorofluoromethane 60-140 2.2 20.0
20.3 10299.519.920.0µg/L1,2,3-Trichloropropane 70-130 1.9 20.0
19.9 99.510120.220.0µg/L1,2,4-Trimethylbenzene 70-130 1.4 20.0
20.0 10010520.920.0µg/L1,3,5-Trimethylbenzene 70-130 4.4 20.0
19.8 99.093.018.620.0µg/LVinyl Acetate 60-140 6.2 20.0
20.8 10411222.320.0µg/LVinyl Chloride 60-140 6.9 20.0
19.8 99.010420.720.0µg/Lo-Xylene 70-130 4.4 20.0
41.2 10310843.040.0µg/Lm,p-Xylene 70-130 4.2 20.0
97.699.04-Bromofluorobenzene (S)70-130
102104Dibromofluoromethane (S)70-130
1051061,2-Dichloroethane - d4 (S)70-130
97.898.0Toluene-d8 (S)70-130
Page 7 of 18Date:05/10/2023 04:30 PM
Page 38 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V32973QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V32972
Associated Lab Samples: 95155
LRB-V32972 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/08/23 15:090.5000.220<0.220µg/LToluene
05/08/23 15:090.5000.210<0.210µg/Lo-Xylene
05/08/23 15:091.000.420<0.420µg/Lm,p-Xylene
05/08/23 15:094-Bromofluorobenzene (S)98.2 70-130
05/08/23 15:09Dibromofluoromethane (S)104 70-130
05/08/23 15:091,2-Dichloroethane - d4 (S)106 70-130
05/08/23 15:09Toluene-d8 (S)96.2 70-130
LCS-V32972 LCSD-V32972Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.9 99.510220.320.0µg/LToluene 70-130 1.9 20.0
20.3 10210120.220.0µg/Lo-Xylene 70-130 0.4 20.0
41.1 10310642.240.0µg/Lm,p-Xylene 70-130 2.6 20.0
99.099.44-Bromofluorobenzene (S)70-130
101103Dibromofluoromethane (S)70-130
1071051,2-Dichloroethane - d4 (S)70-130
96.896.2Toluene-d8 (S)70-130
Page 8 of 18Date:05/10/2023 04:30 PM
Page 39 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
Associated Lab Samples: 95156, 95159
LRB-V32694 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 11:110.0200.002<0.002mg/KgAcetone
05/02/23 11:110.0200.001<0.001mg/KgAcrolein
05/02/23 11:110.0200.0008<0.0008mg/KgAcrylonitrile
05/02/23 11:110.0050.0006<0.0006mg/KgBenzene
05/02/23 11:110.0050.0005<0.0005mg/KgBromobenzene
05/02/23 11:110.0050.0008<0.0008mg/KgBromochloromethane
05/02/23 11:110.0050.001<0.001mg/KgBromodichloromethane
05/02/23 11:110.0050.001<0.001mg/KgBromoform
05/02/23 11:110.0100.001<0.001mg/KgBromomethane
05/02/23 11:110.0050.0005<0.0005mg/Kgn-Butylbenzene
05/02/23 11:110.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/02/23 11:110.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/02/23 11:110.0050.0006<0.0006mg/KgCarbon Disulfide
05/02/23 11:110.0050.001<0.001mg/KgCarbon Tetrachloride
05/02/23 11:110.0050.0007<0.0007mg/KgChlorobenzene
05/02/23 11:110.0050.0009<0.0009mg/KgChlorodibromomethane
05/02/23 11:110.0100.0009<0.0009mg/KgChloroethane
05/02/23 11:110.0050.001<0.001mg/KgChloroform
05/02/23 11:110.0100.0006<0.0006mg/KgChloromethane
05/02/23 11:110.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/02/23 11:110.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/02/23 11:110.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/02/23 11:110.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/02/23 11:110.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/02/23 11:110.0050.0006<0.0006mg/KgDibromomethane
05/02/23 11:110.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/02/23 11:110.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 9 of 18Date:05/10/2023 04:30 PM
Page 40 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
Associated Lab Samples: 95156, 95159
LRB-V32694 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 11:110.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/02/23 11:110.0100.001<0.001mg/KgDichlorodifluoromethane
05/02/23 11:110.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/02/23 11:110.0050.001<0.001mg/Kg1,2-Dichloroethane
05/02/23 11:110.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/02/23 11:110.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/02/23 11:110.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/02/23 11:110.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/02/23 11:110.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/02/23 11:110.0050.001<0.001mg/Kg2,2-Dichloropropane
05/02/23 11:110.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/02/23 11:110.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/02/23 11:110.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/02/23 11:110.0050.0006<0.0006mg/KgEthylbenzene
05/02/23 11:110.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/02/23 11:110.0100.0008<0.0008mg/KgHexachlorobutadiene
05/02/23 11:110.0100.0007<0.0007mg/Kgn-Hexane
05/02/23 11:110.0200.0006<0.0006mg/Kg2-Hexanone
05/02/23 11:110.0050.0005<0.0005mg/KgIsopropylbenzene
05/02/23 11:110.0050.001<0.001mg/Kg4-Isopropyl toluene
05/02/23 11:110.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/02/23 11:110.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/02/23 11:110.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/02/23 11:110.0100.001<0.001mg/KgMethylene Chloride
05/02/23 11:110.0100.0010<0.0010mg/KgNaphthalene
05/02/23 11:110.0050.0005<0.0005mg/Kgn-Propylbenzene
05/02/23 11:110.0050.001<0.001mg/KgStyrene
Page 10 of 18Date:05/10/2023 04:30 PM
Page 41 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
Associated Lab Samples: 95156, 95159
LRB-V32694 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 11:110.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/02/23 11:110.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/02/23 11:110.0050.0009<0.0009mg/KgTetrachloroethene
05/02/23 11:110.0050.0007<0.0007mg/KgToluene
05/02/23 11:110.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/02/23 11:110.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/02/23 11:110.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/02/23 11:110.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/02/23 11:110.0050.0009<0.0009mg/KgTrichloroethene
05/02/23 11:110.0100.002<0.002mg/KgTrichlorofluoromethane
05/02/23 11:110.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/02/23 11:110.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/02/23 11:110.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/02/23 11:110.0100.0005<0.0005mg/KgVinyl Acetate
05/02/23 11:110.0100.0005<0.0005mg/KgVinyl Chloride
05/02/23 11:110.0050.0005<0.0005mg/Kgo-Xylene
05/02/23 11:110.0100.001<0.001mg/Kgm,p-Xylene
05/02/23 11:114-Bromofluorobenzene (S)97.8 70-130
05/02/23 11:11Dibromofluoromethane (S)96.6 84-123
05/02/23 11:11Toluene-d8 (S)90.2 76-129
LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.105 1051200.1200.100mg/KgAcetone 29-198 13.3 20
0.088 88.090.30.0900.100mg/KgAcrolein 70-130 2.5 20
Page 11 of 18Date:05/10/2023 04:30 PM
Page 42 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.101 10197.20.0970.100mg/KgAcrylonitrile 65-134 3.8 20
0.055 1101110.0550.050mg/KgBenzene 74-127 0.7 20
0.044 88.692.80.0460.050mg/KgBromobenzene 73-125 4.6 20
0.059 1201190.0590.050mg/KgBromochloromethane 72-134 1.0 20
0.057 1161160.0580.050mg/KgBromodichloromethane 75-122 0.5 20
0.052 1051060.0530.050mg/KgBromoform 66-135 1.5 20
0.056 11395.00.0470.050mg/KgBromomethane 20-180 17.1 20
0.045 90.695.20.0470.050mg/Kgn-Butylbenzene 65-135 4.9 20
0.044 89.493.40.0460.050mg/Kgsec-Butyl benzene 66-131 4.3 20
0.044 89.293.00.0460.050mg/Kgtert-Butyl benzene 67-132 4.1 20
0.052 1061110.0550.050mg/KgCarbon Disulfide 61-129 4.7 20
0.058 1161180.0590.050mg/KgCarbon Tetrachloride 64-143 1.8 20
0.050 1021040.0520.050mg/KgChlorobenzene 74-118 2.5 20
0.051 1041040.0520.050mg/KgChlorodibromomethane 73-122 0.5 20
0.049 99.81080.0540.050mg/KgChloroethane 33-149 8.2 20
0.056 1141170.0580.050mg/KgChloroform 73-127 2.9 20
0.052 1041040.0520.050mg/KgChloromethane 45-143 0.3 20
0.044 89.893.20.0460.050mg/Kg2-Chlorotoluene 67-124 3.7 20
0.044 89.893.20.0460.050mg/Kg4-Chlorotoluene 71-126 3.7 20
0.054 1091100.0540.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.7 20
0.050 1011020.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.1 20
0.054 1081050.0520.050mg/Kg1,2-Dibromoethane 70-132 2.6 20
0.055 1111170.0580.050mg/KgDibromomethane 74-133 4.5 20
0.046 92.497.40.0480.050mg/Kg1,2-Dichlorobenzene 72-123 5.2 20
0.046 93.495.80.0470.050mg/Kg1,3-Dichlorobenzene 71-120 2.5 20
0.045 91.095.00.0470.050mg/Kg1,4-Dichlorobenzene 71-123 4.3 20
Page 12 of 18Date:05/10/2023 04:30 PM
Page 43 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1001040.0510.050mg/KgDichlorodifluoromethane 26-146 3.5 20
0.053 1071130.0560.050mg/Kg1,1-Dichloroethane 74-127 4.7 20
0.053 1061080.0530.050mg/Kg1,2-Dichloroethane 68-128 1.1 20
0.052 1061120.0550.050mg/Kg1,1-Dichloroethene 67-149 5.5 20
0.054 1081090.0540.050mg/Kgcis-1,2-Dichloroethene 76-134 0.9 20
0.052 1061110.0550.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.6 20
0.053 1071130.0560.050mg/Kg1,2-Dichloropropane 73-130 5.2 20
0.051 1021030.0510.050mg/Kg1,3-Dichloropropane 75-124 0.3 20
0.055 1101140.0570.050mg/Kg2,2-Dichloropropane 50-142 3.3 20
0.055 1101160.0580.050mg/Kg1,1-Dichloropropene 71-130 5.4 20
0.057 1151150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 0.3 20
0.059 1181190.0590.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.5 20
0.048 96.898.60.0490.050mg/KgEthylbenzene 74-128 1.8 20
0.107 1071080.1080.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.047 94.81010.0500.050mg/KgHexachlorobutadiene 64-125 6.1 20
0.055 1111250.0620.050mg/Kgn-Hexane 70-130 11.6 20
0.049 98.41220.0610.050mg/Kg2-Hexanone 61-157 21.4*20
0.045 90.494.80.0470.050mg/KgIsopropylbenzene 68-126 4.7 20
0.045 90.695.40.0470.050mg/Kg4-Isopropyl toluene 68-129 5.1 20
0.040 80.499.80.0490.050mg/KgMethyl Ethyl Ketone (MEK)63-149 21.5*20
0.055 1101100.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.3 20
0.058 1161200.0600.050mg/Kg4-Methyl-2-Pentanone 57-162 3.2 20
0.045 91.892.00.0460.050mg/KgMethylene Chloride 74-129 0.2 20
0.046 93.499.20.0490.050mg/KgNaphthalene 57-157 6.0 20
0.044 89.492.40.0460.050mg/Kgn-Propylbenzene 67-130 3.3 20
0.051 1031040.0520.050mg/KgStyrene 77-121 1.3 20
Page 13 of 18* QC Fail Date:05/10/2023 04:30 PM
Page 44 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32695QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32694
LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1011010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.0 20
0.045 90.093.00.0460.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.2 20
0.056 1121160.0570.050mg/KgTetrachloroethene 68-130 3.3 20
0.053 1081080.0540.050mg/KgToluene 71-129 0.7 20
0.047 95.01050.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 10.1 20
0.049 99.41060.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 6.0 20
0.055 1101140.0560.050mg/Kg1,1,1-Trichloroethane 67-131 2.8 20
0.051 1031050.0520.050mg/Kg1,1,2-Trichloroethane 70-133 1.7 20
0.055 1121160.0580.050mg/KgTrichloroethene 75-133 4.2 20
0.042 85.482.00.0410.050mg/KgTrichlorofluoromethane 44-146 4.0 20
0.048 97.694.00.0470.050mg/Kg1,2,3-Trichloropropane 60-137 3.7 20
0.045 90.892.80.0460.050mg/Kg1,2,4-Trimethylbenzene 69-129 2.1 20
0.044 88.493.60.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.7 20
0.058 11897.80.0480.050mg/KgVinyl Acetate 60-140 18.5 20
0.051 1021060.0530.050mg/KgVinyl Chloride 48-147 4.0 20
0.048 96.499.20.0490.050mg/Kgo-Xylene 74-126 2.8 20
0.099 99.31020.1020.100mg/Kgm,p-Xylene 75-124 2.6 20
97.81014-Bromofluorobenzene (S)70-130
10196.2Dibromofluoromethane (S)84-123
90.289.6Toluene-d8 (S)76-129
Page 14 of 18Date:05/10/2023 04:30 PM
Page 45 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
EDB and DBCP by Microextraction GC/ECD
EPA-504.1
V32736QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-504.1(PREP)
QC Prep:V32711
Associated Lab Samples: 95155
LRB-V32711 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/03/23 10:590.02000.00330<0.00330µg/L1,2-Dibromoethane
LCS-V32711 LCSD-V32711Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.329 132*1290.3220.250µg/L1,2-Dibromoethane 70-130 2.1 20.0
V 94925-DUP-V32711Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/03/23 12:180.9<0.0209< 0.0209µg/L1,2-Dibromoethane
V 94924-MS-V32711Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
0.330 1260.2610.0105µg/L1,2-Dibromoethane 70-130
Page 15 of 18* QC Fail Date:05/10/2023 04:30 PM
Page 46 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V32651QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V32650
Associated Lab Samples: 95155
LRB-V32650 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/01/23 13:5850.011.5<11.5µg/LAliphatic C5-C8
05/01/23 13:5850.025.8<25.8µg/LAliphatic C9-C12
05/01/23 13:5850.04.02<4.02µg/LAromatic C9-C10
05/01/23 13:582,5-Dibromotoluene (FID) (S)80.3 70-130
05/01/23 13:582,5-Dibromotoluene (PID) (S)89.2 70-130
LCS-V32650 LCSD-V32650Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
358 119120359300µg/LAliphatic C5-C8 70-130 0.2 50.0
336 112110331300µg/LAliphatic C9-C12 70-130 1.4 50.0
111 111104104100µg/LAromatic C9-C10 70-130 6.5 50.0
98.81022,5-Dibromotoluene (FID) (S)70-130
12096.22,5-Dibromotoluene (PID) (S)70-130
Page 16 of 18Date:05/10/2023 04:30 PM
Page 47 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V32693QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V32692
Associated Lab Samples: 95156, 95157, 95158, 95159
LRB-V32692 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 16:208.001.22<1.22mg/KgAliphatic C5-C8
05/02/23 16:208.004.56<4.56mg/KgAliphatic C9-C12
05/02/23 16:208.000.624<0.624mg/KgAromatic C9-C10
05/02/23 16:202,5-Dibromotoluene (FID) (S)80.8 70-130
05/02/23 16:202,5-Dibromotoluene (PID) (S)112 70-130
LCS-V32692 LCSD-V32692Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.1 10097.531.232.0mg/KgAliphatic C5-C8 70-130 2.8 50
35.9 11211035.132.0mg/KgAliphatic C9-C12 70-130 2.2 50
13.1 12212313.210.7mg/KgAromatic C9-C10 70-130 0.7 50
81.677.02,5-Dibromotoluene (FID) (S)70-130
1121122,5-Dibromotoluene (PID) (S)70-130
Page 17 of 18Date:05/10/2023 04:30 PM
Page 48 of 51
Quality Control Data
23-121-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
Dry Weight Determination
SW-DRYWT
V32710QC Analytical Batch:
Analysis Method:
Analysis Description:
V 95156-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/03/23 10:501.519.319.6%Moisture
V 95200-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/03/23 10:500.921.521.7%Moisture
Page 18 of 18Date:05/10/2023 04:30 PM
Page 49 of 51
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-121-0003
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.1C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Did not receive containers for moisture for samples MW-1-10' & MW-1-15'.
Signature:Angelo Norvell Date & Time:05/01/2023 10:33:04
Special precautions or instructions included?
Comments:
Page 50 of 51
Pa
g
e

5
1

o
f

5
1

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

7/20/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-188-0019 Client Project Description: Handy Corner
GRI #6389
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/7/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 52
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-188-0019
Page 2 of 52
Report Number:
Sample Summary Table
Client Project Description:
23-188-0019
Handy Corner
GRI #6389
Lab No Client Sample ID Matrix Date Collected Date Received
07/05/2023 11:36Aqueous 89040 Trip Blanks 07/07/2023 14:05
07/05/2023 15:04Aqueous 89041 MW-2 07/07/2023 14:05
07/05/2023 15:22Aqueous 89042 MW-3 07/07/2023 14:05
07/05/2023 15:56Aqueous 89043 MW-4 07/07/2023 14:05
Page 3 of 52
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-188-0019
Report Limit
Project:Handy Corner
V 89041MW-2
0.021 07/12/2023 16:396010DLeadmg/L 0.002
J0.242 07/12/2023 10:326200Bo-Xylene µg/L 0.210
J0.432 07/12/2023 10:326200Bm,p-Xylene µg/L 0.420
J0.674 07/12/2023 10:326200BXylene (Total)µg/L 0.210
V 89042MW-3
0.012 07/12/2023 16:446010DLeadmg/L 0.002
104 07/12/2023 04:366200BAcetoneµg/L 18.0
325 07/12/2023 04:366200BBenzeneµg/L 1.80
J4.32 07/12/2023 04:366200Bn-Butylbenzene µg/L 1.80
J4.09 07/12/2023 04:366200Bsec-Butyl benzene µg/L 2.00
37.7 07/12/2023 04:366200BChloroformµg/L 2.20
14.8 07/12/2023 04:366200BDi-Isopropyl Ether (DIPE)µg/L 5.00
310 07/12/2023 04:366200BEthylbenzeneµg/L 1.70
37.1 07/12/2023 04:366200B2-Hexanone µg/L 3.80
27.1 07/12/2023 04:366200BIsopropylbenzeneµg/L 1.80
J2.61 07/12/2023 04:366200B4-Isopropyl toluene µg/L 0.890
83.1 07/12/2023 04:366200BMethyl Ethyl Ketone (MEK)µg/L 7.10
17.6 07/12/2023 04:366200BMethyl tert-butyl ether (MTBE)µg/L 1.40
41.8 07/12/2023 04:366200B4-Methyl-2-Pentanone µg/L 0.780
35.2 07/12/2023 04:366200BNaphthaleneµg/L 4.70
54.7 07/12/2023 04:366200Bn-Propylbenzene µg/L 1.90
422 07/12/2023 04:366200Btert-Butyl Alcohol (TBA)µg/L 16.0
994 07/12/2023 04:366200Btert-Amyl Alcohol (TAA)µg/L 19.0
788 07/12/2023 04:366200BTolueneµg/L 2.20
471 07/12/2023 04:366200B1,2,4-Trimethylbenzene µg/L 1.90
99.2 07/12/2023 04:366200B1,3,5-Trimethylbenzene µg/L 1.80
859 07/12/2023 04:366200Bo-Xylene µg/L 2.10
3110 07/12/2023 18:286200Bm,p-Xylene µg/L 42.0
3970 07/12/2023 04:366200BXylene (Total)µg/L 2.10
1370 07/10/2023 17:22CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 115
731 07/10/2023 17:22CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 258
1720 07/10/2023 17:22CALCULATIONAromatic C9-C10 (Adjusted)µg/L 40.2
2480 07/10/2023 17:22MADEP-VPH Aliphatic C5-C8 µg/L 115
6730 07/10/2023 17:22MADEP-VPH Aliphatic C9-C12 µg/L 258
1720 07/10/2023 17:22MADEP-VPH Aromatic C9-C10 µg/L 40.2
Page 4 of 52
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-188-0019
Report Limit
Project:Handy Corner
V 89043MW-4
0.066 07/12/2023 16:486010DLeadmg/L 0.012
J0.451 07/12/2023 01:426200BBenzeneµg/L 0.180
0.765 07/12/2023 01:426200BEthylbenzeneµg/L 0.170
1.84 07/12/2023 01:426200BTolueneµg/L 0.220
0.621 07/12/2023 01:426200B1,2,4-Trimethylbenzene µg/L 0.190
J0.231 07/12/2023 01:426200B1,3,5-Trimethylbenzene µg/L 0.180
1.26 07/12/2023 01:426200Bo-Xylene µg/L 0.210
4.83 07/12/2023 01:426200Bm,p-Xylene µg/L 0.420
6.09 07/12/2023 01:426200BXylene (Total)µg/L 0.210
J29.3 07/10/2023 15:24MADEP-VPH Aliphatic C9-C12 µg/L 25.8
Page 5 of 52

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Handy Corner Lab Report Number: 23-188-0019
Date: 7/20/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: Ethanol QC Batch No: V35229/V35227
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V35284/V35278
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 6 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
89040 Matrix:
7/5/2023 11:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
<1.80 µg/L 1.80 10.0Acetone 1 07/11/23 13:41 V35229TBL
<0.180 µg/L 0.180 0.500Benzene 1 07/11/23 13:41 V35229TBL
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 13:41 V35229TBL
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 13:41 V35229TBL
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 13:41 V35229TBL
<1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 13:41 V35229TBL
<0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 13:41 V35229TBL
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 13:41 V35229TBL
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 13:41 V35229TBL
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 13:41 V35229TBL
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 13:41 V35229TBL
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 13:41 V35229TBL
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 13:41 V35229TBL
<0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 13:41 V35229TBL
<0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 13:41 V35229TBL
<0.220 µg/L 0.220 0.500Chloromethane 1 07/11/23 13:41 V35229TBL
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 13:41 V35229TBL
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 13:41 V35229TBL
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/11/23 13:41 V35229TBL
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 13:41 V35229TBL
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 13:41 V35229TBL
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 13:41 V35229TBL
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 13:41 V35229TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
89040 Matrix:
7/5/2023 11:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 13:41 V35229TBL
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 13:41 V35229TBL
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 13:41 V35229TBL
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 13:41 V35229TBL
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 13:41 V35229TBL
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 13:41 V35229TBL
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 13:41 V35229TBL
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 13:41 V35229TBL
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 13:41 V35229TBL
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 13:41 V35229TBL
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 13:41 V35229TBL
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 13:41 V35229TBL
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 13:41 V35229TBL
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 13:41 V35229TBL
<42.0 µg/L 42.0 200Ethanol 1 07/11/23 13:41 V35229TBL
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 13:41 V35229TBL
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 13:41 V35229TBL
<0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 13:41 V35229TBL
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 13:41 V35229TBL
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 13:41 V35229TBL
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 13:41 V35229TBL
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 13:41 V35229TBL
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 13:41 V35229TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
89040 Matrix:
7/5/2023 11:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 13:41 V35229TBL
<0.470 µg/L 0.470 1.00Naphthalene 1 07/11/23 13:41 V35229TBL
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 13:41 V35229TBL
<0.220 µg/L 0.220 0.500Styrene 1 07/11/23 13:41 V35229TBL
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 13:41 V35229TBL
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 13:41 V35229TBL
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 13:41 V35229TBL
<0.220 µg/L 0.220 0.500Toluene 1 07/11/23 13:41 V35229TBL
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 13:41 V35229TBL
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 13:41 V35229TBL
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 13:41 V35229TBL
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 13:41 V35229TBL
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 13:41 V35229TBL
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 13:41 V35229TBL
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 13:41 V35229TBL
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 13:41 V35229TBL
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 13:41 V35229TBL
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 13:41 V35229TBL
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 13:41 V35229TBL
<0.210 µg/L 0.210 0.500o-Xylene 1 07/11/23 13:41 V35229TBL
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/11/23 13:41 V35229TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
89040 Matrix:
7/5/2023 11:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/11/23 13:41 V35229
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/11/23 13:411 TBL V35229
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%07/11/23 13:411 TBL V35229
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%07/11/23 13:411 TBL V35229
Surrogate: Toluene-d8 92.6 Limits: 70-130%07/11/23 13:411 TBL V35229
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
89041 Matrix:
7/5/2023 15:04
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/12/23 10:32 6200BENM
0.021 mg/L 0.002 0.006Lead 1 07/12/23 16:39 6010DJKC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
89041 Matrix:
7/5/2023 15:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35278 07/11/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 07/12/23 10:32 V35284ENM
<0.180 µg/L 0.180 0.500Benzene 1 07/12/23 10:32 V35284ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/12/23 10:32 V35284ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/12/23 10:32 V35284ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/12/23 10:32 V35284ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/12/23 10:32 V35284ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/12/23 10:32 V35284ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/12/23 10:32 V35284ENM
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/12/23 10:32 V35284ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/12/23 10:32 V35284ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/12/23 10:32 V35284ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/12/23 10:32 V35284ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/12/23 10:32 V35284ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/12/23 10:32 V35284ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/12/23 10:32 V35284ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 07/12/23 10:32 V35284ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/12/23 10:32 V35284ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/12/23 10:32 V35284ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/12/23 10:32 V35284ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/12/23 10:32 V35284ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/12/23 10:32 V35284ENM
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/12/23 10:32 V35284ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/12/23 10:32 V35284ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
89041 Matrix:
7/5/2023 15:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35278 07/11/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/12/23 10:32 V35284ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/12/23 10:32 V35284ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/12/23 10:32 V35284ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/12/23 10:32 V35284ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/12/23 10:32 V35284ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/12/23 10:32 V35284ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/12/23 10:32 V35284ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/12/23 10:32 V35284ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/12/23 10:32 V35284ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/12/23 10:32 V35284ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/12/23 10:32 V35284ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/12/23 10:32 V35284ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/12/23 10:32 V35284ENM
<42.0 µg/L 42.0 200Ethanol 1 07/12/23 10:32 V35284ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/12/23 10:32 V35284ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/12/23 10:32 V35284ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 07/12/23 10:32 V35284ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/12/23 10:32 V35284ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/12/23 10:32 V35284ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/12/23 10:32 V35284ENM
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/12/23 10:32 V35284ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/12/23 10:32 V35284ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/12/23 10:32 V35284ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
89041 Matrix:
7/5/2023 15:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35278 07/11/23 09:00
<0.470 µg/L 0.470 1.00Naphthalene 1 07/12/23 10:32 V35284ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/12/23 10:32 V35284ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/12/23 10:32 V35284ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/12/23 10:32 V35284ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/12/23 10:32 V35284ENM
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/12/23 10:32 V35284ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/12/23 10:32 V35284ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/12/23 10:32 V35284ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/12/23 10:32 V35284ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/12/23 10:32 V35284ENM
<0.220 µg/L 0.220 0.500Toluene 1 07/12/23 10:32 V35284ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/12/23 10:32 V35284ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/12/23 10:32 V35284ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/12/23 10:32 V35284ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/12/23 10:32 V35284ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/12/23 10:32 V35284ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/12/23 10:32 V35284ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/12/23 10:32 V35284ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/12/23 10:32 V35284ENM
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/12/23 10:32 V35284ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/12/23 10:32 V35284ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/12/23 10:32 V35284ENM
0.242 J µg/L 0.210 0.500o-Xylene 1 07/12/23 10:32 V35284ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
89041 Matrix:
7/5/2023 15:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35278 07/11/23 09:00
0.432 J µg/L 0.420 1.00m,p-Xylene 1 07/12/23 10:32 V35284ENM
0.674 J µg/L 0.210 0.500Xylene (Total)1 07/12/23 10:32 V35284KCC
Surrogate: 4-Bromofluorobenzene 92.0 Limits: 70-130%07/12/23 10:321 ENM V35284
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%07/12/23 10:321 ENM V35284
Surrogate: 1,2-Dichloroethane - d4 92.2 Limits: 70-130%07/12/23 10:321 ENM V35284
Surrogate: Toluene-d8 91.4 Limits: 70-130%07/12/23 10:321 ENM V35284
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V35162 07/11/23 09:46
<0.00343 µg/L 0.00343 0.02081,2-Dibromoethane 1 07/11/23 14:09 V35214TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
89041 Matrix:
7/5/2023 15:04
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 07/10/23 15:01
<25.8 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 07/10/23 15:01
<4.02 µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 07/10/23 15:01
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V35150 07/10/23 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 07/10/23 15:01 V35151TBL
<25.8 µg/L 25.8 50.0Aliphatic C9-C12 1 07/10/23 15:01 V35151TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 07/10/23 15:01 V35151TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)83.0 Limits: 70-130%07/10/23 15:011 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)100 Limits: 70-130%07/10/23 15:011 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
89042 Matrix:
7/5/2023 15:22
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 07/12/23 04:36 6200BTBL
0.012 mg/L 0.002 0.006Lead 1 07/12/23 16:44 6010DJKC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
89042 Matrix:
7/5/2023 15:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35234 07/11/23 08:00 V35302 07/12/23 09:00
104 µg/L 18.0 100Acetone 10 07/12/23 04:36 V35235TBL
325 µg/L 1.80 5.00Benzene 10 07/12/23 04:36 V35235TBL
<2.10 µg/L 2.10 5.00Bromobenzene 10 07/12/23 04:36 V35235TBL
<4.20 µg/L 4.20 10.0Bromochloromethane 10 07/12/23 04:36 V35235TBL
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 07/12/23 04:36 V35235TBL
<15.0 µg/L 15.0 50.0Bromoform 10 07/12/23 04:36 V35235TBL
<2.80 µg/L 2.80 10.0Bromomethane 10 07/12/23 04:36 V35235TBL
4.32 J µg/L 1.80 5.00n-Butylbenzene 10 07/12/23 04:36 V35235TBL
4.09 J µg/L 2.00 5.00sec-Butyl benzene 10 07/12/23 04:36 V35235TBL
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 07/12/23 04:36 V35235TBL
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 07/12/23 04:36 V35235TBL
<1.90 µg/L 1.90 5.00Chlorobenzene 10 07/12/23 04:36 V35235TBL
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 07/12/23 04:36 V35235TBL
<4.30 µg/L 4.30 10.0Chloroethane 10 07/12/23 04:36 V35235TBL
37.7 µg/L 2.20 5.00Chloroform 10 07/12/23 04:36 V35235TBL
<2.20 µg/L 2.20 5.00Chloromethane 10 07/12/23 04:36 V35235TBL
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 07/12/23 04:36 V35235TBL
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 07/12/23 04:36 V35235TBL
14.8 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 07/12/23 04:36 V35235TBL
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 07/12/23 04:36 V35235TBL
<2.30 µg/L 2.30 5.00Dibromomethane 10 07/12/23 04:36 V35235TBL
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 07/12/23 04:36 V35235TBL
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 07/12/23 04:36 V35235TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
89042 Matrix:
7/5/2023 15:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35234 07/11/23 08:00 V35302 07/12/23 09:00
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 07/12/23 04:36 V35235TBL
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 07/12/23 04:36 V35235TBL
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 07/12/23 04:36 V35235TBL
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 07/12/23 04:36 V35235TBL
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 07/12/23 04:36 V35235TBL
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 07/12/23 04:36 V35235TBL
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 07/12/23 04:36 V35235TBL
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 07/12/23 04:36 V35235TBL
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 07/12/23 04:36 V35235TBL
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 07/12/23 04:36 V35235TBL
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 07/12/23 04:36 V35235TBL
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 07/12/23 04:36 V35235TBL
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 07/12/23 04:36 V35235TBL
<420 µg/L 420 2000Ethanol 10 07/12/23 04:36 V35235TBL
310 µg/L 1.70 5.00Ethylbenzene 10 07/12/23 04:36 V35235TBL
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 07/12/23 04:36 V35235TBL
37.1 µg/L 3.80 10.02-Hexanone 10 07/12/23 04:36 V35235TBL
27.1 µg/L 1.80 5.00Isopropylbenzene 10 07/12/23 04:36 V35235TBL
2.61 J µg/L 0.890 5.004-Isopropyl toluene 10 07/12/23 04:36 V35235TBL
83.1 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 07/12/23 04:36 V35235TBL
17.6 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 07/12/23 04:36 V35235TBL
41.8 µg/L 0.780 10.04-Methyl-2-Pentanone 10 07/12/23 04:36 V35235TBL
<3.30 µg/L 3.30 20.0Methylene Chloride 10 07/12/23 04:36 V35235TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
89042 Matrix:
7/5/2023 15:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35234 07/11/23 08:00 V35302 07/12/23 09:00
35.2 µg/L 4.70 10.0Naphthalene 10 07/12/23 04:36 V35235TBL
54.7 µg/L 1.90 5.00n-Propylbenzene 10 07/12/23 04:36 V35235TBL
<2.20 µg/L 2.20 5.00Styrene 10 07/12/23 04:36 V35235TBL
422 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 07/12/23 04:36 V35235TBL
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 07/12/23 04:36 V35235TBL
994 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 07/12/23 04:36 V35235TBL
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 07/12/23 04:36 V35235TBL
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 07/12/23 04:36 V35235TBL
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 07/12/23 04:36 V35235TBL
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 07/12/23 04:36 V35235TBL
788 µg/L 2.20 5.00Toluene 10 07/12/23 04:36 V35235TBL
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 07/12/23 04:36 V35235TBL
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 07/12/23 04:36 V35235TBL
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 07/12/23 04:36 V35235TBL
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 07/12/23 04:36 V35235TBL
<1.80 µg/L 1.80 5.00Trichloroethene 10 07/12/23 04:36 V35235TBL
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 07/12/23 04:36 V35235TBL
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 07/12/23 04:36 V35235TBL
471 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 07/12/23 04:36 V35235TBL
99.2 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 07/12/23 04:36 V35235TBL
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 07/12/23 04:36 V35235TBL
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 07/12/23 04:36 V35235TBL
859 µg/L 2.10 5.00o-Xylene 10 07/12/23 04:36 V35235TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
89042 Matrix:
7/5/2023 15:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35234 07/11/23 08:00 V35302 07/12/23 09:00
3110 µg/L 42.0 100m,p-Xylene 100 07/12/23 18:28 V35303MSA
3970 µg/L 2.10 5.00Xylene (Total)10 07/12/23 04:36 V35303
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/12/23 04:3610 TBL V35235
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%07/12/23 04:3610 TBL V35235
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%07/12/23 04:3610 TBL V35235
Surrogate: Toluene-d8 90.6 Limits: 70-130%07/12/23 04:3610 TBL V35235
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%07/12/23 18:28100 MSA V35303
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%07/12/23 18:28100 MSA V35303
Surrogate: 1,2-Dichloroethane - d4 99.8 Limits: 70-130%07/12/23 18:28100 MSA V35303
Surrogate: Toluene-d8 91.2 Limits: 70-130%07/12/23 18:28100 MSA V35303
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V35162 07/11/23 09:46
<0.00338 µg/L 0.00338 0.02051,2-Dibromoethane 1 07/11/23 14:29 V35214TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
89042 Matrix:
7/5/2023 15:22
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
1370 µg/L 115 500Aliphatic C5-C8 (Adjusted)10 07/10/23 17:22
731 µg/L 258 500Aliphatics C9-C12 (Adjusted)10 07/10/23 17:22
1720 µg/L 40.2 500Aromatic C9-C10 (Adjusted)10 07/10/23 17:22
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V35150 07/10/23 08:00
2480 µg/L 115 500Aliphatic C5-C8 10 07/10/23 17:22 V35151TBL
6730 µg/L 258 500Aliphatic C9-C12 10 07/10/23 17:22 V35151TBL
1720 µg/L 40.2 500Aromatic C9-C10 10 07/10/23 17:22 V35151TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)90.9 Limits: 70-130%07/10/23 17:2210 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)110 Limits: 70-130%07/10/23 17:2210 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
89043 Matrix:
7/5/2023 15:56
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/12/23 01:42 6200BTBL
0.066 mg/L 0.012 0.030Lead 5 07/12/23 16:48 6010DJKC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
89043 Matrix:
7/5/2023 15:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35234 07/11/23 08:00
<1.80 µg/L 1.80 10.0Acetone 1 07/12/23 01:42 V35235TBL
0.451 J µg/L 0.180 0.500Benzene 1 07/12/23 01:42 V35235TBL
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/12/23 01:42 V35235TBL
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/12/23 01:42 V35235TBL
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/12/23 01:42 V35235TBL
<1.50 µg/L 1.50 5.00Bromoform 1 07/12/23 01:42 V35235TBL
<0.280 µg/L 0.280 1.00Bromomethane 1 07/12/23 01:42 V35235TBL
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/12/23 01:42 V35235TBL
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/12/23 01:42 V35235TBL
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/12/23 01:42 V35235TBL
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/12/23 01:42 V35235TBL
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/12/23 01:42 V35235TBL
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/12/23 01:42 V35235TBL
<0.430 µg/L 0.430 1.00Chloroethane 1 07/12/23 01:42 V35235TBL
<0.220 µg/L 0.220 0.500Chloroform 1 07/12/23 01:42 V35235TBL
<0.220 µg/L 0.220 0.500Chloromethane 1 07/12/23 01:42 V35235TBL
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/12/23 01:42 V35235TBL
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/12/23 01:42 V35235TBL
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/12/23 01:42 V35235TBL
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/12/23 01:42 V35235TBL
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/12/23 01:42 V35235TBL
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/12/23 01:42 V35235TBL
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/12/23 01:42 V35235TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
89043 Matrix:
7/5/2023 15:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35234 07/11/23 08:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/12/23 01:42 V35235TBL
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/12/23 01:42 V35235TBL
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/12/23 01:42 V35235TBL
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/12/23 01:42 V35235TBL
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/12/23 01:42 V35235TBL
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/12/23 01:42 V35235TBL
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/12/23 01:42 V35235TBL
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/12/23 01:42 V35235TBL
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/12/23 01:42 V35235TBL
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/12/23 01:42 V35235TBL
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/12/23 01:42 V35235TBL
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/12/23 01:42 V35235TBL
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/12/23 01:42 V35235TBL
<42.0 µg/L 42.0 200Ethanol 1 07/12/23 01:42 V35235TBL
0.765 µg/L 0.170 0.500Ethylbenzene 1 07/12/23 01:42 V35235TBL
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/12/23 01:42 V35235TBL
<0.380 µg/L 0.380 1.002-Hexanone 1 07/12/23 01:42 V35235TBL
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/12/23 01:42 V35235TBL
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/12/23 01:42 V35235TBL
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/12/23 01:42 V35235TBL
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/12/23 01:42 V35235TBL
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/12/23 01:42 V35235TBL
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/12/23 01:42 V35235TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
89043 Matrix:
7/5/2023 15:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35234 07/11/23 08:00
<0.470 µg/L 0.470 1.00Naphthalene 1 07/12/23 01:42 V35235TBL
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/12/23 01:42 V35235TBL
<0.220 µg/L 0.220 0.500Styrene 1 07/12/23 01:42 V35235TBL
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/12/23 01:42 V35235TBL
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/12/23 01:42 V35235TBL
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/12/23 01:42 V35235TBL
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/12/23 01:42 V35235TBL
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/12/23 01:42 V35235TBL
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/12/23 01:42 V35235TBL
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/12/23 01:42 V35235TBL
1.84 µg/L 0.220 0.500Toluene 1 07/12/23 01:42 V35235TBL
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/12/23 01:42 V35235TBL
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/12/23 01:42 V35235TBL
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/12/23 01:42 V35235TBL
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/12/23 01:42 V35235TBL
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/12/23 01:42 V35235TBL
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/12/23 01:42 V35235TBL
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/12/23 01:42 V35235TBL
0.621 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/12/23 01:42 V35235TBL
0.231 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/12/23 01:42 V35235TBL
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/12/23 01:42 V35235TBL
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/12/23 01:42 V35235TBL
1.26 µg/L 0.210 0.500o-Xylene 1 07/12/23 01:42 V35235TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
89043 Matrix:
7/5/2023 15:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35234 07/11/23 08:00
4.83 µg/L 0.420 1.00m,p-Xylene 1 07/12/23 01:42 V35235TBL
6.09 µg/L 0.210 0.500Xylene (Total)1 07/12/23 01:42 V35235KCC
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%07/12/23 01:421 TBL V35235
Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%07/12/23 01:421 TBL V35235
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%07/12/23 01:421 TBL V35235
Surrogate: Toluene-d8 92.4 Limits: 70-130%07/12/23 01:421 TBL V35235
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V35162 07/11/23 09:46
<0.00347 µg/L 0.00347 0.02101,2-Dibromoethane 1 07/11/23 14:50 V35214TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-188-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #6389 Received : 07/07/2023
Handy Corner
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
89043 Matrix:
7/5/2023 15:56
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 07/10/23 15:24
<25.8 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 07/10/23 15:24
<4.02 µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 07/10/23 15:24
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V35150 07/10/23 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 07/10/23 15:24 V35151TBL
29.3 J µg/L 25.8 50.0Aliphatic C9-C12 1 07/10/23 15:24 V35151TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 07/10/23 15:24 V35151TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)87.7 Limits: 70-130%07/10/23 15:241 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)110 Limits: 70-130%07/10/23 15:241 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 28 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Metals Analysis
6010D
V35283QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V35160
Associated Lab Samples: 89041, 89042, 89043
LRB-V35160 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/12/23 16:310.0060.002<0.002mg/LLead
LCS-V35160Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1150.1150.100mg/LLead 80-120
V 89048-MS-V35160 V 89048-MSD-V35160Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.112 1120.1140.1000.100< 0.002mg/LLead 114 75-125 1.7 20.0
V 89048-PDS-V35160Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
07/12/23 17:191060.264mg/LLead
Page 1 of 22Date:07/20/2023 11:37 AM
Page 29 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
Associated Lab Samples: 89040
LRB-V35227 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/11/23 12:5210.01.80<1.80µg/LAcetone
07/11/23 12:520.5000.180<0.180µg/LBenzene
07/11/23 12:520.5000.210<0.210µg/LBromobenzene
07/11/23 12:521.000.420<0.420µg/LBromochloromethane
07/11/23 12:520.5000.160<0.160µg/LBromodichloromethane
07/11/23 12:525.001.50<1.50µg/LBromoform
07/11/23 12:521.000.280<0.280µg/LBromomethane
07/11/23 12:520.5000.180<0.180µg/Ln-Butylbenzene
07/11/23 12:520.5000.200<0.200µg/Lsec-Butyl benzene
07/11/23 12:522.000.920<0.920µg/Ltert-Butyl benzene
07/11/23 12:520.5000.180<0.180µg/LCarbon Tetrachloride
07/11/23 12:520.5000.190<0.190µg/LChlorobenzene
07/11/23 12:520.5000.190<0.190µg/LChlorodibromomethane
07/11/23 12:521.000.430<0.430µg/LChloroethane
07/11/23 12:520.5000.220<0.220µg/LChloroform
07/11/23 12:520.5000.220<0.220µg/LChloromethane
07/11/23 12:520.5000.200<0.200µg/L2-Chlorotoluene
07/11/23 12:520.5000.200<0.200µg/L4-Chlorotoluene
07/11/23 12:520.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/11/23 12:522.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/11/23 12:520.5000.200<0.200µg/L1,2-Dibromoethane
07/11/23 12:520.5000.230<0.230µg/LDibromomethane
07/11/23 12:520.5000.220<0.220µg/L1,2-Dichlorobenzene
07/11/23 12:520.5000.190<0.190µg/L1,3-Dichlorobenzene
07/11/23 12:520.5000.210<0.210µg/L1,4-Dichlorobenzene
07/11/23 12:525.001.20<1.20µg/LDichlorodifluoromethane
07/11/23 12:520.5000.240<0.240µg/L1,1-Dichloroethane
Page 2 of 22Date:07/20/2023 11:37 AM
Page 30 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
Associated Lab Samples: 89040
LRB-V35227 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/11/23 12:520.5000.150<0.150µg/L1,2-Dichloroethane
07/11/23 12:520.5000.150<0.150µg/L1,1-Dichloroethene
07/11/23 12:520.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/11/23 12:520.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/11/23 12:520.5000.190<0.190µg/L1,2-Dichloropropane
07/11/23 12:520.5000.130<0.130µg/L1,3-Dichloropropane
07/11/23 12:522.000.210<0.210µg/L2,2-Dichloropropane
07/11/23 12:520.5000.200<0.200µg/L1,1-Dichloropropene
07/11/23 12:520.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/11/23 12:520.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/11/23 12:5220042.0<42.0µg/LEthanol
07/11/23 12:520.5000.170<0.170µg/LEthylbenzene
07/11/23 12:523.000.350<0.350µg/LHexachlorobutadiene
07/11/23 12:521.000.380<0.380µg/L2-Hexanone
07/11/23 12:520.5000.180<0.180µg/LIsopropylbenzene
07/11/23 12:520.5000.089<0.089µg/L4-Isopropyl toluene
07/11/23 12:525.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/11/23 12:521.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/11/23 12:521.000.078<0.078µg/L4-Methyl-2-Pentanone
07/11/23 12:522.000.330<0.330µg/LMethylene Chloride
07/11/23 12:521.000.470<0.470µg/LNaphthalene
07/11/23 12:520.5000.190<0.190µg/Ln-Propylbenzene
07/11/23 12:520.5000.220<0.220µg/LStyrene
07/11/23 12:520.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
07/11/23 12:520.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/11/23 12:520.5000.220<0.220µg/LTetrachloroethene
07/11/23 12:520.5000.220<0.220µg/LToluene
Page 3 of 22Date:07/20/2023 11:37 AM
Page 31 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
Associated Lab Samples: 89040
LRB-V35227 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/11/23 12:520.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/11/23 12:520.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/11/23 12:520.5000.160<0.160µg/L1,1,1-Trichloroethane
07/11/23 12:520.5000.096<0.096µg/L1,1,2-Trichloroethane
07/11/23 12:520.5000.180<0.180µg/LTrichloroethene
07/11/23 12:520.5000.180<0.180µg/LTrichlorofluoromethane
07/11/23 12:520.5000.270<0.270µg/L1,2,3-Trichloropropane
07/11/23 12:520.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/11/23 12:520.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/11/23 12:525.001.00<1.00µg/LVinyl Acetate
07/11/23 12:520.5000.170<0.170µg/LVinyl Chloride
07/11/23 12:520.5000.210<0.210µg/Lo-Xylene
07/11/23 12:521.000.420<0.420µg/Lm,p-Xylene
07/11/23 12:524-Bromofluorobenzene (S)101 70-130
07/11/23 12:52Dibromofluoromethane (S)95.4 70-130
07/11/23 12:521,2-Dichloroethane - d4 (S)98.6 70-130
07/11/23 12:52Toluene-d8 (S)92.4 70-130
LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
29.3 73.272.028.840.0µg/LAcetone 40-160 1.7 20.0
21.9 11011122.120.0µg/LBenzene 70-130 0.9 20.0
20.3 10210521.020.0µg/LBromobenzene 70-130 3.3 20.0
22.5 11311322.520.0µg/LBromochloromethane 70-130 0.0 20.0
22.8 11411623.120.0µg/LBromodichloromethane 70-130 1.3 20.0
Page 4 of 22Date:07/20/2023 11:37 AM
Page 32 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.1 10610521.020.0µg/LBromoform 70-130 0.4 20.0
16.8 84.077.515.520.0µg/LBromomethane 60-140 8.0 20.0
21.1 10610921.720.0µg/Ln-Butylbenzene 70-130 2.8 20.0
21.1 10611021.920.0µg/Lsec-Butyl benzene 70-130 3.7 20.0
20.9 10510821.620.0µg/Ltert-Butyl benzene 70-130 3.2 20.0
22.1 11111322.520.0µg/LCarbon Tetrachloride 70-130 1.7 20.0
21.2 10610721.420.0µg/LChlorobenzene 70-130 0.9 20.0
21.1 10610621.220.0µg/LChlorodibromomethane 70-130 0.4 20.0
21.8 10910721.420.0µg/LChloroethane 60-140 1.8 20.0
22.2 11111022.020.0µg/LChloroform 70-130 0.9 20.0
19.3 96.591.018.220.0µg/LChloromethane 60-140 5.8 20.0
21.5 10811022.020.0µg/L2-Chlorotoluene 70-130 2.2 20.0
20.8 10410621.220.0µg/L4-Chlorotoluene 70-130 1.9 20.0
22.4 11211222.320.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.4 20.0
18.7 93.593.018.620.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.5 20.0
21.3 10710420.820.0µg/L1,2-Dibromoethane 70-130 2.3 20.0
23.0 11511422.720.0µg/LDibromomethane 70-130 1.3 20.0
20.1 10110320.620.0µg/L1,2-Dichlorobenzene 70-130 2.4 20.0
20.3 10210420.720.0µg/L1,3-Dichlorobenzene 70-130 1.9 20.0
19.9 99.510320.620.0µg/L1,4-Dichlorobenzene 70-130 3.4 20.0
19.5 97.599.019.820.0µg/LDichlorodifluoromethane 60-140 1.5 20.0
22.4 11211222.420.0µg/L1,1-Dichloroethane 70-130 0.0 20.0
22.9 11511623.120.0µg/L1,2-Dichloroethane 70-130 0.8 20.0
22.5 11311523.020.0µg/L1,1-Dichloroethene 70-130 2.1 20.0
22.8 11411623.220.0µg/Lcis-1,2-Dichloroethene 70-130 1.7 20.0
22.8 11411422.720.0µg/Ltrans-1,2-Dichloroethene 70-130 0.4 20.0
Page 5 of 22Date:07/20/2023 11:37 AM
Page 33 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.8 11411422.820.0µg/L1,2-Dichloropropane 70-130 0.0 20.0
20.5 10310320.620.0µg/L1,3-Dichloropropane 70-130 0.4 20.0
23.4 11712124.120.0µg/L2,2-Dichloropropane 70-130 2.9 20.0
22.2 11111422.720.0µg/L1,1-Dichloropropene 70-130 2.2 20.0
22.5 11311522.920.0µg/Lcis-1,3-Dichloropropene 70-130 1.7 20.0
23.3 11711623.220.0µg/Ltrans-1,3-Dichloropropene 70-130 0.4 20.0
658 132106532500µg/LEthanol 60-140 21.1*20.0
21.1 10610921.720.0µg/LEthylbenzene 70-130 2.8 20.0
20.4 10210821.620.0µg/LHexachlorobutadiene 70-130 5.7 20.0
18.1 90.591.018.220.0µg/L2-Hexanone 60-140 0.5 20.0
21.1 10610921.820.0µg/LIsopropylbenzene 70-130 3.2 20.0
21.2 10611021.920.0µg/L4-Isopropyl toluene 70-130 3.2 20.0
17.3 86.579.515.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 8.4 20.0
21.2 10610520.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.4 20.0
22.9 11511322.520.0µg/L4-Methyl-2-Pentanone 60-140 1.7 20.0
23.4 11711522.920.0µg/LMethylene Chloride 70-130 2.1 20.0
19.3 96.597.519.520.0µg/LNaphthalene 70-130 1.0 20.0
21.5 10811222.320.0µg/Ln-Propylbenzene 70-130 3.6 20.0
21.6 10810621.120.0µg/LStyrene 70-130 2.3 20.0
20.7 10410721.320.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.8 20.0
19.5 97.510020.020.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.5 20.0
21.0 10510821.520.0µg/LTetrachloroethene 70-130 2.3 20.0
22.4 11211422.820.0µg/LToluene 70-130 1.7 20.0
21.5 10810921.820.0µg/L1,2,3-Trichlorobenzene 70-130 1.3 20.0
19.5 97.510220.420.0µg/L1,2,4-Trichlorobenzene 70-130 4.5 20.0
22.6 11311522.920.0µg/L1,1,1-Trichloroethane 70-130 1.3 20.0
Page 6 of 22* QC Fail Date:07/20/2023 11:37 AM
Page 34 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.6 11311523.020.0µg/L1,1,2-Trichloroethane 70-130 1.7 20.0
21.8 10911122.220.0µg/LTrichloroethene 70-130 1.8 20.0
21.5 10810921.820.0µg/LTrichlorofluoromethane 60-140 1.3 20.0
20.5 10310420.820.0µg/L1,2,3-Trichloropropane 70-130 1.4 20.0
20.9 10510821.620.0µg/L1,2,4-Trimethylbenzene 70-130 3.2 20.0
21.2 10610921.820.0µg/L1,3,5-Trimethylbenzene 70-130 2.7 20.0
23.3 11711823.620.0µg/LVinyl Acetate 60-140 1.2 20.0
20.2 10110420.820.0µg/LVinyl Chloride 60-140 2.9 20.0
21.7 10911122.120.0µg/Lo-Xylene 70-130 1.8 20.0
45.8 11511646.540.0µg/Lm,p-Xylene 70-130 1.5 20.0
1011024-Bromofluorobenzene (S)70-130
96.095.4Dibromofluoromethane (S)70-130
1021021,2-Dichloroethane - d4 (S)70-130
92.893.2Toluene-d8 (S)70-130
Page 7 of 22Date:07/20/2023 11:37 AM
Page 35 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35235QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35234
Associated Lab Samples: 89042, 89043
LRB-V35234 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/23 01:1710.01.80<1.80µg/LAcetone
07/12/23 01:170.5000.180<0.180µg/LBenzene
07/12/23 01:170.5000.210<0.210µg/LBromobenzene
07/12/23 01:171.000.420<0.420µg/LBromochloromethane
07/12/23 01:170.5000.160<0.160µg/LBromodichloromethane
07/12/23 01:175.001.50<1.50µg/LBromoform
07/12/23 01:171.000.280<0.280µg/LBromomethane
07/12/23 01:170.5000.180<0.180µg/Ln-Butylbenzene
07/12/23 01:170.5000.200<0.200µg/Lsec-Butyl benzene
07/12/23 01:172.000.920<0.920µg/Ltert-Butyl benzene
07/12/23 01:170.5000.180<0.180µg/LCarbon Tetrachloride
07/12/23 01:170.5000.190<0.190µg/LChlorobenzene
07/12/23 01:170.5000.190<0.190µg/LChlorodibromomethane
07/12/23 01:171.000.430<0.430µg/LChloroethane
07/12/23 01:170.5000.220<0.220µg/LChloroform
07/12/23 01:170.5000.220<0.220µg/LChloromethane
07/12/23 01:170.5000.200<0.200µg/L2-Chlorotoluene
07/12/23 01:170.5000.200<0.200µg/L4-Chlorotoluene
07/12/23 01:170.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/12/23 01:172.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/12/23 01:170.5000.230<0.230µg/LDibromomethane
07/12/23 01:170.5000.220<0.220µg/L1,2-Dichlorobenzene
07/12/23 01:170.5000.190<0.190µg/L1,3-Dichlorobenzene
07/12/23 01:170.5000.210<0.210µg/L1,4-Dichlorobenzene
07/12/23 01:175.001.20<1.20µg/LDichlorodifluoromethane
07/12/23 01:170.5000.240<0.240µg/L1,1-Dichloroethane
07/12/23 01:170.5000.150<0.150µg/L1,2-Dichloroethane
Page 8 of 22Date:07/20/2023 11:37 AM
Page 36 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35235QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35234
Associated Lab Samples: 89042, 89043
LRB-V35234 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/23 01:170.5000.150<0.150µg/L1,1-Dichloroethene
07/12/23 01:170.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/12/23 01:170.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/12/23 01:170.5000.190<0.190µg/L1,2-Dichloropropane
07/12/23 01:170.5000.130<0.130µg/L1,3-Dichloropropane
07/12/23 01:172.000.210<0.210µg/L2,2-Dichloropropane
07/12/23 01:170.5000.200<0.200µg/L1,1-Dichloropropene
07/12/23 01:170.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/12/23 01:170.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/12/23 01:1720042.0<42.0µg/LEthanol
07/12/23 01:170.5000.170<0.170µg/LEthylbenzene
07/12/23 01:173.000.350<0.350µg/LHexachlorobutadiene
07/12/23 01:171.000.380<0.380µg/L2-Hexanone
07/12/23 01:170.5000.180<0.180µg/LIsopropylbenzene
07/12/23 01:170.5000.089<0.089µg/L4-Isopropyl toluene
07/12/23 01:175.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/12/23 01:171.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/12/23 01:171.000.078<0.078µg/L4-Methyl-2-Pentanone
07/12/23 01:172.000.330<0.330µg/LMethylene Chloride
07/12/23 01:171.000.470<0.470µg/LNaphthalene
07/12/23 01:170.5000.190<0.190µg/Ln-Propylbenzene
07/12/23 01:170.5000.220<0.220µg/LStyrene
07/12/23 01:1710.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
07/12/23 01:1710.00.350<0.350µg/Ltert-Butyl formate (TBF)
07/12/23 01:1710.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
07/12/23 01:1710.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
07/12/23 01:170.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
Page 9 of 22Date:07/20/2023 11:37 AM
Page 37 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35235QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35234
Associated Lab Samples: 89042, 89043
LRB-V35234 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/23 01:170.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/12/23 01:170.5000.220<0.220µg/LTetrachloroethene
07/12/23 01:170.5000.220<0.220µg/LToluene
07/12/23 01:170.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/12/23 01:170.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/12/23 01:170.5000.160<0.160µg/L1,1,1-Trichloroethane
07/12/23 01:170.5000.096<0.096µg/L1,1,2-Trichloroethane
07/12/23 01:170.5000.180<0.180µg/LTrichloroethene
07/12/23 01:170.5000.180<0.180µg/LTrichlorofluoromethane
07/12/23 01:170.5000.270<0.270µg/L1,2,3-Trichloropropane
07/12/23 01:170.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/12/23 01:170.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/12/23 01:175.001.00<1.00µg/LVinyl Acetate
07/12/23 01:170.5000.170<0.170µg/LVinyl Chloride
07/12/23 01:170.5000.210<0.210µg/Lo-Xylene
07/12/23 01:171.000.420<0.420µg/Lm,p-Xylene
07/12/23 01:1710.01.00<1.00µg/L3,3-Dimethyl-1-butanol
07/12/23 01:174-Bromofluorobenzene (S)103 70-130
07/12/23 01:17Dibromofluoromethane (S)96.8 70-130
07/12/23 01:171,2-Dichloroethane - d4 (S)102 70-130
07/12/23 01:17Toluene-d8 (S)91.6 70-130
LCS-V35234 LCSD-V35234Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
33.4 83.582.533.040.0µg/LAcetone 40-160 1.2 20.0
Page 10 of 22Date:07/20/2023 11:37 AM
Page 38 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35235QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35234
LCS-V35234 LCSD-V35234Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.1 11110721.420.0µg/LBenzene 70-130 3.2 20.0
20.0 10099.519.920.0µg/LBromobenzene 70-130 0.5 20.0
23.0 11511122.120.0µg/LBromochloromethane 70-130 3.9 20.0
23.2 11611422.820.0µg/LBromodichloromethane 70-130 1.7 20.0
21.2 10610621.220.0µg/LBromoform 70-130 0.0 20.0
15.8 79.080.516.120.0µg/LBromomethane 60-140 1.8 20.0
20.3 10210020.020.0µg/Ln-Butylbenzene 70-130 1.4 20.0
20.7 10410220.320.0µg/Lsec-Butyl benzene 70-130 1.9 20.0
20.7 10410220.320.0µg/Ltert-Butyl benzene 70-130 1.9 20.0
22.3 11210821.620.0µg/LCarbon Tetrachloride 70-130 3.1 20.0
21.3 10710320.620.0µg/LChlorobenzene 70-130 3.3 20.0
21.2 10610721.320.0µg/LChlorodibromomethane 70-130 0.4 20.0
21.0 10510420.820.0µg/LChloroethane 60-140 0.9 20.0
22.3 11210921.720.0µg/LChloroform 70-130 2.7 20.0
18.9 94.588.017.620.0µg/LChloromethane 60-140 7.1 20.0
21.2 10610420.820.0µg/L2-Chlorotoluene 70-130 1.9 20.0
20.5 10310020.020.0µg/L4-Chlorotoluene 70-130 2.4 20.0
22.4 11211122.120.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.3 20.0
19.5 97.599.519.920.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.0 20.0
22.7 11411723.320.0µg/LDibromomethane 70-130 2.6 20.0
19.9 99.599.019.820.0µg/L1,2-Dichlorobenzene 70-130 0.5 20.0
20.1 10198.019.620.0µg/L1,3-Dichlorobenzene 70-130 2.5 20.0
19.8 99.097.519.520.0µg/L1,4-Dichlorobenzene 70-130 1.5 20.0
20.1 10196.519.320.0µg/LDichlorodifluoromethane 60-140 4.0 20.0
22.3 11210721.320.0µg/L1,1-Dichloroethane 70-130 4.5 20.0
23.4 11711422.720.0µg/L1,2-Dichloroethane 70-130 3.0 20.0
Page 11 of 22Date:07/20/2023 11:37 AM
Page 39 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35235QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35234
LCS-V35234 LCSD-V35234Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.5 11311022.020.0µg/L1,1-Dichloroethene 70-130 2.2 20.0
23.3 11711122.220.0µg/Lcis-1,2-Dichloroethene 70-130 4.8 20.0
22.5 11310821.620.0µg/Ltrans-1,2-Dichloroethene 70-130 4.0 20.0
22.7 11411022.020.0µg/L1,2-Dichloropropane 70-130 3.1 20.0
20.6 10310420.820.0µg/L1,3-Dichloropropane 70-130 0.9 20.0
20.0 10095.019.020.0µg/L2,2-Dichloropropane 70-130 5.1 20.0
22.5 11310821.620.0µg/L1,1-Dichloropropene 70-130 4.0 20.0
22.4 11211021.920.0µg/Lcis-1,3-Dichloropropene 70-130 2.2 20.0
23.0 11511522.920.0µg/Ltrans-1,3-Dichloropropene 70-130 0.4 20.0
676 135134669500µg/LEthanol 60-140 1.0 20.0
21.1 10610420.720.0µg/LEthylbenzene 70-130 1.9 20.0
20.1 10110120.120.0µg/LHexachlorobutadiene 70-130 0.0 20.0
19.2 96.096.019.220.0µg/L2-Hexanone 60-140 0.0 20.0
20.9 10510220.420.0µg/LIsopropylbenzene 70-130 2.4 20.0
20.9 10510220.320.0µg/L4-Isopropyl toluene 70-130 2.9 20.0
17.5 87.582.516.520.0µg/LMethyl Ethyl Ketone (MEK)60-140 5.8 20.0
21.6 10810721.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.3 20.0
23.8 11911723.420.0µg/L4-Methyl-2-Pentanone 60-140 1.6 20.0
23.3 11711322.620.0µg/LMethylene Chloride 70-130 3.0 20.0
20.9 10510821.620.0µg/LNaphthalene 70-130 3.2 20.0
21.1 10610320.520.0µg/Ln-Propylbenzene 70-130 2.8 20.0
20.8 10410220.420.0µg/LStyrene 70-130 1.9 20.0
54.5 13613955.540.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.8 20.0
35.3 88.294.537.840.0µg/Ltert-Butyl formate (TBF)40-140 6.8 20.0
24.9 12512825.520.0µg/Ltert-Amyl Alcohol (TAA)40-140 2.3 20.0
44.1 11010943.440.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.6 20.0
Page 12 of 22Date:07/20/2023 11:37 AM
Page 40 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35235QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35234
LCS-V35234 LCSD-V35234Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.0 10510420.720.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.4 20.0
18.5 92.595.019.020.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.6 20.0
21.2 10610120.120.0µg/LTetrachloroethene 70-130 5.3 20.0
22.6 11311222.320.0µg/LToluene 70-130 1.3 20.0
25.4 12712525.020.0µg/L1,2,3-Trichlorobenzene 70-130 1.5 20.0
20.5 10310320.520.0µg/L1,2,4-Trichlorobenzene 70-130 0.0 20.0
22.5 11311222.320.0µg/L1,1,1-Trichloroethane 70-130 0.8 20.0
23.5 11811523.020.0µg/L1,1,2-Trichloroethane 70-130 2.1 20.0
23.4 11711022.020.0µg/LTrichloroethene 70-130 6.1 20.0
22.6 11310921.720.0µg/LTrichlorofluoromethane 60-140 4.0 20.0
21.2 10610520.920.0µg/L1,2,3-Trichloropropane 70-130 1.4 20.0
20.7 10410220.420.0µg/L1,2,4-Trimethylbenzene 70-130 1.4 20.0
20.7 10410220.320.0µg/L1,3,5-Trimethylbenzene 70-130 1.9 20.0
16.8 84.092.018.420.0µg/LVinyl Acetate 60-140 9.0 20.0
20.9 10510120.220.0µg/LVinyl Chloride 60-140 3.4 20.0
21.8 10910721.320.0µg/Lo-Xylene 70-130 2.3 20.0
45.8 11511244.740.0µg/Lm,p-Xylene 70-130 2.4 20.0
23.0 11511523.020.0µg/L3,3-Dimethyl-1-butanol 70-130 0.0 20.0
1011024-Bromofluorobenzene (S)70-130
96.895.8Dibromofluoromethane (S)70-130
1041041,2-Dichloroethane - d4 (S)70-130
92.093.8Toluene-d8 (S)70-130
Page 13 of 22Date:07/20/2023 11:37 AM
Page 41 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35284QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35278
Associated Lab Samples: 89041
LRB-V35278 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/23 04:0510.01.80<1.80µg/LAcetone
07/12/23 04:050.5000.180<0.180µg/LBenzene
07/12/23 04:050.5000.210<0.210µg/LBromobenzene
07/12/23 04:051.000.420<0.420µg/LBromochloromethane
07/12/23 04:050.5000.160<0.160µg/LBromodichloromethane
07/12/23 04:055.001.50<1.50µg/LBromoform
07/12/23 04:051.000.280<0.280µg/LBromomethane
07/12/23 04:050.5000.180<0.180µg/Ln-Butylbenzene
07/12/23 04:050.5000.200<0.200µg/Lsec-Butyl benzene
07/12/23 04:052.000.920<0.920µg/Ltert-Butyl benzene
07/12/23 04:050.5000.180<0.180µg/LCarbon Tetrachloride
07/12/23 04:050.5000.190<0.190µg/LChlorobenzene
07/12/23 04:050.5000.190<0.190µg/LChlorodibromomethane
07/12/23 04:051.000.430<0.430µg/LChloroethane
07/12/23 04:050.5000.220<0.220µg/LChloroform
07/12/23 04:050.5000.220<0.220µg/LChloromethane
07/12/23 04:050.5000.200<0.200µg/L2-Chlorotoluene
07/12/23 04:050.5000.200<0.200µg/L4-Chlorotoluene
07/12/23 04:050.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/12/23 04:052.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/12/23 04:050.5000.230<0.230µg/LDibromomethane
07/12/23 04:050.5000.220<0.220µg/L1,2-Dichlorobenzene
07/12/23 04:050.5000.190<0.190µg/L1,3-Dichlorobenzene
07/12/23 04:050.5000.210<0.210µg/L1,4-Dichlorobenzene
07/12/23 04:055.001.20<1.20µg/LDichlorodifluoromethane
07/12/23 04:050.5000.240<0.240µg/L1,1-Dichloroethane
07/12/23 04:050.5000.150<0.150µg/L1,2-Dichloroethane
Page 14 of 22Date:07/20/2023 11:37 AM
Page 42 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35284QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35278
Associated Lab Samples: 89041
LRB-V35278 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/23 04:050.5000.150<0.150µg/L1,1-Dichloroethene
07/12/23 04:050.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/12/23 04:050.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/12/23 04:050.5000.190<0.190µg/L1,2-Dichloropropane
07/12/23 04:050.5000.130<0.130µg/L1,3-Dichloropropane
07/12/23 04:052.000.210<0.210µg/L2,2-Dichloropropane
07/12/23 04:050.5000.200<0.200µg/L1,1-Dichloropropene
07/12/23 04:050.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/12/23 04:050.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/12/23 04:0520042.0<42.0µg/LEthanol
07/12/23 04:050.5000.170<0.170µg/LEthylbenzene
07/12/23 04:053.000.350<0.350µg/LHexachlorobutadiene
07/12/23 04:051.000.380<0.380µg/L2-Hexanone
07/12/23 04:050.5000.180<0.180µg/LIsopropylbenzene
07/12/23 04:050.5000.089<0.089µg/L4-Isopropyl toluene
07/12/23 04:055.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/12/23 04:051.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/12/23 04:051.000.078<0.078µg/L4-Methyl-2-Pentanone
07/12/23 04:052.000.330<0.330µg/LMethylene Chloride
07/12/23 04:051.000.470<0.470µg/LNaphthalene
07/12/23 04:050.5000.190<0.190µg/Ln-Propylbenzene
07/12/23 04:050.5000.220<0.220µg/LStyrene
07/12/23 04:0510.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
07/12/23 04:0510.00.350<0.350µg/Ltert-Butyl formate (TBF)
07/12/23 04:0510.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
07/12/23 04:0510.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
07/12/23 04:050.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
Page 15 of 22Date:07/20/2023 11:37 AM
Page 43 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35284QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35278
Associated Lab Samples: 89041
LRB-V35278 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/23 04:050.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/12/23 04:050.5000.220<0.220µg/LTetrachloroethene
07/12/23 04:050.5000.220<0.220µg/LToluene
07/12/23 04:050.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/12/23 04:050.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/12/23 04:050.5000.160<0.160µg/L1,1,1-Trichloroethane
07/12/23 04:050.5000.096<0.096µg/L1,1,2-Trichloroethane
07/12/23 04:050.5000.180<0.180µg/LTrichloroethene
07/12/23 04:050.5000.180<0.180µg/LTrichlorofluoromethane
07/12/23 04:050.5000.270<0.270µg/L1,2,3-Trichloropropane
07/12/23 04:050.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/12/23 04:050.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/12/23 04:055.001.00<1.00µg/LVinyl Acetate
07/12/23 04:050.5000.170<0.170µg/LVinyl Chloride
07/12/23 04:050.5000.210<0.210µg/Lo-Xylene
07/12/23 04:051.000.420<0.420µg/Lm,p-Xylene
07/12/23 04:0510.01.00<1.00µg/L3,3-Dimethyl-1-butanol
07/12/23 04:054-Bromofluorobenzene (S)93.6 70-130
07/12/23 04:05Dibromofluoromethane (S)97.4 70-130
07/12/23 04:051,2-Dichloroethane - d4 (S)92.6 70-130
07/12/23 04:05Toluene-d8 (S)91.8 70-130
LCS-V35278 LCSD-V35278Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.5 91.292.737.140.0µg/LAcetone 40-160 1.6 20.0
Page 16 of 22Date:07/20/2023 11:37 AM
Page 44 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35284QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35278
LCS-V35278 LCSD-V35278Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.8 99.010020.020.0µg/LBenzene 70-130 1.0 20.0
17.4 87.087.517.520.0µg/LBromobenzene 70-130 0.5 20.0
20.7 10410521.020.0µg/LBromochloromethane 70-130 1.4 20.0
19.1 95.597.519.520.0µg/LBromodichloromethane 70-130 2.0 20.0
18.6 93.096.019.220.0µg/LBromoform 70-130 3.1 20.0
17.4 87.084.016.820.0µg/LBromomethane 60-140 3.5 20.0
17.8 89.088.017.620.0µg/Ln-Butylbenzene 70-130 1.1 20.0
17.4 87.087.017.420.0µg/Lsec-Butyl benzene 70-130 0.0 20.0
18.0 90.091.018.220.0µg/Ltert-Butyl benzene 70-130 1.1 20.0
19.4 97.098.519.720.0µg/LCarbon Tetrachloride 70-130 1.5 20.0
19.7 98.599.019.820.0µg/LChlorobenzene 70-130 0.5 20.0
18.3 91.596.519.320.0µg/LChlorodibromomethane 70-130 5.3 20.0
20.6 10310621.220.0µg/LChloroethane 60-140 2.8 20.0
19.6 98.098.019.620.0µg/LChloroform 70-130 0.0 20.0
16.2 81.077.515.520.0µg/LChloromethane 60-140 4.4 20.0
17.3 86.585.517.120.0µg/L2-Chlorotoluene 70-130 1.1 20.0
17.0 85.084.516.920.0µg/L4-Chlorotoluene 70-130 0.5 20.0
17.8 89.088.517.720.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.5 20.0
17.8 89.088.517.720.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.5 20.0
20.0 10099.019.820.0µg/LDibromomethane 70-130 1.0 20.0
18.9 94.595.519.120.0µg/L1,2-Dichlorobenzene 70-130 1.0 20.0
19.2 96.095.019.020.0µg/L1,3-Dichlorobenzene 70-130 1.0 20.0
18.3 91.593.518.720.0µg/L1,4-Dichlorobenzene 70-130 2.1 20.0
19.3 96.593.518.720.0µg/LDichlorodifluoromethane 60-140 3.1 20.0
19.3 96.595.519.120.0µg/L1,1-Dichloroethane 70-130 1.0 20.0
19.5 97.597.519.520.0µg/L1,2-Dichloroethane 70-130 0.0 20.0
Page 17 of 22Date:07/20/2023 11:37 AM
Page 45 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35284QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35278
LCS-V35278 LCSD-V35278Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.4 97.010020.020.0µg/L1,1-Dichloroethene 70-130 3.0 20.0
18.7 93.594.518.920.0µg/Lcis-1,2-Dichloroethene 70-130 1.0 20.0
19.7 98.597.519.520.0µg/Ltrans-1,2-Dichloroethene 70-130 1.0 20.0
19.1 95.597.519.520.0µg/L1,2-Dichloropropane 70-130 2.0 20.0
18.3 91.592.518.520.0µg/L1,3-Dichloropropane 70-130 1.0 20.0
16.9 84.584.516.920.0µg/L2,2-Dichloropropane 70-130 0.0 20.0
20.7 10410521.020.0µg/L1,1-Dichloropropene 70-130 1.4 20.0
18.4 92.095.019.020.0µg/Lcis-1,3-Dichloropropene 70-130 3.2 20.0
18.5 92.590.518.120.0µg/Ltrans-1,3-Dichloropropene 70-130 2.1 20.0
537 10788.6443500µg/LEthanol 60-140 19.1 20.0
17.9 89.591.518.320.0µg/LEthylbenzene 70-130 2.2 20.0
19.2 96.098.519.720.0µg/LHexachlorobutadiene 70-130 2.5 20.0
14.5 72.576.015.220.0µg/L2-Hexanone 60-140 4.7 20.0
18.0 90.089.517.920.0µg/LIsopropylbenzene 70-130 0.5 20.0
18.3 91.590.518.120.0µg/L4-Isopropyl toluene 70-130 1.0 20.0
17.1 85.576.015.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 11.7 20.0
19.7 98.597.019.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.5 20.0
16.0 80.081.016.220.0µg/L4-Methyl-2-Pentanone 60-140 1.2 20.0
19.3 96.596.519.320.0µg/LMethylene Chloride 70-130 0.0 20.0
14.7 73.571.014.220.0µg/LNaphthalene 70-130 3.4 20.0
17.5 87.587.017.420.0µg/Ln-Propylbenzene 70-130 0.5 20.0
18.7 93.597.019.420.0µg/LStyrene 70-130 3.6 20.0
28.4 71.073.529.440.0µg/Ltert-Butyl Alcohol (TBA)40-140 3.4 20.0
35.1 87.792.737.140.0µg/Ltert-Butyl formate (TBF)40-140 5.5 20.0
20.2 10189.017.820.0µg/Ltert-Amyl Alcohol (TAA)40-140 12.6 20.0
39.2 98.098.039.240.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.0 20.0
Page 18 of 22Date:07/20/2023 11:37 AM
Page 46 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35284QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35278
LCS-V35278 LCSD-V35278Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.2 96.096.019.220.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.0 20.0
17.1 85.586.517.320.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.1 20.0
19.7 98.510120.120.0µg/LTetrachloroethene 70-130 2.0 20.0
19.4 97.096.519.320.0µg/LToluene 70-130 0.5 20.0
19.4 97.099.519.920.0µg/L1,2,3-Trichlorobenzene 70-130 2.5 20.0
20.4 10210120.120.0µg/L1,2,4-Trichlorobenzene 70-130 1.4 20.0
20.1 10110220.320.0µg/L1,1,1-Trichloroethane 70-130 0.9 20.0
20.6 10310220.320.0µg/L1,1,2-Trichloroethane 70-130 1.4 20.0
21.4 10710721.420.0µg/LTrichloroethene 70-130 0.0 20.0
21.4 10710621.120.0µg/LTrichlorofluoromethane 60-140 1.4 20.0
18.2 91.084.516.920.0µg/L1,2,3-Trichloropropane 70-130 7.4 20.0
18.0 90.089.017.820.0µg/L1,2,4-Trimethylbenzene 70-130 1.1 20.0
18.0 90.089.017.820.0µg/L1,3,5-Trimethylbenzene 70-130 1.1 20.0
16.1 80.592.018.420.0µg/LVinyl Acetate 60-140 13.3 20.0
19.2 96.098.519.720.0µg/LVinyl Chloride 60-140 2.5 20.0
18.4 92.093.018.620.0µg/Lo-Xylene 70-130 1.0 20.0
39.0 97.598.239.340.0µg/Lm,p-Xylene 70-130 0.7 20.0
15.5 77.511322.620.0µg/L3,3-Dimethyl-1-butanol 70-130 37.2*20.0
91.891.44-Bromofluorobenzene (S)70-130
96.496.4Dibromofluoromethane (S)70-130
93.093.61,2-Dichloroethane - d4 (S)70-130
92.293.0Toluene-d8 (S)70-130
Page 19 of 22* QC Fail Date:07/20/2023 11:37 AM
Page 47 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35303QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35302
Associated Lab Samples: 89042
LRB-V35302 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/23 15:351.000.420<0.420µg/Lm,p-Xylene
07/12/23 15:354-Bromofluorobenzene (S)102 70-130
07/12/23 15:35Dibromofluoromethane (S)94.8 70-130
07/12/23 15:351,2-Dichloroethane - d4 (S)98.0 70-130
07/12/23 15:35Toluene-d8 (S)91.6 70-130
LCS-V35302 LCSD-V35302Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
44.8 11211445.740.0µg/Lm,p-Xylene 70-130 1.9 20.0
1031034-Bromofluorobenzene (S)70-130
95.095.6Dibromofluoromethane (S)70-130
1011031,2-Dichloroethane - d4 (S)70-130
92.491.6Toluene-d8 (S)70-130
Page 20 of 22Date:07/20/2023 11:37 AM
Page 48 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
EDB and DBCP by Microextraction GC/ECD
EPA-504.1
V35214QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-504.1(PREP)
QC Prep:V35162
Associated Lab Samples: 89041, 89042, 89043
LRB-V35162 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/11/23 10:060.02000.00330<0.00330µg/L1,2-Dibromoethane
LCS-V35162 LCSD-V35162Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.271 10899.60.2490.250µg/L1,2-Dibromoethane 70-130 8.4 20.0
V 89021-DUP-V35162Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/11/23 12:180.016.416.4µg/L1,2-Dibromoethane
V 89006-MS-V35162Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
0.312 1200.261< 0.00345µg/L1,2-Dibromoethane 70-130
Page 21 of 22Date:07/20/2023 11:37 AM
Page 49 of 52
Quality Control Data
23-188-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Handy Corner
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V35151QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V35150
Associated Lab Samples: 89041, 89042, 89043
LRB-V35150 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/10/23 14:3750.011.5<11.5µg/LAliphatic C5-C8
07/10/23 14:3750.025.8<25.8µg/LAliphatic C9-C12
07/10/23 14:3750.04.02<4.02µg/LAromatic C9-C10
07/10/23 14:372,5-Dibromotoluene (FID) (S)83.9 70-130
07/10/23 14:372,5-Dibromotoluene (PID) (S)88.3 70-130
LCS-V35150 LCSD-V35150Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
262 87.387.0261300µg/LAliphatic C5-C8 70-130 0.3 50.0
348 116116347300µg/LAliphatic C9-C12 70-130 0.2 50.0
119 119117117100µg/LAromatic C9-C10 70-130 1.6 50.0
82.877.72,5-Dibromotoluene (FID) (S)70-130
98.088.22,5-Dibromotoluene (PID) (S)70-130
Page 22 of 22Date:07/20/2023 11:37 AM
Page 50 of 52
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-188-0019
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:07/07/2023 18:21:30
Special precautions or instructions included?
Comments:
Page 51 of 52
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