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Home My WebLink AboutMO-29901_48992_CA_LSA_20230731 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 July 31, 2023 Mr. Ryan Mills NCDEQ-UST Section Mooresville Regional Office 610 East Center Ave. Mooresville, NC 28115 Re: High-Risk Limited Site Assessment Report Handy Corner 2076 Startown Road Lincolnton, Lincoln County North Carolina Facility ID Number: 0-014377 Incident Number: 48992 GRI Project Number: 6389 Dear Mr. Mills, Please find enclosed the referenced report for the abovementioned site. If you have any questions, please contact Joanna Alley at 704-845-4010. Sincerely, Geological Resources, Inc. Johanna Moats AP/AR Coordinator Enclosure Cc: Mr. Jimmy White, Nisbet Oil Company, file 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Engineering Certification: C-2727 • Geology Certification: C-127 High-Risk Limited Site Assessment Report Handy Corner 2076 Startown Road Lincolnton, Lincoln County North Carolina Facility ID Number: 0-014377 Incident Number: 48992 GRI Project Number: 6389 Prepared for: Jimmy White Nisbet Oil Company 1818 Baxter Street Charlotte, North Carolina 28204 July 31, 2023 Joanna Alley, P.E. Project Manager ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 i EXECUTIVE SUMMARY The Handy Corner site is located at 2076 Startown Road in Lincolnton, Lincoln County, North Carolina. The property operates as a petroleum retail facility and convenience store. The site is covered by asphalt, concrete, and grass. There are one 10,000-gallon and two 6,000-gallon gasoline USTs and one 10,000- gallon and one 2,000-gallon diesel USTs currently in use at the site with five associated gasoline, one kerosene, and two diesel dispensers. The surrounding properties are residential. On January 4, 2023, a site check was conducted at the subject site due to a non-passing spill bucket for the 10,000-gallon RUL gasoline UST. The concentration of GRO exceeded the RAL; therefore, an LSA was required. A receptor survey was conducted on April 26, 2023. Nineteen water supply wells were identified within a 1,500-foot radius of the site, of which eleven are potable and located within 1,000 feet of the source area. Three of those water supply wells were identified within a 250-foot radius of the site. Public water is available along Startown Road but is not available along Clarks Creek Road or Carlos Road. No surface water bodies were identified within a 500-foot radius of the site. On April 26, 2023, one Type II monitoring well was installed at the UST basin. Soil samples were collected at 10-foot intervals during the installation of MW-1. All of the reported contaminant concentrations were below the soil-to-water MCCs. On April 26, 2023, a ground water sample was collected from MW-1. The concentrations of benzene, bromodichloromethane, lead, and C9-C10 aromatics reported in the ground water sample collected from MW-1 exceeded the MACs. Please note that bromodichloromethane is not a petroleum constituent. Based on the reported ground water contaminant concentrations and the presence of water supply wells within a 250-foot radius of the site and potable water supply wells within a 1,000-foot radius of the site, a Phase II LSA was required to be completed at the site. On July 5, 2023, three additional Type II monitoring wells were installed at the site in order to determine the ground water flow direction. A ground water sample was collected from each well following installation. The concentrations of benzene, toluene, xylenes, naphthalene, TAA, TBA, 1,2,4- trimethylbenzene, lead, C5-C8 aliphatics, C9-C12 aliphatics, and/or C9-C10 aromatics reported in the ground water samples collected from MW-2, MW-3, and MW-4 exceeded the MACs. All of the reported concentrations were below the GCLs. No free product was observed at the site. Based on the presence of water supply well within 250 feet of the site, the presence of potable water supply wells within 1,000 feet of the site, and the reported contaminant concentrations exceeding the MACs, the site risk should be classified as high and a CSA should be conducted at the site. Based on the relatively limited contamination at the site, it is recommended to resample all wells prior to conducting the CSA to confirm the results of the April and July 2023 sampling events. The water supply wells located ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 ii within 250 feet of the site should also be sampled. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 iii SITE INFORMATION 1. Site Identification  Handy Corner (Facility ID 0-014377)  Incident Number 48992 – High Risk  Location of Source Area: 2076 Startown Road Lincolnton, NC 28092 Lincoln County (Figure 1) 35.512600°N, 81.262114°W (Topographical Map) 2. Information about Contacts Associated with the Leaking UST System UST Owner Nisbet Oil Company (Table 1) 1818 Baxter Street Charlotte, NC 28204 JWhite@nisbetoil.com 704-332-7755 UST Operator Handy Corner 2076 Startown Road Lincolnton, NC 28092 Email: Unknown 704-732-6050 Property Owner Rhodes & Beal Oil Co., Inc. 1404 E Main St. Lincolnton, NC 28092 Email Unknown 704-735-2508 Property Occupant Handy Corner 2076 Startown Road Lincolnton, NC 28092 Email: Unknown 704-732-6050 Consultant/Contractor Geological Resources, Inc. 3502 Hayes Road Monroe, NC 28110 jra@geologicalresourcesinc.com 704-845-4010 Analytical Laboratory Waypoint Analytical 449 Springbrook Road Charlotte, NC 28217 State Certification Nos. 37735 & 402 704-529-6364 3. Information about Release  Release was discovered on January 4, 2023  An unknown amount of product was released from the leaking UST System via a non-passing spill bucket  One (1) 10,000-gallon gasoline UST, two (2) 6,000-gallon gasoline USTs, one (1) 10,000-gallon diesel UST, and one (1) 2,000-gallon diesel UST are in use at the site (Table 2) Certification: I, Eric M. Eubanks, a Licensed Geologist for Geological Resources, Inc., do certify that the information contained in this report is correct and accurate to the best of my knowledge. Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The certification numbers of the corporation are C-127 and C-2727, respectively. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 iv ACRONYMS ACM: Asbestos Containing Materials AFVR: Aggressive Fluid-Vapor Recovery ARR: Acknowledgement of Report Receipt AS: Air Sparging AST: Aboveground Storage Tank ASTM: American Society for Testing and Materials BGS: Below Ground Surface CAP: Corrective Action Plan CFR: Code of Federal Regulations CSA: Comprehensive Site Assessment DPE: Dual Phase Extraction DRO: Total Petroleum Hydrocarbons Diesel Range Organics DWM: Division of Waste Management DWR: Department of Water Resources EPA: Environmental Protection Agency EPH: Extractible Petroleum Hydrocarbons ESA: Environmental Site Assessment GCL: Gross Contamination Level GRI: Geological Resources, Inc. GRO: Total Petroleum Hydrocarbons Gasoline Range Organics LSA: Limited Site Assessment MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202 MADEP: Massachusetts Department of Environmental Protection MCC: Maximum Contaminant Concentrations MMPE: Mobile Multi-Phase Extraction NAPL: Non-Aqueous Phase Liquid, “Free Product” NCDEQ: North Carolina Department of Environmental Quality NCDOT: North Carolina Department of Transportation NFA: Notice of No Further Action NORR: Notice of Regulatory Requirements NOV: Notice of Violation NPDES: National Pollutant Discharge Elimination System NRP: Notice of Residual Petroleum O&M: Operation and Maintenance PAHs: Polynuclear Aromatic Hydrocarbons PCA: Pre-Construction Assessment RAL: Regulatory Action Level RUL: Regular Unleaded SCLs: Soil Cleanup Level SPCC: Spill Prevention Control and Countermeasures SVE: Soil Vapor Extraction SVOCs: Semi-Volatile Organic Compounds SWAP: Source Water Assessment and Protection SWPPP: Stormwater Pollution Prevention Plan TCLP: Toxicity Characteristic Leaching Procedure (EPA Method SW-846 1311) TOC: Top of Casing TPH: Total Petroleum Hydrocarbons USGS: United States Geological Survey UST: Underground Storage Tank UVF: Ultraviolet Fluorescence VOCs: Volatile Organic Compounds VPH: Volatile Petroleum Hydrocarbons ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 TABLE OF CONTENTS EXECUTIVE SUMMARY ....................................................................................................................... i SITE INFORMATION ........................................................................................................................... iii ACRONYMS ....................................................................................................................................... iv 1. RISK CHARACTERIZATION .....................................................................................................1 2. RECEPTOR INFORMATION .....................................................................................................4 3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................5 4. SITE INVESTIGATION .............................................................................................................6 5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................8 6. LIMITATIONS ........................................................................................................................9 FIGURES Figure 1: Site Location Map Figure 2A: Site Vicinity Map Figure 2B: Zoning Map Figure 3: Site Map Figure 4: Water Table Surface Map Figure 5: Soil Quality Map Figure 6: Ground Water Quality Map TABLES Table 1: UST Owner/Operator Information Table 2: UST System Information Table 3: Land Use Information Table 4: Receptor Information Table 5: Adjacent Property Owner Information Table 6: Well Construction and Gauging Information Table 7: Summary of Soil Sample Analytical Results Table 8: Summary of Ground Water Sample Analytical Results APPENDICES Appendix A: Water Use Questionnaires Appendix B: Lincoln County Property Cards Appendix C: Well Permit, Well Construction Records and Subsurface Logs Appendix D: State Correspondence Appendix E: Laboratory Analytical Reports ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 1 1. RISK CHARACTERIZATION Limited Site Assessment Risk Classification and Land Use Form Part I – Groundwater/Surface Water/Vapor Impacts High Risk 1. Has the release contaminated any water supply well including any well used for non-drinking purposes? NO 2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release? YES Eleven potable water supply wells are located within 1,000 feet of the source area. A Site Vicinity Map is included as Figure 2A. 3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water, filling swimming pools) located within 250 feet of the source area of the release? YES Three water supply wells (WSW-1, WSW-11, and WSW-12) are located within 250 feet of the source area. 4. Does ground water within 500 feet of the source area of the release have the potential for future use (there is no other source of water supply other than the groundwater)? NO Public water is available along Startown Road but is not available along Clarks Creek Road or Carlos Road. 5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined space or pose any other serious threat to public health, public safety or the environment? NO 6. Are there any other factors that would cause the release to pose an imminent danger to public health, public safety, or the environment? NO If YES, explain: Intermediate Risk 7. Is a surface water body located within 500 feet of the source area of the release? NO If YES, does the maximum groundwater contaminant concentration exceed the surface water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? N/A 8. Is the source area of the release located within an approved or planned wellhead protection area as defined in 42 USC 300h-7(e)? NO ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 2 9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled “Geology of North Carolina” published by the Department in 1985? NO 10. If YES, is the source area of the release located in an area in which there is recharge to an unconfined or semi-confined deeper aquifer that is being used or may be used as a source of drinking water? N/A If YES, describe. 11. Do the levels of ground water contamination for any contaminant exceed the gross contamination levels established by the Department? NO All of the reported concentrations were below the GCLs. Part II - Land Use Property Containing Source Area of Release The questions below pertain to the property containing the source area of the release. 1. Does the property contain one or more primary or secondary residences (permanent or temporary)? NO Explain: The subject property is an active convenience store and petroleum retail facility. 2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly? NO Explain: The subject property is an active convenience store and petroleum retail facility. 3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped? YES Explain: The subject property is an active convenience store and petroleum retail facility. 4. Do children visit the property? YES Explain: The site is currently a convenience store and children would likely visit the property. 5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)? NO Explain: The property is easily accessible to pedestrian and vehicular traffic. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 3 6. Do pavement, buildings, or other structures cap the contaminated soil? YES Explain: The site is currently covered with concrete, asphalt, and grass. If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain capped in the foreseeable future? The site is expected to remain in operation as an active convenience store and petroleum retail facility for the foreseeable future. 7. What is the zoning status of the property? According to the Lincoln County Zoning Map, the site is zoned B-N (Neighborhood Business). 8. Is the use of the property likely to change in the next 20 years? NO Explain: The subject property is currently an active convenience store and petroleum retail facility and likely remain a convenience store for the foreseeable future. Property Surrounding Source Area of Release The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property containing source area of the release): 9. What is the distance from the source area of the release to the nearest primary or secondary residence (permanent or temporary)? The closest primary residence is 2065 Startown Road located approximately 145 feet west- southwest of the UST basin. 10. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly? No places of public assembly are located within 1,500 feet of the source area at the site. 11. What is the zoning status of properties in the surrounding area? According to the Lincoln County Official Zoning Map, the surrounding areas are zoned Residential (R-25, R-S, R-SF, R-T and PRD). 12. Briefly characterize the use and activities of the land in the surrounding area. The area surrounding the site is residential. Land use information is included in Table 3. A zoning map is included as Figure 2B. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 4 2. RECEPTOR INFORMATION 1. Water Supply Wells: A receptor survey was conducted on April 26, 2023. Nineteen water supply wells were identified within a 1,500-foot radius of the site, of which eleven (WSW-1 through WSW-5, WSW-9, and WSW-11 through WSW-15) are potable and located within 1,000 feet of the source area. Three water supply wells (WSW-1, WSW-11, and WSW-12) are located within a 250-foot radius of the site. Receptor information is provided in Table 4. Returned water use questionnaires are included as Appendix A. 2. Public Water Supplies: Are public water supplies available within 1,500 feet of the source area of the release? YES If yes, where is the location of the nearest public water lines and the source(s) of the public water supply. Explain: Municipal water is available to the site and along Startown Road but is not available along Clarks Creek Road or Carlos Road. 3. Surface Water: Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the source area of the release. This information must be shown on the USGS topographic map. No surface water bodies were identified within a 500-foot radius of the site. An unnamed stream and a pond are located approximately 1,020 feet southeast and 1,280 feet west of the site, respectively. 4. Wellhead Protection Areas: Identify all planned or approved wellhead protection areas in the vicinity of the source area. This information must be shown on the USGS topographic map. Wellhead protection areas are defined in 42 USC 300h-7(e). On July 12, 2023, GRI personnel accessed the NCDEQ SWAP Program’s website to identify wellhead protection areas in the vicinity of the subject site. The site is not located within a wellhead protection area. 5. Deep Aquifers in the Coastal Plain Physiographic Region: The site is not located in the Coastal Plain Physiographic Region. 6. Subsurface Structures: A house with a basement was observed at 814 Clarks Creek Road. The water main and other underground utilities run along Startown Road, and several underground utility lines were observed on the property. 7. Property Owners and Occupants: The names and addresses of the owners of properties adjacent to the site are presented in Table 5. Property boundaries are shown on Figure 2A. Property cards for the adjacent property owners ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 5 are attached as Appendix B. 3. SITE GEOLOGY AND HYDROGEOLOGY According to the 1985 Geologic Map of North Carolina, the site is located in the Inner Piedmont Belt. The bedrock is generally described as an amphibolite and biotite gneiss interlayered with minor layers and lenses of hornblende gneiss, metagabbro, mica schist, and granite. The soil samples collected during well installation activities were red to brown silts and fine sands. The depth to ground water during the July 5, 2023 gauging event ranged from 25.26 to 28.15 feet below the top of well casing. A copy of the well permit, well construction records and subsurface logs are included as Appendix C. A Site Map is included as Figure 3. Well construction and gauging information is included in Table 6. Photographs of the newly installed monitoring wells are shown below: ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 6 4. SITE INVESTIGATION On January 4, 2023, a site check was conducted at the subject site due to a non-passing spill bucket for the 10,000-gallon RUL gasoline UST. The concentration of GRO exceeded the RAL; therefore, an LSA was required. One Type II monitoring well (MW-1) was installed at the UST basin by a North Carolina licensed well contractor on April 26, 2023 to assess the identified release at the site. MW-1 was installed to a total depth of 35 feet BGS with a 15-foot screened interval set to bracket the water table at the time of installation. Based on the ground water contaminant concentrations in the ground water sample collected from MW- 1, the presence of water supply wells within a 250-foot radius of the site, and potable water supply wells within a 1,000-foot radius of the site, three additional Type II monitoring wells were required to be installed at the site in order to determine the ground water flow direction. Monitoring wells MW-2 through MW-4 were installed at the site on July 5, 2023 to a total depth of 35 feet BGS each with a screened interval of 15 feet. A copy of the NCDEQ agreement to proceed to a High Risk LSA is included in Appendix D. Monitoring wells MW-1 through MW-4 were gauged on July 5, 2023. The depth to ground water ranged from 25.26 to 28.15 feet below TOC. The ground water elevation ranged from 73.54 to 76.36 during the July 2023 ground water gauging event. Ground water flow was generally towards the southeast with a horizontal gradient of approximately 0.03 feet per foot. A Water Table Surface Map is included as Figure 4. Gauging data from the July 2023 gauging event is included in Table 6. A summary of the current gauging data is shown below: Well ID Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (ft.) Groundwater Elevation (ft.) MW-1 20 - 35 35 100.00 25.79 74.21 MW-2 20 - 35 35 102.49 26.13 76.36 MW-3 20 - 35 35 98.80 25.26 73.54 MW-4 20 - 35 35 102.50 28.15 74.35 1. Soil Sampling: Soil sample (CS-2) was collected on January 4, 2023 during Site Check activities and submitted for laboratory analysis of GRO by EPA Method 8015D. The concentration of GRO reported in the soil samples collected from CS-2 exceeded the RAL. No free product was noted at the site. On April 26, 2023, four soil samples (MW-1-5’, MW-1-10’, MW-1-15’, and MW-1-20’) were collected at 5-foot intervals during the installation of monitoring well MW-1. The soil samples were submitted for analysis of VPH by the MADEP Method. Soil samples MW-1-5’ and MW-1-20’ were also submitted for analysis of VOCs by EPA Method 8260B. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 7 All of the reported contaminant concentrations were below the soil-to-water MCCs. A Soil Quality Map has been included as Figure 5. A summary of the soil sample analytical results is presented in Table 7. A copy of the laboratory analytical report from the April 2023 soil sampling event has been included in Appendix E. A copy of the current soil sampling data collected during the LSA activities is shown below: Sa m p l e I D Sa m p l e D e p t h (f t - B G S ) Be n z e n e To l u e n e Et h y l b e n z e n e To t a l X y l e n e s MT B E Na p h t h a l e n e Soil to Water MCC (mg/kg) 0.0072 5.4 8 6 0.085 0.2 Residential SCLs (mg/kg) 12 1,250 60.3 3,120 156 5.5 MW-1-5' 5 <0.0007 <0.0008 <0.0007 <0.0006 0.0009 J <0.001 MW-1-10' 10 NR NR NR NR NR NR MW-1-15' 15 NR NR NR NR NR NR MW-1-20' 20 <0.0008 0.0009 J <0.0008 0.005 J 0.002 J <0.001 2. Ground Water Sampling: On April 26, 2023, MW-1 was gauged, purged, and sampled in accordance with NCDEQ guidelines. The ground water sample was submitted for analysis of VOCs by EPA Method 6200B, EDB by EPA Method 504.1, total lead by EPA Method 6010, and VPH by the MADEP Method. The concentrations of benzene, bromodichloromethane, lead, and C9-C10 aromatics reported in the ground water sample collected from MW-1 exceeded the MACs. Please note that bromodichloromethane is not a petroleum constituent. All of the reported contaminant concentrations were below the GCLs. On July 5, 2023, monitoring wells MW-2 through MW-4 were gauged, purged, and sampled in accordance with NCDEQ guidelines. The ground water samples were submitted for analysis of VOCs, EDB, total lead and VPH. The concentrations of benzene, toluene, xylenes, naphthalene, TAA, TBA, 1,2,4-trimethylbenzene, lead, C5-C8 aliphatics, C9-C12 aliphatics and/or C9-C10 aromatics reported in the ground water samples collected from MW-2, MW-3, and MW-4. All of the reported concentrations were below the GCLs. No free product was observed at the site. A Ground Water Quality Map is included as Figure 6. A summary of the ground water analytical data is included in Table 8. Copies of the laboratory analytical reports are included in Appendix E. A summary of the current ground water sampling data is shown below: Contaminant of Concern  Be n z e n e To l u e n e Et h y l b e n z e n e Xy l e n e s MT B E Na p h t h a l e n e Well ID MAC (µg/l) 1 600 600 500 20 6 GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000 MW-1 38.7 135 41.6 377 0.969 J <0.470 ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 8 Contaminant of Concern  Be n z e n e To l u e n e Et h y l b e n z e n e Xy l e n e s MT B E Na p h t h a l e n e Well ID MAC (µg/l) 1 600 600 500 20 6 GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000 MW-2 <0.180 <0.220 <0.170 0.674 J <0.140 <0.470 MW-3 325 788 310 3,970 17.6 35.2 MW-4 0.451 J 1.84 0.765 6.09 <0.140 <0.470 3. Quality Control: The soil and ground water samples were immediately placed in laboratory-supplied containers after collection, which were then placed in iced coolers. New disposable bailers were used to sample the monitoring well and new nitrile gloves were worn during soil and ground water sampling. Samples were logged using proper chain-of-custody procedures. The samples were transported to a North Carolina certified laboratory for analysis. A laboratory supplied trip blank was included in the sample cooler. No detectable concentrations of requested method constituents were reported in the trip blank. 5. CONCLUSIONS AND RECOMMENDATIONS  The site is an active convenience store and petroleum retail facility. Land use in the area consists of residential properties.  A receptor survey was conducted on April 26, 2023. Nineteen water supply wells were identified within a 1,500-foot radius of the site, of which eleven are potable and located within 1,000 feet of the source area. Three of those water supply wells were identified within a 250-foot radius of the site. Public water is available along Startown Road but is not available along Clarks Creek Road or Carlos Road.  No surface water bodies were identified within a 500-foot radius of the site.  On April 26, 2023, one Type II monitoring well was installed at the UST basin. Soil samples were collected at 5-foot intervals during the installation of MW-1. All of the reported contaminant concentrations were below the soil-to-water MCCs.  On April 26, 2023, a ground water sample was collected from MW-1. The concentrations of benzene, bromodichloromethane, lead, and C9-C10 aromatics reported in the ground water sample collected from MW-1 exceeded the MACs. Please note that bromodichloromethane is not a petroleum constituent.  On July 5, 2023, three additional Type II monitoring wells were installed at the site in order to determine the ground water flow direction. A ground water sample was collected from each well following installation. The concentrations of benzene, toluene, xylenes, naphthalene, TAA, TBA, 1,2,4-trimethylbenzene, lead, C5-C8 aliphatics, C9-C12 aliphatics and/or C9-C10 aromatics reported in the ground water samples collected from MW-2, MW-3, and MW-4 exceeded the ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. High-Risk Limited Site Assessment Report Prepared on: July 31, 2023 Handy Corner Project Manager: Joanna Alley, P.E. GRI Project No. 6389 9 MACs. All of the reported concentrations were below the GCLs. No free product was observed at the site.  Based on the presence of water supply wells within 250 feet of the site, the presence of potable water supply wells within 1,000 feet of the site, and the reported contaminant concentrations exceeding the MACs, the site risk should be classified as high and a CSA should be conducted at the site. Based on the relatively limited contamination at the site, it is recommended to resample all wells prior to conducting the CSA to confirm the results of the April and July 2023 sampling events. The water supply wells located within 250 feet of the site should also be sampled. 6. LIMITATIONS This report has been prepared for the exclusive use of Nisbet Oil Company for specific application to the referenced site in Lincoln County, North Carolina. The assessment was conducted based on the scope of work and level of effort specified by NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of geology and hydrogeology practices in the State of North Carolina, available information and our professional judgment. No other warranty is expressed or implied. The data that are presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from these data. FIGURES SITE LOCATION Figure 1 Site Location Map Handy Corner 2076 Startown Road Lincolnton, North Carolina Lincoln County Incident No. 48992 GRI Project No. 6389500 M 2000 FT Date: 05/03/2023 Location: 35.512600° N -81.262114° W D a d TABLES UST ID Number 1 - 5 Facility ID Number Owner or Operator? Owner UST ID Number 1 - 5 Facility ID Number Owner or Operator? Owner UST ID Number 1 - 5 Facility ID Number Owner or Operator? Owner Address Telephone Number Unknown Unknown 0-014377 Name of Owner or Operator Dates of Ownership / Operation Unknown 6/6/1979 - 6/6/1989 0-014377 TABLE 1 UST OWNER/OPERATOR INFORMATION HANDY CORNER (INCIDENT NO. 48992) 1818 Baxter Street, Charlotte NC 28235 704-332-7755 Name of Owner or Operator Dates of Ownership / Operation Nisbet Oil Company 7/1/2005 - Present Address Telephone Number Address Telephone Number 1404 E. Main Street, Lincolnton, NC 28092 704-735-2508 0-014377 Name of Owner or Operator Dates of Ownership / Operation Rhodes & Beal Oil Co. 6/6/1989 - 7/1/2005 Page 1 of 1 Date: 07/11/23 Was Release Associated with UST System? (Yes / No) 1 Gasoline Gasoline 10,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current Yes 2 Gasoline Gasoline 6,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current Yes 3 Gasoline Gasoline 6,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current Yes 4 Diesel Diesel 10,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current No 5 Diesel Diesel 2,000 6/6/1979 Single Wall Steel Unknown Single Wall FRP* Current No Notes: *Piping material information was provided in the UST-10B Form TABLE 2 UST SYSTEM INFORMATION HANDY CORNER (INCIDENT NO. 48992) UST ID No. Current or Most Recent Contents Previous Contents Capacity (gallons) Date Installed Construction Details Tank Dimensions Description of Associated Product Piping and Pumps Status of UST Facility ID #: 0-014377 Page 1 of 1 Date: 07/11/23 Facility ID # : 00-0-0000014377 Map ID No. Land Use Feature Zoning Description Address Distance from Source Area (feet) n/a B-N Neighborhood Business N/A N/A n/a R-S Residential N/A N/A n/a R-SF Residential Single- Family N/A N/A n/a R-T Transitional Residential N/A N/A n/a R-25 Residential N/A N/A n/a R-O Residential N/A N/A n/a PRD Planned Residential District (City Zoning)N/A N/A Note: • Properties are keyed to Figure 2B. TABLE 3 LAND USE INFORMATION HANDY CORNER (INCIDENT NO. 48992) Page 1 of 1 Facility ID # : 0-014377 Well ID. Tax Parcel I.D. Well Owner Mailing Address Well Address Well Status (Active/In-Active) Well Use (Potable / Non- Potable etc.) Municipal Water Available Yes/No Connected to Municipal Water Yes/No Distance from source area of release (ft.) WSW-1 59078 Bradley C. and Jennifer S. Keneda 2098 Startown Rd, Lincolnton, NC 28092 2098 Startown Rd, Lincolnton, NC 28092 Active Potable Yes No ~240 WSW-2 59077 Sandi E. Alvarado 2110 Startown Rd, Lincolnton, NC 28092 2110 Startown Rd, Lincolnton, NC 28092 Active Potable Yes No ~485 WSW-3 59076 Ruth B. Johnson Estate of the High Judy Johnson As Executrix 1643 Startown Rd, Lincolnton, NC 28092 2126 Startown Rd, Lincolnton, NC 28092 Active Potable Yes No ~610 WSW-4 59075 Brett J. and Connie G. Silvia Life Estate 2138 Startown Rd, Lincolnton, NC 28092 2138 Startown Rd, Lincolnton, NC 28092 Active Potable Yes No ~765 WSW-5 73256 James K. Payseur (Delores)2146 Startown Rd, Lincolnton, NC 28092 2146 Startown Rd*, Lincolnton, NC 28092 Active Potable Yes No ~845 WSW-6 19155 John D. and Dawn M. Harrison 1146 Carlos Rd, Lincolnton, NC 28092 1146 Carlos Rd, Lincolnton, NC 28092 Active Potable No No ~1,310 WSW-7 19527 Jaden and Chelsea Angle 1132 Carlos Rd, Lincolnton, NC 28092 1132 Carlos Rd, Lincolnton, NC 28092 Active Potable No No ~1,410 WSW-8 19544 Stoney G. and Jennifer R. Haynes 1127 Carlos Rd, Lincolnton, NC 28092 1127 Carlos Rd, Lincolnton, NC 28092 Active Potable No No ~1,190 WSW-9 19057 Michael T. and Bethanna W. Macomson 2121 Startown Rd, Lincolnton, NC 28092 2133 Startown Rd, Lincolnton, NC 28092 Active Potable Yes No ~730 WSW-10 22826 Steven H. Bennett 3594 Maple Ridge Rd, Maiden, NC 28650 2151 Startown Rd, Lincolnton, NC 28092 Active Non-Potable Yes Yes ~860 WSW-11 2085 Startown Rd, Lincolnton, NC 28092 Active Potable Yes No ~240 WSW-12 2065 Startown Rd, Lincolnton, NC 28092 Active Potable Yes No ~220 WSW-13 18052 Luther Barker 862 Clarks Creek Rd, Lincolnton, NC 28092 862 Clarks Creek Rd, Lincolnton, NC 28092 Active Potable No No ~535 WSW-14 16614 Donald and Kay Lawing 852 Clarks Creek Rd, Lincolnton, NC 28092 852 Clarks Creek Rd, Lincolnton, NC 28092 Active Potable No No ~460 WSW-15 16707 J. Stephen High, Inc.1620 Startown Rd, Lincolnton, NC 28092 814 Clarks Creek Rd, Lincolnton, NC 28092 Active Potable No No ~900 WSW-16 19541 Heirs of John T. and Amy M. Carter 792 Clarks Creek Rd, Lincolnton, NC 28092 792 Clarks Creek Rd, Lincolnton, NC 28092 Active Potable No No ~1,015 WSW-17 16138 Glenda M. Rose 760 Clarks Creek Rd, Lincolnton, NC 28092 760 Clarks Creek Rd, Lincolnton, NC 28092 Active Potable No No ~1,365 WSW-18 19266 Melanie B. Givens 780 Clarks Creek Rd, Lincolnton, NC 28092 780 Clarks Creek Rd, Lincolnton, NC 28092 Active Potable No No ~1,190 WSW-19 19238 Robert L. and Deborah Goins 790 Clarks Creek Rd, Lincolnton, NC 28092 790 Clarks Creek Rd, Lincolnton, NC 28092 Active Potable No No ~1,020 William C. and Dianne P. Painter Life Estate16181 2085 Startown Rd, Lincolnton, NC 28092 Well Depth: 500 feet Well Depth: 50 feet Well Depth: 90 feet Well Depth: 40 feet TABLE 4 RECEPTOR INFORMATION HANDY CORNER (INCIDENT NO. 48992) Date: 07/26/23 Well Construction Details (Depth, Screened Interval, Type of Well, ect.) Page 1 of 2 Receptor ID Latitude/ Longitude of Any Significant Points Up or Down- Gradient Distance from the source area of release (ft.) n/a n/a Up ~1,280 n/a n/a Down ~1,020 Notes: • Receptors are shown on Figure 2A. • n/a: not applicable. • *: WSW-5 is located on an adjacent parcel to 2146 Startown Road that does not have an address; however, WSW-5 services 2146 Startown Road. Pond West of the site Unknown Unknown Unnamed Stream Southeast of the site Unknown Unknown Description Location Contact/Phone Number Usage Page 2 of 2 Date: 05/05/23 Facility ID #: 0-014377 Tax Parcel I.D. Property Owner Name Property Owner Address 52985 (site) Rhodes & Beal Oil Co., Inc.1404 E Main St. Lincolnton, NC 28092 90391 Nisbet Oil Company 1818 Baxter St. Charlotte NC 28204 18052 Luther Barker 862 Clarks Creek Rd. Lincolnton, NC 28092 16614 Donald and Kay Lawing 852 Clark Creek Rd. Lincolnton, NC 28092 15415 BBC Clark Creek, LLC 7224 Jameson Way Stanley, NC 28164 16181 William C. and Dianne P. Painter Life Estate 2085 Startown Rd. Lincolnton, NC 28092 Note: • Properties are keyed to Figure 2A. TABLE 5 ADJACENT PROPERTY OWNER INFORMATION HANDY CORNER (INCIDENT NO. 48992) Page 1 of 1 APPENDICES APPENDIX A Water Use Questionnaires APPENDIX B Lincoln County Property Cards 7/12/23, 8:36 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=52985 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 52985 Owner RHODES & BEAL OIL CO INC Map 3624 Mailing DBA HANDY CORNER 1404 E MAIN ST Account 0061681 Address LINCOLNTON, NC 28092 Deed 854 227 Last Transaction Date 01/04/1994 Sale Price $105,000 Plat Subdivision Lot Land Value $116,090 Improvement Value $199,222 Total Value $315,312 Previous Parcel -----All values for Tax Year 2023 ----- Description LAND & SERVICE STA.Deed Acres 2.284 Address 2076 STARTOWN RD Tax Acres 1.888 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement CONVIENCE STORE Value $140,924 Main Sq Feet 2700 Stories 1 Year Built 1978 Zoning District Calc Acres B-N 1.89 Voting Precinct Calc Acres ST36 1.89 Watershed 1.89 Sewer District 1.89 Census County Tract Block 109 070800 3039 1.4 109 070800 3040 0.49 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.89 7/12/23, 8:36 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=90391 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 90391 Owner NISBET OIL COMPANY Map 3624 Mailing 1818 BAXTER STREET Account 0235711 Address CHARLOTTE, NC 28204 Deed 2274 179 Last Transaction Date 10/14/2011 Sale Price $12,000 Plat G 74 Subdivision LANDON HEIGHTS Lot PT 5 Land Value $2,448 Improvement Value $0 Total Value $2,448 Previous Parcel 18052 -----All values for Tax Year 2023 ----- Description PT5 LANDON HEIGHTS Deed Acres 0.39 Address STARTOWN RD Tax Acres 0.34 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement Value Main Sq Feet Stories Year Built Zoning District Calc Acres R-SF 0.34 Voting Precinct Calc Acres ST36 0.34 Watershed 0.34 Sewer District 0.34 Census County Tract Block 109 070800 3040 0.34 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 0.34 7/12/23, 8:37 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=18052 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 18052 Owner BARKER LUTHER Map 3624 Mailing 862 CLARKS CREEK RD Account 0220551 Address LINCOLNTON, NC 28092-7342 Deed 3051 899 Last Transaction Date 06/15/2021 Sale Price $180,000 Plat G 74 Subdivision LANDON HEIGHTS Lot PT 5 & PT 8 Land Value $29,802 Improvement Value $183,773 Total Value $213,575 Previous Parcel -----All values for Tax Year 2023 ----- Description PT#5 & PT#8 LANDON HGHTS Deed Acres 1.959 Address 862 CLARKS CREEK RD Tax Acres 1.982 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement CONVENTIONAL (PRE WWII)Value $172,998 Main Sq Feet 1887 Stories 1 Year Built 1906 Zoning District Calc Acres R-SF 1.98 Voting Precinct Calc Acres ST36 1.98 Watershed 1.98 Sewer District 1.98 Census County Tract Block 109 070800 3039 1.71 109 070800 3040 0.27 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.98 7/12/23, 8:35 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16614 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for landconveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 16614 Owner LAWING DONALDLAWING KAY Map 3624 Mailing 852 CLARK CREEK RD Account 09941 Address LINCOLNTON, NC 280920000 Deed 643 575 Last Transaction Date 01/01/1992 Sale Price $0 Plat Subdivision Lot Land Value $33,924 Improvement Value $291,450 Total Value $325,374 Previous Parcel -----All values for Tax Year 2023 ----- Description REEP - RD 1282 Deed Acres 1.73 Address 852 CLARKS CREEK RD Tax Acres 1.545 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement CAPE COD Value $277,639 Main Sq Feet 2080 Stories 1 Year Built 1986 Zoning District Calc Acres R-SF 1.54 Voting Precinct Calc Acres ST36 1.54 Watershed 1.54 Sewer District 1.54 Census County Tract Block 109 070800 3039 1.54 109 070800 3040 0.01 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.54 7/12/23, 8:37 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=15415 1/2 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 15415 Owner BBC CLARK CREEK LLC Map 3624 Mailing 7224 JAMESON WAY Account 0291545 Address STANLEY, NC 28164 Deed 3180 688 Last Transaction Date 07/14/2022 Sale Price $0 Plat Subdivision Lot Land Value $724,736 Improvement Value $0 Total Value $724,736 Previous Parcel -----All values for Tax Year 2023 ----- Description STARTOWN RD INTERSECTION Deed Acres 86.906 Address CLARKS CREEK RD Tax Acres 84.654 Township LINCOLNTON Tax/Fire District LINCOLNTON Main Improvement Value Main Sq Feet Stories Year Built Zoning District Calc Acres PRD 84.65 Voting Precinct Calc Acres ST36 84.65 Watershed 84.65 Sewer District 84.65 Census County Tract Block 109 070800 4007 81.92 109 070800 4008 2.73 Flood Zone Description Panel X NO FLOOD HAZARD 3710363400 4.93 X NO FLOOD HAZARD 3710362400 67.68 7/12/23, 8:37 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=15415 2/2 SHAX 3710363400 0.76 AEFW FLOODWAY AREA - 100 YEAR FLOOD HAZARD 3710362400 0.82 SHAX 3710362400 0.57 AE SPECIAL FLOOD HAZARD AREA BASE ELEVATIONDETERMINED - 100 YEAR 3710362400 3.33 AE SPECIAL FLOOD HAZARD AREA BASE ELEVATIONDETERMINED - 100 YEAR 3710363400 3.05 AEFW FLOODWAY AREA - 100 YEAR FLOOD HAZARD 3710363400 3.51 7/12/23, 8:37 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16181 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. 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The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 16181 Owner PAINTER WILLIAM CLINTON LIFESTPAINTER DIANNE P LIFE ESTATE Map 3624 Mailing 2085 STARTOWN ROAD Account 0266573 Address LINCOLNTON, NC 28092 Deed 2729 100 Last Transaction Date 03/13/2018 Sale Price $0 Plat Subdivision Lot Land Value $431,617 Improvement Value $305,247 Total Value $736,864 Previous Parcel -----All values for Tax Year 2023 ----- Description SMITH LAND - RD 1005 Deed Acres 0 Address 2085 STARTOWN RD Tax Acres 30.752 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $133,245 Main Sq Feet 1200 Stories 1 Year Built 1948 Zoning District Calc Acres R-25 27.48 R-SF 3.27 Voting Precinct Calc Acres ST36 30.75 Watershed 25.97 4.78 Sewer District 30.75 Census County Tract Block 109 070800 4012 30.75 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 30.75 7/12/23, 8:38 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=59078 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. 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The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 59078 Owner KENEDA BRADLEY CHRISTOPHERKENEDA JENNIFER STATON Map 3624 Mailing 2098 STARTOWN ROAD Account 0108314 Address LINCOLNTON, NC 28092-9698 Deed 910 61 Last Transaction Date 07/27/1995 Sale Price $85,500 Plat G 74 Subdivision LANDON HEIGHTS Lot 4 Land Value $33,836 Improvement Value $220,773 Total Value $254,609 Previous Parcel -----All values for Tax Year 2023 ----- Description #4 LANDON HEIGHTS Deed Acres 1.047 Address 2098 STARTOWN RD Tax Acres 0.966 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $206,121 Main Sq Feet 1400 Stories 1 Year Built 1995 Zoning District Calc Acres R-SF 0.97 Voting Precinct Calc Acres ST36 0.97 Watershed 0.04 0.93 Sewer District 0.97 Census County Tract Block 109 070800 3040 0.97 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 0.97 7/12/23, 8:38 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=59077 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 59077 Owner SANDI ELADIO ALVARADO Map 3624 Mailing 2110 STARTOWN ROAD Account 0273282 Address LINCOLNTON, NC 28092 Deed 2827 200 Last Transaction Date 06/27/2019 Sale Price $210,000 Plat G 74 Subdivision LANDON HEIGHTS Lot 3 Land Value $34,381 Improvement Value $232,684 Total Value $267,065 Previous Parcel -----All values for Tax Year 2023 ----- Description #3 LANDON HEIGHTS Deed Acres 1.156 Address 2110 STARTOWN RD Tax Acres 1.053 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $226,299 Main Sq Feet 1570 Stories 1 Year Built 1995 Zoning District Calc Acres R-SF 1.05 Voting Precinct Calc Acres ST36 1.05 Watershed 0.35 0.7 Sewer District 1.05 Census County Tract Block 109 070800 3040 1.05 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.05 7/12/23, 8:39 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=59076 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 59076 Owner JOHNSON RUTH B ESTATE OF THEHIGH JUDY JOHNSON AS EXECUTRIX Map 3624 Mailing 1643 STARTOWN RD Account 0277493 Address LINCOLNTON, NC 28092 Deed 2907 540 Last Transaction Date 05/12/2020 Sale Price $173,500 Plat G 74 Subdivision LANDON HEIGHTS Lot 2 Land Value $34,115 Improvement Value $243,847 Total Value $277,962 Previous Parcel -----All values for Tax Year 2023 ----- Description #2 LANDON HEIGHTS Deed Acres 1.128 Address 2126 STARTOWN RD Tax Acres 1.016 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $243,847 Main Sq Feet 1680 Stories 1 Year Built 1994 Zoning District Calc Acres R-SF 1.02 Voting Precinct Calc Acres ST36 1.02 Watershed 0.82 0.2 Sewer District 1.02 Census County Tract Block 109 070800 3039 0.22 109 070800 3040 0.8 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.02 7/12/23, 8:39 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=59075 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 59075 Owner SILVA BRETT J LIFE ESTATESILVA CONNIE G LIFE ESTATE Map 3624 Mailing 2138 STARTOWN ROAD Account 0268098 Address LINCOLNTON, NC 28092 Deed 2753 736 Last Transaction Date 06/29/2018 Sale Price $0 Plat G 74 Subdivision LANDON HEIGHTS Lot 1 Land Value $33,928 Improvement Value $277,771 Total Value $311,699 Previous Parcel -----All values for Tax Year 2023 ----- Description #1 LANDON HEIGHTS Deed Acres 1.1 Address 2138 STARTOWN RD Tax Acres 0.985 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement CAPE COD Value $264,304 Main Sq Feet 2100 Stories 1.5 Year Built 1993 Zoning District Calc Acres R-SF 0.99 Voting Precinct Calc Acres ST36 0.99 Watershed 0.99 Sewer District 0.99 Census County Tract Block 109 070800 3039 0.99 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 0.99 7/12/23, 8:39 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=73256 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 73256 Owner PAYSEUR JAMES KEITH (DELORES) Map 3624 Mailing 2146 STARTOWN RD Account 11277 Address LINCOLNTON, NC 28092 Deed 1018 623 Last Transaction Date 12/04/1997 Sale Price $0 Plat G 74 Subdivision LANDON HEIGHTS Lot 7A Land Value $3,639 Improvement Value $0 Total Value $3,639 Previous Parcel 59080 -----All values for Tax Year 2023 ----- Description #7A LANDON HEIGHTS Deed Acres 0.682 Address CARLOS RD Tax Acres 0.674 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement Value Main Sq Feet Stories Year Built Zoning District Calc Acres R-SF 0.67 Voting Precinct Calc Acres ST36 0.67 Watershed 0.67 Sewer District 0.67 Census County Tract Block 109 070800 3039 0.67 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 0.67 7/12/23, 8:45 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19155 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 19155 Owner HARRISON JOHN DAVIDHARRISON DAWN M Map 3625 Mailing 1146 CARLOS RD Account 0130069 Address LINCOLNTON, NC 28092-9508 Deed 1053 76 Last Transaction Date 06/24/1998 Sale Price $129,500 Plat Subdivision LINCOLN PARK Lot PT LTS 76 84 85 Land Value $30,158 Improvement Value $352,031 Total Value $382,189 Previous Parcel -----All values for Tax Year 2023 ----- Description PT76 84 85 LIN PK Deed Acres 0 Address 1146 CARLOS RD Tax Acres 0.817 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement SPLIT LEVEL Value $337,568 Main Sq Feet 2385 Stories 1 Year Built 1972 Zoning District Calc Acres R-SF 0.82 Voting Precinct Calc Acres ST36 0.82 Watershed 0.68 0.14 Sewer District 0.82 Census County Tract Block 109 070800 3039 0.82 Flood Zone Description Panel X NO FLOOD HAZARD 3710362500 0.82 7/12/23, 8:45 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19527 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 19527 Owner ANGLE JADENANGLE CHELSEA Map 3625 Mailing 1132 CARLOS ROAD Account 0279225 Address LINCOLNTON, NC 28092 Deed 2925 708 Last Transaction Date 07/08/2020 Sale Price $290,000 Plat Subdivision LINCOLN PARK Lot PT 75 & 76 Land Value $28,000 Improvement Value $360,422 Total Value $388,422 Previous Parcel -----All values for Tax Year 2023 ----- Description LIN PK 75&76 STARTOW Deed Acres 0 Address 1132 CARLOS RD Tax Acres 0.713 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $230,008 Main Sq Feet 1624 Stories 1 Year Built 1972 Zoning District Calc Acres R-SF 0.71 Voting Precinct Calc Acres ST36 0.71 Watershed 0.17 0.55 Sewer District 0.71 Census County Tract Block 109 070800 3039 0.71 Flood Zone Description Panel X NO FLOOD HAZARD 3710362500 0.71 7/12/23, 8:44 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19544 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 19544 Owner HAYNES STONEY GHAYNES JENNIFER R Map 3625 Mailing 1127 CARLOS RD Account 0257691 Address LINCOLNTON, NC 28092 Deed 2567 863 Last Transaction Date 02/05/2016 Sale Price $235,000 Plat Subdivision Lot Land Value $91,925 Improvement Value $364,092 Total Value $456,017 Previous Parcel -----All values for Tax Year 2023 ----- Description CROWELL RD 1005 Deed Acres 5.958 Address 1127 CARLOS RD Tax Acres 5.513 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $353,759 Main Sq Feet 2335 Stories 1 Year Built 1967 Zoning District Calc Acres R-SF 5.51 Voting Precinct Calc Acres ST36 5.51 Watershed 5.08 0.43 Sewer District 5.51 Census County Tract Block 109 070800 3039 5.51 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.38 X NO FLOOD HAZARD 3710362500 4.13 7/12/23, 8:42 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19057 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 19057 Owner MACOMSON MICHAEL TALBOTTMACOMSON BETHANNA W Map 3624 Mailing 2121 STARTOWN RD Account 0127797 Address LINCOLNTON, NC 28092 Deed 1033 476 Last Transaction Date 03/13/1998 Sale Price $275,000 Plat Subdivision Lot Land Value $35,353 Improvement Value $317,984 Total Value $353,337 Previous Parcel -----All values for Tax Year 2023 ----- Description SMITH LAND & HOME RD 1005 Deed Acres 0 Address 2133 STARTOWN RD Tax Acres 1.188 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $315,716 Main Sq Feet 2624 Stories 1 Year Built 1968 Zoning District Calc Acres R-SF 1.19 Voting Precinct Calc Acres ST36 1.19 Watershed 1.19 Sewer District 1.19 Census County Tract Block 109 070800 4012 1.19 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.19 7/12/23, 8:42 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=22826 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 22826 Owner BENNETT STEVEN H Map 3624 Mailing 3594 MAPLE RIDGE LANE Account 0271978 Address MAIDEN, NC 28650 Deed 2803 794 Last Transaction Date 03/19/2019 Sale Price $26,000 Plat Subdivision Lot Land Value $33,256 Improvement Value $199,263 Total Value $232,519 Previous Parcel -----All values for Tax Year 2023 ----- Description HEEDICK LD RD 1005 Deed Acres 1 Address 2151 STARTOWN RD Tax Acres 0.845 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $198,163 Main Sq Feet 1458 Stories 1 Year Built 1953 Zoning District Calc Acres R-SF 0.85 Voting Precinct Calc Acres ST36 0.85 Watershed 0.85 Sewer District 0.85 Census County Tract Block 109 070800 4012 0.85 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 0.85 7/12/23, 8:40 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16181 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 16181 Owner PAINTER WILLIAM CLINTON LIFESTPAINTER DIANNE P LIFE ESTATE Map 3624 Mailing 2085 STARTOWN ROAD Account 0266573 Address LINCOLNTON, NC 28092 Deed 2729 100 Last Transaction Date 03/13/2018 Sale Price $0 Plat Subdivision Lot Land Value $431,617 Improvement Value $305,247 Total Value $736,864 Previous Parcel -----All values for Tax Year 2023 ----- Description SMITH LAND - RD 1005 Deed Acres 0 Address 2085 STARTOWN RD Tax Acres 30.752 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $133,245 Main Sq Feet 1200 Stories 1 Year Built 1948 Zoning District Calc Acres R-25 27.48 R-SF 3.27 Voting Precinct Calc Acres ST36 30.75 Watershed 25.97 4.78 Sewer District 30.75 Census County Tract Block 109 070800 4012 30.75 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 30.75 7/12/23, 8:37 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=18052 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 18052 Owner BARKER LUTHER Map 3624 Mailing 862 CLARKS CREEK RD Account 0220551 Address LINCOLNTON, NC 28092-7342 Deed 3051 899 Last Transaction Date 06/15/2021 Sale Price $180,000 Plat G 74 Subdivision LANDON HEIGHTS Lot PT 5 & PT 8 Land Value $29,802 Improvement Value $183,773 Total Value $213,575 Previous Parcel -----All values for Tax Year 2023 ----- Description PT#5 & PT#8 LANDON HGHTS Deed Acres 1.959 Address 862 CLARKS CREEK RD Tax Acres 1.982 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement CONVENTIONAL (PRE WWII)Value $172,998 Main Sq Feet 1887 Stories 1 Year Built 1906 Zoning District Calc Acres R-SF 1.98 Voting Precinct Calc Acres ST36 1.98 Watershed 1.98 Sewer District 1.98 Census County Tract Block 109 070800 3039 1.71 109 070800 3040 0.27 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.98 7/12/23, 8:35 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16614 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for landconveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 16614 Owner LAWING DONALDLAWING KAY Map 3624 Mailing 852 CLARK CREEK RD Account 09941 Address LINCOLNTON, NC 280920000 Deed 643 575 Last Transaction Date 01/01/1992 Sale Price $0 Plat Subdivision Lot Land Value $33,924 Improvement Value $291,450 Total Value $325,374 Previous Parcel -----All values for Tax Year 2023 ----- Description REEP - RD 1282 Deed Acres 1.73 Address 852 CLARKS CREEK RD Tax Acres 1.545 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement CAPE COD Value $277,639 Main Sq Feet 2080 Stories 1 Year Built 1986 Zoning District Calc Acres R-SF 1.54 Voting Precinct Calc Acres ST36 1.54 Watershed 1.54 Sewer District 1.54 Census County Tract Block 109 070800 3039 1.54 109 070800 3040 0.01 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.54 7/12/23, 8:42 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16707 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 16707 Owner J STEPHEN HIGH INC Map 3624 Mailing 1620 STARTOWN RD Account 0157151 Address LINCOLNTON, NC 28092-8041 Deed 2508 801 Last Transaction Date 07/14/2022 Sale Price $0 Plat Subdivision Lot Land Value $38,136 Improvement Value $186,926 Total Value $225,062 Previous Parcel -----All values for Tax Year 2023 ----- Description SMITH LD RD 1282 Deed Acres 2.75 Address 814 CLARKS CREEK RD Tax Acres 2.13 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $186,926 Main Sq Feet 1681 Stories 1 Year Built 1965 Zoning District Calc Acres R-SF 2.13 Voting Precinct Calc Acres ST36 2.13 Watershed 2.13 Sewer District 2.13 Census County Tract Block 109 070800 3039 2.13 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 2.13 7/12/23, 8:43 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19541 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 19541 Owner CARTER JOHN T HEIRS OFCARTER AMY M HEIRS OF AKA MORRISON AMY HEIRS OF Map 3624 Mailing 792 CLARKS CREEK Account 0295479 Address LINCOLNTON, NC 28092 Deed LC110 102 Last Transaction Date 02/18/2023 Sale Price $0 Plat Subdivision Lot Land Value $27,998 Improvement Value $136,742 Total Value $164,740 Previous Parcel -----All values for Tax Year 2023 ----- Description SMITH-REEP LD- HMSIT Deed Acres 0.6 Address 792 CLARKS CREEK RD Tax Acres 0.545 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement RANCH Value $136,467 Main Sq Feet 1446 Stories 1 Year Built 1966 Zoning District Calc Acres R-SF 0.55 Voting Precinct Calc Acres ST36 0.55 Watershed 0.55 Sewer District 0.55 Census County Tract Block 109 070800 3039 0.55 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 0.55 7/12/23, 8:44 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=16138 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 16138 Owner ROSE GLENDA MORGAN Map 3624 Mailing 760 CLARK CREEK RD Account 0089843 Address LINCOLNTON, NC 28092 Deed 18E 279 Last Transaction Date 04/24/2018 Sale Price $0 Plat Subdivision Lot Land Value $51,081 Improvement Value $106,089 Total Value $157,170 Previous Parcel -----All values for Tax Year 2023 ----- Description HOMESITE RD 1282 Deed Acres 3.86 Address 760 CLARKS CREEK RD Tax Acres 3.928 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement BUNGALOW Value $103,914 Main Sq Feet 1426 Stories 1 Year Built 1940 Zoning District Calc Acres R-SF 3.93 Voting Precinct Calc Acres ST36 3.93 Watershed 3.93 Sewer District 3.93 Census County Tract Block 109 070800 3039 3.93 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 3 X NO FLOOD HAZARD 3710362500 0.93 7/12/23, 8:43 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19266 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 19266 Owner GIVENS MELANIE BREWER Map 3624 Mailing 780 CLARK CREEK RD Account 0248454 Address LINCOLNTON, NC 28092-7341 Deed 2510 857 Last Transaction Date 07/14/2022 Sale Price $0 Plat Subdivision Lot Land Value $38,172 Improvement Value $91,737 Total Value $129,909 Previous Parcel -----All values for Tax Year 2023 ----- Description SMITH LD & D/W R1282 Deed Acres 0 Address 780 CLARKS CREEK RD Tax Acres 2.135 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement MANUFACTURED HOME Value $88,383 Main Sq Feet 1680 Stories 1 Year Built 1986 Zoning District Calc Acres R-SF 2.13 Voting Precinct Calc Acres ST36 2.13 Watershed 2.13 Sewer District 2.13 Census County Tract Block 109 070800 3039 2.13 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 2.1 X NO FLOOD HAZARD 3710362500 0.04 7/12/23, 8:43 AM Map with Parcel Information https://arcgisserver.lincolncounty.org/taxparcelviewer/PropertyReport.aspx?vacinity=false&akpar=19238 1/1 Lincoln County, NC Office of the Tax Administrator, GIS Mapping Division Lincoln County and its mapping contractors assume no legal responsibility forthe information contained on this map. This map is not to be used for land conveyance. The map is based on NC State Plane Coordinate System 1983 NAD.Date: 7/12/2023 Parcel ID 19238 Owner GOINS ROBERT LGOINS DEBORAH Map 3624 Mailing 790 CLARK CREEK RD Account 07094 Address LINCOLNTON, NC 280920000 Deed 2477 165 Last Transaction Date 07/14/2022 Sale Price $0 Plat Subdivision Lot Land Value $29,199 Improvement Value $88,806 Total Value $118,005 Previous Parcel -----All values for Tax Year 2023 ----- Description HOMESITE W/DW RD1282 Deed Acres 1.29 Address 790 CLARKS CREEK RD Tax Acres 1.216 Township LINCOLNTON Tax/Fire District NORTH 321 Main Improvement MANUFACTURED HOME Value $81,071 Main Sq Feet 1456 Stories 1 Year Built 1986 Zoning District Calc Acres R-SF 1.22 Voting Precinct Calc Acres ST36 1.22 Watershed 1.22 Sewer District 1.22 Census County Tract Block 109 070800 3039 1.22 Flood Zone Description Panel X NO FLOOD HAZARD 3710362400 1.22 APPENDIX C Well Permit, Well Construction Records, and Subsurface Logs North Carolina Department of Environmental Quality | Division of Water Resources Mooresville Regional Office | 601 East Center Avenue, Suite 301 | Mooresville, NC 28115 704.663.1699 March 27, 2023 Mr. Jim White (via email) Nisbet Oil Company 1818 Baxter Street Charlotte, NC 28204 RE: Monitoring Well Construction Permit Permit # WM0301269 2076 Startown Road, Lincolnton Lincoln County Dear Mr. White, In accordance with your completed application received on March 27, 2023, we are forwarding herewith Monitoring Well Construction Permit Numbered WM0301269 and issued for the construction of four (4) monitoring wells located near the subject site in Lincolnton, Lincoln County. This Permit will be effective for one year from the date of issuance and shall be subject to the conditions and limitations as specified therein. Should you have any questions, please contact Edward Watson at (704) 235-2199, or by email at edward.watson@ncdenr.gov. Sincerely, Andrew H. Pitner, P.G., Assistant Regional Supervisor Mooresville Regional Office Water Quality Regional Operations Section Division of Water Resources CC: WQROS, Central Office (via Laserfiche) Joanna Alley, Geological Resources, Inc. (via email) Geological Resources, Inc. (via email) NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws, Rules and Regulations. PERMISSION IS HEREBY GRANTED TO Nisbet Oil Company (Geological Resources, Inc. as Agent) FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of four (4) monitoring wells owned by Nisbet Oil Company, at the subject site located at 2076 Startown Road, in Lincolnton, Lincoln County. This Permit is issued in accordance with the application received on March 27, 2023, in conformity with specifications and supporting data, all of which are filed with the Department of Environmental Quality and are considered integral parts of this Permit. This Permit is for well construction only, and does not waive any provision or requirement of any other applicable law or regulation. Construction of any well under this Permit shall be in strict compliance with the North Carolina Well Construction Regulations and Standards (15A NCAC 02C .0100), and other State and Local Laws and regulations pertaining to well construction. If any requirements or limitations specified in this Permit are unacceptable, you have a right to an adjudicatory hearing upon written request within 30 days of receipt of this Permit. The request must be in the form of a written petition conforming to Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding. This Permit will be effective for one year from the date of its issuance and shall be subject to other specified conditions, limitations, or exceptions as follows: 1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these wells are being installed as part of an investigation for contamination from an underground storage tank or dry cleaner incident. 2. Issuance of this Permit does not supersede any other agreement, permit, or requirement issued by another agency. 3. The well(s) shall be located and constructed as shown on the attachments submitted as part of the Permit application. 4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC 02C .0108(o). 5. Well construction records (GW-1) for each well shall be submitted to the Division of Water Resources’ Information Processing Unit within 30 days of the well completion. 6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A NCAC 02C .0113 and a well abandonment record (GW-30) shall be submitted to the Division of Water Resources’ Information Processing Unit within 30 days of the well abandonment. 7. If the well penetrates any water-bearing zone that contains contaminated waters, the upper three feet of the well shall be grouted within one day after the casing is set or the well abandoned. 8. Temporary wells must be permanently abandoned or converted to a permanent well within seven days (168 hours) of completion of drilling the borehole. Permit issued the 27th day of March 2023 FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION _______________________________________________ Andrew H. Pitner, P.G., Assistant Regional Supervisor Division of Water Resources By Authority of the Environmental Management Commission Permit No. # WM0301269 Site Name:Date: Project Number:Log Completed By: Company:Drill Type: Driller:License Number: Boring ID:Depth: Diameter:Completion Details: PID Lab From To (ppm)Sample Description Color Moisture Odor Depth (ft)Lithology SITE INFORMATION DRILLING INFORMATION BORING INFORMATION Photo 1: Preclearing Photo 2: Completion Handy Corner 6389 4/26/23 Jase Bowers Geological Resources, Inc. Sam Bowers Solid Stem Auger 3220-A MW-1 6" 35' Well installed at completion 0 0.5 Asphalt 0.5 9.5 MW-1-5'Silt Red Dry 9.5 10 MW-1-10'Weathered rock 10 35 MW-1-15'Silt Brown Moist MW-1-20' Site Name:Date: Project Number:Log Completed By: Company:Drill Type: Driller:License Number: Boring ID:Top of Casing: Diameter:Depth to Water: From (ft)To (ft)From (ft)To (ft)Diameter (in) From (ft)To (ft)From (ft)To (ft)Diameter (in) From (ft)To (ft)From (ft)To (ft)Diameter (in) Sand Bentonite Grout Screen Casing SITE INFORMATION DRILLING INFORMATION WELL CONSTRUCTION INFORMATION DIAGRAM -MONITORING WELL Sand Bentonite Grout Screen Inner Casing Outer Casing Handy Corner 6389 4/26/23 Jase Bowers Geological Resources, Inc. Sam Bowers Solid Stem Auger 3220-A MW-1 6" 100.00 26.23 18 35 16 18 0 16 0 0 0 0 20 2 20 35 2 16 18 35 20 35 WELL CONSTRUCTION RECORD This form canbe usedforsingle or multiple wells FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013 1.Well Contractor Information: Well ContractorName NC WellContractor Certification Number CompanyName 2.Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, Injection, etc.) 3.Well Use (check well use): Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared)□Irrigation Non-Water Supply Well:□Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks) 4.Date Well(s)Completed:____________Well ID#______________________ 5a.Well Location: Facility/Owner Name Facility ID#(if applicable) Physical Address,City,and Zip County Parcel Identification No.(PIN) 5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient) N W 6.Is (are)the well(s):□Permanent or □Temporary 7.Is this a repair to an existing well:□Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8.Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9.Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10.Static water level below topof casing: (ft.)If water level is above casing, use “+” 11.Borehole diameter: (in.) 12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.) FOR WATER SUPPLY WELLS ONLY: 13a.Yield (gpm) Method oftest: 13b.Disinfection type: Amount: 14.WATER ZONES FROM TO DESCRIPTION ft.ft. ft.ft. 15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL ft.ft.in. 16.INNER CASING OR TUBING(geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft.ft.in. ft.ft.in. 17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL ft.ft.in. ft.ft.in. 18.GROUT FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT ft.ft. ft.ft. ft.ft. 19.SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENTMETHOD ft.ft. ft.ft. 20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.) ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. 21.REMARKS 22.Certification: Signatureof Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing: Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617 24b.For Injection Wells ONLY:In addition to sending the form to the address in 24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing: Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636 24c.For Water Supply &Injection Wells: Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed. For Internal UseONLY: _______________ Sam Bowers 3220-A Geological Resources, Inc. WM0301269 4/26/23 MW-1 Handy Corner 00-0-0000014377 2076 Startown Rd, Lincolnton, 28092 Lincoln 52985 35.51237333 81.26185667 35 26.23 6" Solid Stem Auger 26.23 35 Brown Silt 0 0 0 0 20 2 Sch 40 PVC 20 35 2 0.010 Sch 40 PVC 0 16 grout pour 16 18 bentonite pour 18 35 #2 Sand Pour 0 0.5 Asphalt 0.5 9.5 Silt 9.5 10 Weathered rock 10 35 Silt 4/26/23 Site Name:Date: Project Number:Log Completed By: Company:Drill Type: Driller:License Number: Boring ID:Depth: Diameter:Completion Details: PID Lab From To (ppm)Sample Description Color Moisture Odor Depth (ft)Lithology SITE INFORMATION DRILLING INFORMATION BORING INFORMATION Photo 1: Preclearing Photo 2: Completion Handy Corner 6389 7/5/23 Jase Bowers Geological Resources, Inc. Matt Steele Solid Stem Auger 4548-A MW-2 6" 35' Well installed at completion 0 6 Silt Brown Dry 6 11 Silt Red Dry 11 26 Silt Brown Dry 26 28 Silt Brown Moist 28 35 Fine Sand Brown Wet Site Name:Date: Project Number:Log Completed By: Company:Drill Type: Driller:License Number: Boring ID:Top of Casing: Diameter:Depth to Water: From (ft)To (ft)From (ft)To (ft)Diameter (in) From (ft)To (ft)From (ft)To (ft)Diameter (in) From (ft)To (ft)From (ft)To (ft)Diameter (in) Sand Bentonite Grout Screen Casing SITE INFORMATION DRILLING INFORMATION WELL CONSTRUCTION INFORMATION DIAGRAM -MONITORING WELL Sand Bentonite Grout Screen Inner Casing Outer Casing Handy Corner 6389 7/5/23 Jase Bowers Geological Resources, Inc. Matt Steele Solid Stem Auger 4548-A MW-2 6" 102.49 26.13 18 35 16 18 0 16 0 20 2 20 35 2 16 18 35 20 35 WELL CONSTRUCTION RECORD This form canbe usedforsingle or multiple wells FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013 1.Well Contractor Information: Well ContractorName NC WellContractor Certification Number CompanyName 2.Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, Injection, etc.) 3.Well Use (check well use): Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared)□Irrigation Non-Water Supply Well:□Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks) 4.Date Well(s)Completed:____________Well ID#______________________ 5a.Well Location: Facility/Owner Name Facility ID#(if applicable) Physical Address,City,and Zip County Parcel Identification No.(PIN) 5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient) N W 6.Is (are)the well(s):□Permanent or □Temporary 7.Is this a repair to an existing well:□Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8.Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9.Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10.Static water level below topof casing: (ft.)If water level is above casing, use “+” 11.Borehole diameter: (in.) 12.Well construction method:(i.e.auger,rotary,cable,direct push,etc.) FOR WATER SUPPLY WELLS ONLY: 13a.Yield (gpm) Method oftest: 13b.Disinfection type: Amount: 14.WATER ZONES FROM TO DESCRIPTION ft.ft. ft.ft. 15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL ft.ft.in. 16.INNER CASING OR TUBING(geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft.ft.in. ft.ft.in. 17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL ft.ft.in. ft.ft.in. 18.GROUT FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT ft.ft. ft.ft. ft.ft. 19.SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENTMETHOD ft.ft. ft.ft. 20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.) ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. 21.REMARKS 22.Certification: Signatureof Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing: Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617 24b.For Injection Wells ONLY:In addition to sending the form to the address in 24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing: Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636 24c.For Water Supply &Injection Wells: Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed. For Internal UseONLY: _______________ Matt Steele 4548-A Geological Resources, Inc. WM0301269 7/5/23 MW-2 Handy Corner 00-0-0000014377 2076 Startown Rd, Lincolnton, 28092 Lincoln 52985 35.51246718 81.26197593 1 35 26.13 6" Solid Stem Auger 26.13 28 Silt 28 35 Fine Sand 0 20 2 Sch 40 PVC 20 35 2 0.010 Sch 40 PVC 0 16 grout pour 16 18 bentonite pour 18 35 #2 Sand Pour 0 6 Silt 6 11 Silt 11 26 Silt 26 28 Silt 28 35 Fine Sand 7/5/23 Site Name:Date: Project Number:Log Completed By: Company:Drill Type: Driller:License Number: Boring ID:Depth: Diameter:Completion Details: PID Lab From To (ppm)Sample Description Color Moisture Odor Depth (ft)Lithology SITE INFORMATION DRILLING INFORMATION BORING INFORMATION Photo 1: Preclearing Photo 2: Completion Handy Corner 6389 7/5/23 Jase Bowers Geological Resources, Inc. Matt Steele Solid Stem Auger 4548-A MW-3 6" 35' Well installed at completion 0 0.4 Asphalt 0.4 12 Silt Red Dry 12 26 Silt Brown Dry 26 28 Silt Brown Moist 28 35 Fine Sand Brown Wet Site Name:Date: Project Number:Log Completed By: Company:Drill Type: Driller:License Number: Boring ID:Top of Casing: Diameter:Depth to Water: From (ft)To (ft)From (ft)To (ft)Diameter (in) From (ft)To (ft)From (ft)To (ft)Diameter (in) From (ft)To (ft)From (ft)To (ft)Diameter (in) Sand Bentonite Grout Screen Casing SITE INFORMATION DRILLING INFORMATION WELL CONSTRUCTION INFORMATION DIAGRAM -MONITORING WELL Sand Bentonite Grout Screen Inner Casing Outer Casing Handy Corner 6389 7/5/23 Jase Bowers Geological Resources, Inc. Matt Steele Solid Stem Auger 4548-A MW-3 6" 98.80 25.26 18 35 16 18 0 16 0 20 2 20 35 2 16 18 35 20 35 WELL CONSTRUCTION RECORD This form canbe usedforsingle or multiple wells FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013 1.Well Contractor Information: Well ContractorName NC WellContractor Certification Number CompanyName 2.Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, Injection, etc.) 3.Well Use (check well use): Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared)□Irrigation Non-Water Supply Well:□Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks) 4.Date Well(s)Completed:____________Well ID#______________________ 5a.Well Location: Facility/Owner Name Facility ID#(if applicable) Physical Address,City,and Zip County Parcel Identification No.(PIN) 5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient) N W 6.Is (are)the well(s):□Permanent or □Temporary 7.Is this a repair to an existing well:□Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8.Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9.Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10.Static water level below topof casing: (ft.)If water level is above casing, use “+” 11.Borehole diameter: (in.) 12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.) FOR WATER SUPPLY WELLS ONLY: 13a.Yield (gpm) Method oftest: 13b.Disinfection type: Amount: 14.WATER ZONES FROM TO DESCRIPTION ft.ft. ft.ft. 15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL ft.ft.in. 16.INNER CASING OR TUBING(geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft.ft.in. ft.ft.in. 17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL ft.ft.in. ft.ft.in. 18.GROUT FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT ft.ft. ft.ft. ft.ft. 19.SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENTMETHOD ft.ft. ft.ft. 20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.) ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. 21.REMARKS 22.Certification: Signatureof Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing: Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617 24b.For Injection Wells ONLY:In addition to sending the form to the address in 24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing: Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636 24c.For Water Supply &Injection Wells: Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed. For Internal UseONLY: _______________ Matt Steele 4548-A Geological Resources, Inc. WM0301269 7/5/23 MW-3 Handy Corner 00-0-0000014377 2076 Startown Rd, Lincolnton, 28092 Lincoln 52985 35.51237493 81.26171790 1 35 25.26 6" Solid Stem Auger 25.26 28 Silt 28 35 Fine Sand 0 20 2 Sch 40 PVC 20 35 2 0.010 Sch 40 PVC 0 16 grout pour 16 18 bentonite pour 18 35 #2 Sand Pour 0 0.4 Asphalt 0.4 12 Silt 12 26 Silt 26 28 Silt 28 35 Fine Sand 7/5/23 Site Name:Date: Project Number:Log Completed By: Company:Drill Type: Driller:License Number: Boring ID:Depth: Diameter:Completion Details: PID Lab From To (ppm)Sample Description Color Moisture Odor Depth (ft)Lithology SITE INFORMATION DRILLING INFORMATION BORING INFORMATION Photo 1: Preclearing Photo 2: Completion Handy Corner 6389 7/5/23 Jase Bowers Geological Resources, Inc. Matt Steele Solid Stem Auger 4548-A MW-4 6" 35' Well installed at completion 0 7 Silt Brown Dry 7 12 Silt Red Dry 12 27 Silt Brown Dry 27 29 Silt Brown Moist 29 35 Fine Sand Brown Wet Site Name:Date: Project Number:Log Completed By: Company:Drill Type: Driller:License Number: Boring ID:Top of Casing: Diameter:Depth to Water: From (ft)To (ft)From (ft)To (ft)Diameter (in) From (ft)To (ft)From (ft)To (ft)Diameter (in) From (ft)To (ft)From (ft)To (ft)Diameter (in) Sand Bentonite Grout Screen Casing SITE INFORMATION DRILLING INFORMATION WELL CONSTRUCTION INFORMATION DIAGRAM -MONITORING WELL Sand Bentonite Grout Screen Inner Casing Outer Casing Handy Corner 6389 7/5/23 Jase Bowers Geological Resources, Inc. Matt Steele Solid Stem Auger 4548-A MW-4 6" 102.50 28.15 18 35 16 18 0 16 0 20 2 20 35 2 16 18 35 20 35 WELL CONSTRUCTION RECORD This form canbe usedforsingle or multiple wells FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013 1.Well Contractor Information: Well ContractorName NC WellContractor Certification Number CompanyName 2.Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, Injection, etc.) 3.Well Use (check well use): Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single) □Industrial/Commercial □Residential Water Supply (shared)□Irrigation Non-Water Supply Well:□Monitoring □Recovery Injection Well: □Aquifer Recharge □Groundwater Remediation □Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage □Experimental Technology □Subsidence Control □Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks) 4.Date Well(s)Completed:____________Well ID#______________________ 5a.Well Location: Facility/Owner Name Facility ID#(if applicable) Physical Address,City,and Zip County Parcel Identification No.(PIN) 5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient) N W 6.Is (are)the well(s):□Permanent or □Temporary 7.Is this a repair to an existing well:□Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8.Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9.Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10.Static water level below topof casing: (ft.)If water level is above casing, use “+” 11.Borehole diameter: (in.) 12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.) FOR WATER SUPPLY WELLS ONLY: 13a.Yield (gpm) Method oftest: 13b.Disinfection type:Amount: 14.WATER ZONES FROM TO DESCRIPTION ft.ft. ft.ft. 15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL ft.ft.in. 16.INNER CASING OR TUBING(geothermal closed-loop) FROM TO DIAMETER THICKNESS MATERIAL ft.ft.in. ft.ft.in. 17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL ft.ft.in. ft.ft.in. 18.GROUT FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT ft.ft. ft.ft. ft.ft. 19.SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENTMETHOD ft.ft. ft.ft. 20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.) ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. ft.ft. 21.REMARKS 22.Certification: Signatureof Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing: Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617 24b.For Injection Wells ONLY:In addition to sending the form to the address in 24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing: Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636 24c.For Water Supply &Injection Wells: Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed. For Internal UseONLY: _______________ Matt Steele 4548-A Geological Resources, Inc. WM0301269 7/5/23 MW-4 Handy Corner 00-0-0000014377 2076 Startown Rd, Lincolnton, 28092 Lincoln 52985 35.51230351 81.26193415 1 35 28.15 6" Solid Stem Auger 28.15 29 Silt 29 35 Fine Sand 0 20 2 Sch 40 PVC 20 35 2 0.010 Sch 40 PVC 0 16 grout pour 16 18 bentonite pour 18 35 #2 Sand Pour 0 7 Silt 7 12 Silt 12 27 Silt 27 29 Silt 29 35 Fine Sand 7/5/23 APPENDIX D State Correspondence 1 Joanna Alley From:Mills, Ryan <ryan.mills@ncdenr.gov> Sent:Monday, May 15, 2023 9:23 PM To:Joanna Alley Subject:RE: [External] Handy Corner I’m not sure if I answered this or not, but yes please go ahead with the High risk LSA work. Ryan Mills Environmental Program Consultant, Division of Waste Management UST Section – Corrective Action Branch North Carolina Department of Environmental Quality 704.235.2175 (Office) Ryan.Mills@ncdenr.gov From: Joanna Alley <jra@geologicalresourcesinc.com> Sent: Thursday, May 11, 2023 9:50 AM To: Mills, Ryan <ryan.mills@ncdenr.gov> Cc: Taraban, Ron <ron.taraban@ncdenr.gov> Subject: RE: [External] Handy Corner CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. A Site Check was submi ed by a previous consultant and we submi ed the UST-61 form to Ron in March. I a ached the email we sent to Ron that includes the Site Check and the UST-61 form. This site does not have a prior release so we do not need a TA, but to go to the High Risk LSA, we do have you get your agreement that the site meets the criteria (High Risk AND exceeds the applicable standards by a factor of 10). There were a lot of potable wells within 1,000 feet and the contaminant concentra ons were above 10x 2L. Best Regards, Joanna Alley, P.E. Project Manager Geological Resources, Inc. 2021 Winner of the Union County Chamber Excellence In Business Award 3502 Hayes Road | Monroe, NC 28110 | website | facebook | 704-845-4010-office | 704-698-1244-direct | 704-845-4012-fax 2 From: Mills, Ryan <ryan.mills@ncdenr.gov> Sent: Thursday, May 11, 2023 9:43 AM To: Joanna Alley <jra@geologicalresourcesinc.com> Cc: Taraban, Ron <ron.taraban@ncdenr.gov> Subject: RE: [External] Handy Corner Where is this located? Was a UST-61 turned in or a Site Check? Ryan Mills Environmental Program Consultant, Division of Waste Management UST Section – Corrective Action Branch North Carolina Department of Environmental Quality 704.235.2175 (Office) Ryan.Mills@ncdenr.gov From: Joanna Alley <jra@geologicalresourcesinc.com> Sent: Thursday, May 11, 2023 8:42 AM To: Mills, Ryan <ryan.mills@ncdenr.gov> Cc: Taraban, Ron <ron.taraban@ncdenr.gov> Subject: [External] Handy Corner CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the Report Message button located on your Outlook menu bar on the Home tab. Good Morning Ryan, I believe this site will be yours since is it Lincoln County. We performed a LSA and determined this site will be high risk. I also just received the analy cal results and we have hit over 10x 2L, so this needs to go to a High Risk LSA. Do we have your agreement on this? Best Regards, Joanna Alley, P.E. Project Manager Geological Resources, Inc. 2021 Winner of the Union County Chamber Excellence In Business Award 3502 Hayes Road | Monroe, NC 28110 | website | facebook | 704-845-4010-office | 704-698-1244-direct | 704-845-4012-fax APPENDIX E Laboratory Analytical Reports Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. 5/10/2023 Geological Resources, Inc. Joanna Alley 3502 Hayes Road Monroe, NC, 28110 Ref: Analytical Testing Lab Report Number: 23-121-0003 Client Project Description: Handy Corner GRI #6389 Dear Joanna Alley: Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/1/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Page 1 of 51 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202337735State ProgramNorth Carolina 12/31/2023402State ProgramNorth Carolina 07/31/202399012State ProgramSouth Carolina 12/31/202299012State ProgramSouth Carolina Page 1 of 1 00016/23-121-0003 Page 2 of 51 Report Number: Sample Summary Table Client Project Description: 23-121-0003 Handy Corner GRI #6389 Lab No Client Sample ID Matrix Date Collected Date Received 04/26/2023 14:14Aqueous 95155 MW-1 05/01/2023 16:51 04/26/2023 09:56Solids 95156 MW-1-5'05/01/2023 16:51 04/26/2023 10:08Solids 95157 MW-1-10'05/01/2023 16:51 04/26/2023 10:12Solids 95158 MW-1-15'05/01/2023 16:51 04/26/2023 10:19Solids 95159 MW-1-20'05/01/2023 16:51 04/26/2023 08:30Aqueous 95160 TB 05/01/2023 16:51 Page 3 of 51 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-121-0003 Report Limit Project:Handy Corner V 95155MW-1 0.414 05/04/2023 15:296010DLeadmg/L 0.120 38.7 05/07/2023 23:486200BBenzeneµg/L 0.180 0.929 05/07/2023 23:486200BBromodichloromethaneµg/L 0.160 J0.211 05/07/2023 23:486200Bn-Butylbenzene µg/L 0.180 J0.450 05/07/2023 23:486200Bsec-Butyl benzene µg/L 0.200 30.5 05/07/2023 23:486200BChloroformµg/L 0.220 1.61 05/07/2023 23:486200BDi-Isopropyl Ether (DIPE)µg/L 0.500 41.6 05/07/2023 23:486200BEthylbenzeneµg/L 0.170 20.0 05/07/2023 23:486200B2-Hexanone µg/L 0.380 3.07 05/07/2023 23:486200BIsopropylbenzeneµg/L 0.180 J0.241 05/07/2023 23:486200B4-Isopropyl toluene µg/L 0.089 7.98 05/07/2023 23:486200BMethyl Ethyl Ketone (MEK)µg/L 0.710 J0.969 05/07/2023 23:486200BMethyl tert-butyl ether (MTBE)µg/L 0.140 25.7 05/07/2023 23:486200B4-Methyl-2-Pentanone µg/L 0.078 J0.416 05/07/2023 23:486200BMethylene Chloride µg/L 0.330 4.91 05/07/2023 23:486200Bn-Propylbenzene µg/L 0.190 135 05/08/2023 20:366200BTolueneµg/L 2.20 48.4 05/07/2023 23:486200B1,2,4-Trimethylbenzene µg/L 0.190 26.9 05/07/2023 23:486200B1,3,5-Trimethylbenzene µg/L 0.180 131 05/08/2023 20:366200Bo-Xylene µg/L 2.10 246 05/08/2023 20:366200Bm,p-Xylene µg/L 4.20 377 05/08/2023 20:366200BXylene (Total)µg/L 2.10 235 05/01/2023 14:22CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 11.5 241 05/01/2023 14:22CALCULATIONAromatic C9-C10 (Adjusted)µg/L 4.02 409 05/01/2023 14:22MADEP-VPH Aliphatic C5-C8 µg/L 11.5 665 05/01/2023 14:22MADEP-VPH Aliphatic C9-C12 µg/L 25.8 241 05/01/2023 14:22MADEP-VPH Aromatic C9-C10 µg/L 4.02 V 95156MW-1-5' J0.013 05/02/2023 12:328260DAcetonemg/Kg - dry 0.002 J0.0009 05/02/2023 12:328260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008 19.6 05/03/2023 10:50SW-DRYWT Moisture % V 95159MW-1-20' 0.098 05/02/2023 12:598260DAcetonemg/Kg - dry 0.003 0.032 05/02/2023 12:598260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008 J0.002 05/02/2023 12:598260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008 J0.0009 05/02/2023 12:598260DToluenemg/Kg - dry 0.0009 Page 4 of 51 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-121-0003 Report Limit Project:Handy Corner V 95159MW-1-20' J0.001 05/02/2023 12:598260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006 J0.0007 05/02/2023 12:598260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007 J0.002 05/02/2023 12:598260Do-Xylene mg/Kg - dry 0.0007 J0.002 05/02/2023 12:598260Dm,p-Xylene mg/Kg - dry 0.001 J0.005 05/02/2023 12:598260DXylene (Total)mg/Kg - dry 0.0007 23.5 05/03/2023 10:50SW-DRYWT Moisture % Page 5 of 51 Client: Geological Resources, Inc. CASE NARRATIVE Project: Handy Corner Lab Report Number: 23-121-0003 Date: 5/10/2023 EDB and DBCP by Microextraction GC/ECD Method EPA-504.1 Analyte: 1,2-Dibromoethane QC Batch No: V32736/V32711 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Massachusetts VPH Method MADEP-VPH Sample 95156 (MW-1-5') QC Batch No: V32693 No VPH vials received. Sample prepared from bulk container. Sample 95159 (MW-1-20') QC Batch No: V32693 No VPH vials received. Sample prepared from bulk container. Sample 95156 (MW-1-5') Analyte: 2,5-Dibromotoluene (PID) QC Batch No: V32693/V32692 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits. Sample 95159 (MW-1-20') Analyte: 2,5-Dibromotoluene (PID) QC Batch No: V32693/V32692 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits. Metals Analysis Method 6010D Sample 95155 (MW-1) QC Batch No: V32792/V32658 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 94887 Analyte: Lead QC Batch No: V32755/V32658 LLC failed high. Sample concentration BRL. Result not affected. Volatile Organic Compounds - GC/MS Method 8260D Analyte: 2-Butanone QC Batch No: V32695/V32694 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Page 6 of 51 Analyte: 2-Hexanone QC Batch No: V32695/V32694 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: Trichloroethene QC Batch No: V32695/V32694 CCV result is above control limits but within method parameters. Results are reported but considered estimated. Page 7 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1 95155 Matrix: 4/26/2023 14:14 Aqueous Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 0.414 mg/L 0.120 0.300Lead 50 05/04/23 15:29 6010DJKC Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 8 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1 95155 Matrix: 4/26/2023 14:14 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V32933 05/07/23 09:00 V32972 05/08/23 09:00 <1.80 µg/L 1.80 10.0Acetone 1 05/07/23 23:48 V32934MSA 38.7 µg/L 0.180 0.500Benzene 1 05/07/23 23:48 V32934MSA <0.210 µg/L 0.210 0.500Bromobenzene 1 05/07/23 23:48 V32934MSA <0.420 µg/L 0.420 1.00Bromochloromethane 1 05/07/23 23:48 V32934MSA 0.929 µg/L 0.160 0.500Bromodichloromethane 1 05/07/23 23:48 V32934MSA <1.50 µg/L 1.50 5.00Bromoform 1 05/07/23 23:48 V32934MSA <0.280 µg/L 0.280 1.00Bromomethane 1 05/07/23 23:48 V32934MSA 0.211 J µg/L 0.180 0.500n-Butylbenzene 1 05/07/23 23:48 V32934MSA 0.450 J µg/L 0.200 0.500sec-Butyl benzene 1 05/07/23 23:48 V32934MSA <0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/07/23 23:48 V32934MSA <0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/07/23 23:48 V32934MSA <0.190 µg/L 0.190 0.500Chlorobenzene 1 05/07/23 23:48 V32934MSA <0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/07/23 23:48 V32934MSA <0.430 µg/L 0.430 1.00Chloroethane 1 05/07/23 23:48 V32934MSA 30.5 µg/L 0.220 0.500Chloroform 1 05/07/23 23:48 V32934MSA <0.220 µg/L 0.220 0.500Chloromethane 1 05/07/23 23:48 V32934MSA <0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/07/23 23:48 V32934MSA <0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/07/23 23:48 V32934MSA 1.61 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 05/07/23 23:48 V32934MSA <1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/07/23 23:48 V32934MSA <0.230 µg/L 0.230 0.500Dibromomethane 1 05/07/23 23:48 V32934MSA <0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/07/23 23:48 V32934MSA Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 9 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1 95155 Matrix: 4/26/2023 14:14 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V32933 05/07/23 09:00 V32972 05/08/23 09:00 <0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/07/23 23:48 V32934MSA <0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/07/23 23:48 V32934MSA <1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/07/23 23:48 V32934MSA <0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/07/23 23:48 V32934MSA <0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/07/23 23:48 V32934MSA <0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/07/23 23:48 V32934MSA <0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/07/23 23:48 V32934MSA <0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/07/23 23:48 V32934MSA <0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/07/23 23:48 V32934MSA <0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/07/23 23:48 V32934MSA <0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/07/23 23:48 V32934MSA <0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/07/23 23:48 V32934MSA <0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/07/23 23:48 V32934MSA <0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/07/23 23:48 V32934MSA <42.0 µg/L 42.0 200Ethanol 1 05/07/23 23:48 V32934MSA 41.6 µg/L 0.170 0.500Ethylbenzene 1 05/07/23 23:48 V32934MSA <0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 05/07/23 23:48 V32934MSA 20.0 µg/L 0.380 1.002-Hexanone 1 05/07/23 23:48 V32934MSA 3.07 µg/L 0.180 0.500Isopropylbenzene 1 05/07/23 23:48 V32934MSA 0.241 J µg/L 0.089 0.5004-Isopropyl toluene 1 05/07/23 23:48 V32934MSA 7.98 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/07/23 23:48 V32934MSA 0.969 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 05/07/23 23:48 V32934MSA Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 10 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1 95155 Matrix: 4/26/2023 14:14 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V32933 05/07/23 09:00 V32972 05/08/23 09:00 25.7 µg/L 0.078 1.004-Methyl-2-Pentanone 1 05/07/23 23:48 V32934MSA 0.416 J µg/L 0.330 2.00Methylene Chloride 1 05/07/23 23:48 V32934MSA <0.470 µg/L 0.470 1.00Naphthalene 1 05/07/23 23:48 V32934MSA 4.91 µg/L 0.190 0.500n-Propylbenzene 1 05/07/23 23:48 V32934MSA <0.220 µg/L 0.220 0.500Styrene 1 05/07/23 23:48 V32934MSA <0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/07/23 23:48 V32934MSA <0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/07/23 23:48 V32934MSA <0.220 µg/L 0.220 0.500Tetrachloroethene 1 05/07/23 23:48 V32934MSA 135 µg/L 2.20 5.00Toluene 10 05/08/23 20:36 V32973MSA <0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 05/07/23 23:48 V32934MSA <0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 05/07/23 23:48 V32934MSA <0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/07/23 23:48 V32934MSA <0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/07/23 23:48 V32934MSA <0.180 µg/L 0.180 0.500Trichloroethene 1 05/07/23 23:48 V32934MSA <0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/07/23 23:48 V32934MSA <0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 05/07/23 23:48 V32934MSA 48.4 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 05/07/23 23:48 V32934MSA 26.9 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/07/23 23:48 V32934MSA <1.00 µg/L 1.00 5.00Vinyl Acetate 1 05/07/23 23:48 V32934MSA <0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/07/23 23:48 V32934MSA 131 µg/L 2.10 5.00o-Xylene 10 05/08/23 20:36 V32973MSA 246 µg/L 4.20 10.0m,p-Xylene 10 05/08/23 20:36 V32973MSA Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 11 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1 95155 Matrix: 4/26/2023 14:14 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V32933 05/07/23 09:00 V32972 05/08/23 09:00 377 µg/L 2.10 5.00Xylene (Total)10 05/08/23 20:36 V32973 Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%05/07/23 23:481 MSA V32934 Surrogate: Dibromofluoromethane 103 Limits: 70-130%05/07/23 23:481 MSA V32934 Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%05/07/23 23:481 MSA V32934 Surrogate: Toluene-d8 99.4 Limits: 70-130%05/07/23 23:481 MSA V32934 Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/08/23 20:3610 MSA V32973 Surrogate: Dibromofluoromethane 106 Limits: 70-130%05/08/23 20:3610 MSA V32973 Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%05/08/23 20:3610 MSA V32973 Surrogate: Toluene-d8 97.2 Limits: 70-130%05/08/23 20:3610 MSA V32973 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF EPA-504.1(PREP) EPA-504.1 Prep Batch(es):V32711 05/03/23 10:20 <0.00338 µg/L 0.00338 0.02051,2-Dibromoethane 1 05/03/23 13:55 V32736TJW Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 12 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1 95155 Matrix: 4/26/2023 14:14 Aqueous Analytical Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF CALCULATION 235 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 05/01/23 14:22 <25.8 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 05/01/23 14:22 241 µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 05/01/23 14:22 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF MAVPH (Prep) MADEP-VPH Prep Batch(es):V32650 05/01/23 08:00 409 µg/L 11.5 50.0Aliphatic C5-C8 1 05/01/23 14:22 V32651TBL 665 µg/L 25.8 50.0Aliphatic C9-C12 1 05/01/23 14:22 V32651TBL 241 µg/L 4.02 50.0Aromatic C9-C10 1 05/01/23 14:22 V32651TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)88.1 Limits: 70-130%05/01/23 14:221 TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)100 Limits: 70-130%05/01/23 14:221 TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 13 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-5' 95156 Matrix: 4/26/2023 9:56 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 19.6 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 14 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-5' 95156 Matrix: 4/26/2023 9:56 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V32694 05/02/23 08:00 0.013 J mg/Kg - dry 0.002 0.024Acetone 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.024Acrolein 1 05/02/23 12:32 V32695TBL <0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 05/02/23 12:32 V32695TBL <0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/02/23 12:32 V32695TBL <0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 05/02/23 12:32 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 05/02/23 12:32 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/02/23 12:32 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/02/23 12:32 V32695TBL <0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/02/23 12:32 V32695TBL <0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/02/23 12:32 V32695TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 15 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-5' 95156 Matrix: 4/26/2023 9:56 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V32694 05/02/23 08:00 <0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 05/02/23 12:32 V32695TBL <0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/02/23 12:32 V32695TBL <0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/02/23 12:32 V32695TBL <0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 05/02/23 12:32 V32695TBL <0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/02/23 12:32 V32695TBL <0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/02/23 12:32 V32695TBL <0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/02/23 12:32 V32695TBL <0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 12:32 V32695TBL <0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 05/02/23 12:32 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 05/02/23 12:32 V32695TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 16 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-5' 95156 Matrix: 4/26/2023 9:56 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V32694 05/02/23 08:00 <0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/02/23 12:32 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 05/02/23 12:32 V32695TBL 0.0009 J mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/02/23 12:32 V32695TBL <0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/02/23 12:32 V32695TBL <0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/02/23 12:32 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 05/02/23 12:32 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/02/23 12:32 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/02/23 12:32 V32695TBL <0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/02/23 12:32 V32695TBL <0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/02/23 12:32 V32695TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 17 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-5' 95156 Matrix: 4/26/2023 9:56 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V32694 05/02/23 08:00 <0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/02/23 12:32 V32695TBL <0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/02/23 12:32 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/02/23 12:32 V32695 Surrogate: 4-Bromofluorobenzene 85.1 Limits: 70-130%05/02/23 12:321 TBL V32695 Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/02/23 12:321 TBL V32695 Surrogate: Toluene-d8 88.5 Limits: 76-129%05/02/23 12:321 TBL V32695 Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 18 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-5' 95156 Matrix: 4/26/2023 9:56 Solids Analytical Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF CALCULATION <1.52 mg/Kg - dry 1.52 9.95Aliphatic C5-C8 (Adjusted)1 05/02/23 12:32 <5.67 mg/Kg - dry 5.67 9.95Aliphatics C9-C12 (Adjusted)1 05/02/23 12:32 <0.776 mg/Kg - dry 0.776 9.95Aromatic C9-C10 (Adjusted)100 05/02/23 17:08 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF MAVPH (Prep) MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00 <1.52 mg/Kg - dry 1.52 9.95Aliphatic C5-C8 100 05/02/23 17:08 V32693TBL <5.67 mg/Kg - dry 5.67 9.95Aliphatic C9-C12 100 05/02/23 17:08 V32693TBL <0.776 mg/Kg - dry 0.776 9.95Aromatic C9-C10 100 05/02/23 17:08 V32693TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)94.4 Limits: 70-130%05/02/23 17:08100 TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)145 *Limits: 70-130%05/02/23 17:08100 TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 19 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-10' 95157 Matrix: 4/26/2023 10:08 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF MAVPH (Prep) MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00 <1.22 mg/Kg 1.22 8.00Aliphatic C5-C8 100 05/02/23 17:31 V32693TBL <4.56 mg/Kg 4.56 8.00Aliphatic C9-C12 100 05/02/23 17:31 V32693TBL <0.624 mg/Kg 0.624 8.00Aromatic C9-C10 100 05/02/23 17:31 V32693TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)91.2 Limits: 70-130%05/02/23 17:31100 TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)92.2 Limits: 70-130%05/02/23 17:31100 TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 20 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-15' 95158 Matrix: 4/26/2023 10:12 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF MAVPH (Prep) MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00 <1.22 mg/Kg 1.22 8.00Aliphatic C5-C8 100 05/02/23 17:55 V32693TBL <4.56 mg/Kg 4.56 8.00Aliphatic C9-C12 100 05/02/23 17:55 V32693TBL <0.624 mg/Kg 0.624 8.00Aromatic C9-C10 100 05/02/23 17:55 V32693TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)98.1 Limits: 70-130%05/02/23 17:55100 TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)100 Limits: 70-130%05/02/23 17:55100 TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 21 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-20' 95159 Matrix: 4/26/2023 10:19 Solids Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF 23.5 %Moisture 1 05/03/23 10:50 SW-DRYWTPEB Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 22 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-20' 95159 Matrix: 4/26/2023 10:19 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V32694 05/02/23 08:00 0.098 mg/Kg - dry 0.003 0.026Acetone 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/02/23 12:59 V32695TBL <0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/02/23 12:59 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 05/02/23 12:59 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/02/23 12:59 V32695TBL <0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/02/23 12:59 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/02/23 12:59 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/02/23 12:59 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 05/02/23 12:59 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/02/23 12:59 V32695TBL <0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/02/23 12:59 V32695TBL <0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/02/23 12:59 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/02/23 12:59 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/02/23 12:59 V32695TBL <0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/02/23 12:59 V32695TBL <0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/02/23 12:59 V32695TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 23 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-20' 95159 Matrix: 4/26/2023 10:19 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V32694 05/02/23 08:00 <0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/02/23 12:59 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/02/23 12:59 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 05/02/23 12:59 V32695TBL <0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/02/23 12:59 V32695TBL <0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/02/23 12:59 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/02/23 12:59 V32695TBL <0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/02/23 12:59 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/02/23 12:59 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/02/23 12:59 V32695TBL <0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/02/23 12:59 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/02/23 12:59 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/02/23 12:59 V32695TBL <0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/02/23 12:59 V32695TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 24 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-20' 95159 Matrix: 4/26/2023 10:19 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V32694 05/02/23 08:00 <0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/02/23 12:59 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/02/23 12:59 V32695TBL 0.032 mg/Kg - dry 0.0008 0.026Methyl Ethyl Ketone (MEK)1 05/02/23 12:59 V32695TBL 0.002 J mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/02/23 12:59 V32695TBL <0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/02/23 12:59 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/02/23 12:59 V32695TBL <0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/02/23 12:59 V32695TBL 0.0009 J mg/Kg - dry 0.0009 0.006Toluene 1 05/02/23 12:59 V32695TBL <0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/02/23 12:59 V32695TBL <0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/02/23 12:59 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/02/23 12:59 V32695TBL <0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/02/23 12:59 V32695TBL <0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/02/23 12:59 V32695TBL <0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/02/23 12:59 V32695TBL 0.001 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/02/23 12:59 V32695TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 25 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-20' 95159 Matrix: 4/26/2023 10:19 Solids Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 5035 8260D Prep Batch(es):V32694 05/02/23 08:00 0.0007 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/02/23 12:59 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/02/23 12:59 V32695TBL <0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 05/02/23 12:59 V32695TBL 0.002 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/02/23 12:59 V32695TBL 0.002 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/02/23 12:59 V32695TBL 0.005 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/02/23 12:59 V32695KCC Surrogate: 4-Bromofluorobenzene 96.5 Limits: 70-130%05/02/23 12:591 TBL V32695 Surrogate: Dibromofluoromethane 100 Limits: 84-123%05/02/23 12:591 TBL V32695 Surrogate: Toluene-d8 87.8 Limits: 76-129%05/02/23 12:591 TBL V32695 Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 26 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:MW-1-20' 95159 Matrix: 4/26/2023 10:19 Solids Analytical Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF CALCULATION <1.59 mg/Kg - dry 1.59 10.5Aliphatic C5-C8 (Adjusted)100 05/02/23 18:18 <5.96 mg/Kg - dry 5.96 10.5Aliphatics C9-C12 (Adjusted)100 05/02/23 18:18 <0.815 mg/Kg - dry 0.815 10.5Aromatic C9-C10 (Adjusted)100 05/02/23 18:18 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF MAVPH (Prep) MADEP-VPH Prep Batch(es):V32692 05/02/23 08:00 <1.59 mg/Kg - dry 1.59 10.5Aliphatic C5-C8 100 05/02/23 18:18 V32693TBL <5.96 mg/Kg - dry 5.96 10.5Aliphatic C9-C12 100 05/02/23 18:18 V32693TBL <0.815 mg/Kg - dry 0.815 10.5Aromatic C9-C10 100 05/02/23 18:18 V32693TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)95.3 Limits: 70-130%05/02/23 18:18100 TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)134 *Limits: 70-130%05/02/23 18:18100 TBL Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 27 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:TB 95160 Matrix: 4/26/2023 8:30 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V32933 05/07/23 09:00 <1.80 µg/L 1.80 10.0Acetone 1 05/07/23 20:37 V32934MSA <0.180 µg/L 0.180 0.500Benzene 1 05/07/23 20:37 V32934MSA <0.210 µg/L 0.210 0.500Bromobenzene 1 05/07/23 20:37 V32934MSA <0.420 µg/L 0.420 1.00Bromochloromethane 1 05/07/23 20:37 V32934MSA <0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/07/23 20:37 V32934MSA <1.50 µg/L 1.50 5.00Bromoform 1 05/07/23 20:37 V32934MSA <0.280 µg/L 0.280 1.00Bromomethane 1 05/07/23 20:37 V32934MSA <0.180 µg/L 0.180 0.500n-Butylbenzene 1 05/07/23 20:37 V32934MSA <0.200 µg/L 0.200 0.500sec-Butyl benzene 1 05/07/23 20:37 V32934MSA <0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/07/23 20:37 V32934MSA <0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/07/23 20:37 V32934MSA <0.190 µg/L 0.190 0.500Chlorobenzene 1 05/07/23 20:37 V32934MSA <0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/07/23 20:37 V32934MSA <0.430 µg/L 0.430 1.00Chloroethane 1 05/07/23 20:37 V32934MSA <0.220 µg/L 0.220 0.500Chloroform 1 05/07/23 20:37 V32934MSA <0.220 µg/L 0.220 0.500Chloromethane 1 05/07/23 20:37 V32934MSA <0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/07/23 20:37 V32934MSA <0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/07/23 20:37 V32934MSA <0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 05/07/23 20:37 V32934MSA <1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/07/23 20:37 V32934MSA <0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/07/23 20:37 V32934MSA <0.230 µg/L 0.230 0.500Dibromomethane 1 05/07/23 20:37 V32934MSA Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 28 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:TB 95160 Matrix: 4/26/2023 8:30 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V32933 05/07/23 09:00 <0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/07/23 20:37 V32934MSA <0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/07/23 20:37 V32934MSA <0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/07/23 20:37 V32934MSA <1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/07/23 20:37 V32934MSA <0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/07/23 20:37 V32934MSA <0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/07/23 20:37 V32934MSA <0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/07/23 20:37 V32934MSA <0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/07/23 20:37 V32934MSA <0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/07/23 20:37 V32934MSA <0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/07/23 20:37 V32934MSA <0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/07/23 20:37 V32934MSA <0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/07/23 20:37 V32934MSA <0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/07/23 20:37 V32934MSA <0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/07/23 20:37 V32934MSA <0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/07/23 20:37 V32934MSA <42.0 µg/L 42.0 200Ethanol 1 05/07/23 20:37 V32934MSA <0.170 µg/L 0.170 0.500Ethylbenzene 1 05/07/23 20:37 V32934MSA <0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 05/07/23 20:37 V32934MSA <0.380 µg/L 0.380 1.002-Hexanone 1 05/07/23 20:37 V32934MSA <0.180 µg/L 0.180 0.500Isopropylbenzene 1 05/07/23 20:37 V32934MSA <0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/07/23 20:37 V32934MSA <0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/07/23 20:37 V32934MSA Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 29 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:TB 95160 Matrix: 4/26/2023 8:30 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V32933 05/07/23 09:00 <0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 05/07/23 20:37 V32934MSA <0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 05/07/23 20:37 V32934MSA <0.330 µg/L 0.330 2.00Methylene Chloride 1 05/07/23 20:37 V32934MSA <0.470 µg/L 0.470 1.00Naphthalene 1 05/07/23 20:37 V32934MSA <0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/07/23 20:37 V32934MSA <0.220 µg/L 0.220 0.500Styrene 1 05/07/23 20:37 V32934MSA <0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/07/23 20:37 V32934MSA <0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/07/23 20:37 V32934MSA <0.220 µg/L 0.220 0.500Tetrachloroethene 1 05/07/23 20:37 V32934MSA <0.220 µg/L 0.220 0.500Toluene 1 05/07/23 20:37 V32934MSA <0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 05/07/23 20:37 V32934MSA <0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 05/07/23 20:37 V32934MSA <0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/07/23 20:37 V32934MSA <0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/07/23 20:37 V32934MSA <0.180 µg/L 0.180 0.500Trichloroethene 1 05/07/23 20:37 V32934MSA <0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/07/23 20:37 V32934MSA <0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 05/07/23 20:37 V32934MSA <0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 05/07/23 20:37 V32934MSA <0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/07/23 20:37 V32934MSA <1.00 µg/L 1.00 5.00Vinyl Acetate 1 05/07/23 20:37 V32934MSA <0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/07/23 20:37 V32934MSA <0.210 µg/L 0.210 0.500o-Xylene 1 05/07/23 20:37 V32934MSA Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 30 of 51 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-121-0003 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 05/01/2023 Handy Corner Report Date : 05/10/2023 Sample ID : Lab No : Sampled:TB 95160 Matrix: 4/26/2023 8:30 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V32933 05/07/23 09:00 <0.420 µg/L 0.420 1.00m,p-Xylene 1 05/07/23 20:37 V32934MSA <0.21 µg/L 0.210 0.500Xylene (Total)1 05/07/23 20:37 V32934 Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/07/23 20:371 MSA V32934 Surrogate: Dibromofluoromethane 103 Limits: 70-130%05/07/23 20:371 MSA V32934 Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%05/07/23 20:371 MSA V32934 Surrogate: Toluene-d8 96.8 Limits: 70-130%05/07/23 20:371 MSA V32934 Qualifiers/ Definitions Dilution FactorDFOutside QC Limit* Method Quantitation LimitMQLEstimated valueJ Page 31 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Metals Analysis 6010D V32755QC Analytical Batch(es): Analysis Method: Analysis Description: 3005A QC Prep:V32658 Associated Lab Samples: 95155 LRB-V32658 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits 05/03/23 14:160.0060.002<0.002mg/LLead LCS-V32658Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 1050.1050.100mg/LLead 80-120 V 94887-MS-V32658 V 94887-MSD-V32658Matrix Spike & Matrix Spike Duplicate MS Result Parameter Max RPD MS %Rec MSD Result MSD Spike Conc. MS Spike Conc.ResultUnits %Rec Limits MSD %Rec RPD 0.103 1030.1080.1000.100< 0.002mg/LLead 108 75-125 4.7 20.0 V 94887-PDS-V32658Post Digestion Spike Parameter Analyzed% Recovery PDS ResultUnits 05/03/23 16:441010.252mg/LLead Page 1 of 18Date:05/10/2023 04:30 PM Page 32 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V32934QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V32933 Associated Lab Samples: 95155, 95160 LRB-V32933 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/07/23 19:4310.01.80<1.80µg/LAcetone 05/07/23 19:430.5000.180<0.180µg/LBenzene 05/07/23 19:430.5000.210<0.210µg/LBromobenzene 05/07/23 19:431.000.420<0.420µg/LBromochloromethane 05/07/23 19:430.5000.160<0.160µg/LBromodichloromethane 05/07/23 19:435.001.50<1.50µg/LBromoform 05/07/23 19:431.000.280<0.280µg/LBromomethane 05/07/23 19:430.5000.180<0.180µg/Ln-Butylbenzene 05/07/23 19:430.5000.200<0.200µg/Lsec-Butyl benzene 05/07/23 19:432.000.920<0.920µg/Ltert-Butyl benzene 05/07/23 19:430.5000.180<0.180µg/LCarbon Tetrachloride 05/07/23 19:430.5000.190<0.190µg/LChlorobenzene 05/07/23 19:430.5000.190<0.190µg/LChlorodibromomethane 05/07/23 19:431.000.430<0.430µg/LChloroethane 05/07/23 19:430.5000.220<0.220µg/LChloroform 05/07/23 19:430.5000.220<0.220µg/LChloromethane 05/07/23 19:430.5000.200<0.200µg/L2-Chlorotoluene 05/07/23 19:430.5000.200<0.200µg/L4-Chlorotoluene 05/07/23 19:430.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE) 05/07/23 19:432.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane 05/07/23 19:430.5000.200<0.200µg/L1,2-Dibromoethane 05/07/23 19:430.5000.230<0.230µg/LDibromomethane 05/07/23 19:430.5000.220<0.220µg/L1,2-Dichlorobenzene 05/07/23 19:430.5000.190<0.190µg/L1,3-Dichlorobenzene 05/07/23 19:430.5000.210<0.210µg/L1,4-Dichlorobenzene 05/07/23 19:435.001.20<1.20µg/LDichlorodifluoromethane 05/07/23 19:430.5000.240<0.240µg/L1,1-Dichloroethane Page 2 of 18Date:05/10/2023 04:30 PM Page 33 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V32934QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V32933 Associated Lab Samples: 95155, 95160 LRB-V32933 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/07/23 19:430.5000.150<0.150µg/L1,2-Dichloroethane 05/07/23 19:430.5000.150<0.150µg/L1,1-Dichloroethene 05/07/23 19:430.5000.200<0.200µg/Lcis-1,2-Dichloroethene 05/07/23 19:430.5000.180<0.180µg/Ltrans-1,2-Dichloroethene 05/07/23 19:430.5000.190<0.190µg/L1,2-Dichloropropane 05/07/23 19:430.5000.130<0.130µg/L1,3-Dichloropropane 05/07/23 19:432.000.210<0.210µg/L2,2-Dichloropropane 05/07/23 19:430.5000.200<0.200µg/L1,1-Dichloropropene 05/07/23 19:430.5000.210<0.210µg/Lcis-1,3-Dichloropropene 05/07/23 19:430.5000.150<0.150µg/Ltrans-1,3-Dichloropropene 05/07/23 19:4320042.0<42.0µg/LEthanol 05/07/23 19:430.5000.170<0.170µg/LEthylbenzene 05/07/23 19:433.000.350<0.350µg/LHexachlorobutadiene 05/07/23 19:431.000.380<0.380µg/L2-Hexanone 05/07/23 19:430.5000.180<0.180µg/LIsopropylbenzene 05/07/23 19:430.5000.089<0.089µg/L4-Isopropyl toluene 05/07/23 19:435.000.710<0.710µg/LMethyl Ethyl Ketone (MEK) 05/07/23 19:431.000.140<0.140µg/LMethyl tert-butyl ether (MTBE) 05/07/23 19:431.000.078<0.078µg/L4-Methyl-2-Pentanone 05/07/23 19:432.000.330<0.330µg/LMethylene Chloride 05/07/23 19:431.000.470<0.470µg/LNaphthalene 05/07/23 19:430.5000.190<0.190µg/Ln-Propylbenzene 05/07/23 19:430.5000.220<0.220µg/LStyrene 05/07/23 19:430.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane 05/07/23 19:430.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane 05/07/23 19:430.5000.220<0.220µg/LTetrachloroethene 05/07/23 19:430.5000.220<0.220µg/LToluene Page 3 of 18Date:05/10/2023 04:30 PM Page 34 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V32934QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V32933 Associated Lab Samples: 95155, 95160 LRB-V32933 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/07/23 19:430.5000.380<0.380µg/L1,2,3-Trichlorobenzene 05/07/23 19:430.5000.310<0.310µg/L1,2,4-Trichlorobenzene 05/07/23 19:430.5000.160<0.160µg/L1,1,1-Trichloroethane 05/07/23 19:430.5000.096<0.096µg/L1,1,2-Trichloroethane 05/07/23 19:430.5000.180<0.180µg/LTrichloroethene 05/07/23 19:430.5000.180<0.180µg/LTrichlorofluoromethane 05/07/23 19:430.5000.270<0.270µg/L1,2,3-Trichloropropane 05/07/23 19:430.5000.190<0.190µg/L1,2,4-Trimethylbenzene 05/07/23 19:430.5000.180<0.180µg/L1,3,5-Trimethylbenzene 05/07/23 19:435.001.00<1.00µg/LVinyl Acetate 05/07/23 19:430.5000.170<0.170µg/LVinyl Chloride 05/07/23 19:430.5000.210<0.210µg/Lo-Xylene 05/07/23 19:431.000.420<0.420µg/Lm,p-Xylene 05/07/23 19:434-Bromofluorobenzene (S)101 70-130 05/07/23 19:43Dibromofluoromethane (S)102 70-130 05/07/23 19:431,2-Dichloroethane - d4 (S)105 70-130 05/07/23 19:43Toluene-d8 (S)97.0 70-130 LCS-V32933 LCSD-V32933Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 36.1 90.295.538.240.0µg/LAcetone 40-160 5.6 20.0 19.4 97.010320.620.0µg/LBenzene 70-130 6.0 20.0 19.9 99.510320.620.0µg/LBromobenzene 70-130 3.4 20.0 20.7 10410721.420.0µg/LBromochloromethane 70-130 3.3 20.0 20.9 10511021.920.0µg/LBromodichloromethane 70-130 4.6 20.0 Page 4 of 18Date:05/10/2023 04:30 PM Page 35 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V32934QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V32933 LCS-V32933 LCSD-V32933Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 20.6 10310520.920.0µg/LBromoform 70-130 1.4 20.0 19.2 96.098.019.620.0µg/LBromomethane 60-140 2.0 20.0 18.3 91.597.519.520.0µg/Ln-Butylbenzene 70-130 6.3 20.0 19.0 95.010020.020.0µg/Lsec-Butyl benzene 70-130 5.1 20.0 19.6 98.010320.520.0µg/Ltert-Butyl benzene 70-130 4.4 20.0 22.1 11111623.220.0µg/LCarbon Tetrachloride 70-130 4.8 20.0 19.4 97.010721.320.0µg/LChlorobenzene 70-130 9.3 20.0 21.6 10811322.620.0µg/LChlorodibromomethane 70-130 4.5 20.0 20.7 10411021.920.0µg/LChloroethane 60-140 5.6 20.0 21.3 10711222.420.0µg/LChloroform 70-130 5.0 20.0 18.4 92.097.019.420.0µg/LChloromethane 60-140 5.2 20.0 19.1 95.510220.320.0µg/L2-Chlorotoluene 70-130 6.0 20.0 19.6 98.010420.720.0µg/L4-Chlorotoluene 70-130 5.4 20.0 19.3 96.599.019.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 2.5 20.0 20.4 10210420.820.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.9 20.0 20.9 10510320.520.0µg/L1,2-Dibromoethane 70-130 1.9 20.0 20.3 10210020.020.0µg/LDibromomethane 70-130 1.4 20.0 19.7 98.510220.420.0µg/L1,2-Dichlorobenzene 70-130 3.4 20.0 20.2 10110320.520.0µg/L1,3-Dichlorobenzene 70-130 1.4 20.0 19.4 97.010220.420.0µg/L1,4-Dichlorobenzene 70-130 5.0 20.0 21.5 10810921.720.0µg/LDichlorodifluoromethane 60-140 0.9 20.0 20.2 10110821.620.0µg/L1,1-Dichloroethane 70-130 6.6 20.0 20.6 10311022.020.0µg/L1,2-Dichloroethane 70-130 6.5 20.0 20.6 10311021.920.0µg/L1,1-Dichloroethene 70-130 6.1 20.0 19.7 98.510721.420.0µg/Lcis-1,2-Dichloroethene 70-130 8.2 20.0 21.3 10711322.620.0µg/Ltrans-1,2-Dichloroethene 70-130 5.9 20.0 Page 5 of 18Date:05/10/2023 04:30 PM Page 36 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V32934QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V32933 LCS-V32933 LCSD-V32933Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 19.1 95.510621.120.0µg/L1,2-Dichloropropane 70-130 9.9 20.0 19.3 96.598.019.620.0µg/L1,3-Dichloropropane 70-130 1.5 20.0 22.4 11211322.520.0µg/L2,2-Dichloropropane 70-130 0.4 20.0 21.1 10611723.420.0µg/L1,1-Dichloropropene 70-130 10.3 20.0 19.8 99.010721.320.0µg/Lcis-1,3-Dichloropropene 70-130 7.2 20.0 20.8 10410821.620.0µg/Ltrans-1,3-Dichloropropene 70-130 3.7 20.0 543 10993.2466500µg/LEthanol 60-140 15.2 20.0 19.7 98.510320.620.0µg/LEthylbenzene 70-130 4.4 20.0 20.8 10410821.520.0µg/LHexachlorobutadiene 70-130 3.3 20.0 17.6 88.091.018.220.0µg/L2-Hexanone 60-140 3.3 20.0 20.2 10110521.020.0µg/LIsopropylbenzene 70-130 3.8 20.0 20.1 10110520.920.0µg/L4-Isopropyl toluene 70-130 3.9 20.0 17.1 85.574.014.820.0µg/LMethyl Ethyl Ketone (MEK)60-140 14.4 20.0 20.1 10110721.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 6.2 20.0 17.4 87.090.018.020.0µg/L4-Methyl-2-Pentanone 60-140 3.3 20.0 20.5 10310320.620.0µg/LMethylene Chloride 70-130 0.4 20.0 15.8 79.079.515.920.0µg/LNaphthalene 70-130 0.6 20.0 19.1 95.597.519.520.0µg/Ln-Propylbenzene 70-130 2.0 20.0 20.4 10210220.420.0µg/LStyrene 70-130 0.0 20.0 20.9 10511222.320.0µg/L1,1,1,2-Tetrachloroethane 70-130 6.4 20.0 18.6 93.094.518.920.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.6 20.0 20.8 10410721.420.0µg/LTetrachloroethene 70-130 2.8 20.0 20.1 10110420.820.0µg/LToluene 70-130 3.4 20.0 21.4 10710220.320.0µg/L1,2,3-Trichlorobenzene 70-130 5.2 20.0 19.0 95.097.019.420.0µg/L1,2,4-Trichlorobenzene 70-130 2.0 20.0 22.0 11011322.620.0µg/L1,1,1-Trichloroethane 70-130 2.6 20.0 Page 6 of 18Date:05/10/2023 04:30 PM Page 37 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V32934QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V32933 LCS-V32933 LCSD-V32933Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 20.1 10110320.520.0µg/L1,1,2-Trichloroethane 70-130 1.9 20.0 21.6 10811021.920.0µg/LTrichloroethene 70-130 1.3 20.0 22.1 11111322.620.0µg/LTrichlorofluoromethane 60-140 2.2 20.0 20.3 10299.519.920.0µg/L1,2,3-Trichloropropane 70-130 1.9 20.0 19.9 99.510120.220.0µg/L1,2,4-Trimethylbenzene 70-130 1.4 20.0 20.0 10010520.920.0µg/L1,3,5-Trimethylbenzene 70-130 4.4 20.0 19.8 99.093.018.620.0µg/LVinyl Acetate 60-140 6.2 20.0 20.8 10411222.320.0µg/LVinyl Chloride 60-140 6.9 20.0 19.8 99.010420.720.0µg/Lo-Xylene 70-130 4.4 20.0 41.2 10310843.040.0µg/Lm,p-Xylene 70-130 4.2 20.0 97.699.04-Bromofluorobenzene (S)70-130 102104Dibromofluoromethane (S)70-130 1051061,2-Dichloroethane - d4 (S)70-130 97.898.0Toluene-d8 (S)70-130 Page 7 of 18Date:05/10/2023 04:30 PM Page 38 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V32973QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V32972 Associated Lab Samples: 95155 LRB-V32972 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/08/23 15:090.5000.220<0.220µg/LToluene 05/08/23 15:090.5000.210<0.210µg/Lo-Xylene 05/08/23 15:091.000.420<0.420µg/Lm,p-Xylene 05/08/23 15:094-Bromofluorobenzene (S)98.2 70-130 05/08/23 15:09Dibromofluoromethane (S)104 70-130 05/08/23 15:091,2-Dichloroethane - d4 (S)106 70-130 05/08/23 15:09Toluene-d8 (S)96.2 70-130 LCS-V32972 LCSD-V32972Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 19.9 99.510220.320.0µg/LToluene 70-130 1.9 20.0 20.3 10210120.220.0µg/Lo-Xylene 70-130 0.4 20.0 41.1 10310642.240.0µg/Lm,p-Xylene 70-130 2.6 20.0 99.099.44-Bromofluorobenzene (S)70-130 101103Dibromofluoromethane (S)70-130 1071051,2-Dichloroethane - d4 (S)70-130 96.896.2Toluene-d8 (S)70-130 Page 8 of 18Date:05/10/2023 04:30 PM Page 39 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 8260D V32695QC Analytical Batch(es): Analysis Method: Analysis Description: 5035 QC Prep:V32694 Associated Lab Samples: 95156, 95159 LRB-V32694 Matrix: SOLLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/02/23 11:110.0200.002<0.002mg/KgAcetone 05/02/23 11:110.0200.001<0.001mg/KgAcrolein 05/02/23 11:110.0200.0008<0.0008mg/KgAcrylonitrile 05/02/23 11:110.0050.0006<0.0006mg/KgBenzene 05/02/23 11:110.0050.0005<0.0005mg/KgBromobenzene 05/02/23 11:110.0050.0008<0.0008mg/KgBromochloromethane 05/02/23 11:110.0050.001<0.001mg/KgBromodichloromethane 05/02/23 11:110.0050.001<0.001mg/KgBromoform 05/02/23 11:110.0100.001<0.001mg/KgBromomethane 05/02/23 11:110.0050.0005<0.0005mg/Kgn-Butylbenzene 05/02/23 11:110.0050.0006<0.0006mg/Kgsec-Butyl benzene 05/02/23 11:110.0050.0005<0.0005mg/Kgtert-Butyl benzene 05/02/23 11:110.0050.0006<0.0006mg/KgCarbon Disulfide 05/02/23 11:110.0050.001<0.001mg/KgCarbon Tetrachloride 05/02/23 11:110.0050.0007<0.0007mg/KgChlorobenzene 05/02/23 11:110.0050.0009<0.0009mg/KgChlorodibromomethane 05/02/23 11:110.0100.0009<0.0009mg/KgChloroethane 05/02/23 11:110.0050.001<0.001mg/KgChloroform 05/02/23 11:110.0100.0006<0.0006mg/KgChloromethane 05/02/23 11:110.0050.0005<0.0005mg/Kg2-Chlorotoluene 05/02/23 11:110.0050.0004<0.0004mg/Kg4-Chlorotoluene 05/02/23 11:110.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE) 05/02/23 11:110.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane 05/02/23 11:110.0050.0006<0.0006mg/Kg1,2-Dibromoethane 05/02/23 11:110.0050.0006<0.0006mg/KgDibromomethane 05/02/23 11:110.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene 05/02/23 11:110.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene Page 9 of 18Date:05/10/2023 04:30 PM Page 40 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 8260D V32695QC Analytical Batch(es): Analysis Method: Analysis Description: 5035 QC Prep:V32694 Associated Lab Samples: 95156, 95159 LRB-V32694 Matrix: SOLLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/02/23 11:110.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene 05/02/23 11:110.0100.001<0.001mg/KgDichlorodifluoromethane 05/02/23 11:110.0050.0008<0.0008mg/Kg1,1-Dichloroethane 05/02/23 11:110.0050.001<0.001mg/Kg1,2-Dichloroethane 05/02/23 11:110.0050.0007<0.0007mg/Kg1,1-Dichloroethene 05/02/23 11:110.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene 05/02/23 11:110.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene 05/02/23 11:110.0050.0004<0.0004mg/Kg1,2-Dichloropropane 05/02/23 11:110.0050.0006<0.0006mg/Kg1,3-Dichloropropane 05/02/23 11:110.0050.001<0.001mg/Kg2,2-Dichloropropane 05/02/23 11:110.0050.0008<0.0008mg/Kg1,1-Dichloropropene 05/02/23 11:110.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene 05/02/23 11:110.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene 05/02/23 11:110.0050.0006<0.0006mg/KgEthylbenzene 05/02/23 11:110.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE) 05/02/23 11:110.0100.0008<0.0008mg/KgHexachlorobutadiene 05/02/23 11:110.0100.0007<0.0007mg/Kgn-Hexane 05/02/23 11:110.0200.0006<0.0006mg/Kg2-Hexanone 05/02/23 11:110.0050.0005<0.0005mg/KgIsopropylbenzene 05/02/23 11:110.0050.001<0.001mg/Kg4-Isopropyl toluene 05/02/23 11:110.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK) 05/02/23 11:110.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE) 05/02/23 11:110.0200.015<0.015mg/Kg4-Methyl-2-Pentanone 05/02/23 11:110.0100.001<0.001mg/KgMethylene Chloride 05/02/23 11:110.0100.0010<0.0010mg/KgNaphthalene 05/02/23 11:110.0050.0005<0.0005mg/Kgn-Propylbenzene 05/02/23 11:110.0050.001<0.001mg/KgStyrene Page 10 of 18Date:05/10/2023 04:30 PM Page 41 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 8260D V32695QC Analytical Batch(es): Analysis Method: Analysis Description: 5035 QC Prep:V32694 Associated Lab Samples: 95156, 95159 LRB-V32694 Matrix: SOLLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/02/23 11:110.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane 05/02/23 11:110.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane 05/02/23 11:110.0050.0009<0.0009mg/KgTetrachloroethene 05/02/23 11:110.0050.0007<0.0007mg/KgToluene 05/02/23 11:110.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene 05/02/23 11:110.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene 05/02/23 11:110.0050.001<0.001mg/Kg1,1,1-Trichloroethane 05/02/23 11:110.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane 05/02/23 11:110.0050.0009<0.0009mg/KgTrichloroethene 05/02/23 11:110.0100.002<0.002mg/KgTrichlorofluoromethane 05/02/23 11:110.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane 05/02/23 11:110.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene 05/02/23 11:110.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene 05/02/23 11:110.0100.0005<0.0005mg/KgVinyl Acetate 05/02/23 11:110.0100.0005<0.0005mg/KgVinyl Chloride 05/02/23 11:110.0050.0005<0.0005mg/Kgo-Xylene 05/02/23 11:110.0100.001<0.001mg/Kgm,p-Xylene 05/02/23 11:114-Bromofluorobenzene (S)97.8 70-130 05/02/23 11:11Dibromofluoromethane (S)96.6 84-123 05/02/23 11:11Toluene-d8 (S)90.2 76-129 LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 0.105 1051200.1200.100mg/KgAcetone 29-198 13.3 20 0.088 88.090.30.0900.100mg/KgAcrolein 70-130 2.5 20 Page 11 of 18Date:05/10/2023 04:30 PM Page 42 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 8260D V32695QC Analytical Batch(es): Analysis Method: Analysis Description: 5035 QC Prep:V32694 LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 0.101 10197.20.0970.100mg/KgAcrylonitrile 65-134 3.8 20 0.055 1101110.0550.050mg/KgBenzene 74-127 0.7 20 0.044 88.692.80.0460.050mg/KgBromobenzene 73-125 4.6 20 0.059 1201190.0590.050mg/KgBromochloromethane 72-134 1.0 20 0.057 1161160.0580.050mg/KgBromodichloromethane 75-122 0.5 20 0.052 1051060.0530.050mg/KgBromoform 66-135 1.5 20 0.056 11395.00.0470.050mg/KgBromomethane 20-180 17.1 20 0.045 90.695.20.0470.050mg/Kgn-Butylbenzene 65-135 4.9 20 0.044 89.493.40.0460.050mg/Kgsec-Butyl benzene 66-131 4.3 20 0.044 89.293.00.0460.050mg/Kgtert-Butyl benzene 67-132 4.1 20 0.052 1061110.0550.050mg/KgCarbon Disulfide 61-129 4.7 20 0.058 1161180.0590.050mg/KgCarbon Tetrachloride 64-143 1.8 20 0.050 1021040.0520.050mg/KgChlorobenzene 74-118 2.5 20 0.051 1041040.0520.050mg/KgChlorodibromomethane 73-122 0.5 20 0.049 99.81080.0540.050mg/KgChloroethane 33-149 8.2 20 0.056 1141170.0580.050mg/KgChloroform 73-127 2.9 20 0.052 1041040.0520.050mg/KgChloromethane 45-143 0.3 20 0.044 89.893.20.0460.050mg/Kg2-Chlorotoluene 67-124 3.7 20 0.044 89.893.20.0460.050mg/Kg4-Chlorotoluene 71-126 3.7 20 0.054 1091100.0540.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.7 20 0.050 1011020.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.1 20 0.054 1081050.0520.050mg/Kg1,2-Dibromoethane 70-132 2.6 20 0.055 1111170.0580.050mg/KgDibromomethane 74-133 4.5 20 0.046 92.497.40.0480.050mg/Kg1,2-Dichlorobenzene 72-123 5.2 20 0.046 93.495.80.0470.050mg/Kg1,3-Dichlorobenzene 71-120 2.5 20 0.045 91.095.00.0470.050mg/Kg1,4-Dichlorobenzene 71-123 4.3 20 Page 12 of 18Date:05/10/2023 04:30 PM Page 43 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 8260D V32695QC Analytical Batch(es): Analysis Method: Analysis Description: 5035 QC Prep:V32694 LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 0.050 1001040.0510.050mg/KgDichlorodifluoromethane 26-146 3.5 20 0.053 1071130.0560.050mg/Kg1,1-Dichloroethane 74-127 4.7 20 0.053 1061080.0530.050mg/Kg1,2-Dichloroethane 68-128 1.1 20 0.052 1061120.0550.050mg/Kg1,1-Dichloroethene 67-149 5.5 20 0.054 1081090.0540.050mg/Kgcis-1,2-Dichloroethene 76-134 0.9 20 0.052 1061110.0550.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.6 20 0.053 1071130.0560.050mg/Kg1,2-Dichloropropane 73-130 5.2 20 0.051 1021030.0510.050mg/Kg1,3-Dichloropropane 75-124 0.3 20 0.055 1101140.0570.050mg/Kg2,2-Dichloropropane 50-142 3.3 20 0.055 1101160.0580.050mg/Kg1,1-Dichloropropene 71-130 5.4 20 0.057 1151150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 0.3 20 0.059 1181190.0590.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.5 20 0.048 96.898.60.0490.050mg/KgEthylbenzene 74-128 1.8 20 0.107 1071080.1080.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20 0.047 94.81010.0500.050mg/KgHexachlorobutadiene 64-125 6.1 20 0.055 1111250.0620.050mg/Kgn-Hexane 70-130 11.6 20 0.049 98.41220.0610.050mg/Kg2-Hexanone 61-157 21.4*20 0.045 90.494.80.0470.050mg/KgIsopropylbenzene 68-126 4.7 20 0.045 90.695.40.0470.050mg/Kg4-Isopropyl toluene 68-129 5.1 20 0.040 80.499.80.0490.050mg/KgMethyl Ethyl Ketone (MEK)63-149 21.5*20 0.055 1101100.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.3 20 0.058 1161200.0600.050mg/Kg4-Methyl-2-Pentanone 57-162 3.2 20 0.045 91.892.00.0460.050mg/KgMethylene Chloride 74-129 0.2 20 0.046 93.499.20.0490.050mg/KgNaphthalene 57-157 6.0 20 0.044 89.492.40.0460.050mg/Kgn-Propylbenzene 67-130 3.3 20 0.051 1031040.0520.050mg/KgStyrene 77-121 1.3 20 Page 13 of 18* QC Fail Date:05/10/2023 04:30 PM Page 44 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 8260D V32695QC Analytical Batch(es): Analysis Method: Analysis Description: 5035 QC Prep:V32694 LCS-V32694 LCSD-V32694Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 0.050 1011010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.0 20 0.045 90.093.00.0460.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.2 20 0.056 1121160.0570.050mg/KgTetrachloroethene 68-130 3.3 20 0.053 1081080.0540.050mg/KgToluene 71-129 0.7 20 0.047 95.01050.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 10.1 20 0.049 99.41060.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 6.0 20 0.055 1101140.0560.050mg/Kg1,1,1-Trichloroethane 67-131 2.8 20 0.051 1031050.0520.050mg/Kg1,1,2-Trichloroethane 70-133 1.7 20 0.055 1121160.0580.050mg/KgTrichloroethene 75-133 4.2 20 0.042 85.482.00.0410.050mg/KgTrichlorofluoromethane 44-146 4.0 20 0.048 97.694.00.0470.050mg/Kg1,2,3-Trichloropropane 60-137 3.7 20 0.045 90.892.80.0460.050mg/Kg1,2,4-Trimethylbenzene 69-129 2.1 20 0.044 88.493.60.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.7 20 0.058 11897.80.0480.050mg/KgVinyl Acetate 60-140 18.5 20 0.051 1021060.0530.050mg/KgVinyl Chloride 48-147 4.0 20 0.048 96.499.20.0490.050mg/Kgo-Xylene 74-126 2.8 20 0.099 99.31020.1020.100mg/Kgm,p-Xylene 75-124 2.6 20 97.81014-Bromofluorobenzene (S)70-130 10196.2Dibromofluoromethane (S)84-123 90.289.6Toluene-d8 (S)76-129 Page 14 of 18Date:05/10/2023 04:30 PM Page 45 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: EDB and DBCP by Microextraction GC/ECD EPA-504.1 V32736QC Analytical Batch(es): Analysis Method: Analysis Description: EPA-504.1(PREP) QC Prep:V32711 Associated Lab Samples: 95155 LRB-V32711 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits 05/03/23 10:590.02000.00330<0.00330µg/L1,2-Dibromoethane LCS-V32711 LCSD-V32711Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 0.329 132*1290.3220.250µg/L1,2-Dibromoethane 70-130 2.1 20.0 V 94925-DUP-V32711Duplicate Max RPD Parameter AnalyzedRPDDUP Result Result Units 20.0 05/03/23 12:180.9<0.0209< 0.0209µg/L1,2-Dibromoethane V 94924-MS-V32711Matrix Spike MS Result Parameter Max RPD MS %Rec MSD Result MSD Spike Conc. MS Spike Conc.ResultUnits %Rec Limits 0.330 1260.2610.0105µg/L1,2-Dibromoethane 70-130 Page 15 of 18* QC Fail Date:05/10/2023 04:30 PM Page 46 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Massachusetts VPH MADEP-VPH V32651QC Analytical Batch(es): Analysis Method: Analysis Description: MAVPH (Prep) QC Prep:V32650 Associated Lab Samples: 95155 LRB-V32650 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/01/23 13:5850.011.5<11.5µg/LAliphatic C5-C8 05/01/23 13:5850.025.8<25.8µg/LAliphatic C9-C12 05/01/23 13:5850.04.02<4.02µg/LAromatic C9-C10 05/01/23 13:582,5-Dibromotoluene (FID) (S)80.3 70-130 05/01/23 13:582,5-Dibromotoluene (PID) (S)89.2 70-130 LCS-V32650 LCSD-V32650Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 358 119120359300µg/LAliphatic C5-C8 70-130 0.2 50.0 336 112110331300µg/LAliphatic C9-C12 70-130 1.4 50.0 111 111104104100µg/LAromatic C9-C10 70-130 6.5 50.0 98.81022,5-Dibromotoluene (FID) (S)70-130 12096.22,5-Dibromotoluene (PID) (S)70-130 Page 16 of 18Date:05/10/2023 04:30 PM Page 47 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Massachusetts VPH MADEP-VPH V32693QC Analytical Batch(es): Analysis Method: Analysis Description: MAVPH (Prep) QC Prep:V32692 Associated Lab Samples: 95156, 95157, 95158, 95159 LRB-V32692 Matrix: SOLLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/02/23 16:208.001.22<1.22mg/KgAliphatic C5-C8 05/02/23 16:208.004.56<4.56mg/KgAliphatic C9-C12 05/02/23 16:208.000.624<0.624mg/KgAromatic C9-C10 05/02/23 16:202,5-Dibromotoluene (FID) (S)80.8 70-130 05/02/23 16:202,5-Dibromotoluene (PID) (S)112 70-130 LCS-V32692 LCSD-V32692Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 32.1 10097.531.232.0mg/KgAliphatic C5-C8 70-130 2.8 50 35.9 11211035.132.0mg/KgAliphatic C9-C12 70-130 2.2 50 13.1 12212313.210.7mg/KgAromatic C9-C10 70-130 0.7 50 81.677.02,5-Dibromotoluene (FID) (S)70-130 1121122,5-Dibromotoluene (PID) (S)70-130 Page 17 of 18Date:05/10/2023 04:30 PM Page 48 of 51 Quality Control Data 23-121-0003Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner Dry Weight Determination SW-DRYWT V32710QC Analytical Batch: Analysis Method: Analysis Description: V 95156-DUPDuplicate Max RPD Parameter AnalyzedRPDDUP Result Result Units 20.0 05/03/23 10:501.519.319.6%Moisture V 95200-DUPDuplicate Max RPD Parameter AnalyzedRPDDUP Result Result Units 20.0 05/03/23 10:500.921.521.7%Moisture Page 18 of 18Date:05/10/2023 04:30 PM Page 49 of 51 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:23-121-0003 Geological Resources, Inc. 00087 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:IRT15 3.1C Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs ü Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Did not receive containers for moisture for samples MW-1-10' & MW-1-15'. Signature:Angelo Norvell Date & Time:05/01/2023 10:33:04 Special precautions or instructions included? Comments: Page 50 of 51 Pa g e 5 1 o f 5 1 Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. 7/20/2023 Geological Resources, Inc. Joanna Alley 3502 Hayes Road Monroe, NC, 28110 Ref: Analytical Testing Lab Report Number: 23-188-0019 Client Project Description: Handy Corner GRI #6389 Dear Joanna Alley: Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/7/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Page 1 of 52 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202337735State ProgramNorth Carolina 12/31/2023402State ProgramNorth Carolina 07/31/202399012State ProgramSouth Carolina 12/31/202299012State ProgramSouth Carolina Page 1 of 1 00016/23-188-0019 Page 2 of 52 Report Number: Sample Summary Table Client Project Description: 23-188-0019 Handy Corner GRI #6389 Lab No Client Sample ID Matrix Date Collected Date Received 07/05/2023 11:36Aqueous 89040 Trip Blanks 07/07/2023 14:05 07/05/2023 15:04Aqueous 89041 MW-2 07/07/2023 14:05 07/05/2023 15:22Aqueous 89042 MW-3 07/07/2023 14:05 07/05/2023 15:56Aqueous 89043 MW-4 07/07/2023 14:05 Page 3 of 52 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-188-0019 Report Limit Project:Handy Corner V 89041MW-2 0.021 07/12/2023 16:396010DLeadmg/L 0.002 J0.242 07/12/2023 10:326200Bo-Xylene µg/L 0.210 J0.432 07/12/2023 10:326200Bm,p-Xylene µg/L 0.420 J0.674 07/12/2023 10:326200BXylene (Total)µg/L 0.210 V 89042MW-3 0.012 07/12/2023 16:446010DLeadmg/L 0.002 104 07/12/2023 04:366200BAcetoneµg/L 18.0 325 07/12/2023 04:366200BBenzeneµg/L 1.80 J4.32 07/12/2023 04:366200Bn-Butylbenzene µg/L 1.80 J4.09 07/12/2023 04:366200Bsec-Butyl benzene µg/L 2.00 37.7 07/12/2023 04:366200BChloroformµg/L 2.20 14.8 07/12/2023 04:366200BDi-Isopropyl Ether (DIPE)µg/L 5.00 310 07/12/2023 04:366200BEthylbenzeneµg/L 1.70 37.1 07/12/2023 04:366200B2-Hexanone µg/L 3.80 27.1 07/12/2023 04:366200BIsopropylbenzeneµg/L 1.80 J2.61 07/12/2023 04:366200B4-Isopropyl toluene µg/L 0.890 83.1 07/12/2023 04:366200BMethyl Ethyl Ketone (MEK)µg/L 7.10 17.6 07/12/2023 04:366200BMethyl tert-butyl ether (MTBE)µg/L 1.40 41.8 07/12/2023 04:366200B4-Methyl-2-Pentanone µg/L 0.780 35.2 07/12/2023 04:366200BNaphthaleneµg/L 4.70 54.7 07/12/2023 04:366200Bn-Propylbenzene µg/L 1.90 422 07/12/2023 04:366200Btert-Butyl Alcohol (TBA)µg/L 16.0 994 07/12/2023 04:366200Btert-Amyl Alcohol (TAA)µg/L 19.0 788 07/12/2023 04:366200BTolueneµg/L 2.20 471 07/12/2023 04:366200B1,2,4-Trimethylbenzene µg/L 1.90 99.2 07/12/2023 04:366200B1,3,5-Trimethylbenzene µg/L 1.80 859 07/12/2023 04:366200Bo-Xylene µg/L 2.10 3110 07/12/2023 18:286200Bm,p-Xylene µg/L 42.0 3970 07/12/2023 04:366200BXylene (Total)µg/L 2.10 1370 07/10/2023 17:22CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 115 731 07/10/2023 17:22CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 258 1720 07/10/2023 17:22CALCULATIONAromatic C9-C10 (Adjusted)µg/L 40.2 2480 07/10/2023 17:22MADEP-VPH Aliphatic C5-C8 µg/L 115 6730 07/10/2023 17:22MADEP-VPH Aliphatic C9-C12 µg/L 258 1720 07/10/2023 17:22MADEP-VPH Aromatic C9-C10 µg/L 40.2 Page 4 of 52 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-188-0019 Report Limit Project:Handy Corner V 89043MW-4 0.066 07/12/2023 16:486010DLeadmg/L 0.012 J0.451 07/12/2023 01:426200BBenzeneµg/L 0.180 0.765 07/12/2023 01:426200BEthylbenzeneµg/L 0.170 1.84 07/12/2023 01:426200BTolueneµg/L 0.220 0.621 07/12/2023 01:426200B1,2,4-Trimethylbenzene µg/L 0.190 J0.231 07/12/2023 01:426200B1,3,5-Trimethylbenzene µg/L 0.180 1.26 07/12/2023 01:426200Bo-Xylene µg/L 0.210 4.83 07/12/2023 01:426200Bm,p-Xylene µg/L 0.420 6.09 07/12/2023 01:426200BXylene (Total)µg/L 0.210 J29.3 07/10/2023 15:24MADEP-VPH Aliphatic C9-C12 µg/L 25.8 Page 5 of 52 Client: Geological Resources, Inc. CASE NARRATIVE Project: Handy Corner Lab Report Number: 23-188-0019 Date: 7/20/2023 Volatile Organic Compounds - GC/MS Method 6200B Analyte: Ethanol QC Batch No: V35229/V35227 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V35284/V35278 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Page 6 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:Trip Blanks 89040 Matrix: 7/5/2023 11:36 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35227 07/11/23 08:00 <1.80 µg/L 1.80 10.0Acetone 1 07/11/23 13:41 V35229TBL <0.180 µg/L 0.180 0.500Benzene 1 07/11/23 13:41 V35229TBL <0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 13:41 V35229TBL <0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 13:41 V35229TBL <0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 13:41 V35229TBL <1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 13:41 V35229TBL <0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 13:41 V35229TBL <0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 13:41 V35229TBL <0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 13:41 V35229TBL <0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 13:41 V35229TBL <0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 13:41 V35229TBL <0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 13:41 V35229TBL <0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 13:41 V35229TBL <0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 13:41 V35229TBL <0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 13:41 V35229TBL <0.220 µg/L 0.220 0.500Chloromethane 1 07/11/23 13:41 V35229TBL <0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 13:41 V35229TBL <0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 13:41 V35229TBL <0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/11/23 13:41 V35229TBL <1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 13:41 V35229TBL <0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 13:41 V35229TBL <0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 13:41 V35229TBL <0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 13:41 V35229TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 7 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:Trip Blanks 89040 Matrix: 7/5/2023 11:36 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35227 07/11/23 08:00 <0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 13:41 V35229TBL <0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 13:41 V35229TBL <1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 13:41 V35229TBL <0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 13:41 V35229TBL <0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 13:41 V35229TBL <0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 13:41 V35229TBL <0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 13:41 V35229TBL <0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 13:41 V35229TBL <0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 13:41 V35229TBL <0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 13:41 V35229TBL <0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 13:41 V35229TBL <0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 13:41 V35229TBL <0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 13:41 V35229TBL <0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 13:41 V35229TBL <42.0 µg/L 42.0 200Ethanol 1 07/11/23 13:41 V35229TBL <0.170 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 13:41 V35229TBL <0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 13:41 V35229TBL <0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 13:41 V35229TBL <0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 13:41 V35229TBL <0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 13:41 V35229TBL <0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 13:41 V35229TBL <0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 13:41 V35229TBL <0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 13:41 V35229TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 8 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:Trip Blanks 89040 Matrix: 7/5/2023 11:36 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35227 07/11/23 08:00 <0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 13:41 V35229TBL <0.470 µg/L 0.470 1.00Naphthalene 1 07/11/23 13:41 V35229TBL <0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 13:41 V35229TBL <0.220 µg/L 0.220 0.500Styrene 1 07/11/23 13:41 V35229TBL <0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 13:41 V35229TBL <0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 13:41 V35229TBL <0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 13:41 V35229TBL <0.220 µg/L 0.220 0.500Toluene 1 07/11/23 13:41 V35229TBL <0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 13:41 V35229TBL <0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 13:41 V35229TBL <0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 13:41 V35229TBL <0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 13:41 V35229TBL <0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 13:41 V35229TBL <0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 13:41 V35229TBL <0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 13:41 V35229TBL <0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 13:41 V35229TBL <0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 13:41 V35229TBL <1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 13:41 V35229TBL <0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 13:41 V35229TBL <0.210 µg/L 0.210 0.500o-Xylene 1 07/11/23 13:41 V35229TBL <0.420 µg/L 0.420 1.00m,p-Xylene 1 07/11/23 13:41 V35229TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 9 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:Trip Blanks 89040 Matrix: 7/5/2023 11:36 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35227 07/11/23 08:00 <0.21 µg/L 0.210 0.500Xylene (Total)1 07/11/23 13:41 V35229 Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/11/23 13:411 TBL V35229 Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%07/11/23 13:411 TBL V35229 Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%07/11/23 13:411 TBL V35229 Surrogate: Toluene-d8 92.6 Limits: 70-130%07/11/23 13:411 TBL V35229 Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 10 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-2 89041 Matrix: 7/5/2023 15:04 Aqueous Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/12/23 10:32 6200BENM 0.021 mg/L 0.002 0.006Lead 1 07/12/23 16:39 6010DJKC Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 11 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-2 89041 Matrix: 7/5/2023 15:04 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35278 07/11/23 09:00 <1.80 µg/L 1.80 10.0Acetone 1 07/12/23 10:32 V35284ENM <0.180 µg/L 0.180 0.500Benzene 1 07/12/23 10:32 V35284ENM <0.210 µg/L 0.210 0.500Bromobenzene 1 07/12/23 10:32 V35284ENM <0.420 µg/L 0.420 1.00Bromochloromethane 1 07/12/23 10:32 V35284ENM <0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/12/23 10:32 V35284ENM <1.50 µg/L 1.50 5.00Bromoform 1 07/12/23 10:32 V35284ENM <0.280 µg/L 0.280 1.00Bromomethane 1 07/12/23 10:32 V35284ENM <0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/12/23 10:32 V35284ENM <0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/12/23 10:32 V35284ENM <0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/12/23 10:32 V35284ENM <0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/12/23 10:32 V35284ENM <0.190 µg/L 0.190 0.500Chlorobenzene 1 07/12/23 10:32 V35284ENM <0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/12/23 10:32 V35284ENM <0.430 µg/L 0.430 1.00Chloroethane 1 07/12/23 10:32 V35284ENM <0.220 µg/L 0.220 0.500Chloroform 1 07/12/23 10:32 V35284ENM <0.220 µg/L 0.220 0.500Chloromethane 1 07/12/23 10:32 V35284ENM <0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/12/23 10:32 V35284ENM <0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/12/23 10:32 V35284ENM <0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/12/23 10:32 V35284ENM <1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/12/23 10:32 V35284ENM <0.230 µg/L 0.230 0.500Dibromomethane 1 07/12/23 10:32 V35284ENM <0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/12/23 10:32 V35284ENM <0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/12/23 10:32 V35284ENM Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 12 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-2 89041 Matrix: 7/5/2023 15:04 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35278 07/11/23 09:00 <0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/12/23 10:32 V35284ENM <1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/12/23 10:32 V35284ENM <0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/12/23 10:32 V35284ENM <0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/12/23 10:32 V35284ENM <0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/12/23 10:32 V35284ENM <0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/12/23 10:32 V35284ENM <0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/12/23 10:32 V35284ENM <0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/12/23 10:32 V35284ENM <0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/12/23 10:32 V35284ENM <0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/12/23 10:32 V35284ENM <0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/12/23 10:32 V35284ENM <0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/12/23 10:32 V35284ENM <0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/12/23 10:32 V35284ENM <42.0 µg/L 42.0 200Ethanol 1 07/12/23 10:32 V35284ENM <0.170 µg/L 0.170 0.500Ethylbenzene 1 07/12/23 10:32 V35284ENM <0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/12/23 10:32 V35284ENM <0.380 µg/L 0.380 1.002-Hexanone 1 07/12/23 10:32 V35284ENM <0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/12/23 10:32 V35284ENM <0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/12/23 10:32 V35284ENM <0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/12/23 10:32 V35284ENM <0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/12/23 10:32 V35284ENM <0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/12/23 10:32 V35284ENM <0.330 µg/L 0.330 2.00Methylene Chloride 1 07/12/23 10:32 V35284ENM Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 13 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-2 89041 Matrix: 7/5/2023 15:04 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35278 07/11/23 09:00 <0.470 µg/L 0.470 1.00Naphthalene 1 07/12/23 10:32 V35284ENM <0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/12/23 10:32 V35284ENM <0.220 µg/L 0.220 0.500Styrene 1 07/12/23 10:32 V35284ENM <1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/12/23 10:32 V35284ENM <0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/12/23 10:32 V35284ENM <1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/12/23 10:32 V35284ENM <0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/12/23 10:32 V35284ENM <0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/12/23 10:32 V35284ENM <0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/12/23 10:32 V35284ENM <0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/12/23 10:32 V35284ENM <0.220 µg/L 0.220 0.500Toluene 1 07/12/23 10:32 V35284ENM <0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/12/23 10:32 V35284ENM <0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/12/23 10:32 V35284ENM <0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/12/23 10:32 V35284ENM <0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/12/23 10:32 V35284ENM <0.180 µg/L 0.180 0.500Trichloroethene 1 07/12/23 10:32 V35284ENM <0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/12/23 10:32 V35284ENM <0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/12/23 10:32 V35284ENM <0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/12/23 10:32 V35284ENM <0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/12/23 10:32 V35284ENM <1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/12/23 10:32 V35284ENM <0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/12/23 10:32 V35284ENM 0.242 J µg/L 0.210 0.500o-Xylene 1 07/12/23 10:32 V35284ENM Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 14 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-2 89041 Matrix: 7/5/2023 15:04 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35278 07/11/23 09:00 0.432 J µg/L 0.420 1.00m,p-Xylene 1 07/12/23 10:32 V35284ENM 0.674 J µg/L 0.210 0.500Xylene (Total)1 07/12/23 10:32 V35284KCC Surrogate: 4-Bromofluorobenzene 92.0 Limits: 70-130%07/12/23 10:321 ENM V35284 Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%07/12/23 10:321 ENM V35284 Surrogate: 1,2-Dichloroethane - d4 92.2 Limits: 70-130%07/12/23 10:321 ENM V35284 Surrogate: Toluene-d8 91.4 Limits: 70-130%07/12/23 10:321 ENM V35284 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF EPA-504.1(PREP) EPA-504.1 Prep Batch(es):V35162 07/11/23 09:46 <0.00343 µg/L 0.00343 0.02081,2-Dibromoethane 1 07/11/23 14:09 V35214TJW Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 15 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-2 89041 Matrix: 7/5/2023 15:04 Aqueous Analytical Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF CALCULATION <11.5 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 07/10/23 15:01 <25.8 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 07/10/23 15:01 <4.02 µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 07/10/23 15:01 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF MAVPH (Prep) MADEP-VPH Prep Batch(es):V35150 07/10/23 08:00 <11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 07/10/23 15:01 V35151TBL <25.8 µg/L 25.8 50.0Aliphatic C9-C12 1 07/10/23 15:01 V35151TBL <4.02 µg/L 4.02 50.0Aromatic C9-C10 1 07/10/23 15:01 V35151TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)83.0 Limits: 70-130%07/10/23 15:011 TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)100 Limits: 70-130%07/10/23 15:011 TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 16 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-3 89042 Matrix: 7/5/2023 15:22 Aqueous Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF <10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 07/12/23 04:36 6200BTBL 0.012 mg/L 0.002 0.006Lead 1 07/12/23 16:44 6010DJKC Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 17 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-3 89042 Matrix: 7/5/2023 15:22 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35234 07/11/23 08:00 V35302 07/12/23 09:00 104 µg/L 18.0 100Acetone 10 07/12/23 04:36 V35235TBL 325 µg/L 1.80 5.00Benzene 10 07/12/23 04:36 V35235TBL <2.10 µg/L 2.10 5.00Bromobenzene 10 07/12/23 04:36 V35235TBL <4.20 µg/L 4.20 10.0Bromochloromethane 10 07/12/23 04:36 V35235TBL <1.60 µg/L 1.60 5.00Bromodichloromethane 10 07/12/23 04:36 V35235TBL <15.0 µg/L 15.0 50.0Bromoform 10 07/12/23 04:36 V35235TBL <2.80 µg/L 2.80 10.0Bromomethane 10 07/12/23 04:36 V35235TBL 4.32 J µg/L 1.80 5.00n-Butylbenzene 10 07/12/23 04:36 V35235TBL 4.09 J µg/L 2.00 5.00sec-Butyl benzene 10 07/12/23 04:36 V35235TBL <9.20 µg/L 9.20 20.0tert-Butyl benzene 10 07/12/23 04:36 V35235TBL <1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 07/12/23 04:36 V35235TBL <1.90 µg/L 1.90 5.00Chlorobenzene 10 07/12/23 04:36 V35235TBL <1.90 µg/L 1.90 5.00Chlorodibromomethane 10 07/12/23 04:36 V35235TBL <4.30 µg/L 4.30 10.0Chloroethane 10 07/12/23 04:36 V35235TBL 37.7 µg/L 2.20 5.00Chloroform 10 07/12/23 04:36 V35235TBL <2.20 µg/L 2.20 5.00Chloromethane 10 07/12/23 04:36 V35235TBL <2.00 µg/L 2.00 5.002-Chlorotoluene 10 07/12/23 04:36 V35235TBL <2.00 µg/L 2.00 5.004-Chlorotoluene 10 07/12/23 04:36 V35235TBL 14.8 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 07/12/23 04:36 V35235TBL <11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 07/12/23 04:36 V35235TBL <2.30 µg/L 2.30 5.00Dibromomethane 10 07/12/23 04:36 V35235TBL <2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 07/12/23 04:36 V35235TBL <1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 07/12/23 04:36 V35235TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 18 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-3 89042 Matrix: 7/5/2023 15:22 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35234 07/11/23 08:00 V35302 07/12/23 09:00 <2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 07/12/23 04:36 V35235TBL <12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 07/12/23 04:36 V35235TBL <2.40 µg/L 2.40 5.001,1-Dichloroethane 10 07/12/23 04:36 V35235TBL <1.50 µg/L 1.50 5.001,2-Dichloroethane 10 07/12/23 04:36 V35235TBL <1.50 µg/L 1.50 5.001,1-Dichloroethene 10 07/12/23 04:36 V35235TBL <2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 07/12/23 04:36 V35235TBL <1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 07/12/23 04:36 V35235TBL <1.90 µg/L 1.90 5.001,2-Dichloropropane 10 07/12/23 04:36 V35235TBL <1.30 µg/L 1.30 5.001,3-Dichloropropane 10 07/12/23 04:36 V35235TBL <2.10 µg/L 2.10 20.02,2-Dichloropropane 10 07/12/23 04:36 V35235TBL <2.00 µg/L 2.00 5.001,1-Dichloropropene 10 07/12/23 04:36 V35235TBL <2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 07/12/23 04:36 V35235TBL <1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 07/12/23 04:36 V35235TBL <420 µg/L 420 2000Ethanol 10 07/12/23 04:36 V35235TBL 310 µg/L 1.70 5.00Ethylbenzene 10 07/12/23 04:36 V35235TBL <3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 07/12/23 04:36 V35235TBL 37.1 µg/L 3.80 10.02-Hexanone 10 07/12/23 04:36 V35235TBL 27.1 µg/L 1.80 5.00Isopropylbenzene 10 07/12/23 04:36 V35235TBL 2.61 J µg/L 0.890 5.004-Isopropyl toluene 10 07/12/23 04:36 V35235TBL 83.1 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 07/12/23 04:36 V35235TBL 17.6 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 07/12/23 04:36 V35235TBL 41.8 µg/L 0.780 10.04-Methyl-2-Pentanone 10 07/12/23 04:36 V35235TBL <3.30 µg/L 3.30 20.0Methylene Chloride 10 07/12/23 04:36 V35235TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 19 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-3 89042 Matrix: 7/5/2023 15:22 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35234 07/11/23 08:00 V35302 07/12/23 09:00 35.2 µg/L 4.70 10.0Naphthalene 10 07/12/23 04:36 V35235TBL 54.7 µg/L 1.90 5.00n-Propylbenzene 10 07/12/23 04:36 V35235TBL <2.20 µg/L 2.20 5.00Styrene 10 07/12/23 04:36 V35235TBL 422 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 07/12/23 04:36 V35235TBL <3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 07/12/23 04:36 V35235TBL 994 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 07/12/23 04:36 V35235TBL <2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 07/12/23 04:36 V35235TBL <1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 07/12/23 04:36 V35235TBL <1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 07/12/23 04:36 V35235TBL <2.20 µg/L 2.20 5.00Tetrachloroethene 10 07/12/23 04:36 V35235TBL 788 µg/L 2.20 5.00Toluene 10 07/12/23 04:36 V35235TBL <3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 07/12/23 04:36 V35235TBL <3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 07/12/23 04:36 V35235TBL <1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 07/12/23 04:36 V35235TBL <0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 07/12/23 04:36 V35235TBL <1.80 µg/L 1.80 5.00Trichloroethene 10 07/12/23 04:36 V35235TBL <1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 07/12/23 04:36 V35235TBL <2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 07/12/23 04:36 V35235TBL 471 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 07/12/23 04:36 V35235TBL 99.2 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 07/12/23 04:36 V35235TBL <10.0 µg/L 10.0 50.0Vinyl Acetate 10 07/12/23 04:36 V35235TBL <1.70 µg/L 1.70 5.00Vinyl Chloride 10 07/12/23 04:36 V35235TBL 859 µg/L 2.10 5.00o-Xylene 10 07/12/23 04:36 V35235TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 20 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-3 89042 Matrix: 7/5/2023 15:22 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35234 07/11/23 08:00 V35302 07/12/23 09:00 3110 µg/L 42.0 100m,p-Xylene 100 07/12/23 18:28 V35303MSA 3970 µg/L 2.10 5.00Xylene (Total)10 07/12/23 04:36 V35303 Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/12/23 04:3610 TBL V35235 Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%07/12/23 04:3610 TBL V35235 Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%07/12/23 04:3610 TBL V35235 Surrogate: Toluene-d8 90.6 Limits: 70-130%07/12/23 04:3610 TBL V35235 Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%07/12/23 18:28100 MSA V35303 Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%07/12/23 18:28100 MSA V35303 Surrogate: 1,2-Dichloroethane - d4 99.8 Limits: 70-130%07/12/23 18:28100 MSA V35303 Surrogate: Toluene-d8 91.2 Limits: 70-130%07/12/23 18:28100 MSA V35303 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF EPA-504.1(PREP) EPA-504.1 Prep Batch(es):V35162 07/11/23 09:46 <0.00338 µg/L 0.00338 0.02051,2-Dibromoethane 1 07/11/23 14:29 V35214TJW Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 21 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-3 89042 Matrix: 7/5/2023 15:22 Aqueous Analytical Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF CALCULATION 1370 µg/L 115 500Aliphatic C5-C8 (Adjusted)10 07/10/23 17:22 731 µg/L 258 500Aliphatics C9-C12 (Adjusted)10 07/10/23 17:22 1720 µg/L 40.2 500Aromatic C9-C10 (Adjusted)10 07/10/23 17:22 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF MAVPH (Prep) MADEP-VPH Prep Batch(es):V35150 07/10/23 08:00 2480 µg/L 115 500Aliphatic C5-C8 10 07/10/23 17:22 V35151TBL 6730 µg/L 258 500Aliphatic C9-C12 10 07/10/23 17:22 V35151TBL 1720 µg/L 40.2 500Aromatic C9-C10 10 07/10/23 17:22 V35151TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)90.9 Limits: 70-130%07/10/23 17:2210 TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)110 Limits: 70-130%07/10/23 17:2210 TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 22 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-4 89043 Matrix: 7/5/2023 15:56 Aqueous Test Results Units MDL MQL By Analytical Method Date / Time Analyzed DF <1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/12/23 01:42 6200BTBL 0.066 mg/L 0.012 0.030Lead 5 07/12/23 16:48 6010DJKC Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 23 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-4 89043 Matrix: 7/5/2023 15:56 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35234 07/11/23 08:00 <1.80 µg/L 1.80 10.0Acetone 1 07/12/23 01:42 V35235TBL 0.451 J µg/L 0.180 0.500Benzene 1 07/12/23 01:42 V35235TBL <0.210 µg/L 0.210 0.500Bromobenzene 1 07/12/23 01:42 V35235TBL <0.420 µg/L 0.420 1.00Bromochloromethane 1 07/12/23 01:42 V35235TBL <0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/12/23 01:42 V35235TBL <1.50 µg/L 1.50 5.00Bromoform 1 07/12/23 01:42 V35235TBL <0.280 µg/L 0.280 1.00Bromomethane 1 07/12/23 01:42 V35235TBL <0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/12/23 01:42 V35235TBL <0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/12/23 01:42 V35235TBL <0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/12/23 01:42 V35235TBL <0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/12/23 01:42 V35235TBL <0.190 µg/L 0.190 0.500Chlorobenzene 1 07/12/23 01:42 V35235TBL <0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/12/23 01:42 V35235TBL <0.430 µg/L 0.430 1.00Chloroethane 1 07/12/23 01:42 V35235TBL <0.220 µg/L 0.220 0.500Chloroform 1 07/12/23 01:42 V35235TBL <0.220 µg/L 0.220 0.500Chloromethane 1 07/12/23 01:42 V35235TBL <0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/12/23 01:42 V35235TBL <0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/12/23 01:42 V35235TBL <0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/12/23 01:42 V35235TBL <1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/12/23 01:42 V35235TBL <0.230 µg/L 0.230 0.500Dibromomethane 1 07/12/23 01:42 V35235TBL <0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/12/23 01:42 V35235TBL <0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/12/23 01:42 V35235TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 24 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-4 89043 Matrix: 7/5/2023 15:56 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35234 07/11/23 08:00 <0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/12/23 01:42 V35235TBL <1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/12/23 01:42 V35235TBL <0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/12/23 01:42 V35235TBL <0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/12/23 01:42 V35235TBL <0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/12/23 01:42 V35235TBL <0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/12/23 01:42 V35235TBL <0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/12/23 01:42 V35235TBL <0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/12/23 01:42 V35235TBL <0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/12/23 01:42 V35235TBL <0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/12/23 01:42 V35235TBL <0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/12/23 01:42 V35235TBL <0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/12/23 01:42 V35235TBL <0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/12/23 01:42 V35235TBL <42.0 µg/L 42.0 200Ethanol 1 07/12/23 01:42 V35235TBL 0.765 µg/L 0.170 0.500Ethylbenzene 1 07/12/23 01:42 V35235TBL <0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/12/23 01:42 V35235TBL <0.380 µg/L 0.380 1.002-Hexanone 1 07/12/23 01:42 V35235TBL <0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/12/23 01:42 V35235TBL <0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/12/23 01:42 V35235TBL <0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/12/23 01:42 V35235TBL <0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/12/23 01:42 V35235TBL <0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/12/23 01:42 V35235TBL <0.330 µg/L 0.330 2.00Methylene Chloride 1 07/12/23 01:42 V35235TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 25 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-4 89043 Matrix: 7/5/2023 15:56 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35234 07/11/23 08:00 <0.470 µg/L 0.470 1.00Naphthalene 1 07/12/23 01:42 V35235TBL <0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/12/23 01:42 V35235TBL <0.220 µg/L 0.220 0.500Styrene 1 07/12/23 01:42 V35235TBL <1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/12/23 01:42 V35235TBL <0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/12/23 01:42 V35235TBL <1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/12/23 01:42 V35235TBL <0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/12/23 01:42 V35235TBL <0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/12/23 01:42 V35235TBL <0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/12/23 01:42 V35235TBL <0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/12/23 01:42 V35235TBL 1.84 µg/L 0.220 0.500Toluene 1 07/12/23 01:42 V35235TBL <0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/12/23 01:42 V35235TBL <0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/12/23 01:42 V35235TBL <0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/12/23 01:42 V35235TBL <0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/12/23 01:42 V35235TBL <0.180 µg/L 0.180 0.500Trichloroethene 1 07/12/23 01:42 V35235TBL <0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/12/23 01:42 V35235TBL <0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/12/23 01:42 V35235TBL 0.621 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/12/23 01:42 V35235TBL 0.231 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/12/23 01:42 V35235TBL <1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/12/23 01:42 V35235TBL <0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/12/23 01:42 V35235TBL 1.26 µg/L 0.210 0.500o-Xylene 1 07/12/23 01:42 V35235TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 26 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-4 89043 Matrix: 7/5/2023 15:56 Aqueous Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF 6200 PT 6200B Prep Batch(es):V35234 07/11/23 08:00 4.83 µg/L 0.420 1.00m,p-Xylene 1 07/12/23 01:42 V35235TBL 6.09 µg/L 0.210 0.500Xylene (Total)1 07/12/23 01:42 V35235KCC Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%07/12/23 01:421 TBL V35235 Surrogate: Dibromofluoromethane 95.6 Limits: 70-130%07/12/23 01:421 TBL V35235 Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%07/12/23 01:421 TBL V35235 Surrogate: Toluene-d8 92.4 Limits: 70-130%07/12/23 01:421 TBL V35235 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF EPA-504.1(PREP) EPA-504.1 Prep Batch(es):V35162 07/11/23 09:46 <0.00347 µg/L 0.00347 0.02101,2-Dibromoethane 1 07/11/23 14:50 V35214TJW Qualifiers/ Definitions Estimated valueJDilution FactorDF Method Quantitation LimitMQL Page 27 of 52 , REPORT OF ANALYSISReport Number : Project Information : NC 28110 23-188-0019 00087 Geological Resources, Inc. 3502 Hayes Road Joanna Alley Monroe Danyale Love Project Manager GRI #6389 Received : 07/07/2023 Handy Corner Report Date : 07/20/2023 Sample ID : Lab No : Sampled:MW-4 89043 Matrix: 7/5/2023 15:56 Aqueous Analytical Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF CALCULATION <11.5 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 07/10/23 15:24 <25.8 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 07/10/23 15:24 <4.02 µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 07/10/23 15:24 Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF MAVPH (Prep) MADEP-VPH Prep Batch(es):V35150 07/10/23 08:00 <11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 07/10/23 15:24 V35151TBL 29.3 J µg/L 25.8 50.0Aliphatic C9-C12 1 07/10/23 15:24 V35151TBL <4.02 µg/L 4.02 50.0Aromatic C9-C10 1 07/10/23 15:24 V35151TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)87.7 Limits: 70-130%07/10/23 15:241 TBL MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)110 Limits: 70-130%07/10/23 15:241 TBL Qualifiers/ Definitions Estimated valueJDilution FactorDF Page 28 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Metals Analysis 6010D V35283QC Analytical Batch(es): Analysis Method: Analysis Description: 3005A QC Prep:V35160 Associated Lab Samples: 89041, 89042, 89043 LRB-V35160 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits 07/12/23 16:310.0060.002<0.002mg/LLead LCS-V35160Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 1150.1150.100mg/LLead 80-120 V 89048-MS-V35160 V 89048-MSD-V35160Matrix Spike & Matrix Spike Duplicate MS Result Parameter Max RPD MS %Rec MSD Result MSD Spike Conc. MS Spike Conc.ResultUnits %Rec Limits MSD %Rec RPD 0.112 1120.1140.1000.100< 0.002mg/LLead 114 75-125 1.7 20.0 V 89048-PDS-V35160Post Digestion Spike Parameter Analyzed% Recovery PDS ResultUnits 07/12/23 17:191060.264mg/LLead Page 1 of 22Date:07/20/2023 11:37 AM Page 29 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35229QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35227 Associated Lab Samples: 89040 LRB-V35227 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/11/23 12:5210.01.80<1.80µg/LAcetone 07/11/23 12:520.5000.180<0.180µg/LBenzene 07/11/23 12:520.5000.210<0.210µg/LBromobenzene 07/11/23 12:521.000.420<0.420µg/LBromochloromethane 07/11/23 12:520.5000.160<0.160µg/LBromodichloromethane 07/11/23 12:525.001.50<1.50µg/LBromoform 07/11/23 12:521.000.280<0.280µg/LBromomethane 07/11/23 12:520.5000.180<0.180µg/Ln-Butylbenzene 07/11/23 12:520.5000.200<0.200µg/Lsec-Butyl benzene 07/11/23 12:522.000.920<0.920µg/Ltert-Butyl benzene 07/11/23 12:520.5000.180<0.180µg/LCarbon Tetrachloride 07/11/23 12:520.5000.190<0.190µg/LChlorobenzene 07/11/23 12:520.5000.190<0.190µg/LChlorodibromomethane 07/11/23 12:521.000.430<0.430µg/LChloroethane 07/11/23 12:520.5000.220<0.220µg/LChloroform 07/11/23 12:520.5000.220<0.220µg/LChloromethane 07/11/23 12:520.5000.200<0.200µg/L2-Chlorotoluene 07/11/23 12:520.5000.200<0.200µg/L4-Chlorotoluene 07/11/23 12:520.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE) 07/11/23 12:522.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane 07/11/23 12:520.5000.200<0.200µg/L1,2-Dibromoethane 07/11/23 12:520.5000.230<0.230µg/LDibromomethane 07/11/23 12:520.5000.220<0.220µg/L1,2-Dichlorobenzene 07/11/23 12:520.5000.190<0.190µg/L1,3-Dichlorobenzene 07/11/23 12:520.5000.210<0.210µg/L1,4-Dichlorobenzene 07/11/23 12:525.001.20<1.20µg/LDichlorodifluoromethane 07/11/23 12:520.5000.240<0.240µg/L1,1-Dichloroethane Page 2 of 22Date:07/20/2023 11:37 AM Page 30 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35229QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35227 Associated Lab Samples: 89040 LRB-V35227 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/11/23 12:520.5000.150<0.150µg/L1,2-Dichloroethane 07/11/23 12:520.5000.150<0.150µg/L1,1-Dichloroethene 07/11/23 12:520.5000.200<0.200µg/Lcis-1,2-Dichloroethene 07/11/23 12:520.5000.180<0.180µg/Ltrans-1,2-Dichloroethene 07/11/23 12:520.5000.190<0.190µg/L1,2-Dichloropropane 07/11/23 12:520.5000.130<0.130µg/L1,3-Dichloropropane 07/11/23 12:522.000.210<0.210µg/L2,2-Dichloropropane 07/11/23 12:520.5000.200<0.200µg/L1,1-Dichloropropene 07/11/23 12:520.5000.210<0.210µg/Lcis-1,3-Dichloropropene 07/11/23 12:520.5000.150<0.150µg/Ltrans-1,3-Dichloropropene 07/11/23 12:5220042.0<42.0µg/LEthanol 07/11/23 12:520.5000.170<0.170µg/LEthylbenzene 07/11/23 12:523.000.350<0.350µg/LHexachlorobutadiene 07/11/23 12:521.000.380<0.380µg/L2-Hexanone 07/11/23 12:520.5000.180<0.180µg/LIsopropylbenzene 07/11/23 12:520.5000.089<0.089µg/L4-Isopropyl toluene 07/11/23 12:525.000.710<0.710µg/LMethyl Ethyl Ketone (MEK) 07/11/23 12:521.000.140<0.140µg/LMethyl tert-butyl ether (MTBE) 07/11/23 12:521.000.078<0.078µg/L4-Methyl-2-Pentanone 07/11/23 12:522.000.330<0.330µg/LMethylene Chloride 07/11/23 12:521.000.470<0.470µg/LNaphthalene 07/11/23 12:520.5000.190<0.190µg/Ln-Propylbenzene 07/11/23 12:520.5000.220<0.220µg/LStyrene 07/11/23 12:520.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane 07/11/23 12:520.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane 07/11/23 12:520.5000.220<0.220µg/LTetrachloroethene 07/11/23 12:520.5000.220<0.220µg/LToluene Page 3 of 22Date:07/20/2023 11:37 AM Page 31 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35229QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35227 Associated Lab Samples: 89040 LRB-V35227 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/11/23 12:520.5000.380<0.380µg/L1,2,3-Trichlorobenzene 07/11/23 12:520.5000.310<0.310µg/L1,2,4-Trichlorobenzene 07/11/23 12:520.5000.160<0.160µg/L1,1,1-Trichloroethane 07/11/23 12:520.5000.096<0.096µg/L1,1,2-Trichloroethane 07/11/23 12:520.5000.180<0.180µg/LTrichloroethene 07/11/23 12:520.5000.180<0.180µg/LTrichlorofluoromethane 07/11/23 12:520.5000.270<0.270µg/L1,2,3-Trichloropropane 07/11/23 12:520.5000.190<0.190µg/L1,2,4-Trimethylbenzene 07/11/23 12:520.5000.180<0.180µg/L1,3,5-Trimethylbenzene 07/11/23 12:525.001.00<1.00µg/LVinyl Acetate 07/11/23 12:520.5000.170<0.170µg/LVinyl Chloride 07/11/23 12:520.5000.210<0.210µg/Lo-Xylene 07/11/23 12:521.000.420<0.420µg/Lm,p-Xylene 07/11/23 12:524-Bromofluorobenzene (S)101 70-130 07/11/23 12:52Dibromofluoromethane (S)95.4 70-130 07/11/23 12:521,2-Dichloroethane - d4 (S)98.6 70-130 07/11/23 12:52Toluene-d8 (S)92.4 70-130 LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 29.3 73.272.028.840.0µg/LAcetone 40-160 1.7 20.0 21.9 11011122.120.0µg/LBenzene 70-130 0.9 20.0 20.3 10210521.020.0µg/LBromobenzene 70-130 3.3 20.0 22.5 11311322.520.0µg/LBromochloromethane 70-130 0.0 20.0 22.8 11411623.120.0µg/LBromodichloromethane 70-130 1.3 20.0 Page 4 of 22Date:07/20/2023 11:37 AM Page 32 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35229QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35227 LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 21.1 10610521.020.0µg/LBromoform 70-130 0.4 20.0 16.8 84.077.515.520.0µg/LBromomethane 60-140 8.0 20.0 21.1 10610921.720.0µg/Ln-Butylbenzene 70-130 2.8 20.0 21.1 10611021.920.0µg/Lsec-Butyl benzene 70-130 3.7 20.0 20.9 10510821.620.0µg/Ltert-Butyl benzene 70-130 3.2 20.0 22.1 11111322.520.0µg/LCarbon Tetrachloride 70-130 1.7 20.0 21.2 10610721.420.0µg/LChlorobenzene 70-130 0.9 20.0 21.1 10610621.220.0µg/LChlorodibromomethane 70-130 0.4 20.0 21.8 10910721.420.0µg/LChloroethane 60-140 1.8 20.0 22.2 11111022.020.0µg/LChloroform 70-130 0.9 20.0 19.3 96.591.018.220.0µg/LChloromethane 60-140 5.8 20.0 21.5 10811022.020.0µg/L2-Chlorotoluene 70-130 2.2 20.0 20.8 10410621.220.0µg/L4-Chlorotoluene 70-130 1.9 20.0 22.4 11211222.320.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.4 20.0 18.7 93.593.018.620.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.5 20.0 21.3 10710420.820.0µg/L1,2-Dibromoethane 70-130 2.3 20.0 23.0 11511422.720.0µg/LDibromomethane 70-130 1.3 20.0 20.1 10110320.620.0µg/L1,2-Dichlorobenzene 70-130 2.4 20.0 20.3 10210420.720.0µg/L1,3-Dichlorobenzene 70-130 1.9 20.0 19.9 99.510320.620.0µg/L1,4-Dichlorobenzene 70-130 3.4 20.0 19.5 97.599.019.820.0µg/LDichlorodifluoromethane 60-140 1.5 20.0 22.4 11211222.420.0µg/L1,1-Dichloroethane 70-130 0.0 20.0 22.9 11511623.120.0µg/L1,2-Dichloroethane 70-130 0.8 20.0 22.5 11311523.020.0µg/L1,1-Dichloroethene 70-130 2.1 20.0 22.8 11411623.220.0µg/Lcis-1,2-Dichloroethene 70-130 1.7 20.0 22.8 11411422.720.0µg/Ltrans-1,2-Dichloroethene 70-130 0.4 20.0 Page 5 of 22Date:07/20/2023 11:37 AM Page 33 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35229QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35227 LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 22.8 11411422.820.0µg/L1,2-Dichloropropane 70-130 0.0 20.0 20.5 10310320.620.0µg/L1,3-Dichloropropane 70-130 0.4 20.0 23.4 11712124.120.0µg/L2,2-Dichloropropane 70-130 2.9 20.0 22.2 11111422.720.0µg/L1,1-Dichloropropene 70-130 2.2 20.0 22.5 11311522.920.0µg/Lcis-1,3-Dichloropropene 70-130 1.7 20.0 23.3 11711623.220.0µg/Ltrans-1,3-Dichloropropene 70-130 0.4 20.0 658 132106532500µg/LEthanol 60-140 21.1*20.0 21.1 10610921.720.0µg/LEthylbenzene 70-130 2.8 20.0 20.4 10210821.620.0µg/LHexachlorobutadiene 70-130 5.7 20.0 18.1 90.591.018.220.0µg/L2-Hexanone 60-140 0.5 20.0 21.1 10610921.820.0µg/LIsopropylbenzene 70-130 3.2 20.0 21.2 10611021.920.0µg/L4-Isopropyl toluene 70-130 3.2 20.0 17.3 86.579.515.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 8.4 20.0 21.2 10610520.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.4 20.0 22.9 11511322.520.0µg/L4-Methyl-2-Pentanone 60-140 1.7 20.0 23.4 11711522.920.0µg/LMethylene Chloride 70-130 2.1 20.0 19.3 96.597.519.520.0µg/LNaphthalene 70-130 1.0 20.0 21.5 10811222.320.0µg/Ln-Propylbenzene 70-130 3.6 20.0 21.6 10810621.120.0µg/LStyrene 70-130 2.3 20.0 20.7 10410721.320.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.8 20.0 19.5 97.510020.020.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.5 20.0 21.0 10510821.520.0µg/LTetrachloroethene 70-130 2.3 20.0 22.4 11211422.820.0µg/LToluene 70-130 1.7 20.0 21.5 10810921.820.0µg/L1,2,3-Trichlorobenzene 70-130 1.3 20.0 19.5 97.510220.420.0µg/L1,2,4-Trichlorobenzene 70-130 4.5 20.0 22.6 11311522.920.0µg/L1,1,1-Trichloroethane 70-130 1.3 20.0 Page 6 of 22* QC Fail Date:07/20/2023 11:37 AM Page 34 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35229QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35227 LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 22.6 11311523.020.0µg/L1,1,2-Trichloroethane 70-130 1.7 20.0 21.8 10911122.220.0µg/LTrichloroethene 70-130 1.8 20.0 21.5 10810921.820.0µg/LTrichlorofluoromethane 60-140 1.3 20.0 20.5 10310420.820.0µg/L1,2,3-Trichloropropane 70-130 1.4 20.0 20.9 10510821.620.0µg/L1,2,4-Trimethylbenzene 70-130 3.2 20.0 21.2 10610921.820.0µg/L1,3,5-Trimethylbenzene 70-130 2.7 20.0 23.3 11711823.620.0µg/LVinyl Acetate 60-140 1.2 20.0 20.2 10110420.820.0µg/LVinyl Chloride 60-140 2.9 20.0 21.7 10911122.120.0µg/Lo-Xylene 70-130 1.8 20.0 45.8 11511646.540.0µg/Lm,p-Xylene 70-130 1.5 20.0 1011024-Bromofluorobenzene (S)70-130 96.095.4Dibromofluoromethane (S)70-130 1021021,2-Dichloroethane - d4 (S)70-130 92.893.2Toluene-d8 (S)70-130 Page 7 of 22Date:07/20/2023 11:37 AM Page 35 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35235QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35234 Associated Lab Samples: 89042, 89043 LRB-V35234 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/12/23 01:1710.01.80<1.80µg/LAcetone 07/12/23 01:170.5000.180<0.180µg/LBenzene 07/12/23 01:170.5000.210<0.210µg/LBromobenzene 07/12/23 01:171.000.420<0.420µg/LBromochloromethane 07/12/23 01:170.5000.160<0.160µg/LBromodichloromethane 07/12/23 01:175.001.50<1.50µg/LBromoform 07/12/23 01:171.000.280<0.280µg/LBromomethane 07/12/23 01:170.5000.180<0.180µg/Ln-Butylbenzene 07/12/23 01:170.5000.200<0.200µg/Lsec-Butyl benzene 07/12/23 01:172.000.920<0.920µg/Ltert-Butyl benzene 07/12/23 01:170.5000.180<0.180µg/LCarbon Tetrachloride 07/12/23 01:170.5000.190<0.190µg/LChlorobenzene 07/12/23 01:170.5000.190<0.190µg/LChlorodibromomethane 07/12/23 01:171.000.430<0.430µg/LChloroethane 07/12/23 01:170.5000.220<0.220µg/LChloroform 07/12/23 01:170.5000.220<0.220µg/LChloromethane 07/12/23 01:170.5000.200<0.200µg/L2-Chlorotoluene 07/12/23 01:170.5000.200<0.200µg/L4-Chlorotoluene 07/12/23 01:170.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE) 07/12/23 01:172.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane 07/12/23 01:170.5000.230<0.230µg/LDibromomethane 07/12/23 01:170.5000.220<0.220µg/L1,2-Dichlorobenzene 07/12/23 01:170.5000.190<0.190µg/L1,3-Dichlorobenzene 07/12/23 01:170.5000.210<0.210µg/L1,4-Dichlorobenzene 07/12/23 01:175.001.20<1.20µg/LDichlorodifluoromethane 07/12/23 01:170.5000.240<0.240µg/L1,1-Dichloroethane 07/12/23 01:170.5000.150<0.150µg/L1,2-Dichloroethane Page 8 of 22Date:07/20/2023 11:37 AM Page 36 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35235QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35234 Associated Lab Samples: 89042, 89043 LRB-V35234 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/12/23 01:170.5000.150<0.150µg/L1,1-Dichloroethene 07/12/23 01:170.5000.200<0.200µg/Lcis-1,2-Dichloroethene 07/12/23 01:170.5000.180<0.180µg/Ltrans-1,2-Dichloroethene 07/12/23 01:170.5000.190<0.190µg/L1,2-Dichloropropane 07/12/23 01:170.5000.130<0.130µg/L1,3-Dichloropropane 07/12/23 01:172.000.210<0.210µg/L2,2-Dichloropropane 07/12/23 01:170.5000.200<0.200µg/L1,1-Dichloropropene 07/12/23 01:170.5000.210<0.210µg/Lcis-1,3-Dichloropropene 07/12/23 01:170.5000.150<0.150µg/Ltrans-1,3-Dichloropropene 07/12/23 01:1720042.0<42.0µg/LEthanol 07/12/23 01:170.5000.170<0.170µg/LEthylbenzene 07/12/23 01:173.000.350<0.350µg/LHexachlorobutadiene 07/12/23 01:171.000.380<0.380µg/L2-Hexanone 07/12/23 01:170.5000.180<0.180µg/LIsopropylbenzene 07/12/23 01:170.5000.089<0.089µg/L4-Isopropyl toluene 07/12/23 01:175.000.710<0.710µg/LMethyl Ethyl Ketone (MEK) 07/12/23 01:171.000.140<0.140µg/LMethyl tert-butyl ether (MTBE) 07/12/23 01:171.000.078<0.078µg/L4-Methyl-2-Pentanone 07/12/23 01:172.000.330<0.330µg/LMethylene Chloride 07/12/23 01:171.000.470<0.470µg/LNaphthalene 07/12/23 01:170.5000.190<0.190µg/Ln-Propylbenzene 07/12/23 01:170.5000.220<0.220µg/LStyrene 07/12/23 01:1710.01.60<1.60µg/Ltert-Butyl Alcohol (TBA) 07/12/23 01:1710.00.350<0.350µg/Ltert-Butyl formate (TBF) 07/12/23 01:1710.01.90<1.90µg/Ltert-Amyl Alcohol (TAA) 07/12/23 01:1710.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME) 07/12/23 01:170.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane Page 9 of 22Date:07/20/2023 11:37 AM Page 37 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35235QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35234 Associated Lab Samples: 89042, 89043 LRB-V35234 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/12/23 01:170.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane 07/12/23 01:170.5000.220<0.220µg/LTetrachloroethene 07/12/23 01:170.5000.220<0.220µg/LToluene 07/12/23 01:170.5000.380<0.380µg/L1,2,3-Trichlorobenzene 07/12/23 01:170.5000.310<0.310µg/L1,2,4-Trichlorobenzene 07/12/23 01:170.5000.160<0.160µg/L1,1,1-Trichloroethane 07/12/23 01:170.5000.096<0.096µg/L1,1,2-Trichloroethane 07/12/23 01:170.5000.180<0.180µg/LTrichloroethene 07/12/23 01:170.5000.180<0.180µg/LTrichlorofluoromethane 07/12/23 01:170.5000.270<0.270µg/L1,2,3-Trichloropropane 07/12/23 01:170.5000.190<0.190µg/L1,2,4-Trimethylbenzene 07/12/23 01:170.5000.180<0.180µg/L1,3,5-Trimethylbenzene 07/12/23 01:175.001.00<1.00µg/LVinyl Acetate 07/12/23 01:170.5000.170<0.170µg/LVinyl Chloride 07/12/23 01:170.5000.210<0.210µg/Lo-Xylene 07/12/23 01:171.000.420<0.420µg/Lm,p-Xylene 07/12/23 01:1710.01.00<1.00µg/L3,3-Dimethyl-1-butanol 07/12/23 01:174-Bromofluorobenzene (S)103 70-130 07/12/23 01:17Dibromofluoromethane (S)96.8 70-130 07/12/23 01:171,2-Dichloroethane - d4 (S)102 70-130 07/12/23 01:17Toluene-d8 (S)91.6 70-130 LCS-V35234 LCSD-V35234Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 33.4 83.582.533.040.0µg/LAcetone 40-160 1.2 20.0 Page 10 of 22Date:07/20/2023 11:37 AM Page 38 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35235QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35234 LCS-V35234 LCSD-V35234Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 22.1 11110721.420.0µg/LBenzene 70-130 3.2 20.0 20.0 10099.519.920.0µg/LBromobenzene 70-130 0.5 20.0 23.0 11511122.120.0µg/LBromochloromethane 70-130 3.9 20.0 23.2 11611422.820.0µg/LBromodichloromethane 70-130 1.7 20.0 21.2 10610621.220.0µg/LBromoform 70-130 0.0 20.0 15.8 79.080.516.120.0µg/LBromomethane 60-140 1.8 20.0 20.3 10210020.020.0µg/Ln-Butylbenzene 70-130 1.4 20.0 20.7 10410220.320.0µg/Lsec-Butyl benzene 70-130 1.9 20.0 20.7 10410220.320.0µg/Ltert-Butyl benzene 70-130 1.9 20.0 22.3 11210821.620.0µg/LCarbon Tetrachloride 70-130 3.1 20.0 21.3 10710320.620.0µg/LChlorobenzene 70-130 3.3 20.0 21.2 10610721.320.0µg/LChlorodibromomethane 70-130 0.4 20.0 21.0 10510420.820.0µg/LChloroethane 60-140 0.9 20.0 22.3 11210921.720.0µg/LChloroform 70-130 2.7 20.0 18.9 94.588.017.620.0µg/LChloromethane 60-140 7.1 20.0 21.2 10610420.820.0µg/L2-Chlorotoluene 70-130 1.9 20.0 20.5 10310020.020.0µg/L4-Chlorotoluene 70-130 2.4 20.0 22.4 11211122.120.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.3 20.0 19.5 97.599.519.920.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.0 20.0 22.7 11411723.320.0µg/LDibromomethane 70-130 2.6 20.0 19.9 99.599.019.820.0µg/L1,2-Dichlorobenzene 70-130 0.5 20.0 20.1 10198.019.620.0µg/L1,3-Dichlorobenzene 70-130 2.5 20.0 19.8 99.097.519.520.0µg/L1,4-Dichlorobenzene 70-130 1.5 20.0 20.1 10196.519.320.0µg/LDichlorodifluoromethane 60-140 4.0 20.0 22.3 11210721.320.0µg/L1,1-Dichloroethane 70-130 4.5 20.0 23.4 11711422.720.0µg/L1,2-Dichloroethane 70-130 3.0 20.0 Page 11 of 22Date:07/20/2023 11:37 AM Page 39 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35235QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35234 LCS-V35234 LCSD-V35234Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 22.5 11311022.020.0µg/L1,1-Dichloroethene 70-130 2.2 20.0 23.3 11711122.220.0µg/Lcis-1,2-Dichloroethene 70-130 4.8 20.0 22.5 11310821.620.0µg/Ltrans-1,2-Dichloroethene 70-130 4.0 20.0 22.7 11411022.020.0µg/L1,2-Dichloropropane 70-130 3.1 20.0 20.6 10310420.820.0µg/L1,3-Dichloropropane 70-130 0.9 20.0 20.0 10095.019.020.0µg/L2,2-Dichloropropane 70-130 5.1 20.0 22.5 11310821.620.0µg/L1,1-Dichloropropene 70-130 4.0 20.0 22.4 11211021.920.0µg/Lcis-1,3-Dichloropropene 70-130 2.2 20.0 23.0 11511522.920.0µg/Ltrans-1,3-Dichloropropene 70-130 0.4 20.0 676 135134669500µg/LEthanol 60-140 1.0 20.0 21.1 10610420.720.0µg/LEthylbenzene 70-130 1.9 20.0 20.1 10110120.120.0µg/LHexachlorobutadiene 70-130 0.0 20.0 19.2 96.096.019.220.0µg/L2-Hexanone 60-140 0.0 20.0 20.9 10510220.420.0µg/LIsopropylbenzene 70-130 2.4 20.0 20.9 10510220.320.0µg/L4-Isopropyl toluene 70-130 2.9 20.0 17.5 87.582.516.520.0µg/LMethyl Ethyl Ketone (MEK)60-140 5.8 20.0 21.6 10810721.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.3 20.0 23.8 11911723.420.0µg/L4-Methyl-2-Pentanone 60-140 1.6 20.0 23.3 11711322.620.0µg/LMethylene Chloride 70-130 3.0 20.0 20.9 10510821.620.0µg/LNaphthalene 70-130 3.2 20.0 21.1 10610320.520.0µg/Ln-Propylbenzene 70-130 2.8 20.0 20.8 10410220.420.0µg/LStyrene 70-130 1.9 20.0 54.5 13613955.540.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.8 20.0 35.3 88.294.537.840.0µg/Ltert-Butyl formate (TBF)40-140 6.8 20.0 24.9 12512825.520.0µg/Ltert-Amyl Alcohol (TAA)40-140 2.3 20.0 44.1 11010943.440.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.6 20.0 Page 12 of 22Date:07/20/2023 11:37 AM Page 40 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35235QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35234 LCS-V35234 LCSD-V35234Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 21.0 10510420.720.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.4 20.0 18.5 92.595.019.020.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.6 20.0 21.2 10610120.120.0µg/LTetrachloroethene 70-130 5.3 20.0 22.6 11311222.320.0µg/LToluene 70-130 1.3 20.0 25.4 12712525.020.0µg/L1,2,3-Trichlorobenzene 70-130 1.5 20.0 20.5 10310320.520.0µg/L1,2,4-Trichlorobenzene 70-130 0.0 20.0 22.5 11311222.320.0µg/L1,1,1-Trichloroethane 70-130 0.8 20.0 23.5 11811523.020.0µg/L1,1,2-Trichloroethane 70-130 2.1 20.0 23.4 11711022.020.0µg/LTrichloroethene 70-130 6.1 20.0 22.6 11310921.720.0µg/LTrichlorofluoromethane 60-140 4.0 20.0 21.2 10610520.920.0µg/L1,2,3-Trichloropropane 70-130 1.4 20.0 20.7 10410220.420.0µg/L1,2,4-Trimethylbenzene 70-130 1.4 20.0 20.7 10410220.320.0µg/L1,3,5-Trimethylbenzene 70-130 1.9 20.0 16.8 84.092.018.420.0µg/LVinyl Acetate 60-140 9.0 20.0 20.9 10510120.220.0µg/LVinyl Chloride 60-140 3.4 20.0 21.8 10910721.320.0µg/Lo-Xylene 70-130 2.3 20.0 45.8 11511244.740.0µg/Lm,p-Xylene 70-130 2.4 20.0 23.0 11511523.020.0µg/L3,3-Dimethyl-1-butanol 70-130 0.0 20.0 1011024-Bromofluorobenzene (S)70-130 96.895.8Dibromofluoromethane (S)70-130 1041041,2-Dichloroethane - d4 (S)70-130 92.093.8Toluene-d8 (S)70-130 Page 13 of 22Date:07/20/2023 11:37 AM Page 41 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35284QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35278 Associated Lab Samples: 89041 LRB-V35278 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/12/23 04:0510.01.80<1.80µg/LAcetone 07/12/23 04:050.5000.180<0.180µg/LBenzene 07/12/23 04:050.5000.210<0.210µg/LBromobenzene 07/12/23 04:051.000.420<0.420µg/LBromochloromethane 07/12/23 04:050.5000.160<0.160µg/LBromodichloromethane 07/12/23 04:055.001.50<1.50µg/LBromoform 07/12/23 04:051.000.280<0.280µg/LBromomethane 07/12/23 04:050.5000.180<0.180µg/Ln-Butylbenzene 07/12/23 04:050.5000.200<0.200µg/Lsec-Butyl benzene 07/12/23 04:052.000.920<0.920µg/Ltert-Butyl benzene 07/12/23 04:050.5000.180<0.180µg/LCarbon Tetrachloride 07/12/23 04:050.5000.190<0.190µg/LChlorobenzene 07/12/23 04:050.5000.190<0.190µg/LChlorodibromomethane 07/12/23 04:051.000.430<0.430µg/LChloroethane 07/12/23 04:050.5000.220<0.220µg/LChloroform 07/12/23 04:050.5000.220<0.220µg/LChloromethane 07/12/23 04:050.5000.200<0.200µg/L2-Chlorotoluene 07/12/23 04:050.5000.200<0.200µg/L4-Chlorotoluene 07/12/23 04:050.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE) 07/12/23 04:052.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane 07/12/23 04:050.5000.230<0.230µg/LDibromomethane 07/12/23 04:050.5000.220<0.220µg/L1,2-Dichlorobenzene 07/12/23 04:050.5000.190<0.190µg/L1,3-Dichlorobenzene 07/12/23 04:050.5000.210<0.210µg/L1,4-Dichlorobenzene 07/12/23 04:055.001.20<1.20µg/LDichlorodifluoromethane 07/12/23 04:050.5000.240<0.240µg/L1,1-Dichloroethane 07/12/23 04:050.5000.150<0.150µg/L1,2-Dichloroethane Page 14 of 22Date:07/20/2023 11:37 AM Page 42 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35284QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35278 Associated Lab Samples: 89041 LRB-V35278 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/12/23 04:050.5000.150<0.150µg/L1,1-Dichloroethene 07/12/23 04:050.5000.200<0.200µg/Lcis-1,2-Dichloroethene 07/12/23 04:050.5000.180<0.180µg/Ltrans-1,2-Dichloroethene 07/12/23 04:050.5000.190<0.190µg/L1,2-Dichloropropane 07/12/23 04:050.5000.130<0.130µg/L1,3-Dichloropropane 07/12/23 04:052.000.210<0.210µg/L2,2-Dichloropropane 07/12/23 04:050.5000.200<0.200µg/L1,1-Dichloropropene 07/12/23 04:050.5000.210<0.210µg/Lcis-1,3-Dichloropropene 07/12/23 04:050.5000.150<0.150µg/Ltrans-1,3-Dichloropropene 07/12/23 04:0520042.0<42.0µg/LEthanol 07/12/23 04:050.5000.170<0.170µg/LEthylbenzene 07/12/23 04:053.000.350<0.350µg/LHexachlorobutadiene 07/12/23 04:051.000.380<0.380µg/L2-Hexanone 07/12/23 04:050.5000.180<0.180µg/LIsopropylbenzene 07/12/23 04:050.5000.089<0.089µg/L4-Isopropyl toluene 07/12/23 04:055.000.710<0.710µg/LMethyl Ethyl Ketone (MEK) 07/12/23 04:051.000.140<0.140µg/LMethyl tert-butyl ether (MTBE) 07/12/23 04:051.000.078<0.078µg/L4-Methyl-2-Pentanone 07/12/23 04:052.000.330<0.330µg/LMethylene Chloride 07/12/23 04:051.000.470<0.470µg/LNaphthalene 07/12/23 04:050.5000.190<0.190µg/Ln-Propylbenzene 07/12/23 04:050.5000.220<0.220µg/LStyrene 07/12/23 04:0510.01.60<1.60µg/Ltert-Butyl Alcohol (TBA) 07/12/23 04:0510.00.350<0.350µg/Ltert-Butyl formate (TBF) 07/12/23 04:0510.01.90<1.90µg/Ltert-Amyl Alcohol (TAA) 07/12/23 04:0510.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME) 07/12/23 04:050.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane Page 15 of 22Date:07/20/2023 11:37 AM Page 43 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35284QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35278 Associated Lab Samples: 89041 LRB-V35278 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/12/23 04:050.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane 07/12/23 04:050.5000.220<0.220µg/LTetrachloroethene 07/12/23 04:050.5000.220<0.220µg/LToluene 07/12/23 04:050.5000.380<0.380µg/L1,2,3-Trichlorobenzene 07/12/23 04:050.5000.310<0.310µg/L1,2,4-Trichlorobenzene 07/12/23 04:050.5000.160<0.160µg/L1,1,1-Trichloroethane 07/12/23 04:050.5000.096<0.096µg/L1,1,2-Trichloroethane 07/12/23 04:050.5000.180<0.180µg/LTrichloroethene 07/12/23 04:050.5000.180<0.180µg/LTrichlorofluoromethane 07/12/23 04:050.5000.270<0.270µg/L1,2,3-Trichloropropane 07/12/23 04:050.5000.190<0.190µg/L1,2,4-Trimethylbenzene 07/12/23 04:050.5000.180<0.180µg/L1,3,5-Trimethylbenzene 07/12/23 04:055.001.00<1.00µg/LVinyl Acetate 07/12/23 04:050.5000.170<0.170µg/LVinyl Chloride 07/12/23 04:050.5000.210<0.210µg/Lo-Xylene 07/12/23 04:051.000.420<0.420µg/Lm,p-Xylene 07/12/23 04:0510.01.00<1.00µg/L3,3-Dimethyl-1-butanol 07/12/23 04:054-Bromofluorobenzene (S)93.6 70-130 07/12/23 04:05Dibromofluoromethane (S)97.4 70-130 07/12/23 04:051,2-Dichloroethane - d4 (S)92.6 70-130 07/12/23 04:05Toluene-d8 (S)91.8 70-130 LCS-V35278 LCSD-V35278Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 36.5 91.292.737.140.0µg/LAcetone 40-160 1.6 20.0 Page 16 of 22Date:07/20/2023 11:37 AM Page 44 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35284QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35278 LCS-V35278 LCSD-V35278Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 19.8 99.010020.020.0µg/LBenzene 70-130 1.0 20.0 17.4 87.087.517.520.0µg/LBromobenzene 70-130 0.5 20.0 20.7 10410521.020.0µg/LBromochloromethane 70-130 1.4 20.0 19.1 95.597.519.520.0µg/LBromodichloromethane 70-130 2.0 20.0 18.6 93.096.019.220.0µg/LBromoform 70-130 3.1 20.0 17.4 87.084.016.820.0µg/LBromomethane 60-140 3.5 20.0 17.8 89.088.017.620.0µg/Ln-Butylbenzene 70-130 1.1 20.0 17.4 87.087.017.420.0µg/Lsec-Butyl benzene 70-130 0.0 20.0 18.0 90.091.018.220.0µg/Ltert-Butyl benzene 70-130 1.1 20.0 19.4 97.098.519.720.0µg/LCarbon Tetrachloride 70-130 1.5 20.0 19.7 98.599.019.820.0µg/LChlorobenzene 70-130 0.5 20.0 18.3 91.596.519.320.0µg/LChlorodibromomethane 70-130 5.3 20.0 20.6 10310621.220.0µg/LChloroethane 60-140 2.8 20.0 19.6 98.098.019.620.0µg/LChloroform 70-130 0.0 20.0 16.2 81.077.515.520.0µg/LChloromethane 60-140 4.4 20.0 17.3 86.585.517.120.0µg/L2-Chlorotoluene 70-130 1.1 20.0 17.0 85.084.516.920.0µg/L4-Chlorotoluene 70-130 0.5 20.0 17.8 89.088.517.720.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.5 20.0 17.8 89.088.517.720.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.5 20.0 20.0 10099.019.820.0µg/LDibromomethane 70-130 1.0 20.0 18.9 94.595.519.120.0µg/L1,2-Dichlorobenzene 70-130 1.0 20.0 19.2 96.095.019.020.0µg/L1,3-Dichlorobenzene 70-130 1.0 20.0 18.3 91.593.518.720.0µg/L1,4-Dichlorobenzene 70-130 2.1 20.0 19.3 96.593.518.720.0µg/LDichlorodifluoromethane 60-140 3.1 20.0 19.3 96.595.519.120.0µg/L1,1-Dichloroethane 70-130 1.0 20.0 19.5 97.597.519.520.0µg/L1,2-Dichloroethane 70-130 0.0 20.0 Page 17 of 22Date:07/20/2023 11:37 AM Page 45 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35284QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35278 LCS-V35278 LCSD-V35278Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 19.4 97.010020.020.0µg/L1,1-Dichloroethene 70-130 3.0 20.0 18.7 93.594.518.920.0µg/Lcis-1,2-Dichloroethene 70-130 1.0 20.0 19.7 98.597.519.520.0µg/Ltrans-1,2-Dichloroethene 70-130 1.0 20.0 19.1 95.597.519.520.0µg/L1,2-Dichloropropane 70-130 2.0 20.0 18.3 91.592.518.520.0µg/L1,3-Dichloropropane 70-130 1.0 20.0 16.9 84.584.516.920.0µg/L2,2-Dichloropropane 70-130 0.0 20.0 20.7 10410521.020.0µg/L1,1-Dichloropropene 70-130 1.4 20.0 18.4 92.095.019.020.0µg/Lcis-1,3-Dichloropropene 70-130 3.2 20.0 18.5 92.590.518.120.0µg/Ltrans-1,3-Dichloropropene 70-130 2.1 20.0 537 10788.6443500µg/LEthanol 60-140 19.1 20.0 17.9 89.591.518.320.0µg/LEthylbenzene 70-130 2.2 20.0 19.2 96.098.519.720.0µg/LHexachlorobutadiene 70-130 2.5 20.0 14.5 72.576.015.220.0µg/L2-Hexanone 60-140 4.7 20.0 18.0 90.089.517.920.0µg/LIsopropylbenzene 70-130 0.5 20.0 18.3 91.590.518.120.0µg/L4-Isopropyl toluene 70-130 1.0 20.0 17.1 85.576.015.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 11.7 20.0 19.7 98.597.019.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.5 20.0 16.0 80.081.016.220.0µg/L4-Methyl-2-Pentanone 60-140 1.2 20.0 19.3 96.596.519.320.0µg/LMethylene Chloride 70-130 0.0 20.0 14.7 73.571.014.220.0µg/LNaphthalene 70-130 3.4 20.0 17.5 87.587.017.420.0µg/Ln-Propylbenzene 70-130 0.5 20.0 18.7 93.597.019.420.0µg/LStyrene 70-130 3.6 20.0 28.4 71.073.529.440.0µg/Ltert-Butyl Alcohol (TBA)40-140 3.4 20.0 35.1 87.792.737.140.0µg/Ltert-Butyl formate (TBF)40-140 5.5 20.0 20.2 10189.017.820.0µg/Ltert-Amyl Alcohol (TAA)40-140 12.6 20.0 39.2 98.098.039.240.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.0 20.0 Page 18 of 22Date:07/20/2023 11:37 AM Page 46 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35284QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35278 LCS-V35278 LCSD-V35278Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 19.2 96.096.019.220.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.0 20.0 17.1 85.586.517.320.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.1 20.0 19.7 98.510120.120.0µg/LTetrachloroethene 70-130 2.0 20.0 19.4 97.096.519.320.0µg/LToluene 70-130 0.5 20.0 19.4 97.099.519.920.0µg/L1,2,3-Trichlorobenzene 70-130 2.5 20.0 20.4 10210120.120.0µg/L1,2,4-Trichlorobenzene 70-130 1.4 20.0 20.1 10110220.320.0µg/L1,1,1-Trichloroethane 70-130 0.9 20.0 20.6 10310220.320.0µg/L1,1,2-Trichloroethane 70-130 1.4 20.0 21.4 10710721.420.0µg/LTrichloroethene 70-130 0.0 20.0 21.4 10710621.120.0µg/LTrichlorofluoromethane 60-140 1.4 20.0 18.2 91.084.516.920.0µg/L1,2,3-Trichloropropane 70-130 7.4 20.0 18.0 90.089.017.820.0µg/L1,2,4-Trimethylbenzene 70-130 1.1 20.0 18.0 90.089.017.820.0µg/L1,3,5-Trimethylbenzene 70-130 1.1 20.0 16.1 80.592.018.420.0µg/LVinyl Acetate 60-140 13.3 20.0 19.2 96.098.519.720.0µg/LVinyl Chloride 60-140 2.5 20.0 18.4 92.093.018.620.0µg/Lo-Xylene 70-130 1.0 20.0 39.0 97.598.239.340.0µg/Lm,p-Xylene 70-130 0.7 20.0 15.5 77.511322.620.0µg/L3,3-Dimethyl-1-butanol 70-130 37.2*20.0 91.891.44-Bromofluorobenzene (S)70-130 96.496.4Dibromofluoromethane (S)70-130 93.093.61,2-Dichloroethane - d4 (S)70-130 92.293.0Toluene-d8 (S)70-130 Page 19 of 22* QC Fail Date:07/20/2023 11:37 AM Page 47 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Volatile Organic Compounds - GC/MS 6200B V35303QC Analytical Batch(es): Analysis Method: Analysis Description: 6200 PT QC Prep:V35302 Associated Lab Samples: 89042 LRB-V35302 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/12/23 15:351.000.420<0.420µg/Lm,p-Xylene 07/12/23 15:354-Bromofluorobenzene (S)102 70-130 07/12/23 15:35Dibromofluoromethane (S)94.8 70-130 07/12/23 15:351,2-Dichloroethane - d4 (S)98.0 70-130 07/12/23 15:35Toluene-d8 (S)91.6 70-130 LCS-V35302 LCSD-V35302Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 44.8 11211445.740.0µg/Lm,p-Xylene 70-130 1.9 20.0 1031034-Bromofluorobenzene (S)70-130 95.095.6Dibromofluoromethane (S)70-130 1011031,2-Dichloroethane - d4 (S)70-130 92.491.6Toluene-d8 (S)70-130 Page 20 of 22Date:07/20/2023 11:37 AM Page 48 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: EDB and DBCP by Microextraction GC/ECD EPA-504.1 V35214QC Analytical Batch(es): Analysis Method: Analysis Description: EPA-504.1(PREP) QC Prep:V35162 Associated Lab Samples: 89041, 89042, 89043 LRB-V35162 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits 07/11/23 10:060.02000.00330<0.00330µg/L1,2-Dibromoethane LCS-V35162 LCSD-V35162Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 0.271 10899.60.2490.250µg/L1,2-Dibromoethane 70-130 8.4 20.0 V 89021-DUP-V35162Duplicate Max RPD Parameter AnalyzedRPDDUP Result Result Units 20.0 07/11/23 12:180.016.416.4µg/L1,2-Dibromoethane V 89006-MS-V35162Matrix Spike MS Result Parameter Max RPD MS %Rec MSD Result MSD Spike Conc. MS Spike Conc.ResultUnits %Rec Limits 0.312 1200.261< 0.00345µg/L1,2-Dibromoethane 70-130 Page 21 of 22Date:07/20/2023 11:37 AM Page 49 of 52 Quality Control Data 23-188-0019Report No: Project Description: Client ID:Geological Resources, Inc. Handy Corner QC Prep Batch Method: Massachusetts VPH MADEP-VPH V35151QC Analytical Batch(es): Analysis Method: Analysis Description: MAVPH (Prep) QC Prep:V35150 Associated Lab Samples: 89041, 89042, 89043 LRB-V35150 Matrix: AQULab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 07/10/23 14:3750.011.5<11.5µg/LAliphatic C5-C8 07/10/23 14:3750.025.8<25.8µg/LAliphatic C9-C12 07/10/23 14:3750.04.02<4.02µg/LAromatic C9-C10 07/10/23 14:372,5-Dibromotoluene (FID) (S)83.9 70-130 07/10/23 14:372,5-Dibromotoluene (PID) (S)88.3 70-130 LCS-V35150 LCSD-V35150Laboratory Control Sample & LCSD LCSD ResultParameter Max RPD LCSD % Rec LCS %Rec LCS Result Spike Conc.Units % Rec Limits RPD 262 87.387.0261300µg/LAliphatic C5-C8 70-130 0.3 50.0 348 116116347300µg/LAliphatic C9-C12 70-130 0.2 50.0 119 119117117100µg/LAromatic C9-C10 70-130 1.6 50.0 82.877.72,5-Dibromotoluene (FID) (S)70-130 98.088.22,5-Dibromotoluene (PID) (S)70-130 Page 22 of 22Date:07/20/2023 11:37 AM Page 50 of 52 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:23-188-0019 Geological Resources, Inc. 00087 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:IRT15 3.3C Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)? Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Signature:Angelo Norvell Date & Time:07/07/2023 18:21:30 Special precautions or instructions included? Comments: Page 51 of 52 Pa g e 5 2 o f 5 2