MO-29861_49044_CA_LSA_20230929

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
October 2, 2023

Mr. Ryan Mills
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Limited Site Assessment Report
Yogi Foods
3005 Wilkesboro Highway
Statesville, Iredell County
North Carolina
Facility ID Number: 0-029113
Incident Number: 49044
GRI Project Number: 6473

Dear Mr. Mills,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Xavier Farmer at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Ashokkumar D. Mavani; Bhavani Statesville, LLC, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Limited Site Assessment Report
Yogi Foods
3005 Wilkesboro Hwy
Statesville, Iredell County
North Carolina 28625
Facility ID Number: 0-029113
Incident Number: 49044
GRI Project Number: 6473

Prepared for:

Mr. Ashokkumar D. Mavani
Bhavani Statesville, LLC
124 Quail Springs Road
Statesville, North Carolina 28611

September 29, 2023

Xavier T. Farmer, G.I.T.
Project Manager
Samuel L. McKay III, P.G.
Report Reviewer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
ii
EXECUTIVE SUMMARY
The Yogi Foods site is located at 3005 Wilkesboro Hwy in Statesville, Iredell County, North Carolina. The
property operates as a petroleum retail facility and convenience store. The site is covered by concrete,
asphalt, and grass. There is one 8,000-gallon gasoline UST, two 6,000-gallon gasoline USTs, one 8,000-
gallon diesel UST, one 1,000-gallon kerosene UST, and one 1,000-gallon off-road diesel UST currently in
use at the site with eight associated dispenser islands. One 8,000-gallon gasoline UST, two 6,000-gallon
gasoline USTs, and one 8,000-gallon diesel UST were removed from the site in August 1994.

On May 23, 2023, the previous consultant, Paragon Environmental Consultants, Inc. (Paragon) conducted
a site check at the site which included the installation of 15 soil borings in the vicinity of the UST system
components. A monitoring well, MW-1, was also installed on May 23, 2023. A ground water sample
collected from MW-1 on May 24, 2023, exhibited concentrations of benzene, MTBE, and EDB that
exceeded the MACs. The concentration of EDB exceeded ten times the 2L standard.

A receptor survey was conducted by GRI personnel on June 26, 2023. Nine water supply wells (WSW-1
through WSW-9) were identified within a 1,500-foot radius of the site. Three of the wells, WSW-3, WSW-
5 and WSW-8 are located within 1,000-feet of the source area and are used for potable sources of water.
WSW-1 and WSW-2 are inactive. WSW-4, WSW-6, WSW-7 and WSW-9 are located beyond 1,000 feet of
the source area and are used for potable and non-potable sources of water. With the exception of Weston
Road, public water is available to the subject site and to all surrounding properties.

Three (3) additional North Carolina Type II monitoring wells (MW-2 through MW-4) were installed at the
site by GRI personnel on August 28, 2023. Soil samples were collected at five-foot intervals during the
installation of the monitoring wells. A concentration of MTBE that exceeded the soil-to-ground water
MSCC was reported in the soil sample, MW-4-15’. Concentrations of benzo(a)anthracene,
benzo(b)fluoranthene and benzo(a)pyrene that exceeded the MSCCs were reported in the soil sample
collected MW-3-5’. None of the detectable concentrations exceeded the Residential MSCCs.

Ground water samples were collected from existing monitoring well, MW-1 and the newly installed
monitoring wells, MW-2 through MW-4 on August 28, 2023. Due to limited sample volumes in the
monitoring wells, GRI returned to the site on September 5, 2023 and September 7, 2023 to fill additional
sampling containers with ground water from MW-1, MW-2 and MW-4. Estimated and/or detectable
concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, isopropylbenzene, n-
propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, TAA, TBA, 1-methynaphthalene, 2-
methylnaphthalene, EDB, lead, C5-C8 aliphatics, C9-C12 aliphatics and C9-C22 aromatics that exceeded
the MACs were reported were reported in the ground water samples collected from MW-1, MW-2 and/or
MW-4. A concentration of lead that exceeded the MAC was reported in MW-1, MW-3, and MW-4. None
of the concentrations exceed the GCLs.

Based on this information, the site risk should be characterized as high, and a CSA should be completed.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
iii
SITE INFORMATION
1. Site Identification
 Yogi Foods (Facility ID 0-029113)
 Incident Number 49044 – Risk Ranking High
 Location of Source Area: 3005 Wilkesboro Hwy
Statesville, NC 28625
Iredell County (Figures 1 and 2A)
35.869617°N, 80.940124 °W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System
UST Owner
Bhavani Statesville, LLC
124 Quail Springs Rd.
Statesville, NC 28611
[e-mail]
412-886-7828

UST Operator
Maa Shakti Corp. Inc.
3003 Wilkesboro Hwy.
Statesville, NC 28625
[e-mail]
412-886-7828

Property Owner
Bhavani Statesville, LLC
124 Quail Springs Rd.
Statesville, NC 28611
[e-mail]
412-886-7828

Property Occupant
Yogi Foods
3005 Wilkesboro Hwy.
Statesville, NC 28625
[e-mail]
412-886-7828

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical
449 Springbrook Road
Charlotte, NC 28217
State Certification No. 37735/402
704-529-6364
3. Information about Release
 Release was discovered on January 27, 2023.
 An unknown amount of product was released from the leaking UST.
 One 8,000-gallon UST, two 6,000-gallon gasoline UST, one 8,000-gallon diesel UST, one 1,000-gallon
kerosene UST, and one 1,000-gallon off-road diesel UST, associated dispensers and product piping are
active at the site. One 8,000-gallon UST, two 6,000-gallon gasoline USTs, and one 8,000-gallon diesel
UST were removed from the site in August 1994.

Certification:

I, Samuel L. McKay III, P.G., a Licensed Geologist for Geological Resources, Inc., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the corporation are C-127 and C-2727, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MSCC: Maximum Soil Contaminant
Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWAP: Source Water Assessment and
Protection
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
TABLE OF CONTENTS

EXECUTIVE SUMMARY ....................................................................................................................... ii
SITE INFORMATION ........................................................................................................................... iii
ACRONYMS ....................................................................................................................................... iii
1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................3
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................4
4. SITE INVESTIGATION .............................................................................................................5
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................7
6. LIMITATIONS ........................................................................................................................8

FIGURES
Figure 1: Site Location Map
Figure 2A: Site Vicinity Map
Figure 2B: Zoning Map
Figure 3: Site Map
Figure 4: Soil Quality Map (8/28/23)
Figure 5: Water Table Surface Map (8/28/23)
Figure 6: Ground Water Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Land Use Information
Table 4: Receptor Information
Table 5: Adjacent Property Owner Information
Table 6: Summary of Soil Sample Analytical Results
Table 7: Well Construction and Gauging Information
Table 8: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Iredell County Property Cards
Appendix B: Well Construction Records and Subsurface Logs
Appendix C: State Correspondence
Appendix D: Laboratory Reports – Soil and Ground Water

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? YES

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
YES
An inactive water supply well (WSW-1) is located on-site, approximately 10 feet from the source
area.

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

With the exception of structures located along Weston Road (greater than 500 feet from the
source area), public water is available to the site and surrounding properties.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? NO

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? N/A

8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? NO

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
2
10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? NO
If YES, describe.
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? NO

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:
The subject property is an active convenience store, petroleum retail facility and tire shop.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store, petroleum retail facility and tire shop.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store, petroleum retail facility and tire shop.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:
The property is easily accessible to pedestrian and vehicular traffic.
6. Do pavement, buildings, or other structures cap the contaminated soil? YES
Explain:
The site is currently covered with concrete, asphalt, and grass.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
3
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?
The site is expected to remain in operation as an active convenience store and petroleum retail
facility for the foreseeable future.
7. What is the zoning status of the property?
According to the Iredell County Official Zoning Map, the site is zoned NB (Neighborhood Business).
8. Is the use of the property likely to change in the next 20 years? NO
Explain:
The subject property is currently an active convenience store and petroleum retail facility and will
likely remain a convenience store for the foreseeable future.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is 3008 Wilkesboro Hwy, located approximately 130 feet northeast
of the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

Yadkin Baptist Church is located at 2980 Wilkesboro Hwy, approximately 550 feet southeast of
the source area.

11. What is the zoning status of properties in the surrounding area?

According to the Iredell County Official Zoning Map, the surrounding areas are zoned Residential
(RA, R-20) and Business (NB, GB(CD)).

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is a mixture of commercial, institutional, and residential. Land use
information is included in Table 3. A zoning map is included as Figure 2B.

2. RECEPTOR INFORMATION
1. Water Supply Wells:
A receptor survey was conducted on June 26, 2023. Nine water supply wells (WSW-1 through
WSW-9) were identified within a 1,500-foot radius of the site. Three of the wells, WSW-3, WSW-
5 and WSW-8 are located within 1,000-feet of the source area and are used for potable sources

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
4
of water. WSW-1 and WSW-2 are inactive. WSW-4, WSW-6, WSW-7 and WSW-9 are located
beyond 1,000 feet of the source area and are used for potable and non-potable sources of water.
A Site Location Map is included as Figure 1 and a Site Vicinity Map showing property boundaries
for the site and surrounding properties and water supply well locations is included as Figure 2A.

2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and a majority of the surrounding properties. With the
exception of Weston Road which is not currently serviced by municipal water, water lines run
along the public streets in the area. Public water is supplied by the Iredell Water Corporation.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
One unnamed pond is located approximately 800 feet northwest of the source area.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On July 10, 2023, GRI personnel accessed the NCDEQ SWAP Program’s website to identify
wellhead protection areas in the vicinity of the subject site. The site is not located within a
wellhead protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is not located in the Coastal Plain Physiographic Region.

6. Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. The water main
and other underground utilities run along Wilkesboro Hwy.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
4. Property boundaries are shown on Figure 2A. Property cards for the adjacent property owners
are attached as Appendix A.

3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is in the Chauga Belt of the Inner Piedmont
Physiographic Region. The unit is described as Interlayered with minor layers and lenses of hornblende
gneiss, metagabbro, mica schist, and granitic rock. Monitoring wells MW-1 through MW-4 were gauged

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
5
on August 28, 2023. The depth to ground water during the August 2023 gauging event ranged from 21.93
feet to 23.69 below the tops of well casing. A copy of the well construction records and subsurface logs
are included as Appendix B. A Site Map is included as Figure 3. Well construction and gauging information
is included in Table 6.

4. SITE INVESTIGATION
A ground water sample collected during Phase II ESA activities conducted at the site in January 2023
exhibited a concentration of MTBE that exceeded the MAC. The petroleum release was reported to the
NCDEQ on March 3, 3023. A site check was subsequently conducted at the site in May 2023 by Paragon
Environmental Consultants, Inc. A concentration of TPH-GRO that exceeded the RAL was reported in one
soil sample (GP-6) of fifteen soil samples collected in vicinity of the UST components at the site. The site
check also included the installation of monitoring well MW-1 on May 23, 2023. The monitoring well was
installed near the southwestern corner of the UST basin to a total depth of 25 feet bgs with a screened
interval of 15 feet. Concentrations of benzene, MTBE and EDB detected in the ground water sample
collected from MW-1 on May 24, 2023, exceeded the MACs. Based on this information, a LSA was
required. A copy of the NORR has been included in Appendix C.

Following receptor survey activities conducted by GRI in June 2023, which identified nine (9) water supply
wells (WSW-1 through WSW-9) within the 1,500 foot search radii and surface water within 1,000-feet of
the source area, three (3) additional monitoring wells (MW-2, MW-3 and MW-4) were installed on August
28, 2023. The monitoring wells were installed to total depths of 25 feet bgs and completed with 10-foot
screened intervals. Monitoring wells MW-1 through MW-4 were gauged and purged on August 28, 2023.
Due to low water volumes sampling of certain chemicals of concern from the monitoring wells occurred
either on August 28, September 05, and/or September 07, 2023.

Monitoring wells MW-1 through MW-4 were gauged on August 28, 2023. The depths to ground water
ranged from 21.93 feet to 23.69 feet. The ground water elevation ranged from 75.86 to 78.07 feet during
the August 2023 ground water gauging event. Ground water flow was generally to the north with a
horizontal gradient of 0.03 feet per foot. A Water Table Surface Map is included as Figure 5. Gauging
data from the August 2023 gauging event is included in Table 6. A summary of the current gauging data
is shown below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Groundwater
Elevation
(ft.)
MW-1 10-25 25 100.00 21.93 78.07
MW-2 15-25 25 98.89 23.03 75.86
MW-3 15-25 25 101.35 23.69 77.66
MW-4 15-25 25 99.50 23.34 76.16

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
6
1. Soil Sampling:

A site check was conducted at the site in May 2023 by Paragon Environmental Consultants, Inc. A
concentration of TPH-GRO that exceeded the RAL was reported in one soil sample (GP-6) of fifteen soil
samples collected in vicinity of the UST components at the site.

On August 28, 2023, soil samples were collected during the installation of MW-2, MW-3 and MW-4 at 5-
foot intervals. The soil samples were submitted for analysis of VPH/EPH by the MADEP Method. Soil
samples MW-2-5’, MW-2-15’, MW-3-5’, MW-3-15’, MW-4-5’ and MW-4-15’ were also submitted for
analysis of VOCs and SVOCs by EPA Methods 8260 and 8270, respectively. The soil samples were
submitted to a North Carolina certified laboratory for analysis of VOCs, SVOCs and/or EPH/VPH by
Methods 8260, 8270 and the MADEP Method, respectively. A concentration of MTBE that exceeded the
MCC was reported in the soil sample MW-4-15’. Concentrations of benzo(a)anthracene,
benzo(b)fluoranthene and benzo(a)pyrene that exceeded the MSCCs were reported in the soil sample
collected from MW-3-5’. None of the detectable concentrations exceeded the Residential MSCCs. A soil
quality map is included as Figure 4. A summary of soil sample analytical results is included in Table 7. The
laboratory report is included as Appendix D. A copy of the current soil sampling data is shown below:

2. Ground Water Sampling:

A ground water sample collected from a temporary monitoring well during Phase II ESA activities
conducted at the site in January 2023 exhibited a concentration of MTBE that exceeded the MAC.
Following the installation of the North Carolina Type II monitoring well, MW-1, on May 23, 2023, a ground
water sample was collected from the well on the following day. Concentrations of benzene, MTBE and
EDB detected in the ground water sample collected from MW-1 on May 24, 2023, exceeded the MACs.
Based on the presence of potable water supply wells within 1,000 feet of the source area, additional
monitoring wells were needed to complete a High Risk LSA.

Sa
m
p
l
e

I
D
Da
t
e

C
o
l
l
e
c
t
e
d

(m
m
/
d
d
/
y
y
)
Sa
m
p
l
e

D
e
p
t
h
(f
t
-
B
G
S
)
Ga
s
o
l
i
n
e
-
R
a
n
g
e

T
P
H
Be
n
z
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
MT
B
E
Na
p
h
t
h
a
l
e
n
e
Be
n
z
o
(
a
)
a
n
t
h
r
a
c
e
n
e
Be
n
z
o
(
b
)
f
l
u
o
r
a
n
t
h
e
n
e
Be
n
z
o
(
a
)

p
y
r
e
n
e
50 NA NA NA NA NA NA NA NA NA
NE 0.0072 5.4 8 6 0.085 0.2 0.17 0.6 0.058
NE 12 1,250 60.3 3,120 156 5.5 6.6 6.6 0.66
MW-2-5'08/28/23 5 NR <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001 <0.175 <0.184 <0.186
MW-2-10'08/28/23 10 NR <0.0008 <0.0009 <0.0008 <0.0007 <0.0009 <0.001 NR NR NR
MW-2-15'08/28/23 15 NR <0.0008 <0.0009 <0.0008 <0.0007 <0.0008 <0.001 <0.225 <0.236 <0.237
MW-3-5'08/28/23 5 NR <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001 0.905 1.24 1.05
MW-3-10'08/28/23 10 NR <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001 NR NR NR
MW-3-15'08/28/23 15 NR <0.0008 <0.0009 <0.0008 <0.0007 <0.0008 <0.001 <0.181 <0.190 <0.191
MW-4-5'08/28/23 5 NR 0.001 J <0.0008 0.002 J 0.009 J 0.010 <0.001 <0.174 <0.183 <0.184
MW-4-10'08/28/23 10 NR <0.0008 <0.0009 <0.0008 0.002 J 0.001 J <0.001 NR NR NR
MW-4-15'08/28/23 15 NR <0.0008 0.001 J 0.001 J 0.009 J 0.226 <0.001 <0.186 <0.195 <0.197
Residential SCL
RAL (mg/kg)
Soil to Water MCC (mg/kg)

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
7
Following the installation of additional North Carolina Type II monitoring wells MW-2 through MW-4 on
August 28, 2023, ground water samples were collected from each of the newly installed monitoring wells
as well as MW-1. Due to limited sample volumes in the monitoring wells, GRI returned to the site on
September 5, 2023 and September 7, 2023 to fill additional sampling containers with ground water from
MW-1, MW-2 and MW-4. Estimated and/or detectable concentrations of benzene, toluene,
ethylbenzene, xylenes, MTBE, naphthalene, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene,
1,3,5-trimethylbenzene, TAA, TBA, 1-methynaphthalene, 2-methylnaphthalene, EDB, lead, C5-C8
aliphatics, C9-C12 aliphatics and C9-C22 aromatics that exceeded the MACs were reported in the ground
water samples collected from MW-1, MW-2 and/or MW-4. A concentration of lead that exceeded the
MAC was reported in MW-1, MW-3, and MW-4. None of the concentrations exceed the GCLs. A ground
water quality map is included as Figure 6. A summary of ground water sample analytical results is included
in Table 8. The laboratory analytical reports are included as Appendix D. A summary of the current
ground water sampling data from August 2023 is shown below:

Contaminant of
Concern
→
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

ED
B

Well
ID
MAC (µg/l) 1 600 600 500 20 6 0.02
GCL (µg/l) 5,000 260,000 80,000 50,000 20,000 6,000 50
MW-1 5.52 0.513 0.445 J 28.7 186 <0.470 <0.00500
MW-2 86.1 3.34 18.1 96.0 1,550 10.5 0.161
MW-3 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 <0.00347
MW-4 760 30,100 3,660 18,400 2,420 498 0.742

5. CONCLUSIONS AND RECOMMENDATIONS
• The site is an active convenience store, petroleum retail facility and tire shop. Land use in the
area consists of commercial, institutional, and residential properties.
• On August 28, 2023, three Type II monitoring wells (MW-2, MW-3 and MW-4) were installed in
order to delineate the horizontal contaminant plume and triangulate ground water flow direction.
During the installation of new wells, soil samples were collected at five-foot intervals. A
concentration of MTBE in soil sample MW-4-15’ and concentrations of benzo(a)anthracene,
benzo(b)fluoranthene and benzo(a)pyrene that exceeded the MSCCs were reported in the soil
sample collected from MW-3-5’. None of the detectable concentrations exceeded the Residential
MSCCs.
• On August 28, 2023, (and subsequent site visits on September 5 and September 7, 2023), ground
water samples were collected from existing MW-1 and the newly installed wells MW-2, MW-3,
and MW-4. Estimated and/or detectable concentrations of benzene, toluene, ethylbenzene,
xylenes, MTBE, naphthalene, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-
trimethylbenzene, TAA, TBA, 1-methynaphthalene, 2-methylnaphthalene, EDB, lead, C5-C8
aliphatics, C9-C12 aliphatics and C9-C22 aromatics that exceeded the MACs were reported in the

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Limited Site Assessment Report
Prepared on: September 29, 2023 Yogi Foods
Project Manager: Xavier T. Farmer, G.I.T. GRI Project No. 6473
8
ground water samples collected from MW-1, MW-2 and/or MW-4. A concentration of lead that
exceeded the MAC was reported in MW-1, MW-3, and MW-4. None of the concentrations exceed
the GCLs.
• A receptor survey was conducted by GRI personnel in June 2023. Nine water supply wells (WSW-
1 through WSW-9) were identified within a 1,500-foot radius of the site. Three of the wells, WSW-
3, WSW-5 and WSW-8 are located within 1,000-feet of the source area and are used for potable
sources of water. WSW-1 and WSW-2 are inactive. WSW-4, WSW-6, WSW-7 and WSW-9 are
located beyond 1,000 feet of the source area and are used for potable and non-potable sources
of water. With the exception of Weston Road, public water is available to the subject site and to
all surrounding properties.
• Based on this information, the site risk should be characterized as high, and a CSA should be
completed.

6. LIMITATIONS
This report has been prepared for the exclusive use of Bhavani Statesville, LLC for specific application to
the referenced site in Iredell County, North Carolina. The assessment was conducted based on the scope
of work and level of effort specified by NCDEQ and with resources adequate only for that scope of work.
Our findings have been developed in accordance with generally accepted standards of geology and
hydrogeology practices in the State of North Carolina, available information and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATION
Figure 1
Site Location
Yogi Foods
3005 Wilkesboro Highway
Statesville, North Carolina
Iredell County
Incident No. 49044
GRI Project No. 6473
500 M
2000 FT
Date: 06/24/2023 Location: 35.869617° N -80.940124°W
D
a
d
1
1
Date: 09/27/23
EPA
504.1 EPA 6010
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 70 70 400 400 40 10 1 30 0.02 15
5,000 260,000 80,000 50,000 20,000 6,000 30,500 26,100 28,500 24,100 40,000 10,000 1,000 12,500 50 15,000
05/24/23 2.21 J <2.20 <1.70 13.4 134 <4.70 <1.80 <1.90 <1.90 <1.80 <19.0 107 NR NR 0.239 <2
08/28/23 5.52 0.513 0.445 J 28.7 186 <0.470 0.554 0.212 J 4.02 0.207 J 31.8 74.7 <1.27 <0.739 <0.00500 891
09/07/23 NR NR NR NR NR NR NR NR NR NR NR NR <1.14 <0.666 NR NR
08/28/23 86.1 3.34 18.1 96.0 1,550 10.5 1.48 2.54 11.6 0.377 J 238 158 NR NR 0.161 4 J
09/05/23 NR NR NR NR NR NR NR NR NR NR NR NR <1.14 0.768 J NR NR
MW-3 08/28/23 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 <0.180 <0.190 0.228 J <0.180 <1.90 <1.60 <1.16 <0.679 <0.00347 72
08/28/23 760 30,100 3,660 18,400 2,420 498 261 593 3,660 1,030 <190 497 J NR NR 0.742 44
09/05/23 NR NR NR NR NR NR NR NR NR NR NR NR 34.7 61.0 NR NR
05/24/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.190 <0.190 <0.180 <1.90 <1.60 NR NR NR NR
08/28/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.190 <0.190 <0.180 NR NR NR NR NR NR
Notes:
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report.
• GCL: Gross contamination level.
• Concentrations in bold face type indicate the MAC was below the reported concentration.
• Results in italics indicate the GCLs were below the reported concentrations.
• J: Estimated value.
• NE: Not established.
• S: Toxicity exceeds solubility, no visible sheen or free product in water or on sediment or shoreline per 15A NCAC 02B .0211 & .0220
• NR: Not requested.
Trip Blank
• Refer to laboratory reports for other detectable concentrations which did not exceed the MACs.
Le
a
d
MW-1
MW-2
MW-4
MAC (μg/l)
GCL (μg/l)
MT
B
E
Na
p
h
t
h
a
l
e
n
e
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Contaminant of Concern

Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
Analytical Method

n-
P
r
o
p
y
l
b
e
n
z
e
n
e
1,2
,
4
-
Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,3
,
5
-
Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
ED
B
TABLE 8
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
YOGI FOODS (INCIDENT NO. 49044)
Method 625
1-
Me
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
2-
Me
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
EPA 6200B
te
r
t
-
B
u
t
y
l

A
l
c
o
h
o
l
(T
B
A
)
te
r
t
-
A
m
y
l

A
l
c
h
o
h
o
l

(T
A
A
)
Page 1 of 1

TABLES
UST ID Number A1 - A6 Facility ID Number
Owner or Operator?
Owner
UST ID Number A1 - A6 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1 - A6 Facility ID Number
Owner or Operator?
Owner
124 Quail Springs Road
Statesville, NC 28611 412-886-7828
Name of Owner or Operator Dates of Ownership / Operation
Bhavani Statesville, LLC 05/12/2022 - Current
Address Telephone Number
00-0-0000029113
TABLE 1
UST OWNER/OPERATOR INFORMATION
YOGI FOODS (INCIDENT NO. 49044)
Address Telephone Number
Unknown Unknown
00-0-0000029113
Name of Owner or Operator Dates of Ownership / Operation
Franco Energy 04/01/2000 - 04/06/2010
Address Telephone Number
P.O. Box 68 Gastonia, NC 28054-0068 704-824-3561
00-0-0000029113
Name of Owner or Operator Dates of Ownership / Operation
United Oil of the Carolinas 07/06/2010 - 05/12/2022
Page 1 of 1
Date: 07/06/23
Was Release
Associated
with UST
System?
(Yes / No)
A1 Gasoline/Gas
Mix Unknown 8,000 10/1/1994 Single Wall
Steel/FRP 8' x 21' 4"Single Wall FRP Current No
A2 Gasoline/Gas
Mix Unknown 6,000 10/1/1994 Single Wall
Steel/FRP 8' x 16'Single Wall FRP Current Yes
A3 Gasoline/Gas
Mix Unknown 6,000 10/1/1994 Single Wall
Steel/FRP 8' x 16'Single Wall FRP Current No
A4 Highway Diesel Unknown 8,000 10/1/1994 Single Wall
Steel/FRP 8' x 21' 4"Single Wall FRP Current No
A5 Kerosene/Kero
Mix Unknown 1,000 10/1/1994 Single Wall
Steel/FRP 46" x 12'Single Wall FRP Current No
A6 Off-Road Diesel Unknown 1,000 10/1/1996 Single Wall
Steel/FRP 46" x 12'Single Wall FRP Current No
1 Unknown Unknown 9,999 1/1/1964 Unknown Unknown Unknown Removed No
2 Unknown Unknown 3,500 1/1/1964 Unknown Unknown Unknown Removed No
3 Unknown Unknown 3,500 1/1/1964 Unknown Unknown Unknown Removed No
4 Unknown Unknown 3,500 1/1/1964 Unknown Unknown Unknown Removed No
TABLE 2
UST SYSTEM INFORMATION
YOGI FOODS (INCIDENT NO. 49044)
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
Facility ID #: 0-029113
Page 1 of 1
Date: 07/10/2023 Facility ID # : 00-0-0000029113
Map ID No.Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
1 Yadkin Baptist Church RA Church 2980 Wilkesboro Hwy,
Statesville, NC 28625 ~450' SE
n/a NB Neighborhood Business n/a 0
n/a GB-CD General Buisness,
Conditional n/a ~120' S
n/a RA Residential Agricultural n/a ~80' E
n/a R-20 Single Family Residential n/a ~530' SW
Note:
• Properties are keyed to Figure 2B.
TABLE 3
LAND USE INFORMATION
YOGI FOODS (INCIDENT NO. 49044)
Page 1 of 1
Facility ID # : 0-029113
Well ID.Parcel PIN Well Owner Mailing Address Well Address Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municpal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Distance
from source
area of
release
(ft.)
WSW-1 4727479053.000 Bhavani Statesville, LLC 124 Quail Springs Road
Statesville, NC 28677
3001 Wilkesboro Hwy
Statesville, NC 28625 Inactive Non-Potable Yes Yes ~10' S
WSW-2 4727561673.000 Dirt Creek Management, LLC 133 Sportsman Dr.
Statesville, NC 28625
2987 Wilkesboro Hwy
Statesville, NC 28625 Inactive Unk.Yes Yes ~480' S
WSW-3 4727561673.000 Yadkin Baptist Church of Statesville,
Inc
2980 Wilkesboro Hwy
Statesville, NC 28625
2994 Wilkesboro Hwy
Statesville, NC 28625 Active Potable Yes No ~750' SE
WSW-4 4727566257.000 Trinity Volunteer Fire Department
Inc Active Non-Potable Yes Yes ~1,200' S
WSW-5 Active Potable No No ~750' W
WSW-6 Active Potable No No ~1,375' W
WSW-7 4727660891.000 Larry & Deborah R. Sprinkle 139 Yadkin Valley Rd.
Statesville, NC 28625
139 Yadkin Valley Rd.
Statesville, NC 28625 Active Potable Unk.No ~1,400' SE
WSW-8 4727575443.000 Joshua B. & Stefanie Byrd 121 Persimmon Cir.
Statesville, NC 28625
121 Persimmon Cir.
Statesville, NC 28625 Active Potable Yes No ~790' NE
WSW-9 4727578908.000 Herbert P. & Patricia Campbell 166 Persimmon Cir.
Statesville, NC 28625
166 Persimmon Cir.
Statesville, NC 28625 Unk.Unk.Yes Yes ~1,400' NE
Receptor ID
Latitude/
Longitude of Any
Significant Points
Up or Down-
Gradient
Distance
from
the source
area
of release
(ft.)
1 35.871783°, -
80.943575°~800' NW
Notes:
• Receptors are shown on Figure 2A.
• n/a: not applicable.
Unk.
Unk.
Unk.
Unk.
TABLE 4
RECEPTOR INFORMATION
YOGI FOODS (INCIDENT NO. 49044)
Date: 07/07/23
Well Construction Details
(Depth, Screened Interval, Type of Well, ect.)
Unk.
Unk.
Unk.
Unk.
Unk.
2968 Wilkesboro Hwy
Statesville, NC 28625
4727472043.000
Unk.
Description Location Contact/Phone Number Usage
Jessica J. & Michael T. Jackson 132 Weston Road
Statesville, NC 28625
Unnamed Pond Immediately North of 168 Clearcut Ln, Statesville, NC Unk.
Page 1 of 1
Date: 07/06/23 Facility ID #: 0-029113
PIN Number Property Owner
Name Property Owner Address Property Owner Address Property Address
4727-47-9053.000 (Site)1009P00000A068 Bhavani Statesville, LLC 124 Quail Springs Rd.
Statesville, NC 28677
2999, 3001, 3003, 3005 Wilkesboro
Hwy, Statesville NC 28611
4727-47-7106.000 1009P00000A066 Mark James Cowles 130 Jacobs Dr.
Statesville, NC 28625
4727-47-7285.000 1009P00000A050 Mark James Cowles 126 Jacobs Dr.
Statesville, NC 28625
4727-47-9287.000 1009P00000A034 Tommy and Sarah Taylor 172 Mason Ln.
Statesville, NC 28625
3023 Wilkesboro Hwy
Statesville, NC
4727-57-3351.000 1009N02000A004 Homer D. Dishman 3016 Wilkesboro Hwy
Statesville, NC 28625
3016 Wilkesboro Hwy
Statesville, NC 28625
4727-57-3133.000 1009N02000A003 Allen L. Crankshaw 3008 Wilkesboro Hwy
Statesville, NC 28625
3008 Wilkesboro Hwy
Statesville, NC 28625
4727-57-3055.000 1009N02000A001 Omar N. Lopez-Vasquez 3004 Wilkesboro Hwy
Statesville, NC 28625
3004 Wilkesboro Hwy
Statesville, NC 28625
4727-56-3999.000 1009L00000A040 3000 Wilkesboro Hwy
Statesville, NC 28625
4727-56-4826.000 1009L00000A001 2994 Wilkesboro Hwy
Statesville, NC 28625
4727-56-0709.000 1009P00000A035 Red Rock Ventures, LLC 2997 Wilkesboro Hwy
Statesville, NC 28625
2997 Wilkesboro Hwy
Statesville, NC 28625
4727-56-0540.000 1009P00000A037 Jerry Marvin Burns 108 Weston Rd.
Statesville, NC 28625
108 Weston Rd.
Statesville, NC 28625
126 Jacobs Dr.
Statesville, NC 28625
Yadkin Baptist Church of
Statesville, Inc.
2980 Wilkesboro Hwy
Statesville, NC 28625
TABLE 5
ADJACENT PROPERTY OWNER INFORMATION
(INCIDENT NO. 49044)
Page 1 of 1
Date: 07/06/23 Facility ID #: 0-029113
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
05/24/23 20.49 ---79.51
08/28/23 21.93 ---78.07
MW-2 08/28/23 08/28/23 15 15 - 25 25 98.89 23.03 ---75.86
MW-3 08/28/23 08/28/23 15 15 - 25 25 101.35 23.69 ---77.66
MW-4 08/28/23 08/28/23 15 15 - 25 25 99.50 23.34 ---76.16
Notes:
• ft BGS : feet below ground surface.
• NA: Not available.
• NM: Not measured.
TABLE 6
WELL CONSTRUCTION AND GAUGING INFORMATION
YOGI FOODS (INCIDENT NO. 49044)
MW-1 05/23/23 10 10 - 25 25 100.00
Page 1 of 1
Date: 9/5/23 Facility ID #: 0-029113
Sa
m
p
l
e

I
D
Da
t
e

C
o
l
l
e
c
t
e
d

(m
m
/
d
d
/
y
y
)
Sa
m
p
l
e

D
e
p
t
h
(f
t
-
B
G
S
)
Be
n
z
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
MT
B
E
Na
p
h
t
h
a
l
e
n
e
Be
n
z
o
(
a
)
a
n
t
h
r
a
c
e
n
e
Be
n
z
o
(
b
)
f
l
u
o
r
a
n
t
h
e
n
e
Be
n
z
o
(
a
)

p
y
r
e
n
e
NA NA NA NA NA NA NA NA NA
0.0072 5.4 8 6 0.085 0.2 0.17 0.6 0.058
12 1,250 60.3 3,120 156 5.5 6.6 6.6 0.66
MW-2-5'08/28/23 5 <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001 <0.175 <0.184 <0.186
MW-2-10'08/28/23 10 <0.0008 <0.0009 <0.0008 <0.0007 <0.0009 <0.001 NR NR NR
MW-2-15'08/28/23 15 <0.0008 <0.0009 <0.0008 <0.0007 <0.0008 <0.001 <0.225 <0.236 <0.237
MW-3-5'08/28/23 5 <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001 0.905 1.24 1.05
MW-3-10'08/28/23 10 <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001 NR NR NR
MW-3-15'08/28/23 15 <0.0008 <0.0009 <0.0008 <0.0007 <0.0008 <0.001 <0.181 <0.190 <0.191
MW-4-5'08/28/23 5 0.001 J <0.0008 0.002 J 0.009 J 0.010 <0.001 <0.174 <0.183 <0.184
MW-4-10'08/28/23 10 <0.0008 <0.0009 <0.0008 0.002 J 0.001 J <0.001 NR NR NR
MW-4-15'08/28/23 15 <0.0008 0.001 J 0.001 J 0.009 J 0.226 <0.001 <0.186 <0.195 <0.197
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• Trip Blank results reported in ug/l (micrograms per liter)
• ft-BGS: feet below ground surface.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• < : Less than the method detection limit specified in the laboratory report
• Concentrations in bold face type indicate the soil to water MCCs were below the reported concentrations.
• Concentrations in italic type indicate the Residential SCLs were below the report concentrations.
• NE: Not Established
• NR: Not Requested.
Residential SCL
RAL (mg/kg)
Soil to Water MCC (mg/kg)
Analytical Method 
TABLE 7
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
YOGI FOODS (INCIDENT NO. 49044)
8260D 8270
Page 1 of 1
Date: 09/27/23 Facility ID #: 0-029113
EPA
504.1 EPA 6010
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 70 70 400 400 40 10 1 30 0.02 15 400 700 700 10,000 200 200 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 26,100 28,500 24,100 40,000 10,000 1,000 12,500 50 15,000 NE NE NE NE NE NE NE
05/24/23 2.21 J <2.20 <1.70 13.4 134 <4.70 <1.80 <1.90 <1.90 <1.80 <19.0 107 NR NR 0.239 <2 53.1 69.4 NR NR <4.02 NR NR
08/28/23 5.52 0.513 0.445 J 28.7 186 <0.470 0.554 0.212 J 4.02 0.207 J 31.8 74.7 <1.27 <0.739 <0.00500 891 125 46.3 J NR NR 7.01 J NR NR
09/07/23 NR NR NR NR NR NR NR NR NR NR NR NR <1.14 <0.666 NR NR NR NR NR NR NR NR NR
08/28/23 86.1 3.34 18.1 96.0 1,550 10.5 1.48 2.54 11.6 0.377 J 238 158 NR NR 0.161 4 J 332 77.4 J 140.9 J <124 39.5 J 330 369.5 J
09/05/23 NR NR NR NR NR NR NR NR NR NR NR NR <1.14 0.768 J NR NR NR NR NR NR NR NR NR
MW-3 08/28/23 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 <0.180 <0.190 0.228 J <0.180 <1.90 <1.60 <1.16 <0.679 <0.00347 72 <11.5 <25.8 <54 <124 <4.02 <61.2 <65.22
08/28/23 760 30,100 3,660 18,400 2,420 498 261 593 3,660 1,030 <190 497 J NR NR 0.742 44 12,000 14,500 NR NR 9,420 NR NR
09/05/23 NR NR NR NR NR NR NR NR NR NR NR NR 34.7 61.0 NR NR NR NR 29.0 J <124 NR 479 NR
05/24/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.190 <0.190 <0.180 <1.90 <1.60 NR NR NR NR <11.5 <25.8 NR NR <4.02 NR NR
08/28/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.180 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR NR NR NR NR NR NR
Notes:
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report.
• GCL: Gross contamination level.
• Concentrations in bold face type indicate the MAC was below the reported concentration.
• Results in italics indicate the GCLs were below the reported concentrations.
• J: Estimated value.
• NE: Not established.
• S: Toxicity exceeds solubility, no visible sheen or free product in water or on sediment or shoreline per 15A NCAC 02B .0211 & .0220
• NR: Not requested.
TABLE 8
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
YOGI FOODS (INCIDENT NO. 49044)
MADEP VPH/EPH
C9
-
C
2
2

A
r
o
m
a
t
i
c
s
C1
9
-
C
3
6

A
l
i
p
h
a
t
i
c
s
Method 625
1-
Me
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
2-
Me
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
C1
1
-
C
2
2

A
r
o
m
a
t
i
c
s
EPA 6200B
te
r
t
-
B
u
t
y
l

A
l
c
o
h
o
l
(T
B
A
)
te
r
t
-
A
m
y
l

A
l
c
h
o
h
o
l

(T
A
A
)
C9
-
C
1
0

A
r
o
m
a
t
i
c
s
C9
-
C
1
8

A
l
i
p
h
a
t
i
c
s
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
Analytical Method

C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
1,2
,
4
-
Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,3
,
5
-
Tr
i
m
e
t
h
y
l
b
e
n
z
e
n
e
ED
B
Trip Blank
• Refer to laboratory reports for other detectable concentrations which did not exceed the MACs.
Le
a
d
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
MW-1
MW-2
MW-4
MAC (μg/l)
GCL (μg/l)
MT
B
E
Na
p
h
t
h
a
l
e
n
e
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Contaminant of Concern

Be
n
z
e
n
e
To
l
u
e
n
e
Page 1 of 1

APPENDICES

APPENDIX A
Iredell County Property Cards

APPENDIX B
Well Construction Records and Boring Logs
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Yogi Foods
6473
9/18/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-2
6"
25'
Well installed at completion
0 0.5 Asphalt
0.5 6 Sandy Silt Brown Dry None
6 25 Silt Orange-brown Wet None

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Yogi Foods
6473
9/18/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-2
6"
98.89
23.03
13 25
11 13
0 11
0
0 15 15
15 25 2
11
13
25
15
25
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
9/18/23 MW-2
Yogi Foods 00-0-0000029113
3005 Wilkesboro Hwy, Statesville
Iredell 4727-47-9053.000
35.869617 80.940124
25
23.03
6"
Solid Stem Auger
0
0 15 15 Sch 40 PVC
15 25 2 0.010 Sch 40 PVC
0 11 grout pour
11 13 bentonite pour
13 25 #2 Sand Pour
0 0.5 Asphalt
0.5 6 Sandy Silt
6 25 Silt
9/18/23
4
4
4
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Yogi Foods
6473
9/18/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-3
6"
25'
Well installed at completion
0 0.5 Asphalt
0.5 9 Sandy Silt with gravel Brown Dry None
9 25 Silt Orange-brown Wet None

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Yogi Foods
6473
9/18/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-3
6"
101.35
23.69
13 25
11 13
0 11
0
0 15 15
15 25 2
11
13
25
15
25
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
9/18/23 MW-3
Yogi Foods 00-0-0000029113
3005 Wilkesboro Hwy, Statesville
Iredell 4727-47-9053.000
35.869617 80.940124
25
23.69
6"
Solid Stem Auger
0
0 15 15 Sch 40 PVC
15 25 2 0.010 Sch 40 PVC
0 11 grout pour
11 13 bentonite pour
13 25 #2 Sand Pour
0 0.5 Asphalt
0.5 9 Sandy Silt with gravel
9 25 Silt
9/18/23
4
4
4
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Yogi Foods
6473
9/18/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-4
6"
25'
Well installed at completion
0 0.5 Asphalt
0.5 3 Silt Dark Red-brown Dry None
3 19 Silt Orange-brown Dry None
19 25 Silt Red-brown Moist Present

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Yogi Foods
6473
9/18/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-4
6"
99.50
23.34
13 25
11 13
0 11
0
0 15 15
15 25 2
11
13
25
15
25
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
9/18/23 MW-4
Yogi Foods 00-0-0000029113
3005 Wilkesboro Hwy, Statesville
Iredell 4727-47-9053.000
35.869617 80.940124
25
23.34
6"
Solid Stem Auger
0
0 15 15 Sch 40 PVC
15 25 2 0.010 Sch 40 PVC
0 11 grout pour
11 13 bentonite pour
13 25 #2 Sand Pour
0 0.5 Asphalt
0.5 3 Silt
3 19 Silt
19 25 Silt
9/18/23
4
4
4

APPENDIX C
State Correspondence

North Carolina Department of Environmental Quality | Division of Waste Management
Mooresville Regional Office | 610 East Center Avenue | Suite 301 | Mooresville, NC 28115 | [phone]

June 7, 2023

Bhavani Statesville, LLC
124 Quail Sprints Road
Statesville, NC 28677

Re: Notice of Regulatory Requirements
15A NCAC 02L .0404 and 02L .0405
Risk-based Assessment and Corrective Action
for Commercial Petroleum Underground Storage
Tanks

Yogi Foods
3001 Wilkesboro Highway, Statesville
Iredell County
Incident Number: 49044
Risk Classification: Pending

Dear Mr.Bhavani:
Information received by this regional office of the Underground Storage Tank Section, Division of Waste
Management, on June 1, 2023, confirms a release or discharge from a petroleum underground storage tank
(UST) system at the above-referenced location. Records indicate that you are the owner or operator of this
UST system. Therefore, as a responsible party, you must comply with the initial response and abatement
action requirements of the Title 15A of the North Carolina Administrative Code (NCAC), Subchapter 02L
.0404 and, if applicable, the assessment and reporting requirements of Title 15A NCAC 02L .0405, within
the timeframes specified in the attached rules. If Title 15A NCAC 02L .0405 is applicable, you must
comply with its requirements even if you do not receive formal notification from the UST Section.
Initial abatement action requirements include the preparation and submittal of an Initial Abatement Action
(IAA) Report, in accordance with Title 15A NCAC 02L .0404 and the most recent version of the Guidelines
for Site Checks, Tank Closure, and Initial Response and Abatement, within 90 days of discovery of the
release.
Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer,
certified by the State of North Carolina, is required to prepare and certify all reports submitted to the
Department of Environmental Quality in accordance with Title 15A NCAC 02L .0103(e) and 02L .0111(e).
Please note that before you sell, transfer, or request a “No Further Action” determination for a property that
has not been remediated to below “unrestricted use” standards, you must file a Notice of Residual Petroleum
("Notice") with the Register of Deeds in the county where the property is located (North Carolina General
Statutes 143B-279.9 and 143B-279.11).
Page 2 of 2
Incident Number 49044 June 7, 2023
North Carolina Department of Environmental Quality | Division of Waste Management
Mooresville Regional Office | 610 East Center Avenue | Suite 301 | Mooresville, NC 28115 | [phone]
Failure to comply with the State's rules in the manner and time specified may result in the assessment
of civil penalties and/or the use of other enforcement mechanisms.
If you have any questions regarding trust fund eligibility or reimbursement from the Commercial Leaking
Petroleum Underground Storage Tank Cleanup Funds, please contact the UST Section Trust Fund Branch
at [phone]. If you have any questions regarding the actions that must be taken or the rules mentioned
in this letter, please contact me at the address or telephone number listed below.
Sincerely,
Ryan C Mills
Environmental Program Consultant
Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ
cc: Brady Freeman, Statesville County Health Department (Via Email)
Benjamin Robinson, L.G., Paragon Environmental Consultants, Inc.(Via Email)

APPENDIX D
Laboratory Reports – Soil and Ground Water Samples

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

9/15/2023
Geological Resources, Inc. Xavier T Farmer
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-244-0003 Client Project Description: Yogi Foods
GRI #6473
Dear Xavier T Farmer:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/31/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 194
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-244-0003
Page 2 of 194
Report Number:
Sample Summary Table
Client Project Description:
23-244-0003
Yogi Foods
GRI #6473
Lab No Client Sample ID Matrix Date Collected Date Received
08/28/2023 11:02Solids 93883 MW-2-5'08/31/2023 16:59
08/28/2023 11:26Solids 93884 MW-2-10'08/31/2023 16:59
08/28/2023 11:30Solids 93885 MW-2-15'08/31/2023 16:59
08/28/2023 11:56Solids 93886 MW-3-5'08/31/2023 16:59
08/28/2023 12:00Solids 93887 MW-3-10'08/31/2023 16:59
08/28/2023 12:03Solids 93888 MW-3-15'08/31/2023 16:59
08/28/2023 12:54Solids 93889 MW-4-5'08/31/2023 16:59
08/28/2023 12:57Solids 93890 MW-4-10'08/31/2023 16:59
08/28/2023 13:00Solids 93891 MW-4-15'08/31/2023 16:59
08/28/2023Aqueous 93892 MW-2 08/31/2023 16:59
08/28/2023 12:56Aqueous 93893 MW-3 08/31/2023 16:59
08/28/2023 17:05Aqueous 93894 MW-4 08/31/2023 16:59
08/28/2023 09:50Aqueous 93895 Trip Blank 08/31/2023 16:59
08/28/2023 14:30Aqueous 93896 MW-1 08/31/2023 16:59
Page 3 of 194
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-244-0003
Report Limit
Project:Yogi Foods
V 93883MW-2-5'
J0.010 09/01/2023 17:538260DAcetonemg/Kg - dry 0.003
J0.005 09/01/2023 17:538260DCarbon Disulfide mg/Kg - dry 0.0008
J0.001 09/01/2023 17:538260Dn-Hexane mg/Kg - dry 0.0008
21.0 09/01/2023 14:50SW-DRYWT Moisture %
V 93884MW-2-10'
28.6 09/01/2023 14:50SW-DRYWT Moisture %
V 93885MW-2-15'
J0.007 09/01/2023 18:478260DAcetonemg/Kg - dry 0.003
26.0 09/01/2023 14:50SW-DRYWT Moisture %
V 93886MW-3-5'
0.039 09/01/2023 19:148260DAcetonemg/Kg - dry 0.002
J0.318 09/07/2023 01:118270EAcenaphthylenemg/Kg - dry 0.131
J0.218 09/07/2023 01:118270EAnthracenemg/Kg - dry 0.178
0.905 09/07/2023 01:118270EBenzo(a)anthracene mg/Kg - dry 0.173
1.05 09/07/2023 01:118270EBenzo(a)pyrene mg/Kg - dry 0.183
1.24 09/07/2023 01:118270EBenzo(b)fluoranthene mg/Kg - dry 0.182
J0.604 09/07/2023 01:118270EBenzo(g,h,i)perylene mg/Kg - dry 0.169
J0.488 09/07/2023 01:118270EBenzo(k)fluoranthene mg/Kg - dry 0.171
0.927 09/07/2023 01:118270EChrysenemg/Kg - dry 0.177
2.06 09/07/2023 01:118270EFluoranthenemg/Kg - dry 0.153
J0.714 09/07/2023 01:118270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.223
J0.466 09/07/2023 01:118270EPhenanthrenemg/Kg - dry 0.259
2.36 09/07/2023 01:118270EPyrenemg/Kg - dry 0.167
19.9 09/01/2023 14:50SW-DRYWT Moisture %
V 93887MW-3-10'
22.0 09/01/2023 14:50SW-DRYWT Moisture %
V 93888MW-3-15'
J0.014 09/01/2023 20:088260DAcetonemg/Kg - dry 0.003
23.4 09/01/2023 14:50SW-DRYWT Moisture %
V 93889MW-4-5'
0.030 09/01/2023 20:358260DAcetonemg/Kg - dry 0.003
J0.001 09/01/2023 20:358260DBenzenemg/Kg - dry 0.0007
J0.002 09/01/2023 20:358260DCarbon Disulfide mg/Kg - dry 0.0008
Page 4 of 194
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-244-0003
Report Limit
Project:Yogi Foods
V 93889MW-4-5'
J0.002 09/01/2023 20:358260DEthylbenzenemg/Kg - dry 0.0007
0.010 09/01/2023 20:358260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.0008 09/01/2023 20:358260Dn-Propylbenzene mg/Kg - dry 0.0007
0.006 09/01/2023 20:358260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.002 09/01/2023 20:358260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.002 09/01/2023 20:358260Do-Xylene mg/Kg - dry 0.0006
J0.007 09/01/2023 20:358260Dm,p-Xylene mg/Kg - dry 0.001
J0.009 09/01/2023 20:358260DXylene (Total)mg/Kg - dry 0.0006
20.3 09/01/2023 14:50SW-DRYWT Moisture %
V 93890MW-4-10'
J0.020 09/01/2023 21:038260DAcetonemg/Kg - dry 0.003
J0.001 09/01/2023 21:038260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0009
J0.003 09/01/2023 21:038260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 09/01/2023 21:038260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0008
J0.002 09/01/2023 21:038260Dm,p-Xylene mg/Kg - dry 0.001
J0.002 09/01/2023 21:038260DXylene (Total)mg/Kg - dry 0.0007
29.1 09/05/2023 11:43SW-DRYWT Moisture %
V 93891MW-4-15'
J0.014 09/01/2023 21:308260DAcetonemg/Kg - dry 0.003
J0.001 09/01/2023 21:308260DCarbon Disulfide mg/Kg - dry 0.0009
J0.001 09/01/2023 21:308260DEthylbenzenemg/Kg - dry 0.0008
0.226 09/01/2023 21:308260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.001 09/01/2023 21:308260DToluenemg/Kg - dry 0.0009
J0.004 09/01/2023 21:308260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
0.009 09/01/2023 21:308260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.005 09/01/2023 21:308260Do-Xylene mg/Kg - dry 0.0007
J0.004 09/01/2023 21:308260Dm,p-Xylene mg/Kg - dry 0.001
J0.009 09/01/2023 21:308260DXylene (Total)mg/Kg - dry 0.0007
25.4 09/05/2023 11:43SW-DRYWT Moisture %
V 93892MW-2
J0.004 09/06/2023 18:576010DLeadmg/L 0.002
J3.69 09/07/2023 06:536200BAcetoneµg/L 1.80
86.1 09/07/2023 06:536200BBenzeneµg/L 0.180
J0.245 09/07/2023 06:536200Bn-Butylbenzene µg/L 0.180
37.4 09/07/2023 06:536200BDi-Isopropyl Ether (DIPE)µg/L 0.500
Page 5 of 194
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-244-0003
Report Limit
Project:Yogi Foods
V 93892MW-2
5.02 09/07/2023 06:536200B1,2-Dichloroethane µg/L 0.150
18.1 09/07/2023 06:536200BEthylbenzeneµg/L 0.170
1.48 09/07/2023 06:536200BIsopropylbenzeneµg/L 0.180
1550 09/15/2023 08:176200BMethyl tert-butyl ether (MTBE)µg/L 14.0
10.5 09/07/2023 06:536200BNaphthaleneµg/L 0.470
2.54 09/07/2023 06:536200Bn-Propylbenzene µg/L 0.190
158 09/07/2023 06:536200Btert-Butyl Alcohol (TBA)µg/L 1.60
238 09/07/2023 16:566200Btert-Amyl Alcohol (TAA)µg/L 19.0
13.4 09/07/2023 06:536200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
3.34 09/07/2023 06:536200BTolueneµg/L 0.220
11.6 09/07/2023 06:536200B1,2,4-Trimethylbenzene µg/L 0.190
J0.377 09/07/2023 06:536200B1,3,5-Trimethylbenzene µg/L 0.180
24.2 09/07/2023 06:536200Bo-Xylene µg/L 0.210
71.8 09/07/2023 06:536200Bm,p-Xylene µg/L 0.420
96.0 09/07/2023 06:536200BXylene (Total)µg/L 0.210
332 09/01/2023 17:36CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 11.5
J77.4 09/01/2023 17:36CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 25.8
J39.5 09/01/2023 17:36CALCULATIONAromatic C9-C10 (Adjusted)µg/L 4.02
0.161 09/08/2023 15:25EPA-504.1 1,2-Dibromoethane µg/L 0.00347
J63.5 09/11/2023 19:18MADEP-EPH Aliphatic C9-C18 µg/L 28.2
330 09/11/2023 19:18MADEP-EPH Aromatic C11-C22 µg/L 61.2
421 09/01/2023 17:36MADEP-VPH Aliphatic C5-C8 µg/L 11.5
231 09/01/2023 17:36MADEP-VPH Aliphatic C9-C12 µg/L 25.8
J39.5 09/01/2023 17:36MADEP-VPH Aromatic C9-C10 µg/L 4.02
V 93893MW-3
0.072 09/06/2023 19:016010DLeadmg/L 0.002
J2.17 09/07/2023 02:206200BAcetoneµg/L 1.80
J0.228 09/07/2023 02:206200B1,2,4-Trimethylbenzene µg/L 0.190
V 93894MW-4
0.044 09/06/2023 19:066010DLeadmg/L 0.012
760 09/07/2023 08:336200BBenzeneµg/L 18.0
J37.1 09/07/2023 08:336200Bn-Butylbenzene µg/L 18.0
J36.7 09/07/2023 08:336200Bsec-Butyl benzene µg/L 20.0
3660 09/07/2023 08:336200BEthylbenzeneµg/L 17.0
261 09/07/2023 08:336200BIsopropylbenzeneµg/L 18.0
2420 09/07/2023 08:336200BMethyl tert-butyl ether (MTBE)µg/L 14.0
Page 6 of 194
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-244-0003
Report Limit
Project:Yogi Foods
V 93894MW-4
498 09/07/2023 08:336200BNaphthaleneµg/L 47.0
593 09/07/2023 08:336200Bn-Propylbenzene µg/L 19.0
J49709/07/2023 08:336200Btert-Butyl Alcohol (TBA)µg/L 160
J11209/07/2023 08:336200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
30100 09/07/2023 19:006200BTolueneµg/L 220
3660 09/07/2023 08:336200B1,2,4-Trimethylbenzene µg/L 19.0
1030 09/07/2023 08:336200B1,3,5-Trimethylbenzene µg/L 18.0
6100 09/07/2023 08:336200Bo-Xylene µg/L 21.0
12300 09/07/2023 08:336200Bm,p-Xylene µg/L 42.0
18400 09/07/2023 08:336200BXylene (Total)µg/L 21.0
12000 09/01/2023 20:44CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 1150
14500 09/01/2023 20:44CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 2580
9420 09/01/2023 20:44CALCULATIONAromatic C9-C10 (Adjusted)µg/L 402
0.742 09/08/2023 16:08EPA-504.1 1,2-Dibromoethane µg/L 0.00345
42900 09/01/2023 20:44MADEP-VPH Aliphatic C5-C8 µg/L 1150
46000 09/01/2023 20:44MADEP-VPH Aliphatic C9-C12 µg/L 2580
9420 09/01/2023 20:44MADEP-VPH Aromatic C9-C10 µg/L 402
V 93896MW-1
0.891 09/07/2023 15:046010DLeadmg/L 0.048
5.52 09/07/2023 02:456200BBenzeneµg/L 0.180
6.36 09/07/2023 02:456200BDi-Isopropyl Ether (DIPE)µg/L 0.500
J0.445 09/07/2023 02:456200BEthylbenzeneµg/L 0.170
0.554 09/07/2023 02:456200BIsopropylbenzeneµg/L 0.180
186 09/07/2023 16:066200BMethyl tert-butyl ether (MTBE)µg/L 1.40
J0.212 09/07/2023 02:456200Bn-Propylbenzene µg/L 0.190
74.7 09/07/2023 02:456200Btert-Butyl Alcohol (TBA)µg/L 1.60
31.8 09/07/2023 02:456200Btert-Amyl Alcohol (TAA)µg/L 1.90
J4.80 09/07/2023 02:456200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
0.513 09/07/2023 02:456200BTolueneµg/L 0.220
4.02 09/07/2023 02:456200B1,2,4-Trimethylbenzene µg/L 0.190
J0.207 09/07/2023 02:456200B1,3,5-Trimethylbenzene µg/L 0.180
20.7 09/07/2023 02:456200Bo-Xylene µg/L 0.210
8.04 09/07/2023 02:456200Bm,p-Xylene µg/L 0.420
28.7 09/07/2023 02:456200BXylene (Total)µg/L 0.210
125 09/01/2023 18:23CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 11.5
J46.3 09/01/2023 18:23CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 25.8
Page 7 of 194
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-244-0003
Report Limit
Project:Yogi Foods
V 93896MW-1
J7.01 09/01/2023 18:23CALCULATIONAromatic C9-C10 (Adjusted)µg/L 4.02
131 09/01/2023 18:23MADEP-VPH Aliphatic C5-C8 µg/L 11.5
82.5 09/01/2023 18:23MADEP-VPH Aliphatic C9-C12 µg/L 25.8
J7.01 09/01/2023 18:23MADEP-VPH Aromatic C9-C10 µg/L 4.02
Page 8 of 194

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Yogi Foods Lab Report Number: 23-244-0003
Date: 9/15/2023
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1 Sample 93893 (MW-3) QC Batch No: V37430/V37391
Surrogate(s) was flagged for low recovery in this project sample. This sample will be re-analyzed for verification. Low surrogates. Associated QC is passing. No more volume for re-extraction.
Sample 93896 (MW-1)
QC Batch No: V37430/V37391 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the
extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due
to the sample matrix.
Analyte: Benzidine QC Batch No: V37430/V37391
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Benzoic Acid QC Batch No: V37430/V37391 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Benzyl alcohol QC Batch No: V37430/V37391
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Volatile Organic Compounds - GC/MS Method 6200B Analyte: 1,2,3-Trichlorobenzene
QC Batch No: V37564/V37563 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: 1,2,3-Trichlorobenzene QC Batch No: V37632/V37563 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Page 9 of 194

Analyte: 1,2,3-Trichlorobenzene
QC Batch No: V37731/V37563 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 3,3-Dimethyl-1-butanol
QC Batch No: V37496/V37563 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Dichlorodifluoromethane
QC Batch No: V37731/V37563 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Vinyl acetate
QC Batch No: V37835/V37563 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: tert-Amyl alcohol
QC Batch No: V37835/V37631 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Metals Analysis Method 6010D Sample 93894 (MW-4) QC Batch No: V37523/V37471
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Volatile Organic Compounds - GC/MS Method 8260D Sample 93884 (MW-2-10') QC Batch No: V37419/V37418 No vials received. Sample prepared from bulk container.
Sample 93887 (MW-3-10')
QC Batch No: V37419/V37418 No vials received. Sample prepared from bulk container. Sample 93785 (SB-7) Analyte: 1,1,1,2-Tetrachloroethane QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7) Analyte: 1,1,1-Trichloroethane QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 10 of 194

Sample 93785 (SB-7)
Analyte: 1,1-Dichloroethane QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7)
Analyte: 1,1-Dichloroethene QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7)
Analyte: 1,1-Dichloropropene QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7)
Analyte: 1,2-Dichloroethane QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7)
Analyte: 1,2-Dichloropropane QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7) Analyte: 1,3-Dichloropropane QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Analyte: 2-Butanone QC Batch No: V37419/V37418 CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and found acceptable. Results are reported but considered estimated.
Sample 93785 (SB-7) Analyte: 2-Butanone QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7) Analyte: 2-Chlorotoluene QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 11 of 194

Sample 93785 (SB-7)
Analyte: 2-Hexanone QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7)
Analyte: Acetone QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7)
Analyte: Acrolein QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7)
Analyte: Acrylonitrile QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7)
Analyte: Benzene QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7) Analyte: Bromochloromethane QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7) Analyte: Bromodichloromethane QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7) Analyte: Carbon Disulfide QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7) Analyte: Chlorobenzene QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 12 of 194

Sample 93785 (SB-7)
Analyte: Chloroform QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7)
Analyte: Chloromethane QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7)
Analyte: cis-1,2-Dichloroethene QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7)
Analyte: Di isopropyl ether QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7)
Analyte: Dibromomethane QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7) Analyte: Ethyl Tertiary Butyl Ether QC Batch No: V37419/V37418
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7) Analyte: Hexane QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7) Analyte: Methylene chloride QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 93785 (SB-7) Analyte: Toluene QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 13 of 194

Sample 93785 (SB-7) Analyte: trans-1,2-Dichloroethene
QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7) Analyte: Vinyl acetate
QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Sample 93785 (SB-7) Analyte: Vinyl chloride
QC Batch No: V37419/V37418 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference. Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 3-Nitroaniline
QC Batch No: V37578/V37441 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 4-Chloroaniline
QC Batch No: V37578/V37441 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Aniline
QC Batch No: V37467/V37441 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Aniline QC Batch No: V37578/V37441 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Sample 93889 (MW-4-5') Analyte: 2,4-Dimethylphenol QC Batch No: V37578/V37540 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 14 of 194

Sample 93889 (MW-4-5')
Analyte: 2-Nitroaniline QC Batch No: V37578/V37540
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93889 (MW-4-5')
Analyte: 3-Nitroaniline QC Batch No: V37578/V37540
Refer to LCS/LCSD.
Sample 93889 (MW-4-5') Analyte: 4-Chloroaniline
QC Batch No: V37578/V37540 Refer to LCS/LCSD.
Sample 93889 (MW-4-5')
Analyte: Aniline QC Batch No: V37578/V37540
Refer to LCS/LCSD.
Sample 93889 (MW-4-5') Analyte: Benzoic Acid QC Batch No: V37578/V37540 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Sample 93889 (MW-4-5') Analyte: N-Nitrosodiphenylamine QC Batch No: V37578/V37540 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 93889 (MW-4-5') Analyte: Pentachlorophenol
QC Batch No: V37578/V37540 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 15 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.0 %Moisture 1 09/01/23 14:50 SW-DRYWTCNC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.010 J mg/Kg - dry 0.003 0.025Acetone 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/01/23 17:53 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 09/01/23 17:53 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 17:53 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/01/23 17:53 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/01/23 17:53 V37419TBL
0.005 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/01/23 17:53 V37419TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/01/23 17:53 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 17:53 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/01/23 17:53 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 17:53 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/01/23 17:53 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/01/23 17:53 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/01/23 17:53 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 17:53 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 17:53 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 09/01/23 17:53 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 17:53 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 17:53 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 09/01/23 17:53 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 17:53 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 09/01/23 17:53 V37419TBL
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 09/01/23 17:53 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 17:53 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 18 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 17:53 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/01/23 17:53 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 17:53 V37419TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/01/23 17:53 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 17:53 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 17:53 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/01/23 17:53 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/01/23 17:53 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 17:53 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/01/23 17:53 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/01/23 17:53 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/01/23 17:53 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 19 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/01/23 17:53 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/01/23 17:53 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/01/23 17:53 V37419
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%09/01/23 17:531 TBL V37419
Surrogate: Dibromofluoromethane 108 Limits: 84-123%09/01/23 17:531 TBL V37419
Surrogate: Toluene-d8 98.8 Limits: 76-129%09/01/23 17:531 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.146 mg/Kg - dry 0.146 0.835Acenaphthene 1 09/07/23 00:48 V37467AMP
<0.132 mg/Kg - dry 0.132 0.835Acenaphthylene 1 09/07/23 00:48 V37467AMP
<0.192 mg/Kg - dry 0.192 0.835Aniline 1 09/07/23 00:48 V37467AMP
<0.181 mg/Kg - dry 0.181 0.835Anthracene 1 09/07/23 00:48 V37467AMP
<0.175 mg/Kg - dry 0.175 0.835Benzo(a)anthracene 1 09/07/23 00:48 V37467AMP
<0.186 mg/Kg - dry 0.186 0.835Benzo(a)pyrene 1 09/07/23 00:48 V37467AMP
<0.184 mg/Kg - dry 0.184 0.835Benzo(b)fluoranthene 1 09/07/23 00:48 V37467AMP
<0.172 mg/Kg - dry 0.172 0.835Benzo(g,h,i)perylene 1 09/07/23 00:48 V37467AMP
<0.173 mg/Kg - dry 0.173 0.835Benzo(k)fluoranthene 1 09/07/23 00:48 V37467AMP
<0.734 mg/Kg - dry 0.734 2.53Benzoic Acid 1 09/07/23 00:48 V37467AMP
<0.132 mg/Kg - dry 0.132 0.835Benzyl alcohol 1 09/07/23 00:48 V37467AMP
<0.149 mg/Kg - dry 0.149 0.835Bis(2-Chloroethoxy)methane 1 09/07/23 00:48 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 20 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.135 mg/Kg - dry 0.135 0.835Bis(2-Chloroethyl)ether 1 09/07/23 00:48 V37467AMP
<0.172 mg/Kg - dry 0.172 0.417Bis(2-Chloroisopropyl)ether 1 09/07/23 00:48 V37467AMP
<0.151 mg/Kg - dry 0.151 0.835Bis(2-ethylhexyl)phthalate 1 09/07/23 00:48 V37467AMP
<0.137 mg/Kg - dry 0.137 0.8354-Bromophenyl phenyl ether 1 09/07/23 00:48 V37467AMP
<0.143 mg/Kg - dry 0.143 0.417Butyl benzyl phthalate 1 09/07/23 00:48 V37467AMP
<0.116 mg/Kg - dry 0.116 0.8354-Chloro-3-methylphenol 1 09/07/23 00:48 V37467AMP
<0.141 mg/Kg - dry 0.141 0.4174-Chloroaniline 1 09/07/23 00:48 V37467AMP
<0.146 mg/Kg - dry 0.146 0.8352-Chloronaphthalene 1 09/07/23 00:48 V37467AMP
<0.124 mg/Kg - dry 0.124 0.8352-Chlorophenol 1 09/07/23 00:48 V37467AMP
<0.159 mg/Kg - dry 0.159 1.274-Chlorophenyl phenyl ether 1 09/07/23 00:48 V37467AMP
<0.179 mg/Kg - dry 0.179 0.835Chrysene 1 09/07/23 00:48 V37467AMP
<0.291 mg/Kg - dry 0.291 0.835Dibenz(a,h)anthracene 1 09/07/23 00:48 V37467AMP
<0.150 mg/Kg - dry 0.150 0.835Dibenzofuran 1 09/07/23 00:48 V37467AMP
<0.119 mg/Kg - dry 0.119 0.8351,2-Dichlorobenzene 1 09/07/23 00:48 V37467AMP
<0.123 mg/Kg - dry 0.123 0.8351,3-Dichlorobenzene 1 09/07/23 00:48 V37467AMP
<0.123 mg/Kg - dry 0.123 0.4171,4-Dichlorobenzene 1 09/07/23 00:48 V37467AMP
<0.186 mg/Kg - dry 0.186 0.8353,3'-Dichlorobenzidine 1 09/07/23 00:48 V37467AMP
<0.121 mg/Kg - dry 0.121 0.8352,4-Dichlorophenol 1 09/07/23 00:48 V37467AMP
<0.227 mg/Kg - dry 0.227 0.835Diethyl phthalate 1 09/07/23 00:48 V37467AMP
<0.220 mg/Kg - dry 0.220 0.835Dimethyl phthalate 1 09/07/23 00:48 V37467AMP
<0.136 mg/Kg - dry 0.136 0.4172,4-Dimethylphenol 1 09/07/23 00:48 V37467AMP
<0.135 mg/Kg - dry 0.135 0.835Di-n-butyl phthalate 1 09/07/23 00:48 V37467AMP
<0.303 mg/Kg - dry 0.303 1.904,6-Dinitro-2-methylphenol 1 09/07/23 00:48 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 21 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.658 mg/Kg - dry 0.658 1.902,4-Dinitrophenol 1 09/07/23 00:48 V37467AMP
<0.122 mg/Kg - dry 0.122 0.8352,4-Dinitrotoluene 1 09/07/23 00:48 V37467AMP
<0.136 mg/Kg - dry 0.136 0.8352,6-Dinitrotoluene 1 09/07/23 00:48 V37467AMP
<0.181 mg/Kg - dry 0.181 0.417Di-n-Octyl Phthalate 1 09/07/23 00:48 V37467AMP
<0.155 mg/Kg - dry 0.155 0.835Fluoranthene 1 09/07/23 00:48 V37467AMP
<0.162 mg/Kg - dry 0.162 0.835Fluorene 1 09/07/23 00:48 V37467AMP
<0.134 mg/Kg - dry 0.134 0.835Hexachlorobenzene 1 09/07/23 00:48 V37467AMP
<0.123 mg/Kg - dry 0.123 0.835Hexachlorobutadiene 1 09/07/23 00:48 V37467AMP
<0.198 mg/Kg - dry 0.198 0.835Hexachlorocyclopentadiene 1 09/07/23 00:48 V37467AMP
<0.100 mg/Kg - dry 0.100 0.835Hexachloroethane 1 09/07/23 00:48 V37467AMP
<0.226 mg/Kg - dry 0.226 0.835Indeno(1,2,3-cd)pyrene 1 09/07/23 00:48 V37467AMP
<0.241 mg/Kg - dry 0.241 0.835Isophorone 1 09/07/23 00:48 V37467AMP
<0.134 mg/Kg - dry 0.134 0.8351-Methylnaphthalene 1 09/07/23 00:48 V37467AMP
<0.126 mg/Kg - dry 0.126 0.8352-Methylnaphthalene 1 09/07/23 00:48 V37467AMP
<0.122 mg/Kg - dry 0.122 0.8352-Methylphenol 1 09/07/23 00:48 V37467AMP
<0.107 mg/Kg - dry 0.107 0.8353&4 Methylphenol 1 09/07/23 00:48 V37467AMP
<0.182 mg/Kg - dry 0.182 0.835Naphthalene 1 09/07/23 00:48 V37467AMP
<0.122 mg/Kg - dry 0.122 0.8352-Nitroaniline 1 09/07/23 00:48 V37467AMP
<0.151 mg/Kg - dry 0.151 0.8353-Nitroaniline 1 09/07/23 00:48 V37467AMP
<0.118 mg/Kg - dry 0.118 0.4174-Nitroaniline 1 09/07/23 00:48 V37467AMP
<0.146 mg/Kg - dry 0.146 0.417Nitrobenzene 1 09/07/23 00:48 V37467AMP
<0.112 mg/Kg - dry 0.112 0.8352-Nitrophenol 1 09/07/23 00:48 V37467AMP
<0.148 mg/Kg - dry 0.148 0.8354-Nitrophenol 1 09/07/23 00:48 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 22 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.332 mg/Kg - dry 0.332 0.835N-Nitrosodimethylamine 1 09/07/23 00:48 V37467AMP
<0.229 mg/Kg - dry 0.229 0.835N-Nitrosodiphenylamine 1 09/07/23 00:48 V37467AMP
<0.149 mg/Kg - dry 0.149 0.835N-Nitroso-di-n-propylamine 1 09/07/23 00:48 V37467AMP
<0.439 mg/Kg - dry 0.439 1.27Pentachlorophenol 1 09/07/23 00:48 V37467AMP
<0.263 mg/Kg - dry 0.263 0.835Phenanthrene 1 09/07/23 00:48 V37467AMP
<0.141 mg/Kg - dry 0.141 0.835Phenol 1 09/07/23 00:48 V37467AMP
<0.169 mg/Kg - dry 0.169 0.835Pyrene 1 09/07/23 00:48 V37467AMP
<0.100 mg/Kg - dry 0.100 0.417Pyridine 1 09/07/23 00:48 V37467AMP
<0.135 mg/Kg - dry 0.135 0.8351,2,4-Trichlorobenzene 1 09/07/23 00:48 V37467AMP
<0.121 mg/Kg - dry 0.121 0.8352,4,5-Trichlorophenol 1 09/07/23 00:48 V37467AMP
<0.122 mg/Kg - dry 0.122 0.8352,4,6-Trichlorophenol 1 09/07/23 00:48 V37467AMP
8270ESurrogate: Phenol-d5 69.1 Limits: 34-121%09/07/23 00:481 AMP
Surrogate: 2-Fluorobiphenyl 85.6 Limits: 44-115%09/07/23 00:481 AMP V37467
Surrogate: 2-Fluorophenol 71.5 Limits: 35-115%09/07/23 00:481 AMP V37467
Surrogate: Nitrobenzene-d5 56.8 Limits: 37-122%09/07/23 00:481 AMP V37467
Surrogate: 4-Terphenyl-d14 95.2 Limits: 54-127%09/07/23 00:481 AMP V37467
Surrogate: 2,4,6-Tribromophenol 73.9 Limits: 39-132%09/07/23 00:481 AMP V37467
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 23 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.54 mg/Kg - dry 1.54 10.1Aliphatic C5-C8 (Adjusted)1 09/01/23 17:53
<5.77 mg/Kg - dry 5.77 10.1Aliphatics C9-C12 (Adjusted)1 09/01/23 17:53
<0.789 mg/Kg - dry 0.789 10.1Aromatic C9-C10 (Adjusted)100 09/01/23 23:29
<17.8 mg/Kg - dry 17.8 63.0Aromatic C11-C22 (Adjusted)1 09/07/23 00:48
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V37493 09/06/23 11:50
<11.6 mg/Kg - dry 11.6 63.0Aliphatic C9-C18 1 09/13/23 10:46 V37620NDL
<15.4 mg/Kg - dry 15.4 63.0Aliphatic C19-C36 1 09/13/23 10:46 V37620NDL
<17.8 mg/Kg - dry 17.8 63.0Aromatic C11-C22 1 09/13/23 10:46 V37620NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 73.9 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: Chlorooctadecane 66.4 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: OTP Surrogate 75.2 Limits: 40-140%09/13/23 10:461 NDL
Surrogate: 2-Fluorobiphenyl 77.9 Limits: 40-140%09/13/23 10:461 NDL V37620
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<1.54 mg/Kg - dry 1.54 10.1Aliphatic C5-C8 100 09/01/23 23:29 V37397TBL
<5.77 mg/Kg - dry 5.77 10.1Aliphatic C9-C12 100 09/01/23 23:29 V37397TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 24 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-5'
93883 Matrix:
8/28/2023 11:02
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<0.789 mg/Kg - dry 0.789 10.1Aromatic C9-C10 100 09/01/23 23:29 V37397TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)98.2 Limits: 70-130%09/01/23 23:29100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)90.7 Limits: 70-130%09/01/23 23:29100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-10'
93884 Matrix:
8/28/2023 11:26
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.6 %Moisture 1 09/01/23 14:50 SW-DRYWTCNC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 26 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-10'
93884 Matrix:
8/28/2023 11:26
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.003 mg/Kg - dry 0.003 0.028Acetone 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.028Acrolein 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.028Acrylonitrile 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 09/01/23 18:20 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 09/01/23 18:20 V37419TBL
<0.002 mg/Kg - dry 0.002 0.014Bromomethane 1 09/01/23 18:20 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 09/01/23 18:20 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 09/01/23 18:20 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 09/01/23 18:20 V37419TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 09/01/23 18:20 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.007Chlorobenzene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorodibromomethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 09/01/23 18:20 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 09/01/23 18:20 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 09/01/23 18:20 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0074-Chlorotoluene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 09/01/23 18:20 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 09/01/23 18:20 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 27 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-10'
93884 Matrix:
8/28/2023 11:26
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0071,2-Dibromoethane 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 09/01/23 18:20 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0071,2-Dichlorobenzene 1 09/01/23 18:20 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,3-Dichlorobenzene 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,4-Dichlorobenzene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.014Dichlorodifluoromethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0071,2-Dichloroethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 09/01/23 18:20 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloropropene 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.070Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 09/01/23 18:20 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.014n-Hexane 1 09/01/23 18:20 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0282-Hexanone 1 09/01/23 18:20 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.007Isopropylbenzene 1 09/01/23 18:20 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 28 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-10'
93884 Matrix:
8/28/2023 11:26
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 09/01/23 18:20 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.028Methyl Ethyl Ketone (MEK)1 09/01/23 18:20 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 09/01/23 18:20 V37419TBL
<0.021 mg/Kg - dry 0.021 0.0284-Methyl-2-Pentanone 1 09/01/23 18:20 V37419TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.014Naphthalene 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007Styrene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 09/01/23 18:20 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0071,1,2,2-Tetrachloroethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 09/01/23 18:20 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.007Toluene 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 09/01/23 18:20 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 09/01/23 18:20 V37419TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 09/01/23 18:20 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 09/01/23 18:20 V37419TBL
<0.002 mg/Kg - dry 0.002 0.014Trichlorofluoromethane 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 09/01/23 18:20 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 09/01/23 18:20 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 09/01/23 18:20 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.014Vinyl Acetate 1 09/01/23 18:20 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 09/01/23 18:20 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 29 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-10'
93884 Matrix:
8/28/2023 11:26
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 09/01/23 18:20 V37419TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 09/01/23 18:20 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 09/01/23 18:20 V37419
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/01/23 18:201 TBL V37419
Surrogate: Dibromofluoromethane 104 Limits: 84-123%09/01/23 18:201 TBL V37419
Surrogate: Toluene-d8 98.8 Limits: 76-129%09/01/23 18:201 TBL V37419
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 30 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-10'
93884 Matrix:
8/28/2023 11:26
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.71 mg/Kg - dry 1.71 11.2Aliphatic C5-C8 (Adjusted)1 09/01/23 18:20
<6.39 mg/Kg - dry 6.39 11.2Aliphatics C9-C12 (Adjusted)1 09/01/23 18:20
<0.873 mg/Kg - dry 0.873 11.2Aromatic C9-C10 (Adjusted)100 09/01/23 23:53
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<1.71 mg/Kg - dry 1.71 11.2Aliphatic C5-C8 100 09/01/23 23:53 V37397TBL
<6.39 mg/Kg - dry 6.39 11.2Aliphatic C9-C12 100 09/01/23 23:53 V37397TBL
<0.873 mg/Kg - dry 0.873 11.2Aromatic C9-C10 100 09/01/23 23:53 V37397TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)90.8 Limits: 70-130%09/01/23 23:53100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)95.6 Limits: 70-130%09/01/23 23:53100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 31 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
26.0 %Moisture 1 09/01/23 14:50 SW-DRYWTCNC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 32 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.007 J mg/Kg - dry 0.003 0.027Acetone 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 09/01/23 18:47 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 18:47 V37419TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 09/01/23 18:47 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 09/01/23 18:47 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 09/01/23 18:47 V37419TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/01/23 18:47 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 18:47 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/01/23 18:47 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 18:47 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 18:47 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 09/01/23 18:47 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 33 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/01/23 18:47 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 09/01/23 18:47 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 18:47 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 18:47 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 09/01/23 18:47 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 18:47 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 18:47 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 09/01/23 18:47 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 09/01/23 18:47 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0272-Hexanone 1 09/01/23 18:47 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 18:47 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 34 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 18:47 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 09/01/23 18:47 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 18:47 V37419TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 18:47 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 18:47 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 09/01/23 18:47 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 18:47 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 18:47 V37419TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 09/01/23 18:47 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 18:47 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 09/01/23 18:47 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 09/01/23 18:47 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 35 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 09/01/23 18:47 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 09/01/23 18:47 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 09/01/23 18:47 V37419
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/01/23 18:471 TBL V37419
Surrogate: Dibromofluoromethane 108 Limits: 84-123%09/01/23 18:471 TBL V37419
Surrogate: Toluene-d8 99.8 Limits: 76-129%09/01/23 18:471 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.187 mg/Kg - dry 0.187 1.07Acenaphthene 1 09/06/23 20:17 V37467AMP
<0.170 mg/Kg - dry 0.170 1.07Acenaphthylene 1 09/06/23 20:17 V37467AMP
<0.245 mg/Kg - dry 0.245 1.07Aniline 1 09/06/23 20:17 V37467AMP
<0.232 mg/Kg - dry 0.232 1.07Anthracene 1 09/06/23 20:17 V37467AMP
<0.225 mg/Kg - dry 0.225 1.07Benzo(a)anthracene 1 09/06/23 20:17 V37467AMP
<0.237 mg/Kg - dry 0.237 1.07Benzo(a)pyrene 1 09/06/23 20:17 V37467AMP
<0.236 mg/Kg - dry 0.236 1.07Benzo(b)fluoranthene 1 09/06/23 20:17 V37467AMP
<0.220 mg/Kg - dry 0.220 1.07Benzo(g,h,i)perylene 1 09/06/23 20:17 V37467AMP
<0.221 mg/Kg - dry 0.221 1.07Benzo(k)fluoranthene 1 09/06/23 20:17 V37467AMP
<0.940 mg/Kg - dry 0.940 3.24Benzoic Acid 1 09/06/23 20:17 V37467AMP
<0.170 mg/Kg - dry 0.170 1.07Benzyl alcohol 1 09/06/23 20:17 V37467AMP
<0.191 mg/Kg - dry 0.191 1.07Bis(2-Chloroethoxy)methane 1 09/06/23 20:17 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 36 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.172 mg/Kg - dry 0.172 1.07Bis(2-Chloroethyl)ether 1 09/06/23 20:17 V37467AMP
<0.220 mg/Kg - dry 0.220 0.535Bis(2-Chloroisopropyl)ether 1 09/06/23 20:17 V37467AMP
<0.194 mg/Kg - dry 0.194 1.07Bis(2-ethylhexyl)phthalate 1 09/06/23 20:17 V37467AMP
<0.177 mg/Kg - dry 0.177 1.074-Bromophenyl phenyl ether 1 09/06/23 20:17 V37467AMP
<0.183 mg/Kg - dry 0.183 0.535Butyl benzyl phthalate 1 09/06/23 20:17 V37467AMP
<0.150 mg/Kg - dry 0.150 1.074-Chloro-3-methylphenol 1 09/06/23 20:17 V37467AMP
<0.181 mg/Kg - dry 0.181 0.5354-Chloroaniline 1 09/06/23 20:17 V37467AMP
<0.187 mg/Kg - dry 0.187 1.072-Chloronaphthalene 1 09/06/23 20:17 V37467AMP
<0.159 mg/Kg - dry 0.159 1.072-Chlorophenol 1 09/06/23 20:17 V37467AMP
<0.204 mg/Kg - dry 0.204 1.624-Chlorophenyl phenyl ether 1 09/06/23 20:17 V37467AMP
<0.229 mg/Kg - dry 0.229 1.07Chrysene 1 09/06/23 20:17 V37467AMP
<0.372 mg/Kg - dry 0.372 1.07Dibenz(a,h)anthracene 1 09/06/23 20:17 V37467AMP
<0.193 mg/Kg - dry 0.193 1.07Dibenzofuran 1 09/06/23 20:17 V37467AMP
<0.152 mg/Kg - dry 0.152 1.071,2-Dichlorobenzene 1 09/06/23 20:17 V37467AMP
<0.158 mg/Kg - dry 0.158 1.071,3-Dichlorobenzene 1 09/06/23 20:17 V37467AMP
<0.158 mg/Kg - dry 0.158 0.5351,4-Dichlorobenzene 1 09/06/23 20:17 V37467AMP
<0.237 mg/Kg - dry 0.237 1.073,3'-Dichlorobenzidine 1 09/06/23 20:17 V37467AMP
<0.155 mg/Kg - dry 0.155 1.072,4-Dichlorophenol 1 09/06/23 20:17 V37467AMP
<0.291 mg/Kg - dry 0.291 1.07Diethyl phthalate 1 09/06/23 20:17 V37467AMP
<0.282 mg/Kg - dry 0.282 1.07Dimethyl phthalate 1 09/06/23 20:17 V37467AMP
<0.175 mg/Kg - dry 0.175 0.5352,4-Dimethylphenol 1 09/06/23 20:17 V37467AMP
<0.172 mg/Kg - dry 0.172 1.07Di-n-butyl phthalate 1 09/06/23 20:17 V37467AMP
<0.389 mg/Kg - dry 0.389 2.434,6-Dinitro-2-methylphenol 1 09/06/23 20:17 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 37 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.843 mg/Kg - dry 0.843 2.432,4-Dinitrophenol 1 09/06/23 20:17 V37467AMP
<0.156 mg/Kg - dry 0.156 1.072,4-Dinitrotoluene 1 09/06/23 20:17 V37467AMP
<0.175 mg/Kg - dry 0.175 1.072,6-Dinitrotoluene 1 09/06/23 20:17 V37467AMP
<0.232 mg/Kg - dry 0.232 0.535Di-n-Octyl Phthalate 1 09/06/23 20:17 V37467AMP
<0.200 mg/Kg - dry 0.200 1.07Fluoranthene 1 09/06/23 20:17 V37467AMP
<0.208 mg/Kg - dry 0.208 1.07Fluorene 1 09/06/23 20:17 V37467AMP
<0.171 mg/Kg - dry 0.171 1.07Hexachlorobenzene 1 09/06/23 20:17 V37467AMP
<0.158 mg/Kg - dry 0.158 1.07Hexachlorobutadiene 1 09/06/23 20:17 V37467AMP
<0.254 mg/Kg - dry 0.254 1.07Hexachlorocyclopentadiene 1 09/06/23 20:17 V37467AMP
<0.128 mg/Kg - dry 0.128 1.07Hexachloroethane 1 09/06/23 20:17 V37467AMP
<0.290 mg/Kg - dry 0.290 1.07Indeno(1,2,3-cd)pyrene 1 09/06/23 20:17 V37467AMP
<0.309 mg/Kg - dry 0.309 1.07Isophorone 1 09/06/23 20:17 V37467AMP
<0.171 mg/Kg - dry 0.171 1.071-Methylnaphthalene 1 09/06/23 20:17 V37467AMP
<0.162 mg/Kg - dry 0.162 1.072-Methylnaphthalene 1 09/06/23 20:17 V37467AMP
<0.156 mg/Kg - dry 0.156 1.072-Methylphenol 1 09/06/23 20:17 V37467AMP
<0.137 mg/Kg - dry 0.137 1.073&4 Methylphenol 1 09/06/23 20:17 V37467AMP
<0.233 mg/Kg - dry 0.233 1.07Naphthalene 1 09/06/23 20:17 V37467AMP
<0.156 mg/Kg - dry 0.156 1.072-Nitroaniline 1 09/06/23 20:17 V37467AMP
<0.194 mg/Kg - dry 0.194 1.073-Nitroaniline 1 09/06/23 20:17 V37467AMP
<0.151 mg/Kg - dry 0.151 0.5354-Nitroaniline 1 09/06/23 20:17 V37467AMP
<0.187 mg/Kg - dry 0.187 0.535Nitrobenzene 1 09/06/23 20:17 V37467AMP
<0.144 mg/Kg - dry 0.144 1.072-Nitrophenol 1 09/06/23 20:17 V37467AMP
<0.189 mg/Kg - dry 0.189 1.074-Nitrophenol 1 09/06/23 20:17 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 38 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.427 mg/Kg - dry 0.427 1.07N-Nitrosodimethylamine 1 09/06/23 20:17 V37467AMP
<0.293 mg/Kg - dry 0.293 1.07N-Nitrosodiphenylamine 1 09/06/23 20:17 V37467AMP
<0.191 mg/Kg - dry 0.191 1.07N-Nitroso-di-n-propylamine 1 09/06/23 20:17 V37467AMP
<0.562 mg/Kg - dry 0.562 1.62Pentachlorophenol 1 09/06/23 20:17 V37467AMP
<0.337 mg/Kg - dry 0.337 1.07Phenanthrene 1 09/06/23 20:17 V37467AMP
<0.181 mg/Kg - dry 0.181 1.07Phenol 1 09/06/23 20:17 V37467AMP
<0.217 mg/Kg - dry 0.217 1.07Pyrene 1 09/06/23 20:17 V37467AMP
<0.128 mg/Kg - dry 0.128 0.535Pyridine 1 09/06/23 20:17 V37467AMP
<0.172 mg/Kg - dry 0.172 1.071,2,4-Trichlorobenzene 1 09/06/23 20:17 V37467AMP
<0.155 mg/Kg - dry 0.155 1.072,4,5-Trichlorophenol 1 09/06/23 20:17 V37467AMP
<0.156 mg/Kg - dry 0.156 1.072,4,6-Trichlorophenol 1 09/06/23 20:17 V37467AMP
8270ESurrogate: Phenol-d5 58.3 Limits: 34-121%09/06/23 20:171 AMP
Surrogate: 2-Fluorobiphenyl 69.5 Limits: 44-115%09/06/23 20:171 AMP V37467
Surrogate: 2-Fluorophenol 61.8 Limits: 35-115%09/06/23 20:171 AMP V37467
Surrogate: Nitrobenzene-d5 62.5 Limits: 37-122%09/06/23 20:171 AMP V37467
Surrogate: 4-Terphenyl-d14 74.5 Limits: 54-127%09/06/23 20:171 AMP V37467
Surrogate: 2,4,6-Tribromophenol 60.0 Limits: 39-132%09/06/23 20:171 AMP V37467
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 39 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.65 mg/Kg - dry 1.65 10.8Aliphatic C5-C8 (Adjusted)1 09/01/23 18:47
<6.16 mg/Kg - dry 6.16 10.8Aliphatics C9-C12 (Adjusted)1 09/01/23 18:47
<0.843 mg/Kg - dry 0.843 10.8Aromatic C9-C10 (Adjusted)100 09/02/23 00:16
<19.1 mg/Kg - dry 19.1 67.3Aromatic C11-C22 (Adjusted)1 09/06/23 20:17
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V37493 09/06/23 11:50
<12.4 mg/Kg - dry 12.4 67.3Aliphatic C9-C18 1 09/13/23 10:46 V37620NDL
<16.5 mg/Kg - dry 16.5 67.3Aliphatic C19-C36 1 09/13/23 10:46 V37620NDL
<19.1 mg/Kg - dry 19.1 67.3Aromatic C11-C22 1 09/13/23 10:46 V37620NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 74.1 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: Chlorooctadecane 64.4 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: OTP Surrogate 70.0 Limits: 40-140%09/13/23 10:461 NDL
Surrogate: 2-Fluorobiphenyl 77.1 Limits: 40-140%09/13/23 10:461 NDL V37620
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<1.65 mg/Kg - dry 1.65 10.8Aliphatic C5-C8 100 09/02/23 00:16 V37397TBL
<6.16 mg/Kg - dry 6.16 10.8Aliphatic C9-C12 100 09/02/23 00:16 V37397TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 40 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2-15'
93885 Matrix:
8/28/2023 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<0.843 mg/Kg - dry 0.843 10.8Aromatic C9-C10 100 09/02/23 00:16 V37397TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)91.9 Limits: 70-130%09/02/23 00:16100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)88.4 Limits: 70-130%09/02/23 00:16100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 41 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.9 %Moisture 1 09/01/23 14:50 SW-DRYWTCNC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 42 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.039 mg/Kg - dry 0.002 0.024Acetone 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 09/01/23 19:14 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/01/23 19:14 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 19:14 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/01/23 19:14 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/01/23 19:14 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 19:14 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/01/23 19:14 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 19:14 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 19:14 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 09/01/23 19:14 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 43 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/01/23 19:14 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 19:14 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 09/01/23 19:14 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/01/23 19:14 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 19:14 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 19:14 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 19:14 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 19:14 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/01/23 19:14 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/01/23 19:14 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 19:14 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 44 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 19:14 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 09/01/23 19:14 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 19:14 V37419TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 19:14 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 19:14 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/01/23 19:14 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 19:14 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/01/23 19:14 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/01/23 19:14 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/01/23 19:14 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 45 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/01/23 19:14 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/01/23 19:14 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/01/23 19:14 V37419KCC
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%09/01/23 19:141 TBL V37419
Surrogate: Dibromofluoromethane 107 Limits: 84-123%09/01/23 19:141 TBL V37419
Surrogate: Toluene-d8 98.7 Limits: 76-129%09/01/23 19:141 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.144 mg/Kg - dry 0.144 0.823Acenaphthene 1 09/07/23 01:11 V37467AMP
0.318 J mg/Kg - dry 0.131 0.823Acenaphthylene 1 09/07/23 01:11 V37467AMP
<0.189 mg/Kg - dry 0.189 0.823Aniline 1 09/07/23 01:11 V37467AMP
0.218 J mg/Kg - dry 0.178 0.823Anthracene 1 09/07/23 01:11 V37467AMP
0.905 mg/Kg - dry 0.173 0.823Benzo(a)anthracene 1 09/07/23 01:11 V37467AMP
1.05 mg/Kg - dry 0.183 0.823Benzo(a)pyrene 1 09/07/23 01:11 V37467AMP
1.24 mg/Kg - dry 0.182 0.823Benzo(b)fluoranthene 1 09/07/23 01:11 V37467AMP
0.604 J mg/Kg - dry 0.169 0.823Benzo(g,h,i)perylene 1 09/07/23 01:11 V37467AMP
0.488 J mg/Kg - dry 0.171 0.823Benzo(k)fluoranthene 1 09/07/23 01:11 V37467AMP
<0.724 mg/Kg - dry 0.724 2.50Benzoic Acid 1 09/07/23 01:11 V37467AMP
<0.131 mg/Kg - dry 0.131 0.823Benzyl alcohol 1 09/07/23 01:11 V37467AMP
<0.147 mg/Kg - dry 0.147 0.823Bis(2-Chloroethoxy)methane 1 09/07/23 01:11 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 46 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.133 mg/Kg - dry 0.133 0.823Bis(2-Chloroethyl)ether 1 09/07/23 01:11 V37467AMP
<0.169 mg/Kg - dry 0.169 0.411Bis(2-Chloroisopropyl)ether 1 09/07/23 01:11 V37467AMP
<0.149 mg/Kg - dry 0.149 0.823Bis(2-ethylhexyl)phthalate 1 09/07/23 01:11 V37467AMP
<0.136 mg/Kg - dry 0.136 0.8234-Bromophenyl phenyl ether 1 09/07/23 01:11 V37467AMP
<0.141 mg/Kg - dry 0.141 0.411Butyl benzyl phthalate 1 09/07/23 01:11 V37467AMP
<0.115 mg/Kg - dry 0.115 0.8234-Chloro-3-methylphenol 1 09/07/23 01:11 V37467AMP
<0.139 mg/Kg - dry 0.139 0.4114-Chloroaniline 1 09/07/23 01:11 V37467AMP
<0.144 mg/Kg - dry 0.144 0.8232-Chloronaphthalene 1 09/07/23 01:11 V37467AMP
<0.122 mg/Kg - dry 0.122 0.8232-Chlorophenol 1 09/07/23 01:11 V37467AMP
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 09/07/23 01:11 V37467AMP
0.927 mg/Kg - dry 0.177 0.823Chrysene 1 09/07/23 01:11 V37467AMP
<0.287 mg/Kg - dry 0.287 0.823Dibenz(a,h)anthracene 1 09/07/23 01:11 V37467AMP
<0.148 mg/Kg - dry 0.148 0.823Dibenzofuran 1 09/07/23 01:11 V37467AMP
<0.117 mg/Kg - dry 0.117 0.8231,2-Dichlorobenzene 1 09/07/23 01:11 V37467AMP
<0.121 mg/Kg - dry 0.121 0.8231,3-Dichlorobenzene 1 09/07/23 01:11 V37467AMP
<0.121 mg/Kg - dry 0.121 0.4111,4-Dichlorobenzene 1 09/07/23 01:11 V37467AMP
<0.183 mg/Kg - dry 0.183 0.8233,3'-Dichlorobenzidine 1 09/07/23 01:11 V37467AMP
<0.119 mg/Kg - dry 0.119 0.8232,4-Dichlorophenol 1 09/07/23 01:11 V37467AMP
<0.224 mg/Kg - dry 0.224 0.823Diethyl phthalate 1 09/07/23 01:11 V37467AMP
<0.217 mg/Kg - dry 0.217 0.823Dimethyl phthalate 1 09/07/23 01:11 V37467AMP
<0.134 mg/Kg - dry 0.134 0.4112,4-Dimethylphenol 1 09/07/23 01:11 V37467AMP
<0.133 mg/Kg - dry 0.133 0.823Di-n-butyl phthalate 1 09/07/23 01:11 V37467AMP
<0.299 mg/Kg - dry 0.299 1.874,6-Dinitro-2-methylphenol 1 09/07/23 01:11 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 47 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.649 mg/Kg - dry 0.649 1.872,4-Dinitrophenol 1 09/07/23 01:11 V37467AMP
<0.120 mg/Kg - dry 0.120 0.8232,4-Dinitrotoluene 1 09/07/23 01:11 V37467AMP
<0.134 mg/Kg - dry 0.134 0.8232,6-Dinitrotoluene 1 09/07/23 01:11 V37467AMP
<0.178 mg/Kg - dry 0.178 0.411Di-n-Octyl Phthalate 1 09/07/23 01:11 V37467AMP
2.06 mg/Kg - dry 0.153 0.823Fluoranthene 1 09/07/23 01:11 V37467AMP
<0.159 mg/Kg - dry 0.159 0.823Fluorene 1 09/07/23 01:11 V37467AMP
<0.132 mg/Kg - dry 0.132 0.823Hexachlorobenzene 1 09/07/23 01:11 V37467AMP
<0.121 mg/Kg - dry 0.121 0.823Hexachlorobutadiene 1 09/07/23 01:11 V37467AMP
<0.196 mg/Kg - dry 0.196 0.823Hexachlorocyclopentadiene 1 09/07/23 01:11 V37467AMP
<0.098 mg/Kg - dry 0.098 0.823Hexachloroethane 1 09/07/23 01:11 V37467AMP
0.714 J mg/Kg - dry 0.223 0.823Indeno(1,2,3-cd)pyrene 1 09/07/23 01:11 V37467AMP
<0.238 mg/Kg - dry 0.238 0.823Isophorone 1 09/07/23 01:11 V37467AMP
<0.132 mg/Kg - dry 0.132 0.8231-Methylnaphthalene 1 09/07/23 01:11 V37467AMP
<0.124 mg/Kg - dry 0.124 0.8232-Methylnaphthalene 1 09/07/23 01:11 V37467AMP
<0.121 mg/Kg - dry 0.121 0.8232-Methylphenol 1 09/07/23 01:11 V37467AMP
<0.105 mg/Kg - dry 0.105 0.8233&4 Methylphenol 1 09/07/23 01:11 V37467AMP
<0.179 mg/Kg - dry 0.179 0.823Naphthalene 1 09/07/23 01:11 V37467AMP
<0.120 mg/Kg - dry 0.120 0.8232-Nitroaniline 1 09/07/23 01:11 V37467AMP
<0.149 mg/Kg - dry 0.149 0.8233-Nitroaniline 1 09/07/23 01:11 V37467AMP
<0.116 mg/Kg - dry 0.116 0.4114-Nitroaniline 1 09/07/23 01:11 V37467AMP
<0.144 mg/Kg - dry 0.144 0.411Nitrobenzene 1 09/07/23 01:11 V37467AMP
<0.110 mg/Kg - dry 0.110 0.8232-Nitrophenol 1 09/07/23 01:11 V37467AMP
<0.146 mg/Kg - dry 0.146 0.8234-Nitrophenol 1 09/07/23 01:11 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 48 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.328 mg/Kg - dry 0.328 0.823N-Nitrosodimethylamine 1 09/07/23 01:11 V37467AMP
<0.225 mg/Kg - dry 0.225 0.823N-Nitrosodiphenylamine 1 09/07/23 01:11 V37467AMP
<0.147 mg/Kg - dry 0.147 0.823N-Nitroso-di-n-propylamine 1 09/07/23 01:11 V37467AMP
<0.433 mg/Kg - dry 0.433 1.25Pentachlorophenol 1 09/07/23 01:11 V37467AMP
0.466 J mg/Kg - dry 0.259 0.823Phenanthrene 1 09/07/23 01:11 V37467AMP
<0.139 mg/Kg - dry 0.139 0.823Phenol 1 09/07/23 01:11 V37467AMP
2.36 mg/Kg - dry 0.167 0.823Pyrene 1 09/07/23 01:11 V37467AMP
<0.098 mg/Kg - dry 0.098 0.411Pyridine 1 09/07/23 01:11 V37467AMP
<0.133 mg/Kg - dry 0.133 0.8231,2,4-Trichlorobenzene 1 09/07/23 01:11 V37467AMP
<0.120 mg/Kg - dry 0.120 0.8232,4,5-Trichlorophenol 1 09/07/23 01:11 V37467AMP
<0.120 mg/Kg - dry 0.120 0.8232,4,6-Trichlorophenol 1 09/07/23 01:11 V37467AMP
8270ESurrogate: Phenol-d5 79.9 Limits: 34-121%09/07/23 01:111 AMP
Surrogate: 2-Fluorobiphenyl 97.6 Limits: 44-115%09/07/23 01:111 AMP V37467
Surrogate: 2-Fluorophenol 83.2 Limits: 35-115%09/07/23 01:111 AMP V37467
Surrogate: Nitrobenzene-d5 89.8 Limits: 37-122%09/07/23 01:111 AMP V37467
Surrogate: 4-Terphenyl-d14 104 Limits: 54-127%09/07/23 01:111 AMP V37467
Surrogate: 2,4,6-Tribromophenol 83.2 Limits: 39-132%09/07/23 01:111 AMP V37467
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 49 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.52 mg/Kg - dry 1.52 9.99Aliphatic C5-C8 (Adjusted)1 09/01/23 19:14
<5.69 mg/Kg - dry 5.69 9.99Aliphatics C9-C12 (Adjusted)1 09/01/23 19:14
<0.779 mg/Kg - dry 0.779 9.99Aromatic C9-C10 (Adjusted)100 09/02/23 00:40
<17.7 mg/Kg - dry 17.7 62.4Aromatic C11-C22 (Adjusted)1 09/13/23 10:46
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V37493 09/06/23 11:50
<11.5 mg/Kg - dry 11.5 62.4Aliphatic C9-C18 1 09/13/23 10:46 V37620NDL
<15.2 mg/Kg - dry 15.2 62.4Aliphatic C19-C36 1 09/13/23 10:46 V37620NDL
<17.7 mg/Kg - dry 17.7 62.4Aromatic C11-C22 1 09/13/23 10:46 V37620NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 73.5 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: Chlorooctadecane 65.1 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: OTP Surrogate 72.3 Limits: 40-140%09/13/23 10:461 NDL
Surrogate: 2-Fluorobiphenyl 78.5 Limits: 40-140%09/13/23 10:461 NDL V37620
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<1.52 mg/Kg - dry 1.52 9.99Aliphatic C5-C8 100 09/02/23 00:40 V37397TBL
<5.69 mg/Kg - dry 5.69 9.99Aliphatic C9-C12 100 09/02/23 00:40 V37397TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 50 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-5'
93886 Matrix:
8/28/2023 11:56
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<0.779 mg/Kg - dry 0.779 9.99Aromatic C9-C10 100 09/02/23 00:40 V37397TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)81.1 Limits: 70-130%09/02/23 00:40100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)88.7 Limits: 70-130%09/02/23 00:40100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 51 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-10'
93887 Matrix:
8/28/2023 12:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.0 %Moisture 1 09/01/23 14:50 SW-DRYWTCNC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 52 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-10'
93887 Matrix:
8/28/2023 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.003 mg/Kg - dry 0.003 0.025Acetone 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/01/23 19:41 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 19:41 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/01/23 19:41 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/01/23 19:41 V37419TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/01/23 19:41 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 19:41 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/01/23 19:41 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 19:41 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/01/23 19:41 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 53 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-10'
93887 Matrix:
8/28/2023 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/01/23 19:41 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 19:41 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 19:41 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 09/01/23 19:41 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 19:41 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 09/01/23 19:41 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/01/23 19:41 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 19:41 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 54 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-10'
93887 Matrix:
8/28/2023 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 19:41 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/01/23 19:41 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 19:41 V37419TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 19:41 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 19:41 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/01/23 19:41 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 19:41 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/01/23 19:41 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/01/23 19:41 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/01/23 19:41 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 55 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-10'
93887 Matrix:
8/28/2023 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/01/23 19:41 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/01/23 19:41 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/01/23 19:41 V37419
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%09/01/23 19:411 TBL V37419
Surrogate: Dibromofluoromethane 105 Limits: 84-123%09/01/23 19:411 TBL V37419
Surrogate: Toluene-d8 100 Limits: 76-129%09/01/23 19:411 TBL V37419
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 56 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-10'
93887 Matrix:
8/28/2023 12:00
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.56 mg/Kg - dry 1.56 10.3Aliphatic C5-C8 (Adjusted)1 09/01/23 19:41
<5.85 mg/Kg - dry 5.85 10.3Aliphatics C9-C12 (Adjusted)1 09/01/23 19:41
<0.800 mg/Kg - dry 0.800 10.3Aromatic C9-C10 (Adjusted)100 09/02/23 01:03
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<1.56 mg/Kg - dry 1.56 10.3Aliphatic C5-C8 100 09/02/23 01:03 V37397TBL
<5.85 mg/Kg - dry 5.85 10.3Aliphatic C9-C12 100 09/02/23 01:03 V37397TBL
<0.800 mg/Kg - dry 0.800 10.3Aromatic C9-C10 100 09/02/23 01:03 V37397TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)100 Limits: 70-130%09/02/23 01:03100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)103 Limits: 70-130%09/02/23 01:03100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 57 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.4 %Moisture 1 09/01/23 14:50 SW-DRYWTCNC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 58 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.014 J mg/Kg - dry 0.003 0.026Acetone 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 09/01/23 20:08 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 09/01/23 20:08 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 20:08 V37419TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 09/01/23 20:08 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 09/01/23 20:08 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/01/23 20:08 V37419TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/01/23 20:08 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 20:08 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/01/23 20:08 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 20:08 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 20:08 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 09/01/23 20:08 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 59 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/01/23 20:08 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 20:08 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 20:08 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 09/01/23 20:08 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 20:08 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 20:08 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 20:08 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 09/01/23 20:08 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 09/01/23 20:08 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 09/01/23 20:08 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 20:08 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 60 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 20:08 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.026Methyl Ethyl Ketone (MEK)1 09/01/23 20:08 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 20:08 V37419TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 20:08 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 20:08 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 09/01/23 20:08 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 20:08 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 20:08 V37419TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 09/01/23 20:08 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/01/23 20:08 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 20:08 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 09/01/23 20:08 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 09/01/23 20:08 V37419TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 61 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 09/01/23 20:08 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 09/01/23 20:08 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 09/01/23 20:08 V37419
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/01/23 20:081 TBL V37419
Surrogate: Dibromofluoromethane 107 Limits: 84-123%09/01/23 20:081 TBL V37419
Surrogate: Toluene-d8 98.9 Limits: 76-129%09/01/23 20:081 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.151 mg/Kg - dry 0.151 0.861Acenaphthene 1 09/06/23 20:39 V37467AMP
<0.137 mg/Kg - dry 0.137 0.861Acenaphthylene 1 09/06/23 20:39 V37467AMP
<0.198 mg/Kg - dry 0.198 0.861Aniline 1 09/06/23 20:39 V37467AMP
<0.186 mg/Kg - dry 0.186 0.861Anthracene 1 09/06/23 20:39 V37467AMP
<0.181 mg/Kg - dry 0.181 0.861Benzo(a)anthracene 1 09/06/23 20:39 V37467AMP
<0.191 mg/Kg - dry 0.191 0.861Benzo(a)pyrene 1 09/06/23 20:39 V37467AMP
<0.190 mg/Kg - dry 0.190 0.861Benzo(b)fluoranthene 1 09/06/23 20:39 V37467AMP
<0.177 mg/Kg - dry 0.177 0.861Benzo(g,h,i)perylene 1 09/06/23 20:39 V37467AMP
<0.178 mg/Kg - dry 0.178 0.861Benzo(k)fluoranthene 1 09/06/23 20:39 V37467AMP
<0.757 mg/Kg - dry 0.757 2.61Benzoic Acid 1 09/06/23 20:39 V37467AMP
<0.137 mg/Kg - dry 0.137 0.861Benzyl alcohol 1 09/06/23 20:39 V37467AMP
<0.154 mg/Kg - dry 0.154 0.861Bis(2-Chloroethoxy)methane 1 09/06/23 20:39 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 62 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.139 mg/Kg - dry 0.139 0.861Bis(2-Chloroethyl)ether 1 09/06/23 20:39 V37467AMP
<0.177 mg/Kg - dry 0.177 0.430Bis(2-Chloroisopropyl)ether 1 09/06/23 20:39 V37467AMP
<0.156 mg/Kg - dry 0.156 0.861Bis(2-ethylhexyl)phthalate 1 09/06/23 20:39 V37467AMP
<0.142 mg/Kg - dry 0.142 0.8614-Bromophenyl phenyl ether 1 09/06/23 20:39 V37467AMP
<0.147 mg/Kg - dry 0.147 0.430Butyl benzyl phthalate 1 09/06/23 20:39 V37467AMP
<0.120 mg/Kg - dry 0.120 0.8614-Chloro-3-methylphenol 1 09/06/23 20:39 V37467AMP
<0.146 mg/Kg - dry 0.146 0.4304-Chloroaniline 1 09/06/23 20:39 V37467AMP
<0.151 mg/Kg - dry 0.151 0.8612-Chloronaphthalene 1 09/06/23 20:39 V37467AMP
<0.128 mg/Kg - dry 0.128 0.8612-Chlorophenol 1 09/06/23 20:39 V37467AMP
<0.164 mg/Kg - dry 0.164 1.314-Chlorophenyl phenyl ether 1 09/06/23 20:39 V37467AMP
<0.185 mg/Kg - dry 0.185 0.861Chrysene 1 09/06/23 20:39 V37467AMP
<0.300 mg/Kg - dry 0.300 0.861Dibenz(a,h)anthracene 1 09/06/23 20:39 V37467AMP
<0.155 mg/Kg - dry 0.155 0.861Dibenzofuran 1 09/06/23 20:39 V37467AMP
<0.123 mg/Kg - dry 0.123 0.8611,2-Dichlorobenzene 1 09/06/23 20:39 V37467AMP
<0.127 mg/Kg - dry 0.127 0.8611,3-Dichlorobenzene 1 09/06/23 20:39 V37467AMP
<0.127 mg/Kg - dry 0.127 0.4301,4-Dichlorobenzene 1 09/06/23 20:39 V37467AMP
<0.191 mg/Kg - dry 0.191 0.8613,3'-Dichlorobenzidine 1 09/06/23 20:39 V37467AMP
<0.125 mg/Kg - dry 0.125 0.8612,4-Dichlorophenol 1 09/06/23 20:39 V37467AMP
<0.234 mg/Kg - dry 0.234 0.861Diethyl phthalate 1 09/06/23 20:39 V37467AMP
<0.227 mg/Kg - dry 0.227 0.861Dimethyl phthalate 1 09/06/23 20:39 V37467AMP
<0.140 mg/Kg - dry 0.140 0.4302,4-Dimethylphenol 1 09/06/23 20:39 V37467AMP
<0.139 mg/Kg - dry 0.139 0.861Di-n-butyl phthalate 1 09/06/23 20:39 V37467AMP
<0.313 mg/Kg - dry 0.313 1.964,6-Dinitro-2-methylphenol 1 09/06/23 20:39 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 63 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.678 mg/Kg - dry 0.678 1.962,4-Dinitrophenol 1 09/06/23 20:39 V37467AMP
<0.126 mg/Kg - dry 0.126 0.8612,4-Dinitrotoluene 1 09/06/23 20:39 V37467AMP
<0.140 mg/Kg - dry 0.140 0.8612,6-Dinitrotoluene 1 09/06/23 20:39 V37467AMP
<0.186 mg/Kg - dry 0.186 0.430Di-n-Octyl Phthalate 1 09/06/23 20:39 V37467AMP
<0.160 mg/Kg - dry 0.160 0.861Fluoranthene 1 09/06/23 20:39 V37467AMP
<0.167 mg/Kg - dry 0.167 0.861Fluorene 1 09/06/23 20:39 V37467AMP
<0.138 mg/Kg - dry 0.138 0.861Hexachlorobenzene 1 09/06/23 20:39 V37467AMP
<0.127 mg/Kg - dry 0.127 0.861Hexachlorobutadiene 1 09/06/23 20:39 V37467AMP
<0.204 mg/Kg - dry 0.204 0.861Hexachlorocyclopentadiene 1 09/06/23 20:39 V37467AMP
<0.103 mg/Kg - dry 0.103 0.861Hexachloroethane 1 09/06/23 20:39 V37467AMP
<0.233 mg/Kg - dry 0.233 0.861Indeno(1,2,3-cd)pyrene 1 09/06/23 20:39 V37467AMP
<0.249 mg/Kg - dry 0.249 0.861Isophorone 1 09/06/23 20:39 V37467AMP
<0.138 mg/Kg - dry 0.138 0.8611-Methylnaphthalene 1 09/06/23 20:39 V37467AMP
<0.130 mg/Kg - dry 0.130 0.8612-Methylnaphthalene 1 09/06/23 20:39 V37467AMP
<0.126 mg/Kg - dry 0.126 0.8612-Methylphenol 1 09/06/23 20:39 V37467AMP
<0.110 mg/Kg - dry 0.110 0.8613&4 Methylphenol 1 09/06/23 20:39 V37467AMP
<0.187 mg/Kg - dry 0.187 0.861Naphthalene 1 09/06/23 20:39 V37467AMP
<0.126 mg/Kg - dry 0.126 0.8612-Nitroaniline 1 09/06/23 20:39 V37467AMP
<0.156 mg/Kg - dry 0.156 0.8613-Nitroaniline 1 09/06/23 20:39 V37467AMP
<0.121 mg/Kg - dry 0.121 0.4304-Nitroaniline 1 09/06/23 20:39 V37467AMP
<0.151 mg/Kg - dry 0.151 0.430Nitrobenzene 1 09/06/23 20:39 V37467AMP
<0.115 mg/Kg - dry 0.115 0.8612-Nitrophenol 1 09/06/23 20:39 V37467AMP
<0.152 mg/Kg - dry 0.152 0.8614-Nitrophenol 1 09/06/23 20:39 V37467AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 64 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.343 mg/Kg - dry 0.343 0.861N-Nitrosodimethylamine 1 09/06/23 20:39 V37467AMP
<0.236 mg/Kg - dry 0.236 0.861N-Nitrosodiphenylamine 1 09/06/23 20:39 V37467AMP
<0.154 mg/Kg - dry 0.154 0.861N-Nitroso-di-n-propylamine 1 09/06/23 20:39 V37467AMP
<0.453 mg/Kg - dry 0.453 1.31Pentachlorophenol 1 09/06/23 20:39 V37467AMP
<0.271 mg/Kg - dry 0.271 0.861Phenanthrene 1 09/06/23 20:39 V37467AMP
<0.146 mg/Kg - dry 0.146 0.861Phenol 1 09/06/23 20:39 V37467AMP
<0.174 mg/Kg - dry 0.174 0.861Pyrene 1 09/06/23 20:39 V37467AMP
<0.103 mg/Kg - dry 0.103 0.430Pyridine 1 09/06/23 20:39 V37467AMP
<0.139 mg/Kg - dry 0.139 0.8611,2,4-Trichlorobenzene 1 09/06/23 20:39 V37467AMP
<0.125 mg/Kg - dry 0.125 0.8612,4,5-Trichlorophenol 1 09/06/23 20:39 V37467AMP
<0.126 mg/Kg - dry 0.126 0.8612,4,6-Trichlorophenol 1 09/06/23 20:39 V37467AMP
8270ESurrogate: Phenol-d5 79.3 Limits: 34-121%09/06/23 20:391 AMP
Surrogate: 2-Fluorobiphenyl 93.4 Limits: 44-115%09/06/23 20:391 AMP V37467
Surrogate: 2-Fluorophenol 82.0 Limits: 35-115%09/06/23 20:391 AMP V37467
Surrogate: Nitrobenzene-d5 85.6 Limits: 37-122%09/06/23 20:391 AMP V37467
Surrogate: 4-Terphenyl-d14 98.8 Limits: 54-127%09/06/23 20:391 AMP V37467
Surrogate: 2,4,6-Tribromophenol 85.9 Limits: 39-132%09/06/23 20:391 AMP V37467
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 65 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.76 mg/Kg - dry 1.76 11.6Aliphatic C5-C8 (Adjusted)1 09/01/23 20:08
<6.62 mg/Kg - dry 6.62 11.6Aliphatics C9-C12 (Adjusted)1 09/01/23 20:08
<0.904 mg/Kg - dry 0.904 11.6Aromatic C9-C10 (Adjusted)100 09/02/23 01:27
<18.7 mg/Kg - dry 18.7 65.7Aromatic C11-C22 (Adjusted)1 09/06/23 20:39
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V37493 09/06/23 11:50
<12.1 mg/Kg - dry 12.1 65.7Aliphatic C9-C18 1 09/13/23 10:46 V37620NDL
<16.1 mg/Kg - dry 16.1 65.7Aliphatic C19-C36 1 09/13/23 10:46 V37620NDL
<18.7 mg/Kg - dry 18.7 65.7Aromatic C11-C22 1 09/13/23 10:46 V37620NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 79.1 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: Chlorooctadecane 69.8 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: OTP Surrogate 79.1 Limits: 40-140%09/13/23 10:461 NDL
Surrogate: 2-Fluorobiphenyl 82.3 Limits: 40-140%09/13/23 10:461 NDL V37620
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<1.76 mg/Kg - dry 1.76 11.6Aliphatic C5-C8 100 09/02/23 01:27 V37397TBL
<6.62 mg/Kg - dry 6.62 11.6Aliphatic C9-C12 100 09/02/23 01:27 V37397TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 66 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3-15'
93888 Matrix:
8/28/2023 12:03
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<0.904 mg/Kg - dry 0.904 11.6Aromatic C9-C10 100 09/02/23 01:27 V37397TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)80.3 Limits: 70-130%09/02/23 01:27100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)90.2 Limits: 70-130%09/02/23 01:27100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 67 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.3 %Moisture 1 09/01/23 14:50 SW-DRYWTCNC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 68 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
0.030 mg/Kg - dry 0.003 0.025Acetone 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/01/23 20:35 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 09/01/23 20:35 V37422TBL
0.001 J mg/Kg - dry 0.0007 0.006Benzene 1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 20:35 V37422TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/01/23 20:35 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/01/23 20:35 V37422TBL
0.002 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/01/23 20:35 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 20:35 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/01/23 20:35 V37422TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 20:35 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/01/23 20:35 V37422TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 69 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/01/23 20:35 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/01/23 20:35 V37422TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 20:35 V37422TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 20:35 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 09/01/23 20:35 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/01/23 20:35 V37422TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 20:35 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 20:35 V37422TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 09/01/23 20:35 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 20:35 V37422TBL
0.002 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 20:35 V37422TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/01/23 20:35 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/01/23 20:35 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 20:35 V37422TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 70 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 20:35 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/01/23 20:35 V37422TBL
0.010 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 20:35 V37422TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/01/23 20:35 V37422TBL
0.0008 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 20:35 V37422TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 20:35 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/01/23 20:35 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/01/23 20:35 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 20:35 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 20:35 V37422TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/01/23 20:35 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/01/23 20:35 V37422TBL
0.006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/01/23 20:35 V37422TBL
0.002 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/01/23 20:35 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/01/23 20:35 V37422TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 71 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
0.002 J mg/Kg - dry 0.0006 0.006o-Xylene 1 09/01/23 20:35 V37422TBL
0.007 J mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/01/23 20:35 V37422TBL
0.009 J mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/01/23 20:35 V37422KCC
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/01/23 20:351 TBL V37422
Surrogate: Dibromofluoromethane 107 Limits: 84-123%09/01/23 20:351 TBL V37422
Surrogate: Toluene-d8 99.1 Limits: 76-129%09/01/23 20:351 TBL V37422
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37540 09/07/23 10:00
<0.145 mg/Kg - dry 0.145 0.828Acenaphthene 1 09/08/23 16:00 V37578AMP
<0.131 mg/Kg - dry 0.131 0.828Acenaphthylene 1 09/08/23 16:00 V37578AMP
<0.190 mg/Kg - dry 0.190 0.828Aniline 1 09/08/23 16:00 V37578AMP
<0.179 mg/Kg - dry 0.179 0.828Anthracene 1 09/08/23 16:00 V37578AMP
<0.174 mg/Kg - dry 0.174 0.828Benzo(a)anthracene 1 09/08/23 16:00 V37578AMP
<0.184 mg/Kg - dry 0.184 0.828Benzo(a)pyrene 1 09/08/23 16:00 V37578AMP
<0.183 mg/Kg - dry 0.183 0.828Benzo(b)fluoranthene 1 09/08/23 16:00 V37578AMP
<0.170 mg/Kg - dry 0.170 0.828Benzo(g,h,i)perylene 1 09/08/23 16:00 V37578AMP
<0.171 mg/Kg - dry 0.171 0.828Benzo(k)fluoranthene 1 09/08/23 16:00 V37578AMP
<0.727 mg/Kg - dry 0.727 2.51Benzoic Acid 1 09/08/23 16:00 V37578AMP
<0.131 mg/Kg - dry 0.131 0.828Benzyl alcohol 1 09/08/23 16:00 V37578AMP
<0.148 mg/Kg - dry 0.148 0.828Bis(2-Chloroethoxy)methane 1 09/08/23 16:00 V37578AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 72 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37540 09/07/23 10:00
<0.134 mg/Kg - dry 0.134 0.828Bis(2-Chloroethyl)ether 1 09/08/23 16:00 V37578AMP
<0.170 mg/Kg - dry 0.170 0.414Bis(2-Chloroisopropyl)ether 1 09/08/23 16:00 V37578AMP
<0.150 mg/Kg - dry 0.150 0.828Bis(2-ethylhexyl)phthalate 1 09/08/23 16:00 V37578AMP
<0.136 mg/Kg - dry 0.136 0.8284-Bromophenyl phenyl ether 1 09/08/23 16:00 V37578AMP
<0.141 mg/Kg - dry 0.141 0.414Butyl benzyl phthalate 1 09/08/23 16:00 V37578AMP
<0.115 mg/Kg - dry 0.115 0.8284-Chloro-3-methylphenol 1 09/08/23 16:00 V37578AMP
<0.140 mg/Kg - dry 0.140 0.4144-Chloroaniline 1 09/08/23 16:00 V37578AMP
<0.145 mg/Kg - dry 0.145 0.8282-Chloronaphthalene 1 09/08/23 16:00 V37578AMP
<0.123 mg/Kg - dry 0.123 0.8282-Chlorophenol 1 09/08/23 16:00 V37578AMP
<0.158 mg/Kg - dry 0.158 1.254-Chlorophenyl phenyl ether 1 09/08/23 16:00 V37578AMP
<0.178 mg/Kg - dry 0.178 0.828Chrysene 1 09/08/23 16:00 V37578AMP
<0.288 mg/Kg - dry 0.288 0.828Dibenz(a,h)anthracene 1 09/08/23 16:00 V37578AMP
<0.149 mg/Kg - dry 0.149 0.828Dibenzofuran 1 09/08/23 16:00 V37578AMP
<0.118 mg/Kg - dry 0.118 0.8281,2-Dichlorobenzene 1 09/08/23 16:00 V37578AMP
<0.122 mg/Kg - dry 0.122 0.8281,3-Dichlorobenzene 1 09/08/23 16:00 V37578AMP
<0.122 mg/Kg - dry 0.122 0.4141,4-Dichlorobenzene 1 09/08/23 16:00 V37578AMP
<0.184 mg/Kg - dry 0.184 0.8283,3'-Dichlorobenzidine 1 09/08/23 16:00 V37578AMP
<0.120 mg/Kg - dry 0.120 0.8282,4-Dichlorophenol 1 09/08/23 16:00 V37578AMP
<0.225 mg/Kg - dry 0.225 0.828Diethyl phthalate 1 09/08/23 16:00 V37578AMP
<0.218 mg/Kg - dry 0.218 0.828Dimethyl phthalate 1 09/08/23 16:00 V37578AMP
<0.135 mg/Kg - dry 0.135 0.4142,4-Dimethylphenol 1 09/08/23 16:00 V37578AMP
<0.134 mg/Kg - dry 0.134 0.828Di-n-butyl phthalate 1 09/08/23 16:00 V37578AMP
<0.301 mg/Kg - dry 0.301 1.884,6-Dinitro-2-methylphenol 1 09/08/23 16:00 V37578AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 73 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37540 09/07/23 10:00
<0.652 mg/Kg - dry 0.652 1.882,4-Dinitrophenol 1 09/08/23 16:00 V37578AMP
<0.121 mg/Kg - dry 0.121 0.8282,4-Dinitrotoluene 1 09/08/23 16:00 V37578AMP
<0.135 mg/Kg - dry 0.135 0.8282,6-Dinitrotoluene 1 09/08/23 16:00 V37578AMP
<0.179 mg/Kg - dry 0.179 0.414Di-n-Octyl Phthalate 1 09/08/23 16:00 V37578AMP
<0.154 mg/Kg - dry 0.154 0.828Fluoranthene 1 09/08/23 16:00 V37578AMP
<0.160 mg/Kg - dry 0.160 0.828Fluorene 1 09/08/23 16:00 V37578AMP
<0.132 mg/Kg - dry 0.132 0.828Hexachlorobenzene 1 09/08/23 16:00 V37578AMP
<0.122 mg/Kg - dry 0.122 0.828Hexachlorobutadiene 1 09/08/23 16:00 V37578AMP
<0.196 mg/Kg - dry 0.196 0.828Hexachlorocyclopentadiene 1 09/08/23 16:00 V37578AMP
<0.099 mg/Kg - dry 0.099 0.828Hexachloroethane 1 09/08/23 16:00 V37578AMP
<0.224 mg/Kg - dry 0.224 0.828Indeno(1,2,3-cd)pyrene 1 09/08/23 16:00 V37578AMP
<0.239 mg/Kg - dry 0.239 0.828Isophorone 1 09/08/23 16:00 V37578AMP
<0.132 mg/Kg - dry 0.132 0.8281-Methylnaphthalene 1 09/08/23 16:00 V37578AMP
<0.125 mg/Kg - dry 0.125 0.8282-Methylnaphthalene 1 09/08/23 16:00 V37578AMP
<0.121 mg/Kg - dry 0.121 0.8282-Methylphenol 1 09/08/23 16:00 V37578AMP
<0.106 mg/Kg - dry 0.106 0.8283&4 Methylphenol 1 09/08/23 16:00 V37578AMP
<0.180 mg/Kg - dry 0.180 0.828Naphthalene 1 09/08/23 16:00 V37578AMP
<0.121 mg/Kg - dry 0.121 0.8282-Nitroaniline 1 09/08/23 16:00 V37578AMP
<0.150 mg/Kg - dry 0.150 0.8283-Nitroaniline 1 09/08/23 16:00 V37578AMP
<0.117 mg/Kg - dry 0.117 0.4144-Nitroaniline 1 09/08/23 16:00 V37578AMP
<0.145 mg/Kg - dry 0.145 0.414Nitrobenzene 1 09/08/23 16:00 V37578AMP
<0.111 mg/Kg - dry 0.111 0.8282-Nitrophenol 1 09/08/23 16:00 V37578AMP
<0.146 mg/Kg - dry 0.146 0.8284-Nitrophenol 1 09/08/23 16:00 V37578AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 74 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37540 09/07/23 10:00
<0.329 mg/Kg - dry 0.329 0.828N-Nitrosodimethylamine 1 09/08/23 16:00 V37578AMP
<0.227 mg/Kg - dry 0.227 0.828N-Nitrosodiphenylamine 1 09/08/23 16:00 V37578AMP
<0.148 mg/Kg - dry 0.148 0.828N-Nitroso-di-n-propylamine 1 09/08/23 16:00 V37578AMP
<0.435 mg/Kg - dry 0.435 1.25Pentachlorophenol 1 09/08/23 16:00 V37578AMP
<0.260 mg/Kg - dry 0.260 0.828Phenanthrene 1 09/08/23 16:00 V37578AMP
<0.140 mg/Kg - dry 0.140 0.828Phenol 1 09/08/23 16:00 V37578AMP
<0.168 mg/Kg - dry 0.168 0.828Pyrene 1 09/08/23 16:00 V37578AMP
<0.099 mg/Kg - dry 0.099 0.414Pyridine 1 09/08/23 16:00 V37578AMP
<0.134 mg/Kg - dry 0.134 0.8281,2,4-Trichlorobenzene 1 09/08/23 16:00 V37578AMP
<0.120 mg/Kg - dry 0.120 0.8282,4,5-Trichlorophenol 1 09/08/23 16:00 V37578AMP
<0.121 mg/Kg - dry 0.121 0.8282,4,6-Trichlorophenol 1 09/08/23 16:00 V37578AMP
8270ESurrogate: Phenol-d5 74.2 Limits: 34-121%09/08/23 16:001 AMP
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%09/08/23 16:001 AMP V37578
Surrogate: 2-Fluorophenol 80.2 Limits: 35-115%09/08/23 16:001 AMP V37578
Surrogate: Nitrobenzene-d5 95.8 Limits: 37-122%09/08/23 16:001 AMP V37578
Surrogate: 4-Terphenyl-d14 102 Limits: 54-127%09/08/23 16:001 AMP V37578
Surrogate: 2,4,6-Tribromophenol 101 Limits: 39-132%09/08/23 16:001 AMP V37578
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 75 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.53 mg/Kg - dry 1.53 10.0Aliphatic C5-C8 (Adjusted)100 09/02/23 01:51
<11.6 mg/Kg - dry 11.6 62.9Aliphatics C9-C12 (Adjusted)1 09/13/23 10:46
<0.782 mg/Kg - dry 0.782 10.0Aromatic C9-C10 (Adjusted)100 09/02/23 01:51
<17.8 mg/Kg - dry 17.8 62.9Aromatic C11-C22 (Adjusted)1 09/08/23 16:00
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V37493 09/06/23 11:50
<11.6 mg/Kg - dry 11.6 62.9Aliphatic C9-C18 1 09/13/23 10:46 V37620NDL
<15.3 mg/Kg - dry 15.3 62.9Aliphatic C19-C36 1 09/13/23 10:46 V37620NDL
<17.8 mg/Kg - dry 17.8 62.9Aromatic C11-C22 1 09/13/23 10:46 V37620NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 69.6 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: Chlorooctadecane 63.7 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: OTP Surrogate 72.3 Limits: 40-140%09/13/23 10:461 NDL
Surrogate: 2-Fluorobiphenyl 74.6 Limits: 40-140%09/13/23 10:461 NDL V37620
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<1.53 mg/Kg - dry 1.53 10.0Aliphatic C5-C8 100 09/02/23 01:51 V37397TBL
<5.72 mg/Kg - dry 5.72 10.0Aliphatic C9-C12 100 09/02/23 01:51 V37397TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 76 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-5'
93889 Matrix:
8/28/2023 12:54
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<0.782 mg/Kg - dry 0.782 10.0Aromatic C9-C10 100 09/02/23 01:51 V37397TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)86.6 Limits: 70-130%09/02/23 01:51100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)93.7 Limits: 70-130%09/02/23 01:51100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 77 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-10'
93890 Matrix:
8/28/2023 12:57
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
29.1 %Moisture 1 09/05/23 11:43 SW-DRYWTCNC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 78 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-10'
93890 Matrix:
8/28/2023 12:57
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
0.020 J mg/Kg - dry 0.003 0.028Acetone 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.028Acrolein 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.028Acrylonitrile 1 09/01/23 21:03 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 09/01/23 21:03 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 09/01/23 21:03 V37422TBL
<0.002 mg/Kg - dry 0.002 0.014Bromomethane 1 09/01/23 21:03 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 09/01/23 21:03 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 09/01/23 21:03 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 09/01/23 21:03 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 09/01/23 21:03 V37422TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 09/01/23 21:03 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.007Chlorobenzene 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorodibromomethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 09/01/23 21:03 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 09/01/23 21:03 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 09/01/23 21:03 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 09/01/23 21:03 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 09/01/23 21:03 V37422TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 79 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-10'
93890 Matrix:
8/28/2023 12:57
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0071,2-Dibromoethane 1 09/01/23 21:03 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 09/01/23 21:03 V37422TBL
<0.0004 mg/Kg - dry 0.0004 0.0071,2-Dichlorobenzene 1 09/01/23 21:03 V37422TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,3-Dichlorobenzene 1 09/01/23 21:03 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,4-Dichlorobenzene 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.014Dichlorodifluoromethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0071,2-Dichloroethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 09/01/23 21:03 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 09/01/23 21:03 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloropropene 1 09/01/23 21:03 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 09/01/23 21:03 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.070Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 09/01/23 21:03 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.014n-Hexane 1 09/01/23 21:03 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.0282-Hexanone 1 09/01/23 21:03 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.007Isopropylbenzene 1 09/01/23 21:03 V37422TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 80 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-10'
93890 Matrix:
8/28/2023 12:57
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 09/01/23 21:03 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.028Methyl Ethyl Ketone (MEK)1 09/01/23 21:03 V37422TBL
0.001 J mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 09/01/23 21:03 V37422TBL
<0.021 mg/Kg - dry 0.021 0.0284-Methyl-2-Pentanone 1 09/01/23 21:03 V37422TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.014Naphthalene 1 09/01/23 21:03 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 09/01/23 21:03 V37422TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 09/01/23 21:03 V37422TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 09/01/23 21:03 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.007Toluene 1 09/01/23 21:03 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 09/01/23 21:03 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 09/01/23 21:03 V37422TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 09/01/23 21:03 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 09/01/23 21:03 V37422TBL
<0.002 mg/Kg - dry 0.002 0.014Trichlorofluoromethane 1 09/01/23 21:03 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 09/01/23 21:03 V37422TBL
0.003 J mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 09/01/23 21:03 V37422TBL
0.001 J mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 09/01/23 21:03 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.014Vinyl Acetate 1 09/01/23 21:03 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 09/01/23 21:03 V37422TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 81 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-10'
93890 Matrix:
8/28/2023 12:57
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 09/01/23 21:03 V37422TBL
0.002 J mg/Kg - dry 0.001 0.014m,p-Xylene 1 09/01/23 21:03 V37422TBL
0.002 J mg/Kg - dry 0.0007 0.007Xylene (Total)1 09/01/23 21:03 V37422KCC
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/01/23 21:031 TBL V37422
Surrogate: Dibromofluoromethane 106 Limits: 84-123%09/01/23 21:031 TBL V37422
Surrogate: Toluene-d8 99.0 Limits: 76-129%09/01/23 21:031 TBL V37422
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 82 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-10'
93890 Matrix:
8/28/2023 12:57
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.72 mg/Kg - dry 1.72 11.3Aliphatic C5-C8 (Adjusted)1 09/01/23 21:03
<6.43 mg/Kg - dry 6.43 11.3Aliphatics C9-C12 (Adjusted)100 09/02/23 02:14
<0.880 mg/Kg - dry 0.880 11.3Aromatic C9-C10 (Adjusted)100 09/02/23 02:14
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<1.72 mg/Kg - dry 1.72 11.3Aliphatic C5-C8 100 09/02/23 02:14 V37397TBL
<6.43 mg/Kg - dry 6.43 11.3Aliphatic C9-C12 100 09/02/23 02:14 V37397TBL
<0.880 mg/Kg - dry 0.880 11.3Aromatic C9-C10 100 09/02/23 02:14 V37397TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)87.5 Limits: 70-130%09/02/23 02:14100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)84.7 Limits: 70-130%09/02/23 02:14100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 83 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.4 %Moisture 1 09/05/23 11:43 SW-DRYWTCNC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 84 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
0.014 J mg/Kg - dry 0.003 0.026Acetone 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 09/01/23 21:30 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 09/01/23 21:30 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 21:30 V37422TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 09/01/23 21:30 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 09/01/23 21:30 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 09/01/23 21:30 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 09/01/23 21:30 V37422TBL
0.001 J mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 09/01/23 21:30 V37422TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/01/23 21:30 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 21:30 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 09/01/23 21:30 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/01/23 21:30 V37422TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 21:30 V37422TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 21:30 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 09/01/23 21:30 V37422TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 85 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/01/23 21:30 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 09/01/23 21:30 V37422TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 21:30 V37422TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 21:30 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 09/01/23 21:30 V37422TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 21:30 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 21:30 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 09/01/23 21:30 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 21:30 V37422TBL
0.001 J mg/Kg - dry 0.0008 0.006Ethylbenzene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 09/01/23 21:30 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 09/01/23 21:30 V37422TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 09/01/23 21:30 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 21:30 V37422TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 86 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 21:30 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 09/01/23 21:30 V37422TBL
0.226 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 21:30 V37422TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 09/01/23 21:30 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 21:30 V37422TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 21:30 V37422TBL
0.001 J mg/Kg - dry 0.0009 0.006Toluene 1 09/01/23 21:30 V37422TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 09/01/23 21:30 V37422TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 21:30 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 21:30 V37422TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 21:30 V37422TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 09/01/23 21:30 V37422TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 09/01/23 21:30 V37422TBL
0.004 J mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 09/01/23 21:30 V37422TBL
0.009 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 21:30 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 09/01/23 21:30 V37422TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 09/01/23 21:30 V37422TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 87 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37420 09/01/23 08:00
0.005 J mg/Kg - dry 0.0007 0.006o-Xylene 1 09/01/23 21:30 V37422TBL
0.004 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 09/01/23 21:30 V37422TBL
0.009 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 09/01/23 21:30 V37422KCC
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/01/23 21:301 TBL V37422
Surrogate: Dibromofluoromethane 107 Limits: 84-123%09/01/23 21:301 TBL V37422
Surrogate: Toluene-d8 98.6 Limits: 76-129%09/01/23 21:301 TBL V37422
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37540 09/07/23 10:00
<0.155 mg/Kg - dry 0.155 0.886Acenaphthene 1 09/08/23 17:09 V37578AMP
<0.140 mg/Kg - dry 0.140 0.886Acenaphthylene 1 09/08/23 17:09 V37578AMP
<0.203 mg/Kg - dry 0.203 0.886Aniline 1 09/08/23 17:09 V37578AMP
<0.191 mg/Kg - dry 0.191 0.886Anthracene 1 09/08/23 17:09 V37578AMP
<0.186 mg/Kg - dry 0.186 0.886Benzo(a)anthracene 1 09/08/23 17:09 V37578AMP
<0.197 mg/Kg - dry 0.197 0.886Benzo(a)pyrene 1 09/08/23 17:09 V37578AMP
<0.195 mg/Kg - dry 0.195 0.886Benzo(b)fluoranthene 1 09/08/23 17:09 V37578AMP
<0.182 mg/Kg - dry 0.182 0.886Benzo(g,h,i)perylene 1 09/08/23 17:09 V37578AMP
<0.183 mg/Kg - dry 0.183 0.886Benzo(k)fluoranthene 1 09/08/23 17:09 V37578AMP
<0.777 mg/Kg - dry 0.777 2.68Benzoic Acid 1 09/08/23 17:09 V37578AMP
<0.140 mg/Kg - dry 0.140 0.886Benzyl alcohol 1 09/08/23 17:09 V37578AMP
<0.158 mg/Kg - dry 0.158 0.886Bis(2-Chloroethoxy)methane 1 09/08/23 17:09 V37578AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 88 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37540 09/07/23 10:00
<0.143 mg/Kg - dry 0.143 0.886Bis(2-Chloroethyl)ether 1 09/08/23 17:09 V37578AMP
<0.182 mg/Kg - dry 0.182 0.442Bis(2-Chloroisopropyl)ether 1 09/08/23 17:09 V37578AMP
<0.160 mg/Kg - dry 0.160 0.886Bis(2-ethylhexyl)phthalate 1 09/08/23 17:09 V37578AMP
<0.146 mg/Kg - dry 0.146 0.8864-Bromophenyl phenyl ether 1 09/08/23 17:09 V37578AMP
<0.151 mg/Kg - dry 0.151 0.442Butyl benzyl phthalate 1 09/08/23 17:09 V37578AMP
<0.123 mg/Kg - dry 0.123 0.8864-Chloro-3-methylphenol 1 09/08/23 17:09 V37578AMP
<0.150 mg/Kg - dry 0.150 0.4424-Chloroaniline 1 09/08/23 17:09 V37578AMP
<0.155 mg/Kg - dry 0.155 0.8862-Chloronaphthalene 1 09/08/23 17:09 V37578AMP
<0.131 mg/Kg - dry 0.131 0.8862-Chlorophenol 1 09/08/23 17:09 V37578AMP
<0.168 mg/Kg - dry 0.168 1.344-Chlorophenyl phenyl ether 1 09/08/23 17:09 V37578AMP
<0.190 mg/Kg - dry 0.190 0.886Chrysene 1 09/08/23 17:09 V37578AMP
<0.308 mg/Kg - dry 0.308 0.886Dibenz(a,h)anthracene 1 09/08/23 17:09 V37578AMP
<0.159 mg/Kg - dry 0.159 0.886Dibenzofuran 1 09/08/23 17:09 V37578AMP
<0.126 mg/Kg - dry 0.126 0.8861,2-Dichlorobenzene 1 09/08/23 17:09 V37578AMP
<0.130 mg/Kg - dry 0.130 0.8861,3-Dichlorobenzene 1 09/08/23 17:09 V37578AMP
<0.130 mg/Kg - dry 0.130 0.4421,4-Dichlorobenzene 1 09/08/23 17:09 V37578AMP
<0.197 mg/Kg - dry 0.197 0.8863,3'-Dichlorobenzidine 1 09/08/23 17:09 V37578AMP
<0.128 mg/Kg - dry 0.128 0.8862,4-Dichlorophenol 1 09/08/23 17:09 V37578AMP
<0.241 mg/Kg - dry 0.241 0.886Diethyl phthalate 1 09/08/23 17:09 V37578AMP
<0.233 mg/Kg - dry 0.233 0.886Dimethyl phthalate 1 09/08/23 17:09 V37578AMP
<0.144 mg/Kg - dry 0.144 0.4422,4-Dimethylphenol 1 09/08/23 17:09 V37578AMP
<0.143 mg/Kg - dry 0.143 0.886Di-n-butyl phthalate 1 09/08/23 17:09 V37578AMP
<0.321 mg/Kg - dry 0.321 2.014,6-Dinitro-2-methylphenol 1 09/08/23 17:09 V37578AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 89 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37540 09/07/23 10:00
<0.697 mg/Kg - dry 0.697 2.012,4-Dinitrophenol 1 09/08/23 17:09 V37578AMP
<0.129 mg/Kg - dry 0.129 0.8862,4-Dinitrotoluene 1 09/08/23 17:09 V37578AMP
<0.144 mg/Kg - dry 0.144 0.8862,6-Dinitrotoluene 1 09/08/23 17:09 V37578AMP
<0.191 mg/Kg - dry 0.191 0.442Di-n-Octyl Phthalate 1 09/08/23 17:09 V37578AMP
<0.164 mg/Kg - dry 0.164 0.886Fluoranthene 1 09/08/23 17:09 V37578AMP
<0.171 mg/Kg - dry 0.171 0.886Fluorene 1 09/08/23 17:09 V37578AMP
<0.142 mg/Kg - dry 0.142 0.886Hexachlorobenzene 1 09/08/23 17:09 V37578AMP
<0.130 mg/Kg - dry 0.130 0.886Hexachlorobutadiene 1 09/08/23 17:09 V37578AMP
<0.210 mg/Kg - dry 0.210 0.886Hexachlorocyclopentadiene 1 09/08/23 17:09 V37578AMP
<0.106 mg/Kg - dry 0.106 0.886Hexachloroethane 1 09/08/23 17:09 V37578AMP
<0.239 mg/Kg - dry 0.239 0.886Indeno(1,2,3-cd)pyrene 1 09/08/23 17:09 V37578AMP
<0.256 mg/Kg - dry 0.256 0.886Isophorone 1 09/08/23 17:09 V37578AMP
<0.142 mg/Kg - dry 0.142 0.8861-Methylnaphthalene 1 09/08/23 17:09 V37578AMP
<0.134 mg/Kg - dry 0.134 0.8862-Methylnaphthalene 1 09/08/23 17:09 V37578AMP
<0.130 mg/Kg - dry 0.130 0.8862-Methylphenol 1 09/08/23 17:09 V37578AMP
<0.113 mg/Kg - dry 0.113 0.8863&4 Methylphenol 1 09/08/23 17:09 V37578AMP
<0.193 mg/Kg - dry 0.193 0.886Naphthalene 1 09/08/23 17:09 V37578AMP
<0.129 mg/Kg - dry 0.129 0.8862-Nitroaniline 1 09/08/23 17:09 V37578AMP
<0.160 mg/Kg - dry 0.160 0.8863-Nitroaniline 1 09/08/23 17:09 V37578AMP
<0.125 mg/Kg - dry 0.125 0.4424-Nitroaniline 1 09/08/23 17:09 V37578AMP
<0.155 mg/Kg - dry 0.155 0.442Nitrobenzene 1 09/08/23 17:09 V37578AMP
<0.119 mg/Kg - dry 0.119 0.8862-Nitrophenol 1 09/08/23 17:09 V37578AMP
<0.156 mg/Kg - dry 0.156 0.8864-Nitrophenol 1 09/08/23 17:09 V37578AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 90 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37540 09/07/23 10:00
<0.352 mg/Kg - dry 0.352 0.886N-Nitrosodimethylamine 1 09/08/23 17:09 V37578AMP
<0.242 mg/Kg - dry 0.242 0.886N-Nitrosodiphenylamine 1 09/08/23 17:09 V37578AMP
<0.158 mg/Kg - dry 0.158 0.886N-Nitroso-di-n-propylamine 1 09/08/23 17:09 V37578AMP
<0.465 mg/Kg - dry 0.465 1.34Pentachlorophenol 1 09/08/23 17:09 V37578AMP
<0.278 mg/Kg - dry 0.278 0.886Phenanthrene 1 09/08/23 17:09 V37578AMP
<0.150 mg/Kg - dry 0.150 0.886Phenol 1 09/08/23 17:09 V37578AMP
<0.179 mg/Kg - dry 0.179 0.886Pyrene 1 09/08/23 17:09 V37578AMP
<0.106 mg/Kg - dry 0.106 0.442Pyridine 1 09/08/23 17:09 V37578AMP
<0.143 mg/Kg - dry 0.143 0.8861,2,4-Trichlorobenzene 1 09/08/23 17:09 V37578AMP
<0.129 mg/Kg - dry 0.129 0.8862,4,5-Trichlorophenol 1 09/08/23 17:09 V37578AMP
<0.129 mg/Kg - dry 0.129 0.8862,4,6-Trichlorophenol 1 09/08/23 17:09 V37578AMP
8270ESurrogate: Phenol-d5 74.9 Limits: 34-121%09/08/23 17:091 AMP
Surrogate: 2-Fluorobiphenyl 89.2 Limits: 44-115%09/08/23 17:091 AMP V37578
Surrogate: 2-Fluorophenol 80.2 Limits: 35-115%09/08/23 17:091 AMP V37578
Surrogate: Nitrobenzene-d5 96.4 Limits: 37-122%09/08/23 17:091 AMP V37578
Surrogate: 4-Terphenyl-d14 105 Limits: 54-127%09/08/23 17:091 AMP V37578
Surrogate: 2,4,6-Tribromophenol 107 Limits: 39-132%09/08/23 17:091 AMP V37578
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 91 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.64 mg/Kg - dry 1.64 10.7Aliphatic C5-C8 (Adjusted)100 09/02/23 02:38
<12.4 mg/Kg - dry 12.4 67.2Aliphatics C9-C12 (Adjusted)1 09/13/23 10:46
<0.836 mg/Kg - dry 0.836 10.7Aromatic C9-C10 (Adjusted)100 09/02/23 02:38
<19.0 mg/Kg - dry 19.0 67.2Aromatic C11-C22 (Adjusted)1 09/08/23 17:09
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V37493 09/06/23 11:50
<12.4 mg/Kg - dry 12.4 67.2Aliphatic C9-C18 1 09/13/23 10:46 V37620NDL
<16.4 mg/Kg - dry 16.4 67.2Aliphatic C19-C36 1 09/13/23 10:46 V37620NDL
<19.0 mg/Kg - dry 19.0 67.2Aromatic C11-C22 1 09/13/23 10:46 V37620NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 72.6 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: Chlorooctadecane 68.6 Limits: 40-140%09/13/23 10:461 NDL
MADEP-EPHSurrogate: OTP Surrogate 73.8 Limits: 40-140%09/13/23 10:461 NDL
Surrogate: 2-Fluorobiphenyl 77.1 Limits: 40-140%09/13/23 10:461 NDL V37620
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<1.64 mg/Kg - dry 1.64 10.7Aliphatic C5-C8 100 09/02/23 02:38 V37397TBL
<6.11 mg/Kg - dry 6.11 10.7Aliphatic C9-C12 100 09/02/23 02:38 V37397TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 92 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4-15'
93891 Matrix:
8/28/2023 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37396 09/01/23 08:00
<0.836 mg/Kg - dry 0.836 10.7Aromatic C9-C10 100 09/02/23 02:38 V37397TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)78.5 Limits: 70-130%09/02/23 02:38100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)86.3 Limits: 70-130%09/02/23 02:38100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 93 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2
93892 Matrix:
8/28/2023 0:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/07/23 06:53 6200BMSA
0.004 J mg/L 0.002 0.006Lead 1 09/06/23 18:57 6010DJKC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 94 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2
93892 Matrix:
8/28/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
V37909 09/14/23 09:00
3.69 J µg/L 1.80 10.0Acetone 1 09/07/23 06:53 V37564MSA
86.1 µg/L 0.180 0.500Benzene 1 09/07/23 06:53 V37564MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/07/23 06:53 V37564MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/07/23 06:53 V37564MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/07/23 06:53 V37564MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/07/23 06:53 V37564MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/07/23 06:53 V37564MSA
0.245 J µg/L 0.180 0.500n-Butylbenzene 1 09/07/23 06:53 V37564MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/07/23 06:53 V37564MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/07/23 06:53 V37564MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/07/23 06:53 V37564MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/07/23 06:53 V37564MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/07/23 06:53 V37564MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/07/23 06:53 V37564MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/07/23 06:53 V37564MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/07/23 06:53 V37564MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/07/23 06:53 V37564MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/07/23 06:53 V37564MSA
37.4 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/07/23 06:53 V37564MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/07/23 06:53 V37564MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/07/23 06:53 V37564MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/07/23 06:53 V37564MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/07/23 06:53 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 95 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2
93892 Matrix:
8/28/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
V37909 09/14/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/07/23 06:53 V37564MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/07/23 06:53 V37564MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/07/23 06:53 V37564MSA
5.02 µg/L 0.150 0.5001,2-Dichloroethane 1 09/07/23 06:53 V37564MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/07/23 06:53 V37564MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/07/23 06:53 V37564MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/07/23 06:53 V37564MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/07/23 06:53 V37564MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/07/23 06:53 V37564MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/07/23 06:53 V37564MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/07/23 06:53 V37564MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/07/23 06:53 V37564MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/07/23 06:53 V37564MSA
<42.0 µg/L 42.0 200Ethanol 1 09/07/23 06:53 V37564MSA
18.1 µg/L 0.170 0.500Ethylbenzene 1 09/07/23 06:53 V37564MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/07/23 06:53 V37564MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/07/23 06:53 V37564MSA
1.48 µg/L 0.180 0.500Isopropylbenzene 1 09/07/23 06:53 V37564MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/07/23 06:53 V37564MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/07/23 06:53 V37564MSA
1550 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/15/23 08:17 V37910ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/07/23 06:53 V37564MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/07/23 06:53 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 96 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2
93892 Matrix:
8/28/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
V37909 09/14/23 09:00
10.5 µg/L 0.470 1.00Naphthalene 1 09/07/23 06:53 V37564MSA
2.54 µg/L 0.190 0.500n-Propylbenzene 1 09/07/23 06:53 V37564MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/07/23 06:53 V37564MSA
158 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/07/23 06:53 V37564MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/07/23 06:53 V37564MSA
238 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 09/07/23 16:56 V37632MSA
13.4 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/07/23 06:53 V37564MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/07/23 06:53 V37564MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/07/23 06:53 V37564MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/07/23 06:53 V37564MSA
3.34 µg/L 0.220 0.500Toluene 1 09/07/23 06:53 V37564MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/07/23 06:53 V37564MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/07/23 06:53 V37564MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/07/23 06:53 V37564MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/07/23 06:53 V37564MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/07/23 06:53 V37564MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/07/23 06:53 V37564MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/07/23 06:53 V37564MSA
11.6 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/07/23 06:53 V37564MSA
0.377 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/07/23 06:53 V37564MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/07/23 06:53 V37564MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/07/23 06:53 V37564MSA
24.2 µg/L 0.210 0.500o-Xylene 1 09/07/23 06:53 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 97 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2
93892 Matrix:
8/28/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
V37909 09/14/23 09:00
71.8 µg/L 0.420 1.00m,p-Xylene 1 09/07/23 06:53 V37564MSA
96.0 µg/L 0.210 0.500Xylene (Total)1 09/07/23 06:53 V37564
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%09/07/23 06:531 MSA V37564
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%09/07/23 06:531 MSA V37564
Surrogate: 1,2-Dichloroethane - d4 96.8 Limits: 70-130%09/07/23 06:531 MSA V37564
Surrogate: Toluene-d8 98.8 Limits: 70-130%09/07/23 06:531 MSA V37564
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%09/07/23 16:5610 MSA V37632
Surrogate: Dibromofluoromethane 95.8 Limits: 70-130%09/07/23 16:5610 MSA V37632
Surrogate: 1,2-Dichloroethane - d4 97.0 Limits: 70-130%09/07/23 16:5610 MSA V37632
Surrogate: Toluene-d8 97.6 Limits: 70-130%09/07/23 16:5610 MSA V37632
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%09/15/23 08:17100 ENM V37910
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%09/15/23 08:17100 ENM V37910
Surrogate: 1,2-Dichloroethane - d4 96.4 Limits: 70-130%09/15/23 08:17100 ENM V37910
Surrogate: Toluene-d8 99.4 Limits: 70-130%09/15/23 08:17100 ENM V37910
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V37608 09/08/23 12:55
0.161 µg/L 0.00347 0.02101,2-Dibromoethane 1 09/08/23 15:25 V37661TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 98 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2
93892 Matrix:
8/28/2023 0:00
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
332 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 09/01/23 17:36
77.4 J µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 09/01/23 17:36
39.5 J µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 09/01/23 17:36
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V37556 09/07/23 15:11
63.5 J µg/L 28.2 350Aliphatic C9-C18 1 09/11/23 19:18 V37698NDL
<124 µg/L 124 500Aliphatic C19-C36 1 09/11/23 19:18 V37698NDL
330 µg/L 61.2 250Aromatic C11-C22 1 09/11/23 19:18 V37698NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 95.5 Limits: 40-140%09/11/23 19:181 NDL
MADEP-EPHSurrogate: Chlorooctadecane 61.0 Limits: 40-140%09/11/23 19:181 NDL
MADEP-EPHSurrogate: OTP Surrogate 73.0 Limits: 40-140%09/11/23 19:181 NDL
Surrogate: 2-Fluorobiphenyl 100 Limits: 40-140%09/11/23 19:181 NDL V37698
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37398 09/01/23 08:00
421 µg/L 11.5 50.0Aliphatic C5-C8 1 09/01/23 17:36 V37399TBL
231 µg/L 25.8 50.0Aliphatic C9-C12 1 09/01/23 17:36 V37399TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 99 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-2
93892 Matrix:
8/28/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37398 09/01/23 08:00
39.5 J µg/L 4.02 50.0Aromatic C9-C10 1 09/01/23 17:36 V37399TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)100 Limits: 70-130%09/01/23 17:361 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)91.8 Limits: 70-130%09/01/23 17:361 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 100 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/07/23 02:20 6200BMSA
0.072 mg/L 0.002 0.006Lead 1 09/06/23 19:01 6010DJKC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 101 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00
2.17 J µg/L 1.80 10.0Acetone 1 09/07/23 02:20 V37564MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/07/23 02:20 V37564MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/07/23 02:20 V37564MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/07/23 02:20 V37564MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/07/23 02:20 V37564MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/07/23 02:20 V37564MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/07/23 02:20 V37564MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/07/23 02:20 V37564MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/07/23 02:20 V37564MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/07/23 02:20 V37564MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/07/23 02:20 V37564MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/07/23 02:20 V37564MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/07/23 02:20 V37564MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/07/23 02:20 V37564MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/07/23 02:20 V37564MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/07/23 02:20 V37564MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/07/23 02:20 V37564MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/07/23 02:20 V37564MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/07/23 02:20 V37564MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/07/23 02:20 V37564MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/07/23 02:20 V37564MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/07/23 02:20 V37564MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/07/23 02:20 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 102 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/07/23 02:20 V37564MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/07/23 02:20 V37564MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/07/23 02:20 V37564MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/07/23 02:20 V37564MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/07/23 02:20 V37564MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/07/23 02:20 V37564MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/07/23 02:20 V37564MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/07/23 02:20 V37564MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/07/23 02:20 V37564MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/07/23 02:20 V37564MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/07/23 02:20 V37564MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/07/23 02:20 V37564MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/07/23 02:20 V37564MSA
<42.0 µg/L 42.0 200Ethanol 1 09/07/23 02:20 V37564MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/07/23 02:20 V37564MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/07/23 02:20 V37564MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/07/23 02:20 V37564MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/07/23 02:20 V37564MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/07/23 02:20 V37564MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/07/23 02:20 V37564MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/07/23 02:20 V37564MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/07/23 02:20 V37564MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/07/23 02:20 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 103 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/07/23 02:20 V37564MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/07/23 02:20 V37564MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/07/23 02:20 V37564MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/07/23 02:20 V37564MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/07/23 02:20 V37564MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/07/23 02:20 V37564MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/07/23 02:20 V37564MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/07/23 02:20 V37564MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/07/23 02:20 V37564MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/07/23 02:20 V37564MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/07/23 02:20 V37564MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/07/23 02:20 V37564MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/07/23 02:20 V37564MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/07/23 02:20 V37564MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/07/23 02:20 V37564MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/07/23 02:20 V37564MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/07/23 02:20 V37564MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/07/23 02:20 V37564MSA
0.228 J µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/07/23 02:20 V37564MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/07/23 02:20 V37564MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/07/23 02:20 V37564MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/07/23 02:20 V37564MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/07/23 02:20 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 104 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/07/23 02:20 V37564MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/07/23 02:20 V37564
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%09/07/23 02:201 MSA V37564
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%09/07/23 02:201 MSA V37564
Surrogate: 1,2-Dichloroethane - d4 99.6 Limits: 70-130%09/07/23 02:201 MSA V37564
Surrogate: Toluene-d8 98.6 Limits: 70-130%09/07/23 02:201 MSA V37564
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37391 09/04/23 13:30
<0.308 µg/L 0.308 2.04Acenaphthene 1 09/05/23 19:21 V37430AMP
<0.302 µg/L 0.302 2.04Acenaphthylene 1 09/05/23 19:21 V37430AMP
<0.852 µg/L 0.852 2.04Anthracene 1 09/05/23 19:21 V37430AMP
<1.35 M µg/L 1.35 10.2Benzidine 1 09/05/23 19:21 V37430AMP
<0.649 µg/L 0.649 2.04Benzo(a)anthracene 1 09/05/23 19:21 V37430AMP
<1.04 µg/L 1.04 2.04Benzo(a)pyrene 1 09/05/23 19:21 V37430AMP
<2.54 µg/L 2.54 5.10Benzo(b)fluoranthene 1 09/05/23 19:21 V37430AMP
<1.03 µg/L 1.03 5.10Benzo(g,h,i)perylene 1 09/05/23 19:21 V37430AMP
<2.03 µg/L 2.03 5.10Benzo(k)fluoranthene 1 09/05/23 19:21 V37430AMP
<1.12 µg/L 1.12 10.2Benzoic Acid 1 09/05/23 19:21 V37430AMP
<0.697 µg/L 0.697 5.10Benzyl alcohol 1 09/05/23 19:21 V37430AMP
<0.477 µg/L 0.477 5.10Bis(2-Chloroethoxy)methane 1 09/05/23 19:21 V37430AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 105 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37391 09/04/23 13:30
<1.06 µg/L 1.06 5.10Bis(2-Chloroethyl)ether 1 09/05/23 19:21 V37430AMP
<1.10 µg/L 1.10 5.10Bis(2-Chloroisopropyl)ether 1 09/05/23 19:21 V37430AMP
<3.53 µg/L 3.53 10.2Bis(2-ethylhexyl)phthalate 1 09/05/23 19:21 V37430AMP
<1.13 µg/L 1.13 5.104-Bromophenyl phenyl ether 1 09/05/23 19:21 V37430AMP
<1.87 µg/L 1.87 5.10Butyl benzyl phthalate 1 09/05/23 19:21 V37430AMP
<1.20 µg/L 1.20 5.104-Chloro-3-methylphenol 1 09/05/23 19:21 V37430AMP
<7.53 µg/L 7.53 20.42-Chloronaphthalene 1 09/05/23 19:21 V37430AMP
<0.956 µg/L 0.956 10.22-Chlorophenol 1 09/05/23 19:21 V37430AMP
<1.74 µg/L 1.74 5.104-Chlorophenyl phenyl ether 1 09/05/23 19:21 V37430AMP
<0.413 µg/L 0.413 2.04Chrysene 1 09/05/23 19:21 V37430AMP
<0.442 µg/L 0.442 2.04Dibenz(a,h)anthracene 1 09/05/23 19:21 V37430AMP
<0.873 µg/L 0.873 5.10Dibenzofuran 1 09/05/23 19:21 V37430AMP
<2.04 µg/L 2.04 5.101,2-Dichlorobenzene 1 09/05/23 19:21 V37430AMP
<2.04 µg/L 2.04 5.101,3-Dichlorobenzene 1 09/05/23 19:21 V37430AMP
<2.09 µg/L 2.09 5.101,4-Dichlorobenzene 1 09/05/23 19:21 V37430AMP
<1.93 µg/L 1.93 5.103,3'-Dichlorobenzidine 1 09/05/23 19:21 V37430AMP
<1.49 µg/L 1.49 10.22,4-Dichlorophenol 1 09/05/23 19:21 V37430AMP
<0.759 µg/L 0.759 5.10Diethyl phthalate 1 09/05/23 19:21 V37430AMP
<0.957 µg/L 0.957 5.10Dimethyl phthalate 1 09/05/23 19:21 V37430AMP
<1.60 µg/L 1.60 20.42,4-Dimethylphenol 1 09/05/23 19:21 V37430AMP
<2.10 µg/L 2.10 5.10Di-n-butyl phthalate 1 09/05/23 19:21 V37430AMP
<2.11 µg/L 2.11 10.24,6-Dinitro-2-methylphenol 1 09/05/23 19:21 V37430AMP
<1.96 µg/L 1.96 10.22,4-Dinitrophenol 1 09/05/23 19:21 V37430AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 106 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37391 09/04/23 13:30
<1.13 µg/L 1.13 5.102,4-Dinitrotoluene 1 09/05/23 19:21 V37430AMP
<0.825 µg/L 0.825 5.102,6-Dinitrotoluene 1 09/05/23 19:21 V37430AMP
<1.68 µg/L 1.68 5.10Di-n-Octyl Phthalate 1 09/05/23 19:21 V37430AMP
<0.255 µg/L 0.255 2.04Fluoranthene 1 09/05/23 19:21 V37430AMP
<0.823 µg/L 0.823 2.04Fluorene 1 09/05/23 19:21 V37430AMP
<0.998 µg/L 0.998 5.10Hexachlorobenzene 1 09/05/23 19:21 V37430AMP
<2.78 µg/L 2.78 5.10Hexachlorobutadiene 1 09/05/23 19:21 V37430AMP
<2.09 µg/L 2.09 5.10Hexachlorocyclopentadiene 1 09/05/23 19:21 V37430AMP
<1.80 µg/L 1.80 5.10Hexachloroethane 1 09/05/23 19:21 V37430AMP
<0.486 µg/L 0.486 2.04Indeno(1,2,3-cd)pyrene 1 09/05/23 19:21 V37430AMP
<0.452 µg/L 0.452 5.10Isophorone 1 09/05/23 19:21 V37430AMP
<1.16 µg/L 1.16 2.041-Methylnaphthalene 1 09/05/23 19:21 V37430AMP
<0.679 µg/L 0.679 2.042-Methylnaphthalene 1 09/05/23 19:21 V37430AMP
<0.742 µg/L 0.742 2.04Naphthalene 1 09/05/23 19:21 V37430AMP
<0.923 µg/L 0.923 5.10Nitrobenzene 1 09/05/23 19:21 V37430AMP
<0.502 µg/L 0.502 5.102-Nitrophenol 1 09/05/23 19:21 V37430AMP
<1.25 µg/L 1.25 10.24-Nitrophenol 1 09/05/23 19:21 V37430AMP
<1.12 µg/L 1.12 5.10N-Nitrosodiphenylamine 1 09/05/23 19:21 V37430AMP
<0.653 µg/L 0.653 5.10N-Nitroso-di-n-propylamine 1 09/05/23 19:21 V37430AMP
<1.46 µg/L 1.46 5.10Pentachlorophenol 1 09/05/23 19:21 V37430AMP
<0.436 µg/L 0.436 2.04Phenanthrene 1 09/05/23 19:21 V37430AMP
<0.664 µg/L 0.664 5.10Phenol 1 09/05/23 19:21 V37430AMP
<0.442 µg/L 0.442 2.04Pyrene 1 09/05/23 19:21 V37430AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 107 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37391 09/04/23 13:30
<2.25 µg/L 2.25 5.101,2,4-Trichlorobenzene 1 09/05/23 19:21 V37430AMP
<1.35 µg/L 1.35 5.102,4,6-Trichlorophenol 1 09/05/23 19:21 V37430AMP
625.1Surrogate: Phenol-d5 9.12 *Limits: 10-63%09/05/23 19:211 AMP
Surrogate: 2-Fluorobiphenyl 63.9 Limits: 49-118%09/05/23 19:211 AMP V37430
Surrogate: 2-Fluorophenol 14.5 *Limits: 22-84%09/05/23 19:211 AMP V37430
Surrogate: Nitrobenzene-d5 59.0 Limits: 43-123%09/05/23 19:211 AMP V37430
Surrogate: 4-Terphenyl-d14 73.5 Limits: 49-151%09/05/23 19:211 AMP V37430
Surrogate: 2,4,6-Tribromophenol 29.2 *Limits: 31-144%09/05/23 19:211 AMP V37430
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V37608 09/08/23 12:55
<0.00347 µg/L 0.00347 0.02101,2-Dibromoethane 1 09/08/23 15:45 V37661TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 108 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 09/01/23 17:59
<25.8 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 09/01/23 17:59
<4.02 µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 09/01/23 17:59
<61.2 µg/L 61.2 250Aromatic C11-C22 (Adjusted)1 09/05/23 19:21
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V37556 09/07/23 15:11
<28.2 µg/L 28.2 350Aliphatic C9-C18 1 09/11/23 19:55 V37698NDL
<124 µg/L 124 500Aliphatic C19-C36 1 09/11/23 19:55 V37698NDL
<61.2 µg/L 61.2 250Aromatic C11-C22 1 09/11/23 19:55 V37698NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 73.0 Limits: 40-140%09/11/23 19:551 NDL
MADEP-EPHSurrogate: Chlorooctadecane 56.8 Limits: 40-140%09/11/23 19:551 NDL
MADEP-EPHSurrogate: OTP Surrogate 58.6 Limits: 40-140%09/11/23 19:551 NDL
Surrogate: 2-Fluorobiphenyl 78.3 Limits: 40-140%09/11/23 19:551 NDL V37698
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37398 09/01/23 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 09/01/23 17:59 V37399TBL
<25.8 µg/L 25.8 50.0Aliphatic C9-C12 1 09/01/23 17:59 V37399TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 109 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-3
93893 Matrix:
8/28/2023 12:56
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37398 09/01/23 08:00
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 09/01/23 17:59 V37399TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)96.5 Limits: 70-130%09/01/23 17:591 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)93.7 Limits: 70-130%09/01/23 17:591 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 110 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4
93894 Matrix:
8/28/2023 17:05
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 09/07/23 08:33 6200BMSA
0.044 mg/L 0.012 0.030Lead 5 09/06/23 19:06 6010DJKC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 111 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4
93894 Matrix:
8/28/2023 17:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
<180 µg/L 180 1000Acetone 100 09/07/23 08:33 V37564MSA
760 µg/L 18.0 50.0Benzene 100 09/07/23 08:33 V37564MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/07/23 08:33 V37564MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/07/23 08:33 V37564MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/07/23 08:33 V37564MSA
<150 µg/L 150 500Bromoform 100 09/07/23 08:33 V37564MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/07/23 08:33 V37564MSA
37.1 J µg/L 18.0 50.0n-Butylbenzene 100 09/07/23 08:33 V37564MSA
36.7 J µg/L 20.0 50.0sec-Butyl benzene 100 09/07/23 08:33 V37564MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/07/23 08:33 V37564MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/07/23 08:33 V37564MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/07/23 08:33 V37564MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/07/23 08:33 V37564MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/07/23 08:33 V37564MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/07/23 08:33 V37564MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 09/07/23 08:33 V37564MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/07/23 08:33 V37564MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/07/23 08:33 V37564MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/07/23 08:33 V37564MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/07/23 08:33 V37564MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/07/23 08:33 V37564MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/07/23 08:33 V37564MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/07/23 08:33 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 112 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4
93894 Matrix:
8/28/2023 17:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/07/23 08:33 V37564MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 09/07/23 08:33 V37564MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/07/23 08:33 V37564MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/07/23 08:33 V37564MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/07/23 08:33 V37564MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/07/23 08:33 V37564MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/07/23 08:33 V37564MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 09/07/23 08:33 V37564MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/07/23 08:33 V37564MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/07/23 08:33 V37564MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/07/23 08:33 V37564MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/07/23 08:33 V37564MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/07/23 08:33 V37564MSA
<4200 µg/L 4200 20000Ethanol 100 09/07/23 08:33 V37564MSA
3660 µg/L 17.0 50.0Ethylbenzene 100 09/07/23 08:33 V37564MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/07/23 08:33 V37564MSA
<38.0 µg/L 38.0 1002-Hexanone 100 09/07/23 08:33 V37564MSA
261 µg/L 18.0 50.0Isopropylbenzene 100 09/07/23 08:33 V37564MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/07/23 08:33 V37564MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/07/23 08:33 V37564MSA
2420 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/07/23 08:33 V37564MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/07/23 08:33 V37564MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 09/07/23 08:33 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 113 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4
93894 Matrix:
8/28/2023 17:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
498 µg/L 47.0 100Naphthalene 100 09/07/23 08:33 V37564MSA
593 µg/L 19.0 50.0n-Propylbenzene 100 09/07/23 08:33 V37564MSA
<22.0 µg/L 22.0 50.0Styrene 100 09/07/23 08:33 V37564MSA
497 J µg/L 160 1000tert-Butyl Alcohol (TBA)100 09/07/23 08:33 V37564MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 09/07/23 08:33 V37564MSA
<190 µg/L 190 1000tert-Amyl Alcohol (TAA)100 09/07/23 08:33 V37564MSA
112 J µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 09/07/23 08:33 V37564MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/07/23 08:33 V37564MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/07/23 08:33 V37564MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/07/23 08:33 V37564MSA
30100 µg/L 220 500Toluene 1000 09/07/23 19:00 V37632MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/07/23 08:33 V37564MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/07/23 08:33 V37564MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/07/23 08:33 V37564MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/07/23 08:33 V37564MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/07/23 08:33 V37564MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/07/23 08:33 V37564MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/07/23 08:33 V37564MSA
3660 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/07/23 08:33 V37564MSA
1030 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/07/23 08:33 V37564MSA
<100 µg/L 100 500Vinyl Acetate 100 09/07/23 08:33 V37564MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 09/07/23 08:33 V37564MSA
6100 µg/L 21.0 50.0o-Xylene 100 09/07/23 08:33 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 114 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4
93894 Matrix:
8/28/2023 17:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
12300 µg/L 42.0 100m,p-Xylene 100 09/07/23 08:33 V37564MSA
18400 µg/L 21.0 50.0Xylene (Total)100 09/07/23 08:33 V37564
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%09/07/23 08:33100 MSA V37564
Surrogate: Dibromofluoromethane 98.0 Limits: 70-130%09/07/23 08:33100 MSA V37564
Surrogate: 1,2-Dichloroethane - d4 96.6 Limits: 70-130%09/07/23 08:33100 MSA V37564
Surrogate: Toluene-d8 97.2 Limits: 70-130%09/07/23 08:33100 MSA V37564
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%09/07/23 19:001000 MSA V37632
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%09/07/23 19:001000 MSA V37632
Surrogate: 1,2-Dichloroethane - d4 98.4 Limits: 70-130%09/07/23 19:001000 MSA V37632
Surrogate: Toluene-d8 97.8 Limits: 70-130%09/07/23 19:001000 MSA V37632
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V37608 09/08/23 12:55
0.742 µg/L 0.00345 0.02091,2-Dibromoethane 1 09/08/23 16:08 V37661TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 115 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-4
93894 Matrix:
8/28/2023 17:05
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
12000 µg/L 1150 5000Aliphatic C5-C8 (Adjusted)100 09/01/23 20:44
14500 µg/L 2580 5000Aliphatics C9-C12 (Adjusted)100 09/01/23 20:44
9420 µg/L 402 5000Aromatic C9-C10 (Adjusted)100 09/01/23 20:44
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37398 09/01/23 08:00
42900 µg/L 1150 5000Aliphatic C5-C8 100 09/01/23 20:44 V37399TBL
46000 µg/L 2580 5000Aliphatic C9-C12 100 09/01/23 20:44 V37399TBL
9420 µg/L 402 5000Aromatic C9-C10 100 09/01/23 20:44 V37399TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)87.4 Limits: 70-130%09/01/23 20:44100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)89.3 Limits: 70-130%09/01/23 20:44100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 116 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:Trip Blank
93895 Matrix:
8/28/2023 9:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/05/23 15:03 V37496MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/05/23 15:03 V37496MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/05/23 15:03 V37496MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/05/23 15:03 V37496MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/05/23 15:03 V37496MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/05/23 15:03 V37496MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/05/23 15:03 V37496MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/05/23 15:03 V37496MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/05/23 15:03 V37496MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/05/23 15:03 V37496MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/05/23 15:03 V37496MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/05/23 15:03 V37496MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/05/23 15:03 V37496MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/05/23 15:03 V37496MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/05/23 15:03 V37496MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/05/23 15:03 V37496MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/05/23 15:03 V37496MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/05/23 15:03 V37496MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/05/23 15:03 V37496MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/05/23 15:03 V37496MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/05/23 15:03 V37496MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/05/23 15:03 V37496MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/05/23 15:03 V37496MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 117 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:Trip Blank
93895 Matrix:
8/28/2023 9:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/05/23 15:03 V37496MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/05/23 15:03 V37496MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/05/23 15:03 V37496MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/05/23 15:03 V37496MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/05/23 15:03 V37496MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/05/23 15:03 V37496MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/05/23 15:03 V37496MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/05/23 15:03 V37496MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/05/23 15:03 V37496MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/05/23 15:03 V37496MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/05/23 15:03 V37496MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/05/23 15:03 V37496MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/05/23 15:03 V37496MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/05/23 15:03 V37496MSA
<42.0 µg/L 42.0 200Ethanol 1 09/05/23 15:03 V37496MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/05/23 15:03 V37496MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/05/23 15:03 V37496MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/05/23 15:03 V37496MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/05/23 15:03 V37496MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/05/23 15:03 V37496MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/05/23 15:03 V37496MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/05/23 15:03 V37496MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/05/23 15:03 V37496MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 118 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:Trip Blank
93895 Matrix:
8/28/2023 9:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/05/23 15:03 V37496MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/05/23 15:03 V37496MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/05/23 15:03 V37496MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/05/23 15:03 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/05/23 15:03 V37496MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/05/23 15:03 V37496MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/05/23 15:03 V37496MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/05/23 15:03 V37496MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/05/23 15:03 V37496MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/05/23 15:03 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/05/23 15:03 V37496MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/05/23 15:03 V37496MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/05/23 15:03 V37496MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/05/23 15:03 V37496MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/05/23 15:03 V37496MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/05/23 15:03 V37496MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/05/23 15:03 V37496MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/05/23 15:03 V37496MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/05/23 15:03 V37496MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/05/23 15:03 V37496MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/05/23 15:03 V37496MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 119 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:Trip Blank
93895 Matrix:
8/28/2023 9:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/05/23 15:03 V37496
Surrogate: 4-Bromofluorobenzene 96.8 Limits: 70-130%09/05/23 15:031 MSA V37496
Surrogate: Dibromofluoromethane 100 Limits: 70-130%09/05/23 15:031 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 87.0 Limits: 70-130%09/05/23 15:031 MSA V37496
Surrogate: Toluene-d8 99.0 Limits: 70-130%09/05/23 15:031 MSA V37496
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 120 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
93896 Matrix:
8/28/2023 14:30
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/07/23 02:45 6200BMSA
0.891 mg/L 0.048 0.120Lead 20 09/07/23 15:04 6010D
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 121 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
93896 Matrix:
8/28/2023 14:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/07/23 02:45 V37564MSA
5.52 µg/L 0.180 0.500Benzene 1 09/07/23 02:45 V37564MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/07/23 02:45 V37564MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/07/23 02:45 V37564MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/07/23 02:45 V37564MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/07/23 02:45 V37564MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/07/23 02:45 V37564MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/07/23 02:45 V37564MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/07/23 02:45 V37564MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/07/23 02:45 V37564MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/07/23 02:45 V37564MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/07/23 02:45 V37564MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/07/23 02:45 V37564MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/07/23 02:45 V37564MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/07/23 02:45 V37564MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/07/23 02:45 V37564MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/07/23 02:45 V37564MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/07/23 02:45 V37564MSA
6.36 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/07/23 02:45 V37564MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/07/23 02:45 V37564MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/07/23 02:45 V37564MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/07/23 02:45 V37564MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/07/23 02:45 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 122 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
93896 Matrix:
8/28/2023 14:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/07/23 02:45 V37564MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/07/23 02:45 V37564MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/07/23 02:45 V37564MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/07/23 02:45 V37564MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/07/23 02:45 V37564MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/07/23 02:45 V37564MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/07/23 02:45 V37564MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/07/23 02:45 V37564MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/07/23 02:45 V37564MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/07/23 02:45 V37564MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/07/23 02:45 V37564MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/07/23 02:45 V37564MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/07/23 02:45 V37564MSA
<42.0 µg/L 42.0 200Ethanol 1 09/07/23 02:45 V37564MSA
0.445 J µg/L 0.170 0.500Ethylbenzene 1 09/07/23 02:45 V37564MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/07/23 02:45 V37564MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/07/23 02:45 V37564MSA
0.554 µg/L 0.180 0.500Isopropylbenzene 1 09/07/23 02:45 V37564MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/07/23 02:45 V37564MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/07/23 02:45 V37564MSA
186 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 09/07/23 16:06 V37632MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/07/23 02:45 V37564MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/07/23 02:45 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 123 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
93896 Matrix:
8/28/2023 14:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/07/23 02:45 V37564MSA
0.212 J µg/L 0.190 0.500n-Propylbenzene 1 09/07/23 02:45 V37564MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/07/23 02:45 V37564MSA
74.7 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/07/23 02:45 V37564MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/07/23 02:45 V37564MSA
31.8 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/07/23 02:45 V37564MSA
4.80 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/07/23 02:45 V37564MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/07/23 02:45 V37564MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/07/23 02:45 V37564MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/07/23 02:45 V37564MSA
0.513 µg/L 0.220 0.500Toluene 1 09/07/23 02:45 V37564MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/07/23 02:45 V37564MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/07/23 02:45 V37564MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/07/23 02:45 V37564MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/07/23 02:45 V37564MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/07/23 02:45 V37564MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/07/23 02:45 V37564MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/07/23 02:45 V37564MSA
4.02 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/07/23 02:45 V37564MSA
0.207 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/07/23 02:45 V37564MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/07/23 02:45 V37564MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/07/23 02:45 V37564MSA
20.7 µg/L 0.210 0.500o-Xylene 1 09/07/23 02:45 V37564MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 124 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
93896 Matrix:
8/28/2023 14:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37563 09/06/23 14:00 V37631 09/07/23 09:00
8.04 µg/L 0.420 1.00m,p-Xylene 1 09/07/23 02:45 V37564MSA
28.7 µg/L 0.210 0.500Xylene (Total)1 09/07/23 02:45 V37564
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%09/07/23 02:451 MSA V37564
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%09/07/23 02:451 MSA V37564
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%09/07/23 02:451 MSA V37564
Surrogate: Toluene-d8 99.6 Limits: 70-130%09/07/23 02:451 MSA V37564
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%09/07/23 16:0610 MSA V37632
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%09/07/23 16:0610 MSA V37632
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%09/07/23 16:0610 MSA V37632
Surrogate: Toluene-d8 98.2 Limits: 70-130%09/07/23 16:0610 MSA V37632
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37391 09/04/23 13:30
<0.335 µg/L 0.335 2.22Acenaphthene 1 09/05/23 19:43 V37430AMP
<0.329 µg/L 0.329 2.22Acenaphthylene 1 09/05/23 19:43 V37430AMP
<0.927 µg/L 0.927 2.22Anthracene 1 09/05/23 19:43 V37430AMP
<1.47 M µg/L 1.47 11.1Benzidine 1 09/05/23 19:43 V37430AMP
<0.707 µg/L 0.707 2.22Benzo(a)anthracene 1 09/05/23 19:43 V37430AMP
<1.13 µg/L 1.13 2.22Benzo(a)pyrene 1 09/05/23 19:43 V37430AMP
<2.77 µg/L 2.77 5.56Benzo(b)fluoranthene 1 09/05/23 19:43 V37430AMP
<1.12 µg/L 1.12 5.56Benzo(g,h,i)perylene 1 09/05/23 19:43 V37430AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 125 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
93896 Matrix:
8/28/2023 14:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37391 09/04/23 13:30
<2.21 µg/L 2.21 5.56Benzo(k)fluoranthene 1 09/05/23 19:43 V37430AMP
<1.22 µg/L 1.22 11.1Benzoic Acid 1 09/05/23 19:43 V37430AMP
<0.760 µg/L 0.760 5.56Benzyl alcohol 1 09/05/23 19:43 V37430AMP
<0.520 µg/L 0.520 5.56Bis(2-Chloroethoxy)methane 1 09/05/23 19:43 V37430AMP
<1.16 µg/L 1.16 5.56Bis(2-Chloroethyl)ether 1 09/05/23 19:43 V37430AMP
<1.20 µg/L 1.20 5.56Bis(2-Chloroisopropyl)ether 1 09/05/23 19:43 V37430AMP
<3.84 µg/L 3.84 11.1Bis(2-ethylhexyl)phthalate 1 09/05/23 19:43 V37430AMP
<1.23 µg/L 1.23 5.564-Bromophenyl phenyl ether 1 09/05/23 19:43 V37430AMP
<2.03 µg/L 2.03 5.56Butyl benzyl phthalate 1 09/05/23 19:43 V37430AMP
<1.31 µg/L 1.31 5.564-Chloro-3-methylphenol 1 09/05/23 19:43 V37430AMP
<8.19 µg/L 8.19 22.22-Chloronaphthalene 1 09/05/23 19:43 V37430AMP
<1.04 µg/L 1.04 11.12-Chlorophenol 1 09/05/23 19:43 V37430AMP
<1.90 µg/L 1.90 5.564-Chlorophenyl phenyl ether 1 09/05/23 19:43 V37430AMP
<0.449 µg/L 0.449 2.22Chrysene 1 09/05/23 19:43 V37430AMP
<0.481 µg/L 0.481 2.22Dibenz(a,h)anthracene 1 09/05/23 19:43 V37430AMP
<0.951 µg/L 0.951 5.56Dibenzofuran 1 09/05/23 19:43 V37430AMP
<2.22 µg/L 2.22 5.561,2-Dichlorobenzene 1 09/05/23 19:43 V37430AMP
<2.22 µg/L 2.22 5.561,3-Dichlorobenzene 1 09/05/23 19:43 V37430AMP
<2.28 µg/L 2.28 5.561,4-Dichlorobenzene 1 09/05/23 19:43 V37430AMP
<2.10 µg/L 2.10 5.563,3'-Dichlorobenzidine 1 09/05/23 19:43 V37430AMP
<1.62 µg/L 1.62 11.12,4-Dichlorophenol 1 09/05/23 19:43 V37430AMP
<0.828 µg/L 0.828 5.56Diethyl phthalate 1 09/05/23 19:43 V37430AMP
<1.04 µg/L 1.04 5.56Dimethyl phthalate 1 09/05/23 19:43 V37430AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 126 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
93896 Matrix:
8/28/2023 14:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37391 09/04/23 13:30
<1.74 µg/L 1.74 22.22,4-Dimethylphenol 1 09/05/23 19:43 V37430AMP
<2.29 µg/L 2.29 5.56Di-n-butyl phthalate 1 09/05/23 19:43 V37430AMP
<2.30 µg/L 2.30 11.14,6-Dinitro-2-methylphenol 1 09/05/23 19:43 V37430AMP
<2.13 µg/L 2.13 11.12,4-Dinitrophenol 1 09/05/23 19:43 V37430AMP
<1.23 µg/L 1.23 5.562,4-Dinitrotoluene 1 09/05/23 19:43 V37430AMP
<0.899 µg/L 0.899 5.562,6-Dinitrotoluene 1 09/05/23 19:43 V37430AMP
<1.83 µg/L 1.83 5.56Di-n-Octyl Phthalate 1 09/05/23 19:43 V37430AMP
<0.277 µg/L 0.277 2.22Fluoranthene 1 09/05/23 19:43 V37430AMP
<0.895 µg/L 0.895 2.22Fluorene 1 09/05/23 19:43 V37430AMP
<1.09 µg/L 1.09 5.56Hexachlorobenzene 1 09/05/23 19:43 V37430AMP
<3.04 µg/L 3.04 5.56Hexachlorobutadiene 1 09/05/23 19:43 V37430AMP
<2.28 µg/L 2.28 5.56Hexachlorocyclopentadiene 1 09/05/23 19:43 V37430AMP
<1.96 µg/L 1.96 5.56Hexachloroethane 1 09/05/23 19:43 V37430AMP
<0.529 µg/L 0.529 2.22Indeno(1,2,3-cd)pyrene 1 09/05/23 19:43 V37430AMP
<0.493 µg/L 0.493 5.56Isophorone 1 09/05/23 19:43 V37430AMP
<1.27 µg/L 1.27 2.221-Methylnaphthalene 1 09/05/23 19:43 V37430AMP
<0.739 µg/L 0.739 2.222-Methylnaphthalene 1 09/05/23 19:43 V37430AMP
<0.808 µg/L 0.808 2.22Naphthalene 1 09/05/23 19:43 V37430AMP
<1.01 µg/L 1.01 5.56Nitrobenzene 1 09/05/23 19:43 V37430AMP
<0.548 µg/L 0.548 5.562-Nitrophenol 1 09/05/23 19:43 V37430AMP
<1.37 µg/L 1.37 11.14-Nitrophenol 1 09/05/23 19:43 V37430AMP
<1.22 µg/L 1.22 5.56N-Nitrosodiphenylamine 1 09/05/23 19:43 V37430AMP
<0.712 µg/L 0.712 5.56N-Nitroso-di-n-propylamine 1 09/05/23 19:43 V37430AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 127 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
93896 Matrix:
8/28/2023 14:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37391 09/04/23 13:30
<1.59 µg/L 1.59 5.56Pentachlorophenol 1 09/05/23 19:43 V37430AMP
<0.475 µg/L 0.475 2.22Phenanthrene 1 09/05/23 19:43 V37430AMP
<0.723 µg/L 0.723 5.56Phenol 1 09/05/23 19:43 V37430AMP
<0.481 µg/L 0.481 2.22Pyrene 1 09/05/23 19:43 V37430AMP
<2.46 µg/L 2.46 5.561,2,4-Trichlorobenzene 1 09/05/23 19:43 V37430AMP
<1.47 µg/L 1.47 5.562,4,6-Trichlorophenol 1 09/05/23 19:43 V37430AMP
625.1Surrogate: Phenol-d5 7.68 *Limits: 10-63%09/05/23 19:431 AMP
Surrogate: 2-Fluorobiphenyl 59.5 Limits: 49-118%09/05/23 19:431 AMP V37430
Surrogate: 2-Fluorophenol 12.3 *Limits: 22-84%09/05/23 19:431 AMP V37430
Surrogate: Nitrobenzene-d5 57.6 Limits: 43-123%09/05/23 19:431 AMP V37430
Surrogate: 4-Terphenyl-d14 58.5 Limits: 49-151%09/05/23 19:431 AMP V37430
Surrogate: 2,4,6-Tribromophenol 19.7 *Limits: 31-144%09/05/23 19:431 AMP V37430
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V37608 09/08/23 12:55
<0.00500 µg/L 0.00500 0.03031,2-Dibromoethane 1 09/08/23 16:28 V37661TJW
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 128 of 194
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-244-0003
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 08/31/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
93896 Matrix:
8/28/2023 14:30
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
125 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 09/01/23 18:23
46.3 J µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 09/01/23 18:23
7.01 J µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 09/01/23 18:23
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V37398 09/01/23 08:00
131 µg/L 11.5 50.0Aliphatic C5-C8 1 09/01/23 18:23 V37399TBL
82.5 µg/L 25.8 50.0Aliphatic C9-C12 1 09/01/23 18:23 V37399TBL
7.01 J µg/L 4.02 50.0Aromatic C9-C10 1 09/01/23 18:23 V37399TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)118 Limits: 70-130%09/01/23 18:231 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)113 Limits: 70-130%09/01/23 18:231 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Page 129 of 194
Sample ID Report Lab NoLRB‐V37391 23‐244‐0003 LRB
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
No TICs Detected N.D. ug/L 1 625 9/5/2023 18:13 APANN V37430
Sample ID Report Lab NoMW‐3 23‐244‐0003 93893
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
No TICs Detected N.D. ug/L 1 625 9/5/2023 19:21 APANN V37430
Sample ID Report Lab No
MW‐1 23‐244‐0003 93896
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Octadecanoic acid 10250 ug/L 1 625 9/5/2023 19:43 APANN V37430
Page 130 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Metals Analysis
6010D
V37523QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V37471
Associated Lab Samples: 93892, 93893, 93894, 93896
LRB-V37471 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/06/23 18:080.0060.002<0.002mg/LLead
LCS-V37471Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1060.1060.100mg/LLead 80-120
V 94259-MS-V37471 V 94259-MSD-V37471Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.105 1050.1050.1000.100< 0.002mg/LLead 105 75-125 0.0 20.0
V 94259-PDS-V37471Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/06/23 18:391110.276mg/LLead
Page 1 of 61Date:09/15/2023 05:49 PM
Page 131 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
Associated Lab Samples: 93895
LRB-V37495 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/05/23 14:3810.01.80<1.80µg/LAcetone
09/05/23 14:380.5000.180<0.180µg/LBenzene
09/05/23 14:380.5000.210<0.210µg/LBromobenzene
09/05/23 14:381.000.420<0.420µg/LBromochloromethane
09/05/23 14:380.5000.160<0.160µg/LBromodichloromethane
09/05/23 14:385.001.50<1.50µg/LBromoform
09/05/23 14:381.000.280<0.280µg/LBromomethane
09/05/23 14:380.5000.180<0.180µg/Ln-Butylbenzene
09/05/23 14:380.5000.200<0.200µg/Lsec-Butyl benzene
09/05/23 14:382.000.920<0.920µg/Ltert-Butyl benzene
09/05/23 14:380.5000.180<0.180µg/LCarbon Tetrachloride
09/05/23 14:380.5000.190<0.190µg/LChlorobenzene
09/05/23 14:380.5000.190<0.190µg/LChlorodibromomethane
09/05/23 14:381.000.430<0.430µg/LChloroethane
09/05/23 14:380.5000.220<0.220µg/LChloroform
09/05/23 14:380.5000.220<0.220µg/LChloromethane
09/05/23 14:380.5000.200<0.200µg/L2-Chlorotoluene
09/05/23 14:380.5000.200<0.200µg/L4-Chlorotoluene
09/05/23 14:380.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/05/23 14:382.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/05/23 14:380.5000.200<0.200µg/L1,2-Dibromoethane
09/05/23 14:380.5000.230<0.230µg/LDibromomethane
09/05/23 14:380.5000.220<0.220µg/L1,2-Dichlorobenzene
09/05/23 14:380.5000.190<0.190µg/L1,3-Dichlorobenzene
09/05/23 14:380.5000.210<0.210µg/L1,4-Dichlorobenzene
09/05/23 14:385.001.20<1.20µg/LDichlorodifluoromethane
09/05/23 14:380.5000.240<0.240µg/L1,1-Dichloroethane
Page 2 of 61Date:09/15/2023 05:49 PM
Page 132 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
Associated Lab Samples: 93895
LRB-V37495 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/05/23 14:380.5000.150<0.150µg/L1,2-Dichloroethane
09/05/23 14:380.5000.150<0.150µg/L1,1-Dichloroethene
09/05/23 14:380.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/05/23 14:380.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/05/23 14:380.5000.190<0.190µg/L1,2-Dichloropropane
09/05/23 14:380.5000.130<0.130µg/L1,3-Dichloropropane
09/05/23 14:382.000.210<0.210µg/L2,2-Dichloropropane
09/05/23 14:380.5000.200<0.200µg/L1,1-Dichloropropene
09/05/23 14:380.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/05/23 14:380.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/05/23 14:3820042.0<42.0µg/LEthanol
09/05/23 14:380.5000.170<0.170µg/LEthylbenzene
09/05/23 14:383.000.350<0.350µg/LHexachlorobutadiene
09/05/23 14:381.000.380<0.380µg/L2-Hexanone
09/05/23 14:380.5000.180<0.180µg/LIsopropylbenzene
09/05/23 14:380.5000.089<0.089µg/L4-Isopropyl toluene
09/05/23 14:385.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/05/23 14:381.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/05/23 14:381.000.078<0.078µg/L4-Methyl-2-Pentanone
09/05/23 14:382.000.330<0.330µg/LMethylene Chloride
09/05/23 14:381.000.470<0.470µg/LNaphthalene
09/05/23 14:380.5000.190<0.190µg/Ln-Propylbenzene
09/05/23 14:380.5000.220<0.220µg/LStyrene
09/05/23 14:380.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
09/05/23 14:380.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/05/23 14:380.5000.220<0.220µg/LTetrachloroethene
09/05/23 14:380.5000.220<0.220µg/LToluene
Page 3 of 61Date:09/15/2023 05:49 PM
Page 133 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
Associated Lab Samples: 93895
LRB-V37495 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/05/23 14:380.5000.380<0.380µg/L1,2,3-Trichlorobenzene
09/05/23 14:380.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/05/23 14:380.5000.160<0.160µg/L1,1,1-Trichloroethane
09/05/23 14:380.5000.096<0.096µg/L1,1,2-Trichloroethane
09/05/23 14:380.5000.180<0.180µg/LTrichloroethene
09/05/23 14:380.5000.180<0.180µg/LTrichlorofluoromethane
09/05/23 14:380.5000.270<0.270µg/L1,2,3-Trichloropropane
09/05/23 14:380.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/05/23 14:380.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/05/23 14:385.001.00<1.00µg/LVinyl Acetate
09/05/23 14:380.5000.170<0.170µg/LVinyl Chloride
09/05/23 14:380.5000.210<0.210µg/Lo-Xylene
09/05/23 14:381.000.420<0.420µg/Lm,p-Xylene
09/05/23 14:384-Bromofluorobenzene (S)96.4 70-130
09/05/23 14:38Dibromofluoromethane (S)102 70-130
09/05/23 14:381,2-Dichloroethane - d4 (S)90.0 70-130
09/05/23 14:38Toluene-d8 (S)101 70-130
LCS-V37495 LCSD-V37495Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.2 93.078.531.440.0µg/LAcetone 40-160 16.9 20.0
20.9 10510420.820.0µg/LBenzene 70-130 0.4 20.0
19.0 95.097.019.420.0µg/LBromobenzene 70-130 2.0 20.0
21.7 10910420.820.0µg/LBromochloromethane 70-130 4.2 20.0
19.1 95.594.518.920.0µg/LBromodichloromethane 70-130 1.0 20.0
Page 4 of 61Date:09/15/2023 05:49 PM
Page 134 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
LCS-V37495 LCSD-V37495Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.6 88.089.517.920.0µg/LBromoform 70-130 1.6 20.0
22.4 11210721.420.0µg/LBromomethane 60-140 4.5 20.0
20.8 10410821.520.0µg/Ln-Butylbenzene 70-130 3.3 20.0
20.4 10210420.720.0µg/Lsec-Butyl benzene 70-130 1.4 20.0
19.0 95.098.519.720.0µg/Ltert-Butyl benzene 70-130 3.6 20.0
20.2 10110220.320.0µg/LCarbon Tetrachloride 70-130 0.4 20.0
19.7 98.510120.120.0µg/LChlorobenzene 70-130 2.0 20.0
19.2 96.099.019.820.0µg/LChlorodibromomethane 70-130 3.0 20.0
20.4 10210520.920.0µg/LChloroethane 60-140 2.4 20.0
20.0 10010020.020.0µg/LChloroform 70-130 0.0 20.0
19.1 95.595.519.120.0µg/LChloromethane 60-140 0.0 20.0
19.3 96.595.019.020.0µg/L2-Chlorotoluene 70-130 1.5 20.0
18.7 93.596.519.320.0µg/L4-Chlorotoluene 70-130 3.1 20.0
20.6 10310220.420.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.9 20.0
19.2 96.095.019.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.0 20.0
19.6 98.098.519.720.0µg/L1,2-Dibromoethane 70-130 0.5 20.0
17.9 89.591.518.320.0µg/LDibromomethane 70-130 2.2 20.0
19.5 97.510120.220.0µg/L1,2-Dichlorobenzene 70-130 3.5 20.0
20.0 10010320.520.0µg/L1,3-Dichlorobenzene 70-130 2.4 20.0
19.9 99.598.519.720.0µg/L1,4-Dichlorobenzene 70-130 1.0 20.0
18.5 92.593.018.620.0µg/LDichlorodifluoromethane 60-140 0.5 20.0
20.7 10410320.620.0µg/L1,1-Dichloroethane 70-130 0.4 20.0
16.8 84.083.016.620.0µg/L1,2-Dichloroethane 70-130 1.1 20.0
23.1 11610120.120.0µg/L1,1-Dichloroethene 70-130 13.8 20.0
19.6 98.099.519.920.0µg/Lcis-1,2-Dichloroethene 70-130 1.5 20.0
22.1 11110120.120.0µg/Ltrans-1,2-Dichloroethene 70-130 9.4 20.0
Page 5 of 61Date:09/15/2023 05:49 PM
Page 135 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
LCS-V37495 LCSD-V37495Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.8 99.010220.420.0µg/L1,2-Dichloropropane 70-130 2.9 20.0
19.2 96.097.519.520.0µg/L1,3-Dichloropropane 70-130 1.5 20.0
20.3 10210320.520.0µg/L2,2-Dichloropropane 70-130 0.9 20.0
22.7 11411322.620.0µg/L1,1-Dichloropropene 70-130 0.4 20.0
19.9 99.597.019.420.0µg/Lcis-1,3-Dichloropropene 70-130 2.5 20.0
18.6 93.094.018.820.0µg/Ltrans-1,3-Dichloropropene 70-130 1.0 20.0
493 98.688.4442500µg/LEthanol 60-140 10.9 20.0
19.1 95.594.018.820.0µg/LEthylbenzene 70-130 1.5 20.0
19.8 99.010420.720.0µg/LHexachlorobutadiene 70-130 4.4 20.0
18.1 90.586.017.220.0µg/L2-Hexanone 60-140 5.0 20.0
20.2 10110320.520.0µg/LIsopropylbenzene 70-130 1.4 20.0
20.7 10410420.820.0µg/L4-Isopropyl toluene 70-130 0.4 20.0
16.6 83.096.019.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 14.5 20.0
21.4 10710020.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 6.7 20.0
17.7 88.587.017.420.0µg/L4-Methyl-2-Pentanone 60-140 1.7 20.0
21.8 10995.019.020.0µg/LMethylene Chloride 70-130 13.7 20.0
18.0 90.093.518.720.0µg/LNaphthalene 70-130 3.8 20.0
19.7 98.510120.120.0µg/Ln-Propylbenzene 70-130 2.0 20.0
21.0 10510220.320.0µg/LStyrene 70-130 3.3 20.0
20.5 10310721.320.0µg/L1,1,1,2-Tetrachloroethane 70-130 3.8 20.0
19.5 97.599.019.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.5 20.0
20.1 10110220.320.0µg/LTetrachloroethene 70-130 0.9 20.0
19.5 97.598.519.720.0µg/LToluene 70-130 1.0 20.0
18.7 93.597.019.420.0µg/L1,2,3-Trichlorobenzene 70-130 3.6 20.0
18.9 94.599.019.820.0µg/L1,2,4-Trichlorobenzene 70-130 4.6 20.0
20.3 10210120.220.0µg/L1,1,1-Trichloroethane 70-130 0.4 20.0
Page 6 of 61Date:09/15/2023 05:49 PM
Page 136 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
LCS-V37495 LCSD-V37495Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.7 98.510320.620.0µg/L1,1,2-Trichloroethane 70-130 4.4 20.0
20.8 10410120.120.0µg/LTrichloroethene 70-130 3.4 20.0
21.1 10610821.520.0µg/LTrichlorofluoromethane 60-140 1.8 20.0
19.4 97.095.519.120.0µg/L1,2,3-Trichloropropane 70-130 1.5 20.0
20.1 10199.519.920.0µg/L1,2,4-Trimethylbenzene 70-130 1.0 20.0
19.6 98.098.519.720.0µg/L1,3,5-Trimethylbenzene 70-130 0.5 20.0
20.1 10198.519.720.0µg/LVinyl Acetate 60-140 2.0 20.0
21.8 10911021.920.0µg/LVinyl Chloride 60-140 0.4 20.0
19.6 98.098.019.620.0µg/Lo-Xylene 70-130 0.0 20.0
39.5 98.710040.140.0µg/Lm,p-Xylene 70-130 1.5 20.0
91.493.44-Bromofluorobenzene (S)70-130
99.498.8Dibromofluoromethane (S)70-130
90.089.41,2-Dichloroethane - d4 (S)70-130
99.6100Toluene-d8 (S)70-130
Page 7 of 61Date:09/15/2023 05:49 PM
Page 137 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37564QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37563
Associated Lab Samples: 93892, 93893, 93894, 93896
LRB-V37563 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/23 01:3010.01.80<1.80µg/LAcetone
09/07/23 01:300.5000.180<0.180µg/LBenzene
09/07/23 01:300.5000.210<0.210µg/LBromobenzene
09/07/23 01:301.000.420<0.420µg/LBromochloromethane
09/07/23 01:300.5000.160<0.160µg/LBromodichloromethane
09/07/23 01:305.001.50<1.50µg/LBromoform
09/07/23 01:301.000.280<0.280µg/LBromomethane
09/07/23 01:300.5000.180<0.180µg/Ln-Butylbenzene
09/07/23 01:300.5000.200<0.200µg/Lsec-Butyl benzene
09/07/23 01:302.000.920<0.920µg/Ltert-Butyl benzene
09/07/23 01:300.5000.180<0.180µg/LCarbon Tetrachloride
09/07/23 01:300.5000.190<0.190µg/LChlorobenzene
09/07/23 01:300.5000.190<0.190µg/LChlorodibromomethane
09/07/23 01:301.000.430<0.430µg/LChloroethane
09/07/23 01:300.5000.220<0.220µg/LChloroform
09/07/23 01:300.5000.220<0.220µg/LChloromethane
09/07/23 01:300.5000.200<0.200µg/L2-Chlorotoluene
09/07/23 01:300.5000.200<0.200µg/L4-Chlorotoluene
09/07/23 01:300.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/07/23 01:302.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/07/23 01:300.5000.230<0.230µg/LDibromomethane
09/07/23 01:300.5000.220<0.220µg/L1,2-Dichlorobenzene
09/07/23 01:300.5000.190<0.190µg/L1,3-Dichlorobenzene
09/07/23 01:300.5000.210<0.210µg/L1,4-Dichlorobenzene
09/07/23 01:305.001.20<1.20µg/LDichlorodifluoromethane
09/07/23 01:300.5000.240<0.240µg/L1,1-Dichloroethane
09/07/23 01:300.5000.150<0.150µg/L1,2-Dichloroethane
Page 8 of 61Date:09/15/2023 05:49 PM
Page 138 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37564QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37563
Associated Lab Samples: 93892, 93893, 93894, 93896
LRB-V37563 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/23 01:300.5000.150<0.150µg/L1,1-Dichloroethene
09/07/23 01:300.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/07/23 01:300.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/07/23 01:300.5000.190<0.190µg/L1,2-Dichloropropane
09/07/23 01:300.5000.130<0.130µg/L1,3-Dichloropropane
09/07/23 01:302.000.210<0.210µg/L2,2-Dichloropropane
09/07/23 01:300.5000.200<0.200µg/L1,1-Dichloropropene
09/07/23 01:300.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/07/23 01:300.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/07/23 01:3020042.0<42.0µg/LEthanol
09/07/23 01:300.5000.170<0.170µg/LEthylbenzene
09/07/23 01:303.000.350<0.350µg/LHexachlorobutadiene
09/07/23 01:301.000.380<0.380µg/L2-Hexanone
09/07/23 01:300.5000.180<0.180µg/LIsopropylbenzene
09/07/23 01:300.5000.089<0.089µg/L4-Isopropyl toluene
09/07/23 01:305.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/07/23 01:301.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/07/23 01:301.000.078<0.078µg/L4-Methyl-2-Pentanone
09/07/23 01:302.000.330<0.330µg/LMethylene Chloride
09/07/23 01:301.000.470<0.470µg/LNaphthalene
09/07/23 01:300.5000.190<0.190µg/Ln-Propylbenzene
09/07/23 01:300.5000.220<0.220µg/LStyrene
09/07/23 01:3010.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
09/07/23 01:3010.00.350<0.350µg/Ltert-Butyl formate (TBF)
09/07/23 01:3010.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
09/07/23 01:3010.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
09/07/23 01:300.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
Page 9 of 61Date:09/15/2023 05:49 PM
Page 139 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37564QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37563
Associated Lab Samples: 93892, 93893, 93894, 93896
LRB-V37563 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/23 01:300.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/07/23 01:300.5000.220<0.220µg/LTetrachloroethene
09/07/23 01:300.5000.220<0.220µg/LToluene
09/07/23 01:300.5000.380<0.380µg/L1,2,3-Trichlorobenzene
09/07/23 01:300.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/07/23 01:300.5000.160<0.160µg/L1,1,1-Trichloroethane
09/07/23 01:300.5000.096<0.096µg/L1,1,2-Trichloroethane
09/07/23 01:300.5000.180<0.180µg/LTrichloroethene
09/07/23 01:300.5000.180<0.180µg/LTrichlorofluoromethane
09/07/23 01:300.5000.270<0.270µg/L1,2,3-Trichloropropane
09/07/23 01:300.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/07/23 01:300.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/07/23 01:305.001.00<1.00µg/LVinyl Acetate
09/07/23 01:300.5000.170<0.170µg/LVinyl Chloride
09/07/23 01:300.5000.210<0.210µg/Lo-Xylene
09/07/23 01:301.000.420<0.420µg/Lm,p-Xylene
09/07/23 01:3010.01.00<1.00µg/L3,3-Dimethyl-1-butanol
09/07/23 01:304-Bromofluorobenzene (S)102 70-130
09/07/23 01:30Dibromofluoromethane (S)99.0 70-130
09/07/23 01:301,2-Dichloroethane - d4 (S)96.6 70-130
09/07/23 01:30Toluene-d8 (S)100 70-130
LCS-V37563 LCSD-V37563Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
28.9 72.267.527.040.0µg/LAcetone 40-160 6.7 20.0
Page 10 of 61Date:09/15/2023 05:49 PM
Page 140 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37564QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37563
LCS-V37563 LCSD-V37563Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.1 11111122.220.0µg/LBenzene 70-130 0.4 20.0
21.7 10910821.520.0µg/LBromobenzene 70-130 0.9 20.0
21.4 10710520.920.0µg/LBromochloromethane 70-130 2.3 20.0
21.1 10610420.820.0µg/LBromodichloromethane 70-130 1.4 20.0
19.7 98.598.019.620.0µg/LBromoform 70-130 0.5 20.0
22.3 11211021.920.0µg/LBromomethane 60-140 1.8 20.0
21.7 10910821.620.0µg/Ln-Butylbenzene 70-130 0.4 20.0
21.1 10610721.320.0µg/Lsec-Butyl benzene 70-130 0.9 20.0
21.2 10610621.120.0µg/Ltert-Butyl benzene 70-130 0.4 20.0
22.0 11011022.020.0µg/LCarbon Tetrachloride 70-130 0.0 20.0
21.4 10710821.620.0µg/LChlorobenzene 70-130 0.9 20.0
21.1 10610320.620.0µg/LChlorodibromomethane 70-130 2.3 20.0
22.2 11111322.520.0µg/LChloroethane 60-140 1.3 20.0
21.3 10710621.120.0µg/LChloroform 70-130 0.9 20.0
19.5 97.510120.120.0µg/LChloromethane 60-140 3.0 20.0
21.5 10810721.320.0µg/L2-Chlorotoluene 70-130 0.9 20.0
21.6 10810921.820.0µg/L4-Chlorotoluene 70-130 0.9 20.0
21.3 10710621.220.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.4 20.0
23.1 11610721.320.0µg/L1,2-Dibromo-3-Chloropropane 70-130 8.1 20.0
21.8 10910320.620.0µg/LDibromomethane 70-130 5.6 20.0
22.1 11110921.720.0µg/L1,2-Dichlorobenzene 70-130 1.8 20.0
21.4 10710621.220.0µg/L1,3-Dichlorobenzene 70-130 0.9 20.0
21.3 10710621.120.0µg/L1,4-Dichlorobenzene 70-130 0.9 20.0
21.2 10610821.620.0µg/LDichlorodifluoromethane 60-140 1.8 20.0
21.9 11011022.020.0µg/L1,1-Dichloroethane 70-130 0.4 20.0
20.7 10410320.520.0µg/L1,2-Dichloroethane 70-130 0.9 20.0
Page 11 of 61Date:09/15/2023 05:49 PM
Page 141 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37564QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37563
LCS-V37563 LCSD-V37563Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
23.2 11611523.020.0µg/L1,1-Dichloroethene 70-130 0.8 20.0
22.0 11011022.020.0µg/Lcis-1,2-Dichloroethene 70-130 0.0 20.0
22.4 11211122.120.0µg/Ltrans-1,2-Dichloroethene 70-130 1.3 20.0
21.7 10910821.520.0µg/L1,2-Dichloropropane 70-130 0.9 20.0
21.3 10710521.020.0µg/L1,3-Dichloropropane 70-130 1.4 20.0
19.6 98.098.519.720.0µg/L2,2-Dichloropropane 70-130 0.5 20.0
23.4 11711723.320.0µg/L1,1-Dichloropropene 70-130 0.4 20.0
21.3 10710621.120.0µg/Lcis-1,3-Dichloropropene 70-130 0.9 20.0
21.6 10810621.120.0µg/Ltrans-1,3-Dichloropropene 70-130 2.3 20.0
491 98.298.6493500µg/LEthanol 60-140 0.4 20.0
21.5 10810721.420.0µg/LEthylbenzene 70-130 0.4 20.0
21.1 10610420.820.0µg/LHexachlorobutadiene 70-130 1.4 20.0
19.8 99.092.518.520.0µg/L2-Hexanone 60-140 6.7 20.0
22.2 11111021.920.0µg/LIsopropylbenzene 70-130 1.3 20.0
21.7 10910921.720.0µg/L4-Isopropyl toluene 70-130 0.0 20.0
19.4 97.089.517.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 8.0 20.0
21.9 11010721.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.3 20.0
21.7 10910120.120.0µg/L4-Methyl-2-Pentanone 60-140 7.6 20.0
21.8 10911022.020.0µg/LMethylene Chloride 70-130 0.9 20.0
24.6 12311823.520.0µg/LNaphthalene 70-130 4.5 20.0
22.0 11011021.920.0µg/Ln-Propylbenzene 70-130 0.4 20.0
21.6 10810821.520.0µg/LStyrene 70-130 0.4 20.0
42.8 10710542.040.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.8 20.0
37.1 92.710240.740.0µg/Ltert-Butyl formate (TBF)40-140 9.2 20.0
17.5 87.588.517.720.0µg/Ltert-Amyl Alcohol (TAA)40-140 1.1 20.0
44.8 11211043.940.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 2.0 20.0
Page 12 of 61Date:09/15/2023 05:49 PM
Page 142 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37564QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37563
LCS-V37563 LCSD-V37563Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.7 10911021.920.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.9 20.0
20.9 10510120.220.0µg/L1,1,2,2-Tetrachloroethane 70-130 3.4 20.0
21.6 10810821.520.0µg/LTetrachloroethene 70-130 0.4 20.0
22.3 11211022.020.0µg/LToluene 70-130 1.3 20.0
27.4 137*12825.520.0µg/L1,2,3-Trichlorobenzene 70-130 7.1 20.0
23.6 11811522.920.0µg/L1,2,4-Trichlorobenzene 70-130 3.0 20.0
21.8 10910921.820.0µg/L1,1,1-Trichloroethane 70-130 0.0 20.0
21.5 10810521.020.0µg/L1,1,2-Trichloroethane 70-130 2.3 20.0
22.8 11411222.420.0µg/LTrichloroethene 70-130 1.7 20.0
22.2 11111222.320.0µg/LTrichlorofluoromethane 60-140 0.4 20.0
22.1 11110220.420.0µg/L1,2,3-Trichloropropane 70-130 8.0 20.0
21.8 10910821.620.0µg/L1,2,4-Trimethylbenzene 70-130 0.9 20.0
21.7 10910921.720.0µg/L1,3,5-Trimethylbenzene 70-130 0.0 20.0
17.0 85.098.519.720.0µg/LVinyl Acetate 60-140 14.7 20.0
23.2 11611823.520.0µg/LVinyl Chloride 60-140 1.2 20.0
21.3 10710721.320.0µg/Lo-Xylene 70-130 0.0 20.0
45.9 11511546.140.0µg/Lm,p-Xylene 70-130 0.4 20.0
17.8 89.082.516.520.0µg/L3,3-Dimethyl-1-butanol 70-130 7.5 20.0
10099.04-Bromofluorobenzene (S)70-130
98.697.6Dibromofluoromethane (S)70-130
99.899.41,2-Dichloroethane - d4 (S)70-130
99.4101Toluene-d8 (S)70-130
Page 13 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 143 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37632QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37631
Associated Lab Samples: 93892, 93894, 93896
LRB-V37631 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/23 13:371.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/07/23 13:3710.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
09/07/23 13:370.5000.220<0.220µg/LToluene
09/07/23 13:374-Bromofluorobenzene (S)99.2 70-130
09/07/23 13:37Dibromofluoromethane (S)98.6 70-130
09/07/23 13:371,2-Dichloroethane - d4 (S)96.0 70-130
09/07/23 13:37Toluene-d8 (S)97.2 70-130
LCS-V37631 LCSD-V37631Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.1 11111021.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.9 20.0
22.2 11194.018.820.0µg/Ltert-Amyl Alcohol (TAA)40-140 16.5 20.0
22.3 11211422.820.0µg/LToluene 70-130 2.2 20.0
99.299.84-Bromofluorobenzene (S)70-130
97.297.4Dibromofluoromethane (S)70-130
97.697.21,2-Dichloroethane - d4 (S)70-130
99.499.4Toluene-d8 (S)70-130
Page 14 of 61Date:09/15/2023 05:49 PM
Page 144 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37910QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37909
Associated Lab Samples: 93892
LRB-V37909 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/15/23 04:511.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/15/23 04:514-Bromofluorobenzene (S)99.4 70-130
09/15/23 04:51Dibromofluoromethane (S)101 70-130
09/15/23 04:511,2-Dichloroethane - d4 (S)97.6 70-130
09/15/23 04:51Toluene-d8 (S)100 70-130
LCS-V37909 LCSD-V37909Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.9 11010921.720.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.9 20.0
95.297.04-Bromofluorobenzene (S)70-130
10196.4Dibromofluoromethane (S)70-130
97.497.81,2-Dichloroethane - d4 (S)70-130
101100Toluene-d8 (S)70-130
Page 15 of 61Date:09/15/2023 05:49 PM
Page 145 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37430QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37391
Associated Lab Samples: 93893, 93896
LRB-V37391 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/05/23 18:132.000.302<0.302µg/LAcenaphthene
09/05/23 18:132.000.297<0.297µg/LAcenaphthylene
09/05/23 18:132.000.836<0.836µg/LAnthracene
09/05/23 18:1310.01.32<1.32µg/LBenzidine
09/05/23 18:132.000.637<0.637µg/LBenzo(a)anthracene
09/05/23 18:132.001.02<1.02µg/LBenzo(a)pyrene
09/05/23 18:135.002.49<2.49µg/LBenzo(b)fluoranthene
09/05/23 18:135.001.01<1.01µg/LBenzo(g,h,i)perylene
09/05/23 18:135.001.99<1.99µg/LBenzo(k)fluoranthene
09/05/23 18:1310.01.10<1.10µg/LBenzoic Acid
09/05/23 18:135.000.684<0.684µg/LBenzyl alcohol
09/05/23 18:135.000.468<0.468µg/LBis(2-Chloroethoxy)methane
09/05/23 18:135.001.04<1.04µg/LBis(2-Chloroethyl)ether
09/05/23 18:135.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
09/05/23 18:1310.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
09/05/23 18:135.001.11<1.11µg/L4-Bromophenyl phenyl ether
09/05/23 18:135.001.83<1.83µg/LButyl benzyl phthalate
09/05/23 18:135.001.18<1.18µg/L4-Chloro-3-methylphenol
09/05/23 18:1320.07.38<7.38µg/L2-Chloronaphthalene
09/05/23 18:1310.00.938<0.938µg/L2-Chlorophenol
09/05/23 18:135.001.71<1.71µg/L4-Chlorophenyl phenyl ether
09/05/23 18:132.000.405<0.405µg/LChrysene
09/05/23 18:132.000.434<0.434µg/LDibenz(a,h)anthracene
09/05/23 18:135.000.856<0.856µg/LDibenzofuran
09/05/23 18:135.002.00<2.00µg/L1,2-Dichlorobenzene
09/05/23 18:135.002.00<2.00µg/L1,3-Dichlorobenzene
09/05/23 18:135.002.05<2.05µg/L1,4-Dichlorobenzene
Page 16 of 61Date:09/15/2023 05:49 PM
Page 146 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37430QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37391
Associated Lab Samples: 93893, 93896
LRB-V37391 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/05/23 18:135.001.89<1.89µg/L3,3'-Dichlorobenzidine
09/05/23 18:1310.01.46<1.46µg/L2,4-Dichlorophenol
09/05/23 18:135.000.745<0.745µg/LDiethyl phthalate
09/05/23 18:135.000.939<0.939µg/LDimethyl phthalate
09/05/23 18:1320.01.57<1.57µg/L2,4-Dimethylphenol
09/05/23 18:135.002.06<2.06µg/LDi-n-butyl phthalate
09/05/23 18:1310.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
09/05/23 18:1310.01.92<1.92µg/L2,4-Dinitrophenol
09/05/23 18:135.001.11<1.11µg/L2,4-Dinitrotoluene
09/05/23 18:135.000.809<0.809µg/L2,6-Dinitrotoluene
09/05/23 18:135.001.65<1.65µg/LDi-n-Octyl Phthalate
09/05/23 18:132.000.250<0.250µg/LFluoranthene
09/05/23 18:132.000.807<0.807µg/LFluorene
09/05/23 18:135.000.979<0.979µg/LHexachlorobenzene
09/05/23 18:135.002.73<2.73µg/LHexachlorobutadiene
09/05/23 18:135.002.05<2.05µg/LHexachlorocyclopentadiene
09/05/23 18:135.001.76<1.76µg/LHexachloroethane
09/05/23 18:132.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
09/05/23 18:135.000.444<0.444µg/LIsophorone
09/05/23 18:132.001.14<1.14µg/L1-Methylnaphthalene
09/05/23 18:132.000.666<0.666µg/L2-Methylnaphthalene
09/05/23 18:132.000.728<0.728µg/LNaphthalene
09/05/23 18:135.000.905<0.905µg/LNitrobenzene
09/05/23 18:135.000.493<0.493µg/L2-Nitrophenol
09/05/23 18:1310.01.23<1.23µg/L4-Nitrophenol
09/05/23 18:135.001.10<1.10µg/LN-Nitrosodiphenylamine
09/05/23 18:135.000.641<0.641µg/LN-Nitroso-di-n-propylamine
Page 17 of 61Date:09/15/2023 05:49 PM
Page 147 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37430QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37391
Associated Lab Samples: 93893, 93896
LRB-V37391 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/05/23 18:135.001.43<1.43µg/LPentachlorophenol
09/05/23 18:132.000.428<0.428µg/LPhenanthrene
09/05/23 18:135.000.651<0.651µg/LPhenol
09/05/23 18:132.000.434<0.434µg/LPyrene
09/05/23 18:135.002.21<2.21µg/L1,2,4-Trichlorobenzene
09/05/23 18:135.001.32<1.32µg/L2,4,6-Trichlorophenol
09/05/23 18:132-Fluorobiphenyl (S)65.6 49-118
09/05/23 18:132-Fluorophenol (S)35.4 22-84
09/05/23 18:13Nitrobenzene-d5 (S)61.4 43-123
09/05/23 18:134-Terphenyl-d14 (S)78.0 49-151
09/05/23 18:132,4,6-Tribromophenol (S)68.6 31-144
09/05/23 18:13Phenol-d5 (S)23.4 10-63
LCS-V37391 LCSD-V37391Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
34.7 69.465.832.950.0µg/LAcenaphthene 47-145 5.3 20.0
33.9 67.865.432.750.0µg/LAcenaphthylene 33-145 3.6 20.0
39.1 78.273.436.750.0µg/LAnthracene 27-133 6.3 20.0
7.02 14.0*35.217.650.0µg/LBenzidine 15-150 85.9*20.0
37.8 75.670.835.450.0µg/LBenzo(a)anthracene 33-143 6.5 20.0
39.6 79.274.837.450.0µg/LBenzo(a)pyrene 17-163 5.7 20.0
37.6 75.271.435.750.0µg/LBenzo(b)fluoranthene 24-159 5.1 20.0
36.3 72.669.434.750.0µg/LBenzo(g,h,i)perylene 10-219 4.5 20.0
36.3 72.669.034.550.0µg/LBenzo(k)fluoranthene 11-162 5.0 20.0
11.9 23.811.55.7750.0µg/LBenzoic Acid 10-125 69.3*20.0
Page 18 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 148 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37430QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37391
LCS-V37391 LCSD-V37391Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
66.7 133*120*59.850.0µg/LBenzyl alcohol 16-107 10.9 20.0
30.8 61.655.827.950.0µg/LBis(2-Chloroethoxy)methane 33-184 9.8 20.0
31.8 63.659.629.850.0µg/LBis(2-Chloroethyl)ether 12-158 6.4 20.0
31.2 62.458.429.250.0µg/LBis(2-Chloroisopropyl)ether 36-166 6.6 20.0
41.0 82.076.638.350.0µg/LBis(2-ethylhexyl)phthalate 10-158 6.8 20.0
40.6 81.275.237.650.0µg/L4-Bromophenyl phenyl ether 53-127 7.6 20.0
38.8 77.673.036.550.0µg/LButyl benzyl phthalate 10-152 6.1 20.0
35.0 70.062.631.350.0µg/L4-Chloro-3-methylphenol 22-147 11.1 20.0
33.5 67.063.631.850.0µg/L2-Chloronaphthalene 60-118 5.2 20.0
31.4 62.857.028.550.0µg/L2-Chlorophenol 23-134 9.6 20.0
37.3 74.670.435.250.0µg/L4-Chlorophenyl phenyl ether 25-158 5.7 20.0
37.1 74.269.634.850.0µg/LChrysene 17-168 6.3 20.0
28.8 57.654.827.450.0µg/LDibenz(a,h)anthracene 10-227 4.9 20.0
34.1 68.264.832.450.0µg/LDibenzofuran 39-114 5.1 20.0
28.8 57.654.427.250.0µg/L1,2-Dichlorobenzene 32-129 5.7 20.0
28.0 56.052.226.150.0µg/L1,3-Dichlorobenzene 20-124 7.0 20.0
28.4 56.852.626.350.0µg/L1,4-Dichlorobenzene 20-124 7.6 20.0
38.8 77.672.236.150.0µg/L3,3'-Dichlorobenzidine 10-262 7.2 20.0
33.8 67.661.830.950.0µg/L2,4-Dichlorophenol 39-135 8.9 20.0
38.0 76.073.036.550.0µg/LDiethyl phthalate 10-114 4.0 20.0
38.2 76.472.836.450.0µg/LDimethyl phthalate 10-112 4.8 20.0
35.8 71.677.638.850.0µg/L2,4-Dimethylphenol 32-119 8.0 20.0
42.4 84.879.839.950.0µg/LDi-n-butyl phthalate 10-118 6.0 20.0
32.3 64.657.828.950.0µg/L4,6-Dinitro-2-methylphenol 10-181 11.1 20.0
30.8 61.656.028.050.0µg/L2,4-Dinitrophenol 10-191 9.5 20.0
37.3 74.672.636.350.0µg/L2,4-Dinitrotoluene 39-139 2.7 20.0
Page 19 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 149 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37430QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37391
LCS-V37391 LCSD-V37391Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.0 74.071.235.650.0µg/L2,6-Dinitrotoluene 50-158 3.8 20.0
39.9 79.877.438.750.0µg/LDi-n-Octyl Phthalate 10-146 3.0 20.0
36.2 72.469.234.650.0µg/LFluoranthene 26-137 4.5 20.0
35.3 70.667.633.850.0µg/LFluorene 59-121 4.3 20.0
39.5 79.074.037.050.0µg/LHexachlorobenzene 10-152 6.5 20.0
30.2 60.456.828.450.0µg/LHexachlorobutadiene 24-116 6.1 20.0
31.5 63.059.429.750.0µg/LHexachlorocyclopentadiene 32-117 5.8 20.0
27.0 54.049.024.550.0µg/LHexachloroethane 40-113 9.7 20.0
37.7 75.470.435.250.0µg/LIndeno(1,2,3-cd)pyrene 10-171 6.8 20.0
28.0 56.051.825.950.0µg/LIsophorone 21-196 7.7 20.0
29.9 59.855.827.950.0µg/L1-Methylnaphthalene 40-135 6.9 20.0
30.1 60.255.827.950.0µg/L2-Methylnaphthalene 18-121 7.5 20.0
28.0 56.052.226.150.0µg/LNaphthalene 21-133 7.0 20.0
27.0 54.051.025.550.0µg/LNitrobenzene 35-180 5.7 20.0
30.4 60.854.627.350.0µg/L2-Nitrophenol 29-182 10.7 20.0
20.6 41.241.220.650.0µg/L4-Nitrophenol 10-132 0.0 20.0
45.0 90.084.642.350.0µg/LN-Nitrosodiphenylamine 69-152 6.1 20.0
34.7 69.463.631.850.0µg/LN-Nitroso-di-n-propylamine 10-230 8.7 20.0
50.8 10295.847.950.0µg/LPentachlorophenol 14-176 5.8 20.0
37.1 74.269.834.950.0µg/LPhenanthrene 54-120 6.1 20.0
15.4 30.829.014.550.0µg/LPhenol 10-112 6.0 20.0
36.3 72.669.034.550.0µg/LPyrene 52-115 5.0 20.0
28.3 56.652.226.150.0µg/L1,2,4-Trichlorobenzene 44-142 8.0 20.0
33.6 67.265.232.650.0µg/L2,4,6-Trichlorophenol 37-144 3.0 20.0
66.264.22-Fluorobiphenyl (S)49-118
33.632.72-Fluorophenol (S)22-84
Page 20 of 61Date:09/15/2023 05:49 PM
Page 150 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37430QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37391
LCS-V37391 LCSD-V37391Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
56.652.4Nitrobenzene-d5 (S)43-123
76.873.44-Terphenyl-d14 (S)49-151
70.869.42,4,6-Tribromophenol (S)31-144
23.322.3Phenol-d5 (S)10-63
Page 21 of 61Date:09/15/2023 05:49 PM
Page 151 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
Associated Lab Samples: 93883, 93884, 93885, 93886, 93887, 93888
LRB-V37418 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 11:050.0200.002<0.002mg/KgAcetone
09/01/23 11:050.0200.001<0.001mg/KgAcrolein
09/01/23 11:050.0200.0008<0.0008mg/KgAcrylonitrile
09/01/23 11:050.0050.0006<0.0006mg/KgBenzene
09/01/23 11:050.0050.0005<0.0005mg/KgBromobenzene
09/01/23 11:050.0050.0008<0.0008mg/KgBromochloromethane
09/01/23 11:050.0050.001<0.001mg/KgBromodichloromethane
09/01/23 11:050.0050.001<0.001mg/KgBromoform
09/01/23 11:050.0100.001<0.001mg/KgBromomethane
09/01/23 11:050.0050.0005<0.0005mg/Kgn-Butylbenzene
09/01/23 11:050.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/01/23 11:050.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/01/23 11:050.0050.0006<0.0006mg/KgCarbon Disulfide
09/01/23 11:050.0050.001<0.001mg/KgCarbon Tetrachloride
09/01/23 11:050.0050.0007<0.0007mg/KgChlorobenzene
09/01/23 11:050.0050.0009<0.0009mg/KgChlorodibromomethane
09/01/23 11:050.0100.0009<0.0009mg/KgChloroethane
09/01/23 11:050.0050.001<0.001mg/KgChloroform
09/01/23 11:050.0100.0006<0.0006mg/KgChloromethane
09/01/23 11:050.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/01/23 11:050.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/01/23 11:050.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/01/23 11:050.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/01/23 11:050.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/01/23 11:050.0050.0006<0.0006mg/KgDibromomethane
09/01/23 11:050.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/01/23 11:050.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 22 of 61Date:09/15/2023 05:49 PM
Page 152 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
Associated Lab Samples: 93883, 93884, 93885, 93886, 93887, 93888
LRB-V37418 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 11:050.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/01/23 11:050.0100.001<0.001mg/KgDichlorodifluoromethane
09/01/23 11:050.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/01/23 11:050.0050.001<0.001mg/Kg1,2-Dichloroethane
09/01/23 11:050.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/01/23 11:050.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/01/23 11:050.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/01/23 11:050.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/01/23 11:050.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/01/23 11:050.0050.001<0.001mg/Kg2,2-Dichloropropane
09/01/23 11:050.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/01/23 11:050.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/01/23 11:050.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/01/23 11:050.0050.0006<0.0006mg/KgEthylbenzene
09/01/23 11:050.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/01/23 11:050.0100.0008<0.0008mg/KgHexachlorobutadiene
09/01/23 11:050.0100.0007<0.0007mg/Kgn-Hexane
09/01/23 11:050.0200.0006<0.0006mg/Kg2-Hexanone
09/01/23 11:050.0050.0005<0.0005mg/KgIsopropylbenzene
09/01/23 11:050.0050.001<0.001mg/Kg4-Isopropyl toluene
09/01/23 11:050.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/01/23 11:050.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/01/23 11:050.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/01/23 11:050.0100.001<0.001mg/KgMethylene Chloride
09/01/23 11:050.0100.0010<0.0010mg/KgNaphthalene
09/01/23 11:050.0050.0005<0.0005mg/Kgn-Propylbenzene
09/01/23 11:050.0050.001<0.001mg/KgStyrene
Page 23 of 61Date:09/15/2023 05:49 PM
Page 153 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
Associated Lab Samples: 93883, 93884, 93885, 93886, 93887, 93888
LRB-V37418 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 11:050.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/01/23 11:050.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/01/23 11:050.0050.0009<0.0009mg/KgTetrachloroethene
09/01/23 11:050.0050.0007<0.0007mg/KgToluene
09/01/23 11:050.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/01/23 11:050.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/01/23 11:050.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/01/23 11:050.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/01/23 11:050.0050.0009<0.0009mg/KgTrichloroethene
09/01/23 11:050.0100.002<0.002mg/KgTrichlorofluoromethane
09/01/23 11:050.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/01/23 11:050.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/01/23 11:050.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/01/23 11:050.0100.0005<0.0005mg/KgVinyl Acetate
09/01/23 11:050.0100.0005<0.0005mg/KgVinyl Chloride
09/01/23 11:050.0050.0005<0.0005mg/Kgo-Xylene
09/01/23 11:050.0100.001<0.001mg/Kgm,p-Xylene
09/01/23 11:054-Bromofluorobenzene (S)103 70-130
09/01/23 11:05Dibromofluoromethane (S)105 84-123
09/01/23 11:05Toluene-d8 (S)99.2 76-129
LCS-V37418Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.50.0960.100mg/KgAcetone 29-198
1060.1060.100mg/KgAcrolein 70-130
1120.1120.100mg/KgAcrylonitrile 65-134
Page 24 of 61Date:09/15/2023 05:49 PM
Page 154 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
LCS-V37418Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.40.0480.050mg/KgBenzene 74-127
99.00.0490.050mg/KgBromobenzene 73-125
1040.0510.050mg/KgBromochloromethane 72-134
98.20.0490.050mg/KgBromodichloromethane 75-122
1060.0520.050mg/KgBromoform 66-135
91.00.0450.050mg/KgBromomethane 20-180
1010.0500.050mg/Kgn-Butylbenzene 65-135
99.00.0490.050mg/Kgsec-Butyl benzene 66-131
99.60.0490.050mg/Kgtert-Butyl benzene 67-132
85.40.0420.050mg/KgCarbon Disulfide 61-129
96.00.0480.050mg/KgCarbon Tetrachloride 64-143
98.60.0490.050mg/KgChlorobenzene 74-118
1020.0500.050mg/KgChlorodibromomethane 73-122
95.60.0470.050mg/KgChloroethane 33-149
94.60.0470.050mg/KgChloroform 73-127
83.60.0410.050mg/KgChloromethane 45-143
98.80.0490.050mg/Kg2-Chlorotoluene 67-124
98.80.0490.050mg/Kg4-Chlorotoluene 71-126
92.20.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159
1160.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157
1050.0520.050mg/Kg1,2-Dibromoethane 70-132
99.80.0490.050mg/KgDibromomethane 74-133
1060.0530.050mg/Kg1,2-Dichlorobenzene 72-123
1040.0520.050mg/Kg1,3-Dichlorobenzene 71-120
1000.0500.050mg/Kg1,4-Dichlorobenzene 71-123
1010.0500.050mg/KgDichlorodifluoromethane 26-146
94.00.0470.050mg/Kg1,1-Dichloroethane 74-127
Page 25 of 61Date:09/15/2023 05:49 PM
Page 155 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
LCS-V37418Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.00.0460.050mg/Kg1,2-Dichloroethane 68-128
88.00.0440.050mg/Kg1,1-Dichloroethene 67-149
96.60.0480.050mg/Kgcis-1,2-Dichloroethene 76-134
91.00.0450.050mg/Kgtrans-1,2-Dichloroethene 73-132
96.80.0480.050mg/Kg1,2-Dichloropropane 73-130
1020.0500.050mg/Kg1,3-Dichloropropane 75-124
92.20.0460.050mg/Kg2,2-Dichloropropane 50-142
93.60.0460.050mg/Kg1,1-Dichloropropene 71-130
1030.0510.050mg/Kgcis-1,3-Dichloropropene 71-125
1060.0530.050mg/Kgtrans-1,3-Dichloropropene 68-123
94.60.0470.050mg/KgEthylbenzene 74-128
96.60.0960.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130
1060.0520.050mg/KgHexachlorobutadiene 64-125
98.60.0490.050mg/Kgn-Hexane 70-130
93.40.0460.050mg/Kg2-Hexanone 61-157
98.80.0490.050mg/KgIsopropylbenzene 68-126
1010.0500.050mg/Kg4-Isopropyl toluene 68-129
80.40.0400.050mg/KgMethyl Ethyl Ketone (MEK)63-149
99.60.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130
1000.0500.050mg/Kg4-Methyl-2-Pentanone 57-162
86.00.0430.050mg/KgMethylene Chloride 74-129
1170.0580.050mg/KgNaphthalene 57-157
97.20.0480.050mg/Kgn-Propylbenzene 67-130
1030.0510.050mg/KgStyrene 77-121
1010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115
1040.0520.050mg/Kg1,1,2,2-Tetrachloroethane 56-126
98.60.0490.050mg/KgTetrachloroethene 68-130
Page 26 of 61Date:09/15/2023 05:49 PM
Page 156 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
LCS-V37418Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.00.0480.050mg/KgToluene 71-129
1130.0560.050mg/Kg1,2,3-Trichlorobenzene 68-130
1120.0560.050mg/Kg1,2,4-Trichlorobenzene 66-125
91.60.0450.050mg/Kg1,1,1-Trichloroethane 67-131
1000.0500.050mg/Kg1,1,2-Trichloroethane 70-133
96.60.0480.050mg/KgTrichloroethene 75-133
81.20.0400.050mg/KgTrichlorofluoromethane 44-146
1100.0540.050mg/Kg1,2,3-Trichloropropane 60-137
1020.0510.050mg/Kg1,2,4-Trimethylbenzene 69-129
1000.0500.050mg/Kg1,3,5-Trimethylbenzene 69-128
1070.0530.050mg/KgVinyl Acetate 60-140
79.00.0390.050mg/KgVinyl Chloride 48-147
98.40.0490.050mg/Kgo-Xylene 74-126
96.70.0960.100mg/Kgm,p-Xylene 75-124
1034-Bromofluorobenzene (S)70-130
104Dibromofluoromethane (S)84-123
102Toluene-d8 (S)76-129
V 93785-MS-V37418 V 93785-MSD-V37418Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.022 16.7*0.0260.1000.1000.005mg/KgAcetone 21.0*34-143 17.6 49
0.018 18.7*0.0360.1000.100<0.001mg/KgAcrolein 36.0*70-130 63.2*20
0.050 50.1*0.0600.1000.100<0.0008mg/KgAcrylonitrile 60.0*65-134 17.9 30
0.027 55.0*0.0240.0500.050<0.0006mg/KgBenzene 48.0*60-135 13.5 20
0.024 48.00.0230.0500.050<0.0005mg/KgBromobenzene 46.8 45-135 2.5 25
Page 27 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 157 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
V 93785-MS-V37418 V 93785-MSD-V37418Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.027 54.2*0.0270.0500.050<0.0008mg/KgBromochloromethane 55.2 55-136 1.8 18
0.025 51.6*0.0250.0500.050<0.001mg/KgBromodichloromethane 50.0*55-127 3.1 17
0.026 52.20.0280.0500.050<0.001mg/KgBromoform 56.6 40-136 8.0 35
0.029 58.00.0240.0500.050<0.001mg/KgBromomethane 49.6 30-137 15.6 30
0.023 46.60.0210.0500.050<0.0005mg/Kgn-Butylbenzene 42.8 23-148 8.5 39
0.025 50.80.0220.0500.050<0.0006mg/Kgsec-Butyl benzene 45.4 34-144 11.2 28
0.026 52.20.0230.0500.050<0.0005mg/Kgtert-Butyl benzene 47.2 36-150 10.0 29
0.026 52.40.0210.0500.050<0.0006mg/KgCarbon Disulfide 43.0*49-139 19.7 26
0.029 58.00.0240.0500.050<0.001mg/KgCarbon Tetrachloride 49.4 48-153 16.0 23
0.026 52.8*0.0240.0500.050<0.0007mg/KgChlorobenzene 48.8*57-125 7.8 14
0.025 51.40.0260.0500.050<0.0009mg/KgChlorodibromomethane 53.6 49-127 4.1 24
0.030 60.40.0240.0500.050<0.0009mg/KgChloroethane 49.4 16-177 20.0 47
0.027 54.6*0.0240.0500.050<0.001mg/KgChloroform 49.8*56-137 9.1 18
0.020 41.20.0170.0500.050<0.0006mg/KgChloromethane 34.6*40-145 17.4 26
0.024 49.20.0220.0500.050<0.0005mg/Kg2-Chlorotoluene 45.8*46-132 7.1 29
0.024 49.20.0220.0500.050<0.0004mg/Kg4-Chlorotoluene 45.6 44-135 7.5 23
0.023 46.4*0.0220.0500.050<0.0007mg/KgDi-Isopropyl Ether (DIPE)44.8*51-155 3.5 13
0.025 51.00.0300.0500.050<0.0004mg/Kg1,2-Dibromo-3-Chloropropane 60.6 27-132 17.2 25
0.026 53.40.0280.0500.050<0.0006mg/Kg1,2-Dibromoethane 57.0 49-132 6.5 15
0.025 51.4*0.0260.0500.050<0.0006mg/KgDibromomethane 53.6*59-133 4.1 15
0.024 48.80.0240.0500.050<0.0003mg/Kg1,2-Dichlorobenzene 48.6 42-130 0.4 21
0.023 47.00.0230.0500.050<0.0004mg/Kg1,3-Dichlorobenzene 46.2 41-129 1.7 24
0.022 45.60.0220.0500.050<0.0006mg/Kg1,4-Dichlorobenzene 45.8 44-134 0.4 21
0.016 33.00.0130.0500.050<0.001mg/KgDichlorodifluoromethane 26.4 25-151 22.2 37
0.026 53.6*0.0230.0500.050<0.0008mg/Kg1,1-Dichloroethane 47.2*59-137 12.6 21
0.024 48.6*0.0230.0500.050<0.001mg/Kg1,2-Dichloroethane 47.6*51-131 2.0 13
Page 28 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 158 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
V 93785-MS-V37418 V 93785-MSD-V37418Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.027 54.20.0230.0500.050<0.0007mg/Kg1,1-Dichloroethene 46.4*54-162 15.5 22
0.026 52.6*0.0230.0500.050<0.0008mg/Kgcis-1,2-Dichloroethene 47.2*58-140 10.8 28
0.027 54.6*0.0230.0500.050<0.001mg/Kgtrans-1,2-Dichloroethene 46.6*57-141 15.8 18
0.025 51.2*0.0240.0500.050<0.0004mg/Kg1,2-Dichloropropane 49.2*55-138 3.9 16
0.025 51.0*0.0260.0500.050<0.0006mg/Kg1,3-Dichloropropane 52.2*53-129 2.3 15
0.026 53.60.0220.0500.050<0.001mg/Kg2,2-Dichloropropane 44.8 30-147 17.8 20
0.028 56.40.0230.0500.050<0.0008mg/Kg1,1-Dichloropropene 47.8*55-137 16.5 19
0.025 51.40.0250.0500.050<0.0005mg/Kgcis-1,3-Dichloropropene 50.4 42-135 1.9 32
0.025 50.60.0260.0500.050<0.0008mg/Kgtrans-1,3-Dichloropropene 52.0 41-124 2.7 20
0.026 53.20.0230.0500.050<0.0006mg/KgEthylbenzene 46.6 44-144 13.2 19
0.048 48.7*0.0490.1000.100<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)49.4*70-130 1.4 20
0.021 43.60.0210.0500.050<0.0008mg/KgHexachlorobutadiene 43.4 30-126 0.4 26
0.028 56.0*0.0240.0500.050<0.0007mg/Kgn-Hexane 48.0*70-130 15.3 20
0.011 23.6*0.0170.0500.050<0.0006mg/Kg2-Hexanone 35.6 30-147 40.5 42
0.026 53.40.0230.0500.050<0.0005mg/KgIsopropylbenzene 47.0 41-140 12.7 27
0.024 49.80.0220.0500.050<0.001mg/Kg4-Isopropyl toluene 45.6 32-144 8.8 22
0.010 20.0*0.0120.0500.050<0.0007mg/KgMethyl Ethyl Ketone (MEK)25.8 24-160 25.3 42
0.025 50.20.0260.0500.050<0.0006mg/KgMethyl tert-butyl ether (MTBE)52.4 49-135 4.2 22
0.021 42.00.0280.0500.050<0.015mg/Kg4-Methyl-2-Pentanone 56.0 25-163 28.5 44
0.024 48.8*0.0220.0500.050<0.001mg/KgMethylene Chloride 45.8*53-144 6.3 14
0.026 52.60.0280.0500.050<0.0010mg/KgNaphthalene 56.6 32-127 7.3 44
0.025 50.60.0220.0500.050<0.0005mg/Kgn-Propylbenzene 44.6 35-144 12.6 27
0.026 53.20.0240.0500.050<0.001mg/KgStyrene 48.4 42-132 9.4 28
0.026 53.4*0.0250.0500.050<0.001mg/Kg1,1,1,2-Tetrachloroethane 50.6*60-120 5.3 15
0.025 50.40.0270.0500.050<0.0003mg/Kg1,1,2,2-Tetrachloroethane 55.2 39-135 9.0 22
0.028 56.80.0240.0500.050<0.0009mg/KgTetrachloroethene 49.2 47-142 14.3 26
Page 29 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 159 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
V 93785-MS-V37418 V 93785-MSD-V37418Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.027 55.0*0.0240.0500.050<0.0007mg/KgToluene 48.6*57-135 12.3 22
0.021 42.20.0220.0500.050<0.0005mg/Kg1,2,3-Trichlorobenzene 45.8 34-120 8.1 41
0.020 41.40.0210.0500.050<0.0006mg/Kg1,2,4-Trichlorobenzene 43.0 35-116 3.7 62
0.028 56.40.0240.0500.050<0.001mg/Kg1,1,1-Trichloroethane 48.6*52-139 14.8 21
0.024 49.40.0260.0500.050<0.0005mg/Kg1,1,2-Trichloroethane 53.0 44-140 7.0 21
0.028 56.20.0240.0500.050<0.0009mg/KgTrichloroethene 48.4 38-164 14.9 18
0.026 52.20.0210.0500.050<0.002mg/KgTrichlorofluoromethane 42.8 30-157 19.7 27
0.025 51.60.0290.0500.050<0.0007mg/Kg1,2,3-Trichloropropane 59.4 45-139 14.0 25
0.025 50.60.0230.0500.050<0.0005mg/Kg1,2,4-Trimethylbenzene 46.2 38-142 9.0 24
0.025 51.00.0230.0500.050<0.0005mg/Kg1,3,5-Trimethylbenzene 46.2 44-140 9.8 29
<0.0005 0.0*0.0030.0500.050<0.0005mg/KgVinyl Acetate 6.6*61-154 151*35
0.023 47.40.0170.0500.050<0.0005mg/KgVinyl Chloride 35.4*40-156 28.9 35
0.026 52.80.0240.0500.050<0.0005mg/Kgo-Xylene 48.0 43-143 9.5 17
0.052 52.70.0460.1000.100<0.001mg/Kgm,p-Xylene 46.9 36-148 11.6 20
1024-Bromofluorobenzene (S)101 70-130
105Dibromofluoromethane (S)106 84-123
102Toluene-d8 (S)100 76-129
Page 30 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 160 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37422QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37420
Associated Lab Samples: 93889, 93890, 93891
LRB-V37420 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 11:050.0200.002<0.002mg/KgAcetone
09/01/23 11:050.0200.001<0.001mg/KgAcrolein
09/01/23 11:050.0200.0008<0.0008mg/KgAcrylonitrile
09/01/23 11:050.0050.0006<0.0006mg/KgBenzene
09/01/23 11:050.0050.0005<0.0005mg/KgBromobenzene
09/01/23 11:050.0050.0008<0.0008mg/KgBromochloromethane
09/01/23 11:050.0050.001<0.001mg/KgBromodichloromethane
09/01/23 11:050.0050.001<0.001mg/KgBromoform
09/01/23 11:050.0100.001<0.001mg/KgBromomethane
09/01/23 11:050.0050.0005<0.0005mg/Kgn-Butylbenzene
09/01/23 11:050.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/01/23 11:050.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/01/23 11:050.0050.0006<0.0006mg/KgCarbon Disulfide
09/01/23 11:050.0050.001<0.001mg/KgCarbon Tetrachloride
09/01/23 11:050.0050.0007<0.0007mg/KgChlorobenzene
09/01/23 11:050.0050.0009<0.0009mg/KgChlorodibromomethane
09/01/23 11:050.0100.0009<0.0009mg/KgChloroethane
09/01/23 11:050.0050.001<0.001mg/KgChloroform
09/01/23 11:050.0100.0006<0.0006mg/KgChloromethane
09/01/23 11:050.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/01/23 11:050.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/01/23 11:050.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/01/23 11:050.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/01/23 11:050.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/01/23 11:050.0050.0006<0.0006mg/KgDibromomethane
09/01/23 11:050.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/01/23 11:050.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 31 of 61Date:09/15/2023 05:49 PM
Page 161 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37422QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37420
Associated Lab Samples: 93889, 93890, 93891
LRB-V37420 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 11:050.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/01/23 11:050.0100.001<0.001mg/KgDichlorodifluoromethane
09/01/23 11:050.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/01/23 11:050.0050.001<0.001mg/Kg1,2-Dichloroethane
09/01/23 11:050.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/01/23 11:050.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/01/23 11:050.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/01/23 11:050.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/01/23 11:050.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/01/23 11:050.0050.001<0.001mg/Kg2,2-Dichloropropane
09/01/23 11:050.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/01/23 11:050.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/01/23 11:050.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/01/23 11:050.0050.0006<0.0006mg/KgEthylbenzene
09/01/23 11:050.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/01/23 11:050.0100.0008<0.0008mg/KgHexachlorobutadiene
09/01/23 11:050.0100.0007<0.0007mg/Kgn-Hexane
09/01/23 11:050.0200.0006<0.0006mg/Kg2-Hexanone
09/01/23 11:050.0050.0005<0.0005mg/KgIsopropylbenzene
09/01/23 11:050.0050.001<0.001mg/Kg4-Isopropyl toluene
09/01/23 11:050.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/01/23 11:050.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/01/23 11:050.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/01/23 11:050.0100.001<0.001mg/KgMethylene Chloride
09/01/23 11:050.0100.0010<0.0010mg/KgNaphthalene
09/01/23 11:050.0050.0005<0.0005mg/Kgn-Propylbenzene
09/01/23 11:050.0050.001<0.001mg/KgStyrene
Page 32 of 61Date:09/15/2023 05:49 PM
Page 162 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37422QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37420
Associated Lab Samples: 93889, 93890, 93891
LRB-V37420 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 11:050.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/01/23 11:050.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/01/23 11:050.0050.0009<0.0009mg/KgTetrachloroethene
09/01/23 11:050.0050.0007<0.0007mg/KgToluene
09/01/23 11:050.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/01/23 11:050.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/01/23 11:050.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/01/23 11:050.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/01/23 11:050.0050.0009<0.0009mg/KgTrichloroethene
09/01/23 11:050.0100.002<0.002mg/KgTrichlorofluoromethane
09/01/23 11:050.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/01/23 11:050.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/01/23 11:050.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/01/23 11:050.0100.0005<0.0005mg/KgVinyl Acetate
09/01/23 11:050.0100.0005<0.0005mg/KgVinyl Chloride
09/01/23 11:050.0050.0005<0.0005mg/Kgo-Xylene
09/01/23 11:050.0100.001<0.001mg/Kgm,p-Xylene
09/01/23 11:054-Bromofluorobenzene (S)103 70-130
09/01/23 11:05Dibromofluoromethane (S)105 84-123
09/01/23 11:05Toluene-d8 (S)99.2 76-129
LCS-V37420 LCSD-V37420Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.396.50.0960.100mg/KgAcetone 29-198 0.8 20
0.118 1181060.1060.100mg/KgAcrolein 70-130 10.7 20
Page 33 of 61Date:09/15/2023 05:49 PM
Page 163 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37422QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37420
LCS-V37420 LCSD-V37420Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.117 1171120.1120.100mg/KgAcrylonitrile 65-134 4.3 20
0.045 91.696.40.0480.050mg/KgBenzene 74-127 5.1 20
0.048 96.499.00.0490.050mg/KgBromobenzene 73-125 2.6 20
0.052 1051040.0510.050mg/KgBromochloromethane 72-134 0.7 20
0.047 95.298.20.0490.050mg/KgBromodichloromethane 75-122 3.1 20
0.055 1101060.0520.050mg/KgBromoform 66-135 4.2 20
0.040 81.091.00.0450.050mg/KgBromomethane 20-180 11.6 20
0.046 93.41010.0500.050mg/Kgn-Butylbenzene 65-135 7.6 20
0.045 91.099.00.0490.050mg/Kgsec-Butyl benzene 66-131 8.4 20
0.046 92.099.60.0490.050mg/Kgtert-Butyl benzene 67-132 7.9 20
0.039 79.285.40.0420.050mg/KgCarbon Disulfide 61-129 7.5 20
0.044 89.496.00.0480.050mg/KgCarbon Tetrachloride 64-143 7.1 20
0.047 94.898.60.0490.050mg/KgChlorobenzene 74-118 3.9 20
0.050 1011020.0500.050mg/KgChlorodibromomethane 73-122 0.5 20
0.043 86.295.60.0470.050mg/KgChloroethane 33-149 10.3 20
0.046 92.294.60.0470.050mg/KgChloroform 73-127 2.5 20
0.040 81.483.60.0410.050mg/KgChloromethane 45-143 2.6 20
0.046 93.698.80.0490.050mg/Kg2-Chlorotoluene 67-124 5.4 20
0.046 93.698.80.0490.050mg/Kg4-Chlorotoluene 71-126 5.4 20
0.044 89.892.20.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.6 20
0.061 1231160.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 6.3 20
0.053 1071050.0520.050mg/Kg1,2-Dibromoethane 70-132 1.8 20
0.050 10099.80.0490.050mg/KgDibromomethane 74-133 0.5 20
0.051 1031060.0530.050mg/Kg1,2-Dichlorobenzene 72-123 2.6 20
0.049 98.21040.0520.050mg/Kg1,3-Dichlorobenzene 71-120 6.1 20
0.048 97.01000.0500.050mg/Kg1,4-Dichlorobenzene 71-123 3.2 20
Page 34 of 61Date:09/15/2023 05:49 PM
Page 164 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37422QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37420
LCS-V37420 LCSD-V37420Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 91.41010.0500.050mg/KgDichlorodifluoromethane 26-146 9.9 20
0.044 88.694.00.0470.050mg/Kg1,1-Dichloroethane 74-127 5.9 20
0.045 91.493.00.0460.050mg/Kg1,2-Dichloroethane 68-128 1.7 20
0.040 81.488.00.0440.050mg/Kg1,1-Dichloroethene 67-149 7.7 20
0.045 91.696.60.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 5.3 20
0.043 86.691.00.0450.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.9 20
0.047 94.096.80.0480.050mg/Kg1,2-Dichloropropane 73-130 2.9 20
0.050 1001020.0500.050mg/Kg1,3-Dichloropropane 75-124 1.7 20
0.043 87.892.20.0460.050mg/Kg2,2-Dichloropropane 50-142 4.8 20
0.043 87.293.60.0460.050mg/Kg1,1-Dichloropropene 71-130 7.0 20
0.050 1011030.0510.050mg/Kgcis-1,3-Dichloropropene 71-125 1.5 20
0.053 1071060.0530.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.1 20
0.044 88.694.60.0470.050mg/KgEthylbenzene 74-128 6.5 20
0.095 95.996.60.0960.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.7 20
0.048 96.01060.0520.050mg/KgHexachlorobutadiene 64-125 9.7 20
0.044 88.298.60.0490.050mg/Kgn-Hexane 70-130 11.1 20
0.048 96.693.40.0460.050mg/Kg2-Hexanone 61-157 3.3 20
0.046 92.698.80.0490.050mg/KgIsopropylbenzene 68-126 6.4 20
0.047 94.01010.0500.050mg/Kg4-Isopropyl toluene 68-129 7.3 20
0.042 84.880.40.0400.050mg/KgMethyl Ethyl Ketone (MEK)63-149 5.3 20
0.050 10099.60.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.8 20
0.052 1051000.0500.050mg/Kg4-Methyl-2-Pentanone 57-162 4.4 20
0.041 83.286.00.0430.050mg/KgMethylene Chloride 74-129 3.3 20
0.059 1181170.0580.050mg/KgNaphthalene 57-157 0.5 20
0.045 91.297.20.0480.050mg/Kgn-Propylbenzene 67-130 6.3 20
0.049 98.81030.0510.050mg/KgStyrene 77-121 3.7 20
Page 35 of 61Date:09/15/2023 05:49 PM
Page 165 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37422QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37420
LCS-V37420 LCSD-V37420Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 98.01010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 2.6 20
0.053 1071040.0520.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.8 20
0.046 92.298.60.0490.050mg/KgTetrachloroethene 68-130 6.7 20
0.046 92.496.00.0480.050mg/KgToluene 71-129 3.8 20
0.053 1081130.0560.050mg/Kg1,2,3-Trichlorobenzene 68-130 4.3 20
0.053 1081120.0560.050mg/Kg1,2,4-Trichlorobenzene 66-125 4.3 20
0.043 86.691.60.0450.050mg/Kg1,1,1-Trichloroethane 67-131 5.6 20
0.049 99.21000.0500.050mg/Kg1,1,2-Trichloroethane 70-133 1.2 20
0.046 92.296.60.0480.050mg/KgTrichloroethene 75-133 4.6 20
0.036 73.481.20.0400.050mg/KgTrichlorofluoromethane 44-146 10.0 20
0.057 1141100.0540.050mg/Kg1,2,3-Trichloropropane 60-137 4.2 20
0.048 96.01020.0510.050mg/Kg1,2,4-Trimethylbenzene 69-129 6.2 20
0.047 94.41000.0500.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.7 20
0.057 1161070.0530.050mg/KgVinyl Acetate 60-140 7.3 20
0.035 71.879.00.0390.050mg/KgVinyl Chloride 48-147 9.5 20
0.046 92.898.40.0490.050mg/Kgo-Xylene 74-126 5.8 20
0.090 90.896.70.0960.100mg/Kgm,p-Xylene 75-124 6.2 20
1021034-Bromofluorobenzene (S)70-130
104104Dibromofluoromethane (S)84-123
100102Toluene-d8 (S)76-129
Page 36 of 61Date:09/15/2023 05:49 PM
Page 166 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
Associated Lab Samples: 93883, 93885, 93886, 93888
LRB-V37441 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/23 17:150.6600.116<0.116mg/KgAcenaphthene
09/06/23 17:150.6600.105<0.105mg/KgAcenaphthylene
09/06/23 17:150.6600.152<0.152mg/KgAniline
09/06/23 17:150.6600.143<0.143mg/KgAnthracene
09/06/23 17:150.6600.139<0.139mg/KgBenzo(a)anthracene
09/06/23 17:150.6600.147<0.147mg/KgBenzo(a)pyrene
09/06/23 17:150.6600.146<0.146mg/KgBenzo(b)fluoranthene
09/06/23 17:150.6600.136<0.136mg/KgBenzo(g,h,i)perylene
09/06/23 17:150.6600.137<0.137mg/KgBenzo(k)fluoranthene
09/06/23 17:152.000.580<0.580mg/KgBenzoic Acid
09/06/23 17:150.6600.105<0.105mg/KgBenzyl alcohol
09/06/23 17:150.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
09/06/23 17:150.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
09/06/23 17:150.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
09/06/23 17:150.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
09/06/23 17:150.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
09/06/23 17:150.3300.113<0.113mg/KgButyl benzyl phthalate
09/06/23 17:150.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
09/06/23 17:150.3300.112<0.112mg/Kg4-Chloroaniline
09/06/23 17:150.6600.116<0.116mg/Kg2-Chloronaphthalene
09/06/23 17:150.6600.098<0.098mg/Kg2-Chlorophenol
09/06/23 17:151.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
09/06/23 17:150.6600.142<0.142mg/KgChrysene
09/06/23 17:150.6600.230<0.230mg/KgDibenz(a,h)anthracene
09/06/23 17:150.6600.119<0.119mg/KgDibenzofuran
09/06/23 17:150.6600.094<0.094mg/Kg1,2-Dichlorobenzene
09/06/23 17:150.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 37 of 61Date:09/15/2023 05:49 PM
Page 167 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
Associated Lab Samples: 93883, 93885, 93886, 93888
LRB-V37441 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/23 17:150.3300.097<0.097mg/Kg1,4-Dichlorobenzene
09/06/23 17:150.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
09/06/23 17:150.6600.095<0.095mg/Kg2,4-Dichlorophenol
09/06/23 17:150.6600.180<0.180mg/KgDiethyl phthalate
09/06/23 17:150.6600.174<0.174mg/KgDimethyl phthalate
09/06/23 17:150.3300.108<0.108mg/Kg2,4-Dimethylphenol
09/06/23 17:150.6600.107<0.107mg/KgDi-n-butyl phthalate
09/06/23 17:151.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
09/06/23 17:151.500.520<0.520mg/Kg2,4-Dinitrophenol
09/06/23 17:150.6600.096<0.096mg/Kg2,4-Dinitrotoluene
09/06/23 17:150.6600.108<0.108mg/Kg2,6-Dinitrotoluene
09/06/23 17:150.3300.143<0.143mg/KgDi-n-Octyl Phthalate
09/06/23 17:150.6600.123<0.123mg/KgFluoranthene
09/06/23 17:150.6600.128<0.128mg/KgFluorene
09/06/23 17:150.6600.106<0.106mg/KgHexachlorobenzene
09/06/23 17:150.6600.097<0.097mg/KgHexachlorobutadiene
09/06/23 17:150.6600.157<0.157mg/KgHexachlorocyclopentadiene
09/06/23 17:150.6600.079<0.079mg/KgHexachloroethane
09/06/23 17:150.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
09/06/23 17:150.6600.191<0.191mg/KgIsophorone
09/06/23 17:150.6600.106<0.106mg/Kg1-Methylnaphthalene
09/06/23 17:150.6600.100<0.100mg/Kg2-Methylnaphthalene
09/06/23 17:150.6600.097<0.097mg/Kg2-Methylphenol
09/06/23 17:150.6600.084<0.084mg/Kg3&4 Methylphenol
09/06/23 17:150.6600.144<0.144mg/KgNaphthalene
09/06/23 17:150.6600.096<0.096mg/Kg2-Nitroaniline
09/06/23 17:150.6600.120<0.120mg/Kg3-Nitroaniline
Page 38 of 61Date:09/15/2023 05:49 PM
Page 168 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
Associated Lab Samples: 93883, 93885, 93886, 93888
LRB-V37441 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/23 17:150.3300.093<0.093mg/Kg4-Nitroaniline
09/06/23 17:150.3300.116<0.116mg/KgNitrobenzene
09/06/23 17:150.6600.088<0.088mg/Kg2-Nitrophenol
09/06/23 17:150.6600.117<0.117mg/Kg4-Nitrophenol
09/06/23 17:150.6600.263<0.263mg/KgN-Nitrosodimethylamine
09/06/23 17:150.6600.181<0.181mg/KgN-Nitrosodiphenylamine
09/06/23 17:150.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
09/06/23 17:151.000.347<0.347mg/KgPentachlorophenol
09/06/23 17:150.6600.208<0.208mg/KgPhenanthrene
09/06/23 17:150.6600.112<0.112mg/KgPhenol
09/06/23 17:150.6600.134<0.134mg/KgPyrene
09/06/23 17:150.3300.079<0.079mg/KgPyridine
09/06/23 17:150.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
09/06/23 17:150.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
09/06/23 17:150.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
09/06/23 17:152-Fluorobiphenyl (S)77.8 44-115
09/06/23 17:152-Fluorophenol (S)65.7 35-115
09/06/23 17:15Nitrobenzene-d5 (S)74.8 37-122
09/06/23 17:154-Terphenyl-d14 (S)83.8 54-127
09/06/23 17:152,4,6-Tribromophenol (S)65.4 39-132
09/06/23 17:15Phenol-d5 (S)66.6 34-121
LCS-V37441Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
79.61.331.67mg/KgAcenaphthene 40-123
76.61.281.67mg/KgAcenaphthylene 32-132
Page 39 of 61Date:09/15/2023 05:49 PM
Page 169 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
LCS-V37441Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
210*3.501.67mg/KgAniline 12-197
86.21.441.67mg/KgAnthracene 47-123
84.41.411.67mg/KgBenzo(a)anthracene 49-126
94.61.581.67mg/KgBenzo(a)pyrene 45-129
89.81.501.67mg/KgBenzo(b)fluoranthene 45-132
82.01.371.67mg/KgBenzo(g,h,i)perylene 43-134
86.21.441.67mg/KgBenzo(k)fluoranthene 47-132
61.61.031.67mg/KgBenzoic Acid 10-83
83.81.401.67mg/KgBenzyl alcohol 29-122
74.21.241.67mg/KgBis(2-Chloroethoxy)methane 36-121
73.61.231.67mg/KgBis(2-Chloroethyl)ether 31-120
82.01.371.67mg/KgBis(2-Chloroisopropyl)ether 33-131
86.81.451.67mg/KgBis(2-ethylhexyl)phthalate 51-133
86.21.441.67mg/Kg4-Bromophenyl phenyl ether 46-124
91.61.531.67mg/KgButyl benzyl phthalate 48-132
77.81.301.67mg/Kg4-Chloro-3-methylphenol 45-122
93.41.561.67mg/Kg4-Chloroaniline 17-106
77.81.301.67mg/Kg2-Chloronaphthalene 41-114
79.61.331.67mg/Kg2-Chlorophenol 34-121
83.81.401.67mg/Kg4-Chlorophenyl phenyl ether 45-121
83.21.391.67mg/KgChrysene 50-124
66.41.111.67mg/KgDibenz(a,h)anthracene 45-134
78.41.311.67mg/KgDibenzofuran 44-120
73.61.231.67mg/Kg1,2-Dichlorobenzene 33-117
71.21.191.67mg/Kg1,3-Dichlorobenzene 30-115
70.61.181.67mg/Kg1,4-Dichlorobenzene 31-115
77.81.301.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 40 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 170 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
LCS-V37441Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
77.81.301.67mg/Kg2,4-Dichlorophenol 40-122
86.21.441.67mg/KgDiethyl phthalate 50-124
83.21.391.67mg/KgDimethyl phthalate 48-124
91.61.531.67mg/Kg2,4-Dimethylphenol 30-127
94.01.571.67mg/KgDi-n-butyl phthalate 51-128
85.01.421.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
88.61.481.67mg/Kg2,4-Dinitrophenol 27-129
86.21.441.67mg/Kg2,4-Dinitrotoluene 48-126
85.01.421.67mg/Kg2,6-Dinitrotoluene 46-124
93.41.561.67mg/KgDi-n-Octyl Phthalate 45-140
79.01.321.67mg/KgFluoranthene 50-127
81.41.361.67mg/KgFluorene 43-125
85.01.421.67mg/KgHexachlorobenzene 45-122
69.41.161.67mg/KgHexachlorobutadiene 32-123
67.01.121.67mg/KgHexachlorocyclopentadiene 32-117
70.61.181.67mg/KgHexachloroethane 28-117
83.81.401.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
67.01.121.67mg/KgIsophorone 30-122
68.21.141.67mg/Kg1-Methylnaphthalene 40-119
68.21.141.67mg/Kg2-Methylnaphthalene 38-122
82.01.371.67mg/Kg2-Methylphenol 32-122
75.41.261.67mg/Kg3&4 Methylphenol 34-119
66.41.111.67mg/KgNaphthalene 35-123
87.41.461.67mg/Kg2-Nitroaniline 44-127
87.41.461.67mg/Kg3-Nitroaniline 33-119
88.01.471.67mg/Kg4-Nitroaniline 63-147
67.61.131.67mg/KgNitrobenzene 34-122
Page 41 of 61Date:09/15/2023 05:49 PM
Page 171 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
LCS-V37441Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
72.41.211.67mg/Kg2-Nitrophenol 36-123
91.01.521.67mg/Kg4-Nitrophenol 30-132
61.61.031.67mg/KgN-Nitrosodimethylamine 10-146
1031.721.67mg/KgN-Nitrosodiphenylamine 38-127
80.81.351.67mg/KgN-Nitroso-di-n-propylamine 36-120
99.41.661.67mg/KgPentachlorophenol 25-133
83.21.391.67mg/KgPhenanthrene 50-121
77.21.291.67mg/KgPhenol 34-121
83.81.401.67mg/KgPyrene 47-127
53.30.8911.67mg/KgPyridine 10-80
67.01.121.67mg/Kg1,2,4-Trichlorobenzene 34-118
79.01.321.67mg/Kg2,4,5-Trichlorophenol 41-124
79.01.321.67mg/Kg2,4,6-Trichlorophenol 39-126
77.22-Fluorobiphenyl (S)44-115
70.22-Fluorophenol (S)35-115
70.6Nitrobenzene-d5 (S)37-122
85.64-Terphenyl-d14 (S)54-127
72.02,4,6-Tribromophenol (S)39-132
69.9Phenol-d5 (S)34-121
V 93785-MS-V37441 V 93785-MSD-V37441Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.18 70.61.211.661.67<0.116mg/KgAcenaphthene 72.8 40-123 2.5 20
1.16 69.41.191.661.67<0.105mg/KgAcenaphthylene 71.6 32-132 2.5 20
2.86 1712.861.661.67<0.152mg/KgAniline 172 12-197 0.0 20
Page 42 of 61Date:09/15/2023 05:49 PM
Page 172 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
V 93785-MS-V37441 V 93785-MSD-V37441Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.30 77.81.291.661.67<0.143mg/KgAnthracene 77.7 47-123 0.7 20
1.25 74.81.251.661.67<0.139mg/KgBenzo(a)anthracene 75.3 49-126 0.0 20
1.43 85.61.401.661.67<0.147mg/KgBenzo(a)pyrene 84.3 45-129 2.1 20
1.30 77.81.281.661.67<0.146mg/KgBenzo(b)fluoranthene 77.1 45-132 1.5 20
1.26 75.41.241.661.67<0.136mg/KgBenzo(g,h,i)perylene 74.6 43-134 1.6 20
1.32 79.01.301.661.67<0.137mg/KgBenzo(k)fluoranthene 78.3 47-132 1.5 20
1.12 67.01.041.661.67<0.580mg/KgBenzoic Acid 62.6 10-83 7.4 20
1.23 73.61.191.661.67<0.105mg/KgBenzyl alcohol 71.6 29-122 3.3 20
1.10 65.81.101.661.67<0.118mg/KgBis(2-Chloroethoxy)methane 66.2 36-121 0.0 20
1.04 62.21.061.661.67<0.107mg/KgBis(2-Chloroethyl)ether 63.8 31-120 1.9 20
1.18 70.61.201.661.67<0.136mg/KgBis(2-Chloroisopropyl)ether 72.2 33-131 1.6 20
1.31 78.41.301.661.67<0.120mg/KgBis(2-ethylhexyl)phthalate 78.3 51-133 0.7 20
1.29 77.21.251.661.67<0.109mg/Kg4-Bromophenyl phenyl ether 75.3 46-124 3.1 20
1.39 83.21.371.661.67<0.113mg/KgButyl benzyl phthalate 82.5 48-132 1.4 20
1.16 69.41.161.661.67<0.092mg/Kg4-Chloro-3-methylphenol 69.8 45-122 0.0 20
1.32 79.01.331.661.67<0.112mg/Kg4-Chloroaniline 80.1 17-106 0.7 20
1.17 70.01.191.661.67<0.116mg/Kg2-Chloronaphthalene 71.6 41-114 1.6 20
1.16 69.41.171.661.67<0.098mg/Kg2-Chlorophenol 70.4 34-121 0.8 20
1.27 76.01.271.661.67<0.126mg/Kg4-Chlorophenyl phenyl ether 76.5 45-121 0.0 20
1.27 76.01.251.661.67<0.142mg/KgChrysene 75.3 50-124 1.5 20
1.02 61.01.011.661.67<0.230mg/KgDibenz(a,h)anthracene 60.8 45-134 0.9 20
1.19 71.21.201.661.67<0.119mg/KgDibenzofuran 72.2 44-120 0.8 20
1.07 64.01.051.661.67<0.094mg/Kg1,2-Dichlorobenzene 63.2 33-117 1.8 20
1.01 60.41.001.661.67<0.097mg/Kg1,3-Dichlorobenzene 60.2 30-115 0.9 20
0.998 59.71.001.661.67<0.097mg/Kg1,4-Dichlorobenzene 60.2 31-115 0.2 20
1.15 68.81.141.661.67<0.147mg/Kg3,3'-Dichlorobenzidine 68.6 22-121 0.8 20
Page 43 of 61Date:09/15/2023 05:49 PM
Page 173 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
V 93785-MS-V37441 V 93785-MSD-V37441Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.12 67.01.161.661.67<0.095mg/Kg2,4-Dichlorophenol 69.8 40-122 3.5 20
1.29 77.21.261.661.67<0.180mg/KgDiethyl phthalate 75.9 50-124 2.3 20
1.25 74.81.261.661.67<0.174mg/KgDimethyl phthalate 75.9 48-124 0.7 30
1.49 89.21.481.661.67<0.108mg/Kg2,4-Dimethylphenol 89.1 30-127 0.6 20
1.42 85.01.381.661.67<0.107mg/KgDi-n-butyl phthalate 83.1 51-128 2.8 20
1.29 77.21.191.661.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 71.6 29-132 8.0 20
1.29 77.21.241.661.67<0.520mg/Kg2,4-Dinitrophenol 74.6 27-129 3.9 20
1.28 76.61.261.661.67<0.096mg/Kg2,4-Dinitrotoluene 75.9 48-126 1.5 20
1.26 75.41.261.661.67<0.108mg/Kg2,6-Dinitrotoluene 75.9 46-124 0.0 20
1.41 84.41.371.661.67<0.143mg/KgDi-n-Octyl Phthalate 82.5 45-140 2.8 20
1.21 72.41.171.661.67<0.123mg/KgFluoranthene 70.4 50-127 3.3 20
1.23 73.61.241.661.67<0.128mg/KgFluorene 74.6 43-125 0.8 20
1.24 74.21.231.661.67<0.106mg/KgHexachlorobenzene 74.0 45-122 0.8 20
1.00 59.81.041.661.67<0.097mg/KgHexachlorobutadiene 62.6 32-123 3.9 20
1.05 62.81.051.661.67<0.157mg/KgHexachlorocyclopentadiene 63.2 32-117 0.0 20
1.00 59.81.021.661.67<0.079mg/KgHexachloroethane 61.4 28-117 1.9 20
1.27 76.01.241.661.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 74.6 45-133 2.3 20
0.961 57.50.9761.661.67<0.191mg/KgIsophorone 58.7 30-122 1.5 20
1.04 62.21.061.661.67<0.106mg/Kg1-Methylnaphthalene 63.8 40-119 1.9 20
1.00 59.81.041.661.67<0.100mg/Kg2-Methylnaphthalene 62.6 38-122 3.9 20
1.16 69.41.201.661.67<0.097mg/Kg2-Methylphenol 72.2 32-122 3.3 20
1.06 63.41.081.661.67<0.084mg/Kg3&4 Methylphenol 65.0 34-119 1.8 20
0.974 58.30.9871.661.67<0.144mg/KgNaphthalene 59.4 35-123 1.3 20
1.33 79.61.311.661.67<0.096mg/Kg2-Nitroaniline 78.9 44-127 1.5 20
1.28 76.61.301.661.67<0.120mg/Kg3-Nitroaniline 78.3 33-119 1.5 20
1.29 77.21.311.661.67<0.093mg/Kg4-Nitroaniline 78.9 63-147 1.5 20
Page 44 of 61Date:09/15/2023 05:49 PM
Page 174 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
V 93785-MS-V37441 V 93785-MSD-V37441Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.983 58.80.9801.661.67<0.116mg/KgNitrobenzene 59.0 34-122 0.3 20
1.05 62.81.041.661.67<0.088mg/Kg2-Nitrophenol 62.6 32-123 0.9 20
1.39 83.21.351.661.67<0.117mg/Kg4-Nitrophenol 81.3 30-132 2.9 20
0.918 54.90.9111.661.67<0.263mg/KgN-Nitrosodimethylamine 54.8 10-146 0.7 30
1.53 91.61.511.661.67<0.181mg/KgN-Nitrosodiphenylamine 90.9 38-127 1.3 20
1.14 68.21.181.661.67<0.118mg/KgN-Nitroso-di-n-propylamine 71.0 36-120 3.4 20
1.60 95.81.571.661.67<0.347mg/KgPentachlorophenol 94.5 25-133 1.8 20
1.27 76.01.221.661.67<0.208mg/KgPhenanthrene 73.4 50-121 4.0 20
1.12 67.01.131.661.67<0.112mg/KgPhenol 68.0 34-121 0.8 20
1.30 77.81.301.661.67<0.134mg/KgPyrene 78.3 47-127 0.0 20
0.801 47.90.7941.661.67<0.079mg/KgPyridine 47.8 10-80 0.8 20
0.994 59.50.9911.661.67<0.107mg/Kg1,2,4-Trichlorobenzene 59.6 34-118 0.3 20
1.23 73.61.211.661.67<0.096mg/Kg2,4,5-Trichlorophenol 72.8 41-124 1.6 20
1.23 73.61.201.661.67<0.096mg/Kg2,4,6-Trichlorophenol 72.2 39-126 2.4 20
68.82-Fluorobiphenyl (S)68.0 44-115
61.52-Fluorophenol (S)60.9 35-115
59.8Nitrobenzene-d5 (S)57.2 37-122
77.24-Terphenyl-d14 (S)74.6 54-127
64.82,4,6-Tribromophenol (S)62.1 39-132
60.6Phenol-d5 (S)58.2 34-121
Page 45 of 61Date:09/15/2023 05:49 PM
Page 175 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37578QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37540
Associated Lab Samples: 93889, 93891
LRB-V37540 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/08/23 15:130.6600.116<0.116mg/KgAcenaphthene
09/08/23 15:130.6600.105<0.105mg/KgAcenaphthylene
09/08/23 15:130.6600.152<0.152mg/KgAniline
09/08/23 15:130.6600.143<0.143mg/KgAnthracene
09/08/23 15:130.6600.139<0.139mg/KgBenzo(a)anthracene
09/08/23 15:130.6600.147<0.147mg/KgBenzo(a)pyrene
09/08/23 15:130.6600.146<0.146mg/KgBenzo(b)fluoranthene
09/08/23 15:130.6600.136<0.136mg/KgBenzo(g,h,i)perylene
09/08/23 15:130.6600.137<0.137mg/KgBenzo(k)fluoranthene
09/08/23 15:132.000.580<0.580mg/KgBenzoic Acid
09/08/23 15:130.6600.105<0.105mg/KgBenzyl alcohol
09/08/23 15:130.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
09/08/23 15:130.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
09/08/23 15:130.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
09/08/23 15:130.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
09/08/23 15:130.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
09/08/23 15:130.3300.113<0.113mg/KgButyl benzyl phthalate
09/08/23 15:130.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
09/08/23 15:130.3300.112<0.112mg/Kg4-Chloroaniline
09/08/23 15:130.6600.116<0.116mg/Kg2-Chloronaphthalene
09/08/23 15:130.6600.098<0.098mg/Kg2-Chlorophenol
09/08/23 15:131.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
09/08/23 15:130.6600.142<0.142mg/KgChrysene
09/08/23 15:130.6600.230<0.230mg/KgDibenz(a,h)anthracene
09/08/23 15:130.6600.119<0.119mg/KgDibenzofuran
09/08/23 15:130.6600.094<0.094mg/Kg1,2-Dichlorobenzene
09/08/23 15:130.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 46 of 61Date:09/15/2023 05:49 PM
Page 176 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37578QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37540
Associated Lab Samples: 93889, 93891
LRB-V37540 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/08/23 15:130.3300.097<0.097mg/Kg1,4-Dichlorobenzene
09/08/23 15:130.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
09/08/23 15:130.6600.095<0.095mg/Kg2,4-Dichlorophenol
09/08/23 15:130.6600.180<0.180mg/KgDiethyl phthalate
09/08/23 15:130.6600.174<0.174mg/KgDimethyl phthalate
09/08/23 15:130.3300.108<0.108mg/Kg2,4-Dimethylphenol
09/08/23 15:130.6600.107<0.107mg/KgDi-n-butyl phthalate
09/08/23 15:131.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
09/08/23 15:131.500.520<0.520mg/Kg2,4-Dinitrophenol
09/08/23 15:130.6600.096<0.096mg/Kg2,4-Dinitrotoluene
09/08/23 15:130.6600.108<0.108mg/Kg2,6-Dinitrotoluene
09/08/23 15:130.3300.143<0.143mg/KgDi-n-Octyl Phthalate
09/08/23 15:130.6600.123<0.123mg/KgFluoranthene
09/08/23 15:130.6600.128<0.128mg/KgFluorene
09/08/23 15:130.6600.106<0.106mg/KgHexachlorobenzene
09/08/23 15:130.6600.097<0.097mg/KgHexachlorobutadiene
09/08/23 15:130.6600.157<0.157mg/KgHexachlorocyclopentadiene
09/08/23 15:130.6600.079<0.079mg/KgHexachloroethane
09/08/23 15:130.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
09/08/23 15:130.6600.191<0.191mg/KgIsophorone
09/08/23 15:130.6600.106<0.106mg/Kg1-Methylnaphthalene
09/08/23 15:130.6600.100<0.100mg/Kg2-Methylnaphthalene
09/08/23 15:130.6600.097<0.097mg/Kg2-Methylphenol
09/08/23 15:130.6600.084<0.084mg/Kg3&4 Methylphenol
09/08/23 15:130.6600.144<0.144mg/KgNaphthalene
09/08/23 15:130.6600.096<0.096mg/Kg2-Nitroaniline
09/08/23 15:130.6600.120<0.120mg/Kg3-Nitroaniline
Page 47 of 61Date:09/15/2023 05:49 PM
Page 177 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37578QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37540
Associated Lab Samples: 93889, 93891
LRB-V37540 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/08/23 15:130.3300.093<0.093mg/Kg4-Nitroaniline
09/08/23 15:130.3300.116<0.116mg/KgNitrobenzene
09/08/23 15:130.6600.088<0.088mg/Kg2-Nitrophenol
09/08/23 15:130.6600.117<0.117mg/Kg4-Nitrophenol
09/08/23 15:130.6600.263<0.263mg/KgN-Nitrosodimethylamine
09/08/23 15:130.6600.181<0.181mg/KgN-Nitrosodiphenylamine
09/08/23 15:130.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
09/08/23 15:131.000.347<0.347mg/KgPentachlorophenol
09/08/23 15:130.6600.208<0.208mg/KgPhenanthrene
09/08/23 15:130.6600.112<0.112mg/KgPhenol
09/08/23 15:130.6600.134<0.134mg/KgPyrene
09/08/23 15:130.3300.079<0.079mg/KgPyridine
09/08/23 15:130.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
09/08/23 15:130.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
09/08/23 15:130.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
09/08/23 15:132-Fluorobiphenyl (S)92.8 44-115
09/08/23 15:132-Fluorophenol (S)84.6 35-115
09/08/23 15:13Nitrobenzene-d5 (S)101 37-122
09/08/23 15:134-Terphenyl-d14 (S)105 54-127
09/08/23 15:132,4,6-Tribromophenol (S)90.0 39-132
09/08/23 15:13Phenol-d5 (S)80.4 34-121
LCS-V37540Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
95.21.591.67mg/KgAcenaphthene 40-123
98.21.641.67mg/KgAcenaphthylene 32-132
Page 48 of 61Date:09/15/2023 05:49 PM
Page 178 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37578QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37540
LCS-V37540Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
230*3.841.67mg/KgAniline 12-197
1081.811.67mg/KgAnthracene 47-123
1041.741.67mg/KgBenzo(a)anthracene 49-126
1141.911.67mg/KgBenzo(a)pyrene 45-129
1071.781.67mg/KgBenzo(b)fluoranthene 45-132
1001.671.67mg/KgBenzo(g,h,i)perylene 43-134
1101.831.67mg/KgBenzo(k)fluoranthene 47-132
62.81.051.67mg/KgBenzoic Acid 10-83
94.61.581.67mg/KgBenzyl alcohol 29-122
92.81.551.67mg/KgBis(2-Chloroethoxy)methane 36-121
80.81.351.67mg/KgBis(2-Chloroethyl)ether 31-120
89.21.491.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1141.911.67mg/KgBis(2-ethylhexyl)phthalate 51-133
1051.751.67mg/Kg4-Bromophenyl phenyl ether 46-124
1131.891.67mg/KgButyl benzyl phthalate 48-132
1041.731.67mg/Kg4-Chloro-3-methylphenol 45-122
116*1.941.67mg/Kg4-Chloroaniline 17-106
94.01.571.67mg/Kg2-Chloronaphthalene 41-114
89.21.491.67mg/Kg2-Chlorophenol 34-121
1011.691.67mg/Kg4-Chlorophenyl phenyl ether 45-121
1041.731.67mg/KgChrysene 50-124
82.61.381.67mg/KgDibenz(a,h)anthracene 45-134
97.61.631.67mg/KgDibenzofuran 44-120
83.21.391.67mg/Kg1,2-Dichlorobenzene 33-117
78.41.311.67mg/Kg1,3-Dichlorobenzene 30-115
79.01.321.67mg/Kg1,4-Dichlorobenzene 31-115
98.81.651.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 49 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 179 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37578QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37540
LCS-V37540Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1021.701.67mg/Kg2,4-Dichlorophenol 40-122
1041.741.67mg/KgDiethyl phthalate 50-124
1051.761.67mg/KgDimethyl phthalate 48-124
1171.951.67mg/Kg2,4-Dimethylphenol 30-127
1171.951.67mg/KgDi-n-butyl phthalate 51-128
1041.731.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
79.61.331.67mg/Kg2,4-Dinitrophenol 27-129
1111.851.67mg/Kg2,4-Dinitrotoluene 48-126
1161.941.67mg/Kg2,6-Dinitrotoluene 46-124
1171.961.67mg/KgDi-n-Octyl Phthalate 45-140
98.21.641.67mg/KgFluoranthene 50-127
98.81.651.67mg/KgFluorene 43-125
1031.721.67mg/KgHexachlorobenzene 45-122
89.21.491.67mg/KgHexachlorobutadiene 32-123
74.81.251.67mg/KgHexachlorocyclopentadiene 32-117
80.21.341.67mg/KgHexachloroethane 28-117
1001.671.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
82.61.381.67mg/KgIsophorone 30-122
86.81.451.67mg/Kg1-Methylnaphthalene 40-119
89.21.491.67mg/Kg2-Methylnaphthalene 38-122
89.21.491.67mg/Kg2-Methylphenol 32-122
87.41.461.67mg/Kg3&4 Methylphenol 34-119
86.21.441.67mg/KgNaphthalene 35-123
1222.041.67mg/Kg2-Nitroaniline 44-127
122*2.041.67mg/Kg3-Nitroaniline 33-119
1202.001.67mg/Kg4-Nitroaniline 63-147
94.61.581.67mg/KgNitrobenzene 34-122
Page 50 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 180 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37578QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37540
LCS-V37540Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1101.831.67mg/Kg2-Nitrophenol 36-123
98.81.651.67mg/Kg4-Nitrophenol 30-132
74.21.241.67mg/KgN-Nitrosodimethylamine 10-146
1272.121.67mg/KgN-Nitrosodiphenylamine 38-127
87.41.461.67mg/KgN-Nitroso-di-n-propylamine 36-120
1282.141.67mg/KgPentachlorophenol 25-133
1021.701.67mg/KgPhenanthrene 50-121
83.81.401.67mg/KgPhenol 34-121
1021.711.67mg/KgPyrene 47-127
61.61.031.67mg/KgPyridine 10-80
83.81.401.67mg/Kg1,2,4-Trichlorobenzene 34-118
1061.771.67mg/Kg2,4,5-Trichlorophenol 41-124
1021.711.67mg/Kg2,4,6-Trichlorophenol 39-126
93.42-Fluorobiphenyl (S)44-115
79.22-Fluorophenol (S)35-115
94.0Nitrobenzene-d5 (S)37-122
1054-Terphenyl-d14 (S)54-127
1032,4,6-Tribromophenol (S)39-132
73.5Phenol-d5 (S)34-121
V 93889-MS-V37540 V 93889-MSD-V37540Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.62 97.01.611.671.67<0.116mg/KgAcenaphthene 96.4 40-123 0.6 20
1.65 98.81.651.671.67<0.105mg/KgAcenaphthylene 98.8 32-132 0.0 20
3.81 228*3.941.671.67<0.152mg/KgAniline 236*12-197 3.3 20
Page 51 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 181 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37578QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37540
V 93889-MS-V37540 V 93889-MSD-V37540Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.83 1101.811.671.67<0.143mg/KgAnthracene 108 47-123 1.0 20
1.81 1081.811.671.67<0.139mg/KgBenzo(a)anthracene 108 49-126 0.0 20
1.99 1192.011.671.67<0.147mg/KgBenzo(a)pyrene 120 45-129 1.0 20
1.89 1131.881.671.67<0.146mg/KgBenzo(b)fluoranthene 113 45-132 0.5 20
1.76 1051.761.671.67<0.136mg/KgBenzo(g,h,i)perylene 105 43-134 0.0 20
1.73 1041.721.671.67<0.137mg/KgBenzo(k)fluoranthene 103 47-132 0.5 20
1.85 111*1.891.671.67<0.580mg/KgBenzoic Acid 113*10-83 2.1 20
1.65 98.81.731.671.67<0.105mg/KgBenzyl alcohol 104 29-122 4.7 20
1.60 95.81.641.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 98.2 36-121 2.4 20
1.37 82.01.431.671.67<0.107mg/KgBis(2-Chloroethyl)ether 85.6 31-120 4.2 20
1.52 91.01.591.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 95.2 33-131 4.5 20
1.95 1171.941.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 116 51-133 0.5 20
1.81 1081.801.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 108 46-124 0.5 20
1.93 1161.901.671.67<0.113mg/KgButyl benzyl phthalate 114 48-132 1.5 20
1.75 1051.761.671.67<0.092mg/Kg4-Chloro-3-methylphenol 105 45-122 0.5 20
1.91 114*1.911.671.67<0.112mg/Kg4-Chloroaniline 114*17-106 0.0 20
1.60 95.81.631.671.67<0.116mg/Kg2-Chloronaphthalene 97.6 41-114 1.8 20
1.54 92.21.601.671.67<0.098mg/Kg2-Chlorophenol 95.8 34-121 3.8 20
1.75 1051.741.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 104 45-121 0.5 20
1.74 1041.721.671.67<0.142mg/KgChrysene 103 50-124 1.1 20
1.59 95.21.551.671.67<0.230mg/KgDibenz(a,h)anthracene 92.8 45-134 2.5 20
1.64 98.21.661.671.67<0.119mg/KgDibenzofuran 99.4 44-120 1.2 20
1.39 83.21.441.671.67<0.094mg/Kg1,2-Dichlorobenzene 86.2 33-117 3.5 20
1.31 78.41.401.671.67<0.097mg/Kg1,3-Dichlorobenzene 83.8 30-115 6.6 20
1.34 80.21.411.671.67<0.097mg/Kg1,4-Dichlorobenzene 84.4 31-115 5.0 20
1.67 1001.711.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 102 22-121 2.3 20
Page 52 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 182 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37578QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37540
V 93889-MS-V37540 V 93889-MSD-V37540Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.69 1011.711.671.67<0.095mg/Kg2,4-Dichlorophenol 102 40-122 1.1 20
1.77 1061.781.671.67<0.180mg/KgDiethyl phthalate 107 50-124 0.5 20
1.76 1051.761.671.67<0.174mg/KgDimethyl phthalate 105 48-124 0.0 30
2.23 134*2.251.671.67<0.108mg/Kg2,4-Dimethylphenol 135*30-127 0.8 20
1.97 1181.941.671.67<0.107mg/KgDi-n-butyl phthalate 116 51-128 1.5 20
1.75 1051.741.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 104 29-132 0.5 20
1.83 1101.861.671.67<0.520mg/Kg2,4-Dinitrophenol 111 27-129 1.6 20
1.84 1101.931.671.67<0.096mg/Kg2,4-Dinitrotoluene 116 48-126 4.7 20
1.94 1161.981.671.67<0.108mg/Kg2,6-Dinitrotoluene 119 46-124 2.0 20
2.02 1212.031.671.67<0.143mg/KgDi-n-Octyl Phthalate 122 45-140 0.4 20
1.65 98.81.611.671.67<0.123mg/KgFluoranthene 96.4 50-127 2.4 20
1.69 1011.721.671.67<0.128mg/KgFluorene 103 43-125 1.7 20
1.85 1111.811.671.67<0.106mg/KgHexachlorobenzene 108 45-122 2.1 20
1.58 94.61.591.671.67<0.097mg/KgHexachlorobutadiene 95.2 32-123 0.6 20
1.04 62.21.001.671.67<0.157mg/KgHexachlorocyclopentadiene 59.8 32-117 3.9 20
1.32 79.01.411.671.67<0.079mg/KgHexachloroethane 84.4 28-117 6.5 20
1.79 1071.831.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 110 45-133 2.2 20
1.41 84.41.421.671.67<0.191mg/KgIsophorone 85.0 30-122 0.7 20
1.47 88.01.491.671.67<0.106mg/Kg1-Methylnaphthalene 89.2 40-119 1.3 20
1.49 89.21.561.671.67<0.100mg/Kg2-Methylnaphthalene 93.4 38-122 4.5 20
1.50 89.81.531.671.67<0.097mg/Kg2-Methylphenol 91.6 32-122 1.9 20
1.46 87.41.441.671.67<0.085mg/Kg3&4 Methylphenol 86.2 34-119 1.3 20
1.47 88.01.501.671.67<0.144mg/KgNaphthalene 89.8 35-123 2.0 20
2.14 128*2.171.671.67<0.096mg/Kg2-Nitroaniline 130*44-127 1.3 20
2.14 128*2.171.671.67<0.120mg/Kg3-Nitroaniline 130*33-119 1.3 20
1.93 1161.951.671.67<0.093mg/Kg4-Nitroaniline 117 63-147 1.0 20
Page 53 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 183 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37578QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37540
V 93889-MS-V37540 V 93889-MSD-V37540Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.59 95.21.661.671.67<0.116mg/KgNitrobenzene 99.4 34-122 4.3 20
1.85 1111.911.671.67<0.088mg/Kg2-Nitrophenol 114 32-123 3.1 20
1.81 1081.811.671.67<0.117mg/Kg4-Nitrophenol 108 30-132 0.0 20
1.20 71.81.281.671.67<0.263mg/KgN-Nitrosodimethylamine 76.6 10-146 6.4 30
2.15 129*2.141.671.67<0.181mg/KgN-Nitrosodiphenylamine 128*38-127 0.4 20
1.47 88.01.541.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 92.2 36-120 4.6 20
2.66 159*2.571.671.67<0.347mg/KgPentachlorophenol 154*25-133 3.4 20
1.72 1031.681.671.67<0.208mg/KgPhenanthrene 101 50-121 2.3 20
1.41 84.41.421.671.67<0.112mg/KgPhenol 85.0 34-121 0.7 20
1.73 1041.761.671.67<0.134mg/KgPyrene 105 47-127 1.7 20
1.02 61.01.111.671.67<0.079mg/KgPyridine 66.4 10-80 8.4 20
1.47 88.01.541.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 92.2 34-118 4.6 20
1.84 1101.881.671.67<0.096mg/Kg2,4,5-Trichlorophenol 113 41-124 2.1 20
1.81 1081.831.671.67<0.096mg/Kg2,4,6-Trichlorophenol 110 39-126 1.0 20
92.82-Fluorobiphenyl (S)94.0 44-115
81.42-Fluorophenol (S)83.4 35-115
97.6Nitrobenzene-d5 (S)101 37-122
1084-Terphenyl-d14 (S)107 54-127
1112,4,6-Tribromophenol (S)109 39-132
75.7Phenol-d5 (S)75.0 34-121
Page 54 of 61* QC Fail Date:09/15/2023 05:49 PM
Page 184 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
EDB and DBCP by Microextraction GC/ECD
EPA-504.1
V37661QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-504.1(PREP)
QC Prep:V37608
Associated Lab Samples: 93892, 93893, 93894, 93896
LRB-V37608 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/08/23 13:360.02000.00330<0.00330µg/L1,2-Dibromoethane
LCS-V37608 LCSD-V37608Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.313 1251280.3190.250µg/L1,2-Dibromoethane 70-130 1.8 20.0
V 93893-DUP-V37608Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/08/23 15:040.4<0.0209< 0.0209µg/L1,2-Dibromoethane
V 93892-MS-V37608Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
0.495 1280.2610.161µg/L1,2-Dibromoethane 70-130
Page 55 of 61Date:09/15/2023 05:49 PM
Page 185 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V37620QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V37493
Associated Lab Samples: 93883, 93885, 93886, 93888, 93889, 93891
LRB-V37493 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/13/23 10:4650.09.20<9.20mg/KgAliphatic C9-C18
09/13/23 10:4650.012.2<12.2mg/KgAliphatic C19-C36
09/13/23 10:4650.014.2<14.2mg/KgAromatic C11-C22
09/13/23 10:462-Fluorobiphenyl (S)67.7 40-140
09/13/23 10:462-Bromonaphthalene (S)62.0 40-140
09/13/23 10:46Chlorooctadecane (S)66.6 40-140
09/13/23 10:46OTP Surrogate (S)64.2 40-140
LCS-V37493 LCSD-V37493Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
42.5 70.854.332.660.0mg/KgAliphatic C9-C18 40-140 26.3 50
75.6 94.583.366.780.0mg/KgAliphatic C19-C36 40-140 12.5 50
147 86.468.8117170mg/KgAromatic C11-C22 40-140 22.7 50
76.071.22-Fluorobiphenyl (S)40-140
71.766.52-Bromonaphthalene (S)40-140
66.663.2Chlorooctadecane (S)40-140
69.362.5OTP Surrogate (S)40-140
Page 56 of 61Date:09/15/2023 05:49 PM
Page 186 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V37698QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V37556
Associated Lab Samples: 93892, 93893
LRB-V37556 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/13/23 10:4835028.2<28.2µg/LAliphatic C9-C18
09/13/23 10:48500124<124µg/LAliphatic C19-C36
09/13/23 10:4825061.2<61.2µg/LAromatic C11-C22
09/13/23 10:482-Fluorobiphenyl (S)73.0 40-140
09/13/23 10:482-Bromonaphthalene (S)67.2 40-140
09/13/23 10:48Chlorooctadecane (S)65.2 40-140
09/13/23 10:48OTP Surrogate (S)65.0 40-140
LCS-V37556 LCSD-V37556Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
416 69.382.8497600µg/LAliphatic C9-C18 40-140 17.7 50.0
822 103115918800µg/LAliphatic C19-C36 40-140 11.0 50.0
1630 95.810718201700µg/LAromatic C11-C22 40-140 11.0 50.0
80.780.02-Fluorobiphenyl (S)40-140
76.575.22-Bromonaphthalene (S)40-140
60.371.7Chlorooctadecane (S)40-140
69.074.5OTP Surrogate (S)40-140
Page 57 of 61Date:09/15/2023 05:49 PM
Page 187 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V37397QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V37396
Associated Lab Samples: 93883, 93884, 93885, 93886, 93887, 93888, 93889, 93890, 93891
LRB-V37396 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 23:068.001.22<1.22mg/KgAliphatic C5-C8
09/01/23 23:068.004.56<4.56mg/KgAliphatic C9-C12
09/01/23 23:068.000.624<0.624mg/KgAromatic C9-C10
09/01/23 23:062,5-Dibromotoluene (FID) (S)84.9 70-130
09/01/23 23:062,5-Dibromotoluene (PID) (S)83.7 70-130
LCS-V37396 LCSD-V37396Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
34.7 10810834.632.0mg/KgAliphatic C5-C8 70-130 0.2 50
36.8 11511336.332.0mg/KgAliphatic C9-C12 70-130 1.3 50
12.9 12111912.710.7mg/KgAromatic C9-C10 70-130 1.5 50
74.878.52,5-Dibromotoluene (FID) (S)70-130
77.691.42,5-Dibromotoluene (PID) (S)70-130
Page 58 of 61Date:09/15/2023 05:49 PM
Page 188 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V37399QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V37398
Associated Lab Samples: 93892, 93893, 93894, 93896
LRB-V37398 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 14:5150.011.5<11.5µg/LAliphatic C5-C8
09/01/23 14:5150.025.8<25.8µg/LAliphatic C9-C12
09/01/23 14:5150.04.02<4.02µg/LAromatic C9-C10
09/01/23 14:512,5-Dibromotoluene (FID) (S)105 70-130
09/01/23 14:512,5-Dibromotoluene (PID) (S)103 70-130
LCS-V37398 LCSD-V37398Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
317 106103310300µg/LAliphatic C5-C8 70-130 2.2 50.0
347 116113339300µg/LAliphatic C9-C12 70-130 2.3 50.0
110 110111111100µg/LAromatic C9-C10 70-130 0.9 50.0
80.585.52,5-Dibromotoluene (FID) (S)70-130
92.988.22,5-Dibromotoluene (PID) (S)70-130
Page 59 of 61Date:09/15/2023 05:49 PM
Page 189 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
Dry Weight Determination
SW-DRYWT
V37380QC Analytical Batch:
Analysis Method:
Analysis Description:
V 93849-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/01/23 14:503.812.913.4%Moisture
Page 60 of 61Date:09/15/2023 05:49 PM
Page 190 of 194
Quality Control Data
23-244-0003Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
Dry Weight Determination
SW-DRYWT
V37425QC Analytical Batch:
Analysis Method:
Analysis Description:
V 93890-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/05/23 11:433.030.029.1%Moisture
V 94062-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/05/23 11:430.025.725.7%Moisture
Page 61 of 61Date:09/15/2023 05:49 PM
Page 191 of 194
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-244-0003
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
We did not receive bottles for 625/EPH on sample MW-4 and EPH on sample
MW-1.
Signature:Angelo Norvell Date & Time:09/01/2023 09:30:32
Special precautions or instructions included?
Comments:
Page 192 of 194
Page 193 of 194
Page 194 of 194

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

9/14/2023
Geological Resources, Inc. Xavier T Farmer
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-248-0020 Client Project Description: Yogi Foods
GRI #6473
Dear Xavier T Farmer:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/5/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 22
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-248-0020
Page 2 of 22
Report Number:
Sample Summary Table
Client Project Description:
23-248-0020
Yogi Foods
GRI #6473
Lab No Client Sample ID Matrix Date Collected Date Received
09/05/2023 09:07Aqueous 94261 MW-2 09/05/2023 15:10
09/05/2023 09:55Aqueous 94262 MW-4 09/05/2023 15:10
Page 3 of 22
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-248-0020
Report Limit
Project:Yogi Foods
V 94261MW-2
J0.768 09/09/2023 17:07625.1 2-Methylnaphthalene µg/L 0.666
3.00 09/09/2023 17:07625.1 Naphthalene µg/L 0.728
V 94262MW-4
34.7 09/09/2023 17:30625.1 1-Methylnaphthalene µg/L 1.14
61.0 09/09/2023 17:30625.1 2-Methylnaphthalene µg/L 0.666
150 09/09/2023 17:30625.1 Naphthalene µg/L 0.728
479 09/09/2023 17:30CALCULATIONAromatic C11-C22 (Adjusted)µg/L 61.2
J29.0 09/12/2023 14:15MADEP-EPH Aliphatic C9-C18 µg/L 28.2
629 09/12/2023 14:15MADEP-EPH Aromatic C11-C22 µg/L 61.2
Page 4 of 22

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Yogi Foods Lab Report Number: 23-248-0020
Date: 9/14/2023
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1 Analyte: 2-Chloronaphthalene QC Batch No: V37633/V37598
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Benzidine QC Batch No: V37633/V37598
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Dibenz(a,h)anthracene QC Batch No: V37633/V37598
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 5 of 22
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-248-0020
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 09/05/2023
Yogi Foods
Report Date : 09/14/2023
Sample ID :
Lab No :
Sampled:MW-2
94261 Matrix:
9/5/2023 9:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37598 09/08/23 10:12
<0.302 µg/L 0.302 2.00Acenaphthene 1 09/09/23 17:07 V37633AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 09/09/23 17:07 V37633AMP
<0.836 µg/L 0.836 2.00Anthracene 1 09/09/23 17:07 V37633AMP
<1.32 µg/L 1.32 10.0Benzidine 1 09/09/23 17:07 V37633AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 09/09/23 17:07 V37633AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 09/09/23 17:07 V37633AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 09/09/23 17:07 V37633AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 09/09/23 17:07 V37633AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 09/09/23 17:07 V37633AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 09/09/23 17:07 V37633AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 09/09/23 17:07 V37633AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 09/09/23 17:07 V37633AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 09/09/23 17:07 V37633AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 09/09/23 17:07 V37633AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 09/09/23 17:07 V37633AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 09/09/23 17:07 V37633AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 09/09/23 17:07 V37633AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 09/09/23 17:07 V37633AMP
<7.38 M µg/L 7.38 20.02-Chloronaphthalene 1 09/09/23 17:07 V37633AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 09/09/23 17:07 V37633AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 09/09/23 17:07 V37633AMP
<0.405 µg/L 0.405 2.00Chrysene 1 09/09/23 17:07 V37633AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 09/09/23 17:07 V37633AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 6 of 22
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-248-0020
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 09/05/2023
Yogi Foods
Report Date : 09/14/2023
Sample ID :
Lab No :
Sampled:MW-2
94261 Matrix:
9/5/2023 9:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37598 09/08/23 10:12
<0.856 µg/L 0.856 5.00Dibenzofuran 1 09/09/23 17:07 V37633AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 09/09/23 17:07 V37633AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 09/09/23 17:07 V37633AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 09/09/23 17:07 V37633AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 09/09/23 17:07 V37633AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 09/09/23 17:07 V37633AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 09/09/23 17:07 V37633AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 09/09/23 17:07 V37633AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 09/09/23 17:07 V37633AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 09/09/23 17:07 V37633AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 09/09/23 17:07 V37633AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 09/09/23 17:07 V37633AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 09/09/23 17:07 V37633AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 09/09/23 17:07 V37633AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 09/09/23 17:07 V37633AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 09/09/23 17:07 V37633AMP
<0.807 µg/L 0.807 2.00Fluorene 1 09/09/23 17:07 V37633AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 09/09/23 17:07 V37633AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 09/09/23 17:07 V37633AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 09/09/23 17:07 V37633AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 09/09/23 17:07 V37633AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 09/09/23 17:07 V37633AMP
<0.444 µg/L 0.444 5.00Isophorone 1 09/09/23 17:07 V37633AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 7 of 22
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-248-0020
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 09/05/2023
Yogi Foods
Report Date : 09/14/2023
Sample ID :
Lab No :
Sampled:MW-2
94261 Matrix:
9/5/2023 9:07
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37598 09/08/23 10:12
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 09/09/23 17:07 V37633AMP
0.768 J µg/L 0.666 2.002-Methylnaphthalene 1 09/09/23 17:07 V37633AMP
3.00 µg/L 0.728 2.00Naphthalene 1 09/09/23 17:07 V37633AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 09/09/23 17:07 V37633AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 09/09/23 17:07 V37633AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 09/09/23 17:07 V37633AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 09/09/23 17:07 V37633AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 09/09/23 17:07 V37633AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 09/09/23 17:07 V37633AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 09/09/23 17:07 V37633AMP
<0.651 µg/L 0.651 5.00Phenol 1 09/09/23 17:07 V37633AMP
<0.434 µg/L 0.434 2.00Pyrene 1 09/09/23 17:07 V37633AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 09/09/23 17:07 V37633AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 09/09/23 17:07 V37633AMP
625.1Surrogate: Phenol-d5 24.7 Limits: 10-63%09/09/23 17:071 AMP
Surrogate: 2-Fluorobiphenyl 70.6 Limits: 49-118%09/09/23 17:071 AMP V37633
Surrogate: 2-Fluorophenol 36.0 Limits: 22-84%09/09/23 17:071 AMP V37633
Surrogate: Nitrobenzene-d5 73.6 Limits: 43-123%09/09/23 17:071 AMP V37633
Surrogate: 4-Terphenyl-d14 92.8 Limits: 49-151%09/09/23 17:071 AMP V37633
Surrogate: 2,4,6-Tribromophenol 89.5 Limits: 31-144%09/09/23 17:071 AMP V37633
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 8 of 22
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-248-0020
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 09/05/2023
Yogi Foods
Report Date : 09/14/2023
Sample ID :
Lab No :
Sampled:MW-4
94262 Matrix:
9/5/2023 9:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37598 09/08/23 10:12
<0.302 µg/L 0.302 2.00Acenaphthene 1 09/09/23 17:30 V37633AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 09/09/23 17:30 V37633AMP
<0.836 µg/L 0.836 2.00Anthracene 1 09/09/23 17:30 V37633AMP
<1.32 µg/L 1.32 10.0Benzidine 1 09/09/23 17:30 V37633AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 09/09/23 17:30 V37633AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 09/09/23 17:30 V37633AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 09/09/23 17:30 V37633AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 09/09/23 17:30 V37633AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 09/09/23 17:30 V37633AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 09/09/23 17:30 V37633AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 09/09/23 17:30 V37633AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 09/09/23 17:30 V37633AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 09/09/23 17:30 V37633AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 09/09/23 17:30 V37633AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 09/09/23 17:30 V37633AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 09/09/23 17:30 V37633AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 09/09/23 17:30 V37633AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 09/09/23 17:30 V37633AMP
<7.38 M µg/L 7.38 20.02-Chloronaphthalene 1 09/09/23 17:30 V37633AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 09/09/23 17:30 V37633AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 09/09/23 17:30 V37633AMP
<0.405 µg/L 0.405 2.00Chrysene 1 09/09/23 17:30 V37633AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 09/09/23 17:30 V37633AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 9 of 22
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-248-0020
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 09/05/2023
Yogi Foods
Report Date : 09/14/2023
Sample ID :
Lab No :
Sampled:MW-4
94262 Matrix:
9/5/2023 9:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37598 09/08/23 10:12
<0.856 µg/L 0.856 5.00Dibenzofuran 1 09/09/23 17:30 V37633AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 09/09/23 17:30 V37633AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 09/09/23 17:30 V37633AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 09/09/23 17:30 V37633AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 09/09/23 17:30 V37633AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 09/09/23 17:30 V37633AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 09/09/23 17:30 V37633AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 09/09/23 17:30 V37633AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 09/09/23 17:30 V37633AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 09/09/23 17:30 V37633AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 09/09/23 17:30 V37633AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 09/09/23 17:30 V37633AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 09/09/23 17:30 V37633AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 09/09/23 17:30 V37633AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 09/09/23 17:30 V37633AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 09/09/23 17:30 V37633AMP
<0.807 µg/L 0.807 2.00Fluorene 1 09/09/23 17:30 V37633AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 09/09/23 17:30 V37633AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 09/09/23 17:30 V37633AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 09/09/23 17:30 V37633AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 09/09/23 17:30 V37633AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 09/09/23 17:30 V37633AMP
<0.444 µg/L 0.444 5.00Isophorone 1 09/09/23 17:30 V37633AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 10 of 22
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-248-0020
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 09/05/2023
Yogi Foods
Report Date : 09/14/2023
Sample ID :
Lab No :
Sampled:MW-4
94262 Matrix:
9/5/2023 9:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37598 09/08/23 10:12
34.7 µg/L 1.14 2.001-Methylnaphthalene 1 09/09/23 17:30 V37633AMP
61.0 µg/L 0.666 2.002-Methylnaphthalene 1 09/09/23 17:30 V37633AMP
150 µg/L 0.728 2.00Naphthalene 1 09/09/23 17:30 V37633AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 09/09/23 17:30 V37633AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 09/09/23 17:30 V37633AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 09/09/23 17:30 V37633AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 09/09/23 17:30 V37633AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 09/09/23 17:30 V37633AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 09/09/23 17:30 V37633AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 09/09/23 17:30 V37633AMP
<0.651 µg/L 0.651 5.00Phenol 1 09/09/23 17:30 V37633AMP
<0.434 µg/L 0.434 2.00Pyrene 1 09/09/23 17:30 V37633AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 09/09/23 17:30 V37633AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 09/09/23 17:30 V37633AMP
625.1Surrogate: Phenol-d5 26.9 Limits: 10-63%09/09/23 17:301 AMP
Surrogate: 2-Fluorobiphenyl 71.0 Limits: 49-118%09/09/23 17:301 AMP V37633
Surrogate: 2-Fluorophenol 43.3 Limits: 22-84%09/09/23 17:301 AMP V37633
Surrogate: Nitrobenzene-d5 75.6 Limits: 43-123%09/09/23 17:301 AMP V37633
Surrogate: 4-Terphenyl-d14 89.6 Limits: 49-151%09/09/23 17:301 AMP V37633
Surrogate: 2,4,6-Tribromophenol 93.5 Limits: 31-144%09/09/23 17:301 AMP V37633
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 11 of 22
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-248-0020
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #6473 Received : 09/05/2023
Yogi Foods
Report Date : 09/14/2023
Sample ID :
Lab No :
Sampled:MW-4
94262 Matrix:
9/5/2023 9:55
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
479 µg/L 61.2 250Aromatic C11-C22 (Adjusted)1 09/09/23 17:30
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V37556 09/07/23 15:11
29.0 J µg/L 28.2 350Aliphatic C9-C18 1 09/12/23 14:15 V37698NDL
<124 µg/L 124 500Aliphatic C19-C36 1 09/12/23 14:15 V37698NDL
629 µg/L 61.2 250Aromatic C11-C22 1 09/12/23 14:15 V37698NDL
MADEP-EPHSurrogate: 2-Bromonaphthalene 94.3 Limits: 40-140%09/12/23 14:151 NDL
MADEP-EPHSurrogate: Chlorooctadecane 50.5 Limits: 40-140%09/12/23 14:151 NDL
MADEP-EPHSurrogate: OTP Surrogate 66.4 Limits: 40-140%09/12/23 14:151 NDL
Surrogate: 2-Fluorobiphenyl 92.0 Limits: 40-140%09/12/23 14:151 NDL V37698
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 12 of 22
Sample ID Report Lab NoLRB‐V37598 23‐248‐0020 LRB
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
No TICs Detected N.D. ug/L 1 625 9/9/2023 12:52 APANN V37633
Sample ID Report Lab NoMW‐2 23‐248‐0020 94261
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Toluene 31080 ug/L 1 625 9/9/2023 17:07 APANN V37633
Hexanol, methyl‐11700 ug/L 1 625 9/9/2023 17:07 APANN V37633
Benzene, 1,3‐dimethyl‐40270 ug/L 1 625 9/9/2023 17:07 APANN V37633
Benzene, 1,2‐ dimethyl‐18300 ug/L 1 625 9/9/2023 17:07 APANN V37633
Octadecane 14290 ug/L 1 625 9/9/2023 17:07 APANN V37633
Sample ID Report Lab NoMW‐4 23‐248‐0020 94262
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Toluene 2716030 ug/L 1 625 9/9/2023 17:30 APANN V37633
Ethylbenzene 745730 ug/L 1 625 9/9/2023 17:30 APANN V37633
Benzene, 1,3‐dimethyl‐1322970 ug/L 1 625 9/9/2023 17:30 APANN V37633
Benzene, propyl‐230000 ug/L 1 625 9/9/2023 17:30 APANN V37633
Benzene, 1‐ethyl‐3‐methyl‐797350 ug/L 1 625 9/9/2023 17:30 APANN V37633
Benzene, 1,2,3‐trimethyl‐359400 ug/L 1 625 9/9/2023 17:30 APANN V37633
Benzene, 1‐ethyl‐2‐methyl‐338460 ug/L 1 625 9/9/2023 17:30 APANN V37633
Benzene, 1,3,5‐trimethyl‐1037860 ug/L 1 625 9/9/2023 17:30 APANN V37633
Indane 173520 ug/L 1 625 9/9/2023 17:30 APANN V37633
Benzene, 4‐ethyl‐1,2‐
dimethyl‐189950 ug/L 1 625 9/9/2023 17:30 APANN V37633
Page 13 of 22
Quality Control Data
23-248-0020Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37633QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37598
Associated Lab Samples: 94261, 94262
LRB-V37598 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/23 12:522.000.302<0.302µg/LAcenaphthene
09/09/23 12:522.000.297<0.297µg/LAcenaphthylene
09/09/23 12:522.000.836<0.836µg/LAnthracene
09/09/23 12:5210.01.32<1.32µg/LBenzidine
09/09/23 12:522.000.637<0.637µg/LBenzo(a)anthracene
09/09/23 12:522.001.02<1.02µg/LBenzo(a)pyrene
09/09/23 12:525.002.49<2.49µg/LBenzo(b)fluoranthene
09/09/23 12:525.001.01<1.01µg/LBenzo(g,h,i)perylene
09/09/23 12:525.001.99<1.99µg/LBenzo(k)fluoranthene
09/09/23 12:5210.01.10<1.10µg/LBenzoic Acid
09/09/23 12:525.000.684<0.684µg/LBenzyl alcohol
09/09/23 12:525.000.468<0.468µg/LBis(2-Chloroethoxy)methane
09/09/23 12:525.001.04<1.04µg/LBis(2-Chloroethyl)ether
09/09/23 12:525.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
09/09/23 12:5210.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
09/09/23 12:525.001.11<1.11µg/L4-Bromophenyl phenyl ether
09/09/23 12:525.001.83<1.83µg/LButyl benzyl phthalate
09/09/23 12:525.001.18<1.18µg/L4-Chloro-3-methylphenol
09/09/23 12:5220.07.38<7.38µg/L2-Chloronaphthalene
09/09/23 12:5210.00.938<0.938µg/L2-Chlorophenol
09/09/23 12:525.001.71<1.71µg/L4-Chlorophenyl phenyl ether
09/09/23 12:522.000.405<0.405µg/LChrysene
09/09/23 12:522.000.434<0.434µg/LDibenz(a,h)anthracene
09/09/23 12:525.000.856<0.856µg/LDibenzofuran
09/09/23 12:525.002.00<2.00µg/L1,2-Dichlorobenzene
09/09/23 12:525.002.00<2.00µg/L1,3-Dichlorobenzene
09/09/23 12:525.002.05<2.05µg/L1,4-Dichlorobenzene
Page 1 of 7Date:09/14/2023 06:16 PM
Page 14 of 22
Quality Control Data
23-248-0020Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37633QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37598
Associated Lab Samples: 94261, 94262
LRB-V37598 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/23 12:525.001.89<1.89µg/L3,3'-Dichlorobenzidine
09/09/23 12:5210.01.46<1.46µg/L2,4-Dichlorophenol
09/09/23 12:525.000.745<0.745µg/LDiethyl phthalate
09/09/23 12:525.000.939<0.939µg/LDimethyl phthalate
09/09/23 12:5220.01.57<1.57µg/L2,4-Dimethylphenol
09/09/23 12:525.002.06<2.06µg/LDi-n-butyl phthalate
09/09/23 12:5210.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
09/09/23 12:5210.01.92<1.92µg/L2,4-Dinitrophenol
09/09/23 12:525.001.11<1.11µg/L2,4-Dinitrotoluene
09/09/23 12:525.000.809<0.809µg/L2,6-Dinitrotoluene
09/09/23 12:525.001.65<1.65µg/LDi-n-Octyl Phthalate
09/09/23 12:522.000.250<0.250µg/LFluoranthene
09/09/23 12:522.000.807<0.807µg/LFluorene
09/09/23 12:525.000.979<0.979µg/LHexachlorobenzene
09/09/23 12:525.002.73<2.73µg/LHexachlorobutadiene
09/09/23 12:525.002.05<2.05µg/LHexachlorocyclopentadiene
09/09/23 12:525.001.76<1.76µg/LHexachloroethane
09/09/23 12:522.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
09/09/23 12:525.000.444<0.444µg/LIsophorone
09/09/23 12:522.001.14<1.14µg/L1-Methylnaphthalene
09/09/23 12:522.000.666<0.666µg/L2-Methylnaphthalene
09/09/23 12:522.000.728<0.728µg/LNaphthalene
09/09/23 12:525.000.905<0.905µg/LNitrobenzene
09/09/23 12:525.000.493<0.493µg/L2-Nitrophenol
09/09/23 12:5210.01.23<1.23µg/L4-Nitrophenol
09/09/23 12:525.001.10<1.10µg/LN-Nitrosodiphenylamine
09/09/23 12:525.000.641<0.641µg/LN-Nitroso-di-n-propylamine
Page 2 of 7Date:09/14/2023 06:16 PM
Page 15 of 22
Quality Control Data
23-248-0020Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37633QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37598
Associated Lab Samples: 94261, 94262
LRB-V37598 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/23 12:525.001.43<1.43µg/LPentachlorophenol
09/09/23 12:522.000.428<0.428µg/LPhenanthrene
09/09/23 12:525.000.651<0.651µg/LPhenol
09/09/23 12:522.000.434<0.434µg/LPyrene
09/09/23 12:525.002.21<2.21µg/L1,2,4-Trichlorobenzene
09/09/23 12:525.001.32<1.32µg/L2,4,6-Trichlorophenol
09/09/23 12:522-Fluorobiphenyl (S)52.6 49-118
09/09/23 12:522-Fluorophenol (S)33.6 22-84
09/09/23 12:52Nitrobenzene-d5 (S)56.6 43-123
09/09/23 12:524-Terphenyl-d14 (S)66.2 49-151
09/09/23 12:522,4,6-Tribromophenol (S)66.1 31-144
09/09/23 12:52Phenol-d5 (S)22.2 10-63
LCS-V37598 LCSD-V37598Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
34.0 68.062.031.050.0µg/LAcenaphthene 47-145 9.2 20.0
34.0 68.061.830.950.0µg/LAcenaphthylene 33-145 9.5 20.0
40.5 81.072.236.150.0µg/LAnthracene 27-133 11.4 20.0
33.1 66.247.823.950.0µg/LBenzidine 15-150 32.2*20.0
41.4 82.874.637.350.0µg/LBenzo(a)anthracene 33-143 10.4 20.0
44.6 89.280.240.150.0µg/LBenzo(a)pyrene 17-163 10.6 20.0
40.4 80.873.236.650.0µg/LBenzo(b)fluoranthene 24-159 9.8 20.0
39.5 79.071.635.850.0µg/LBenzo(g,h,i)perylene 10-219 9.8 20.0
43.1 86.276.638.350.0µg/LBenzo(k)fluoranthene 11-162 11.7 20.0
21.0 42.045.422.750.0µg/LBenzoic Acid 10-125 7.7 20.0
Page 3 of 7* QC Fail Date:09/14/2023 06:16 PM
Page 16 of 22
Quality Control Data
23-248-0020Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37633QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37598
LCS-V37598 LCSD-V37598Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
38.9 77.873.036.550.0µg/LBenzyl alcohol 16-107 6.3 20.0
34.4 68.865.032.550.0µg/LBis(2-Chloroethoxy)methane 33-184 5.6 20.0
28.0 56.051.225.650.0µg/LBis(2-Chloroethyl)ether 12-158 8.9 20.0
31.2 62.457.028.550.0µg/LBis(2-Chloroisopropyl)ether 36-166 9.0 20.0
43.9 87.880.640.350.0µg/LBis(2-ethylhexyl)phthalate 10-158 8.5 20.0
39.3 78.668.234.150.0µg/L4-Bromophenyl phenyl ether 53-127 14.1 20.0
42.6 85.278.039.050.0µg/LButyl benzyl phthalate 10-152 8.8 20.0
41.7 83.475.037.550.0µg/L4-Chloro-3-methylphenol 22-147 10.6 20.0
31.9 63.858.6*29.350.0µg/L2-Chloronaphthalene 60-118 8.4 20.0
31.6 63.257.828.950.0µg/L2-Chlorophenol 23-134 8.9 20.0
37.6 75.267.433.750.0µg/L4-Chlorophenyl phenyl ether 25-158 10.9 20.0
40.7 81.473.836.950.0µg/LChrysene 17-168 9.7 20.0
75.1 15011758.450.0µg/LDibenz(a,h)anthracene 10-227 25.0*20.0
34.9 69.863.831.950.0µg/LDibenzofuran 39-114 8.9 20.0
23.5 47.043.421.750.0µg/L1,2-Dichlorobenzene 32-129 7.9 20.0
22.9 45.842.221.150.0µg/L1,3-Dichlorobenzene 20-124 8.1 20.0
23.1 46.242.421.250.0µg/L1,4-Dichlorobenzene 20-124 8.5 20.0
42.3 84.676.238.150.0µg/L3,3'-Dichlorobenzidine 10-262 10.4 20.0
36.9 73.867.833.950.0µg/L2,4-Dichlorophenol 39-135 8.4 20.0
40.6 81.273.236.650.0µg/LDiethyl phthalate 10-114 10.3 20.0
40.4 80.872.636.350.0µg/LDimethyl phthalate 10-112 10.6 20.0
50.3 10191.045.550.0µg/L2,4-Dimethylphenol 32-119 10.0 20.0
44.3 88.679.439.750.0µg/LDi-n-butyl phthalate 10-118 10.9 20.0
44.0 88.079.439.750.0µg/L4,6-Dinitro-2-methylphenol 10-181 10.2 20.0
54.0 10898.649.350.0µg/L2,4-Dinitrophenol 10-191 9.0 20.0
43.4 86.877.238.650.0µg/L2,4-Dinitrotoluene 39-139 11.7 20.0
Page 4 of 7* QC Fail Date:09/14/2023 06:16 PM
Page 17 of 22
Quality Control Data
23-248-0020Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37633QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37598
LCS-V37598 LCSD-V37598Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
45.7 91.478.439.250.0µg/L2,6-Dinitrotoluene 50-158 15.3 20.0
44.7 89.481.840.950.0µg/LDi-n-Octyl Phthalate 10-146 8.8 20.0
37.6 75.267.833.950.0µg/LFluoranthene 26-137 10.3 20.0
36.7 73.466.633.350.0µg/LFluorene 59-121 9.7 20.0
40.4 80.872.236.150.0µg/LHexachlorobenzene 10-152 11.2 20.0
25.9 51.848.024.050.0µg/LHexachlorobutadiene 24-116 7.6 20.0
24.8 49.645.822.950.0µg/LHexachlorocyclopentadiene 32-117 7.9 20.0
22.3 44.640.820.450.0µg/LHexachloroethane 40-113 8.8 20.0
39.8 79.671.835.950.0µg/LIndeno(1,2,3-cd)pyrene 10-171 10.3 20.0
32.4 64.860.830.450.0µg/LIsophorone 21-196 6.3 20.0
28.9 57.854.427.250.0µg/L1-Methylnaphthalene 40-135 6.0 20.0
28.8 57.652.626.350.0µg/L2-Methylnaphthalene 18-121 9.0 20.0
27.8 55.651.025.550.0µg/LNaphthalene 21-133 8.6 20.0
32.3 64.660.030.050.0µg/LNitrobenzene 35-180 7.3 20.0
38.8 77.670.435.250.0µg/L2-Nitrophenol 29-182 9.7 20.0
22.8 45.640.420.250.0µg/L4-Nitrophenol 10-132 12.0 20.0
46.5 93.084.842.450.0µg/LN-Nitrosodiphenylamine 69-152 9.2 20.0
32.9 65.862.231.150.0µg/LN-Nitroso-di-n-propylamine 10-230 5.6 20.0
51.6 10397.048.550.0µg/LPentachlorophenol 14-176 6.1 20.0
38.4 76.870.035.050.0µg/LPhenanthrene 54-120 9.2 20.0
15.2 30.426.813.450.0µg/LPhenol 10-112 12.5 20.0
38.6 77.270.835.450.0µg/LPyrene 52-115 8.6 20.0
25.2 50.447.623.850.0µg/L1,2,4-Trichlorobenzene 44-142 5.7 20.0
39.0 78.068.834.450.0µg/L2,4,6-Trichlorophenol 37-144 12.5 20.0
64.860.02-Fluorobiphenyl (S)49-118
36.434.52-Fluorophenol (S)22-84
Page 5 of 7Date:09/14/2023 06:16 PM
Page 18 of 22
Quality Control Data
23-248-0020Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37633QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37598
LCS-V37598 LCSD-V37598Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
67.061.2Nitrobenzene-d5 (S)43-123
79.474.44-Terphenyl-d14 (S)49-151
78.973.02,4,6-Tribromophenol (S)31-144
23.522.2Phenol-d5 (S)10-63
Page 6 of 7Date:09/14/2023 06:16 PM
Page 19 of 22
Quality Control Data
23-248-0020Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V37698QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V37556
Associated Lab Samples: 94262
LRB-V37556 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/13/23 10:4835028.2<28.2µg/LAliphatic C9-C18
09/13/23 10:48500124<124µg/LAliphatic C19-C36
09/13/23 10:4825061.2<61.2µg/LAromatic C11-C22
09/13/23 10:482-Fluorobiphenyl (S)73.0 40-140
09/13/23 10:482-Bromonaphthalene (S)67.2 40-140
09/13/23 10:48Chlorooctadecane (S)65.2 40-140
09/13/23 10:48OTP Surrogate (S)65.0 40-140
LCS-V37556 LCSD-V37556Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
416 69.382.8497600µg/LAliphatic C9-C18 40-140 17.7 50.0
822 103115918800µg/LAliphatic C19-C36 40-140 11.0 50.0
1630 95.810718201700µg/LAromatic C11-C22 40-140 11.0 50.0
80.780.02-Fluorobiphenyl (S)40-140
76.575.22-Bromonaphthalene (S)40-140
60.371.7Chlorooctadecane (S)40-140
69.074.5OTP Surrogate (S)40-140
Page 7 of 7Date:09/14/2023 06:16 PM
Page 20 of 22
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-248-0020
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.4C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Only received an HCL Amber Liter for sample MW-1.
Signature:Angelo Norvell Date & Time:09/05/2023 18:25:19
Special precautions or instructions included?
Comments:
Page 21 of 22
Page 22 of 22

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

9/15/2023
Geological Resources, Inc. Xavier T Farmer
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-251-0013 Client Project Description: Yogi Foods
GRI #N/A
Dear Xavier T Farmer:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/8/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 16
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-251-0013
Page 2 of 16
Report Number:
Sample Summary Table
Client Project Description:
23-251-0013
Yogi Foods
GRI #N/A
Lab No Client Sample ID Matrix Date Collected Date Received
09/07/2023 19:00Aqueous 94530 MW-1 09/08/2023 12:53
Page 3 of 16
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-251-0013
Report Limit
Project:Yogi Foods
No Analytes Detected
Page 4 of 16
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-251-0013
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #N/A Received : 09/08/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
94530 Matrix:
9/7/2023 19:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37727 09/12/23 10:21
<0.302 µg/L 0.302 2.00Acenaphthene 1 09/12/23 20:24 V37747AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 09/12/23 20:24 V37747AMP
<0.836 µg/L 0.836 2.00Anthracene 1 09/12/23 20:24 V37747AMP
<1.32 µg/L 1.32 10.0Benzidine 1 09/12/23 20:24 V37747AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 09/12/23 20:24 V37747AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 09/12/23 20:24 V37747AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 09/12/23 20:24 V37747AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 09/12/23 20:24 V37747AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 09/12/23 20:24 V37747AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 09/12/23 20:24 V37747AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 09/12/23 20:24 V37747AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 09/12/23 20:24 V37747AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 09/12/23 20:24 V37747AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 09/12/23 20:24 V37747AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 09/12/23 20:24 V37747AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 09/12/23 20:24 V37747AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 09/12/23 20:24 V37747AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 09/12/23 20:24 V37747AMP
<7.38 µg/L 7.38 20.02-Chloronaphthalene 1 09/12/23 20:24 V37747AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 09/12/23 20:24 V37747AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 09/12/23 20:24 V37747AMP
<0.405 µg/L 0.405 2.00Chrysene 1 09/12/23 20:24 V37747AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 09/12/23 20:24 V37747AMP
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 5 of 16
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-251-0013
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #N/A Received : 09/08/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
94530 Matrix:
9/7/2023 19:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37727 09/12/23 10:21
<0.856 µg/L 0.856 5.00Dibenzofuran 1 09/12/23 20:24 V37747AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 09/12/23 20:24 V37747AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 09/12/23 20:24 V37747AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 09/12/23 20:24 V37747AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 09/12/23 20:24 V37747AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 09/12/23 20:24 V37747AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 09/12/23 20:24 V37747AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 09/12/23 20:24 V37747AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 09/12/23 20:24 V37747AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 09/12/23 20:24 V37747AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 09/12/23 20:24 V37747AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 09/12/23 20:24 V37747AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 09/12/23 20:24 V37747AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 09/12/23 20:24 V37747AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 09/12/23 20:24 V37747AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 09/12/23 20:24 V37747AMP
<0.807 µg/L 0.807 2.00Fluorene 1 09/12/23 20:24 V37747AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 09/12/23 20:24 V37747AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 09/12/23 20:24 V37747AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 09/12/23 20:24 V37747AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 09/12/23 20:24 V37747AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 09/12/23 20:24 V37747AMP
<0.444 µg/L 0.444 5.00Isophorone 1 09/12/23 20:24 V37747AMP
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 6 of 16
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-251-0013
00087
Geological Resources, Inc.
3502 Hayes Road
Xavier T Farmer
Monroe
Danyale Love
Project Manager
GRI #N/A Received : 09/08/2023
Yogi Foods
Report Date : 09/15/2023
Sample ID :
Lab No :
Sampled:MW-1
94530 Matrix:
9/7/2023 19:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V37727 09/12/23 10:21
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 09/12/23 20:24 V37747AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 09/12/23 20:24 V37747AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 09/12/23 20:24 V37747AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 09/12/23 20:24 V37747AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 09/12/23 20:24 V37747AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 09/12/23 20:24 V37747AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 09/12/23 20:24 V37747AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 09/12/23 20:24 V37747AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 09/12/23 20:24 V37747AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 09/12/23 20:24 V37747AMP
<0.651 µg/L 0.651 5.00Phenol 1 09/12/23 20:24 V37747AMP
<0.434 µg/L 0.434 2.00Pyrene 1 09/12/23 20:24 V37747AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 09/12/23 20:24 V37747AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 09/12/23 20:24 V37747AMP
625.1Surrogate: Phenol-d5 22.1 Limits: 10-63%09/12/23 20:241 AMP
Surrogate: 2-Fluorobiphenyl 58.2 Limits: 49-118%09/12/23 20:241 AMP V37747
Surrogate: 2-Fluorophenol 33.5 Limits: 22-84%09/12/23 20:241 AMP V37747
Surrogate: Nitrobenzene-d5 55.4 Limits: 43-123%09/12/23 20:241 AMP V37747
Surrogate: 4-Terphenyl-d14 71.6 Limits: 49-151%09/12/23 20:241 AMP V37747
Surrogate: 2,4,6-Tribromophenol 60.9 Limits: 31-144%09/12/23 20:241 AMP V37747
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 7 of 16
Sample ID Report Lab NoLRB‐V37727 23‐251‐0013 LRB
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Butane, methoxy‐methyl‐65670 ug/L 1 625 9/12/2023 17:45 APANN V37747
Sample ID Report Lab NoMW‐1 23‐251‐0013 94530
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Butane, methoxy‐methyl‐61950 ug/L 1 625 9/12/2023 20:24 APANN V37747
Page 8 of 16
Quality Control Data
23-251-0013Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37747QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37727
Associated Lab Samples: 94530
LRB-V37727 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/12/23 17:452.000.302<0.302µg/LAcenaphthene
09/12/23 17:452.000.297<0.297µg/LAcenaphthylene
09/12/23 17:452.000.836<0.836µg/LAnthracene
09/12/23 17:4510.01.32<1.32µg/LBenzidine
09/12/23 17:452.000.637<0.637µg/LBenzo(a)anthracene
09/12/23 17:452.001.02<1.02µg/LBenzo(a)pyrene
09/12/23 17:455.002.49<2.49µg/LBenzo(b)fluoranthene
09/12/23 17:455.001.01<1.01µg/LBenzo(g,h,i)perylene
09/12/23 17:455.001.99<1.99µg/LBenzo(k)fluoranthene
09/12/23 17:4510.01.10<1.10µg/LBenzoic Acid
09/12/23 17:455.000.684<0.684µg/LBenzyl alcohol
09/12/23 17:455.000.468<0.468µg/LBis(2-Chloroethoxy)methane
09/12/23 17:455.001.04<1.04µg/LBis(2-Chloroethyl)ether
09/12/23 17:455.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
09/12/23 17:4510.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
09/12/23 17:455.001.11<1.11µg/L4-Bromophenyl phenyl ether
09/12/23 17:455.001.83<1.83µg/LButyl benzyl phthalate
09/12/23 17:455.001.18<1.18µg/L4-Chloro-3-methylphenol
09/12/23 17:4520.07.38<7.38µg/L2-Chloronaphthalene
09/12/23 17:4510.00.938<0.938µg/L2-Chlorophenol
09/12/23 17:455.001.71<1.71µg/L4-Chlorophenyl phenyl ether
09/12/23 17:452.000.405<0.405µg/LChrysene
09/12/23 17:452.000.434<0.434µg/LDibenz(a,h)anthracene
09/12/23 17:455.000.856<0.856µg/LDibenzofuran
09/12/23 17:455.002.00<2.00µg/L1,2-Dichlorobenzene
09/12/23 17:455.002.00<2.00µg/L1,3-Dichlorobenzene
09/12/23 17:455.002.05<2.05µg/L1,4-Dichlorobenzene
Page 1 of 6Date:09/15/2023 06:08 PM
Page 9 of 16
Quality Control Data
23-251-0013Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37747QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37727
Associated Lab Samples: 94530
LRB-V37727 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/12/23 17:455.001.89<1.89µg/L3,3'-Dichlorobenzidine
09/12/23 17:4510.01.46<1.46µg/L2,4-Dichlorophenol
09/12/23 17:455.000.745<0.745µg/LDiethyl phthalate
09/12/23 17:455.000.939<0.939µg/LDimethyl phthalate
09/12/23 17:4520.01.57<1.57µg/L2,4-Dimethylphenol
09/12/23 17:455.002.06<2.06µg/LDi-n-butyl phthalate
09/12/23 17:4510.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
09/12/23 17:4510.01.92<1.92µg/L2,4-Dinitrophenol
09/12/23 17:455.001.11<1.11µg/L2,4-Dinitrotoluene
09/12/23 17:455.000.809<0.809µg/L2,6-Dinitrotoluene
09/12/23 17:455.001.65<1.65µg/LDi-n-Octyl Phthalate
09/12/23 17:452.000.250<0.250µg/LFluoranthene
09/12/23 17:452.000.807<0.807µg/LFluorene
09/12/23 17:455.000.979<0.979µg/LHexachlorobenzene
09/12/23 17:455.002.73<2.73µg/LHexachlorobutadiene
09/12/23 17:455.002.05<2.05µg/LHexachlorocyclopentadiene
09/12/23 17:455.001.76<1.76µg/LHexachloroethane
09/12/23 17:452.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
09/12/23 17:455.000.444<0.444µg/LIsophorone
09/12/23 17:452.001.14<1.14µg/L1-Methylnaphthalene
09/12/23 17:452.000.666<0.666µg/L2-Methylnaphthalene
09/12/23 17:452.000.728<0.728µg/LNaphthalene
09/12/23 17:455.000.905<0.905µg/LNitrobenzene
09/12/23 17:455.000.493<0.493µg/L2-Nitrophenol
09/12/23 17:4510.01.23<1.23µg/L4-Nitrophenol
09/12/23 17:455.001.10<1.10µg/LN-Nitrosodiphenylamine
09/12/23 17:455.000.641<0.641µg/LN-Nitroso-di-n-propylamine
Page 2 of 6Date:09/15/2023 06:08 PM
Page 10 of 16
Quality Control Data
23-251-0013Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37747QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37727
Associated Lab Samples: 94530
LRB-V37727 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/12/23 17:455.001.43<1.43µg/LPentachlorophenol
09/12/23 17:452.000.428<0.428µg/LPhenanthrene
09/12/23 17:455.000.651<0.651µg/LPhenol
09/12/23 17:452.000.434<0.434µg/LPyrene
09/12/23 17:455.002.21<2.21µg/L1,2,4-Trichlorobenzene
09/12/23 17:455.001.32<1.32µg/L2,4,6-Trichlorophenol
09/12/23 17:452-Fluorobiphenyl (S)75.4 49-118
09/12/23 17:452-Fluorophenol (S)40.4 22-84
09/12/23 17:45Nitrobenzene-d5 (S)72.8 43-123
09/12/23 17:454-Terphenyl-d14 (S)85.0 49-151
09/12/23 17:452,4,6-Tribromophenol (S)74.5 31-144
09/12/23 17:45Phenol-d5 (S)25.7 10-63
LCS-V37727 LCSD-V37727Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.8 65.671.435.750.0µg/LAcenaphthene 47-145 8.4 20.0
32.6 65.271.435.750.0µg/LAcenaphthylene 33-145 9.0 20.0
37.1 74.279.639.850.0µg/LAnthracene 27-133 7.0 20.0
23.4 46.843.021.550.0µg/LBenzidine 15-150 8.4 20.0
35.2 70.475.837.950.0µg/LBenzo(a)anthracene 33-143 7.3 20.0
38.8 77.683.841.950.0µg/LBenzo(a)pyrene 17-163 7.6 20.0
36.4 72.879.639.850.0µg/LBenzo(b)fluoranthene 24-159 8.9 20.0
33.7 67.471.235.650.0µg/LBenzo(g,h,i)perylene 10-219 5.4 20.0
35.2 70.477.238.650.0µg/LBenzo(k)fluoranthene 11-162 9.2 20.0
15.6 31.234.617.350.0µg/LBenzoic Acid 10-125 10.3 20.0
Page 3 of 6Date:09/15/2023 06:08 PM
Page 11 of 16
Quality Control Data
23-251-0013Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37747QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37727
LCS-V37727 LCSD-V37727Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
29.7 59.463.431.750.0µg/LBenzyl alcohol 16-107 6.5 20.0
29.7 59.465.432.750.0µg/LBis(2-Chloroethoxy)methane 33-184 9.6 20.0
26.4 52.860.030.050.0µg/LBis(2-Chloroethyl)ether 12-158 12.7 20.0
29.5 59.067.433.750.0µg/LBis(2-Chloroisopropyl)ether 36-166 13.2 20.0
37.2 74.479.239.650.0µg/LBis(2-ethylhexyl)phthalate 10-158 6.2 20.0
35.2 70.478.039.050.0µg/L4-Bromophenyl phenyl ether 53-127 10.2 20.0
36.1 72.277.438.750.0µg/LButyl benzyl phthalate 10-152 6.9 20.0
30.2 60.464.832.450.0µg/L4-Chloro-3-methylphenol 22-147 7.0 20.0
32.0 64.070.635.350.0µg/L2-Chloronaphthalene 60-118 9.8 20.0
28.0 56.063.031.550.0µg/L2-Chlorophenol 23-134 11.7 20.0
34.9 69.876.638.350.0µg/L4-Chlorophenyl phenyl ether 25-158 9.2 20.0
35.8 71.676.638.350.0µg/LChrysene 17-168 6.7 20.0
22.7 45.443.221.650.0µg/LDibenz(a,h)anthracene 10-227 4.9 20.0
32.8 65.672.036.050.0µg/LDibenzofuran 39-114 9.3 20.0
25.5 51.057.828.950.0µg/L1,2-Dichlorobenzene 32-129 12.5 20.0
24.7 49.456.228.150.0µg/L1,3-Dichlorobenzene 20-124 12.8 20.0
24.7 49.456.028.050.0µg/L1,4-Dichlorobenzene 20-124 12.5 20.0
35.7 71.477.638.850.0µg/L3,3'-Dichlorobenzidine 10-262 8.3 20.0
29.2 58.463.631.850.0µg/L2,4-Dichlorophenol 39-135 8.5 20.0
36.4 72.877.638.850.0µg/LDiethyl phthalate 10-114 6.3 20.0
35.9 71.877.238.650.0µg/LDimethyl phthalate 10-112 7.2 20.0
40.0 80.085.842.950.0µg/L2,4-Dimethylphenol 32-119 6.9 20.0
38.9 77.883.441.750.0µg/LDi-n-butyl phthalate 10-118 6.9 20.0
37.8 75.681.240.650.0µg/L4,6-Dinitro-2-methylphenol 10-181 7.1 20.0
34.2 68.478.039.050.0µg/L2,4-Dinitrophenol 10-191 13.1 20.0
36.3 72.679.039.550.0µg/L2,4-Dinitrotoluene 39-139 8.4 20.0
Page 4 of 6Date:09/15/2023 06:08 PM
Page 12 of 16
Quality Control Data
23-251-0013Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37747QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37727
LCS-V37727 LCSD-V37727Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
35.5 71.076.638.350.0µg/L2,6-Dinitrotoluene 50-158 7.5 20.0
36.7 73.479.839.950.0µg/LDi-n-Octyl Phthalate 10-146 8.3 20.0
33.6 67.274.037.050.0µg/LFluoranthene 26-137 9.6 20.0
34.0 68.074.437.250.0µg/LFluorene 59-121 8.9 20.0
35.0 70.076.838.450.0µg/LHexachlorobenzene 10-152 9.2 20.0
24.9 49.856.028.050.0µg/LHexachlorobutadiene 24-116 11.7 20.0
25.3 50.655.227.650.0µg/LHexachlorocyclopentadiene 32-117 8.6 20.0
24.1 48.255.427.750.0µg/LHexachloroethane 40-113 13.8 20.0
33.6 67.272.636.350.0µg/LIndeno(1,2,3-cd)pyrene 10-171 7.7 20.0
28.2 56.461.030.550.0µg/LIsophorone 21-196 7.8 20.0
26.3 52.658.829.450.0µg/L1-Methylnaphthalene 40-135 11.1 20.0
26.3 52.658.829.450.0µg/L2-Methylnaphthalene 18-121 11.1 20.0
25.8 51.657.028.550.0µg/LNaphthalene 21-133 9.9 20.0
25.1 50.255.227.650.0µg/LNitrobenzene 35-180 9.4 20.0
27.1 54.259.229.650.0µg/L2-Nitrophenol 29-182 8.8 20.0
17.4 34.836.418.250.0µg/L4-Nitrophenol 10-132 4.4 20.0
43.0 86.093.446.750.0µg/LN-Nitrosodiphenylamine 69-152 8.2 20.0
30.6 61.269.234.650.0µg/LN-Nitroso-di-n-propylamine 10-230 12.2 20.0
40.4 80.884.842.450.0µg/LPentachlorophenol 14-176 4.8 20.0
35.9 71.877.838.950.0µg/LPhenanthrene 54-120 8.0 20.0
13.5 27.029.814.950.0µg/LPhenol 10-112 9.8 20.0
35.5 71.076.038.050.0µg/LPyrene 52-115 6.8 20.0
24.6 49.255.627.850.0µg/L1,2,4-Trichlorobenzene 44-142 12.2 20.0
33.7 67.473.636.850.0µg/L2,4,6-Trichlorophenol 37-144 8.7 20.0
64.271.42-Fluorobiphenyl (S)49-118
32.236.02-Fluorophenol (S)22-84
Page 5 of 6Date:09/15/2023 06:08 PM
Page 13 of 16
Quality Control Data
23-251-0013Report No:
Project Description:
Client ID:Geological Resources, Inc.
Yogi Foods
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V37747QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V37727
LCS-V37727 LCSD-V37727Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
52.458.6Nitrobenzene-d5 (S)43-123
72.078.44-Terphenyl-d14 (S)49-151
66.471.32,4,6-Tribromophenol (S)31-144
21.323.4Phenol-d5 (S)10-63
Page 6 of 6Date:09/15/2023 06:08 PM
Page 14 of 16
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-251-0013
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.1C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:09/08/2023 15:16:47
Special precautions or instructions included?
Comments:
Page 15 of 16
Page 16 of 16