MO-28920_48124_CA_MMPE_20231215_Ruscho 4

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
December 15, 2023

Mr. Ryan Mills
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Mobile Multi-Phase Extraction Report
October-November 2023
Former Rushco Food Store #4
1901 West Innes Street
Salisbury, Rowan County
North Carolina
Facility ID Number: 0-00-0000030414
Incident Number: 48124
GRI Project Number: 5721

Dear Mr. Mills,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Sam McKay at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Joey Rusher; Rusher Oil Company, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Mobile Multi-Phase Extraction Report
October – November, 2023
Former Rushco Food Store #4
1901 West Innes Street
Salisbury, Rowan County
North Carolina
Facility ID Number: 0-00-0000030414
Incident Number: 48124
GRI Project Number: 5721

Prepared for:

Mr. Joey Rusher
Rusher Oil Company, Inc.
Post Office Box 1483
Salisbury, North Carolina 28145

December 15, 2023

Samuel L. McKay, III, P.G.
Project Manager
Eric M. Eubanks, P.G.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Mobile Multi-Phase Extraction Report
Prepared on: December 15, 2023 Former Rushco Food Store #4
Project Manager: Samuel L. McKay, III, P.G. GRI Project No. 5721
i
EXECUTIVE SUMMARY
Former Rushco Food Store #4 is located at 1901 West Innes Street in Salisbury, Rowan County, North
Carolina. The property operates as a petroleum retail facility and convenience store. During due diligence
activities conducted in October 2021, reportable soil violations were identified at the site, and an LSA was
required by NCDEQ. There are two 10,000-gallon gasoline USTs and one 7,500-gallon gasoline UST
currently in use at the site with three associated gasoline dispensers. The surrounding properties are
commercial, residential, and institutional. According to the information determined during receptor
survey activities, no water supply wells were identified within 1,500 feet of the site. Public water is
available to the site and surrounding properties within a 1,500-foot radius of the site.

A MMPE event was conducted at the site between October 9 and October 13, 2023, on monitoring wells
MW-1, MW-4, and MW-6. A total of 3,960 gallons of affected ground water was recovered during the
MMPE event. No measurable free product was recovered during this MMPE event. No free product was
observed in any of the vacuum wells or observation wells. The average fluid recovery rate was 41.25
gallons per hour. Based on mass-removal calculations an additional 507.77 pounds or 82.54 gallons of
vapor phase hydrocarbons were removed at an average rate of 0.86 gallons per hour.

Based on this information, the risk classification for the site should remain intermediate risk. MMPE
events should continue to be conducted at the site until contaminant concentrations are below the GCLs.
Semi-annual ground water monitoring should continue at the site. The next sampling event is tentatively
scheduled for May 2024.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Mobile Multi-Phase Extraction Report
Prepared on: December 15, 2023 Former Rushco Food Store #4
Project Manager: Samuel L. McKay, III, P.G. GRI Project No. 5721
ii
SITE INFORMATION
1. Site Identification
 Former Rushco Food Store #4 (Facility ID 0-00-0000030414)
 Incident Number 48124 – Intermediate Risk (I115D)
 Location of Source Area: 1901 West Innes Street
Salisbury, NC 28056
Rowan County
35.2141990°N, 81.1334670°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
Sampson Bladen Oil Company, Inc.
510 Commerce Street
Clinton, NC 28329
Email Unknown
[phone]

UST/AST Operator
Sampson Bladen Oil Company, Inc.
510 Commerce Street
Clinton, NC 28329
Email Unknown
[phone]

Property Owner
Sampson Bladen Oil Company, Inc.
510 Commerce Street
Clinton, NC 28329
Email Unknown
[phone]

Property Occupant
Han-Dee Hugo’s #225
1901 West Innes Street
Salisbury, NC 28144
Email Unknown
[phone]

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 28217
State Cert. Nos. 37735 and 402
[phone]
3. Information about Release
 Release was discovered on October 20, 2021
 An unknown amount of product was released from the leaking UST System
 Two (2) 10,000-gallon gasoline USTs, one (1) 7,500-gallon gasoline UST, and associated pumps
and product piping are active at the site

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Mobile Multi-Phase Extraction Report
Prepared on: December 15, 2023 Former Rushco Food Store #4
Project Manager: Samuel L. McKay, III, P.G. GRI Project No. 5721
iii
ACRONYMS
ACM: Asbestos Containing Materials
AES: Advanced Environmental Services, Inc.
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Mobile Multi-Phase Extraction Report
Prepared on: December 15, 2023 Former Rushco Food Store #4
Project Manager: Samuel L. McKay, III, P.G. GRI Project No. 5721
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 MMPE EVENT ..........................................................................................................................1
3.0 CONCLUSIONS .........................................................................................................................3
4.0 LIMITATIONS ...........................................................................................................................3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Well Construction and Gauging Information
Table 4: Summary of MMPE Sample Analytical Results
Table 5: Free Product Recovery Results
Table 6: Free Product Recovery Event Information
Table 7: Free Product Recovery Cost Summary

APPENDICES
Appendix A: State Correspondence
Appendix B: Laboratory Analytical Reports
Appendix C: MMPE Report and Disposal Manifest

Certification:
I, Samuel L. McKay, III, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The certification
numbers of the corporation are C-127 and C-2727, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Mobile Multi-Phase Extraction Report
Prepared on: December 15, 2023 Former Rushco Food Store #4
Project Manager: Samuel L. McKay, III, P.G. GRI Project No. 5721
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the October 2023 MMPE event and the November 2023 ground water sampling
event at the Former Rushco Food Store #4 site, located at 1901 West Innes Street in Salisbury, Rowan
County, North Carolina. A topographic map of the general site location and the surrounding area is
included as Figure 1. These activities were conducted in accordance with GRI Proposal No. 23-486, which
was submitted to the NCDEQ on August 2, 2023, and was approved as Task Authorization No. 48124-4 on
August 3, 2023. State correspondence is included as Appendix A.

The site is currently owned by Sampson Bladen Oil Company, Inc. and is operated by Han-Dee Hugo as a
petroleum retail facility and convenience store. Two 10,000-gallon gasoline USTs, one 7,500-gallon
gasoline UST, and associated pumps and product piping are active at the site. UST owner/operator
information and UST system information are included as Table 1 and Table 2, respectively. The Registered
Tank Report is shown below:

Seven Type II monitoring wells (MW-1 through MW-7) and one Type III monitoring well (TW-1) were
installed at the site during previous ground water assessment activities. A Site Map showing the locations
of the monitoring wells and the structures on-site is included as Figure 2.
2.0 MMPE EVENT
An MMPE event was conducted at the site by AES under the supervision of GRI beginning on October 9,
2023, and ending on October 13, 2023. Monitoring wells MW-1, MW-4, and MW-6 were used as
extraction wells during the October 2023 MMPE event. The MMPE equipment included a liquid ring
pump, a 6,000-gallon capacity tanker, flexible vacuum hoses, 6-inch diameter discharge stack, 1.5-inch
diameter PVC stinger pipes and associated couplings and pipe fittings to manifold to three wells
simultaneously. The MMPE system was rated for 25” Hg at 280 CFM. All extraction wells (MW-1, MW-4,
and MW-6) were gauged and sampled prior to the start of the event. Free product was not observed

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Mobile Multi-Phase Extraction Report
Prepared on: December 15, 2023 Former Rushco Food Store #4
Project Manager: Samuel L. McKay, III, P.G. GRI Project No. 5721
2
during MMPE activities. Samples were collected prior to the start of the MMPE and submitted for
laboratory analysis of VOCs using EPA Method 602. Elevated concentrations of benzene, toluene,
ethylbenzene, xylenes, MTBE, naphthalene, and IPE were reported in the ground water samples collected
from MW-1, MW-4, and MW-6. The stinger pipe depths ranged from 24 feet to 26 feet in MW-1, MW-4,
and MW-6 over the course of the event. Well construction and gauging information is presented in Table
3. A summary of the MMPE sample analytical results is included in Table 4. A copy of the laboratory
analytical report is included as Appendix B.

Monitoring wells MW-1, MW-4, and MW-6 were each vacuumed continuously for the 96-hour event.
During the event, measurements of relative humidity, temperature, vacuum, exhaust velocity and off-gas
concentrations were recorded at the discharge stack a minimum of two times per 24-hour period. Vacuum
at the extraction wells ranged from 16 to 17 in. Hg. System vacuum ranged from 22 to 23 in. Hg. The
effluent velocity ranged from 1,100 to 1,150 feet per minute. The system temperature ranged from 120
to 136°F and relative humidity ranged from 44.0 to 60.0 percent. The VOC off-gas concentration ranged
from 8,800 ppm to 18,000 ppm during the event. No free product was measured in any of the wells
associated with the MMPE event. A summary of the gauging data obtained before start up and at the
conclusion of the MMPE event is presented in Table 5. A copy of the MMPE report and calculations is
included as Appendix B. A summary of the gauging data for the October 2023 MMPE event is listed below:
Well ID
Product Thickness
before Recovery
(feet)
Product Thickness
after Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of Product
Recovered as Liquid
(gallons)
MW-1 0.00 0.00
6,202 0.00 MW-2 0.00 0.00
MW-9 0.00 0.00

The results of the MMPE event indicate that a total of 3,960 gallons of liquids were removed during the
event. Of the total liquids extracted, no measurable free product was removed during the event. Based
on 96 hours of operation, the average liquid recovery rate was 41.25 gallons per hour. Based on mass-
removal calculations, an additional 507.77 pounds or 82.54 gallons of vapor phase hydrocarbons were
removed. Based on 96 hours of operation, an average of 0.86 gallons of vapor phase hydrocarbons were
removed per hour by the MMPE system. A summary of free product recovery data is included in Table 5.
Summaries of MMPE event information and cost analysis are provided in Tables 6 and 7, respectively. At
the conclusion of the MMPE event, all wastewater was transported to a permitted facility for disposal.
Copies of the disposal manifests are included in Appendix C. A summary of the free product recovery data
from the October 2023 event is listed below:
Well ID
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered
as Liquid
(gallons)
Total
Amount of
Product
Recovered
(gallons)
MW-1
1,119 48.7 12,067 82.54 3,960 0.00 82.54 MW-4
MW-6
Totals to Date 82.54 3,960 0.00 82.54

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Mobile Multi-Phase Extraction Report
Prepared on: December 15, 2023 Former Rushco Food Store #4
Project Manager: Samuel L. McKay, III, P.G. GRI Project No. 5721
3

Approximately 30 days after the conclusion of the MMPE, ground water samples were collected from
MW-1, MW-4, and MW-6. The concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE,
naphthalene, TAA, TBA, 2-hexanone, isopropylbenzene, IPE, MIBK, n-propylbenzene, styrene, 1,2,4-
trimethylbenzene, and/or 1,3,5-trimethylbenzene reported in the ground water samples collected from
MW-1, MW-4, and MW-6 exceeded the MACs. The reported concentrations of benzene and MTBE
reported in the ground water sample collected from MW-4 exceeded the GCLs. Free product was not
observed at the site. In general, contaminant concentrations in ground water were reduced after the
MMPE. A summary of the post-MMPE sample analytical results is included in Table 4. A copy of the
laboratory analytical report is included as Appendix B.

Based on these results, the MMPE was successful at removing petroleum contamination from the site.
3.0 CONCLUSIONS
 An MMPE event was conducted at the site from October 9 to October 13, 2023 on MW-1, MW-4,
and MW-6.
 A total of 3,960 gallons of affected ground water were recovered during the MMPE event. At the
conclusion of the event, no free product was measured in any of the wells associated with the
MMPE event. The average liquid recovery rate was 41.25 gallons per hour. An additional 82.54
gallons of vapor phase hydrocarbons were removed at an average rate of 0.86 gallons per hour.
 Based on this information, the risk classification for the site should remain intermediate risk.
MMPE events should continue to be conducted at the site until contaminant concentrations are
below the GCLs.
4.0 LIMITATIONS
This report has been prepared for the exclusive use of Rusher Oil Company, Inc. for specific application to
the referenced site in Rowan County, North Carolina. The assessment was conducted based on the scope
of work and level of effort desired by the NCDEQ and with resources adequate only for that scope of work.
Our findings have been developed in accordance with generally accepted standards of environmental
practices in the State of North Carolina, available information, and our professional judgment. No other
warranty is expressed or implied.

The data that is presented in this report is indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from this data.

FIGURES
SITE LOCATION
Figure 1
Site Location
Rushco Food Store 4
1901 West Innes Street
Salisbury, North Carolina
Rowan County
Incident No. 48124
GRI Project No. 5721
500 M
2000 FT
Date: 02/12/2022 Location: 35.686822° N -80.483554° W
D
a
d

TABLES
UST ID Number 1-3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 & 2 Facility ID Number
Owner or Operator?
Owner/Operator
Address Telephone Number
Unknown Unknown
00-0-00000030414
Name of Owner or Operator Dates of Ownership / Operation
Unknown 09/26/1969 - 09/26/1971
Address Telephone Number
P.O. Box 1483, Salisbury, NC, 28145 704-633-3211
00-0-00000030414
Name of Owner or Operator Dates of Ownership / Operation
Rusher Oil Company, Inc.08/17/2004 - 11/10/2021
Address Telephone Number
Unknown Unknown
00-0-00000030414
Name of Owner or Operator Dates of Ownership / Operation
Unknown 09/26/1971 - 08/17/2004
00-0-00000030414
TABLE 1
UST OWNER/OPERATOR INFORMATION
RUSHCO #4 (INCIDENT NO. 48124)
P.O. Box 469, Clinton, NC 28328 910-862-3197
Name of Owner or Operator Dates of Ownership / Operation
Sampson-Bladen Oil Co.11/10/2021 - present
Address Telephone Number
Page 1 of 1
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline,
Gas Mix NA 10,000 9/26/1969 Single Wall Steel Unknwon Single Wall FRP Current Yes
2 Gasoline,
Gas Mix NA 10,000 9/26/1969 Single Wall Steel Unknwon Single Wall FRP Current No
3 Gasoline,
Gas Mix NA 7,500 9/26/1971 Single Wall Steel Unknwon Single Wall FRP Current No
TABLE 2
UST SYSTEM INFORMATION
RUSHCO #4 (INCIDENT NO. 48124)
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
Facility ID #: 00-0-0000030414Date: 02/10/22
Page 1 of 1
Facility ID #: 00-0-0000030414
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
03/14/22 NM 23.73 ---NM
03/01/23 23.88 ---76.12
08/24/23 22.98 ---77.02
10/09/23 23.72 ---76.28
10/13/23 27.45 ---72.55
11/16/23 24.69 ---75.31
03/01/23 25.35 ---74.56
08/24/23 23.34 ---76.57
10/09/23 25.05 ---74.86
03/01/23 23.96 ---75.96
08/24/23 23.01 ---76.91
10/09/23 23.68 ---76.24
03/01/23 23.51 ---76.02
08/24/23 22.59 ---76.94
10/09/23 23.32 ---76.21
10/13/23 25.68 ---73.85
11/16/23 24.37 ---75.16
MW-5 08/11/23 08/24/23 20 20-30 30 100.12 25.38 ---74.74
08/24/23 23.48 ---76.62
10/09/23 24.22 ---75.88
10/13/23 25.35 ---74.75
11/16/23 25.14 ---74.96
MW-7 08/11/23 08/24/23 20 20-30 30 99.37 21.96 ---77.41
03/01/23 23.87 ---76.25
08/24/23 22.90 ---77.22
Notes:
• ft BGS : feet below ground surface.
• NM: Not measured.
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
RUSHCO #4 (INCIDENT NO. 48124)
Date: 12/11/23
15 15-35 35
5550-55
20 20-30 30
20
100.12
100.00
99.91
TW-1
MW-1
MW-2
MW-4
MW-6
MW-3
02/21/23
03/14/22
02/20/23
02/20/23
08/11/23
02/20/23
50
20 20-30 30 100.10
20-30 30 99.92
20 20-30 30 99.53
Page 1 of 1
Date: 12/11/23 Facility ID #: 00-0-0000030414
EPA 504.1 SW846
6010D
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 6,000 40 10 0.4 40 70 70 5 100 70 70 400 400 0.02 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 6,000,000 40,000 10,000 400 40,000 30,500 70,000 5,000 100,000 26,100 70,000 28,500 24100 50 15,000 NE NE NE
03/14/22 5,710 11,300 4,200 13,700 3,740 829 *17,500 5,210 J **130 J 276 J **411 J *2,470 707 0.025 74.7 10,800 <35 5,860
03/01/23 6,290 6,390 2,420 6,320 4,070 543 J <1,800 10,700 3,220 J 9.94 186 101 300 <3.30 132 281 48.6 1,710 381 NR NR NR NR NR
08/24/23 13,000 30,800 3,220 16,500 11,300 1,150 3,020 41,400 17,600 <15.0 238 107 602 <33.0 151 296 71.8 2,170 546 NR NR NR NR NR
10/09/23 11,600 24,900 2,810 15,300 13,100 769 NR NR NR NR NR NR 674 NR NR NR NR NR NR NR NR NR NR NR
11/16/23 5,000 8,220 2,720 10,400 5,020 1,390 3,140 7,150 J 4,690 <15.0 197 116 242 <33.0 129 340 71.7 2,370 622 NR NR NR NR NR
03/01/23 91.1 60.2 971 657 458 662 <18.0 348 512 <1.50 <3.80 80.6 47.6 7.14 J 14.1 190 32.8 867 39.8 <0.0222 <2 2,180 1,930 4,320
08/24/23 161 66.0 43.9 J 44.2 J 713 <47.0 <180 1,000 <35.0 <15.0 <38.0 <18.0 51.3 <33.0 <7.80 30.2 J <22.0 45.4 J <18.0 NR NR NR NR NR
03/01/23 3,430 21,400 4,490 19,100 32.7 918 <18.0 196 <16.0 <1.50 <3.80 104 9.03 <3.30 <0.780 296 170 2,210 547 <0.0206 <2 26,400 15,200 5,660
08/24/23 1,340 13,400 4,170 17,800 16.5 1,130 <1.80 440.50 E 11.4 <0.150 <0.380 117 3.91 <0.330 <0.078 330 163 2,860 701 NR NR NR NR NR
03/01/23 26,900 54,700 4,130 19,600 32,400 967 6,600 J 23,700 4,670 J <1.50 233 100 1,190 <3.30 <0.780 307 155 2,450 588 0.810 3 J 51,400 15,600 5,690
08/24/23 22,100 46,900 3,180 18,600 15,400 892 1,590 5,310 1,420 <15.0 <38.0 84.9 686 <33.0 <7.80 234 135 2,060 552 NR NR NR NR NR
10/09/23 19,400 43,200 3,480 20,100 13,800 635 NR NR NR NR NR NR 650 NR NR NR NR NR NR NR NR NR NR NR
11/16/23 15,800 30,100 2,050 11,300 20,300 902 4,260 10,600 3,800 <15.0 175 67.0 697 <33.0 84.9 J 182 89.3 1,430 392 NR NR NR NR NR
MW-5 08/24/23 760 1,150 2,560 10,300 7,580 1,310 495 J 858 J 877 J <15.0 <38.0 130 232 <33.0 <7.80 372 102 2,740 668 <0.0207 2 J 5,650 5,990 10,300
08/24/23 4,530 27,400 3,900 17,200 <14.0 1,080 831 J 2,260 <160 <15.0 <38.0 101 135 <33.0 <7.80 308 206 2,260 551 <0.0207 6 33,100 14,900 7,430
10/09/23 3,930 19,900 3,900 17,000 356 757 NR NR NR NR NR NR 154 NR NR NR NR NR NR NR NR NR NR NR
11/16/23 4,680 28,500 4,340 19,000 369 1,490 <180 4,660 <160 <15.0 <38.0 119 118 <33.0 <7.80 378 229 2,800 741 NR NR NR NR NR
MW-7 08/24/23 1.36 3.11 0.668 2.75 30.0 <0.470 18.2 24.8 14.4 <0.150 <0.380 <0.180 9.05 0.454 J <0.078 <0.190 <0.220 0.769 0.256 J <0.0208 8 89.2 26.0 <4.02
03/01/23 0.508 3.31 1.21 5.16 0.496 J <0.470 32.1 <1.90 <1.60 <0.150 <0.380 <0.180 <0.500 <0.330 <0.078 <0.190 <0.220 1.40 0.461 J <0.0208 <2 <11.5 37.0 J 13.9 J
08/24/23 <0.180 <0.220 <0.170 0.211 J <0.140 <0.470 5.58 J <1.90 <1.60 <0.150 <0.380 0.222 J <0.500 <0.330 <0.078 <0.190 <0.220 <0.190 <0.180 NR NR NR NR NR
03/14/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 *NR NR **<0.13 <0.13 **<0.13 *<0.13 <0.13 NR NR NR NR NR
03/01/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.80 NR NR <0.150 <0.380 <0.180 <0.500 0.336 J <0.078 <0.190 <0.220 <0.190 <0.180 NR NR NR NR NR
08/24/23 <0.180 <0.220 <0.170 <0.21 <0.140 <0.470 <1.80 NR NR <0.150 <0.380 <0.180 <0.500 <0.330 <0.078 <0.190 <0.220 <0.190 <0.180 NR NR NR NR NR
10/09/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR NR NR NR NR <0.500 NR NR NR NR NR NR NR NR NR NR NR
11/16/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 2.51 J NR NR <0.150 <0.380 <0.180 <0.500 <0.330 <0.078 <0.190 <0.220 <0.190 <0.180 NR NR NR NR NR
Notes:
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• 2B Standard: North Carolina surface water standards for Class C waters specified in T15A NCAC 2B.0200 or EPA Nathional Criteria.
• < : Less than the method detection limit specified in the laboratory report.
• GCL: Gross contamination level.
• Concentrations in bold face type indicate the MAC was below the reported concentration.
• Underlined results indicate 10 times the 2B Standards were below the reported concentrations.
• Results in italics indicate the GCLs were below the reported concentrations.
• J: Estimated value.
• NE: Not established.
• S: Toxicity exceeds solubility, no visible sheen or free product in water or on sediment or shoreline per 15A NCAC 02B .0211 & .0220
• NR: Not reported.
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RUSHCO #4 (INCIDENT NO. 48124)
Analytical Method
SM 6200B MADEP VPH
Contaminant of Concern

Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
t
a
l

X
y
l
e
n
e
s
C9
-
C
1
0

A
r
o
m
a
t
i
c
s
Le
a
d
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
St
y
r
e
n
e
Me
t
h
y
l

i
s
o
b
u
t
y
l

k
e
t
o
n
e

(M
I
B
K
)
Ac
e
t
o
n
e
1,
2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
2-
H
e
x
a
n
o
n
e
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
• Refer to laboratory report for other detectable concentrations which did not exceed the MACs.
MAC (μg/l)
GCL (μg/l)
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
TW-1
MW-1
MW-4
MW-6
Trip Blank
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
MW-3
MW-2
Date: 12/11/23
Method of Measurement:
Well ID
Product Type
(gas, diesel,
etc.)
Date of Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product
Thickness
before
Recovery
(feet)
Product
Thickness
after
Recovery
(feet)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
MW-1 ------
MW-2 ------
MW-9 ------
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• **: No free product was observed during initial gauging event; however, free product entered the well during purging activities.
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and/or Field Notes).
0.00
TABLE 5
FREE PRODUCT RECOVERY RESULTS
RUSHCO #4 (INCIDENT NO. 48124)
Facility ID#: 0-030414
Interface probe at top-of-casing
Gasoline 10/09/23 - 10/13/23 MMPE 2 3,960
Page 1 of 1
Date: 12/11/23
MW-1
MW-4
MW-6
82.54 3,960 0 82.54
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.15
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid (gallons)
Total Amount
of Product
Recovered
(gallons)
TABLE 6
FREE PRODUCT RECOVERY EVENT INFORMATION
RUSHCO #4 (INCIDENT NO. 48124)
Facility ID #: 0-030414
Well ID Date (mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
10/09/23 - 10/13/23 MMPE 1,119 48.7 12,067 82.54 3,960 0 82.54
Totals
SUMMARY OF FLUID REMOVAL
Current Event 4,042.54 82.54
Total To Date 4,042.54 82.54
Page 1 of 1
Date: 12/11/23 Facility ID #: 0-030414
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Free Product plus
Ground Water
Recovered
(gallons)
Cost of Free
Product Recovery
Event
Cost Per Gallon
(total fluids)Comments
MW-1, MW-4 and
MW-6 MMPE 10/09/23 -
10/13/23 4,042.54 $11,352.00 $2.81 Cost per gallon for the event is based on a total volume
of 4,042.54 gallons of free product and water.
4,042.54 $11,352.00 $2.81
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
TABLE 7
FREE PRODUCT RECOVERY COST SUMMARY
RUSHCO #4 (INCIDENT NO. 48124)
TOTAL (to date)
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, MMPE sampling, MMPE sampling analytical, report
preparation (pre-2015 only) and project management.
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence
Site Name City / County /Rowan Incident #48124
Resp Pty Name / Contact Incident Mgr Region MOR
(Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #3
Consultant / Project Mgr Sam McKay
Telephone / Fax Number Task Authorization Number:4 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I-115-D RRA Date:5/11/2022
Proposal# / Scope Dates % Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
Task #Lab /
SubCode RO

A
u
t
h
Proposed
Rate/Price
(Consultant)CO

A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
4.031 6 /wells Y $110.00 Y $660.00 $660.00 /
4.090 #220 3 /samples Y $40.00 Y $120.00 $120.00 /
4.090 #240 3 /samples Y $94.00 Y $282.00 $282.00 /
4.090 #271 2 /samples Y $66.00 Y $132.00 $132.00 /
4.091 2 /shipments Y $60.00 Y $120.00 $120.00 /
6.022 1 /report Y $500.00 Y $500.00 $500.00 /
7.201 8 /hours Y $93.00 Y $744.00 $744.00 /
7.420 1 /event Y $2,500.00 Y $2,500.00 $2,500.00 /
7.420 1 /event Y $1,500.00 Y $1,500.00 $1,500.00 /
7.420 1 /event Y $2,500.00 Y $2,500.00 $2,500.00 /
7.420 5000 /gallons Y $0.35 Y $1,750.00 $1,750.00 /
12.030 4 /nights Y $157.00 Y $628.00 $628.00 /
12.050 3 /trips Y $250.00 Y $750.00 $750.00 /
12.055 3 /trips Y $50.00 Y $150.00 $150.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed
TOTAL:$12,336.00 $12,336.00 TOTAL:
Total Standard Costs (Not Third Party)$12,336.00 $12,336.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:8/2/23 by:(PM)(Reserved for RO)
RO Review:8/3/23 by:(IM)Joint UST Preapproval Confirmed By:
CO Review:8/3/23 by:(STF)RP or Designee Receipt Confirmation By:
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
DWM/UST ePATA 4/1/2022
SM
Proposed
Units / Type
(Consultant)
Ryan Mills
ActiveYES
23-486 October 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
100.00%
[e-mail]
Rusher Oil Company Joey Rusher
Geological Resources, Inc.
Salisbury
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
Rushco 4 (former)
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATArequest
as a "Change Order" in the provided space above priorto conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have beenwithin12monthsofthecompletiondateoftheFIRSTcompletedtasktoremainwithintheStatuteofLimitations.All ePATAs submitted within a claim are closed withthatandmaynot be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimed
below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
RCM
LP
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality -Division of Waste Management
8/3/2023
8/3/2023
5721 Received AUG 03 2023

APPENDIX B
Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/17/2023
Geological Resources, Inc. Sam McKay
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-282-0016 Client Project Description: Rushco 4 (Former)
GRI #5721
Dear Sam McKay:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/9/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 13
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-282-0016
Page 2 of 13
Report Number:
Sample Summary Table
Client Project Description:
23-282-0016
Rushco 4 (Former)
GRI #5721
Lab No Client Sample ID Matrix Date Collected Date Received
10/09/2023 12:03Aqueous 97190 MW-1 10/09/2023 14:48
10/09/2023 12:25Aqueous 97191 MW-4 10/09/2023 14:48
10/09/2023 12:15Aqueous 97192 MW-6 10/09/2023 14:48
10/09/2023 10:50Aqueous 97193 Trip Blank 10/09/2023 14:48
Page 3 of 13
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-282-0016
Report Limit
Project:Rushco 4 (Former)
V 97190MW-1
11600 10/13/2023 06:476200BBenzeneµg/L 180
674 10/12/2023 09:486200BDi-Isopropyl Ether (DIPE)µg/L 50.0
2810 10/12/2023 09:486200BEthylbenzeneµg/L 17.0
13100 10/13/2023 06:476200BMethyl tert-butyl ether (MTBE)µg/L 140
769 10/12/2023 09:486200BNaphthaleneµg/L 47.0
24900 10/13/2023 06:476200BTolueneµg/L 220
5040 10/12/2023 09:486200Bo-Xylene µg/L 21.0
10300 10/12/2023 09:486200Bm,p-Xylene µg/L 42.0
15300 10/12/2023 09:486200BXylene (Total)µg/L 21.0
V 97191MW-4
19400 10/13/2023 07:126200BBenzeneµg/L 180
650 10/12/2023 10:136200BDi-Isopropyl Ether (DIPE)µg/L 50.0
3480 10/12/2023 10:136200BEthylbenzeneµg/L 17.0
13800 10/13/2023 07:126200BMethyl tert-butyl ether (MTBE)µg/L 140
635 10/12/2023 10:136200BNaphthaleneµg/L 47.0
43200 10/13/2023 07:126200BTolueneµg/L 220
6700 10/12/2023 10:136200Bo-Xylene µg/L 21.0
13400 10/12/2023 10:136200Bm,p-Xylene µg/L 42.0
20100 10/12/2023 10:136200BXylene (Total)µg/L 21.0
V 97192MW-6
3930 10/12/2023 10:376200BBenzeneµg/L 18.0
154 10/12/2023 10:376200BDi-Isopropyl Ether (DIPE)µg/L 50.0
3900 10/12/2023 10:376200BEthylbenzeneµg/L 17.0
356 10/12/2023 10:376200BMethyl tert-butyl ether (MTBE)µg/L 14.0
757 10/12/2023 10:376200BNaphthaleneµg/L 47.0
19900 10/13/2023 08:006200BTolueneµg/L 220
5200 10/12/2023 10:376200Bo-Xylene µg/L 21.0
11800 10/12/2023 10:376200Bm,p-Xylene µg/L 42.0
17000 10/12/2023 10:376200BXylene (Total)µg/L 21.0
Page 4 of 13
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-282-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 10/09/2023
Rushco 4 (Former)
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:MW-1
97190 Matrix:
10/9/2023 12:03
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38961 10/11/23 14:00 V39055 10/12/23 09:00
11600 µg/L 180 500Benzene 1000 10/13/23 06:47 V39056MSA
674 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 10/12/23 09:48 V38962MSA
2810 µg/L 17.0 50.0Ethylbenzene 100 10/12/23 09:48 V38962MSA
13100 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 10/13/23 06:47 V39056MSA
769 µg/L 47.0 100Naphthalene 100 10/12/23 09:48 V38962MSA
24900 µg/L 220 500Toluene 1000 10/13/23 06:47 V39056MSA
5040 µg/L 21.0 50.0o-Xylene 100 10/12/23 09:48 V38962MSA
10300 µg/L 42.0 100m,p-Xylene 100 10/12/23 09:48 V38962MSA
15300 µg/L 21.0 50.0Xylene (Total)100 10/12/23 09:48 V38962
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%10/12/23 09:48100 MSA V38962
Surrogate: Dibromofluoromethane 99.2 Limits: 70-130%10/12/23 09:48100 MSA V38962
Surrogate: 1,2-Dichloroethane - d4 94.0 Limits: 70-130%10/12/23 09:48100 MSA V38962
Surrogate: Toluene-d8 102 Limits: 70-130%10/12/23 09:48100 MSA V38962
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%10/13/23 06:471000 MSA V39056
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%10/13/23 06:471000 MSA V39056
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%10/13/23 06:471000 MSA V39056
Surrogate: Toluene-d8 99.8 Limits: 70-130%10/13/23 06:471000 MSA V39056
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 5 of 13
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-282-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 10/09/2023
Rushco 4 (Former)
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:MW-4
97191 Matrix:
10/9/2023 12:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38961 10/11/23 14:00 V39055 10/12/23 09:00
19400 µg/L 180 500Benzene 1000 10/13/23 07:12 V39056MSA
650 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 10/12/23 10:13 V38962MSA
3480 µg/L 17.0 50.0Ethylbenzene 100 10/12/23 10:13 V38962MSA
13800 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 10/13/23 07:12 V39056MSA
635 µg/L 47.0 100Naphthalene 100 10/12/23 10:13 V38962MSA
43200 µg/L 220 500Toluene 1000 10/13/23 07:12 V39056MSA
6700 µg/L 21.0 50.0o-Xylene 100 10/12/23 10:13 V38962MSA
13400 µg/L 42.0 100m,p-Xylene 100 10/12/23 10:13 V38962MSA
20100 µg/L 21.0 50.0Xylene (Total)100 10/12/23 10:13 V38962
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%10/12/23 10:13100 MSA V38962
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%10/12/23 10:13100 MSA V38962
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%10/12/23 10:13100 MSA V38962
Surrogate: Toluene-d8 103 Limits: 70-130%10/12/23 10:13100 MSA V38962
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/13/23 07:121000 MSA V39056
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%10/13/23 07:121000 MSA V39056
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%10/13/23 07:121000 MSA V39056
Surrogate: Toluene-d8 101 Limits: 70-130%10/13/23 07:121000 MSA V39056
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 6 of 13
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-282-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 10/09/2023
Rushco 4 (Former)
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:MW-6
97192 Matrix:
10/9/2023 12:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38961 10/11/23 14:00 V39055 10/12/23 09:00
3930 µg/L 18.0 50.0Benzene 100 10/12/23 10:37 V38962MSA
154 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 10/12/23 10:37 V38962MSA
3900 µg/L 17.0 50.0Ethylbenzene 100 10/12/23 10:37 V38962MSA
356 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 10/12/23 10:37 V38962MSA
757 µg/L 47.0 100Naphthalene 100 10/12/23 10:37 V38962MSA
19900 µg/L 220 500Toluene 1000 10/13/23 08:00 V39056MSA
5200 µg/L 21.0 50.0o-Xylene 100 10/12/23 10:37 V38962MSA
11800 µg/L 42.0 100m,p-Xylene 100 10/12/23 10:37 V38962MSA
17000 µg/L 21.0 50.0Xylene (Total)100 10/12/23 10:37 V38962
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/12/23 10:37100 MSA V38962
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%10/12/23 10:37100 MSA V38962
Surrogate: 1,2-Dichloroethane - d4 92.6 Limits: 70-130%10/12/23 10:37100 MSA V38962
Surrogate: Toluene-d8 102 Limits: 70-130%10/12/23 10:37100 MSA V38962
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%10/13/23 08:001000 MSA V39056
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%10/13/23 08:001000 MSA V39056
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%10/13/23 08:001000 MSA V39056
Surrogate: Toluene-d8 99.2 Limits: 70-130%10/13/23 08:001000 MSA V39056
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 7 of 13
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-282-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 10/09/2023
Rushco 4 (Former)
Report Date : 10/17/2023
Sample ID :
Lab No :
Sampled:Trip Blank
97193 Matrix:
10/9/2023 10:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38961 10/11/23 14:00
<0.180 µg/L 0.180 0.500Benzene 1 10/12/23 03:18 V38962MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 10/12/23 03:18 V38962MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 10/12/23 03:18 V38962MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 10/12/23 03:18 V38962MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 10/12/23 03:18 V38962MSA
<0.220 µg/L 0.220 0.500Toluene 1 10/12/23 03:18 V38962MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 10/12/23 03:18 V38962MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 10/12/23 03:18 V38962MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 10/12/23 03:18 V38962
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/12/23 03:181 MSA V38962
Surrogate: Dibromofluoromethane 99.4 Limits: 70-130%10/12/23 03:181 MSA V38962
Surrogate: 1,2-Dichloroethane - d4 96.8 Limits: 70-130%10/12/23 03:181 MSA V38962
Surrogate: Toluene-d8 102 Limits: 70-130%10/12/23 03:181 MSA V38962
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 8 of 13
Quality Control Data
23-282-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38962QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38961
Associated Lab Samples: 97190, 97191, 97192, 97193
LRB-V38961 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/12/23 02:540.5000.180<0.180µg/LBenzene
10/12/23 02:540.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
10/12/23 02:540.5000.170<0.170µg/LEthylbenzene
10/12/23 02:541.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
10/12/23 02:541.000.470<0.470µg/LNaphthalene
10/12/23 02:540.5000.220<0.220µg/LToluene
10/12/23 02:540.5000.210<0.210µg/Lo-Xylene
10/12/23 02:541.000.420<0.420µg/Lm,p-Xylene
10/12/23 02:544-Bromofluorobenzene (S)101 70-130
10/12/23 02:54Dibromofluoromethane (S)101 70-130
10/12/23 02:541,2-Dichloroethane - d4 (S)94.0 70-130
10/12/23 02:54Toluene-d8 (S)103 70-130
LCS-V38961 LCSD-V38961Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
23.6 11812124.220.0µg/LBenzene 70-130 2.5 20.0
22.3 11211322.620.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.3 20.0
23.1 11612023.920.0µg/LEthylbenzene 70-130 3.4 20.0
20.9 10598.019.620.0µg/LMethyl tert-butyl ether (MTBE)70-130 6.4 20.0
19.2 96.084.016.820.0µg/LNaphthalene 70-130 13.3 20.0
23.2 11612023.920.0µg/LToluene 70-130 2.9 20.0
23.0 11511923.820.0µg/Lo-Xylene 70-130 3.4 20.0
49.1 12312750.840.0µg/Lm,p-Xylene 70-130 3.4 20.0
10199.64-Bromofluorobenzene (S)70-130
99.4101Dibromofluoromethane (S)70-130
Page 1 of 3Date:10/17/2023 08:29 AM
Page 9 of 13
Quality Control Data
23-282-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38962QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38961
LCS-V38961 LCSD-V38961Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
95.692.01,2-Dichloroethane - d4 (S)70-130
102102Toluene-d8 (S)70-130
Page 2 of 3Date:10/17/2023 08:29 AM
Page 10 of 13
Quality Control Data
23-282-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V39056QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V39055
Associated Lab Samples: 97190, 97191, 97192
LRB-V39055 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/13/23 01:310.5000.180<0.180µg/LBenzene
10/13/23 01:311.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
10/13/23 01:310.5000.220<0.220µg/LToluene
10/13/23 01:314-Bromofluorobenzene (S)102 70-130
10/13/23 01:31Dibromofluoromethane (S)99.6 70-130
10/13/23 01:311,2-Dichloroethane - d4 (S)97.4 70-130
10/13/23 01:31Toluene-d8 (S)100 70-130
LCS-V39055 LCSD-V39055Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.4 10710721.420.0µg/LBenzene 70-130 0.0 20.0
21.9 11010520.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 4.6 20.0
21.1 10610621.220.0µg/LToluene 70-130 0.4 20.0
99.098.24-Bromofluorobenzene (S)70-130
10198.0Dibromofluoromethane (S)70-130
10398.61,2-Dichloroethane - d4 (S)70-130
100100Toluene-d8 (S)70-130
Page 3 of 3Date:10/17/2023 08:29 AM
Page 11 of 13
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-282-0016
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Caitlyn Cummins Date & Time:10/09/2023 16:08:05
Special precautions or instructions included?
Comments:
Page 12 of 13
Page 13 of 13

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/29/2023
Geological Resources, Inc. Sam McKay
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-321-0005 Client Project Description: Rushco 4 (Former)
GRI #5721
Dear Sam McKay:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/17/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 35
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-321-0005
Page 2 of 35
Report Number:
Sample Summary Table
Client Project Description:
23-321-0005
Rushco 4 (Former)
GRI #5721
Lab No Client Sample ID Matrix Date Collected Date Received
11/16/2023 10:02Aqueous 89722 MW-1 11/17/2023 11:03
11/16/2023 10:15Aqueous 89723 MW-4 11/17/2023 11:03
11/16/2023 10:25Aqueous 89724 MW-6 11/17/2023 11:03
11/16/2023Aqueous 89725 Trip Blank 11/17/2023 11:03
Page 3 of 35
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-321-0005
Report Limit
Project:Rushco 4 (Former)
V 89722MW-1
3140 11/22/2023 11:016200BAcetoneµg/L 180
5000 11/22/2023 11:016200BBenzeneµg/L 18.0
J38.1 11/22/2023 11:016200Bn-Butylbenzene µg/L 18.0
J20.9 11/22/2023 11:016200Bsec-Butyl benzene µg/L 20.0
J22.3 11/22/2023 11:016200BChloroformµg/L 22.0
242 11/22/2023 11:016200BDi-Isopropyl Ether (DIPE)µg/L 50.0
2720 11/22/2023 11:016200BEthylbenzeneµg/L 17.0
197 11/22/2023 11:016200B2-Hexanone µg/L 38.0
116 11/22/2023 11:016200BIsopropylbenzeneµg/L 18.0
1430 11/22/2023 11:016200BMethyl Ethyl Ketone (MEK)µg/L 71.0
5020 11/22/2023 11:016200BMethyl tert-butyl ether (MTBE)µg/L 14.0
129 11/22/2023 11:016200B4-Methyl-2-Pentanone µg/L 7.80
1390 11/22/2023 11:016200BNaphthaleneµg/L 47.0
340 11/22/2023 11:016200Bn-Propylbenzene µg/L 19.0
71.7 11/22/2023 11:016200BStyreneµg/L 22.0
4690 11/22/2023 11:016200Btert-Butyl Alcohol (TBA)µg/L 160
J715011/28/2023 14:116200Btert-Amyl Alcohol (TAA)µg/L 1900
8220 11/22/2023 11:016200BTolueneµg/L 22.0
2370 11/22/2023 11:016200B1,2,4-Trimethylbenzene µg/L 19.0
622 11/22/2023 11:016200B1,3,5-Trimethylbenzene µg/L 18.0
2810 11/22/2023 11:016200Bo-Xylene µg/L 21.0
7570 11/22/2023 11:016200Bm,p-Xylene µg/L 42.0
10400 11/22/2023 11:016200BXylene (Total)µg/L 21.0
V 89723MW-4
4260 11/22/2023 11:266200BAcetoneµg/L 180
15800 11/28/2023 14:376200BBenzeneµg/L 180
697 11/22/2023 11:266200BDi-Isopropyl Ether (DIPE)µg/L 50.0
2050 11/22/2023 11:266200BEthylbenzeneµg/L 17.0
175 11/22/2023 11:266200B2-Hexanone µg/L 38.0
67.0 11/22/2023 11:266200BIsopropylbenzeneµg/L 18.0
1930 11/22/2023 11:266200BMethyl Ethyl Ketone (MEK)µg/L 71.0
20300 11/28/2023 14:376200BMethyl tert-butyl ether (MTBE)µg/L 140
J84.9 11/22/2023 11:266200B4-Methyl-2-Pentanone µg/L 7.80
902 11/22/2023 11:266200BNaphthaleneµg/L 47.0
182 11/22/2023 11:266200Bn-Propylbenzene µg/L 19.0
89.3 11/22/2023 11:266200BStyreneµg/L 22.0
Page 4 of 35
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-321-0005
Report Limit
Project:Rushco 4 (Former)
V 89723MW-4
3800 11/22/2023 11:266200Btert-Butyl Alcohol (TBA)µg/L 160
10600 11/28/2023 14:376200Btert-Amyl Alcohol (TAA)µg/L 1900
J98.9 11/22/2023 11:266200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
30100 11/28/2023 14:376200BTolueneµg/L 220
1430 11/22/2023 11:266200B1,2,4-Trimethylbenzene µg/L 19.0
392 11/22/2023 11:266200B1,3,5-Trimethylbenzene µg/L 18.0
3660 11/22/2023 11:266200Bo-Xylene µg/L 21.0
7590 11/22/2023 11:266200Bm,p-Xylene µg/L 42.0
11300 11/22/2023 11:266200BXylene (Total)µg/L 21.0
V 89724MW-6
4680 11/22/2023 11:516200BBenzeneµg/L 18.0
J35.3 11/22/2023 11:516200Bn-Butylbenzene µg/L 18.0
118 11/22/2023 11:516200BDi-Isopropyl Ether (DIPE)µg/L 50.0
4340 11/22/2023 11:516200BEthylbenzeneµg/L 17.0
119 11/22/2023 11:516200BIsopropylbenzeneµg/L 18.0
369 11/22/2023 11:516200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1490 11/22/2023 11:516200BNaphthaleneµg/L 47.0
378 11/22/2023 11:516200Bn-Propylbenzene µg/L 19.0
229 11/22/2023 11:516200BStyreneµg/L 22.0
4660 11/22/2023 11:516200Btert-Amyl Alcohol (TAA)µg/L 190
28500 11/28/2023 15:026200BTolueneµg/L 220
2800 11/22/2023 11:516200B1,2,4-Trimethylbenzene µg/L 19.0
741 11/22/2023 11:516200B1,3,5-Trimethylbenzene µg/L 18.0
5770 11/22/2023 11:516200Bo-Xylene µg/L 21.0
13200 11/22/2023 11:516200Bm,p-Xylene µg/L 42.0
19000 11/22/2023 11:516200BXylene (Total)µg/L 21.0
V 89725Trip Blank
J2.51 11/22/2023 04:016200BAcetoneµg/L 1.80
J2.64 11/22/2023 04:016200BMethyl Ethyl Ketone (MEK)µg/L 0.710
Page 5 of 35

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Rushco 4 (Former) Lab Report Number: 23-321-0005
Date: 11/29/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: Bromomethane QC Batch No: V40525/V40524
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias. LCS and/or LCSD saw low recovery for this compound. CCV saw recovery within method parameters for this
compound. A low level standard at or below the MQL was run and saw recovery for this compound, indicating the ability to see appropriate recovery at the low end of instrumentation.
Analyte: Chloroethane
QC Batch No: V40525/V40524 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
LCS and/or LCSD saw low recovery for this compound. CCV saw recovery within method parameters for this compound. A low level standard at or below the MQL was run and saw recovery for this compound, indicating the
ability to see appropriate recovery at the low end of instrumentation.
Analyte: Chloromethane QC Batch No: V40525/V40524 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias. LCS and/or LCSD saw low recovery for this compound. CCV saw recovery within method parameters for this
compound. A low level standard at or below the MQL was run and saw recovery for this compound, indicating the ability to see appropriate recovery at the low end of instrumentation.
Analyte: Dichlorodifluoromethane QC Batch No: V40525/V40524 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
LCS and/or LCSD saw low recovery for this compound. CCV saw recovery within method parameters for this compound. A low level standard at or below the MQL was run and saw recovery for this compound, indicating the ability to see appropriate recovery at the low end of instrumentation. Analyte: Trichlorofluoromethane QC Batch No: V40525/V40524
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. LCS and/or LCSD saw low recovery for this compound. CCV saw recovery within method parameters for this compound. A low level standard at or below the MQL was run and saw recovery for this compound, indicating the ability to see appropriate recovery at the low end of instrumentation.
Page 6 of 35

Analyte: Vinyl acetate QC Batch No: V40662/V40524
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Vinyl chloride QC Batch No: V40525/V40524
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias. LCS and/or LCSD saw low recovery for this compound. CCV saw recovery within method parameters for this
compound. A low level standard at or below the MQL was run and saw recovery for this compound, indicating the ability to see appropriate recovery at the low end of instrumentation.

Page 7 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-1
89722 Matrix:
11/16/2023 10:02
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 11/22/23 11:01 6200BMSA
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%11/22/23 11:01100 MSA V40525
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%11/22/23 11:01100 MSA V40525
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%11/22/23 11:01100 MSA V40525
Surrogate: Toluene-d8 103 Limits: 70-130%11/22/23 11:01100 MSA V40525
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%11/28/23 14:111000 MSA V40662
Surrogate: Dibromofluoromethane 100 Limits: 70-130%11/28/23 14:111000 MSA V40662
Surrogate: 1,2-Dichloroethane - d4 93.6 Limits: 70-130%11/28/23 14:111000 MSA V40662
Surrogate: Toluene-d8 98.6 Limits: 70-130%11/28/23 14:111000 MSA V40662
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 8 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-1
89722 Matrix:
11/16/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
3140 µg/L 180 1000Acetone 100 11/22/23 11:01 V40525MSA
5000 µg/L 18.0 50.0Benzene 100 11/22/23 11:01 V40525MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 11/22/23 11:01 V40525MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 11/22/23 11:01 V40525MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 11/22/23 11:01 V40525MSA
<150 µg/L 150 500Bromoform 100 11/22/23 11:01 V40525MSA
<28.0 M µg/L 28.0 100Bromomethane 100 11/22/23 11:01 V40525MSA
38.1 J µg/L 18.0 50.0n-Butylbenzene 100 11/22/23 11:01 V40525MSA
20.9 J µg/L 20.0 50.0sec-Butyl benzene 100 11/22/23 11:01 V40525MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 11/22/23 11:01 V40525MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 11/22/23 11:01 V40525MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 11/22/23 11:01 V40525MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 11/22/23 11:01 V40525MSA
<43.0 M µg/L 43.0 100Chloroethane 100 11/22/23 11:01 V40525MSA
22.3 J µg/L 22.0 50.0Chloroform 100 11/22/23 11:01 V40525MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 11/22/23 11:01 V40525MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 11/22/23 11:01 V40525MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 11/22/23 11:01 V40525MSA
242 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 11/22/23 11:01 V40525MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 11/22/23 11:01 V40525MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 11/22/23 11:01 V40525MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 11/22/23 11:01 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 9 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-1
89722 Matrix:
11/16/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 11/22/23 11:01 V40525MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 11/22/23 11:01 V40525MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 11/22/23 11:01 V40525MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 11/22/23 11:01 V40525MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 11/22/23 11:01 V40525MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 11/22/23 11:01 V40525MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 11/22/23 11:01 V40525MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 11/22/23 11:01 V40525MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 11/22/23 11:01 V40525MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 11/22/23 11:01 V40525MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 11/22/23 11:01 V40525MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 11/22/23 11:01 V40525MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 11/22/23 11:01 V40525MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 11/22/23 11:01 V40525MSA
<4200 µg/L 4200 20000Ethanol 100 11/22/23 11:01 V40525MSA
2720 µg/L 17.0 50.0Ethylbenzene 100 11/22/23 11:01 V40525MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 11/22/23 11:01 V40525MSA
197 µg/L 38.0 1002-Hexanone 100 11/22/23 11:01 V40525MSA
116 µg/L 18.0 50.0Isopropylbenzene 100 11/22/23 11:01 V40525MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 11/22/23 11:01 V40525MSA
1430 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 11/22/23 11:01 V40525MSA
5020 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 11/22/23 11:01 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 10 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-1
89722 Matrix:
11/16/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
129 µg/L 7.80 1004-Methyl-2-Pentanone 100 11/22/23 11:01 V40525MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 11/22/23 11:01 V40525MSA
1390 µg/L 47.0 100Naphthalene 100 11/22/23 11:01 V40525MSA
340 µg/L 19.0 50.0n-Propylbenzene 100 11/22/23 11:01 V40525MSA
71.7 µg/L 22.0 50.0Styrene 100 11/22/23 11:01 V40525MSA
4690 µg/L 160 1000tert-Butyl Alcohol (TBA)100 11/22/23 11:01 V40525MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 11/22/23 11:01 V40525MSA
7150 J µg/L 1900 10000tert-Amyl Alcohol (TAA)1000 11/28/23 14:11 V40662MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 11/22/23 11:01 V40525MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 11/22/23 11:01 V40525MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 11/22/23 11:01 V40525MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 11/22/23 11:01 V40525MSA
8220 µg/L 22.0 50.0Toluene 100 11/22/23 11:01 V40525MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 11/22/23 11:01 V40525MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 11/22/23 11:01 V40525MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 11/22/23 11:01 V40525MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 11/22/23 11:01 V40525MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 11/22/23 11:01 V40525MSA
<18.0 M µg/L 18.0 50.0Trichlorofluoromethane 100 11/22/23 11:01 V40525MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 11/22/23 11:01 V40525MSA
2370 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 11/22/23 11:01 V40525MSA
622 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 11/22/23 11:01 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 11 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-1
89722 Matrix:
11/16/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
<100 µg/L 100 500Vinyl Acetate 100 11/22/23 11:01 V40525MSA
<17.0 M µg/L 17.0 50.0Vinyl Chloride 100 11/22/23 11:01 V40525MSA
2810 µg/L 21.0 50.0o-Xylene 100 11/22/23 11:01 V40525MSA
7570 µg/L 42.0 100m,p-Xylene 100 11/22/23 11:01 V40525MSA
10400 µg/L 21.0 50.0Xylene (Total)100 11/22/23 11:01 V40525
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%11/22/23 11:01100 MSA V40525
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%11/22/23 11:01100 MSA V40525
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%11/22/23 11:01100 MSA V40525
Surrogate: Toluene-d8 103 Limits: 70-130%11/22/23 11:01100 MSA V40525
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%11/28/23 14:111000 MSA V40662
Surrogate: Dibromofluoromethane 100 Limits: 70-130%11/28/23 14:111000 MSA V40662
Surrogate: 1,2-Dichloroethane - d4 93.6 Limits: 70-130%11/28/23 14:111000 MSA V40662
Surrogate: Toluene-d8 98.6 Limits: 70-130%11/28/23 14:111000 MSA V40662
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 12 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-4
89723 Matrix:
11/16/2023 10:15
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 11/22/23 11:26 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%11/22/23 11:26100 MSA V40525
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%11/22/23 11:26100 MSA V40525
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%11/22/23 11:26100 MSA V40525
Surrogate: Toluene-d8 102 Limits: 70-130%11/22/23 11:26100 MSA V40525
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/28/23 14:371000 MSA V40662
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/28/23 14:371000 MSA V40662
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%11/28/23 14:371000 MSA V40662
Surrogate: Toluene-d8 99.2 Limits: 70-130%11/28/23 14:371000 MSA V40662
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 13 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-4
89723 Matrix:
11/16/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
4260 µg/L 180 1000Acetone 100 11/22/23 11:26 V40525MSA
15800 µg/L 180 500Benzene 1000 11/28/23 14:37 V40662MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 11/22/23 11:26 V40525MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 11/22/23 11:26 V40525MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 11/22/23 11:26 V40525MSA
<150 µg/L 150 500Bromoform 100 11/22/23 11:26 V40525MSA
<28.0 M µg/L 28.0 100Bromomethane 100 11/22/23 11:26 V40525MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 11/22/23 11:26 V40525MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 11/22/23 11:26 V40525MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 11/22/23 11:26 V40525MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 11/22/23 11:26 V40525MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 11/22/23 11:26 V40525MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 11/22/23 11:26 V40525MSA
<43.0 M µg/L 43.0 100Chloroethane 100 11/22/23 11:26 V40525MSA
<22.0 µg/L 22.0 50.0Chloroform 100 11/22/23 11:26 V40525MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 11/22/23 11:26 V40525MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 11/22/23 11:26 V40525MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 11/22/23 11:26 V40525MSA
697 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 11/22/23 11:26 V40525MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 11/22/23 11:26 V40525MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 11/22/23 11:26 V40525MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 11/22/23 11:26 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 14 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-4
89723 Matrix:
11/16/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 11/22/23 11:26 V40525MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 11/22/23 11:26 V40525MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 11/22/23 11:26 V40525MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 11/22/23 11:26 V40525MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 11/22/23 11:26 V40525MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 11/22/23 11:26 V40525MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 11/22/23 11:26 V40525MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 11/22/23 11:26 V40525MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 11/22/23 11:26 V40525MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 11/22/23 11:26 V40525MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 11/22/23 11:26 V40525MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 11/22/23 11:26 V40525MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 11/22/23 11:26 V40525MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 11/22/23 11:26 V40525MSA
<4200 µg/L 4200 20000Ethanol 100 11/22/23 11:26 V40525MSA
2050 µg/L 17.0 50.0Ethylbenzene 100 11/22/23 11:26 V40525MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 11/22/23 11:26 V40525MSA
175 µg/L 38.0 1002-Hexanone 100 11/22/23 11:26 V40525MSA
67.0 µg/L 18.0 50.0Isopropylbenzene 100 11/22/23 11:26 V40525MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 11/22/23 11:26 V40525MSA
1930 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 11/22/23 11:26 V40525MSA
20300 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 11/28/23 14:37 V40662MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 15 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-4
89723 Matrix:
11/16/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
84.9 J µg/L 7.80 1004-Methyl-2-Pentanone 100 11/22/23 11:26 V40525MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 11/22/23 11:26 V40525MSA
902 µg/L 47.0 100Naphthalene 100 11/22/23 11:26 V40525MSA
182 µg/L 19.0 50.0n-Propylbenzene 100 11/22/23 11:26 V40525MSA
89.3 µg/L 22.0 50.0Styrene 100 11/22/23 11:26 V40525MSA
3800 µg/L 160 1000tert-Butyl Alcohol (TBA)100 11/22/23 11:26 V40525MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 11/22/23 11:26 V40525MSA
10600 µg/L 1900 10000tert-Amyl Alcohol (TAA)1000 11/28/23 14:37 V40662MSA
98.9 J µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 11/22/23 11:26 V40525MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 11/22/23 11:26 V40525MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 11/22/23 11:26 V40525MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 11/22/23 11:26 V40525MSA
30100 µg/L 220 500Toluene 1000 11/28/23 14:37 V40662MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 11/22/23 11:26 V40525MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 11/22/23 11:26 V40525MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 11/22/23 11:26 V40525MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 11/22/23 11:26 V40525MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 11/22/23 11:26 V40525MSA
<18.0 M µg/L 18.0 50.0Trichlorofluoromethane 100 11/22/23 11:26 V40525MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 11/22/23 11:26 V40525MSA
1430 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 11/22/23 11:26 V40525MSA
392 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 11/22/23 11:26 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 16 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-4
89723 Matrix:
11/16/2023 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
<100 µg/L 100 500Vinyl Acetate 100 11/22/23 11:26 V40525MSA
<17.0 M µg/L 17.0 50.0Vinyl Chloride 100 11/22/23 11:26 V40525MSA
3660 µg/L 21.0 50.0o-Xylene 100 11/22/23 11:26 V40525MSA
7590 µg/L 42.0 100m,p-Xylene 100 11/22/23 11:26 V40525MSA
11300 µg/L 21.0 50.0Xylene (Total)100 11/22/23 11:26 V40525
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%11/22/23 11:26100 MSA V40525
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%11/22/23 11:26100 MSA V40525
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%11/22/23 11:26100 MSA V40525
Surrogate: Toluene-d8 102 Limits: 70-130%11/22/23 11:26100 MSA V40525
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/28/23 14:371000 MSA V40662
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/28/23 14:371000 MSA V40662
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 70-130%11/28/23 14:371000 MSA V40662
Surrogate: Toluene-d8 99.2 Limits: 70-130%11/28/23 14:371000 MSA V40662
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 17 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-6
89724 Matrix:
11/16/2023 10:25
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 11/22/23 11:51 6200BMSA
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%11/22/23 11:51100 MSA V40525
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%11/22/23 11:51100 MSA V40525
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%11/22/23 11:51100 MSA V40525
Surrogate: Toluene-d8 103 Limits: 70-130%11/22/23 11:51100 MSA V40525
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/28/23 15:021000 MSA V40662
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/28/23 15:021000 MSA V40662
Surrogate: 1,2-Dichloroethane - d4 95.6 Limits: 70-130%11/28/23 15:021000 MSA V40662
Surrogate: Toluene-d8 97.6 Limits: 70-130%11/28/23 15:021000 MSA V40662
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 18 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-6
89724 Matrix:
11/16/2023 10:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
<180 µg/L 180 1000Acetone 100 11/22/23 11:51 V40525MSA
4680 µg/L 18.0 50.0Benzene 100 11/22/23 11:51 V40525MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 11/22/23 11:51 V40525MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 11/22/23 11:51 V40525MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 11/22/23 11:51 V40525MSA
<150 µg/L 150 500Bromoform 100 11/22/23 11:51 V40525MSA
<28.0 M µg/L 28.0 100Bromomethane 100 11/22/23 11:51 V40525MSA
35.3 J µg/L 18.0 50.0n-Butylbenzene 100 11/22/23 11:51 V40525MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 11/22/23 11:51 V40525MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 11/22/23 11:51 V40525MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 11/22/23 11:51 V40525MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 11/22/23 11:51 V40525MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 11/22/23 11:51 V40525MSA
<43.0 M µg/L 43.0 100Chloroethane 100 11/22/23 11:51 V40525MSA
<22.0 µg/L 22.0 50.0Chloroform 100 11/22/23 11:51 V40525MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 11/22/23 11:51 V40525MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 11/22/23 11:51 V40525MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 11/22/23 11:51 V40525MSA
118 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 11/22/23 11:51 V40525MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 11/22/23 11:51 V40525MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 11/22/23 11:51 V40525MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 11/22/23 11:51 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 19 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-6
89724 Matrix:
11/16/2023 10:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 11/22/23 11:51 V40525MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 11/22/23 11:51 V40525MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 11/22/23 11:51 V40525MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 11/22/23 11:51 V40525MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 11/22/23 11:51 V40525MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 11/22/23 11:51 V40525MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 11/22/23 11:51 V40525MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 11/22/23 11:51 V40525MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 11/22/23 11:51 V40525MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 11/22/23 11:51 V40525MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 11/22/23 11:51 V40525MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 11/22/23 11:51 V40525MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 11/22/23 11:51 V40525MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 11/22/23 11:51 V40525MSA
<4200 µg/L 4200 20000Ethanol 100 11/22/23 11:51 V40525MSA
4340 µg/L 17.0 50.0Ethylbenzene 100 11/22/23 11:51 V40525MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 11/22/23 11:51 V40525MSA
<38.0 µg/L 38.0 1002-Hexanone 100 11/22/23 11:51 V40525MSA
119 µg/L 18.0 50.0Isopropylbenzene 100 11/22/23 11:51 V40525MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 11/22/23 11:51 V40525MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 11/22/23 11:51 V40525MSA
369 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 11/22/23 11:51 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 20 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-6
89724 Matrix:
11/16/2023 10:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 11/22/23 11:51 V40525MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 11/22/23 11:51 V40525MSA
1490 µg/L 47.0 100Naphthalene 100 11/22/23 11:51 V40525MSA
378 µg/L 19.0 50.0n-Propylbenzene 100 11/22/23 11:51 V40525MSA
229 µg/L 22.0 50.0Styrene 100 11/22/23 11:51 V40525MSA
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 11/22/23 11:51 V40525MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 11/22/23 11:51 V40525MSA
4660 µg/L 190 1000tert-Amyl Alcohol (TAA)100 11/22/23 11:51 V40525MSA
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 11/22/23 11:51 V40525MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 11/22/23 11:51 V40525MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 11/22/23 11:51 V40525MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 11/22/23 11:51 V40525MSA
28500 µg/L 220 500Toluene 1000 11/28/23 15:02 V40662MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 11/22/23 11:51 V40525MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 11/22/23 11:51 V40525MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 11/22/23 11:51 V40525MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 11/22/23 11:51 V40525MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 11/22/23 11:51 V40525MSA
<18.0 M µg/L 18.0 50.0Trichlorofluoromethane 100 11/22/23 11:51 V40525MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 11/22/23 11:51 V40525MSA
2800 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 11/22/23 11:51 V40525MSA
741 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 11/22/23 11:51 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 21 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:MW-6
89724 Matrix:
11/16/2023 10:25
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00 V40661 11/27/23 09:00
<100 µg/L 100 500Vinyl Acetate 100 11/22/23 11:51 V40525MSA
<17.0 M µg/L 17.0 50.0Vinyl Chloride 100 11/22/23 11:51 V40525MSA
5770 µg/L 21.0 50.0o-Xylene 100 11/22/23 11:51 V40525MSA
13200 µg/L 42.0 100m,p-Xylene 100 11/22/23 11:51 V40525MSA
19000 µg/L 21.0 50.0Xylene (Total)100 11/22/23 11:51 V40525
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%11/22/23 11:51100 MSA V40525
Surrogate: Dibromofluoromethane 99.8 Limits: 70-130%11/22/23 11:51100 MSA V40525
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%11/22/23 11:51100 MSA V40525
Surrogate: Toluene-d8 103 Limits: 70-130%11/22/23 11:51100 MSA V40525
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/28/23 15:021000 MSA V40662
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/28/23 15:021000 MSA V40662
Surrogate: 1,2-Dichloroethane - d4 95.6 Limits: 70-130%11/28/23 15:021000 MSA V40662
Surrogate: Toluene-d8 97.6 Limits: 70-130%11/28/23 15:021000 MSA V40662
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 22 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89725 Matrix:
11/16/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00
2.51 J µg/L 1.80 10.0Acetone 1 11/22/23 04:01 V40525MSA
<0.180 µg/L 0.180 0.500Benzene 1 11/22/23 04:01 V40525MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 11/22/23 04:01 V40525MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 11/22/23 04:01 V40525MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 11/22/23 04:01 V40525MSA
<1.50 µg/L 1.50 5.00Bromoform 1 11/22/23 04:01 V40525MSA
<0.280 M µg/L 0.280 1.00Bromomethane 1 11/22/23 04:01 V40525MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 11/22/23 04:01 V40525MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 11/22/23 04:01 V40525MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 11/22/23 04:01 V40525MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 11/22/23 04:01 V40525MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 11/22/23 04:01 V40525MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 11/22/23 04:01 V40525MSA
<0.430 M µg/L 0.430 1.00Chloroethane 1 11/22/23 04:01 V40525MSA
<0.220 µg/L 0.220 0.500Chloroform 1 11/22/23 04:01 V40525MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 11/22/23 04:01 V40525MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 11/22/23 04:01 V40525MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 11/22/23 04:01 V40525MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 11/22/23 04:01 V40525MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 11/22/23 04:01 V40525MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 11/22/23 04:01 V40525MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 11/22/23 04:01 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 23 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89725 Matrix:
11/16/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 11/22/23 04:01 V40525MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 11/22/23 04:01 V40525MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 11/22/23 04:01 V40525MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 11/22/23 04:01 V40525MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 11/22/23 04:01 V40525MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 11/22/23 04:01 V40525MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 11/22/23 04:01 V40525MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 11/22/23 04:01 V40525MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 11/22/23 04:01 V40525MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 11/22/23 04:01 V40525MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 11/22/23 04:01 V40525MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 11/22/23 04:01 V40525MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 11/22/23 04:01 V40525MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 11/22/23 04:01 V40525MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 11/22/23 04:01 V40525MSA
<42.0 µg/L 42.0 200Ethanol 1 11/22/23 04:01 V40525MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 11/22/23 04:01 V40525MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 11/22/23 04:01 V40525MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 11/22/23 04:01 V40525MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 11/22/23 04:01 V40525MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 11/22/23 04:01 V40525MSA
2.64 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 11/22/23 04:01 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 24 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89725 Matrix:
11/16/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 11/22/23 04:01 V40525MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 11/22/23 04:01 V40525MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 11/22/23 04:01 V40525MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 11/22/23 04:01 V40525MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 11/22/23 04:01 V40525MSA
<0.220 µg/L 0.220 0.500Styrene 1 11/22/23 04:01 V40525MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 11/22/23 04:01 V40525MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 11/22/23 04:01 V40525MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 11/22/23 04:01 V40525MSA
<0.220 µg/L 0.220 0.500Toluene 1 11/22/23 04:01 V40525MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 11/22/23 04:01 V40525MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 11/22/23 04:01 V40525MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 11/22/23 04:01 V40525MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 11/22/23 04:01 V40525MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 11/22/23 04:01 V40525MSA
<0.180 M µg/L 0.180 0.500Trichlorofluoromethane 1 11/22/23 04:01 V40525MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 11/22/23 04:01 V40525MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 11/22/23 04:01 V40525MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 11/22/23 04:01 V40525MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 11/22/23 04:01 V40525MSA
<0.170 M µg/L 0.170 0.500Vinyl Chloride 1 11/22/23 04:01 V40525MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 11/22/23 04:01 V40525MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 25 of 35
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-321-0005
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5721 Received : 11/17/2023
Rushco 4 (Former)
Report Date : 11/29/2023
Sample ID :
Lab No :
Sampled:Trip Blank
89725 Matrix:
11/16/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V40524 11/21/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 11/22/23 04:01 V40525MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 11/22/23 04:01 V40525
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/22/23 04:011 MSA V40525
Surrogate: Dibromofluoromethane 102 Limits: 70-130%11/22/23 04:011 MSA V40525
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%11/22/23 04:011 MSA V40525
Surrogate: Toluene-d8 104 Limits: 70-130%11/22/23 04:011 MSA V40525
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 26 of 35
Quality Control Data
23-321-0005Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40525QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40524
Associated Lab Samples: 89722, 89723, 89724, 89725
LRB-V40524 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/22/23 03:3610.01.80<1.80µg/LAcetone
11/22/23 03:360.5000.180<0.180µg/LBenzene
11/22/23 03:360.5000.210<0.210µg/LBromobenzene
11/22/23 03:361.000.420<0.420µg/LBromochloromethane
11/22/23 03:360.5000.160<0.160µg/LBromodichloromethane
11/22/23 03:365.001.50<1.50µg/LBromoform
11/22/23 03:361.000.280<0.280µg/LBromomethane
11/22/23 03:360.5000.180<0.180µg/Ln-Butylbenzene
11/22/23 03:360.5000.200<0.200µg/Lsec-Butyl benzene
11/22/23 03:362.000.920<0.920µg/Ltert-Butyl benzene
11/22/23 03:360.5000.180<0.180µg/LCarbon Tetrachloride
11/22/23 03:360.5000.190<0.190µg/LChlorobenzene
11/22/23 03:360.5000.190<0.190µg/LChlorodibromomethane
11/22/23 03:361.000.430<0.430µg/LChloroethane
11/22/23 03:360.5000.220<0.220µg/LChloroform
11/22/23 03:360.5000.220<0.220µg/LChloromethane
11/22/23 03:360.5000.200<0.200µg/L2-Chlorotoluene
11/22/23 03:360.5000.200<0.200µg/L4-Chlorotoluene
11/22/23 03:360.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
11/22/23 03:362.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
11/22/23 03:360.5000.200<0.200µg/L1,2-Dibromoethane
11/22/23 03:360.5000.230<0.230µg/LDibromomethane
11/22/23 03:360.5000.220<0.220µg/L1,2-Dichlorobenzene
11/22/23 03:360.5000.190<0.190µg/L1,3-Dichlorobenzene
11/22/23 03:360.5000.210<0.210µg/L1,4-Dichlorobenzene
11/22/23 03:365.001.20<1.20µg/LDichlorodifluoromethane
11/22/23 03:360.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 7Date:11/29/2023 03:32 PM
Page 27 of 35
Quality Control Data
23-321-0005Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40525QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40524
Associated Lab Samples: 89722, 89723, 89724, 89725
LRB-V40524 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/22/23 03:360.5000.150<0.150µg/L1,2-Dichloroethane
11/22/23 03:360.5000.150<0.150µg/L1,1-Dichloroethene
11/22/23 03:360.5000.200<0.200µg/Lcis-1,2-Dichloroethene
11/22/23 03:360.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
11/22/23 03:360.5000.190<0.190µg/L1,2-Dichloropropane
11/22/23 03:360.5000.130<0.130µg/L1,3-Dichloropropane
11/22/23 03:362.000.210<0.210µg/L2,2-Dichloropropane
11/22/23 03:360.5000.200<0.200µg/L1,1-Dichloropropene
11/22/23 03:360.5000.210<0.210µg/Lcis-1,3-Dichloropropene
11/22/23 03:360.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
11/22/23 03:3620042.0<42.0µg/LEthanol
11/22/23 03:360.5000.170<0.170µg/LEthylbenzene
11/22/23 03:363.000.350<0.350µg/LHexachlorobutadiene
11/22/23 03:361.000.380<0.380µg/L2-Hexanone
11/22/23 03:360.5000.180<0.180µg/LIsopropylbenzene
11/22/23 03:360.5000.089<0.089µg/L4-Isopropyl toluene
11/22/23 03:365.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
11/22/23 03:361.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
11/22/23 03:361.000.078<0.078µg/L4-Methyl-2-Pentanone
11/22/23 03:362.000.330<0.330µg/LMethylene Chloride
11/22/23 03:361.000.470<0.470µg/LNaphthalene
11/22/23 03:360.5000.190<0.190µg/Ln-Propylbenzene
11/22/23 03:360.5000.220<0.220µg/LStyrene
11/22/23 03:3610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
11/22/23 03:3610.00.350<0.350µg/Ltert-Butyl formate (TBF)
11/22/23 03:3610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
11/22/23 03:3610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 7Date:11/29/2023 03:32 PM
Page 28 of 35
Quality Control Data
23-321-0005Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40525QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40524
Associated Lab Samples: 89722, 89723, 89724, 89725
LRB-V40524 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/22/23 03:360.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
11/22/23 03:360.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
11/22/23 03:360.5000.220<0.220µg/LTetrachloroethene
11/22/23 03:360.5000.220<0.220µg/LToluene
11/22/23 03:360.5000.380<0.380µg/L1,2,3-Trichlorobenzene
11/22/23 03:360.5000.310<0.310µg/L1,2,4-Trichlorobenzene
11/22/23 03:360.5000.160<0.160µg/L1,1,1-Trichloroethane
11/22/23 03:360.5000.096<0.096µg/L1,1,2-Trichloroethane
11/22/23 03:360.5000.180<0.180µg/LTrichloroethene
11/22/23 03:360.5000.180<0.180µg/LTrichlorofluoromethane
11/22/23 03:360.5000.270<0.270µg/L1,2,3-Trichloropropane
11/22/23 03:360.5000.190<0.190µg/L1,2,4-Trimethylbenzene
11/22/23 03:360.5000.180<0.180µg/L1,3,5-Trimethylbenzene
11/22/23 03:365.001.00<1.00µg/LVinyl Acetate
11/22/23 03:360.5000.170<0.170µg/LVinyl Chloride
11/22/23 03:360.5000.210<0.210µg/Lo-Xylene
11/22/23 03:361.000.420<0.420µg/Lm,p-Xylene
11/22/23 03:3610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
11/22/23 03:364-Bromofluorobenzene (S)104 70-130
11/22/23 03:36Dibromofluoromethane (S)100 70-130
11/22/23 03:361,2-Dichloroethane - d4 (S)98.0 70-130
11/22/23 03:36Toluene-d8 (S)103 70-130
Page 3 of 7Date:11/29/2023 03:32 PM
Page 29 of 35
Quality Control Data
23-321-0005Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40525QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40524
LCS-V40524 LCSD-V40524Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
53.6 13414758.740.0µg/LAcetone 40-160 9.0 20.0
20.1 10110320.620.0µg/LBenzene 70-130 2.4 20.0
21.3 10710921.820.0µg/LBromobenzene 70-130 2.3 20.0
19.6 98.010320.520.0µg/LBromochloromethane 70-130 4.4 20.0
19.0 95.010120.120.0µg/LBromodichloromethane 70-130 5.6 20.0
19.5 97.510520.920.0µg/LBromoform 70-130 6.9 20.0
7.74 38.7*46.3*9.2620.0µg/LBromomethane 60-140 17.8 20.0
21.3 10711222.320.0µg/Ln-Butylbenzene 70-130 4.5 20.0
21.0 10510821.520.0µg/Lsec-Butyl benzene 70-130 2.3 20.0
21.0 10510921.720.0µg/Ltert-Butyl benzene 70-130 3.2 20.0
19.3 96.599.519.920.0µg/LCarbon Tetrachloride 70-130 3.0 20.0
20.7 10410821.520.0µg/LChlorobenzene 70-130 3.7 20.0
20.6 10310420.820.0µg/LChlorodibromomethane 70-130 0.9 20.0
11.1 55.5*56.0*11.220.0µg/LChloroethane 60-140 0.8 20.0
19.8 99.010220.320.0µg/LChloroform 70-130 2.4 20.0
2.84 14.2*17.4*3.4820.0µg/LChloromethane 60-140 20.2*20.0
21.1 10610821.620.0µg/L2-Chlorotoluene 70-130 2.3 20.0
21.1 10610821.520.0µg/L4-Chlorotoluene 70-130 1.8 20.0
19.9 99.510520.920.0µg/LDi-Isopropyl Ether (DIPE)70-130 4.9 20.0
22.9 11510821.620.0µg/L1,2-Dibromo-3-Chloropropane 70-130 5.8 20.0
20.8 10410921.720.0µg/L1,2-Dibromoethane 70-130 4.2 20.0
20.0 10010220.420.0µg/LDibromomethane 70-130 1.9 20.0
21.1 10611022.020.0µg/L1,2-Dichlorobenzene 70-130 4.1 20.0
21.3 10710921.720.0µg/L1,3-Dichlorobenzene 70-130 1.8 20.0
20.8 10410821.620.0µg/L1,4-Dichlorobenzene 70-130 3.7 20.0
<1.20 0.0*0.0*<1.2020.0µg/LDichlorodifluoromethane 60-140 0.0 20.0
Page 4 of 7* QC Fail Date:11/29/2023 03:32 PM
Page 30 of 35
Quality Control Data
23-321-0005Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40525QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40524
LCS-V40524 LCSD-V40524Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.9 99.510621.120.0µg/L1,1-Dichloroethane 70-130 5.8 20.0
19.4 97.099.519.920.0µg/L1,2-Dichloroethane 70-130 2.5 20.0
20.1 10110420.820.0µg/L1,1-Dichloroethene 70-130 3.4 20.0
19.7 98.510320.620.0µg/Lcis-1,2-Dichloroethene 70-130 4.4 20.0
19.8 99.010120.220.0µg/Ltrans-1,2-Dichloroethene 70-130 2.0 20.0
19.6 98.010220.420.0µg/L1,2-Dichloropropane 70-130 4.0 20.0
20.3 10210721.420.0µg/L1,3-Dichloropropane 70-130 5.2 20.0
16.9 84.587.517.520.0µg/L2,2-Dichloropropane 70-130 3.4 20.0
21.0 10510921.820.0µg/L1,1-Dichloropropene 70-130 3.7 20.0
18.5 92.597.519.520.0µg/Lcis-1,3-Dichloropropene 70-130 5.2 20.0
18.5 92.597.019.420.0µg/Ltrans-1,3-Dichloropropene 70-130 4.7 20.0
459 91.8108538500µg/LEthanol 60-140 15.8 20.0
20.6 10310621.220.0µg/LEthylbenzene 70-130 2.8 20.0
20.8 10410921.820.0µg/LHexachlorobutadiene 70-130 4.6 20.0
23.2 11612324.620.0µg/L2-Hexanone 60-140 5.8 20.0
21.8 10911222.320.0µg/LIsopropylbenzene 70-130 2.2 20.0
21.5 10811222.420.0µg/L4-Isopropyl toluene 70-130 4.1 20.0
20.7 10412023.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 14.3 20.0
19.6 98.010420.720.0µg/LMethyl tert-butyl ether (MTBE)70-130 5.4 20.0
19.6 98.010120.220.0µg/L4-Methyl-2-Pentanone 60-140 3.0 20.0
19.4 97.010320.520.0µg/LMethylene Chloride 70-130 5.5 20.0
25.9 13011823.520.0µg/LNaphthalene 70-130 9.7 20.0
21.3 10710921.820.0µg/Ln-Propylbenzene 70-130 2.3 20.0
20.9 10511021.920.0µg/LStyrene 70-130 4.6 20.0
40.4 10110742.940.0µg/Ltert-Butyl Alcohol (TBA)40-140 6.0 20.0
25.5 63.763.725.540.0µg/Ltert-Butyl formate (TBF)40-140 0.0 20.0
Page 5 of 7Date:11/29/2023 03:32 PM
Page 31 of 35
Quality Control Data
23-321-0005Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40525QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40524
LCS-V40524 LCSD-V40524Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
16.9 84.598.019.620.0µg/Ltert-Amyl Alcohol (TAA)40-140 14.7 20.0
42.6 10711244.840.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 5.0 20.0
21.0 10510821.620.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.8 20.0
20.2 10110520.920.0µg/L1,1,2,2-Tetrachloroethane 70-130 3.4 20.0
21.0 10510921.720.0µg/LTetrachloroethene 70-130 3.2 20.0
19.8 99.010320.620.0µg/LToluene 70-130 3.9 20.0
23.9 12011923.820.0µg/L1,2,3-Trichlorobenzene 70-130 0.4 20.0
22.3 11211022.020.0µg/L1,2,4-Trichlorobenzene 70-130 1.3 20.0
19.6 98.010320.620.0µg/L1,1,1-Trichloroethane 70-130 4.9 20.0
19.0 95.010220.320.0µg/L1,1,2-Trichloroethane 70-130 6.6 20.0
21.1 10610921.820.0µg/LTrichloroethene 70-130 3.2 20.0
11.6 58.0*61.512.320.0µg/LTrichlorofluoromethane 60-140 5.8 20.0
20.0 10010120.220.0µg/L1,2,3-Trichloropropane 70-130 0.9 20.0
21.5 10811122.120.0µg/L1,2,4-Trimethylbenzene 70-130 2.7 20.0
21.7 10911122.120.0µg/L1,3,5-Trimethylbenzene 70-130 1.8 20.0
13.7 68.573.014.620.0µg/LVinyl Acetate 60-140 6.3 20.0
4.71 23.5*24.9*4.9920.0µg/LVinyl Chloride 60-140 5.7 20.0
20.7 10410821.520.0µg/Lo-Xylene 70-130 3.7 20.0
43.6 10911445.740.0µg/Lm,p-Xylene 70-130 4.7 20.0
19.2 96.010120.120.0µg/L3,3-Dimethyl-1-butanol 70-130 4.5 20.0
10099.04-Bromofluorobenzene (S)70-130
99.6100Dibromofluoromethane (S)70-130
1011021,2-Dichloroethane - d4 (S)70-130
105104Toluene-d8 (S)70-130
Page 6 of 7* QC Fail Date:11/29/2023 03:32 PM
Page 32 of 35
Quality Control Data
23-321-0005Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco 4 (Former)
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V40662QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V40661
Associated Lab Samples: 89722, 89723, 89724
LRB-V40661 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/28/23 06:570.5000.180<0.180µg/LBenzene
11/28/23 06:571.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
11/28/23 06:5710.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
11/28/23 06:570.5000.220<0.220µg/LToluene
11/28/23 06:574-Bromofluorobenzene (S)103 70-130
11/28/23 06:57Dibromofluoromethane (S)100 70-130
11/28/23 06:571,2-Dichloroethane - d4 (S)91.8 70-130
11/28/23 06:57Toluene-d8 (S)99.0 70-130
LCS-V40661 LCSD-V40661Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.0 10010721.320.0µg/LBenzene 70-130 6.2 20.0
19.5 97.597.519.520.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.0 20.0
18.1 90.579.015.820.0µg/Ltert-Amyl Alcohol (TAA)40-140 13.5 20.0
20.1 10110420.820.0µg/LToluene 70-130 3.4 20.0
97.098.84-Bromofluorobenzene (S)70-130
101103Dibromofluoromethane (S)70-130
97.498.81,2-Dichloroethane - d4 (S)70-130
10098.2Toluene-d8 (S)70-130
Page 7 of 7Date:11/29/2023 03:32 PM
Page 33 of 35
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-321-0005
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:11/17/2023 11:14:42
Special precautions or instructions included?
Comments:
Page 34 of 35
Page 35 of 35

APPENDIX C
MMPE Report and Disposal Manifest