MO-27703_47020_CA_MRP_20230731

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

August 1, 2023

Mr. Ryan Mills
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Ground Water Monitoring Report
June 2023
Mikey’s 1 Station 19
1407 North Main Street
China Grove, Rowan County
North Carolina
Facility ID Number: 0-00-0000021906
Incident Number: 47020
GRI Project Number: 4486

Dear Mr. Mills,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Joanna Alley at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Salim Nimji; SNS Group, LLC, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
June 2023
Mikey’s 1 Station 19
1407 North Main Street
China Grove, Rowan County
North Carolina
Facility ID Number: 0-00-0000021906
Incident Number: 47020
GRI Project Number: 4486

Prepared for:

Mr. Salim Nimji
SNS Group, LLC
Post Office Box 4329
Mooresville, North Carolina 28117

July 31, 2023

Joanna Alley, P.E.
Project Manager

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
i
EXECUTIVE SUMMARY
Mikey’s 1 Station 19 is located at 1407 North Main Street in China Grove, Rowan County, North Carolina.
The site is currently owned and operated by SNS Group, LLC as a petroleum retail facility. A site check
was conducted in April 2020 following the receipt of non-passing hydrostatic testing results for the 4,000-
gallon diesel and the 12,000-gallon regular gasoline UST spill buckets that confirmed the presence of a
release. Three 4,000-gallon gasoline, one 4,000-gallon diesel, and one 12,000-gallon gasoline USTs are
currently in use at the site along with five associated dispensers. The adjoining properties are a mixture
of residential, commercial, and industrial properties. According to the information determined during
receptor survey activities, one potable water supply well was identified within 1,000 feet of the site.
Municipal water is available to the site and adjacent properties from Salisbury-Rowan Utilities; however,
public water is not available on Red Fox Lane.

A CAP has not yet been developed for the site and no corrective action has been performed to date.

Two additional Type II monitoring wells (MW-9 and MW-10) were installed on June 28, 2023, each to a
total depth of 20 feet BGS with a screened interval of 10 feet. On June 29, 2023, ten monitoring wells and
one telescoping well were gauged, purged, and sampled. No free product was observed at the site. The
concentrations of benzene, ethylbenzene, xylenes, MTBE, naphthalene, TAA, TBA, methyl chloride,
isopropylbenzene, IPE, n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, bis(2-
ethylhexyl) phthalate, 1-methylnaphthalene and/or 2-methylnaphthalene reported in the ground water
samples collected from MW-1 through MW-5, MW-9, MW-10, and TW-1 exceeded the MACs. All reported
contaminant concentrations were below the GCLs. Please note that although the reported concentrations
of methyl chloride and bis(2-ethylhexyl) phthalate exceeded the MACs, these are not considered
petroleum constituents.

Based on this information, the risk classification for the site should remain high risk. Additional monitoring
wells are necessary to define the horizontal extent of the plume to the west of MW-9 and to the south of
MW-3. Please note that due to utilities in the right-of-way and the approximate distance to move across
either street for assessment, additional wells may not be practical. The owner of water supply well WSW-
2 should be contacted to determine if she would be willing to connect to municipal water. The next
sampling event is tentatively scheduled for December 2023.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
ii
SITE INFORMATION
1. Site Identification
 Mikey’s 1 Station 19 (Facility ID 0-00-0000021906)
 Incident Number 47020 – High Risk (H-135-D)
 Location of Source Area: 1407 North Main Street
China Grove, NC 28023
Rowan County
35.578228°N, 80.565818°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
SNS Group, LLC
P.O. Box 4329
Mooresville, NC 28117
Email: Unknown
704-799-9929

UST/AST Operator
SNS Group, LLC
P.O. Box 4329
Mooresville, NC 28117
Email: Unknown
704-799-9929

Property Owner
SNS Group, LLC
P.O. Box 4329
Mooresville, NC 28117
Email: Unknown
704-799-9929

Property Occupant
SNS Group, LLC
P.O. Box 4329
Mooresville, NC 28117
Email: Unknown
704-799-9929

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
SGS North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, FL 32811
State Certification No. 573
407-425-6700
3. Information about Release
 A release was discovered on May 8, 2020.
 An unknown amount of product was released from the leaking UST System via non-passing spill buckets.
 Three 4,000-gallon gasoline, one 4,000-gallon diesel and one 12,000-gallon gasoline USTs are
currently in use at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 MONITORING WELL INSTALLATION ..........................................................................................3
3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................3
4.0 FREE PRODUCT REMOVAL ........................................................................................................4
5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4
6.0 CONCLUSIONS .........................................................................................................................4
7.0 LIMITATIONS ...........................................................................................................................5
8.0 STATEMENTS AND CERTIFICATION ...........................................................................................5

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3A: Site Vicinity Map
Figure 3B: Zoning Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Benzene Isoconcentration Map
Figure 7: Ethylbenzene Isoconcentration Map
Figure 8: Xylenes Isoconcentration Map
Figure 9: MTBE Isoconcentration Map
Figure 10: Naphthalene Isoconcentration Map
Figure 11: Cross Section A-A’
Figure 12: Cross Section B-B’

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Receptor Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Land Use Information
Appendix C: Incident Reports

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
Appendix D: Subsurface Logs and Well Construction Records
Appendix E: Historical Soil Quality Information
Appendix F: Laboratory Analytical Report

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the June 2023 monitoring well installation and ground water sampling activities
at the Mikey’s 1 Station 19 site, located at 1407 North Main Street in China Grove, Rowan County, North
Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 22-701, which
was submitted to the NCDEQ on March 16, 2023, and was approved as Task Authorization No. 47020-3
on April 18, 2023. A change order was submitted on April 24, 2023 and was approved as Task
Authorization No. 47020-3.1 on April 24, 2023. State correspondence is included as Appendix A.

The site is currently owned and operated by SNS Group, LLC as a petroleum retail facility. On April 18,
2019, during annual compliance testing activities, non-passing spill buckets were reported for the 4,000-
gallon diesel and the 12,000-gallon regular gasoline USTs. Therefore, a Site Check was required by the
NCDEQ. On April 15, 2020, GRI conducted a Site Check at the non-passing spill buckets that confirmed
the presence of a release. There are three 4,000-gallon gasoline, one 4,000-gallon diesel and one 12,000-
gallon gasoline USTs currently in use at the site with five associated dispensers. UST owner/operator
information and UST system information are included as Tables 1 and 2, respectively. The Registered
Tank Report is shown below:

The site and surrounding area are a mixture of residential, commercial, and industrial properties. A copy
of the Land Use table has been included as Appendix B. The site contains one building and is primarily
capped with concrete and asphalt. The overall topography at the site is relatively flat. Eight Type II
monitoring wells (MW-1 through MW-8) and one Type III telescoping monitoring well (TW-1) were
installed at the site during previous ground water assessment activities. A Site Map showing the locations
of the monitoring wells and the structures on-site is included as Figure 2.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
2

On June 9, 2020, GRI personnel conducted a receptor survey at the site. Ten water supply wells are
located within 1,500 feet of the site. Of the ten water supply wells, one potable water supply well is
located within 1,000 feet of the site. No water supply wells were located within 250 feet of the site.
Municipal water is available to the site and adjacent properties from Salisbury-Rowan Utilities; however,
public water is not available on Red Fox Lane. Water lines run along the public streets in the area. No
surface water bodies were identified within 1,500 feet of the site during the June 9, 2020 receptor survey.
Receptor information is provided in Table 3. Adjacent property owner information is presented in Table
4. A Site Vicinity Map showing the adjacent properties and a Zoning Map showing the zoning information
are included as Figures 3A and 3B, respectively.

No incidents have been reported on any adjacent property. A copy of the NCDEQ Incident Report for the
subject release is included as Appendix C. A map showing the location of the incident and vicinity is shown
below:

A CAP has not been developed for the site. To date, no corrective action has been performed. Please
note that projected milestones will be established in the CAP.

Based on this information, the site was classified as high risk. Additional monitoring wells should be
installed to define the plume to the west of MW-9 and across the street to the south of MW-3. Please
note that telescoping well TW-1 contains contamination above the MAC; however, based on the relatively
low concentrations, further vertical assessment is not warranted at this time.
47020

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
3
2.0 MONITORING WELL INSTALLATION
On June 28, 2023, two Type II monitoring wells (MW-9 and MW-10) were installed to the west and
southeast of MW-8 to help define the horizontal extent of the contaminant plume. GRI personnel
attempted to install a third additional Type II monitoring well to the south of MW-3 on June 28, 2023, but
due to the presence of multiple utility lines and fill material that could not be pre-cleared with a hand
auger, this monitoring well was not installed. Monitoring wells MW-9 and MW-10 were each installed to
total depths of 20 feet BGS with screened intervals of 10 feet. Copies of the subsurface logs and Well
Construction Records are included in Appendix D.
3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Soil assessment was not conducted during the current scope of work. Historical soil quality information
and soil excavation information has been included as Appendix E.

On June 29, 2023, ten Type II monitoring wells (MW-1 through MW-10) and one telescoping well (TW-1)
were gauged, purged, and sampled in accordance with the NCDEQ guidelines. No free product was
observed at the site. Depths to ground water in the Type II monitoring wells ranged from 9.60 feet to
15.40 feet below TOC. Ground water elevations in the Type II monitoring wells ranged from 85.51 feet to
89.78 feet. Ground water flow at the site was generally toward the west and south from a ground water
high located between MW-4 and MW-5. Horizontal gradients were approximately 0.05 feet per foot to
the west and south. The vertical gradient between monitoring well MW-1 and telescoping well TW-1 was
approximately 0.003 feet per foot in the downward direction. Well construction and gauging information
is presented in Table 5. A Water Table Surface Map based on the Type II monitoring wells is included as
Figure 4. A summary of the current ground water gauging data is shown below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 10 - 20 20 100.00 13.48 --- 86.52
MW-2 10 - 20 20 99.96 13.73 --- 86.23
MW-3 10 - 20 20 99.62 12.65 --- 86.97
MW-4 10 - 20 20 99.93 10.20 --- 89.73
MW-5 10 - 20 20 99.38 9.60 --- 89.78
MW-6 10 - 20 20 98.13 10.68 --- 87.45
MW-7 10 - 20 20 99.40 13.89 --- 85.51
MW-8 10 - 20 20 100.72 14.34 --- 86.38
MW-9 10 - 20 20 101.06 14.41 --- 86.65
MW-10 10 - 20 20 101.81 15.40 --- 86.41
TW-1 35 - 40 40 100.09 13.65 --- 86.44

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B and EPA Method 625. The concentrations of benzene, ethylbenzene, xylenes, MTBE,
naphthalene, TAA, TBA, methyl chloride, isopropylbenzene, IPE, n-propylbenzene, 1,2,4-
trimethylbenzene, 1,3,5-trimethylbenzene, bis(2-ethylhexyl) phthalate, 1-methylnaphthalene and/or 2-

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
4
methylnaphthalene reported in the ground water samples collected from MW-1 through MW-5, MW-9,
MW-10, and TW-1 exceeded the MACs. All reported contaminant concentrations were below the GCLs.
Please note that although the reported concentrations of methyl chloride and bis(2-ethylhexyl) phthalate
exceeded the MACs, these are not considered petroleum constituents. A summary of the analytical
results for ground water samples collected on June 29, 2023, is presented in Table 6. A Ground Water
Quality Map based on the June 2023 data is included as Figure 5. Isoconcentration maps and cross sections
have been included as Figures 6 through 12. A complete report of laboratory analyses of the ground water
samples collected from the monitoring wells during the June 2023 sampling event has been included as
Appendix F. A summary of the current ground water analytical data is shown below:

Contaminant
of Concern →
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well
ID
MACs (μg/l) 1 600 600 500 20 6
GCLs (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 751 <22.0 89.9 <21.0 753 <47.0
MW-2 0.721 <0.220 <0.170 <0.210 21.7 <0.470
MW-3 75.5 6.70 11.30 3.66 12.2 11.0
MW-4 330 114 241 1,820 63.5 J <47.0
MW-5 0.429 J 0.233 J <0.170 <0.210 1.88 <0.470
MW-6 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-7 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-8 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-9 2,420 423 1,520 9,670 <14.0 2,620
MW-10 1.69 0.751 9.01 60.4 <0.140 4.92
TW-1 5.99 <0.220 <0.170 3.99 J <0.140 <0.470

The baseline contaminant mass at the site will be determined once the plume has been defined.

The site is in the Charlotte Belt of North Carolina. The water table has a seasonal high depth to water of
approximately ten to fifteen feet BGS.

A CAP has not yet been developed for the site and no corrective action has been performed to date.
4.0 FREE PRODUCT REMOVAL
Free product has historically not been present at the site.
5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Due to the site being in the assessment phase, no natural attenuation monitoring plan is currently in place
at the site.
6.0 CONCLUSIONS
• On June 28, 2023, two Type II monitoring wells (MW-9 and MW-10) were installed to the west
and southeast of MW-8.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 31, 2023 Mikey’s 1 Station 19
Project Manager: Joanna Alley, P.E. GRI Project No. 4486
5
• GRI personnel attempted to install a third additional Type II monitoring well to the south of MW-
3 on June 28, 2023, but due to the presence of multiple utility lines and fill material that could not
be pre-cleared with a hand auger, this monitoring well was not installed.
• On June 29, 2023, ten Type II monitoring wells and one telescoping well were gauged, purged,
and sampled. No free product was observed at the site. Ground water flow at the site was
generally toward the west and south from a ground water high located between MW-4 and MW-
5. Horizontal gradients were approximately 0.05 feet per foot to the west and south. The vertical
gradient between monitoring well MW-1 and telescoping well TW-1 was approximately 0.003 feet
per foot in the downward direction.
• The concentrations of benzene, ethylbenzene, xylenes, MTBE, naphthalene, TAA, TBA, methyl
chloride, isopropylbenzene, IPE, n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-
trimethylbenzene, bis(2-ethylhexyl) phthalate, 1-methylnaphthalene and/or 2-
methylnaphthalene reported in the ground water samples collected from MW-1 through MW-5,
MW-9, MW-10, and TW-1 exceeded the MACs. All reported contaminant concentrations were
below the GCLs. Please note that although the reported concentrations of methyl chloride and
bis(2-ethylhexyl) phthalate exceeded the MACs, these are not considered petroleum constituents.
• Based on this information, the risk classification for the site should remain high risk. Additional
monitoring wells are necessary to define the horizontal extent of the plume to the west of MW-9
and to the south of MW-3. Please note that due to utilities in the right-of-way and the
approximate distance to move across either street for assessment, additional wells may not be
practical. The owner of water supply well WSW-2 should be contacted to determine if she would
be willing to connect to municipal water. The next sampling event is tentatively scheduled for
December 2023.
7.0 LIMITATIONS
This report has been prepared for the exclusive use of SNS Group, LLC for specific application to the
referenced site in Rowan County, North Carolina. The assessment was conducted based on the scope of
work and level of effort desired by the NCDEQ and with resources adequate only for that scope of work.
Our findings have been developed in accordance with generally accepted standards of environmental
practices in the State of North Carolina, available information, and our professional judgment. No other
warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
8.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO

FIGURES
SITE LOCATION
Figure 1
Site Location
Mikeys 1, Station 19
1407 N. Main Street China Grove,
Rowan County, NC
Incident No. 47020
GRI Project No. 4486
500 M
2000 FT
Date: 05/12/2020 Location: 35.578228° N -80.565818° W
D
a
d
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J
SITE
117 048
117 028
117 022
117 169
117 032
117 203
117 009
117 05002
117 029A
117 034
117 037
117 154
117 161
117 057
117 033
117 180
WSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
WSW-10
MAIN ST
US 29 HWY
SHUE RD
NC 152 HWY
I 85
RECOVERY RD
TRIPS END RD
RED FOX LN
MADISON RD
HILLSIDE DR
KLONDALE ST
ARBOR DR
BEAVER ST
LIBERTY ST
WASHINGTON ST
STRATUS DR
MYRTLE GOODNIGHT RD
OLD ROCKWELL RD E NC 152 ON
MILLER ST
RAILROAD AV
CHINA GROVE SCHOOL RD
YOST TOWN RD
KNIGHT ST
GILLON ST
SPRING BRANCH LN
I 85
US 29 HWY
MILLER ST
HUFFMAN ST
FIGURE 3A: SITE VICINITY MAPMIKEYS 1, STATION 191407 NORTH MAIN STREETCHINA GROVE, ROWAN COUNTYNORTH CAROLINAINCIDENT NO. 47020GRI NO. 4486
PREPARED BY:GEOLOGICAL RESOURCES, INC.MAY 20, 2020
³
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
0 300150Feet1 inch = 300 feet
500-FOOT RADIUS
LEGEND
"J Water Supply Well
lakes
newstreams
centerlines
Adjacent Parcels and Well Owners
Rowan County Tax Parcels
"J
"J
"J
"J
"J
"J
"J
"J
"J
"J
SITE
WSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
WSW-10
MAIN ST
US 29 HWY
SHUE RD
NC 152 HWY
I 85
RECOVERY RD
TRIPS END RD
RED FOX LN
MADISON RD
HILLSIDE DR
KLONDALE ST
ARBOR DR
BEAVER ST
LIBERTY ST
WASHINGTON ST
STRATUS DR
MYRTLE GOODNIGHT RD
OLD ROCKWELL RD E NC 152 ON
MILLER ST
RAILROAD AV
CHINA GROVE SCHOOL RD
YOST TOWN RD
KNIGHT ST
GILLON ST
SPRING BRANCH LN
I 85
US 29 HWY
MILLER ST
HUFFMAN ST
FIGURE 3B: ZONING MAPMIKEYS 1, STATION 191407 NORTH MAIN STREETCHINA GROVE, ROWAN COUNTYNORTH CAROLINAINCIDENT NO. 47020GRI NO. 4486
PREPARED BY:GEOLOGICAL RESOURCES, INC.MAY 20, 2020
³
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
0 300150Feet1 inch = 300 feet
500-FOOT RADIUS
LEGEND
ZONING - RS
ZONING - LI
ZONING - RT
ZONING - RM
ZONING - HB
ZONING - RMH
ZONING - NC
"J Water Supply Well
lakes
newstreams
centerlines
Rowan County Tax Parcels

TABLES
UST ID Number 1-5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-4 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-4 Facility ID Number
Owner or Operator?
Owner
Unknown Unknown
Address Telephone Number
00-0-0000021906
Iredell Leasing Co 08/30/1988 - 01/01/1997
Name of Owner or Operator Dates of Ownership / Operation
00-0-0000021906
TABLE 1
UST OWNER/OPERATOR INFORMATION
MIKEYS 1 STATION 19 (INCIDENT NO. 47020)
P.O. Box 4329 704-799-9929
Name of Owner or Operator Dates of Ownership / Operation
SNG Goup, LLC 10/25/2012 - Current
Address Telephone Number
Address Telephone Number
P.O. Box 88, Mooresville, NC 28115 704-664-1566
00-0-0000021906
Name of Owner or Operator Dates of Ownership / Operation
J. T. Alexander & Son, Inc. 01/01/1997 - 10/25/2012
Address Telephone Number
P.O. Box 88, Mooresville, NC 28115 704-664-1566
00-0-0000021906
Name of Owner or Operator Dates of Ownership / Operation
J. T. Alexander & Son, Inc. 10/07/1997 - 10/25/2012
Page 1 of 1
Date: 05/11/2020
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Kerosene 4,000 8/16/1985 Single Wall Steel 64" x 24' DW Flex Piping Current No
2 Diesel NA 4,000 8/16/1985 Single Wall Steel 64" x 24' DW Flex Piping Current Yes
3 Gasoline NA 4,000 8/16/1985 Single Wall FRP 64" x 24' DW Flex Piping Current No
4 Gasoline NA 4,000 8/16/1985 Single Wall Steel 64" x 24' DW Flex Piping Current No
5 Gasoline NA 12,000 10/07/1997 Single Wall FRP 8' x 31' 11" DW Flex Piping Current Yes
TABLE 2
UST SYSTEM INFORMATION
MIKEYS 1 STATION 19 (INCIDENT NO. 47020)
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
Facility ID #: 00-0-0000021906
Previous
Contents
Page 1 of 1
Date: 07/25/23 Facility ID #: 00-0-0000021906
Well ID Parcel ID No. Well Owner Mailing Address Well Location Address
Well Use
(Potable/
Agriculture, etc.)
Public Water
Connected
Distance from
source area of
release
(ft.)
WSW-1 117009 China Grove Apartments, LLC 8950 Caldwell Road
Mount Ulla, NC 28125
255 Shoe Road
China Grove, NC 28023 Not in Use Yes ~540 NW
WSW-2 117161 Casie Loraine Caudill 208 Beaver Street
China Grove, NC 28023
208 Beaver Street
China Grove, NC 28023 Potable No, Available ~980 S
WSW-3 117169 Keith Watson & WF Rebecca Watson 255 Red Fox Lane
China Grove, NC 28023
255 Red Fox Lane
China Grove, NC 28023 Potable No ~1,250 N
WSW-4 117034 Bentley's Rentals Inc.Post Office Box 626
Concord, NC 28026
1435 N. Main Street
China Grove, NC 28023 Not in Use Yes ~1,100 NE
WSW-5 117028 Ruby G. Winecoff 295 Red Fox Lane
China Grove, NC 28023
295 Red Fox Lane
China Grove, NC 28023 Potable No ~1,340 N
WSW-6 117029A John E. & Tara L. Loeb 3201 Cold Springs Road South
Concord, NC 28025
265 Red Fox Lane
China Grove, NC 28023 Potable No ~1,290 N
WSW-7 117180 Gary Propst et al.1925 East NC 152 Highway
China Grove, NC 28023
1925 E NC 152 Hwy
China Grove, NC 28023 Potable No ~1,170 NE
WSW-8 117032 Daniel Landaverde Martinez & WF
Maria Azucena Orozco Hernandez
155 Red Fox Lane
China Grove, NC 28023
155 Red Fox Lane
China Grove, NC 28023 Potable No ~1,100 NE
WSW-9 117033 Deborah Robson et al.5316 Randolph Road
Kannapolis, NC 28081
135 Red Fox Lane
China Grove, NC 28023 Potable No ~1,160 NE
WSW-10 117037 James Michael Gentry et al.6531 Weldon Circle
Concord, NC 28027
1515 N. Main Street
China Grove, NC 28023 Potable No ~1,300 NE
Notes:
• Water supply wells are shown on Figure 3A
• Ft. BGS : Feet below ground surface
TABLE 3
RECEPTOR INFORMATION
MIKEYS 1 STATION 19 (INCIDENT NO. 47020)
Page 1 of 1
Date: 06/29/20 Facility ID #: 00-0-0000021906
Parcel I.D. Property Owner Name Property Owner Address
117203 (site) SNS Group LLC P.O. Box 4329
Mooresville, NC 28117
117022 Panjwani Investments LLC P.O. Box 4329
Mooresville, NC 28117
117048 Food Lion LLC P.O. Box 1330
Salisbury, NC 28145
11705002 NC Department of Transportation 1546 Mail Service Center
Raleigh, NC 27611
117057 William Todd Morrison 6211 Kentwood Drive
Kannapolis, NC 28081
117154 Walter H. Reese 1302 N. Main Street
China Grove, NC 28023
Note:
• Properties are keyed to Figure 3A.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
MIKEYS 1 STATION 19 (INCIDENT NO. 47020)
Page 1 of 1
Date: 07/24/23 Facility ID #: 00-0-0000021906
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Ground Water
Elevation
(ft.)
Comments
06/09/20 13.04 ---86.96
09/15/20 13.38 ---86.62
09/15/21 13.40 ---86.60
09/27/21 13.58 ---86.42
06/02/22 14.43 ---85.57
06/29/23 13.48 ---86.52
09/15/20 13.64 ---86.32
09/15/21 13.56 ---86.40
09/27/21 13.73 ---86.23
06/02/22 14.62 ---85.34
06/29/23 13.73 ---86.23
09/15/20 13.53 ---86.09
09/15/21 13.13 ---86.49
09/27/21 13.26 ---86.36
06/02/22 13.97 ---85.65
06/29/23 12.65 ---86.97
09/15/20 16.40 ---83.53
09/15/21 14.04 ---85.89
09/27/21 13.57 ---86.36
06/02/22 15.59 ---84.34
06/29/23 10.20 ---89.73
09/15/21 18.28 ---81.10
09/27/21 11.25 ---88.13
06/02/22 10.05 ---89.33
06/29/23 9.60 ---89.78
09/15/21 15.50 ---82.63
09/27/21 15.03 ---83.10
06/02/22 15.11 ---83.02
06/29/23 10.68 ---87.45
09/14/21
09/13/21
99.38
98.13
20
20
10 - 20
10 - 20
10
10
MW-5
MW-6
10 10 - 20
10 10 - 20
10 10 - 20
20 99.96
20 99.62
20 99.93
MW-2 09/15/20
MW-3 09/15/20
MW-4 09/15/20
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
MIKEYS 1 STATION 19 (INCIDENT NO. 47020)
MW-1 06/08/20 10 10 - 20 20 100.00
Page 1 of 2
Date: 07/24/23 Facility ID #: 00-0-0000021906
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Ground Water
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
MIKEYS 1 STATION 19 (INCIDENT NO. 47020)
09/15/21 14.49 ---84.91
09/27/21 13.94 ---85.46
06/02/22 14.90 ---84.50
06/29/23 13.89 ---85.51
09/15/21 14.10 ---86.62
09/27/21 14.28 ---86.44
06/02/22 15.19 ---85.53
06/29/23 14.34 ---86.38
MW-9 06/28/23 06/29/23 10 10 - 20 20 101.06 14.41 ---86.65
MW-10 06/28/23 06/29/23 10 10 - 20 20 101.81 15.40 ---86.41
09/15/21 13.55 ---86.54
09/27/21 13.62 ---86.47
06/02/22 14.57 ---85.52
06/29/23 13.65 ---86.44
Notes:
• ft BGS : feet below ground surface.
• NM: Not measured.
09/13/21
09/14/21
09/14/21
99.40
100.72
100.09
20
20
40
10 - 20
10 - 20
35 - 40
10
10
35
MW-7
MW-8
TW-1
Page 2 of 2
Date: 07/24/23 Facility ID #: 00-0-0000021906
EPA
504.1 EPA 6010
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 40 0.6 10 0.4 3 0.4 70 70 5 70 0.7 400 400 0.02 3 1 30 15 400 700 200 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 NE 10,000 400 3,000 400 30,500 70,000 5,000 26,100 700 28,500 24,100 50 135 1,000 12,000 15,000 NE NE NE NE NE NE
06/09/20 3,120 707 1,770 3,200 273 642 6,030 <13 <200 <13 <20 <13 53.3 128 <100 142 <13 817 263 <0.0091 <9.5 140 275 70.3 13,200 3,340 J 7,150 7,210 <50 589 J
09/15/21 462 59.3 192 305 839 62.8 5,020 <2.5 2,790 <2.5 5.2 J <2.5 8.8 J 121 5.2 J 25.2 <2.5 146 52.5 NR NR NR NR NR NR NR NR NR NR NR
06/02/22 34.6 2.3 15.6 23.9 647 E 10.0 4,170 <0.13 2,570 <0.13 2.4 <0.13 1.7 101 1.4 JB 3.8 <0.13 11.7 6.7 NR <1.1 4.1 J 7.6 NR NR NR NR NR NR NR
06/29/23 751 <22.0 89.9 <21.0 753 <47.0 6,020 <16.0 3,850 <19.0 <22.0 <15.0 <18.0 159 <33.0 <19.0 <22.0 <19.0 <18.0 NR <3.49 2.10 2.57 NR NR NR NR NR NR NR
09/15/20 3280 16.4 J <13 <25 57.0 111 8,120 <13 <200 <13 <20 118 17.4 J 251 <100 <13 <13 <13 <13 NR <1.0 7.2 13.1 11.6 3,320 245 54.1 J <49 <49 688
09/15/21 2,810 14.0 J <13 <25 470 117 9,640 <13 952 J <13 <20 83.2 16.4 J 241 <20 <13 <13 <13 <13 NR NR NR NR NR NR NR NR NR NR NR
06/02/22 2,970 21.3 J <13 <25 112 185 5,980 <13 <200 <13 <20 93.3 23.6 J 264 157 JB <13 <13 <13 <13 NR <1.0 7.7 15.9 NR NR NR NR NR NR NR
06/29/23 0.721 <0.220 <0.170 <0.210 21.7 <0.470 <1.90 <0.160 <1.60 <0.190 <0.220 <0.150 <0.180 0.866 <0.330 <0.190 <0.220 <0.190 <0.180 NR <3.46 <1.14 <0.666 NR NR NR NR NR NR NR
09/15/20 28.0 0.31 J 0.71 2.8 29.8 12.0 339 <0.13 477 <0.13 <0.20 <0.13 1.5 17.9 <1.0 0.54 <0.13 0.86 <0.13 NR <1.0 1.0 J 0.81 J <5.0 101 <35 <35 <50 <50 207
09/15/21 0.64 J <0.63 13.7 <1.3 20.8 1.1 J 1,240 <0.63 1,350 <0.63 <1.0 <0.63 5.1 116 <1.0 10.3 <0.63 <0.63 <0.63 NR NR NR NR NR NR NR NR NR NR NR
06/02/22 183 3.5 66.9 3.3 J 22.1 33.4 1,080 <0.31 1,610 <0.31 <0.50 0.46 J 10 134 10.9 B 22.0 <0.31 11.5 0.68 J NR <0.99 7.9 0.73 J NR NR NR NR NR NR NR
06/29/23 75.5 6.70 11.3 3.66 12.2 11.0 599 JH <0.160 955 <0.190 5.20 <0.150 3.57 124 <0.330 7.32 <0.220 0.249 J <0.180 NR <3.46 4.13 <0.666 NR NR NR NR NR NR NR
09/15/20 684 135 780 1,030 465 435 1,360 <1.3 1,870 <1.3 2.1 J <1.3 83.6 36.5 10.1 J 245 4.8 J 532 158 NR <9.9 107 164 55.0 4,870 3,620 1,280 825 <49 533
09/15/21 962 352 2,160 7,710 698 1,010 2,570 <13 3,680 <13 36.6 J <13 143 145 36.6 J 442 <13 3,450 904 NR NR NR NR NR NR NR NR NR NR NR
06/02/22 931 74.1 1,790 6,210 498 1,080 <200 <13 964 J <13 27.2 J <13 195 124 151 JB 586 <13 3,600 967 NR <9.6 528 1,280 NR NR NR NR NR NR NR
06/29/23 330 114 241 1,820 63.5 J <47.0 209 J <16.0 178 J <19.0 <22.0 <15.0 <18.0 <50.0 <33.0 46.1 J <22.0 1,120 344 NR 4.32 J 23.6 33.4 NR NR NR NR NR NR NR
09/27/21 0.50 <0.13 <0.13 2.6 4.2 <0.13 <2.0 <0.13 9.8 J <0.13 <0.20 <0.13 0.20 J 1.6 <1.0 0.21 J <0.13 0.35 J 0.20 J <0.0093 1.4 J <0.50 <0.57 6.9 <35 <35 <35 <50 59.8 JB NA
06/02/22 <0.63 <0.63 <0.63 1.3 J 3.8 <0.63 <4.0 <0.63 <4.0 <0.63 <1.0 <0.63 <0.63 1.8 7.7 JB <0.63 <0.63 <0.63 <0.63 NR <0.96 <0.50 <0.58 NR NR NR NR NR NR NR
06/29/23 0.429 J 0.233 J <0.170 <0.210 1.88 <0.470 <1.90 <0.160 4.34 J <0.190 <0.220 <0.150 <0.180 1.15 <0.330 <0.190 <0.220 0.299 J <0.180 NR 3.58 J <1.15 <0.672 NR NR NR NR NR NR NR
09/27/21 <0.13 <0.13 0.26 J 0.31 J <0.13 <0.13 <2.0 <0.13 <2.0 <0.13 <0.20 <0.13 <0.13 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13 <0.0092 <0.95 <0.50 <0.57 <5.0 <35 <35 <35 <48 52.4 JB NA
06/02/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.13 <2.0 <0.13 <0.20 <0.13 <0.13 <0.13 1.1 JB <0.13 <0.13 <0.13 <0.13 NR <0.96 <0.50 <0.58 NR NR NR NR NR NR NR
06/29/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.160 <1.60 <0.190 <0.220 <0.150 <0.180 <0.500 <0.330 <0.190 <0.220 <0.190 <0.180 NR <3.46 <1.14 <0.666 NR NR NR NR NR NR NR
09/27/21 <0.13 <0.13 0.14 J 0.26 J <0.13 <0.13 <2.0 <0.13 <2.0 <0.13 <0.20 <0.13 <0.13 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13 <0.0094 <0.95 <0.50 <0.57 12.6 <35 <35 <35 <50 53.1 JB NA
06/02/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <0.13 <2.0 <0.13 <0.20 <0.13 <0.13 1.0 1.2 JB <0.13 <0.13 <0.13 <0.13 NR <0.96 <0.50 <0.58 NR NR NR NR NR NR NR
06/29/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.160 <1.60 <0.190 <0.220 <0.150 <0.180 <0.500 <0.330 <0.190 <0.220 <0.190 <0.180 NR <3.84 <1.27 <0.739 NR NR NR NR NR NR NR
09/15/21 1,010 99.1 697 4,530 <6.3 343 3,360 <6.3 <100 <6.3 <10 9.7 J 53.2 20.7 J 147 B 111 <6.3 1,030 298 0.15 <1.0 27.0 66.4 <5.0 4,970 J <35 8,030 <190 <190 987 B
06/02/22 691 61.0 322 2,100 <3.1 187 1,740 <3.1 <50 <3.1 <5.0 9.4 J 25.5 15.8 234 B 44.2 <3.1 429 134 NR <0.96 14.1 33.3 NR NR NR NR NR NR NR
06/29/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.160 <1.60 <0.190 <0.220 <0.150 <0.180 <0.500 <0.330 <0.190 <0.220 <0.190 <0.180 NR <3.84 <1.27 <0.739 NR NR NR NR NR NR NR
MW-9 06/29/23 2,420 423 1,520 9,670 <14.0 2,620 4,910 <16.0 <160 <19.0 <22.0 <15.0 91.1 80.1 <33.0 188 <22.0 1,630 458 NR <3.84 24.2 63.5 NR NR NR NR NR NR NR
MW-10 06/29/23 1.69 0.751 9.01 60.4 <0.140 4.92 <1.90 <0.160 <1.60 <0.190 <0.220 <0.150 1.28 <0.500 <0.330 2.90 <0.220 22.5 7.38 NR <3.84 <1.27 1.27 J NR NR NR NR NR NR NR
09/15/21 0.25 J 0.78 <0.13 <0.25 <0.13 0.26 J <2.0 2.9 <2.0 0.58 <0.20 <0.13 <0.13 <0.13 1.0 JB <0.13 <0.13 <0.13 <0.13 <0.0037 <0.95 <0.50 <0.57 <10 <35 <35 <35 <98 <98 1,320 B
06/02/22 6.0 <0.13 <0.13 3.7 <0.13 2.3 <2.0 <0.13 <2.0 <0.13 <0.20 <0.13 1.1 0.23 J 1.2 JB <0.13 <0.13 1.3 0.63 NR <1.0 0.69 J 1.4 J NR NR NR NR NR NR NR
06/29/23 5.99 <0.220 <0.170 3.99 J <0.140 <0.470 <1.90 <0.160 <1.60 <0.190 <0.220 <0.150 0.662 <0.500 <0.330 <0.190 <0.220 2.39 0.885 NR <3.46 <1.14 <0.666 NR NR NR NR NR NR NR
09/14/21 <0.13 0.50 <0.13 <0.25 <0.13 0.26 J NR <0.13 NR <0.13 <0.20 <0.13 <0.13 <0.13 <0.20 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR
06/02/22 <0.13 1.9 <0.13 <0.25 <0.13 <0.13 NR <0.13 NR <0.13 <0.20 <0.13 <0.13 <0.13 2.2 B <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR NR
06/29/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR <0.160 NR <0.190 <0.220 <0.150 <0.180 <0.500 <0.330 <0.190 <0.220 <0.190 <0.180 NR NR NR NR NR NR NR NR NR NR NR
Notes:• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• 2B Standard: North Carolina surface water standards for Class C waters specified in T15A NCAC 2B.0200 or EPA Nathional Criteria.
• < : Less than the method detection limit specified in the laboratory report.• GCL: Gross contamination level.
• Concentrations in bold face type indicate the MAC was below the reported concentration.
• Underlined results indicate 10 times the 2B Standards were below the reported concentrations.
• Results in italics indicate the GCLs were below the reported concentrations. • J: Estimated value.
• B: Analyte found in associated Method Blank.
• NA: Not Analyzed.
• NE: Not established.• S: Toxicity exceeds solubility, no visible sheen or free product in water or on sediment or shoreline per 15A NCAC 02B .0211 & .0220
• NR: Not reported.
• Refer to laboratory report for other detectable concentrations which did not exceed the MACs.
EPA 625.1
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TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MIKEYS 1 STATION 19 (INCIDENT NO. 47020)
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Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence
Site Name City / County /Rowan Incident #47020
Resp Pty Name / Contact Incident Mgr Region MOR
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #2
Consultant / Project Mgr /Joanna R Alley
Telephone / Fax Number /Task Authorization Number:3 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:H-135-D RRA Date:3/8/2021
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
w Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
3r
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d
?
Task #Lab /
SubCode RO

A
u
t
h
Proposed
Rate/Price
(Consultant)CO

A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
3.101 60 /feet Y $12.50 Y $750.00 $750.00 /
3.113 60 /feet Y $50.00 Y $3,000.00 $3,000.00 /
3.118 60 /feet Y $5.00 Y $300.00 $300.00 /
3.351 3 /wells Y $80.00 Y $240.00 $240.00 /
3.397 1 /Mobe Y $100.00 Y $100.00 $100.00 /
3.398 1 /Mobe Y $350.00 Y $350.00 $350.00 /
4.031 12 /wells Y $110.00 Y $1,320.00 $1,320.00 /
4.090 #240 12 /samples Y $94.00 Y $1,128.00 $1,128.00 /
4.090 #272 1 /sample Y $66.00 Y $66.00 $66.00 /
4.090 #301 12 /samples Y $208.00 Y $2,496.00 $2,496.00 /
4.091 1 /shipment Y $60.00 Y $60.00 $60.00 /
6.090 1 /report Y $1,125.00 Y $1,125.00 $1,125.00 /
12.050 1 /trip Y $250.00 Y $250.00 $250.00 /
12.055 1 /trip Y $50.00 Y $50.00 $50.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$11,235.00 $11,235.00 TOTAL:
Total Standard Costs (Not Third Party)$11,235.00 $11,235.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:3/16/23 by:(PM)(Reserved for RO)
RO Review:4/14/23 by:(IM)Joint UST Preapproval Confirmed By:Date1
CO Review:4/18/23 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
DIRECTED COSTS
China Grove
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Mikeys 1 Station 19
Note: This Electronic Preapproval Task Authorization (ePATA) shall be used to receive preapproval from the UST Section. A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If, following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form, you must complete and submit a separate ePATA request
designated as a "Change Order"inthe provided space above prior to conducting those tasks. Include a copy of the prior ePATA form for confirmation. Please attach this formto
the cover of the corresponding claim when requesting reimbursement. IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion dateof the FIRST completed task to remain within the Statuteof Limitations. All ePATAs submitted within a claim are closed with that
claim, and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed. Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
RCM
LP
(Initials)
JRA
Proposed
Units / Type
(Consultant)
Ryan Mills
ActiveYES
22-701 April 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
[e-mail]
SNS Group, LLC Salim Nimji
Geological Resources, Inc.
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management
4/18/2023
Site Name City / County /Rowan Incident #47020
Resp Pty Name / Contact Incident Mgr Region MOR
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #3
Consultant / Project Mgr /Joanna R Alley
Telephone / Fax Number /Task Authorization Number:3 ChangeOrd:1
Project Mgr Email Site Risk / Rank / Abatement:H-135-D RRA Date:3/8/2021
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
w Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
3r
d

P
t
y

D
e
d
?
Task #Lab /
SubCode RO

A
u
t
h
Proposed
Rate/Price
(Consultant)CO

A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
3.080 1 /permit Y $250.00 Y $250.00 $250.00 /
3.310 1 /agreement Y $625.00 Y $625.00 $625.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$875.00 $875.00 TOTAL:
Total Standard Costs (Not Third Party)$875.00 $875.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:4/24/23 by:(PM)(Reserved for RO)
RO Review:4/24/23 by:(IM)Joint UST Preapproval Confirmed By:Date1
CO Review:4/24/23 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
JRA
Proposed
Units / Type
(Consultant)
Ryan Mills
ActiveYES
23-273 May 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
1
[e-mail]
SNS Group, LLC Salim Nimji
Geological Resources, Inc.
DIRECTED COSTS
China Grove
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Mikeys 1 Station 19
Note: This Electronic Preapproval Task Authorization (ePATA) shall be used to receive preapproval from the UST Section. A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If, following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form, you must complete and submit a separate ePATA request
designated as a "Change Order"inthe provided space above prior to conducting those tasks. Include a copy of the prior ePATA form for confirmation. Please attach this formto
the cover of the corresponding claim when requesting reimbursement. IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion dateof the FIRST completed task to remain within the Statuteof Limitations. All ePATAs submitted within a claim are closed with that
claim, and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed. Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
RCM
LP
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management
4/24/2023

APPENDIX B
Land Use Information
Date: 10/8/21 Facility ID # : 00-0-0000021906
Map ID No. Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
1 China Grove Middle School RT School 1013 North Main Street
China Grove, NC 28023 ~850
n/a HB Highway Business n/a n/a
n/a NC Neighborhood Center n/a n/a
n/a RMH Manufactured Home n/a n/a
n/a RM Mixed Residential n/a n/a
n/a RT Town Residential n/a n/a
n/a RS Suburban Residential n/a n/a
n/a LI Light Industrial n/a n/a
Note:
• Properties are keyed to Figure 3.
APPENDIX B
LAND USE INFORMATION
MIKEYS 1 STATION 19 (INCIDENT NO. 47020)
Page 1 of 1

APPENDIX C
Incident Report
NCDEQ Incident Report
RP/Company SNS GROUP LLC
RPAddress POB 4329
RPCity MOORESVILLE
Contact ALI SAMEER
RPState NC
TELEPHONE [phone]
IncidentNumber 47020 USTNum MO-27703
IncidentName MIKEYS 1, STATION 19
FacilID
Address 1407 N. MAIN STREET
CityTown CHINA GROVE State
ZipCode 28023-
DateOccurred 5 /8 /2020
DateReported 5 /11/2020
ConfRisk H
CloseOut
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr RABLongitude-80.565818 Latitude 35.578228
County ROWAN
LSA2 10/6/2020 3/8/2021
CSAM 12/13/2021 12/22/2021
Thursday, June 23, 2022 Page 1 of 1

APPENDIX D
Subsurface Logs and Well Construction Records

North Carolina Department of Environmental Quality | Division of Water Resources
Mooresville Regional Office | 601 East Center Avenue, Suite 301 | Mooresville, NC 28115
704.663.1699
June 19, 2023

Mr. Salim Nimji
SNS Group, LLC
1407 N. Main St.
China Grove, NC 20023
RE: Monitoring Well Construction Permit
Permit # WM0301291
1407 N. Main St., China Grove
Rowan County

Dear Mr. Nimji,

In accordance with your completed application received on June 14, 2023, we are forwarding
herewith Monitoring Well Construction Permit Numbered WM0301291 and issued for the
construction of one (1) monitoring well located near the subject site in China Grove, Rowan County.

This Permit will be effective for one year from the date of issuance and shall be subject to the
conditions and limitations as specified therein.

Should you have any questions, please contact Edward Watson at [phone], or by
email at [e-mail].

Sincerely,

Andrew H. Pitner, P.G., Regional Supervisor
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources

CC: WQROS, Central Office (via Laserfiche)
Joanna Alley, Geological Resources, Inc. (via email)

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES
PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL
In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws,
Rules and Regulations.
PERMISSION IS HEREBY GRANTED TO
SNS Group, LLC (Geological Resources, Inc. as Agent)

FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of one (1) monitoring well owned by SNS Group,
LLC, at the subject site located at 1407 N. Main St., in China Grove, Rowan County. This Permit is issued in accordance
with the application received on June 14 2023, in conformity with specifications and supporting data, all of which are filed
with the Department of Environmental Quality and are considered integral parts of this Permit.
This Permit is for well construction only, and does not waive any provision or requirement of any other applicable law or
regulation. Construction of any well under this Permit shall be in strict compliance with the North Carolina Well Construction
Regulations and Standards (15A NCAC 02C .0100), and other State and Local Laws and regulations pertaining to well
construction.

If any requirements or limitations specified in this Permit are unacceptable, you have a right to an adjudicatory hearing upon
written request within 30 days of receipt of this Permit. The request must be in the form of a written petition conforming to
Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service
Center, Raleigh, North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding.
This Permit will be effective for one year from the date of its issuance and shall be subject to other specified conditions,
limitations, or exceptions as follows:

1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these wells are being installed as
part of an investigation for contamination from an underground storage tank or dry cleaner incident.
2. Issuance of this Permit does not supersede any other agreement, permit, or requirement issued by another agency.
3. The well(s) shall be located and constructed as shown on the attachments submitted as part of the Permit application.
4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC 02C .0108(o).
5. Well construction records (GW-1) for each well shall be submitted to the Division of Water Resources’ Information
Processing Unit within 30 days of the well completion.
6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A NCAC 02C .0113 and a
well abandonment record (GW-30) shall be submitted to the Division of Water Resources’ Information Processing
Unit within 30 days of the well abandonment.
7. If the well penetrates any water-bearing zone that contains contaminated waters, the upper three feet of the well
shall be grouted within one day after the casing is set or the well abandoned.
8. Temporary wells must be permanently abandoned or converted to a permanent well within seven days (168 hours)
of completion of drilling the borehole.

Permit issued the 19th day of June 2023

FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION

_______________________________________________
Andrew H. Pitner, P.G., Regional Supervisor
Division of Water Resources
By Authority of the Environmental Management Commission
Permit No. # WM0301291
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Mikeys 1 Station 19
4486
06/28/23
L. Weathersby
Geological Resources, Inc.
Matt Steele
Solid Flight Auger
4548-A
MW-9
6"
20
Well installed at completion
0 1 Silt/gravel brown
1 12 Silt red Dry
12 15 Silt red Moist
15 20 Fine sand brown Wet

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM -MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Mikeys 1 Station 19
4486
06/28/23
L. Weathersby
Geological Resources, Inc.
Matt Steele
Solid Flight Auger
4548-A
MW-9
6"
101.06
14.41
8 20
6 8
0 6
0 10 2
10 20 2
6
8
20
10
20
WELL CONSTRUCTION RECORD
This form canbe usedforsingle or multiple wells
FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013
1.Well Contractor Information:
Well ContractorName
NC WellContractor Certification Number
CompanyName
2.Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3.Well Use (check well use):
Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)□Irrigation
Non-Water Supply Well:□Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks)
4.Date Well(s)Completed:____________Well ID#______________________
5a.Well Location:
Facility/Owner Name Facility ID#(if applicable)

Physical Address,City,and Zip
County Parcel Identification No.(PIN)
5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient)
N W
6.Is (are)the well(s):□Permanent or □Temporary
7.Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
9.Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below topof casing: (ft.)If water level is above casing, use “+”
11.Borehole diameter: (in.)
12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.)
FOR WATER SUPPLY WELLS ONLY:
13a.Yield (gpm) Method oftest:
13b.Disinfection type:Amount:
14.WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16.INNER CASING OR TUBING(geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS
22.Certification:
Signatureof Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617
24b.For Injection Wells ONLY:In addition to sending the form to the address in
24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636
24c.For Water Supply &Injection Wells:
Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed.
For Internal UseONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
WM0301291
06/28/23 MW-9
Mikeys 1 Station 19 0-0000021906
1407 North Main Street, China Grove, NC
Rowan 5636-01-49-4142
35.578228 80.565818
1
20
14.41
6"
Solid Flight Auger
0 10 2 Sch 40 PVC
10 20 2 0.010 Sch 40 PVC
0 6 grout pour
6 8 bentonite pour
8 20 #2 Sand Pour
0 1 Silt/gravel
1 12 Silt
12 15 Silt
15 20 Fine sand
06/28/23
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Mikeys 1 Station 19
4486
06/28/23
L. Weathersby
Geological Resources, Inc.
Matt Steele
Solid Flight Auger
4548-A
MW-10
6"
20
Well installed at completion
0 1 Silt/gravel brown Dry
1 10 Silt red Dry
10 14 Silt tan Moist
14 20 Fine sand brown Wet

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM -MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Mikeys 1 Station 19
4486
06/28/23
L. Weathersby
Geological Resources, Inc.
Matt Steele
Solid Flight Auger
4548-A
MW-10
6"
101.81
15.40
8 20
6 8
0 6
0 10 2
10 20 2
6
8
20
10
20
WELL CONSTRUCTION RECORD
This form canbe usedforsingle or multiple wells
FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013
1.Well Contractor Information:
Well ContractorName
NC WellContractor Certification Number
CompanyName
2.Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3.Well Use (check well use):
Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)□Irrigation
Non-Water Supply Well:□Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks)
4.Date Well(s)Completed:____________Well ID#______________________
5a.Well Location:
Facility/Owner Name Facility ID#(if applicable)

Physical Address,City,and Zip
County Parcel Identification No.(PIN)
5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient)
N W
6.Is (are)the well(s):□Permanent or □Temporary
7.Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
9.Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below topof casing: (ft.)If water level is above casing, use “+”
11.Borehole diameter: (in.)
12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.)
FOR WATER SUPPLY WELLS ONLY:
13a.Yield (gpm) Method oftest:
13b.Disinfection type: Amount:
14.WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16.INNER CASING OR TUBING(geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS
22.Certification:
Signatureof Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617
24b.For Injection Wells ONLY:In addition to sending the form to the address in
24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636
24c.For Water Supply &Injection Wells:
Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed.
For Internal UseONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
WM0101291
06/28/23 MW-10
Mikeys 1 Station 19 0-0000021906
1407 North Main Street, China Grove, NC
Rowan 5636-01-49-4142
35.578228 80.565818
1
20
15.40
6"
Solid Flight Auger
0 10 2 Sch 40 PVC
10 20 2 0.010 Sch 40 PVC
0 6 grout pour
6 8 bentonite pour
8 20 #2 Sand Pour
0 1 Silt/gravel
1 10 Silt
10 14 Silt
14 20 Fine sand
06/28/23

APPENDIX E
Historical Soil Quality Information
Date: 12/6/21 Facility ID #: 00-0-0000021906
MADEP
EPH
Sa
m
p
l
e

I
D
Da
t
e

C
o
l
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c
t
e
d

(m
m
/
d
d
/
y
y
)
Sa
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D
e
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(f
t
-
B
G
S
)
Ga
s
o
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-
R
a
n
g
e

T
P
H
Di
e
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e
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-
R
a
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e

T
P
H
Be
n
z
e
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To
l
u
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Et
h
y
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To
t
a
l

X
y
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MT
B
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B
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a
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Te
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(P
C
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)
C5
-
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8

A
l
i
p
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a
t
i
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-
C
1
2

A
l
i
p
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a
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s
t
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d

C
9
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A
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50 100 NE NE NE NE NE NE NE NE NE NE NE
NE NE 0.0056 4.3 4.9 4.6 0.1 16.0 0.0074 68 540 31 31
NE NE 18 1,200 1,560 3,129 350 9,385 1.1 939 1,500 469 469
SB-D-2'04/15/20 2 455 102 NR NR NR NR NR NR NR NR NR NR NR
SB-R-2'04/15/20 2 526 402 NR NR NR NR NR NR NR NR NR NR NR
MW-1 (5')11/28/18 5 NR NR 0.0026 J <0.015 <0.0015 <0.0031 <0.0015 0.0243 J <0.0019 <3.9 <3.9 <3.9 6.76 JB
MW-1 (10')11/28/18 10 NR NR <0.0012 <0.0099 <0.00099 <0.0021 0.0116 0.0469 0.0017 J <2.3 <2.3 <2.3 <4.8
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• UVF samples analyzed in the field
• Trip Blank results reported in ug/l (micrograms per liter)
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• < : Less than the method detection limit specified in the laboratory report
• NE: Not Established
• NR: Not Re Requested
• J: Estimated concentration.
• B: Analyte reported in associated blank.
UVF
TABLE 6
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
MIKEYS 1 STATION 19 (INCIDENT NO. 47020)
Analytical Method →MADEP VPHEPA Method 8260B
• Refer to laboratory report for other detectable concentrations which did not exceed the MACs.
RAL (mg/kg)
Soil to Water MCC (mg/kg)
Residential SCLs (mg/kg)
Page 1 of 1
47020

APPENDIX F
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

7/20/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-181-0037 Client Project Description: Mickey's 1, Station 19
GRI #4486
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/30/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 133
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-181-0037
Page 2 of 133
Report Number:
Sample Summary Table
Client Project Description:
23-181-0037
Mickey's 1, Station 19
GRI #4486
Lab No Client Sample ID Matrix Date Collected Date Received
06/29/2023 07:28Aqueous 99734 Trip Blanks 06/30/2023 10:00
06/29/2023 08:21Aqueous 99735 TW-1 06/30/2023 10:00
06/29/2023 08:36Aqueous 99736 MW-1 06/30/2023 10:00
06/29/2023 08:50Aqueous 99737 MW-2 06/30/2023 10:00
06/29/2023 09:04Aqueous 99738 MW-3 06/30/2023 10:00
06/29/2023 09:17Aqueous 99739 MW-4 06/30/2023 10:00
06/29/2023 09:31Aqueous 99740 MW-5 06/30/2023 10:00
06/29/2023 09:47Aqueous 99741 MW-6 06/30/2023 10:00
06/29/2023 10:02Aqueous 99742 MW-7 06/30/2023 10:00
06/29/2023 10:16Aqueous 99743 MW-8 06/30/2023 10:00
06/29/2023 10:29Aqueous 99744 MW-9 06/30/2023 10:00
06/29/2023 10:43Aqueous 99745 MW-10 06/30/2023 10:00
Page 3 of 133
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-181-0037
Report Limit
Project:Mickey's 1, Station 19
V 99735TW-1
5.99 07/11/2023 17:026200BBenzeneµg/L 0.180
J0.251 07/11/2023 17:026200Bn-Butylbenzene µg/L 0.180
J0.249 07/11/2023 17:026200Bsec-Butyl benzene µg/L 0.200
0.662 07/11/2023 17:026200BIsopropylbenzeneµg/L 0.180
2.39 07/11/2023 17:026200B1,2,4-Trimethylbenzene µg/L 0.190
0.885 07/11/2023 17:026200B1,3,5-Trimethylbenzene µg/L 0.180
3.04 07/11/2023 17:026200Bo-Xylene µg/L 0.210
J0.949 07/11/2023 17:026200Bm,p-Xylene µg/L 0.420
J3.99 07/11/2023 17:026200BXylene (Total)µg/L 0.210
J1.20 07/06/2023 15:11625.1 Naphthalene µg/L 0.728
V 99736MW-1
751 07/11/2023 22:066200BBenzeneµg/L 18.0
159 07/11/2023 22:066200BDi-Isopropyl Ether (DIPE)µg/L 50.0
89.9 07/11/2023 22:066200BEthylbenzeneµg/L 17.0
753 07/11/2023 22:066200BMethyl tert-butyl ether (MTBE)µg/L 14.0
3850 07/11/2023 22:066200Btert-Butyl Alcohol (TBA)µg/L 160
6020 07/11/2023 22:066200Btert-Amyl Alcohol (TAA)µg/L 190
J33.8 07/11/2023 22:066200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
J0.936 07/06/2023 15:34625.1 2,6-Dinitrotoluene µg/L 0.817
2.10 07/06/2023 15:34625.1 1-Methylnaphthalene µg/L 1.15
2.57 07/06/2023 15:34625.1 2-Methylnaphthalene µg/L 0.672
9.45 07/06/2023 15:34625.1 Naphthalene µg/L 0.735
V 99737MW-2
0.721 07/11/2023 17:296200BBenzeneµg/L 0.180
0.866 07/11/2023 17:296200BDi-Isopropyl Ether (DIPE)µg/L 0.500
21.7 07/11/2023 17:296200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J0.603 07/11/2023 17:296200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
V 99738MW-3
30.5 07/11/2023 17:576200BAcetoneµg/L 1.80
75.5 07/11/2023 17:576200BBenzeneµg/L 0.180
1.14 07/11/2023 17:576200Bn-Butylbenzene µg/L 0.180
0.739 07/11/2023 17:576200Bsec-Butyl benzene µg/L 0.200
5.20 07/11/2023 17:576200BChloromethaneµg/L 0.220
124 07/12/2023 17:146200BDi-Isopropyl Ether (DIPE)µg/L 5.00
11.3 07/11/2023 17:576200BEthylbenzeneµg/L 0.170
Page 4 of 133
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-181-0037
Report Limit
Project:Mickey's 1, Station 19
V 99738MW-3
3.57 07/11/2023 17:576200BIsopropylbenzeneµg/L 0.180
12.2 07/11/2023 17:576200BMethyl tert-butyl ether (MTBE)µg/L 0.140
11.0 07/11/2023 17:576200BNaphthaleneµg/L 0.470
7.32 07/11/2023 17:576200Bn-Propylbenzene µg/L 0.190
955 07/12/2023 17:146200Btert-Butyl Alcohol (TBA)µg/L 16.0
J59907/14/2023 21:506200Btert-Amyl Alcohol (TAA)µg/L 190
J4.39 07/11/2023 17:576200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
6.70 07/11/2023 17:576200BTolueneµg/L 0.220
J0.249 07/11/2023 17:576200B1,2,4-Trimethylbenzene µg/L 0.190
1.37 07/11/2023 17:576200Bo-Xylene µg/L 0.210
2.29 07/11/2023 17:576200Bm,p-Xylene µg/L 0.420
3.66 07/11/2023 17:576200BXylene (Total)µg/L 0.210
4.13 07/06/2023 16:19625.1 1-Methylnaphthalene µg/L 1.14
8.79 07/06/2023 16:19625.1 Naphthalene µg/L 0.728
V 99739MW-4
330 07/11/2023 22:336200BBenzeneµg/L 18.0
241 07/11/2023 22:336200BEthylbenzeneµg/L 17.0
J63.5 07/11/2023 22:336200BMethyl tert-butyl ether (MTBE)µg/L 14.0
J46.1 07/11/2023 22:336200Bn-Propylbenzene µg/L 19.0
J17807/11/2023 22:336200Btert-Butyl Alcohol (TBA)µg/L 160
J20907/11/2023 22:336200Btert-Amyl Alcohol (TAA)µg/L 190
114 07/11/2023 22:336200BTolueneµg/L 22.0
1120 07/11/2023 22:336200B1,2,4-Trimethylbenzene µg/L 19.0
344 07/11/2023 22:336200B1,3,5-Trimethylbenzene µg/L 18.0
221 07/11/2023 22:336200Bo-Xylene µg/L 21.0
1600 07/11/2023 22:336200Bm,p-Xylene µg/L 42.0
1820 07/11/2023 22:336200BXylene (Total)µg/L 21.0
J4.32 07/06/2023 16:41625.1 Bis(2-ethylhexyl)phthalate µg/L 3.49
J12.9 07/06/2023 16:41625.1 2,4-Dimethylphenol µg/L 1.59
23.6 07/06/2023 16:41625.1 1-Methylnaphthalene µg/L 1.15
33.4 07/06/2023 16:41625.1 2-Methylnaphthalene µg/L 0.672
52.9 07/06/2023 16:41625.1 Naphthalene µg/L 0.735
V 99740MW-5
10.8 07/13/2023 22:246200BAcetoneµg/L 1.80
J0.429 07/13/2023 22:246200BBenzeneµg/L 0.180
1.15 07/13/2023 22:246200BDi-Isopropyl Ether (DIPE)µg/L 0.500
Page 5 of 133
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-181-0037
Report Limit
Project:Mickey's 1, Station 19
V 99740MW-5
J0.252 07/13/2023 22:246200B4-Isopropyl toluene µg/L 0.089
J2.36 07/13/2023 22:246200BMethyl Ethyl Ketone (MEK)µg/L 0.710
1.88 07/13/2023 22:246200BMethyl tert-butyl ether (MTBE)µg/L 0.140
2.70 07/13/2023 22:246200B4-Methyl-2-Pentanone µg/L 0.078
J4.34 07/13/2023 22:246200Btert-Butyl Alcohol (TBA)µg/L 1.60
J0.233 07/13/2023 22:246200BTolueneµg/L 0.220
J0.299 07/13/2023 22:246200B1,2,4-Trimethylbenzene µg/L 0.190
J1.11 07/06/2023 17:04625.1 Benzoic Acid µg/L 1.11
J3.58 07/06/2023 17:04625.1 Bis(2-ethylhexyl)phthalate µg/L 3.49
V 99743MW-8
J0.922 07/11/2023 19:206200BMethyl Ethyl Ketone (MEK)µg/L 0.710
V 99744MW-9
2420 07/11/2023 20:446200BBenzeneµg/L 18.0
J23.3 07/11/2023 20:446200Bn-Butylbenzene µg/L 18.0
80.1 07/11/2023 20:446200BDi-Isopropyl Ether (DIPE)µg/L 50.0
1520 07/11/2023 20:446200BEthylbenzeneµg/L 17.0
91.1 07/11/2023 20:446200BIsopropylbenzeneµg/L 18.0
2620 07/11/2023 20:446200BNaphthaleneµg/L 47.0
188 07/11/2023 20:446200Bn-Propylbenzene µg/L 19.0
4910 07/11/2023 20:446200Btert-Amyl Alcohol (TAA)µg/L 190
423 07/11/2023 20:446200BTolueneµg/L 22.0
1630 07/11/2023 20:446200B1,2,4-Trimethylbenzene µg/L 19.0
458 07/11/2023 20:446200B1,3,5-Trimethylbenzene µg/L 18.0
2970 07/11/2023 20:446200Bo-Xylene µg/L 21.0
6700 07/11/2023 20:446200Bm,p-Xylene µg/L 42.0
9670 07/11/2023 20:446200BXylene (Total)µg/L 21.0
J3.11 07/06/2023 18:34625.1 2,4-Dimethylphenol µg/L 1.74
24.2 07/06/2023 18:34625.1 1-Methylnaphthalene µg/L 1.27
63.5 07/06/2023 18:34625.1 2-Methylnaphthalene µg/L 0.739
295 07/07/2023 11:33625.1 Naphthalene µg/L 1.62
V 99745MW-10
J7.08 07/11/2023 14:316200BAcetoneµg/L 1.80
1.69 07/11/2023 14:316200BBenzeneµg/L 0.180
0.717 07/11/2023 14:316200Bn-Butylbenzene µg/L 0.180
J0.421 07/11/2023 14:316200Bsec-Butyl benzene µg/L 0.200
Page 6 of 133
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-181-0037
Report Limit
Project:Mickey's 1, Station 19
V 99745MW-10
9.01 07/11/2023 14:316200BEthylbenzeneµg/L 0.170
1.28 07/11/2023 14:316200BIsopropylbenzeneµg/L 0.180
J0.480 07/11/2023 14:316200B4-Isopropyl toluene µg/L 0.089
J0.324 07/11/2023 14:316200B4-Methyl-2-Pentanone µg/L 0.078
4.92 07/11/2023 14:316200BNaphthaleneµg/L 0.470
2.90 07/11/2023 14:316200Bn-Propylbenzene µg/L 0.190
0.751 07/11/2023 14:316200BTolueneµg/L 0.220
22.5 07/11/2023 14:316200B1,2,4-Trimethylbenzene µg/L 0.190
7.38 07/11/2023 14:316200B1,3,5-Trimethylbenzene µg/L 0.180
17.3 07/11/2023 14:316200Bo-Xylene µg/L 0.210
43.1 07/11/2023 14:316200Bm,p-Xylene µg/L 0.420
60.4 07/11/2023 14:316200BXylene (Total)µg/L 0.210
J1.27 07/06/2023 18:56625.1 2-Methylnaphthalene µg/L 0.739
3.32 07/06/2023 18:56625.1 Naphthalene µg/L 0.808
Page 7 of 133

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Mickey's 1, Station 19 Lab Report Number: 23-181-0037
Date: 7/20/2023
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1 Sample 99742 (MW-7) Analyte: 2-Fluorobiphenyl
QC Batch No: V34997/V34962 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Analyte: Benzidine
QC Batch No: V34997/V34962 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Volatile Organic Compounds - GC/MS Method 6200B Sample 99738 (MW-3) QC Batch No: V35409/V35241
The analysis for this sample was performed outside the EPA required holding time. Original sample was run within hold. Sample dilution run outside of hold, but confirms original results.
Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V35244/V35241 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Dichlorodifluoromethane
QC Batch No: V35348/V35241 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Ethanol QC Batch No: V35229/V35241 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: tert-Butyl formate
QC Batch No: V35348/V35241 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Page 8 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
99734 Matrix:
6/29/2023 7:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 07/11/23 15:11 V35244ENM
<0.180 µg/L 0.180 0.500Benzene 1 07/11/23 15:11 V35244ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 15:11 V35244ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 15:11 V35244ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 15:11 V35244ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 15:11 V35244ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 15:11 V35244ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 15:11 V35244ENM
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 15:11 V35244ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 15:11 V35244ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 15:11 V35244ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 15:11 V35244ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 15:11 V35244ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 15:11 V35244ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 15:11 V35244ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 07/11/23 15:11 V35244ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 15:11 V35244ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 15:11 V35244ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/11/23 15:11 V35244ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 15:11 V35244ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 15:11 V35244ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 15:11 V35244ENM
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 15:11 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 9 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
99734 Matrix:
6/29/2023 7:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 15:11 V35244ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 15:11 V35244ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 15:11 V35244ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 15:11 V35244ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 15:11 V35244ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 15:11 V35244ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 15:11 V35244ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 15:11 V35244ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 15:11 V35244ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 15:11 V35244ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 15:11 V35244ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 15:11 V35244ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 15:11 V35244ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 15:11 V35244ENM
<42.0 µg/L 42.0 200Ethanol 1 07/11/23 15:11 V35244ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 15:11 V35244ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 15:11 V35244ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 15:11 V35244ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 15:11 V35244ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 15:11 V35244ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 15:11 V35244ENM
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 15:11 V35244ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 15:11 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 10 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
99734 Matrix:
6/29/2023 7:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 15:11 V35244ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 07/11/23 15:11 V35244ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 15:11 V35244ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/11/23 15:11 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 15:11 V35244ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 15:11 V35244ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 15:11 V35244ENM
<0.220 µg/L 0.220 0.500Toluene 1 07/11/23 15:11 V35244ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 15:11 V35244ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 15:11 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 15:11 V35244ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 15:11 V35244ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 15:11 V35244ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 15:11 V35244ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 15:11 V35244ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 15:11 V35244ENM
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 15:11 V35244ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 15:11 V35244ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 15:11 V35244ENM
<0.210 µg/L 0.210 0.500o-Xylene 1 07/11/23 15:11 V35244ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/11/23 15:11 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 11 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
99734 Matrix:
6/29/2023 7:28
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/11/23 15:11 V35244
Surrogate: 4-Bromofluorobenzene 93.8 Limits: 70-130%07/11/23 15:111 ENM V35244
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%07/11/23 15:111 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 94.0 Limits: 70-130%07/11/23 15:111 ENM V35244
Surrogate: Toluene-d8 91.6 Limits: 70-130%07/11/23 15:111 ENM V35244
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 12 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:TW-1
99735 Matrix:
6/29/2023 8:21
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/11/23 17:02 6200BENM
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%07/11/23 17:021 ENM V35244
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%07/11/23 17:021 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 92.4 Limits: 70-130%07/11/23 17:021 ENM V35244
Surrogate: Toluene-d8 92.0 Limits: 70-130%07/11/23 17:021 ENM V35244
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 13 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:TW-1
99735 Matrix:
6/29/2023 8:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 07/11/23 17:02 V35244ENM
5.99 µg/L 0.180 0.500Benzene 1 07/11/23 17:02 V35244ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 17:02 V35244ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 17:02 V35244ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 17:02 V35244ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 17:02 V35244ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 17:02 V35244ENM
0.251 J µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 17:02 V35244ENM
0.249 J µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 17:02 V35244ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 17:02 V35244ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 17:02 V35244ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 17:02 V35244ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 17:02 V35244ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 17:02 V35244ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 17:02 V35244ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 07/11/23 17:02 V35244ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 17:02 V35244ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 17:02 V35244ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/11/23 17:02 V35244ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 17:02 V35244ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 17:02 V35244ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 17:02 V35244ENM
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 17:02 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 14 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:TW-1
99735 Matrix:
6/29/2023 8:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 17:02 V35244ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 17:02 V35244ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 17:02 V35244ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 17:02 V35244ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 17:02 V35244ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 17:02 V35244ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 17:02 V35244ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 17:02 V35244ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 17:02 V35244ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 17:02 V35244ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 17:02 V35244ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 17:02 V35244ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 17:02 V35244ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 17:02 V35244ENM
<42.0 µg/L 42.0 200Ethanol 1 07/11/23 17:02 V35244ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 17:02 V35244ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 17:02 V35244ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 17:02 V35244ENM
0.662 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 17:02 V35244ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 17:02 V35244ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 17:02 V35244ENM
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 17:02 V35244ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 17:02 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 15 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:TW-1
99735 Matrix:
6/29/2023 8:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 17:02 V35244ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 07/11/23 17:02 V35244ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 17:02 V35244ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/11/23 17:02 V35244ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/11/23 17:02 V35244ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/11/23 17:02 V35244ENM
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/11/23 17:02 V35244ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/11/23 17:02 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 17:02 V35244ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 17:02 V35244ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 17:02 V35244ENM
<0.220 µg/L 0.220 0.500Toluene 1 07/11/23 17:02 V35244ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 17:02 V35244ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 17:02 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 17:02 V35244ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 17:02 V35244ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 17:02 V35244ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 17:02 V35244ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 17:02 V35244ENM
2.39 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 17:02 V35244ENM
0.885 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 17:02 V35244ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 17:02 V35244ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 17:02 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 16 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:TW-1
99735 Matrix:
6/29/2023 8:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
3.04 µg/L 0.210 0.500o-Xylene 1 07/11/23 17:02 V35244ENM
0.949 J µg/L 0.420 1.00m,p-Xylene 1 07/11/23 17:02 V35244ENM
3.99 J µg/L 0.210 0.500Xylene (Total)1 07/11/23 17:02 V35244
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%07/11/23 17:021 ENM V35244
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%07/11/23 17:021 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 92.4 Limits: 70-130%07/11/23 17:021 ENM V35244
Surrogate: Toluene-d8 92.0 Limits: 70-130%07/11/23 17:021 ENM V35244
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.302 µg/L 0.302 2.00Acenaphthene 1 07/06/23 15:11 V34997AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 07/06/23 15:11 V34997AMP
<0.836 µg/L 0.836 2.00Anthracene 1 07/06/23 15:11 V34997AMP
<1.32 M µg/L 1.32 10.0Benzidine 1 07/06/23 15:11 V34997AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 07/06/23 15:11 V34997AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 07/06/23 15:11 V34997AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 07/06/23 15:11 V34997AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 07/06/23 15:11 V34997AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 07/06/23 15:11 V34997AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 07/06/23 15:11 V34997AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 07/06/23 15:11 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 17 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:TW-1
99735 Matrix:
6/29/2023 8:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 07/06/23 15:11 V34997AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 07/06/23 15:11 V34997AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 07/06/23 15:11 V34997AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 07/06/23 15:11 V34997AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 07/06/23 15:11 V34997AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 07/06/23 15:11 V34997AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 07/06/23 15:11 V34997AMP
<7.38 µg/L 7.38 20.02-Chloronaphthalene 1 07/06/23 15:11 V34997AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 07/06/23 15:11 V34997AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 07/06/23 15:11 V34997AMP
<0.405 µg/L 0.405 2.00Chrysene 1 07/06/23 15:11 V34997AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 07/06/23 15:11 V34997AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 07/06/23 15:11 V34997AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 07/06/23 15:11 V34997AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 07/06/23 15:11 V34997AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 07/06/23 15:11 V34997AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 07/06/23 15:11 V34997AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 07/06/23 15:11 V34997AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 07/06/23 15:11 V34997AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 07/06/23 15:11 V34997AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 07/06/23 15:11 V34997AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 07/06/23 15:11 V34997AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 07/06/23 15:11 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 18 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:TW-1
99735 Matrix:
6/29/2023 8:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 07/06/23 15:11 V34997AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 07/06/23 15:11 V34997AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 07/06/23 15:11 V34997AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 07/06/23 15:11 V34997AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 07/06/23 15:11 V34997AMP
<0.807 µg/L 0.807 2.00Fluorene 1 07/06/23 15:11 V34997AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 07/06/23 15:11 V34997AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 07/06/23 15:11 V34997AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 07/06/23 15:11 V34997AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 07/06/23 15:11 V34997AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 07/06/23 15:11 V34997AMP
<0.444 µg/L 0.444 5.00Isophorone 1 07/06/23 15:11 V34997AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 07/06/23 15:11 V34997AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 07/06/23 15:11 V34997AMP
1.20 J µg/L 0.728 2.00Naphthalene 1 07/06/23 15:11 V34997AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 07/06/23 15:11 V34997AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 07/06/23 15:11 V34997AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 07/06/23 15:11 V34997AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 07/06/23 15:11 V34997AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 07/06/23 15:11 V34997AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 07/06/23 15:11 V34997AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 07/06/23 15:11 V34997AMP
<0.651 µg/L 0.651 5.00Phenol 1 07/06/23 15:11 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 19 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:TW-1
99735 Matrix:
6/29/2023 8:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.434 µg/L 0.434 2.00Pyrene 1 07/06/23 15:11 V34997AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 07/06/23 15:11 V34997AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 07/06/23 15:11 V34997AMP
625.1Surrogate: Phenol-d5 21.0 Limits: 10-63%07/06/23 15:111 AMP
Surrogate: 2-Fluorobiphenyl 66.2 Limits: 49-118%07/06/23 15:111 AMP V34997
Surrogate: 2-Fluorophenol 35.0 Limits: 22-84%07/06/23 15:111 AMP V34997
Surrogate: Nitrobenzene-d5 58.4 Limits: 43-123%07/06/23 15:111 AMP V34997
Surrogate: 4-Terphenyl-d14 78.2 Limits: 49-151%07/06/23 15:111 AMP V34997
Surrogate: 2,4,6-Tribromophenol 62.1 Limits: 31-144%07/06/23 15:111 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 20 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-1
99736 Matrix:
6/29/2023 8:36
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 07/11/23 22:06 6200BENM
Surrogate: 4-Bromofluorobenzene 92.8 Limits: 70-130%07/11/23 22:06100 ENM V35244
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%07/11/23 22:06100 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%07/11/23 22:06100 ENM V35244
Surrogate: Toluene-d8 91.6 Limits: 70-130%07/11/23 22:06100 ENM V35244
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 21 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-1
99736 Matrix:
6/29/2023 8:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<180 µg/L 180 1000Acetone 100 07/11/23 22:06 V35244ENM
751 µg/L 18.0 50.0Benzene 100 07/11/23 22:06 V35244ENM
<21.0 µg/L 21.0 50.0Bromobenzene 100 07/11/23 22:06 V35244ENM
<42.0 µg/L 42.0 100Bromochloromethane 100 07/11/23 22:06 V35244ENM
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 07/11/23 22:06 V35244ENM
<150 µg/L 150 500Bromoform 100 07/11/23 22:06 V35244ENM
<28.0 µg/L 28.0 100Bromomethane 100 07/11/23 22:06 V35244ENM
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 07/11/23 22:06 V35244ENM
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 07/11/23 22:06 V35244ENM
<92.0 µg/L 92.0 200tert-Butyl benzene 100 07/11/23 22:06 V35244ENM
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 07/11/23 22:06 V35244ENM
<19.0 µg/L 19.0 50.0Chlorobenzene 100 07/11/23 22:06 V35244ENM
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 07/11/23 22:06 V35244ENM
<43.0 µg/L 43.0 100Chloroethane 100 07/11/23 22:06 V35244ENM
<22.0 µg/L 22.0 50.0Chloroform 100 07/11/23 22:06 V35244ENM
<22.0 µg/L 22.0 50.0Chloromethane 100 07/11/23 22:06 V35244ENM
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 07/11/23 22:06 V35244ENM
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 07/11/23 22:06 V35244ENM
159 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 07/11/23 22:06 V35244ENM
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 07/11/23 22:06 V35244ENM
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 07/11/23 22:06 V35244ENM
<23.0 µg/L 23.0 50.0Dibromomethane 100 07/11/23 22:06 V35244ENM
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 07/11/23 22:06 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 22 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-1
99736 Matrix:
6/29/2023 8:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 07/11/23 22:06 V35244ENM
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 07/11/23 22:06 V35244ENM
<120 µg/L 120 500Dichlorodifluoromethane 100 07/11/23 22:06 V35244ENM
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 07/11/23 22:06 V35244ENM
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 07/11/23 22:06 V35244ENM
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 07/11/23 22:06 V35244ENM
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 07/11/23 22:06 V35244ENM
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 07/11/23 22:06 V35244ENM
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 07/11/23 22:06 V35244ENM
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 07/11/23 22:06 V35244ENM
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 07/11/23 22:06 V35244ENM
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 07/11/23 22:06 V35244ENM
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 07/11/23 22:06 V35244ENM
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 07/11/23 22:06 V35244ENM
<4200 µg/L 4200 20000Ethanol 100 07/11/23 22:06 V35244ENM
89.9 µg/L 17.0 50.0Ethylbenzene 100 07/11/23 22:06 V35244ENM
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 07/11/23 22:06 V35244ENM
<38.0 µg/L 38.0 1002-Hexanone 100 07/11/23 22:06 V35244ENM
<18.0 µg/L 18.0 50.0Isopropylbenzene 100 07/11/23 22:06 V35244ENM
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 07/11/23 22:06 V35244ENM
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 07/11/23 22:06 V35244ENM
753 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 07/11/23 22:06 V35244ENM
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 07/11/23 22:06 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 23 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-1
99736 Matrix:
6/29/2023 8:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<33.0 µg/L 33.0 200Methylene Chloride 100 07/11/23 22:06 V35244ENM
<47.0 µg/L 47.0 100Naphthalene 100 07/11/23 22:06 V35244ENM
<19.0 µg/L 19.0 50.0n-Propylbenzene 100 07/11/23 22:06 V35244ENM
<22.0 µg/L 22.0 50.0Styrene 100 07/11/23 22:06 V35244ENM
3850 µg/L 160 1000tert-Butyl Alcohol (TBA)100 07/11/23 22:06 V35244ENM
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 07/11/23 22:06 V35244ENM
6020 µg/L 190 1000tert-Amyl Alcohol (TAA)100 07/11/23 22:06 V35244ENM
33.8 J µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 07/11/23 22:06 V35244ENM
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 07/11/23 22:06 V35244ENM
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 07/11/23 22:06 V35244ENM
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 07/11/23 22:06 V35244ENM
<22.0 µg/L 22.0 50.0Toluene 100 07/11/23 22:06 V35244ENM
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 07/11/23 22:06 V35244ENM
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 07/11/23 22:06 V35244ENM
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 07/11/23 22:06 V35244ENM
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 07/11/23 22:06 V35244ENM
<18.0 µg/L 18.0 50.0Trichloroethene 100 07/11/23 22:06 V35244ENM
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 07/11/23 22:06 V35244ENM
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 07/11/23 22:06 V35244ENM
<19.0 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 07/11/23 22:06 V35244ENM
<18.0 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 07/11/23 22:06 V35244ENM
<100 µg/L 100 500Vinyl Acetate 100 07/11/23 22:06 V35244ENM
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 07/11/23 22:06 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 24 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-1
99736 Matrix:
6/29/2023 8:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<21.0 µg/L 21.0 50.0o-Xylene 100 07/11/23 22:06 V35244ENM
<42.0 µg/L 42.0 100m,p-Xylene 100 07/11/23 22:06 V35244ENM
<21 µg/L 21.0 50.0Xylene (Total)100 07/11/23 22:06 V35244
Surrogate: 4-Bromofluorobenzene 92.8 Limits: 70-130%07/11/23 22:06100 ENM V35244
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%07/11/23 22:06100 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%07/11/23 22:06100 ENM V35244
Surrogate: Toluene-d8 91.6 Limits: 70-130%07/11/23 22:06100 ENM V35244
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.305 µg/L 0.305 2.02Acenaphthene 1 07/06/23 15:34 V34997AMP
<0.299 µg/L 0.299 2.02Acenaphthylene 1 07/06/23 15:34 V34997AMP
<0.844 µg/L 0.844 2.02Anthracene 1 07/06/23 15:34 V34997AMP
<1.33 M µg/L 1.33 10.1Benzidine 1 07/06/23 15:34 V34997AMP
<0.643 µg/L 0.643 2.02Benzo(a)anthracene 1 07/06/23 15:34 V34997AMP
<1.03 µg/L 1.03 2.02Benzo(a)pyrene 1 07/06/23 15:34 V34997AMP
<2.51 µg/L 2.51 5.05Benzo(b)fluoranthene 1 07/06/23 15:34 V34997AMP
<1.02 µg/L 1.02 5.05Benzo(g,h,i)perylene 1 07/06/23 15:34 V34997AMP
<2.01 µg/L 2.01 5.05Benzo(k)fluoranthene 1 07/06/23 15:34 V34997AMP
<1.11 µg/L 1.11 10.1Benzoic Acid 1 07/06/23 15:34 V34997AMP
<0.690 µg/L 0.690 5.05Benzyl alcohol 1 07/06/23 15:34 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 25 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-1
99736 Matrix:
6/29/2023 8:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.472 µg/L 0.472 5.05Bis(2-Chloroethoxy)methane 1 07/06/23 15:34 V34997AMP
<1.05 µg/L 1.05 5.05Bis(2-Chloroethyl)ether 1 07/06/23 15:34 V34997AMP
<1.09 µg/L 1.09 5.05Bis(2-Chloroisopropyl)ether 1 07/06/23 15:34 V34997AMP
<3.49 µg/L 3.49 10.1Bis(2-ethylhexyl)phthalate 1 07/06/23 15:34 V34997AMP
<1.12 µg/L 1.12 5.054-Bromophenyl phenyl ether 1 07/06/23 15:34 V34997AMP
<1.85 µg/L 1.85 5.05Butyl benzyl phthalate 1 07/06/23 15:34 V34997AMP
<1.19 µg/L 1.19 5.054-Chloro-3-methylphenol 1 07/06/23 15:34 V34997AMP
<7.45 µg/L 7.45 20.22-Chloronaphthalene 1 07/06/23 15:34 V34997AMP
<0.947 µg/L 0.947 10.12-Chlorophenol 1 07/06/23 15:34 V34997AMP
<1.73 µg/L 1.73 5.054-Chlorophenyl phenyl ether 1 07/06/23 15:34 V34997AMP
<0.409 µg/L 0.409 2.02Chrysene 1 07/06/23 15:34 V34997AMP
<0.438 µg/L 0.438 2.02Dibenz(a,h)anthracene 1 07/06/23 15:34 V34997AMP
<0.864 µg/L 0.864 5.05Dibenzofuran 1 07/06/23 15:34 V34997AMP
<2.02 µg/L 2.02 5.051,2-Dichlorobenzene 1 07/06/23 15:34 V34997AMP
<2.02 µg/L 2.02 5.051,3-Dichlorobenzene 1 07/06/23 15:34 V34997AMP
<2.07 µg/L 2.07 5.051,4-Dichlorobenzene 1 07/06/23 15:34 V34997AMP
<1.91 µg/L 1.91 5.053,3'-Dichlorobenzidine 1 07/06/23 15:34 V34997AMP
<1.47 µg/L 1.47 10.12,4-Dichlorophenol 1 07/06/23 15:34 V34997AMP
<0.752 µg/L 0.752 5.05Diethyl phthalate 1 07/06/23 15:34 V34997AMP
<0.948 µg/L 0.948 5.05Dimethyl phthalate 1 07/06/23 15:34 V34997AMP
<1.59 µg/L 1.59 20.22,4-Dimethylphenol 1 07/06/23 15:34 V34997AMP
<2.08 µg/L 2.08 5.05Di-n-butyl phthalate 1 07/06/23 15:34 V34997AMP
<2.09 µg/L 2.09 10.14,6-Dinitro-2-methylphenol 1 07/06/23 15:34 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 26 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-1
99736 Matrix:
6/29/2023 8:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<1.94 µg/L 1.94 10.12,4-Dinitrophenol 1 07/06/23 15:34 V34997AMP
<1.12 µg/L 1.12 5.052,4-Dinitrotoluene 1 07/06/23 15:34 V34997AMP
0.936 J µg/L 0.817 5.052,6-Dinitrotoluene 1 07/06/23 15:34 V34997AMP
<1.67 µg/L 1.67 5.05Di-n-Octyl Phthalate 1 07/06/23 15:34 V34997AMP
<0.252 µg/L 0.252 2.02Fluoranthene 1 07/06/23 15:34 V34997AMP
<0.815 µg/L 0.815 2.02Fluorene 1 07/06/23 15:34 V34997AMP
<0.988 µg/L 0.988 5.05Hexachlorobenzene 1 07/06/23 15:34 V34997AMP
<2.76 µg/L 2.76 5.05Hexachlorobutadiene 1 07/06/23 15:34 V34997AMP
<2.07 µg/L 2.07 5.05Hexachlorocyclopentadiene 1 07/06/23 15:34 V34997AMP
<1.78 µg/L 1.78 5.05Hexachloroethane 1 07/06/23 15:34 V34997AMP
<0.481 µg/L 0.481 2.02Indeno(1,2,3-cd)pyrene 1 07/06/23 15:34 V34997AMP
<0.448 µg/L 0.448 5.05Isophorone 1 07/06/23 15:34 V34997AMP
2.10 µg/L 1.15 2.021-Methylnaphthalene 1 07/06/23 15:34 V34997AMP
2.57 µg/L 0.672 2.022-Methylnaphthalene 1 07/06/23 15:34 V34997AMP
9.45 µg/L 0.735 2.02Naphthalene 1 07/06/23 15:34 V34997AMP
<0.914 µg/L 0.914 5.05Nitrobenzene 1 07/06/23 15:34 V34997AMP
<0.497 µg/L 0.497 5.052-Nitrophenol 1 07/06/23 15:34 V34997AMP
<1.24 µg/L 1.24 10.14-Nitrophenol 1 07/06/23 15:34 V34997AMP
<1.11 µg/L 1.11 5.05N-Nitrosodiphenylamine 1 07/06/23 15:34 V34997AMP
<0.647 µg/L 0.647 5.05N-Nitroso-di-n-propylamine 1 07/06/23 15:34 V34997AMP
<1.44 µg/L 1.44 5.05Pentachlorophenol 1 07/06/23 15:34 V34997AMP
<0.432 µg/L 0.432 2.02Phenanthrene 1 07/06/23 15:34 V34997AMP
<0.657 µg/L 0.657 5.05Phenol 1 07/06/23 15:34 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 27 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-1
99736 Matrix:
6/29/2023 8:36
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.438 µg/L 0.438 2.02Pyrene 1 07/06/23 15:34 V34997AMP
<2.23 µg/L 2.23 5.051,2,4-Trichlorobenzene 1 07/06/23 15:34 V34997AMP
<1.33 µg/L 1.33 5.052,4,6-Trichlorophenol 1 07/06/23 15:34 V34997AMP
625.1Surrogate: Phenol-d5 28.2 Limits: 10-63%07/06/23 15:341 AMP
Surrogate: 2-Fluorobiphenyl 67.9 Limits: 49-118%07/06/23 15:341 AMP V34997
Surrogate: 2-Fluorophenol 41.7 Limits: 22-84%07/06/23 15:341 AMP V34997
Surrogate: Nitrobenzene-d5 63.2 Limits: 43-123%07/06/23 15:341 AMP V34997
Surrogate: 4-Terphenyl-d14 76.2 Limits: 49-151%07/06/23 15:341 AMP V34997
Surrogate: 2,4,6-Tribromophenol 61.5 Limits: 31-144%07/06/23 15:341 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 28 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
99737 Matrix:
6/29/2023 8:50
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/11/23 17:29 6200BENM
Surrogate: 4-Bromofluorobenzene 94.6 Limits: 70-130%07/11/23 17:291 ENM V35244
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%07/11/23 17:291 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 93.0 Limits: 70-130%07/11/23 17:291 ENM V35244
Surrogate: Toluene-d8 92.4 Limits: 70-130%07/11/23 17:291 ENM V35244
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 29 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
99737 Matrix:
6/29/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 07/11/23 17:29 V35244ENM
0.721 µg/L 0.180 0.500Benzene 1 07/11/23 17:29 V35244ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 17:29 V35244ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 17:29 V35244ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 17:29 V35244ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 17:29 V35244ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 17:29 V35244ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 17:29 V35244ENM
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 17:29 V35244ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 17:29 V35244ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 17:29 V35244ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 17:29 V35244ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 17:29 V35244ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 17:29 V35244ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 17:29 V35244ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 07/11/23 17:29 V35244ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 17:29 V35244ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 17:29 V35244ENM
0.866 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/11/23 17:29 V35244ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 17:29 V35244ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 17:29 V35244ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 17:29 V35244ENM
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 17:29 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 30 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
99737 Matrix:
6/29/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 17:29 V35244ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 17:29 V35244ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 17:29 V35244ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 17:29 V35244ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 17:29 V35244ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 17:29 V35244ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 17:29 V35244ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 17:29 V35244ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 17:29 V35244ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 17:29 V35244ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 17:29 V35244ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 17:29 V35244ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 17:29 V35244ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 17:29 V35244ENM
<42.0 µg/L 42.0 200Ethanol 1 07/11/23 17:29 V35244ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 17:29 V35244ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 17:29 V35244ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 17:29 V35244ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 17:29 V35244ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 17:29 V35244ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 17:29 V35244ENM
21.7 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 17:29 V35244ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 17:29 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 31 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
99737 Matrix:
6/29/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 17:29 V35244ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 07/11/23 17:29 V35244ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 17:29 V35244ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/11/23 17:29 V35244ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/11/23 17:29 V35244ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/11/23 17:29 V35244ENM
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/11/23 17:29 V35244ENM
0.603 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/11/23 17:29 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 17:29 V35244ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 17:29 V35244ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 17:29 V35244ENM
<0.220 µg/L 0.220 0.500Toluene 1 07/11/23 17:29 V35244ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 17:29 V35244ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 17:29 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 17:29 V35244ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 17:29 V35244ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 17:29 V35244ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 17:29 V35244ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 17:29 V35244ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 17:29 V35244ENM
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 17:29 V35244ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 17:29 V35244ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 17:29 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 32 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
99737 Matrix:
6/29/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 07/11/23 17:29 V35244ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/11/23 17:29 V35244ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/11/23 17:29 V35244
Surrogate: 4-Bromofluorobenzene 94.6 Limits: 70-130%07/11/23 17:291 ENM V35244
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%07/11/23 17:291 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 93.0 Limits: 70-130%07/11/23 17:291 ENM V35244
Surrogate: Toluene-d8 92.4 Limits: 70-130%07/11/23 17:291 ENM V35244
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.302 µg/L 0.302 2.00Acenaphthene 1 07/06/23 15:56 V34997AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 07/06/23 15:56 V34997AMP
<0.836 µg/L 0.836 2.00Anthracene 1 07/06/23 15:56 V34997AMP
<1.32 M µg/L 1.32 10.0Benzidine 1 07/06/23 15:56 V34997AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 07/06/23 15:56 V34997AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 07/06/23 15:56 V34997AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 07/06/23 15:56 V34997AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 07/06/23 15:56 V34997AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 07/06/23 15:56 V34997AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 07/06/23 15:56 V34997AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 07/06/23 15:56 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 33 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
99737 Matrix:
6/29/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 07/06/23 15:56 V34997AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 07/06/23 15:56 V34997AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 07/06/23 15:56 V34997AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 07/06/23 15:56 V34997AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 07/06/23 15:56 V34997AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 07/06/23 15:56 V34997AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 07/06/23 15:56 V34997AMP
<7.38 µg/L 7.38 20.02-Chloronaphthalene 1 07/06/23 15:56 V34997AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 07/06/23 15:56 V34997AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 07/06/23 15:56 V34997AMP
<0.405 µg/L 0.405 2.00Chrysene 1 07/06/23 15:56 V34997AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 07/06/23 15:56 V34997AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 07/06/23 15:56 V34997AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 07/06/23 15:56 V34997AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 07/06/23 15:56 V34997AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 07/06/23 15:56 V34997AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 07/06/23 15:56 V34997AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 07/06/23 15:56 V34997AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 07/06/23 15:56 V34997AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 07/06/23 15:56 V34997AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 07/06/23 15:56 V34997AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 07/06/23 15:56 V34997AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 07/06/23 15:56 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 34 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
99737 Matrix:
6/29/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 07/06/23 15:56 V34997AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 07/06/23 15:56 V34997AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 07/06/23 15:56 V34997AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 07/06/23 15:56 V34997AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 07/06/23 15:56 V34997AMP
<0.807 µg/L 0.807 2.00Fluorene 1 07/06/23 15:56 V34997AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 07/06/23 15:56 V34997AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 07/06/23 15:56 V34997AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 07/06/23 15:56 V34997AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 07/06/23 15:56 V34997AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 07/06/23 15:56 V34997AMP
<0.444 µg/L 0.444 5.00Isophorone 1 07/06/23 15:56 V34997AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 07/06/23 15:56 V34997AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 07/06/23 15:56 V34997AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 07/06/23 15:56 V34997AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 07/06/23 15:56 V34997AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 07/06/23 15:56 V34997AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 07/06/23 15:56 V34997AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 07/06/23 15:56 V34997AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 07/06/23 15:56 V34997AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 07/06/23 15:56 V34997AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 07/06/23 15:56 V34997AMP
<0.651 µg/L 0.651 5.00Phenol 1 07/06/23 15:56 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 35 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-2
99737 Matrix:
6/29/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.434 µg/L 0.434 2.00Pyrene 1 07/06/23 15:56 V34997AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 07/06/23 15:56 V34997AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 07/06/23 15:56 V34997AMP
625.1Surrogate: Phenol-d5 24.5 Limits: 10-63%07/06/23 15:561 AMP
Surrogate: 2-Fluorobiphenyl 62.6 Limits: 49-118%07/06/23 15:561 AMP V34997
Surrogate: 2-Fluorophenol 39.6 Limits: 22-84%07/06/23 15:561 AMP V34997
Surrogate: Nitrobenzene-d5 55.4 Limits: 43-123%07/06/23 15:561 AMP V34997
Surrogate: 4-Terphenyl-d14 71.8 Limits: 49-151%07/06/23 15:561 AMP V34997
Surrogate: 2,4,6-Tribromophenol 55.7 Limits: 31-144%07/06/23 15:561 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 36 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
99738 Matrix:
6/29/2023 9:04
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/11/23 17:57 6200BENM
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%07/11/23 17:571 ENM V35244
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%07/11/23 17:571 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 93.6 Limits: 70-130%07/11/23 17:571 ENM V35244
Surrogate: Toluene-d8 93.8 Limits: 70-130%07/11/23 17:571 ENM V35244
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/12/23 17:1410 MSA V35303
Surrogate: Dibromofluoromethane 95.0 Limits: 70-130%07/12/23 17:1410 MSA V35303
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%07/12/23 17:1410 MSA V35303
Surrogate: Toluene-d8 92.4 Limits: 70-130%07/12/23 17:1410 MSA V35303
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/14/23 21:50100 MSA V35409
Surrogate: Dibromofluoromethane 101 Limits: 70-130%07/14/23 21:50100 MSA V35409
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%07/14/23 21:50100 MSA V35409
Surrogate: Toluene-d8 98.2 Limits: 70-130%07/14/23 21:50100 MSA V35409
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 37 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
99738 Matrix:
6/29/2023 9:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00 V35302 07/12/23 09:00
V35406 07/14/23 09:00
30.5 µg/L 1.80 10.0Acetone 1 07/11/23 17:57 V35244ENM
75.5 µg/L 0.180 0.500Benzene 1 07/11/23 17:57 V35244ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 17:57 V35244ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 17:57 V35244ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 17:57 V35244ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 17:57 V35244ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 17:57 V35244ENM
1.14 µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 17:57 V35244ENM
0.739 µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 17:57 V35244ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 17:57 V35244ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 17:57 V35244ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 17:57 V35244ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 17:57 V35244ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 17:57 V35244ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 17:57 V35244ENM
5.20 µg/L 0.220 0.500Chloromethane 1 07/11/23 17:57 V35244ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 17:57 V35244ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 17:57 V35244ENM
124 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 07/12/23 17:14 V35303MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 17:57 V35244ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 17:57 V35244ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 17:57 V35244ENM
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 17:57 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 38 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
99738 Matrix:
6/29/2023 9:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00 V35302 07/12/23 09:00
V35406 07/14/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 17:57 V35244ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 17:57 V35244ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 17:57 V35244ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 17:57 V35244ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 17:57 V35244ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 17:57 V35244ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 17:57 V35244ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 17:57 V35244ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 17:57 V35244ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 17:57 V35244ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 17:57 V35244ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 17:57 V35244ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 17:57 V35244ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 17:57 V35244ENM
<42.0 µg/L 42.0 200Ethanol 1 07/11/23 17:57 V35244ENM
11.3 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 17:57 V35244ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 17:57 V35244ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 17:57 V35244ENM
3.57 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 17:57 V35244ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 17:57 V35244ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 17:57 V35244ENM
12.2 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 17:57 V35244ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 17:57 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 39 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
99738 Matrix:
6/29/2023 9:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00 V35302 07/12/23 09:00
V35406 07/14/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 17:57 V35244ENM
11.0 µg/L 0.470 1.00Naphthalene 1 07/11/23 17:57 V35244ENM
7.32 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 17:57 V35244ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/11/23 17:57 V35244ENM
955 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 07/12/23 17:14 V35303MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/11/23 17:57 V35244ENM
599 JH µg/L 190 1000tert-Amyl Alcohol (TAA)100 07/14/23 21:50 V35409MSA
4.39 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/11/23 17:57 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 17:57 V35244ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 17:57 V35244ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 17:57 V35244ENM
6.70 µg/L 0.220 0.500Toluene 1 07/11/23 17:57 V35244ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 17:57 V35244ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 17:57 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 17:57 V35244ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 17:57 V35244ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 17:57 V35244ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 17:57 V35244ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 17:57 V35244ENM
0.249 J µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 17:57 V35244ENM
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 17:57 V35244ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 17:57 V35244ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 17:57 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 40 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
99738 Matrix:
6/29/2023 9:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00 V35302 07/12/23 09:00
V35406 07/14/23 09:00
1.37 µg/L 0.210 0.500o-Xylene 1 07/11/23 17:57 V35244ENM
2.29 µg/L 0.420 1.00m,p-Xylene 1 07/11/23 17:57 V35244ENM
3.66 µg/L 0.210 0.500Xylene (Total)1 07/11/23 17:57 V35244
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%07/11/23 17:571 ENM V35244
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%07/11/23 17:571 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 93.6 Limits: 70-130%07/11/23 17:571 ENM V35244
Surrogate: Toluene-d8 93.8 Limits: 70-130%07/11/23 17:571 ENM V35244
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/12/23 17:1410 MSA V35303
Surrogate: Dibromofluoromethane 95.0 Limits: 70-130%07/12/23 17:1410 MSA V35303
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%07/12/23 17:1410 MSA V35303
Surrogate: Toluene-d8 92.4 Limits: 70-130%07/12/23 17:1410 MSA V35303
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/14/23 21:50100 MSA V35409
Surrogate: Dibromofluoromethane 101 Limits: 70-130%07/14/23 21:50100 MSA V35409
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%07/14/23 21:50100 MSA V35409
Surrogate: Toluene-d8 98.2 Limits: 70-130%07/14/23 21:50100 MSA V35409
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.302 µg/L 0.302 2.00Acenaphthene 1 07/06/23 16:19 V34997AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 07/06/23 16:19 V34997AMP
<0.836 µg/L 0.836 2.00Anthracene 1 07/06/23 16:19 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 41 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
99738 Matrix:
6/29/2023 9:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<1.32 M µg/L 1.32 10.0Benzidine 1 07/06/23 16:19 V34997AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 07/06/23 16:19 V34997AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 07/06/23 16:19 V34997AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 07/06/23 16:19 V34997AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 07/06/23 16:19 V34997AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 07/06/23 16:19 V34997AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 07/06/23 16:19 V34997AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 07/06/23 16:19 V34997AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 07/06/23 16:19 V34997AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 07/06/23 16:19 V34997AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 07/06/23 16:19 V34997AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 07/06/23 16:19 V34997AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 07/06/23 16:19 V34997AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 07/06/23 16:19 V34997AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 07/06/23 16:19 V34997AMP
<7.38 µg/L 7.38 20.02-Chloronaphthalene 1 07/06/23 16:19 V34997AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 07/06/23 16:19 V34997AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 07/06/23 16:19 V34997AMP
<0.405 µg/L 0.405 2.00Chrysene 1 07/06/23 16:19 V34997AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 07/06/23 16:19 V34997AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 07/06/23 16:19 V34997AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 07/06/23 16:19 V34997AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 07/06/23 16:19 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 42 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
99738 Matrix:
6/29/2023 9:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 07/06/23 16:19 V34997AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 07/06/23 16:19 V34997AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 07/06/23 16:19 V34997AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 07/06/23 16:19 V34997AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 07/06/23 16:19 V34997AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 07/06/23 16:19 V34997AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 07/06/23 16:19 V34997AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 07/06/23 16:19 V34997AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 07/06/23 16:19 V34997AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 07/06/23 16:19 V34997AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 07/06/23 16:19 V34997AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 07/06/23 16:19 V34997AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 07/06/23 16:19 V34997AMP
<0.807 µg/L 0.807 2.00Fluorene 1 07/06/23 16:19 V34997AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 07/06/23 16:19 V34997AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 07/06/23 16:19 V34997AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 07/06/23 16:19 V34997AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 07/06/23 16:19 V34997AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 07/06/23 16:19 V34997AMP
<0.444 µg/L 0.444 5.00Isophorone 1 07/06/23 16:19 V34997AMP
4.13 µg/L 1.14 2.001-Methylnaphthalene 1 07/06/23 16:19 V34997AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 07/06/23 16:19 V34997AMP
8.79 µg/L 0.728 2.00Naphthalene 1 07/06/23 16:19 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 43 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-3
99738 Matrix:
6/29/2023 9:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.905 µg/L 0.905 5.00Nitrobenzene 1 07/06/23 16:19 V34997AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 07/06/23 16:19 V34997AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 07/06/23 16:19 V34997AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 07/06/23 16:19 V34997AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 07/06/23 16:19 V34997AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 07/06/23 16:19 V34997AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 07/06/23 16:19 V34997AMP
<0.651 µg/L 0.651 5.00Phenol 1 07/06/23 16:19 V34997AMP
<0.434 µg/L 0.434 2.00Pyrene 1 07/06/23 16:19 V34997AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 07/06/23 16:19 V34997AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 07/06/23 16:19 V34997AMP
625.1Surrogate: Phenol-d5 27.9 Limits: 10-63%07/06/23 16:191 AMP
Surrogate: 2-Fluorobiphenyl 77.8 Limits: 49-118%07/06/23 16:191 AMP V34997
Surrogate: 2-Fluorophenol 46.7 Limits: 22-84%07/06/23 16:191 AMP V34997
Surrogate: Nitrobenzene-d5 71.2 Limits: 43-123%07/06/23 16:191 AMP V34997
Surrogate: 4-Terphenyl-d14 87.6 Limits: 49-151%07/06/23 16:191 AMP V34997
Surrogate: 2,4,6-Tribromophenol 73.0 Limits: 31-144%07/06/23 16:191 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 44 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
99739 Matrix:
6/29/2023 9:17
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 07/11/23 22:33 6200BENM
Surrogate: 4-Bromofluorobenzene 92.8 Limits: 70-130%07/11/23 22:33100 ENM V35244
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%07/11/23 22:33100 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 92.4 Limits: 70-130%07/11/23 22:33100 ENM V35244
Surrogate: Toluene-d8 91.8 Limits: 70-130%07/11/23 22:33100 ENM V35244
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 45 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
99739 Matrix:
6/29/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<180 µg/L 180 1000Acetone 100 07/11/23 22:33 V35244ENM
330 µg/L 18.0 50.0Benzene 100 07/11/23 22:33 V35244ENM
<21.0 µg/L 21.0 50.0Bromobenzene 100 07/11/23 22:33 V35244ENM
<42.0 µg/L 42.0 100Bromochloromethane 100 07/11/23 22:33 V35244ENM
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 07/11/23 22:33 V35244ENM
<150 µg/L 150 500Bromoform 100 07/11/23 22:33 V35244ENM
<28.0 µg/L 28.0 100Bromomethane 100 07/11/23 22:33 V35244ENM
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 07/11/23 22:33 V35244ENM
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 07/11/23 22:33 V35244ENM
<92.0 µg/L 92.0 200tert-Butyl benzene 100 07/11/23 22:33 V35244ENM
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 07/11/23 22:33 V35244ENM
<19.0 µg/L 19.0 50.0Chlorobenzene 100 07/11/23 22:33 V35244ENM
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 07/11/23 22:33 V35244ENM
<43.0 µg/L 43.0 100Chloroethane 100 07/11/23 22:33 V35244ENM
<22.0 µg/L 22.0 50.0Chloroform 100 07/11/23 22:33 V35244ENM
<22.0 µg/L 22.0 50.0Chloromethane 100 07/11/23 22:33 V35244ENM
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 07/11/23 22:33 V35244ENM
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 07/11/23 22:33 V35244ENM
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 07/11/23 22:33 V35244ENM
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 07/11/23 22:33 V35244ENM
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 07/11/23 22:33 V35244ENM
<23.0 µg/L 23.0 50.0Dibromomethane 100 07/11/23 22:33 V35244ENM
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 07/11/23 22:33 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 46 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
99739 Matrix:
6/29/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 07/11/23 22:33 V35244ENM
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 07/11/23 22:33 V35244ENM
<120 µg/L 120 500Dichlorodifluoromethane 100 07/11/23 22:33 V35244ENM
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 07/11/23 22:33 V35244ENM
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 07/11/23 22:33 V35244ENM
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 07/11/23 22:33 V35244ENM
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 07/11/23 22:33 V35244ENM
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 07/11/23 22:33 V35244ENM
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 07/11/23 22:33 V35244ENM
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 07/11/23 22:33 V35244ENM
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 07/11/23 22:33 V35244ENM
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 07/11/23 22:33 V35244ENM
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 07/11/23 22:33 V35244ENM
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 07/11/23 22:33 V35244ENM
<4200 µg/L 4200 20000Ethanol 100 07/11/23 22:33 V35244ENM
241 µg/L 17.0 50.0Ethylbenzene 100 07/11/23 22:33 V35244ENM
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 07/11/23 22:33 V35244ENM
<38.0 µg/L 38.0 1002-Hexanone 100 07/11/23 22:33 V35244ENM
<18.0 µg/L 18.0 50.0Isopropylbenzene 100 07/11/23 22:33 V35244ENM
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 07/11/23 22:33 V35244ENM
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 07/11/23 22:33 V35244ENM
63.5 J µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 07/11/23 22:33 V35244ENM
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 07/11/23 22:33 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 47 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
99739 Matrix:
6/29/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<33.0 µg/L 33.0 200Methylene Chloride 100 07/11/23 22:33 V35244ENM
<47.0 µg/L 47.0 100Naphthalene 100 07/11/23 22:33 V35244ENM
46.1 J µg/L 19.0 50.0n-Propylbenzene 100 07/11/23 22:33 V35244ENM
<22.0 µg/L 22.0 50.0Styrene 100 07/11/23 22:33 V35244ENM
178 J µg/L 160 1000tert-Butyl Alcohol (TBA)100 07/11/23 22:33 V35244ENM
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 07/11/23 22:33 V35244ENM
209 J µg/L 190 1000tert-Amyl Alcohol (TAA)100 07/11/23 22:33 V35244ENM
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 07/11/23 22:33 V35244ENM
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 07/11/23 22:33 V35244ENM
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 07/11/23 22:33 V35244ENM
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 07/11/23 22:33 V35244ENM
114 µg/L 22.0 50.0Toluene 100 07/11/23 22:33 V35244ENM
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 07/11/23 22:33 V35244ENM
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 07/11/23 22:33 V35244ENM
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 07/11/23 22:33 V35244ENM
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 07/11/23 22:33 V35244ENM
<18.0 µg/L 18.0 50.0Trichloroethene 100 07/11/23 22:33 V35244ENM
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 07/11/23 22:33 V35244ENM
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 07/11/23 22:33 V35244ENM
1120 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 07/11/23 22:33 V35244ENM
344 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 07/11/23 22:33 V35244ENM
<100 µg/L 100 500Vinyl Acetate 100 07/11/23 22:33 V35244ENM
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 07/11/23 22:33 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 48 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
99739 Matrix:
6/29/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
221 µg/L 21.0 50.0o-Xylene 100 07/11/23 22:33 V35244ENM
1600 µg/L 42.0 100m,p-Xylene 100 07/11/23 22:33 V35244ENM
1820 µg/L 21.0 50.0Xylene (Total)100 07/11/23 22:33 V35244
Surrogate: 4-Bromofluorobenzene 92.8 Limits: 70-130%07/11/23 22:33100 ENM V35244
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%07/11/23 22:33100 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 92.4 Limits: 70-130%07/11/23 22:33100 ENM V35244
Surrogate: Toluene-d8 91.8 Limits: 70-130%07/11/23 22:33100 ENM V35244
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.305 µg/L 0.305 2.02Acenaphthene 1 07/06/23 16:41 V34997AMP
<0.299 µg/L 0.299 2.02Acenaphthylene 1 07/06/23 16:41 V34997AMP
<0.844 µg/L 0.844 2.02Anthracene 1 07/06/23 16:41 V34997AMP
<1.33 M µg/L 1.33 10.1Benzidine 1 07/06/23 16:41 V34997AMP
<0.643 µg/L 0.643 2.02Benzo(a)anthracene 1 07/06/23 16:41 V34997AMP
<1.03 µg/L 1.03 2.02Benzo(a)pyrene 1 07/06/23 16:41 V34997AMP
<2.51 µg/L 2.51 5.05Benzo(b)fluoranthene 1 07/06/23 16:41 V34997AMP
<1.02 µg/L 1.02 5.05Benzo(g,h,i)perylene 1 07/06/23 16:41 V34997AMP
<2.01 µg/L 2.01 5.05Benzo(k)fluoranthene 1 07/06/23 16:41 V34997AMP
<1.11 µg/L 1.11 10.1Benzoic Acid 1 07/06/23 16:41 V34997AMP
<0.690 µg/L 0.690 5.05Benzyl alcohol 1 07/06/23 16:41 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 49 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
99739 Matrix:
6/29/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.472 µg/L 0.472 5.05Bis(2-Chloroethoxy)methane 1 07/06/23 16:41 V34997AMP
<1.05 µg/L 1.05 5.05Bis(2-Chloroethyl)ether 1 07/06/23 16:41 V34997AMP
<1.09 µg/L 1.09 5.05Bis(2-Chloroisopropyl)ether 1 07/06/23 16:41 V34997AMP
4.32 J µg/L 3.49 10.1Bis(2-ethylhexyl)phthalate 1 07/06/23 16:41 V34997AMP
<1.12 µg/L 1.12 5.054-Bromophenyl phenyl ether 1 07/06/23 16:41 V34997AMP
<1.85 µg/L 1.85 5.05Butyl benzyl phthalate 1 07/06/23 16:41 V34997AMP
<1.19 µg/L 1.19 5.054-Chloro-3-methylphenol 1 07/06/23 16:41 V34997AMP
<7.45 µg/L 7.45 20.22-Chloronaphthalene 1 07/06/23 16:41 V34997AMP
<0.947 µg/L 0.947 10.12-Chlorophenol 1 07/06/23 16:41 V34997AMP
<1.73 µg/L 1.73 5.054-Chlorophenyl phenyl ether 1 07/06/23 16:41 V34997AMP
<0.409 µg/L 0.409 2.02Chrysene 1 07/06/23 16:41 V34997AMP
<0.438 µg/L 0.438 2.02Dibenz(a,h)anthracene 1 07/06/23 16:41 V34997AMP
<0.864 µg/L 0.864 5.05Dibenzofuran 1 07/06/23 16:41 V34997AMP
<2.02 µg/L 2.02 5.051,2-Dichlorobenzene 1 07/06/23 16:41 V34997AMP
<2.02 µg/L 2.02 5.051,3-Dichlorobenzene 1 07/06/23 16:41 V34997AMP
<2.07 µg/L 2.07 5.051,4-Dichlorobenzene 1 07/06/23 16:41 V34997AMP
<1.91 µg/L 1.91 5.053,3'-Dichlorobenzidine 1 07/06/23 16:41 V34997AMP
<1.47 µg/L 1.47 10.12,4-Dichlorophenol 1 07/06/23 16:41 V34997AMP
<0.752 µg/L 0.752 5.05Diethyl phthalate 1 07/06/23 16:41 V34997AMP
<0.948 µg/L 0.948 5.05Dimethyl phthalate 1 07/06/23 16:41 V34997AMP
12.9 J µg/L 1.59 20.22,4-Dimethylphenol 1 07/06/23 16:41 V34997AMP
<2.08 µg/L 2.08 5.05Di-n-butyl phthalate 1 07/06/23 16:41 V34997AMP
<2.09 µg/L 2.09 10.14,6-Dinitro-2-methylphenol 1 07/06/23 16:41 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 50 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
99739 Matrix:
6/29/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<1.94 µg/L 1.94 10.12,4-Dinitrophenol 1 07/06/23 16:41 V34997AMP
<1.12 µg/L 1.12 5.052,4-Dinitrotoluene 1 07/06/23 16:41 V34997AMP
<0.817 µg/L 0.817 5.052,6-Dinitrotoluene 1 07/06/23 16:41 V34997AMP
<1.67 µg/L 1.67 5.05Di-n-Octyl Phthalate 1 07/06/23 16:41 V34997AMP
<0.252 µg/L 0.252 2.02Fluoranthene 1 07/06/23 16:41 V34997AMP
<0.815 µg/L 0.815 2.02Fluorene 1 07/06/23 16:41 V34997AMP
<0.988 µg/L 0.988 5.05Hexachlorobenzene 1 07/06/23 16:41 V34997AMP
<2.76 µg/L 2.76 5.05Hexachlorobutadiene 1 07/06/23 16:41 V34997AMP
<2.07 µg/L 2.07 5.05Hexachlorocyclopentadiene 1 07/06/23 16:41 V34997AMP
<1.78 µg/L 1.78 5.05Hexachloroethane 1 07/06/23 16:41 V34997AMP
<0.481 µg/L 0.481 2.02Indeno(1,2,3-cd)pyrene 1 07/06/23 16:41 V34997AMP
<0.448 µg/L 0.448 5.05Isophorone 1 07/06/23 16:41 V34997AMP
23.6 µg/L 1.15 2.021-Methylnaphthalene 1 07/06/23 16:41 V34997AMP
33.4 µg/L 0.672 2.022-Methylnaphthalene 1 07/06/23 16:41 V34997AMP
52.9 µg/L 0.735 2.02Naphthalene 1 07/06/23 16:41 V34997AMP
<0.914 µg/L 0.914 5.05Nitrobenzene 1 07/06/23 16:41 V34997AMP
<0.497 µg/L 0.497 5.052-Nitrophenol 1 07/06/23 16:41 V34997AMP
<1.24 µg/L 1.24 10.14-Nitrophenol 1 07/06/23 16:41 V34997AMP
<1.11 µg/L 1.11 5.05N-Nitrosodiphenylamine 1 07/06/23 16:41 V34997AMP
<0.647 µg/L 0.647 5.05N-Nitroso-di-n-propylamine 1 07/06/23 16:41 V34997AMP
<1.44 µg/L 1.44 5.05Pentachlorophenol 1 07/06/23 16:41 V34997AMP
<0.432 µg/L 0.432 2.02Phenanthrene 1 07/06/23 16:41 V34997AMP
<0.657 µg/L 0.657 5.05Phenol 1 07/06/23 16:41 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 51 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-4
99739 Matrix:
6/29/2023 9:17
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.438 µg/L 0.438 2.02Pyrene 1 07/06/23 16:41 V34997AMP
<2.23 µg/L 2.23 5.051,2,4-Trichlorobenzene 1 07/06/23 16:41 V34997AMP
<1.33 µg/L 1.33 5.052,4,6-Trichlorophenol 1 07/06/23 16:41 V34997AMP
625.1Surrogate: Phenol-d5 24.4 Limits: 10-63%07/06/23 16:411 AMP
Surrogate: 2-Fluorobiphenyl 73.3 Limits: 49-118%07/06/23 16:411 AMP V34997
Surrogate: 2-Fluorophenol 41.2 Limits: 22-84%07/06/23 16:411 AMP V34997
Surrogate: Nitrobenzene-d5 64.2 Limits: 43-123%07/06/23 16:411 AMP V34997
Surrogate: 4-Terphenyl-d14 88.5 Limits: 49-151%07/06/23 16:411 AMP V34997
Surrogate: 2,4,6-Tribromophenol 74.7 Limits: 31-144%07/06/23 16:411 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 52 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-5
99740 Matrix:
6/29/2023 9:31
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/13/23 22:24 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/13/23 22:241 MSA V35348
Surrogate: Dibromofluoromethane 102 Limits: 70-130%07/13/23 22:241 MSA V35348
Surrogate: 1,2-Dichloroethane - d4 99.2 Limits: 70-130%07/13/23 22:241 MSA V35348
Surrogate: Toluene-d8 98.6 Limits: 70-130%07/13/23 22:241 MSA V35348
Surrogate: 4-Bromofluorobenzene 91.8 Limits: 70-130%07/11/23 23:01100 ENM V35244
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%07/11/23 23:01100 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 92.6 Limits: 70-130%07/11/23 23:01100 ENM V35244
Surrogate: Toluene-d8 92.8 Limits: 70-130%07/11/23 23:01100 ENM V35244
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 53 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-5
99740 Matrix:
6/29/2023 9:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35347 07/13/23 09:00
10.8 µg/L 1.80 10.0Acetone 1 07/13/23 22:24 V35348MSA
0.429 J µg/L 0.180 0.500Benzene 1 07/13/23 22:24 V35348MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/13/23 22:24 V35348MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/13/23 22:24 V35348MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/13/23 22:24 V35348MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/13/23 22:24 V35348MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 07/13/23 22:24 V35348MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/13/23 22:24 V35348MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/13/23 22:24 V35348MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/13/23 22:24 V35348MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/13/23 22:24 V35348MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/13/23 22:24 V35348MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/13/23 22:24 V35348MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/13/23 22:24 V35348MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/13/23 22:24 V35348MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/13/23 22:24 V35348MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/13/23 22:24 V35348MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/13/23 22:24 V35348MSA
1.15 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/13/23 22:24 V35348MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/13/23 22:24 V35348MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/13/23 22:24 V35348MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/13/23 22:24 V35348MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/13/23 22:24 V35348MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 54 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-5
99740 Matrix:
6/29/2023 9:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35347 07/13/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/13/23 22:24 V35348MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/13/23 22:24 V35348MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/13/23 22:24 V35348MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/13/23 22:24 V35348MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/13/23 22:24 V35348MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/13/23 22:24 V35348MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/13/23 22:24 V35348MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/13/23 22:24 V35348MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/13/23 22:24 V35348MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/13/23 22:24 V35348MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/13/23 22:24 V35348MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/13/23 22:24 V35348MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/13/23 22:24 V35348MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/13/23 22:24 V35348MSA
<42.0 µg/L 42.0 200Ethanol 1 07/13/23 22:24 V35348MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/13/23 22:24 V35348MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/13/23 22:24 V35348MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 07/13/23 22:24 V35348MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/13/23 22:24 V35348MSA
0.252 J µg/L 0.089 0.5004-Isopropyl toluene 1 07/13/23 22:24 V35348MSA
2.36 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/13/23 22:24 V35348MSA
1.88 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/13/23 22:24 V35348MSA
2.70 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/13/23 22:24 V35348MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 55 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-5
99740 Matrix:
6/29/2023 9:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35347 07/13/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/13/23 22:24 V35348MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 07/13/23 22:24 V35348MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/13/23 22:24 V35348MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/13/23 22:24 V35348MSA
4.34 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/13/23 22:24 V35348MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/13/23 22:24 V35348MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/13/23 22:24 V35348MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/13/23 22:24 V35348MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/13/23 22:24 V35348MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/13/23 22:24 V35348MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/13/23 22:24 V35348MSA
0.233 J µg/L 0.220 0.500Toluene 1 07/13/23 22:24 V35348MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/13/23 22:24 V35348MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/13/23 22:24 V35348MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/13/23 22:24 V35348MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/13/23 22:24 V35348MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/13/23 22:24 V35348MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/13/23 22:24 V35348MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/13/23 22:24 V35348MSA
0.299 J µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/13/23 22:24 V35348MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/13/23 22:24 V35348MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/13/23 22:24 V35348MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/13/23 22:24 V35348MSA
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 56 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-5
99740 Matrix:
6/29/2023 9:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35347 07/13/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 07/13/23 22:24 V35348MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/13/23 22:24 V35348MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/13/23 22:24 V35348
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/13/23 22:241 MSA V35348
Surrogate: Dibromofluoromethane 102 Limits: 70-130%07/13/23 22:241 MSA V35348
Surrogate: 1,2-Dichloroethane - d4 99.2 Limits: 70-130%07/13/23 22:241 MSA V35348
Surrogate: Toluene-d8 98.6 Limits: 70-130%07/13/23 22:241 MSA V35348
Surrogate: 4-Bromofluorobenzene 91.8 Limits: 70-130%07/11/23 23:01100 ENM V35244
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%07/11/23 23:01100 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 92.6 Limits: 70-130%07/11/23 23:01100 ENM V35244
Surrogate: Toluene-d8 92.8 Limits: 70-130%07/11/23 23:01100 ENM V35244
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.305 µg/L 0.305 2.02Acenaphthene 1 07/06/23 17:04 V34997AMP
<0.299 µg/L 0.299 2.02Acenaphthylene 1 07/06/23 17:04 V34997AMP
<0.844 µg/L 0.844 2.02Anthracene 1 07/06/23 17:04 V34997AMP
<1.33 M µg/L 1.33 10.1Benzidine 1 07/06/23 17:04 V34997AMP
<0.643 µg/L 0.643 2.02Benzo(a)anthracene 1 07/06/23 17:04 V34997AMP
<1.03 µg/L 1.03 2.02Benzo(a)pyrene 1 07/06/23 17:04 V34997AMP
<2.51 µg/L 2.51 5.05Benzo(b)fluoranthene 1 07/06/23 17:04 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 57 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-5
99740 Matrix:
6/29/2023 9:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<1.02 µg/L 1.02 5.05Benzo(g,h,i)perylene 1 07/06/23 17:04 V34997AMP
<2.01 µg/L 2.01 5.05Benzo(k)fluoranthene 1 07/06/23 17:04 V34997AMP
1.11 J µg/L 1.11 10.1Benzoic Acid 1 07/06/23 17:04 V34997AMP
<0.690 µg/L 0.690 5.05Benzyl alcohol 1 07/06/23 17:04 V34997AMP
<0.472 µg/L 0.472 5.05Bis(2-Chloroethoxy)methane 1 07/06/23 17:04 V34997AMP
<1.05 µg/L 1.05 5.05Bis(2-Chloroethyl)ether 1 07/06/23 17:04 V34997AMP
<1.09 µg/L 1.09 5.05Bis(2-Chloroisopropyl)ether 1 07/06/23 17:04 V34997AMP
3.58 J µg/L 3.49 10.1Bis(2-ethylhexyl)phthalate 1 07/06/23 17:04 V34997AMP
<1.12 µg/L 1.12 5.054-Bromophenyl phenyl ether 1 07/06/23 17:04 V34997AMP
<1.85 µg/L 1.85 5.05Butyl benzyl phthalate 1 07/06/23 17:04 V34997AMP
<1.19 µg/L 1.19 5.054-Chloro-3-methylphenol 1 07/06/23 17:04 V34997AMP
<7.45 µg/L 7.45 20.22-Chloronaphthalene 1 07/06/23 17:04 V34997AMP
<0.947 µg/L 0.947 10.12-Chlorophenol 1 07/06/23 17:04 V34997AMP
<1.73 µg/L 1.73 5.054-Chlorophenyl phenyl ether 1 07/06/23 17:04 V34997AMP
<0.409 µg/L 0.409 2.02Chrysene 1 07/06/23 17:04 V34997AMP
<0.438 µg/L 0.438 2.02Dibenz(a,h)anthracene 1 07/06/23 17:04 V34997AMP
<0.864 µg/L 0.864 5.05Dibenzofuran 1 07/06/23 17:04 V34997AMP
<2.02 µg/L 2.02 5.051,2-Dichlorobenzene 1 07/06/23 17:04 V34997AMP
<2.02 µg/L 2.02 5.051,3-Dichlorobenzene 1 07/06/23 17:04 V34997AMP
<2.07 µg/L 2.07 5.051,4-Dichlorobenzene 1 07/06/23 17:04 V34997AMP
<1.91 µg/L 1.91 5.053,3'-Dichlorobenzidine 1 07/06/23 17:04 V34997AMP
<1.47 µg/L 1.47 10.12,4-Dichlorophenol 1 07/06/23 17:04 V34997AMP
<0.752 µg/L 0.752 5.05Diethyl phthalate 1 07/06/23 17:04 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 58 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-5
99740 Matrix:
6/29/2023 9:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.948 µg/L 0.948 5.05Dimethyl phthalate 1 07/06/23 17:04 V34997AMP
<1.59 µg/L 1.59 20.22,4-Dimethylphenol 1 07/06/23 17:04 V34997AMP
<2.08 µg/L 2.08 5.05Di-n-butyl phthalate 1 07/06/23 17:04 V34997AMP
<2.09 µg/L 2.09 10.14,6-Dinitro-2-methylphenol 1 07/06/23 17:04 V34997AMP
<1.94 µg/L 1.94 10.12,4-Dinitrophenol 1 07/06/23 17:04 V34997AMP
<1.12 µg/L 1.12 5.052,4-Dinitrotoluene 1 07/06/23 17:04 V34997AMP
<0.817 µg/L 0.817 5.052,6-Dinitrotoluene 1 07/06/23 17:04 V34997AMP
<1.67 µg/L 1.67 5.05Di-n-Octyl Phthalate 1 07/06/23 17:04 V34997AMP
<0.252 µg/L 0.252 2.02Fluoranthene 1 07/06/23 17:04 V34997AMP
<0.815 µg/L 0.815 2.02Fluorene 1 07/06/23 17:04 V34997AMP
<0.988 µg/L 0.988 5.05Hexachlorobenzene 1 07/06/23 17:04 V34997AMP
<2.76 µg/L 2.76 5.05Hexachlorobutadiene 1 07/06/23 17:04 V34997AMP
<2.07 µg/L 2.07 5.05Hexachlorocyclopentadiene 1 07/06/23 17:04 V34997AMP
<1.78 µg/L 1.78 5.05Hexachloroethane 1 07/06/23 17:04 V34997AMP
<0.481 µg/L 0.481 2.02Indeno(1,2,3-cd)pyrene 1 07/06/23 17:04 V34997AMP
<0.448 µg/L 0.448 5.05Isophorone 1 07/06/23 17:04 V34997AMP
<1.15 µg/L 1.15 2.021-Methylnaphthalene 1 07/06/23 17:04 V34997AMP
<0.672 µg/L 0.672 2.022-Methylnaphthalene 1 07/06/23 17:04 V34997AMP
<0.735 µg/L 0.735 2.02Naphthalene 1 07/06/23 17:04 V34997AMP
<0.914 µg/L 0.914 5.05Nitrobenzene 1 07/06/23 17:04 V34997AMP
<0.497 µg/L 0.497 5.052-Nitrophenol 1 07/06/23 17:04 V34997AMP
<1.24 µg/L 1.24 10.14-Nitrophenol 1 07/06/23 17:04 V34997AMP
<1.11 µg/L 1.11 5.05N-Nitrosodiphenylamine 1 07/06/23 17:04 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 59 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-5
99740 Matrix:
6/29/2023 9:31
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.647 µg/L 0.647 5.05N-Nitroso-di-n-propylamine 1 07/06/23 17:04 V34997AMP
<1.44 µg/L 1.44 5.05Pentachlorophenol 1 07/06/23 17:04 V34997AMP
<0.432 µg/L 0.432 2.02Phenanthrene 1 07/06/23 17:04 V34997AMP
<0.657 µg/L 0.657 5.05Phenol 1 07/06/23 17:04 V34997AMP
<0.438 µg/L 0.438 2.02Pyrene 1 07/06/23 17:04 V34997AMP
<2.23 µg/L 2.23 5.051,2,4-Trichlorobenzene 1 07/06/23 17:04 V34997AMP
<1.33 µg/L 1.33 5.052,4,6-Trichlorophenol 1 07/06/23 17:04 V34997AMP
625.1Surrogate: Phenol-d5 24.5 Limits: 10-63%07/06/23 17:041 AMP
Surrogate: 2-Fluorobiphenyl 68.3 Limits: 49-118%07/06/23 17:041 AMP V34997
Surrogate: 2-Fluorophenol 38.7 Limits: 22-84%07/06/23 17:041 AMP V34997
Surrogate: Nitrobenzene-d5 60.8 Limits: 43-123%07/06/23 17:041 AMP V34997
Surrogate: 4-Terphenyl-d14 80.6 Limits: 49-151%07/06/23 17:041 AMP V34997
Surrogate: 2,4,6-Tribromophenol 65.4 Limits: 31-144%07/06/23 17:041 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 60 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-6
99741 Matrix:
6/29/2023 9:47
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/11/23 18:25 6200BENM
Surrogate: 4-Bromofluorobenzene 93.8 Limits: 70-130%07/11/23 18:251 ENM V35244
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%07/11/23 18:251 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 92.8 Limits: 70-130%07/11/23 18:251 ENM V35244
Surrogate: Toluene-d8 92.2 Limits: 70-130%07/11/23 18:251 ENM V35244
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 61 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-6
99741 Matrix:
6/29/2023 9:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 07/11/23 18:25 V35244ENM
<0.180 µg/L 0.180 0.500Benzene 1 07/11/23 18:25 V35244ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 18:25 V35244ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 18:25 V35244ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 18:25 V35244ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 18:25 V35244ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 18:25 V35244ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 18:25 V35244ENM
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 18:25 V35244ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 18:25 V35244ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 18:25 V35244ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 18:25 V35244ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 18:25 V35244ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 18:25 V35244ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 18:25 V35244ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 07/11/23 18:25 V35244ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 18:25 V35244ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 18:25 V35244ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/11/23 18:25 V35244ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 18:25 V35244ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 18:25 V35244ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 18:25 V35244ENM
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 18:25 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 62 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-6
99741 Matrix:
6/29/2023 9:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 18:25 V35244ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 18:25 V35244ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 18:25 V35244ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 18:25 V35244ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 18:25 V35244ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 18:25 V35244ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 18:25 V35244ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 18:25 V35244ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 18:25 V35244ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 18:25 V35244ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 18:25 V35244ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 18:25 V35244ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 18:25 V35244ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 18:25 V35244ENM
<42.0 µg/L 42.0 200Ethanol 1 07/11/23 18:25 V35244ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 18:25 V35244ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 18:25 V35244ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 18:25 V35244ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 18:25 V35244ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 18:25 V35244ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 18:25 V35244ENM
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 18:25 V35244ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 18:25 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 63 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-6
99741 Matrix:
6/29/2023 9:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 18:25 V35244ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 07/11/23 18:25 V35244ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 18:25 V35244ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/11/23 18:25 V35244ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/11/23 18:25 V35244ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/11/23 18:25 V35244ENM
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/11/23 18:25 V35244ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/11/23 18:25 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 18:25 V35244ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 18:25 V35244ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 18:25 V35244ENM
<0.220 µg/L 0.220 0.500Toluene 1 07/11/23 18:25 V35244ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 18:25 V35244ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 18:25 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 18:25 V35244ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 18:25 V35244ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 18:25 V35244ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 18:25 V35244ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 18:25 V35244ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 18:25 V35244ENM
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 18:25 V35244ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 18:25 V35244ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 18:25 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 64 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-6
99741 Matrix:
6/29/2023 9:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 07/11/23 18:25 V35244ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/11/23 18:25 V35244ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/11/23 18:25 V35244
Surrogate: 4-Bromofluorobenzene 93.8 Limits: 70-130%07/11/23 18:251 ENM V35244
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%07/11/23 18:251 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 92.8 Limits: 70-130%07/11/23 18:251 ENM V35244
Surrogate: Toluene-d8 92.2 Limits: 70-130%07/11/23 18:251 ENM V35244
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.302 µg/L 0.302 2.00Acenaphthene 1 07/06/23 17:26 V34997AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 07/06/23 17:26 V34997AMP
<0.836 µg/L 0.836 2.00Anthracene 1 07/06/23 17:26 V34997AMP
<1.32 M µg/L 1.32 10.0Benzidine 1 07/06/23 17:26 V34997AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 07/06/23 17:26 V34997AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 07/06/23 17:26 V34997AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 07/06/23 17:26 V34997AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 07/06/23 17:26 V34997AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 07/06/23 17:26 V34997AMP
<1.10 µg/L 1.10 10.0Benzoic Acid 1 07/06/23 17:26 V34997AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 07/06/23 17:26 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 65 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-6
99741 Matrix:
6/29/2023 9:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 07/06/23 17:26 V34997AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 07/06/23 17:26 V34997AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 07/06/23 17:26 V34997AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 07/06/23 17:26 V34997AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 07/06/23 17:26 V34997AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 07/06/23 17:26 V34997AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 07/06/23 17:26 V34997AMP
<7.38 µg/L 7.38 20.02-Chloronaphthalene 1 07/06/23 17:26 V34997AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 07/06/23 17:26 V34997AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 07/06/23 17:26 V34997AMP
<0.405 µg/L 0.405 2.00Chrysene 1 07/06/23 17:26 V34997AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 07/06/23 17:26 V34997AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 07/06/23 17:26 V34997AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 07/06/23 17:26 V34997AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 07/06/23 17:26 V34997AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 07/06/23 17:26 V34997AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 07/06/23 17:26 V34997AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 07/06/23 17:26 V34997AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 07/06/23 17:26 V34997AMP
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 07/06/23 17:26 V34997AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 07/06/23 17:26 V34997AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 07/06/23 17:26 V34997AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 07/06/23 17:26 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 66 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-6
99741 Matrix:
6/29/2023 9:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 07/06/23 17:26 V34997AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 07/06/23 17:26 V34997AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 07/06/23 17:26 V34997AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 07/06/23 17:26 V34997AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 07/06/23 17:26 V34997AMP
<0.807 µg/L 0.807 2.00Fluorene 1 07/06/23 17:26 V34997AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 07/06/23 17:26 V34997AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 07/06/23 17:26 V34997AMP
<2.05 µg/L 2.05 5.00Hexachlorocyclopentadiene 1 07/06/23 17:26 V34997AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 07/06/23 17:26 V34997AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 07/06/23 17:26 V34997AMP
<0.444 µg/L 0.444 5.00Isophorone 1 07/06/23 17:26 V34997AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 07/06/23 17:26 V34997AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 07/06/23 17:26 V34997AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 07/06/23 17:26 V34997AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 07/06/23 17:26 V34997AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 07/06/23 17:26 V34997AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 07/06/23 17:26 V34997AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 07/06/23 17:26 V34997AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 07/06/23 17:26 V34997AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 07/06/23 17:26 V34997AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 07/06/23 17:26 V34997AMP
<0.651 µg/L 0.651 5.00Phenol 1 07/06/23 17:26 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 67 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-6
99741 Matrix:
6/29/2023 9:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.434 µg/L 0.434 2.00Pyrene 1 07/06/23 17:26 V34997AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 07/06/23 17:26 V34997AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 07/06/23 17:26 V34997AMP
625.1Surrogate: Phenol-d5 27.1 Limits: 10-63%07/06/23 17:261 AMP
Surrogate: 2-Fluorobiphenyl 71.8 Limits: 49-118%07/06/23 17:261 AMP V34997
Surrogate: 2-Fluorophenol 43.1 Limits: 22-84%07/06/23 17:261 AMP V34997
Surrogate: Nitrobenzene-d5 61.0 Limits: 43-123%07/06/23 17:261 AMP V34997
Surrogate: 4-Terphenyl-d14 83.0 Limits: 49-151%07/06/23 17:261 AMP V34997
Surrogate: 2,4,6-Tribromophenol 64.4 Limits: 31-144%07/06/23 17:261 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 68 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-7
99742 Matrix:
6/29/2023 10:02
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/11/23 18:52 6200BENM
Surrogate: 4-Bromofluorobenzene 93.2 Limits: 70-130%07/11/23 18:521 ENM V35244
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%07/11/23 18:521 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 93.2 Limits: 70-130%07/11/23 18:521 ENM V35244
Surrogate: Toluene-d8 91.8 Limits: 70-130%07/11/23 18:521 ENM V35244
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 69 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-7
99742 Matrix:
6/29/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 07/11/23 18:52 V35244ENM
<0.180 µg/L 0.180 0.500Benzene 1 07/11/23 18:52 V35244ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 18:52 V35244ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 18:52 V35244ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 18:52 V35244ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 18:52 V35244ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 18:52 V35244ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 18:52 V35244ENM
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 18:52 V35244ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 18:52 V35244ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 18:52 V35244ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 18:52 V35244ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 18:52 V35244ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 18:52 V35244ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 18:52 V35244ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 07/11/23 18:52 V35244ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 18:52 V35244ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 18:52 V35244ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/11/23 18:52 V35244ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 18:52 V35244ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 18:52 V35244ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 18:52 V35244ENM
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 18:52 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 70 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-7
99742 Matrix:
6/29/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 18:52 V35244ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 18:52 V35244ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 18:52 V35244ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 18:52 V35244ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 18:52 V35244ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 18:52 V35244ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 18:52 V35244ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 18:52 V35244ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 18:52 V35244ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 18:52 V35244ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 18:52 V35244ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 18:52 V35244ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 18:52 V35244ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 18:52 V35244ENM
<42.0 µg/L 42.0 200Ethanol 1 07/11/23 18:52 V35244ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 18:52 V35244ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 18:52 V35244ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 18:52 V35244ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 18:52 V35244ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 18:52 V35244ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 18:52 V35244ENM
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 18:52 V35244ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 18:52 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 71 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-7
99742 Matrix:
6/29/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 18:52 V35244ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 07/11/23 18:52 V35244ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 18:52 V35244ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/11/23 18:52 V35244ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/11/23 18:52 V35244ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/11/23 18:52 V35244ENM
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/11/23 18:52 V35244ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/11/23 18:52 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 18:52 V35244ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 18:52 V35244ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 18:52 V35244ENM
<0.220 µg/L 0.220 0.500Toluene 1 07/11/23 18:52 V35244ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 18:52 V35244ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 18:52 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 18:52 V35244ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 18:52 V35244ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 18:52 V35244ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 18:52 V35244ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 18:52 V35244ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 18:52 V35244ENM
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 18:52 V35244ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 18:52 V35244ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 18:52 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 72 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-7
99742 Matrix:
6/29/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 07/11/23 18:52 V35244ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/11/23 18:52 V35244ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/11/23 18:52 V35244
Surrogate: 4-Bromofluorobenzene 93.2 Limits: 70-130%07/11/23 18:521 ENM V35244
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%07/11/23 18:521 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 93.2 Limits: 70-130%07/11/23 18:521 ENM V35244
Surrogate: Toluene-d8 91.8 Limits: 70-130%07/11/23 18:521 ENM V35244
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.335 µg/L 0.335 2.22Acenaphthene 1 07/06/23 17:49 V34997AMP
<0.329 µg/L 0.329 2.22Acenaphthylene 1 07/06/23 17:49 V34997AMP
<0.927 µg/L 0.927 2.22Anthracene 1 07/06/23 17:49 V34997AMP
<1.47 M µg/L 1.47 11.1Benzidine 1 07/06/23 17:49 V34997AMP
<0.707 µg/L 0.707 2.22Benzo(a)anthracene 1 07/06/23 17:49 V34997AMP
<1.13 µg/L 1.13 2.22Benzo(a)pyrene 1 07/06/23 17:49 V34997AMP
<2.77 µg/L 2.77 5.56Benzo(b)fluoranthene 1 07/06/23 17:49 V34997AMP
<1.12 µg/L 1.12 5.56Benzo(g,h,i)perylene 1 07/06/23 17:49 V34997AMP
<2.21 µg/L 2.21 5.56Benzo(k)fluoranthene 1 07/06/23 17:49 V34997AMP
<1.22 µg/L 1.22 11.1Benzoic Acid 1 07/06/23 17:49 V34997AMP
<0.760 µg/L 0.760 5.56Benzyl alcohol 1 07/06/23 17:49 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 73 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-7
99742 Matrix:
6/29/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.520 µg/L 0.520 5.56Bis(2-Chloroethoxy)methane 1 07/06/23 17:49 V34997AMP
<1.16 µg/L 1.16 5.56Bis(2-Chloroethyl)ether 1 07/06/23 17:49 V34997AMP
<1.20 µg/L 1.20 5.56Bis(2-Chloroisopropyl)ether 1 07/06/23 17:49 V34997AMP
<3.84 µg/L 3.84 11.1Bis(2-ethylhexyl)phthalate 1 07/06/23 17:49 V34997AMP
<1.23 µg/L 1.23 5.564-Bromophenyl phenyl ether 1 07/06/23 17:49 V34997AMP
<2.03 µg/L 2.03 5.56Butyl benzyl phthalate 1 07/06/23 17:49 V34997AMP
<1.31 µg/L 1.31 5.564-Chloro-3-methylphenol 1 07/06/23 17:49 V34997AMP
<8.19 µg/L 8.19 22.22-Chloronaphthalene 1 07/06/23 17:49 V34997AMP
<1.04 µg/L 1.04 11.12-Chlorophenol 1 07/06/23 17:49 V34997AMP
<1.90 µg/L 1.90 5.564-Chlorophenyl phenyl ether 1 07/06/23 17:49 V34997AMP
<0.449 µg/L 0.449 2.22Chrysene 1 07/06/23 17:49 V34997AMP
<0.481 µg/L 0.481 2.22Dibenz(a,h)anthracene 1 07/06/23 17:49 V34997AMP
<0.951 µg/L 0.951 5.56Dibenzofuran 1 07/06/23 17:49 V34997AMP
<2.22 µg/L 2.22 5.561,2-Dichlorobenzene 1 07/06/23 17:49 V34997AMP
<2.22 µg/L 2.22 5.561,3-Dichlorobenzene 1 07/06/23 17:49 V34997AMP
<2.28 µg/L 2.28 5.561,4-Dichlorobenzene 1 07/06/23 17:49 V34997AMP
<2.10 µg/L 2.10 5.563,3'-Dichlorobenzidine 1 07/06/23 17:49 V34997AMP
<1.62 µg/L 1.62 11.12,4-Dichlorophenol 1 07/06/23 17:49 V34997AMP
<0.828 µg/L 0.828 5.56Diethyl phthalate 1 07/06/23 17:49 V34997AMP
<1.04 µg/L 1.04 5.56Dimethyl phthalate 1 07/06/23 17:49 V34997AMP
<1.74 µg/L 1.74 22.22,4-Dimethylphenol 1 07/06/23 17:49 V34997AMP
<2.29 µg/L 2.29 5.56Di-n-butyl phthalate 1 07/06/23 17:49 V34997AMP
<2.30 µg/L 2.30 11.14,6-Dinitro-2-methylphenol 1 07/06/23 17:49 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 74 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-7
99742 Matrix:
6/29/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<2.13 µg/L 2.13 11.12,4-Dinitrophenol 1 07/06/23 17:49 V34997AMP
<1.23 µg/L 1.23 5.562,4-Dinitrotoluene 1 07/06/23 17:49 V34997AMP
<0.899 µg/L 0.899 5.562,6-Dinitrotoluene 1 07/06/23 17:49 V34997AMP
<1.83 µg/L 1.83 5.56Di-n-Octyl Phthalate 1 07/06/23 17:49 V34997AMP
<0.277 µg/L 0.277 2.22Fluoranthene 1 07/06/23 17:49 V34997AMP
<0.895 µg/L 0.895 2.22Fluorene 1 07/06/23 17:49 V34997AMP
<1.09 µg/L 1.09 5.56Hexachlorobenzene 1 07/06/23 17:49 V34997AMP
<3.04 µg/L 3.04 5.56Hexachlorobutadiene 1 07/06/23 17:49 V34997AMP
<2.28 µg/L 2.28 5.56Hexachlorocyclopentadiene 1 07/06/23 17:49 V34997AMP
<1.96 µg/L 1.96 5.56Hexachloroethane 1 07/06/23 17:49 V34997AMP
<0.529 µg/L 0.529 2.22Indeno(1,2,3-cd)pyrene 1 07/06/23 17:49 V34997AMP
<0.493 µg/L 0.493 5.56Isophorone 1 07/06/23 17:49 V34997AMP
<1.27 µg/L 1.27 2.221-Methylnaphthalene 1 07/06/23 17:49 V34997AMP
<0.739 µg/L 0.739 2.222-Methylnaphthalene 1 07/06/23 17:49 V34997AMP
<0.808 µg/L 0.808 2.22Naphthalene 1 07/06/23 17:49 V34997AMP
<1.01 µg/L 1.01 5.56Nitrobenzene 1 07/06/23 17:49 V34997AMP
<0.548 µg/L 0.548 5.562-Nitrophenol 1 07/06/23 17:49 V34997AMP
<1.37 µg/L 1.37 11.14-Nitrophenol 1 07/06/23 17:49 V34997AMP
<1.22 µg/L 1.22 5.56N-Nitrosodiphenylamine 1 07/06/23 17:49 V34997AMP
<0.712 µg/L 0.712 5.56N-Nitroso-di-n-propylamine 1 07/06/23 17:49 V34997AMP
<1.59 µg/L 1.59 5.56Pentachlorophenol 1 07/06/23 17:49 V34997AMP
<0.475 µg/L 0.475 2.22Phenanthrene 1 07/06/23 17:49 V34997AMP
<0.723 µg/L 0.723 5.56Phenol 1 07/06/23 17:49 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 75 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-7
99742 Matrix:
6/29/2023 10:02
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.481 µg/L 0.481 2.22Pyrene 1 07/06/23 17:49 V34997AMP
<2.46 µg/L 2.46 5.561,2,4-Trichlorobenzene 1 07/06/23 17:49 V34997AMP
<1.47 µg/L 1.47 5.562,4,6-Trichlorophenol 1 07/06/23 17:49 V34997AMP
625.1Surrogate: Phenol-d5 49.1 Limits: 10-63%07/06/23 17:491 AMP
Surrogate: 2-Fluorobiphenyl 135 *Limits: 49-118%07/06/23 17:491 AMP V34997
Surrogate: 2-Fluorophenol 76.0 Limits: 22-84%07/06/23 17:491 AMP V34997
Surrogate: Nitrobenzene-d5 120 Limits: 43-123%07/06/23 17:491 AMP V34997
Surrogate: 4-Terphenyl-d14 150 Limits: 49-151%07/06/23 17:491 AMP V34997
Surrogate: 2,4,6-Tribromophenol 126 Limits: 31-144%07/06/23 17:491 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 76 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-8
99743 Matrix:
6/29/2023 10:16
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/11/23 19:20 6200BENM
Surrogate: 4-Bromofluorobenzene 91.4 Limits: 70-130%07/11/23 19:201 ENM V35244
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%07/11/23 19:201 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 91.6 Limits: 70-130%07/11/23 19:201 ENM V35244
Surrogate: Toluene-d8 92.6 Limits: 70-130%07/11/23 19:201 ENM V35244
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 77 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-8
99743 Matrix:
6/29/2023 10:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 07/11/23 19:20 V35244ENM
<0.180 µg/L 0.180 0.500Benzene 1 07/11/23 19:20 V35244ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 19:20 V35244ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 19:20 V35244ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 19:20 V35244ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 19:20 V35244ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 19:20 V35244ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 19:20 V35244ENM
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 19:20 V35244ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 19:20 V35244ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 19:20 V35244ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 19:20 V35244ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 19:20 V35244ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 19:20 V35244ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 19:20 V35244ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 07/11/23 19:20 V35244ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 19:20 V35244ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 19:20 V35244ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/11/23 19:20 V35244ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 19:20 V35244ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 19:20 V35244ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 19:20 V35244ENM
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 19:20 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 78 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-8
99743 Matrix:
6/29/2023 10:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 19:20 V35244ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 19:20 V35244ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 19:20 V35244ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 19:20 V35244ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 19:20 V35244ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 19:20 V35244ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 19:20 V35244ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 19:20 V35244ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 19:20 V35244ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 19:20 V35244ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 19:20 V35244ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 19:20 V35244ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 19:20 V35244ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 19:20 V35244ENM
<42.0 µg/L 42.0 200Ethanol 1 07/11/23 19:20 V35244ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 19:20 V35244ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 19:20 V35244ENM
<0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 19:20 V35244ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 19:20 V35244ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 19:20 V35244ENM
0.922 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 19:20 V35244ENM
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 19:20 V35244ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 19:20 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 79 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-8
99743 Matrix:
6/29/2023 10:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 19:20 V35244ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 07/11/23 19:20 V35244ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 19:20 V35244ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/11/23 19:20 V35244ENM
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/11/23 19:20 V35244ENM
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/11/23 19:20 V35244ENM
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/11/23 19:20 V35244ENM
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/11/23 19:20 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 19:20 V35244ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 19:20 V35244ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 19:20 V35244ENM
<0.220 µg/L 0.220 0.500Toluene 1 07/11/23 19:20 V35244ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 19:20 V35244ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 19:20 V35244ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 19:20 V35244ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 19:20 V35244ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 19:20 V35244ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 19:20 V35244ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 19:20 V35244ENM
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 19:20 V35244ENM
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 19:20 V35244ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 19:20 V35244ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 19:20 V35244ENM
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 80 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-8
99743 Matrix:
6/29/2023 10:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35241 07/11/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 07/11/23 19:20 V35244ENM
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/11/23 19:20 V35244ENM
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/11/23 19:20 V35244
Surrogate: 4-Bromofluorobenzene 91.4 Limits: 70-130%07/11/23 19:201 ENM V35244
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%07/11/23 19:201 ENM V35244
Surrogate: 1,2-Dichloroethane - d4 91.6 Limits: 70-130%07/11/23 19:201 ENM V35244
Surrogate: Toluene-d8 92.6 Limits: 70-130%07/11/23 19:201 ENM V35244
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.335 µg/L 0.335 2.22Acenaphthene 1 07/06/23 18:11 V34997AMP
<0.329 µg/L 0.329 2.22Acenaphthylene 1 07/06/23 18:11 V34997AMP
<0.927 µg/L 0.927 2.22Anthracene 1 07/06/23 18:11 V34997AMP
<1.47 M µg/L 1.47 11.1Benzidine 1 07/06/23 18:11 V34997AMP
<0.707 µg/L 0.707 2.22Benzo(a)anthracene 1 07/06/23 18:11 V34997AMP
<1.13 µg/L 1.13 2.22Benzo(a)pyrene 1 07/06/23 18:11 V34997AMP
<2.77 µg/L 2.77 5.56Benzo(b)fluoranthene 1 07/06/23 18:11 V34997AMP
<1.12 µg/L 1.12 5.56Benzo(g,h,i)perylene 1 07/06/23 18:11 V34997AMP
<2.21 µg/L 2.21 5.56Benzo(k)fluoranthene 1 07/06/23 18:11 V34997AMP
<1.22 µg/L 1.22 11.1Benzoic Acid 1 07/06/23 18:11 V34997AMP
<0.760 µg/L 0.760 5.56Benzyl alcohol 1 07/06/23 18:11 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 81 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-8
99743 Matrix:
6/29/2023 10:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.520 µg/L 0.520 5.56Bis(2-Chloroethoxy)methane 1 07/06/23 18:11 V34997AMP
<1.16 µg/L 1.16 5.56Bis(2-Chloroethyl)ether 1 07/06/23 18:11 V34997AMP
<1.20 µg/L 1.20 5.56Bis(2-Chloroisopropyl)ether 1 07/06/23 18:11 V34997AMP
<3.84 µg/L 3.84 11.1Bis(2-ethylhexyl)phthalate 1 07/06/23 18:11 V34997AMP
<1.23 µg/L 1.23 5.564-Bromophenyl phenyl ether 1 07/06/23 18:11 V34997AMP
<2.03 µg/L 2.03 5.56Butyl benzyl phthalate 1 07/06/23 18:11 V34997AMP
<1.31 µg/L 1.31 5.564-Chloro-3-methylphenol 1 07/06/23 18:11 V34997AMP
<8.19 µg/L 8.19 22.22-Chloronaphthalene 1 07/06/23 18:11 V34997AMP
<1.04 µg/L 1.04 11.12-Chlorophenol 1 07/06/23 18:11 V34997AMP
<1.90 µg/L 1.90 5.564-Chlorophenyl phenyl ether 1 07/06/23 18:11 V34997AMP
<0.449 µg/L 0.449 2.22Chrysene 1 07/06/23 18:11 V34997AMP
<0.481 µg/L 0.481 2.22Dibenz(a,h)anthracene 1 07/06/23 18:11 V34997AMP
<0.951 µg/L 0.951 5.56Dibenzofuran 1 07/06/23 18:11 V34997AMP
<2.22 µg/L 2.22 5.561,2-Dichlorobenzene 1 07/06/23 18:11 V34997AMP
<2.22 µg/L 2.22 5.561,3-Dichlorobenzene 1 07/06/23 18:11 V34997AMP
<2.28 µg/L 2.28 5.561,4-Dichlorobenzene 1 07/06/23 18:11 V34997AMP
<2.10 µg/L 2.10 5.563,3'-Dichlorobenzidine 1 07/06/23 18:11 V34997AMP
<1.62 µg/L 1.62 11.12,4-Dichlorophenol 1 07/06/23 18:11 V34997AMP
<0.828 µg/L 0.828 5.56Diethyl phthalate 1 07/06/23 18:11 V34997AMP
<1.04 µg/L 1.04 5.56Dimethyl phthalate 1 07/06/23 18:11 V34997AMP
<1.74 µg/L 1.74 22.22,4-Dimethylphenol 1 07/06/23 18:11 V34997AMP
<2.29 µg/L 2.29 5.56Di-n-butyl phthalate 1 07/06/23 18:11 V34997AMP
<2.30 µg/L 2.30 11.14,6-Dinitro-2-methylphenol 1 07/06/23 18:11 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 82 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-8
99743 Matrix:
6/29/2023 10:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<2.13 µg/L 2.13 11.12,4-Dinitrophenol 1 07/06/23 18:11 V34997AMP
<1.23 µg/L 1.23 5.562,4-Dinitrotoluene 1 07/06/23 18:11 V34997AMP
<0.899 µg/L 0.899 5.562,6-Dinitrotoluene 1 07/06/23 18:11 V34997AMP
<1.83 µg/L 1.83 5.56Di-n-Octyl Phthalate 1 07/06/23 18:11 V34997AMP
<0.277 µg/L 0.277 2.22Fluoranthene 1 07/06/23 18:11 V34997AMP
<0.895 µg/L 0.895 2.22Fluorene 1 07/06/23 18:11 V34997AMP
<1.09 µg/L 1.09 5.56Hexachlorobenzene 1 07/06/23 18:11 V34997AMP
<3.04 µg/L 3.04 5.56Hexachlorobutadiene 1 07/06/23 18:11 V34997AMP
<2.28 µg/L 2.28 5.56Hexachlorocyclopentadiene 1 07/06/23 18:11 V34997AMP
<1.96 µg/L 1.96 5.56Hexachloroethane 1 07/06/23 18:11 V34997AMP
<0.529 µg/L 0.529 2.22Indeno(1,2,3-cd)pyrene 1 07/06/23 18:11 V34997AMP
<0.493 µg/L 0.493 5.56Isophorone 1 07/06/23 18:11 V34997AMP
<1.27 µg/L 1.27 2.221-Methylnaphthalene 1 07/06/23 18:11 V34997AMP
<0.739 µg/L 0.739 2.222-Methylnaphthalene 1 07/06/23 18:11 V34997AMP
<0.808 µg/L 0.808 2.22Naphthalene 1 07/06/23 18:11 V34997AMP
<1.01 µg/L 1.01 5.56Nitrobenzene 1 07/06/23 18:11 V34997AMP
<0.548 µg/L 0.548 5.562-Nitrophenol 1 07/06/23 18:11 V34997AMP
<1.37 µg/L 1.37 11.14-Nitrophenol 1 07/06/23 18:11 V34997AMP
<1.22 µg/L 1.22 5.56N-Nitrosodiphenylamine 1 07/06/23 18:11 V34997AMP
<0.712 µg/L 0.712 5.56N-Nitroso-di-n-propylamine 1 07/06/23 18:11 V34997AMP
<1.59 µg/L 1.59 5.56Pentachlorophenol 1 07/06/23 18:11 V34997AMP
<0.475 µg/L 0.475 2.22Phenanthrene 1 07/06/23 18:11 V34997AMP
<0.723 µg/L 0.723 5.56Phenol 1 07/06/23 18:11 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 83 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-8
99743 Matrix:
6/29/2023 10:16
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.481 µg/L 0.481 2.22Pyrene 1 07/06/23 18:11 V34997AMP
<2.46 µg/L 2.46 5.561,2,4-Trichlorobenzene 1 07/06/23 18:11 V34997AMP
<1.47 µg/L 1.47 5.562,4,6-Trichlorophenol 1 07/06/23 18:11 V34997AMP
625.1Surrogate: Phenol-d5 25.9 Limits: 10-63%07/06/23 18:111 AMP
Surrogate: 2-Fluorobiphenyl 71.6 Limits: 49-118%07/06/23 18:111 AMP V34997
Surrogate: 2-Fluorophenol 40.4 Limits: 22-84%07/06/23 18:111 AMP V34997
Surrogate: Nitrobenzene-d5 59.0 Limits: 43-123%07/06/23 18:111 AMP V34997
Surrogate: 4-Terphenyl-d14 86.3 Limits: 49-151%07/06/23 18:111 AMP V34997
Surrogate: 2,4,6-Tribromophenol 67.0 Limits: 31-144%07/06/23 18:111 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 84 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-9
99744 Matrix:
6/29/2023 10:29
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 07/11/23 20:44 6200BTBL
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/11/23 20:44100 TBL V35229
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%07/11/23 20:44100 TBL V35229
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%07/11/23 20:44100 TBL V35229
Surrogate: Toluene-d8 91.6 Limits: 70-130%07/11/23 20:44100 TBL V35229
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 85 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-9
99744 Matrix:
6/29/2023 10:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
<180 µg/L 180 1000Acetone 100 07/11/23 20:44 V35229TBL
2420 µg/L 18.0 50.0Benzene 100 07/11/23 20:44 V35229TBL
<21.0 µg/L 21.0 50.0Bromobenzene 100 07/11/23 20:44 V35229TBL
<42.0 µg/L 42.0 100Bromochloromethane 100 07/11/23 20:44 V35229TBL
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 07/11/23 20:44 V35229TBL
<150 µg/L 150 500Bromoform 100 07/11/23 20:44 V35229TBL
<28.0 µg/L 28.0 100Bromomethane 100 07/11/23 20:44 V35229TBL
23.3 J µg/L 18.0 50.0n-Butylbenzene 100 07/11/23 20:44 V35229TBL
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 07/11/23 20:44 V35229TBL
<92.0 µg/L 92.0 200tert-Butyl benzene 100 07/11/23 20:44 V35229TBL
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 07/11/23 20:44 V35229TBL
<19.0 µg/L 19.0 50.0Chlorobenzene 100 07/11/23 20:44 V35229TBL
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 07/11/23 20:44 V35229TBL
<43.0 µg/L 43.0 100Chloroethane 100 07/11/23 20:44 V35229TBL
<22.0 µg/L 22.0 50.0Chloroform 100 07/11/23 20:44 V35229TBL
<22.0 µg/L 22.0 50.0Chloromethane 100 07/11/23 20:44 V35229TBL
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 07/11/23 20:44 V35229TBL
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 07/11/23 20:44 V35229TBL
80.1 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 07/11/23 20:44 V35229TBL
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 07/11/23 20:44 V35229TBL
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 07/11/23 20:44 V35229TBL
<23.0 µg/L 23.0 50.0Dibromomethane 100 07/11/23 20:44 V35229TBL
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 07/11/23 20:44 V35229TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 86 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-9
99744 Matrix:
6/29/2023 10:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 07/11/23 20:44 V35229TBL
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 07/11/23 20:44 V35229TBL
<120 µg/L 120 500Dichlorodifluoromethane 100 07/11/23 20:44 V35229TBL
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 07/11/23 20:44 V35229TBL
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 07/11/23 20:44 V35229TBL
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 07/11/23 20:44 V35229TBL
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 07/11/23 20:44 V35229TBL
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 07/11/23 20:44 V35229TBL
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 07/11/23 20:44 V35229TBL
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 07/11/23 20:44 V35229TBL
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 07/11/23 20:44 V35229TBL
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 07/11/23 20:44 V35229TBL
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 07/11/23 20:44 V35229TBL
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 07/11/23 20:44 V35229TBL
<4200 µg/L 4200 20000Ethanol 100 07/11/23 20:44 V35229TBL
1520 µg/L 17.0 50.0Ethylbenzene 100 07/11/23 20:44 V35229TBL
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 07/11/23 20:44 V35229TBL
<38.0 µg/L 38.0 1002-Hexanone 100 07/11/23 20:44 V35229TBL
91.1 µg/L 18.0 50.0Isopropylbenzene 100 07/11/23 20:44 V35229TBL
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 07/11/23 20:44 V35229TBL
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 07/11/23 20:44 V35229TBL
<14.0 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 07/11/23 20:44 V35229TBL
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 07/11/23 20:44 V35229TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 87 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-9
99744 Matrix:
6/29/2023 10:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
<33.0 µg/L 33.0 200Methylene Chloride 100 07/11/23 20:44 V35229TBL
2620 µg/L 47.0 100Naphthalene 100 07/11/23 20:44 V35229TBL
188 µg/L 19.0 50.0n-Propylbenzene 100 07/11/23 20:44 V35229TBL
<22.0 µg/L 22.0 50.0Styrene 100 07/11/23 20:44 V35229TBL
<160 µg/L 160 1000tert-Butyl Alcohol (TBA)100 07/11/23 20:44 V35229TBL
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 07/11/23 20:44 V35229TBL
4910 µg/L 190 1000tert-Amyl Alcohol (TAA)100 07/11/23 20:44 V35229TBL
<28.0 µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 07/11/23 20:44 V35229TBL
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 07/11/23 20:44 V35229TBL
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 07/11/23 20:44 V35229TBL
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 07/11/23 20:44 V35229TBL
423 µg/L 22.0 50.0Toluene 100 07/11/23 20:44 V35229TBL
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 07/11/23 20:44 V35229TBL
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 07/11/23 20:44 V35229TBL
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 07/11/23 20:44 V35229TBL
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 07/11/23 20:44 V35229TBL
<18.0 µg/L 18.0 50.0Trichloroethene 100 07/11/23 20:44 V35229TBL
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 07/11/23 20:44 V35229TBL
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 07/11/23 20:44 V35229TBL
1630 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 07/11/23 20:44 V35229TBL
458 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 07/11/23 20:44 V35229TBL
<100 µg/L 100 500Vinyl Acetate 100 07/11/23 20:44 V35229TBL
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 07/11/23 20:44 V35229TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 88 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-9
99744 Matrix:
6/29/2023 10:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
2970 µg/L 21.0 50.0o-Xylene 100 07/11/23 20:44 V35229TBL
6700 µg/L 42.0 100m,p-Xylene 100 07/11/23 20:44 V35229TBL
9670 µg/L 21.0 50.0Xylene (Total)100 07/11/23 20:44 V35229
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/11/23 20:44100 TBL V35229
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%07/11/23 20:44100 TBL V35229
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%07/11/23 20:44100 TBL V35229
Surrogate: Toluene-d8 91.6 Limits: 70-130%07/11/23 20:44100 TBL V35229
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.335 µg/L 0.335 2.22Acenaphthene 1 07/06/23 18:34 V34997AMP
<0.329 µg/L 0.329 2.22Acenaphthylene 1 07/06/23 18:34 V34997AMP
<0.927 µg/L 0.927 2.22Anthracene 1 07/06/23 18:34 V34997AMP
<1.47 M µg/L 1.47 11.1Benzidine 1 07/06/23 18:34 V34997AMP
<0.707 µg/L 0.707 2.22Benzo(a)anthracene 1 07/06/23 18:34 V34997AMP
<1.13 µg/L 1.13 2.22Benzo(a)pyrene 1 07/06/23 18:34 V34997AMP
<2.77 µg/L 2.77 5.56Benzo(b)fluoranthene 1 07/06/23 18:34 V34997AMP
<1.12 µg/L 1.12 5.56Benzo(g,h,i)perylene 1 07/06/23 18:34 V34997AMP
<2.21 µg/L 2.21 5.56Benzo(k)fluoranthene 1 07/06/23 18:34 V34997AMP
<1.22 µg/L 1.22 11.1Benzoic Acid 1 07/06/23 18:34 V34997AMP
<0.760 µg/L 0.760 5.56Benzyl alcohol 1 07/06/23 18:34 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 89 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-9
99744 Matrix:
6/29/2023 10:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.520 µg/L 0.520 5.56Bis(2-Chloroethoxy)methane 1 07/06/23 18:34 V34997AMP
<1.16 µg/L 1.16 5.56Bis(2-Chloroethyl)ether 1 07/06/23 18:34 V34997AMP
<1.20 µg/L 1.20 5.56Bis(2-Chloroisopropyl)ether 1 07/06/23 18:34 V34997AMP
<3.84 µg/L 3.84 11.1Bis(2-ethylhexyl)phthalate 1 07/06/23 18:34 V34997AMP
<1.23 µg/L 1.23 5.564-Bromophenyl phenyl ether 1 07/06/23 18:34 V34997AMP
<2.03 µg/L 2.03 5.56Butyl benzyl phthalate 1 07/06/23 18:34 V34997AMP
<1.31 µg/L 1.31 5.564-Chloro-3-methylphenol 1 07/06/23 18:34 V34997AMP
<8.19 µg/L 8.19 22.22-Chloronaphthalene 1 07/06/23 18:34 V34997AMP
<1.04 µg/L 1.04 11.12-Chlorophenol 1 07/06/23 18:34 V34997AMP
<1.90 µg/L 1.90 5.564-Chlorophenyl phenyl ether 1 07/06/23 18:34 V34997AMP
<0.449 µg/L 0.449 2.22Chrysene 1 07/06/23 18:34 V34997AMP
<0.481 µg/L 0.481 2.22Dibenz(a,h)anthracene 1 07/06/23 18:34 V34997AMP
<0.951 µg/L 0.951 5.56Dibenzofuran 1 07/06/23 18:34 V34997AMP
<2.22 µg/L 2.22 5.561,2-Dichlorobenzene 1 07/06/23 18:34 V34997AMP
<2.22 µg/L 2.22 5.561,3-Dichlorobenzene 1 07/06/23 18:34 V34997AMP
<2.28 µg/L 2.28 5.561,4-Dichlorobenzene 1 07/06/23 18:34 V34997AMP
<2.10 µg/L 2.10 5.563,3'-Dichlorobenzidine 1 07/06/23 18:34 V34997AMP
<1.62 µg/L 1.62 11.12,4-Dichlorophenol 1 07/06/23 18:34 V34997AMP
<0.828 µg/L 0.828 5.56Diethyl phthalate 1 07/06/23 18:34 V34997AMP
<1.04 µg/L 1.04 5.56Dimethyl phthalate 1 07/06/23 18:34 V34997AMP
3.11 J µg/L 1.74 22.22,4-Dimethylphenol 1 07/06/23 18:34 V34997AMP
<2.29 µg/L 2.29 5.56Di-n-butyl phthalate 1 07/06/23 18:34 V34997AMP
<2.30 µg/L 2.30 11.14,6-Dinitro-2-methylphenol 1 07/06/23 18:34 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 90 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-9
99744 Matrix:
6/29/2023 10:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<2.13 µg/L 2.13 11.12,4-Dinitrophenol 1 07/06/23 18:34 V34997AMP
<1.23 µg/L 1.23 5.562,4-Dinitrotoluene 1 07/06/23 18:34 V34997AMP
<0.899 µg/L 0.899 5.562,6-Dinitrotoluene 1 07/06/23 18:34 V34997AMP
<1.83 µg/L 1.83 5.56Di-n-Octyl Phthalate 1 07/06/23 18:34 V34997AMP
<0.277 µg/L 0.277 2.22Fluoranthene 1 07/06/23 18:34 V34997AMP
<0.895 µg/L 0.895 2.22Fluorene 1 07/06/23 18:34 V34997AMP
<1.09 µg/L 1.09 5.56Hexachlorobenzene 1 07/06/23 18:34 V34997AMP
<3.04 µg/L 3.04 5.56Hexachlorobutadiene 1 07/06/23 18:34 V34997AMP
<2.28 µg/L 2.28 5.56Hexachlorocyclopentadiene 1 07/06/23 18:34 V34997AMP
<1.96 µg/L 1.96 5.56Hexachloroethane 1 07/06/23 18:34 V34997AMP
<0.529 µg/L 0.529 2.22Indeno(1,2,3-cd)pyrene 1 07/06/23 18:34 V34997AMP
<0.493 µg/L 0.493 5.56Isophorone 1 07/06/23 18:34 V34997AMP
24.2 µg/L 1.27 2.221-Methylnaphthalene 1 07/06/23 18:34 V34997AMP
63.5 µg/L 0.739 2.222-Methylnaphthalene 1 07/06/23 18:34 V34997AMP
295 µg/L 1.62 4.44Naphthalene 2 07/07/23 11:33 V34997AMP
<1.01 µg/L 1.01 5.56Nitrobenzene 1 07/06/23 18:34 V34997AMP
<0.548 µg/L 0.548 5.562-Nitrophenol 1 07/06/23 18:34 V34997AMP
<1.37 µg/L 1.37 11.14-Nitrophenol 1 07/06/23 18:34 V34997AMP
<1.22 µg/L 1.22 5.56N-Nitrosodiphenylamine 1 07/06/23 18:34 V34997AMP
<0.712 µg/L 0.712 5.56N-Nitroso-di-n-propylamine 1 07/06/23 18:34 V34997AMP
<1.59 µg/L 1.59 5.56Pentachlorophenol 1 07/06/23 18:34 V34997AMP
<0.475 µg/L 0.475 2.22Phenanthrene 1 07/06/23 18:34 V34997AMP
<0.723 µg/L 0.723 5.56Phenol 1 07/06/23 18:34 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 91 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-9
99744 Matrix:
6/29/2023 10:29
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.481 µg/L 0.481 2.22Pyrene 1 07/06/23 18:34 V34997AMP
<2.46 µg/L 2.46 5.561,2,4-Trichlorobenzene 1 07/06/23 18:34 V34997AMP
<1.47 µg/L 1.47 5.562,4,6-Trichlorophenol 1 07/06/23 18:34 V34997AMP
625.1Surrogate: Phenol-d5 27.9 Limits: 10-63%07/06/23 18:341 AMP
Surrogate: 2-Fluorobiphenyl 70.1 Limits: 49-118%07/06/23 18:341 AMP V34997
Surrogate: 2-Fluorophenol 43.4 Limits: 22-84%07/06/23 18:341 AMP V34997
Surrogate: Nitrobenzene-d5 64.0 Limits: 43-123%07/06/23 18:341 AMP V34997
Surrogate: 4-Terphenyl-d14 81.1 Limits: 49-151%07/06/23 18:341 AMP V34997
Surrogate: 2,4,6-Tribromophenol 67.2 Limits: 31-144%07/06/23 18:341 AMP V34997
625.1Surrogate: Phenol-d5 25.9 Limits: 10-63%07/07/23 11:332 AMP
Surrogate: 2-Fluorobiphenyl 71.8 Limits: 49-118%07/07/23 11:332 AMP V34997
Surrogate: 2-Fluorophenol 45.2 Limits: 22-84%07/07/23 11:332 AMP V34997
Surrogate: Nitrobenzene-d5 63.5 Limits: 43-123%07/07/23 11:332 AMP V34997
Surrogate: 4-Terphenyl-d14 77.7 Limits: 49-151%07/07/23 11:332 AMP V34997
Surrogate: 2,4,6-Tribromophenol 67.8 Limits: 31-144%07/07/23 11:332 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 92 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-10
99745 Matrix:
6/29/2023 10:43
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 07/11/23 14:31 6200BTBL
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/11/23 14:311 TBL V35229
Surrogate: Dibromofluoromethane 95.0 Limits: 70-130%07/11/23 14:311 TBL V35229
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%07/11/23 14:311 TBL V35229
Surrogate: Toluene-d8 92.2 Limits: 70-130%07/11/23 14:311 TBL V35229
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 93 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-10
99745 Matrix:
6/29/2023 10:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
7.08 J µg/L 1.80 10.0Acetone 1 07/11/23 14:31 V35229TBL
1.69 µg/L 0.180 0.500Benzene 1 07/11/23 14:31 V35229TBL
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/11/23 14:31 V35229TBL
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/11/23 14:31 V35229TBL
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/11/23 14:31 V35229TBL
<1.50 µg/L 1.50 5.00Bromoform 1 07/11/23 14:31 V35229TBL
<0.280 µg/L 0.280 1.00Bromomethane 1 07/11/23 14:31 V35229TBL
0.717 µg/L 0.180 0.500n-Butylbenzene 1 07/11/23 14:31 V35229TBL
0.421 J µg/L 0.200 0.500sec-Butyl benzene 1 07/11/23 14:31 V35229TBL
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/11/23 14:31 V35229TBL
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/11/23 14:31 V35229TBL
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/11/23 14:31 V35229TBL
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/11/23 14:31 V35229TBL
<0.430 µg/L 0.430 1.00Chloroethane 1 07/11/23 14:31 V35229TBL
<0.220 µg/L 0.220 0.500Chloroform 1 07/11/23 14:31 V35229TBL
<0.220 µg/L 0.220 0.500Chloromethane 1 07/11/23 14:31 V35229TBL
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/11/23 14:31 V35229TBL
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/11/23 14:31 V35229TBL
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/11/23 14:31 V35229TBL
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/11/23 14:31 V35229TBL
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/11/23 14:31 V35229TBL
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/11/23 14:31 V35229TBL
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/11/23 14:31 V35229TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 94 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-10
99745 Matrix:
6/29/2023 10:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/11/23 14:31 V35229TBL
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/11/23 14:31 V35229TBL
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/11/23 14:31 V35229TBL
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/11/23 14:31 V35229TBL
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/11/23 14:31 V35229TBL
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/11/23 14:31 V35229TBL
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/11/23 14:31 V35229TBL
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/11/23 14:31 V35229TBL
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/11/23 14:31 V35229TBL
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/11/23 14:31 V35229TBL
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/11/23 14:31 V35229TBL
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/11/23 14:31 V35229TBL
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/11/23 14:31 V35229TBL
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/11/23 14:31 V35229TBL
<42.0 µg/L 42.0 200Ethanol 1 07/11/23 14:31 V35229TBL
9.01 µg/L 0.170 0.500Ethylbenzene 1 07/11/23 14:31 V35229TBL
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/11/23 14:31 V35229TBL
<0.380 µg/L 0.380 1.002-Hexanone 1 07/11/23 14:31 V35229TBL
1.28 µg/L 0.180 0.500Isopropylbenzene 1 07/11/23 14:31 V35229TBL
0.480 J µg/L 0.089 0.5004-Isopropyl toluene 1 07/11/23 14:31 V35229TBL
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/11/23 14:31 V35229TBL
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/11/23 14:31 V35229TBL
0.324 J µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/11/23 14:31 V35229TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 95 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-10
99745 Matrix:
6/29/2023 10:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/11/23 14:31 V35229TBL
4.92 µg/L 0.470 1.00Naphthalene 1 07/11/23 14:31 V35229TBL
2.90 µg/L 0.190 0.500n-Propylbenzene 1 07/11/23 14:31 V35229TBL
<0.220 µg/L 0.220 0.500Styrene 1 07/11/23 14:31 V35229TBL
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 07/11/23 14:31 V35229TBL
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/11/23 14:31 V35229TBL
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 07/11/23 14:31 V35229TBL
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/11/23 14:31 V35229TBL
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/11/23 14:31 V35229TBL
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/11/23 14:31 V35229TBL
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/11/23 14:31 V35229TBL
0.751 µg/L 0.220 0.500Toluene 1 07/11/23 14:31 V35229TBL
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/11/23 14:31 V35229TBL
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/11/23 14:31 V35229TBL
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/11/23 14:31 V35229TBL
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/11/23 14:31 V35229TBL
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/11/23 14:31 V35229TBL
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/11/23 14:31 V35229TBL
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/11/23 14:31 V35229TBL
22.5 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/11/23 14:31 V35229TBL
7.38 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/11/23 14:31 V35229TBL
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/11/23 14:31 V35229TBL
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/11/23 14:31 V35229TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 96 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-10
99745 Matrix:
6/29/2023 10:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35227 07/11/23 08:00
17.3 µg/L 0.210 0.500o-Xylene 1 07/11/23 14:31 V35229TBL
43.1 µg/L 0.420 1.00m,p-Xylene 1 07/11/23 14:31 V35229TBL
60.4 µg/L 0.210 0.500Xylene (Total)1 07/11/23 14:31 V35229
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/11/23 14:311 TBL V35229
Surrogate: Dibromofluoromethane 95.0 Limits: 70-130%07/11/23 14:311 TBL V35229
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%07/11/23 14:311 TBL V35229
Surrogate: Toluene-d8 92.2 Limits: 70-130%07/11/23 14:311 TBL V35229
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.335 µg/L 0.335 2.22Acenaphthene 1 07/06/23 18:56 V34997AMP
<0.329 µg/L 0.329 2.22Acenaphthylene 1 07/06/23 18:56 V34997AMP
<0.927 µg/L 0.927 2.22Anthracene 1 07/06/23 18:56 V34997AMP
<1.47 M µg/L 1.47 11.1Benzidine 1 07/06/23 18:56 V34997AMP
<0.707 µg/L 0.707 2.22Benzo(a)anthracene 1 07/06/23 18:56 V34997AMP
<1.13 µg/L 1.13 2.22Benzo(a)pyrene 1 07/06/23 18:56 V34997AMP
<2.77 µg/L 2.77 5.56Benzo(b)fluoranthene 1 07/06/23 18:56 V34997AMP
<1.12 µg/L 1.12 5.56Benzo(g,h,i)perylene 1 07/06/23 18:56 V34997AMP
<2.21 µg/L 2.21 5.56Benzo(k)fluoranthene 1 07/06/23 18:56 V34997AMP
<1.22 µg/L 1.22 11.1Benzoic Acid 1 07/06/23 18:56 V34997AMP
<0.760 µg/L 0.760 5.56Benzyl alcohol 1 07/06/23 18:56 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 97 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-10
99745 Matrix:
6/29/2023 10:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.520 µg/L 0.520 5.56Bis(2-Chloroethoxy)methane 1 07/06/23 18:56 V34997AMP
<1.16 µg/L 1.16 5.56Bis(2-Chloroethyl)ether 1 07/06/23 18:56 V34997AMP
<1.20 µg/L 1.20 5.56Bis(2-Chloroisopropyl)ether 1 07/06/23 18:56 V34997AMP
<3.84 µg/L 3.84 11.1Bis(2-ethylhexyl)phthalate 1 07/06/23 18:56 V34997AMP
<1.23 µg/L 1.23 5.564-Bromophenyl phenyl ether 1 07/06/23 18:56 V34997AMP
<2.03 µg/L 2.03 5.56Butyl benzyl phthalate 1 07/06/23 18:56 V34997AMP
<1.31 µg/L 1.31 5.564-Chloro-3-methylphenol 1 07/06/23 18:56 V34997AMP
<8.19 µg/L 8.19 22.22-Chloronaphthalene 1 07/06/23 18:56 V34997AMP
<1.04 µg/L 1.04 11.12-Chlorophenol 1 07/06/23 18:56 V34997AMP
<1.90 µg/L 1.90 5.564-Chlorophenyl phenyl ether 1 07/06/23 18:56 V34997AMP
<0.449 µg/L 0.449 2.22Chrysene 1 07/06/23 18:56 V34997AMP
<0.481 µg/L 0.481 2.22Dibenz(a,h)anthracene 1 07/06/23 18:56 V34997AMP
<0.951 µg/L 0.951 5.56Dibenzofuran 1 07/06/23 18:56 V34997AMP
<2.22 µg/L 2.22 5.561,2-Dichlorobenzene 1 07/06/23 18:56 V34997AMP
<2.22 µg/L 2.22 5.561,3-Dichlorobenzene 1 07/06/23 18:56 V34997AMP
<2.28 µg/L 2.28 5.561,4-Dichlorobenzene 1 07/06/23 18:56 V34997AMP
<2.10 µg/L 2.10 5.563,3'-Dichlorobenzidine 1 07/06/23 18:56 V34997AMP
<1.62 µg/L 1.62 11.12,4-Dichlorophenol 1 07/06/23 18:56 V34997AMP
<0.828 µg/L 0.828 5.56Diethyl phthalate 1 07/06/23 18:56 V34997AMP
<1.04 µg/L 1.04 5.56Dimethyl phthalate 1 07/06/23 18:56 V34997AMP
<1.74 µg/L 1.74 22.22,4-Dimethylphenol 1 07/06/23 18:56 V34997AMP
<2.29 µg/L 2.29 5.56Di-n-butyl phthalate 1 07/06/23 18:56 V34997AMP
<2.30 µg/L 2.30 11.14,6-Dinitro-2-methylphenol 1 07/06/23 18:56 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 98 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-10
99745 Matrix:
6/29/2023 10:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<2.13 µg/L 2.13 11.12,4-Dinitrophenol 1 07/06/23 18:56 V34997AMP
<1.23 µg/L 1.23 5.562,4-Dinitrotoluene 1 07/06/23 18:56 V34997AMP
<0.899 µg/L 0.899 5.562,6-Dinitrotoluene 1 07/06/23 18:56 V34997AMP
<1.83 µg/L 1.83 5.56Di-n-Octyl Phthalate 1 07/06/23 18:56 V34997AMP
<0.277 µg/L 0.277 2.22Fluoranthene 1 07/06/23 18:56 V34997AMP
<0.895 µg/L 0.895 2.22Fluorene 1 07/06/23 18:56 V34997AMP
<1.09 µg/L 1.09 5.56Hexachlorobenzene 1 07/06/23 18:56 V34997AMP
<3.04 µg/L 3.04 5.56Hexachlorobutadiene 1 07/06/23 18:56 V34997AMP
<2.28 µg/L 2.28 5.56Hexachlorocyclopentadiene 1 07/06/23 18:56 V34997AMP
<1.96 µg/L 1.96 5.56Hexachloroethane 1 07/06/23 18:56 V34997AMP
<0.529 µg/L 0.529 2.22Indeno(1,2,3-cd)pyrene 1 07/06/23 18:56 V34997AMP
<0.493 µg/L 0.493 5.56Isophorone 1 07/06/23 18:56 V34997AMP
<1.27 µg/L 1.27 2.221-Methylnaphthalene 1 07/06/23 18:56 V34997AMP
1.27 J µg/L 0.739 2.222-Methylnaphthalene 1 07/06/23 18:56 V34997AMP
3.32 µg/L 0.808 2.22Naphthalene 1 07/06/23 18:56 V34997AMP
<1.01 µg/L 1.01 5.56Nitrobenzene 1 07/06/23 18:56 V34997AMP
<0.548 µg/L 0.548 5.562-Nitrophenol 1 07/06/23 18:56 V34997AMP
<1.37 µg/L 1.37 11.14-Nitrophenol 1 07/06/23 18:56 V34997AMP
<1.22 µg/L 1.22 5.56N-Nitrosodiphenylamine 1 07/06/23 18:56 V34997AMP
<0.712 µg/L 0.712 5.56N-Nitroso-di-n-propylamine 1 07/06/23 18:56 V34997AMP
<1.59 µg/L 1.59 5.56Pentachlorophenol 1 07/06/23 18:56 V34997AMP
<0.475 µg/L 0.475 2.22Phenanthrene 1 07/06/23 18:56 V34997AMP
<0.723 µg/L 0.723 5.56Phenol 1 07/06/23 18:56 V34997AMP
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 99 of 133
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-181-0037
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4486 Received : 06/30/2023
Mickey's 1, Station 19
Report Date : 07/20/2023
Sample ID :
Lab No :
Sampled:MW-10
99745 Matrix:
6/29/2023 10:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V34962 07/05/23 10:18
<0.481 µg/L 0.481 2.22Pyrene 1 07/06/23 18:56 V34997AMP
<2.46 µg/L 2.46 5.561,2,4-Trichlorobenzene 1 07/06/23 18:56 V34997AMP
<1.47 µg/L 1.47 5.562,4,6-Trichlorophenol 1 07/06/23 18:56 V34997AMP
625.1Surrogate: Phenol-d5 26.0 Limits: 10-63%07/06/23 18:561 AMP
Surrogate: 2-Fluorobiphenyl 75.7 Limits: 49-118%07/06/23 18:561 AMP V34997
Surrogate: 2-Fluorophenol 40.2 Limits: 22-84%07/06/23 18:561 AMP V34997
Surrogate: Nitrobenzene-d5 64.4 Limits: 43-123%07/06/23 18:561 AMP V34997
Surrogate: 4-Terphenyl-d14 88.1 Limits: 49-151%07/06/23 18:561 AMP V34997
Surrogate: 2,4,6-Tribromophenol 72.0 Limits: 31-144%07/06/23 18:561 AMP V34997
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Estimated valueJBeyond holding timeH
Method Quantitation LimitMQLMinimum valueM
Page 100 of 133
Sample ID Report Lab NoLRB‐V34962 23‐181‐0037 LRB
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Hexadecanoic acid 12.2 ug/L 1 625 7/5/2023 18:06 APANN V34997
Sample ID Report Lab NoTW‐1 23‐181‐0037 99735
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Hexadecanoic acid 15.1 ug/L 1 625 7/6/2023 15:11 APANN V34997
Sample ID Report Lab NoMW‐1 23‐181‐0037 99736
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Pentanol, methyl‐214.4 ug/L 1 625 7/6/2023 15:34 APANN V34997
Cyclopentanol, methyl‐108.9 ug/L 1 625 7/6/2023 15:34 APANN V34997
Tetracyclo‐…31.2 ug/L 1 625 7/6/2023 15:34 APANN V34997
Benzene, diethyl‐29.7 ug/L 1 625 7/6/2023 15:34 APANN V34997
Sample ID Report Lab NoMW‐2 23‐181‐0037 99737
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Pentanol, methyl‐12.6 ug/L 1 625 7/6/2023 15:56 APANN V34997
Hexadecanoic acid 16.8 ug/L 1 625 7/6/2023 15:56 APANN V34997
Sample ID Report Lab NoMW‐3 23‐181‐0037 99738
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Pentanol, methyl‐13.2 ug/L 1 625 7/6/2023 16:19 APANN V34997
Indane 45.6 ug/L 1 625 7/6/2023 16:19 APANN V34997
Benzene, diethyl‐14.7 ug/L 1 625 7/6/2023 16:19 APANN V34997
Indan, methyl‐17.9 ug/L 1 625 7/6/2023 16:19 APANN V34997
Page 101 of 133
Sample ID Report Lab NoMW‐4 23‐181‐0037 99739
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Benzene, dimethyl‐60.8 ug/L 1 625 7/6/2023 16:41 APANN V34997
Benzene, ethyl‐methyl‐252.1 ug/L 1 625 7/6/2023 16:41 APANN V34997
Indane 115.6 ug/L 1 625 7/6/2023 16:41 APANN V34997
Benzene, diethyl‐98.6 ug/L 1 625 7/6/2023 16:41 APANN V34997
Benzene, methyl‐…120.1 ug/L 1 625 7/6/2023 16:41 APANN V34997
Benzene, ethyl‐dimethyl‐52.9 ug/L 1 625 7/6/2023 16:41 APANN V34997
Benzene, tetramethyl‐86.6 ug/L 1 625 7/6/2023 16:41 APANN V34997
Benzene, tetramethyl‐68.2 ug/L 1 625 7/6/2023 16:41 APANN V34997
Sample ID Report Lab NoMW‐5 23‐181‐0037 99740
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Cyclopentadecane 34.3 ug/L 1 625 7/6/2023 17:04 APANN V34997
Sample ID Report Lab NoMW‐6 23‐181‐0037 99741
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
No TICs detected N.D. ug/L 1 625 7/6/2023 17:26 APANN V34997
Sample ID Report Lab NoMW‐7 23‐181‐0037 99742
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
No TICs detected N.D. ug/L 1 625 7/6/2023 17:49 APANN V34997
Sample ID Report Lab No
MW‐8 23‐181‐0037 99743
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
No TICs detected N.D. ug/L 1 625 7/6/2023 18:11 APANN V34997
Page 102 of 133
Sample ID Report Lab NoMW‐9 23‐181‐0037 99744
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Pentanol, methyl‐138.6 ug/L 1 625 7/6/2023 18:34 APANN V34997
Cyclopentanol, methyl‐136.4 ug/L 1 625 7/6/2023 18:34 APANN V34997
Ethylbenzene 179.8 ug/L 1 625 7/6/2023 18:34 APANN V34997
Benzene, dimethyl‐432.4 ug/L 1 625 7/6/2023 18:34 APANN V34997
Benzene, ethyl‐methyl‐164.6 ug/L 1 625 7/6/2023 18:34 APANN V34997
Benzene, trimethyl‐261.9 ug/L 1 625 7/6/2023 18:34 APANN V34997
Nezene, ethenyl‐methyl‐102.9 ug/L 1 625 7/6/2023 18:34 APANN V34997
Sample ID Report Lab No
MW‐10 23‐181‐0037 99745
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Benzene, dimethyl‐12.9 ug/L 1 625 7/6/2023 18:56 APANN V34997
Benzene, trimethyl‐13.6 ug/L 1 625 7/6/2023 18:56 APANN V34997
Page 103 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
Associated Lab Samples: 99744, 99745
LRB-V35227 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/11/23 12:5210.01.80<1.80µg/LAcetone
07/11/23 12:520.5000.180<0.180µg/LBenzene
07/11/23 12:520.5000.210<0.210µg/LBromobenzene
07/11/23 12:521.000.420<0.420µg/LBromochloromethane
07/11/23 12:520.5000.160<0.160µg/LBromodichloromethane
07/11/23 12:525.001.50<1.50µg/LBromoform
07/11/23 12:521.000.280<0.280µg/LBromomethane
07/11/23 12:520.5000.180<0.180µg/Ln-Butylbenzene
07/11/23 12:520.5000.200<0.200µg/Lsec-Butyl benzene
07/11/23 12:522.000.920<0.920µg/Ltert-Butyl benzene
07/11/23 12:520.5000.180<0.180µg/LCarbon Tetrachloride
07/11/23 12:520.5000.190<0.190µg/LChlorobenzene
07/11/23 12:520.5000.190<0.190µg/LChlorodibromomethane
07/11/23 12:521.000.430<0.430µg/LChloroethane
07/11/23 12:520.5000.220<0.220µg/LChloroform
07/11/23 12:520.5000.220<0.220µg/LChloromethane
07/11/23 12:520.5000.200<0.200µg/L2-Chlorotoluene
07/11/23 12:520.5000.200<0.200µg/L4-Chlorotoluene
07/11/23 12:520.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/11/23 12:522.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/11/23 12:520.5000.200<0.200µg/L1,2-Dibromoethane
07/11/23 12:520.5000.230<0.230µg/LDibromomethane
07/11/23 12:520.5000.220<0.220µg/L1,2-Dichlorobenzene
07/11/23 12:520.5000.190<0.190µg/L1,3-Dichlorobenzene
07/11/23 12:520.5000.210<0.210µg/L1,4-Dichlorobenzene
07/11/23 12:525.001.20<1.20µg/LDichlorodifluoromethane
07/11/23 12:520.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 27Date:07/20/2023 11:26 AM
Page 104 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
Associated Lab Samples: 99744, 99745
LRB-V35227 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/11/23 12:520.5000.150<0.150µg/L1,2-Dichloroethane
07/11/23 12:520.5000.150<0.150µg/L1,1-Dichloroethene
07/11/23 12:520.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/11/23 12:520.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/11/23 12:520.5000.190<0.190µg/L1,2-Dichloropropane
07/11/23 12:520.5000.130<0.130µg/L1,3-Dichloropropane
07/11/23 12:522.000.210<0.210µg/L2,2-Dichloropropane
07/11/23 12:520.5000.200<0.200µg/L1,1-Dichloropropene
07/11/23 12:520.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/11/23 12:520.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/11/23 12:5220042.0<42.0µg/LEthanol
07/11/23 12:520.5000.170<0.170µg/LEthylbenzene
07/11/23 12:523.000.350<0.350µg/LHexachlorobutadiene
07/11/23 12:521.000.380<0.380µg/L2-Hexanone
07/11/23 12:520.5000.180<0.180µg/LIsopropylbenzene
07/11/23 12:520.5000.089<0.089µg/L4-Isopropyl toluene
07/11/23 12:525.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/11/23 12:521.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/11/23 12:521.000.078<0.078µg/L4-Methyl-2-Pentanone
07/11/23 12:522.000.330<0.330µg/LMethylene Chloride
07/11/23 12:521.000.470<0.470µg/LNaphthalene
07/11/23 12:520.5000.190<0.190µg/Ln-Propylbenzene
07/11/23 12:520.5000.220<0.220µg/LStyrene
07/11/23 12:5210.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
07/11/23 12:5210.00.350<0.350µg/Ltert-Butyl formate (TBF)
07/11/23 12:5210.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
07/11/23 12:5210.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 27Date:07/20/2023 11:26 AM
Page 105 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
Associated Lab Samples: 99744, 99745
LRB-V35227 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/11/23 12:520.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
07/11/23 12:520.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/11/23 12:520.5000.220<0.220µg/LTetrachloroethene
07/11/23 12:520.5000.220<0.220µg/LToluene
07/11/23 12:520.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/11/23 12:520.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/11/23 12:520.5000.160<0.160µg/L1,1,1-Trichloroethane
07/11/23 12:520.5000.096<0.096µg/L1,1,2-Trichloroethane
07/11/23 12:520.5000.180<0.180µg/LTrichloroethene
07/11/23 12:520.5000.180<0.180µg/LTrichlorofluoromethane
07/11/23 12:520.5000.270<0.270µg/L1,2,3-Trichloropropane
07/11/23 12:520.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/11/23 12:520.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/11/23 12:525.001.00<1.00µg/LVinyl Acetate
07/11/23 12:520.5000.170<0.170µg/LVinyl Chloride
07/11/23 12:520.5000.210<0.210µg/Lo-Xylene
07/11/23 12:521.000.420<0.420µg/Lm,p-Xylene
07/11/23 12:5210.01.00<1.00µg/L3,3-Dimethyl-1-butanol
07/11/23 12:524-Bromofluorobenzene (S)101 70-130
07/11/23 12:52Dibromofluoromethane (S)95.4 70-130
07/11/23 12:521,2-Dichloroethane - d4 (S)98.6 70-130
07/11/23 12:52Toluene-d8 (S)92.4 70-130
Page 3 of 27Date:07/20/2023 11:26 AM
Page 106 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
29.3 73.272.028.840.0µg/LAcetone 40-160 1.7 20.0
21.9 11011122.120.0µg/LBenzene 70-130 0.9 20.0
20.3 10210521.020.0µg/LBromobenzene 70-130 3.3 20.0
22.5 11311322.520.0µg/LBromochloromethane 70-130 0.0 20.0
22.8 11411623.120.0µg/LBromodichloromethane 70-130 1.3 20.0
21.1 10610521.020.0µg/LBromoform 70-130 0.4 20.0
16.8 84.077.515.520.0µg/LBromomethane 60-140 8.0 20.0
21.1 10610921.720.0µg/Ln-Butylbenzene 70-130 2.8 20.0
21.1 10611021.920.0µg/Lsec-Butyl benzene 70-130 3.7 20.0
20.9 10510821.620.0µg/Ltert-Butyl benzene 70-130 3.2 20.0
22.1 11111322.520.0µg/LCarbon Tetrachloride 70-130 1.7 20.0
21.2 10610721.420.0µg/LChlorobenzene 70-130 0.9 20.0
21.1 10610621.220.0µg/LChlorodibromomethane 70-130 0.4 20.0
21.8 10910721.420.0µg/LChloroethane 60-140 1.8 20.0
22.2 11111022.020.0µg/LChloroform 70-130 0.9 20.0
19.3 96.591.018.220.0µg/LChloromethane 60-140 5.8 20.0
21.5 10811022.020.0µg/L2-Chlorotoluene 70-130 2.2 20.0
20.8 10410621.220.0µg/L4-Chlorotoluene 70-130 1.9 20.0
22.4 11211222.320.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.4 20.0
18.7 93.593.018.620.0µg/L1,2-Dibromo-3-Chloropropane 70-130 0.5 20.0
21.3 10710420.820.0µg/L1,2-Dibromoethane 70-130 2.3 20.0
23.0 11511422.720.0µg/LDibromomethane 70-130 1.3 20.0
20.1 10110320.620.0µg/L1,2-Dichlorobenzene 70-130 2.4 20.0
20.3 10210420.720.0µg/L1,3-Dichlorobenzene 70-130 1.9 20.0
19.9 99.510320.620.0µg/L1,4-Dichlorobenzene 70-130 3.4 20.0
19.5 97.599.019.820.0µg/LDichlorodifluoromethane 60-140 1.5 20.0
Page 4 of 27Date:07/20/2023 11:26 AM
Page 107 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
22.4 11211222.420.0µg/L1,1-Dichloroethane 70-130 0.0 20.0
22.9 11511623.120.0µg/L1,2-Dichloroethane 70-130 0.8 20.0
22.5 11311523.020.0µg/L1,1-Dichloroethene 70-130 2.1 20.0
22.8 11411623.220.0µg/Lcis-1,2-Dichloroethene 70-130 1.7 20.0
22.8 11411422.720.0µg/Ltrans-1,2-Dichloroethene 70-130 0.4 20.0
22.8 11411422.820.0µg/L1,2-Dichloropropane 70-130 0.0 20.0
20.5 10310320.620.0µg/L1,3-Dichloropropane 70-130 0.4 20.0
23.4 11712124.120.0µg/L2,2-Dichloropropane 70-130 2.9 20.0
22.2 11111422.720.0µg/L1,1-Dichloropropene 70-130 2.2 20.0
22.5 11311522.920.0µg/Lcis-1,3-Dichloropropene 70-130 1.7 20.0
23.3 11711623.220.0µg/Ltrans-1,3-Dichloropropene 70-130 0.4 20.0
658 132106532500µg/LEthanol 60-140 21.1*20.0
21.1 10610921.720.0µg/LEthylbenzene 70-130 2.8 20.0
20.4 10210821.620.0µg/LHexachlorobutadiene 70-130 5.7 20.0
18.1 90.591.018.220.0µg/L2-Hexanone 60-140 0.5 20.0
21.1 10610921.820.0µg/LIsopropylbenzene 70-130 3.2 20.0
21.2 10611021.920.0µg/L4-Isopropyl toluene 70-130 3.2 20.0
17.3 86.579.515.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 8.4 20.0
21.2 10610520.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.4 20.0
22.9 11511322.520.0µg/L4-Methyl-2-Pentanone 60-140 1.7 20.0
23.4 11711522.920.0µg/LMethylene Chloride 70-130 2.1 20.0
19.3 96.597.519.520.0µg/LNaphthalene 70-130 1.0 20.0
21.5 10811222.320.0µg/Ln-Propylbenzene 70-130 3.6 20.0
21.6 10810621.120.0µg/LStyrene 70-130 2.3 20.0
52.7 13213252.940.0µg/Ltert-Butyl Alcohol (TBA)40-140 0.3 20.0
44.1 11011144.540.0µg/Ltert-Butyl formate (TBF)40-140 0.9 20.0
Page 5 of 27* QC Fail Date:07/20/2023 11:26 AM
Page 108 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35229QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35227
LCS-V35227 LCSD-V35227Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
24.1 12112424.820.0µg/Ltert-Amyl Alcohol (TAA)40-140 2.8 20.0
43.4 10910742.840.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.3 20.0
20.7 10410721.320.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.8 20.0
19.5 97.510020.020.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.5 20.0
21.0 10510821.520.0µg/LTetrachloroethene 70-130 2.3 20.0
22.4 11211422.820.0µg/LToluene 70-130 1.7 20.0
21.5 10810921.820.0µg/L1,2,3-Trichlorobenzene 70-130 1.3 20.0
19.5 97.510220.420.0µg/L1,2,4-Trichlorobenzene 70-130 4.5 20.0
22.6 11311522.920.0µg/L1,1,1-Trichloroethane 70-130 1.3 20.0
22.6 11311523.020.0µg/L1,1,2-Trichloroethane 70-130 1.7 20.0
21.8 10911122.220.0µg/LTrichloroethene 70-130 1.8 20.0
21.5 10810921.820.0µg/LTrichlorofluoromethane 60-140 1.3 20.0
20.5 10310420.820.0µg/L1,2,3-Trichloropropane 70-130 1.4 20.0
20.9 10510821.620.0µg/L1,2,4-Trimethylbenzene 70-130 3.2 20.0
21.2 10610921.820.0µg/L1,3,5-Trimethylbenzene 70-130 2.7 20.0
23.3 11711823.620.0µg/LVinyl Acetate 60-140 1.2 20.0
20.2 10110420.820.0µg/LVinyl Chloride 60-140 2.9 20.0
21.7 10911122.120.0µg/Lo-Xylene 70-130 1.8 20.0
45.8 11511646.540.0µg/Lm,p-Xylene 70-130 1.5 20.0
22.2 11110921.820.0µg/L3,3-Dimethyl-1-butanol 70-130 1.8 20.0
1011024-Bromofluorobenzene (S)70-130
96.095.4Dibromofluoromethane (S)70-130
1021021,2-Dichloroethane - d4 (S)70-130
92.893.2Toluene-d8 (S)70-130
Page 6 of 27Date:07/20/2023 11:26 AM
Page 109 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35244QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35241
Associated Lab Samples: 99734, 99735, 99736, 99737, 99738, 99739, 99741, 99742, 99743
LRB-V35241 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/11/23 14:1610.01.80<1.80µg/LAcetone
07/11/23 14:160.5000.180<0.180µg/LBenzene
07/11/23 14:160.5000.210<0.210µg/LBromobenzene
07/11/23 14:161.000.420<0.420µg/LBromochloromethane
07/11/23 14:160.5000.160<0.160µg/LBromodichloromethane
07/11/23 14:165.001.50<1.50µg/LBromoform
07/11/23 14:161.000.280<0.280µg/LBromomethane
07/11/23 14:160.5000.180<0.180µg/Ln-Butylbenzene
07/11/23 14:160.5000.200<0.200µg/Lsec-Butyl benzene
07/11/23 14:162.000.920<0.920µg/Ltert-Butyl benzene
07/11/23 14:160.5000.180<0.180µg/LCarbon Tetrachloride
07/11/23 14:160.5000.190<0.190µg/LChlorobenzene
07/11/23 14:160.5000.190<0.190µg/LChlorodibromomethane
07/11/23 14:161.000.430<0.430µg/LChloroethane
07/11/23 14:160.5000.220<0.220µg/LChloroform
07/11/23 14:160.5000.220<0.220µg/LChloromethane
07/11/23 14:160.5000.200<0.200µg/L2-Chlorotoluene
07/11/23 14:160.5000.200<0.200µg/L4-Chlorotoluene
07/11/23 14:160.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/11/23 14:162.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/11/23 14:160.5000.200<0.200µg/L1,2-Dibromoethane
07/11/23 14:160.5000.230<0.230µg/LDibromomethane
07/11/23 14:160.5000.220<0.220µg/L1,2-Dichlorobenzene
07/11/23 14:160.5000.190<0.190µg/L1,3-Dichlorobenzene
07/11/23 14:160.5000.210<0.210µg/L1,4-Dichlorobenzene
07/11/23 14:165.001.20<1.20µg/LDichlorodifluoromethane
07/11/23 14:160.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 27Date:07/20/2023 11:26 AM
Page 110 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35244QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35241
Associated Lab Samples: 99734, 99735, 99736, 99737, 99738, 99739, 99741, 99742, 99743
LRB-V35241 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/11/23 14:160.5000.150<0.150µg/L1,2-Dichloroethane
07/11/23 14:160.5000.150<0.150µg/L1,1-Dichloroethene
07/11/23 14:160.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/11/23 14:160.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/11/23 14:160.5000.190<0.190µg/L1,2-Dichloropropane
07/11/23 14:160.5000.130<0.130µg/L1,3-Dichloropropane
07/11/23 14:162.000.210<0.210µg/L2,2-Dichloropropane
07/11/23 14:160.5000.200<0.200µg/L1,1-Dichloropropene
07/11/23 14:160.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/11/23 14:160.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/11/23 14:1620042.0<42.0µg/LEthanol
07/11/23 14:160.5000.170<0.170µg/LEthylbenzene
07/11/23 14:163.000.350<0.350µg/LHexachlorobutadiene
07/11/23 14:161.000.380<0.380µg/L2-Hexanone
07/11/23 14:160.5000.180<0.180µg/LIsopropylbenzene
07/11/23 14:160.5000.089<0.089µg/L4-Isopropyl toluene
07/11/23 14:165.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/11/23 14:161.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/11/23 14:161.000.078<0.078µg/L4-Methyl-2-Pentanone
07/11/23 14:162.000.330<0.330µg/LMethylene Chloride
07/11/23 14:161.000.470<0.470µg/LNaphthalene
07/11/23 14:160.5000.190<0.190µg/Ln-Propylbenzene
07/11/23 14:160.5000.220<0.220µg/LStyrene
07/11/23 14:1610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
07/11/23 14:1610.00.350<0.350µg/Ltert-Butyl formate (TBF)
07/11/23 14:1610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
07/11/23 14:1610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 8 of 27Date:07/20/2023 11:26 AM
Page 111 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35244QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35241
Associated Lab Samples: 99734, 99735, 99736, 99737, 99738, 99739, 99741, 99742, 99743
LRB-V35241 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/11/23 14:160.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
07/11/23 14:160.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/11/23 14:160.5000.220<0.220µg/LTetrachloroethene
07/11/23 14:160.5000.220<0.220µg/LToluene
07/11/23 14:160.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/11/23 14:160.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/11/23 14:160.5000.160<0.160µg/L1,1,1-Trichloroethane
07/11/23 14:160.5000.096<0.096µg/L1,1,2-Trichloroethane
07/11/23 14:160.5000.180<0.180µg/LTrichloroethene
07/11/23 14:160.5000.180<0.180µg/LTrichlorofluoromethane
07/11/23 14:160.5000.270<0.270µg/L1,2,3-Trichloropropane
07/11/23 14:160.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/11/23 14:160.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/11/23 14:165.001.00<1.00µg/LVinyl Acetate
07/11/23 14:160.5000.170<0.170µg/LVinyl Chloride
07/11/23 14:160.5000.210<0.210µg/Lo-Xylene
07/11/23 14:161.000.420<0.420µg/Lm,p-Xylene
07/11/23 14:1610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
07/11/23 14:164-Bromofluorobenzene (S)93.2 70-130
07/11/23 14:16Dibromofluoromethane (S)96.0 70-130
07/11/23 14:161,2-Dichloroethane - d4 (S)91.8 70-130
07/11/23 14:16Toluene-d8 (S)92.0 70-130
Page 9 of 27Date:07/20/2023 11:26 AM
Page 112 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35244QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35241
LCS-V35241 LCSD-V35241Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
33.1 82.783.733.540.0µg/LAcetone 40-160 1.2 20.0
19.6 98.099.019.820.0µg/LBenzene 70-130 1.0 20.0
18.0 90.088.517.720.0µg/LBromobenzene 70-130 1.6 20.0
20.3 10210821.620.0µg/LBromochloromethane 70-130 6.2 20.0
19.2 96.095.519.120.0µg/LBromodichloromethane 70-130 0.5 20.0
19.1 95.593.018.620.0µg/LBromoform 70-130 2.6 20.0
17.2 86.087.517.520.0µg/LBromomethane 60-140 1.7 20.0
17.9 89.592.518.520.0µg/Ln-Butylbenzene 70-130 3.2 20.0
17.4 87.090.518.120.0µg/Lsec-Butyl benzene 70-130 3.9 20.0
18.2 91.092.518.520.0µg/Ltert-Butyl benzene 70-130 1.6 20.0
19.1 95.597.019.420.0µg/LCarbon Tetrachloride 70-130 1.5 20.0
19.6 98.099.519.920.0µg/LChlorobenzene 70-130 1.5 20.0
18.0 90.093.518.720.0µg/LChlorodibromomethane 70-130 3.8 20.0
20.6 10310721.420.0µg/LChloroethane 60-140 3.8 20.0
19.6 98.010120.120.0µg/LChloroform 70-130 2.5 20.0
16.0 80.082.516.520.0µg/LChloromethane 60-140 3.0 20.0
17.5 87.589.017.820.0µg/L2-Chlorotoluene 70-130 1.6 20.0
17.1 85.587.517.520.0µg/L4-Chlorotoluene 70-130 2.3 20.0
17.4 87.089.517.920.0µg/LDi-Isopropyl Ether (DIPE)70-130 2.8 20.0
18.8 94.092.018.420.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.1 20.0
19.0 95.096.519.320.0µg/L1,2-Dibromoethane 70-130 1.5 20.0
19.0 95.010220.320.0µg/LDibromomethane 70-130 6.6 20.0
19.0 95.096.019.220.0µg/L1,2-Dichlorobenzene 70-130 1.0 20.0
18.7 93.594.018.820.0µg/L1,3-Dichlorobenzene 70-130 0.5 20.0
18.7 93.594.018.820.0µg/L1,4-Dichlorobenzene 70-130 0.5 20.0
18.7 93.596.019.220.0µg/LDichlorodifluoromethane 60-140 2.6 20.0
Page 10 of 27Date:07/20/2023 11:26 AM
Page 113 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35244QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35241
LCS-V35241 LCSD-V35241Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.9 94.595.519.120.0µg/L1,1-Dichloroethane 70-130 1.0 20.0
18.6 93.098.519.720.0µg/L1,2-Dichloroethane 70-130 5.7 20.0
18.9 94.597.519.520.0µg/L1,1-Dichloroethene 70-130 3.1 20.0
18.7 93.594.018.820.0µg/Lcis-1,2-Dichloroethene 70-130 0.5 20.0
19.0 95.097.019.420.0µg/Ltrans-1,2-Dichloroethene 70-130 2.0 20.0
19.1 95.595.519.120.0µg/L1,2-Dichloropropane 70-130 0.0 20.0
17.8 89.092.018.420.0µg/L1,3-Dichloropropane 70-130 3.3 20.0
19.4 97.099.519.920.0µg/L2,2-Dichloropropane 70-130 2.5 20.0
20.8 10410521.020.0µg/L1,1-Dichloropropene 70-130 0.9 20.0
18.9 94.595.519.120.0µg/Lcis-1,3-Dichloropropene 70-130 1.0 20.0
18.3 91.594.518.920.0µg/Ltrans-1,3-Dichloropropene 70-130 3.2 20.0
446 89.280.0400500µg/LEthanol 60-140 10.8 20.0
17.9 89.591.018.220.0µg/LEthylbenzene 70-130 1.6 20.0
19.1 95.510120.220.0µg/LHexachlorobutadiene 70-130 5.5 20.0
15.2 76.074.014.820.0µg/L2-Hexanone 60-140 2.6 20.0
18.1 90.591.518.320.0µg/LIsopropylbenzene 70-130 1.0 20.0
18.7 93.595.019.020.0µg/L4-Isopropyl toluene 70-130 1.5 20.0
16.5 82.577.015.420.0µg/LMethyl Ethyl Ketone (MEK)60-140 6.8 20.0
19.3 96.599.019.820.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.5 20.0
16.0 80.078.015.620.0µg/L4-Methyl-2-Pentanone 60-140 2.5 20.0
18.9 94.594.518.920.0µg/LMethylene Chloride 70-130 0.0 20.0
14.5 72.573.514.720.0µg/LNaphthalene 70-130 1.3 20.0
17.6 88.088.517.720.0µg/Ln-Propylbenzene 70-130 0.5 20.0
19.1 95.599.019.820.0µg/LStyrene 70-130 3.5 20.0
29.7 74.273.729.540.0µg/Ltert-Butyl Alcohol (TBA)40-140 0.6 20.0
42.7 10711244.740.0µg/Ltert-Butyl formate (TBF)40-140 4.5 20.0
Page 11 of 27Date:07/20/2023 11:26 AM
Page 114 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35244QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35241
LCS-V35241 LCSD-V35241Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.9 10589.517.920.0µg/Ltert-Amyl Alcohol (TAA)40-140 15.4 20.0
38.1 95.296.238.540.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.0 20.0
18.7 93.599.019.820.0µg/L1,1,1,2-Tetrachloroethane 70-130 5.7 20.0
17.7 88.588.517.720.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.0 20.0
20.1 10110220.320.0µg/LTetrachloroethene 70-130 0.9 20.0
19.0 95.096.519.320.0µg/LToluene 70-130 1.5 20.0
19.5 97.599.019.820.0µg/L1,2,3-Trichlorobenzene 70-130 1.5 20.0
19.7 98.510220.320.0µg/L1,2,4-Trichlorobenzene 70-130 3.0 20.0
19.7 98.598.519.720.0µg/L1,1,1-Trichloroethane 70-130 0.0 20.0
19.5 97.599.019.820.0µg/L1,1,2-Trichloroethane 70-130 1.5 20.0
20.9 10510621.120.0µg/LTrichloroethene 70-130 0.9 20.0
20.6 10310520.920.0µg/LTrichlorofluoromethane 60-140 1.4 20.0
18.4 92.090.018.020.0µg/L1,2,3-Trichloropropane 70-130 2.1 20.0
18.1 90.593.018.620.0µg/L1,2,4-Trimethylbenzene 70-130 2.7 20.0
18.3 91.592.518.520.0µg/L1,3,5-Trimethylbenzene 70-130 1.0 20.0
22.5 11311422.820.0µg/LVinyl Acetate 60-140 1.3 20.0
19.0 95.097.519.520.0µg/LVinyl Chloride 60-140 2.5 20.0
18.5 92.593.518.720.0µg/Lo-Xylene 70-130 1.0 20.0
39.1 97.799.039.640.0µg/Lm,p-Xylene 70-130 1.2 20.0
22.9 11582.016.420.0µg/L3,3-Dimethyl-1-butanol 70-130 33.0*20.0
92.891.64-Bromofluorobenzene (S)70-130
95.695.6Dibromofluoromethane (S)70-130
93.294.01,2-Dichloroethane - d4 (S)70-130
92.091.8Toluene-d8 (S)70-130
Page 12 of 27* QC Fail Date:07/20/2023 11:26 AM
Page 115 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35303QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35302
Associated Lab Samples: 99738
LRB-V35302 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/23 15:350.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/12/23 15:3510.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
07/12/23 15:354-Bromofluorobenzene (S)102 70-130
07/12/23 15:35Dibromofluoromethane (S)94.8 70-130
07/12/23 15:351,2-Dichloroethane - d4 (S)98.0 70-130
07/12/23 15:35Toluene-d8 (S)91.6 70-130
LCS-V35302 LCSD-V35302Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
23.4 11711923.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.6 20.0
55.0 13813654.540.0µg/Ltert-Butyl Alcohol (TBA)40-140 0.9 20.0
1031034-Bromofluorobenzene (S)70-130
95.095.6Dibromofluoromethane (S)70-130
1011031,2-Dichloroethane - d4 (S)70-130
92.491.6Toluene-d8 (S)70-130
Page 13 of 27Date:07/20/2023 11:26 AM
Page 116 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35347
Associated Lab Samples: 99740
LRB-V35347 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/13/23 21:5610.01.80<1.80µg/LAcetone
07/13/23 21:560.5000.180<0.180µg/LBenzene
07/13/23 21:560.5000.210<0.210µg/LBromobenzene
07/13/23 21:561.000.420<0.420µg/LBromochloromethane
07/13/23 21:560.5000.160<0.160µg/LBromodichloromethane
07/13/23 21:565.001.50<1.50µg/LBromoform
07/13/23 21:561.000.280<0.280µg/LBromomethane
07/13/23 21:560.5000.180<0.180µg/Ln-Butylbenzene
07/13/23 21:560.5000.200<0.200µg/Lsec-Butyl benzene
07/13/23 21:562.000.920<0.920µg/Ltert-Butyl benzene
07/13/23 21:560.5000.180<0.180µg/LCarbon Tetrachloride
07/13/23 21:560.5000.190<0.190µg/LChlorobenzene
07/13/23 21:560.5000.190<0.190µg/LChlorodibromomethane
07/13/23 21:561.000.430<0.430µg/LChloroethane
07/13/23 21:560.5000.220<0.220µg/LChloroform
07/13/23 21:560.5000.220<0.220µg/LChloromethane
07/13/23 21:560.5000.200<0.200µg/L2-Chlorotoluene
07/13/23 21:560.5000.200<0.200µg/L4-Chlorotoluene
07/13/23 21:560.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/13/23 21:562.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/13/23 21:560.5000.200<0.200µg/L1,2-Dibromoethane
07/13/23 21:560.5000.230<0.230µg/LDibromomethane
07/13/23 21:560.5000.220<0.220µg/L1,2-Dichlorobenzene
07/13/23 21:560.5000.190<0.190µg/L1,3-Dichlorobenzene
07/13/23 21:560.5000.210<0.210µg/L1,4-Dichlorobenzene
07/13/23 21:565.001.20<1.20µg/LDichlorodifluoromethane
07/13/23 21:560.5000.240<0.240µg/L1,1-Dichloroethane
Page 14 of 27Date:07/20/2023 11:26 AM
Page 117 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35347
Associated Lab Samples: 99740
LRB-V35347 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/13/23 21:560.5000.150<0.150µg/L1,2-Dichloroethane
07/13/23 21:560.5000.150<0.150µg/L1,1-Dichloroethene
07/13/23 21:560.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/13/23 21:560.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/13/23 21:560.5000.190<0.190µg/L1,2-Dichloropropane
07/13/23 21:560.5000.130<0.130µg/L1,3-Dichloropropane
07/13/23 21:562.000.210<0.210µg/L2,2-Dichloropropane
07/13/23 21:560.5000.200<0.200µg/L1,1-Dichloropropene
07/13/23 21:560.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/13/23 21:560.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/13/23 21:5620042.0<42.0µg/LEthanol
07/13/23 21:560.5000.170<0.170µg/LEthylbenzene
07/13/23 21:563.000.350<0.350µg/LHexachlorobutadiene
07/13/23 21:561.000.380<0.380µg/L2-Hexanone
07/13/23 21:560.5000.180<0.180µg/LIsopropylbenzene
07/13/23 21:560.5000.089<0.089µg/L4-Isopropyl toluene
07/13/23 21:565.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/13/23 21:561.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/13/23 21:561.000.078<0.078µg/L4-Methyl-2-Pentanone
07/13/23 21:562.000.330<0.330µg/LMethylene Chloride
07/13/23 21:561.000.470<0.470µg/LNaphthalene
07/13/23 21:560.5000.190<0.190µg/Ln-Propylbenzene
07/13/23 21:560.5000.220<0.220µg/LStyrene
07/13/23 21:5610.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
07/13/23 21:5610.00.350<0.350µg/Ltert-Butyl formate (TBF)
07/13/23 21:5610.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
07/13/23 21:5610.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 15 of 27Date:07/20/2023 11:26 AM
Page 118 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35347
Associated Lab Samples: 99740
LRB-V35347 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/13/23 21:560.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
07/13/23 21:560.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/13/23 21:560.5000.220<0.220µg/LTetrachloroethene
07/13/23 21:560.5000.220<0.220µg/LToluene
07/13/23 21:560.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/13/23 21:560.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/13/23 21:560.5000.160<0.160µg/L1,1,1-Trichloroethane
07/13/23 21:560.5000.096<0.096µg/L1,1,2-Trichloroethane
07/13/23 21:560.5000.180<0.180µg/LTrichloroethene
07/13/23 21:560.5000.180<0.180µg/LTrichlorofluoromethane
07/13/23 21:560.5000.270<0.270µg/L1,2,3-Trichloropropane
07/13/23 21:560.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/13/23 21:560.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/13/23 21:565.001.00<1.00µg/LVinyl Acetate
07/13/23 21:560.5000.170<0.170µg/LVinyl Chloride
07/13/23 21:560.5000.210<0.210µg/Lo-Xylene
07/13/23 21:561.000.420<0.420µg/Lm,p-Xylene
07/13/23 21:5610.01.00<1.00µg/L3,3-Dimethyl-1-butanol
07/13/23 21:564-Bromofluorobenzene (S)99.6 70-130
07/13/23 21:56Dibromofluoromethane (S)101 70-130
07/13/23 21:561,2-Dichloroethane - d4 (S)99.0 70-130
07/13/23 21:56Toluene-d8 (S)99.2 70-130
Page 16 of 27Date:07/20/2023 11:26 AM
Page 119 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35347
LCS-V35347Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
166*66.340.0µg/Ltert-Butyl formate (TBF)40-140
LCS-V35347 LCSD-V35347Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.5 81.275.230.140.0µg/LAcetone 40-160 7.6 20.0
21.7 10910721.420.0µg/LBenzene 70-130 1.3 20.0
21.9 11011022.020.0µg/LBromobenzene 70-130 0.4 20.0
22.6 11311021.920.0µg/LBromochloromethane 70-130 3.1 20.0
21.4 10710420.720.0µg/LBromodichloromethane 70-130 3.3 20.0
22.4 11210821.520.0µg/LBromoform 70-130 4.1 20.0
26.8 13413426.820.0µg/LBromomethane 60-140 0.0 20.0
22.5 11311122.220.0µg/Ln-Butylbenzene 70-130 1.3 20.0
21.5 10810821.520.0µg/Lsec-Butyl benzene 70-130 0.0 20.0
21.6 10810621.120.0µg/Ltert-Butyl benzene 70-130 2.3 20.0
21.1 10610721.320.0µg/LCarbon Tetrachloride 70-130 0.9 20.0
22.1 11111122.220.0µg/LChlorobenzene 70-130 0.4 20.0
22.1 11111122.120.0µg/LChlorodibromomethane 70-130 0.0 20.0
22.5 11311322.620.0µg/LChloroethane 60-140 0.4 20.0
21.3 10710621.220.0µg/LChloroform 70-130 0.4 20.0
20.6 10311322.620.0µg/LChloromethane 60-140 9.2 20.0
21.6 10810921.720.0µg/L2-Chlorotoluene 70-130 0.4 20.0
21.7 10910921.820.0µg/L4-Chlorotoluene 70-130 0.4 20.0
21.1 10610520.920.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.9 20.0
22.0 11011222.320.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.3 20.0
21.7 10910721.420.0µg/L1,2-Dibromoethane 70-130 1.3 20.0
Page 17 of 27* QC Fail Date:07/20/2023 11:26 AM
Page 120 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35347
LCS-V35347 LCSD-V35347Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.4 10710621.120.0µg/LDibromomethane 70-130 1.4 20.0
22.2 11110921.820.0µg/L1,2-Dichlorobenzene 70-130 1.8 20.0
21.9 11010821.620.0µg/L1,3-Dichlorobenzene 70-130 1.3 20.0
21.2 10610520.920.0µg/L1,4-Dichlorobenzene 70-130 1.4 20.0
22.5 11311623.220.0µg/LDichlorodifluoromethane 60-140 3.0 20.0
22.1 11110821.620.0µg/L1,1-Dichloroethane 70-130 2.2 20.0
20.2 10110120.120.0µg/L1,2-Dichloroethane 70-130 0.4 20.0
21.7 10910621.120.0µg/L1,1-Dichloroethene 70-130 2.8 20.0
21.8 10910821.620.0µg/Lcis-1,2-Dichloroethene 70-130 0.9 20.0
21.8 10910721.420.0µg/Ltrans-1,2-Dichloroethene 70-130 1.8 20.0
21.8 10911021.920.0µg/L1,2-Dichloropropane 70-130 0.4 20.0
21.0 10510921.820.0µg/L1,3-Dichloropropane 70-130 3.7 20.0
21.9 11011222.420.0µg/L2,2-Dichloropropane 70-130 2.2 20.0
22.8 11411322.620.0µg/L1,1-Dichloropropene 70-130 0.8 20.0
22.4 11211022.020.0µg/Lcis-1,3-Dichloropropene 70-130 1.8 20.0
22.5 11310821.520.0µg/Ltrans-1,3-Dichloropropene 70-130 4.5 20.0
556 11186.4432500µg/LEthanol 60-140 25.1*20.0
20.7 10410621.120.0µg/LEthylbenzene 70-130 1.9 20.0
21.0 10511022.020.0µg/LHexachlorobutadiene 70-130 4.6 20.0
19.4 97.094.518.920.0µg/L2-Hexanone 60-140 2.6 20.0
22.1 11111122.220.0µg/LIsopropylbenzene 70-130 0.4 20.0
22.6 11311322.620.0µg/L4-Isopropyl toluene 70-130 0.0 20.0
16.9 84.581.516.320.0µg/LMethyl Ethyl Ketone (MEK)60-140 3.6 20.0
22.1 11110921.720.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.8 20.0
20.7 10497.019.420.0µg/L4-Methyl-2-Pentanone 60-140 6.4 20.0
22.5 11311122.120.0µg/LMethylene Chloride 70-130 1.7 20.0
Page 18 of 27* QC Fail Date:07/20/2023 11:26 AM
Page 121 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35347
LCS-V35347 LCSD-V35347Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.6 93.092.018.420.0µg/LNaphthalene 70-130 1.0 20.0
21.4 10710721.320.0µg/Ln-Propylbenzene 70-130 0.4 20.0
22.1 11111022.020.0µg/LStyrene 70-130 0.4 20.0
34.8 87.083.733.540.0µg/Ltert-Butyl Alcohol (TBA)40-140 3.8 20.0
22.6 11311022.020.0µg/Ltert-Amyl Alcohol (TAA)40-140 2.6 20.0
43.6 10910843.140.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.1 20.0
22.2 11110921.820.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.8 20.0
22.5 11311122.120.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.7 20.0
21.6 10811122.120.0µg/LTetrachloroethene 70-130 2.2 20.0
21.6 10810621.120.0µg/LToluene 70-130 2.3 20.0
21.1 10610521.020.0µg/L1,2,3-Trichlorobenzene 70-130 0.4 20.0
23.6 11811823.620.0µg/L1,2,4-Trichlorobenzene 70-130 0.0 20.0
21.7 10910821.620.0µg/L1,1,1-Trichloroethane 70-130 0.4 20.0
22.2 11110921.820.0µg/L1,1,2-Trichloroethane 70-130 1.8 20.0
22.0 11010621.220.0µg/LTrichloroethene 70-130 3.7 20.0
22.1 11111222.320.0µg/LTrichlorofluoromethane 60-140 0.9 20.0
20.7 10410420.820.0µg/L1,2,3-Trichloropropane 70-130 0.4 20.0
21.5 10810821.520.0µg/L1,2,4-Trimethylbenzene 70-130 0.0 20.0
21.8 10910921.720.0µg/L1,3,5-Trimethylbenzene 70-130 0.4 20.0
24.1 12112825.620.0µg/LVinyl Acetate 60-140 6.0 20.0
23.0 11511723.320.0µg/LVinyl Chloride 60-140 1.2 20.0
21.7 10910821.620.0µg/Lo-Xylene 70-130 0.4 20.0
44.6 11211144.340.0µg/Lm,p-Xylene 70-130 0.6 20.0
20.1 10199.519.920.0µg/L3,3-Dimethyl-1-butanol 70-130 1.0 20.0
99.898.64-Bromofluorobenzene (S)70-130
10299.6Dibromofluoromethane (S)70-130
Page 19 of 27Date:07/20/2023 11:26 AM
Page 122 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35347
LCS-V35347 LCSD-V35347Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
10299.81,2-Dichloroethane - d4 (S)70-130
100100Toluene-d8 (S)70-130
Page 20 of 27Date:07/20/2023 11:26 AM
Page 123 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35409QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35406
Associated Lab Samples: 99738
LRB-V35406 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/14/23 14:3010.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
07/14/23 14:304-Bromofluorobenzene (S)101 70-130
07/14/23 14:30Dibromofluoromethane (S)102 70-130
07/14/23 14:301,2-Dichloroethane - d4 (S)97.8 70-130
07/14/23 14:30Toluene-d8 (S)98.8 70-130
LCS-V35406 LCSD-V35406Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
16.4 82.088.517.720.0µg/Ltert-Amyl Alcohol (TAA)40-140 7.6 20.0
97.899.44-Bromofluorobenzene (S)70-130
100102Dibromofluoromethane (S)70-130
99.299.81,2-Dichloroethane - d4 (S)70-130
99.699.2Toluene-d8 (S)70-130
Page 21 of 27Date:07/20/2023 11:26 AM
Page 124 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V34997QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V34962
Associated Lab Samples: 99735, 99736, 99737, 99738, 99739, 99740, 99741, 99742, 99743, 99744, 99745
LRB-V34962 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/05/23 18:062.000.302<0.302µg/LAcenaphthene
07/05/23 18:062.000.297<0.297µg/LAcenaphthylene
07/05/23 18:062.000.836<0.836µg/LAnthracene
07/05/23 18:0610.01.32<1.32µg/LBenzidine
07/05/23 18:062.000.637<0.637µg/LBenzo(a)anthracene
07/05/23 18:062.001.02<1.02µg/LBenzo(a)pyrene
07/05/23 18:065.002.49<2.49µg/LBenzo(b)fluoranthene
07/05/23 18:065.001.01<1.01µg/LBenzo(g,h,i)perylene
07/05/23 18:065.001.99<1.99µg/LBenzo(k)fluoranthene
07/05/23 18:0610.01.10<1.10µg/LBenzoic Acid
07/05/23 18:065.000.684<0.684µg/LBenzyl alcohol
07/05/23 18:065.000.468<0.468µg/LBis(2-Chloroethoxy)methane
07/05/23 18:065.001.04<1.04µg/LBis(2-Chloroethyl)ether
07/05/23 18:065.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
07/05/23 18:0610.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
07/05/23 18:065.001.11<1.11µg/L4-Bromophenyl phenyl ether
07/05/23 18:065.001.83<1.83µg/LButyl benzyl phthalate
07/05/23 18:065.001.18<1.18µg/L4-Chloro-3-methylphenol
07/05/23 18:0620.07.38<7.38µg/L2-Chloronaphthalene
07/05/23 18:0610.00.938<0.938µg/L2-Chlorophenol
07/05/23 18:065.001.71<1.71µg/L4-Chlorophenyl phenyl ether
07/05/23 18:062.000.405<0.405µg/LChrysene
07/05/23 18:062.000.434<0.434µg/LDibenz(a,h)anthracene
07/05/23 18:065.000.856<0.856µg/LDibenzofuran
07/05/23 18:065.002.00<2.00µg/L1,2-Dichlorobenzene
07/05/23 18:065.002.00<2.00µg/L1,3-Dichlorobenzene
07/05/23 18:065.002.05<2.05µg/L1,4-Dichlorobenzene
Page 22 of 27Date:07/20/2023 11:26 AM
Page 125 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V34997QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V34962
Associated Lab Samples: 99735, 99736, 99737, 99738, 99739, 99740, 99741, 99742, 99743, 99744, 99745
LRB-V34962 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/05/23 18:065.001.89<1.89µg/L3,3'-Dichlorobenzidine
07/05/23 18:0610.01.46<1.46µg/L2,4-Dichlorophenol
07/05/23 18:065.000.745<0.745µg/LDiethyl phthalate
07/05/23 18:065.000.939<0.939µg/LDimethyl phthalate
07/05/23 18:0620.01.57<1.57µg/L2,4-Dimethylphenol
07/05/23 18:065.002.06<2.06µg/LDi-n-butyl phthalate
07/05/23 18:0610.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
07/05/23 18:0610.01.92<1.92µg/L2,4-Dinitrophenol
07/05/23 18:065.001.11<1.11µg/L2,4-Dinitrotoluene
07/05/23 18:065.000.809<0.809µg/L2,6-Dinitrotoluene
07/05/23 18:065.001.65<1.65µg/LDi-n-Octyl Phthalate
07/05/23 18:062.000.250<0.250µg/LFluoranthene
07/05/23 18:062.000.807<0.807µg/LFluorene
07/05/23 18:065.000.979<0.979µg/LHexachlorobenzene
07/05/23 18:065.002.73<2.73µg/LHexachlorobutadiene
07/05/23 18:065.002.05<2.05µg/LHexachlorocyclopentadiene
07/05/23 18:065.001.76<1.76µg/LHexachloroethane
07/05/23 18:062.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
07/05/23 18:065.000.444<0.444µg/LIsophorone
07/05/23 18:062.001.14<1.14µg/L1-Methylnaphthalene
07/05/23 18:062.000.666<0.666µg/L2-Methylnaphthalene
07/05/23 18:062.000.728<0.728µg/LNaphthalene
07/05/23 18:065.000.905<0.905µg/LNitrobenzene
07/05/23 18:065.000.493<0.493µg/L2-Nitrophenol
07/05/23 18:0610.01.23<1.23µg/L4-Nitrophenol
07/05/23 18:065.001.10<1.10µg/LN-Nitrosodiphenylamine
07/05/23 18:065.000.641<0.641µg/LN-Nitroso-di-n-propylamine
Page 23 of 27Date:07/20/2023 11:26 AM
Page 126 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V34997QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V34962
Associated Lab Samples: 99735, 99736, 99737, 99738, 99739, 99740, 99741, 99742, 99743, 99744, 99745
LRB-V34962 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/05/23 18:065.001.43<1.43µg/LPentachlorophenol
07/05/23 18:062.000.428<0.428µg/LPhenanthrene
07/05/23 18:065.000.651<0.651µg/LPhenol
07/05/23 18:062.000.434<0.434µg/LPyrene
07/05/23 18:065.002.21<2.21µg/L1,2,4-Trichlorobenzene
07/05/23 18:065.001.32<1.32µg/L2,4,6-Trichlorophenol
07/05/23 18:062-Fluorobiphenyl (S)79.8 49-118
07/05/23 18:062-Fluorophenol (S)45.5 22-84
07/05/23 18:06Nitrobenzene-d5 (S)73.8 43-123
07/05/23 18:064-Terphenyl-d14 (S)88.2 49-151
07/05/23 18:062,4,6-Tribromophenol (S)73.7 31-144
07/05/23 18:06Phenol-d5 (S)26.7 10-63
LCS-V34962 LCSD-V34962Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.6 73.272.636.350.0µg/LAcenaphthene 47-145 0.8 20.0
36.9 73.874.037.050.0µg/LAcenaphthylene 33-145 0.2 20.0
40.9 81.882.041.050.0µg/LAnthracene 27-133 0.2 20.0
7.43 14.8*14.1*7.0850.0µg/LBenzidine 15-150 4.8 20.0
39.7 79.480.640.350.0µg/LBenzo(a)anthracene 33-143 1.5 20.0
43.3 86.685.642.850.0µg/LBenzo(a)pyrene 17-163 1.1 20.0
39.1 78.282.041.050.0µg/LBenzo(b)fluoranthene 24-159 4.7 20.0
39.4 78.879.439.750.0µg/LBenzo(g,h,i)perylene 10-219 0.7 20.0
37.9 75.881.040.550.0µg/LBenzo(k)fluoranthene 11-162 6.6 20.0
17.4 34.829.814.950.0µg/LBenzoic Acid 10-125 15.4 20.0
Page 24 of 27* QC Fail Date:07/20/2023 11:26 AM
Page 127 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V34997QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V34962
LCS-V34962 LCSD-V34962Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
35.4 70.867.833.950.0µg/LBenzyl alcohol 16-107 4.3 20.0
39.1 78.276.438.250.0µg/LBis(2-Chloroethoxy)methane 33-184 2.3 20.0
33.2 66.467.033.550.0µg/LBis(2-Chloroethyl)ether 12-158 0.8 20.0
36.2 72.470.435.250.0µg/LBis(2-Chloroisopropyl)ether 36-166 2.8 20.0
43.5 87.086.443.250.0µg/LBis(2-ethylhexyl)phthalate 10-158 0.6 20.0
39.6 79.280.240.150.0µg/L4-Bromophenyl phenyl ether 53-127 1.2 20.0
44.6 89.284.242.150.0µg/LButyl benzyl phthalate 10-152 5.7 20.0
38.5 77.076.438.250.0µg/L4-Chloro-3-methylphenol 22-147 0.7 20.0
36.6 73.273.236.650.0µg/L2-Chloronaphthalene 60-118 0.0 20.0
33.0 66.066.433.250.0µg/L2-Chlorophenol 23-134 0.6 20.0
38.2 76.478.839.450.0µg/L4-Chlorophenyl phenyl ether 25-158 3.0 20.0
39.2 78.479.839.950.0µg/LChrysene 17-168 1.7 20.0
33.8 67.666.633.350.0µg/LDibenz(a,h)anthracene 10-227 1.4 20.0
36.5 73.074.837.450.0µg/LDibenzofuran 39-114 2.4 20.0
30.7 61.461.430.750.0µg/L1,2-Dichlorobenzene 32-129 0.0 20.0
29.5 59.058.229.150.0µg/L1,3-Dichlorobenzene 20-124 1.3 20.0
29.4 58.858.829.450.0µg/L1,4-Dichlorobenzene 20-124 0.0 20.0
35.4 70.880.040.050.0µg/L3,3'-Dichlorobenzidine 10-262 12.2 20.0
37.5 75.076.038.050.0µg/L2,4-Dichlorophenol 39-135 1.3 20.0
38.9 77.879.639.850.0µg/LDiethyl phthalate 10-114 2.2 20.0
39.2 78.479.839.950.0µg/LDimethyl phthalate 10-112 1.7 20.0
48.9 97.899.449.750.0µg/L2,4-Dimethylphenol 32-119 1.6 20.0
43.6 87.286.243.150.0µg/LDi-n-butyl phthalate 10-118 1.1 20.0
40.0 80.083.241.650.0µg/L4,6-Dinitro-2-methylphenol 10-181 3.9 20.0
40.2 80.475.437.750.0µg/L2,4-Dinitrophenol 10-191 6.4 20.0
40.1 80.281.240.650.0µg/L2,4-Dinitrotoluene 39-139 1.2 20.0
Page 25 of 27Date:07/20/2023 11:26 AM
Page 128 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V34997QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V34962
LCS-V34962 LCSD-V34962Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.0 78.077.638.850.0µg/L2,6-Dinitrotoluene 50-158 0.5 20.0
42.0 84.085.242.650.0µg/LDi-n-Octyl Phthalate 10-146 1.4 20.0
37.6 75.274.637.350.0µg/LFluoranthene 26-137 0.8 20.0
38.4 76.877.238.650.0µg/LFluorene 59-121 0.5 20.0
38.5 77.080.640.350.0µg/LHexachlorobenzene 10-152 4.5 20.0
31.5 63.061.630.850.0µg/LHexachlorobutadiene 24-116 2.2 20.0
27.2 54.452.826.450.0µg/LHexachlorocyclopentadiene 32-117 2.9 20.0
29.2 58.458.829.450.0µg/LHexachloroethane 40-113 0.6 20.0
39.8 79.679.039.550.0µg/LIndeno(1,2,3-cd)pyrene 10-171 0.7 20.0
35.0 70.066.233.150.0µg/LIsophorone 21-196 5.5 20.0
34.0 68.067.433.750.0µg/L1-Methylnaphthalene 40-135 0.8 20.0
33.8 67.667.433.750.0µg/L2-Methylnaphthalene 18-121 0.2 20.0
32.8 65.664.432.250.0µg/LNaphthalene 21-133 1.8 20.0
33.7 67.465.032.550.0µg/LNitrobenzene 35-180 3.6 20.0
35.9 71.871.035.550.0µg/L2-Nitrophenol 29-182 1.1 20.0
13.0 26.026.213.150.0µg/L4-Nitrophenol 10-132 0.7 20.0
48.3 96.693.846.950.0µg/LN-Nitrosodiphenylamine 69-152 2.9 20.0
37.0 74.072.436.250.0µg/LN-Nitroso-di-n-propylamine 10-230 2.1 20.0
43.0 86.088.044.050.0µg/LPentachlorophenol 14-176 2.2 20.0
39.2 78.477.638.850.0µg/LPhenanthrene 54-120 1.0 20.0
16.4 32.829.614.850.0µg/LPhenol 10-112 10.2 20.0
40.4 80.880.840.450.0µg/LPyrene 52-115 0.0 20.0
31.5 63.063.431.750.0µg/L1,2,4-Trichlorobenzene 44-142 0.6 20.0
36.8 73.676.038.050.0µg/L2,4,6-Trichlorophenol 37-144 3.2 20.0
73.475.82-Fluorobiphenyl (S)49-118
40.541.12-Fluorophenol (S)22-84
Page 26 of 27Date:07/20/2023 11:26 AM
Page 129 of 133
Quality Control Data
23-181-0037Report No:
Project Description:
Client ID:Geological Resources, Inc.
Mickey's 1, Station 19
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V34997QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V34962
LCS-V34962 LCSD-V34962Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
67.867.8Nitrobenzene-d5 (S)43-123
83.685.64-Terphenyl-d14 (S)49-151
66.671.22,4,6-Tribromophenol (S)31-144
24.925.1Phenol-d5 (S)10-63
Page 27 of 27Date:07/20/2023 11:26 AM
Page 130 of 133
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-181-0037
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:07/01/2023 09:48:10
Special precautions or instructions included?
Comments:
Page 131 of 133
Page 132 of 133
Page 133 of 133