MO-9217_40687_CA_MRP_20231031_Fast Phils 506

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

October 31, 2023

Ms. Trudy Beverly
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Ground Water Monitoring Report
August - September 2023
Fast Phil’s 506
1541 Salisbury Road
Concord, Iredell County
North Carolina
Facility ID Number: 00-0-0000024533
Incident Number: 40687
GRI Project Number: 4400

Dear Ms. Beverly,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please don’t hesitate to contact Eric Eubanks at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ms. Kimberly Robertson Raymer Real Estate Operations, Inc.; file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
August – September 2023
Fast Phil’s 506
1541 Salisbury Road
Statesville, Iredell County
North Carolina
Facility ID Number: 00-0-0000024533
Incident Number: 40687
GRI Project Number: 4400

Prepared for:

Ms. Kimberly Robertson
Raymer Real Estate Operations, Inc.
Post Office Box 271
Statesville, North Carolina, 28687

October 31, 2023

Eric M. Eubanks, P.G.
Project Manager

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
i
EXECUTIVE SUMMARY
Fast Phil’s 506 is located at 1541 Salisbury Road in Statesville, Iredell County, North Carolina. The site is
currently owned by Raymer Real Estate Operations, Inc. and is operated by Raymer Oil Company as a
petroleum retail facility. Two 10,000-gallon gasoline USTs, one 10,000-gallon diesel UST, and one 14,000-
gallon kerosene UST were removed from the site in June 1991. Currently, one 20,000-gallon gasoline UST,
two 8,000-gallon gasoline USTs, and one 1,000-gallon kerosene UST are active at the site. In December
2016, a Site Check was conducted, and a release was identified. The adjoining properties are commercial.
According to the information determined during receptor survey activities, no water supply wells were
identified within 1,000 feet of the site. Public water is available to the site and surrounding properties
within a 1,500-foot radius of the site.

Although a CAP has not been established for the site, AFVR and MMPE events have been conducted at
the site beginning in September 2018.

An MMPE event was conducted from August 14 to August 18, 2023, at the site on monitoring wells MW-
1, MW-4, and MW-5. A total of 9,766 gallons of affected ground water was recovered during the MMPE
event. No measurable free product was recovered during this MMPE event. At the conclusion of the event,
no free product was measured in any of the vacuumed wells or observation wells. The average fluid
recovery rate was 101.73 gallons per hour. Based on mass-removal calculations, an additional 1,257.62
pounds or 204.43 gallons of vapor phase hydrocarbons were removed at an average rate of 2.13 gallons
per hour.

As directed in NCDEQ correspondence dated February 8, 2022, on September 21, 2023, one Type II
monitoring well (MW-9) was installed across the street to a total depth of 30 feet BGS with a 15-foot
screened interval.

On September 21, 2023, twelve Type II monitoring wells (MW-1 through MW-9, PMW-2, PMW-7, and
PMW-8) and one Type III telescoping well (TW-1) were gauged, purged, and sampled. No free product
was measured in any monitoring well. The reported concentrations of benzene, toluene, ethylbenzene,
xylenes, MTBE, naphthalene, n-butylbenzene, sec-butylbenzene, EDB, 1,1-DCA, 1,2-DCA, 2-hexanone,
isopropylbenzene, IPE, p-isopropyltoluene, MIBK, n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-
trimethylbenzene, 1-methylnaphthalene, 2-methylnaphthalene, lead, C5-C8 aliphatics, C9-C12 aliphatics,
C9-C10 aromatics, and/or C11-C22 aromatics exceeded the MACs in the ground water samples collected
from MW-1, MW-3 through MW-9, PMW-2, PMW-7, PMW-8, and TW-1. The reported concentrations of
benzene and/or MTBE exceeded the GCLs in the ground water samples collected from MW-1, MW-4, MW-
9, and PMW-2. Based on this information, the onsite contaminant mass has decreased by 50.9% since
May 2017. Please note that MW-9 was installed upgradient from the site in the vicinity of Incident No.
20090. Due to the location of the well adjacent to/downgradient of a site previously containing free
product, it is unlikely the contamination reported in MW-9 is attributed to the Fast Phil’s 506 site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
ii
Based on this information, the risk classification for the site should remain intermediate risk. MMPE
events should continue until contaminant concentrations are below the GCLs. Semi-annual ground water
monitoring should continue at the site. However, based on the direction of ground water flow, the source
area of the contamination at the site should be reevaluated. The next sampling event is tentatively
scheduled for March 2024.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
iii
SITE INFORMATION
1. Site Identification
 Fast Phil’s 506 (Facility ID 00-0-0000024533)
 Incident Number 40687 – Intermediate Risk (I125D)
 Location of Source Area: 1541 Salisbury Road
Statesville, NC 28677
Iredell County
35.768617°N, 80.853228°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
Raymer Oil Company
P.O. Box 271
Statesville, NC 28687
[e-mail]
704-619-5659

UST/AST Operator
Raymer Oil Company
P.O. Box 271
Statesville, NC 28687
[e-mail]
704-619-5659

Property Owner
Raymer Real Estate Operations, Inc
P.O. Box 271
Statesville, NC 28687
[e-mail]
704-619-5659

Property Occupant
Fast Phil’s 506
1541 Salisbury Road, East
Statesville, NC 28677
[e-mail]
704-619-5659

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 28217
State Cert. Nos. 37735 and 402
[phone]
3. Information about Release
 Release was discovered on January 6, 2016.
 An unknown amount of product was released from the leaking UST System.
 Two 10,000-gallon gasoline USTs, one 10,000-gallon diesel UST, and one 14,000-gallon kerosene
UST were removed from the site in June 1991. One 20,000-gallon gasoline, two 8,000-gallon
gasoline and one 1,000-gallon kerosene USTs and associated pumps and product piping are active
at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
iv
ACRONYMS
ACM: Asbestos Containing Materials
AES: Advanced Environmental Services, Inc.
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ........................................................................................................................... iii
ACRONYMS ....................................................................................................................................... iv
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 MONITORING WELL INSTALLATION ..........................................................................................3
3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................3
4.0 FREE PRODUCT REMOVAL ........................................................................................................6
5.0 MMPE EVENT ..........................................................................................................................6
6.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................7
7.0 CONCLUSIONS .........................................................................................................................7
8.0 LIMITATIONS ...........................................................................................................................8
9.0 STATEMENTS AND CERTIFICATION ...........................................................................................8

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3a: Site Vicinity Map
Figure 3b: Zoning Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Benzene Isoconcentration Map
Figure 7: MTBE Isoconcentration Map
Figure 8: Cross Section A-A’
Figure 9: Cross Section B-B’
Figure 10: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Receptor Information
Table 4: Adjacent Property Owner Information
Table 5a: Well Construction and Gauging Information
Table 5b: Well Construction and Gauging Information (Pantry #3195)
Table 6: Summary of Ground Water Sample Analytical Results
Table 7: Summary of MMPE Sample Analytical Results
Table 8: Free Product Recovery Results
Table 9: Free Product Recovery Event Information
Table 10: Free Product Recovery Cost Summary

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
APPENDICES
Appendix A: State Correspondence
Appendix B: Land Use Information
Appendix C: Incident Reports
Appendix D: Well Permit, Well Construction Record, and Subsurface Log
Appendix E: Historical Soil Quality Information
Appendix F: Laboratory Analytical Reports
Appendix G: Contaminant Mass Calculations
Appendix H: MMPE Report and Disposal Manifests

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the August 2023 MMPE event and the September 2023 ground water sampling
event at the Fast Phil’s 506 site, located at 1541 Salisbury Road in Statesville, Iredell County, North
Carolina. A topographic map showing the general site location and the surrounding area is included as
Figure 1. These activities were conducted in accordance with GRI Proposal No. 22-332, which was
submitted to NCDEQ on August 29, 2022, and was approved as Task Authorization No. 40687-12 on March
3, 2023. Two change orders were submitted to NCDEQ on March 17, 2023 and May 25, 2023 and approved
as Task Authorization Nos. 40687-12.1 and 40687-12.2 on April 27, 2023 and May 26, 2023, respectively.
State correspondence is included as Appendix A.

The site is currently owned by Raymer Real Estate Operations, Inc. and is operated by Raymer Oil Company
as a petroleum retail facility. In December 2016, a Site Check was conducted at the site and a release was
identified. Two 10,000-gallon gasoline USTs, one 10,000-gallon diesel UST, and one 14,000-gallon
kerosene UST were removed from the site in June 1991. Currently, one 20,000-gallon gasoline UST, two
8,000-gallon gasoline USTs and one 1,000-gallon kerosene UST are in use at the site. UST owner/operator
information and UST system information are included as Tables 1 and 2, respectively. The Registered
Tank Report is shown below:

The site and surrounding area are commercial properties. A copy of the Land Use table is included as
Appendix B. The site contains one building and is primarily capped with concrete, asphalt, and gravel.
The overall topography at the site slopes downward to the southwest. No surface water bodies were

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
2
identified within a 500-foot radius of the site. Eight Type II monitoring wells (MW-1 through MW-8) and
one Type III monitoring well (TW-1) were installed at the site during previous ground water assessment
activities. Two additional Type II monitoring wells (PMW-7 and PMW-8) were installed on-site during
assessment activities for an adjacent site. A Site Map showing the locations of the monitoring wells and
the structures on-site has been included as Figure 2.

On March 6, 2017, GRI personnel conducted a receptor survey. No water supply wells were identified
within a 1,000-foot radius of the site. Municipal water is available to the site and surrounding properties.
Receptor information is provided in Table 3. Adjacent property owner information is presented in Table
4. A Site Vicinity Map showing the adjacent properties and a Zoning Map showing the zoning information
have been included as Figures 3a and 3b, respectively.

Soil contamination was confirmed at the site during closure activities and reported to the NCDENR on
June 12, 1991. On June 14, 1991, free product was observed at the base of one of the former 10,000-
gallon gasoline USTs during UST closure activities, and the site was issued Incident No. 7199. A ground
water treatment system was installed onsite in 1992, which ran until 1998. An NFA was granted for this
incident in 1998 after contaminant levels were lowered to below GCLs.

Two orphan 4,000-gallon and 270-gallon heating oil USTs were removed from the site on June 1, 2006. On
June 19, 2006, soil contamination around the 4,000-gallon UST was suspected and confirmed by TPH
analysis. A release was reported to the NCDENR on June 29, 2006, and the site was issued Incident No.
36123. Approximately 55.26 tons of impacted soil was removed from the site during closure activities. An
NRP was filed for the site and the incident was granted an NFA in January 2009.

Several incidents have been reported on adjacent properties. It is likely that the contaminant plume of
the current incident (No. 40687) is comingled with previous releases onsite (Incidents Nos. 7199 and
36123) and Incident No. 40479, which is the adjacent property to the southwest. Copies of the NCDEQ
Incident Reports are included as Appendix C. A map showing the locations of additional incidents in the
vicinity of the site is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
3

To date, one AFVR event and two MMPE events have been conducted at the site. A total of approximately
21,600 gallons of contaminated ground water and free product have been removed from the site. Based
on this information, the site was classified as intermediate risk and a CSA was conducted in 2017.
2.0 MONITORING WELL INSTALLATION
On September 21, 2023, one Type II monitoring well (MW-9) was installed across the street as directed
by NCDEQ correspondence dated February 8, 2022. MW-9 was installed to a total depth of 30 feet with
a screened interval of 15 feet. Copies of the well permit, well construction record, and subsurface log are
included in Appendix D.
3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Soil assessment was not conducted during the current scope of work. Historical soil quality information
is included as Appendix E.

On September 21, 2023, twelve Type II monitoring wells (MW-1 through MW-9, PMW-2, PMW-7, and
PMW-8) and one Type III monitoring well (TW-1) were gauged, purged, and sampled in accordance with
NCDEQ guidelines. Depths to ground water in the Type II monitoring wells ranged from 17.25 feet to 22.67
feet below TOC. Ground water elevations in the Type II monitoring wells ranged from 79.80 feet to 81.14
feet. Ground water flow on-site was generally to the north-northeast with a horizontal gradient of
approximately 0.01 feet per foot. The vertical gradient at the site, measured between paired wells MW-1
and TW-1, was less than 0.001 feet per foot downward. Well construction and gauging information is

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
4
presented in Tables 5a and 5b. A Water Table Surface Map based on the Type II monitoring wells on-site
is included as Figure 4. A summary of the current ground water gauging data is shown below:

Well ID
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of
Casing (ft.)
Free
Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
MW-1 15 – 30 30 100.00 19.06 --- 80.94
MW-2 15 – 30 30 101.57 21.05 --- 80.52
MW-3 15 – 30 30 102.47 22.67 --- 79.80
MW-4 15 – 30 30 98.98 18.01 --- 80.97
MW-5 15 – 30 30 100.57 19.62 --- 80.95
MW-6 15 – 30 30 98.15 17.25 --- 80.90
MW-7 15 – 30 30 101.31 20.43 --- 80.88
MW-8 15 – 30 30 100.98 20.07 --- 80.91
MW-9 15 – 30 30 98.51 17.37 --- 81.14
PMW-2 15 – 30 30 100.67 19.63 --- 81.04
PMW-7 13 – 28 28 101.13 20.33 --- 80.80
PMW-8 13 – 28 28 100.42 19.47 --- 80.95
TW-1 55 – 60 60 100.50 19.57 --- 80.93

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. The ground water sample collected from MW-9 was also submitted for analyses of
SVOCs by EPA Method 625.1, EDB by EPA Method 504.1, lead by EPA Method 6010D, and VPH and EPH
by the MADEP Methods. The reported concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE,
naphthalene, n-butylbenzene, sec-butylbenzene, EDB, 1,1-DCA, 1,2-DCA, 2-hexanone, isopropylbenzene,
IPE, p-isopropyltoluene, MIBK, n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, 1-
methylnaphthalene, 2-methylnaphthalene, lead, C5-C8 aliphatics, C9-C12 aliphatics, C9-C10 aromatics,
and/or C11-C22 aromatics exceeded the MACs in the ground water samples collected from MW-1, MW-
3 through MW-9, PMW-2, PMW-7, PMW-8, and TW-1. The reported concentrations of benzene and/or
MTBE exceeded the GCLs in the ground water samples collected from MW-1, MW-4, MW-9, and PMW-2.
A summary of the analytical results for ground water samples collected on September 21, 2023, is
presented in Table 6. A Ground Water Quality Map based on the September 2023 data is included as
Figure 5. Benzene and MTBE isoconcentration maps and cross sections are included as Figures 6 through
9. A complete report of laboratory analyses of the ground water samples collected from the monitoring
wells during the September 2023 sampling event is included as Appendix F. A summary of the current
ground water analytical data is shown below:

Contaminant
of Concern 
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well
ID
MACs (μg/l) 1 600 600 500 20 6
GCLs (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 5,660 2,190 1,650 5,430 2,950 1,300
MW-2 <0.180 <0.220 <0.170 <0.210 3.36 <0.470
MW-3 <0.180 <0.220 <0.170 <0.210 26.4 <0.470

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
5
Contaminant
of Concern 
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well
ID
MACs (μg/l) 1 600 600 500 20 6
GCLs (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-4 17,000 41,700 3,830 20,000 14,100 1,030
MW-5 4,580 14,400 2,900 14,800 712 1,090
MW-6 41.1 0.516 1.04 77.6 8.58 176
MW-7 <0.180 <0.220 <0.170 <0.210 44.0 38.5
MW-8 58.5 171 299 1,870 6.48 222
MW-9 29,900 62,300 4,160 22,000 62,700 727
PMW-2 6,880 5,800 3,030 10,400 5,460 938
PMW-7 347 9.96 204 1,190 399 615
PMW-8 1,790 43.7 J 820 167 J 218 826
TW-1 <0.180 <0.220 <0.170 <0.210 0.578 J <0.470

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the May 2017 ground water sampling event as well as the maximum
historical water column height observed in the selected area. Based on the data, the contaminant mass
has been reduced by 50.9% onsite. Contaminant mass calculations are included as Appendix G. A map of
the contaminant mass area has been included as Figure 10. A chart depicting the overall trend in
contaminant mass is shown below:

10.20
10.40
10.60
10.80
11.00
11.20
11.40
0
5,000
10,000
15,000
20,000
25,000
30,000
35,000
40,000
Av
e
r
a
g
e

W
a
t
e
r

C
o
l
u
m
n

H
e
i
g
h
t

(
f
t
)
Co
n
t
a
m
i
n
a
n
t

M
a
s
s

(
g
r
a
m
s
)
Time
Total Contaminant Mass vs. Time
Fast Phil's 506 (Incident No. 40687)
Contaminant Mass (grams)Water Column Height (ft)Linear (Contaminant Mass (grams))

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
6
The site is in the Piedmont Physiographic Province of North Carolina. The water table has a seasonal high
depth to water of approximately fourteen to seventeen feet BGS.
4.0 FREE PRODUCT REMOVAL
Free product has historically been present in MW-1. Currently, free product is not present onsite.
5.0 MMPE EVENT
An MMPE event was conducted at the site by AES under the supervision of GRI beginning on August 14,
2023, and ending on August 18, 2023. Monitoring wells MW-1, MW-4, and MW-5 were used as extraction
wells during the August 2023 MMPE event. The MMPE equipment included a liquid ring pump, a 6,000-
gallon capacity tanker, flexible vacuum hoses, 6-inch diameter discharge stack, 1.5-inch diameter PVC
stinger pipes and associated couplings and pipe fittings to manifold to three wells simultaneously. The
MMPE system was rated at 280 cfm at 25.0 in. Hg. All extraction wells were gauged prior to the start of
the event. Free product was not observed in the extraction wells at any point before, during, or after the
event. Samples were collected from the extraction wells (MW-1, MW-4, and MW-5) prior to the start of
the MMPE event and during the tanker pump out and submitted for laboratory analyses using EPA
Method 602. The stinger pipe depths ranged from 18 feet to 20 feet in MW-1, MW-4, and MW-5 over the
course of the event. A summary of the MMPE sample analytical results is included as Table 7.

Monitoring wells MW-1, MW-4, and MW-5 were each vacuumed continuously for the 96-hour event.
During the event, measurements of relative humidity, temperature, vacuum, exhaust velocity and off-gas
concentrations were recorded at the discharge stack four times per 24-hour period. Vacuum at the
extraction wells varied from 8.0 to 13.0 in. Hg. System vacuum ranged from 20.0 to 21.0 in. Hg. The
effluent velocity ranged from 1,200 to 1,250 feet per minute. The system temperature ranged from 118
to 142°F and relative humidity ranged from 38.0 to 52.0 percent. The VOC off-gas concentration ranged
from 20,000 ppm to 32,000 ppm during the event. No free product was measured in any of the wells
associated with the MMPE event at the conclusion of the event. A summary of the gauging data obtained
before start-up and at the conclusion of the MMPE event is presented in Table 5a. A copy of the MMPE
report and calculations is included as Appendix H. A summary of the gauging data for the August 2023
MMPE event is listed below:

Well ID
Product Thickness
before Recovery
(feet)
Product Thickness
after Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of Product
Recovered as Liquid
(gallons)
MW-1 0.00 0.00
9,766 0.00 MW-4 0.00 0.00
MW-5 0.00 0.00

The results of the MMPE event indicate that a total of 9,766 gallons of liquids were removed during the
event. Of the total liquids extracted, no measurable free product was removed during the event. Based
on 96 hours of operation, the average liquid recovery rate was 101.73 gallons per hour. Based on mass-
removal calculations, an additional 1,257.62 pounds or 204.43 gallons of vapor phase hydrocarbons were
removed. Based on 96 hours of operation, an average of 2.13 gallons of vapor phase hydrocarbons were

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
7
removed per hour by the MMPE system. A summary of free product recovery results is included as Table
8. Summaries of MMPE event information and cost analysis are provided in Tables 9 and 10, respectively.
At the conclusion of the MMPE event, all wastewater was transported to a licensed facility for disposal.
Copies of the disposal manifests are included in Appendix H. A summary of the free product recovery
data from the August 2023 event is listed below:

Well ID
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered
as Liquid
(gallons)
Total
Amount of
Product
Recovered
(gallons)
MW-1
1,211 136 28,444 204.43 9,766 0 204.43 MW-4
MW-5
Totals to Date 596.92 21,003 0 596.92

Although no free product was recovered in liquid form, free-product removal activities extracted over 204
gallons of vaporized product from the site. Given that no liquid free product was observed onsite before
the event, the MMPE was successful at removing petroleum constituents from the site.
6.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
MMPE events are being conducted at the site as the primary method of corrective action. Due to the site
being in the active remediation phase, no natural attenuation monitoring plan is currently in place at the
site.
7.0 CONCLUSIONS
 An MMPE event was conducted at the site from August 14 to August 18, 2023, on MW-1, MW-4,
and MW-5.
 A total of 9,766 gallons of affected ground water were recovered during the MMPE event. At the
conclusion of the event, no free product was measured in any of the wells associated with the
MMPE event. The average liquid recovery rate was 101.73 gallons per hour. An additional 204.43
gallons of vapor phase hydrocarbons were removed at an average rate of 2.13 gallons per hour.
 On September 21, 2023, twelve Type II monitoring wells and one Type III telescoping well were
gauged, purged, and sampled. No free product was measured in any of the monitoring wells.
Ground water flow on-site was generally to the north-northeast with a horizontal gradient of
approximately 0.01 feet per foot.
 The reported concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, n-
butylbenzene, sec-butylbenzene, EDB, 1,1-DCA, 1,2-DCA, 2-hexanone, isopropylbenzene, IPE, p-
isopropyltoluene, MIBK, n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, 1-
methylnaphthalene, 2-methylnaphthalene, lead, C5-C8 aliphatics, C9-C12 aliphatics, C9-C10
aromatics, and/or C11-C22 aromatics exceeded the MACs in the ground water samples collected
from MW-1, MW-3 through MW-9, PMW-2, PMW-7, PMW-8, and TW-1. The reported
concentrations of benzene and/or MTBE exceeded the GCLs in the ground water samples
collected from MW-1, MW-4, MW-9, and PMW-2. Please note that MW-9 was installed

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: October 31, 2023 Fast Phil’s 506
Project Manager: Eric M. Eubanks, P.G. GRI Project No. 4400
8
upgradient from the site in the vicinity of Incident No. 20090. Due to the location of the well
adjacent to/downgradient of a site previously containing free product, it is unlikely the
contamination reported in MW-9 is attributed to the Fast Phil’s 506 site.
 The contaminant mass has been reduced by approximately 50.9% since 2017.
 Based on this information, the risk classification for the site should remain intermediate risk.
MMPE events should continue until contaminant concentrations are below the GCLs. Semi-annual
ground water monitoring should continue at the site. However, based on the direction of ground
water flow, the source area of the contamination at the site should be reevaluated. The next
sampling event is tentatively scheduled for March 2024.
8.0 LIMITATIONS
This report has been prepared for the exclusive use of Raymer Real Estate Operations, Inc. for specific
application to the referenced site in Iredell County, North Carolina. The assessment was conducted based
on the scope of work and level of effort desired by the NCDEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
9.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO

FIGURES
Copyright:© 2013 National Geographic Society, i-cubed
FIGURE 1SITE LOCATION MAPFAST PHIL'S 5061541 SALISBURY ROADSTATESVILLE, IREDELL COUNTY,NORTH CAROLINAINCIDENT NO. 40687GRI PROJECT NO. 4400
PREPARED BY:GEOLOGICAL RESOURCES, INC.MARCH 29, 201702,000 4,0001,000 Feet
SCALE: 1 INCH = 2,000 FEET
MAP CENTER LOCATIONLATITUDE: 35.768617° NLONGITUDE: 80.853228° W
`
SITE LOCATION
³
"J
"J
SITE
4754104475.000
4754004287.000
4743999614.000
4753096991.000
4754001002.000
4753093836.000
4753095679.000
4753092308.000
4744906679.000
4753093513.000
WSW-2
WSW-1
SALISBURY HWY
SHERRILL DR
N BARKLEY RD
INDUSTRIAL DR
SALISBURY RD
GERANIUM DR
OLD SALISBURY RD
E GARNER BAGNAL BLVD
FIGURE 3A: SITE VICINITY MAPFAST PHIL'S 5061541 SALISBURY ROADSTATESVILLE, IREDELL COUNTYNORTH CAROLINAINCIDENT NO. 40687GRI PROJECT NO. 4400
PREPARED BY:GEOLOGICAL RESOURCES, INC.DECEMBER 10, 2021
³
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
"J Water Supply Well
Streets
waterline
Well Owners and Adjacent Properties
nc_iredell_parcels_poly
"J
"J
SITE
WSW-2
WSW-1
SALISBURY HWY
SHERRILL DR
N BARKLEY RD
INDUSTRIAL DR
SALISBURY RD
GERANIUM DR
OLD SALISBURY RD
E GARNER BAGNAL BLVD
FIGURE 3B: ZONING MAPFAST PHIL'S 5061541 SALISBURY ROADSTATESVILLE, IREDELL COUNTYNORTH CAROLINAINCIDENT NO. 40687GRI PROJECT NO. 4400
PREPARED BY:GEOLOGICAL RESOURCES, INC.DECEMBER 10, 2021
³
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
"J Water Supply Well
Streets
waterline
ZONING - R-8MFM
ZONING - HI
ZONING - B-5
nc_iredell_parcels_poly

TABLES
UST ID Number 001 - 004 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 - 4 Facility ID Number
Owner or Operator?
Owner/Operator
Current Owner or Operator Dates of Ownership / Operation
TABLE 1
UST OWNER/OPERATOR INFORMATION
FAST PHIL'S 506 (INCIDENT NO. 40687) 00-0-0000024533
Raymer Oil Company 10/01/1991 to present
Address Telephone Number
P.O. Box 327 Troutman, NC 28166 704-528-6652
Unknown Unknown
00-0-0000024533
Previous Owner or Operator Dates of Ownership / Operation
Unknown 03/07/1970 to 06/10/1991
Address Telephone Number
Page 1 of 1
Date: 10/31/23
001 Gasoline NA 20,000 10/1/1991 Single Wall FRP 10.5' x 31' Single Wall FRP Active Unknown
002 Gasoline NA 8,000 10/1/1991 Single Wall FRP 8' x 21.3' Single Wall FRP Active Unknown
003 Gasoline NA 8,000 10/1/1991 Single Wall FRP 8' x 21.3' Single Wall FRP Active Unknown
004 Kerosene NA 1,000 10/1/1991 Single Wall FRP 5.3' x 6' Single Wall FRP Active Unknown
Tank
Dimensions
Piping Status
of
UST
Was Release
Associated
with UST
System?
TABLE 2
UST SYSTEM INFORMATION
FAST PHIL'S 506 (INCIDENT NO. 40867)
Facility ID # 0-0024533
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Facility ID # : 0-0024533
Well ID. Parcel ID No. Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable
etc.)
Connected to
Municipal Water
Yes/No
Distance from
source area of
release
(ft.)
WSW-1 4754104475 Jenrette Real Estate, LLC 127 Patternote Cove Lane
Mooresville, NC 28117
1401 Industrial Drive
Statesville, NC 28625
Non-Potable
Inactive Yes ~1,033 ft. NE
WSW-2 4744906679 John Leon Tucker 1348 Old Salisbury Road
Statesville, NC 28625
1348 Old Salisbury Road
Statesville, NC 28625
Non-Potable
Inactive Yes ~1,092 ft. NW
Note:
• Water supply wells are keyed to Figure 3A.
TABLE 3
RECEPTOR INFORMATION
FAST PHIL'S 506 (INCIDENT NO. 40687)
Date: 12/10/21
Page 1 of 1
Date: 10/31/23 Facility ID #: 0-0024533
4753093836 (site) Raymer Real Estate Operations, Inc. 1541 Salisbury Highway
Statesville, NC 28625
Post Office Box 271
Statesville, NC 28687
4753095679 Wolff Properties, LLC 1551 Salisbury Highway
Statesville, NC 28625
1551 Salisbury Highway
Statesville, NC 28625
4753093513 Troy F. Cloaninger Jr.1550 Salisbury Highway
Statesville, NC 28625
246 Ashbrook Road
Statesville, NC 28677
4753092308 J.T. Alexander & Son, Inc.1546 Salisbury Highway
Statesville, NC 28625
Post Office Box 88
Mooresville, NC 28115
4743999614 PTM, LP 1532 Salisbury Highway
Statesville, NC 28625
C/O Sheetz, Inc.
5700 6th Ave, Altoona, PA 16602
4754001002 JNG Family Properties, LLC 1535 Salisbury Highway
Statesville, NC 28625
922 Bromley Road
Charlotte, NC 28207
4754004287 Lane Enterprises, Inc.1404 Industrial Drive
Statesville, NC 28625
3905 Hartzdale Drive, Suite 514
Camp Hill, PA 17011
4753096991 ESJ Holdings, LLC 1426 Industrial Drive
Statesville, NC 28625
327 Grace Drive
Wilkesboro, NC 28697
Note:
• Properties are keyed to Figure 3a.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
FAST PHIL'S 506 (INCIDENT NO. 40687)
PIN Property Owner Name Physical Address Property Owner Address
Page 1 of 1
Date:10/4/2023 Facility ID #: 0-0024533
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing (ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
03/07/17 20.38 ---79.62
05/22/17 19.67 ---80.33
03/21/18 19.63 0.11 80.46
09/06/18 19.41 0.13 80.70 Before AFVR
09/06/18 19.63 ---80.37 After AFVR
10/04/18 17.98 0.06 82.07
04/22/19 15.89 0.02 84.13 Hand bailed FP
Installed Sock
10/08/19 18.13 0.05 81.91 Replaced Sock
03/31/20 16.41 ---83.59 Replaced Sock
09/29/20 16.03 ---83.97 Replaced Sock
04/22/21 15.77 ---84.23
09/27/21 18.31 ---81.69 Before MMPE
10/01/21 20.91 ---79.09 After MMPE
11/03/21 18.89 ---81.11
08/14/23 18.71 ---81.29 Before MMPE
08/18/23 20.46 ---79.54 After MMPE
09/21/23 19.06 ---80.94
05/22/17 21.71 ---79.86
10/05/17 20.97 ---80.60
09/21/23 21.05 ---80.52
05/22/17 23.22 ---79.25
10/05/17 23.53 ---78.94
09/21/23 22.67 ---79.80
05/22/17 18.51 ---80.47
10/05/17 17.77 ---81.21
03/21/18 18.29 ---80.69
09/06/18 16.89 ---82.09 Before AFVR
09/06/18 16.97 ---82.01 After AFVR
10/04/18 16.76 ---82.22
04/22/19 14.88 ---84.10
10/08/19 17.04 ---81.94
03/31/20 15.11 ---83.87
09/29/20 15.02 ---83.96
04/22/21 14.74 ---84.24
09/27/21 17.28 ---81.70 Before MMPE
10/01/21 19.54 ---79.44 After MMPE
11/03/21 17.87 ---81.11
08/14/23 17.69 ---81.29 Before MMPE
08/18/23 20.65 ---78.33 After MMPE
09/21/23 18.01 ---80.97
101.57
102.47
MW-2 05/17/17
MW-3 05/17/17
TABLE 5a
WELL CONSTRUCTION AND GAUGING INFORMATION
FAST PHIL'S 506 (INCIDENT NO. 40687)
MW-1 03/06/17 15 15 - 30 30 100.00
98.98MW-4 05/17/17
15 15 - 30 30
15 15 - 30 30
15 15 - 30 30
Page 1 of 2
Date:10/4/2023 Facility ID #: 0-0024533
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing (ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 5a
WELL CONSTRUCTION AND GAUGING INFORMATION
FAST PHIL'S 506 (INCIDENT NO. 40687)
05/22/17 20.06 ---80.51
03/21/18 19.91 ---80.66 Sheen
09/06/18 18.38 ---82.19 Before AFVR
09/06/18 18.45 ---82.12 After AFVR
10/04/18 18.26 ---82.31
04/22/19 16.32 ---84.25
10/08/19 18.78 ---81.79
03/31/20 16.72 ---83.85
09/29/20 16.45 ---84.12
04/22/21 16.15 ---84.42
09/27/21 18.92 ---81.65 Before MMPE
10/01/21 20.45 ---80.12 After MMPE
11/03/21 19.41 ---81.16
08/14/23 19.32 ---81.25 Before MMPE
08/18/23 21.63 ---78.94 After MMPE
09/21/23 19.62 ---80.95
07/11/17 16.59 ---81.56
10/04/18 15.63 ---82.52
09/21/23 17.25 ---80.90
07/11/17 19.80 ---81.51
10/04/18 18.63 ---82.68
09/21/23 20.43 ---80.88
10/05/17 20.35 ---80.63
10/04/18 18.52 ---82.46
09/21/23 20.07 ---80.91
MW-9 09/21/23 09/21/23 15 15 - 30 30 98.51 17.37 ---81.14
05/22/17 20.15 ---80.35
09/21/23 19.57 ---80.93
Notes:
• Elevations relative to a temporary benchmark with an assumed elevation 100.00 ft.
• If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581].
• ft BGS : feet below ground surface.
• NA: Not available.
• NM: Not measured.
100.57
MW-8 10/05/17 15 15 - 30 30 100.98
MW-6 07/11/17
MW-7 07/11/17
MW-5 05/17/17
TW-1 05/19/17
15 15 - 30 30
15 15 - 30
55 55 - 60 60 100.50
30 98.15
15 15 - 30 30 101.31
Page 2 of 2
Date:10/4/2023 Facility ID #: 0-0024533
10/05/17 17.72 ---83.94
03/21/18 20.48 ---81.18 Sheen
04/22/19 17.03 ---84.63 Sheen
10/08/19 19.00 ---82.66
03/31/20 17.49 ---84.17
09/29/20 17.11 ---84.55
04/22/21 16.86 ---84.80
11/03/21 19.78 ---81.88
09/21/23 100.67 19.63 ---81.04
PMW-4 03/30/16 10/05/17 13 13 - 28 28 98.42 16.51 ---81.91
PMW-6 06/21/16 10/05/17 13 13 - 28 28 98.21 16.08 ---82.13
05/22/17 21.02 ---81.12
03/21/18 21.04 ---81.10 Sheen
04/22/19 17.33 ---84.81
09/21/23 101.13 20.33 ---80.80
05/22/17 20.05 ---81.38
03/21/18 20.03 ---81.40 Sheen
04/22/19 16.43 ---85.00
09/21/23 100.42 19.47 ---80.95
Notes:
• Elevations and well construction details from ATC Associates CSA report dated September 30, 2016.
• Elevations for PMW-2, PMW-7 and PMW-8 resurveyed relative to Fast Phil's datum on 09/21/23.
• ft BGS : feet below ground surface.
• NA: Not available.
• NM: Not measured.
101.43
102.1413 - 28 28
13 - 28 28
PMW-7 08/17/16 13
PMW-8 08/17/16 13
TABLE 5b
WELL CONSTRUCTION AND GAUGING INFORMATION
FAST PHIL'S 506 (INCIDENT NO. 40687)
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
(ADJACENT PANTRY #3195 SITE)
Depth to Water
from Top of
Casing (ft.)
Groundwater
Elevation
(ft.)
Free Product
Thickness
(ft.)
Comments
101.66PMW-2 03/30/16 15 15 - 30 30
Page 1 of 1
Date :10/16/23 Facility ID No. 0-0024533
EPA 504.1 SW846
6010D
We
l
l

I
D
Da
t
e

S
a
m
p
l
e
d

(m
m
/
d
d
/
y
y
)
1 600 600 500 20 6 40 128 70 70 3 6 0.4 40 70 70 25 5 100 70 400 400 0.02 1 30 15 400 700 200 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 5,900 8,800 3,000 6,000 400 40,000 25,000 70,000 11,700 5,000 100,000 30,000 28,500 24,100 50 1,000 12,000 15,000 NE NE NE NE NE NE
03/07/17 17,200 5,810 2,360 7,940 55,800 760 NR 1,090 <31 <31 <50 <31 32.7 J *66.0 J 1,120 <31 <250 *218 1,410 364 0.11 NR 303 600 <35,000 198,000 239,000 19,800 <980 3,050 JB
05/22/17 16,300 20,600 6,980 33,600 93,500 4,220 NR NR 340 198 221 <31 <31 *434 1,260 157 <250 *1,830 10,700 2,860 NR NR NR NR NR NR NR NR NR NR
03/21/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/04/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
04/22/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/08/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/31/20 10,400 6,620 1,550 6,340 49,600 320 J NR NR <250 <250 447 J <250 <250 *<250 568 J <250 <2000 *<250 781 J 335 J NR NR NR NR NR NR NR NR NR NR
09/29/20 9,190 7,620 1,980 9,260 28,500 691 NR NR **<200 <130 <130 *<130 362 J <130 <1000 *195 J 1,370 457 J NR NR NR NR NR NR NR NR NR NR
04/22/21 10,500 6,500 1,620 7,120 27,800 629 NR NR **<200 <130 <130 *<130 402 J <130 <1000 *148 J 1,070 388 J NR NR NR NR NR NR NR NR NR NR
09/27/21 11,600 11,300 5,230 28,600 21,700 11,200 NR NR NR NR NR NR *NR 310 J NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
09/29/21 7,170 3,290 1,600 6,670 10,600 1,220 NR NR NR NR NR NR *NR 173 J NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
11/03/21 9,040 E 4,140 1,860 7,050 13,500 E 772 NR NR 43.3 29.5 <0.20 <0.13 6.5 *86.7 314 24.5 <1.0 NR 236 1,650 452 NR NR NR NR NR NR NR NR NR NR
09/21/23 5,660 2,190 1,650 5,430 2,950 1,300 NR NR 28.0 J 23.3 J <22.0 M <24.0 <15.0 <38.0 88.2 66.6 M <8.90 <33.0 <7.80 175 1,330 361 NR NR NR NR NR NR NR NR NR NR
05/22/17 <0.13 0.33 J <0.13 <0.25 78.2 <0.13 NR NR <0.13 <0.13 <0.20 <0.13 <0.13 *<0.13 0.21 J <0.13 <1.0 *<0.13 <0.13 <0.13 <0.0097 NR <0.60 62.5 NR NR NR NR NR NR
09/21/23 <0.180 <0.220 <0.170 <0.210 3.36 <0.470 NR NR <0.180 <0.200 <0.220 M <0.240 <0.150 <0.380 <0.180 <0.500 M <0.089 <0.330 <0.078 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR NR NR NR
05/22/17 0.32 J 0.90 <0.13 0.31 J 35.8 <0.13 NR NR <0.13 <0.13 <0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 0.16 NR <0.57 127 NR NR NR NR NR NR
09/21/23 <0.180 <0.220 <0.170 <0.210 26.4 <0.470 NR NR <0.180 <0.200 <0.220 M <0.240 <0.150 <0.380 <0.180 <0.500 M <0.089 <0.330 <0.078 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR NR NR NR
05/22/17 22,300 41,600 3,750 18,200 19,700 540 NR NR <31 <31 <50 <31 41.6 J *127 J 500 <31 <250 *377 2,790 671 26 NR 133 14.5 NR NR NR NR NR NR
03/21/18 27,400 47,300 3,920 19,700 32,900 959 NR NR <31 <31 <50 <31 <31 *123 J 648 <31 <250 *374 2,520 656 NR NR NR NR NR NR NR NR NR NR
10/04/18 24,300 46,600 3,330 18,400 26,100 448 36,000 702 <63 <63 <100 <63 <63 *98.5 J 530 <63 <500 *256 2,240 536 NR NR NR NR 29,000 <3,500 7,950 J 1,570 <50 502 J
04/22/19 19,400 39,400 3,070 15,200 19,800 435 J NR NR <130 <130 <200 <130 <130 *<130 376 J <130 <1000 *233 J 1,880 549 NR NR NR NR NR NR NR NR NR NR
10/08/19 26,300 49,400 3,430 15,500 27,700 410 J NR NR <130 <130 <200 <130 <130 *<130 520 <130 <1000 *232 J 1,620 480 J NR NR NR NR NR NR NR NR NR NR
03/31/20 23,800 48,500 3,040 18,700 22,100 308 J NR NR <130 <130 244 J <130 <130 *<130 478 J <130 <1000 *226 J 1,660 541 NR NR NR NR NR NR NR NR NR NR
09/29/20 22,500 48,000 3,070 16,300 23,100 322 J NR NR **<200 <130 <130 *<130 426 J <130 <1000 *220 J 1,650 489 J NR NR NR NR NR NR NR NR NR NR
04/22/21 22,300 44,300 2,810 15,000 14,600 383 J NR NR **<200 <130 <130 *<130 391 J <130 <1000 *213 J 1,670 470 J NR NR NR NR NR NR NR NR NR NR
09/27/21 25,800 49,500 2,870 13,600 23,800 521 J NR NR NR NR NR NR *NR 487 J NR *NR NR NR NR NR NR NR NR NR NR NR NR NR
09/29/21 15,600 35,100 2,820 13,400 4,210 333 J NR NR NR NR NR NR *NR 184 J NR *NR NR NR NR NR NR NR NR NR NR NR NR NR
11/03/21 20,500 36,500 3,230 15,900 13,300 658 NR NR <31 <31 <50 <31 <31 *112 J 411 <31 <250 *314 2,200 516 NR NR NR NR NR NR NR NR NR NR
09/21/23 17,000 41,700 3,830 20,000 14,100 1,030 NR NR 36.9 J 30.4 J <22.0 M <24.0 <15.0 499 174 285 M <8.90 <33.0 354 433 3,290 771 NR NR NR NR NR NR NR NR NR NR
05/22/17 8,130 22,400 3,240 15,900 490 568 NR NR <31 <31 <50 <31 <31 *145 94.5 J <31 <250 *410 2,840 670 23.4 148 32.8 NR NR NR NR NR NR
03/21/18 9,640 24,500 3,350 16,800 871 759 NR NR 38.9 J <31 <50 <31 <31 *145 143 <31 <250 *427 2,690 702 NR NR NR NR NR NR NR NR NR NR
10/04/18 8,830 24,800 3,100 16,000 575 525 6,810 <50 <31 <31 <50 <31 <31 *123 J 99.3 J <31 <250 *326 2,370 544 NR NR NR NR 20,000 3,680 J 9,390 2,010 <48 920
04/22/19 9,070 23,000 3,380 16,500 1,750 575 NR NR <63 <63 <100 <63 <63 *136 J 192 J <63 <500 *366 2,580 688 NR NR NR NR NR NR NR NR NR NR
10/08/19 9,920 26,900 3,090 13,400 1,020 433 J NR NR <130 <130 <200 <130 <130 *<130 159 J <130 <1000 *252 J 1,610 440 J NR NR NR NR NR NR NR NR NR NR
03/31/20 9,910 29,000 3,390 17,400 1,010 316 J NR NR <130 <130 <200 <130 <130 *<130 159 J <130 <1000 *301 J 1,700 473 J NR NR NR NR NR NR NR NR NR NR
09/29/20 7,620 23,000 2,820 13,600 733 347 J NR NR **<200 <130 <130 *<130 <130 <130 <1000 *272 J 1,680 461 J NR NR NR NR NR NR NR NR NR NR
04/22/21 6,780 18,700 2,650 11,800 <130 353 J NR NR **<130 <130 <130 *<130 <130 <130 1010 J *260 J 1,640 401 J NR NR NR NR NR NR NR NR NR NR
09/27/21 10,900 31,300 3,210 15,800 743 340 J NR NR NR NR NR NR NR *NR 154 J NR NR *NR NR NR NR NR NR NR NR NR NR NR NR NR
09/29/21 5,080 13,900 2,200 10,500 910 306 NR NR NR NR NR NR NR *NR 74.9 J NR NR *NR NR NR NR NR NR NR NR NR NR NR NR NR
11/03/21 6,360 17,300 2,670 12,900 694 671 NR NR <63 <63 <100 <63 <63 *128 J 105 J <63 <500 *317 2,150 497 NR NR NR NR NR NR NR NR NR NR
09/21/23 4,580 14,400 2,900 14,800 712 1,090 NR NR 87.3 71.2 <22.0 M <24.0 <15.0 469 208 61.9 M 36.3 J <33.0 <7.80 516 3,510 844 NR NR NR NR NR NR NR NR NR NR
07/11/17 13.2 0.38 J 4.0 26.5 1.5 80.1 NR NR 2.2 3.5 <0.20 <0.13 <0.13 *3.9 0.28 J 2.2 <1.0 *4.9 41.9 9.5 NR NR 93.8 NR NR NR NR NR NR NR
10/04/18 21.1 1.7 J 6.7 41.8 1.9 J 201 <10 <1.0 2.5 3.5 <1.0 <0.63 <0.63 *5.2 <0.63 2.8 <5.0 *6.1 59.5 14.0 NR NR NR NR 242 77.9 J 427 133 J <50 1,330
09/21/23 41.1 0.516 1.04 77.6 8.58 176 NR NR 2.95 4.95 <0.220 M <0.240 <0.150 <0.380 10.6 <0.500 M 4.71 <0.330 <0.078 3.47 122 9.40 NR NR NR NR NR NR NR NR NR NR
07/11/17 <0.13 <0.13 <0.13 <0.25 15.3 0.15 J NR NR <0.13 <0.13 <0.20 15.3 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 0.16 J NR NR <0.61 NR NR NR NR NR NR NR
10/04/18 <0.13 <0.13 <0.13 <0.25 13.6 <0.13 <2.0 <0.20 <0.13 <0.13 <0.20 15.2 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR <35 <35 <35 <48 <48 593
09/21/23 <0.180 <0.220 <0.170 <0.210 44.0 38.5 NR NR <0.180 <0.200 <0.220 M 4.66 <0.150 <0.380 <0.180 <0.500 M <0.089 <0.330 <0.078 <0.190 0.439 J <0.180 NR NR NR NR NR NR NR NR NR NR
MAC (µg/l)
GCL (µg/l)
C9
-
C
1
0

A
r
o
m
a
t
i
c
s
C9
-
C
1
8

A
l
i
p
h
a
t
i
c
s
C1
9
-
C
3
6

A
l
i
p
h
a
t
i
c
s
C1
1
-
C
2
2

A
r
o
m
a
t
i
c
s
1-M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
2-M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
Le
a
d
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
Me
t
h
y
l

i
s
o
b
u
t
y
l

k
e
t
o
n
e

(M
I
B
K
)
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
2-
H
e
x
a
n
o
n
e
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r

(IP
E
)
p-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
(4
-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
)
1,1
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
1,2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
To
t
a
l

X
y
l
e
n
e
s
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
(M
T
B
E
)
n-
B
u
t
y
l
b
e
n
z
e
n
e
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FAST PHIL'S 506 (INCIDENT NO. 40687)
Analytical Method
→SM 6200B EPA 625 MADEP VPH MADEP EPH
Na
p
h
t
h
a
l
e
n
e
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
te
r
t
-
A
m
y
l

m
e
t
h
y
l

e
t
h
e
r

(T
A
M
E
)
Contaminant of Concern
→
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Me
t
h
y
l

c
h
l
o
r
i
d
e
(C
h
l
o
r
o
m
e
t
h
a
n
e
)
MW-5
MW-6
MW-7
MW-4
MW-1
MW-2
MW-3
Page 1 of 2
Date :10/16/23 Facility ID No. 0-0024533
EPA 504.1 SW846
6010D
We
l
l

I
D
Da
t
e

S
a
m
p
l
e
d

(m
m
/
d
d
/
y
y
)
1 600 600 500 20 6 40 128 70 70 3 6 0.4 40 70 70 25 5 100 70 400 400 0.02 1 30 15 400 700 200 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 128,000 5,900 8,800 3,000 6,000 400 40,000 25,000 70,000 11,700 5,000 100,000 30,000 28,500 24,100 50 1,000 12,000 15,000 NE NE NE NE NE NE
MAC (µg/l)
GCL (µg/l)
C9
-
C
1
0

A
r
o
m
a
t
i
c
s
C9
-
C
1
8

A
l
i
p
h
a
t
i
c
s
C1
9
-
C
3
6

A
l
i
p
h
a
t
i
c
s
C1
1
-
C
2
2

A
r
o
m
a
t
i
c
s
1-M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
2-M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
Le
a
d
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
2
-
D
i
b
r
o
m
o
e
t
h
a
n
e
(E
D
B
)
Me
t
h
y
l
e
n
e

C
h
l
o
r
i
d
e
Me
t
h
y
l

i
s
o
b
u
t
y
l

k
e
t
o
n
e

(M
I
B
K
)
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
2-
H
e
x
a
n
o
n
e
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
Di
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r

(IP
E
)
p-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
(4
-
I
s
o
p
r
o
p
y
l
t
o
l
u
e
n
e
)
1,1
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
1,2
-
D
i
c
h
l
o
r
o
e
t
h
a
n
e
To
t
a
l

X
y
l
e
n
e
s
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l

e
t
h
e
r
(M
T
B
E
)
n-
B
u
t
y
l
b
e
n
z
e
n
e
se
c
-
B
u
t
y
l
b
e
n
z
e
n
e
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FAST PHIL'S 506 (INCIDENT NO. 40687)
Analytical Method
→SM 6200B EPA 625 MADEP VPH MADEP EPH
Na
p
h
t
h
a
l
e
n
e
te
r
t
-
A
m
y
l

a
l
c
o
h
o
l
(T
A
A
)
te
r
t
-
A
m
y
l

m
e
t
h
y
l

e
t
h
e
r

(T
A
M
E
)
Contaminant of Concern
→
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Me
t
h
y
l

c
h
l
o
r
i
d
e
(C
h
l
o
r
o
m
e
t
h
a
n
e
)
10/05/17 458 3,910 2,160 10,200 <6.3 650 NR NR 35.9 28 <10 <6.3 <6.3 *209 <6.3 18.4 J <50 *486 2,690 727 <0.94 NR 109 6.2 NR NR NR NR NR NR
10/04/18 533 3,080 1,550 7,640 <13 370 <200 <20 30.6 J 25.2 J <20 <13 <13 *181 <13 15.3 J <100 *436 3,120 662 NR NR NR NR 3,730 <1,800 10,500 1,020 <50 793
09/21/23 58.5 171 299 1870 6.48 222 NR NR 19.3 14.4 <0.220 M 8.56 <0.150 <0.380 75.0 0.603 M 9.81 0.453 J <0.078 97.5 1300 170 NR NR NR NR NR NR NR NR NR NR
MW-9 09/21/23 29,900 62,300 4,160 22,000 62,700 727 NR NR 30.9 J 21.2 J <22.0 M <24.0 <15.0 211 197 660 M <8.90 <33.0 <7.80 407 3,140 753 23.8 50.8 91.4 85.0 69,800 14,600 7,020 186 J <124 470
05/22/17 1.6 1.0 0.34 J 1.2 J 4.8 0.24 J NR NR <0.13 <0.13 <0.20 <0.13 3.9 *<0.13 0.15 J <0.13 <1.0 *<0.13 0.22 J <0.13 <0.0097 NR <0.60 6.3 NR NR NR NR NR NR
09/21/23 <0.180 <0.220 <0.170 <0.210 0.578 J <0.470 NR NR <0.180 <0.200 <0.220 M <0.240 6.94 <0.380 <0.180 <0.500 M <0.089 <0.330 <0.078 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR NR NR NR
03/21/18 13,900 43,900 8,010 39,500 26,700 2,790 NR NR 553 293 <100 <63 114 J *672 436 201 J <500 *2,450 13,200 4,060 NR NR NR NR NR NR NR NR NR NR
04/22/19 5,970 15,200 2,230 11,100 5,560 628 NR NR <63 <63 <100 <63 <63 *105 J 165 J <63 548 J *279 2,130 585 NR NR NR NR NR NR NR NR NR NR
10/08/19 11,900 23,700 3,270 14,400 12,600 649 NR NR <63 <63 <100 <63 <63 *111 J 280 <63 <500 *319 2,350 649 NR NR NR NR NR NR NR NR NR NR
03/31/20 14,000 19,900 2,730 14,100 18,300 358 NR NR <63 <63 199 J <63 67.5 J *72.1 J 314 <63 <500 *209 J 1,490 439 NR NR NR NR NR NR NR NR NR NR
09/29/20 14,000 12,600 2,720 11,200 28,800 377 J NR NR **<200 <130 <130 *<130 322 J <130 <1000 *232 J 1,420 419 J NR NR NR NR NR NR NR NR NR NR
04/22/21 14,200 8,960 2,710 10,300 29,900 491 J NR NR **<200 <130 <130 *<130 365 J <130 <1000 *231 J 1,560 462 J NR NR NR NR NR NR NR NR NR NR
11/03/21 13,400 8,430 4,330 18,500 27,500 3,440 NR NR 290 153 J <100 <63 <63 *312 466 111 J <500 *1,200 10,500 2,660 NR NR NR NR NR NR NR NR NR NR
09/21/23 6,880 5,800 3,030 10,400 5,460 938 NR NR 33.4 J <20.0 <22.0 M <24.0 <15.0 103 131 94.0 M 21.7 J <33.0 <7.80 332 2,620 674 NR NR NR NR NR NR NR NR NR NR
05/22/17 739 39.5 552 2,170 3,670 559 NR NR 10.5 J 8.8 J <10 <6.3 <6.3 *30.4 66.4 8.5 J <50 *75.9 574 86.6 NR NR NR NR NR NR NR NR NR NR
03/21/18 827 54.6 425 1,850 4,200 667 NR NR <13 <13 <20 <13 <13 *39.5 J 65.5 <13 <100 *65.6 567 114 NR NR NR NR NR NR NR NR NR NR
04/22/19 637 21.3 J 317 1,230 3,390 568 NR NR <13 <13 <20 <13 <13 *32.7 J 55.2 <13 <100 *50.1 458 81.6 NR NR NR NR NR NR NR NR NR NR
09/21/23 347 9.96 204 1,190 399 615 NR NR 8.27 10.4 <2.20 M <2.40 <1.50 <3.80 37.2 7.70 M 12.1 <3.30 <0.780 49.6 680 152 NR NR NR NR NR NR NR NR NR NR
05/22/17 2,320 27.0 1,030 129 4,770 763 NR NR 81.2 55 <5.0 <3.1 <3.1 *111 53.9 58 <25 *261 107 93.5 NR NR NR NR NR NR NR NR NR NR
03/21/18 2,420 23.3 J 958 106 5,640 E 710 NR NR 41.2 26.5 <10 <6.3 <6.3 *69.5 59.1 29.7 <50 *156 85.3 75.8 NR NR NR NR NR NR NR NR NR NR
04/22/19 1,440 77.6 766 293 405 421 NR NR 11.6 J 10.8 J <10 <6.3 <6.3 *39.7 12.1 J 12.5 J 60.4 J *78.6 98.8 66.8 NR NR NR NR NR NR NR NR NR NR
09/21/23 1,790 43.7 J 820 167 J 218 826 NR NR 23.0 J <20.0 <22.0 M <24.0 <15.0 <38.0 62.9 <50.0 M 22.2 J <33.0 <7.80 102 122 80.5 NR NR NR NR NR NR NR NR NR NR
05/22/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 <0.13 <0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
07/11/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 <0.13 <0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
03/21/18 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 NR NR <0.13 <0.13 <0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
10/04/18 <0.13 0.18 J <0.13 <0.25 <0.13 <0.13 <2.0 <0.20 <0.13 <0.13 <0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
04/22/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 <0.13 <0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
10/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 <0.13 <0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
03/31/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 <0.13 <0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
09/29/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR **<0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
04/22/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR **<0.20 <0.13 <0.13 *<0.13 <0.13 <0.13 <1.0 *<0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
09/27/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR <0.13 NR *NR <0.13 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
11/03/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR <0.13 <0.13 <0.20 <0.45 <0.13 <0.55 <0.13 <0.13 <0.13 1.0 J <0.61 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR
09/21/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.180 <0.200 <0.220 M <0.240 <0.150 <0.380 <0.180 <0.500 M <0.089 <0.330 <0.078 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR NR NR NR
Notes:
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Standard not established.
• NR: Not requested.
• FP: Free product.
• Concentrations in bold face type exceeded the MAC.
• Concentrations in italic face type exceeded the GCL.
• J: Estimated value.
• B: Analyte found in associated method blank.
• < : Less than the method detection limit specified in the laboratory report.
• Other reported compounds above the MACs: 5/22/17; n-butylbenzene in MW-1 and PMW-8, sec-butylbenzene in MW-1, methyl chloride in MW-1, styrene in MW-1 and 1,2,3-trichloropropane in PMW-8: 7/11/17; 1,1-dichloroethane in MW-7:
3/21/18; n-butylbenzene, sec-butylbenzene and styrene in PMW-2: 3/31/20; methyl chloride in MW-1, MW-4 and PMW-2, tetrachloroethene and trichloroethene in MW-4: 4/22/21; methylene chloride in MW-5.
• Refer to laboratory report for other detectable concentrations which did not exceed the MACs.
• *: Concentrations prior to the initial detection in ground water have not been updated.
Trip Blank
PMW-7
PMW-8
TW-1
MW-8
PMW-2
Page 2 of 2
Facility ID #: 0-0024533
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70
5,000 260,000 80,000 50,000 20,000 6,000 70,000
9/27/2021 11,600 11,300 5,230 28,600 21,700 11,200 310 J
9/29/2021 7,170 3,290 1,600 6,670 10,600 1,220 173 J
8/14/2023 4,950 2,660 1,860 6,810 1,870 1,220 61.9
8/16/2023 2,360 1,550 1,080 4,710 6,920 898 103
9/27/2021 25,800 49,500 2,870 13,600 23,800 521 J 487 J
9/29/2021 15,600 35,100 2,820 13,400 4,210 333 J 184 J
8/14/2023 23,400 36,800 3,870 19,900 21,200 848 574
8/16/2023 18,600 32,800 5,690 28,000 18,400 1,450 466
9/27/2021 10,900 31,300 3,210 15,800 743 340 J 154 J
9/29/2021 5,080 13,900 2,200 10,500 910 306 74.9 J
8/14/2023 6,790 15,500 3,180 15,700 882 834 128
8/16/2023 6,430 13,000 3,280 16,200 1,490 1,000 145
04/16/18 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00
08/18/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <0.500
Notes:
reported concentrations in italics are above the GCLs.
MW-4
MW-5
Trip Blank
TABLE 7
SUMMARY OF MMPE SAMPLE ANALYTICAL RESULTS
FAST PHIL'S 506 (INCIDENT NO. 40687)
EPA Method 6200B
Date: 10/17/23
Analytical Method

MAC (μg/l)
Contaminant of Concern

• J: Estimated value.
• Results reported in µg/l (micrograms per liter)• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross Contamination Level.
Xy
l
e
n
e
s
Et
h
y
l
b
e
n
z
e
n
e
To
l
u
e
n
e
Be
n
z
e
n
e
Na
p
h
t
h
a
l
e
n
e

D
I
-
i
s
o
p
r
o
p
y
l

e
t
h
e
r
GCL (μg/l)
• MMPE: Mobile Multi-Phase Extraction
• Concentrations in bold face type indicate the reported concentrations are above the MACs;
MT
B
E
MW-1
Page 1 of 1
Date: 10/17/23
Method of Measurement:
Well ID
Product Type
(gas, diesel,
etc.)
Date of Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product
Thickness
before
Recovery
(feet)
Product
Thickness
after
Recovery
(feet)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
MW-1 Gasoline 09/06/18 AFVR 2 0.13 0.00 1,647 0
MW-1 0.00 0.00
MW-4 0.00 0.00
MW-5 0.00 0.00
MW-1 0.00 0.00
MW-4 0.00 0.00
MW-5 0.00 0.00
Notes :
• Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event
(based on Disposal Manifest and/or Field Notes).
0Gasoline 8/14/2023 - 08/18/23 MMPE 2 9,766
0
TABLE 8
FREE PRODUCT RECOVERY RESULTS
FAST PHIL's 506 (INCIDENT NO. 40687)
Facility ID#: 0-0024533
Interface probe at top-of-casing
Gasoline 09/27/21 - 10/01/21 MMPE 2 9,590
Page 1 of 1
Date: 10/17/23
MW-1 09/06/18 AFVR 719 149 222 0.08 1,647 0 0.08
MW-1
MW-4
MW-5
MW-1
MW-4
MW-5
596.92 21,003 0 596.92
Notes:
• Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.15
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
0 204.431,211 136 28,444 204.43 9,766
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid (gallons)
Total Amount
of Product
Recovered
(gallons)
TABLE 9
FREE PRODUCT RECOVERY EVENT INFORMATION
FAST PHIL's 506 (INCIDENT NO. 40687)
Facility ID #: 0-0024533
Well ID Date (mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
09/27/21 - 10/01/21 MMPE 1,503 152 42,611 392.41 9,590 0 392.41
Totals
SUMMARY OF FLUID REMOVAL
08/14/23 - 08/18/23 MMPE
Current Event 9,970.43 204.43
Total To Date 21,599.92 596.92
Page 1 of 1
Date: 10/16/23 Facility ID #: 0-0024533
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Free Product plus
Ground Water
Recovered
(gallons)
Cost of Free
Product Recovery
Event
Cost Per Gallon
(total fluids)Comments
MW-1 AFVR 09/06/18 1,647.08 $2,590.45 $1.57 Cost per gallon for the event is based on a total volume of
1,647.08 gallons of free product and water.
MW-1, MW-4,
MW-5 MMPE 09/27/21 -
10/01/21 9,982.41 $11,158.65 $1.12 Cost per gallon for the event is based on a total volume of
9,982.41 gallons of free product and water.
MW-1, MW-4,
MW-5 MMPE 08/14/23 -
08/18/23 9,970.43 $11,824.50 $1.19 Cost per gallon for the event is based on a total volume of
9,970.43 gallons of free product and water.
21,599.92 $25,573.60 $1.18
Notes:
• Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
TABLE 10
FREE PRODUCT RECOVERY COST SUMMARY
FAST PHIL's 506 (INCIDENT NO. 40687)
TOTAL (to date)
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, and subcontractor costs.
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

February 8, 2022
D.L. Raymer Raymer Brothers, Inc. PO Box 327 Troutman, NC 28166

Re: Acknowledgement of Report Receipt
Fast Phil’s #506
1541 Salisbury Road, Statesville Iredell County
Incident Number: 40687 Risk Classification: Intermediate Ranking: I-125-D

Dear Mr. Raymer:

The UST Section, Division of Waste Management, is in receipt of the report dated December 21,
2021. The report has been reviewed and will be maintained in the Mooresville Regional Office.
If you have questions regarding the information contained in this letter, please contact me at
[e-mail] or at the address and telephone number listed below.

Sincerely,

Ryan A. Bond, P.G.
Hydrogeologist
Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ

cc: Sam McKay, P.G. – GRI
Mooresville Regional Office | 610 E Center Ave | Suite 301 | Mooresville, NC 28115 | [phone]
MO-9217_40687_G_C_20220208
1
Leslie Maxtone-Graham
From:Bond, Ryan A <[e-mail]>
Sent:Tuesday, February 8, 2022 4:28 PM
To:Sam McKay
Cc:Leslie Maxtone-Graham
Subject:RE: [External] Fast Phil's 506
Attachments:MW9.PNG; MO-9217_40687_G_C_20220208.pdf
Hi Sam,

Attached is the acknowledgement letter. Please forward to Mr. Raymer. After discussions with Trust Fund, below is
what we recommend.

Incident #40687 – Fast Phil's 506
 Perform MMPE using MW1, MW4, and MW5 in February/March.
 Install MW across street in grassy median area (highlighted in attached pic).
 Survey TOC elevations for Pantry #3195 monitoring wells PMW-2, PMW-7, and PMW-8 to the Fast Phil’s 506
datum.
 Perform MIP/LIF analysis.
 Schedule comprehensive sampling event to include all monitoring wells in March/April.

Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115

Branch’s Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch’s Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program

Interactive Maps with DWM Sites and Permitted Facilities:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps
File Review Procedures:
https://deq.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
Online Access to UST Section Documents (Laserfiche):
https://deq.nc.gov/about/divisions/waste-management/laserfiche

Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policy.pdf
https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/UST%20file%20names%20for%20Laserfiche.docx

From: Leslie Maxtone-Graham [mailto:[e-mail]]
Sent: Tuesday, December 21, 2021 11:29 AM
To: Bond, Ryan A <[e-mail]>
Site Name City / County Iredell Incident #40687
Resp Pty Name / Contact Incident Mgr Region MOR
RP Type (Owner/Operator / Landowner / Attny‐in‐fact)Change Order? Prev. TA #11
Consultant / Project Mgr Samuel L. McKay, III
Telephone / Fax Number Task Authorization Number:12 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I‐125‐D RRA Date:4/5/2017
Proposal# / Scope Dates % Commercial (C=100%,  NC=0%,  Both=1%‐99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active  or  NFA Date)
With Claim: [  ] All Main Consultant/Contractor invoices attached? [  ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
3r
d
 Pt
y
 De
d
?
Task #Lab / 
SubCode RO
 Au
t
h
Proposed 
Rate/Price
(Consultant)CO
 Au
t
h
Proposed Task 
Subtotal
(Consultant)
Final 
Preapproved 
Subtotal
(UST Section)
Claimed 
Amount3
(Consultant)
3.060 1 / event Y $975.00 y $975.00 $975.00 /
3.101 30 / feet Y $12.50 y $375.00 $375.00 /
3.113 30 / feet Y $50.00 y $1,500.00 $1,500.00 /
3.118 30 / feet Y $5.00 y $150.00 $150.00 /
3.310 1 / event Y $20,950.00 y $20,950.00 $20,950.00 /
3.351 4 / wells Y $80.00 y $320.00 $320.00 /
3.397 1 / Mobe Y $100.00 y $100.00 $100.00 /
3.398 1 / Mobe Y $350.00 y $350.00 $350.00 /
4.031 19 / wells Y $110.00 y $2,090.00 $2,090.00 /
4.090 #220 7 / samples Y $40.00 y $280.00 $280.00 /
4.090 #272 14 / samples Y $66.00 y $924.00 $924.00 /
4.090 #280 1 / sample Y $45.00 y $45.00 $45.00 /
4.090 #301 1 / sample Y $208.00 y $208.00 $208.00 /
4.090 #330 1 / sample Y $14.00 y $14.00 $14.00 /
4.090 #341 1 / sample Y $56.00 y $56.00 $56.00 /
4.090 #342 1 / sample Y $100.00 y $100.00 $100.00 /
4.091 3 /shipments Y $60.00 y $180.00 $180.00 /
6.090 1 / report Y $1,125.00 y $1,125.00 $1,125.00 /
6.190 1 / Letter Y $500.00 y $500.00 $500.00 /
7.420 1 / event Y $2,325.00 y $2,325.00 $2,325.00 /
7.420 1 / event Y $1,500.00 y $1,500.00 $1,500.00 /
7.420 1 / event Y $2,500.00 y $2,500.00 $2,500.00 /
7.420 5000 / gallons Y $0.35 y $1,750.00 $1,750.00 /
7.420 5000 / gallons Y $0.25 y $1,250.00 $1,250.00 /
12.030 7 / nights Y $151.00 y $1,057.00 $1,057.00 /
12.050 6 / trips Y $250.00 y $1,500.00 $1,500.00 /
12.055 6 / trips Y $50.00 y $300.00 $300.00 /
Requested Preapproved Claimed3
 TOTAL:$42,424.00 $42,424.00 TOTAL:
Total Standard Costs (Not Third Party)$42,424.00 $42,424.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal: 8/29/22 by: (PM)(Reserved for RO)
RO Review: 2/10/23 by: (IM) Joint UST Preapproval Confirmed By: Date1 3/3/2023
CO Review: 3/3/23 by: (STF) RP or Designee Receipt Confirmed By: Date 4
1 ‐ This ePATA expires one year from the Joint UST Preapproval date.  This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 ‐ THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 ‐ Only Tasks included on this ePATA may be claimed.  Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 ‐ Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved.  Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supersede other regulatory deadlines as described in #1 above.  Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 ‐ Tasks approved on Directed ‐ CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
DIRECTED COSTS
Statesville
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704‐845‐4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Fast Phil's 506
Note: This Electronic Preapproval Task Authorization (ePATA) shall be used to receive preapproval from the UST Section. A proposal,including maps andfigures,must be attached to
elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If, following completion of this ePATA, you discover that
unexpected tasks must be performed, incurring costs for tasks not originally included with this form, you must complete and submit a separate ePATA request designated as a "Change
Order" in the provided space above prior to conducting those tasks. Include a copy of the prior ePATA form for confirmation. Please attach this form to the cover of the corresponding
claim when requesting reimbursement. IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been completed within 12 months of the
completion date of the FIRST completed task to remain within the Statute of Limitations. All ePATAs submitted within a claim are closed with that claim, and may not be re-used in a
separate submittal, even for costs or tasks that were not originally claimed. Final reimbursement of costs associated with the Total Claimed amount below may be affected by the
eligibility status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and necessary expenses per 15A NCAC 2P .0402 and
.0404.
TMB
TC
(Initials)
SLM
Proposed 
Units / Type
(Consultant)
Trudy Beverly
ActiveYES
22‐332 September ‐ October 202
704‐845‐4012
Dates of Work
(Consultant)
Started1  /  Completed2
FINAL REIMBURSEMENT
100.00%
[e-mail]
Kim Robertson Raymer Oil Company
Geological Resources, Inc.
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality  ‐Division of Waste Management
Samuel L. McKay III 3/3/2023
4400 Received MAR 03 2023
Site Name City / County /Iredell Incident #40687
Resp Pty Name / Contact Incident Mgr Region MOR
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #12
Consultant / Project Mgr /Sam McKay
Telephone / Fax Number /Task Authorization Number:12 ChangeOrd:1
Project Mgr Email Site Risk / Rank / Abatement:I-125-D RRA Date:4/5/2017
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
w Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
3r
d

P
t
y

D
e
d
?
Task #Lab /
SubCode RO

A
u
t
h
Proposed
Rate/Price
(Consultant)CO

A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
7.201 8 /hours Y $93.00 Y $744.00 $744.00 /
//
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//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$744.00 $744.00 TOTAL:
Total Standard Costs (Not Third Party)$744.00 $744.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:3/17/23 by:(PM)(Reserved for RO)
RO Review:4/25/23 by:(IM)Joint UST Preapproval Confirmed By:Date1
CO Review:4/27/23 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
DIRECTED COSTS
Statesville
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Fast Phil's 506
Note: This Electronic Preapproval Task Authorization (ePATA) shall be used to receive preapproval from the UST Section. A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If, following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form, you must complete and submit a separate ePATA request
designated as a "Change Order"inthe provided space above prior to conducting those tasks. Include a copy of the prior ePATA form for confirmation. Please attach this formto
the cover of the corresponding claim when requesting reimbursement. IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion dateof the FIRST completed task to remain within the Statuteof Limitations. All ePATAs submitted within a claim are closed with that
claim, and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed. Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
RCM
LP
(Initials)
SM
Proposed
Units / Type
(Consultant)
Ryan Mills
ActiveYES
22-332 April - June 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
Yes
[e-mail]
Kim Robertson Raymer Oil Compny
Geological Resources, Inc.
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management
4/27/2023
Sam McKay 4/27/2023
4400 Received APR 27 2023
Site Name City / County /Iredell Incident #40687
Resp Pty Name / Contact Incident Mgr Region MOR
(Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #12
Consultant / Project Mgr Sam McKay
Telephone / Fax Number Task Authorization Number:12 ChangeOrd:2
Project Mgr Email Site Risk / Rank / Abatement:I-125-D RRA Date:4/5/2017
Proposal# / Scope Dates % Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
3r
d

P
t
y

D
e
d
?
Task #Lab /
SubCode RO

A
u
t
h
Proposed
Rate/Price
(Consultant)CO

A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
1.050 1 /agreement Y $300.00 y $300.00 $300.00 /
3.080 1 /permit Y $250.00 y $250.00 $250.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed
TOTAL:$550.00 $550.00 TOTAL:
Total Standard Costs (Not Third Party)$550.00 $550.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:5/25/23 by:(PM)(Reserved for RO)
RO Review:5/25/17 by:(IM)Joint UST Preapproval Confirmed By:
CO Review:5/26/23 by:(STF)RP or Designee Receipt Confirmation By:
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
DWM/UST ePATA 4/1/2022
Proposed
Units / Type
(Consultant)
Ryan Mills
ActiveYES
22-332 April - June 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
100.00%
Yes
[e-mail]
Raymer Oil Compny
Geological Resources, Inc.
Statesville
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
Fast Phil's 506
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request
designated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the priorePATAform for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion date of the FIRST completed task to remain withintheStatuteof Limitations.All ePATAs submittedwithin aclaim are closed with thatclaim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
RCM
TC
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality -Division of Waste Management
5/26/2023
5/26/2023
4400 Received MAY 26 2023

APPENDIX B
Land Use Information
Date: 12/14/21 Facility ID # : 0-0024533
Map ID No.Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
n/a HI Heavy Industrial n/a n/a
n/a B-5 General Business n/a n/a
n/a R-8MFM Medium-Density Multi-
Family Residential n/a n/a
Note:
• Properties are keyed to Figure 3b.
APPENDIX B
LAND USE INFORMATION
FAST PHIL's 506 (INCIDENT NO. 40687)
Page 1 of 1

APPENDIX C
Incident Reports
NCDEQ Incident Report
RP/Company RAYMER BROTHERS INC
RPAddress POB 327
RPCity TROUTMAN
Contact D.L. RAYMER
RPState NC
TELEPHONE [phone]
IncidentNumber 40687 USTNum MO-9217
IncidentName FAST PHILS #506 2
FacilID
Address 1541 SALISBURY ROAD
CityTown STATESVILLE State NC
ZipCode 28166-
DateOccurred 1 /6 /2017
DateReported 1 /12/2017
ConfRisk I
CloseOut
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr RCMLongitude-80.853228 Latitude 35.768610
County IREDE
SCH 1/12/2017 1/19/2017
LSA1 4/3/2017 4/5/2017
CSAM 8/9/2017 8/14/2017 11/14/2017
MRP 10/31/2017 11/13/2017
OTH 11/2/2017 11/14/2017
WELL CONSTRUCTION A SAMPLING REPORT
Monday, October 16, 2023 Page 1 of 2
FPRI 10/25/2018 11/6/2018
MRP 5/28/2019 6/5/2019
MRP 11/25/2019 12/5/2019
RMR 4/20/2020 4/21/2020
RMR 10/29/2020 1/25/2021
RMR 5/26/2021 7/15/2021
RMR 12/21/2021 2/2/2022
Monday, October 16, 2023 Page 2 of 2
NCDEQ Incident Report
RP/Company RAYMER OIL COMPANY
RPAddress PO BOX 271
RPCity STATESVILLE
Contact RAYMER OIL CO
RPState NC
TELEPHONE
IncidentNumber 7199 USTNum MO-3162
IncidentName RAYMER OIL COMPANY
FacilID 00-0-0000026418
Address HWY 70 EAST
CityTown STATESVILLE State NC
ZipCode 28677-
DateOccurred 9 /17/1991
DateReported 9 /17/1991
ConfRisk L
CloseOut 12/1/1998
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr KWCLongitude-80.852940 Latitude 35.768680
County IREDE
CSA 1/23/1992
CAP 9/25/1992 11/3/1992 11/3/1992
Monday, October 16, 2023 Page 1 of 1
NCDEQ Incident Report
RP/Company RAYMER OIL COMPANY
RPAddress P.O. BOX 271
RPCity STATESVILLE
Contact DICK RAYMER
RPState NC
TELEPHONE [phone]
IncidentNumber 36123 USTNum MO-7474
IncidentName RAYMER OIL COMPANY
FacilID
Address 1547 SALISBURY ROAD
CityTown STATESVILLE State NC
ZipCode 28687-
DateOccurred 6 /1 /2006
DateReported 7 /3 /2006
ConfRisk L
CloseOut 12/11/2006
COMMENT
NO PUBLIC NOTICE DOCUMENTATION
RptType Rcvd Rvwd Appvd
Incident Mgr RHTLongitude-80.852802 Latitude 35.768740
County IREDE
20DAY 8/10/2006 8/16/2006 8/16/2006
LSA1 10/18/2006 10/19/2006 10/19/2006
PN 1/26/2009
Tuesday, December 14, 2021 Page 1 of 1
NCDEQ Incident Report
RP/Company THE PANTRY, INC
RPAddress 305 GREGSON DRIVE
RPCity CARY
Contact BRENT PUZAK
RPState NC
TELEPHONE [phone]
IncidentNumber 40479 USTNum MO-8968
IncidentName PANTRY 3195/CIRCLE K #2723195
FacilID
Address 1542 SALISBURY HWY
CityTown STATESVILLE State NC
ZipCode 28677-
DateOccurred 5 /14/2015
DateReported 5 /14/2015
ConfRisk L
CloseOut 6/10/2019
COMMENT
ESA II SHOWED GW CONTAMINATION ON THE NEXT PROPERTY ADJACENT TO THE UST SYSTEM AT THIS SITE.
12/2018 FACILITY IS NOW CIRCLE K #2723195 REMOVING 5 - 10K TANKS. GW CONTAMIATION IS MIGRATING FROM
FAST PHILS #506.
RptType Rcvd Rvwd Appvd
Incident Mgr DSGLongitude-80.854006 Latitude 35.768439
County IREDE
LSA1 9/17/2015 9/28/2015
CSAM 10/7/2016 10/17/2016
report delayed by STF
CLO 3/1/2019 3/12/2019
SARL 5/24/2019 6/6/2019
MRP 5/24/2019 6/6/2019
Monday, October 16, 2023 Page 1 of 1
NCDEQ Incident Report
RP/Company FRANCO DISTRIBUTORS
RPAddress POB 1268
RPCity STATESVILLE
Contact FRANKIE CLOINGER
RPState NC
TELEPHONE [phone]
IncidentNumber 18537 USTNum MO-5342
IncidentName FRANCO DISTRIBUTORS
FacilID 00-0-0000010167
Address 1546 SALISBURY RD., STATESVILL
CityTown STATESVILLE State NC
ZipCode 28677-
DateOccurred 3 /23/1998
DateReported 4 /24/1998
ConfRisk L
CloseOut 12/23/2008
COMMENT
HIGH RISK (05/03/05) WSWS WITHIN 1,000 FT AND WSW ONSITE ACCORDING TO FILE--------------------------------- LSA
done on 12/23, closure issued.
RptType Rcvd Rvwd Appvd
Incident Mgr EFKLongitude-80.853402 Latitude 35.767409
County IREDE
LSA1 12/23/2008 12/23/2008
NFA action letter issued 12/23/2008
Monday, October 16, 2023 Page 1 of 1
NCDEQ Incident Report
RP/Company FRANCO DISTRIBUTORS, INC.
RPAddress PO BOX 1268
RPCity STATESVILLE
Contact FRANKIE CLONINGER
RPState NC
TELEPHONE [phone]
IncidentNumber 20090 USTNum MO-5703
IncidentName STROUDS SERVICE STATION
FacilID 00-0-0000010302
Address 1550 SALISBURY HIGHWAY
CityTown STATESVILLE State NC
ZipCode 28677-
DateOccurred 1 /20/1999
DateReported 3 /5 /1999
ConfRisk I
CloseOut
COMMENT
At one time this was a FP site, ass of June 2009 no FP in wells.
10/2010 - No FP in wells Some contamination may be coming from Fast Phil's across the street
RptType Rcvd Rvwd Appvd
Incident Mgr RCMLongitude-80.852965 Latitude 35.767963
County IREDE
LSA 10/2/2000 7/6/2001
FPRI 6/1/2009 6/26/2009 6/26/2009
No wells contained FP
FPRS 8/6/2010 8/9/2010 8/9/2010
RMR 7/5/2011 7/13/2011 7/25/2011
OTH 7/13/2016 7/14/2016
LETTER REPORT
Monday, October 16, 2023 Page 1 of 1

APPENDIX D
Well Permit, Well Construction Record, and Subsurface Log

North Carolina Department of Environmental Quality | Division of Water Resources
Mooresville Regional Office | 601 East Center Avenue, Suite 301 | Mooresville, NC 28115
704.663.1699
September 18, 2023

Ms. Kim Robertson (via email)
c/o Raymer Real Estate Operations, Inc.
P.O. Box 271
Statesville, NC 28677
RE: Monitoring Well Construction Permit
Permit # WM0301312
Fast Phil’s # 506
1542 Salisbury Hwy., Statesville
Iredell County

Dear Ms. Robertson,

In accordance with your completed application received on September 15, 2023, we are forwarding
herewith Monitoring Well Construction Permit Numbered WM0301312 and issued for the
construction of one (1) monitoring well located near the subject site in Statesville, Iredell County.

This Permit will be effective for one year from the date of issuance and shall be subject to the
conditions and limitations as specified therein.

Should you have any questions, please contact Edward Watson at [phone], or by
email at [e-mail].

Sincerely,

Andrew H. Pitner, P.G., Assistant Regional Supervisor
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources

CC: WQROS, Central Office (via Laserfiche)
Eric Eubanks, Geological Resources (via email)
Sam McKay Geological Resources (via email)

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES
PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL
In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws,
Rules and Regulations.
PERMISSION IS HEREBY GRANTED TO
Raymer Real Estate Operations, Inc. (Geological Resources, Inc as Agent)

FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of one (1) monitoring well owned by Raymer Real
Estate Operations, Inc. at the subject site located at 1542 Salisbury Hwy, Statesville, Iredell County. This Permit is issued
in accordance with the application received on September 16, 2023, in conformity with specifications and supporting data,
all of which are filed with the Department of Environmental Quality and are considered integral parts of this Permit.
This Permit is for well construction only, and does not waive any provision or requirement of any other applicable law or
regulation. Construction of any well under this Permit shall be in strict compliance with the North Carolina Well Construction
Regulations and Standards (15A NCAC 02C .0100), and other State and Local Laws and regulations pertaining to well
construction.

If any requirements or limitations specified in this Permit are unacceptable, you have a right to an adjudicatory hearing upon
written request within 30 days of receipt of this Permit. The request must be in the form of a written petition conforming to
Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service
Center, Raleigh, North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding.
This Permit will be effective for one year from the date of its issuance and shall be subject to other specified conditions,
limitations, or exceptions as follows:

1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these wells are being installed as
part of an investigation for contamination from an underground storage tank or dry cleaner incident.
2. Issuance of this Permit does not supersede any other agreement, permit, or requirement issued by another agency.
3. The well(s) shall be located and constructed as shown on the attachments submitted as part of the Permit application.
4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC 02C .0108(o).
5. Well construction records (GW-1) for each well shall be submitted to the Division of Water Resources’ Information
Processing Unit within 30 days of the well completion.
6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A NCAC 02C .0113 and a
well abandonment record (GW-30) shall be submitted to the Division of Water Resources’ Information Processing
Unit within 30 days of the well abandonment.
7. If the well penetrates any water-bearing zone that contains contaminated waters, the upper three feet of the well
shall be grouted within one day after the casing is set or the well abandoned.
8. Temporary wells must be permanently abandoned or converted to a permanent well within seven days (168 hours)
of completion of drilling the borehole.

Permit issued the 18th day of September 2023

FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION

_______________________________________________
Andrew H. Pitner, P.G., Regional Supervisor
Division of Water Resources
By Authority of the Environmental Management Commission
Permit No. # WM0301312
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Fast Phil's 506
4400
09/21/2023
Eric Eubanks
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-9
6"
30
Well installed at completion
0 0.5 Topsoil
0.5 1 Clayey silt with gravel Red Moist None
1 14 Clayey Silt Red Dry None
14 17 Silty Clay Red Moist Present
17 21 Silty Clay Red Wet Present
21 25 Silty Clay Reddish-brown Wet Present
25 30 Clay, some sand Reddish-brown Wet Present

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM -MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Fast Phil's 506
4400
09/21/2023
Eric Eubanks
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-9
6"
98.51
17.37
12 30
10 12
0 10
0
0 15 2
15 30 2
10
12
30
15
30
WELL CONSTRUCTION RECORD
This form canbe usedforsingle or multiple wells
FormGW-1 North Carolina Departmentof Environmentand Natural Resources –Division ofWaterResources Revised August 2013
1.Well Contractor Information:
Well ContractorName
NC WellContractor Certification Number
CompanyName
2.Well Construction Permit #:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3.Well Use (check well use):
Water Supply Well:□Agricultural □Municipal/Public□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)□Irrigation
Non-Water Supply Well:□Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier□Aquifer Test □StormwaterDrainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer□Geothermal (Heating/Cooling Return)□Other (explain under #21 Remarks)
4.Date Well(s)Completed:____________Well ID#______________________
5a.Well Location:
Facility/Owner Name Facility ID#(if applicable)

Physical Address,City,and Zip
County Parcel Identification No.(PIN)
5b.Latitudeand Longitudein degrees/minutes/secondsor decimal degrees:(if well field,one lat/long is sufficient)
N W
6.Is (are)the well(s):□Permanent or □Temporary
7.Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8.Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
9.Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below topof casing: (ft.)If water level is above casing, use “+”
11.Borehole diameter: (in.)
12.Well construction method: (i.e.auger,rotary,cable,direct push,etc.)
FOR WATER SUPPLY WELLS ONLY:
13a.Yield (gpm) Method oftest:
13b.Disinfection type: Amount:
14.WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15.OUTER CASING (for multi-cased wells)OR LINER(if applicable)FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16.INNER CASING OR TUBING(geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17.SCREENFROMTO DIAMETER SLOTSIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD &AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLING LOG (attach additional sheetsif necessary)FROM TO DESCRIPTION(color,hardness,soil/rock type,grain size,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS
22.Certification:
Signatureof Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23.Site diagram or additional well details:You may use the back of this page to provide additional well site details or wellconstructiondetails.You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a.For All Wells: Submit this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Information Processing Unit,1617 Mail Service Center,Raleigh,NC 27699-1617
24b.For Injection Wells ONLY:In addition to sending the form to the address in
24a above,also submit a copy of this form within 30 days of completion of wellconstructiontothefollowing:
Division of Water Resources,Underground Injection Control Program,1636 Mail Service Center,Raleigh,NC 27699-1636
24c.For Water Supply &Injection Wells:
Also submit one copy of this form within 30 days of completion ofwellconstructiontothecountyhealthdepartmentofthecountywhereconstructed.
For Internal UseONLY:
_______________
Matt Steele
4548-A
Geological Resources, Inc.
WM0301312
09/21/2023 MW-9
Fast Phil's 506 00-0-0000024533
1532 Salisbury Hwy, Statesville, 28677
Iredell 4743999614
35.76821302 80.85340558
1
30
17.37
6"
Solid Stem Auger
0
0 15 2 Sch 40 PVC
15 30 2 0.010 Sch 40 PVC
0 10 grout pour
10 12 bentonite pour
12 30 #2 Sand Pour
0 0.5 Topsoil
0.5 1 Clayey silt with gravel
1 14 Clayey Silt
14 17 Silty Clay
17 21 Silty Clay
21 25 Silty Clay
25 30 Clay, some sand
09/21/2023

APPENDIX E
Historical Soil Quality Information
Date: 07/21/17 Facility ID No. 0-024533
Sample ID UST System
Component
Date
Collected
(mm/dd/yy)
Sample
Depth
(feet)
50 100 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE 0.0056 4.3 4.9 4.6 0.091 0.16 4.3 1.7 1.7 8.5 8.3 0.004 3.6 68 540 31 540 NE 31
NE NE 18 1,200 1,560 3,129 350 313 626 1,564 626 782 782 20 63 939 1,500 469 1,500 31,000 469
SS-1 @ 4'Gasoline Piping 12/21/2016 4 <4.4 NR <0.0015 <0.0013 <0.0013 <0.0034 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-2 @ 4'Gasoline Dispenser 12/21/2016 4 <3.6 NR <0.0013 <0.0012 <0.0011 <0.0030 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-3 @ 4'Gasoline Dispenser 12/21/2016 4 <3.2 NR <0.0013 <0.0011 <0.0011 <0.0029 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-4 @ 4'Gasoline Dispenser 12/21/2016 4 <2.8 NR <0.0011 <0.00099 <0.00096 <0.0025 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-5 @ 4'Gasoline Dispenser 12/21/2016 4 <4.4 NR <0.0015 <0.0014 <0.0013 <0.0034 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-6 @ 4'Gasoline Piping/
Dispenser 12/21/2016 4 60.7 NR 0.0045 J <0.0012 0.0099 0.0579 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-7 @ 4'Gasoline Piping 12/21/2016 4 7.61 J NR 0.101 0.0421 0.0592 0.192 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-8 @ 4'Gasoline Piping 12/21/2016 4 <4.0 NR 0.0885 0.0023 J 0.0189 0.0066 J NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-9 @ 4'Gasoline Piping 12/21/2016 4 1,150 NR 0.242 0.0070 J 0.298 0.0257 J NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-10 @ 4'Gasoline Piping 12/21/2016 4 377 NR 0.123 0.0050 J 1.53 2.26 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-11 @ 4'Gasoline Piping 12/21/2016 4 18.4 NR 0.0463 0.0268 0.456 0.283 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-12 @ 4'Gasoline Piping 12/21/2016 4 <3.3 NR 0.0244 0.0076 0.0017 J 0.0114 J NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-13 @ 4'Kerosene Dispenser 12/21/2016 4 <3.9 5.11 J <0.0015 <0.0013 <0.0013 <0.0033 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-14 @ 4'Kerosene Piping 12/21/2016 4 <3.9 472 <0.0015 <0.0014 <0.0013 <0.0034 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-15 @ 4'Kerosene Piping 12/21/2016 4 <3.1 <3.1 <0.0012 <0.0010 <0.0010 <0.0026 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-16 @ 10'Kerosene UST 12/21/2016 10 <3.6 5.82 J <0.0015 <0.0013 <0.0013 <0.0034 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-17 @ 10'Kerosene UST 12/21/2016 10 <3.4 9.75 <0.0014 <0.0013 <0.0012 <0.0032 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-18 @ 13'Gasoline UST 12/21/2016 13 <4.0 NR <0.0015 <0.0014 <0.0013 <0.0035 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-19 @ 10'Kerosene UST 12/21/2016 10 <5.2 <3.7 <0.0019 <0.0017 <0.0017 <0.0043 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-20 @ 13'Gasoline UST 12/21/2016 13 <3.5 NR <0.0013 <0.0012 <0.0012 <0.0030 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-21 @ 15'Gasoline UST 12/21/2016 15 1,340 NR 3.74 26.1 16.5 75.9 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-22 @ 15'Gasoline UST 12/21/2016 15 7.16 J NR 0.0070 0.0035 J 0.154 0.274 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-23 @ 15'Gasoline UST 12/21/2016 15 <3.7 NR <0.0014 <0.0013 <0.0012 <0.0032 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-24 @ 15'Gasoline UST 12/21/2016 15 <3.8 NR 0.0026 J <0.0013 0.0080 0.0113 J NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-25 @ 4'Gasoline UST 12/21/2016 15 <4.0 NR <0.0015 <0.0013 <0.0013 <0.0034 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-26 @ 15'Gasoline UST 12/21/2016 15 <4.4 NR <0.0019 <0.0017 <0.0016 <0.0042 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SS-26 @ 4'Gasoline Piping 12/21/2016 4 <3.5 NR <0.0016 <0.0014 <0.0014 <0.0036 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
MW-1(10')Phase I LSA 03/06/2017 10 NR NR 0.215 2.96 1.50 7.87 7.15 2.65 0.0844 0.0875 0.661 4.93 1.68 1.27 1.84 <31 160 129 253 79.3 65.9
MW-1(15')Phase I LSA 03/06/2017 15 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 367 1,290 1,080 1,540 <34 188
MW-1(20')Phase I LSA 03/06/2017 20 NR NR 14.3 130 86.5 436 25.6 53.9 9.23 9.68 42.5 262 72.6 8.75 14.4 873 740 1,240 2,270 <67 327
Notes:
• Results reported in milligrams per kilograms (mg/kg).
• < : Less than the method detection limit specified in the laboratory report.
• RAL: Regulatory Action level.
• MCC: Maximum Contaminant Concentration level.
• Concentrations in bold face type exceed the RAL or Soil to water MCC.
• Concentrations in italic face type exceed the residential SCLs.
• NR: Not Requested.
• NE: Not Established.
• SCL: Soil Cleanup Level.
SW846 8270D
TABLE 6
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
FAST PHIL'S 506 (INCIDENT NO. 40687)
C9
-
C
1
8

A
l
i
p
h
a
t
i
c
s
C1
9
-
C
3
6

A
l
i
p
h
a
t
i
c
s
C1
1
-
C
2
2

A
r
o
m
a
t
i
c
s
MADEP VPH MADEP VPH
1-
M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
2-
M
e
t
h
y
l
n
a
p
h
t
h
a
l
e
n
e
C5
-
C
8

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
2

A
l
i
p
h
a
t
i
c
s
C9
-
C
1
0

A
r
o
m
a
t
i
c
s
n-
B
u
t
y
l
b
e
n
z
e
n
e
Is
o
p
r
o
p
y
l
b
e
n
z
e
n
e
n-
P
r
o
p
y
l
b
e
n
z
e
n
e
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
t
a
l

X
y
l
e
n
e
s
Analytical Method →SW846 8015C
Residential Soil Cleanup Levels (mg/kg)
RAL (mg/kg)
Soil to Water MCC (mg/kg)
Contaminant of Concern →
TP
H
-
G
R
O
Be
n
z
e
n
e
TP
H
-
D
R
O
SW846 8260B
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l
-
e
t
h
e
r

(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
Page 1 of 1

APPENDIX F
Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

8/24/2023
Geological Resources, Inc. Eric Eubanks
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-230-0052 Client Project Description: Fast Phil's #506
GRI #4400
Dear Eric Eubanks:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/18/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 17
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-230-0052
Page 2 of 17
Report Number:
Sample Summary Table
Client Project Description:
23-230-0052
Fast Phil's #506
GRI #4400
Lab No Client Sample ID Matrix Date Collected Date Received
08/14/2023 12:21Aqueous 92986 MW-1 08/18/2023 14:03
08/14/2023 11:43Aqueous 92987 MW-4 08/18/2023 14:03
08/14/2023 12:04Aqueous 92988 MW-5 08/18/2023 14:03
08/16/2023 12:20Aqueous 92989 MW-1 Change Out 08/18/2023 14:03
08/16/2023 12:00Aqueous 92990 MW-4 Change Out 08/18/2023 14:03
08/16/2023 12:10Aqueous 92991 MW-5 Change Out 08/18/2023 14:03
08/18/2023Aqueous 92992 Trip Blank 08/18/2023 14:03
Page 3 of 17
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-230-0052
Report Limit
Project:Fast Phil's #506
V 92986MW-1
4950 08/23/2023 05:406200BBenzeneµg/L 18.0
61.9 08/23/2023 05:406200BDi-Isopropyl Ether (DIPE)µg/L 50.0
1860 08/23/2023 05:406200BEthylbenzeneµg/L 17.0
1870 08/23/2023 05:406200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1220 08/23/2023 05:406200BNaphthaleneµg/L 47.0
2660 08/23/2023 05:406200BTolueneµg/L 22.0
1500 08/23/2023 05:406200Bo-Xylene µg/L 21.0
5310 08/23/2023 05:406200Bm,p-Xylene µg/L 42.0
6810 08/23/2023 05:406200BXylene (Total)µg/L 21.0
V 92987MW-4
23400 08/23/2023 20:566200BBenzeneµg/L 180
574 08/23/2023 06:056200BDi-Isopropyl Ether (DIPE)µg/L 50.0
3870 08/23/2023 06:056200BEthylbenzeneµg/L 17.0
21200 08/23/2023 20:566200BMethyl tert-butyl ether (MTBE)µg/L 140
848 08/23/2023 06:056200BNaphthaleneµg/L 47.0
36800 08/23/2023 20:566200BTolueneµg/L 220
6600 08/23/2023 06:056200Bo-Xylene µg/L 21.0
13300 08/23/2023 06:056200Bm,p-Xylene µg/L 42.0
19900 08/23/2023 06:056200BXylene (Total)µg/L 21.0
V 92988MW-5
6790 08/23/2023 06:306200BBenzeneµg/L 18.0
128 08/23/2023 06:306200BDi-Isopropyl Ether (DIPE)µg/L 50.0
3180 08/23/2023 06:306200BEthylbenzeneµg/L 17.0
882 08/23/2023 06:306200BMethyl tert-butyl ether (MTBE)µg/L 14.0
834 08/23/2023 06:306200BNaphthaleneµg/L 47.0
15500 08/23/2023 21:216200BTolueneµg/L 220
5060 08/23/2023 06:306200Bo-Xylene µg/L 21.0
10600 08/23/2023 06:306200Bm,p-Xylene µg/L 42.0
15700 08/23/2023 06:306200BXylene (Total)µg/L 21.0
V 92989MW-1 Change Out
2360 08/23/2023 06:556200BBenzeneµg/L 18.0
103 08/23/2023 06:556200BDi-Isopropyl Ether (DIPE)µg/L 50.0
1080 08/23/2023 06:556200BEthylbenzeneµg/L 17.0
6920 08/23/2023 06:556200BMethyl tert-butyl ether (MTBE)µg/L 14.0
898 08/23/2023 06:556200BNaphthaleneµg/L 47.0
Page 4 of 17
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-230-0052
Report Limit
Project:Fast Phil's #506
V 92989MW-1 Change Out
1550 08/23/2023 06:556200BTolueneµg/L 22.0
1310 08/23/2023 06:556200Bo-Xylene µg/L 21.0
3400 08/23/2023 06:556200Bm,p-Xylene µg/L 42.0
4710 08/23/2023 06:556200BXylene (Total)µg/L 21.0
V 92990MW-4 Change Out
18600 08/23/2023 21:466200BBenzeneµg/L 180
466 08/23/2023 07:206200BDi-Isopropyl Ether (DIPE)µg/L 50.0
5690 08/23/2023 07:206200BEthylbenzeneµg/L 17.0
18400 08/23/2023 21:466200BMethyl tert-butyl ether (MTBE)µg/L 140
1450 08/23/2023 07:206200BNaphthaleneµg/L 47.0
32800 08/23/2023 21:466200BTolueneµg/L 220
9020 08/23/2023 07:206200Bo-Xylene µg/L 21.0
19000 08/23/2023 07:206200Bm,p-Xylene µg/L 42.0
28000 08/23/2023 07:206200BXylene (Total)µg/L 21.0
V 92991MW-5 Change Out
6430 08/23/2023 07:446200BBenzeneµg/L 18.0
145 08/23/2023 07:446200BDi-Isopropyl Ether (DIPE)µg/L 50.0
3280 08/23/2023 07:446200BEthylbenzeneµg/L 17.0
1490 08/23/2023 07:446200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1000 08/23/2023 07:446200BNaphthaleneµg/L 47.0
13000 08/23/2023 22:116200BTolueneµg/L 220
5150 08/23/2023 07:446200Bo-Xylene µg/L 21.0
11000 08/23/2023 07:446200Bm,p-Xylene µg/L 42.0
16200 08/23/2023 07:446200BXylene (Total)µg/L 21.0
Page 5 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-230-0052
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 08/18/2023
Fast Phil's #506
Report Date : 08/24/2023
Sample ID :
Lab No :
Sampled:MW-1
92986 Matrix:
8/14/2023 12:21
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V36969 08/22/23 09:00
4950 µg/L 18.0 50.0Benzene 100 08/23/23 05:40 V36970MSA
61.9 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 08/23/23 05:40 V36970MSA
1860 µg/L 17.0 50.0Ethylbenzene 100 08/23/23 05:40 V36970MSA
1870 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 08/23/23 05:40 V36970MSA
1220 µg/L 47.0 100Naphthalene 100 08/23/23 05:40 V36970MSA
2660 µg/L 22.0 50.0Toluene 100 08/23/23 05:40 V36970MSA
1500 µg/L 21.0 50.0o-Xylene 100 08/23/23 05:40 V36970MSA
5310 µg/L 42.0 100m,p-Xylene 100 08/23/23 05:40 V36970MSA
6810 µg/L 21.0 50.0Xylene (Total)100 08/23/23 05:40 V36970
Surrogate: 4-Bromofluorobenzene 91.6 Limits: 70-130%08/23/23 05:40100 MSA V36970
Surrogate: Dibromofluoromethane 104 Limits: 70-130%08/23/23 05:40100 MSA V36970
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%08/23/23 05:40100 MSA V36970
Surrogate: Toluene-d8 116 Limits: 70-130%08/23/23 05:40100 MSA V36970
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 6 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-230-0052
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 08/18/2023
Fast Phil's #506
Report Date : 08/24/2023
Sample ID :
Lab No :
Sampled:MW-4
92987 Matrix:
8/14/2023 11:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V36969 08/22/23 09:00 V37037 08/23/23 09:00
23400 µg/L 180 500Benzene 1000 08/23/23 20:56 V37038MSA
574 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 08/23/23 06:05 V36970MSA
3870 µg/L 17.0 50.0Ethylbenzene 100 08/23/23 06:05 V36970MSA
21200 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 08/23/23 20:56 V37038MSA
848 µg/L 47.0 100Naphthalene 100 08/23/23 06:05 V36970MSA
36800 µg/L 220 500Toluene 1000 08/23/23 20:56 V37038MSA
6600 µg/L 21.0 50.0o-Xylene 100 08/23/23 06:05 V36970MSA
13300 µg/L 42.0 100m,p-Xylene 100 08/23/23 06:05 V36970MSA
19900 µg/L 21.0 50.0Xylene (Total)100 08/23/23 06:05 V36970
Surrogate: 4-Bromofluorobenzene 92.2 Limits: 70-130%08/23/23 06:05100 MSA V36970
Surrogate: Dibromofluoromethane 106 Limits: 70-130%08/23/23 06:05100 MSA V36970
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%08/23/23 06:05100 MSA V36970
Surrogate: Toluene-d8 113 Limits: 70-130%08/23/23 06:05100 MSA V36970
Surrogate: 4-Bromofluorobenzene 90.6 Limits: 70-130%08/23/23 20:561000 MSA V37038
Surrogate: Dibromofluoromethane 105 Limits: 70-130%08/23/23 20:561000 MSA V37038
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%08/23/23 20:561000 MSA V37038
Surrogate: Toluene-d8 116 Limits: 70-130%08/23/23 20:561000 MSA V37038
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 7 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-230-0052
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 08/18/2023
Fast Phil's #506
Report Date : 08/24/2023
Sample ID :
Lab No :
Sampled:MW-5
92988 Matrix:
8/14/2023 12:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V36969 08/22/23 09:00 V37037 08/23/23 09:00
6790 µg/L 18.0 50.0Benzene 100 08/23/23 06:30 V36970MSA
128 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 08/23/23 06:30 V36970MSA
3180 µg/L 17.0 50.0Ethylbenzene 100 08/23/23 06:30 V36970MSA
882 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 08/23/23 06:30 V36970MSA
834 µg/L 47.0 100Naphthalene 100 08/23/23 06:30 V36970MSA
15500 µg/L 220 500Toluene 1000 08/23/23 21:21 V37038MSA
5060 µg/L 21.0 50.0o-Xylene 100 08/23/23 06:30 V36970MSA
10600 µg/L 42.0 100m,p-Xylene 100 08/23/23 06:30 V36970MSA
15700 µg/L 21.0 50.0Xylene (Total)100 08/23/23 06:30 V36970
Surrogate: 4-Bromofluorobenzene 92.4 Limits: 70-130%08/23/23 06:30100 MSA V36970
Surrogate: Dibromofluoromethane 104 Limits: 70-130%08/23/23 06:30100 MSA V36970
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%08/23/23 06:30100 MSA V36970
Surrogate: Toluene-d8 116 Limits: 70-130%08/23/23 06:30100 MSA V36970
Surrogate: 4-Bromofluorobenzene 91.2 Limits: 70-130%08/23/23 21:211000 MSA V37038
Surrogate: Dibromofluoromethane 106 Limits: 70-130%08/23/23 21:211000 MSA V37038
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%08/23/23 21:211000 MSA V37038
Surrogate: Toluene-d8 114 Limits: 70-130%08/23/23 21:211000 MSA V37038
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 8 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-230-0052
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 08/18/2023
Fast Phil's #506
Report Date : 08/24/2023
Sample ID :
Lab No :
Sampled:MW-1 Change Out
92989 Matrix:
8/16/2023 12:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V36969 08/22/23 09:00
2360 µg/L 18.0 50.0Benzene 100 08/23/23 06:55 V36970MSA
103 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 08/23/23 06:55 V36970MSA
1080 µg/L 17.0 50.0Ethylbenzene 100 08/23/23 06:55 V36970MSA
6920 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 08/23/23 06:55 V36970MSA
898 µg/L 47.0 100Naphthalene 100 08/23/23 06:55 V36970MSA
1550 µg/L 22.0 50.0Toluene 100 08/23/23 06:55 V36970MSA
1310 µg/L 21.0 50.0o-Xylene 100 08/23/23 06:55 V36970MSA
3400 µg/L 42.0 100m,p-Xylene 100 08/23/23 06:55 V36970MSA
4710 µg/L 21.0 50.0Xylene (Total)100 08/23/23 06:55 V36970
Surrogate: 4-Bromofluorobenzene 88.4 Limits: 70-130%08/23/23 06:55100 MSA V36970
Surrogate: Dibromofluoromethane 104 Limits: 70-130%08/23/23 06:55100 MSA V36970
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%08/23/23 06:55100 MSA V36970
Surrogate: Toluene-d8 116 Limits: 70-130%08/23/23 06:55100 MSA V36970
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 9 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-230-0052
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 08/18/2023
Fast Phil's #506
Report Date : 08/24/2023
Sample ID :
Lab No :
Sampled:MW-4 Change Out
92990 Matrix:
8/16/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V36969 08/22/23 09:00 V37037 08/23/23 09:00
18600 µg/L 180 500Benzene 1000 08/23/23 21:46 V37038MSA
466 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 08/23/23 07:20 V36970MSA
5690 µg/L 17.0 50.0Ethylbenzene 100 08/23/23 07:20 V36970MSA
18400 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 08/23/23 21:46 V37038MSA
1450 µg/L 47.0 100Naphthalene 100 08/23/23 07:20 V36970MSA
32800 µg/L 220 500Toluene 1000 08/23/23 21:46 V37038MSA
9020 µg/L 21.0 50.0o-Xylene 100 08/23/23 07:20 V36970MSA
19000 µg/L 42.0 100m,p-Xylene 100 08/23/23 07:20 V36970MSA
28000 µg/L 21.0 50.0Xylene (Total)100 08/23/23 07:20 V36970
Surrogate: 4-Bromofluorobenzene 92.4 Limits: 70-130%08/23/23 07:20100 MSA V36970
Surrogate: Dibromofluoromethane 105 Limits: 70-130%08/23/23 07:20100 MSA V36970
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%08/23/23 07:20100 MSA V36970
Surrogate: Toluene-d8 112 Limits: 70-130%08/23/23 07:20100 MSA V36970
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%08/23/23 21:461000 MSA V37038
Surrogate: Dibromofluoromethane 103 Limits: 70-130%08/23/23 21:461000 MSA V37038
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%08/23/23 21:461000 MSA V37038
Surrogate: Toluene-d8 115 Limits: 70-130%08/23/23 21:461000 MSA V37038
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 10 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-230-0052
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 08/18/2023
Fast Phil's #506
Report Date : 08/24/2023
Sample ID :
Lab No :
Sampled:MW-5 Change Out
92991 Matrix:
8/16/2023 12:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V36969 08/22/23 09:00 V37037 08/23/23 09:00
6430 µg/L 18.0 50.0Benzene 100 08/23/23 07:44 V36970MSA
145 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 08/23/23 07:44 V36970MSA
3280 µg/L 17.0 50.0Ethylbenzene 100 08/23/23 07:44 V36970MSA
1490 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 08/23/23 07:44 V36970MSA
1000 µg/L 47.0 100Naphthalene 100 08/23/23 07:44 V36970MSA
13000 µg/L 220 500Toluene 1000 08/23/23 22:11 V37038MSA
5150 µg/L 21.0 50.0o-Xylene 100 08/23/23 07:44 V36970MSA
11000 µg/L 42.0 100m,p-Xylene 100 08/23/23 07:44 V36970MSA
16200 µg/L 21.0 50.0Xylene (Total)100 08/23/23 07:44 V36970
Surrogate: 4-Bromofluorobenzene 91.2 Limits: 70-130%08/23/23 07:44100 MSA V36970
Surrogate: Dibromofluoromethane 106 Limits: 70-130%08/23/23 07:44100 MSA V36970
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%08/23/23 07:44100 MSA V36970
Surrogate: Toluene-d8 116 Limits: 70-130%08/23/23 07:44100 MSA V36970
Surrogate: 4-Bromofluorobenzene 89.0 Limits: 70-130%08/23/23 22:111000 MSA V37038
Surrogate: Dibromofluoromethane 106 Limits: 70-130%08/23/23 22:111000 MSA V37038
Surrogate: 1,2-Dichloroethane - d4 109 Limits: 70-130%08/23/23 22:111000 MSA V37038
Surrogate: Toluene-d8 112 Limits: 70-130%08/23/23 22:111000 MSA V37038
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 11 of 17
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-230-0052
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 08/18/2023
Fast Phil's #506
Report Date : 08/24/2023
Sample ID :
Lab No :
Sampled:Trip Blank
92992 Matrix:
8/18/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V36969 08/22/23 09:00
<0.180 µg/L 0.180 0.500Benzene 1 08/23/23 01:07 V36970MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 08/23/23 01:07 V36970MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 08/23/23 01:07 V36970MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 08/23/23 01:07 V36970MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 08/23/23 01:07 V36970MSA
<0.220 µg/L 0.220 0.500Toluene 1 08/23/23 01:07 V36970MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 08/23/23 01:07 V36970MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 08/23/23 01:07 V36970MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 08/23/23 01:07 V36970
Surrogate: 4-Bromofluorobenzene 93.6 Limits: 70-130%08/23/23 01:071 MSA V36970
Surrogate: Dibromofluoromethane 104 Limits: 70-130%08/23/23 01:071 MSA V36970
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%08/23/23 01:071 MSA V36970
Surrogate: Toluene-d8 116 Limits: 70-130%08/23/23 01:071 MSA V36970
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 12 of 17
Quality Control Data
23-230-0052Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V36970QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V36969
Associated Lab Samples: 92986, 92987, 92988, 92989, 92990, 92991, 92992
LRB-V36969 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/23/23 00:430.5000.180<0.180µg/LBenzene
08/23/23 00:430.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
08/23/23 00:430.5000.170<0.170µg/LEthylbenzene
08/23/23 00:431.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
08/23/23 00:431.000.470<0.470µg/LNaphthalene
08/23/23 00:430.5000.220<0.220µg/LToluene
08/23/23 00:430.5000.210<0.210µg/Lo-Xylene
08/23/23 00:431.000.420<0.420µg/Lm,p-Xylene
08/23/23 00:434-Bromofluorobenzene (S)94.0 70-130
08/23/23 00:43Dibromofluoromethane (S)105 70-130
08/23/23 00:431,2-Dichloroethane - d4 (S)102 70-130
08/23/23 00:43Toluene-d8 (S)116 70-130
LCS-V36969 LCSD-V36969Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.6 98.096.019.220.0µg/LBenzene 70-130 2.0 20.0
19.0 95.098.019.620.0µg/LDi-Isopropyl Ether (DIPE)70-130 3.1 20.0
21.0 10510821.620.0µg/LEthylbenzene 70-130 2.8 20.0
18.8 94.094.518.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.5 20.0
24.8 12412224.420.0µg/LNaphthalene 70-130 1.6 20.0
15.7 78.578.015.620.0µg/LToluene 70-130 0.6 20.0
21.8 10910921.820.0µg/Lo-Xylene 70-130 0.0 20.0
45.1 11311345.140.0µg/Lm,p-Xylene 70-130 0.0 20.0
90.290.44-Bromofluorobenzene (S)70-130
103105Dibromofluoromethane (S)70-130
Page 1 of 3Date:08/24/2023 04:19 PM
Page 13 of 17
Quality Control Data
23-230-0052Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V36970QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V36969
LCS-V36969 LCSD-V36969Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1021031,2-Dichloroethane - d4 (S)70-130
115118Toluene-d8 (S)70-130
Page 2 of 3Date:08/24/2023 04:19 PM
Page 14 of 17
Quality Control Data
23-230-0052Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37038QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37037
Associated Lab Samples: 92987, 92988, 92990, 92991
LRB-V37037 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/23/23 13:300.5000.180<0.180µg/LBenzene
08/23/23 13:301.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
08/23/23 13:300.5000.220<0.220µg/LToluene
08/23/23 13:304-Bromofluorobenzene (S)91.2 70-130
08/23/23 13:30Dibromofluoromethane (S)105 70-130
08/23/23 13:301,2-Dichloroethane - d4 (S)102 70-130
08/23/23 13:30Toluene-d8 (S)114 70-130
LCS-V37037 LCSD-V37037Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.1 95.596.519.320.0µg/LBenzene 70-130 1.0 20.0
19.0 95.097.519.520.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.5 20.0
15.2 76.077.015.420.0µg/LToluene 70-130 1.3 20.0
92.091.04-Bromofluorobenzene (S)70-130
104105Dibromofluoromethane (S)70-130
1041061,2-Dichloroethane - d4 (S)70-130
116115Toluene-d8 (S)70-130
Page 3 of 3Date:08/24/2023 04:19 PM
Page 15 of 17
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-230-0052
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Caitlyn Cummins Date & Time:08/18/2023 14:36:57
Special precautions or instructions included?
Comments:
Page 16 of 17
Pa
g
e

1
7

o
f

1
7

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/3/2023
Geological Resources, Inc. Eric Eubanks
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-265-0014 Client Project Description: Fast Phil's #506
GRI #4400
Dear Eric Eubanks:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/22/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 101
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-265-0014
Page 2 of 101
Report Number:
Sample Summary Table
Client Project Description:
23-265-0014
Fast Phil's #506
GRI #4400
Lab No Client Sample ID Matrix Date Collected Date Received
09/21/2023 17:20Aqueous 96054 MW-1 09/22/2023 11:40
09/21/2023 16:26Aqueous 96055 MW-2 09/22/2023 11:40
09/21/2023 17:20Aqueous 96056 MW-3 09/22/2023 11:40
09/21/2023 16:45Aqueous 96057 MW-4 09/22/2023 11:40
09/21/2023 16:26Aqueous 96058 MW-5 09/22/2023 11:40
09/21/2023 16:58Aqueous 96059 MW-6 09/22/2023 11:40
09/21/2023 15:58Aqueous 96060 MW-7 09/22/2023 11:40
09/21/2023 16:09Aqueous 96061 MW-8 09/22/2023 11:40
09/21/2023 15:15Aqueous 96062 MW-9 09/22/2023 11:40
09/21/2023 15:35Aqueous 96063 PMW-2 09/22/2023 11:40
09/21/2023 16:12Aqueous 96064 PMW-7 09/22/2023 11:40
09/21/2023 15:55Aqueous 96065 PMW-8 09/22/2023 11:40
09/21/2023 17:09Aqueous 96066 TW-1 09/22/2023 11:40
09/21/2023 12:00Aqueous 96067 TB 09/22/2023 11:40
Page 3 of 101
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0014
Report Limit
Project:Fast Phil's #506
V 96054MW-1
5660 09/28/2023 08:536200BBenzeneµg/L 18.0
J28.0 09/28/2023 08:536200Bn-Butylbenzene µg/L 18.0
J23.3 09/28/2023 08:536200Bsec-Butyl benzene µg/L 20.0
M66.6 09/28/2023 08:536200BDi-Isopropyl Ether (DIPE)µg/L 50.0
1650 09/28/2023 08:536200BEthylbenzeneµg/L 17.0
88.2 09/28/2023 08:536200BIsopropylbenzeneµg/L 18.0
2950 09/28/2023 08:536200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1300 09/28/2023 08:536200BNaphthaleneµg/L 47.0
175 09/28/2023 08:536200Bn-Propylbenzene µg/L 19.0
2190 09/28/2023 08:536200BTolueneµg/L 22.0
1330 09/28/2023 08:536200B1,2,4-Trimethylbenzene µg/L 19.0
361 09/28/2023 08:536200B1,3,5-Trimethylbenzene µg/L 18.0
975 09/28/2023 08:536200Bo-Xylene µg/L 21.0
4450 09/28/2023 08:536200Bm,p-Xylene µg/L 42.0
5430 09/28/2023 08:536200BXylene (Total)µg/L 21.0
V 96055MW-2
3.36 09/28/2023 05:356200BMethyl tert-butyl ether (MTBE)µg/L 0.140
V 96056MW-3
26.4 09/28/2023 06:006200BMethyl tert-butyl ether (MTBE)µg/L 0.140
V 96057MW-4
2380 09/28/2023 09:186200BAcetoneµg/L 180
17000 09/28/2023 23:056200BBenzeneµg/L 180
J36.9 09/28/2023 09:186200Bn-Butylbenzene µg/L 18.0
J30.4 09/28/2023 09:186200Bsec-Butyl benzene µg/L 20.0
M28509/28/2023 09:186200BDi-Isopropyl Ether (DIPE)µg/L 50.0
3830 09/28/2023 09:186200BEthylbenzeneµg/L 17.0
499 09/28/2023 09:186200B2-Hexanone µg/L 38.0
174 09/28/2023 09:186200BIsopropylbenzeneµg/L 18.0
2030 09/28/2023 09:186200BMethyl Ethyl Ketone (MEK)µg/L 71.0
14100 09/28/2023 23:056200BMethyl tert-butyl ether (MTBE)µg/L 140
354 09/28/2023 09:186200B4-Methyl-2-Pentanone µg/L 7.80
1030 09/28/2023 09:186200BNaphthaleneµg/L 47.0
433 09/28/2023 09:186200Bn-Propylbenzene µg/L 19.0
41700 09/28/2023 23:056200BTolueneµg/L 220
3290 09/28/2023 09:186200B1,2,4-Trimethylbenzene µg/L 19.0
Page 4 of 101
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0014
Report Limit
Project:Fast Phil's #506
V 96057MW-4
771 09/28/2023 09:186200B1,3,5-Trimethylbenzene µg/L 18.0
6300 09/28/2023 09:186200Bo-Xylene µg/L 21.0
13700 09/28/2023 09:186200Bm,p-Xylene µg/L 42.0
20000 09/28/2023 09:186200BXylene (Total)µg/L 21.0
V 96058MW-5
J57509/28/2023 09:426200BAcetoneµg/L 180
4580 09/28/2023 09:426200BBenzeneµg/L 18.0
87.3 09/28/2023 09:426200Bn-Butylbenzene µg/L 18.0
71.2 09/28/2023 09:426200Bsec-Butyl benzene µg/L 20.0
M61.9 09/28/2023 09:426200BDi-Isopropyl Ether (DIPE)µg/L 50.0
J26.8 09/28/2023 09:426200B1,1-Dichloroethene µg/L 15.0
2900 09/28/2023 09:426200BEthylbenzeneµg/L 17.0
469 09/28/2023 09:426200B2-Hexanone µg/L 38.0
208 09/28/2023 09:426200BIsopropylbenzeneµg/L 18.0
J36.3 09/28/2023 09:426200B4-Isopropyl toluene µg/L 8.90
831 09/28/2023 09:426200BMethyl Ethyl Ketone (MEK)µg/L 71.0
712 09/28/2023 09:426200BMethyl tert-butyl ether (MTBE)µg/L 14.0
1090 09/28/2023 09:426200BNaphthaleneµg/L 47.0
516 09/28/2023 09:426200Bn-Propylbenzene µg/L 19.0
14400 09/28/2023 23:306200BTolueneµg/L 220
3510 09/28/2023 09:426200B1,2,4-Trimethylbenzene µg/L 19.0
844 09/28/2023 09:426200B1,3,5-Trimethylbenzene µg/L 18.0
4500 09/28/2023 09:426200Bo-Xylene µg/L 21.0
10300 09/28/2023 09:426200Bm,p-Xylene µg/L 42.0
14800 09/28/2023 09:426200BXylene (Total)µg/L 21.0
V 96059MW-6
41.1 09/28/2023 06:256200BBenzeneµg/L 0.180
2.95 09/28/2023 06:256200Bn-Butylbenzene µg/L 0.180
4.95 09/28/2023 06:256200Bsec-Butyl benzene µg/L 0.200
1.04 09/28/2023 06:256200BEthylbenzeneµg/L 0.170
10.6 09/28/2023 06:256200BIsopropylbenzeneµg/L 0.180
4.71 09/28/2023 06:256200B4-Isopropyl toluene µg/L 0.089
8.58 09/28/2023 06:256200BMethyl tert-butyl ether (MTBE)µg/L 0.140
176 09/28/2023 21:026200BNaphthaleneµg/L 4.70
3.47 09/28/2023 06:256200Bn-Propylbenzene µg/L 0.190
0.516 09/28/2023 06:256200BTolueneµg/L 0.220
Page 5 of 101
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0014
Report Limit
Project:Fast Phil's #506
V 96059MW-6
122 09/28/2023 21:026200B1,2,4-Trimethylbenzene µg/L 1.90
9.40 09/28/2023 06:256200B1,3,5-Trimethylbenzene µg/L 0.180
30.3 09/28/2023 06:256200Bo-Xylene µg/L 0.210
47.3 09/28/2023 06:256200Bm,p-Xylene µg/L 0.420
77.6 09/28/2023 06:256200BXylene (Total)µg/L 0.210
V 96060MW-7
4.66 09/28/2023 06:506200B1,1-Dichloroethane µg/L 0.240
44.0 09/28/2023 06:506200BMethyl tert-butyl ether (MTBE)µg/L 0.140
38.5 09/28/2023 06:506200BNaphthaleneµg/L 0.470
J0.439 09/28/2023 06:506200B1,2,4-Trimethylbenzene µg/L 0.190
V 96061MW-8
58.5 09/28/2023 07:146200BBenzeneµg/L 0.180
19.3 09/28/2023 07:146200Bn-Butylbenzene µg/L 0.180
14.4 09/28/2023 07:146200Bsec-Butyl benzene µg/L 0.200
3.01 09/28/2023 07:146200Btert-Butyl benzene µg/L 0.920
M0.603 09/28/2023 07:146200BDi-Isopropyl Ether (DIPE)µg/L 0.500
8.56 09/28/2023 07:146200B1,1-Dichloroethane µg/L 0.240
29.4 09/28/2023 07:146200B1,1-Dichloroethene µg/L 0.150
299 09/28/2023 21:266200BEthylbenzeneµg/L 1.70
75.0 09/28/2023 07:146200BIsopropylbenzeneµg/L 0.180
9.81 09/28/2023 07:146200B4-Isopropyl toluene µg/L 0.089
6.48 09/28/2023 07:146200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J0.453 09/28/2023 07:146200BMethylene Chloride µg/L 0.330
222 09/28/2023 21:266200BNaphthaleneµg/L 4.70
97.5 09/28/2023 07:146200Bn-Propylbenzene µg/L 0.190
171 09/28/2023 21:266200BTolueneµg/L 2.20
1300 10/02/2023 23:586200B1,2,4-Trimethylbenzene µg/L 19.0
170 09/28/2023 21:266200B1,3,5-Trimethylbenzene µg/L 1.80
553 09/28/2023 21:266200Bo-Xylene µg/L 2.10
1320 09/28/2023 21:266200Bm,p-Xylene µg/L 4.20
1870 09/28/2023 21:266200BXylene (Total)µg/L 2.10
V 96062MW-9
0.085 09/27/2023 00:416010DLeadmg/L 0.002
2490 09/28/2023 10:076200BAcetoneµg/L 180
29900 09/28/2023 23:556200BBenzeneµg/L 180
Page 6 of 101
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0014
Report Limit
Project:Fast Phil's #506
V 96062MW-9
J30.9 09/28/2023 10:076200Bn-Butylbenzene µg/L 18.0
J21.2 09/28/2023 10:076200Bsec-Butyl benzene µg/L 20.0
M66009/28/2023 10:076200BDi-Isopropyl Ether (DIPE)µg/L 50.0
4160 09/28/2023 10:076200BEthylbenzeneµg/L 17.0
211 09/28/2023 10:076200B2-Hexanone µg/L 38.0
197 09/28/2023 10:076200BIsopropylbenzeneµg/L 18.0
1560 09/28/2023 10:076200BMethyl Ethyl Ketone (MEK)µg/L 71.0
62700 09/28/2023 23:556200BMethyl tert-butyl ether (MTBE)µg/L 140
727 09/28/2023 10:076200BNaphthaleneµg/L 47.0
407 09/28/2023 10:076200Bn-Propylbenzene µg/L 19.0
62300 09/28/2023 23:556200BTolueneµg/L 220
3140 09/28/2023 10:076200B1,2,4-Trimethylbenzene µg/L 19.0
753 09/28/2023 10:076200B1,3,5-Trimethylbenzene µg/L 18.0
7070 09/28/2023 10:076200Bo-Xylene µg/L 21.0
14900 09/28/2023 10:076200Bm,p-Xylene µg/L 42.0
22000 09/28/2023 10:076200BXylene (Total)µg/L 21.0
49.2 09/28/2023 12:13625.1 Benzyl alcohol µg/L 0.735
50.8 09/28/2023 12:13625.1 1-Methylnaphthalene µg/L 1.23
91.4 09/28/2023 12:13625.1 2-Methylnaphthalene µg/L 0.715
306 09/28/2023 16:43625.1 Naphthalene µg/L 1.57
69800 09/26/2023 11:16CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 11500
14600 09/26/2023 03:29CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 2580
7020 09/26/2023 03:29CALCULATIONAromatic C9-C10 (Adjusted)µg/L 402
470 09/28/2023 12:13CALCULATIONAromatic C11-C22 (Adjusted)µg/L 61.2
23.8 09/26/2023 15:53EPA-504.1 1,2-Dibromoethane µg/L 0.173
J18609/30/2023 19:03MADEP-EPH Aliphatic C9-C18 µg/L 28.2
776 09/30/2023 19:03MADEP-EPH Aromatic C11-C22 µg/L 61.2
162000 09/26/2023 11:16MADEP-VPH Aliphatic C5-C8 µg/L 11500
47700 09/26/2023 03:29MADEP-VPH Aliphatic C9-C12 µg/L 2580
7020 09/26/2023 03:29MADEP-VPH Aromatic C9-C10 µg/L 402
V 96063PMW-2
J49109/28/2023 10:326200BAcetoneµg/L 180
6880 09/28/2023 10:326200BBenzeneµg/L 18.0
J33.4 09/28/2023 10:326200Bn-Butylbenzene µg/L 18.0
M94.0 09/28/2023 10:326200BDi-Isopropyl Ether (DIPE)µg/L 50.0
3030 09/28/2023 10:326200BEthylbenzeneµg/L 17.0
Page 7 of 101
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0014
Report Limit
Project:Fast Phil's #506
V 96063PMW-2
103 09/28/2023 10:326200B2-Hexanone µg/L 38.0
131 09/28/2023 10:326200BIsopropylbenzeneµg/L 18.0
J21.7 09/28/2023 10:326200B4-Isopropyl toluene µg/L 8.90
5460 09/28/2023 10:326200BMethyl tert-butyl ether (MTBE)µg/L 14.0
938 09/28/2023 10:326200BNaphthaleneµg/L 47.0
332 09/28/2023 10:326200Bn-Propylbenzene µg/L 19.0
J34.0 09/28/2023 10:326200BStyreneµg/L 22.0
5800 09/28/2023 10:326200BTolueneµg/L 22.0
2620 09/28/2023 10:326200B1,2,4-Trimethylbenzene µg/L 19.0
674 09/28/2023 10:326200B1,3,5-Trimethylbenzene µg/L 18.0
4010 09/28/2023 10:326200Bo-Xylene µg/L 21.0
6390 09/28/2023 10:326200Bm,p-Xylene µg/L 42.0
10400 09/28/2023 10:326200BXylene (Total)µg/L 21.0
V 96064PMW-7
347 09/28/2023 08:036200BBenzeneµg/L 1.80
8.27 09/28/2023 08:036200Bn-Butylbenzene µg/L 1.80
10.4 09/28/2023 08:036200Bsec-Butyl benzene µg/L 2.00
M7.70 09/28/2023 08:036200BDi-Isopropyl Ether (DIPE)µg/L 5.00
204 09/28/2023 08:036200BEthylbenzeneµg/L 1.70
37.2 09/28/2023 08:036200BIsopropylbenzeneµg/L 1.80
12.1 09/28/2023 08:036200B4-Isopropyl toluene µg/L 0.890
399 09/28/2023 08:036200BMethyl tert-butyl ether (MTBE)µg/L 1.40
615 09/28/2023 08:036200BNaphthaleneµg/L 4.70
49.6 09/28/2023 08:036200Bn-Propylbenzene µg/L 1.90
9.96 09/28/2023 08:036200BTolueneµg/L 2.20
680 09/28/2023 08:036200B1,2,4-Trimethylbenzene µg/L 1.90
152 09/28/2023 08:036200B1,3,5-Trimethylbenzene µg/L 1.80
553 09/28/2023 08:036200Bo-Xylene µg/L 2.10
639 09/28/2023 08:036200Bm,p-Xylene µg/L 4.20
1190 09/28/2023 08:036200BXylene (Total)µg/L 2.10
V 96065PMW-8
1790 09/28/2023 10:576200BBenzeneµg/L 18.0
J23.0 09/28/2023 10:576200Bn-Butylbenzene µg/L 18.0
820 09/28/2023 10:576200BEthylbenzeneµg/L 17.0
62.9 09/28/2023 10:576200BIsopropylbenzeneµg/L 18.0
J22.2 09/28/2023 10:576200B4-Isopropyl toluene µg/L 8.90
Page 8 of 101
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-265-0014
Report Limit
Project:Fast Phil's #506
V 96065PMW-8
218 09/28/2023 10:576200BMethyl tert-butyl ether (MTBE)µg/L 14.0
826 09/28/2023 10:576200BNaphthaleneµg/L 47.0
102 09/28/2023 10:576200Bn-Propylbenzene µg/L 19.0
J43.7 09/28/2023 10:576200BTolueneµg/L 22.0
122 09/28/2023 10:576200B1,2,4-Trimethylbenzene µg/L 19.0
80.5 09/28/2023 10:576200B1,3,5-Trimethylbenzene µg/L 18.0
J26.7 09/28/2023 10:576200Bo-Xylene µg/L 21.0
140 09/28/2023 10:576200Bm,p-Xylene µg/L 42.0
J16709/28/2023 10:576200BXylene (Total)µg/L 21.0
V 96066TW-1
6.94 09/28/2023 16:556200B1,2-Dichloroethane µg/L 0.150
0.520 09/28/2023 16:556200B1,2-Dichloropropane µg/L 0.190
J0.578 09/28/2023 16:556200BMethyl tert-butyl ether (MTBE)µg/L 0.140
0.590 09/28/2023 16:556200BTetrachloroetheneµg/L 0.220
Page 9 of 101

Client: Geological Resources, Inc. CASE NARRATIVE Project: Fast Phil's #506
Lab Report Number: 23-265-0014 Date: 10/3/2023
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1 Analyte: Benzidine
QC Batch No: V38427/V38382 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Benzoic Acid
QC Batch No: V38427/V38382 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 1,2,3-Trichlorobenzene QC Batch No: V38465/V38464
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 1,2,3-Trichlorobenzene QC Batch No: V38531/V38464
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable. Analyte: 1,2,3-Trichlorobenzene QC Batch No: V38609/V38464
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 1,2,4-Trichlorobenzene QC Batch No: V38465/V38464 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 1,2,4-Trichlorobenzene QC Batch No: V38531/V38464 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: 1,2-Dichloropropane QC Batch No: V38465/V38464 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Page 10 of 101

Analyte: Bromomethane
QC Batch No: V38609/V38464 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Carbon Tetrachloride
QC Batch No: V38531/V38464 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Chloromethane
QC Batch No: V38531/V38464 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Analyte: Di isopropyl ether
QC Batch No: V38465/V38464 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Di isopropyl ether
QC Batch No: V38531/V38464 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Dichlorodifluoromethane QC Batch No: V38465/V38464 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Analyte: Dichlorodifluoromethane QC Batch No: V38531/V38464 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Analyte: Ethanol QC Batch No: V38531/V38464 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Hexachlorobutadiene QC Batch No: V38531/V38464 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Page 11 of 101

Analyte: Vinyl chloride QC Batch No: V38465/V38464
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Vinyl chloride QC Batch No: V38531/V38464
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.

Page 12 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-1
96054 Matrix:
9/21/2023 17:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<180 µg/L 180 1000Acetone 100 09/28/23 08:53 V38465MSA
5660 µg/L 18.0 50.0Benzene 100 09/28/23 08:53 V38465MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/28/23 08:53 V38465MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/28/23 08:53 V38465MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/28/23 08:53 V38465MSA
<150 µg/L 150 500Bromoform 100 09/28/23 08:53 V38465MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/28/23 08:53 V38465MSA
28.0 J µg/L 18.0 50.0n-Butylbenzene 100 09/28/23 08:53 V38465MSA
23.3 J µg/L 20.0 50.0sec-Butyl benzene 100 09/28/23 08:53 V38465MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/28/23 08:53 V38465MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/28/23 08:53 V38465MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/28/23 08:53 V38465MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/28/23 08:53 V38465MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/28/23 08:53 V38465MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/28/23 08:53 V38465MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 09/28/23 08:53 V38465MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/28/23 08:53 V38465MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/28/23 08:53 V38465MSA
66.6 M µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/28/23 08:53 V38465MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/28/23 08:53 V38465MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/28/23 08:53 V38465MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/28/23 08:53 V38465MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/28/23 08:53 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 13 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-1
96054 Matrix:
9/21/2023 17:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/28/23 08:53 V38465MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 09/28/23 08:53 V38465MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/28/23 08:53 V38465MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/28/23 08:53 V38465MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/28/23 08:53 V38465MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/28/23 08:53 V38465MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/28/23 08:53 V38465MSA
<19.0 M µg/L 19.0 50.01,2-Dichloropropane 100 09/28/23 08:53 V38465MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/28/23 08:53 V38465MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/28/23 08:53 V38465MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/28/23 08:53 V38465MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/28/23 08:53 V38465MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/28/23 08:53 V38465MSA
<4200 µg/L 4200 20000Ethanol 100 09/28/23 08:53 V38465MSA
1650 µg/L 17.0 50.0Ethylbenzene 100 09/28/23 08:53 V38465MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/28/23 08:53 V38465MSA
<38.0 µg/L 38.0 1002-Hexanone 100 09/28/23 08:53 V38465MSA
88.2 µg/L 18.0 50.0Isopropylbenzene 100 09/28/23 08:53 V38465MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/28/23 08:53 V38465MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/28/23 08:53 V38465MSA
2950 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/28/23 08:53 V38465MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/28/23 08:53 V38465MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 09/28/23 08:53 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 14 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-1
96054 Matrix:
9/21/2023 17:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
1300 µg/L 47.0 100Naphthalene 100 09/28/23 08:53 V38465MSA
175 µg/L 19.0 50.0n-Propylbenzene 100 09/28/23 08:53 V38465MSA
<22.0 µg/L 22.0 50.0Styrene 100 09/28/23 08:53 V38465MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/28/23 08:53 V38465MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/28/23 08:53 V38465MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/28/23 08:53 V38465MSA
2190 µg/L 22.0 50.0Toluene 100 09/28/23 08:53 V38465MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/28/23 08:53 V38465MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/28/23 08:53 V38465MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/28/23 08:53 V38465MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/28/23 08:53 V38465MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/28/23 08:53 V38465MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/28/23 08:53 V38465MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/28/23 08:53 V38465MSA
1330 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/28/23 08:53 V38465MSA
361 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/28/23 08:53 V38465MSA
<100 µg/L 100 500Vinyl Acetate 100 09/28/23 08:53 V38465MSA
<17.0 M µg/L 17.0 50.0Vinyl Chloride 100 09/28/23 08:53 V38465MSA
975 µg/L 21.0 50.0o-Xylene 100 09/28/23 08:53 V38465MSA
4450 µg/L 42.0 100m,p-Xylene 100 09/28/23 08:53 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 15 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-1
96054 Matrix:
9/21/2023 17:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
5430 µg/L 21.0 50.0Xylene (Total)100 09/28/23 08:53 V38465
Surrogate: 4-Bromofluorobenzene 90.0 Limits: 70-130%09/28/23 08:53100 MSA V38465
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%09/28/23 08:53100 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%09/28/23 08:53100 MSA V38465
Surrogate: Toluene-d8 93.8 Limits: 70-130%09/28/23 08:53100 MSA V38465
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 16 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-2
96055 Matrix:
9/21/2023 16:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/28/23 05:35 V38465MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/28/23 05:35 V38465MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/28/23 05:35 V38465MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/28/23 05:35 V38465MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/28/23 05:35 V38465MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/28/23 05:35 V38465MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/28/23 05:35 V38465MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/28/23 05:35 V38465MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/28/23 05:35 V38465MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/28/23 05:35 V38465MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/28/23 05:35 V38465MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/28/23 05:35 V38465MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/28/23 05:35 V38465MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/28/23 05:35 V38465MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/28/23 05:35 V38465MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/28/23 05:35 V38465MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/28/23 05:35 V38465MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/28/23 05:35 V38465MSA
<0.500 M µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/28/23 05:35 V38465MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/28/23 05:35 V38465MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/28/23 05:35 V38465MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/28/23 05:35 V38465MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/28/23 05:35 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 17 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-2
96055 Matrix:
9/21/2023 16:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/28/23 05:35 V38465MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/28/23 05:35 V38465MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/28/23 05:35 V38465MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/28/23 05:35 V38465MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/28/23 05:35 V38465MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/28/23 05:35 V38465MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/28/23 05:35 V38465MSA
<0.190 M µg/L 0.190 0.5001,2-Dichloropropane 1 09/28/23 05:35 V38465MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/28/23 05:35 V38465MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/28/23 05:35 V38465MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/28/23 05:35 V38465MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/28/23 05:35 V38465MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/28/23 05:35 V38465MSA
<42.0 µg/L 42.0 200Ethanol 1 09/28/23 05:35 V38465MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/28/23 05:35 V38465MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/28/23 05:35 V38465MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/28/23 05:35 V38465MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/28/23 05:35 V38465MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/28/23 05:35 V38465MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/28/23 05:35 V38465MSA
3.36 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/28/23 05:35 V38465MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/28/23 05:35 V38465MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/28/23 05:35 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 18 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-2
96055 Matrix:
9/21/2023 16:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/28/23 05:35 V38465MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/28/23 05:35 V38465MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/28/23 05:35 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/28/23 05:35 V38465MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/28/23 05:35 V38465MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/28/23 05:35 V38465MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/28/23 05:35 V38465MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/28/23 05:35 V38465MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/28/23 05:35 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/28/23 05:35 V38465MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/28/23 05:35 V38465MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/28/23 05:35 V38465MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/28/23 05:35 V38465MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/28/23 05:35 V38465MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/28/23 05:35 V38465MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/28/23 05:35 V38465MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/28/23 05:35 V38465MSA
<0.170 M µg/L 0.170 0.500Vinyl Chloride 1 09/28/23 05:35 V38465MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/28/23 05:35 V38465MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/28/23 05:35 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 19 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-2
96055 Matrix:
9/21/2023 16:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/28/23 05:35 V38465
Surrogate: 4-Bromofluorobenzene 89.6 Limits: 70-130%09/28/23 05:351 MSA V38465
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%09/28/23 05:351 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%09/28/23 05:351 MSA V38465
Surrogate: Toluene-d8 96.4 Limits: 70-130%09/28/23 05:351 MSA V38465
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 20 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-3
96056 Matrix:
9/21/2023 17:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/28/23 06:00 V38465MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/28/23 06:00 V38465MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/28/23 06:00 V38465MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/28/23 06:00 V38465MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/28/23 06:00 V38465MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/28/23 06:00 V38465MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/28/23 06:00 V38465MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/28/23 06:00 V38465MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/28/23 06:00 V38465MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/28/23 06:00 V38465MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/28/23 06:00 V38465MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/28/23 06:00 V38465MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/28/23 06:00 V38465MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/28/23 06:00 V38465MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/28/23 06:00 V38465MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/28/23 06:00 V38465MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/28/23 06:00 V38465MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/28/23 06:00 V38465MSA
<0.500 M µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/28/23 06:00 V38465MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/28/23 06:00 V38465MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/28/23 06:00 V38465MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/28/23 06:00 V38465MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/28/23 06:00 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 21 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-3
96056 Matrix:
9/21/2023 17:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/28/23 06:00 V38465MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/28/23 06:00 V38465MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/28/23 06:00 V38465MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/28/23 06:00 V38465MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/28/23 06:00 V38465MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/28/23 06:00 V38465MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/28/23 06:00 V38465MSA
<0.190 M µg/L 0.190 0.5001,2-Dichloropropane 1 09/28/23 06:00 V38465MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/28/23 06:00 V38465MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/28/23 06:00 V38465MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/28/23 06:00 V38465MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/28/23 06:00 V38465MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/28/23 06:00 V38465MSA
<42.0 µg/L 42.0 200Ethanol 1 09/28/23 06:00 V38465MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/28/23 06:00 V38465MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/28/23 06:00 V38465MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/28/23 06:00 V38465MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/28/23 06:00 V38465MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/28/23 06:00 V38465MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/28/23 06:00 V38465MSA
26.4 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/28/23 06:00 V38465MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/28/23 06:00 V38465MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/28/23 06:00 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 22 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-3
96056 Matrix:
9/21/2023 17:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/28/23 06:00 V38465MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/28/23 06:00 V38465MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/28/23 06:00 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/28/23 06:00 V38465MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/28/23 06:00 V38465MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/28/23 06:00 V38465MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/28/23 06:00 V38465MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/28/23 06:00 V38465MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/28/23 06:00 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/28/23 06:00 V38465MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/28/23 06:00 V38465MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/28/23 06:00 V38465MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/28/23 06:00 V38465MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/28/23 06:00 V38465MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/28/23 06:00 V38465MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/28/23 06:00 V38465MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/28/23 06:00 V38465MSA
<0.170 M µg/L 0.170 0.500Vinyl Chloride 1 09/28/23 06:00 V38465MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/28/23 06:00 V38465MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/28/23 06:00 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 23 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-3
96056 Matrix:
9/21/2023 17:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/28/23 06:00 V38465
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%09/28/23 06:001 MSA V38465
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/28/23 06:001 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%09/28/23 06:001 MSA V38465
Surrogate: Toluene-d8 97.2 Limits: 70-130%09/28/23 06:001 MSA V38465
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 24 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-4
96057 Matrix:
9/21/2023 16:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
2380 µg/L 180 1000Acetone 100 09/28/23 09:18 V38465MSA
17000 µg/L 180 500Benzene 1000 09/28/23 23:05 V38531MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/28/23 09:18 V38465MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/28/23 09:18 V38465MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/28/23 09:18 V38465MSA
<150 µg/L 150 500Bromoform 100 09/28/23 09:18 V38465MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/28/23 09:18 V38465MSA
36.9 J µg/L 18.0 50.0n-Butylbenzene 100 09/28/23 09:18 V38465MSA
30.4 J µg/L 20.0 50.0sec-Butyl benzene 100 09/28/23 09:18 V38465MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/28/23 09:18 V38465MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/28/23 09:18 V38465MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/28/23 09:18 V38465MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/28/23 09:18 V38465MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/28/23 09:18 V38465MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/28/23 09:18 V38465MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 09/28/23 09:18 V38465MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/28/23 09:18 V38465MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/28/23 09:18 V38465MSA
285 M µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/28/23 09:18 V38465MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/28/23 09:18 V38465MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/28/23 09:18 V38465MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/28/23 09:18 V38465MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/28/23 09:18 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 25 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-4
96057 Matrix:
9/21/2023 16:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/28/23 09:18 V38465MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 09/28/23 09:18 V38465MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/28/23 09:18 V38465MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/28/23 09:18 V38465MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/28/23 09:18 V38465MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/28/23 09:18 V38465MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/28/23 09:18 V38465MSA
<19.0 M µg/L 19.0 50.01,2-Dichloropropane 100 09/28/23 09:18 V38465MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/28/23 09:18 V38465MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/28/23 09:18 V38465MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/28/23 09:18 V38465MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/28/23 09:18 V38465MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/28/23 09:18 V38465MSA
<4200 µg/L 4200 20000Ethanol 100 09/28/23 09:18 V38465MSA
3830 µg/L 17.0 50.0Ethylbenzene 100 09/28/23 09:18 V38465MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/28/23 09:18 V38465MSA
499 µg/L 38.0 1002-Hexanone 100 09/28/23 09:18 V38465MSA
174 µg/L 18.0 50.0Isopropylbenzene 100 09/28/23 09:18 V38465MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/28/23 09:18 V38465MSA
2030 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/28/23 09:18 V38465MSA
14100 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 09/28/23 23:05 V38531MSA
354 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/28/23 09:18 V38465MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 09/28/23 09:18 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 26 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-4
96057 Matrix:
9/21/2023 16:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
1030 µg/L 47.0 100Naphthalene 100 09/28/23 09:18 V38465MSA
433 µg/L 19.0 50.0n-Propylbenzene 100 09/28/23 09:18 V38465MSA
<22.0 µg/L 22.0 50.0Styrene 100 09/28/23 09:18 V38465MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/28/23 09:18 V38465MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/28/23 09:18 V38465MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/28/23 09:18 V38465MSA
41700 µg/L 220 500Toluene 1000 09/28/23 23:05 V38531MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/28/23 09:18 V38465MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/28/23 09:18 V38465MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/28/23 09:18 V38465MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/28/23 09:18 V38465MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/28/23 09:18 V38465MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/28/23 09:18 V38465MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/28/23 09:18 V38465MSA
3290 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/28/23 09:18 V38465MSA
771 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/28/23 09:18 V38465MSA
<100 µg/L 100 500Vinyl Acetate 100 09/28/23 09:18 V38465MSA
<17.0 M µg/L 17.0 50.0Vinyl Chloride 100 09/28/23 09:18 V38465MSA
6300 µg/L 21.0 50.0o-Xylene 100 09/28/23 09:18 V38465MSA
13700 µg/L 42.0 100m,p-Xylene 100 09/28/23 09:18 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 27 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-4
96057 Matrix:
9/21/2023 16:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
20000 µg/L 21.0 50.0Xylene (Total)100 09/28/23 09:18 V38465
Surrogate: 4-Bromofluorobenzene 88.6 Limits: 70-130%09/28/23 09:18100 MSA V38465
Surrogate: Dibromofluoromethane 100 Limits: 70-130%09/28/23 09:18100 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%09/28/23 09:18100 MSA V38465
Surrogate: Toluene-d8 94.6 Limits: 70-130%09/28/23 09:18100 MSA V38465
Surrogate: 4-Bromofluorobenzene 86.8 Limits: 70-130%09/28/23 23:051000 MSA V38531
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%09/28/23 23:051000 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%09/28/23 23:051000 MSA V38531
Surrogate: Toluene-d8 93.2 Limits: 70-130%09/28/23 23:051000 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 28 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-5
96058 Matrix:
9/21/2023 16:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
575 J µg/L 180 1000Acetone 100 09/28/23 09:42 V38465MSA
4580 µg/L 18.0 50.0Benzene 100 09/28/23 09:42 V38465MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/28/23 09:42 V38465MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/28/23 09:42 V38465MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/28/23 09:42 V38465MSA
<150 µg/L 150 500Bromoform 100 09/28/23 09:42 V38465MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/28/23 09:42 V38465MSA
87.3 µg/L 18.0 50.0n-Butylbenzene 100 09/28/23 09:42 V38465MSA
71.2 µg/L 20.0 50.0sec-Butyl benzene 100 09/28/23 09:42 V38465MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/28/23 09:42 V38465MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/28/23 09:42 V38465MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/28/23 09:42 V38465MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/28/23 09:42 V38465MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/28/23 09:42 V38465MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/28/23 09:42 V38465MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 09/28/23 09:42 V38465MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/28/23 09:42 V38465MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/28/23 09:42 V38465MSA
61.9 M µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/28/23 09:42 V38465MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/28/23 09:42 V38465MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/28/23 09:42 V38465MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/28/23 09:42 V38465MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/28/23 09:42 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 29 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-5
96058 Matrix:
9/21/2023 16:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/28/23 09:42 V38465MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 09/28/23 09:42 V38465MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/28/23 09:42 V38465MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/28/23 09:42 V38465MSA
26.8 J µg/L 15.0 50.01,1-Dichloroethene 100 09/28/23 09:42 V38465MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/28/23 09:42 V38465MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/28/23 09:42 V38465MSA
<19.0 M µg/L 19.0 50.01,2-Dichloropropane 100 09/28/23 09:42 V38465MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/28/23 09:42 V38465MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/28/23 09:42 V38465MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/28/23 09:42 V38465MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/28/23 09:42 V38465MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/28/23 09:42 V38465MSA
<4200 µg/L 4200 20000Ethanol 100 09/28/23 09:42 V38465MSA
2900 µg/L 17.0 50.0Ethylbenzene 100 09/28/23 09:42 V38465MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/28/23 09:42 V38465MSA
469 µg/L 38.0 1002-Hexanone 100 09/28/23 09:42 V38465MSA
208 µg/L 18.0 50.0Isopropylbenzene 100 09/28/23 09:42 V38465MSA
36.3 J µg/L 8.90 50.04-Isopropyl toluene 100 09/28/23 09:42 V38465MSA
831 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/28/23 09:42 V38465MSA
712 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/28/23 09:42 V38465MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/28/23 09:42 V38465MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 09/28/23 09:42 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 30 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-5
96058 Matrix:
9/21/2023 16:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
1090 µg/L 47.0 100Naphthalene 100 09/28/23 09:42 V38465MSA
516 µg/L 19.0 50.0n-Propylbenzene 100 09/28/23 09:42 V38465MSA
<22.0 µg/L 22.0 50.0Styrene 100 09/28/23 09:42 V38465MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/28/23 09:42 V38465MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/28/23 09:42 V38465MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/28/23 09:42 V38465MSA
14400 µg/L 220 500Toluene 1000 09/28/23 23:30 V38531MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/28/23 09:42 V38465MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/28/23 09:42 V38465MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/28/23 09:42 V38465MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/28/23 09:42 V38465MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/28/23 09:42 V38465MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/28/23 09:42 V38465MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/28/23 09:42 V38465MSA
3510 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/28/23 09:42 V38465MSA
844 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/28/23 09:42 V38465MSA
<100 µg/L 100 500Vinyl Acetate 100 09/28/23 09:42 V38465MSA
<17.0 M µg/L 17.0 50.0Vinyl Chloride 100 09/28/23 09:42 V38465MSA
4500 µg/L 21.0 50.0o-Xylene 100 09/28/23 09:42 V38465MSA
10300 µg/L 42.0 100m,p-Xylene 100 09/28/23 09:42 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 31 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-5
96058 Matrix:
9/21/2023 16:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
14800 µg/L 21.0 50.0Xylene (Total)100 09/28/23 09:42 V38465
Surrogate: 4-Bromofluorobenzene 87.8 Limits: 70-130%09/28/23 09:42100 MSA V38465
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/28/23 09:42100 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%09/28/23 09:42100 MSA V38465
Surrogate: Toluene-d8 95.2 Limits: 70-130%09/28/23 09:42100 MSA V38465
Surrogate: 4-Bromofluorobenzene 87.8 Limits: 70-130%09/28/23 23:301000 MSA V38531
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%09/28/23 23:301000 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 106 Limits: 70-130%09/28/23 23:301000 MSA V38531
Surrogate: Toluene-d8 92.8 Limits: 70-130%09/28/23 23:301000 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 32 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-6
96059 Matrix:
9/21/2023 16:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/28/23 06:25 V38465MSA
41.1 µg/L 0.180 0.500Benzene 1 09/28/23 06:25 V38465MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/28/23 06:25 V38465MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/28/23 06:25 V38465MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/28/23 06:25 V38465MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/28/23 06:25 V38465MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/28/23 06:25 V38465MSA
2.95 µg/L 0.180 0.500n-Butylbenzene 1 09/28/23 06:25 V38465MSA
4.95 µg/L 0.200 0.500sec-Butyl benzene 1 09/28/23 06:25 V38465MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/28/23 06:25 V38465MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/28/23 06:25 V38465MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/28/23 06:25 V38465MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/28/23 06:25 V38465MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/28/23 06:25 V38465MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/28/23 06:25 V38465MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/28/23 06:25 V38465MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/28/23 06:25 V38465MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/28/23 06:25 V38465MSA
<0.500 M µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/28/23 06:25 V38465MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/28/23 06:25 V38465MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/28/23 06:25 V38465MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/28/23 06:25 V38465MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/28/23 06:25 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 33 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-6
96059 Matrix:
9/21/2023 16:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/28/23 06:25 V38465MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/28/23 06:25 V38465MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/28/23 06:25 V38465MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/28/23 06:25 V38465MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/28/23 06:25 V38465MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/28/23 06:25 V38465MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/28/23 06:25 V38465MSA
<0.190 M µg/L 0.190 0.5001,2-Dichloropropane 1 09/28/23 06:25 V38465MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/28/23 06:25 V38465MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/28/23 06:25 V38465MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/28/23 06:25 V38465MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/28/23 06:25 V38465MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/28/23 06:25 V38465MSA
<42.0 µg/L 42.0 200Ethanol 1 09/28/23 06:25 V38465MSA
1.04 µg/L 0.170 0.500Ethylbenzene 1 09/28/23 06:25 V38465MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/28/23 06:25 V38465MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/28/23 06:25 V38465MSA
10.6 µg/L 0.180 0.500Isopropylbenzene 1 09/28/23 06:25 V38465MSA
4.71 µg/L 0.089 0.5004-Isopropyl toluene 1 09/28/23 06:25 V38465MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/28/23 06:25 V38465MSA
8.58 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/28/23 06:25 V38465MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/28/23 06:25 V38465MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/28/23 06:25 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 34 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-6
96059 Matrix:
9/21/2023 16:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
176 µg/L 4.70 10.0Naphthalene 10 09/28/23 21:02 V38531MSA
3.47 µg/L 0.190 0.500n-Propylbenzene 1 09/28/23 06:25 V38465MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/28/23 06:25 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/28/23 06:25 V38465MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/28/23 06:25 V38465MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/28/23 06:25 V38465MSA
0.516 µg/L 0.220 0.500Toluene 1 09/28/23 06:25 V38465MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/28/23 06:25 V38465MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/28/23 06:25 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/28/23 06:25 V38465MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/28/23 06:25 V38465MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/28/23 06:25 V38465MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/28/23 06:25 V38465MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/28/23 06:25 V38465MSA
122 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 09/28/23 21:02 V38531MSA
9.40 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/28/23 06:25 V38465MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/28/23 06:25 V38465MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/28/23 06:25 V38465MSA
30.3 µg/L 0.210 0.500o-Xylene 1 09/28/23 06:25 V38465MSA
47.3 µg/L 0.420 1.00m,p-Xylene 1 09/28/23 06:25 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 35 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-6
96059 Matrix:
9/21/2023 16:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
77.6 µg/L 0.210 0.500Xylene (Total)1 09/28/23 06:25 V38465
Surrogate: 4-Bromofluorobenzene 89.8 Limits: 70-130%09/28/23 06:251 MSA V38465
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%09/28/23 06:251 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 110 Limits: 70-130%09/28/23 06:251 MSA V38465
Surrogate: Toluene-d8 93.6 Limits: 70-130%09/28/23 06:251 MSA V38465
Surrogate: 4-Bromofluorobenzene 88.4 Limits: 70-130%09/28/23 21:0210 MSA V38531
Surrogate: Dibromofluoromethane 98.8 Limits: 70-130%09/28/23 21:0210 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%09/28/23 21:0210 MSA V38531
Surrogate: Toluene-d8 89.0 Limits: 70-130%09/28/23 21:0210 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 36 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-7
96060 Matrix:
9/21/2023 15:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 09/28/23 06:50 V38465MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/28/23 06:50 V38465MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/28/23 06:50 V38465MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/28/23 06:50 V38465MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/28/23 06:50 V38465MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/28/23 06:50 V38465MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/28/23 06:50 V38465MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/28/23 06:50 V38465MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/28/23 06:50 V38465MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/28/23 06:50 V38465MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/28/23 06:50 V38465MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/28/23 06:50 V38465MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/28/23 06:50 V38465MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/28/23 06:50 V38465MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/28/23 06:50 V38465MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/28/23 06:50 V38465MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/28/23 06:50 V38465MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/28/23 06:50 V38465MSA
<0.500 M µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/28/23 06:50 V38465MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/28/23 06:50 V38465MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/28/23 06:50 V38465MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/28/23 06:50 V38465MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/28/23 06:50 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 37 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-7
96060 Matrix:
9/21/2023 15:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/28/23 06:50 V38465MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/28/23 06:50 V38465MSA
4.66 µg/L 0.240 0.5001,1-Dichloroethane 1 09/28/23 06:50 V38465MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/28/23 06:50 V38465MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/28/23 06:50 V38465MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/28/23 06:50 V38465MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/28/23 06:50 V38465MSA
<0.190 M µg/L 0.190 0.5001,2-Dichloropropane 1 09/28/23 06:50 V38465MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/28/23 06:50 V38465MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/28/23 06:50 V38465MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/28/23 06:50 V38465MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/28/23 06:50 V38465MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/28/23 06:50 V38465MSA
<42.0 µg/L 42.0 200Ethanol 1 09/28/23 06:50 V38465MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/28/23 06:50 V38465MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/28/23 06:50 V38465MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/28/23 06:50 V38465MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/28/23 06:50 V38465MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/28/23 06:50 V38465MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/28/23 06:50 V38465MSA
44.0 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/28/23 06:50 V38465MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/28/23 06:50 V38465MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/28/23 06:50 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 38 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-7
96060 Matrix:
9/21/2023 15:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
38.5 µg/L 0.470 1.00Naphthalene 1 09/28/23 06:50 V38465MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/28/23 06:50 V38465MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/28/23 06:50 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/28/23 06:50 V38465MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/28/23 06:50 V38465MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/28/23 06:50 V38465MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/28/23 06:50 V38465MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/28/23 06:50 V38465MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/28/23 06:50 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/28/23 06:50 V38465MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/28/23 06:50 V38465MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/28/23 06:50 V38465MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/28/23 06:50 V38465MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/28/23 06:50 V38465MSA
0.439 J µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/28/23 06:50 V38465MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/28/23 06:50 V38465MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/28/23 06:50 V38465MSA
<0.170 M µg/L 0.170 0.500Vinyl Chloride 1 09/28/23 06:50 V38465MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/28/23 06:50 V38465MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/28/23 06:50 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 39 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-7
96060 Matrix:
9/21/2023 15:58
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/28/23 06:50 V38465
Surrogate: 4-Bromofluorobenzene 89.6 Limits: 70-130%09/28/23 06:501 MSA V38465
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/28/23 06:501 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 111 Limits: 70-130%09/28/23 06:501 MSA V38465
Surrogate: Toluene-d8 94.6 Limits: 70-130%09/28/23 06:501 MSA V38465
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 40 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-8
96061 Matrix:
9/21/2023 16:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
V38608 10/02/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/28/23 07:14 V38465MSA
58.5 µg/L 0.180 0.500Benzene 1 09/28/23 07:14 V38465MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/28/23 07:14 V38465MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/28/23 07:14 V38465MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/28/23 07:14 V38465MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/28/23 07:14 V38465MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/28/23 07:14 V38465MSA
19.3 µg/L 0.180 0.500n-Butylbenzene 1 09/28/23 07:14 V38465MSA
14.4 µg/L 0.200 0.500sec-Butyl benzene 1 09/28/23 07:14 V38465MSA
3.01 µg/L 0.920 2.00tert-Butyl benzene 1 09/28/23 07:14 V38465MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/28/23 07:14 V38465MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/28/23 07:14 V38465MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/28/23 07:14 V38465MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/28/23 07:14 V38465MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/28/23 07:14 V38465MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/28/23 07:14 V38465MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/28/23 07:14 V38465MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/28/23 07:14 V38465MSA
0.603 M µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/28/23 07:14 V38465MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/28/23 07:14 V38465MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/28/23 07:14 V38465MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/28/23 07:14 V38465MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/28/23 07:14 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 41 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-8
96061 Matrix:
9/21/2023 16:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
V38608 10/02/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/28/23 07:14 V38465MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/28/23 07:14 V38465MSA
8.56 µg/L 0.240 0.5001,1-Dichloroethane 1 09/28/23 07:14 V38465MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/28/23 07:14 V38465MSA
29.4 µg/L 0.150 0.5001,1-Dichloroethene 1 09/28/23 07:14 V38465MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/28/23 07:14 V38465MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/28/23 07:14 V38465MSA
<0.190 M µg/L 0.190 0.5001,2-Dichloropropane 1 09/28/23 07:14 V38465MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/28/23 07:14 V38465MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/28/23 07:14 V38465MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/28/23 07:14 V38465MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/28/23 07:14 V38465MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/28/23 07:14 V38465MSA
<42.0 µg/L 42.0 200Ethanol 1 09/28/23 07:14 V38465MSA
299 µg/L 1.70 5.00Ethylbenzene 10 09/28/23 21:26 V38531MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/28/23 07:14 V38465MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/28/23 07:14 V38465MSA
75.0 µg/L 0.180 0.500Isopropylbenzene 1 09/28/23 07:14 V38465MSA
9.81 µg/L 0.089 0.5004-Isopropyl toluene 1 09/28/23 07:14 V38465MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/28/23 07:14 V38465MSA
6.48 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/28/23 07:14 V38465MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/28/23 07:14 V38465MSA
0.453 J µg/L 0.330 2.00Methylene Chloride 1 09/28/23 07:14 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 42 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-8
96061 Matrix:
9/21/2023 16:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
V38608 10/02/23 09:00
222 µg/L 4.70 10.0Naphthalene 10 09/28/23 21:26 V38531MSA
97.5 µg/L 0.190 0.500n-Propylbenzene 1 09/28/23 07:14 V38465MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/28/23 07:14 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/28/23 07:14 V38465MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/28/23 07:14 V38465MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/28/23 07:14 V38465MSA
171 µg/L 2.20 5.00Toluene 10 09/28/23 21:26 V38531MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/28/23 07:14 V38465MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/28/23 07:14 V38465MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/28/23 07:14 V38465MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/28/23 07:14 V38465MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/28/23 07:14 V38465MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/28/23 07:14 V38465MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/28/23 07:14 V38465MSA
1300 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 10/02/23 23:58 V38609MSA
170 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 09/28/23 21:26 V38531MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/28/23 07:14 V38465MSA
<0.170 M µg/L 0.170 0.500Vinyl Chloride 1 09/28/23 07:14 V38465MSA
553 µg/L 2.10 5.00o-Xylene 10 09/28/23 21:26 V38531MSA
1320 µg/L 4.20 10.0m,p-Xylene 10 09/28/23 21:26 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 43 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-8
96061 Matrix:
9/21/2023 16:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
V38608 10/02/23 09:00
1870 µg/L 2.10 5.00Xylene (Total)10 09/28/23 21:26 V38531
Surrogate: 4-Bromofluorobenzene 90.4 Limits: 70-130%09/28/23 07:141 MSA V38465
Surrogate: Dibromofluoromethane 98.6 Limits: 70-130%09/28/23 07:141 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 111 Limits: 70-130%09/28/23 07:141 MSA V38465
Surrogate: Toluene-d8 88.8 Limits: 70-130%09/28/23 07:141 MSA V38465
Surrogate: 4-Bromofluorobenzene 91.0 Limits: 70-130%09/28/23 21:2610 MSA V38531
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%09/28/23 21:2610 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%09/28/23 21:2610 MSA V38531
Surrogate: Toluene-d8 92.6 Limits: 70-130%09/28/23 21:2610 MSA V38531
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%10/02/23 23:58100 MSA V38609
Surrogate: Dibromofluoromethane 97.4 Limits: 70-130%10/02/23 23:58100 MSA V38609
Surrogate: 1,2-Dichloroethane - d4 89.0 Limits: 70-130%10/02/23 23:58100 MSA V38609
Surrogate: Toluene-d8 100 Limits: 70-130%10/02/23 23:58100 MSA V38609
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 44 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
0.085 mg/L 0.002 0.006Lead 1 09/27/23 00:41 6010DJKC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 45 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
2490 µg/L 180 1000Acetone 100 09/28/23 10:07 V38465MSA
29900 µg/L 180 500Benzene 1000 09/28/23 23:55 V38531MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/28/23 10:07 V38465MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/28/23 10:07 V38465MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/28/23 10:07 V38465MSA
<150 µg/L 150 500Bromoform 100 09/28/23 10:07 V38465MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/28/23 10:07 V38465MSA
30.9 J µg/L 18.0 50.0n-Butylbenzene 100 09/28/23 10:07 V38465MSA
21.2 J µg/L 20.0 50.0sec-Butyl benzene 100 09/28/23 10:07 V38465MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/28/23 10:07 V38465MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/28/23 10:07 V38465MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/28/23 10:07 V38465MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/28/23 10:07 V38465MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/28/23 10:07 V38465MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/28/23 10:07 V38465MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 09/28/23 10:07 V38465MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/28/23 10:07 V38465MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/28/23 10:07 V38465MSA
660 M µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/28/23 10:07 V38465MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/28/23 10:07 V38465MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/28/23 10:07 V38465MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/28/23 10:07 V38465MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/28/23 10:07 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 46 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/28/23 10:07 V38465MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 09/28/23 10:07 V38465MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/28/23 10:07 V38465MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/28/23 10:07 V38465MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/28/23 10:07 V38465MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/28/23 10:07 V38465MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/28/23 10:07 V38465MSA
<19.0 M µg/L 19.0 50.01,2-Dichloropropane 100 09/28/23 10:07 V38465MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/28/23 10:07 V38465MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/28/23 10:07 V38465MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/28/23 10:07 V38465MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/28/23 10:07 V38465MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/28/23 10:07 V38465MSA
<4200 µg/L 4200 20000Ethanol 100 09/28/23 10:07 V38465MSA
4160 µg/L 17.0 50.0Ethylbenzene 100 09/28/23 10:07 V38465MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/28/23 10:07 V38465MSA
211 µg/L 38.0 1002-Hexanone 100 09/28/23 10:07 V38465MSA
197 µg/L 18.0 50.0Isopropylbenzene 100 09/28/23 10:07 V38465MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 09/28/23 10:07 V38465MSA
1560 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/28/23 10:07 V38465MSA
62700 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 09/28/23 23:55 V38531MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/28/23 10:07 V38465MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 09/28/23 10:07 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 47 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
727 µg/L 47.0 100Naphthalene 100 09/28/23 10:07 V38465MSA
407 µg/L 19.0 50.0n-Propylbenzene 100 09/28/23 10:07 V38465MSA
<22.0 µg/L 22.0 50.0Styrene 100 09/28/23 10:07 V38465MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/28/23 10:07 V38465MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/28/23 10:07 V38465MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/28/23 10:07 V38465MSA
62300 µg/L 220 500Toluene 1000 09/28/23 23:55 V38531MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/28/23 10:07 V38465MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/28/23 10:07 V38465MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/28/23 10:07 V38465MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/28/23 10:07 V38465MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/28/23 10:07 V38465MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/28/23 10:07 V38465MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/28/23 10:07 V38465MSA
3140 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/28/23 10:07 V38465MSA
753 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/28/23 10:07 V38465MSA
<100 µg/L 100 500Vinyl Acetate 100 09/28/23 10:07 V38465MSA
<17.0 M µg/L 17.0 50.0Vinyl Chloride 100 09/28/23 10:07 V38465MSA
7070 µg/L 21.0 50.0o-Xylene 100 09/28/23 10:07 V38465MSA
14900 µg/L 42.0 100m,p-Xylene 100 09/28/23 10:07 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 48 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00 V38530 09/28/23 09:00
22000 µg/L 21.0 50.0Xylene (Total)100 09/28/23 10:07 V38465
Surrogate: 4-Bromofluorobenzene 90.0 Limits: 70-130%09/28/23 10:07100 MSA V38465
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/28/23 10:07100 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%09/28/23 10:07100 MSA V38465
Surrogate: Toluene-d8 95.0 Limits: 70-130%09/28/23 10:07100 MSA V38465
Surrogate: 4-Bromofluorobenzene 88.0 Limits: 70-130%09/28/23 23:551000 MSA V38531
Surrogate: Dibromofluoromethane 101 Limits: 70-130%09/28/23 23:551000 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%09/28/23 23:551000 MSA V38531
Surrogate: Toluene-d8 95.0 Limits: 70-130%09/28/23 23:551000 MSA V38531
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V38382 09/27/23 09:34
<0.324 µg/L 0.324 2.15Acenaphthene 1 09/28/23 12:13 V38427AMP
<0.319 µg/L 0.319 2.15Acenaphthylene 1 09/28/23 12:13 V38427AMP
<0.898 µg/L 0.898 2.15Anthracene 1 09/28/23 12:13 V38427AMP
<1.43 µg/L 1.43 10.8Benzidine 1 09/28/23 12:13 V38427AMP
<0.684 µg/L 0.684 2.15Benzo(a)anthracene 1 09/28/23 12:13 V38427AMP
<1.10 µg/L 1.10 2.15Benzo(a)pyrene 1 09/28/23 12:13 V38427AMP
<2.68 µg/L 2.68 5.38Benzo(b)fluoranthene 1 09/28/23 12:13 V38427AMP
<1.09 µg/L 1.09 5.38Benzo(g,h,i)perylene 1 09/28/23 12:13 V38427AMP
<2.14 µg/L 2.14 5.38Benzo(k)fluoranthene 1 09/28/23 12:13 V38427AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 49 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V38382 09/27/23 09:34
<1.19 µg/L 1.19 10.8Benzoic Acid 1 09/28/23 12:13 V38427AMP
49.2 µg/L 0.735 5.38Benzyl alcohol 1 09/28/23 12:13 V38427AMP
<0.503 µg/L 0.503 5.38Bis(2-Chloroethoxy)methane 1 09/28/23 12:13 V38427AMP
<1.12 µg/L 1.12 5.38Bis(2-Chloroethyl)ether 1 09/28/23 12:13 V38427AMP
<1.16 µg/L 1.16 5.38Bis(2-Chloroisopropyl)ether 1 09/28/23 12:13 V38427AMP
<3.74 µg/L 3.74 10.8Bis(2-ethylhexyl)phthalate 1 09/28/23 12:13 V38427AMP
<1.19 µg/L 1.19 5.384-Bromophenyl phenyl ether 1 09/28/23 12:13 V38427AMP
<1.97 µg/L 1.97 5.38Butyl benzyl phthalate 1 09/28/23 12:13 V38427AMP
<1.27 µg/L 1.27 5.384-Chloro-3-methylphenol 1 09/28/23 12:13 V38427AMP
<7.93 µg/L 7.93 21.52-Chloronaphthalene 1 09/28/23 12:13 V38427AMP
<1.01 µg/L 1.01 10.82-Chlorophenol 1 09/28/23 12:13 V38427AMP
<1.84 µg/L 1.84 5.384-Chlorophenyl phenyl ether 1 09/28/23 12:13 V38427AMP
<0.435 µg/L 0.435 2.15Chrysene 1 09/28/23 12:13 V38427AMP
<0.466 µg/L 0.466 2.15Dibenz(a,h)anthracene 1 09/28/23 12:13 V38427AMP
<0.921 µg/L 0.921 5.38Dibenzofuran 1 09/28/23 12:13 V38427AMP
<2.15 µg/L 2.15 5.381,2-Dichlorobenzene 1 09/28/23 12:13 V38427AMP
<2.15 µg/L 2.15 5.381,3-Dichlorobenzene 1 09/28/23 12:13 V38427AMP
<2.21 µg/L 2.21 5.381,4-Dichlorobenzene 1 09/28/23 12:13 V38427AMP
<2.03 µg/L 2.03 5.383,3'-Dichlorobenzidine 1 09/28/23 12:13 V38427AMP
<1.58 µg/L 1.58 10.82,4-Dichlorophenol 1 09/28/23 12:13 V38427AMP
<0.801 µg/L 0.801 5.38Diethyl phthalate 1 09/28/23 12:13 V38427AMP
<1.01 µg/L 1.01 5.38Dimethyl phthalate 1 09/28/23 12:13 V38427AMP
<1.69 µg/L 1.69 21.52,4-Dimethylphenol 1 09/28/23 12:13 V38427AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 50 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V38382 09/27/23 09:34
<2.22 µg/L 2.22 5.38Di-n-butyl phthalate 1 09/28/23 12:13 V38427AMP
<2.24 µg/L 2.24 10.84,6-Dinitro-2-methylphenol 1 09/28/23 12:13 V38427AMP
<2.07 µg/L 2.07 10.82,4-Dinitrophenol 1 09/28/23 12:13 V38427AMP
<1.19 µg/L 1.19 5.382,4-Dinitrotoluene 1 09/28/23 12:13 V38427AMP
<0.870 µg/L 0.870 5.382,6-Dinitrotoluene 1 09/28/23 12:13 V38427AMP
<1.78 µg/L 1.78 5.38Di-n-Octyl Phthalate 1 09/28/23 12:13 V38427AMP
<0.268 µg/L 0.268 2.15Fluoranthene 1 09/28/23 12:13 V38427AMP
<0.867 µg/L 0.867 2.15Fluorene 1 09/28/23 12:13 V38427AMP
<1.05 µg/L 1.05 5.38Hexachlorobenzene 1 09/28/23 12:13 V38427AMP
<2.94 µg/L 2.94 5.38Hexachlorobutadiene 1 09/28/23 12:13 V38427AMP
<2.21 µg/L 2.21 5.38Hexachlorocyclopentadiene 1 09/28/23 12:13 V38427AMP
<1.89 µg/L 1.89 5.38Hexachloroethane 1 09/28/23 12:13 V38427AMP
<0.512 µg/L 0.512 2.15Indeno(1,2,3-cd)pyrene 1 09/28/23 12:13 V38427AMP
<0.477 µg/L 0.477 5.38Isophorone 1 09/28/23 12:13 V38427AMP
50.8 µg/L 1.23 2.151-Methylnaphthalene 1 09/28/23 12:13 V38427AMP
91.4 µg/L 0.715 2.152-Methylnaphthalene 1 09/28/23 12:13 V38427AMP
306 µg/L 1.57 4.30Naphthalene 2 09/28/23 16:43 V38427AMP
<0.973 µg/L 0.973 5.38Nitrobenzene 1 09/28/23 12:13 V38427AMP
<0.530 µg/L 0.530 5.382-Nitrophenol 1 09/28/23 12:13 V38427AMP
<1.33 µg/L 1.33 10.84-Nitrophenol 1 09/28/23 12:13 V38427AMP
<1.18 µg/L 1.18 5.38N-Nitrosodiphenylamine 1 09/28/23 12:13 V38427AMP
<0.689 µg/L 0.689 5.38N-Nitroso-di-n-propylamine 1 09/28/23 12:13 V38427AMP
<1.54 µg/L 1.54 5.38Pentachlorophenol 1 09/28/23 12:13 V38427AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 51 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V38382 09/27/23 09:34
<0.460 µg/L 0.460 2.15Phenanthrene 1 09/28/23 12:13 V38427AMP
<0.700 µg/L 0.700 5.38Phenol 1 09/28/23 12:13 V38427AMP
<0.466 µg/L 0.466 2.15Pyrene 1 09/28/23 12:13 V38427AMP
<2.38 µg/L 2.38 5.381,2,4-Trichlorobenzene 1 09/28/23 12:13 V38427AMP
<1.42 µg/L 1.42 5.382,4,6-Trichlorophenol 1 09/28/23 12:13 V38427AMP
625.1Surrogate: Phenol-d5 31.9 Limits: 10-63%09/28/23 12:131 AMP
Surrogate: 2-Fluorobiphenyl 71.2 Limits: 49-118%09/28/23 12:131 AMP V38427
Surrogate: 2-Fluorophenol 38.2 Limits: 22-84%09/28/23 12:131 AMP V38427
Surrogate: Nitrobenzene-d5 70.6 Limits: 43-123%09/28/23 12:131 AMP V38427
Surrogate: 4-Terphenyl-d14 81.6 Limits: 49-151%09/28/23 12:131 AMP V38427
Surrogate: 2,4,6-Tribromophenol 86.8 Limits: 31-144%09/28/23 12:131 AMP V38427
625.1Surrogate: Phenol-d5 30.8 Limits: 10-63%09/28/23 16:432 AMP
Surrogate: 2-Fluorobiphenyl 71.2 Limits: 49-118%09/28/23 16:432 AMP V38427
Surrogate: 2-Fluorophenol 39.8 Limits: 22-84%09/28/23 16:432 AMP V38427
Surrogate: Nitrobenzene-d5 62.5 Limits: 43-123%09/28/23 16:432 AMP V38427
Surrogate: 4-Terphenyl-d14 77.9 Limits: 49-151%09/28/23 16:432 AMP V38427
Surrogate: 2,4,6-Tribromophenol 82.8 Limits: 31-144%09/28/23 16:432 AMP V38427
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V38326 09/26/23 10:25
23.8 µg/L 0.173 1.051,2-Dibromoethane 50 09/26/23 15:53 V38379TJW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 52 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
69800 µg/L 11500 50000Aliphatic C5-C8 (Adjusted)1000 09/26/23 11:16
14600 µg/L 2580 5000Aliphatics C9-C12 (Adjusted)100 09/26/23 03:29
7020 µg/L 402 5000Aromatic C9-C10 (Adjusted)100 09/26/23 03:29
470 µg/L 61.2 250Aromatic C11-C22 (Adjusted)1 09/28/23 12:13
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V38500 09/29/23 10:10
186 J µg/L 28.2 350Aliphatic C9-C18 1 09/30/23 19:03 V38527AMP
<124 µg/L 124 500Aliphatic C19-C36 1 09/30/23 19:03 V38527AMP
776 µg/L 61.2 250Aromatic C11-C22 1 09/30/23 19:03 V38527AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 102 Limits: 40-140%09/30/23 19:031 AMP
MADEP-EPHSurrogate: Chlorooctadecane 60.5 Limits: 40-140%09/30/23 19:031 AMP
MADEP-EPHSurrogate: OTP Surrogate 67.6 Limits: 40-140%09/30/23 19:031 AMP
Surrogate: 2-Fluorobiphenyl 98.3 Limits: 40-140%09/30/23 19:031 AMP V38527
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V38340 09/25/23 08:00
162000 µg/L 11500 50000Aliphatic C5-C8 1000 09/26/23 11:16 V38341TBL
47700 µg/L 2580 5000Aliphatic C9-C12 100 09/26/23 03:29 V38341TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 53 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:MW-9
96062 Matrix:
9/21/2023 15:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V38340 09/25/23 08:00
7020 µg/L 402 5000Aromatic C9-C10 100 09/26/23 03:29 V38341TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)112 Limits: 70-130%09/26/23 03:29100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)88.9 Limits: 70-130%09/26/23 03:29100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)92.3 Limits: 70-130%09/26/23 11:161000 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)102 Limits: 70-130%09/26/23 11:161000 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 54 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-2
96063 Matrix:
9/21/2023 15:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
491 J µg/L 180 1000Acetone 100 09/28/23 10:32 V38465MSA
6880 µg/L 18.0 50.0Benzene 100 09/28/23 10:32 V38465MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/28/23 10:32 V38465MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/28/23 10:32 V38465MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/28/23 10:32 V38465MSA
<150 µg/L 150 500Bromoform 100 09/28/23 10:32 V38465MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/28/23 10:32 V38465MSA
33.4 J µg/L 18.0 50.0n-Butylbenzene 100 09/28/23 10:32 V38465MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 09/28/23 10:32 V38465MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/28/23 10:32 V38465MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/28/23 10:32 V38465MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/28/23 10:32 V38465MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/28/23 10:32 V38465MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/28/23 10:32 V38465MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/28/23 10:32 V38465MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 09/28/23 10:32 V38465MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/28/23 10:32 V38465MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/28/23 10:32 V38465MSA
94.0 M µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/28/23 10:32 V38465MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/28/23 10:32 V38465MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/28/23 10:32 V38465MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/28/23 10:32 V38465MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/28/23 10:32 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 55 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-2
96063 Matrix:
9/21/2023 15:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/28/23 10:32 V38465MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 09/28/23 10:32 V38465MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/28/23 10:32 V38465MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/28/23 10:32 V38465MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/28/23 10:32 V38465MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/28/23 10:32 V38465MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/28/23 10:32 V38465MSA
<19.0 M µg/L 19.0 50.01,2-Dichloropropane 100 09/28/23 10:32 V38465MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/28/23 10:32 V38465MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/28/23 10:32 V38465MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/28/23 10:32 V38465MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/28/23 10:32 V38465MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/28/23 10:32 V38465MSA
<4200 µg/L 4200 20000Ethanol 100 09/28/23 10:32 V38465MSA
3030 µg/L 17.0 50.0Ethylbenzene 100 09/28/23 10:32 V38465MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/28/23 10:32 V38465MSA
103 µg/L 38.0 1002-Hexanone 100 09/28/23 10:32 V38465MSA
131 µg/L 18.0 50.0Isopropylbenzene 100 09/28/23 10:32 V38465MSA
21.7 J µg/L 8.90 50.04-Isopropyl toluene 100 09/28/23 10:32 V38465MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/28/23 10:32 V38465MSA
5460 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/28/23 10:32 V38465MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/28/23 10:32 V38465MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 09/28/23 10:32 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 56 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-2
96063 Matrix:
9/21/2023 15:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
938 µg/L 47.0 100Naphthalene 100 09/28/23 10:32 V38465MSA
332 µg/L 19.0 50.0n-Propylbenzene 100 09/28/23 10:32 V38465MSA
34.0 J µg/L 22.0 50.0Styrene 100 09/28/23 10:32 V38465MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/28/23 10:32 V38465MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/28/23 10:32 V38465MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/28/23 10:32 V38465MSA
5800 µg/L 22.0 50.0Toluene 100 09/28/23 10:32 V38465MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/28/23 10:32 V38465MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/28/23 10:32 V38465MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/28/23 10:32 V38465MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/28/23 10:32 V38465MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/28/23 10:32 V38465MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/28/23 10:32 V38465MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/28/23 10:32 V38465MSA
2620 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/28/23 10:32 V38465MSA
674 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/28/23 10:32 V38465MSA
<100 µg/L 100 500Vinyl Acetate 100 09/28/23 10:32 V38465MSA
<17.0 M µg/L 17.0 50.0Vinyl Chloride 100 09/28/23 10:32 V38465MSA
4010 µg/L 21.0 50.0o-Xylene 100 09/28/23 10:32 V38465MSA
6390 µg/L 42.0 100m,p-Xylene 100 09/28/23 10:32 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 57 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-2
96063 Matrix:
9/21/2023 15:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
10400 µg/L 21.0 50.0Xylene (Total)100 09/28/23 10:32 V38465
Surrogate: 4-Bromofluorobenzene 88.0 Limits: 70-130%09/28/23 10:32100 MSA V38465
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/28/23 10:32100 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%09/28/23 10:32100 MSA V38465
Surrogate: Toluene-d8 92.8 Limits: 70-130%09/28/23 10:32100 MSA V38465
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 58 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-7
96064 Matrix:
9/21/2023 16:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<18.0 µg/L 18.0 100Acetone 10 09/28/23 08:03 V38465MSA
347 µg/L 1.80 5.00Benzene 10 09/28/23 08:03 V38465MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 09/28/23 08:03 V38465MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 09/28/23 08:03 V38465MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 09/28/23 08:03 V38465MSA
<15.0 µg/L 15.0 50.0Bromoform 10 09/28/23 08:03 V38465MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 09/28/23 08:03 V38465MSA
8.27 µg/L 1.80 5.00n-Butylbenzene 10 09/28/23 08:03 V38465MSA
10.4 µg/L 2.00 5.00sec-Butyl benzene 10 09/28/23 08:03 V38465MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 09/28/23 08:03 V38465MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 09/28/23 08:03 V38465MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 09/28/23 08:03 V38465MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 09/28/23 08:03 V38465MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 09/28/23 08:03 V38465MSA
<2.20 µg/L 2.20 5.00Chloroform 10 09/28/23 08:03 V38465MSA
<2.20 M µg/L 2.20 5.00Chloromethane 10 09/28/23 08:03 V38465MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 09/28/23 08:03 V38465MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 09/28/23 08:03 V38465MSA
7.70 M µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 09/28/23 08:03 V38465MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 09/28/23 08:03 V38465MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 09/28/23 08:03 V38465MSA
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 09/28/23 08:03 V38465MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 09/28/23 08:03 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 59 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-7
96064 Matrix:
9/21/2023 16:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 09/28/23 08:03 V38465MSA
<12.0 M µg/L 12.0 50.0Dichlorodifluoromethane 10 09/28/23 08:03 V38465MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 09/28/23 08:03 V38465MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 09/28/23 08:03 V38465MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 09/28/23 08:03 V38465MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 09/28/23 08:03 V38465MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 09/28/23 08:03 V38465MSA
<1.90 M µg/L 1.90 5.001,2-Dichloropropane 10 09/28/23 08:03 V38465MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 09/28/23 08:03 V38465MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 09/28/23 08:03 V38465MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 09/28/23 08:03 V38465MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 09/28/23 08:03 V38465MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 09/28/23 08:03 V38465MSA
<420 µg/L 420 2000Ethanol 10 09/28/23 08:03 V38465MSA
204 µg/L 1.70 5.00Ethylbenzene 10 09/28/23 08:03 V38465MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 09/28/23 08:03 V38465MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 09/28/23 08:03 V38465MSA
37.2 µg/L 1.80 5.00Isopropylbenzene 10 09/28/23 08:03 V38465MSA
12.1 µg/L 0.890 5.004-Isopropyl toluene 10 09/28/23 08:03 V38465MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 09/28/23 08:03 V38465MSA
399 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 09/28/23 08:03 V38465MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 09/28/23 08:03 V38465MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 09/28/23 08:03 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 60 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-7
96064 Matrix:
9/21/2023 16:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
615 µg/L 4.70 10.0Naphthalene 10 09/28/23 08:03 V38465MSA
49.6 µg/L 1.90 5.00n-Propylbenzene 10 09/28/23 08:03 V38465MSA
<2.20 µg/L 2.20 5.00Styrene 10 09/28/23 08:03 V38465MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 09/28/23 08:03 V38465MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 09/28/23 08:03 V38465MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 09/28/23 08:03 V38465MSA
9.96 µg/L 2.20 5.00Toluene 10 09/28/23 08:03 V38465MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 09/28/23 08:03 V38465MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 09/28/23 08:03 V38465MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 09/28/23 08:03 V38465MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 09/28/23 08:03 V38465MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 09/28/23 08:03 V38465MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 09/28/23 08:03 V38465MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 09/28/23 08:03 V38465MSA
680 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 09/28/23 08:03 V38465MSA
152 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 09/28/23 08:03 V38465MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 09/28/23 08:03 V38465MSA
<1.70 M µg/L 1.70 5.00Vinyl Chloride 10 09/28/23 08:03 V38465MSA
553 µg/L 2.10 5.00o-Xylene 10 09/28/23 08:03 V38465MSA
639 µg/L 4.20 10.0m,p-Xylene 10 09/28/23 08:03 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 61 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-7
96064 Matrix:
9/21/2023 16:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
1190 µg/L 2.10 5.00Xylene (Total)10 09/28/23 08:03 V38465
Surrogate: 4-Bromofluorobenzene 91.6 Limits: 70-130%09/28/23 08:0310 MSA V38465
Surrogate: Dibromofluoromethane 99.0 Limits: 70-130%09/28/23 08:0310 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%09/28/23 08:0310 MSA V38465
Surrogate: Toluene-d8 95.6 Limits: 70-130%09/28/23 08:0310 MSA V38465
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 62 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-8
96065 Matrix:
9/21/2023 15:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<180 µg/L 180 1000Acetone 100 09/28/23 10:57 V38465MSA
1790 µg/L 18.0 50.0Benzene 100 09/28/23 10:57 V38465MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 09/28/23 10:57 V38465MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 09/28/23 10:57 V38465MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 09/28/23 10:57 V38465MSA
<150 µg/L 150 500Bromoform 100 09/28/23 10:57 V38465MSA
<28.0 µg/L 28.0 100Bromomethane 100 09/28/23 10:57 V38465MSA
23.0 J µg/L 18.0 50.0n-Butylbenzene 100 09/28/23 10:57 V38465MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 09/28/23 10:57 V38465MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 09/28/23 10:57 V38465MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 09/28/23 10:57 V38465MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 09/28/23 10:57 V38465MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 09/28/23 10:57 V38465MSA
<43.0 µg/L 43.0 100Chloroethane 100 09/28/23 10:57 V38465MSA
<22.0 µg/L 22.0 50.0Chloroform 100 09/28/23 10:57 V38465MSA
<22.0 M µg/L 22.0 50.0Chloromethane 100 09/28/23 10:57 V38465MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 09/28/23 10:57 V38465MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 09/28/23 10:57 V38465MSA
<50.0 M µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 09/28/23 10:57 V38465MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 09/28/23 10:57 V38465MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 09/28/23 10:57 V38465MSA
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 09/28/23 10:57 V38465MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 09/28/23 10:57 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 63 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-8
96065 Matrix:
9/21/2023 15:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 09/28/23 10:57 V38465MSA
<120 M µg/L 120 500Dichlorodifluoromethane 100 09/28/23 10:57 V38465MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 09/28/23 10:57 V38465MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 09/28/23 10:57 V38465MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 09/28/23 10:57 V38465MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 09/28/23 10:57 V38465MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 09/28/23 10:57 V38465MSA
<19.0 M µg/L 19.0 50.01,2-Dichloropropane 100 09/28/23 10:57 V38465MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 09/28/23 10:57 V38465MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 09/28/23 10:57 V38465MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 09/28/23 10:57 V38465MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 09/28/23 10:57 V38465MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 09/28/23 10:57 V38465MSA
<4200 µg/L 4200 20000Ethanol 100 09/28/23 10:57 V38465MSA
820 µg/L 17.0 50.0Ethylbenzene 100 09/28/23 10:57 V38465MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 09/28/23 10:57 V38465MSA
<38.0 µg/L 38.0 1002-Hexanone 100 09/28/23 10:57 V38465MSA
62.9 µg/L 18.0 50.0Isopropylbenzene 100 09/28/23 10:57 V38465MSA
22.2 J µg/L 8.90 50.04-Isopropyl toluene 100 09/28/23 10:57 V38465MSA
<71.0 µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 09/28/23 10:57 V38465MSA
218 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 09/28/23 10:57 V38465MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 09/28/23 10:57 V38465MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 09/28/23 10:57 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 64 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-8
96065 Matrix:
9/21/2023 15:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
826 µg/L 47.0 100Naphthalene 100 09/28/23 10:57 V38465MSA
102 µg/L 19.0 50.0n-Propylbenzene 100 09/28/23 10:57 V38465MSA
<22.0 µg/L 22.0 50.0Styrene 100 09/28/23 10:57 V38465MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 09/28/23 10:57 V38465MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 09/28/23 10:57 V38465MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 09/28/23 10:57 V38465MSA
43.7 J µg/L 22.0 50.0Toluene 100 09/28/23 10:57 V38465MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 09/28/23 10:57 V38465MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 09/28/23 10:57 V38465MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 09/28/23 10:57 V38465MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 09/28/23 10:57 V38465MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 09/28/23 10:57 V38465MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 09/28/23 10:57 V38465MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 09/28/23 10:57 V38465MSA
122 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 09/28/23 10:57 V38465MSA
80.5 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 09/28/23 10:57 V38465MSA
<100 µg/L 100 500Vinyl Acetate 100 09/28/23 10:57 V38465MSA
<17.0 M µg/L 17.0 50.0Vinyl Chloride 100 09/28/23 10:57 V38465MSA
26.7 J µg/L 21.0 50.0o-Xylene 100 09/28/23 10:57 V38465MSA
140 µg/L 42.0 100m,p-Xylene 100 09/28/23 10:57 V38465MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 65 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:PMW-8
96065 Matrix:
9/21/2023 15:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38464 09/27/23 14:00
167 J µg/L 21.0 50.0Xylene (Total)100 09/28/23 10:57 V38465
Surrogate: 4-Bromofluorobenzene 88.0 Limits: 70-130%09/28/23 10:57100 MSA V38465
Surrogate: Dibromofluoromethane 100 Limits: 70-130%09/28/23 10:57100 MSA V38465
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%09/28/23 10:57100 MSA V38465
Surrogate: Toluene-d8 95.6 Limits: 70-130%09/28/23 10:57100 MSA V38465
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 66 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TW-1
96066 Matrix:
9/21/2023 17:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/28/23 16:55 V38531MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/28/23 16:55 V38531MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/28/23 16:55 V38531MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/28/23 16:55 V38531MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/28/23 16:55 V38531MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/28/23 16:55 V38531MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/28/23 16:55 V38531MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/28/23 16:55 V38531MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/28/23 16:55 V38531MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/28/23 16:55 V38531MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/28/23 16:55 V38531MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/28/23 16:55 V38531MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/28/23 16:55 V38531MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/28/23 16:55 V38531MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/28/23 16:55 V38531MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/28/23 16:55 V38531MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/28/23 16:55 V38531MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/28/23 16:55 V38531MSA
<0.500 M µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/28/23 16:55 V38531MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/28/23 16:55 V38531MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/28/23 16:55 V38531MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/28/23 16:55 V38531MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/28/23 16:55 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 67 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TW-1
96066 Matrix:
9/21/2023 17:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/28/23 16:55 V38531MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/28/23 16:55 V38531MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/28/23 16:55 V38531MSA
6.94 µg/L 0.150 0.5001,2-Dichloroethane 1 09/28/23 16:55 V38531MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/28/23 16:55 V38531MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/28/23 16:55 V38531MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/28/23 16:55 V38531MSA
0.520 µg/L 0.190 0.5001,2-Dichloropropane 1 09/28/23 16:55 V38531MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/28/23 16:55 V38531MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/28/23 16:55 V38531MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/28/23 16:55 V38531MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/28/23 16:55 V38531MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/28/23 16:55 V38531MSA
<42.0 M µg/L 42.0 200Ethanol 1 09/28/23 16:55 V38531MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/28/23 16:55 V38531MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/28/23 16:55 V38531MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/28/23 16:55 V38531MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/28/23 16:55 V38531MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/28/23 16:55 V38531MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/28/23 16:55 V38531MSA
0.578 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/28/23 16:55 V38531MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/28/23 16:55 V38531MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/28/23 16:55 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 68 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TW-1
96066 Matrix:
9/21/2023 17:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/28/23 16:55 V38531MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/28/23 16:55 V38531MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/28/23 16:55 V38531MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/28/23 16:55 V38531MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/28/23 16:55 V38531MSA
0.590 µg/L 0.220 0.500Tetrachloroethene 1 09/28/23 16:55 V38531MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/28/23 16:55 V38531MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/28/23 16:55 V38531MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/28/23 16:55 V38531MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/28/23 16:55 V38531MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/28/23 16:55 V38531MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/28/23 16:55 V38531MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/28/23 16:55 V38531MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/28/23 16:55 V38531MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/28/23 16:55 V38531MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/28/23 16:55 V38531MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/28/23 16:55 V38531MSA
<0.170 M µg/L 0.170 0.500Vinyl Chloride 1 09/28/23 16:55 V38531MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/28/23 16:55 V38531MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/28/23 16:55 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 69 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TW-1
96066 Matrix:
9/21/2023 17:09
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/28/23 16:55 V38531
Surrogate: 4-Bromofluorobenzene 89.4 Limits: 70-130%09/28/23 16:551 MSA V38531
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%09/28/23 16:551 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 105 Limits: 70-130%09/28/23 16:551 MSA V38531
Surrogate: Toluene-d8 94.0 Limits: 70-130%09/28/23 16:551 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 70 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TB
96067 Matrix:
9/21/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/28/23 15:41 V38531MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/28/23 15:41 V38531MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/28/23 15:41 V38531MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/28/23 15:41 V38531MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/28/23 15:41 V38531MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/28/23 15:41 V38531MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/28/23 15:41 V38531MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/28/23 15:41 V38531MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/28/23 15:41 V38531MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/28/23 15:41 V38531MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/28/23 15:41 V38531MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/28/23 15:41 V38531MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/28/23 15:41 V38531MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/28/23 15:41 V38531MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/28/23 15:41 V38531MSA
<0.220 M µg/L 0.220 0.500Chloromethane 1 09/28/23 15:41 V38531MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/28/23 15:41 V38531MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/28/23 15:41 V38531MSA
<0.500 M µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/28/23 15:41 V38531MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/28/23 15:41 V38531MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/28/23 15:41 V38531MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/28/23 15:41 V38531MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/28/23 15:41 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 71 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TB
96067 Matrix:
9/21/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/28/23 15:41 V38531MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/28/23 15:41 V38531MSA
<1.20 M µg/L 1.20 5.00Dichlorodifluoromethane 1 09/28/23 15:41 V38531MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/28/23 15:41 V38531MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/28/23 15:41 V38531MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/28/23 15:41 V38531MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/28/23 15:41 V38531MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/28/23 15:41 V38531MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/28/23 15:41 V38531MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/28/23 15:41 V38531MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/28/23 15:41 V38531MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/28/23 15:41 V38531MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/28/23 15:41 V38531MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/28/23 15:41 V38531MSA
<42.0 M µg/L 42.0 200Ethanol 1 09/28/23 15:41 V38531MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/28/23 15:41 V38531MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/28/23 15:41 V38531MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/28/23 15:41 V38531MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/28/23 15:41 V38531MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/28/23 15:41 V38531MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/28/23 15:41 V38531MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/28/23 15:41 V38531MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/28/23 15:41 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 72 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TB
96067 Matrix:
9/21/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/28/23 15:41 V38531MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/28/23 15:41 V38531MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/28/23 15:41 V38531MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/28/23 15:41 V38531MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/28/23 15:41 V38531MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/28/23 15:41 V38531MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/28/23 15:41 V38531MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/28/23 15:41 V38531MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/28/23 15:41 V38531MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/28/23 15:41 V38531MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/28/23 15:41 V38531MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/28/23 15:41 V38531MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/28/23 15:41 V38531MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/28/23 15:41 V38531MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/28/23 15:41 V38531MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/28/23 15:41 V38531MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/28/23 15:41 V38531MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/28/23 15:41 V38531MSA
<0.170 M µg/L 0.170 0.500Vinyl Chloride 1 09/28/23 15:41 V38531MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/28/23 15:41 V38531MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/28/23 15:41 V38531MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 73 of 101
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-265-0014
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #4400 Received : 09/22/2023
Fast Phil's #506
Report Date : 10/03/2023
Sample ID :
Lab No :
Sampled:TB
96067 Matrix:
9/21/2023 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V38530 09/28/23 09:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/28/23 15:41 V38531
Surrogate: 4-Bromofluorobenzene 92.4 Limits: 70-130%09/28/23 15:411 MSA V38531
Surrogate: Dibromofluoromethane 99.6 Limits: 70-130%09/28/23 15:411 MSA V38531
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%09/28/23 15:411 MSA V38531
Surrogate: Toluene-d8 91.0 Limits: 70-130%09/28/23 15:411 MSA V38531
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 74 of 101
Sample ID Report Lab NoLRB‐V38382 23‐265‐0014 LRB
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
No TICs Detected N.D. ug/L 1 625 9/28/2023 9:35 APANN V38427
Sample ID Report Lab No
MW‐9 23‐265‐0014 96062
Paramater Result Units
Dilution 
Factor Method Analysis Date/Time Analyst Batch ID
Toluene 989260 ug/L 1 625 9/28/2023 12:13 APANN V38427
Ethylbenzene 499670 ug/L 1 625 9/28/2023 12:13 APANN V38427
Benzene, dimethyl‐598000 ug/L 1 625 9/28/2023 12:13 APANN V38427
Benzene, ethyl‐methyl‐289630 ug/L 1 625 9/28/2023 12:13 APANN V38427
Benzene, trimethyl‐430620 ug/L 1 625 9/28/2023 12:13 APANN V38427
Page 75 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Metals Analysis
6010D
V38390QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V38250
Associated Lab Samples: 96062
LRB-V38250 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/26/23 23:260.0060.002<0.002mg/LLead
LCS-V38250Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1060.1060.100mg/LLead 80-120
V 95727-MS-V38250 V 95727-MSD-V38250Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.108 1050.1070.1000.1000.003mg/LLead 104 75-125 0.9 20.0
V 95727-PDS-V38250Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/26/23 23:391110.279mg/LLead
Page 1 of 23Date:10/03/2023 04:44 PM
Page 76 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38465QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38464
Associated Lab Samples: 96054, 96055, 96056, 96057, 96058, 96059, 96060, 96061, 96062, 96063, 96064, 96065
LRB-V38464 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 02:1710.01.80<1.80µg/LAcetone
09/28/23 02:170.5000.180<0.180µg/LBenzene
09/28/23 02:170.5000.210<0.210µg/LBromobenzene
09/28/23 02:171.000.420<0.420µg/LBromochloromethane
09/28/23 02:170.5000.160<0.160µg/LBromodichloromethane
09/28/23 02:175.001.50<1.50µg/LBromoform
09/28/23 02:171.000.280<0.280µg/LBromomethane
09/28/23 02:170.5000.180<0.180µg/Ln-Butylbenzene
09/28/23 02:170.5000.200<0.200µg/Lsec-Butyl benzene
09/28/23 02:172.000.920<0.920µg/Ltert-Butyl benzene
09/28/23 02:170.5000.180<0.180µg/LCarbon Tetrachloride
09/28/23 02:170.5000.190<0.190µg/LChlorobenzene
09/28/23 02:170.5000.190<0.190µg/LChlorodibromomethane
09/28/23 02:171.000.430<0.430µg/LChloroethane
09/28/23 02:170.5000.220<0.220µg/LChloroform
09/28/23 02:170.5000.220<0.220µg/LChloromethane
09/28/23 02:170.5000.200<0.200µg/L2-Chlorotoluene
09/28/23 02:170.5000.200<0.200µg/L4-Chlorotoluene
09/28/23 02:170.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/28/23 02:172.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/28/23 02:170.5000.230<0.230µg/LDibromomethane
09/28/23 02:170.5000.220<0.220µg/L1,2-Dichlorobenzene
09/28/23 02:170.5000.190<0.190µg/L1,3-Dichlorobenzene
09/28/23 02:170.5000.210<0.210µg/L1,4-Dichlorobenzene
09/28/23 02:175.001.20<1.20µg/LDichlorodifluoromethane
09/28/23 02:170.5000.240<0.240µg/L1,1-Dichloroethane
09/28/23 02:170.5000.150<0.150µg/L1,2-Dichloroethane
Page 2 of 23Date:10/03/2023 04:44 PM
Page 77 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38465QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38464
Associated Lab Samples: 96054, 96055, 96056, 96057, 96058, 96059, 96060, 96061, 96062, 96063, 96064, 96065
LRB-V38464 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 02:170.5000.150<0.150µg/L1,1-Dichloroethene
09/28/23 02:170.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/28/23 02:170.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/28/23 02:170.5000.190<0.190µg/L1,2-Dichloropropane
09/28/23 02:170.5000.130<0.130µg/L1,3-Dichloropropane
09/28/23 02:172.000.210<0.210µg/L2,2-Dichloropropane
09/28/23 02:170.5000.200<0.200µg/L1,1-Dichloropropene
09/28/23 02:170.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/28/23 02:170.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/28/23 02:1720042.0<42.0µg/LEthanol
09/28/23 02:170.5000.170<0.170µg/LEthylbenzene
09/28/23 02:173.000.350<0.350µg/LHexachlorobutadiene
09/28/23 02:171.000.380<0.380µg/L2-Hexanone
09/28/23 02:170.5000.180<0.180µg/LIsopropylbenzene
09/28/23 02:170.5000.089<0.089µg/L4-Isopropyl toluene
09/28/23 02:175.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/28/23 02:171.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/28/23 02:171.000.078<0.078µg/L4-Methyl-2-Pentanone
09/28/23 02:172.000.330<0.330µg/LMethylene Chloride
09/28/23 02:171.000.470<0.470µg/LNaphthalene
09/28/23 02:170.5000.190<0.190µg/Ln-Propylbenzene
09/28/23 02:170.5000.220<0.220µg/LStyrene
09/28/23 02:170.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
09/28/23 02:170.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/28/23 02:170.5000.220<0.220µg/LTetrachloroethene
09/28/23 02:170.5000.220<0.220µg/LToluene
09/28/23 02:170.5000.380<0.380µg/L1,2,3-Trichlorobenzene
Page 3 of 23Date:10/03/2023 04:44 PM
Page 78 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38465QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38464
Associated Lab Samples: 96054, 96055, 96056, 96057, 96058, 96059, 96060, 96061, 96062, 96063, 96064, 96065
LRB-V38464 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 02:170.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/28/23 02:170.5000.160<0.160µg/L1,1,1-Trichloroethane
09/28/23 02:170.5000.096<0.096µg/L1,1,2-Trichloroethane
09/28/23 02:170.5000.180<0.180µg/LTrichloroethene
09/28/23 02:170.5000.180<0.180µg/LTrichlorofluoromethane
09/28/23 02:170.5000.270<0.270µg/L1,2,3-Trichloropropane
09/28/23 02:170.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/28/23 02:170.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/28/23 02:175.001.00<1.00µg/LVinyl Acetate
09/28/23 02:170.5000.170<0.170µg/LVinyl Chloride
09/28/23 02:170.5000.210<0.210µg/Lo-Xylene
09/28/23 02:171.000.420<0.420µg/Lm,p-Xylene
09/28/23 02:174-Bromofluorobenzene (S)90.2 70-130
09/28/23 02:17Dibromofluoromethane (S)102 70-130
09/28/23 02:171,2-Dichloroethane - d4 (S)110 70-130
09/28/23 02:17Toluene-d8 (S)94.4 70-130
LCS-V38464 LCSD-V38464Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
35.0 87.584.733.940.0µg/LAcetone 40-160 3.1 20.0
17.8 89.085.017.020.0µg/LBenzene 70-130 4.5 20.0
18.7 93.590.518.120.0µg/LBromobenzene 70-130 3.2 20.0
20.7 10410320.520.0µg/LBromochloromethane 70-130 0.9 20.0
20.5 10310420.720.0µg/LBromodichloromethane 70-130 0.9 20.0
24.6 12312124.120.0µg/LBromoform 70-130 2.0 20.0
Page 4 of 23Date:10/03/2023 04:44 PM
Page 79 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38465QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38464
LCS-V38464 LCSD-V38464Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.6 88.083.016.620.0µg/LBromomethane 60-140 5.8 20.0
19.2 96.096.019.220.0µg/Ln-Butylbenzene 70-130 0.0 20.0
19.1 95.594.518.920.0µg/Lsec-Butyl benzene 70-130 1.0 20.0
20.4 10299.019.820.0µg/Ltert-Butyl benzene 70-130 2.9 20.0
24.5 12312023.920.0µg/LCarbon Tetrachloride 70-130 2.4 20.0
21.6 10810521.020.0µg/LChlorobenzene 70-130 2.8 20.0
22.8 11411222.320.0µg/LChlorodibromomethane 70-130 2.2 20.0
12.2 61.061.512.320.0µg/LChloroethane 60-140 0.8 20.0
19.7 98.599.519.920.0µg/LChloroform 70-130 1.0 20.0
9.22 46.1*44.5*8.9020.0µg/LChloromethane 60-140 3.5 20.0
18.3 91.587.017.420.0µg/L2-Chlorotoluene 70-130 5.0 20.0
18.9 94.592.518.520.0µg/L4-Chlorotoluene 70-130 2.1 20.0
13.0 65.0*67.0*13.420.0µg/LDi-Isopropyl Ether (DIPE)70-130 3.0 20.0
22.3 11212124.120.0µg/L1,2-Dibromo-3-Chloropropane 70-130 7.7 20.0
21.0 10511021.920.0µg/LDibromomethane 70-130 4.1 20.0
21.4 10710521.020.0µg/L1,2-Dichlorobenzene 70-130 1.8 20.0
21.1 10610621.220.0µg/L1,3-Dichlorobenzene 70-130 0.4 20.0
20.9 10510220.420.0µg/L1,4-Dichlorobenzene 70-130 2.4 20.0
10.4 52.0*51.5*10.320.0µg/LDichlorodifluoromethane 60-140 0.9 20.0
17.7 88.585.517.120.0µg/L1,1-Dichloroethane 70-130 3.4 20.0
22.4 11211322.520.0µg/L1,2-Dichloroethane 70-130 0.4 20.0
19.8 99.096.019.220.0µg/L1,1-Dichloroethene 70-130 3.0 20.0
17.8 89.088.017.620.0µg/Lcis-1,2-Dichloroethene 70-130 1.1 20.0
17.6 88.090.518.120.0µg/Ltrans-1,2-Dichloroethene 70-130 2.8 20.0
13.7 68.5*73.514.720.0µg/L1,2-Dichloropropane 70-130 7.0 20.0
17.6 88.088.517.720.0µg/L1,3-Dichloropropane 70-130 0.5 20.0
Page 5 of 23* QC Fail Date:10/03/2023 04:44 PM
Page 80 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38465QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38464
LCS-V38464 LCSD-V38464Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.3 10210320.520.0µg/L2,2-Dichloropropane 70-130 0.9 20.0
20.4 10299.519.920.0µg/L1,1-Dichloropropene 70-130 2.4 20.0
18.0 90.090.518.120.0µg/Lcis-1,3-Dichloropropene 70-130 0.5 20.0
20.4 10210320.520.0µg/Ltrans-1,3-Dichloropropene 70-130 0.4 20.0
381 76.275.8379500µg/LEthanol 60-140 0.5 20.0
19.7 98.596.519.320.0µg/LEthylbenzene 70-130 2.0 20.0
24.9 12512424.820.0µg/LHexachlorobutadiene 70-130 0.4 20.0
15.0 75.077.515.520.0µg/L2-Hexanone 60-140 3.2 20.0
20.4 10299.519.920.0µg/LIsopropylbenzene 70-130 2.4 20.0
21.6 10810721.420.0µg/L4-Isopropyl toluene 70-130 0.9 20.0
14.5 72.570.514.120.0µg/LMethyl Ethyl Ketone (MEK)60-140 2.7 20.0
19.9 99.510320.520.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.9 20.0
14.7 73.573.514.720.0µg/L4-Methyl-2-Pentanone 60-140 0.0 20.0
14.3 71.572.514.520.0µg/LMethylene Chloride 70-130 1.3 20.0
23.8 11912324.620.0µg/LNaphthalene 70-130 3.3 20.0
18.4 92.089.517.920.0µg/Ln-Propylbenzene 70-130 2.7 20.0
20.8 10410420.720.0µg/LStyrene 70-130 0.4 20.0
22.6 11311523.020.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.7 20.0
15.0 75.073.514.720.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.0 20.0
23.5 11811623.220.0µg/LTetrachloroethene 70-130 1.2 20.0
19.0 95.094.018.820.0µg/LToluene 70-130 1.0 20.0
28.1 141*149*29.820.0µg/L1,2,3-Trichlorobenzene 70-130 5.8 20.0
26.4 132*138*27.520.0µg/L1,2,4-Trichlorobenzene 70-130 4.0 20.0
24.0 12011923.720.0µg/L1,1,1-Trichloroethane 70-130 1.2 20.0
18.6 93.094.518.920.0µg/L1,1,2-Trichloroethane 70-130 1.6 20.0
22.8 11411422.720.0µg/LTrichloroethene 70-130 0.4 20.0
Page 6 of 23* QC Fail Date:10/03/2023 04:44 PM
Page 81 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38465QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38464
LCS-V38464 LCSD-V38464Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
23.2 11611923.820.0µg/LTrichlorofluoromethane 60-140 2.5 20.0
18.3 91.593.018.620.0µg/L1,2,3-Trichloropropane 70-130 1.6 20.0
20.5 10310320.620.0µg/L1,2,4-Trimethylbenzene 70-130 0.4 20.0
20.4 10210120.120.0µg/L1,3,5-Trimethylbenzene 70-130 1.4 20.0
15.5 77.583.516.720.0µg/LVinyl Acetate 60-140 7.4 20.0
10.4 52.0*51.5*10.320.0µg/LVinyl Chloride 60-140 0.9 20.0
20.2 10110120.120.0µg/Lo-Xylene 70-130 0.4 20.0
43.7 10910642.440.0µg/Lm,p-Xylene 70-130 3.0 20.0
87.288.64-Bromofluorobenzene (S)70-130
97.4101Dibromofluoromethane (S)70-130
1091111,2-Dichloroethane - d4 (S)70-130
96.697.8Toluene-d8 (S)70-130
Page 7 of 23* QC Fail Date:10/03/2023 04:44 PM
Page 82 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
Associated Lab Samples: 96057, 96058, 96059, 96061, 96062, 96066, 96067
LRB-V38530 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 15:1610.01.80<1.80µg/LAcetone
09/28/23 15:160.5000.180<0.180µg/LBenzene
09/28/23 15:160.5000.210<0.210µg/LBromobenzene
09/28/23 15:161.000.420<0.420µg/LBromochloromethane
09/28/23 15:160.5000.160<0.160µg/LBromodichloromethane
09/28/23 15:165.001.50<1.50µg/LBromoform
09/28/23 15:161.000.280<0.280µg/LBromomethane
09/28/23 15:160.5000.180<0.180µg/Ln-Butylbenzene
09/28/23 15:160.5000.200<0.200µg/Lsec-Butyl benzene
09/28/23 15:162.000.920<0.920µg/Ltert-Butyl benzene
09/28/23 15:160.5000.180<0.180µg/LCarbon Tetrachloride
09/28/23 15:160.5000.190<0.190µg/LChlorobenzene
09/28/23 15:160.5000.190<0.190µg/LChlorodibromomethane
09/28/23 15:161.000.430<0.430µg/LChloroethane
09/28/23 15:160.5000.220<0.220µg/LChloroform
09/28/23 15:160.5000.220<0.220µg/LChloromethane
09/28/23 15:160.5000.200<0.200µg/L2-Chlorotoluene
09/28/23 15:160.5000.200<0.200µg/L4-Chlorotoluene
09/28/23 15:160.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/28/23 15:162.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/28/23 15:160.5000.200<0.200µg/L1,2-Dibromoethane
09/28/23 15:160.5000.230<0.230µg/LDibromomethane
09/28/23 15:160.5000.220<0.220µg/L1,2-Dichlorobenzene
09/28/23 15:160.5000.190<0.190µg/L1,3-Dichlorobenzene
09/28/23 15:160.5000.210<0.210µg/L1,4-Dichlorobenzene
09/28/23 15:165.001.20<1.20µg/LDichlorodifluoromethane
09/28/23 15:160.5000.240<0.240µg/L1,1-Dichloroethane
Page 8 of 23Date:10/03/2023 04:44 PM
Page 83 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
Associated Lab Samples: 96057, 96058, 96059, 96061, 96062, 96066, 96067
LRB-V38530 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 15:160.5000.150<0.150µg/L1,2-Dichloroethane
09/28/23 15:160.5000.150<0.150µg/L1,1-Dichloroethene
09/28/23 15:160.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/28/23 15:160.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/28/23 15:160.5000.190<0.190µg/L1,2-Dichloropropane
09/28/23 15:160.5000.130<0.130µg/L1,3-Dichloropropane
09/28/23 15:162.000.210<0.210µg/L2,2-Dichloropropane
09/28/23 15:160.5000.200<0.200µg/L1,1-Dichloropropene
09/28/23 15:160.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/28/23 15:160.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/28/23 15:1620042.0<42.0µg/LEthanol
09/28/23 15:160.5000.170<0.170µg/LEthylbenzene
09/28/23 15:163.000.350<0.350µg/LHexachlorobutadiene
09/28/23 15:161.000.380<0.380µg/L2-Hexanone
09/28/23 15:160.5000.180<0.180µg/LIsopropylbenzene
09/28/23 15:160.5000.089<0.089µg/L4-Isopropyl toluene
09/28/23 15:165.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/28/23 15:161.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/28/23 15:161.000.078<0.078µg/L4-Methyl-2-Pentanone
09/28/23 15:162.000.330<0.330µg/LMethylene Chloride
09/28/23 15:161.000.470<0.470µg/LNaphthalene
09/28/23 15:160.5000.190<0.190µg/Ln-Propylbenzene
09/28/23 15:160.5000.220<0.220µg/LStyrene
09/28/23 15:160.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
09/28/23 15:160.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/28/23 15:160.5000.220<0.220µg/LTetrachloroethene
09/28/23 15:160.5000.220<0.220µg/LToluene
Page 9 of 23Date:10/03/2023 04:44 PM
Page 84 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
Associated Lab Samples: 96057, 96058, 96059, 96061, 96062, 96066, 96067
LRB-V38530 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 15:160.5000.380<0.380µg/L1,2,3-Trichlorobenzene
09/28/23 15:160.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/28/23 15:160.5000.160<0.160µg/L1,1,1-Trichloroethane
09/28/23 15:160.5000.096<0.096µg/L1,1,2-Trichloroethane
09/28/23 15:160.5000.180<0.180µg/LTrichloroethene
09/28/23 15:160.5000.180<0.180µg/LTrichlorofluoromethane
09/28/23 15:160.5000.270<0.270µg/L1,2,3-Trichloropropane
09/28/23 15:160.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/28/23 15:160.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/28/23 15:165.001.00<1.00µg/LVinyl Acetate
09/28/23 15:160.5000.170<0.170µg/LVinyl Chloride
09/28/23 15:160.5000.210<0.210µg/Lo-Xylene
09/28/23 15:161.000.420<0.420µg/Lm,p-Xylene
09/28/23 15:164-Bromofluorobenzene (S)90.4 70-130
09/28/23 15:16Dibromofluoromethane (S)100 70-130
09/28/23 15:161,2-Dichloroethane - d4 (S)108 70-130
09/28/23 15:16Toluene-d8 (S)90.2 70-130
LCS-V38530 LCSD-V38530Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.8 10210843.040.0µg/LAcetone 40-160 5.2 20.0
18.5 92.592.018.420.0µg/LBenzene 70-130 0.5 20.0
20.0 10098.519.720.0µg/LBromobenzene 70-130 1.5 20.0
22.7 11411322.520.0µg/LBromochloromethane 70-130 0.8 20.0
21.5 10810721.420.0µg/LBromodichloromethane 70-130 0.4 20.0
Page 10 of 23Date:10/03/2023 04:44 PM
Page 85 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
LCS-V38530 LCSD-V38530Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
25.4 12712725.420.0µg/LBromoform 70-130 0.0 20.0
18.0 90.090.518.120.0µg/LBromomethane 60-140 0.5 20.0
20.8 10410520.920.0µg/Ln-Butylbenzene 70-130 0.4 20.0
21.1 10610220.420.0µg/Lsec-Butyl benzene 70-130 3.3 20.0
22.4 11210821.620.0µg/Ltert-Butyl benzene 70-130 3.6 20.0
28.2 141*137*27.420.0µg/LCarbon Tetrachloride 70-130 2.8 20.0
21.7 10911122.120.0µg/LChlorobenzene 70-130 1.8 20.0
23.4 11711723.420.0µg/LChlorodibromomethane 70-130 0.0 20.0
12.3 61.564.512.920.0µg/LChloroethane 60-140 4.7 20.0
20.9 10510520.920.0µg/LChloroform 70-130 0.0 20.0
9.44 47.2*44.6*8.9320.0µg/LChloromethane 60-140 5.5 20.0
19.7 98.596.519.320.0µg/L2-Chlorotoluene 70-130 2.0 20.0
20.6 10398.019.620.0µg/L4-Chlorotoluene 70-130 4.9 20.0
13.5 67.5*67.5*13.520.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.0 20.0
25.9 13012725.320.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.3 20.0
19.7 98.510220.320.0µg/L1,2-Dibromoethane 70-130 3.0 20.0
21.9 11010120.220.0µg/LDibromomethane 70-130 8.0 20.0
22.9 11511222.420.0µg/L1,2-Dichlorobenzene 70-130 2.2 20.0
23.0 11511522.920.0µg/L1,3-Dichlorobenzene 70-130 0.4 20.0
22.5 11310821.620.0µg/L1,4-Dichlorobenzene 70-130 4.0 20.0
9.80 49.0*49.6*9.9220.0µg/LDichlorodifluoromethane 60-140 1.2 20.0
17.9 89.588.017.620.0µg/L1,1-Dichloroethane 70-130 1.6 20.0
21.7 10910921.820.0µg/L1,2-Dichloroethane 70-130 0.4 20.0
17.5 87.510120.220.0µg/L1,1-Dichloroethene 70-130 14.3 20.0
17.9 89.591.018.220.0µg/Lcis-1,2-Dichloroethene 70-130 1.6 20.0
19.4 97.092.518.520.0µg/Ltrans-1,2-Dichloroethene 70-130 4.7 20.0
Page 11 of 23Date:10/03/2023 04:44 PM
Page 86 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
LCS-V38530 LCSD-V38530Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
14.8 74.074.514.920.0µg/L1,2-Dichloropropane 70-130 0.6 20.0
18.4 92.093.518.720.0µg/L1,3-Dichloropropane 70-130 1.6 20.0
25.4 12712925.720.0µg/L2,2-Dichloropropane 70-130 1.1 20.0
22.4 11210921.820.0µg/L1,1-Dichloropropene 70-130 2.7 20.0
19.2 96.099.519.920.0µg/Lcis-1,3-Dichloropropene 70-130 3.5 20.0
21.0 10510821.520.0µg/Ltrans-1,3-Dichloropropene 70-130 2.3 20.0
297 59.4*86.8434500µg/LEthanol 60-140 37.4*20.0
20.2 10199.519.920.0µg/LEthylbenzene 70-130 1.4 20.0
27.2 136*131*26.220.0µg/LHexachlorobutadiene 70-130 3.7 20.0
15.4 77.080.516.120.0µg/L2-Hexanone 60-140 4.4 20.0
22.4 11210721.420.0µg/LIsopropylbenzene 70-130 4.5 20.0
23.4 11711422.820.0µg/L4-Isopropyl toluene 70-130 2.5 20.0
15.7 78.581.516.320.0µg/LMethyl Ethyl Ketone (MEK)60-140 3.7 20.0
20.7 10410521.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.4 20.0
14.2 71.072.514.520.0µg/L4-Methyl-2-Pentanone 60-140 2.0 20.0
14.6 73.072.014.420.0µg/LMethylene Chloride 70-130 1.3 20.0
25.9 13012224.420.0µg/LNaphthalene 70-130 5.9 20.0
19.9 99.598.519.720.0µg/Ln-Propylbenzene 70-130 1.0 20.0
21.3 10710921.720.0µg/LStyrene 70-130 1.8 20.0
24.5 12312124.120.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.6 20.0
17.6 88.083.516.720.0µg/L1,1,2,2-Tetrachloroethane 70-130 5.2 20.0
24.5 12312124.220.0µg/LTetrachloroethene 70-130 1.2 20.0
19.7 98.596.519.320.0µg/LToluene 70-130 2.0 20.0
32.1 161*157*31.420.0µg/L1,2,3-Trichlorobenzene 70-130 2.2 20.0
29.2 146*144*28.720.0µg/L1,2,4-Trichlorobenzene 70-130 1.7 20.0
24.9 12512124.120.0µg/L1,1,1-Trichloroethane 70-130 3.2 20.0
Page 12 of 23* QC Fail Date:10/03/2023 04:44 PM
Page 87 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38530
LCS-V38530 LCSD-V38530Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.3 96.597.519.520.0µg/L1,1,2-Trichloroethane 70-130 1.0 20.0
22.7 11411322.620.0µg/LTrichloroethene 70-130 0.4 20.0
23.6 11811923.720.0µg/LTrichlorofluoromethane 60-140 0.4 20.0
21.4 10710120.120.0µg/L1,2,3-Trichloropropane 70-130 6.2 20.0
22.4 11211122.120.0µg/L1,2,4-Trimethylbenzene 70-130 1.3 20.0
22.2 11111021.920.0µg/L1,3,5-Trimethylbenzene 70-130 1.3 20.0
25.7 12912725.420.0µg/LVinyl Acetate 60-140 1.1 20.0
10.6 53.0*54.0*10.820.0µg/LVinyl Chloride 60-140 1.8 20.0
21.0 10510320.520.0µg/Lo-Xylene 70-130 2.4 20.0
45.0 11311044.140.0µg/Lm,p-Xylene 70-130 2.0 20.0
91.090.64-Bromofluorobenzene (S)70-130
98.6102Dibromofluoromethane (S)70-130
1021061,2-Dichloroethane - d4 (S)70-130
96.296.2Toluene-d8 (S)70-130
Page 13 of 23* QC Fail Date:10/03/2023 04:44 PM
Page 88 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V38609QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V38608
Associated Lab Samples: 96061
LRB-V38608 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/02/23 16:330.5000.190<0.190µg/L1,2,4-Trimethylbenzene
10/02/23 16:334-Bromofluorobenzene (S)104 70-130
10/02/23 16:33Dibromofluoromethane (S)96.0 70-130
10/02/23 16:331,2-Dichloroethane - d4 (S)90.6 70-130
10/02/23 16:33Toluene-d8 (S)101 70-130
LCS-V38608 LCSD-V38608Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.6 10811021.920.0µg/L1,2,4-Trimethylbenzene 70-130 1.3 20.0
1001004-Bromofluorobenzene (S)70-130
96.494.8Dibromofluoromethane (S)70-130
94.293.21,2-Dichloroethane - d4 (S)70-130
100101Toluene-d8 (S)70-130
Page 14 of 23Date:10/03/2023 04:44 PM
Page 89 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V38427QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V38382
Associated Lab Samples: 96062
LRB-V38382 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 09:352.000.302<0.302µg/LAcenaphthene
09/28/23 09:352.000.297<0.297µg/LAcenaphthylene
09/28/23 09:352.000.836<0.836µg/LAnthracene
09/28/23 09:3510.01.32<1.32µg/LBenzidine
09/28/23 09:352.000.637<0.637µg/LBenzo(a)anthracene
09/28/23 09:352.001.02<1.02µg/LBenzo(a)pyrene
09/28/23 09:355.002.49<2.49µg/LBenzo(b)fluoranthene
09/28/23 09:355.001.01<1.01µg/LBenzo(g,h,i)perylene
09/28/23 09:355.001.99<1.99µg/LBenzo(k)fluoranthene
09/28/23 09:3510.01.10<1.10µg/LBenzoic Acid
09/28/23 09:355.000.684<0.684µg/LBenzyl alcohol
09/28/23 09:355.000.468<0.468µg/LBis(2-Chloroethoxy)methane
09/28/23 09:355.001.04<1.04µg/LBis(2-Chloroethyl)ether
09/28/23 09:355.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
09/28/23 09:3510.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
09/28/23 09:355.001.11<1.11µg/L4-Bromophenyl phenyl ether
09/28/23 09:355.001.83<1.83µg/LButyl benzyl phthalate
09/28/23 09:355.001.18<1.18µg/L4-Chloro-3-methylphenol
09/28/23 09:3520.07.38<7.38µg/L2-Chloronaphthalene
09/28/23 09:3510.00.938<0.938µg/L2-Chlorophenol
09/28/23 09:355.001.71<1.71µg/L4-Chlorophenyl phenyl ether
09/28/23 09:352.000.405<0.405µg/LChrysene
09/28/23 09:352.000.434<0.434µg/LDibenz(a,h)anthracene
09/28/23 09:355.000.856<0.856µg/LDibenzofuran
09/28/23 09:355.002.00<2.00µg/L1,2-Dichlorobenzene
09/28/23 09:355.002.00<2.00µg/L1,3-Dichlorobenzene
09/28/23 09:355.002.05<2.05µg/L1,4-Dichlorobenzene
Page 15 of 23Date:10/03/2023 04:44 PM
Page 90 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V38427QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V38382
Associated Lab Samples: 96062
LRB-V38382 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 09:355.001.89<1.89µg/L3,3'-Dichlorobenzidine
09/28/23 09:3510.01.46<1.46µg/L2,4-Dichlorophenol
09/28/23 09:355.000.745<0.745µg/LDiethyl phthalate
09/28/23 09:355.000.939<0.939µg/LDimethyl phthalate
09/28/23 09:3520.01.57<1.57µg/L2,4-Dimethylphenol
09/28/23 09:355.002.06<2.06µg/LDi-n-butyl phthalate
09/28/23 09:3510.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
09/28/23 09:3510.01.92<1.92µg/L2,4-Dinitrophenol
09/28/23 09:355.001.11<1.11µg/L2,4-Dinitrotoluene
09/28/23 09:355.000.809<0.809µg/L2,6-Dinitrotoluene
09/28/23 09:355.001.65<1.65µg/LDi-n-Octyl Phthalate
09/28/23 09:352.000.250<0.250µg/LFluoranthene
09/28/23 09:352.000.807<0.807µg/LFluorene
09/28/23 09:355.000.979<0.979µg/LHexachlorobenzene
09/28/23 09:355.002.73<2.73µg/LHexachlorobutadiene
09/28/23 09:355.002.05<2.05µg/LHexachlorocyclopentadiene
09/28/23 09:355.001.76<1.76µg/LHexachloroethane
09/28/23 09:352.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
09/28/23 09:355.000.444<0.444µg/LIsophorone
09/28/23 09:352.001.14<1.14µg/L1-Methylnaphthalene
09/28/23 09:352.000.666<0.666µg/L2-Methylnaphthalene
09/28/23 09:352.000.728<0.728µg/LNaphthalene
09/28/23 09:355.000.905<0.905µg/LNitrobenzene
09/28/23 09:355.000.493<0.493µg/L2-Nitrophenol
09/28/23 09:3510.01.23<1.23µg/L4-Nitrophenol
09/28/23 09:355.001.10<1.10µg/LN-Nitrosodiphenylamine
09/28/23 09:355.000.641<0.641µg/LN-Nitroso-di-n-propylamine
Page 16 of 23Date:10/03/2023 04:44 PM
Page 91 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V38427QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V38382
Associated Lab Samples: 96062
LRB-V38382 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/28/23 09:355.001.43<1.43µg/LPentachlorophenol
09/28/23 09:352.000.428<0.428µg/LPhenanthrene
09/28/23 09:355.000.651<0.651µg/LPhenol
09/28/23 09:352.000.434<0.434µg/LPyrene
09/28/23 09:355.002.21<2.21µg/L1,2,4-Trichlorobenzene
09/28/23 09:355.001.32<1.32µg/L2,4,6-Trichlorophenol
09/28/23 09:352-Fluorobiphenyl (S)76.8 49-118
09/28/23 09:352-Fluorophenol (S)42.8 22-84
09/28/23 09:35Nitrobenzene-d5 (S)70.4 43-123
09/28/23 09:354-Terphenyl-d14 (S)84.8 49-151
09/28/23 09:352,4,6-Tribromophenol (S)83.5 31-144
09/28/23 09:35Phenol-d5 (S)28.3 10-63
LCS-V38382 LCSD-V38382Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.6 75.275.837.950.0µg/LAcenaphthene 47-145 0.7 20.0
38.9 77.878.239.150.0µg/LAcenaphthylene 33-145 0.5 20.0
41.1 82.282.241.150.0µg/LAnthracene 27-133 0.0 20.0
19.6 39.256.828.450.0µg/LBenzidine 15-150 36.6*20.0
38.9 77.877.438.750.0µg/LBenzo(a)anthracene 33-143 0.5 20.0
48.8 97.697.648.850.0µg/LBenzo(a)pyrene 17-163 0.0 20.0
47.0 94.093.246.650.0µg/LBenzo(b)fluoranthene 24-159 0.8 20.0
44.0 88.086.643.350.0µg/LBenzo(g,h,i)perylene 10-219 1.6 20.0
43.0 86.087.443.750.0µg/LBenzo(k)fluoranthene 11-162 1.6 20.0
17.3 34.625.812.950.0µg/LBenzoic Acid 10-125 29.1*20.0
Page 17 of 23* QC Fail Date:10/03/2023 04:44 PM
Page 92 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V38427QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V38382
LCS-V38382 LCSD-V38382Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
34.7 69.469.034.550.0µg/LBenzyl alcohol 16-107 0.5 20.0
34.1 68.268.034.050.0µg/LBis(2-Chloroethoxy)methane 33-184 0.2 20.0
32.8 65.667.433.750.0µg/LBis(2-Chloroethyl)ether 12-158 2.7 20.0
32.4 64.866.033.050.0µg/LBis(2-Chloroisopropyl)ether 36-166 1.8 20.0
39.2 78.477.038.550.0µg/LBis(2-ethylhexyl)phthalate 10-158 1.8 20.0
42.5 85.082.841.450.0µg/L4-Bromophenyl phenyl ether 53-127 2.6 20.0
38.5 77.076.238.150.0µg/LButyl benzyl phthalate 10-152 1.0 20.0
35.2 70.470.435.250.0µg/L4-Chloro-3-methylphenol 22-147 0.0 20.0
38.1 76.275.837.950.0µg/L2-Chloronaphthalene 60-118 0.5 20.0
33.5 67.068.434.250.0µg/L2-Chlorophenol 23-134 2.0 20.0
41.5 83.083.241.650.0µg/L4-Chlorophenyl phenyl ether 25-158 0.2 20.0
39.8 79.679.439.750.0µg/LChrysene 17-168 0.2 20.0
38.5 77.078.639.350.0µg/LDibenz(a,h)anthracene 10-227 2.0 20.0
38.7 77.477.838.950.0µg/LDibenzofuran 39-114 0.5 20.0
29.9 59.862.631.350.0µg/L1,2-Dichlorobenzene 32-129 4.5 20.0
29.9 59.860.830.450.0µg/L1,3-Dichlorobenzene 20-124 1.6 20.0
29.1 58.261.230.650.0µg/L1,4-Dichlorobenzene 20-124 5.0 20.0
43.6 87.288.444.250.0µg/L3,3'-Dichlorobenzidine 10-262 1.3 20.0
36.8 73.672.636.350.0µg/L2,4-Dichlorophenol 39-135 1.3 20.0
41.1 82.281.440.750.0µg/LDiethyl phthalate 10-114 0.9 20.0
42.3 84.684.842.450.0µg/LDimethyl phthalate 10-112 0.2 20.0
47.2 94.492.046.050.0µg/L2,4-Dimethylphenol 32-119 2.5 20.0
44.0 88.086.243.150.0µg/LDi-n-butyl phthalate 10-118 2.0 20.0
43.9 87.886.043.050.0µg/L4,6-Dinitro-2-methylphenol 10-181 2.0 20.0
38.5 77.075.237.650.0µg/L2,4-Dinitrophenol 10-191 2.3 20.0
43.0 86.084.842.450.0µg/L2,4-Dinitrotoluene 39-139 1.4 20.0
Page 18 of 23Date:10/03/2023 04:44 PM
Page 93 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V38427QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V38382
LCS-V38382 LCSD-V38382Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
42.2 84.485.242.650.0µg/L2,6-Dinitrotoluene 50-158 0.9 20.0
45.6 91.290.445.250.0µg/LDi-n-Octyl Phthalate 10-146 0.8 20.0
38.4 76.875.237.650.0µg/LFluoranthene 26-137 2.1 20.0
39.4 78.878.039.050.0µg/LFluorene 59-121 1.0 20.0
43.7 87.486.643.350.0µg/LHexachlorobenzene 10-152 0.9 20.0
30.3 60.661.230.650.0µg/LHexachlorobutadiene 24-116 0.9 20.0
39.7 79.476.638.350.0µg/LHexachlorocyclopentadiene 32-117 3.5 20.0
27.6 55.256.028.050.0µg/LHexachloroethane 40-113 1.4 20.0
44.6 89.289.844.950.0µg/LIndeno(1,2,3-cd)pyrene 10-171 0.6 20.0
31.1 62.262.431.250.0µg/LIsophorone 21-196 0.3 20.0
30.3 60.660.830.450.0µg/L1-Methylnaphthalene 40-135 0.3 20.0
30.5 61.060.830.450.0µg/L2-Methylnaphthalene 18-121 0.3 20.0
29.7 59.459.429.750.0µg/LNaphthalene 21-133 0.0 20.0
28.7 57.457.028.550.0µg/LNitrobenzene 35-180 0.6 20.0
33.1 66.266.433.250.0µg/L2-Nitrophenol 29-182 0.3 20.0
17.3 34.634.217.150.0µg/L4-Nitrophenol 10-132 1.1 20.0
48.1 96.297.048.550.0µg/LN-Nitrosodiphenylamine 69-152 0.8 20.0
36.2 72.471.835.950.0µg/LN-Nitroso-di-n-propylamine 10-230 0.8 20.0
44.6 89.286.043.050.0µg/LPentachlorophenol 14-176 3.6 20.0
39.2 78.477.638.850.0µg/LPhenanthrene 54-120 1.0 20.0
17.0 34.034.617.350.0µg/LPhenol 10-112 1.7 20.0
39.6 79.279.639.850.0µg/LPyrene 52-115 0.5 20.0
28.8 57.658.829.450.0µg/L1,2,4-Trichlorobenzene 44-142 2.0 20.0
38.7 77.477.038.550.0µg/L2,4,6-Trichlorophenol 37-144 0.5 20.0
75.875.82-Fluorobiphenyl (S)49-118
38.639.52-Fluorophenol (S)22-84
Page 19 of 23Date:10/03/2023 04:44 PM
Page 94 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V38427QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V38382
LCS-V38382 LCSD-V38382Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
59.259.2Nitrobenzene-d5 (S)43-123
84.882.24-Terphenyl-d14 (S)49-151
86.282.92,4,6-Tribromophenol (S)31-144
24.725.2Phenol-d5 (S)10-63
Page 20 of 23Date:10/03/2023 04:44 PM
Page 95 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
EDB and DBCP by Microextraction GC/ECD
EPA-504.1
V38379QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-504.1(PREP)
QC Prep:V38326
Associated Lab Samples: 96062
LRB-V38326 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/26/23 11:050.02000.00330<0.00330µg/L1,2-Dibromoethane
LCS-V38326 LCSD-V38326Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.244 97.693.60.2340.250µg/L1,2-Dibromoethane 70-130 4.1 20.0
V 96103-DUP-V38326Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/26/23 12:300.0<0.0209< 0.0209µg/L1,2-Dibromoethane
V 95806-MS-V38326Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
0.276 1060.260< 0.00343µg/L1,2-Dibromoethane 70-130
Page 21 of 23Date:10/03/2023 04:44 PM
Page 96 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V38527QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V38500
Associated Lab Samples: 96062
LRB-V38500 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/30/23 12:2335028.2<28.2µg/LAliphatic C9-C18
09/30/23 12:23500124<124µg/LAliphatic C19-C36
09/30/23 12:2325061.2<61.2µg/LAromatic C11-C22
09/30/23 12:232-Fluorobiphenyl (S)76.7 40-140
09/30/23 12:232-Bromonaphthalene (S)76.5 40-140
09/30/23 12:23Chlorooctadecane (S)69.5 40-140
09/30/23 12:23OTP Surrogate (S)62.7 40-140
LCS-V38500 LCSD-V38500Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
256 42.651.5309600µg/LAliphatic C9-C18 40-140 18.7 50.0
670 83.798.8791800µg/LAliphatic C19-C36 40-140 16.5 50.0
1160 68.281.113801700µg/LAromatic C11-C22 40-140 17.3 50.0
75.782.22-Fluorobiphenyl (S)40-140
70.577.02-Bromonaphthalene (S)40-140
62.068.8Chlorooctadecane (S)40-140
57.368.3OTP Surrogate (S)40-140
Page 22 of 23Date:10/03/2023 04:44 PM
Page 97 of 101
Quality Control Data
23-265-0014Report No:
Project Description:
Client ID:Geological Resources, Inc.
Fast Phil's #506
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V38341QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V38340
Associated Lab Samples: 96062
LRB-V38340 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/25/23 21:1250.011.5<11.5µg/LAliphatic C5-C8
09/25/23 21:1250.025.8<25.8µg/LAliphatic C9-C12
09/25/23 21:1250.04.02<4.02µg/LAromatic C9-C10
09/25/23 21:122,5-Dibromotoluene (FID) (S)115 70-130
09/25/23 21:122,5-Dibromotoluene (PID) (S)97.1 70-130
LCS-V38340 LCSD-V38340Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
249 83.082.6248300µg/LAliphatic C5-C8 70-130 0.4 50.0
359 120123368300µg/LAliphatic C9-C12 70-130 2.4 50.0
106 106109109100µg/LAromatic C9-C10 70-130 2.7 50.0
1041032,5-Dibromotoluene (FID) (S)70-130
92.684.72,5-Dibromotoluene (PID) (S)70-130
Page 23 of 23Date:10/03/2023 04:44 PM
Page 98 of 101
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-265-0014
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:09/22/2023 12:42:54
Special precautions or instructions included?
Comments:
Page 99 of 101
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APPENDIX G
Contaminant Mass Calculations
Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water
Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-1
MW-4
MW-5
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average
Mass
(g)
Percent Red. To Date Red.
MW-1 16,300 20,600 6,980 33,600 93,500 4,220 175,200 19.67
MW-4 22,300 41,600 3,750 18,200 19,700 540 106,090 18.51
MW-5 8,130 22,400 3,240 15,900 490 568 50,728 20.06
Average 15,577 28,200 4,657 22,567 37,897 1,776 110,673 19.41
MW-1 9,040 4,140 1,860 7,050 13,500 772 36,362.00 18.89
MW-4 20,500 36,500 3,230 15,900 13,300 658 90,088.00 17.87
MW-5 6,360 17,300 2,670 12,900 694 671 40,595.00 19.41
Average 11,967 19,313 2,587 11,950 9,165 700 55,682 18.72
MW-1 5,660 2,190 1,650 5,430 2,950 1,300 19,180.00 19.06
MW-4 17,000 41,700 3,830 20,000 14,100 1,030 97,660.00 18.01
MW-5 4,580 14,400 2,900 14,800 712 1,090 38,482.00 19.62
Average 9,080 19,430 2,793 13,410 5,921 1,140 51,774 18.90
Date
Average Water
Column Height
(ft.)
05/22/17 10.59
11/03/21 11.28
09/21/23 11.10
Notes:
• FP: Free Product
• Area of the contaminant plume is calculated from Figure #7
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event.
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
16,568 8.4%50.9%
09/21/23 11.10 16,567.80 8.4% 50.9%
11/03/21
05/22/17 ------
46.4%46.4%
10.59
11.28 18,096.42
33,767.54
Area 1
18,096 46.4%46.4%
Total Contaminant Mass
(g)
Percent Reduction Compared
to Previous Event Percent Reduction To Date
33,768 ------
APPENDIX G
PERCENTAGE REDUCTIONS
FAST PHIL's 506 (INCIDENT NO. 40687)
Baseline Event
0.2030 305,1121,525,55953,87510.5919.415,088.921

APPENDIX H
MMPE Report and Disposal Manifests

ADVANCED
ENVIRONMENTAL SERVICES, INC.
“Your Environmental Solutions Partner”

MOBILE
MULTI-PHASE
EXTRACTION REPORT

Site Location:

Fast Phil’s
1541 Salisbury Rd.
Statesville, NC

Prepared for:

Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
PM – Mr. Eric M. Eubanks, PG

September 18, 2023

TABLE OF CONTENTS

EVENT SUMMARY

MMPE FIELD LOG

MASS-REMOVAL CALCULATION

FIELD NOTES

DISPOSAL MANIFESTS

MOBILE MULTI-PHASE EXTRACTION
EVENT SUMMARY

September 18, 2023

Location: Fast Phil’s
1541 Salisbury Rd.
Statesville, NC

Client: Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110

Event Dates: August 14 – 18, 2023
Advanced Job # 08 - 2354

Advanced Personnel: Gary McDaniel and Scott Crook

MMPE System: MMPE system rated 25”hg at 280 CFM
8’ discharge stack - 6” diameter
6,000 - gallon tanker
160’ piping 1.5” hose to 3 wells

Extraction Well: MW-1, MW-4 and MW-5

Well Initial FP / WL(ft) Final FP / WL(ft) Stinger depth(ft) Run Time
/ Changed To
MW-1 18.71 20.46 19 96.0 hours
MW-4 17.69 20.65 18 96.0 hours
MW-5 19.32 21.63 20 96.0 hours

Description of Event:
The MMPE event ran from 12:10 August 14, through 12:10 August 18, 2023. The MMPE
system was active for 96.0 hours. During the event vacuum at the recovery pump ranged from
20.0 to 21.0 inches of mercury (hg) and stabilized at approximately 21.0 inches of mercury.
Airflow rates ranged from 1,200 to 1,250 feet per minute and stabilized at approximately 1,200
feet per minute. System temperature ranged from 118 – 142 degrees F and humidity ranged from
38 to 52 percent. Field gauged volatile organic compounds (VOC’s) decreased from 32,000
parts per-million (PPM) to 27,000 parts per-million (PPM) throughout the event.

Groundwater / Product Mix Recovered:
During the event a total of 9,766 gallons of product/water mix were removed from the site and
properly disposed at a certified North Carolina disposal facility. No free product was visible in
tanker following the event. Total fluids recovered, was measured based on stick readings
conducted during and following the event. Based on 96.0 hours of operation and a total of 9,766
gallons recovered, the average groundwater recovery rate was calculated to be approximately
101.72 gallons per hour.

Events Results:
Based on mass-removal calculations 1,257.62 pounds or 204.43 gallons of VOC’s were
removed as vapor. Following the event, no free product was identified in any well.

MMPE FIELD LOG:
CLIENT: Geological Resources Inc.
JOB NAME: Fast Phil's
LOCATION: Statesville, NC
MMPE EVENT DATES: August 14 - 18, 2023
EXTRACTION POINTS: MW-1, MW-4 and MW-5
AES JOB NUMBER: 08 - 2354
DATE TIME FLOW (f/m) HUM.(%) TEMP. (F)VOC's(ppm)VAC. (hg")GALLONS STINGER/WL's EXTRACTION POINTS (hg")
MW-1 MW-4 MW-5
Stinger(ft)19 18 20
Start 12:10 Initial WL's 18.71 17.69 19.32
08/14/23 12:50 1,250 52.0 118 21,000 20.0 12.0 13.0 12.0
13:50 1,250 46.0 134 20,000 20.0 12.0 13.0 12.0
19:00 1,250 40.0 140 32,000 20.0 12.0 13.0 12.0
20:00 1,200 40.0 140 32,000 21.0 8.0 9.0 8.0
08/15/23 7:50 1,200 46.0 134 31,000 21.0 2,700 gal.8.0 9.0 8.0
9:50 1,200 46.0 134 31,000 21.0 8.0 9.0 8.0
12:50 1,200 40.0 140 31,000 21.0 8.0 9.0 8.0
19:30 1,200 44.0 136 30,000 21.0 8.0 9.0 8.0
08/16/23 8:50 1,200 48.0 132 29,000 21.0 8.0 9.0 8.0
10:50 1,200 46.0 134 30,000 21.0 P/O 5,386 8.0 9.0 8.0
12:50 1,200 42.0 138 30,000 21.0 8.0 9.0 8.0
16:30 1,200 38.0 142 29,000 21.0 8.0 9.0 8.0
08/17/23 8:40 1,200 46.0 134 28,000 21.0 1,830 gal.8.0 9.0 8.0
10:40 1,200 44.0 136 28,000 21.0 8.0 9.0 8.0
14:00 1,200 40.0 140 27,000 21.0 8.0 9.0 8.0
16:00 1,200 40.0 140 27,000 21.0 8.0 9.0 8.0
08/18/23 7:00 1,200 48.0 132 27,000 21.0 3,840 gal.8.0 9.0 8.0
11:20 1,250 42.0 138 29,000 20.0 12.0 13.0 12.0
P/O 4,380
End 12:10 Final WL's 20.46 20.65 21.63
Total fluids: 9,766 gal.
Total free product:0 gal.
DATE TIME STINGER/WL's EXTRACTION POINTS (hg") cont. VACUUM INFLUENCE (h2o") WELL GAUGING (ft)

Stinger(ft)
Initial WL's

Final WL's
End
Page 1 of 1
MOBILE MULTI-PHASE EXTRACTION EVENT
SITE NAME: Fast Phils CLIENT: Geological Resources
INCIDENT NUMBER:
AVERAGE DEPTH TO GROUNDWATER: 17 - 20 feet
DESCRIBE SOIL IN THE SATURATED ZONE:
AVERAGE HYDRAULIC CONDUCTIVITY (if known):
EXTRACTION WELLS USED FOR MMPE: MW-1, MW-4 and MW-5
SPECIFICATIONS OF THE MMPE SYSTEM (cfm @ in Hg): 280 cfm @ 25.0"Hg
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Date Hours Vacuum Velocity Pipe ID Temp Rel Humid Water Water Qstd(inches of Hg)(ft/min)(in)(°F)(%)Vapor (Wt%)Vapor (Vol%)(flow)
8/14/23 24.00 20.25 1238.00 6 133 44.5 0.051 0.076 200
8/15/23 48.00 21.00 1200.00 6 136 44.0 0.054 0.080 192
8/16/23 72.00 21.00 1200.00 6 137 43.5 0.056 0.082 191
8/17/23 96.00 20.25 1238.00 6 136 43.8 0.055 0.081 198
8/18/23
NOTES
Qstd = Flow at DSCFM
Vacuum = The level of vacuum being applied should be recorded from the MMPE system (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the MMPE system)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Bwsw = water vapor % by weight, i.e., pounds of water per pound of dry air, derived from the Psychrometric chart (temp Vs relative humidity)
Bws = water vapor % by volume
EQUATIONS
Bws = (Bwsw/18 lb-mole H20)/[(1/28.84 lb-mole dry air) + (Bwsw/18 lb-mole H2O)]Qstd = (1-Water Vapor) * velocity * (PI * (diameter/24)2) * (528°R/(Temp + 460))
EMISSION CALCULATIONS
Elapsed
Time Flow PPMmeasured PPMwet PPMdry K PPMconc Cc:m Cc PMRc PMRg PMR
(hour)(DSCFM)(ppm)(#C - gas)(mg/dsm3)(lb/dscf)(lb/hour)(lb/hour)(lb)
24 200 26250 26250 28395 1 28395 14168 0.000884508 10.62 12.29 294.94
48 192 30750 30750 33410 1 33410 16671 0.001040742 12.00 13.88 333.21
72 191 29500 29500 32147 1 32147 16040 0.00100138 11.50 13.31 319.39
96 198 27750 27750 30195 1 30195 15066 0.000940591 11.16 12.92 310.09
Total emissions in pounds 1257.62
Total emissions as gallons (pounds / 6.152)204.43
NOTES
PPMmeasured = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping
PPMwet = "wet" concentration
PPMdry = "dry" concentration
K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, or Hexane K = 6)
PPMc= PPMv, Volumetric concentration of VOC emissions as carbon, dry basis at STP
Cc:m = mg/dsm3, mass concentration of VOC emissions as carbon
Mc = 12.01 mg/mg-mole, molecular weight of carbon
K3 = 24.07 dsm3/106 mg-mole, mass to volume conversion factor at STP
Cc = lb/dcsf, mass concentration of VOC emissions as carbon, dry basis at STP
PMRc = lb/hr, pollutant mass removal rate of VOC's as carbon
PMRg = lb/hr, pollutant mass removal rate of of VOC's as gasolinePMR = lb, pollutant mass removal of VOC's as gasoline
EQUATIONS
PPMwet = PPMmeasuredPPMdry = (PPMwet)/(1-Bws)
PPMc = (PPMd)(K)
Cc:m = (PPMc)(Mc / K3)Cc = (Cc:m)(62.43x10-9 lb-m3/mg-ft3)
PMRc = (Cc)(Qstd)(60 minute/hour)
PMRg = (PMRc)(Mg/Mcg)
PMR = (PMRg)(#hours)
MMP£ Field Log
Went: G t . ':-1 '
Site Name: r-=-A Sr V 1-t J L S
Extraction Wella: f"" 1,0 -l , ("\l,...J -i__J, Mu-) -5
8 -l'-{-2. 3
'g :OD
(vi
8-lr-23 . ;
Job -Nambe~ o g z :s S'
EventDates: 8/1 L} -Js/1 is/2. ""3
°" S1~c
(_(__