MO-7591_36228_CA_MRP_20230815_Monitoring Report

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

Excel Civil & Environmental Associates, PLLC
6 2 5 H u n t s m a n C o u r t
G a s t o n i a , N o r t h C a r o l i n a 2 8 0 5 4
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T e l e p h o n e : ( 7 0 4 ) 8 5 3 - 0 8 0 0
F a c s i m i l e : ( 7 0 4 ) 8 5 3 - 3 9 4 9
I n t e r n e t : www.excelengr.com

August 15, 2023

Mr. Ryan Mills
NCDEQ / DWM / UST Section
Mooresville Regional Office
610 East Center Avenue
Mooresville, North Carolina 28115

Re: Monitoring Report
(Former) 321 Mini Mart
2118 North Aspen Street
Lincolnton, North Carolina
Risk Classification: HIGH
Land Use: RESIDENTIAL
MO-7591_36228_CA_20230815_Monitoring Report
EXCEL Project No. 27010

Dear Mr. Mills:

On behalf of Mr. Satish Desai, Excel Civil & Environmental Associates, PLLC is pleased
to submit a copy of the revised Monitoring Report for your approval.

If you have any comments, please do not hesitate to contact me at 704.853.0800.

Sincerely yours,

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC

Aaron Long, P.E.
Project Engineer

p.c. Mr. Satish Desai, Bucksaver, Parlin, NJ

MONITORING REPORT

(FORMER) 321 MINI MART
2118 NORTH ASPEN STREET
LINCOLNTON, LINCOLN COUNTY, NORTH CAROLINA

NCDEQ INCIDENT NO. 36228
EXCEL PROJECT NO. 27010
MO-7591_36228_CA_20230815_MONITORING REPORT

DATE SUBMITTED:
August 15, 2023

SOURCE OF RELEASE:
Former UST System
Amount Unknown

PREPARED FOR:
Mr. Satish Desai
Responsible Party – Current UST Owner
42 Fela Drive
Parlin, New Jersey 08859

PREPARED BY:
Excel Civil & Environmental Associates, PLLC
625 Huntsman Court
Gastonia, North Carolina 28054
Phone [phone]
NC License No. P-0129

www.excelengr.com

Billy Payne Aaron Long, P.E.
EIT – Engineer in Training Principal Engineer
Monitoring Report August 15, 2023
(Former) 321 Mini Mart Incident No. 36228
Lincolnton, North Carolina Excel No. 27010

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
PROJECT SUMMARY

 Groundwater quality samples were collected from four monitoring wells (MW-2R, MW-
3R, MW-6 and VW-1) on June 14 and 15, 2023, and laboratory analyzed for volatile
organic compounds (VOCs) by EPA Method 6200B, Ethylene Dibromide (EDB) and by
EPA Method 504.1. During the site visit, free product was observed in MW-1R. Static
water levels were collected with a decontaminated water level indicator. Additionally,
the four monitoring wells were also analyzed for natural attenuation parameters
(alkalinity, free carbon dioxide, nitrate/sulfate, total organic carbon, iron/manganese, and
methane).

 During the sampling event, free product was observed in MW-1R. Excel returned to the
property the following day and gauged the thickness at 0.69 feet. Additionally, VW-1 had
a strong petroleum odor. Monitoring well MW-1R has not historically shown free product.

 The onsite remediation system was put into operation on November 11, 2009. The air
sparging and soil vapor extraction system is comprised of nine injection wells and seven
vapor extraction wells. The system was shut down on August 31, 2015 per DWM
directive.

 The results of the laboratory data for constituents which exceeded the NCAC 2L
Standards are as follows:
 Benzene: MW-2, MW-3R, MW-6 and VW-1
 Xylenes: VW-1
 Naphthalene: MW-2R, MW-6 and VW-1
 1,2,4-Trimethylbenzene: VW-1

Copies of the laboratory analytical results are included in Appendix E. Natural
attenuation data is provided in Table 5.

 Results of past receptor surveys completed by Excel during assessment activities
indicate that twenty-nine supply wells were identified within 1,500 feet of the property,
four of which are located within 1,000 feet and confirmed as being utilized for drinking
water purposes. According to the USGS Topographical Map the nearest surface water
body is an unnamed tributary of Walker Branch, located approximately 800 feet
southeast of the source area.

DISCUSSION

 Excel conducted a Mann-Kendall constituent trend analysis which relies on three
statistical metrics, an “S” statistic which indicates whether concentration trend vs. time is
generally decreasing or increasing; a confidence factor (CF) which modifies the S
statistic to indicate the degree of confidence in the trend result; and a coefficient of
variation (COV) to distinguish describe the variability in the data set. The analysis
included an evaluation of both the overall reductions in the areal extent and plume
length for constituents of concern as well as an evaluation of the stability of the plume
constituent concentrations for monitor wells in the core and leading edge of the plume.
Monitoring Report August 15, 2023
(Former) 321 Mini Mart Incident No. 36228
Lincolnton, North Carolina Excel No. 27010

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
Mann-Kendall graphs are provided in Appendix C. The graphs depict concentration
trends for monitoring wells MW-1, MW-2 MW-3, MW-6 and VW-1 and indicated the
following:

o Benzene:
 Increasing: MW-1R;
 No Trend: MW-3R, MW-6, VW-1;
 Decreasing: MW-2R
o Toluene:
 No Trend: MW-1R;
 Decreasing: MW-2R, MW-3R
o Ethylbenzene:
 Increasing: MW-1R;
 No Trend: MW-3R;
 Decreasing: MW-2R, MW-6
o Xylenes:
 No Trend: MW-1R, MW-3R;
 Decreasing: MW-2R, MW-6
o MTBE:
 No Trend: MW-1R;
 Decreasing: MW-2R, MW-3R, MW-6, VW-1
o Naphthalene:
 No Trend: MW-1R;
 Increasing: VW-1
 Decreasing: MW-2R, MW-3R, MW-6

RECOMMENDATIONS

Based on the results of the sampling event, a new release appears likely at the subject
property. The current UST system should be evaluated, and repairs should be made as
they are discovered. Excel recommends a full monitoring round be conducted. Adjacent
water supply wells should also be sampled to verify no impact on potential receptors in the
vicinity of the property. A groundwater quality sampling event is proposed for October of
2023 as approved by NCDEQ.

Monitoring Report August 15, 2023
(Former) 321 Mini Mart Incident No. 36228
Lincolnton, North Carolina Excel No. 27010

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
PROJECT INFORMATION
PRIMARY CONSULTANT: Excel Civil & Environmental Associates, PLLC
PROJECT MANAGER: Aaron Lon , PE
SITE CONTACT: Mr. Satish Desai
SITE HISTORY: Excel completed a Phase II ESA at the subject site as
part of a pre-purchase assessment in February-March
2007. The laboratory results from the soil samples
indicated contamination levels exceeding regulatory
action levels. Excel completed a Site Check at the site
in April 2007. At the request of the NCDEQ Excel
completed a Phase II LSA. Groundwater samples
collected as part of the LSA activities revealed
contamination levels which exceeded NCAC 2L
Standards. Additionally, Excel identified twenty-eight
(28) water supply wells within 1,500 feet of the subject
site.
A CSA was completed by Excel in September 2008
defining the horizontal and vertical extent of both soil
and groundwater contamination. In response to a
letter received from NCDEQ, Excel prepared and
submitted a Corrective Action Plan in January 2009.
As per the approved CAP, Excel installed and started
operation of the air sparge and vapor extraction
remediation system in November 2009. The system
was shut down on Au ust 31, 2015.
SURFICIAL AND REGIONAL GEOLOGY:
The subject site is located within the Chauga Belt of
the Inner Piedmont Physiographic Province of North
Carolina. The 1985 USGS Geologic Map of North
Carolina indicates this area as being underlain by
mica schists with other micaceous metamorphic rock
and cherryville granite rock.

During the completion of the monitoring wells at the
property, a brown to orange, silt-clay mixture (CL) was
observed from approximately 1-fbgl to 22-fbgl.
Partially weathered rock (PWR) was encountered from
approximately 22-fbgl to 50-fbgl. The type of soils
observed locations appears consistent with the
surficial sediments common for this area.

SURFICIAL HYDROLOGY:
Groundwater flow across the site appears to be
following with the general topography and flowing to
the south in a direction towards MW-14 and MW-15.
The average hydraulic gradient across the site is
approximately 2.46 feet per day (ft/day). The average
groundwater velocity was calculated to be
approximately 0.08 ft/day (29.2 ft/year). As such, the
lateral migration of dissolved petroleum constituents
appears to be impeded by the local
geological/hydrogeological conditions.

Monitoring Report August 15, 2023
(Former) 321 Mini Mart Incident No. 36228
Lincolnton, North Carolina Excel No. 27010

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
REGULATORY INTERACTION
AGENCY: NCDEQ, MRO, DWM, UST Section
AGENCY CONTACT: Ron Taraban
SITE ACTIVITIES: Semiannual Groundwater samplin of select wells
RISK ASSESSMENT
SENSITIVE RECEPTORS: Water supply wells located offsite, any underground
utilities on-site and within R/Ws of Aspen Street.
CLOSEST POTABLE WELL: SW-7, SW-14, SW-21 and SW-22 are located within
1,000-feet of the site and utilized for drinking water
purposes.
MONITORING
LIQUID LEVEL GAUGING FREQUENCY: Semiannual
GROUNDWATER SAMPLING METHOD: Select wells semiannual basis for VOCs by EPA
6200B, EDB by EPA Method 504.1 and natural
attenuation parameters including alkalinity, free
carbon dioxide by EPA Method 2320, free carbon
dioxide by EPA Method 4500, nitrate and sulfate by
EPA Method 300, total organic carbon by EPA Method
9060, iron and manganese by EPA Method 6010, and
methane b EPA Method RSK175.

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

APPENDICES

APPENDIX A – TABLES

APPENDIX B – FIGURES

APPENDIX C – MANN-KENDALL GRAPHS

APPENDIX D – SUPPLEMENTAL SITE HISTORY TABLES

APPENDIX E – LABORATORY ANALYSES & CHAIN OF CUSTODY FORMS

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

APPENDIX A - TABLES

Table 1 – Summary of Liquid Level Data

Table 2 – Summary of Current and Historical Groundwater Analytical Data

Table 3 – Field Measurements of Groundwater Samples

Table 4 – Potable Wells Information

Table 5 – Natural Attenuation Data

Well ID # Date Installed Total Depth (ft)Screen Interval
(ft)
Top of Casing
(ft)
Depth to
Poduct (ft)
Depth to Water
(ft)
Product
Thickness (ft)
Water Table
Elevation (ft)
MW-1R 5/16/13 30 15 – 30 100.00 17.69 18.38 0.69 81.62
MW-2R 5/16/13 30 15 – 30 100.94 --18.45 --82.49
MW-3R 5/16/13 30 15 – 30 99.38 --17.29 --82.09
MW-6 2/5/08 28 13 – 28 99.30 --17.05 --82.25
VW-1 2/4-5/08 50 45 – 50 99.89 --17.73 --82.16
NOTES:
Liquid level data collected on June 14 - 15, 2023
ft - feet
* WTCM Figure 4 will not reflect MW-6 water level data as shown in table above.
Table 1
2118 North Aspen Street
NCDEQ Incident # 36228
Excel Project No. 27010
Lincolnton, North Carolina
(Former) 321 Mini-Mart
Summary of Liquid Level Data
Well ID Sample
Date
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1 600 600 500 20 70 6 0.02 15 70 70 400 400
6/6/07 18,000 58,000 13,000 71,000 46,000 < 500 NA 51 210 NA NA NA NA
9/1/09
3/10/10 9 67 24 310 190 4.4 680 0.15 < 10 2.5 6.8 150 58
9/2/10 39 250 83 1,070 94 < 2 720 0.54 370 8.5 24 470 120
3/14/11 2 3.2 1.4 10.2 20 0.87 0.94 < 0.5 NA < 0.5 < 0.5 3.7 1.2
9/26/11 300 590 510 2,320 11 65 140 1.9 200 21 49 660 250
3/12-3/13
9/23/13 < 2.5 20 27 590 14 < 2.5 51 0.14 68 3.7 < 2.5 270 110
3/13/14 1.3 J 12 23 380 3.1 0.55 J 33 0.026 40 4.2 14 300 100
9/11/14 < 0.5 < 0.5 0.74 11.9 1.9 < 0.5 1.2 < 0.021 53 1.1 < 0.5 12 5.7
3/26/15 < 0.14 3.6 24 324 7 < 0.26 30 0.042 65 2.1 J 6.2 150 59
9/24/15 < 0.5 1.6 11 169 6 0.73 18 < 0.019 16 2.4 8.3 180 83
3/29/16 5.7 3.3 76 138 4.4 1.9 67 0.26 47 6.8 19 260 60
9/15/16 160 53 83 111 5.2 6.7 72 0.013 J 50 9.0 28 150 84
3/13/17 450 93 24 91 5.6 47 23 < 0.02 210 2.9 7.5 100 6.9
9/29/17 2,700 3,500 260 1,740 < 25 110 < 25 < 0.02 30 < 25 23 J 380 88
3/5/18 1,700 860 160 750 10 76 31 < 0.02 150 9.7 J 24 370 47
9/14/18 3,600 1,500 430 2,400 36 200 89 < 0.0039 76 21 J 48 660 150
7/3/19 3,100 51 410 1,510 24 J 150 50 < 0.004 20 21 J 47 750 170
2/14/20 2,800 280 650 1,820 31 150 87 < 0.004 8.8 J 28.0 77 1,100 250
11/17/20 3,700 1,200 1,300 3,500 58 190 140 < 0.004 11 47.0 100 1,700 460
6/16/21 2,400 3,100 1,100 5,200 55 170 190 < 0.0039 19 37 69 1,300 360
12/28/21 1,900 39 290 490 19 80 29 < 0.0040 140 17 33 490 95
6/27/22 1,700 160 380 970 28 110 60 0.013 JP 17 23 47 750 120
12/5/22 1,700 S 460 310 1,020 15 S 64 67 0.0056 J 230 23 56 650 180
6/14/23
6/11/07 1,300 8,300 1,000 5,900 < 100 370 NA 290 520 NA NA NA NA
9/1/09 2,800 28,000 2,600 22,500 < 50 370 680 570 < 10 83 210 3,200 920
3/10/10 510 3,200 410 4,000 12 77 200 190 20 17 41 870 290
9/2/10 920 6,700 920 7,100 27 < 10 350 82 67 32 70 1,400 410
3/14/11 540 1,900 780 4,600 18 120 210 21 82 35 89 1,200 400
9/26/11 170 210 51 460 57 41 92 0.69 NA 6.8 15 200 81
3/12/12 190 79 360 1,010 6.8 43 130 8.8 61 21 46 450 230
9/12-3/13
9/23/13 < 10 790 530 3,500 < 10 < 10 94 0.90 < 10 60 210 1,300 430
3/13/14 < 0.14 4.7 33 216 < 0.095 < 2.5 6.5 0.081 < 10 6.3 24 150 52
9/11/14 < 0.5 5.4 13 300 < 0.5 < 0.5 2.2 0.150 < 10 0.96 0.59 60 19
3/26/15 1.3 0.66 7 7.32 13 0.82 16 0.130 6.7 J 1 1.6 4.1 1.6
9/24/15
3/29/16 3.7 4.4 29 86 6.5 0.29 J 30 0.85 34 7.3 8.2 23 11
9/16-3/17
9/29/17 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 69 < 0.5 < 0.5 < 0.5 < 0.5
3/5/18 < 2.5 15 35 350 < 2.5 < 2.5 < 2.5 0.018 J 11 3 8 81 36
4/8/20 < 0.4 < 0.4 < 0.4 < 0.8 < 0.4 < 0.4 < 0.4 < 0.0039 7.2 J < 0.4 < 0.4 < 0.4 < 0.4
11/16/20 < 0.4 < 0.4 < 0.4 < 0.8 < 0.4 < 0.4 < 0.4 < 0.0039 < 4.7 < 0.4 < 0.4 < 0.4 < 0.4
6/16/21 < 0.4 < 0.4 < 0.4 < 0.8 < 0.4 < 0.4 < 0.4 < 0.0039 < 4.7 < 0.4 < 0.4 0.66 < 0.4
12/28/21 < 0.4 < 0.4 1.3 5.7 < 0.4 < 0.4 < 0.4 < 0.0040 72 < 0.4 0.44 2.6 1
6/27/22 < 0.4 < 0.4 < 0.4 0.54 < 0.4 < 0.4 < 0.4 < 0.0039 < 4.7 < 0.4 < 0.4 < 0.4 < 0.4
12/5/22 < 0.4 3 43 161 < 0.4 < 0.4 0.81 < 0.004 22 4.2 9.5 67 22
6/14/23 0.51 3.2 28.9 135.8 < 0.5 < 0.5 6.4 < 0.5 NA 4.2 11.2 90.5 20.5
Summary of Current and Historical Groundwater Analytical Data

NOT SAMPLED - OBSERVED TO BE DRY
NCDEQ Incident # 36228
NOT SAMPLED - INSUFFICIENT VOLUME
(Former) 321 Mini-Mart
NCAC 2L
NOT SAMPLED – OBSERVED TO BE DRY
2118 North Aspen Street
Excel Project No. 27010
Lincolnton, North Carolina
NOT SAMPLED – OBSERVED TO BE DRY
NOT SAMPLED – OBSERVED TO BE DRY
MW-1
MW-2
MW-1R
Not Sampled - Free Product
MW-2R
Page 1 of 6
Well ID Sample
Date
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1 600 600 500 20 70 6 0.02 15 70 70 400 400
Summary of Current and Historical Groundwater Analytical Data

NCDEQ Incident # 36228
(Former) 321 Mini-Mart
NCAC 2L
2118 North Aspen Street
Excel Project No. 27010
Lincolnton, North Carolina
7/24/07 5,600 14,000 4,700 27,000 2,200 210 680 4.3 18 NA NA NA NA
9/1/09
3/10/10 3,100 4,900 760 10,700 4,700 110 640 1.8 < 10 30 73 2,500 750
9/2/10 260 580 70 3,500 2,300 45 110 3 21 9 20 1,400 460
3/14/11 < 0.5 < 0.5 < 0.5 < 1 24 0.51 < 0.5 < 0.019 14 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 3.3 < 0.5 < 0.5 0.11 120 < 0.5 < 0.5 0.56 < 0.5
3/12/12 1.2 5.5 < 0.5 4.9 17 < 0.5 < 0.5 0.34 10 < 0.5 < 0.5 0.97 1
9/12-3/13
9/23/13 19 8.7 49 106 42 < 2.5 27 0.021 15 5.5 19 170 37
3/13/14 1.3 < 0.5 2.6 1.95 3.1 < 0.5 1.5 < 0.02 55 < 0.5 1.5 6.5 1.3
9/11/14 1.7 1.2 3 15.8 2.7 < 0.5 0.65 < 0.021 39 < 0.5 1.3 9.8 2.2
3/25/15 6.2 3.3 14 36 27 1.6 10 < 0.0045 12 1.8 5 22 2.5
9/24/15 2.7 < 0.5 0.8 < 1 9.6 < 0.5 3.1 < 0.019 300 1 2 0.25 J < 0.5
3/29/16 9.1 0.96 14 8.4 13 1.7 19 < 0.019 22 4.4 8 12 < 0.5
9/15/16 11 2.2 17 18.8 14 0.81 12 < 0.0084 58 2.7 6.7 13 3.2
3/13/17 330 13 11 24.9 18 11 13 < 0.02 990 6.3 9.8 5.1 < 2.0
9/29/17 2.7 1.3 1.1 3.19 J < 0.5 < 0.5 < 0.5 < 0.02 8.5 J < 0.5 < 0.5 1.2 < 0.5
3/5/18
7/3/19 410 4.7 12 52 < 2 12 < 2 < 0.004 190 3.3 < 2 19 < 2
2/14/20 160 3.4 22 16.5 < 0.4 5.2 4.9 < 0.004 130 2.9 4.6 11 2.3
11/17/20 3.8 1.8 1.6 5 < 0.4 < 0.4 1.3 < 0.004 < 4.7 < 0.4 < 0.4 3.7 1.3
6/16/21 6.8 < 0.4 < 0.4 < 0.8 1.4 6.8 < 0.4 < 0.004 150 0.6 < 0.4 < 0.4 < 0.4
12/28/21 8.3 0.42 J 4.5 2.85 4.5 20 3.6 < 0.0043 700 2.3 8.9 0.83 < 0.4
6/27/22 < 0.4 < 0.4 < 0.4 < 0.8 0.52 1.5 0.64 < 0.0039 94 < 0.4 < 0.4 < 0.4 < 0.4
12/5/22
6/14/23 21 51.9 10.8 27.7 0.85 < 0.5 3.1 < 0.5 NA 1.3 2.1 4.2 1.8
7/24/07 270 < 1 < 1 < 1 36 1.5 NA < 0.021 < 3 NA NA NA NA
9/1/09 31 < 0.5 0.67 1.74 1.3 < 0.5 < 0.5 < 0.019 < 10 2.2 0.75 < 0.5 0.61
3/10/10 310 100 190 1,600 550 20 28 0.063 < 10 16 31 520 350
9/2/10 < 0.5 < 0.5 < 0.5 < 1 5.6 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 7.8 < 0.5 < 0.5 < 0.019 23 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 2.1 < 0.5 < 0.5 < 0.02 79 < 0.5 < 0.5 < 0.5 < 0.5
3/12/12 < 0.5 < 0.5 < 0.5 < 1 0.95 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/24/12
3/19/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 18 < 0.5 < 0.5 < 0.5 < 0.5
9/23/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/13/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/11/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/25/15 < 0.027 < 0.17 < 0.17 < 0.34 < 0.019 < 0.052 < 0.17 < 0.0045 < 4.7 < 0.029 < 0.024 < 0.17 < 0.17
9/24/15 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 8.5 J < 0.5 < 0.5 < 0.5 < 0.5
2/2/08 < 1 0.28 < 1 0.23 < 1 < 1 NA < 0.019 16 NA NA NA NA
9/1/09 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/2/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 180 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/7/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/24/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
NOT SAMPLED - OBSERVED TO BE DRY
NOT SAMPLED – OBSERVED TO BE DRY
NOT SAMPLED – OBSERVED TO BE DRY
NOT SAMPLED - OBSERVED TO BE DRY
MW-5
MW-4
NOT SAMPLED – OBSERVED TO BE DRY
MW-3R
MW-3
Page 2 of 6
Well ID Sample
Date
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Xy
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MT
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IP
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Na
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a
l
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ED
B
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a
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Is
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o
p
y
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b
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n
z
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n
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n-
P
r
o
p
y
l
b
e
n
z
e
n
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1,
2
,
4
-
T
r
i
m
e
t
h
y
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b
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n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1 600 600 500 20 70 6 0.02 15 70 70 400 400
Summary of Current and Historical Groundwater Analytical Data

NCDEQ Incident # 36228
(Former) 321 Mini-Mart
NCAC 2L
2118 North Aspen Street
Excel Project No. 27010
Lincolnton, North Carolina
7/24/07 1,500 3,000 1,000 5,400 1,100 200 NA 2.8 3.4 NA NA NA NA
9/1/09
3/10/10 550 1,300 1,100 7,500 290 48 970 2.2 < 10 98 360 3,800 1,000
9/2/10 15 67 79 630 150 7.6 47 0.26 18 6.1 21 240 82
3/14/11 < 0.5 1.8 7.3 42 4.6 < 0.5 1.4 < 0.019 < 10 0.52 1.4 17 7.6
9/26/11 21 190 260 2,170 180 7.1 190 0.13 18 24 64 1,000 380
3/12/12 < 0.5 < 0.5 < 0.5 < 1 5.3 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 1.3 < 0.5
9/24/12 < 25 390 970 5,600 < 25 < 25 440 < 0.019 0.028 65 220 2,100 500
3/19/13 7.6 4.2 150 126 11 < 2.5 180 < 0.02 16 30 64 280 53
9/23/13 8.4 2.9 24 31 9.9 1.5 28 < 0.02 < 10 5.4 12 66 < 0.5
3/13/14 17 33 74 94 16 2.2 38 0.026 < 10 6.6 16 58 31
9/11/14 0.77 < 0.5 0.81 1.5 1.9 < 0.5 1.4 < 0.019 17 < 0.5 < 0.5 0.7 1.1
3/25/15 0.97 0.71 5.6 4.8 6.7 < 0.052 5.2 < 0.0046 71 1.6 3.5 2 0.36 J
9/24/15 8.2 26 130 253 18 1.5 60 < 0.019 17 16 48 180 49
3/29/16 19 2.7 24 17.7 9.3 3.7 52 < 0.019 6.8 J 12 20 24 9.9
9/15/16 83 12 47 26 11 1.5 32 < 0.0084 24 8.1 16 11 3.3
3/13/17 150 7.1 49 111 9 6.3 41 < 0.019 46 8.1 19 99 30
9/29/17 340 23 39 57 4.3 10 14 < 0.020 < 10 5.7 13 54 17
3/5/18 310 11 65 136 < 5 8.8 7.6 0.0055 J 14 6.8 15 89 48
9/14/18 210 110 100 33.7 11 11 79 < 0.0039 17 17 36 48 6.7
7/3/19 12 7.7 19 2.64 2.6 1.1 13 < 0.0039 48 3.8 8.9 5 < 0.4
2/14/20 4.3 0.76 4.1 2 0.76 0.75 2.5 < 0.0039 39 0.63 1.4 1.2 < 0.4
11/17/20 43 10 45 36 8.7 6.5 30 < 0.0039 27 5.6 9.6 13 1.8
6/16/21 7.9 2.3 17 7.6 3.1 1.2 6.4 < 0.004 45 2.2 3.8 4.2 < 0.4
12/28/21
6/27/22 3.9 <0.4 12 2.5 2.3 2.3 11 <0.0039 420 4.4 8.3 2.2 0.61
12/5/22
6/14/23 53.4 31.1 9.8 19.9 4.1 < 0.5 29.8 < 0.5 NA 8.6 7.8 2.7 0.62
2/2/08 11 0.36 0.18 10 41 4.8 NA 0.11 210 NA NA NA NA
9/1/09 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10 1.6 < 0.5 < 0.5 1.7 7.5 1.2 0.55 < 0.019 < 10 < 0.5 < 0.5 0.63 < 0.5
9/2/10
3/14/11 < 0.5 < 0.5 < 0.5 < 1 17 1.4 < 0.5 < 0.019 22 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 21 190 260 2,240 180 8 170 0.13 79 22 60 1,000 350
3/12/12 < 0.5 < 0.5 < 0.5 < 1 0.88 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/28/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 15 < 0.5 < 0.5 < 0.5 < 0.5
3/19/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 23 < 0.5 < 0.5 < 0.5 < 0.5
9/23/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/13/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 23 < 0.5 < 0.5 < 0.5 < 0.5
9/11/14 < 0.5 < 0.5 < 0.5 < 1 0.85 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/25/15 < 0.027 < 0.17 < 0.17 < 0.34 1.4 < 0.052 < 0.17 < 0.0045 < 4.7 < 0.029 < 0.024 < 0.17 < 0.17
9/24/15 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 0.23 J < 0.02 48 < 0.5 < 0.5 < 0.5 < 0.5
2/2/08 < 1 < 1 < 1 < 1 < 1 < 1 NA < 0.02 5.2 NA NA NA NA
9/1/09 < 0.5 < 0.5 < 0.5 < 0.5 1.1 < 0.5 < 0.5 < 0.02 16 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 31 < 0.5 < 0.5 < 0.5 < 0.5
9/2/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 29 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.5 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 0.68 < 0.5 15 < 0.02 < 10 < 0.5 < 0.5 0.5 < 0.5
3/7/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 0.5 < 0.5
9/28/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 55 < 0.5 < 0.5 < 0.5 < 0.5
3/19/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/24/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/13/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/11/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/26/15 < 0.027 < 0.17 < 0.17 < 0.34 < 0.019 < 0.052 < 0.17 < 0.0045 < 4.7 < 0.029 < 0.024 < 0.17 < 0.17
9/24/15 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 13 < 0.5 < 0.5 < 0.5 < 0.5
NOT SAMPLED – NOT LOCATED
NOT SAMPLED – FREE PRODUCT OBSERVED
NOT SAMPLED - OBSERVED TO BE DRY
NOT SAMPLED - OBSERVED TO BE DRY
MW-7
MW-8
MW-6
Page 3 of 6
Well ID Sample
Date
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1,
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4
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1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1 600 600 500 20 70 6 0.02 15 70 70 400 400
Summary of Current and Historical Groundwater Analytical Data

NCDEQ Incident # 36228
(Former) 321 Mini-Mart
NCAC 2L
2118 North Aspen Street
Excel Project No. 27010
Lincolnton, North Carolina
2/2/08 4.7 7.4 3.8 16 2.5 0.61 NA < 0.02 20 NA NA NA NA
9/1/09 < 0.5 < 0.5 < 0.5 < 0.5 1.7 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10 < 0.5 < 0.5 < 0.5 < 1 1.3 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/2/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 18 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 13 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 0.65 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/7/12 < 0.5 < 0.5 < 0.5 < 1 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/24/12 < 0.5 < 0.5 < 0.5 < 1 0.5 < 0.5 < 0.5 < 0.02 32 < 0.5 < 0.5 < 0.5 < 0.5
3/19/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 32 < 0.5 < 0.5 < 0.5 < 0.5
9/23/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/13/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/11/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 13 < 0.5 < 0.5 < 0.5 < 0.5
3/25/15 < 0.027 < 0.17 < 0.17 < 0.34 < 0.019 < 0.052 < 0.17 < 0.0044 10 < 0.029 < 0.024 < 0.17 < 0.17
9/24/15 < 0.5 < 0.5 < 0.5 < 0.1 < 0.5 < 0.5 < 0.5 < 0.02 46 < 0.5 < 0.5 < 0.5 < 0.5
5/13/08 < 1 < 1 < 1 < 1 1.4 0.74 NA 0.014 4.9 NA NA NA NA
9/1/09 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/2/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 32 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/7/12 < 0.5 < 0.5 < 0.5 < 1 10 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/28/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
5/13/08 290 150 360 850 140 46 NA 0.16 75 NA NA NA NA
9/1/09 670 690 760 2,510 200 53 430 0.31 < 10 68 200 1,500 330
3/10/10 500 880 1,100 5,200 270 48 690 0.45 < 10 90 260 2,800 640
9/2/10 37 1.2 4.7 16.6 43 7.9 69 0.038 41 7.9 8.7 330 42
3/14/11 3.9 < 0.5 < 0.5 < 1 87 16 1.1 < 0.019 15 0.75 < 0.5 6.7 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 5.4 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/7/12 < 0.5 < 0.5 < 0.5 < 1 9 0.69 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/24/12 < 0.5 < 0.5 < 0.5 < 1 5.7 < 0.5 < 0.5 < 0.02 25 < 0.5 < 0.5 < 0.5 < 0.5
3/19/13 < 0.5 < 0.5 < 0.5 < 1 5.9 < 0.5 < 0.5 < 0.02 30 < 0.5 < 0.5 < 0.5 < 0.5
9/23/13 < 0.5 < 0.5 < 0.5 < 1 2.2 < 0.5 < 0.5 < 0.02 10 < 0.5 < 0.5 < 0.5 < 0.5
3/13/14 < 0.5 < 0.5 < 0.5 < 1 4.2 0.62 < 0.5 < 0.02 16 < 0.5 < 0.5 < 0.5 < 0.5
9/11/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/25/15 < 0.027 < 0.17 < 0.17 < 0.34 0.36 J < 0.052 < 0.17 < 0.0045 33 < 0.029 < 0.024 < 0.17 < 0.17
9/24/15 < 0.5 < 0.5 < 0.5 < 1 0.38 J < 0.5 < 0.5 < 0.019 18 < 0.5 < 0.5 < 0.5 < 0.5
5/13/08 < 1 < 1 < 1 < 1 < 1 < 1 NA < 0.02 27 NA NA NA NA
9/1/09 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/2/10 < 0.5 < 0.5 < 0.5 < 1 1.4 2.2 < 0.5 < 0.019 25 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 19 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 2.4 2.6 0.9 < 0.02 11 < 0.5 < 0.5 < 0.5 < 0.5
3/7/12
9/28/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
MW-13 5/13/08 < 1 < 1 < 1 < 1 < 1 < 1 NA < 0.019 < 0.02 NA NA NA NA
NOT SAMPLED – OBSERVED TO BE DRY
MW-9
MW-10
MW-11
MW-12
Page 4 of 6
Well ID Sample
Date
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1,
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1 600 600 500 20 70 6 0.02 15 70 70 400 400
Summary of Current and Historical Groundwater Analytical Data

NCDEQ Incident # 36228
(Former) 321 Mini-Mart
NCAC 2L
2118 North Aspen Street
Excel Project No. 27010
Lincolnton, North Carolina
5/13/08 < 1 < 1 < 1 < 1 0.57 1.6 NA < 0.02 5.2 NA NA NA NA
9/1/09 < 0.5 < 0.5 < 0.5 < 0.5 0.53 0.57 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10 < 0.5 < 0.5 < 0.5 < 1 1.1 2.8 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/2/10 < 0.5 < 0.5 < 0.5 < 1 4.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 1.6 1.4 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 2.2 2.8 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/7/12 < 0.5 < 0.5 < 0.5 < 1 1.2 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/28/12 < 0.5 < 0.5 < 0.5 < 1 1.9 0.73 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
MW-15 5/13/08 < 1 < 1 < 1 < 1 4.1 5.6 NA < 0.019 8 NA NA NA NA
2/2/08 910 1,700 450 2,000 400 100 NA 4.7 < 10 NA NA NA NA
9/1/09 1,800 1,900 870 2,290 650 110 340 3.5 < 10 48 120 920 110
3/10/10 910 190 270 354 460 77 280 1.7 < 10 39 56 640 29
9/2/10 71 61 19 61 88 10 24 0.28 24 2.4 2.3 44 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 13 < 0.5 < 0.5 < 0.5 < 0.5
3/12/12 < 0.5 < 0.5 < 0.5 < 1 1.3 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/24/12 4.2 < 0.5 5.2 < 1 26 1.4 6 0.034 < 10 < 0.5 1.1 < 0.5 < 0.5
3/19/13 7.2 < 0.5 < 0.5 < 1 39 5.9 8 0.03 < 10 2.1 1.8 1.1 < 0.5
9/23/13 5.9 < 0.5 4.9 < 1 22 4 15 < 0.02 < 10 2.7 1.7 < 0.5 < 0.5
3/13/14 15 3 37 12.7 12 4.1 22 < 0.02 < 10 4.1 6.2 7.6 3
9/11/14 < 0.5 < 0.5 < 0.5 < 1 1.2 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/26/15 4.4 0.34 J 6.3 0.32 J 9.7 2.5 9.2 < 0.0045 < 4.7 2.8 2.3 < 0.17 < 0.17
9/24/15 38 11 190 38 2.3 J 3.8 68 0.053 < 10 11 26 46 < 2.5
3/29/16 6.2 < 0.5 7 < 1 3.1 1.8 14 < 0.02 < 10 3 2.3 < 0.5 < 0.5
9/15/16 1.2 4.9 4.9 13.7 0.81 < 0.4 1.9 < 0.0082 5.1 J < 0.4 0.6 1 < 0.4
3/13/17 0.87 < 0.4 < 0.4 < 0.8 < 0.4 < 0.4 < 0.4 < 0.02 < 4.7 < 0.4 < 0.4 < 0.4 < 0.4
9/19/17 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/5/18 10 2.8 0.41 J 2.5 < 0.5 4.4 < 0.5 < 0.02 23 < 0.5 < 0.5 < 0.5 < 0.5
9/14/18 < 0.4 1.3 < 0.4 < 0.8 < 0.4 < 0.4 < 0.4 < 0.0039 < 4.7 < 0.4 < 0.4 < 0.4 < 0.4
7/3/19 < 0.4 < 0.4 < 0.4 < 0.8 < 0.4 < 0.4 < 0.4 < 0.0038 6.0 J < 0.4 < 0.4 < 0.4 < 0.4
2/14/20 < 0.4 < 0.4 < 0.4 < 0.8 < 0.4 < 0.4 < 0.4 < 0.0039 14 < 0.4 < 0.4 < 0.4 < 0.4
11/17/20 < 0.4 < 0.4 < 0.4 < 0.8 < 0.4 < 0.4 < 0.4 < 0.0038 21 < 0.4 < 0.4 < 0.4 < 0.4
6/17/21 18 13 7.2 18 < 0.4 1 0.66 < 0.004 21 0.44 J 0.79 6.5 1.6
12/28/21 1.1 < 0.4 0.95 1.75 < 0.4 < 0.4 0.44 J < 0.004 150 < 0.40 0.52 5.6 1.3
6/27/22 1.1 <0.4 0.61 3.40 <0.4 <0.4 0.61 <0.0039 4.9 J <0.4 <0.4 3.2 0.85
12/5/22 6.0 < 0.4 13.00 1.60 1.9 3 22 < 0.0039 9 J 9.2 8.4 8.4 < 0.4
6/14/23 178 856 144 782 < 2.5 13.9 165 < 2.5 NA 11.4 44.7 482 116
VW-2 1/6/09 14 24 7.7 46 7 3.6 NA 0.059 NA NA NA NA NA
3/12/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/19/13
3/12/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/19/13
SW-5 3/19/13
9/2/09 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10
9/2/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 29 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/24/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/19/13
NOT SAMPLED – NO ACCESS
NOT SAMPLED – INACTIVE
NOT SAMPLED – INACTIVE
NOT SAMPLED – DOES NOT EXIST
NOT SAMPLED – INACTIVE
SW-1
SW-4
SW-6
MW-14
VW-1
Page 5 of 6
Well ID Sample
Date
Be
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e
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e
To
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ED
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P
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1,
2
,
4
-
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1,
3
,
5
-
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1 600 600 500 20 70 6 0.02 15 70 70 400 400
Summary of Current and Historical Groundwater Analytical Data

NCDEQ Incident # 36228
(Former) 321 Mini-Mart
NCAC 2L
2118 North Aspen Street
Excel Project No. 27010
Lincolnton, North Carolina
9/2/09 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10
9/2/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 12 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.5 13 < 0.5 < 0.5 < 0.5 < 0.5
9/24/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.5 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/19/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 0.019 10 < 0.5 < 0.5 < 0.5 < 0.5
9/23/13 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/13/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/11/14 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 22 < 0.5 < 0.5 < 0.5 < 0.5
3/26/15
9/24/15 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/29/16 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
SW-8 3/19/13
9/2/09 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/10/10 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/14/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.019 < 10 < 0.5 < 0.5 < 0.5 < 0.5
9/26/11 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.5 13 < 0.5 < 0.5 < 0.5 < 0.5
3/12/12 < 0.5 < 0.5 < 0.5 < 1 < 0.5 < 0.5 < 0.5 < 0.02 < 10 < 0.5 < 0.5 < 0.5 < 0.5
3/19/13
NOTES:
Data provided in ug/L EDB - Ethylene Dibromide
NA - Not Analyzed NCAC - North Carolina Administrative Code
MTBE - Methyl tert-butyl ether Data in BOLD and Highlighted exceeds NCAC 2L Groundwater Standard
IPE - Diispropyl ether J - Estimated result between practical quantitation limit and method detection limit
ND-Not Detectable
Additional Results above NCAC 2L Stds for 3/13/17 Sampling: VW-1: 1-2-Dichloroethane 0.92 ug/L and Vinyl Chloride 12 ug/L
NOT SAMPLED – INACTIVE
NOT SAMPLED – NO ACCESS
NOT SAMPLED – DOES NOT EXIST
NOT SAMPLED – NO ACCESS
SW-9
SW-7
Page 6 of 6
Well ID #pH
(SU)
DO
(ppm)
Temperature
(°C)
Specific
Conductivity
(µS/cm)
ORP
(mV)
Turbidity
(NTU)
MW-1R
MW-2R 5.93 5.75 23.20 0.229 150 49.9
MW-3R 6.11 4.11 24.15 0.161 115 995
MW-6 6.35 5.77 22.62 0.130 43 350
VW-1 6.49 5.76 20.18 0.084 226 NM
NOTES:
SU - Standard Units S/cm - microSiemens per centimeter
oC - degrees Celsius ORP - Oxygen Reduction Potential
NTU - Nephelometric Turbidity Units mV - milliVolts
Data Collected June 14 - 15, 2023 NM - Equipment Error
FP Observed
Table 3
Lincolnton, North Carolina
Excel Project No. 27010
2118 North Aspen Street
(Former) 321 Mini-Mart
Field Measurements of Groundwater Samples
NCDEQ Incident # 36228
WELL ID #OWNER NAME & ADDRESS DISTANCE FROM
SOURCE WELL STATUS
SW-1 Robert Martin / 2124 N. Aspen Street 150’ N Inactive
SW-2 Robert Martin / 2102 & 2106 N. Aspen Street 175’ S Inactive
SW-3 Lincoln Co. Farm Bureau / 2396 N. Aspen Street 230’ S Inactive
SW-4 Marshall Withers / 100 Keever Street 250’ E Inactive
SW-5 Marshall Withers / 100 Keever Street 300’ E Inactive
SW-6 John Avery / 102 Keever Street 350’ E Inactive
SW-7 Jack Bailey / 2144 N. Aspen Street 345’ N Drinking
SW-9 Paul Joseph / 107 Keever Street 345’ N Inactive
SW-10 Edward Lobo / 108 Keever Street 402’ E Inactive
SW-11 Edith Martin / 112 Keever Street 520’ NE Unknown
SW-12 Greg Guggisbey / 205 Elizabeth Avenue 430’ SE Inactive
SW-13 Fred Mullinax / 105 Eastview Drive 540’ S Unknown
SW-14 Evelyn Lail / 111 Carpenter Street 615’ E Drinking
SW-15 Eddie Holly / 2225 N. Aspen Street 600’ N Inactive
SW-16 Michael Keener / 2499 N. Aspen Street 700’ N Unknown
SW-17 Michael Mull / 105 Carpenter Street 660’ E Unknown
SW-18 Michael Mull / 112 Carpenter Street 775’ E Unknown
SW-19 Ute Coffey / 110 Shell Street 990’ E Unknown
SW-20 Daphine Houser / 2350 N. Aspen Street 800’ S Unknown
SW-21 Bob Ramseur / 1907 N. Aspen Street 750’ S Drinking
SW-22 Janet Alvey / 2246 N. Aspen Street 990’ N Drinking
SW-23 E.L. Rudisill, Jr. / 114 Mull Road 1,230’ NE Inactive
SW-24 Larry Hudson / 100 Auton Street 1,275’ E Unknown
SW-25 Clyde Lingerfelt / 108 Auton Street 1,350’ E Unknown
SW-26 Liberty Tabernacle / 161 Shell Street 1,450’ SE Unknown
SW-27 Jeffery Ray Scronce / 162 Shell Street 1,330’ SE Irrigation
SW-28 Mike Scronce / 172 Shell Street 1,330’ SE Drinking
NOTES:
Data obtained from Lincoln County GIS and returned well surveys
Table 4
Excel Project No. 27010
Lincolnton, North Carolina
2118 North Aspen Street
(Former) 321 Mini-Mart
Potable Wells Information
NCDEQ Incident # 36228
TABLE 5
NATURAL ATTENUATION DATA
(Former) 321 Mini Mart
2118 North Aspen Street
Lincolnton, North Carolina
NCDEQ Incident # 36228
Excel Project No. 27010
Al
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Di
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M
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(m
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14-Feb-20 140 280 < 0.2 0.031 15 150 40 39
17-Nov-20 170 250 5.9 < 0.02 24 91 43 69
16-Jun-21 31 290 1.8 0.650 8 5.2 J 16 3.7
28-Dec-21 66 110 1.4 < 0.02 6 150 110 52 S
27-Jun-22 88 H 560 0.94 J 0.013 J 17.6 60 B 33 61
5-Dec-22 90 660 0.32 J 0.170 9.9 16 B 76 59
14-Jun-23
8-Apr-20 < 20 54 0.53 J 0.19 1.2 4.1 B J 6.7 1.2
16-Nov-20 < 20 32 0.98 B J 1.4 H 0.6 J 2.5 J 4.9 0.39
21-Jun-21 28 100 5.7 0.35 < 0.42 < 2.5 3.8 0.39
28-Dec-21 < 20 33 0.82 J 0.20 1.3 8.6 J 130 3.8
27-Jun-22 < 20 H 88 0.71 J 0.25 < 2.0 21 B 3.8 0.34
5-Dec-22 < 20 250 0.88 J 0.19 2.2 200 B 48 1.2
14-Jun-23 8.6 25.5 < 1 < 0.1 < 1 49 8.33 1.96
14-Feb-20 96 170 1.1 0.20 19 1,600 49 3.5
17-Nov-20 < 20 < 27 0.65 J 0.48 0.94 J 2.6 J 0.41 0.031
16-Jun-21 140 270 8.4 0.16 8.2 570 72 7.5
28-Dec-21 93 180 2.5 0.23 12 220 270 35
27-Jun-22 59 H 360 25.0 0.15 < 2.0 55 B 35 39
5-Dec-22
14-Jun-23 55.4 44.1 1.8 < 0.1 15.3 388 29.2 2.94
14-Feb-20 43 90 1.7 0.26 3.7 1,600 13 1.2
17-Nov-20 68 170 < 0.25 0.035 5.0 5,000 B 26 7.3
21-Jun-21 45 190 1.7 0.098 6.1 2,600 25 6.2
28-Dec-21
27-Jun-22 29 H 210 13 0.086 < 2.0 130 B 99 27
5-Dec-22
14-Jun-23 30.9 74.3 11.1 < 0.1 2.4 75.3 6.12 12.9
14-Feb-20 < 20 46 < 0.2 0.046 1.1 3.7 J 8.3 0.098
17-Nov-20 < 20 72 0.46 J 3.8 1.3 2.6 J 10 0.38
21-Jun-21 180 880 < 1.3 < 0.025 H 38.0 130 68 48
28-Dec-21 20 57 1.8 0.56 3.3 < 2.5 50 4.8
27-Jun-22 24 H 68 1.4 1.4 < 2.0 < 2.5 2.8 0.16
5-Dec-22 40 280 1.8 0.37 2.4 57 B 15 5.4
14-Jun-23 27.4 20.4 1.5 0.48 < 1 < 10 0.764 2.36
Notes:
Data provided in units as shown H- Out of Holding time
J - Estimated value
B - Detected in method blank
ND-Not Detected
VW-1
Well ID Date
Sampled
NATURAL ATTENUATION ANALYTICAL DATA
Not Sampled - Observed to Be Dry
Not Sampled - Observed to Be Dry
Not Sampled - Observed to Be Dry
MW-2R
MW-3R
MW-6
MW-1R
Not Sampled - Free Product Observed

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

APPENDIX B - FIGURES

Figure 1 – Site Vicinity

Figure 2 – Site Plan

Figure 3 – Potable Wells Map

Figure 4 – Water Table Contour Map

Figure 5 – Benzene in Groundwater Map

Figure 6 – MTBE in Groundwater Map

Figure 7 – Naphthalene in Groundwater Map

Figure 8 – EDB in Groundwater Map

EXCEL CIVIL & ENVIRONMENTAL
ASSOCIATES, PLLC
625 HUNTSMAN COURT
GASTONIA, NC 28054
[phone]
Figure 1 – Topographical Map 
N Source: U.S.G.S. 7.5 Minute Topographic Map
Lincolnton East, Quadrangle, 1993
EXCEL CIVIL & ENVIRONMENTAL
ASSOCIATES, PLLC
625 HUNTSMAN COURT
GASTONIA, NC 28054
[phone]
Figure 3
Potable Wells Map 
N Source: Lincoln County GIS

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

APPENDIX C – MANN-KENDALL GRAPHS

Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:mg/L
Sam lin Point ID:MW-1&R MW-2&R MW-3&R MW-6 W-1
Sampling SamplingEvent Date
1 06/06/07 18.00 1.30 5.60
2 02/02/08 0.910
3 07/24/07 1.50
4 09/01/09 2.80 1.80
5 03/10/10 0.0090 0.5100 3.10 0.550 0.9100
6 09/02/10 0.0390 0.9200 0.2600 0.0150 0.0710
7 03/14/11 0.0020 0.5400 0.0005 0.0005 0.0005
8 09/26/11 0.3000 0.1700 0.0005 0.0210 0.0005
9 03/12/12 0.1900 0.0012 0.0005 0.0005
10 09/24/12 0.0250 0.0042
11 03/19/13 0.0076 0.0072
12 09/23/13 0.0025 0.0100 0.0190 0.0084 0.0059
13 03/13/14 0.0013 0.0001 0.0013 0.0170 0.0150
14 09/11/14 0.0005 0.0005 0.0017 0.0008 0.0005
15 03/26/15 0.0001 0.0013 0.0062 0.0010 0.0044
16 09/24/15 0.0005 0.0027 0.0082 0.0380
17 03/29/16 0.0057 0.0037 0.0091 0.0190 0.0062
18 09/15/16 0.1600 0.0110 0.0830 0.0012
19 03/13/17 0.4500 0.3300 0.1500 0.0009
20 09/29/17 2.70 0.0005 0.0027 0.3400 0.0005
21 03/05/18 1.70 0.0025 0.3100 0.0100
22 09/14/18 3.6000 0.210000 0.000400
23 07/03/19 3.10 0.4100 0.0120 0.0004
24 02/14/20 2.8 0.16 0.0043
25 11/17/20 3.7 0.0038 0.043
26 06/17/21 2.4 0.0004 0.0068 0.0079 0.018
27 12/28/21 1.9 0.0004 0.0083 0.0011
28 06/27/22 1.7 0.0004 0.0004 0.0039 0.0011
29 12/05/22 1.7 0.0004 0.006
30 06/15/23 0.00051 0.021 0.0534 0.178
31
32
33
34
35
Coefficient of Variation:1.95 2.06 2.93 2.32 2.71Mann-Kendall Statistic S :81 -112 7 9 -58
Confidence Factor:98.3% >99.9% 56.6% 57.3% 89.4%
Concentration Trend:Increasing Decreasing No Trend No Trend No Trend
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water , 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
A. Long
27010
GSI Environmental Inc., www.gsi-net.com
BENZENE CONCENTRATION (mg/L)
7-Aug-23
(Former) 321 Mini Mart Benzene
0.0001
0.001
0.01
0.1
1
10
100
01/04 10/06 07/09 04/12 12/14 09/17 06/20 03/23 12/25
Co
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Sampling Date
MW-1&R
MW-2&R
MW-3&R
MW-6
VW-1
Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:m /L
Sam lin Point ID:MW-1&R MW-2&R MW-3&R MW-6 W-1
Sampling SamplingEvent Date
1 06/06/07 46.0 0.100
2 02/02/08 0.40
3 07/24/07 2.2 1.1
4 09/01/09 0.050 0.29 0.65
5 03/10/10 0.1900 0.012 4.7 0.15 0.46
6 09/02/10 0.0940 0.027 2.3 0.0046 0.088
7 03/14/11 0.0200 0.018 0.024 0.18 0.0005
8 09/26/11 0.0110 0.057 0.0033 0.0005
9 03/12/12 0.0068 0.017 0.0053 0.0013
10 09/24/12 0.025 0.026
11 03/19/13 0.011 0.039
12 09/23/13 0.0140 0.0100 0.042 0.0099 0.022
13 03/13/14 0.0031 0.0095 0.0031 0.016 0.012
14 09/11/14 0.0019 0.0005 0.0027 0.0019 0.0012
15 03/26/15 0.0070 0.0130 0.027 0.0067 0.0097
16 09/24/15 0.0060 0.0096 0.018 0.0023
17 03/29/16 0.0044 0.0065 0.013 0.0093 0.0031
18 09/15/16 0.0052 0.014 0.011 0.00081
19 03/13/17 0.0056 0.018 0.009 0.0004
20 09/29/17 0.0250 0.0005 0.0005 0.0043 0.0005
21 03/05/18 0.0100 0.0025 0.005 0.0005
22 09/14/18 0.0360 0.011 0.000400
23 07/03/19 0.024 0.002 0.0026 0.0004
24 02/14/20 0.031 0.00076
25 11/17/20 0.058 0.0087
26 06/17/21 0.055 0.0014 0.0031
27 12/28/21 0.019 0.0004 0.0045 0.0004
28 06/27/22 0.028 0.0004 0.00052 0.0023 0.0004
29 12/05/22 0.015 0.0004 0.0019
30 06/15/23 0.0005 0.00085 0.00041 0.00025
31
32
33
34
35
Coefficient of Variation:4.72 1.51 2.58 2.98 2.46Mann-Kendall Statistic S :9 -109 -108 -169 -188Confidence Factor:58.3% >99.9% >99.9% >99.9% >99.9%
Concentration Trend:No Trend Decreasing Decreasing Decreasing Decreasing
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water, 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
MTBE CONCENTRATION (mg/L)
GSI Environmental Inc., www.gsi-net.com
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
7-Aug-23 27010
(Former) 321 Mini Mart MTBE
A. Long
0.0001
0.001
0.01
0.1
1
10
100
01/04 10/06 07/09 04/12 12/14 09/17 06/20 03/23 12/25
Co
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e
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t
r
a
t
i
o
n

(
m
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/
L
)
Sampling Date
MW-1&R
MW-2&R
MW-3&R
MW-6
VW-1
Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:m /L
Sam lin Point ID:MW-1&R MW-2&R MW-3&R
Sampling SamplingEvent Date
1 06/06/07 58.00
2 06/11/07 8.30
3 02/02/08
4 07/24/07 14.00
5 09/01/09 28.00
6 03/10/10 0.0670 3.200 4.90
7 09/02/10 0.2500 6.700 0.5800
8 03/14/11 0.0032 1.900 0.0005
9 09/26/11 0.5900 0.210 0.0005
10 03/12/12 0.079 0.0055
11 09/24/12
12 03/19/131309/23/13 0.0200 0.790 0.0087
14 03/13/14 0.0120 0.0047 0.0005
15 09/11/14 0.0005 0.0054 0.0012
16 03/26/15 0.0036 0.0007 0.0033
17 09/24/15 0.0016 0.0005
18 03/29/16 0.0033 0.0044 0.0010
19 09/15/16 0.0530 0.0022
20 03/13/17 0.0930 0.0130
21 09/29/17 3.50 0.0005 0.0013
22 03/05/18 0.860 0.015
23 09/14/18 1.500
24 07/03/19 0.051 0.0047
25 02/14/20 0.28 0.015
26 11/17/20 1.2 0.0004 0.0018
27 06/17/21 3.1 0.0004 0.0004
28 12/28/21 0.039 0.0004 0.00042
29 06/27/22 0.16 0.0004 0.0004
30 12/05/22 0.46 0.003
31 06/15/23 0.0032 0.00519
32
33
34
35
Coefficient of Variation:3.93 2.62 3.50Mann-Kendall Statistic S :47 -136 -60Confidence Factor:88.6% >99.9% 95.2%
Concentration Trend:No Trend Decreasing Decreasing
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water, 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
TOLUENE CONCENTRATION (mg/L)
GSI Environmental Inc., www.gsi-net.com
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
7-Aug-23 27010
(Former) 321 Mini Mart Toluene
A. Long
0.0001
0.001
0.01
0.1
1
10
100
01/04 10/06 07/09 04/12 12/14 09/17 06/20 03/23 12/25
Co
n
c
e
n
t
r
a
t
i
o
n

(
m
g
/
L
)
Sampling Date
MW-1&R
MW-2&R
MW-3&R
Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:m /L
Sam lin Point ID:MW-1&R MW-2&R MW-3&R MW-6
Sampling SamplingEvent Date
1 06/06/07 13.00
2 06/11/07 1.00
3 02/02/08
4 07/24/07 4.70 1.00
5 09/01/09 2.600
6 03/10/10 0.0240 0.410 0.760000 1.1000
7 09/02/10 0.0830 0.920 0.700000 0.0790
8 03/14/11 0.0014 0.780 0.000500 0.0073
9 09/26/11 0.5100 0.051 0.000500 0.2600
10 03/12/12 0.360 0.000500 0.0005
11 09/24/12 0.9700
12 03/19/13 0.1500
13 09/23/13 0.0270 0.530 0.049000 0.0240
14 03/13/14 0.0230 0.033 0.002600 0.0740
15 09/11/14 0.00074 0.013 0.003000 0.00081
16 03/26/15 0.0240 0.007 0.014000 0.0056
17 09/24/15 0.0110 0.000800 0.1300
18 03/29/16 0.0760 0.029 0.014000 0.0240
19 09/15/16 0.0830 0.017000 0.0470
20 03/13/17 0.0240 0.011000 0.0490
21 09/29/17 0.2600 0.0005 0.001100 0.0390
22 03/05/18 0.1600 0.035 0.0650
23 09/14/18 0.4300 0.1000
24 07/03/19 0.41 0.012 0.019
25 02/14/20 0.65 0.022 0.0041
26 11/17/20 1.3 0.0016 0.045
27 06/17/21 1.1 0.017
28 12/18/21 0.29 0.0013 0.0045
29 06/27/22 0.38 0.0004 0.0004 0.012
30 12/05/22 0.31 0.043
31 06/15/23 0.0289 0.0208 0.0098
32
33
34
35
Coefficient of Variation:3.21 1.71 3.42 1.94Mann-Kendall Statistic S :91 -97 -26 -101Confidence Factor:99.2% >99.9% 77.2% 99.1%
Concentration Trend:Increasing Decreasing No Trend Decreasing
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water, 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
ETHYLBENZENE CONCENTRATION (mg/L)
GSI Environmental Inc., www.gsi-net.com
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
7-Aug-23 27010
(Former) 321 Mini Mart Ethylbenzene
A. Long
0.0001
0.001
0.01
0.1
1
10
100
01/04 10/06 07/09 04/12 12/14 09/17 06/20 03/23 12/25
Co
n
c
e
n
t
r
a
t
i
o
n

(
m
g
/
L
)
Sampling Date
MW-1&R
MW-2&R
MW-3&R
MW-6
Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:m /L
Sam lin Point ID:MW-1&R MW-2&R MW-3&R MW-6
Sampling SamplingEvent Date
1 06/06/07 71.00
2 06/11/07 5.90
3 02/02/08
4 07/24/07 27.00 5.40
5 09/01/09 22.50
6 03/10/10 0.3100 4.000 10.70 7.50
7 09/02/10 1.0700 7.100 3.50 0.6300
8 03/14/11 0.0102 4.600 0.00100 0.0420
9 09/26/11 2.3200 0.460 0.00100 2.1700
10 03/12/12 1.010 0.00490 0.0010
11 09/24/12 5.6000
12 03/19/13 0.1260
13 09/23/13 0.5900 3.500 0.10600 0.0310
14 03/13/14 0.3800 0.216 0.00195 0.0940
15 09/11/14 0.0119 0.300 0.01580 0.0015
16 03/26/15 0.3240 0.00732 0.03600 0.0048
17 09/24/15 0.1690 0.00100 0.2530
18 03/29/16 0.1380 0.086 0.00840 0.0177
19 09/15/16 0.1110 0.01880 0.0260
20 03/13/17 0.0910 0.02490 0.1110
21 09/29/17 1.7400 0.001 0.00319 0.0570
22 03/05/18 0.7500 0.350 0.1360
23 09/14/18 2.4000 0.0337
24 07/03/19 1.51 0.052 0.00264
25 02/14/20 1.82 0.0165 0.002
26 11/17/20 3.5 0.005 0.036
27 6/17/21 5.2 0.0076
28 12/28/21 0.49 0.0057 0.0029
29 6/27/22 0.87 0.00054 0.0008 0.0025
30 1/19/23 1.02 0.161
31 6/15/23 0.1358 0.0277 0.0199
32
33
34
35
Coefficient of Variation:3.51 1.94 3.15 2.31Mann-Kendall Statistic S :47 -103 -41 -116Confidence Factor:88.6% >99.9% 88.5% 99.7%
Concentration Trend:No Trend Decreasing No Trend Decreasing
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water, 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
XYLENES CONCENTRATION (mg/L)
GSI Environmental Inc., www.gsi-net.com
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
7-Aug-23 27010
(Former) 321 Mini Mart Xylenes
A. Long
0.0001
0.001
0.01
0.1
1
10
100
01/04 10/06 07/09 04/12 12/14 09/17 06/20 03/23 12/25
Co
n
c
e
n
t
r
a
t
i
o
n

(
m
g
/
L
)
Sampling Date
MW-1&R
MW-2&R
MW-3&R
MW-6
Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:mg/L
Sam lin Point ID:MW-1&R MW-2&R MW-3&R MW-6 W-1
Sampling SamplingEvent Date
1 06/06/07
2 06/11/07302/02/08
4 07/24/07 0.680
5 09/01/09 0.680
6 03/10/10 0.680 0.200 0.640 0.970
7 09/02/10 0.720 0.350 0.110 0.0470
8 03/14/11 0.00094 0.210 0.0005 0.0014
9 09/26/11 0.140 0.092 0.0005 0.1900
10 03/12/12 0.130 0.0005 0.0005
11 09/24/12 0.4400
12 03/19/13 0.1800
13 09/23/13 0.051 0.094 0.0270 0.0280
14 03/13/14 0.033 0.0065 0.0015 0.0380
15 09/11/14 0.0012 0.0022 0.00065 0.0014
16 03/26/15 0.030 0.016 0.0100 0.0052
17 09/24/15 0.018 0.0031 0.0600
18 03/29/16 0.067 0.030 0.0190 0.0520
19 09/15/16 0.072 0.0120 0.0320
20 03/13/17 0.023 0.0130 0.0410 0.000400
21 09/29/17 0.025 0.0005 0.0005 0.0140 0.000500
22 03/05/18 0.031 0.0025 0.0076 0.000500
23 09/14/18 0.089 0.079 0.0004
24 07/03/19 0.05 0.002 0.013 0.0004
25 02/14/20 0.087 0.0049 0.0025 0.0004
26 11/17/20 0.14 0.0013 0.03 0.0004
27 06/17/21 0.19 0.0004 0.03 0.00066
28 12/28/21 0.029 0.0036 0.0064 0.00041
29 06/27/22 0.06 0.004 0.00064 0.011 0.00061
30 12/05/22 0.067 0.00081 0.022
31 06/15/23 0.0064 0.0031 0.0298 0.16532
33
34
35
Coefficient of Variation:1.64 1.59 2.76 2.22 2.96Mann-Kendall Statistic S :19 -80 -54 -70 31
Confidence Factor:69.2% >99.9% 93.2% 94.6% 98.1%
Concentration Trend:No Trend Decreasing Prob. Decreasing Prob. Decreasing Increasing
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water , 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
NAPHTHALENE CONCENTRATION (mg/L)
GSI Environmental Inc., www.gsi-net.com
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
7-Aug-23 27010
(Former) 321 Mini Mart Naphthalene
A. Long
0.0001
0.001
0.01
0.1
1
01/04 10/06 07/09 04/12 12/14 09/17 06/20 03/23 12/25
Co
n
c
e
n
t
r
a
t
i
o
n

(
m
g
/
L
)
Sampling Date
MW-1&R
MW-2&R
MW-3&R
MW-6
VW-1

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

APPENDIX D – SUPPLEMENTAL SITE HISTORY TABLES

TABLE B‐2: SITE HISTORY ‐ UST/AST OWNER/OPERATOR and OTHER RESPONSIBLE PARTY 
INFORMATION 
(FORMER) 321 MINI MART 
2118 NORTH ASPEN STREET, LINCOLNTON, NORTH CAROLINA 
NCDEQ Incident No. 36228 
Excel Project No. 27010 

UST ID Number MO‐7591 

Facility ID Number 00‐0‐0000029957 

Owner Name (and Contact) Dates of Operation 
(mm/dd/yy to mm/dd/yy) 
Aum Shree Ganeshji, Inc. 2011 to present 
Street Address 
2118 North Aspen Street 
City State Zip Telephone Number 
Lincolnton NC 28092   
Operator Name (and Contact) Dates of Operation 
(mm/dd/yy to mm/dd/yy) 
Aum Shree Ganeshji, Inc. 2011 to present 
Street Address 
2118 North Aspen Street 
City State Zip Telephone Number 
Lincolnton NC 28092   
Other Incidents Onsite or Commingled/In Close Proximity 
Incident Number  Date Incident 
Occurred  
Name of Responsible Party  
for Other Incident  
Date Incident 
Reported  
 Date Incident Closed 
(i/a)  
Street Address 

City State Zip Telephone Number 

TABLE B‐5:  PUBLIC and PRIVATE WATER SUPPLY WELL and OTHER RECEPTOR INFORMATION 
(FORMER) 321 MINI MART 
2118 NORTH ASPEN STREET, LINCOLNTON, NORTH CAROLINA 
NCDEQ Incident No. 36228 
Excel Project No. 27010 

Well ID #  Property Owner Property Address Well Status 
SW-1 Robert Martin 2124 N. Aspen Street Inactive
SW-2 Robert Martin 2102 & 2106 N. Aspen Street Inactive
SW-3 Lincoln Co. Farm Bureau 2396 N. Aspen Street Inactive
SW-4 Marshall Withers 100 Keever Street Inactive
SW-5 Marshall Withers 100 Keever Street Inactive
SW-6 John Avery 102 Keever Street Inactive
SW-7 Jack Bailey 2144 N. Aspen Street Drinking
SW-9 Paul Joseph 107 Keever Street Inactive
SW-10 Edward Lobo 108 Keever Street Inactive
SW-11 Edith Martin 112 Keever Street Unknown
SW-12 Greg Guggisbey 205 Elizabeth Avenue Inactive
SW-13 Fred Mullinax 105 Eastview Drive Unknown
SW-14 Evelyn Lail 111 Carpenter Street Drinking
SW-15 Eddie Holly 2225 N. Aspen Street Inactive
SW-16 Michael Keener 2499 N. Aspen Street Unknown
SW-17 Michael Mull 105 Carpenter Street Unknown
SW-18 Michael Mull 112 Carpenter Street Unknown
SW-19 Ute Coffey 110 Shell Street Unknown
SW-20 Daphine Houser 2350 N. Aspen Street Unknown
SW-21 Bob Ramseur 1907 N. Aspen Street Drinking
SW-22 Janet Alvey 2246 N. Aspen Street Drinking
SW-23 E.L. Rudisill, Jr. 114 Mull Road Inactive
SW-24 Larry Hudson 100 Auton Street Unknown
SW-25 Clyde Lingerfelt 108 Auton Street Unknown
SW-26 Liberty Tabernacle 161 Shell Street Unknown
SW-27 Jeffery Ray Scronce 162 Shell Street Irrigation
SW-28 Mike Scronce 172 Shell Street Drinking
Notes: 
 ‐ Data obtained from Lincoln County GIS and returned well surveys

TABLE B‐7:  MONITORING and REMEDIATION WELL CONSTRUCTION INFORMATION
(FORMER) 321 MINI MART
2118 NORTH ASPEN STREET, LINCOLNTON, NORTH CAROLINA
NCDEQ Incident No. 36228
Excel Project No. 27010
Well ID
Number
MW-1 6/5/2007 22 7 – 22 100.00
MW-1R 5/16/2013 30 15 – 30 100.00
MW-2 6/5/2007 25 10 – 25 100.94
MW-2R 5/16/2013 30 15 – 30 100.94
MW-3 7/23/2007 25 10 – 25 99.38
MW-3R 5/16/2013 30 15 – 30 99.38
MW-4 7/23/2007 25 10 – 25 100.64
MW-5 2/5/2008 28 13 – 28 100.35
MW-6 2/5/2008 28 13 – 28 99.30
MW-7 2/4/2008 28 13 – 28 101.47
MW-8 2/4/2008 28 13 – 28 101.34
MW-9 2/4/2008 28 13 – 28 101.08
MW-10 5/9/2008 28 13 – 28 97.89
MW-11 5/9/2008 28 13 – 28 98.86
MW-12 5/9/2008 28 13 – 28 101.99
MW-13 5/9/2008 30 15 – 30 102.61
MW-14 8/7/2008 31 16 – 31 101.81
MW-15 8/7/2008 28 13 – 28 97.73
VW-1 2/4-5/08 50 45 – 50 --
VW-2 12/22-23/08 65 60 – 65 --
NOTES:
Elevation data based on assumed datum of 100.00’
Data provided in feet unless otherwise noted
Total
Depth
Top of
Casing
Elevation
Screen
Interval
Date
Installed
Interim Reporting Tables
Table B-12: Evaluation of Change in Contaminant Mass
Revision Date: 8/7/23 Incident Number and Name: (Former) 321 Mini Mart Facility ID#: 00-0-0000029957
Initial Mass Estimate /
Projected Milestones
(from CAP)
Initial
Baseline
Milestones1 End /
Closure (Label 1) (Label 2) (Label 3) (Label 4) (Label 5) (Label 6) (Label 7) (Label 8) (Label 9)
Projected Mass Reduction
(%): 0% Active
Y1
Active
Y2
Active
Y3
Active
Y4
Active
Y5 MNA MNA MNA MNA
Soil Source Zone Mass
(Pro ected):
Smear Source Zone Mass
(Pro ected):
Total Mass:
Baseline/Milestone (Proj) 199

Measured / Calculated
Change in Contaminant
Mass (from sampling)
Milestone Sampling / Measurement Event Dates1
2007 2009 2010 2011 2013 2014 2015 2016 2017 12/2022 6/2023
Measured Mass2 -
Soil Source Zone:
Smear Source Zone:
LNAPL 2,960,000
Groundwater Zone: 193,079 49,459 23,730 15,000 2,405 38 117 164 1,672 1,019 1,027 199

Removed Mass3 -
Excavated from Soil/Smear:
Extracted as Vapor/Gas:
Extracted as Liquid:
Total Mass Removed (est.):

Revised Total Mass (est.)4: 193,079 49,459 23,730 15,000 2,405 38 117 164 1,672 1,019 2,961,027 199
Estimated Reduction Rate5: 74.4% 52% 36.8% 84% 98.4% -208% -40% -91.9% 39.5% -2,904%
Reference Milestone (label
rom above)
Reference Milestone (value
rom above)
Reduction Progress vs
Milestone6: -969.2 -247.5 -118.2 -74.4 -11.1 0.81 0.41 0.18 -7.4 - 4.1 - 14,878
1. Milestones are defined in the CAP. Label column headers with a representative title (‘Active Y1’, ‘MNA Yr 5’ etc.) Add sheets/columns as needed to more effectively track progress.
Interim Reporting Tables
2. Calculate the measured mass for each unit by multiplying the analytical result by the representative volume (weight, pore space, etc.). (See https://www3.epa.gov/region02/rcra/ra2.pdf)
3. Calculate removed amounts based on excavation screening and/or system effluent monitoring, multiplied by total volume excavated or the system throughput during that period.
4. Where measured from sampling/screening in situ, use the total Measured Mass. Where not screened (or if not representative), use prior Total Mass less current Total Mass Removed.
5. This equals the % reduction from the prior mass (current Total Mass ÷ prior Total Mass). Very large negative values may indicate a new contribution and may require investigation.
6. This equals the current mass reduction % progress (1 - (Revised Total Mass ÷ Applicable Milestone)). Zero or positive values indicate that the associated milestone has been reached

EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com

APPENDIX E - LABORATORY ANALYSES & CHAIN OF CUSTODY FORM

#=CL#
July 05, 2023
LIMS USE: FR - DONNA FARRIS
LIMS OBJECT ID: 92672791
92672791
Project:
Pace Project No.:
RE:
Donna Farris
Excel Civil & Environmental Assoc.
625 Huntsman Ct.
Gastonia, NC 28054
321 MINI MART
Dear Donna Farris:
Enclosed are the analytical results for sample(s) received by the laboratory on June 15, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni for
[e-mail]
Project Manager
Tyriek Hooks
[phone]
Enclosures
cc: Ms. Donna Farris, Excel Environmental Assoc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92672791
321 MINI MART
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
Virginia Certification #: 460204
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 39
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92672791
321 MINI MART
Lab ID Sample ID Matrix Date Collected Date Received
92672791001 MW-2R Water 06/14/23 13:30 06/15/23 14:24
92672791002 MW-3R Water 06/14/23 15:00 06/15/23 14:24
92672791003 MW-6 Water 06/14/23 15:45 06/15/23 14:24
92672791004 VW-1 Water 06/14/23 12:00 06/15/23 14:24
92672791005 TRIP BLANK Water 06/15/23 14:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92672791
321 MINI MART
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92672791001 MW-2R RSK 175 Modified 1 PASI-CTEG
EPA 6010D 2 PASI-GADRB
SM 6200B 63 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
SM 5310B-2014 1 PASI-AMJP
SM 4500-CO2 D-2011 2 PASI-AKDF1
92672791002 MW-3R RSK 175 Modified 1 PASI-CTEG
EPA 6010D 2 PASI-GADRB
SM 6200B 63 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
SM 5310B-2014 1 PASI-AMJP
SM 4500-CO2 D-2011 2 PASI-AKDF1
92672791003 MW-6 RSK 175 Modified 1 PASI-CTEG
EPA 6010D 2 PASI-GADRB
SM 6200B 63 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
SM 5310B-2014 1 PASI-AMJP
SM 4500-CO2 D-2011 2 PASI-AKDF1
92672791004 VW-1 RSK 175 Modified 1 PASI-CTEG
EPA 6010D 2 PASI-GADRB
SM 6200B 63 PASI-CLMB
SM 2320B-2011 1 PASI-ASMS
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
SM 5310B-2014 1 PASI-AMJP
SM 4500-CO2 D-2011 2 PASI-AKDF1
92672791005 TRIP BLANK SM 6200B 63 PASI-CSAS
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: MW-2R Lab ID: 92672791001 Collected: 06/14/23 13:30 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
RSK 175 Headspace
Methane 49.0 ug/L 06/20/23 11:09 74-82-810.0 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Iron 8330 ug/L 06/20/23 14:34 7439-89-606/20/23 10:5340.0 1
Manganese 1960 ug/L 06/20/23 14:34 7439-96-506/20/23 10:5340.0 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 0.51 ug/L 06/26/23 15:47 71-43-20.50 1
Bromobenzene ND ug/L 06/26/23 15:47 108-86-10.50 1
Bromochloromethane ND ug/L 06/26/23 15:47 74-97-50.50 1
Bromodichloromethane ND ug/L 06/26/23 15:47 75-27-40.50 1
Bromoform ND ug/L 06/26/23 15:47 75-25-20.50 1
Bromomethane ND ug/L 06/26/23 15:47 74-83-95.0 1
n-Butylbenzene ND ug/L 06/26/23 15:47 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/26/23 15:47 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/26/23 15:47 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/26/23 15:47 56-23-50.50 1
Chlorobenzene ND ug/L 06/26/23 15:47 108-90-70.50 1
Chloroethane ND ug/L 06/26/23 15:47 75-00-31.0 1
Chloroform ND ug/L 06/26/23 15:47 67-66-30.50 1
Chloromethane ND ug/L 06/26/23 15:47 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/26/23 15:47 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/26/23 15:47 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/26/23 15:47 96-12-81.0 1
Dibromochloromethane ND ug/L 06/26/23 15:47 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/26/23 15:47 106-93-40.50 1
Dibromomethane ND ug/L 06/26/23 15:47 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/26/23 15:47 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/26/23 15:47 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/26/23 15:47 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/26/23 15:47 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/26/23 15:47 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/26/23 15:47 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/26/23 15:47 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/26/23 15:47 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/26/23 15:47 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/26/23 15:47 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/26/23 15:47 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/26/23 15:47 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/26/23 15:47 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/26/23 15:47 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/26/23 15:47 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/26/23 15:47 108-20-30.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: MW-2R Lab ID: 92672791001 Collected: 06/14/23 13:30 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Ethylbenzene 28.9 ug/L 06/26/23 15:47 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/26/23 15:47 87-68-32.0 1
Isopropylbenzene (Cumene)4.2 ug/L 06/26/23 15:47 98-82-80.50 1
Methylene Chloride ND ug/L 06/26/23 15:47 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/26/23 15:47 1634-04-40.50 1
Naphthalene 6.4 ug/L 06/26/23 15:47 91-20-32.0 1
n-Propylbenzene 11.2 ug/L 06/26/23 15:47 103-65-10.50 1
Styrene ND ug/L 06/26/23 15:47 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/26/23 15:47 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/26/23 15:47 79-34-50.50 1
Tetrachloroethene ND ug/L 06/26/23 15:47 127-18-40.50 1
Toluene 3.2 ug/L 06/26/23 15:47 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/26/23 15:47 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/26/23 15:47 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/26/23 15:47 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/26/23 15:47 79-00-50.50 1
Trichloroethene ND ug/L 06/26/23 15:47 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/26/23 15:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/26/23 15:47 96-18-40.50 1
1,2,4-Trimethylbenzene 90.5 ug/L 06/26/23 15:47 95-63-60.50 1
1,3,5-Trimethylbenzene 20.5 ug/L 06/26/23 15:47 108-67-80.50 1
Vinyl chloride ND ug/L 06/26/23 15:47 75-01-41.0 1
m&p-Xylene 97.0 ug/L 06/26/23 15:47 179601-23-11.0 1
o-Xylene 38.8 ug/L 06/26/23 15:47 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %06/26/23 15:47 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/26/23 15:47 460-00-470-130 1
Toluene-d8 (S)103 %06/26/23 15:47 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 8.6 mg/L 06/24/23 17:215.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC anions 48hr
Nitrate as N ND mg/L 06/15/23 21:59 14797-55-80.10 1
Sulfate ND mg/L 06/15/23 21:59 14808-79-81.0 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon ND mg/L 06/28/23 05:57 7440-44-01.0 1
Analytical Method: SM 4500-CO2 D-2011
Pace Analytical Services - Asheville
Carbon Dioxide Calculation
Carbon dioxide 33.0 mg/L 06/26/23 13:39 124-38-9 N25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: MW-2R Lab ID: 92672791001 Collected: 06/14/23 13:30 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 4500-CO2 D-2011
Pace Analytical Services - Asheville
Carbon Dioxide Calculation
Carbon Dioxide, Free 25.5 mg/L 06/26/23 13:39 124-38-9 N21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: MW-3R Lab ID: 92672791002 Collected: 06/14/23 15:00 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
RSK 175 Headspace
Methane 388 ug/L 06/20/23 11:25 74-82-810.0 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Iron 29200 ug/L 06/20/23 14:39 7439-89-606/20/23 10:5340.0 1
Manganese 2940 ug/L 06/20/23 14:39 7439-96-506/20/23 10:5340.0 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 21.0 ug/L 06/26/23 15:12 71-43-20.50 1
Bromobenzene ND ug/L 06/26/23 15:12 108-86-10.50 1
Bromochloromethane ND ug/L 06/26/23 15:12 74-97-50.50 1
Bromodichloromethane ND ug/L 06/26/23 15:12 75-27-40.50 1
Bromoform ND ug/L 06/26/23 15:12 75-25-20.50 1
Bromomethane ND ug/L 06/26/23 15:12 74-83-95.0 1
n-Butylbenzene ND ug/L 06/26/23 15:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/26/23 15:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/26/23 15:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/26/23 15:12 56-23-50.50 1
Chlorobenzene ND ug/L 06/26/23 15:12 108-90-70.50 1
Chloroethane ND ug/L 06/26/23 15:12 75-00-31.0 1
Chloroform ND ug/L 06/26/23 15:12 67-66-30.50 1
Chloromethane ND ug/L 06/26/23 15:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/26/23 15:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/26/23 15:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/26/23 15:12 96-12-81.0 1
Dibromochloromethane ND ug/L 06/26/23 15:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/26/23 15:12 106-93-40.50 1
Dibromomethane ND ug/L 06/26/23 15:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/26/23 15:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/26/23 15:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/26/23 15:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/26/23 15:12 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/26/23 15:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/26/23 15:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/26/23 15:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/26/23 15:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/26/23 15:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/26/23 15:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/26/23 15:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/26/23 15:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/26/23 15:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/26/23 15:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/26/23 15:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/26/23 15:12 108-20-30.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: MW-3R Lab ID: 92672791002 Collected: 06/14/23 15:00 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Ethylbenzene 10.8 ug/L 06/26/23 15:12 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/26/23 15:12 87-68-32.0 1
Isopropylbenzene (Cumene)1.3 ug/L 06/26/23 15:12 98-82-80.50 1
Methylene Chloride ND ug/L 06/26/23 15:12 75-09-22.0 1
Methyl-tert-butyl ether 0.85 ug/L 06/26/23 15:12 1634-04-40.50 1
Naphthalene 3.1 ug/L 06/26/23 15:12 91-20-32.0 1
n-Propylbenzene 2.1 ug/L 06/26/23 15:12 103-65-10.50 1
Styrene ND ug/L 06/26/23 15:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/26/23 15:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/26/23 15:12 79-34-50.50 1
Tetrachloroethene ND ug/L 06/26/23 15:12 127-18-40.50 1
Toluene 51.9 ug/L 06/26/23 15:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/26/23 15:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/26/23 15:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/26/23 15:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/26/23 15:12 79-00-50.50 1
Trichloroethene ND ug/L 06/26/23 15:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/26/23 15:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/26/23 15:12 96-18-40.50 1
1,2,4-Trimethylbenzene 4.2 ug/L 06/26/23 15:12 95-63-60.50 1
1,3,5-Trimethylbenzene 1.8 ug/L 06/26/23 15:12 108-67-80.50 1
Vinyl chloride ND ug/L 06/26/23 15:12 75-01-41.0 1
m&p-Xylene 23.1 ug/L 06/26/23 15:12 179601-23-11.0 1
o-Xylene 4.6 ug/L 06/26/23 15:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %06/26/23 15:12 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/26/23 15:12 460-00-470-130 1
Toluene-d8 (S)100 %06/26/23 15:12 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 55.4 mg/L 06/24/23 17:265.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC anions 48hr
Nitrate as N ND mg/L 06/15/23 22:14 14797-55-80.10 1
Sulfate 1.8 mg/L 06/15/23 22:14 14808-79-81.0 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon 15.3 mg/L 06/28/23 06:15 7440-44-01.0 1
Analytical Method: SM 4500-CO2 D-2011
Pace Analytical Services - Asheville
Carbon Dioxide Calculation
Carbon dioxide 92.8 mg/L 06/26/23 13:39 124-38-9 N25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: MW-3R Lab ID: 92672791002 Collected: 06/14/23 15:00 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 4500-CO2 D-2011
Pace Analytical Services - Asheville
Carbon Dioxide Calculation
Carbon Dioxide, Free 44.1 mg/L 06/26/23 13:39 124-38-9 N21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: MW-6 Lab ID: 92672791003 Collected: 06/14/23 15:45 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
RSK 175 Headspace
Methane 75.3 ug/L 06/20/23 11:41 74-82-810.0 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Iron 6120 ug/L 06/20/23 14:44 7439-89-606/20/23 10:5340.0 1
Manganese 12900 ug/L 06/20/23 14:44 7439-96-506/20/23 10:5340.0 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 53.4 ug/L 06/26/23 15:29 71-43-20.50 1
Bromobenzene ND ug/L 06/26/23 15:29 108-86-10.50 1
Bromochloromethane ND ug/L 06/26/23 15:29 74-97-50.50 1
Bromodichloromethane ND ug/L 06/26/23 15:29 75-27-40.50 1
Bromoform ND ug/L 06/26/23 15:29 75-25-20.50 1
Bromomethane ND ug/L 06/26/23 15:29 74-83-95.0 1
n-Butylbenzene ND ug/L 06/26/23 15:29 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/26/23 15:29 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/26/23 15:29 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/26/23 15:29 56-23-50.50 1
Chlorobenzene ND ug/L 06/26/23 15:29 108-90-70.50 1
Chloroethane ND ug/L 06/26/23 15:29 75-00-31.0 1
Chloroform ND ug/L 06/26/23 15:29 67-66-30.50 1
Chloromethane ND ug/L 06/26/23 15:29 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/26/23 15:29 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/26/23 15:29 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/26/23 15:29 96-12-81.0 1
Dibromochloromethane ND ug/L 06/26/23 15:29 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/26/23 15:29 106-93-40.50 1
Dibromomethane ND ug/L 06/26/23 15:29 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/26/23 15:29 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/26/23 15:29 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/26/23 15:29 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/26/23 15:29 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/26/23 15:29 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/26/23 15:29 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/26/23 15:29 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/26/23 15:29 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/26/23 15:29 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/26/23 15:29 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/26/23 15:29 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/26/23 15:29 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/26/23 15:29 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/26/23 15:29 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/26/23 15:29 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/26/23 15:29 108-20-30.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: MW-6 Lab ID: 92672791003 Collected: 06/14/23 15:45 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Ethylbenzene 9.8 ug/L 06/26/23 15:29 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/26/23 15:29 87-68-32.0 1
Isopropylbenzene (Cumene)8.6 ug/L 06/26/23 15:29 98-82-80.50 1
Methylene Chloride ND ug/L 06/26/23 15:29 75-09-22.0 1
Methyl-tert-butyl ether 4.1 ug/L 06/26/23 15:29 1634-04-40.50 1
Naphthalene 29.8 ug/L 06/26/23 15:29 91-20-32.0 1
n-Propylbenzene 7.8 ug/L 06/26/23 15:29 103-65-10.50 1
Styrene ND ug/L 06/26/23 15:29 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/26/23 15:29 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/26/23 15:29 79-34-50.50 1
Tetrachloroethene ND ug/L 06/26/23 15:29 127-18-40.50 1
Toluene 31.1 ug/L 06/26/23 15:29 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/26/23 15:29 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/26/23 15:29 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/26/23 15:29 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/26/23 15:29 79-00-50.50 1
Trichloroethene ND ug/L 06/26/23 15:29 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/26/23 15:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/26/23 15:29 96-18-40.50 1
1,2,4-Trimethylbenzene 2.7 ug/L 06/26/23 15:29 95-63-60.50 1
1,3,5-Trimethylbenzene 0.62 ug/L 06/26/23 15:29 108-67-80.50 1
Vinyl chloride ND ug/L 06/26/23 15:29 75-01-41.0 1
m&p-Xylene 11.2 ug/L 06/26/23 15:29 179601-23-11.0 1
o-Xylene 8.7 ug/L 06/26/23 15:29 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)110 %06/26/23 15:29 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %06/26/23 15:29 460-00-470-130 1
Toluene-d8 (S)99 %06/26/23 15:29 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 30.9 mg/L 06/24/23 17:335.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC anions 48hr
Nitrate as N ND mg/L 06/15/23 22:29 14797-55-80.10 1
Sulfate 11.1 mg/L 06/15/23 22:29 14808-79-81.0 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon 2.4 mg/L 06/28/23 06:33 7440-44-01.0 1
Analytical Method: SM 4500-CO2 D-2011
Pace Analytical Services - Asheville
Carbon Dioxide Calculation
Carbon dioxide 101 mg/L 06/26/23 13:39 124-38-9 N25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: MW-6 Lab ID: 92672791003 Collected: 06/14/23 15:45 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 4500-CO2 D-2011
Pace Analytical Services - Asheville
Carbon Dioxide Calculation
Carbon Dioxide, Free 74.3 mg/L 06/26/23 13:39 124-38-9 N21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: VW-1 Lab ID: 92672791004 Collected: 06/14/23 12:00 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
RSK 175 Headspace
Methane ND ug/L 06/20/23 11:56 74-82-810.0 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Iron 764 ug/L 06/20/23 14:49 7439-89-606/20/23 10:5340.0 1
Manganese 2360 ug/L 06/20/23 14:49 7439-96-506/20/23 10:5340.0 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 178 ug/L 06/26/23 16:59 71-43-22.5 5
Bromobenzene ND ug/L 06/26/23 16:59 108-86-12.5 5
Bromochloromethane ND ug/L 06/26/23 16:59 74-97-52.5 5
Bromodichloromethane ND ug/L 06/26/23 16:59 75-27-42.5 5
Bromoform ND ug/L 06/26/23 16:59 75-25-22.5 5
Bromomethane ND ug/L 06/26/23 16:59 74-83-925.0 5
n-Butylbenzene ND ug/L 06/26/23 16:59 104-51-82.5 5
sec-Butylbenzene ND ug/L 06/26/23 16:59 135-98-82.5 5
tert-Butylbenzene ND ug/L 06/26/23 16:59 98-06-62.5 5
Carbon tetrachloride ND ug/L 06/26/23 16:59 56-23-52.5 5
Chlorobenzene ND ug/L 06/26/23 16:59 108-90-72.5 5
Chloroethane ND ug/L 06/26/23 16:59 75-00-35.0 5
Chloroform ND ug/L 06/26/23 16:59 67-66-32.5 5
Chloromethane ND ug/L 06/26/23 16:59 74-87-35.0 5
2-Chlorotoluene ND ug/L 06/26/23 16:59 95-49-82.5 5
4-Chlorotoluene ND ug/L 06/26/23 16:59 106-43-42.5 5
1,2-Dibromo-3-chloropropane ND ug/L 06/26/23 16:59 96-12-85.0 5
Dibromochloromethane ND ug/L 06/26/23 16:59 124-48-12.5 5
1,2-Dibromoethane (EDB)ND ug/L 06/26/23 16:59 106-93-42.5 5
Dibromomethane ND ug/L 06/26/23 16:59 74-95-32.5 5
1,2-Dichlorobenzene ND ug/L 06/26/23 16:59 95-50-12.5 5
1,3-Dichlorobenzene ND ug/L 06/26/23 16:59 541-73-12.5 5
1,4-Dichlorobenzene ND ug/L 06/26/23 16:59 106-46-72.5 5
Dichlorodifluoromethane ND ug/L 06/26/23 16:59 75-71-82.5 5
1,1-Dichloroethane ND ug/L 06/26/23 16:59 75-34-32.5 5
1,2-Dichloroethane ND ug/L 06/26/23 16:59 107-06-22.5 5
1,1-Dichloroethene ND ug/L 06/26/23 16:59 75-35-42.5 5
cis-1,2-Dichloroethene ND ug/L 06/26/23 16:59 156-59-22.5 5
trans-1,2-Dichloroethene ND ug/L 06/26/23 16:59 156-60-52.5 5
1,2-Dichloropropane ND ug/L 06/26/23 16:59 78-87-52.5 5
1,3-Dichloropropane ND ug/L 06/26/23 16:59 142-28-92.5 5
2,2-Dichloropropane ND ug/L 06/26/23 16:59 594-20-72.5 5
1,1-Dichloropropene ND ug/L 06/26/23 16:59 563-58-62.5 5
cis-1,3-Dichloropropene ND ug/L 06/26/23 16:59 10061-01-52.5 5
trans-1,3-Dichloropropene ND ug/L 06/26/23 16:59 10061-02-62.5 5
Diisopropyl ether 13.9 ug/L 06/26/23 16:59 108-20-32.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: VW-1 Lab ID: 92672791004 Collected: 06/14/23 12:00 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Ethylbenzene 144 ug/L 06/26/23 16:59 100-41-42.5 5
Hexachloro-1,3-butadiene ND ug/L 06/26/23 16:59 87-68-310.0 5
Isopropylbenzene (Cumene)11.4 ug/L 06/26/23 16:59 98-82-82.5 5
Methylene Chloride ND ug/L 06/26/23 16:59 75-09-210.0 5
Methyl-tert-butyl ether ND ug/L 06/26/23 16:59 1634-04-42.5 5
Naphthalene 165 ug/L 06/26/23 16:59 91-20-310.0 5
n-Propylbenzene 44.7 ug/L 06/26/23 16:59 103-65-12.5 5
Styrene ND ug/L 06/26/23 16:59 100-42-52.5 5
1,1,1,2-Tetrachloroethane ND ug/L 06/26/23 16:59 630-20-62.5 5
1,1,2,2-Tetrachloroethane ND ug/L 06/26/23 16:59 79-34-52.5 5
Tetrachloroethene ND ug/L 06/26/23 16:59 127-18-42.5 5
Toluene 856 ug/L 06/26/23 16:59 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 06/26/23 16:59 87-61-610.0 5
1,2,4-Trichlorobenzene ND ug/L 06/26/23 16:59 120-82-110.0 5
1,1,1-Trichloroethane ND ug/L 06/26/23 16:59 71-55-62.5 5
1,1,2-Trichloroethane ND ug/L 06/26/23 16:59 79-00-52.5 5
Trichloroethene ND ug/L 06/26/23 16:59 79-01-62.5 5
Trichlorofluoromethane ND ug/L 06/26/23 16:59 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 06/26/23 16:59 96-18-42.5 5
1,2,4-Trimethylbenzene 482 ug/L 06/26/23 16:59 95-63-62.5 5
1,3,5-Trimethylbenzene 116 ug/L 06/26/23 16:59 108-67-82.5 5
Vinyl chloride ND ug/L 06/26/23 16:59 75-01-45.0 5
m&p-Xylene 540 ug/L 06/26/23 16:59 179601-23-15.0 5
o-Xylene 242 ug/L 06/26/23 16:59 95-47-62.5 5
Surrogates
1,2-Dichloroethane-d4 (S)101 %06/26/23 16:59 17060-07-070-130 5
4-Bromofluorobenzene (S)99 %06/26/23 16:59 460-00-470-130 5
Toluene-d8 (S)102 %06/26/23 16:59 2037-26-570-130 5
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 27.4 mg/L 06/24/23 17:495.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC anions 48hr
Nitrate as N 0.48 mg/L 06/15/23 21:29 14797-55-80.10 1
Sulfate 1.5 mg/L 06/15/23 21:29 14808-79-81.0 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon ND mg/L 06/28/23 06:51 7440-44-01.0 1
Analytical Method: SM 4500-CO2 D-2011
Pace Analytical Services - Asheville
Carbon Dioxide Calculation
Carbon dioxide 44.5 mg/L 06/26/23 13:39 124-38-9 N25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: VW-1 Lab ID: 92672791004 Collected: 06/14/23 12:00 Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 4500-CO2 D-2011
Pace Analytical Services - Asheville
Carbon Dioxide Calculation
Carbon Dioxide, Free 20.4 mg/L 06/26/23 13:39 124-38-9 N21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: TRIP BLANK Lab ID: 92672791005 Collected:Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 06/24/23 06:56 71-43-20.50 1
Bromobenzene ND ug/L 06/24/23 06:56 108-86-10.50 1
Bromochloromethane ND ug/L 06/24/23 06:56 74-97-50.50 1
Bromodichloromethane ND ug/L 06/24/23 06:56 75-27-40.50 1
Bromoform ND ug/L 06/24/23 06:56 75-25-20.50 1
Bromomethane ND ug/L 06/24/23 06:56 74-83-95.0 1
n-Butylbenzene ND ug/L 06/24/23 06:56 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/24/23 06:56 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/24/23 06:56 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/24/23 06:56 56-23-50.50 1
Chlorobenzene ND ug/L 06/24/23 06:56 108-90-70.50 1
Chloroethane ND ug/L 06/24/23 06:56 75-00-31.0 1
Chloroform ND ug/L 06/24/23 06:56 67-66-30.50 1
Chloromethane ND ug/L 06/24/23 06:56 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/24/23 06:56 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/24/23 06:56 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/24/23 06:56 96-12-81.0 1
Dibromochloromethane ND ug/L 06/24/23 06:56 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/24/23 06:56 106-93-40.50 1
Dibromomethane ND ug/L 06/24/23 06:56 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/24/23 06:56 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/24/23 06:56 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/24/23 06:56 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/24/23 06:56 75-71-8 IH0.50 1
1,1-Dichloroethane ND ug/L 06/24/23 06:56 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/24/23 06:56 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/24/23 06:56 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/24/23 06:56 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/24/23 06:56 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/24/23 06:56 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/24/23 06:56 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/24/23 06:56 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/24/23 06:56 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/24/23 06:56 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/24/23 06:56 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/24/23 06:56 108-20-30.50 1
Ethylbenzene ND ug/L 06/24/23 06:56 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/24/23 06:56 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/24/23 06:56 98-82-80.50 1
Methylene Chloride ND ug/L 06/24/23 06:56 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/24/23 06:56 1634-04-40.50 1
Naphthalene ND ug/L 06/24/23 06:56 91-20-32.0 1
n-Propylbenzene ND ug/L 06/24/23 06:56 103-65-10.50 1
Styrene ND ug/L 06/24/23 06:56 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/24/23 06:56 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/24/23 06:56 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92672791
321 MINI MART
Sample: TRIP BLANK Lab ID: 92672791005 Collected:Received: 06/15/23 14:24 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 06/24/23 06:56 127-18-40.50 1
Toluene ND ug/L 06/24/23 06:56 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/24/23 06:56 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/24/23 06:56 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/24/23 06:56 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/24/23 06:56 79-00-50.50 1
Trichloroethene ND ug/L 06/24/23 06:56 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/24/23 06:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/24/23 06:56 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/24/23 06:56 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/24/23 06:56 108-67-80.50 1
Vinyl chloride ND ug/L 06/24/23 06:56 75-01-41.0 1
m&p-Xylene ND ug/L 06/24/23 06:56 179601-23-11.0 1
o-Xylene ND ug/L 06/24/23 06:56 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)82 %06/24/23 06:56 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %06/24/23 06:56 460-00-470-130 1
Toluene-d8 (S)95 %06/24/23 06:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
781659
RSK 175 Modified
RSK 175 Modified
RSK 175 HEADSPACE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92672791001, 92672791002, 92672791003, 92672791004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4055101
Associated Lab Samples:92672791001, 92672791002, 92672791003, 92672791004
Matrix: Water
Analyzed
Methane ug/L ND 10.0 06/20/23 10:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4055102LABORATORY CONTROL SAMPLE:
LCSSpike
Methane ug/L 322297 108 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4057483MATRIX SPIKE SAMPLE:
MSSpike
Result
92673012008
Methane ug/L 304297 100 70-130ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92673088004
4057481SAMPLE DUPLICATE:
Methane ug/L 7J 207.1J
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92673012005
4057482SAMPLE DUPLICATE:
Methane ug/L 6J 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
781630
EPA 3010A
EPA 6010D
6010D ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92672791001, 92672791002, 92672791003, 92672791004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4054961
Associated Lab Samples:92672791001, 92672791002, 92672791003, 92672791004
Matrix: Water
Analyzed
Iron ug/L ND 40.0 06/20/23 14:25
Manganese ug/L ND 40.0 06/20/23 14:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4054962LABORATORY CONTROL SAMPLE:
LCSSpike
Iron ug/L 9431000 94 80-120
Manganese ug/L 9711000 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4055092MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92672979006
4055093
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Iron ug/L 1000 89 75-12595 3 2010002271920 1980
Manganese ug/L 1000 93 75-12593 0 20100071.8 1000 1000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782720
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92672791005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4060279
Associated Lab Samples:92672791005
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/24/23 03:58
1,1,1-Trichloroethane ug/L ND 0.50 06/24/23 03:58
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/24/23 03:58
1,1,2-Trichloroethane ug/L ND 0.50 06/24/23 03:58
1,1-Dichloroethane ug/L ND 0.50 06/24/23 03:58
1,1-Dichloroethene ug/L ND 0.50 06/24/23 03:58
1,1-Dichloropropene ug/L ND 0.50 06/24/23 03:58
1,2,3-Trichlorobenzene ug/L ND 2.0 06/24/23 03:58
1,2,3-Trichloropropane ug/L ND 0.50 06/24/23 03:58
1,2,4-Trichlorobenzene ug/L ND 2.0 06/24/23 03:58
1,2,4-Trimethylbenzene ug/L ND 0.50 06/24/23 03:58
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/24/23 03:58
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/24/23 03:58
1,2-Dichlorobenzene ug/L ND 0.50 06/24/23 03:58
1,2-Dichloroethane ug/L ND 0.50 06/24/23 03:58
1,2-Dichloropropane ug/L ND 0.50 06/24/23 03:58
1,3,5-Trimethylbenzene ug/L ND 0.50 06/24/23 03:58
1,3-Dichlorobenzene ug/L ND 0.50 06/24/23 03:58
1,3-Dichloropropane ug/L ND 0.50 06/24/23 03:58
1,4-Dichlorobenzene ug/L ND 0.50 06/24/23 03:58
2,2-Dichloropropane ug/L ND 0.50 06/24/23 03:58
2-Chlorotoluene ug/L ND 0.50 06/24/23 03:58
4-Chlorotoluene ug/L ND 0.50 06/24/23 03:58
Benzene ug/L ND 0.50 06/24/23 03:58
Bromobenzene ug/L ND 0.50 06/24/23 03:58
Bromochloromethane ug/L ND 0.50 06/24/23 03:58
Bromodichloromethane ug/L ND 0.50 06/24/23 03:58
Bromoform ug/L ND 0.50 06/24/23 03:58
Bromomethane ug/L ND 5.0 06/24/23 03:58
Carbon tetrachloride ug/L ND 0.50 06/24/23 03:58
Chlorobenzene ug/L ND 0.50 06/24/23 03:58
Chloroethane ug/L ND 1.0 06/24/23 03:58
Chloroform ug/L ND 0.50 06/24/23 03:58
Chloromethane ug/L ND 1.0 06/24/23 03:58
cis-1,2-Dichloroethene ug/L ND 0.50 06/24/23 03:58
cis-1,3-Dichloropropene ug/L ND 0.50 06/24/23 03:58
Dibromochloromethane ug/L ND 0.50 06/24/23 03:58
Dibromomethane ug/L ND 0.50 06/24/23 03:58
Dichlorodifluoromethane ug/L ND 0.50 IH06/24/23 03:58
Diisopropyl ether ug/L ND 0.50 06/24/23 03:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4060279
Associated Lab Samples:92672791005
Matrix: Water
Analyzed
Ethylbenzene ug/L ND 0.50 06/24/23 03:58
Hexachloro-1,3-butadiene ug/L ND 2.0 06/24/23 03:58
Isopropylbenzene (Cumene)ug/L ND 0.50 06/24/23 03:58
m&p-Xylene ug/L ND 1.0 06/24/23 03:58
Methyl-tert-butyl ether ug/L ND 0.50 06/24/23 03:58
Methylene Chloride ug/L ND 2.0 06/24/23 03:58
n-Butylbenzene ug/L ND 0.50 06/24/23 03:58
n-Propylbenzene ug/L ND 0.50 06/24/23 03:58
Naphthalene ug/L ND 2.0 06/24/23 03:58
o-Xylene ug/L ND 0.50 06/24/23 03:58
sec-Butylbenzene ug/L ND 0.50 06/24/23 03:58
Styrene ug/L ND 0.50 06/24/23 03:58
tert-Butylbenzene ug/L ND 0.50 06/24/23 03:58
Tetrachloroethene ug/L ND 0.50 06/24/23 03:58
Toluene ug/L ND 0.50 06/24/23 03:58
trans-1,2-Dichloroethene ug/L ND 0.50 06/24/23 03:58
trans-1,3-Dichloropropene ug/L ND 0.50 06/24/23 03:58
Trichloroethene ug/L ND 0.50 06/24/23 03:58
Trichlorofluoromethane ug/L ND 1.0 06/24/23 03:58
Vinyl chloride ug/L ND 1.0 06/24/23 03:58
1,2-Dichloroethane-d4 (S)%83 70-130 06/24/23 03:58
4-Bromofluorobenzene (S)%94 70-130 06/24/23 03:58
Toluene-d8 (S)%97 70-130 06/24/23 03:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4060280LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.720 109 60-140
1,1,1-Trichloroethane ug/L 19.320 97 60-140
1,1,2,2-Tetrachloroethane ug/L 20.220 101 60-140
1,1,2-Trichloroethane ug/L 21.020 105 60-140
1,1-Dichloroethane ug/L 17.920 89 60-140
1,1-Dichloroethene ug/L 20.020 100 60-140
1,1-Dichloropropene ug/L 19.620 98 60-140
1,2,3-Trichlorobenzene ug/L 21.520 108 60-140
1,2,3-Trichloropropane ug/L 18.820 94 60-140
1,2,4-Trichlorobenzene ug/L 21.520 107 60-140
1,2,4-Trimethylbenzene ug/L 20.320 102 60-140
1,2-Dibromo-3-chloropropane ug/L 21.020 105 60-140
1,2-Dibromoethane (EDB)ug/L 21.820 109 60-140
1,2-Dichlorobenzene ug/L 21.220 106 60-140
1,2-Dichloroethane ug/L 17.020 85 60-140
1,2-Dichloropropane ug/L 19.920 99 60-140
1,3,5-Trimethylbenzene ug/L 19.920 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4060280LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 21.120 105 60-140
1,3-Dichloropropane ug/L 19.320 97 60-140
1,4-Dichlorobenzene ug/L 20.320 101 60-140
2,2-Dichloropropane ug/L 16.220 81 60-140
2-Chlorotoluene ug/L 18.820 94 60-140
4-Chlorotoluene ug/L 19.520 98 60-140
Benzene ug/L 20.520 102 60-140
Bromobenzene ug/L 20.720 104 60-140
Bromochloromethane ug/L 20.020 100 60-140
Bromodichloromethane ug/L 19.620 98 60-140
Bromoform ug/L 21.320 106 60-140
Bromomethane ug/L 16.320 82 60-140
Carbon tetrachloride ug/L 21.320 107 60-140
Chlorobenzene ug/L 20.820 104 60-140
Chloroethane ug/L 18.920 95 60-140
Chloroform ug/L 18.120 91 60-140
Chloromethane ug/L 16.920 84 60-140
cis-1,2-Dichloroethene ug/L 17.820 89 60-140
cis-1,3-Dichloropropene ug/L 20.020 100 60-140
Dibromochloromethane ug/L 21.820 109 60-140
Dibromomethane ug/L 25.220 126 60-140
Dichlorodifluoromethane ug/L 23.3 IH20116 60-140
Diisopropyl ether ug/L 16.220 81 60-140
Ethylbenzene ug/L 19.720 98 60-140
Hexachloro-1,3-butadiene ug/L 21.520 107 60-140
Isopropylbenzene (Cumene)ug/L 21.220 106 60-140
m&p-Xylene ug/L 40.140 100 60-140
Methyl-tert-butyl ether ug/L 17.420 87 60-140
Methylene Chloride ug/L 16.620 83 60-140
n-Butylbenzene ug/L 18.920 95 60-140
n-Propylbenzene ug/L 18.520 93 60-140
Naphthalene ug/L 21.920 109 60-140
o-Xylene ug/L 21.120 106 60-140
sec-Butylbenzene ug/L 19.720 98 60-140
Styrene ug/L 22.120 110 60-140
tert-Butylbenzene ug/L 16.620 83 60-140
Tetrachloroethene ug/L 21.620 108 60-140
Toluene ug/L 20.020 100 60-140
trans-1,2-Dichloroethene ug/L 18.720 93 60-140
trans-1,3-Dichloropropene ug/L 19.620 98 60-140
Trichloroethene ug/L 22.220 111 60-140
Trichlorofluoromethane ug/L 20.220 101 60-140
Vinyl chloride ug/L 16.620 83 60-140
1,2-Dichloroethane-d4 (S)%82 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4060281MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92672652004
4060282
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L M12014560-140141 3 3020ND29.1 28.2
1,1,1-Trichloroethane ug/L 20 135 60-140130 3 3020ND27.0 26.1
1,1,2,2-Tetrachloroethane ug/L 20 130 60-140125 4 3020ND26.0 25.0
1,1,2-Trichloroethane ug/L 20 134 60-140130 3 3020ND26.7 26.0
1,1-Dichloroethane ug/L 20 124 60-140121 3 3020ND24.7 24.1
1,1-Dichloroethene ug/L M12014460-140137 5 3020ND28.7 27.4
1,1-Dichloropropene ug/L M12014260-140137 3 3020ND28.5 27.5
1,2,3-Trichlorobenzene ug/L M12015260-140137 10 3020ND30.3 27.5
1,2,3-Trichloropropane ug/L 20 121 60-140115 5 3020ND24.2 23.0
1,2,4-Trichlorobenzene ug/L M12015060-140137 9 3020ND30.1 27.4
1,2,4-Trimethylbenzene ug/L 20 139 60-140133 4 3020ND27.7 26.6
1,2-Dibromo-3-
chloropropane ug/L M12014460-140135 6 3020ND28.8 27.1
1,2-Dibromoethane (EDB) ug/L 20 140 60-140135 4 3020ND28.0 26.9
1,2-Dichlorobenzene ug/L 20 137 60-140133 3 3020ND27.3 26.6
1,2-Dichloroethane ug/L 20 117 60-140112 4 3020ND23.3 22.4
1,2-Dichloropropane ug/L 20 130 60-140126 3 3020ND26.0 25.3
1,3,5-Trimethylbenzene ug/L 20 136 60-140130 4 3020ND27.1 26.1
1,3-Dichlorobenzene ug/L 20 139 60-140133 5 3020ND27.8 26.5
1,3-Dichloropropane ug/L 20 127 60-140121 4 3020ND25.4 24.2
1,4-Dichlorobenzene ug/L 20 137 60-140130 5 3020ND27.4 26.1
2,2-Dichloropropane ug/L 20 134 60-140128 5 3020ND26.9 25.6
2-Chlorotoluene ug/L 20 128 60-140123 3 3020ND25.5 24.7
4-Chlorotoluene ug/L 20 132 60-140126 5 3020ND26.4 25.1
Benzene ug/L 20 134 60-140130 3 3020ND26.9 26.0
Bromobenzene ug/L 20 137 60-140131 5 3020ND27.5 26.2
Bromochloromethane ug/L 20 134 60-140132 2 3020ND26.9 26.3
Bromodichloromethane ug/L 20 130 60-140126 3 3020ND25.9 25.2
Bromoform ug/L 20 140 60-140135 3 3020ND28.0 27.0
Bromomethane ug/L 20 106 60-140105 1 3020ND21.2 21.0
Carbon tetrachloride ug/L M12014860-140144 3 3020ND29.6 28.7
Chlorobenzene ug/L 20 137 60-140133 3 3020ND27.5 26.6
Chloroethane ug/L 20 126 60-140120 5 3020ND25.2 24.1
Chloroform ug/L 20 124 60-140121 2 3020ND24.8 24.2
Chloromethane ug/L 20 105 60-14099 5 3020ND21.0 19.9
cis-1,2-Dichloroethene ug/L 20 124 60-140118 4 3020ND24.7 23.7
cis-1,3-Dichloropropene ug/L 20 132 60-140128 3 3020ND26.4 25.6
Dibromochloromethane ug/L M12014960-140142 4 3020ND29.7 28.5
Dibromomethane ug/L M12015660-140153 2 3020ND31.2 30.6
Dichlorodifluoromethane ug/L IH,M12014860-140143 3 3020ND29.5 28.6
Diisopropyl ether ug/L 20 114 60-140109 4 3020ND22.7 21.8
Ethylbenzene ug/L 20 132 60-140128 3 3020ND26.4 25.6
Hexachloro-1,3-butadiene ug/L M12016660-140157 5 3020ND33.1 31.4
Isopropylbenzene
(Cumene)
ug/L M12014360-140140 2 3020ND28.6 28.0
m&p-Xylene ug/L 40 134 60-140131 2 3040ND53.6 52.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4060281MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92672652004
4060282
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 119 60-140115 3 30201.3 25.1 24.4
Methylene Chloride ug/L 20 111 60-140107 4 3020ND22.3 21.4
n-Butylbenzene ug/L 20 140 60-140133 5 3020ND28.0 26.5
n-Propylbenzene ug/L 20 129 60-140124 4 3020ND25.8 24.8
Naphthalene ug/L M12015060-140138 9 3020ND30.1 27.6
o-Xylene ug/L 20 137 60-140134 3 3020ND27.4 26.7
sec-Butylbenzene ug/L 20 138 60-140132 5 3020ND27.7 26.4
Styrene ug/L M12014860-140141 4 3020ND29.5 28.3
tert-Butylbenzene ug/L 20 114 60-140110 4 3020ND22.8 22.0
Tetrachloroethene ug/L M12014860-140144 3 3020ND29.6 28.8
Toluene ug/L 20 128 60-140125 3 3020ND25.6 24.9
trans-1,2-Dichloroethene ug/L 20 131 60-140127 3 3020ND26.2 25.4
trans-1,3-Dichloropropene ug/L 20 133 60-140128 4 3020ND26.6 25.7
Trichloroethene ug/L M12014760-140144 2 3020ND29.4 28.7
Trichlorofluoromethane ug/L M12014860-140141 5 3020ND29.6 28.2
Vinyl chloride ug/L 20 113 60-140107 5 3020ND22.6 21.5
1,2-Dichloroethane-d4 (S) %83 70-13083
4-Bromofluorobenzene (S) %96 70-13098
Toluene-d8 (S)%93 70-13094
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782988
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92672791001, 92672791002, 92672791003, 92672791004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4061168
Associated Lab Samples:92672791001, 92672791002, 92672791003, 92672791004
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/26/23 13:07
1,1,1-Trichloroethane ug/L ND 0.50 06/26/23 13:07
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/26/23 13:07
1,1,2-Trichloroethane ug/L ND 0.50 06/26/23 13:07
1,1-Dichloroethane ug/L ND 0.50 06/26/23 13:07
1,1-Dichloroethene ug/L ND 0.50 06/26/23 13:07
1,1-Dichloropropene ug/L ND 0.50 06/26/23 13:07
1,2,3-Trichlorobenzene ug/L ND 2.0 06/26/23 13:07
1,2,3-Trichloropropane ug/L ND 0.50 06/26/23 13:07
1,2,4-Trichlorobenzene ug/L ND 2.0 06/26/23 13:07
1,2,4-Trimethylbenzene ug/L ND 0.50 06/26/23 13:07
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/26/23 13:07
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/26/23 13:07
1,2-Dichlorobenzene ug/L ND 0.50 06/26/23 13:07
1,2-Dichloroethane ug/L ND 0.50 06/26/23 13:07
1,2-Dichloropropane ug/L ND 0.50 06/26/23 13:07
1,3,5-Trimethylbenzene ug/L ND 0.50 06/26/23 13:07
1,3-Dichlorobenzene ug/L ND 0.50 06/26/23 13:07
1,3-Dichloropropane ug/L ND 0.50 06/26/23 13:07
1,4-Dichlorobenzene ug/L ND 0.50 06/26/23 13:07
2,2-Dichloropropane ug/L ND 0.50 06/26/23 13:07
2-Chlorotoluene ug/L ND 0.50 06/26/23 13:07
4-Chlorotoluene ug/L ND 0.50 06/26/23 13:07
Benzene ug/L ND 0.50 06/26/23 13:07
Bromobenzene ug/L ND 0.50 06/26/23 13:07
Bromochloromethane ug/L ND 0.50 06/26/23 13:07
Bromodichloromethane ug/L ND 0.50 06/26/23 13:07
Bromoform ug/L ND 0.50 06/26/23 13:07
Bromomethane ug/L ND 5.0 06/26/23 13:07
Carbon tetrachloride ug/L ND 0.50 06/26/23 13:07
Chlorobenzene ug/L ND 0.50 06/26/23 13:07
Chloroethane ug/L ND 1.0 06/26/23 13:07
Chloroform ug/L ND 0.50 06/26/23 13:07
Chloromethane ug/L ND 1.0 06/26/23 13:07
cis-1,2-Dichloroethene ug/L ND 0.50 06/26/23 13:07
cis-1,3-Dichloropropene ug/L ND 0.50 06/26/23 13:07
Dibromochloromethane ug/L ND 0.50 06/26/23 13:07
Dibromomethane ug/L ND 0.50 06/26/23 13:07
Dichlorodifluoromethane ug/L ND 0.50 06/26/23 13:07
Diisopropyl ether ug/L ND 0.50 06/26/23 13:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4061168
Associated Lab Samples:92672791001, 92672791002, 92672791003, 92672791004
Matrix: Water
Analyzed
Ethylbenzene ug/L ND 0.50 06/26/23 13:07
Hexachloro-1,3-butadiene ug/L ND 2.0 06/26/23 13:07
Isopropylbenzene (Cumene)ug/L ND 0.50 06/26/23 13:07
m&p-Xylene ug/L ND 1.0 06/26/23 13:07
Methyl-tert-butyl ether ug/L ND 0.50 06/26/23 13:07
Methylene Chloride ug/L ND 2.0 06/26/23 13:07
n-Butylbenzene ug/L ND 0.50 06/26/23 13:07
n-Propylbenzene ug/L ND 0.50 06/26/23 13:07
Naphthalene ug/L ND 2.0 06/26/23 13:07
o-Xylene ug/L ND 0.50 06/26/23 13:07
sec-Butylbenzene ug/L ND 0.50 06/26/23 13:07
Styrene ug/L ND 0.50 06/26/23 13:07
tert-Butylbenzene ug/L ND 0.50 06/26/23 13:07
Tetrachloroethene ug/L ND 0.50 06/26/23 13:07
Toluene ug/L ND 0.50 06/26/23 13:07
trans-1,2-Dichloroethene ug/L ND 0.50 06/26/23 13:07
trans-1,3-Dichloropropene ug/L ND 0.50 06/26/23 13:07
Trichloroethene ug/L ND 0.50 06/26/23 13:07
Trichlorofluoromethane ug/L ND 1.0 06/26/23 13:07
Vinyl chloride ug/L ND 1.0 06/26/23 13:07
1,2-Dichloroethane-d4 (S)%98 70-130 06/26/23 13:07
4-Bromofluorobenzene (S)%101 70-130 06/26/23 13:07
Toluene-d8 (S)%100 70-130 06/26/23 13:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4061169LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.120 101 60-140
1,1,1-Trichloroethane ug/L 20.920 104 60-140
1,1,2,2-Tetrachloroethane ug/L 21.220 106 60-140
1,1,2-Trichloroethane ug/L 21.420 107 60-140
1,1-Dichloroethane ug/L 20.320 101 60-140
1,1-Dichloroethene ug/L 20.720 104 60-140
1,1-Dichloropropene ug/L 22.320 111 60-140
1,2,3-Trichlorobenzene ug/L 21.520 107 60-140
1,2,3-Trichloropropane ug/L 19.720 99 60-140
1,2,4-Trichlorobenzene ug/L 21.120 105 60-140
1,2,4-Trimethylbenzene ug/L 19.720 99 60-140
1,2-Dibromo-3-chloropropane ug/L 19.320 97 60-140
1,2-Dibromoethane (EDB)ug/L 20.520 103 60-140
1,2-Dichlorobenzene ug/L 20.920 104 60-140
1,2-Dichloroethane ug/L 20.920 105 60-140
1,2-Dichloropropane ug/L 20.620 103 60-140
1,3,5-Trimethylbenzene ug/L 20.320 102 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4061169LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 20.320 101 60-140
1,3-Dichloropropane ug/L 20.620 103 60-140
1,4-Dichlorobenzene ug/L 20.220 101 60-140
2,2-Dichloropropane ug/L 20.520 103 60-140
2-Chlorotoluene ug/L 20.620 103 60-140
4-Chlorotoluene ug/L 20.320 101 60-140
Benzene ug/L 19.920 100 60-140
Bromobenzene ug/L 19.720 99 60-140
Bromochloromethane ug/L 19.720 98 60-140
Bromodichloromethane ug/L 20.520 102 60-140
Bromoform ug/L 20.320 101 60-140
Bromomethane ug/L 15.020 75 60-140
Carbon tetrachloride ug/L 20.920 104 60-140
Chlorobenzene ug/L 19.820 99 60-140
Chloroethane ug/L 18.820 94 60-140
Chloroform ug/L 20.520 103 60-140
Chloromethane ug/L 17.920 90 60-140
cis-1,2-Dichloroethene ug/L 20.020 100 60-140
cis-1,3-Dichloropropene ug/L 20.520 103 60-140
Dibromochloromethane ug/L 19.520 97 60-140
Dibromomethane ug/L 20.020 100 60-140
Dichlorodifluoromethane ug/L 21.520 108 60-140
Diisopropyl ether ug/L 19.020 95 60-140
Ethylbenzene ug/L 19.520 98 60-140
Hexachloro-1,3-butadiene ug/L 21.520 108 60-140
Isopropylbenzene (Cumene)ug/L 20.220 101 60-140
m&p-Xylene ug/L 39.240 98 60-140
Methyl-tert-butyl ether ug/L 19.920 100 60-140
Methylene Chloride ug/L 19.720 99 60-140
n-Butylbenzene ug/L 20.920 105 60-140
n-Propylbenzene ug/L 20.020 100 60-140
Naphthalene ug/L 21.020 105 60-140
o-Xylene ug/L 19.120 96 60-140
sec-Butylbenzene ug/L 20.220 101 60-140
Styrene ug/L 19.420 97 60-140
tert-Butylbenzene ug/L 19.220 96 60-140
Tetrachloroethene ug/L 20.220 101 60-140
Toluene ug/L 18.920 94 60-140
trans-1,2-Dichloroethene ug/L 20.320 101 60-140
trans-1,3-Dichloropropene ug/L 20.520 103 60-140
Trichloroethene ug/L 20.420 102 60-140
Trichlorofluoromethane ug/L 20.020 100 60-140
Vinyl chloride ug/L 15.820 79 60-140
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
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Page 28 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4061170MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673894002
4061171
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 113 60-140120 5 3020ND22.7 23.9
1,1,1-Trichloroethane ug/L 20 125 60-140131 5 3020ND24.9 26.1
1,1,2,2-Tetrachloroethane ug/L 20 111 60-140118 6 3020ND22.3 23.7
1,1,2-Trichloroethane ug/L 20 117 60-140125 6 3020ND23.5 24.9
1,1-Dichloroethane ug/L 20 123 60-140127 3 3020ND24.5 25.3
1,1-Dichloroethene ug/L 20 133 60-140139 4 3020ND26.6 27.8
1,1-Dichloropropene ug/L 20 132 60-140138 4 3020ND26.4 27.7
1,2,3-Trichlorobenzene ug/L 20 115 60-140123 7 3020ND22.9 24.7
1,2,3-Trichloropropane ug/L 20 106 60-140113 7 3020ND21.1 22.7
1,2,4-Trichlorobenzene ug/L 20 114 60-140119 4 3020ND22.8 23.8
1,2,4-Trimethylbenzene ug/L 20 116 60-140118 1 3020ND23.2 23.5
1,2-Dibromo-3-
chloropropane ug/L 20 96 60-140104 8 3020ND19.2 20.8
1,2-Dibromoethane (EDB) ug/L 20 111 60-140116 4 3020ND22.2 23.2
1,2-Dichlorobenzene ug/L 20 115 60-140121 4 3020ND23.1 24.1
1,2-Dichloroethane ug/L 20 118 60-140125 5 3020ND23.7 25.0
1,2-Dichloropropane ug/L 20 119 60-140122 2 3020ND23.9 24.3
1,3,5-Trimethylbenzene ug/L 20 117 60-140121 3 3020ND23.4 24.2
1,3-Dichlorobenzene ug/L 20 113 60-140117 3 3020ND22.7 23.4
1,3-Dichloropropane ug/L 20 114 60-140120 5 3020ND22.8 24.0
1,4-Dichlorobenzene ug/L 20 111 60-140117 5 3020ND22.2 23.3
2,2-Dichloropropane ug/L 20 119 60-140124 4 3020ND23.8 24.7
2-Chlorotoluene ug/L 20 116 60-140121 5 3020ND23.1 24.3
4-Chlorotoluene ug/L 20 113 60-140117 3 3020ND22.7 23.4
Benzene ug/L 20 120 60-140124 4 3020ND23.9 24.8
Bromobenzene ug/L 20 109 60-140115 5 3020ND21.9 22.9
Bromochloromethane ug/L 20 117 60-140121 4 3020ND23.4 24.3
Bromodichloromethane ug/L 20 113 60-140118 4 3020ND22.5 23.5
Bromoform ug/L 20 105 60-140113 8 3020ND20.9 22.6
Bromomethane ug/L 20 73 60-14083 12 3020ND14.7 16.5
Carbon tetrachloride ug/L 20 120 60-140128 6 3020ND24.0 25.5
Chlorobenzene ug/L 20 112 60-140117 5 3020ND22.3 23.4
Chloroethane ug/L 20 134 60-140136 1 3020ND26.8 27.2
Chloroform ug/L 20 123 60-140125 2 3020ND24.6 25.0
Chloromethane ug/L 20 129 60-140133 3 3020ND25.7 26.6
cis-1,2-Dichloroethene ug/L 20 115 60-140123 6 30204.7 27.7 29.4
cis-1,3-Dichloropropene ug/L 20 114 60-140119 5 3020ND22.8 23.9
Dibromochloromethane ug/L 20 107 60-140115 7 3020ND21.5 23.0
Dibromomethane ug/L 20 112 60-140118 5 3020ND22.4 23.6
Dichlorodifluoromethane ug/L M12018560-140191 3 3020ND37.0 38.3
Diisopropyl ether ug/L 20 109 60-140114 4 3020ND21.9 22.8
Ethylbenzene ug/L 20 112 60-140118 5 3020ND22.3 23.5
Hexachloro-1,3-butadiene ug/L 20 121 60-140121 0 3020ND24.2 24.2
Isopropylbenzene
(Cumene)
ug/L 20 116 60-140122 5 3020ND23.2 24.4
m&p-Xylene ug/L 40 111 60-140116 4 3040ND44.5 46.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4061170MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673894002
4061171
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 109 60-140117 6 3020ND21.9 23.3
Methylene Chloride ug/L 20 118 60-140121 2 3020ND23.6 24.1
n-Butylbenzene ug/L 20 122 60-140124 2 3020ND24.5 24.9
n-Propylbenzene ug/L 20 116 60-140120 4 3020ND23.1 23.9
Naphthalene ug/L 20 116 60-140119 3 3020ND23.1 23.8
o-Xylene ug/L 20 108 60-140113 5 3020ND21.6 22.7
sec-Butylbenzene ug/L 20 118 60-140121 3 3020ND23.5 24.3
Styrene ug/L 20 108 60-140115 6 3020ND21.6 22.9
tert-Butylbenzene ug/L 20 93 60-14096 3 3020ND18.6 19.2
Tetrachloroethene ug/L 20 111 60-140117 5 3020ND22.3 23.5
Toluene ug/L 20 108 60-140114 6 3020ND21.5 22.9
trans-1,2-Dichloroethene ug/L 20 125 60-140129 3 3020ND24.9 25.7
trans-1,3-Dichloropropene ug/L 20 112 60-140120 7 3020ND22.4 23.9
Trichloroethene ug/L 20 120 60-140127 6 3020ND24.0 25.4
Trichlorofluoromethane ug/L M12013660-140142 4 3020ND27.3 28.3
Vinyl chloride ug/L 20 115 60-140126 7 30207.2 30.2 32.4
1,2-Dichloroethane-d4 (S) %102 70-130105
4-Bromofluorobenzene (S) %100 70-130100
Toluene-d8 (S)%100 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782630
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92672791001, 92672791002, 92672791003, 92672791004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4059617
Associated Lab Samples:92672791001, 92672791002, 92672791003, 92672791004
Matrix: Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 06/24/23 15:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4059618LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 52.150 104 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4059619LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 53.150 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4059620MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92672899001
4059621
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 109 80-120107 0 2550193247 246
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4059622MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92672899002
4059623
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 105 80-120101 4 2550ND52.5 50.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
780913
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92672791001, 92672791002, 92672791003, 92672791004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4051539
Associated Lab Samples:92672791001, 92672791002, 92672791003, 92672791004
Matrix: Water
Analyzed
Nitrate as N mg/L ND 0.10 06/15/23 20:59
Sulfate mg/L ND 1.0 06/15/23 20:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4051540LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrate as N mg/L 2.42.5 94 90-110
Sulfate mg/L 50.450 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4051541MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92672791003
4051542
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrate as N mg/L 2.5 97 90-110100 3 102.5ND 2.5 2.6
Sulfate mg/L 50 98 90-110101 2 105011.1 60.2 61.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92672791
321 MINI MART
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783317
SM 5310B-2014
SM 5310B-2014
5310B TOC
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92672791001, 92672791002, 92672791003, 92672791004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4062643
Associated Lab Samples:92672791001, 92672791002, 92672791003, 92672791004
Matrix: Water
Analyzed
Total Organic Carbon mg/L ND 1.0 06/27/23 22:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4062644LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon mg/L 24.225 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062645MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673071002
4062646
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon mg/L 25 93 90-11091 2 10255.7 29.1 28.4
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4062647MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673071003
4062648
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon mg/L 25 95 90-11094 0 10254.7 28.4 28.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 39
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92672791
321 MINI MART
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 39
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92672791
321 MINI MART
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92672791001 781659MW-2R RSK 175 Modified
92672791002 781659MW-3R RSK 175 Modified
92672791003 781659MW-6 RSK 175 Modified
92672791004 781659VW-1 RSK 175 Modified
92672791001 781630 781720MW-2R EPA 3010A EPA 6010D
92672791002 781630 781720MW-3R EPA 3010A EPA 6010D
92672791003 781630 781720MW-6 EPA 3010A EPA 6010D
92672791004 781630 781720VW-1 EPA 3010A EPA 6010D
92672791001 782988MW-2R SM 6200B
92672791002 782988MW-3R SM 6200B
92672791003 782988MW-6 SM 6200B
92672791004 782988VW-1 SM 6200B
92672791005 782720TRIP BLANK SM 6200B
92672791001 782630MW-2R SM 2320B-2011
92672791002 782630MW-3R SM 2320B-2011
92672791003 782630MW-6 SM 2320B-2011
92672791004 782630VW-1 SM 2320B-2011
92672791001 780913MW-2R EPA 300.0 Rev 2.1 1993
92672791002 780913MW-3R EPA 300.0 Rev 2.1 1993
92672791003 780913MW-6 EPA 300.0 Rev 2.1 1993
92672791004 780913VW-1 EPA 300.0 Rev 2.1 1993
92672791001 783317MW-2R SM 5310B-2014
92672791002 783317MW-3R SM 5310B-2014
92672791003 783317MW-6 SM 5310B-2014
92672791004 783317VW-1 SM 5310B-2014
92672791001 783045MW-2R SM 4500-CO2 D-2011
92672791002 783045MW-3R SM 4500-CO2 D-2011
92672791003 783045MW-6 SM 4500-CO2 D-2011
92672791004 783045VW-1 SM 4500-CO2 D-2011
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/05/2023 04:54 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 39
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