MO-6637_27368_CA_SAR_20231102_Littles Super Market

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
November 2, 2023

Mr. Ryan Mills
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Soil Assessment Report
October 2023
Little’s Super Market
8200 North Carolina Highway 90 East
Stony Point, Alexander County
North Carolina
Facility ID Number: 0-00-0000001931
Incident Number: 27368
GRI Project Number: 3043

Dear Mr. Mills,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Joanna Alley at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ms. Gail Williams; Shell Brothers Distributors, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Soil Assessment Report
October 2023
Little’s Super Market
8200 North Carolina Highway 90 East
Stony Point, Alexander County
North Carolina
Facility ID Number: 0-00-0000001931
Incident Number: 27368
GRI Project Number: 3043

Prepared for:

Ms. Gail Williams
Shell Brothers Distributors, Inc.
1 Fountain Manor Drive, Unit C
Greensboro, North Carolina, 27405

November 2, 2023

Joanna Alley, P.E.
Project Manager
Xavier T. Farmer, G.I.T.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: November 2, 2023 Little’s Super Market
Project Manager: Joanna Alley, P.E. GRI Project No. 3043
ii

EXECUTIVE SUMMARY
Little’s Super Market is located at 8200 NC Highway 90 East in Stony Point, Alexander County, North
Carolina. The adjoining properties are residential and commercial. The site is currently occupied by The
Redeemer’s House, Inc. A release was discovered at the site when petroleum-impacted ground water
and soil were encountered during UST closure activities conducted in December 2002. Fourteen water
supply wells are located within 1,000 feet of the source area, three of which are potable. Two water
supply wells were identified within a 250-foot radius of the site.
Based on an Active Remediation Monitoring Report prepared by EA in March 2011, an SVE/AS
remediation system was installed at the site and became operational in May 2010. The system was
turned off in October 2020 as directed by the September 21, 2020 correspondence from the NCDEQ. In
a subsequent ARR dated October 22, 2021, the NCDEQ recommended that the remediation system be
returned to service for an additional 6 months. The system briefly returned to service but is currently in
need of repairs.
On October 5, 2023, five soil borings (SB-1 through SB-5) were advanced to total depths of 16 to 25 feet
BGS, each. PID values were collected every 2 feet from all borings. The soil samples with the highest PID
values in the unsaturated zone, saturated zone and/or smear zone were submitted for UVF analysis.
Once analyzed by the UVF method, the sample with the highest contaminant concentrations from each
boring was submitted for contaminant-specific analysis by method 8260D. A concentration of GRO that
exceeded the RAL was reported in soil sample SB-1-12’. No contaminant concentrations exceeded the
MCCs.
Based on this information, the risk classification for the site should remain intermediate risk. Although
there was an RAL exceedance for TPH-GRO in the soil, the petroleum contamination present at the site
appears to be more prevalent in ground water. A comprehensive sampling event including natural
attenuation parameters should be conducted at the site. Following the sampling event, GRI
recommends conducting a pilot test using injections to determine if full scale application of injectables is
a feasible remedial strategy. The next sampling event is tentatively scheduled for December 2023.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: November 2, 2023 Little’s Super Market
Project Manager: Joanna Alley, P.E. GRI Project No. 3043
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant
Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: November 2, 2023 Little’s Super Market
Project Manager: Joanna Alley, P.E. GRI Project No. 3043
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ ii
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 SOIL ANALYTICAL RESULTS .......................................................................................................2
3.0 SOIL CLEANUP PLAN ................................................................................................................2
4.0 CONCLUSIONS .........................................................................................................................2
5.0 LIMITATIONS ...........................................................................................................................3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Site Vicinity Map
Figure 4: Soil Quality Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Receptor Information
Table 4: Adjacent Property Owner Information
Table 5: Soil Sample Screening Results
Table 6: Summary of Soil Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Subsurface Logs
Appendix C: UVF Analytical Report
Appendix D: Laboratory Analytical Report

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: November 2, 2023 Little’s Super Market
Project Manager: Joanna Alley, P.E. GRI Project No. 3043
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the April and May 2023 soil assessment event at the Little’s Super Market
site, located at 8200 North Carolina Highway 90 East in Stony Point, Alexander County, North Carolina
(Figure 1). These activities were conducted in accordance with GRI Proposal No. 23-525, which was
submitted to NCDEQ on November 21, 2022, and was approved as Task Authorization No. 27368-80 on
August 22, 2023. State correspondence is included as Appendix A.

The site is currently owned by the Redeemer’s House, Inc. and operated as a church. It has historically
operated as a country store, former petroleum retail facility, and automotive repair facility. The three
6,000-gallon gasoline USTs and one 1,000-gallon kerosene UST were removed in December 2002. Two
1,200-gallon gasoline USTs, one 1,000-gallon diesel UST, and two 750-gallon USTs of unknown contents
were closed in place in December 1984 and were removed in January 2010. UST capacities and contents
are based on Initial Abatement Activities conducted in January 2010. No USTs are currently installed at
the site. UST owner/operator information and UST system information are included as Tables 1 and 2,
respectively. The Registered Tank Report is shown below:

The site and surrounding area are a mixture of residential and commercial properties. The site contains
two buildings (the store and the remediation building) and is primarily capped with concrete and
asphalt. The overall topography at the site is relatively flat and the property slopes downward to the
southwest. To date, eighteen Type II monitoring wells (MW-1 through MW-11, MW-11R and MW-12
through MW-17) and one Type III telescoping well (DW-1) were installed at the site during previous
ground water assessment activities. A Site Map showing the locations of the monitoring wells and the
structures on-site is included as Figure 2.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: November 2, 2023 Little’s Super Market
Project Manager: Joanna Alley, P.E. GRI Project No. 3043
2

On November 25 and December 17, 2013, GRI personnel updated the receptor survey. Twenty-two
water supply wells were located within a 1,500-foot radius of the source area. Three potable water
supply wells were located within a 1,000-foot radius of the site and two non-potable water supply wells
are located with a 250-foot radius of the site. Please note that the owner of water supply well WSW-5
would like to use the well for drinking water in the future. To date, the concentrations of benzene,
naphthalene, 1,2-DCA, bromodichloromethane and/or dibromochloromethane reported in WSW-5,
WSW-16, and WSW-18 have historically exceeded the MACs. This contamination was reported to the
NCDEQ during each sampling event. Municipal water is available to the site and surrounding properties.
No surface water bodies were identified with a 500-foot radius of the site. Receptor information is
provided in Table 3. Adjacent property owner information is presented in Table 4. A Site Vicinity Map
showing the adjacent properties is included as Figure 3.
2.0 SOIL ANALYTICAL RESULTS
On October 5, 2023, ten soil borings (SB-1 through SB-5 and SB-7 through SB-11) were advanced to total
depths of 20 feet BGS, each. PID values were collected from all borings in 2-foot intervals. The 4 soil
samples from each boring with the highest PID values above the water table were submitted for onsite
analysis of TPH-GRO and TPH-DRO using a mobile UVF laboratory. The highest UVF sample from each
boring was then submitted for laboratory analysis of VOCs by Method 8260D.

Concentrations of GRO that exceeded the RAL were reported in soil samples SB-1-12’. The locations of
the soil borings are shown on Figure 4. The subsurface logs are included as Appendix B. The soil
screening results are presented in Table 5. Soil sample analytical results are included as Table 6. Copies
of the October UVF analytical reports are included as Appendix C. Soil Sample laboratory analytical
results are included as Appendix D. A summary of the soil analytical data is shown below:

Analytical
Method → PID EPA Methods 8105D
GRO & 8015B DRO
Sa
m
p
l
e

I
D

Sa
m
p
l
e

D
e
p
t
h

(f
t
-BG
S
)

PI
D

R
e
a
d
i
n
g
s

TP
H
-GR
O

TP
H
-DR
O

RALs (mg/kg) 50 100
SB-1-2' 2 7.0 --- ---
SB-1-4' 4 26.5 --- ---
SB-1-6' 6 29.4 --- ---
SB-1-8' 8 56.3 <10 2.6
SB-1-10' 10 78.1 --- ---
SB-1-12' 12 175.3 283.6 18.0
Analytical
Method → PID EPA Methods 8105D
GRO & 8015B DRO
Sa
m
p
l
e

I
D

Sa
m
p
l
e

D
e
p
t
h

(f
t
-BG
S
)

PI
D

R
e
a
d
i
n
g
s

TP
H
-GR
O

TP
H
-DR
O

RALs (mg/kg) 50 100
SB-1-14' 14 163.5 --- ---
SB-1-16' 16 170.2 --- ---
SB-1-18' 18 12.9 --- ---
SB-1-20' 20 22.1 --- ---
SB-1-22' 22 17.9 --- ---
SB-1-24' 24 2,356 <10 3.2

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: November 2, 2023 Little’s Super Market
Project Manager: Joanna Alley, P.E. GRI Project No. 3043
2
Analytical
Method → PID EPA Methods 8105D
GRO & 8015B DRO
Sa
m
p
l
e

I
D

Sa
m
p
l
e

D
e
p
t
h

(f
t
-BG
S
)

PI
D

R
e
a
d
i
n
g
s

TP
H
-GR
O

TP
H
-DR
O

RALs (mg/kg) 50 100
SB-1-25' 25 2,836 --- ---
SB-2-2' 2 11.5 --- ---
SB-2-4' 4 86.5 --- ---
SB-2-6' 6 35.5 <20 <4
SB-2-8' 8 16.8 --- ---
SB-2-10' 10 17.9 --- ---
SB-2-12' 12 11.4 --- ---
SB-2-14' 14 17.7 --- ---
SB-2-16' 16 9.4 <20 <4
SB-3-2' 2 4.6 --- ---
SB-3-4' 4 4.3 --- ---
SB-3-6' 6 3.1 <10 <2
SB-3-8' 8 2.1 --- ---
SB-3-10' 10 3.9 --- ---
SB-3-12' 12 3.6 --- ---
SB-3-14' 14 1.2 --- ---
SB-3-16' 16 1.7 <10 3.8
Analytical
Method → PID EPA Methods 8105D
GRO & 8015B DRO
Sa
m
p
l
e

I
D

Sa
m
p
l
e

D
e
p
t
h

(f
t
-BG
S
)

PI
D

R
e
a
d
i
n
g
s

TP
H
-GR
O

TP
H
-DR
O

RALs (mg/kg) 50 100
SB-4-2' 2 9.7 --- ---
SB-4-4' 4 6.4 --- ---
SB-4-6' 6 5.9 <10 <2
SB-4-8' 8 23.3 --- ---
SB-4-10' 10 13.2 --- ---
SB-4-12' 12 3.6 --- ---
SB-4-14' 14 3.0 <10 6.4
SB-4-16' 16 26.5 --- ---
SB-5-2' 2 26.2 --- ---
SB-5-4' 4 57.9 --- ---
SB-5-6' 6 69.8 <20 <4
SB-5-8' 8 52.5 --- ---
SB-5-10' 10 46.1 --- ---
SB-5-12' 12 37.4 --- ---
SB-5-14' 14 31.5 <20 22.0
SB-5-16' 16 21.1 --- ---
3.0 SOIL CLEANUP PLAN
Although there was an RAL exceedance for TPH-GRO in the soil, the laboratory analytical report
indicated that no chemicals of concern exceeded the MACs.
4.0 CONCLUSIONS
• On October 5, 2023, five soil borings (SB-1 through SB-5) were advanced to total depths of 20
feet BGS, each. Each boring was screened at 2-foot intervals using a PID and the 2 to 3 soil
samples from each boring with the highest PID values were submitted for onsite analysis of TPH-
GRO and TPH-DRO. The highest UVF value from each boring was submitted for laboratory
analysis by Method 8260D.
• A concentration of GRO that exceeded the RAL were reported in soil samples SB-1-12’.
• Based on this information, the risk classification for the site should remain intermediate risk.
Although there was an RAL exceedance for TPH-GRO in the soil, the petroleum contamination
present at the site appears to be more prevalent in ground water. A comprehensive sampling

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: November 2, 2023 Little’s Super Market
Project Manager: Joanna Alley, P.E. GRI Project No. 3043
3
event including natural attenuation parameters should be conducted at the site. Following the
sampling event, GRI recommends conducting a pilot test using injections to determine if full
scale application of injectables is a feasible remedial strategy. The next sampling event is
tentatively scheduled for December 2023.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of Shell Brothers Distributors, Inc. for specific
application to the referenced site in Alexander County, North Carolina. The assessment was conducted
based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards
of environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise
locations sampled and at the time the samples were collected. In addition, the data obtained from
samples would be interpreted as being meaningful with respect to parameters indicated in the
laboratory report. No additional information can logically be inferred from these data.

FIGURES
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SITE
3797177866
3787977564
3797175371
3797069921
3797073415
3787978905
3797179070
3797067468
3797067109
3797172403
3797176054
3787968618
37971628493797161967
3797271069
3797270291
3797078578
3787965872
3797078209
3797072659
3797088281
3797078233
3797166641
3797074154
3797077325
3797170121
NC 90 HWY
US 64 HWY
BARNES LN
LENTZ RD
MOOSE DR
LEE RD
GWALTNEY RD
ROMMIE LN
STONY POINT SCHOOL RD
BENNETT RD
PRICE CT
WALTER ST
MILL HILL CT
SHUFORD RD RURITAN PARK RD
GABRIEL LN
CIRCLE LOOP
BIG HOUSE LN
ALEXANDER RD
HAGER CHURCH LOOP
SPRINGFIELD DR
WSW-9
WSW-8
WSW-7
WSW-5
WSW-17
WSW-28
WSW-15
WSW-38
WSW-36 WSW-34
WSW-32
WSW-31
WSW-24WSW-23
WSW-22
WSW-20
WSW-18
WSW-14
WSW-12
WSW-10
WSW-19
WSW-16
WSW-32A

PREPARED BY:GEOLOGICAL RESOURCES, INC.AUGUST 8, 2013UPDATED: NOVEMBER 25, 2013
³
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
446 315
500-FOOT RADIUS
LEGEND
"J Water Supply Well
Streets_2000ft
ncrivers
hydromaj_poly
Adjacent Properties and Well Owners
nc_alexander_parcels_poly
FIGURE 3: SITE VICINITY MAP
LITTLE'S SUPER MARKET
8200 NC HWY 90STONY POINT, ALEXANDER COUNTY
NORTH CAROLINA
INCIDENT NO. 27368
GRI PROJECT NO. 3043

TABLES
UST ID Number 1-3 Facility ID Number
Owner or Operator?
Owner
UST ID Number 4 Facility ID Number
Owner or Operator?
Owner
UST ID Number 5-9 Facility ID Number
Owner or Operator?
Owner
Name of Owner or Operator Dates of Ownership / Operation
TABLE 1
UST OWNER/OPERATOR INFORMATION
LITTLE'S SUPER MARKET (INCIDENT NO. 27368)
0-001931
Address Telephone Number
Shell Brothers Distributors, Inc.05/08/1984 - 12/03/2002
Address Telephone Number
1024 Browning Road, Greensboro, NC 27410 336-339-1394
0-001931
Name of Owner or Operator Dates of Ownership / Operation
Shell Brothers Distributors, Inc.01/01/1984 - 12/03/2002
Shell Brothers Distributors, Inc.01/01/1984 - 01/24/2010
Address Telephone Number
1024 Browning Road, Greensboro, NC 27410 336-339-1394
1024 Browning Road, Greensboro, NC 27410 336-339-1394
0-001931
Name of Owner or Operator Dates of Ownership / Operation
Page 1 of 1
Date: 01/30/18
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Unknown 6,000 5/8/1984 Single Wall Steel 8' x 16"Other Removed
(12/03/2002)Unknown
2 Gasoline Unknown 6,000 5/8/1984 Single Wall Steel 8' x 16"Other Removed
(12/03/2002)Unknown
3 Gasoline Unknown 6,000 5/8/1984 Single Wall Steel 8' x 16"Other Removed
(12/03/2002)Unknown
4 Kerosene Unknown 1,000 5/9/1981 Single Wall Steel 64" x 6'Other Removed
(12/03/2002)Unknown
5 Gasoline Unknown 1,200 5/14/1961 Single Wall Steel 4' x 12'Single Wall
Steel
Removed
(01/24 2010)Unknown
6 Gasoline Unknown 1,200 5/14/1961 Single Wall Steel 4' x 12'Single Wall
Steel
Removed
(01/24 2010)Unknown
7 Diesel Unknown 1,000 5/14/1961 Single Wall Steel 64" x 6'Single Wall
Steel
Removed
(01/24 2010)Unknown
8 Unknown Unknown 750 5/14/1961 Single Wall Steel 4' x 8'Single Wall
Steel
Removed
(01/24 2010)Unknown
9 Unknown Unknown 750 Unknown Single Wall Steel 4' x 8'Unknown Removed
(01/24 2010)Unknown
Tank
Dimensions
(diameter x length)
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
LITTLE'S SUPER MARKET (INCIDENT NO. 27368)
Facility ID #: 0-001931
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Facility ID # : 0-001931
Well ID.Parcel ID No.Lot Number (Old
Parcel ID)Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable, etc.)
Municipal
Water
Connected?
Approximate
distance from
source area of
release (ft.)
Comments
WSW-5 Irrigation Yes 290' SE Would like to use well for drinking water.
WSW-5A Abandoned Yes 290' SE Reported by Mr. Price that the well was
abandoned. Located next to WSW-5.
WSW-7 0000464 0025 10 Price Court
Stony Point, NC 28678 Not In Use Yes 210' SE Well is underneath mud room of residence;
no pump in well.
WSW-8 0000351 H-9D 0027 Erik Justen & Michael Morrison 434 Bethlehem Road, Statesville, NC
28677
8170 Hwy 90 East
Stony Point, NC 28678 Irrigation Yes 140' NW
WSW-9 0000111 H-9D 0029 Jacob & Catie Matlock 8137 Hwy 90 East
Stony Point, NC 28678
8138 Hwy 90 East
Stony Point, NC 28678 Not In Use Yes 340' NW
WSW-10 0000303 H-9D 0061 Toni Cagle 210 Halyburton Rd,
Stony Point, NC 28678
8117 Hwy 90 East
Stony Point, NC 28678 Unknown Yes 440' NNW VACANT
WSW-11 0000059 H-9D 0024 Velma Patterson 88 Bennett 89, 105 Bennett Road
Stony Point, NC 28678 Unknown Yes 450' W (Center of
property)
Well not located on property during survey
update.
WSW-12 0000061 H-9D 0019 Cameron Morris 105 Bennett Road
Stony Point, NC 28678
106 Bennett Road
Stony Point, NC 28678 Unknown Yes 570' W
WSW-13 0000443 H-9D 0023 Sherry L. Morrison & Melissa
A. Brasells
236 Bennett Road
Stony Point, NC 28678
236 Bennett Road
Stony Point, NC 28678 Unknown Yes 1,198' W (Center
of property)
Well not located on property during survey
update.
WSW-14 0000542 H-9C 0003 Juanita Mallard 24 Mallard Lane
Hiddenite, NC 28636
243 Bennett Road
Stony Point, NC 28678 Unknown Yes 1,295' W Water meter not located in resurvey.
WSW-15 0000476 H-9D 0012 Lavonjula Chapman 160 Sugar Hill Lane,
Hiddenite, NC 28636
9 Walter Street
Stony Point, NC 28678 Potable No ~1,500 WSW
WSW-16 0000223 H-9 0006 Gary G. Gwaltney 174 Gwaltney Road
Stony Point, NC 28678
174 Gwaltney Road
Stony Point, NC 28678 Potable No 570' SSW 176 Gwaltney Road also uses this well.
WSW-17 0000076 H-9D 0010 V&J Enterprises, LLC 75 Liberty Estates Lane,
taylorsville, NC 28681
7954 Hwy 90 East
Stony Point, NC 28678
Potable (per
previous survey)No 1,346' NW
Water meter not located in resurvey. Well
not located; left water use survey, not
returned. Previously KA 7930 Hwy 90 E.
WSW-18 137718 H-9 0005H Jimmy R. & Dora W. Gwaltney 177 Gwaltney Road
Stony Point, NC 28678
177 Gwaltney Road
Stony Point, NC 28678 Potable No 960' SSW
WSW-19 0000108 H-9D 0028 Ronald F. Chapman & Others 128 Little John Road
Statesville, NC 28625
8154 Hwy 90 East
Stony Point, NC 28678 Potable No 255' NW
WSW-20 0000197 H-9D 0064 Parker D. & Morgan H. Downs 45 Rommie Lane
Stony Point, NC 28678
45 Rommie Lane
Stony Point, NC 28678 Not in Use Yes 570' E
WSW-21 0000402 H-9C 0007 Lawrence I. Boyer P.O. Box 258
Stony Point, NC 28678
8312 Hwy 90 East
Stony Point, NC 28678 Unknown Yes 500' SE Well not located on property during survey
update.
WSW-22 0000332 H-9D 0068 Allen Russell & Janet Cull 116 Rommie Lane
Stony Point, NC 28678
116 Rommie Lane
Stony Point, NC 28678 Irrigation Yes 1,100' E
WSW-23 0000452 H-9D 0069 Rea A. Decoteau 84 Rommie Lane
Stony Point, NC 28678
84 Rommie Lane
Stony Point, NC 28678 Potable No 950' E Water meter not located in resurvey.
TABLE 3
RECEPTOR INFORMATION
LITTLE'S SUPER MARKET (INCIDENT NO. 27368)
Date: 10/10/23
0021725 H-9D 0025B 31 Price Court
Stony Point, NC 28678Larry N. Price P.O. Box 629
Stony Point, NC 28678
Page 1 of 2
Facility ID # : 0-001931
Well ID.Parcel ID No.Lot Number (Old
Parcel ID)Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable, etc.)
Municipal
Water
Connected?
Approximate
distance from
source area of
release (ft.)
Comments
TABLE 3
RECEPTOR INFORMATION
LITTLE'S SUPER MARKET (INCIDENT NO. 27368)
Date: 10/10/23
0021725 H-9D 0025B 31 Price Court
Stony Point, NC 28678Larry N. Price P.O. Box 629
Stony Point, NC 28678
WSW-24 0000251 H-9D 0071 Lisa A. Reape 104 Barnes Lane
Stony Point, NC 28678
105 Barnes Lane
Stony Point, NC 28678 Irrigation Yes 1,150' E
WSW-25 0000366 H-9D 0097 William A. St. Clair 116 Barnes Lane
Stony Point, NC 28678
116 Barnes Lane
Stony Point, NC 28678 Unknown Yes 1,232' E Well not located on property during survey
update.
WSW-26 0000140 H-9D 0095 Desiree Brown 157 Barnes Lane
Stony Point, NC 28678
158 Barnes Lane
Stony Point, NC 28678 Unknown Yes 1,403' E Well not located on property during survey
update.
WSW-28 0000063 H-9C 0008 Alisha C. Elliot & Carl W, Custer 4312 Princeton Drive,
Little River, SC 29566
8350 Hwy 90 East
Stony Point, NC 28678 Not In Use Yes 800' SE
WSW-29 0000315 H-9C 0016 Jimmy L. & James L. Fox 64 Hager Church Loop
Stony Point, NC 28678
72 Hager Church Loop
Stony Point, NC 28678 Destroyed No 1,289' SE
88 and 108 Hagar Church Road also use
this well. Could be the same well previously
identified as WSW-38. Currently the
property is a vacant lot.
WSW-30 0000608 H-9C 0271 Cooper Orduno Realty, LLC 11 Ruritan Park Road
Stony Point, NC 28678
11 Ruritan Park Road
Stony Point, NC 28678 Unknown Yes 1,435' SE
Address on previous table was 11 Stony
Point School Road. Well not located on
property during survey update.
WSW-31 0000498 H-9D 0034 Wesley M. & Melinda P.
Hammer
257 Earl Isenhour Lane
Taylorsville NC 28678
8072 Hwy 90 East
Stony Point, NC 28678 Irrigation Yes 650 ' NW Two bored wells, not in use, are also
located on this property.
WSW-32 35 Circle Loop
Stony Point, NC 28678
35 Circle Loop
Stony Point, NC 28678 Not In Use Yes 1,110' N
WSW-32A 35 Circle Loop
Stony Point, NC 28678
35 Circle Loop
Stony Point, NC 28678 Not In Use Yes 1,020' N Former community well that is no longer in
use and is reportedly capped
WSW-33 0000182 H-9D 0046 Mark A. & Ashley N. Riley 65 Circle Loop
Stony Point, NC 28678
65 Circle Loop
Stony Point, NC 28678 Unknown Yes 1,208' NW Well not located on property during survey
update.
WSW-34 0000249 H-9D 0036 Tyler Williams 818 2nd Street Place Northeast
Unit 76, Hickory, NC 28601
8016 Hwy 90 East
Stony Point, NC 28678 Not In Use Yes 940' NW
WSW-35 0000595 H-9D 0037 Clifford & Belinda Hartsoe 7992 Hwy 90 East
Stony Point, NC 28678
7992 Hwy 90 East
Stony Point, NC 28678 Unknown Yes 1,004' NW Well not located on property during survey
update.
WSW-36 0000610 H-9D 0011 Bryan W. White 7984 Hwy 90 East
Stony Point, NC 28678
7984 Hwy 90 East
Stony Point, NC 28678 Unknown Yes 1,170' NW
WSW-38 0000446 H-9C 0017 Edward L Goodin 118 Heritage Circle
Taylorsville, NC 28681
88 Hager Church Loop
Stony Point, NC 28678 Potable No 1,370' SSW A community well that reportedly also
serves 108, 120 & 128 Hager Church Rd
Notes:
• Water supply wells are keyed to Figure 3.
• Ft. BGS : Feet below ground surface
• Municipal water connection status confirmed by Energy United Water Corporation in fax to GRI personnel on February 5, 2014.
0000285 H-9D 0044 Samantha A. Gray
Page 2 of 2
Date: 10/10/23 Facility ID #: 0-001931
3797170121 (site)The Redeemer's House, Inc.8200 NC Hwy 90 East, Stony Point, NC 28678
3797078233 Erik Justen & Michael Morrison 434 Bethlehem Road, Statesville, NC 28677
3797172403 Jeffrey A. & Brenda Warren P.O. Box 261, Stony Point, NC 28678
3797177866 Gregory S. & Timothy F. Rufty 675 York Road, Stony Point, NC 28678
3797175371 Roger V. & Patricia Payne 5559 Cheatham Ford Road, Hiddenite, NC 28636
3797069921 Larry Sam Cha & Chue Lee 8212 NC Hwy 90 E, Stony Point, NC 28678
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
LITTLE'S SUPER MARKET (INCIDENT NO. 27368)
Pin Number Property Owner Name Address
Page 1 of 1
Date: 10/10/23 Facility ID #: 0-001931
Analytical Method →PID
50 100
SB-1-2'2 7.0 ------
SB-1-4'4 26.5 ------
SB-1-6'6 29.4 ------
SB-1-8'8 56.3 <10 2.6
SB-1-10'10 78.1 ------
SB-1-12'12 175.3 283.6 18.0
SB-1-14'14 163.5 ------
SB-1-16'16 170.2 ------
SB-1-18'18 12.9 ------
SB-1-20'20 22.1 ------
SB-1-22'22 17.9 ------
SB-1-24'24 2,356 <10 3.2
SB-1-25'25 2,836 ------
SB-2-2'2 11.5 ------
SB-2-4'4 86.5 ------
SB-2-6'6 35.5 <20 <4
SB-2-8'8 16.8 ------
SB-2-10'10 17.9 ------
SB-2-12'12 11.4 ------
SB-2-14'14 17.7 ------
SB-2-16'16 9.4 <20 <4
SB-3-2'2 4.6 ------
SB-3-4'4 4.3 ------
SB-3-6'6 3.1 <10 <2
SB-3-8'8 2.1 ------
SB-3-10'10 3.9 ------
SB-3-12'12 3.6 ------
SB-3-14'14 1.2 ------
SB-3-16'16 1.7 <10 3.8
Sa
m
p
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I
D
Sa
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e

D
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(f
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-
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(
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-
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Or
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i
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s

(
T
P
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-
D
R
O
)
EPA Methods 8105D GRO
& 8015B DRO
PI
D

R
e
a
d
i
n
g
s
RALs (mg/kg)
TABLE 5
SOIL SAMPLE FIELD SCREENING RESULTS
LITTLE'S SUPER MARKET (INCIDENT NO. 27368)
Date: 10/10/23 Facility ID #: 0-001931
Analytical Method →PID
50 100
Sa
m
p
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e

I
D
Sa
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D
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(f
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-
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-
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Or
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(
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-
D
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)
EPA Methods 8105D GRO
& 8015B DRO
PI
D

R
e
a
d
i
n
g
s
RALs (mg/kg)
TABLE 5
SOIL SAMPLE FIELD SCREENING RESULTS
LITTLE'S SUPER MARKET (INCIDENT NO. 27368)
SB-4-2'2 9.7 ------
SB-4-4'4 6.4 ------
SB-4-6'6 5.9 <10 <2
SB-4-8'8 23.3 ------
SB-4-10'10 13.2 ------
SB-4-12'12 3.6 ------
SB-4-14'14 3.0 <10 6.4
SB-4-16'16 26.5 ------
SB-5-2'2 26.2 ------
SB-5-4'4 57.9 ------
SB-5-6'6 69.8 <20 <4
SB-5-8'8 52.5 ------
SB-5-10'10 46.1 ------
SB-5-12'12 37.4 ------
SB-5-14'14 31.5 <20 22.0
SB-5-16'16 21.1 ------
Notes:
• Results reported in mg/kg (milligrams per kilogram).
• ft-BGS: feet below ground surface.
• MSCCs: Maximum Soil Contaminant Concentration Levels.
• <: Less than the reporting limit specified in the laboratory report.
• J: Estimated value.
• Concentrations in bold face type exceed the soil-to-water
MSCCs. Concentrations in italics exceed the residential MSCCs.
• For other detectable contaminant concentrations below the
MSCCs, please refer to the laboratory analytical report.
• Samples that received contaminant specific analysis are labeled red.
Date: 10/12/23 Facility ID #: 0-001931
→
NE NE 0.0072 5.4 8 6 0.085 0.2
NE NE 12 1,250 60.3 3,120 156 5.5
50 100 NE NE NE NE NE NE
SB-1-12'10/05/23 12 283.6 18.0 <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001
SB-2-16'10/05/23 16 <20 <4 <0.0008 <0.0009 <0.0008 <0.0007 <0.0009 <0.001
SB-3-16'10/05/23 16 <10 3.8 <0.0007 <0.0008 0.0010 J 0.008 J <0.0008 <0.001
SB-4-14'10/05/23 14 <10 6.4 <0.0007 <0.0008 <0.0007 <0.0006 <0.0008 <0.001
SB-5-14'10/05/23 14 <20 22.0 <0.0008 0.001 J <0.0008 <0.0007 <0.0008 <0.001
Notes:
• Results reported in mg/kg (milligrams per kilogram).
• ft-BGS: feet below ground surface.
• MSCCs: Maximum Soil Contaminant Concentration Levels.
• <: Less than the reporting limit specified in the laboratory report.
• J: Estimated value.
• Concentrations in bold face type exceed the soil-to-water
MSCCs. Concentrations in italics exceed the residential MSCCs.
• For other detectable contaminant concentrations below the
MSCCs, please refer to the laboratory analytical report.
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
LITTLE'S SUPER MARKET (INCIDENT NO. 27368)
TABLE 6
8260D
Soil-to-Water MCCs (mg/kg)
Na
p
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t
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a
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e
n
e
MT
B
E
Xy
l
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n
e
s
Analytical Method EPA Methods 8105D GRO
& 8015B DRO
Residential SCLs
Be
n
z
e
n
e
RALs (mg/kg)
To
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Et
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APPENDICES

APPENDIX A
State Correspondence
Site Name City / County /Alexander Incident #27368
Resp Pty Name / Contact Incident Mgr Region MOR
(Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #79
Consultant / Project Mgr Joanna R Alley
Telephone / Fax Number Task Authorization Number:80 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:H-307-D RRA Date:
Proposal# / Scope Dates % Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
Task #Lab /
SubCode RO

A
u
t
h
Proposed
Rate/Price
(Consultant)CO

A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
3.101 200 /feet Y $12.50 Y $2,500.00 $2,500.00 /
3.111 200 /feet Y $20.00 Y $4,000.00 $4,000.00 /
3.310 1 /event Y $625.00 Y $625.00 $625.00 /
3.397 1 /Mobe Y $100.00 Y $100.00 $100.00 /
3.398 1 /Mobe Y $350.00 Y $350.00 $350.00 /
4.080 24 /sample pt.Y $45.00 Y $1,080.00 $1,080.00 /
4.090 #409 8 /samples Y $84.00 Y $672.00 $672.00 /
4.091 1 /shipment Y $60.00 Y $60.00 $60.00 /
6.081 1 /site Y $670.00 Y $670.00 $670.00 /
12.050 2 /trips Y $250.00 Y $500.00 $500.00 /
12.055 2 /trips Y $50.00 y $100.00 $100.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed
TOTAL:$10,657.00 $10,657.00 TOTAL:
Total Standard Costs (Not Third Party)$10,657.00 $10,657.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:8/15/23 by:(PM)(Reserved for RO)
RO Review:8/16/23 by:(IM)Joint UST Preapproval Confirmed By:
CO Review:8/21/23 by:(STF)RP or Designee Receipt Confirmation By:
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
DWM/UST ePATA 4/1/2022
Stony Point
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
Little's Super Market
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATArequest
as a "Change Order" in the provided space above priorto conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have beenwithin12monthsofthecompletiondateoftheFIRSTcompletedtasktoremainwithintheStatuteofLimitations.All ePATAs submitted within a claim are closed withthatandmaynot be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimed
below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
RCM
LP
(Initials)
JRA
Proposed
Units / Type
(Consultant)
Ryan Mills
ActiveYES
23-525 September 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
100.00%
[e-mail]
Shell Brothers Distributers Gail Williams
Geological Resources, Inc.
Dept of Environmental Quality -Division of Waste Management
8/22/2023
8/22/23

APPENDIX B
Subsurface Logs
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Little's Super Market
3043
10/5/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Direct Push
4548-A
SB-1
3.25"
25
Abandoned with grout
0 0.5 Asphalt
0.5 3 Silty Clay and gravel Brown Dry None
3 25 Silty Clay Orange-Red Dry None

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Little's Super Market
3043
10/5/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Direct Push
4548-A
SB-2
3.25"
16
Abandoned with grout
0 0.5 Asphalt
0.5 3 Silty Clay Tan Dry None
3 16 Silty Clay Orange Moist None

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Little's Super Market
3043
10/5/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Direct Push
4548-A
SB-3
3.25"
16
Abandoned with grout
0 0.5 Asphalt
0.5 3 Silty Clay Tan Dry None
3 16 Silty Clay Orange None

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Little's Super Market
3043
10/5/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Direct Push
4548-A
SB-4
3.25"
16
Abandoned with grout
0 0.5 Asphalt
0.5 6 Silty Clay Tan Dry None
6 16 Silty Clay Orange Moist None

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Photo 1: Preclearing Photo 2: Completion
Little's Super Market
3043
10/5/23
Xavier T. Farmer
Geological Resources, Inc.
Matt Steele
Direct Push
4548-A
SB-5
3.25"
16
Abandoned with grout
0 0.5 Asphalt
0.5 7 Silty Clay Tan Dry None
7 16 Silty Clay Orange Moist None

APPENDIX C
UVF Analytical Report

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
UVF Trilogy Analytical Report

Samples Collected: October 5, 2023
Samples Analyzed: October 5, 2023
Site Name: Little’s Super Market
Site Address: 8200 NC-90 East, Stony Point, NC
GRI Project Number: 3043

October 6, 2023

Xavier T. Farmer, G.I.T.
Operator

Technical Procedures
Calibration
The UFV Trilogy has standard calibrations stored for the following analysis:
 GRO
 DRO
 Total PAH
 Target PAH
 Heavy PAH
Prior to use, calibration standards are used to perform a 5-point verification on the factory stored
calibrations for GRO and DRO. The calibration standards used are as follows:
GRO
 0.5 ppm
 1 ppm
 3 ppm
 5 ppm
 10 ppm
DRO
 0.1 ppm
 0.5 ppm
 1 ppm
 3 ppm
 5 ppm
Operation
Sample Extraction
 5mg of soil are weighed into a clean extraction jar
 Methanol is added to the extraction jar to create a 2x or 4x dilution
o 2x Dilution: 10 mL of methanol
o 4x Dilution: 20 mL of methanol
 The extraction jar is shaken for several minutes to thoroughly mix the soil with solvent
(methanol)
 The mixture is allowed to settle for several minutes
 A clean syringe is used to draw liquid from the extraction jar
 A clean filter is attached to the end of the syringe and the liquid dispensed through the filter
into a clean test tube
 This liquid is referred to as the extraction
Dilution Preparation
 An adjustable micropipette is used to precisely measure out the amount of extract needed for
the dilution
 The measured out amount of the extract is added to a clean test tube and methanol is added
dilute the extract. Examples of dilutions are shown below:

Extract Amount
500 μL
200 μL
100 μL
50 μL
25 μL

Add Solvent to the
5 mL line
5 mL line
5 mL line
5 mL line
5 mL line
2x Extract
Dilution Factor
20x
50x
100x
200x
400x
4x Extract
Dilution Factor
40x
100x
200x
400x
800x

Technical Procedures
Sample Analyzation
 The dilution is shaken to thoroughly mix, then poured into a clean glass cuvette
 The desired module is inserted into the UVF Trilogy and the corresponding factory calibration is
selected
 “Measure Fluorescence” is pressed on the touchscreen and the reading is recorded
 The reading should be between the concentrations of the calibration standards (GRO: 0.5-10
ppm; DRO 0.1-5 ppm)
o Reading below the calibration standard range are recorded as below the detection limit
 Detection Limit = (lower range of calibration standards range) x dilution factor
(i.e. a GRO sample with a 100x dilution factor has a detection limit of 50 ppm)
o Readings above the calibration standard range should be further diluted and reanalyzed
o Negative readings are an indication of quenching (see below)
 The reading is multiplied by the dilution factor to calculate the final concentration
 Check suspected contaminated samples for quenching by running additional dilutions
o According to the siteLAB Quick Reference Guide:
“Quenching” can occur when the detector is swamped by too many hydrocarbons or
organic interferences, producing low or negative concentrations. Test the sample at
multiple dilutions to confirm results are linear and accurate.”
QA/QC
Method Blank
 A method blank of methanol will be analyzed following calibration and following the last sample
analyzed each day
Duplicates
 One duplicate will be analyzed for every 20 samples
 The duplicate will be prepared from the extract of the sample and diluted to the same factor as
the sample analyzed
Project Name:Date Collected:
Project Number:Date Analysed:
Project Manager:Operator:
Sample ID Matrix Dilution
Factor x
GRO
Output
(ppm)
=GRO Value
(mg/Kg)
Dilution
Factor x
DRO
Output
(ppm)
=DRO Value
(mg/Kg)
SB-1-8'Soil 20 <0.5 <10 20 0.13 2.6
SB-1-12'Soil 40 7.09 283.6 20 0.9 18
SB-1-24'Soil 20 <0.5 <10 20 0.16 3.2
SB-2-6'Soil 40 <0.5 <20 40 <0.1 <4
SB-2-16'Soil 40 <0.5 <20 40 <0.1 <4
SB-3-6'Soil 20 <0.5 <10 20 <0.1 <2
SB-3-16'Soil 20 <0.5 <10 20 0.19 3.8
SB-4-6'Soil 20 <0.5 <10 20 <0.1 <2
SB-4-14'Soil 20 <0.5 <10 20 0.32 6.4
SB-5-6'Soil 40 <0.5 <20 40 <0.1 <4
SB-5-14'Soil 40 <0.5 <20 40 0.55 22
DUP-A Soil 40 <0.5 <20 40 0.55 22
UVF Analytical Report
siteLAB UVF Trilogy
10/5/2023
10/5/2023
Xavier Farmer
Little's Super Market
3043
Joanna Alley
Report Date:
10/6/2023
Page:
1 of 1
Page:
1 of 1

APPENDIX D
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/10/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-278-0021 Client Project Description: Littles Super Market
GRI #3043
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/5/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 38
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Page 1 of 1 00016/23-278-0021
Page 2 of 38
Report Number:
Sample Summary Table
Client Project Description:
23-278-0021
Littles Super Market
GRI #3043
Lab No Client Sample ID Matrix Date Collected Date Received
10/05/2023 13:17Solids 96940 SB-1-1-12'10/05/2023 15:18
10/05/2023 13:22Solids 96941 SB-2-16'10/05/2023 15:18
10/05/2023 13:28Solids 96942 SB-3-16'10/05/2023 15:18
10/05/2023 13:33Solids 96943 SB-4-14'10/05/2023 15:18
10/05/2023 13:39Solids 96944 SB-5-14'10/05/2023 15:18
Page 3 of 38
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-278-0021
Report Limit
Project:Littles Super Market
V 96940SB-1-1-12'
J0.006 10/05/2023 20:298260DAcetonemg/Kg - dry 0.002
J0.0008 10/05/2023 20:298260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
18.9 10/06/2023 09:30SW-DRYWT Moisture %
V 96941SB-2-16'
J0.009 10/05/2023 22:188260DAcetonemg/Kg - dry 0.003
30.5 10/06/2023 09:30SW-DRYWT Moisture %
V 96942SB-3-16'
J0.006 10/05/2023 20:568260DAcetonemg/Kg - dry 0.002
J0.0010 10/05/2023 20:568260DEthylbenzenemg/Kg - dry 0.0007
J0.003 10/05/2023 20:568260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.001 10/05/2023 20:568260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.004 10/05/2023 20:568260Do-Xylene mg/Kg - dry 0.0006
J0.004 10/05/2023 20:568260Dm,p-Xylene mg/Kg - dry 0.001
J0.008 10/05/2023 20:568260DXylene (Total)mg/Kg - dry 0.0006
18.5 10/06/2023 09:30SW-DRYWT Moisture %
V 96943SB-4-14'
J0.004 10/05/2023 21:248260DAcetonemg/Kg - dry 0.002
17.8 10/06/2023 09:30SW-DRYWT Moisture %
V 96944SB-5-14'
J0.013 10/05/2023 21:518260DAcetonemg/Kg - dry 0.003
J0.001 10/05/2023 21:518260DToluenemg/Kg - dry 0.0009
23.7 10/06/2023 09:30SW-DRYWT Moisture %
Page 4 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-1-1-12'
96940 Matrix:
10/5/2023 13:17
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.9 %Moisture 1 10/06/23 09:30 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 5 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-1-1-12'
96940 Matrix:
10/5/2023 13:17
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
0.006 J mg/Kg - dry 0.002 0.024Acetone 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/05/23 20:29 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/05/23 20:29 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/05/23 20:29 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/05/23 20:29 V38721TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 10/05/23 20:29 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/05/23 20:29 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/05/23 20:29 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/05/23 20:29 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/05/23 20:29 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/05/23 20:29 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/05/23 20:29 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/05/23 20:29 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/05/23 20:29 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/05/23 20:29 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-1-1-12'
96940 Matrix:
10/5/2023 13:17
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/05/23 20:29 V38721TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/05/23 20:29 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 10/05/23 20:29 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/05/23 20:29 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/05/23 20:29 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/05/23 20:29 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/05/23 20:29 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 10/05/23 20:29 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/05/23 20:29 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/05/23 20:29 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/05/23 20:29 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/05/23 20:29 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-1-1-12'
96940 Matrix:
10/5/2023 13:17
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/05/23 20:29 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/05/23 20:29 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/05/23 20:29 V38721TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/05/23 20:29 V38721TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/05/23 20:29 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 10/05/23 20:29 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/05/23 20:29 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/05/23 20:29 V38721TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/05/23 20:29 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/05/23 20:29 V38721TBL
0.0008 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/05/23 20:29 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/05/23 20:29 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/05/23 20:29 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/05/23 20:29 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-1-1-12'
96940 Matrix:
10/5/2023 13:17
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/05/23 20:29 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/05/23 20:29 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/05/23 20:29 V38721
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%10/05/23 20:291 TBL V38721
Surrogate: Dibromofluoromethane 105 Limits: 84-123%10/05/23 20:291 TBL V38721
Surrogate: Toluene-d8 93.6 Limits: 76-129%10/05/23 20:291 TBL V38721
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-2-16'
96941 Matrix:
10/5/2023 13:22
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
30.5 %Moisture 1 10/06/23 09:30 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-2-16'
96941 Matrix:
10/5/2023 13:22
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
0.009 J mg/Kg - dry 0.003 0.028Acetone 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.028Acrolein 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.028Acrylonitrile 1 10/05/23 22:18 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 10/05/23 22:18 V38721TBL
<0.002 mg/Kg - dry 0.002 0.014Bromomethane 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 10/05/23 22:18 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 10/05/23 22:18 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 10/05/23 22:18 V38721TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 10/05/23 22:18 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.007Chlorobenzene 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorodibromomethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 10/05/23 22:18 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 10/05/23 22:18 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 10/05/23 22:18 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 10/05/23 22:18 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-2-16'
96941 Matrix:
10/5/2023 13:22
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0071,2-Dibromoethane 1 10/05/23 22:18 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 10/05/23 22:18 V38721TBL
<0.0004 mg/Kg - dry 0.0004 0.0071,2-Dichlorobenzene 1 10/05/23 22:18 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,3-Dichlorobenzene 1 10/05/23 22:18 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,4-Dichlorobenzene 1 10/05/23 22:18 V38721TBL
<0.002 mg/Kg - dry 0.002 0.014Dichlorodifluoromethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0071,2-Dichloroethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 10/05/23 22:18 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 10/05/23 22:18 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloropropene 1 10/05/23 22:18 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 10/05/23 22:18 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.071Ethyl Tertiary Butyl Ether (ETBE)1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 10/05/23 22:18 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.014n-Hexane 1 10/05/23 22:18 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0282-Hexanone 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 10/05/23 22:18 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-2-16'
96941 Matrix:
10/5/2023 13:22
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 10/05/23 22:18 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.028Methyl Ethyl Ketone (MEK)1 10/05/23 22:18 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 10/05/23 22:18 V38721TBL
<0.021 mg/Kg - dry 0.021 0.0284-Methyl-2-Pentanone 1 10/05/23 22:18 V38721TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.014Naphthalene 1 10/05/23 22:18 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 10/05/23 22:18 V38721TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 10/05/23 22:18 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 10/05/23 22:18 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.007Toluene 1 10/05/23 22:18 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 10/05/23 22:18 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 10/05/23 22:18 V38721TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 10/05/23 22:18 V38721TBL
<0.003 mg/Kg - dry 0.003 0.014Trichlorofluoromethane 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 10/05/23 22:18 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Acetate 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 10/05/23 22:18 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-2-16'
96941 Matrix:
10/5/2023 13:22
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 10/05/23 22:18 V38721TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 10/05/23 22:18 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 10/05/23 22:18 V38721
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%10/05/23 22:181 TBL V38721
Surrogate: Dibromofluoromethane 102 Limits: 84-123%10/05/23 22:181 TBL V38721
Surrogate: Toluene-d8 93.8 Limits: 76-129%10/05/23 22:181 TBL V38721
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-3-16'
96942 Matrix:
10/5/2023 13:28
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.5 %Moisture 1 10/06/23 09:30 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-3-16'
96942 Matrix:
10/5/2023 13:28
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
0.006 J mg/Kg - dry 0.002 0.024Acetone 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/05/23 20:56 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/05/23 20:56 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/05/23 20:56 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/05/23 20:56 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/05/23 20:56 V38721TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 10/05/23 20:56 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/05/23 20:56 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/05/23 20:56 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/05/23 20:56 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/05/23 20:56 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/05/23 20:56 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/05/23 20:56 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/05/23 20:56 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/05/23 20:56 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/05/23 20:56 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/05/23 20:56 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-3-16'
96942 Matrix:
10/5/2023 13:28
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/05/23 20:56 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/05/23 20:56 V38721TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/05/23 20:56 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/05/23 20:56 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 10/05/23 20:56 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/05/23 20:56 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/05/23 20:56 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/05/23 20:56 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/05/23 20:56 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 10/05/23 20:56 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/05/23 20:56 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/05/23 20:56 V38721TBL
0.0010 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 10/05/23 20:56 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/05/23 20:56 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/05/23 20:56 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/05/23 20:56 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/05/23 20:56 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-3-16'
96942 Matrix:
10/5/2023 13:28
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/05/23 20:56 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/05/23 20:56 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/05/23 20:56 V38721TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 10/05/23 20:56 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/05/23 20:56 V38721TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/05/23 20:56 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/05/23 20:56 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 10/05/23 20:56 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/05/23 20:56 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/05/23 20:56 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/05/23 20:56 V38721TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/05/23 20:56 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/05/23 20:56 V38721TBL
0.003 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/05/23 20:56 V38721TBL
0.001 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/05/23 20:56 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/05/23 20:56 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/05/23 20:56 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-3-16'
96942 Matrix:
10/5/2023 13:28
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
0.004 J mg/Kg - dry 0.0006 0.006o-Xylene 1 10/05/23 20:56 V38721TBL
0.004 J mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/05/23 20:56 V38721TBL
0.008 J mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/05/23 20:56 V38721
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%10/05/23 20:561 TBL V38721
Surrogate: Dibromofluoromethane 104 Limits: 84-123%10/05/23 20:561 TBL V38721
Surrogate: Toluene-d8 94.4 Limits: 76-129%10/05/23 20:561 TBL V38721
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-4-14'
96943 Matrix:
10/5/2023 13:33
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.8 %Moisture 1 10/06/23 09:30 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-4-14'
96943 Matrix:
10/5/2023 13:33
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
0.004 J mg/Kg - dry 0.002 0.024Acetone 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/05/23 21:24 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/05/23 21:24 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/05/23 21:24 V38721TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/05/23 21:24 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/05/23 21:24 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/05/23 21:24 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/05/23 21:24 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/05/23 21:24 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/05/23 21:24 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/05/23 21:24 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-4-14'
96943 Matrix:
10/5/2023 13:33
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/05/23 21:24 V38721TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/05/23 21:24 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/05/23 21:24 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 10/05/23 21:24 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/05/23 21:24 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/05/23 21:24 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/05/23 21:24 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/05/23 21:24 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 10/05/23 21:24 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/05/23 21:24 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/05/23 21:24 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/05/23 21:24 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-4-14'
96943 Matrix:
10/5/2023 13:33
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/05/23 21:24 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/05/23 21:24 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/05/23 21:24 V38721TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/05/23 21:24 V38721TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/05/23 21:24 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 10/05/23 21:24 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/05/23 21:24 V38721TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/05/23 21:24 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/05/23 21:24 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/05/23 21:24 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-4-14'
96943 Matrix:
10/5/2023 13:33
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/05/23 21:24 V38721TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/05/23 21:24 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/05/23 21:24 V38721
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%10/05/23 21:241 TBL V38721
Surrogate: Dibromofluoromethane 103 Limits: 84-123%10/05/23 21:241 TBL V38721
Surrogate: Toluene-d8 93.0 Limits: 76-129%10/05/23 21:241 TBL V38721
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-5-14'
96944 Matrix:
10/5/2023 13:39
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.7 %Moisture 1 10/06/23 09:30 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-5-14'
96944 Matrix:
10/5/2023 13:39
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
0.013 J mg/Kg - dry 0.003 0.026Acetone 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 10/05/23 21:51 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 10/05/23 21:51 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/05/23 21:51 V38721TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 10/05/23 21:51 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 10/05/23 21:51 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/05/23 21:51 V38721TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 10/05/23 21:51 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/05/23 21:51 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 10/05/23 21:51 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/05/23 21:51 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 10/05/23 21:51 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 10/05/23 21:51 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-5-14'
96944 Matrix:
10/5/2023 13:39
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/05/23 21:51 V38721TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/05/23 21:51 V38721TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/05/23 21:51 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 10/05/23 21:51 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/05/23 21:51 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/05/23 21:51 V38721TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 10/05/23 21:51 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 10/05/23 21:51 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 10/05/23 21:51 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 10/05/23 21:51 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/05/23 21:51 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-5-14'
96944 Matrix:
10/5/2023 13:39
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/05/23 21:51 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 10/05/23 21:51 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/05/23 21:51 V38721TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/05/23 21:51 V38721TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/05/23 21:51 V38721TBL
0.001 J mg/Kg - dry 0.0009 0.006Toluene 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 10/05/23 21:51 V38721TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/05/23 21:51 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/05/23 21:51 V38721TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 10/05/23 21:51 V38721TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/05/23 21:51 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/05/23 21:51 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 10/05/23 21:51 V38721TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 10/05/23 21:51 V38721TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 38
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-278-0021
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3043 Received : 10/05/2023
Littles Super Market
Report Date : 10/10/2023
Sample ID :
Lab No :
Sampled:SB-5-14'
96944 Matrix:
10/5/2023 13:39
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V38720 10/05/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 10/05/23 21:51 V38721TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 10/05/23 21:51 V38721TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 10/05/23 21:51 V38721
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%10/05/23 21:511 TBL V38721
Surrogate: Dibromofluoromethane 106 Limits: 84-123%10/05/23 21:511 TBL V38721
Surrogate: Toluene-d8 92.8 Limits: 76-129%10/05/23 21:511 TBL V38721
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 38
Quality Control Data
23-278-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Littles Super Market
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38720
Associated Lab Samples: 96940, 96941, 96942, 96943, 96944
LRB-V38720 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/05/23 20:020.0200.002<0.002mg/KgAcetone
10/05/23 20:020.0200.001<0.001mg/KgAcrolein
10/05/23 20:020.0200.0008<0.0008mg/KgAcrylonitrile
10/05/23 20:020.0050.0006<0.0006mg/KgBenzene
10/05/23 20:020.0050.0005<0.0005mg/KgBromobenzene
10/05/23 20:020.0050.0008<0.0008mg/KgBromochloromethane
10/05/23 20:020.0050.001<0.001mg/KgBromodichloromethane
10/05/23 20:020.0050.001<0.001mg/KgBromoform
10/05/23 20:020.0100.001<0.001mg/KgBromomethane
10/05/23 20:020.0050.0005<0.0005mg/Kgn-Butylbenzene
10/05/23 20:020.0050.0006<0.0006mg/Kgsec-Butyl benzene
10/05/23 20:020.0050.0005<0.0005mg/Kgtert-Butyl benzene
10/05/23 20:020.0050.0006<0.0006mg/KgCarbon Disulfide
10/05/23 20:020.0050.001<0.001mg/KgCarbon Tetrachloride
10/05/23 20:020.0050.0007<0.0007mg/KgChlorobenzene
10/05/23 20:020.0050.0009<0.0009mg/KgChlorodibromomethane
10/05/23 20:020.0100.0009<0.0009mg/KgChloroethane
10/05/23 20:020.0050.001<0.001mg/KgChloroform
10/05/23 20:020.0100.0006<0.0006mg/KgChloromethane
10/05/23 20:020.0050.0005<0.0005mg/Kg2-Chlorotoluene
10/05/23 20:020.0050.0004<0.0004mg/Kg4-Chlorotoluene
10/05/23 20:020.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
10/05/23 20:020.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
10/05/23 20:020.0050.0006<0.0006mg/Kg1,2-Dibromoethane
10/05/23 20:020.0050.0006<0.0006mg/KgDibromomethane
10/05/23 20:020.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
10/05/23 20:020.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 1 of 7Date:10/10/2023 03:40 PM
Page 30 of 38
Quality Control Data
23-278-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Littles Super Market
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38720
Associated Lab Samples: 96940, 96941, 96942, 96943, 96944
LRB-V38720 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/05/23 20:020.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
10/05/23 20:020.0100.001<0.001mg/KgDichlorodifluoromethane
10/05/23 20:020.0050.0008<0.0008mg/Kg1,1-Dichloroethane
10/05/23 20:020.0050.001<0.001mg/Kg1,2-Dichloroethane
10/05/23 20:020.0050.0007<0.0007mg/Kg1,1-Dichloroethene
10/05/23 20:020.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
10/05/23 20:020.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
10/05/23 20:020.0050.0004<0.0004mg/Kg1,2-Dichloropropane
10/05/23 20:020.0050.0006<0.0006mg/Kg1,3-Dichloropropane
10/05/23 20:020.0050.001<0.001mg/Kg2,2-Dichloropropane
10/05/23 20:020.0050.0008<0.0008mg/Kg1,1-Dichloropropene
10/05/23 20:020.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
10/05/23 20:020.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
10/05/23 20:020.0050.0006<0.0006mg/KgEthylbenzene
10/05/23 20:020.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
10/05/23 20:020.0100.0008<0.0008mg/KgHexachlorobutadiene
10/05/23 20:020.0100.0007<0.0007mg/Kgn-Hexane
10/05/23 20:020.0200.0006<0.0006mg/Kg2-Hexanone
10/05/23 20:020.0050.0005<0.0005mg/KgIsopropylbenzene
10/05/23 20:020.0050.001<0.001mg/Kg4-Isopropyl toluene
10/05/23 20:020.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
10/05/23 20:020.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
10/05/23 20:020.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
10/05/23 20:020.0100.001<0.001mg/KgMethylene Chloride
10/05/23 20:020.0100.0010<0.0010mg/KgNaphthalene
10/05/23 20:020.0050.0005<0.0005mg/Kgn-Propylbenzene
10/05/23 20:020.0050.001<0.001mg/KgStyrene
Page 2 of 7Date:10/10/2023 03:40 PM
Page 31 of 38
Quality Control Data
23-278-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Littles Super Market
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38720
Associated Lab Samples: 96940, 96941, 96942, 96943, 96944
LRB-V38720 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/05/23 20:020.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
10/05/23 20:020.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
10/05/23 20:020.0050.0009<0.0009mg/KgTetrachloroethene
10/05/23 20:020.0050.0007<0.0007mg/KgToluene
10/05/23 20:020.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
10/05/23 20:020.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
10/05/23 20:020.0050.001<0.001mg/Kg1,1,1-Trichloroethane
10/05/23 20:020.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
10/05/23 20:020.0050.0009<0.0009mg/KgTrichloroethene
10/05/23 20:020.0100.002<0.002mg/KgTrichlorofluoromethane
10/05/23 20:020.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
10/05/23 20:020.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
10/05/23 20:020.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
10/05/23 20:020.0100.0005<0.0005mg/KgVinyl Acetate
10/05/23 20:020.0100.0005<0.0005mg/KgVinyl Chloride
10/05/23 20:020.0050.0005<0.0005mg/Kgo-Xylene
10/05/23 20:020.0100.001<0.001mg/Kgm,p-Xylene
10/05/23 20:024-Bromofluorobenzene (S)99.4 70-130
10/05/23 20:02Dibromofluoromethane (S)101 84-123
10/05/23 20:02Toluene-d8 (S)94.0 76-129
LCS-V38720 LCSD-V38720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.118 1181220.1220.100mg/KgAcetone 29-198 3.3 20
0.123 1231230.1230.100mg/KgAcrolein 70-130 0.0 20
Page 3 of 7Date:10/10/2023 03:40 PM
Page 32 of 38
Quality Control Data
23-278-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Littles Super Market
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38720
LCS-V38720 LCSD-V38720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.120 1201140.1140.100mg/KgAcrylonitrile 65-134 5.1 20
0.046 92.897.20.0480.050mg/KgBenzene 74-127 4.6 20
0.043 86.487.40.0430.050mg/KgBromobenzene 73-125 1.1 20
0.049 98.295.00.0470.050mg/KgBromochloromethane 72-134 3.3 20
0.050 1011000.0500.050mg/KgBromodichloromethane 75-122 0.9 20
0.048 97.81040.0520.050mg/KgBromoform 66-135 6.3 20
0.055 1111090.0540.050mg/KgBromomethane 20-180 1.8 20
0.042 85.292.40.0460.050mg/Kgn-Butylbenzene 65-135 8.1 20
0.040 81.086.40.0430.050mg/Kgsec-Butyl benzene 66-131 6.4 20
0.041 82.286.60.0430.050mg/Kgtert-Butyl benzene 67-132 5.2 20
0.044 89.095.00.0470.050mg/KgCarbon Disulfide 61-129 6.5 20
0.046 92.097.60.0480.050mg/KgCarbon Tetrachloride 64-143 5.9 20
0.043 87.292.20.0460.050mg/KgChlorobenzene 74-118 5.5 20
0.047 94.097.00.0480.050mg/KgChlorodibromomethane 73-122 3.1 20
0.051 1031090.0540.050mg/KgChloroethane 33-149 5.6 20
0.046 93.897.40.0480.050mg/KgChloroform 73-127 3.7 20
0.048 97.01060.0530.050mg/KgChloromethane 45-143 9.2 20
0.042 84.486.60.0430.050mg/Kg2-Chlorotoluene 67-124 2.5 20
0.042 84.486.60.0430.050mg/Kg4-Chlorotoluene 71-126 2.5 20
0.052 1051040.0520.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.1 20
0.050 10198.00.0490.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.8 20
0.050 1001020.0510.050mg/Kg1,2-Dibromoethane 70-132 1.7 20
0.052 1041050.0520.050mg/KgDibromomethane 74-133 0.3 20
0.043 87.490.60.0450.050mg/Kg1,2-Dichlorobenzene 72-123 3.5 20
0.043 87.289.60.0440.050mg/Kg1,3-Dichlorobenzene 71-120 2.7 20
0.042 85.887.60.0430.050mg/Kg1,4-Dichlorobenzene 71-123 2.0 20
Page 4 of 7Date:10/10/2023 03:40 PM
Page 33 of 38
Quality Control Data
23-278-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Littles Super Market
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38720
LCS-V38720 LCSD-V38720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.040 81.289.80.0440.050mg/KgDichlorodifluoromethane 26-146 10.0 20
0.048 97.095.60.0470.050mg/Kg1,1-Dichloroethane 74-127 1.4 20
0.051 1031040.0520.050mg/Kg1,2-Dichloroethane 68-128 0.7 20
0.044 88.696.80.0480.050mg/Kg1,1-Dichloroethene 67-149 8.8 20
0.049 98.698.20.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 0.4 20
0.048 96.81000.0500.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.4 20
0.049 99.81010.0500.050mg/Kg1,2-Dichloropropane 73-130 0.9 20
0.045 91.895.40.0470.050mg/Kg1,3-Dichloropropane 75-124 3.8 20
0.047 95.298.40.0490.050mg/Kg2,2-Dichloropropane 50-142 3.3 20
0.046 92.896.80.0480.050mg/Kg1,1-Dichloropropene 71-130 4.2 20
0.050 1011020.0510.050mg/Kgcis-1,3-Dichloropropene 71-125 1.3 20
0.054 1091060.0530.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.6 20
0.043 86.693.80.0460.050mg/KgEthylbenzene 74-128 7.9 20
0.103 10398.30.0980.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 4.6 20
0.042 84.692.40.0460.050mg/KgHexachlorobutadiene 64-125 8.8 20
0.044 89.095.20.0470.050mg/Kgn-Hexane 70-130 6.7 20
0.047 94.81010.0500.050mg/Kg2-Hexanone 61-157 6.3 20
0.041 82.885.60.0420.050mg/KgIsopropylbenzene 68-126 3.3 20
0.041 83.087.60.0430.050mg/Kg4-Isopropyl toluene 68-129 5.3 20
0.047 94.695.60.0470.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.0 20
0.051 1031010.0500.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.3 20
0.054 1091020.0500.050mg/Kg4-Methyl-2-Pentanone 57-162 7.2 20
0.047 95.499.40.0490.050mg/KgMethylene Chloride 74-129 4.1 20
0.046 92.695.60.0470.050mg/KgNaphthalene 57-157 3.1 20
0.041 83.286.80.0430.050mg/Kgn-Propylbenzene 67-130 4.2 20
0.047 94.41010.0500.050mg/KgStyrene 77-121 6.5 20
Page 5 of 7Date:10/10/2023 03:40 PM
Page 34 of 38
Quality Control Data
23-278-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Littles Super Market
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V38721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V38720
LCS-V38720 LCSD-V38720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.095.40.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 5.8 20
0.046 92.091.60.0450.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.4 20
0.045 91.095.20.0470.050mg/KgTetrachloroethene 68-130 4.5 20
0.045 91.495.60.0470.050mg/KgToluene 71-129 4.4 20
0.045 91.697.00.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 5.7 20
0.046 92.899.20.0490.050mg/Kg1,2,4-Trichlorobenzene 66-125 6.6 20
0.046 92.297.60.0480.050mg/Kg1,1,1-Trichloroethane 67-131 5.6 20
0.047 95.21000.0500.050mg/Kg1,1,2-Trichloroethane 70-133 5.1 20
0.045 91.895.00.0470.050mg/KgTrichloroethene 75-133 3.4 20
0.046 93.299.00.0490.050mg/KgTrichlorofluoromethane 44-146 6.0 20
0.045 90.089.00.0440.050mg/Kg1,2,3-Trichloropropane 60-137 1.1 20
0.041 83.688.80.0440.050mg/Kg1,2,4-Trimethylbenzene 69-129 6.0 20
0.041 83.488.20.0440.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.5 20
0.049 99.41080.0530.050mg/KgVinyl Acetate 60-140 8.1 20
0.046 93.81010.0500.050mg/KgVinyl Chloride 48-147 7.1 20
0.044 88.896.00.0480.050mg/Kgo-Xylene 74-126 7.7 20
0.088 88.496.40.0960.100mg/Kgm,p-Xylene 75-124 8.6 20
96.896.64-Bromofluorobenzene (S)70-130
103101Dibromofluoromethane (S)84-123
96.299.2Toluene-d8 (S)76-129
Page 6 of 7Date:10/10/2023 03:40 PM
Page 35 of 38
Quality Control Data
23-278-0021Report No:
Project Description:
Client ID:Geological Resources, Inc.
Littles Super Market
Dry Weight Determination
SW-DRYWT
V38727QC Analytical Batch:
Analysis Method:
Analysis Description:
V 96944-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 10/06/23 09:300.823.923.7%Moisture
Page 7 of 7Date:10/10/2023 03:40 PM
Page 36 of 38
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-278-0021
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 2.1C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:10/05/2023 16:28:35
Special precautions or instructions included?
Comments:
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