MO-4892_16588_CA_MRP_20230915

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

September 18, 2023

Mr. Ryan Mills
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Ground Water Monitoring Report
August 2023
Rushco Food Store #5
601 Jake Alexander Boulevard West
Salisbury, Rowan County
North Carolina
Facility ID Number: 00-0-0000018080
Incident Number: 16588
GRI Project Number: 5722

Dear Mr. Mills,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Sam MaKay at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Joey Rusher; Rusher Oil Company, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
August 24, 2023
Rushco Food Store #5
601 Jake Alexander Boulevard West
Salisbury, Rowan County
North Carolina 28144
Facility ID Number: 00-0-0000018080
Incident Number: 16588
GRI Project Number: 5722

September 15, 2023

Samuel L. McKay III, P.G.
Project Manager
Xavier T. Farmer, G.I.T.
Report Writer
Prepared for:
Mr. Joey Rusher
Rusher Oil Company, Inc.
Post Office Box 1483
Salisbury, NC 28145-1483

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 15, 2023 Rushco Food Store #5
Project Manager: Samuel L. McKay III, P.G. GRI Project No. 5722
i
EXECUTIVE SUMMARY
Rushco Food Store #5 is located at 601 Jake Alexander Boulevard West in Salisbury, Rowan County, North
Carolina. The site is currently owned and operated by Clark Stores, LLC as a petroleum retail facility and
convenience store. The ground water assessment was done as a follow up to incident number 16588.
Currently, one compartmentalized 30,000-gallon gasoline UST, subdivided into a 10,000-gallon gasoline
compartment and a 20,000-gallon gasoline compartment is in use at the site. The adjoining properties
are a mixture of multi-family residential, single family residential, and commercial properties. According
to the information determined during receptor survey activities, no water supply wells were identified
within 1,500 feet of the site. Public water is available to the site and surrounding properties within a
1,500-foot radius of the site. The site is not in a Wellhead Protection Area. An unnamed tributary to Grants
Creek lies within 500 feet of the source area.

On August 24, 2023, four monitoring wells, one telescoping well, and one surface water body were
gauged, purged and/or sampled. Free product was not observed at the site. The concentrations of MTBE,
and TBA reported in the ground water samples collected from MW-1, MW-4 and/or TW-1 exceeded the
MACs. An estimated concentration of MTBE was detected in the surface water sample (SW-1) but did not
exceed the MACs. All of the reported contaminant concentrations were below the 10 times 2B surface
water standards and the GCLs.

Based on this information, the incident should be closed with a Notice of Residual Petroleum and No
Further Action.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 15, 2023 Rushco Food Store #5
Project Manager: Samuel L. McKay III, P.G. GRI Project No. 5722
ii
SITE INFORMATION
1. Site Identification
 Rushco Food Store #5 (Facility ID 00-0-0000018080)
 Incident Number 16588 – Intermediate Risk (I55R)
 Location of Source Area: 601 Jake Alexander Boulevard West
Salisbury, NC 28144
Rowan County
35.662775°N, 80.500645°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
Sampson-Bladen Oil Co, Inc.
P.O. Box 469
Clinton, NC 28328
[e-mail]
704-633-3211

UST Operator
Sampson-Bladen Oil Co, Inc.
P.O. Box 469
Clinton, NC 28328
[e-mail]
704-633-3211

Property Owner
Clark Stores, LLC
P.O. Box 469
Clinton, NC 28328
Email Unknown
Phone No. Unknown

Property Occupant
Han-Dee Hugo’s #224
P.O. Box 469
Clinton, NC 28328
Email Unknown
Phone No. Unknown

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Rd.
Charlotte, NC 28217
State Certification No. 377353
and 402
704-529-6364
3. Information about Release
 Release was discovered on October 14, 1996.
 An unknown amount of product was released from the leaking UST System.
 One 30,000-gallon compartmentalized gasoline UST, subdivided into a 10,000-gallon gasoline
compartment and a 20,000-gallon gasoline compartment is in use at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 15, 2023 Rushco Food Store #5
Project Manager: Samuel L. McKay III, P.G. GRI Project No. 5722
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
HERR: HAZMAT Emergency Response and
Remediation, Inc.
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: September 15, 2023 Rushco Food Store #5
Project Manager: Samuel L. McKay III, P.G. GRI Project No. 5722
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................5
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................6
3.0 FREE PRODUCT REMOVAL ........................................................................................................8
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................8
5.0 CONCLUSIONS .........................................................................................................................8
6.0 LIMITATIONS ...........................................................................................................................8
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................9

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Site Vicinity Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Receptor Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Incident Reports
Appendix C: Historical Soil Quality Information
Appendix D: Laboratory Analytical Report

1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the August 2023 ground water sampling event at the Rushco Food Store #5
site; located at 601 Jake Alexander Boulevard West in Salisbury, Rowan County, North Carolina. A
topographic map showing the general site location and the surrounding area is included as Figure 1. These
activities were conducted in accordance with GRI Proposal No. 23-458, which was submitted to the
NCDEQ on July 20, 2023, and was approved as Task Authorization No. 16588-1 on July 25, 2023. State
correspondence has been included as Appendix A.

The site is currently owned and operated by Clark Stores, LLC as a petroleum retail facility and convenience
store. Currently, one compartmentalized 30,000-gallon gasoline UST, subdivided into a 10,000-gallon
gasoline compartment and a 20,000-gallon gasoline compartment is in use at the site. UST
owner/operator information and UST system information are included as Tables 1 and 2, respectively.
The Registered Tank Report is shown below:

The site and surrounding area is a mixture of multi-family residential, single-family residential, and
commercial properties. The site contains one building and is primarily capped with concrete and asphalt.
The overall topography at the site is inclined with a down gradient from south to north. Four Type II
monitoring wells (MW-1 through MW-4), and one telescoping monitoring well (TW-1) were installed at
the site during previous ground water assessment activities. A Site Map showing the locations of the
monitoring wells and the structures on-site is included as Figure 2.

On August 24, 2023, GRI personnel conducted an updated receptor survey at the site. No Water Supply
Wells were found within 1,500 feet of the site. The site is not in a Wellhead Protection Area. An unnamed
tributary to Grants Creek is located approximately 450 feet northeast of the subject site. Receptor
information is included in Table 3. Adjacent property owner information is included in Table 4. A Site
Vicinity Map showing the adjacent properties is included as Figure 3.

No additional releases exist at the site.

One incident (Incident No. 36974) has been reported on an adjacent property. Copies of the NCDEQ
Incident Report are included as Appendix B. A map showing the locations of additional incidents in the
vicinity of the site is shown below:

No CAP has been planned or implemented for the site.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Soil assessment was not conducted during the current scope of work. Historical soil quality information
is included as Appendix C.
36974 Site

On August 24, 2023, four Type II monitoring wells (MW-1 through MW-4), one telescoping well (TW-1),
and one surface water body (SW-1) were gauged, purged and/or sampled in accordance with the NCDEQ
guidelines. Free product was not observed at the site. Depths to ground water in the Type II monitoring
wells ranged from 7.76 feet to 21.05 feet. Ground water elevations in the Type II monitoring wells ranged
from 78.36 feet to 92.89 feet. Ground water flow was generally to the north with a horizontal gradient of
approximately 0.05 feet per foot. The vertical gradient between wells MW-1 and TW-1 was approximately
0.42 feet per foot in the downward direction. Well construction and gauging information is included in
Table 5. A Water Table Surface Map based on the Type II monitoring wells is included as Figure 4. A
summary of the current ground water gauging data is shown below:
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 5 – 20 20 100.00 7.76 --- 92.24
MW-2 10 – 25 25 97.69 19.33 --- 78.36
MW-3 10 – 25 25 99.45 21.05 --- 78.40
MW-4 5 – 20 20 104.93 12.04 --- 92.89
TW-1 40 - 45 45 99.35 21.90 --- 77.45

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B with oxygenates. The concentrations of MTBE, and TBA reported in the ground water
samples collected from MW-1, MW-4 and/or TW-1 exceeded the MACs. An estimated concentration of
MTBE was detected in SW-1 but did not exceed the MAC. All of the reported contaminant concentrations
were below the 10 times 2B surface water standards and the GCLs. A summary of the analytical results
for ground water samples collected on August 24, 2023. is included in Table 6. A Ground Water Quality
Map based on the August 2023 data is included as Figure 5. A complete report of laboratory analyses of
the ground water samples collected from the monitoring wells during the August 2023 sampling event is
included as Appendix D. A summary of the current ground water analytical data is shown below:

Contaminant
of Concern →
Be
n
z
e
n
e

To
l
u
e
n
e

Et
h
y
l
b
e
n
z
e
n
e

Xy
l
e
n
e
s

MT
B
E

Na
p
h
t
h
a
l
e
n
e

Well
ID
MACs (μg/l) 1 600 600 500 20 6
GCL (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 0.795 0.292 J 0.229 J <0.210 534 <0.470
MW-2 <0.180 <0.220 <0.170 <0.210 0.274 J <0.470
MW-3 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-4 <0.180 <0.220 <0.170 <0.210 185 <0.470
TW-1 <0.180 <0.220 <0.170 <0.210 360 <0.470
SW-1 <0.180 <0.220 <0.170 <0.210 0.212 J <0.470

The site is located in the Piedmont Physiographic Province of North Carolina. The seasonal high ground
water table is approximately seven feet BGS.

3.0 FREE PRODUCT REMOVAL
To the knowledge of GRI, no free product has been observed at the site.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
The site is in the active assessment phase. No natural attenuation monitoring plan is in place at the site.
5.0 CONCLUSIONS
• On August 24, 2023, GRI personnel conducted an updated receptor survey at the site. No Water
Supply Wells were found within 1,500 feet of the site. The site is not in a Wellhead Protection
Area. An unnamed tributary to Grants Creek is located approximately 450 feet northeast of the
subject site.
• On August 24, 2023, four Type II monitoring wells, one telescoping well, and one surface water
body were gauged, purged and/or sampled. Free product was not observed in any of the wells at
the site. Ground water flow was generally to the north with a horizontal gradient of
approximately 0.05 feet per foot. The vertical gradient between paired wells MW-1 and TW-1
was approximately 0.418 feet per foot in the downward direction.
• The concentrations of MTBE and TBA reported in the ground water samples collected from MW-
1, MW-4 and/or TW-1 exceeded the MACs. An estimated concentration of MTBE was detected
in the surface water sample, but was below the MAC. All of the reported contaminant
concentrations were below the 10 times 2B surface water standards and the GCLs.
• Based on this information, the incident should be closed with a Notice of Residual Petroleum and
No Further Action.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Rusher Oil Company, Inc. and the NCDEQ for specific
application to the referenced site in Rowan County, North Carolina. The assessment was conducted based
on the scope of work and level of effort desired by the NCDEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described
in more detail in the report text above.)

6 Certification:
I, Samuel L. McKay III, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice engineering and geology in North Carolina. The
certification number of the company or corporation is C-2727/C-127.

FIGURES
SITE LOCATION
Figure 1
Site Location
Rushco Food Store 5
601 Jake Alexander Blvd
Salisbury, North Carolina
Rowan County
Incident No. 16588
GRI Project No. 5722
500 M
2000 FT
Date: 06/27/2021 Location: 35.662775° N -80.500645° W
D
a
d

TABLES
UST ID Number 6, 6B Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 6, 6B Facility ID Number
Owner or Operator?
Owner/OperatorRusher Oil Company 08/17/2004 - 11/10/2021
P.O. Box 1483 Salisbury, NC 28145-1483
0-018080
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
704-633-3211
P.O. Box 469 Clinton, NC 28328 910-862-3197
Telephone Number
TABLE 1
UST OWNER/OPERATOR INFORMATION
RUSHCO FOOD STORE 5 (INCIDENT NO. 18080)
0-018080
Name of Owner or Operator Dates of Ownership / Operation
Sampson-Bladen Oil Company, Inc.11/10/2021 - Present
Address
Page 1 of 1
Date: 08/29/2023
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline,
Gas Mix Unk.6,000 7/29/1971 Single Wall Steel Unk.Single Wall Steel Removed No
2 Gasoline,
Gas Mix Unk.6,000 7/29/1971 Single Wall Steel Unk.Single Wall Steel Removed No
3 Gasoline,
Gas Mix Unk.6,000 7/31/1971 Single Wall Steel Unk.Single Wall Steel Removed No
4 Diesel Unk.3,000 9/23/1983 Single Wall Steel Unk.Single Wall FRP Removed No
5 Kerosene,
Kero Mix Unk.3,000 9/22/1985 Other Unk.Other Removed No
6 Gasoline,
Gas Mix Unk.20,000 4/1/1997 Single Wall FRP Unk.Single Wall FRP Current Yes
6B Gasoline,
Gas Mix Unk.10,000 4/1/1997 Single Wall FRP Unk.Single Wall FRP Current Yes
Notes:
• FRP: Fiberglass reinforced plastic.
TABLE 2
UST SYSTEM INFORMATION
RUSHCO FOOD STORES 5 (INCIDENT NO. 16588)
Facility ID # : 0-018080
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Page 1 of 1
Facility ID # : 0-018080
Well ID.Parcel ID No.Well Owner Mailing Address Well Address Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municpal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Distance
from source
area of
release
(ft.)
Receptor
ID
Latitude/
Longitude of Any
Significant Points
Up or Down-
Gradient
Distance
from
the source
area
of release
(ft.)
n/a n/a Down ~450
Notes:
• Receptors are shown on Figure 3.
• n/a: not applicable.
Unnamed Tributary of Grants Creek Approximately northeast of subject property n/a n/a
No Water Supply Wells found.
Description Location Contact/Phone Number Usage
TABLE 3
RECEPTOR INFORMATION
RUSHCO FOOD STORE 5 (INCIDENT NO. 16588)
Date: 09/12/23
Well Construction Details
(Depth, Screened Interval, Type of Well, ect.)
Page 1 of 1
Date: 08/29/2023 Facility ID # : 0-018080
Parcel Number Owner Name Address
061-233
(Subject Site)Clark Stores, LLC P.O. Box 469,
Clinton, NC 28329
061-1150001 Beth S. Gordon Et Al.1205 Lincolnton Rd,
Salisbury, NC 28147
061-152 Westland Center, LLC 525 W. Jake Alexander Blvd,
Raleigh, NC 28145
061-105 Alligood Tire and Alignment, LLC 600 W. Jake Alexander Blvd,
Raleigh, NC 28145
061-202 John F. Leatherman III 524 W.. Jake Alexander Blvd,
Salisbury, NC 28145
061-234 O, Inc.1006 Mooresville Rd, Mooresville, NC
28145
Note:
• Properties are keyed to Figure 3.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
RUSHCO FOOD STORES 5 (INCIDENT NO. 16588)
Page 1 of 1
Date: 08/29/2023
Well ID Date
Installed
Date Water
Level
Well
Casing
Screened
Interval
Bottom
of Well
Top of
Casing
Depth to
Water from
Free Product
Thickness
Ground
Water Comments
MW-1 07/28/04 08/24/23 5 5 - 20 20 100.00 7.76 ---92.24
MW-2 08/21/04 08/24/23 10 10 - 25 25 97.69 19.33 ---78.36
MW-3 08/21/04 08/24/23 10 10 - 25 25 99.45 21.05 ---78.40
MW-4 08/21/04 08/24/23 5 5 - 20 20 104.93 12.04 ---92.89
TW-1 08/21/04 08/24/23 40 40 - 45 45 99.35 21.90 ---77.45
Notes:
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
RUSHCO FOOD STORE 5 (INCIDENT NO. 16588)
Facility ID # : 0-018080
• ft BGS : feet below ground surface.
• NM : Not measured.
• Elevation relative to mean sea level.
Page 1 of 1
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 10 400 400
510 110 1,300 6,700 15,000 120 NE 3,900 2,150
5,000 260,000 80,000 50,000 20,000 6,000 10,000 28,500 24,100
MW-1 08/24/23 0.795 0.292 J 0.229 J <0.210 534 <0.470 9.12 J 0.523 <0.180
MW-2 08/24/23 <0.180 <0.220 <0.170 <0.210 0.274 J <0.470 <1.60 <0.190 <0.180
MW-3 08/24/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.60 <0.190 <0.180
MW-4 08/24/23 <0.180 <0.220 <0.170 <0.210 185 <0.470 12.2 <0.190 <0.180
TW-1 08/24/23 <0.180 <0.220 <0.170 <0.210 360 <0.470 4.06 J <0.190 <0.180
SW-1 08/24/23 <0.180 <0.220 <0.170 <0.210 0.212 J <0.470 <1.60 <0.190 <0.180
Trip Blank 08/24/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR <0.190 <0.180
Notes:
1,
2
,
4
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
1,
3
,
5
-
T
r
i
m
e
t
h
y
l
b
e
n
z
e
n
e
10 x 2B (μg/l)
TABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RUSHCO FOOD STORE 5 (INCIDENT NO. 16588)
Date: 09/12/23 Facility ID #: 0-018080
Analytical Method
→EPA Method 6200B
MACs (μg/l)
GCL (μg/l)
Na
p
h
t
h
a
l
e
n
e
te
r
t
-
B
u
t
y
l

a
l
c
o
h
o
l
(T
B
A
)
Contaminant of Concern
→
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
MT
B
E
• For other compounds reported which did not exceed the MACs, refer to the laboratory reports.
• Concentrations in italics indicate the GCLs were below the reported concentrations.
• Concentrations in bold face type indicate the MACs were below the reported concentrations.
• J: Estimated value.
• Results reported in µg/l (micrograms per liter)
• MAC: Maximum Allowable Concenration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Standard not established.
• < : Less than the method detection limit specified in the laboratory report.
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

North Carolina Department of Environmental Quality | Division of Waste Management
Mooresville Regional Office | 610 East Center Avenue | Suite 301 | Mooresville, NC 28115 | [phone]

July 17, 2023

Rusher Oil Company
Mr. Joey Rusher
P.O. Box 1482
Salisbury, NC 28144

Re: Notice of Regulatory Requirements
15A NCAC 02L .0110(d) [Intermediate Risk]
Risk-based Assessment and Corrective Action
For Petroleum Underground Storage Tanks

Rushco Food #5
601 W Jake Alexander Blvd.
Rowan County
Incident Number: 16588
Risk Classification: Intermediate
Ranking: I-55-R

Dear Mr. Rusher:

The report received on August 30, 2004, has been reviewed by the UST Section, Division of Waste
Management, Mooresville Regional Office. The risk posed by the discharge or release at the subject site is
classified by the Department of Environmental Quality as intermediate, as stipulated under Title 15A
NCAC 02L .0406. The land use at the site is classified as industrial/commercial. Title 15A NCAC 02L
.0407(a) requires you to notify the Department of any changes that might affect the risk or land use
classifications that have been assigned.
The review indicates that corrective action is necessary to remediate environmental contamination. Title
15A NCAC 02L .0407(d) [Intermediate Risk] requires you to comply with the assessment and cleanup
requirements of Title 15A NCAC 02N .0706, Title15A NCAC 02L .0106(c), Title 15A NCAC 02L .0110,
and Title 15A NCAC 02L .0111. A Groundwater Monitoring Report prepared in accordance with
these requirements and a new Receptor Survey completed by October 17, 2023, would suffice in
moving forward with an NRP if the surface water body can be eliminated as per UST MRO staff.
For additional reference, please refer to the most recent version of the Guidelines for Site Checks, Tank
Closures, and Initial Response and Abatement. Report requirements can be found in the most recent version
of the Comprehensive Appendices for Correction Guidelines. Reports must contain the information
specified in the report template presented in Appendix A of the Guidelines. The report template is attached
for your information.
Failure to comply in the manner and time specified may result in the assessment of civil penalties
and/or the use of other enforcement mechanisms.
Page 2 of 2 Incident Number16588 July 17, 2017

North Carolina Department of Environmental Quality | Division of Waste Management
Mooresville Regional Office | 610 East Center Avenue | Suite 301 | Mooresville, NC 28115 | [phone]

The Department of Environmental Quality requires that all work not determined to be an emergency
response or associated with risk assessment (i.e., the Limited Site Assessment Report, per Title 15A NCAC
02L .0405) must be preapproved if State Trust Fund reimbursement is anticipated. To comply with this
requirement, a completed Preapproval/Claim Authorization Form, encompassing the required remedial
activities, must be received in this office within 14 days of the date of this letter. Upon completion of the
preapproved activities, you should submit your claim promptly. Reimbursement funds are budgeted based
on completed preapprovals, but delays in reimbursement or even denial due to exceeding the statute of
limitations on claiming eligible costs can result where claims are not submitted immediately following work
completion.
Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer,
certified by the State of North Carolina, is required to prepare and certify all reports submitted to the
Department in accordance with 15A NCAC 02L .0103(e) and 02L .0111(e) if required.
If you have any questions regarding trust fund eligibility or reimbursement from the Commercial Leaking
Petroleum Underground Storage Tank Cleanup Fund, please contact the UST Section Trust Fund Branch
at [phone]. If you have any questions regarding the actions that must be taken or the rules mentioned
in this letter, please contact me at [e-mail] or at 704-235-2175.

Sincerely,

Ryan C Mills
Environmental Program Consultant
Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ

cc: Brady Freeman, Iredell County Health Department (Via Email)
Tomie Benton, Geological Resources, Inc. (Via Email) Sam McKay, Geological Resources, Inc. (Via Email)

APPENDIX B
Incident Reports
NCDEQ Incident Report
RP/Company RUSHER OIL COMPANY
RPAddress PO BOX 1483
RPCity SALISBURY
Contact JOEY RUSHER
RPState NC
TELEPHONE [phone]
IncidentNumber 16588 USTNum MO-4892
IncidentName RUSHCO FOOD #5
FacilID 00-0-0000018080
Address 601 W JAKE ALEXANDER BLVD
CityTown SALISBURY State NC
ZipCode 28144-
DateOccurred 10/14/1996
DateReported 12/12/1996
ConfRisk I
CloseOut
COMMENT
Removal of five USTs - gasoline diesel and kerosene. TPH as high as 507 ppm. LSA required. Phase II LSA completed.
Soil < residential and groundwater > 2L. Surface water within 500 feet and groundwater contamination > 10 X 2B.
RptType Rcvd Rvwd Appvd
Incident Mgr RABLongitude-80.500556 Latitude 35.662500
County ROWAN
LSA2 8/30/2004 9/3/2004 9/3/2004
LSA indicates soil < residential, groundwater > 2L and surface water within
500 feet and groundwater contamination > 10 X 2B.
Sunday, August 7, 2022 Page 1 of 1
NCDEQ Incident Report
RP/Company JERRY'S SHELL
RPAddress 600 WEST JAKE ALEXANDER BLVD
RPCity SALISBURY
Contact JERRY ALLIGOOD
RPState NC
TELEPHONE [phone]
IncidentNumber 36974 USTNum MO-8427
IncidentName JERRY'S SHELL
FacilID 00-0-0000031876
Address 600 WEST JAKE ALEXANDER BLVD
CityTown SALISBURY State NC
ZipCode 28144-
DateOccurred 8 /2 /2011
DateReported 9 /29/2011
ConfRisk L
CloseOut 9/18/2012
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr DSGLongitude-80.499987 Latitude 35.662480
County ROWAN
SCH 9/29/2011 9/30/2011
LSA1 9/30/2011 9/30/2011
DR 9/18/2012 9/19/2012
PN 10/1/2012 10/2/2012
Tuesday, September 12, 2023 Page 1 of 1

APPENDIX C
Historical Soil Quality Information

APPENDIX D
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

9/8/2023
Geological Resources, Inc. Sam McKay
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-240-0001 Client Project Description: Rushco #5
GRI #5722
Dear Sam McKay:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/25/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 53
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-240-0001
Page 2 of 53
Report Number:
Sample Summary Table
Client Project Description:
23-240-0001
Rushco #5
GRI #5722
Lab No Client Sample ID Matrix Date Collected Date Received
08/24/2023 10:04Aqueous 93496 MW-1 08/25/2023 15:17
08/24/2023 10:12Aqueous 93497 MW-2 08/25/2023 15:17
08/24/2023 10:22Aqueous 93498 MW-3 08/25/2023 15:17
08/24/2023 10:33Aqueous 93499 MW-4 08/25/2023 15:17
08/24/2023 10:51Aqueous 93500 TW-1 08/25/2023 15:17
08/24/2023 11:05Aqueous 93501 SW-1 08/25/2023 15:17
08/24/2023 09:45Aqueous 93502 TB 08/25/2023 15:17
Page 3 of 53
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-240-0001
Report Limit
Project:Rushco #5
V 93496MW-1
0.795 09/05/2023 16:206200BBenzeneµg/L 0.180
J0.361 09/05/2023 16:206200Bsec-Butyl benzene µg/L 0.200
2.90 09/05/2023 16:206200BDi-Isopropyl Ether (DIPE)µg/L 0.500
J0.229 09/05/2023 16:206200BEthylbenzeneµg/L 0.170
534 09/06/2023 19:546200BMethyl tert-butyl ether (MTBE)µg/L 1.40
J9.12 09/05/2023 16:206200Btert-Butyl Alcohol (TBA)µg/L 1.60
15.4 09/05/2023 16:206200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
J0.292 09/05/2023 16:206200BTolueneµg/L 0.220
0.523 09/05/2023 16:206200B1,2,4-Trimethylbenzene µg/L 0.190
V 93497MW-2
J0.274 09/06/2023 16:296200BMethyl tert-butyl ether (MTBE)µg/L 0.140
V 93499MW-4
185 09/06/2023 20:206200BMethyl tert-butyl ether (MTBE)µg/L 1.40
12.2 09/05/2023 17:386200Btert-Butyl Alcohol (TBA)µg/L 1.60
J0.496 09/05/2023 17:386200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
V 93500TW-1
2.43 09/05/2023 18:036200BDi-Isopropyl Ether (DIPE)µg/L 0.500
360 09/06/2023 20:466200BMethyl tert-butyl ether (MTBE)µg/L 1.40
J4.06 09/05/2023 18:036200Btert-Butyl Alcohol (TBA)µg/L 1.60
J2.57 09/05/2023 18:036200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
V 93501SW-1
J0.212 09/05/2023 18:296200BMethyl tert-butyl ether (MTBE)µg/L 0.140
Page 4 of 53

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Rushco #5 Lab Report Number: 23-240-0001
Date: 9/8/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 3,3-Dimethyl-1-butanol QC Batch No: V37496/V37495
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 5 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-1
93496 Matrix:
8/24/2023 10:04
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/05/23 16:20 6200BMSA
Surrogate: 4-Bromofluorobenzene 95.0 Limits: 70-130%09/05/23 16:201 MSA V37496
Surrogate: Dibromofluoromethane 113 Limits: 70-130%09/05/23 16:201 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%09/05/23 16:201 MSA V37496
Surrogate: Toluene-d8 100 Limits: 70-130%09/05/23 16:201 MSA V37496
Surrogate: 4-Bromofluorobenzene 96.8 Limits: 70-130%09/06/23 19:5410 MSA V37553
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/06/23 19:5410 MSA V37553
Surrogate: 1,2-Dichloroethane - d4 91.0 Limits: 70-130%09/06/23 19:5410 MSA V37553
Surrogate: Toluene-d8 99.6 Limits: 70-130%09/06/23 19:5410 MSA V37553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-1
93496 Matrix:
8/24/2023 10:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/05/23 16:20 V37496MSA
0.795 µg/L 0.180 0.500Benzene 1 09/05/23 16:20 V37496MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/05/23 16:20 V37496MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/05/23 16:20 V37496MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/05/23 16:20 V37496MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/05/23 16:20 V37496MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/05/23 16:20 V37496MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/05/23 16:20 V37496MSA
0.361 J µg/L 0.200 0.500sec-Butyl benzene 1 09/05/23 16:20 V37496MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/05/23 16:20 V37496MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/05/23 16:20 V37496MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/05/23 16:20 V37496MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/05/23 16:20 V37496MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/05/23 16:20 V37496MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/05/23 16:20 V37496MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/05/23 16:20 V37496MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/05/23 16:20 V37496MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/05/23 16:20 V37496MSA
2.90 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/05/23 16:20 V37496MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/05/23 16:20 V37496MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/05/23 16:20 V37496MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/05/23 16:20 V37496MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/05/23 16:20 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-1
93496 Matrix:
8/24/2023 10:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/05/23 16:20 V37496MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/05/23 16:20 V37496MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/05/23 16:20 V37496MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/05/23 16:20 V37496MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/05/23 16:20 V37496MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/05/23 16:20 V37496MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/05/23 16:20 V37496MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/05/23 16:20 V37496MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/05/23 16:20 V37496MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/05/23 16:20 V37496MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/05/23 16:20 V37496MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/05/23 16:20 V37496MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/05/23 16:20 V37496MSA
<42.0 µg/L 42.0 200Ethanol 1 09/05/23 16:20 V37496MSA
0.229 J µg/L 0.170 0.500Ethylbenzene 1 09/05/23 16:20 V37496MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/05/23 16:20 V37496MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/05/23 16:20 V37496MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/05/23 16:20 V37496MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/05/23 16:20 V37496MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/05/23 16:20 V37496MSA
534 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 09/06/23 19:54 V37553MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/05/23 16:20 V37496MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/05/23 16:20 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-1
93496 Matrix:
8/24/2023 10:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/05/23 16:20 V37496MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/05/23 16:20 V37496MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/05/23 16:20 V37496MSA
9.12 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/05/23 16:20 V37496MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/05/23 16:20 V37496MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/05/23 16:20 V37496MSA
15.4 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/05/23 16:20 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/05/23 16:20 V37496MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/05/23 16:20 V37496MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/05/23 16:20 V37496MSA
0.292 J µg/L 0.220 0.500Toluene 1 09/05/23 16:20 V37496MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/05/23 16:20 V37496MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/05/23 16:20 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/05/23 16:20 V37496MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/05/23 16:20 V37496MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/05/23 16:20 V37496MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/05/23 16:20 V37496MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/05/23 16:20 V37496MSA
0.523 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/05/23 16:20 V37496MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/05/23 16:20 V37496MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/05/23 16:20 V37496MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/05/23 16:20 V37496MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/05/23 16:20 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-1
93496 Matrix:
8/24/2023 10:04
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/05/23 16:20 V37496MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/05/23 16:20 V37496
Surrogate: 4-Bromofluorobenzene 95.0 Limits: 70-130%09/05/23 16:201 MSA V37496
Surrogate: Dibromofluoromethane 113 Limits: 70-130%09/05/23 16:201 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 107 Limits: 70-130%09/05/23 16:201 MSA V37496
Surrogate: Toluene-d8 100 Limits: 70-130%09/05/23 16:201 MSA V37496
Surrogate: 4-Bromofluorobenzene 96.8 Limits: 70-130%09/06/23 19:5410 MSA V37553
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/06/23 19:5410 MSA V37553
Surrogate: 1,2-Dichloroethane - d4 91.0 Limits: 70-130%09/06/23 19:5410 MSA V37553
Surrogate: Toluene-d8 99.6 Limits: 70-130%09/06/23 19:5410 MSA V37553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-2
93497 Matrix:
8/24/2023 10:12
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/06/23 16:29 6200BMSA
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%09/06/23 16:291 MSA V37553
Surrogate: Dibromofluoromethane 104 Limits: 70-130%09/06/23 16:291 MSA V37553
Surrogate: 1,2-Dichloroethane - d4 92.2 Limits: 70-130%09/06/23 16:291 MSA V37553
Surrogate: Toluene-d8 100 Limits: 70-130%09/06/23 16:291 MSA V37553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-2
93497 Matrix:
8/24/2023 10:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37551 09/06/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/06/23 16:29 V37553MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/06/23 16:29 V37553MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/06/23 16:29 V37553MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/06/23 16:29 V37553MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/06/23 16:29 V37553MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/06/23 16:29 V37553MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/06/23 16:29 V37553MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/06/23 16:29 V37553MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/06/23 16:29 V37553MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/06/23 16:29 V37553MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/06/23 16:29 V37553MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/06/23 16:29 V37553MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/06/23 16:29 V37553MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/06/23 16:29 V37553MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/06/23 16:29 V37553MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/06/23 16:29 V37553MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/06/23 16:29 V37553MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/06/23 16:29 V37553MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/06/23 16:29 V37553MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/06/23 16:29 V37553MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/06/23 16:29 V37553MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/06/23 16:29 V37553MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/06/23 16:29 V37553MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-2
93497 Matrix:
8/24/2023 10:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37551 09/06/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/06/23 16:29 V37553MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/06/23 16:29 V37553MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/06/23 16:29 V37553MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/06/23 16:29 V37553MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/06/23 16:29 V37553MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/06/23 16:29 V37553MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/06/23 16:29 V37553MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/06/23 16:29 V37553MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/06/23 16:29 V37553MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/06/23 16:29 V37553MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/06/23 16:29 V37553MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/06/23 16:29 V37553MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/06/23 16:29 V37553MSA
<42.0 µg/L 42.0 200Ethanol 1 09/06/23 16:29 V37553MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/06/23 16:29 V37553MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/06/23 16:29 V37553MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/06/23 16:29 V37553MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/06/23 16:29 V37553MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/06/23 16:29 V37553MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/06/23 16:29 V37553MSA
0.274 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/06/23 16:29 V37553MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/06/23 16:29 V37553MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/06/23 16:29 V37553MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-2
93497 Matrix:
8/24/2023 10:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37551 09/06/23 09:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/06/23 16:29 V37553MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/06/23 16:29 V37553MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/06/23 16:29 V37553MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/06/23 16:29 V37553MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/06/23 16:29 V37553MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/06/23 16:29 V37553MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/06/23 16:29 V37553MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/06/23 16:29 V37553MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/06/23 16:29 V37553MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/06/23 16:29 V37553MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/06/23 16:29 V37553MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/06/23 16:29 V37553MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/06/23 16:29 V37553MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/06/23 16:29 V37553MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/06/23 16:29 V37553MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/06/23 16:29 V37553MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/06/23 16:29 V37553MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/06/23 16:29 V37553MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/06/23 16:29 V37553MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/06/23 16:29 V37553MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/06/23 16:29 V37553MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/06/23 16:29 V37553MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/06/23 16:29 V37553MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-2
93497 Matrix:
8/24/2023 10:12
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37551 09/06/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/06/23 16:29 V37553MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/06/23 16:29 V37553
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%09/06/23 16:291 MSA V37553
Surrogate: Dibromofluoromethane 104 Limits: 70-130%09/06/23 16:291 MSA V37553
Surrogate: 1,2-Dichloroethane - d4 92.2 Limits: 70-130%09/06/23 16:291 MSA V37553
Surrogate: Toluene-d8 100 Limits: 70-130%09/06/23 16:291 MSA V37553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-3
93498 Matrix:
8/24/2023 10:22
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/05/23 17:12 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%09/05/23 17:121 MSA V37496
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/05/23 17:121 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 87.8 Limits: 70-130%09/05/23 17:121 MSA V37496
Surrogate: Toluene-d8 99.4 Limits: 70-130%09/05/23 17:121 MSA V37496
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-3
93498 Matrix:
8/24/2023 10:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/05/23 17:12 V37496MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/05/23 17:12 V37496MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/05/23 17:12 V37496MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/05/23 17:12 V37496MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/05/23 17:12 V37496MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/05/23 17:12 V37496MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/05/23 17:12 V37496MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/05/23 17:12 V37496MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/05/23 17:12 V37496MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/05/23 17:12 V37496MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/05/23 17:12 V37496MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/05/23 17:12 V37496MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/05/23 17:12 V37496MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/05/23 17:12 V37496MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/05/23 17:12 V37496MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/05/23 17:12 V37496MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/05/23 17:12 V37496MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/05/23 17:12 V37496MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/05/23 17:12 V37496MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/05/23 17:12 V37496MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/05/23 17:12 V37496MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/05/23 17:12 V37496MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/05/23 17:12 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-3
93498 Matrix:
8/24/2023 10:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/05/23 17:12 V37496MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/05/23 17:12 V37496MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/05/23 17:12 V37496MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/05/23 17:12 V37496MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/05/23 17:12 V37496MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/05/23 17:12 V37496MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/05/23 17:12 V37496MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/05/23 17:12 V37496MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/05/23 17:12 V37496MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/05/23 17:12 V37496MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/05/23 17:12 V37496MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/05/23 17:12 V37496MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/05/23 17:12 V37496MSA
<42.0 µg/L 42.0 200Ethanol 1 09/05/23 17:12 V37496MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/05/23 17:12 V37496MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/05/23 17:12 V37496MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/05/23 17:12 V37496MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/05/23 17:12 V37496MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/05/23 17:12 V37496MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/05/23 17:12 V37496MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/05/23 17:12 V37496MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/05/23 17:12 V37496MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/05/23 17:12 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-3
93498 Matrix:
8/24/2023 10:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/05/23 17:12 V37496MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/05/23 17:12 V37496MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/05/23 17:12 V37496MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/05/23 17:12 V37496MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/05/23 17:12 V37496MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/05/23 17:12 V37496MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/05/23 17:12 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/05/23 17:12 V37496MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/05/23 17:12 V37496MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/05/23 17:12 V37496MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/05/23 17:12 V37496MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/05/23 17:12 V37496MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/05/23 17:12 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/05/23 17:12 V37496MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/05/23 17:12 V37496MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/05/23 17:12 V37496MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/05/23 17:12 V37496MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/05/23 17:12 V37496MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/05/23 17:12 V37496MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/05/23 17:12 V37496MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/05/23 17:12 V37496MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/05/23 17:12 V37496MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/05/23 17:12 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-3
93498 Matrix:
8/24/2023 10:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/05/23 17:12 V37496MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/05/23 17:12 V37496
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%09/05/23 17:121 MSA V37496
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/05/23 17:121 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 87.8 Limits: 70-130%09/05/23 17:121 MSA V37496
Surrogate: Toluene-d8 99.4 Limits: 70-130%09/05/23 17:121 MSA V37496
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-4
93499 Matrix:
8/24/2023 10:33
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/05/23 17:38 6200BMSA
Surrogate: 4-Bromofluorobenzene 94.8 Limits: 70-130%09/05/23 17:381 MSA V37496
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/05/23 17:381 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 88.4 Limits: 70-130%09/05/23 17:381 MSA V37496
Surrogate: Toluene-d8 99.4 Limits: 70-130%09/05/23 17:381 MSA V37496
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%09/06/23 20:2010 MSA V37553
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/06/23 20:2010 MSA V37553
Surrogate: 1,2-Dichloroethane - d4 90.8 Limits: 70-130%09/06/23 20:2010 MSA V37553
Surrogate: Toluene-d8 99.6 Limits: 70-130%09/06/23 20:2010 MSA V37553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-4
93499 Matrix:
8/24/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/05/23 17:38 V37496MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/05/23 17:38 V37496MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/05/23 17:38 V37496MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/05/23 17:38 V37496MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/05/23 17:38 V37496MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/05/23 17:38 V37496MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/05/23 17:38 V37496MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/05/23 17:38 V37496MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/05/23 17:38 V37496MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/05/23 17:38 V37496MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/05/23 17:38 V37496MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/05/23 17:38 V37496MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/05/23 17:38 V37496MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/05/23 17:38 V37496MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/05/23 17:38 V37496MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/05/23 17:38 V37496MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/05/23 17:38 V37496MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/05/23 17:38 V37496MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/05/23 17:38 V37496MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/05/23 17:38 V37496MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/05/23 17:38 V37496MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/05/23 17:38 V37496MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/05/23 17:38 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-4
93499 Matrix:
8/24/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/05/23 17:38 V37496MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/05/23 17:38 V37496MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/05/23 17:38 V37496MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/05/23 17:38 V37496MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/05/23 17:38 V37496MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/05/23 17:38 V37496MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/05/23 17:38 V37496MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/05/23 17:38 V37496MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/05/23 17:38 V37496MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/05/23 17:38 V37496MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/05/23 17:38 V37496MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/05/23 17:38 V37496MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/05/23 17:38 V37496MSA
<42.0 µg/L 42.0 200Ethanol 1 09/05/23 17:38 V37496MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/05/23 17:38 V37496MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/05/23 17:38 V37496MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/05/23 17:38 V37496MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/05/23 17:38 V37496MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/05/23 17:38 V37496MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/05/23 17:38 V37496MSA
185 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 09/06/23 20:20 V37553MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/05/23 17:38 V37496MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/05/23 17:38 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-4
93499 Matrix:
8/24/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/05/23 17:38 V37496MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/05/23 17:38 V37496MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/05/23 17:38 V37496MSA
12.2 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/05/23 17:38 V37496MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/05/23 17:38 V37496MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/05/23 17:38 V37496MSA
0.496 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/05/23 17:38 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/05/23 17:38 V37496MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/05/23 17:38 V37496MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/05/23 17:38 V37496MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/05/23 17:38 V37496MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/05/23 17:38 V37496MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/05/23 17:38 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/05/23 17:38 V37496MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/05/23 17:38 V37496MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/05/23 17:38 V37496MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/05/23 17:38 V37496MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/05/23 17:38 V37496MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/05/23 17:38 V37496MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/05/23 17:38 V37496MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/05/23 17:38 V37496MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/05/23 17:38 V37496MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/05/23 17:38 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:MW-4
93499 Matrix:
8/24/2023 10:33
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/05/23 17:38 V37496MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/05/23 17:38 V37496
Surrogate: 4-Bromofluorobenzene 94.8 Limits: 70-130%09/05/23 17:381 MSA V37496
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/05/23 17:381 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 88.4 Limits: 70-130%09/05/23 17:381 MSA V37496
Surrogate: Toluene-d8 99.4 Limits: 70-130%09/05/23 17:381 MSA V37496
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%09/06/23 20:2010 MSA V37553
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/06/23 20:2010 MSA V37553
Surrogate: 1,2-Dichloroethane - d4 90.8 Limits: 70-130%09/06/23 20:2010 MSA V37553
Surrogate: Toluene-d8 99.6 Limits: 70-130%09/06/23 20:2010 MSA V37553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:TW-1
93500 Matrix:
8/24/2023 10:51
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/05/23 18:03 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%09/05/23 18:031 MSA V37496
Surrogate: Dibromofluoromethane 104 Limits: 70-130%09/05/23 18:031 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 90.0 Limits: 70-130%09/05/23 18:031 MSA V37496
Surrogate: Toluene-d8 99.6 Limits: 70-130%09/05/23 18:031 MSA V37496
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%09/06/23 20:4610 MSA V37553
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/06/23 20:4610 MSA V37553
Surrogate: 1,2-Dichloroethane - d4 90.6 Limits: 70-130%09/06/23 20:4610 MSA V37553
Surrogate: Toluene-d8 100 Limits: 70-130%09/06/23 20:4610 MSA V37553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:TW-1
93500 Matrix:
8/24/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/05/23 18:03 V37496MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/05/23 18:03 V37496MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/05/23 18:03 V37496MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/05/23 18:03 V37496MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/05/23 18:03 V37496MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/05/23 18:03 V37496MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/05/23 18:03 V37496MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/05/23 18:03 V37496MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/05/23 18:03 V37496MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/05/23 18:03 V37496MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/05/23 18:03 V37496MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/05/23 18:03 V37496MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/05/23 18:03 V37496MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/05/23 18:03 V37496MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/05/23 18:03 V37496MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/05/23 18:03 V37496MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/05/23 18:03 V37496MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/05/23 18:03 V37496MSA
2.43 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/05/23 18:03 V37496MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/05/23 18:03 V37496MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/05/23 18:03 V37496MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/05/23 18:03 V37496MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/05/23 18:03 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:TW-1
93500 Matrix:
8/24/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/05/23 18:03 V37496MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/05/23 18:03 V37496MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/05/23 18:03 V37496MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/05/23 18:03 V37496MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/05/23 18:03 V37496MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/05/23 18:03 V37496MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/05/23 18:03 V37496MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/05/23 18:03 V37496MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/05/23 18:03 V37496MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/05/23 18:03 V37496MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/05/23 18:03 V37496MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/05/23 18:03 V37496MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/05/23 18:03 V37496MSA
<42.0 µg/L 42.0 200Ethanol 1 09/05/23 18:03 V37496MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/05/23 18:03 V37496MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/05/23 18:03 V37496MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/05/23 18:03 V37496MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/05/23 18:03 V37496MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/05/23 18:03 V37496MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/05/23 18:03 V37496MSA
360 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 09/06/23 20:46 V37553MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/05/23 18:03 V37496MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/05/23 18:03 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:TW-1
93500 Matrix:
8/24/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/05/23 18:03 V37496MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/05/23 18:03 V37496MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/05/23 18:03 V37496MSA
4.06 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/05/23 18:03 V37496MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/05/23 18:03 V37496MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/05/23 18:03 V37496MSA
2.57 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/05/23 18:03 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/05/23 18:03 V37496MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/05/23 18:03 V37496MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/05/23 18:03 V37496MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/05/23 18:03 V37496MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/05/23 18:03 V37496MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/05/23 18:03 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/05/23 18:03 V37496MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/05/23 18:03 V37496MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/05/23 18:03 V37496MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/05/23 18:03 V37496MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/05/23 18:03 V37496MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/05/23 18:03 V37496MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/05/23 18:03 V37496MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/05/23 18:03 V37496MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/05/23 18:03 V37496MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/05/23 18:03 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:TW-1
93500 Matrix:
8/24/2023 10:51
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00 V37551 09/06/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/05/23 18:03 V37496MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/05/23 18:03 V37496
Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%09/05/23 18:031 MSA V37496
Surrogate: Dibromofluoromethane 104 Limits: 70-130%09/05/23 18:031 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 90.0 Limits: 70-130%09/05/23 18:031 MSA V37496
Surrogate: Toluene-d8 99.6 Limits: 70-130%09/05/23 18:031 MSA V37496
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%09/06/23 20:4610 MSA V37553
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/06/23 20:4610 MSA V37553
Surrogate: 1,2-Dichloroethane - d4 90.6 Limits: 70-130%09/06/23 20:4610 MSA V37553
Surrogate: Toluene-d8 100 Limits: 70-130%09/06/23 20:4610 MSA V37553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:SW-1
93501 Matrix:
8/24/2023 11:05
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 09/05/23 18:29 6200BMSA
Surrogate: 4-Bromofluorobenzene 95.6 Limits: 70-130%09/05/23 18:291 MSA V37496
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/05/23 18:291 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 89.0 Limits: 70-130%09/05/23 18:291 MSA V37496
Surrogate: Toluene-d8 100 Limits: 70-130%09/05/23 18:291 MSA V37496
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:SW-1
93501 Matrix:
8/24/2023 11:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/05/23 18:29 V37496MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/05/23 18:29 V37496MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/05/23 18:29 V37496MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/05/23 18:29 V37496MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/05/23 18:29 V37496MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/05/23 18:29 V37496MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/05/23 18:29 V37496MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/05/23 18:29 V37496MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/05/23 18:29 V37496MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/05/23 18:29 V37496MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/05/23 18:29 V37496MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/05/23 18:29 V37496MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/05/23 18:29 V37496MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/05/23 18:29 V37496MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/05/23 18:29 V37496MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/05/23 18:29 V37496MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/05/23 18:29 V37496MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/05/23 18:29 V37496MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/05/23 18:29 V37496MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/05/23 18:29 V37496MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/05/23 18:29 V37496MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/05/23 18:29 V37496MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/05/23 18:29 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:SW-1
93501 Matrix:
8/24/2023 11:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/05/23 18:29 V37496MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/05/23 18:29 V37496MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/05/23 18:29 V37496MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/05/23 18:29 V37496MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/05/23 18:29 V37496MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/05/23 18:29 V37496MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/05/23 18:29 V37496MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/05/23 18:29 V37496MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/05/23 18:29 V37496MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/05/23 18:29 V37496MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/05/23 18:29 V37496MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/05/23 18:29 V37496MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/05/23 18:29 V37496MSA
<42.0 µg/L 42.0 200Ethanol 1 09/05/23 18:29 V37496MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/05/23 18:29 V37496MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/05/23 18:29 V37496MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/05/23 18:29 V37496MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/05/23 18:29 V37496MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/05/23 18:29 V37496MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/05/23 18:29 V37496MSA
0.212 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/05/23 18:29 V37496MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/05/23 18:29 V37496MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/05/23 18:29 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:SW-1
93501 Matrix:
8/24/2023 11:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.470 µg/L 0.470 1.00Naphthalene 1 09/05/23 18:29 V37496MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/05/23 18:29 V37496MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/05/23 18:29 V37496MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 09/05/23 18:29 V37496MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 09/05/23 18:29 V37496MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 09/05/23 18:29 V37496MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 09/05/23 18:29 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/05/23 18:29 V37496MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/05/23 18:29 V37496MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/05/23 18:29 V37496MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/05/23 18:29 V37496MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/05/23 18:29 V37496MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/05/23 18:29 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/05/23 18:29 V37496MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/05/23 18:29 V37496MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/05/23 18:29 V37496MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/05/23 18:29 V37496MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/05/23 18:29 V37496MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/05/23 18:29 V37496MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/05/23 18:29 V37496MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/05/23 18:29 V37496MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/05/23 18:29 V37496MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/05/23 18:29 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:SW-1
93501 Matrix:
8/24/2023 11:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/05/23 18:29 V37496MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/05/23 18:29 V37496
Surrogate: 4-Bromofluorobenzene 95.6 Limits: 70-130%09/05/23 18:291 MSA V37496
Surrogate: Dibromofluoromethane 103 Limits: 70-130%09/05/23 18:291 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 89.0 Limits: 70-130%09/05/23 18:291 MSA V37496
Surrogate: Toluene-d8 100 Limits: 70-130%09/05/23 18:291 MSA V37496
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:TB
93502 Matrix:
8/24/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<1.80 µg/L 1.80 10.0Acetone 1 09/05/23 15:29 V37496MSA
<0.180 µg/L 0.180 0.500Benzene 1 09/05/23 15:29 V37496MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/05/23 15:29 V37496MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/05/23 15:29 V37496MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/05/23 15:29 V37496MSA
<1.50 µg/L 1.50 5.00Bromoform 1 09/05/23 15:29 V37496MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 09/05/23 15:29 V37496MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 09/05/23 15:29 V37496MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/05/23 15:29 V37496MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/05/23 15:29 V37496MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/05/23 15:29 V37496MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/05/23 15:29 V37496MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 09/05/23 15:29 V37496MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 09/05/23 15:29 V37496MSA
<0.220 µg/L 0.220 0.500Chloroform 1 09/05/23 15:29 V37496MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 09/05/23 15:29 V37496MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/05/23 15:29 V37496MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/05/23 15:29 V37496MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 09/05/23 15:29 V37496MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/05/23 15:29 V37496MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/05/23 15:29 V37496MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/05/23 15:29 V37496MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/05/23 15:29 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:TB
93502 Matrix:
8/24/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/05/23 15:29 V37496MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/05/23 15:29 V37496MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/05/23 15:29 V37496MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/05/23 15:29 V37496MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 09/05/23 15:29 V37496MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/05/23 15:29 V37496MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/05/23 15:29 V37496MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/05/23 15:29 V37496MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/05/23 15:29 V37496MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/05/23 15:29 V37496MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/05/23 15:29 V37496MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 09/05/23 15:29 V37496MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/05/23 15:29 V37496MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/05/23 15:29 V37496MSA
<42.0 µg/L 42.0 200Ethanol 1 09/05/23 15:29 V37496MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/05/23 15:29 V37496MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 09/05/23 15:29 V37496MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 09/05/23 15:29 V37496MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 09/05/23 15:29 V37496MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/05/23 15:29 V37496MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/05/23 15:29 V37496MSA
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 09/05/23 15:29 V37496MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 09/05/23 15:29 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:TB
93502 Matrix:
8/24/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.330 µg/L 0.330 2.00Methylene Chloride 1 09/05/23 15:29 V37496MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 09/05/23 15:29 V37496MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 09/05/23 15:29 V37496MSA
<0.220 µg/L 0.220 0.500Styrene 1 09/05/23 15:29 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/05/23 15:29 V37496MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/05/23 15:29 V37496MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/05/23 15:29 V37496MSA
<0.220 µg/L 0.220 0.500Toluene 1 09/05/23 15:29 V37496MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 09/05/23 15:29 V37496MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 09/05/23 15:29 V37496MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/05/23 15:29 V37496MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/05/23 15:29 V37496MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/05/23 15:29 V37496MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/05/23 15:29 V37496MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 09/05/23 15:29 V37496MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 09/05/23 15:29 V37496MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/05/23 15:29 V37496MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 09/05/23 15:29 V37496MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/05/23 15:29 V37496MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 09/05/23 15:29 V37496MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/05/23 15:29 V37496MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 53
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-240-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Sam McKay
Monroe
Danyale Love
Project Manager
GRI #5722 Received : 08/25/2023
Rushco #5
Report Date : 09/08/2023
Sample ID :
Lab No :
Sampled:TB
93502 Matrix:
8/24/2023 9:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V37495 09/05/23 09:00
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/05/23 15:29 V37496
Surrogate: 4-Bromofluorobenzene 94.8 Limits: 70-130%09/05/23 15:291 MSA V37496
Surrogate: Dibromofluoromethane 104 Limits: 70-130%09/05/23 15:291 MSA V37496
Surrogate: 1,2-Dichloroethane - d4 89.4 Limits: 70-130%09/05/23 15:291 MSA V37496
Surrogate: Toluene-d8 97.8 Limits: 70-130%09/05/23 15:291 MSA V37496
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
Associated Lab Samples: 93496, 93498, 93499, 93500, 93501, 93502
LRB-V37495 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/05/23 14:3810.01.80<1.80µg/LAcetone
09/05/23 14:380.5000.180<0.180µg/LBenzene
09/05/23 14:380.5000.210<0.210µg/LBromobenzene
09/05/23 14:381.000.420<0.420µg/LBromochloromethane
09/05/23 14:380.5000.160<0.160µg/LBromodichloromethane
09/05/23 14:385.001.50<1.50µg/LBromoform
09/05/23 14:381.000.280<0.280µg/LBromomethane
09/05/23 14:380.5000.180<0.180µg/Ln-Butylbenzene
09/05/23 14:380.5000.200<0.200µg/Lsec-Butyl benzene
09/05/23 14:382.000.920<0.920µg/Ltert-Butyl benzene
09/05/23 14:380.5000.180<0.180µg/LCarbon Tetrachloride
09/05/23 14:380.5000.190<0.190µg/LChlorobenzene
09/05/23 14:380.5000.190<0.190µg/LChlorodibromomethane
09/05/23 14:381.000.430<0.430µg/LChloroethane
09/05/23 14:380.5000.220<0.220µg/LChloroform
09/05/23 14:380.5000.220<0.220µg/LChloromethane
09/05/23 14:380.5000.200<0.200µg/L2-Chlorotoluene
09/05/23 14:380.5000.200<0.200µg/L4-Chlorotoluene
09/05/23 14:380.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/05/23 14:382.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/05/23 14:380.5000.200<0.200µg/L1,2-Dibromoethane
09/05/23 14:380.5000.230<0.230µg/LDibromomethane
09/05/23 14:380.5000.220<0.220µg/L1,2-Dichlorobenzene
09/05/23 14:380.5000.190<0.190µg/L1,3-Dichlorobenzene
09/05/23 14:380.5000.210<0.210µg/L1,4-Dichlorobenzene
09/05/23 14:385.001.20<1.20µg/LDichlorodifluoromethane
09/05/23 14:380.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 12Date:09/08/2023 11:23 AM
Page 40 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
Associated Lab Samples: 93496, 93498, 93499, 93500, 93501, 93502
LRB-V37495 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/05/23 14:380.5000.150<0.150µg/L1,2-Dichloroethane
09/05/23 14:380.5000.150<0.150µg/L1,1-Dichloroethene
09/05/23 14:380.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/05/23 14:380.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/05/23 14:380.5000.190<0.190µg/L1,2-Dichloropropane
09/05/23 14:380.5000.130<0.130µg/L1,3-Dichloropropane
09/05/23 14:382.000.210<0.210µg/L2,2-Dichloropropane
09/05/23 14:380.5000.200<0.200µg/L1,1-Dichloropropene
09/05/23 14:380.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/05/23 14:380.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/05/23 14:3820042.0<42.0µg/LEthanol
09/05/23 14:380.5000.170<0.170µg/LEthylbenzene
09/05/23 14:383.000.350<0.350µg/LHexachlorobutadiene
09/05/23 14:381.000.380<0.380µg/L2-Hexanone
09/05/23 14:380.5000.180<0.180µg/LIsopropylbenzene
09/05/23 14:380.5000.089<0.089µg/L4-Isopropyl toluene
09/05/23 14:385.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/05/23 14:381.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/05/23 14:381.000.078<0.078µg/L4-Methyl-2-Pentanone
09/05/23 14:382.000.330<0.330µg/LMethylene Chloride
09/05/23 14:381.000.470<0.470µg/LNaphthalene
09/05/23 14:380.5000.190<0.190µg/Ln-Propylbenzene
09/05/23 14:380.5000.220<0.220µg/LStyrene
09/05/23 14:3810.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
09/05/23 14:3810.00.350<0.350µg/Ltert-Butyl formate (TBF)
09/05/23 14:3810.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
09/05/23 14:3810.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 12Date:09/08/2023 11:23 AM
Page 41 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
Associated Lab Samples: 93496, 93498, 93499, 93500, 93501, 93502
LRB-V37495 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/05/23 14:380.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
09/05/23 14:380.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/05/23 14:380.5000.220<0.220µg/LTetrachloroethene
09/05/23 14:380.5000.220<0.220µg/LToluene
09/05/23 14:380.5000.380<0.380µg/L1,2,3-Trichlorobenzene
09/05/23 14:380.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/05/23 14:380.5000.160<0.160µg/L1,1,1-Trichloroethane
09/05/23 14:380.5000.096<0.096µg/L1,1,2-Trichloroethane
09/05/23 14:380.5000.180<0.180µg/LTrichloroethene
09/05/23 14:380.5000.180<0.180µg/LTrichlorofluoromethane
09/05/23 14:380.5000.270<0.270µg/L1,2,3-Trichloropropane
09/05/23 14:380.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/05/23 14:380.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/05/23 14:385.001.00<1.00µg/LVinyl Acetate
09/05/23 14:380.5000.170<0.170µg/LVinyl Chloride
09/05/23 14:380.5000.210<0.210µg/Lo-Xylene
09/05/23 14:381.000.420<0.420µg/Lm,p-Xylene
09/05/23 14:3810.01.00<1.00µg/L3,3-Dimethyl-1-butanol
09/05/23 14:384-Bromofluorobenzene (S)96.4 70-130
09/05/23 14:38Dibromofluoromethane (S)102 70-130
09/05/23 14:381,2-Dichloroethane - d4 (S)90.0 70-130
09/05/23 14:38Toluene-d8 (S)101 70-130
Page 3 of 12Date:09/08/2023 11:23 AM
Page 42 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
LCS-V37495 LCSD-V37495Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.2 93.078.531.440.0µg/LAcetone 40-160 16.9 20.0
20.9 10510420.820.0µg/LBenzene 70-130 0.4 20.0
19.0 95.097.019.420.0µg/LBromobenzene 70-130 2.0 20.0
21.7 10910420.820.0µg/LBromochloromethane 70-130 4.2 20.0
19.1 95.594.518.920.0µg/LBromodichloromethane 70-130 1.0 20.0
17.6 88.089.517.920.0µg/LBromoform 70-130 1.6 20.0
22.4 11210721.420.0µg/LBromomethane 60-140 4.5 20.0
20.8 10410821.520.0µg/Ln-Butylbenzene 70-130 3.3 20.0
20.4 10210420.720.0µg/Lsec-Butyl benzene 70-130 1.4 20.0
19.0 95.098.519.720.0µg/Ltert-Butyl benzene 70-130 3.6 20.0
20.2 10110220.320.0µg/LCarbon Tetrachloride 70-130 0.4 20.0
19.7 98.510120.120.0µg/LChlorobenzene 70-130 2.0 20.0
19.2 96.099.019.820.0µg/LChlorodibromomethane 70-130 3.0 20.0
20.4 10210520.920.0µg/LChloroethane 60-140 2.4 20.0
20.0 10010020.020.0µg/LChloroform 70-130 0.0 20.0
19.1 95.595.519.120.0µg/LChloromethane 60-140 0.0 20.0
19.3 96.595.019.020.0µg/L2-Chlorotoluene 70-130 1.5 20.0
18.7 93.596.519.320.0µg/L4-Chlorotoluene 70-130 3.1 20.0
20.6 10310220.420.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.9 20.0
19.2 96.095.019.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.0 20.0
19.6 98.098.519.720.0µg/L1,2-Dibromoethane 70-130 0.5 20.0
17.9 89.591.518.320.0µg/LDibromomethane 70-130 2.2 20.0
19.5 97.510120.220.0µg/L1,2-Dichlorobenzene 70-130 3.5 20.0
20.0 10010320.520.0µg/L1,3-Dichlorobenzene 70-130 2.4 20.0
19.9 99.598.519.720.0µg/L1,4-Dichlorobenzene 70-130 1.0 20.0
18.5 92.593.018.620.0µg/LDichlorodifluoromethane 60-140 0.5 20.0
Page 4 of 12Date:09/08/2023 11:23 AM
Page 43 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
LCS-V37495 LCSD-V37495Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.7 10410320.620.0µg/L1,1-Dichloroethane 70-130 0.4 20.0
16.8 84.083.016.620.0µg/L1,2-Dichloroethane 70-130 1.1 20.0
23.1 11610120.120.0µg/L1,1-Dichloroethene 70-130 13.8 20.0
19.6 98.099.519.920.0µg/Lcis-1,2-Dichloroethene 70-130 1.5 20.0
22.1 11110120.120.0µg/Ltrans-1,2-Dichloroethene 70-130 9.4 20.0
19.8 99.010220.420.0µg/L1,2-Dichloropropane 70-130 2.9 20.0
19.2 96.097.519.520.0µg/L1,3-Dichloropropane 70-130 1.5 20.0
20.3 10210320.520.0µg/L2,2-Dichloropropane 70-130 0.9 20.0
22.7 11411322.620.0µg/L1,1-Dichloropropene 70-130 0.4 20.0
19.9 99.597.019.420.0µg/Lcis-1,3-Dichloropropene 70-130 2.5 20.0
18.6 93.094.018.820.0µg/Ltrans-1,3-Dichloropropene 70-130 1.0 20.0
493 98.688.4442500µg/LEthanol 60-140 10.9 20.0
19.1 95.594.018.820.0µg/LEthylbenzene 70-130 1.5 20.0
19.8 99.010420.720.0µg/LHexachlorobutadiene 70-130 4.4 20.0
18.1 90.586.017.220.0µg/L2-Hexanone 60-140 5.0 20.0
20.2 10110320.520.0µg/LIsopropylbenzene 70-130 1.4 20.0
20.7 10410420.820.0µg/L4-Isopropyl toluene 70-130 0.4 20.0
16.6 83.096.019.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 14.5 20.0
21.4 10710020.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 6.7 20.0
17.7 88.587.017.420.0µg/L4-Methyl-2-Pentanone 60-140 1.7 20.0
21.8 10995.019.020.0µg/LMethylene Chloride 70-130 13.7 20.0
18.0 90.093.518.720.0µg/LNaphthalene 70-130 3.8 20.0
19.7 98.510120.120.0µg/Ln-Propylbenzene 70-130 2.0 20.0
21.0 10510220.320.0µg/LStyrene 70-130 3.3 20.0
50.4 12612449.640.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.6 20.0
39.7 99.210441.440.0µg/Ltert-Butyl formate (TBF)40-140 4.1 20.0
Page 5 of 12Date:09/08/2023 11:23 AM
Page 44 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37496QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37495
LCS-V37495 LCSD-V37495Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.7 10485.517.120.0µg/Ltert-Amyl Alcohol (TAA)40-140 19.0 20.0
40.2 10110140.240.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.0 20.0
20.5 10310721.320.0µg/L1,1,1,2-Tetrachloroethane 70-130 3.8 20.0
19.5 97.599.019.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.5 20.0
20.1 10110220.320.0µg/LTetrachloroethene 70-130 0.9 20.0
19.5 97.598.519.720.0µg/LToluene 70-130 1.0 20.0
18.7 93.597.019.420.0µg/L1,2,3-Trichlorobenzene 70-130 3.6 20.0
18.9 94.599.019.820.0µg/L1,2,4-Trichlorobenzene 70-130 4.6 20.0
20.3 10210120.220.0µg/L1,1,1-Trichloroethane 70-130 0.4 20.0
19.7 98.510320.620.0µg/L1,1,2-Trichloroethane 70-130 4.4 20.0
20.8 10410120.120.0µg/LTrichloroethene 70-130 3.4 20.0
21.1 10610821.520.0µg/LTrichlorofluoromethane 60-140 1.8 20.0
19.4 97.095.519.120.0µg/L1,2,3-Trichloropropane 70-130 1.5 20.0
20.1 10199.519.920.0µg/L1,2,4-Trimethylbenzene 70-130 1.0 20.0
19.6 98.098.519.720.0µg/L1,3,5-Trimethylbenzene 70-130 0.5 20.0
20.1 10198.519.720.0µg/LVinyl Acetate 60-140 2.0 20.0
21.8 10911021.920.0µg/LVinyl Chloride 60-140 0.4 20.0
19.6 98.098.019.620.0µg/Lo-Xylene 70-130 0.0 20.0
39.5 98.710040.140.0µg/Lm,p-Xylene 70-130 1.5 20.0
21.4 10778.015.620.0µg/L3,3-Dimethyl-1-butanol 70-130 31.3*20.0
91.493.44-Bromofluorobenzene (S)70-130
99.498.8Dibromofluoromethane (S)70-130
90.089.41,2-Dichloroethane - d4 (S)70-130
99.6100Toluene-d8 (S)70-130
Page 6 of 12* QC Fail Date:09/08/2023 11:23 AM
Page 45 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37551
Associated Lab Samples: 93496, 93497, 93499, 93500
LRB-V37551 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/23 16:0310.01.80<1.80µg/LAcetone
09/06/23 16:030.5000.180<0.180µg/LBenzene
09/06/23 16:030.5000.210<0.210µg/LBromobenzene
09/06/23 16:031.000.420<0.420µg/LBromochloromethane
09/06/23 16:030.5000.160<0.160µg/LBromodichloromethane
09/06/23 16:035.001.50<1.50µg/LBromoform
09/06/23 16:031.000.280<0.280µg/LBromomethane
09/06/23 16:030.5000.180<0.180µg/Ln-Butylbenzene
09/06/23 16:030.5000.200<0.200µg/Lsec-Butyl benzene
09/06/23 16:032.000.920<0.920µg/Ltert-Butyl benzene
09/06/23 16:030.5000.180<0.180µg/LCarbon Tetrachloride
09/06/23 16:030.5000.190<0.190µg/LChlorobenzene
09/06/23 16:030.5000.190<0.190µg/LChlorodibromomethane
09/06/23 16:031.000.430<0.430µg/LChloroethane
09/06/23 16:030.5000.220<0.220µg/LChloroform
09/06/23 16:030.5000.220<0.220µg/LChloromethane
09/06/23 16:030.5000.200<0.200µg/L2-Chlorotoluene
09/06/23 16:030.5000.200<0.200µg/L4-Chlorotoluene
09/06/23 16:030.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
09/06/23 16:032.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/06/23 16:030.5000.230<0.230µg/LDibromomethane
09/06/23 16:030.5000.220<0.220µg/L1,2-Dichlorobenzene
09/06/23 16:030.5000.190<0.190µg/L1,3-Dichlorobenzene
09/06/23 16:030.5000.210<0.210µg/L1,4-Dichlorobenzene
09/06/23 16:035.001.20<1.20µg/LDichlorodifluoromethane
09/06/23 16:030.5000.240<0.240µg/L1,1-Dichloroethane
09/06/23 16:030.5000.150<0.150µg/L1,2-Dichloroethane
Page 7 of 12Date:09/08/2023 11:23 AM
Page 46 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37551
Associated Lab Samples: 93496, 93497, 93499, 93500
LRB-V37551 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/23 16:030.5000.150<0.150µg/L1,1-Dichloroethene
09/06/23 16:030.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/06/23 16:030.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/06/23 16:030.5000.190<0.190µg/L1,2-Dichloropropane
09/06/23 16:030.5000.130<0.130µg/L1,3-Dichloropropane
09/06/23 16:032.000.210<0.210µg/L2,2-Dichloropropane
09/06/23 16:030.5000.200<0.200µg/L1,1-Dichloropropene
09/06/23 16:030.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/06/23 16:030.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/06/23 16:0320042.0<42.0µg/LEthanol
09/06/23 16:030.5000.170<0.170µg/LEthylbenzene
09/06/23 16:033.000.350<0.350µg/LHexachlorobutadiene
09/06/23 16:031.000.380<0.380µg/L2-Hexanone
09/06/23 16:030.5000.180<0.180µg/LIsopropylbenzene
09/06/23 16:030.5000.089<0.089µg/L4-Isopropyl toluene
09/06/23 16:035.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/06/23 16:031.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/06/23 16:031.000.078<0.078µg/L4-Methyl-2-Pentanone
09/06/23 16:032.000.330<0.330µg/LMethylene Chloride
09/06/23 16:031.000.470<0.470µg/LNaphthalene
09/06/23 16:030.5000.190<0.190µg/Ln-Propylbenzene
09/06/23 16:030.5000.220<0.220µg/LStyrene
09/06/23 16:0310.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
09/06/23 16:0310.00.350<0.350µg/Ltert-Butyl formate (TBF)
09/06/23 16:0310.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
09/06/23 16:0310.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
09/06/23 16:030.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
Page 8 of 12Date:09/08/2023 11:23 AM
Page 47 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37551
Associated Lab Samples: 93496, 93497, 93499, 93500
LRB-V37551 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/23 16:030.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/06/23 16:030.5000.220<0.220µg/LTetrachloroethene
09/06/23 16:030.5000.220<0.220µg/LToluene
09/06/23 16:030.5000.380<0.380µg/L1,2,3-Trichlorobenzene
09/06/23 16:030.5000.310<0.310µg/L1,2,4-Trichlorobenzene
09/06/23 16:030.5000.160<0.160µg/L1,1,1-Trichloroethane
09/06/23 16:030.5000.096<0.096µg/L1,1,2-Trichloroethane
09/06/23 16:030.5000.180<0.180µg/LTrichloroethene
09/06/23 16:030.5000.180<0.180µg/LTrichlorofluoromethane
09/06/23 16:030.5000.270<0.270µg/L1,2,3-Trichloropropane
09/06/23 16:030.5000.190<0.190µg/L1,2,4-Trimethylbenzene
09/06/23 16:030.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/06/23 16:035.001.00<1.00µg/LVinyl Acetate
09/06/23 16:030.5000.170<0.170µg/LVinyl Chloride
09/06/23 16:030.5000.210<0.210µg/Lo-Xylene
09/06/23 16:031.000.420<0.420µg/Lm,p-Xylene
09/06/23 16:0310.01.00<1.00µg/L3,3-Dimethyl-1-butanol
09/06/23 16:034-Bromofluorobenzene (S)97.4 70-130
09/06/23 16:03Dibromofluoromethane (S)103 70-130
09/06/23 16:031,2-Dichloroethane - d4 (S)92.4 70-130
09/06/23 16:03Toluene-d8 (S)101 70-130
LCS-V37551 LCSD-V37551Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
33.4 83.575.730.340.0µg/LAcetone 40-160 9.7 20.0
Page 9 of 12Date:09/08/2023 11:23 AM
Page 48 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37551
LCS-V37551 LCSD-V37551Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.6 10310420.820.0µg/LBenzene 70-130 0.9 20.0
18.3 91.592.018.420.0µg/LBromobenzene 70-130 0.5 20.0
22.2 11110821.520.0µg/LBromochloromethane 70-130 3.2 20.0
18.6 93.091.018.220.0µg/LBromodichloromethane 70-130 2.1 20.0
17.6 88.082.516.520.0µg/LBromoform 70-130 6.4 20.0
21.2 10610821.620.0µg/LBromomethane 60-140 1.8 20.0
19.5 97.510220.320.0µg/Ln-Butylbenzene 70-130 4.0 20.0
18.9 94.598.519.720.0µg/Lsec-Butyl benzene 70-130 4.1 20.0
18.6 93.096.519.320.0µg/Ltert-Butyl benzene 70-130 3.6 20.0
20.3 10299.519.920.0µg/LCarbon Tetrachloride 70-130 1.9 20.0
19.8 99.010020.020.0µg/LChlorobenzene 70-130 1.0 20.0
19.1 95.592.018.420.0µg/LChlorodibromomethane 70-130 3.7 20.0
18.2 91.094.018.820.0µg/LChloroethane 60-140 3.2 20.0
20.2 10110420.720.0µg/LChloroform 70-130 2.4 20.0
16.8 84.085.017.020.0µg/LChloromethane 60-140 1.1 20.0
18.6 93.095.519.120.0µg/L2-Chlorotoluene 70-130 2.6 20.0
18.6 93.093.518.720.0µg/L4-Chlorotoluene 70-130 0.5 20.0
20.7 10499.519.920.0µg/LDi-Isopropyl Ether (DIPE)70-130 3.9 20.0
17.3 86.587.517.520.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.1 20.0
18.1 90.587.017.420.0µg/LDibromomethane 70-130 3.9 20.0
19.0 95.096.519.320.0µg/L1,2-Dichlorobenzene 70-130 1.5 20.0
19.3 96.510020.020.0µg/L1,3-Dichlorobenzene 70-130 3.5 20.0
19.1 95.598.019.620.0µg/L1,4-Dichlorobenzene 70-130 2.5 20.0
15.4 77.080.516.120.0µg/LDichlorodifluoromethane 60-140 4.4 20.0
21.1 10610721.320.0µg/L1,1-Dichloroethane 70-130 0.9 20.0
16.9 84.584.016.820.0µg/L1,2-Dichloroethane 70-130 0.5 20.0
Page 10 of 12Date:09/08/2023 11:23 AM
Page 49 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37551
LCS-V37551 LCSD-V37551Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.3 96.510120.120.0µg/L1,1-Dichloroethene 70-130 4.0 20.0
19.9 99.598.519.720.0µg/Lcis-1,2-Dichloroethene 70-130 1.0 20.0
20.2 10110420.820.0µg/Ltrans-1,2-Dichloroethene 70-130 2.9 20.0
19.7 98.510220.420.0µg/L1,2-Dichloropropane 70-130 3.4 20.0
19.1 95.590.518.120.0µg/L1,3-Dichloropropane 70-130 5.3 20.0
20.2 10110621.220.0µg/L2,2-Dichloropropane 70-130 4.8 20.0
22.0 11011122.220.0µg/L1,1-Dichloropropene 70-130 0.9 20.0
19.0 95.094.518.920.0µg/Lcis-1,3-Dichloropropene 70-130 0.5 20.0
17.9 89.589.017.820.0µg/Ltrans-1,3-Dichloropropene 70-130 0.5 20.0
469 93.886.6433500µg/LEthanol 60-140 7.9 20.0
18.7 93.593.518.720.0µg/LEthylbenzene 70-130 0.0 20.0
17.3 86.592.518.520.0µg/LHexachlorobutadiene 70-130 6.7 20.0
17.9 89.585.517.120.0µg/L2-Hexanone 60-140 4.5 20.0
19.3 96.599.519.920.0µg/LIsopropylbenzene 70-130 3.0 20.0
19.4 97.010120.220.0µg/L4-Isopropyl toluene 70-130 4.0 20.0
17.9 89.589.017.820.0µg/LMethyl Ethyl Ketone (MEK)60-140 0.5 20.0
20.9 10599.019.820.0µg/LMethyl tert-butyl ether (MTBE)70-130 5.4 20.0
17.2 86.081.016.220.0µg/L4-Methyl-2-Pentanone 60-140 5.9 20.0
20.1 10110220.320.0µg/LMethylene Chloride 70-130 0.9 20.0
15.6 78.077.515.520.0µg/LNaphthalene 70-130 0.6 20.0
18.8 94.097.519.520.0µg/Ln-Propylbenzene 70-130 3.6 20.0
19.9 99.597.519.520.0µg/LStyrene 70-130 2.0 20.0
47.3 11811345.340.0µg/Ltert-Butyl Alcohol (TBA)40-140 4.3 20.0
37.8 94.597.539.040.0µg/Ltert-Butyl formate (TBF)40-140 3.1 20.0
18.5 92.592.018.420.0µg/Ltert-Amyl Alcohol (TAA)40-140 0.5 20.0
39.9 99.795.538.240.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 4.3 20.0
Page 11 of 12Date:09/08/2023 11:23 AM
Page 50 of 53
Quality Control Data
23-240-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Rushco #5
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V37553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V37551
LCS-V37551 LCSD-V37551Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.0 10098.019.620.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.0 20.0
18.9 94.594.018.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.5 20.0
19.9 99.599.019.820.0µg/LTetrachloroethene 70-130 0.5 20.0
19.5 97.596.519.320.0µg/LToluene 70-130 1.0 20.0
16.4 82.084.016.820.0µg/L1,2,3-Trichlorobenzene 70-130 2.4 20.0
16.4 82.085.017.020.0µg/L1,2,4-Trichlorobenzene 70-130 3.5 20.0
20.4 10298.519.720.0µg/L1,1,1-Trichloroethane 70-130 3.4 20.0
20.0 10091.018.220.0µg/L1,1,2-Trichloroethane 70-130 9.4 20.0
19.6 98.010120.120.0µg/LTrichloroethene 70-130 2.5 20.0
19.0 95.096.519.320.0µg/LTrichlorofluoromethane 60-140 1.5 20.0
18.1 90.591.518.320.0µg/L1,2,3-Trichloropropane 70-130 1.0 20.0
19.5 97.598.519.720.0µg/L1,2,4-Trimethylbenzene 70-130 1.0 20.0
18.9 94.597.019.420.0µg/L1,3,5-Trimethylbenzene 70-130 2.6 20.0
18.7 93.598.019.620.0µg/LVinyl Acetate 60-140 4.6 20.0
19.6 98.010220.420.0µg/LVinyl Chloride 60-140 4.0 20.0
19.1 95.595.019.020.0µg/Lo-Xylene 70-130 0.5 20.0
38.7 96.797.238.940.0µg/Lm,p-Xylene 70-130 0.5 20.0
21.1 10695.519.120.0µg/L3,3-Dimethyl-1-butanol 70-130 9.9 20.0
92.093.84-Bromofluorobenzene (S)70-130
103102Dibromofluoromethane (S)70-130
91.090.81,2-Dichloroethane - d4 (S)70-130
10099.8Toluene-d8 (S)70-130
Page 12 of 12Date:09/08/2023 11:23 AM
Page 51 of 53
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-240-0001
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:08/28/2023 09:04:48
Special precautions or instructions included?
Comments:
Page 52 of 53
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