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HomeMy WebLinkAboutMO-4537_15139_CA_MRP_20230721
3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012
July 21, 2023
Mr. Ryan Bond
NCDEQ-UST Section
Winston-Salem Regional Office
450 W. Hanes Mill Road
Suite 300
Winston-Salem, NC 27105
Re: Ground Water Monitoring Report
June 2023
The Corner Store
896 Oakridge Farm Highway
Mooresville, Iredell County
North Carolina
Facility ID Number: 0-00-0000017677
Incident Number: 15139
GRI Project Number: 3992
Dear Mr. Bond,
Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Joanna Alley at 704-845-4010.
Sincerely,
Geological Resources, Inc.
Leslie Maxtone-Graham
Administrative Assistant
Enclosure
Cc: Ms. Linda Beam, file
3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
June 2023
The Corner Store
896 Oakridge Farm Highway
Mooresville, Iredell County
North Carolina
Facility ID Number: 0-00-0000017677
Incident Number: 15139
GRI Project Number: 3992
Prepared for:
Ms. Linda Beam
Post Office Box 304
Mooresville, North Carolina 28115
July 21, 2023
Joanna Alley, P.E.
Project Manager
Eric M. Eubanks, P.G.
Report Writer
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 21, 2023 The Corner Store
Project Manager: Joanna Alley, P.E. GRI Project No. 3992
i
EXECUTIVE SUMMARY
The Corner Store is located at 896 Oakridge Farm Highway in Mooresville, Iredell County, North Carolina.
The site is currently owned by Race City Exxon, Inc. and is operated by D Mart, Inc. as a petroleum retail
facility. Two releases were discovered at the site during UST removal activities in 1995 and 2000.
Currently, one 12,000-gallon gasoline and two 6,000-gallon gasoline USTs are active at the site. The
adjoining properties are a mixture of single family residential, and commercial properties. According to
the information determined during updated receptor survey activities conducted on June 27, 2023,
eleven, potable water supply wells were identified within a 1,000-foot radius of the site and one inactive,
non-potable water supply well was located within a 250-foot radius of the site. Municipal water at the
time of the receptor survey was available to the site and some, but not all, of the surrounding properties.
A CAP prepared by Applied Earth Sciences, Inc., dated March 8, 2004, was approved by the NCDEQ on
April 10, 2007. The CAP recommended in-situ air sparging combined with soil vapor extraction
technologies to remediate impacted soils and ground water. The remediation system was installed in the
spring of 2009 and started on April 7, 2009. The remediation system at the site was deactivated in March
2014 and a passive remedial method implemented in September 2016. On September 14, 2016, oxygen
release material, in the form of socks, was placed in air sparging wells AS-1 through AS-4 and monitoring
wells MW-1A and MW-6. The socks have been periodically replaced.
On June 27, 2023, four monitoring wells, three air sparge wells, and two water supply wells were gauged
and/or sampled. No free product was observed at the site. An unknown oil that appears to be used
cooking oil based on field observations was present in AS-4; therefore, AS-4 was not sampled. The
concentrations of benzene, toluene, xylenes, MTBE, and/or 2-hexanone reported in the ground water
samples collected from MW-1A, MW-6, and AS-2 exceeded the MACs. Concentrations of MTBE and/or
acetone not exceeding the MACs were reported in the ground water samples collected from water supply
wells WSW-3 and WSW-11. All reported contaminant concentrations were below the GCLs. Although the
reported concentrations of 2-hexanone in the ground water samples collected from MW-6 and AS-2
exceeded the MAC, this is not considered a petroleum constituent.
Based on this information, the risk classification for the site should remain high risk. GRI recommends the
continued use of oxygen release compounds in site monitoring wells and semi-annual ground water
monitoring. The next sampling event is tentatively scheduled for December 2023.
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 21, 2023 The Corner Store
Project Manager: Joanna Alley, P.E. GRI Project No. 3992
ii
SITE INFORMATION
1. Site Identification
The Corner Store (Facility ID 0-00-0000017677)
Incident Number 15139 – High Risk (H250D)
Location of Source Area: 896 Oakridge Farm Highway
Mooresville, NC 28115
Iredell County
35.607716°N, 80.791846°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System
UST/AST Owner
Race City Exxon, Inc.
896 Oakridge Farm Highway
Mooresville, NC 28115
Email Unknown
704-799-3630
UST/AST Operator
D-Mart, Inc.
9709 Cockerham Lane
Huntersville, NC 28078
dmartinc12@gmail.com
704-902-7305
Property Owner
Race City Exxon, Inc.
896 Oakridge Farm Highway
Mooresville, NC 28115
Email Unknown
704-799-3630
Property Occupant
D Mart #6
896 Oakridge Farm Highway
Mooresville, NC 28115
dmartinc12@gmail.com
704-799-3630
Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
jra@geologicalresourcesinc.com
704-845-4010
Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 28217
State Cert. Nos. 37735 and 402
(704) 529-6364
3. Information about Release
Two releases were discovered at the site in January 1995 (Incident No. 15139) and November
2000 (Incident No. 22782).
An unknown amount of product was released from the leaking UST System
One 12,000-gallon gasoline UST and two 6,000-gallon gasoline USTs are active at the site. One
8,000-gallon gasoline UST, one 5,000-gallon gasoline UST, two 4,000-gallon gasoline USTs and one
550-gallon kerosene UST have been removed from the site.
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 21, 2023 The Corner Store
Project Manager: Joanna Alley, P.E. GRI Project No. 3992
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 21, 2023 The Corner Store
Project Manager: Joanna Alley, P.E. GRI Project No. 3992
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................3
3.0 FREE PRODUCT REMOVAL ........................................................................................................4
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4
5.0 CONCLUSIONS .........................................................................................................................5
6.0 LIMITATIONS ...........................................................................................................................5
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................5
FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3A: Site Vicinity Map
Figure 3B: Zoning Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Receptor Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Ground Water Dissolved Oxygen Information
Table 7: Summary of Ground Water Sample Analytical Results
APPENDICES
Appendix A: State Correspondence
Appendix B: Land Use Information
Appendix C: Incident Reports
Appendix D: Historical Soil Quality Information
Appendix E: Laboratory Analytical Report
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 21, 2023 The Corner Store
Project Manager: Joanna Alley, P.E. GRI Project No. 3992
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the June 2023 ground water sampling, sock replacement, and updated receptor
survey activities at The Corner Store, located at 896 Oakridge Farm Highway in Mooresville, Iredell County,
North Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 23-279,
which was submitted to the NCDEQ on June 2, 2023, and was approved as Task Authorization No. 15139-
47 on June 5, 2023. State correspondence is included as Appendix A.
The site is currently owned by Race City Exxon, Inc. and is operated as a retail facility and convenience
store named D Mart #6. During the removal of a 550-gallon kerosene UST on January 16, 1995, a
petroleum release was identified at the site. One 8,000-gallon gasoline UST, one 5,000-gallon gasoline
UST, two 4,000-gallon gasoline USTs and one 550-gallon kerosene UST have been removed from the site.
Currently, one 12,000-gallon gasoline and two 6,000-gallon gasoline USTs are active at the site. UST
owner/operator information and UST system information are included in Tables 1 and 2, respectively. The
Registered Tank Report is shown below:
The site and surrounding area are a mixture of single family residential and commercial properties. A copy
of the Land Use table is included as Appendix B. The site contains two buildings (the store and a storage
garage) and is primarily capped with concrete, asphalt, and grass. The overall topography at the site is
relatively flat. No surface water bodies were identified within a 500-foot radius of the site. Ten Type II
monitoring wells (MW-1 through MW-10) and four replacement wells (MW-1A, MW-3A, MW-4A and MW-
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 21, 2023 The Corner Store
Project Manager: Joanna Alley, P.E. GRI Project No. 3992
2
5A) were installed at the site during previous ground water assessment activities. A Site Map showing the
locations of the monitoring wells and the structures on-site has been included as Figure 2.
On June 27, 2023, GRI personnel conducted an updated receptor survey. Eleven potable water supply
wells (WSW-3 through WSW-5, WSW-8 through WSW-12, WSW-19, WSW-21, and WSW-23) were
identified within a 1,000-foot radius of the site and one inactive, non-potable water supply well (WSW-2)
was located within a 250-foot radius of the site. The ground water sampling event conducted in December
2015 detected a benzene concentration above the MAC in water supply well WSW-2. The well owner was
notified, and bottled water was provided. On January 7, 2016, a GAC filtration system was installed on
WSW-2. The residence using water supply well WSW-2 was eventually connected to municipal water on
July 18, 2018, and well WSW-2 is currently inactive. Municipal water is currently available to the site and
some, but not all surrounding properties. Receptor information is provided in Table 3. Adjacent property
owner information is presented in Table 4. A Site Vicinity Map showing the adjacent properties and a
Zoning Map showing the zoning information have been included as Figures 3A and 3B, respectively.
During the removal of a 550-gallon kerosene UST on January 16, 1995, a petroleum release was identified
at the site and issued Incident No. 15139. During the removal of two 4,000-gallon gasoline USTs, one
5,000-gallon gasoline UST and one 8,000-gallon gasoline UST on November 3, 2000, a subsequent release
at the site was identified and assigned Incident No. 22782. During initial abatement activities,
approximately 500 tons of gasoline impacted soils were excavated from the UST basin and approximately
50 tons from beneath the dispenser island. The two releases at the site are considered to be commingled
due to their proximity – the kerosene UST and the three gasoline USTs were located in the same UST
basin. The two incidents have been combined and reported under Incident Number 15139.
One incident (Incident No. 40553) has been reported on an adjacent property. Copies of the NCDEQ
Incident Reports are included as Appendix C. A map showing the locations of additional incidents in the
vicinity of the site is shown below:
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 21, 2023 The Corner Store
Project Manager: Joanna Alley, P.E. GRI Project No. 3992
3
Two CAPs have been submitted for the two incidents: the first in 1997 and the second in 2004. An in-situ
AS and SVE system was installed in 2009 and operated until 2014. Please note that no projected
milestones were established in the CAPs.
Based on this information, the site was classified as high risk.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Soil assessment was not conducted during the current scope of work. Historical soil quality information
and soil excavation information is included as Appendix D.
On June 27, 2023, four Type II monitoring wells (MW-1A, MW-4A, MW-6, and MW-10), three air sparge
wells (AS-1, AS-2, and AS-4), and two water supply wells (WSW-3 and WSW-11) were gauged, purged,
and/or sampled in accordance with NCDEQ guidelines. An unknown oil was encountered in AS-4;
therefore, this well was not sampled. Based on appearance and smell, it is believed that the unknown oil
is used cooking oil. The well cap and previously installed o-sock canister were missing from the well and
a cooking oil container is located approximately 30 feet from AS-4. Depths to ground water in the Type II
monitoring wells ranged from 36.03 feet to 42.59 feet below TOC. Relative ground water elevations in the
Type II monitoring wells ranged from 56.91 feet to 57.62 feet. Ground water flow was generally
convergent towards MW-1A with an average horizontal gradient of less than 0.01 feet per foot. Well
construction and gauging information is presented in Table 5. A Water Table Surface Map based on the
Type II monitoring wells is included as Figure 4. A summary of the current ground water gauging data is
shown below:
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1A 40 - 55 55 99.50 42.59 --- 56.91
MW-4A 40 - 55 55 99.44 42.37 --- 57.07
MW-6 35 – 45 45 100.08 42.46 --- 57.62
MW-10 35 – 55 55 98.85 41.78 --- 57.07
AS-1 Unknown 57.6 Unknown 39.02 --- Unknown
AS-2 Unknown 55.32 Unknown 36.03 --- Unknown
AS-4 Unknown 56.07 Unknown 42.04 41.97 Unknown
Adventus Remediation Technologies oxygen release material EHC-OTM in the form of socks were initially
installed at the site on September 14, 2016, in monitoring wells MW-1A and MW-6 and air sparge wells
AS-1 through AS-4 under Injection Permit Number WI0300331. The EHC-OTM socks were replaced
approximately every 6 months through July 2020. Due to repeated damage to air sparge well AS-3 from
truck traffic, well AS-3 was abandoned on August 30, 2018. On June 8, 2021, and January 27, 2022, the
EHC-OTM socks were removed from the above listed wells, excluding MW-6, and replaced with new EHC-
OTM socks. During June 2023 sock replacement activities, the EHC-OTM socks could not be removed from
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 21, 2023 The Corner Store
Project Manager: Joanna Alley, P.E. GRI Project No. 3992
4
either AS-2 or MW-6. The EHC-OTM socks were replaced in wells MW-1A and AS-1. Due to technical
difficulties with the YSI probe, dissolved oxygen readings could not be collected during the June 2023
ground water sampling activities. Historical dissolved oxygen and temperature readings are included in
Table 6.
Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. No free product was observed at the site. The concentrations of benzene, toluene,
xylenes, MTBE, and/or 2-hexanone reported in the ground water samples collected from MW-1A, MW-6,
and AS-2 exceeded the MACs. Concentrations of MTBE and/or acetone not exceeding the MACs were
reported in the ground water samples collected from water supply wells WSW-3 and WSW-11. All
reported contaminant concentrations were below the GCLs. Although the reported concentrations of 2-
hexanone in the ground water samples collected from MW-6 and AS-2 exceeded the MAC, this is not
considered a petroleum constituent. A summary of the analytical results for ground water samples
collected on June 27, 2023, is presented in Table 7. A Ground Water Quality Map based on the June 2023
data is included as Figure 5. A complete report of laboratory analyses of the ground water samples
collected from the monitoring wells during the June 2023 sampling event is included as Appendix E. A
summary of the current ground water analytical data is shown below:
Contaminant
of Concern
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
Xy
l
e
n
e
s
MT
B
E
Na
p
h
t
h
a
l
e
n
e
Well
ID
MACs (μg/l) 1 600 600 500 20 6
GCLs (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1A <0.180 <0.220 <0.170 <0.210 440 <0.470
MW-4A <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-6 70.7 968 26.5 J 1,100 671 <47.0
MW-10 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
AS-1 <0.180 1.36 <0.170 6.84 <0.140 <0.470
AS-2 <0.180 3.67 <0.170 3.13 <0.140 <0.470
AS-4 NS NS NS NS NS NS
WSW-3 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
WSW-11 <0.180 <0.220 <0.170 <0.210 0.559 J <0.470
Please note, the CAPs did not include a baseline contaminant mass calculation; therefore, calculating the
contaminant mass reduction has not been performed.
The site is in the Charlotte Belt Physiographic Province of North Carolina. The water table has a seasonal
high depth to water of approximately thirty-nine to forty-three feet BGS.
3.0 FREE PRODUCT REMOVAL
Free product has not historically been present at this site.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
No natural attenuation monitoring plan is currently in place at the site.
___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: July 21, 2023 The Corner Store
Project Manager: Joanna Alley, P.E. GRI Project No. 3992
5
5.0 CONCLUSIONS
On June 27, 2023, four Type II monitoring wells, three air sparge wells, and two water supply wells
were gauged, purged, and/or sampled. Air sparge well AS-4 could not be sampled due to the
presence of and unknown oil in the casing. Based on appearance and odor, the unknown oil is
assumed to be used cooking oil. Ground water flow was generally convergent towards MW-1A
with an average horizontal gradient of less than 0.01 feet per foot.
The concentrations of benzene, toluene, xylenes, MTBE, and/or 2-hexanone reported in the
ground water samples collected from MW-1A, MW-6, and AS-2 exceeded the MACs.
Concentrations of MTBE and/or acetone not exceeding the MACs were reported in the ground
water samples collected from water supply wells WSW-3 and WSW-11. All reported contaminant
concentrations were below the GCLs. Although the reported concentrations of 2-hexanone in the
ground water samples collected from MW-6 and AS-2 exceeded the MAC, this is not considered
a petroleum constituent. No free product was observed at the site.
Based on this information, the risk classification for the site should remain high risk. GRI
recommends the continued use of oxygen release compounds in site monitoring wells and semi-
annual ground water monitoring. The next sampling event is tentatively scheduled for December
2023.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Linda Beam for specific application to the
referenced site in Iredell County, North Carolina. The assessment was conducted based on the scope of
work and level of effort desired by the NCDEQ and with resources adequate only for that scope of work.
Our findings have been developed in accordance with generally accepted standards of environmental
practices in the State of North Carolina, available information, and our professional judgment. No other
warranty is expressed or implied.
The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
FIGURES
Copyright:© 2013 National Geographic Society, i-cubed
FIGURE 1
0 2,000 4,0001,000 Feet
SCALE: 1 INCH = 2,000 FEET
MAP CENTER LOCATIONLATITUDE: 35.607716° NLONGITUDE: 80.791846° W
`
SITE LOCATION
³
SITE LOCATION MAPTHE CORNER STORE896 OAKRIDGE FARM HIGHWAYMOORESVILLE, IREDELL COUNTY,NORTH CAROLINA INCIDENT NO. 15139GRI PROJECT NO. 3992
PREPARED BY:GEOLOGICAL RESOURCES, INC.JUNE 6, 2016
TABLES
UST ID Number A1 - A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 4 Facility ID Number
Owner or Operator?
Owner/Operator
Telephone Number
P.O. Box 304, Mooresville, NC 28115 (704) 663-4743
00-0-0000017677
Name of Owner or Operator Dates of Ownership / Operation
Randy Lynn Beam 10/01/1980 - 11/03/2000
Address
(704) 663-4743
00-0-0000017677
Name of Owner or Operator Dates of Ownership / Operation
Randy Lynn Beam 10/01/1983 - 11/03/2000
Address Telephone Number
Randy Lynn Beam 09/23/1982 - 01/16/1995
Address Telephone Number
P.O. Box 304, Mooresville, NC 28115 (704) 663-4743
TABLE 1
UST OWNER/OPERATOR INFORMATION
THE CORNER STORE (INCIDENT NO. 15139)
Name of Owner or Operator Dates of Ownership / Operation
00-0-0000017677
Name of Owner or Operator Dates of Ownership / Operation
Race City Exxon, Inc. 06/01/2001 - Present
Address Telephone Number
896 Oakridge Farm Road, Mooresville, NC 28115 (704) 799-3630
00-0-0000017677
P.O. Box 304, Mooresville, NC 28115
Page 1 of 1
Date: 06/17/19
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline NA 8,000 10/01/1983 Single Wall Steel 8' x 21.3' Other (Removed
11/03/2000)Yes
2 Gasoline NA 5,000 10/01/1983 Single Wall Steel 8' x 13.4' Other (Removed
11/03/2000)Yes
3 Gasoline NA 4,000 10/01/1983 Single Wall Steel 64" x 24' Other (Removed
11/03/2000)Yes
4 Gasoline NA 4,000 10/01/1980 Single Wall Steel 64" x 24' Other (Removed
11/03/2000)Yes
5 Kerosene NA 550 09/23/1982 Single Wall Steel 46" x 6.2' Single Wall Steel (Removed
01/16/1995)Yes
A1 Gasoline NA 12,000 06/01/2001 Single Wall
Steel/FRP 8' x 31.9' Other Current No
A2 Gasoline NA 6,000 06/01/2001 Single Wall
Steel/FRP 8' x 16' Other Current No
A3 Gasoline NA 6,000 06/01/2001 Single Wall
Steel/FRP 8' x 16' Other Current No
Tank
Dimensions
Description of
Associated
Product Piping
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
THE CORNER STORE (INCIDENT NO. 15139)
Facility ID #: 0-017677
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Facility ID # : 0-017677
Well ID.Parcel ID No.Well Owner Mailing Address Well Address Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municpal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Well Construction Details
(Depth, Screened Interval, Type of Well,
ect.)
Distance
from source
area of
release
(ft.)
WSW-1 4668703931 Race City Exxon, Inc.P.O. Box 28
Mooresville, NC 28115
896 Oakridge Farm Hwy
Mooresville, NC 28115 Abandoned N/A Yes Yes N/A N/A
WSW-2 4668703800 Diana Kim Welch 896 Mt Ulla Hwy
Mooresville, NC 28115
896 Mt Ulla Hwy
Mooresville, NC 28115 Inactive Non-Potable Yes Yes Unknown ~85' S
WSW-3 4668703648 Spencer P. Biondo, Reagan Pavlick 890 Mt Ulla Hwy
Mooresville, NC 28115
890 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~275' S
WSW-4 4668703519 Samuel & Nicole Occhiato 886 Mt Ulla Hwy
Mooresville, NC 28115
886 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~350' S
WSW-5 4668702570 Gilbert C. Sherrill 241 Timberland Loop
Mooresville, NC 28115
882 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~400' S
WSW-6 4668700277 Buck Mountain Creek, LLC 131 Keel Ct
Mooresville, NC 28117
105 Beam Drive
Mooresville, NC 28115 Abandoned N/A Yes No N/A N/A
WSW-7 4667791942 Drake 8 Properties, LLC 126 Fox Hollow Rd
Mooresville, NC 28117
108 Beam Drive
Mooresville, NC 28115 Destroyed N/A Yes No N/A N/A
WSW-8 4668609923 899 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~385' W
WSW-9 4668609728 889 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~470' W
WSW-10 4668609644 Dewayne A. & Melody T. Jones 9610 Hwy 152 West
Mooresville, NC 28115
881 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~615' SW
WSW-11 4668706812 Brawley Properties, RLLLP P.O. Box 4564
Mooresville, NC 28117
908 Oakridge Farm Hwy
Mooresville, NC 28115 Active Potable No No Unknown ~415' E
WSW-12 4668708672 All About You Holdings, LLC 208 Silverspring Pl
Mooresville, NC 28117
920 Oakridge Farm Hwy
Mooresville, NC 28115 Active Potable No No Unknown ~730' E
WSW-13 Destroyed N/A Yes Yes N/A N/A
WSW-14 Active Potable No No Unknown ~1,110' E
WSW-15 4668806703 Front Porch Dev, LLC 954 Oak Ridge Farm Hwy
Mooresville, NC 28115
954 Oakridge Farm Hwy
Mooresville, NC 28115 Active Potable No No Unknown ~1,425' E
WSW-16 4668810180 Belk Real Estate & Holdings, LLC 630 Belk Rd
Mt Ulla, NC 28125
933 Oakridge Farm Hwy
Mooresville, NC 28115 Active Potable No No Unknown ~1,130' E
WSW-17 4668818153 Jane Kennedy Mills 128 Pepaw Dr
Mooresville, NC 28115
128 Pepaw Drive
Mooresville, NC 28115 Active Potable Yes Yes Unknown >1,500' NE
WSW-18 4668810707 Frances E. Long 948 Mt Ulla Hwy
Mooresville, NC 28115
948 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~1,025' N
WSW-19 4668717509 Melba Long 938 Mt Ulla Hwy
Mooresville, NC 28115
938 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~850' N
WSW-20 4668715279 Rusher Oil Company P.O. Box 1483
Salisbury, NC 28145
932 Mt Ulla Hwy
Mooresville, NC 28115 Destroyed N/A Yes N/A N/A N/A
WSW-21 4668711687 Robert D. Nantz & Jean N. Walkup 951 Mt Ulla Hwy
Mooresville, NC 28115
915 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~475' NW
WSW-22 4668715279 Rusher Oil Company P.O. Box 1483
Salisbury, NC 28145
903 Oakridge Farm Hwy, Mooresville,
NC 28115 Destroyed N/A Yes Yes N/A N/A
WSW-23 4668616222 Ollie Enterprises, LLC 103 Essex Ct
Mooresville, NC 28117
863 Oakridge Farm Hwy, Mooresville,
NC 28115 Inactive Potable Yes Yes Unknown ~845' NW
WSW-24 4668604786 David A. Berg 711 N Main St
Mt Holly, NC 28120
844 Oakridge Farm Hwy, Mooresville,
NC 28115 Active Potable Yes No Unknown ~1,255' W
WSW-25 4668614251 Ollie Enterprises, LLC 103 Essex Ct
Mooresville, NC 28117
849 Oakridge Farm Hwy, Mooresville,
NC 28115 Active Potable Yes No Unknown ~1,210' W
WSW-26 4668711687 Robert D. Nantz & Jean N. Walkup 951 Mt Ulla Hwy
Mooresville, NC 28115
951 Mt Ulla Hwy
Mooresville, NC 28115 Active Potable Yes No Unknown ~1,100' N
Notes:
• Receptors are shown on Figure 3.
• n/a: not applicable.
• Receptors in gray have been removed from the Site Vicinity Map.
TABLE 3
RECEPTOR INFORMATION
THE CORNER STORE (INCIDENT NO. 15139)
Date: 07/20/23
4668801741 Arc Investments 928, LLC 111 Alexander Acres Rd
Mooresville, NC 28115
928 Oakridge Farm Hwy
Mooresville, NC 28115
MP Leasing, LLLP P.O. Box 28
Mooresville, NC 28115
Page 1 of 1
Date: 06/27/19 Facility ID # : 0-017677
Parcel Number Owner Name Owners Address
4668703931 (Site) Race City Exxon, Inc.P.O. Box 28
Mooresville, NC 28115
4668715279 Rusher Oil Company P.O. Box 1483
Salisbury, NC 28145
4668704893 Brawley Properties, RLLLP P.O. Box 4564
Mooresville, NC 28117
4668703800 Diana Kim Welch 896 Mt. Ulla Highway
Mooresville, NC 28115
4668609923 MP Leasing, LLLP P.O. Box 28
Mooresville, NC 28115
4668711687 Robert Nantz & Jean Walkup 951 Mt. Ulla Highway
Mooresville, NC 28115
Note:
• Properties are keyed to Figure 3.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
THE CORNER STORE (INCIDENT NO. 15139)
Page 1 of 1
Date: 07/13/23 Facility ID # : 0-017677
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Ground Water
Elevation
(ft.)
Comments
08/08/13 41.23 --- 58.27
03/24/14 42.08 --- 57.42
12/01/15 45.96 --- 53.54
05/18/16 42.98 --- 56.52
12/08/16 45.53 --- 53.97
06/21/17 46.52 --- 52.98
12/04/17 45.81 --- 53.69
07/17/18 44.98 --- 54.52
01/21/19 43.61 --- 55.89
07/08/19 39.59 --- 59.91
01/17/20 43.49 --- 56.01
07/29/20 40.05 --- 59.45
06/24/21 38.46 --- 61.04
01/27/22 43.12 --- 56.38
07/25/22 43.42 --- 56.08
06/27/23 42.59 --- 56.91
08/08/13 41.05 --- 59.14
03/24/14 40.37 --- 59.82
12/01/15 43.08 --- 57.11
07/25/22 NM --- NM Not found
04/26/12 NA --- NA
05/18/16 41.91 --- 56.62
12/08/16 Dry --- ---
07/25/22 NM --- NM Not found
08/08/13 42.18 --- 57.26
03/24/14 43.80 --- 55.64
12/01/15 46.19 --- 53.25
05/18/16 42.99 --- 56.45
12/08/16 45.74 --- 53.70
06/21/17 45.42 --- 54.02
12/04/17 45.97 --- 53.47
07/17/18 44.66 --- 54.78
01/21/19 42.67 --- 56.77
07/08/19 39.38 --- 60.06
01/17/20 42.68 --- 56.76
07/29/20 39.70 --- 59.74
06/24/21 38.31 --- 61.13
01/27/22 43.15 --- 56.29
07/25/22 43.54 --- 55.90
06/27/23 42.37 --- 57.07
03/24/14 40.32 --- 58.92
12/01/15 43.40 --- 55.84
07/25/22 39.53 --- 59.71
08/08/13 40.08 --- 60.00
03/24/14 41.98 --- 58.10
12/01/15 43.67 --- 56.41
05/18/16 40.61 --- 59.47
12/08/16 43.06 --- 57.02
06/21/17 44.28 --- 55.80
12/04/17 44.65 --- 55.43
07/17/18 42.53 --- 57.55
01/21/19 40.49 --- 59.59
07/08/19 36.82 --- 63.26
01/17/20 40.89 --- 59.19
07/29/20 36.22 --- 63.86
06/24/21 36.22 --- 63.86
01/27/22 38.98 --- 61.10
07/25/22 39.81 --- 60.27
06/27/23 42.46 --- 57.62
08/08/13 42.51 --- 56.02
03/24/14 43.09 --- 55.44
12/01/15 45.55 --- 52.98
05/18/16 41.98 --- 56.55
07/25/22 NM --- NM Not found
08/08/13 41.15 --- 58.48
03/24/14 43.26 --- 56.37
12/01/15 43.98 --- 55.65
05/18/16 40.41 --- 59.22
07/25/22 40.03 --- 59.60
08/08/13 41.98 --- 57.27
03/24/14 40.95 --- 58.30
12/01/15 45.78 --- 53.47
07/25/22 43.48 --- 55.77
MW-1A 02/11/03 40 40 - 55 55
5540 - 55
MW-6
4002/11/03MW-9
MW-8 40 - 554002/11/03 55 99.63
99.25
100.08
05/31/02MW-7
(1-inch well)39.5
55
11/21/01 35 35 - 45 45
39.505/31/02MW-5A
(1-Inch well)
MW-4A 01/28/02 40 40 - 55
100.19
99.50
54.539.5 - 54.5
30 - 45 45
99.24
99.44
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
THE CORNER STORE (INCIDENT NO. 15139)
5040 - 5040 98.5304/30/01MW-3A
MW-2 03/20/95 30
98.5354.539.5 - 54.5
Page 1 of 2
Date: 07/13/23 Facility ID # : 0-017677
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Ground Water
Elevation
(ft.)
Comments
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
THE CORNER STORE (INCIDENT NO. 15139)
05/18/16 42.69 --- 56.16
12/08/16 45.11 --- 53.74
06/21/17 44.79 --- 54.06
12/04/17 45.36 --- 53.49
07/17/18 44.05 --- 54.80
01/21/19 43.43 --- 55.42
07/08/19 38.79 --- 60.06
01/17/20 42.06 --- 56.79
07/29/20 39.11 --- 59.74
06/24/21 37.69 --- 61.16
01/27/22 42.48 --- 56.37
07/25/22 42.98 --- 55.87
06/27/23 41.78 --- 57.07
01/27/22 40.01 --- NM
07/25/22 40.96 --- NM
06/27/23 39.02 --- NM
01/27/22 37.58 --- NM
07/25/22 28.67 --- NM
06/27/23 36.03 --- NM
01/27/22 43.17 --- NM
07/25/22 43.85 --- NM
06/27/23 42.04 41.97*** NM See notes
08/08/13 42.50 --- 56.91
12/01/15 45.91 --- 53.50
05/18/16 42.90 --- 56.51
07/25/22 43.41 --- 56.00
Notes:
• Well construction information and gauging data prior to 2015 from the Remediation Monitoring Report dated April 1, 2014,
prepared by Irminger Consulting, Inc..
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] +
[free product thickness x 0.8581].
• *** : An unknown oil was present in AS-4 during the 06/27/23 sampling event. Based on appearance and odor, the oil did not appear to be petroleum and is
suspected to be used cooking oil
• ft BGS : feet below ground surface.
• NA: Not available.
• NM: Not measured.
AS-1 Unknown
AS-2 Unknown
AS-4 Unknown
MW-10 05/18/16 35 35 - 55 55
05/26/95VE-1 6058 - 6058
Unknown
Unknown Unknown 56.07
Unknown 57.6
Unknown 55.32
Unknown
98.85
Unknown Unknown
Unknown
99.41
Page 2 of 2
Date: 07/13/23 Facility ID # : 0-017677
Well ID Date Measured
(mm/dd/yy)
Dissolved Oxygen
(mg/l)
Temperature
( C° )Comments
09/14/16 1.56 18.25 O-SOXs Installed
12/08/16 20.51 15.67
06/21/17 9.83 18.88
12/04/17 NM NM
07/17/18 21.04 NM
01/21/19 9.40 NM
07/08/19 20.07 NM
01/17/20 36.69 14.50
07/29/20 9.52 NM
06/08/21 6.23 NM
01/27/22 9.70 NM
07/25/22 5.25 NM
06/27/23 NM NM O-Sox Replaced
09/14/16 1.75 19.98
12/08/16 NM MN
09/14/16 NM NM
12/08/16 NM NM
09/14/16 3.89 17.43
12/08/16 2.95 15.10
06/21/17 4.92 17.48
12/04/17 NM NM
07/17/18 6.40 NM
01/21/19 6.45 NM
07/08/19 4.26 NM
01/17/20 5.15 14.50
07/29/20 4.38 NM
06/08/21 6.46 NM
01/27/22 3.02 NM
07/25/22 4.41 NM
09/14/16 NM NM
12/08/16 NM NM
09/14/16 1.62 19.12 O-SOXs Installed
12/08/16 10.32 17.56
06/21/17 5.95 19.85
12/04/17 NM NM
07/17/18 11.88 NM
01/21/19 6.17 NM
07/08/19 10.18 NM
01/17/20 16.89 16.30
07/29/20 8.10 NM
06/08/21 6.77 NM
01/27/22 2.78 NM
07/25/22 2.76 NM
06/27/23 NM NM O-Sox Stuck in well;
could not dislodge
09/14/16 NM NM
12/08/16 NM NM
09/14/16 NM NM
12/08/16 NM NM
09/14/16 NM NM
12/08/16 NM NM
09/14/16 3.95 17.42
12/08/16 4.31 15.04
06/21/17 4.16 17.43
12/04/17 NM NM
07/17/18 6.72 NM
01/21/19 4.40 NM
07/08/19 2.14 NM
01/17/20 4.48 14.40
07/29/20 5.02 NM
06/08/21 4.83 NM
01/27/22 4.07 NM
07/25/22 2.02 NM
01/27/22 16.07 NM
07/25/22 3.00 NM
06/27/23 NM NM O-Sox Replaced
01/27/22 14.41 NM
07/25/22 2.72 NM
06/27/23 NM NM O-Sox Stuck in well;
could not dislodge
01/27/22 15.92 NM
07/25/22 5.41 NM
06/27/23 NM NM Canister Missing
09/14/16 NM NM
12/08/16 NM NM
Notes:
• Oxygen release material EHC-O in the form of socks were placed in air sparging wells AS-1
through AS-4, monitoring wells MW-1A and MW-6 on September 14, 2016.
Socks have been replaced semi-annually since September 2016.
• Dissolved oxygen readings made before purging well.
• NM: Not measured.
MW-1A
AS-1
AS-2
MW-6
AS-4
MW-8
TABLE 6
GROUND WATER DISSOLVED OXYGEN INFORMATION
THE CORNER STORE (INCIDENT NO. 15139)
VE-1
Oxygen release
material in well
Oxygen release
material in well
MW-7
(1-inch well)
MW-5A
(1-Inch well)
MW-4A
Oxygen release
material in well
MW-10
MW-9
MW-3A
MW-2
Oxygen release
material in well
Oxygen release
material in well
Page 1 of 1
Date: 07/13/23 Facility ID # : 0-017677
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 3 0.02 0.4 40 5 0.2 0.7 3 400 400
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 14,750 3,000 50 400 40,000 5,000 200 700 3,000 28,500 24,100
02/12/03 20 ND 1.8 3.8 1.1 ND *************
02/19/04 <1.0 <1.0 <1.0 <2.0 24 NA *************
11/09/04 ND ND ND ND 140 NA *************
02/20/07 ND ND ND ND 290 NA *************
06/30/09 <1.0 <1.0 <1.0 <1.0 49.1 NA *************
12/11/09 <1.0 <1.0 <1.0 <2.0 <1.0 NA *************
09/01/10 <1.0 <1.0 <1.0 <2.0 40.1 NA *************
03/19/11 <1.0 <1.0 <1.0 <2.0 238 <1.0 *************
09/20/11 <1.0 <1.0 <1.0 <2.0 372 <1.0 *************
04/26/12 <1.0 <1.0 <1.0 <2.0 620 <1.0 *************
01/10/13 <1.0 <1.0 <1.0 <2.0 733 <2.0 *************
08/08/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
03/24/14 <5.0 <5.0 <5.0 <15.0 1,260 <10.0 *************
12/01/15 <8.6 <8.3 <7.6 <22 1,610 <6.1 *************
05/18/16 <1.3 <1.3 <1.3 <3.1 1,100 <1.3 *************
12/08/16 <1.3 <1.3 <1.3 <3.1 1,770 <1.3 *************
06/21/17 <1.3 <1.3 <1.3 <2.5 1,270 <1.3 *************
12/04/17 <6.3 <6.3 <6.3 <13 1,320 <6.3 **<6.3 <10 <6.3 <6.3 *<50 <6.3 <6.3 <6.3 <6.3 <6.3
07/17/18 <3.1 <3.1 <3.1 <6.2 1,150 <3.1 **<3.1 8.4 J <3.1 <3.1 *<25 <3.1 <3.1 <3.1 <3.1 <3.1
01/21/19 <0.27 <0.29 <0.20 <0.16 573 <0.10 **<0.16 <0.066 <0.24 <0.12 *<0.080 <0.12 <0.22 <0.18 <0.15 <0.16
07/08/19 <1.3 <1.3 <1.3 <2.5 844 <1.3 **<1.3 <2.0 <1.3 <1.3 *<10 <1.3 <1.3 <1.3 <1.3 <1.3
01/17/20 <2.5 <2.5 <2.5 <5.0 611 <2.5 **<2.5 <4.0 <2.5 <2.5 *<20 <2.5 <2.5 <2.5 <2.5 <2.5
07/29/20 <2.5 <2.5 <2.5 <5.0 666 <2.5 **<2.5 <4.0 <2.5 <2.5 *<20 <2.5 20.8 17.6 <2.5 <2.5
06/24/21 <1.3 <1.3 <1.3 <2.6 247 <1.3 **<1.3 ****28.7 B ***<1.3 <1.3
01/27/22 <0.13 <0.13 <0.13 <0.25 632 0.14 J 11.9 428 <0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 1.8 0.77
07/25/22 <0.13 <0.13 <0.13 <1.5 501 <0.13 NR NR 0.17 J 1.9 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 0.79 0.37 J
06/27/23 <0.180 <0.220 <0.170 <0.210 440 <0.470 NR NR <0.920 <0.220 <0.200 <0.150 <0.380 <0.330 <0.160 <0.220 <0.180 <0.190 <0.180
02/20/07 ND ND ND ND ND NA *************
12/22/09 <1.0 <1.0 <1.0 <1.0 <1.0 NA *************
09/01/10 NA NA NA NA NA NA *************
11/15/10 <1.0 142 <1.0 1.3 <1.0 34 *************
03/19/11 <1.0 4.2 <1.0 1.2 <1.0 28.6 *************
09/20/11 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
04/26/12
01/10/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
08/08/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
12/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 *************
07/25/22 NS NS NS NS NS NS *************
01/10/13 NS NS NS NS NS NS *************
12/01/15 NS NS NS NS NS NS *************
05/18/16 <0.13 1.4 <0.13 <0.31 <0.13 <0.13 *************
07/25/22 NS NS NS NS NS NS *************
02/20/07 ND ND ND ND ND NA *************
06/30/09 <1.0 <1.0 <1.0 <1.0 <1.0 NA *************
12/11/09 <1.0 <1.0 <1.0 <2.0 24 NA *************
09/01/10 <1.0 <1.0 <1.0 <2.0 <1.0 NA *************
03/19/11 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
09/20/11 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
04/26/12 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
01/10/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
08/08/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
12/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 *************
05/18/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 *************
12/08/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 *************
06/21/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 *************
12/04/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/17/18 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
01/21/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 **<0.16 <0.066 <0.24 <0.12 *<0.080 <0.12 <0.22 <0.18 <0.15 <0.16
07/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
01/17/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/29/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/24/21 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
01/27/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/25/22 <0.13 <0.13 <0.13 <1.5 <0.13 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/27/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.920 <0.220 <0.200 <0.150 <0.380 <0.330 <0.160 <0.220 <0.180 <0.190 <0.180
02/20/07 ND ND ND ND ND NA *************
12/22/09 <1.0 <1.0 <1.0 <2.0 <1.0 NA *************
09/01/10 NS NS NS NS NS NS *************
03/19/11 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
09/20/11 NS NS NS NS NS NS *************
04/26/12 <1.0 <1.0 <1.0 <2.0 1.7 <1.0 *************
01/01/13 <1.0 <1.0 <1.0 <2.0 1.7 <2.0 *************
12/01/15 <0.17 <0.17 <0.15 <0.43 0.34 J <0.12 *************
07/25/22 <0.13 <0.13 <0.13 <1.5 11.5 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
05/31/02 9,000 31,000 1,200 16,800 8,300 NA *************
02/11/03 4,600 8,700 <1,000 8,900 10,000 NA *************
02/19/04 4,100 13,000 <1,000 20,300 33,000 NA *************
11/09/04 4,700 17,000 <1,000 22,000 41,000 NA *************
02/20/07 3,700 13,000 ND 19,600 36,000 NA *************
12/22/09 12.0 90.4 16.3 887 247 163 *************
09/01/10 6.1 46.7 <5.0 473 267 56.7 *************
03/28/11 11.9 96.5 8.6 825 570 134 *************
09/20/11 NS NS NS NS NS NS *************
04/26/12
01/10/13 <1.0 2.6 <1.0 20.2 2.4 7.4 *************
08/08/13 1.6 5.2 <1.0 25.1 4.1 7.2 *************
03/24/14 1.8 <1.0 <1.0 33.2 6.7 10.3 *************
12/01/15 8.6 35.8 4.0 69.1 25.7 12.1 *************
05/18/16 18.5 36.2 10.7 151 89.1 21.7 *************
12/08/16 7.5 22.4 4.6 60 98.4 9.0 *************
06/21/17 2.0 17 1.7 22.4 94.7 3.0 *************
12/04/17 2.8 22.6 2.0 30.7 114 2.9 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 15.0 9.8
07/17/18 1.5 6.9 0.62 10.8 71.2 2.2 **<0.13 1.3 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 5.3 4.7
01/21/19 1.7 7.5 0.95 19.4 157 3.7 **<0.16 <0.066 <0.24 <0.12 *<0.080 <0.12 <0.22 <0.18 8.6 9.3
07/08/19 2.9 11.4 1.9 J 24.8 114 6.7 **<0.63 <1.0 <0.63 <0.63 *<5.0 <0.63 <0.63 <0.63 11.2 14.5
01/17/20 7.2 J 8.0 J 4.6 J 46.3 512 12.9 **<2.5 5.8 J <2.5 <2.5 *<20 <2.5 <2.5 <2.5 17.6 32.7
07/29/20 97.1 1,240 85.4 1,230 1,680 361 **<2.5 <4.0 <2.5 <2.5 *<20 <2.5 <2.5 <2.5 255 147
06/24/21 221 6,040 229 4,710 1,930 861 **224 ****418 B ***1,130 434
01/27/22 244 4,950 284 3,950 2,210 994 321 <10 <0.63 3.7 5.4 1.8 J *<5.0 <0.63 <0.63 <0.63 1,060 553
07/25/22 151 2,800 E 180 2,880 2,000 827 NR NR <6.3 11.1 4.3 <6.3 NR 65.4 J 17.4 <6.3 <6.3 817 399
06/27/23 70.7 968 26.5 J 1,100 671 <47.0 NR NR <92.0 <22.0 <20.0 <15.0 68.5 J <33.0 <16.0 <22.0 <18.0 177 196
02/11/03 ND ND ND ND ND NA *************
02/19/04 <1.0 <1.0 <1.0 <2.0 <1.0 NA *************
11/09/04 ND ND ND ND ND NA *************
02/20/07 ND ND ND ND ND NA *************
04/26/12 ND ND ND ND ND NA *************
01/10/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
08/08/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
12/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 *************
05/18/16 <0.13 1.4 0.73 4.4 <0.13 9.9 B *************
07/25/22 NS NS NS NS NS NS *************
02/12/03 ND ND ND ND 1.3 NA *************
02/19/04 <1.0 <1.0 <1.0 <2.0 1.5 NA *************
11/09/04 ND ND ND ND ND NA *************
02/20/07 ND ND ND ND ND NA *************
06/30/09 <1.0 <1.0 <1.0 <1.0 <1.0 NA *************
12/11/09 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
09/01/10 NS NS NS NS NS NS *************
03/19/11 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
09/20/11 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
04/26/12 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
01/10/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
08/08/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
12/01/15 <0.17 <0.17 <0.15 <0.43 0.35 J <0.12 *************
05/18/16 <0.13 <0.13 <0.13 <0.31 0.29 J <0.13 *************
07/25/22 <0.13 <0.13 <0.13 <1.5 9.7 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
2-
H
e
x
a
n
o
n
e
Dry
Dry
1,
3
,
5
-
T
r
i
m
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t
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y
l
b
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n
z
e
n
e
1,
1
,
2
,
2
-
T
e
t
r
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t
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a
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Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
(P
C
E
)
MAC (µg/l)
GCL (µg/l)
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
(T
C
E
)
1,
2
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4
-
T
r
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Me
t
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l
c
h
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(C
h
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t
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a
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)
1,
2
-
D
i
c
h
l
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t
h
a
n
e
1,
2
-
D
i
b
r
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m
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t
h
a
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e
(E
D
B
)
te
r
t
-
B
u
t
y
l
a
l
c
o
h
o
l
(T
B
A
)
te
r
t
-
B
u
t
y
l
b
e
n
z
e
n
e
Contaminant of Concern
→
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
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e
To
t
a
l
X
y
l
e
n
e
s
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l
e
t
h
e
r
(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
Analytical Method →EPA Method 6200B
Me
t
h
y
l
e
n
e
C
h
l
o
r
i
d
e
TABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
THE CORNER STORE (INCIDENT NO. 15139)
te
r
t
-
A
m
y
l
a
l
c
o
h
o
l
(T
A
A
)
MW-8
MW-7
MW-5A
MW-3A
MW-2
MW-4A
MW-6
MW-1A
MW-4A
(cont.)
MW-6
(cont.)
Page 1 of 2
Date: 07/13/23 Facility ID # : 0-017677
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 3 0.02 0.4 40 5 0.2 0.7 3 400 400
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 14,750 3,000 50 400 40,000 5,000 200 700 3,000 28,500 24,100
2-
H
e
x
a
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o
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1,
3
,
5
-
T
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m
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t
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b
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z
e
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e
1,
1
,
2
,
2
-
T
e
t
r
a
c
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l
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o
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t
h
a
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e
Te
t
r
a
c
h
l
o
r
o
e
t
h
e
n
e
(P
C
E
)
MAC (µg/l)
GCL (µg/l)
Tr
i
c
h
l
o
r
o
e
t
h
e
n
e
(T
C
E
)
1,
2
,
4
-
T
r
i
m
e
t
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y
l
b
e
n
z
e
n
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Me
t
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y
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c
h
l
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r
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e
(C
h
l
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m
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t
h
a
n
e
)
1,
2
-
D
i
c
h
l
o
r
o
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t
h
a
n
e
1,
2
-
D
i
b
r
o
m
o
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t
h
a
n
e
(E
D
B
)
te
r
t
-
B
u
t
y
l
a
l
c
o
h
o
l
(T
B
A
)
te
r
t
-
B
u
t
y
l
b
e
n
z
e
n
e
Contaminant of Concern
→
Be
n
z
e
n
e
To
l
u
e
n
e
Et
h
y
l
b
e
n
z
e
n
e
To
t
a
l
X
y
l
e
n
e
s
Me
t
h
y
l
-
t
e
r
t
-
b
u
t
y
l
e
t
h
e
r
(M
T
B
E
)
Na
p
h
t
h
a
l
e
n
e
Analytical Method →EPA Method 6200B
Me
t
h
y
l
e
n
e
C
h
l
o
r
i
d
e
TABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
THE CORNER STORE (INCIDENT NO. 15139)
te
r
t
-
A
m
y
l
a
l
c
o
h
o
l
(T
A
A
)
02/19/04 <1.0 <1.0 <1.0 <2.0 <1.0 NA *************
11/09/04 ND ND ND ND 1.5 NA *************
02/20/07 ND ND ND ND 4.3 NA *************
12/22/09 <1.0 <1.0 <1.0 <2.0 2.5 <1.0 *************
09/01/10 NS NS NS NS NS NS *************
03/19/11 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 *************
09/20/11 <1.0 <1.0 <1.0 <2.0 2.8 <1.0 *************
04/26/12 <1.0 <1.0 <1.0 <2.0 6.8 <1.0 *************
01/10/13 <1.0 <1.0 <1.0 <2.0 2.1 <2.0 *************
08/08/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
12/01/15 <0.17 <0.17 <0.15 <0.43 1.9 <0.12 *************
07/25/22 <0.13 <0.13 <0.13 <1.5 3.2 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
05/18/16 <0.13 <0.13 <0.13 <0.31 7.3 <0.13 *************
12/08/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 *************
06/21/17 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 *************
12/04/17 <0.13 <0.13 <0.13 <0.25 <0.13 0.59 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/17/18 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
01/21/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 **<0.16 <0.066 <0.24 <0.12 *<0.080 <0.12 <0.22 <0.18 <0.15 <0.16
07/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
01/17/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/29/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/24/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
01/27/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/25/22 <0.13 <0.13 <0.13 <1.5 <0.13 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/27/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.920 <0.220 <0.200 <0.150 <0.380 <0.330 <0.160 <0.220 <0.180 <0.190 <0.180
01/27/22 0.22 J <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/25/22 <0.13 <0.13 <0.13 <1.5 <0.13 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/27/23 <0.180 1.36 <0.170 6.84 <0.140 <0.470 NR NR <0.920 <0.220 <0.200 <0.150 21.3 <0.330 <0.160 <0.220 <0.180 2.79 2.02
01/27/22 <0.13 44.9 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 0.77 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/25/22 <0.13 108 <0.13 <1.5 <0.13 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR 6.5 JB <0.13 <0.13 <0.13 <0.13 <0.13
06/27/23 <0.180 3.67 <0.170 3.13 <0.140 <0.470 NR NR <0.920 <0.220 <0.200 <0.150 52.5 <0.330 <0.160 <0.220 <0.180 1.90 1.61
01/27/22 0.20 J <0.13 <0.13 <0.25 634 <0.13 <2.0 <2.0 <0.13 0.27 J <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/25/22 <0.13 <0.13 <0.13 <1.5 48.6 <0.13 NR NR <0.13 0.44 J <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/27/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/19/04 <1.0 <1.0 <1.0 <2.0 <1.0 NA *************
11/09/04 ND ND ND ND ND NA *************
02/20/07 2.9 ND ND ND 4.3 NA *************
06/30/09 <1.0 <1.0 <1.0 <2.0 <1.0 NA *************
09/01/10 NS NS NS NS NS NS *************
03/19/11 NS NS NS NS NS NS *************
09/20/11 NS NS NS NS NS NS *************
04/26/12 <1.0 <1.0 <1.0 <2.0 <1.0 NA *************
01/10/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
12/01/15 <0.17 <0.17 <0.15 <0.43 54.8 E <0.12 *************
05/18/16 <0.13 <0.13 <0.13 <0.31 68.3 E <0.13 *************
07/25/22 <0.13 <0.13 <0.13 <1.5 1,500 <0.13 NR NR <0.13 7.0 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
08/08/13 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
03/24/14 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
12/01/15 7.5 <0.17 <0.15 0.46 J <0.16 <0.12 *************
06/21/17 124 <0.13 <0.13 11.9 <0.13 2.5 *************
12/04/17 40.5 <0.13 <0.13 4.4 <0.13 0.67 **<0.13 <0.20 <0.13 4.5 *<1.0 <0.13 <0.13 <0.13 1.3 <0.13
07/17/18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/18/16 1.3 <0.13 <0.13 <0.31 <0.13 <0.13 *************
12/08/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 *************
06/21/17 3.5 <0.13 <0.13 0.28 J <0.13 <0.13 *************
08/28/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <1.0 ***<0.13 <0.13
12/04/17 0.22 J <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 0.84 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/17/18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/14 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0 *************
12/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 *************
05/18/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 *************
12/04/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/17/18 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
01/21/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
01/17/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/29/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/24/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/27/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/25/22 <0.13 <0.13 <0.13 <1.5 <0.13 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/27/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.920 <0.220 <0.200 <0.150 <0.380 <0.330 <0.160 <0.220 <0.180 <0.190 <0.180
05/18/16 <0.13 <0.13 <0.13 <0.31 0.18 J <0.13 *************
12/04/17 <0.13 <0.13 <0.13 <0.25 0.29 J <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/17/18 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 0.14 J <0.13 <0.13 <0.13
01/21/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/08/19 <0.13 <0.13 <0.13 <0.25 0.47 J <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 0.29 J <0.13 <0.13 <0.13
01/17/20 <0.13 <0.13 <0.13 <0.25 0.70 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 0.32 J <0.13 <0.13 <0.13
07/29/20 <0.13 <0.13 <0.13 <0.25 0.28 J <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 0.20 J <0.13 <0.13 <0.13
06/24/21 <0.13 <0.13 <0.13 <0.25 0.61 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 0.20 J <0.13 <0.13 <0.13
01/27/22 <0.13 <0.13 <0.13 <0.25 1.0 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 0.31 J <0.13 <0.13 <0.13
07/25/22 <0.13 <0.13 <0.13 <1.5 0.84 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/27/23 <0.180 <0.220 <0.170 <0.210 0.559 J <0.470 NR NR <0.920 <0.220 <0.200 <0.150 <0.380 <0.330 <0.160 <0.220 <0.180 <0.190 <0.180
12/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 *************
05/18/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 *************
06/21/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 *************
12/04/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/17/18 <0.13 <0.13 <0.13 <0.26 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
01/21/19 <0.27 <0.29 <0.20 <0.16 <0.068 <0.10 **<0.16 <0.066 <0.24 <0.12 *0.13 J <0.12 <0.22 <0.18 <0.15 <0.16
07/08/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/29/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/24/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 **<0.13 <0.20 <0.13 <0.13 *1.3 J <0.13 <0.13 <0.13 <0.13 <0.13
01/27/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <2.0 <2.0 <0.13 <0.20 <0.13 <0.13 *<1.0 <0.13 <0.13 <0.13 <0.13 <0.13
07/25/22 <0.13 <0.13 <0.13 <1.5 <0.13 <0.13 NR NR <0.13 <0.20 <0.13 <0.13 NR <1.0 <0.13 <0.13 <0.13 <0.13 <0.13
06/27/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 NR NR <0.920 <0.220 <0.200 <0.150 <0.380 <0.330 <0.160 <0.220 <0.180 <0.190 <0.180
Notes:
• Analytical results from 2014 and earlier from Remediation Monitoring Report dated April 1, 2014
by Irminger Consulting, Inc.
• *: Concentrations prior to the initial detection in a water supply well have not been updated.
• < : Less than the method detection limit specified in the laboratory report.
• NR: Not Requested; ND: Not Detected; NS: Not Sampled, NA: Not available.
• J: Estimated value.
• E: Value exceeds calibration range.
• B: Indicates analyte found in associated method blank.
• Concentrations in bold exceeded the MACs.
• Concentrations in italics exceeded the GCLs.
• Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no standard has been established.
• Other reported compounds above the MAC: 05/18/16 - 1,2-dichloroethane in WSW-2; 06/21/17 - 1,2-dichloroethane in WSW-2 (Before GAC) and
WSW-2 (After GAC); 12/04/17 - 1,2-dichloroethane in WSW-2 (Before GAC) and WSW-2 (After GAC); 07/17/18 - methyl chloride in MW-1A;
1/17/20 - methyl chloride in MW-6; 07/29/20 - tetrachloroethene and trichloroethene in MW-1A.
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum allowable concentrations as specified in T15A NCAC 2L.0202.
• GCL : Gross contamination level.
• FP : Free product.
WSW-3
WSW-11
Trip Blank
WSW-2
(Before
GAC)
WSW-2
(After GAC)
VE-1
MW-9
MW-10
AS-1
AS-2
AS-4
Page 2 of 2
APPENDICES
APPENDIX A
State Correspondence
April 27, 2023
Linda BeamP.O. Box 304
Mooresville, NC 28115(Via Email)
Re: Acknowledgement of Report Receipt
Corner Store
896 Oak Ridge Farm Road
Mooresville, Iredell County
Incident Number: 15139
Risk Classification: High
Ranking: H-250-D
Dear Ms. Beam:
The UST Section, Division of Waste Management, is in receipt of the report dated September
13, 2022. The report has been reviewed and will be maintained in the Mooresville Regional Office.
The UST Section agrees with the recommendations presented in the report. Please update the
receptor survey since the last one was completed in 2002. In addition to the receptor survey please continue to use oxygen release compounds in site monitoring wells and conduct semi-annual ground
water monitoring.
If you have questions regarding the information contained in this letter, please contact me at Ryan.Mills@ncdenr.gov or at 704-235-2175.
Sincerely,
Ryan C. Mills
Hydrogeologist
Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ
cc: Joanna Alley, P.E., Geological Engineers, Inc. (Via Email)
Site Name City / County /Iredell Incident #15139
Resp Pty Name / Contact Incident Mgr Region MOR
(Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #46
Consultant / Project Mgr Joanna R. Alley
Telephone / Fax Number Task Authorization Number:47 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:H-250-D RRA Date:8/27/2018
Proposal# / Scope Dates % Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.
3r
d
P
t
y
D
e
d
?
Task #Lab /
SubCode RO
A
u
t
h
Proposed
Rate/Price
(Consultant)CO
A
u
t
h
Proposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
1.025 1 /site Y $740.00 Y $740.00 $740.00 /
2.281 5 /socks Y $30.00 Y $150.00 $150.00 /
2.290 5 /socks Y $135.00 Y $675.00 $675.00 /
4.031 7 /wells Y $110.00 Y $770.00 $770.00 /
4.041 1 /well Y $75.00 Y $75.00 $75.00 /
y 4.045 1 /well Y $75.00 Y $75.00 $75.00 /
4.090 #272 9 /samples Y $66.00 Y $594.00 $594.00 /
4.091 1 /shipment Y $60.00 Y $60.00 $60.00 /y 4.095 #272 1 /sample Y $66.00 Y $66.00 $66.00 /
6.090 1 /report Y $1,125.00 Y $1,125.00 $1,125.00 /
12.050 1 /trip Y $250.00 Y $250.00 $250.00 /
12.055 1 /trip Y $50.00 Y $50.00 $50.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed
TOTAL:$4,630.00 $4,630.00 TOTAL:
Total Standard Costs (Not Third Party)$4,489.00 $4,489.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $141.00 $141.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:6/2/23 by:(PM)(Reserved for RO)
RO Review:6/5/23 by:(IM)Joint UST Preapproval Confirmed By:
CO Review:6/5/23 by:(STF)RP or Designee Receipt Confirmation By:
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
DWM/UST ePATA 4/1/2022
DIRECTED COSTS
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request
designated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the priorePATAform for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion date of the FIRST completed task to remain withintheStatuteof Limitations.All ePATAs submittedwithin aclaim are closed with thatclaim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
RCM
LP
(Initials)
JRA
Proposed
Units / Type
(Consultant)
Ryan Mills
ActiveYES
23-279 June-July 2023
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
100.00%
No
JRA@geologicalresourcesinc.com
Linda Beam
Geological Resources, Inc.
Dept of Environmental Quality -Division of Waste Management
6/5/2023
06/06/23
3992 Received JUN 06 2023
APPENDIX B
Land Use Information
Date: 07/14/23 Facility ID # : 00-0-0000017677
Map ID No. Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
n/a R2 Residential n/a n/a
n/a R3 Residential n/a n/a
n/a R5 Residential n/a n/a
n/a RG Residential General n/a n/a
n/a RLS Residential Limited
Service n/a n/a
n/a RLI Residential Low-
Intensity n/a n/a
n/a HB Highway Business n/a n/a
n/a CC Community Commercial n/a n/a
Note:
• Properties are keyed to Figure 3B.
APPENDIX B
LAND USE INFORMATION
THE CORNER STORE (INCIDENT NO. 15139)
Page 1 of 1
APPENDIX C
Incident Reports
NCDEQ Incident Report
RP/Company CP WAGS NORTH CAROLINA, LLC
RPAddress 6230 RIVER CHASE CIRCLE
RPCity ATLANTA
Contact GERAARD GUNTHERT
RPState GA
TELEPHONE
IncidentNumber 40553 USTNum MO-9067
IncidentName OAKRIDGE FARM HIGHWAY PROPERTY
FacilID
Address 893,899,903 OAKRIDGE FARM HWY
CityTown MOORESVILLE State NC
ZipCode 28115-
DateOccurred 10/29/2015
DateReported 11/25/2015
ConfRisk L
CloseOut 12/17/2015
COMMENT
RptType Rcvd Rvwd Appvd
Incident Mgr DSGLongitude-80.791656 Latitude 35.608500
County IREDE
CLO 11/25/2015 12/17/2015
Thursday, July 13, 2023 Page 1 of 1
NCDEQ Incident Report
RP/Company CORNER STORE
RPAddress 312 EAST GRAY STREET
RPCity MOORESVILLE
Contact LINDA BEAM
RPState NC
TELEPHONE 7046634743
IncidentNumber 15139 USTNum MO-4537
IncidentName CORNER STORE
FacilID 00-0-0000017677
Address 896 OAK RIDGE FARM HWY
CityTown MOORESVILLE State NC
ZipCode 28115-
DateOccurred 12/14/1994
DateReported 12/14/1994
ConfRisk H
CloseOut
COMMENT
EVALUATE SOIL SAMPLE RESULTS AND CONSIDER SYS SHUTDOWN AND GW MON FOR CLOSURE SYS SHUTDOWN
DUE TO UST EXCAVATION RELATED TO INC# 22782 PLUMES FOR TWO INCIDENTS COMINGLED ADD SYS
OPERATION/MONITORING PENDING REQ FOR INC#22782 As of November 2009 System has been running for 1
quarter and all constituents below 2L
April 2014
The system has been operating sufficiently, and the latest report indicates that only two wells exhibit violations of 15A
NCAC 2L.
RptType Rcvd Rvwd Appvd
Incident Mgr RCMLongitude-80.792014 Latitude 35.607842
County IREDE
CSA 12/20/1995 2/23/1996
CAP 10/11/1996 4/15/1997
RMR 5/3/2000
RMR 9/8/2000
Thursday, July 13, 2023 Page 1 of 4
RMR 5/18/2001
RMR 6/25/2002
CAP 3/8/2004 8/5/2004
RMR 1/7/2005
MRP 3/28/2007 4/10/2007 4/10/2007
RMRI 10/20/2009 10/23/2009 10/27/2009
RMR 10/20/2009 10/23/2009 10/27/2009
First quarter report
RMR 1/21/2010 1/26/2010 1/26/2010
RMRI 10/14/2010 10/15/2010 10/25/2010
RMR 5/30/2012 6/5/2012 6/7/2012
Thursday, July 13, 2023 Page 2 of 4
RMR 9/16/2013 9/23/2013
RMR 4/29/2014 4/28/2014
RMR 12/31/2015 1/5/2016
OTH 1/29/2016 1/29/2016
RMR 6/27/2016 7/7/2016
RMR 1/9/2017
RMR 7/19/2017 7/26/2017
RMR 12/28/2017 1/4/2018
RMR 8/10/2018 8/15/2018
RMR 2/22/2019 2/28/2019
Thursday, July 13, 2023 Page 3 of 4
RMR 2/10/2020 2/12/2020 2/14/2020
RMR 8/19/2020 8/20/2020
RMR 9/3/2021
RMR 2/28/2022 3/7/2022
RMR 9/14/2022 12/1/2022 12/1/2022
On July 25, 2022, seven monitoring wells, three air sparge wells, one vapor
extraction well, and two water supply wells were sampled. No free product
was observed at the site. The concentrations of benzene, toluene, xylenes,
MTBE, naphthalene, methyl chloride, EDB, methylene chloride, 1,1,2,2-
tetrachloroethane, and/or 1,2,4-trimethylbenzene reported in the ground
water samples collected from MW-1A, MW-6, AS-2, AS-4, and VE-1
exceeded the MACs. A concentration of MTBE not exceeding the MACs was
reported in the ground water sample collected from water supply well
WSW-11. All reported contaminant concentrations were below the GCLs.
Based on this information, the risk classification for the site should remain
high risk. GRI recommends the updating the receptor survey information
(last updated in 2002). In addition to the receptor survey update, GRI
recommends the continued use of oxygen release compounds in site
monitoring wells and semi-annual ground water monitoring.
Thursday, July 13, 2023 Page 4 of 4
APPENDIX D
Historical Soil Quality Information
APPENDIX E
Laboratory Analytical Report
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
7/10/2023
Geological Resources, Inc. Joanna Alley
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-178-0016 Client Project Description: The Corner Store
GRI #3992
Dear Joanna Alley:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/27/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 56
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-178-0016
Page 2 of 56
Report Number:
Sample Summary Table
Client Project Description:
23-178-0016
The Corner Store
GRI #3992
Lab No Client Sample ID Matrix Date Collected Date Received
06/27/2023 08:26Aqueous 99372 MW-1A 06/27/2023 14:00
06/27/2023 08:55Aqueous 99373 MW-4A 06/27/2023 14:00
06/27/2023 07:57Aqueous 99374 MW-6 06/27/2023 14:00
06/27/2023 08:41Aqueous 99375 MW-10 06/27/2023 14:00
06/27/2023 07:32Aqueous 99376 AS-1 06/27/2023 14:00
06/27/2023 07:50Aqueous 99377 AS-2 06/27/2023 14:00
06/27/2023 09:15Aqueous 99378 WSW-3 06/27/2023 14:00
06/27/2023 09:05Aqueous 99379 WSW-11 06/27/2023 14:00
06/27/2023 06:30Aqueous 99380 Trip Blank 06/27/2023 14:00
Page 3 of 56
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-178-0016
Report Limit
Project:The Corner Store
V 99372MW-1A
J4.89 07/06/2023 06:476200BAcetoneµg/L 1.80
2.77 07/06/2023 06:476200BDi-Isopropyl Ether (DIPE)µg/L 0.500
440 07/07/2023 01:506200BMethyl tert-butyl ether (MTBE)µg/L 1.40
V 99374MW-6
J35507/06/2023 10:556200BAcetoneµg/L 180
70.7 07/06/2023 10:556200BBenzeneµg/L 18.0
J26.5 07/06/2023 10:556200BEthylbenzeneµg/L 17.0
J68.5 07/06/2023 10:556200B2-Hexanone µg/L 38.0
J10507/06/2023 10:556200BMethyl Ethyl Ketone (MEK)µg/L 71.0
671 07/06/2023 10:556200BMethyl tert-butyl ether (MTBE)µg/L 14.0
968 07/06/2023 10:556200BTolueneµg/L 22.0
177 07/06/2023 10:556200B1,2,4-Trimethylbenzene µg/L 19.0
196 07/06/2023 10:556200B1,3,5-Trimethylbenzene µg/L 18.0
725 07/06/2023 10:556200Bo-Xylene µg/L 21.0
371 07/06/2023 10:556200Bm,p-Xylene µg/L 42.0
1100 07/06/2023 10:556200BXylene (Total)µg/L 21.0
V 99376AS-1
J9.55 07/06/2023 20:476200BAcetoneµg/L 1.80
21.3 07/06/2023 20:476200B2-Hexanone µg/L 0.380
1.36 07/06/2023 20:476200BTolueneµg/L 0.220
2.79 07/06/2023 20:476200B1,2,4-Trimethylbenzene µg/L 0.190
2.02 07/06/2023 20:476200B1,3,5-Trimethylbenzene µg/L 0.180
3.80 07/06/2023 20:476200Bo-Xylene µg/L 0.210
3.04 07/06/2023 20:476200Bm,p-Xylene µg/L 0.420
6.84 07/06/2023 20:476200BXylene (Total)µg/L 0.210
V 99377AS-2
J8.88 07/06/2023 21:156200BAcetoneµg/L 1.80
52.5 07/06/2023 21:156200B2-Hexanone µg/L 0.380
J1.75 07/06/2023 21:156200BMethyl Ethyl Ketone (MEK)µg/L 0.710
3.67 07/06/2023 21:156200BTolueneµg/L 0.220
1.90 07/06/2023 21:156200B1,2,4-Trimethylbenzene µg/L 0.190
1.61 07/06/2023 21:156200B1,3,5-Trimethylbenzene µg/L 0.180
1.76 07/06/2023 21:156200Bo-Xylene µg/L 0.210
1.37 07/06/2023 21:156200Bm,p-Xylene µg/L 0.420
3.13 07/06/2023 21:156200BXylene (Total)µg/L 0.210
Page 4 of 56
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-178-0016
Report Limit
Project:The Corner Store
V 99378WSW-3
11.1 07/06/2023 08:106200BAcetoneµg/L 1.80
V 99379WSW-11
J1.89 07/06/2023 08:386200BAcetoneµg/L 1.80
J0.559 07/06/2023 08:386200BMethyl tert-butyl ether (MTBE)µg/L 0.140
Page 5 of 56
Client: Geological Resources, Inc. CASE NARRATIVE
Project: The Corner Store Lab Report Number: 23-178-0016
Date: 7/7/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: Ethanol QC Batch No: V35083/V35033
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 6 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-1A
99372 Matrix:
6/27/2023 8:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00 V35074 07/06/23 09:00
4.89 J µg/L 1.80 10.0Acetone 1 07/06/23 06:47 V35034MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/06/23 06:47 V35034MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/06/23 06:47 V35034MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/06/23 06:47 V35034MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/06/23 06:47 V35034MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/06/23 06:47 V35034MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 07/06/23 06:47 V35034MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/06/23 06:47 V35034MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/06/23 06:47 V35034MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/06/23 06:47 V35034MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/06/23 06:47 V35034MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/06/23 06:47 V35034MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/06/23 06:47 V35034MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/06/23 06:47 V35034MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/06/23 06:47 V35034MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/06/23 06:47 V35034MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/06/23 06:47 V35034MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/06/23 06:47 V35034MSA
2.77 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/06/23 06:47 V35034MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/06/23 06:47 V35034MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/06/23 06:47 V35034MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/06/23 06:47 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-1A
99372 Matrix:
6/27/2023 8:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00 V35074 07/06/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/06/23 06:47 V35034MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/06/23 06:47 V35034MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/06/23 06:47 V35034MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/06/23 06:47 V35034MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/06/23 06:47 V35034MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/06/23 06:47 V35034MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/06/23 06:47 V35034MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/06/23 06:47 V35034MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/06/23 06:47 V35034MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/06/23 06:47 V35034MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/06/23 06:47 V35034MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/06/23 06:47 V35034MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/06/23 06:47 V35034MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/06/23 06:47 V35034MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/06/23 06:47 V35034MSA
<42.0 µg/L 42.0 200Ethanol 1 07/06/23 06:47 V35034MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/06/23 06:47 V35034MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/06/23 06:47 V35034MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 07/06/23 06:47 V35034MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/06/23 06:47 V35034MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/06/23 06:47 V35034MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/06/23 06:47 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-1A
99372 Matrix:
6/27/2023 8:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00 V35074 07/06/23 09:00
440 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 07/07/23 01:50 V35083ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/06/23 06:47 V35034MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/06/23 06:47 V35034MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 07/06/23 06:47 V35034MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/06/23 06:47 V35034MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/06/23 06:47 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/06/23 06:47 V35034MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/06/23 06:47 V35034MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/06/23 06:47 V35034MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/06/23 06:47 V35034MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/06/23 06:47 V35034MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/06/23 06:47 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/06/23 06:47 V35034MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/06/23 06:47 V35034MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/06/23 06:47 V35034MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/06/23 06:47 V35034MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/06/23 06:47 V35034MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/06/23 06:47 V35034MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/06/23 06:47 V35034MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/06/23 06:47 V35034MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/06/23 06:47 V35034MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/06/23 06:47 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-1A
99372 Matrix:
6/27/2023 8:26
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00 V35074 07/06/23 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/06/23 06:47 V35034MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/06/23 06:47 V35034
Surrogate: 4-Bromofluorobenzene 95.0 Limits: 70-130%07/06/23 06:471 MSA V35034
Surrogate: Dibromofluoromethane 96.6 Limits: 70-130%07/06/23 06:471 MSA V35034
Surrogate: 1,2-Dichloroethane - d4 94.0 Limits: 70-130%07/06/23 06:471 MSA V35034
Surrogate: Toluene-d8 94.2 Limits: 70-130%07/06/23 06:471 MSA V35034
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%07/07/23 01:5010 ENM V35083
Surrogate: Dibromofluoromethane 96.2 Limits: 70-130%07/07/23 01:5010 ENM V35083
Surrogate: 1,2-Dichloroethane - d4 92.4 Limits: 70-130%07/07/23 01:5010 ENM V35083
Surrogate: Toluene-d8 94.4 Limits: 70-130%07/07/23 01:5010 ENM V35083
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-4A
99373 Matrix:
6/27/2023 8:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 07/06/23 07:15 V35034MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/06/23 07:15 V35034MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/06/23 07:15 V35034MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/06/23 07:15 V35034MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/06/23 07:15 V35034MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/06/23 07:15 V35034MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 07/06/23 07:15 V35034MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/06/23 07:15 V35034MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/06/23 07:15 V35034MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/06/23 07:15 V35034MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/06/23 07:15 V35034MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/06/23 07:15 V35034MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/06/23 07:15 V35034MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/06/23 07:15 V35034MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/06/23 07:15 V35034MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/06/23 07:15 V35034MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/06/23 07:15 V35034MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/06/23 07:15 V35034MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/06/23 07:15 V35034MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/06/23 07:15 V35034MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/06/23 07:15 V35034MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/06/23 07:15 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-4A
99373 Matrix:
6/27/2023 8:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/06/23 07:15 V35034MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/06/23 07:15 V35034MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/06/23 07:15 V35034MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/06/23 07:15 V35034MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/06/23 07:15 V35034MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/06/23 07:15 V35034MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/06/23 07:15 V35034MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/06/23 07:15 V35034MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/06/23 07:15 V35034MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/06/23 07:15 V35034MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/06/23 07:15 V35034MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/06/23 07:15 V35034MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/06/23 07:15 V35034MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/06/23 07:15 V35034MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/06/23 07:15 V35034MSA
<42.0 µg/L 42.0 200Ethanol 1 07/06/23 07:15 V35034MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/06/23 07:15 V35034MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/06/23 07:15 V35034MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 07/06/23 07:15 V35034MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/06/23 07:15 V35034MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/06/23 07:15 V35034MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/06/23 07:15 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-4A
99373 Matrix:
6/27/2023 8:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/06/23 07:15 V35034MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/06/23 07:15 V35034MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/06/23 07:15 V35034MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 07/06/23 07:15 V35034MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/06/23 07:15 V35034MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/06/23 07:15 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/06/23 07:15 V35034MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/06/23 07:15 V35034MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/06/23 07:15 V35034MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/06/23 07:15 V35034MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/06/23 07:15 V35034MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/06/23 07:15 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/06/23 07:15 V35034MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/06/23 07:15 V35034MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/06/23 07:15 V35034MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/06/23 07:15 V35034MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/06/23 07:15 V35034MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/06/23 07:15 V35034MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/06/23 07:15 V35034MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/06/23 07:15 V35034MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/06/23 07:15 V35034MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/06/23 07:15 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-4A
99373 Matrix:
6/27/2023 8:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/06/23 07:15 V35034MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/06/23 07:15 V35034
Surrogate: 4-Bromofluorobenzene 94.2 Limits: 70-130%07/06/23 07:151 MSA V35034
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%07/06/23 07:151 MSA V35034
Surrogate: 1,2-Dichloroethane - d4 93.6 Limits: 70-130%07/06/23 07:151 MSA V35034
Surrogate: Toluene-d8 93.8 Limits: 70-130%07/06/23 07:151 MSA V35034
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-6
99374 Matrix:
6/27/2023 7:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
355 J µg/L 180 1000Acetone 100 07/06/23 10:55 V35034MSA
70.7 µg/L 18.0 50.0Benzene 100 07/06/23 10:55 V35034MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 07/06/23 10:55 V35034MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 07/06/23 10:55 V35034MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 07/06/23 10:55 V35034MSA
<150 µg/L 150 500Bromoform 100 07/06/23 10:55 V35034MSA
<28.0 µg/L 28.0 100Bromomethane 100 07/06/23 10:55 V35034MSA
<18.0 µg/L 18.0 50.0n-Butylbenzene 100 07/06/23 10:55 V35034MSA
<20.0 µg/L 20.0 50.0sec-Butyl benzene 100 07/06/23 10:55 V35034MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 07/06/23 10:55 V35034MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 07/06/23 10:55 V35034MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 07/06/23 10:55 V35034MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 07/06/23 10:55 V35034MSA
<43.0 µg/L 43.0 100Chloroethane 100 07/06/23 10:55 V35034MSA
<22.0 µg/L 22.0 50.0Chloroform 100 07/06/23 10:55 V35034MSA
<22.0 µg/L 22.0 50.0Chloromethane 100 07/06/23 10:55 V35034MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 07/06/23 10:55 V35034MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 07/06/23 10:55 V35034MSA
<50.0 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 07/06/23 10:55 V35034MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 07/06/23 10:55 V35034MSA
<20.0 µg/L 20.0 50.01,2-Dibromoethane 100 07/06/23 10:55 V35034MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 07/06/23 10:55 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-6
99374 Matrix:
6/27/2023 7:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 07/06/23 10:55 V35034MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 07/06/23 10:55 V35034MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 07/06/23 10:55 V35034MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 07/06/23 10:55 V35034MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 07/06/23 10:55 V35034MSA
<15.0 µg/L 15.0 50.01,2-Dichloroethane 100 07/06/23 10:55 V35034MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 07/06/23 10:55 V35034MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 07/06/23 10:55 V35034MSA
<18.0 µg/L 18.0 50.0trans-1,2-Dichloroethene 100 07/06/23 10:55 V35034MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 07/06/23 10:55 V35034MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 07/06/23 10:55 V35034MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 07/06/23 10:55 V35034MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 07/06/23 10:55 V35034MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 07/06/23 10:55 V35034MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 07/06/23 10:55 V35034MSA
<4200 µg/L 4200 20000Ethanol 100 07/06/23 10:55 V35034MSA
26.5 J µg/L 17.0 50.0Ethylbenzene 100 07/06/23 10:55 V35034MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 07/06/23 10:55 V35034MSA
68.5 J µg/L 38.0 1002-Hexanone 100 07/06/23 10:55 V35034MSA
<18.0 µg/L 18.0 50.0Isopropylbenzene 100 07/06/23 10:55 V35034MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 07/06/23 10:55 V35034MSA
105 J µg/L 71.0 500Methyl Ethyl Ketone (MEK)100 07/06/23 10:55 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-6
99374 Matrix:
6/27/2023 7:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
671 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 07/06/23 10:55 V35034MSA
<7.80 µg/L 7.80 1004-Methyl-2-Pentanone 100 07/06/23 10:55 V35034MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 07/06/23 10:55 V35034MSA
<47.0 µg/L 47.0 100Naphthalene 100 07/06/23 10:55 V35034MSA
<19.0 µg/L 19.0 50.0n-Propylbenzene 100 07/06/23 10:55 V35034MSA
<22.0 µg/L 22.0 50.0Styrene 100 07/06/23 10:55 V35034MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 07/06/23 10:55 V35034MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 07/06/23 10:55 V35034MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 07/06/23 10:55 V35034MSA
968 µg/L 22.0 50.0Toluene 100 07/06/23 10:55 V35034MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 07/06/23 10:55 V35034MSA
<31.0 µg/L 31.0 50.01,2,4-Trichlorobenzene 100 07/06/23 10:55 V35034MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 07/06/23 10:55 V35034MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 07/06/23 10:55 V35034MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 07/06/23 10:55 V35034MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 07/06/23 10:55 V35034MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 07/06/23 10:55 V35034MSA
177 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 07/06/23 10:55 V35034MSA
196 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 07/06/23 10:55 V35034MSA
<100 µg/L 100 500Vinyl Acetate 100 07/06/23 10:55 V35034MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 07/06/23 10:55 V35034MSA
725 µg/L 21.0 50.0o-Xylene 100 07/06/23 10:55 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-6
99374 Matrix:
6/27/2023 7:57
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
371 µg/L 42.0 100m,p-Xylene 100 07/06/23 10:55 V35034MSA
1100 µg/L 21.0 50.0Xylene (Total)100 07/06/23 10:55 V35034
Surrogate: 4-Bromofluorobenzene 93.2 Limits: 70-130%07/06/23 10:55100 MSA V35034
Surrogate: Dibromofluoromethane 99.2 Limits: 70-130%07/06/23 10:55100 MSA V35034
Surrogate: 1,2-Dichloroethane - d4 94.6 Limits: 70-130%07/06/23 10:55100 MSA V35034
Surrogate: Toluene-d8 94.8 Limits: 70-130%07/06/23 10:55100 MSA V35034
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-10
99375 Matrix:
6/27/2023 8:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 07/06/23 07:42 V35034MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/06/23 07:42 V35034MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/06/23 07:42 V35034MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/06/23 07:42 V35034MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/06/23 07:42 V35034MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/06/23 07:42 V35034MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 07/06/23 07:42 V35034MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/06/23 07:42 V35034MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/06/23 07:42 V35034MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/06/23 07:42 V35034MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/06/23 07:42 V35034MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/06/23 07:42 V35034MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/06/23 07:42 V35034MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/06/23 07:42 V35034MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/06/23 07:42 V35034MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/06/23 07:42 V35034MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/06/23 07:42 V35034MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/06/23 07:42 V35034MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/06/23 07:42 V35034MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/06/23 07:42 V35034MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/06/23 07:42 V35034MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/06/23 07:42 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-10
99375 Matrix:
6/27/2023 8:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/06/23 07:42 V35034MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/06/23 07:42 V35034MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/06/23 07:42 V35034MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/06/23 07:42 V35034MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/06/23 07:42 V35034MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/06/23 07:42 V35034MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/06/23 07:42 V35034MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/06/23 07:42 V35034MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/06/23 07:42 V35034MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/06/23 07:42 V35034MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/06/23 07:42 V35034MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/06/23 07:42 V35034MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/06/23 07:42 V35034MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/06/23 07:42 V35034MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/06/23 07:42 V35034MSA
<42.0 µg/L 42.0 200Ethanol 1 07/06/23 07:42 V35034MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/06/23 07:42 V35034MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/06/23 07:42 V35034MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 07/06/23 07:42 V35034MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/06/23 07:42 V35034MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/06/23 07:42 V35034MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/06/23 07:42 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-10
99375 Matrix:
6/27/2023 8:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/06/23 07:42 V35034MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/06/23 07:42 V35034MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/06/23 07:42 V35034MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 07/06/23 07:42 V35034MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/06/23 07:42 V35034MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/06/23 07:42 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/06/23 07:42 V35034MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/06/23 07:42 V35034MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/06/23 07:42 V35034MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/06/23 07:42 V35034MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/06/23 07:42 V35034MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/06/23 07:42 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/06/23 07:42 V35034MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/06/23 07:42 V35034MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/06/23 07:42 V35034MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/06/23 07:42 V35034MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/06/23 07:42 V35034MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/06/23 07:42 V35034MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/06/23 07:42 V35034MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/06/23 07:42 V35034MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/06/23 07:42 V35034MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/06/23 07:42 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:MW-10
99375 Matrix:
6/27/2023 8:41
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/06/23 07:42 V35034MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/06/23 07:42 V35034
Surrogate: 4-Bromofluorobenzene 93.8 Limits: 70-130%07/06/23 07:421 MSA V35034
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%07/06/23 07:421 MSA V35034
Surrogate: 1,2-Dichloroethane - d4 92.8 Limits: 70-130%07/06/23 07:421 MSA V35034
Surrogate: Toluene-d8 93.8 Limits: 70-130%07/06/23 07:421 MSA V35034
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:AS-1
99376 Matrix:
6/27/2023 7:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35074 07/06/23 09:00
9.55 J µg/L 1.80 10.0Acetone 1 07/06/23 20:47 V35083ENM
<0.180 µg/L 0.180 0.500Benzene 1 07/06/23 20:47 V35083ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/06/23 20:47 V35083ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/06/23 20:47 V35083ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/06/23 20:47 V35083ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/06/23 20:47 V35083ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/06/23 20:47 V35083ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/06/23 20:47 V35083ENM
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/06/23 20:47 V35083ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/06/23 20:47 V35083ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/06/23 20:47 V35083ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/06/23 20:47 V35083ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/06/23 20:47 V35083ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/06/23 20:47 V35083ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/06/23 20:47 V35083ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 07/06/23 20:47 V35083ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/06/23 20:47 V35083ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/06/23 20:47 V35083ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/06/23 20:47 V35083ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/06/23 20:47 V35083ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/06/23 20:47 V35083ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/06/23 20:47 V35083ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:AS-1
99376 Matrix:
6/27/2023 7:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35074 07/06/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/06/23 20:47 V35083ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/06/23 20:47 V35083ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/06/23 20:47 V35083ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/06/23 20:47 V35083ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/06/23 20:47 V35083ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/06/23 20:47 V35083ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/06/23 20:47 V35083ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/06/23 20:47 V35083ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/06/23 20:47 V35083ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/06/23 20:47 V35083ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/06/23 20:47 V35083ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/06/23 20:47 V35083ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/06/23 20:47 V35083ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/06/23 20:47 V35083ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/06/23 20:47 V35083ENM
<42.0 µg/L 42.0 200Ethanol 1 07/06/23 20:47 V35083ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/06/23 20:47 V35083ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/06/23 20:47 V35083ENM
21.3 µg/L 0.380 1.002-Hexanone 1 07/06/23 20:47 V35083ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/06/23 20:47 V35083ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/06/23 20:47 V35083ENM
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/06/23 20:47 V35083ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:AS-1
99376 Matrix:
6/27/2023 7:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35074 07/06/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/06/23 20:47 V35083ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/06/23 20:47 V35083ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/06/23 20:47 V35083ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 07/06/23 20:47 V35083ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/06/23 20:47 V35083ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/06/23 20:47 V35083ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/06/23 20:47 V35083ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/06/23 20:47 V35083ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/06/23 20:47 V35083ENM
1.36 µg/L 0.220 0.500Toluene 1 07/06/23 20:47 V35083ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/06/23 20:47 V35083ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/06/23 20:47 V35083ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/06/23 20:47 V35083ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/06/23 20:47 V35083ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/06/23 20:47 V35083ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/06/23 20:47 V35083ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/06/23 20:47 V35083ENM
2.79 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/06/23 20:47 V35083ENM
2.02 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/06/23 20:47 V35083ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/06/23 20:47 V35083ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/06/23 20:47 V35083ENM
3.80 µg/L 0.210 0.500o-Xylene 1 07/06/23 20:47 V35083ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:AS-1
99376 Matrix:
6/27/2023 7:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35074 07/06/23 09:00
3.04 µg/L 0.420 1.00m,p-Xylene 1 07/06/23 20:47 V35083ENM
6.84 µg/L 0.210 0.500Xylene (Total)1 07/06/23 20:47 V35083
Surrogate: 4-Bromofluorobenzene 93.2 Limits: 70-130%07/06/23 20:471 ENM V35083
Surrogate: Dibromofluoromethane 96.4 Limits: 70-130%07/06/23 20:471 ENM V35083
Surrogate: 1,2-Dichloroethane - d4 93.2 Limits: 70-130%07/06/23 20:471 ENM V35083
Surrogate: Toluene-d8 94.8 Limits: 70-130%07/06/23 20:471 ENM V35083
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:AS-2
99377 Matrix:
6/27/2023 7:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35074 07/06/23 09:00
8.88 J µg/L 1.80 10.0Acetone 1 07/06/23 21:15 V35083ENM
<0.180 µg/L 0.180 0.500Benzene 1 07/06/23 21:15 V35083ENM
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/06/23 21:15 V35083ENM
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/06/23 21:15 V35083ENM
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/06/23 21:15 V35083ENM
<1.50 µg/L 1.50 5.00Bromoform 1 07/06/23 21:15 V35083ENM
<0.280 µg/L 0.280 1.00Bromomethane 1 07/06/23 21:15 V35083ENM
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/06/23 21:15 V35083ENM
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/06/23 21:15 V35083ENM
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/06/23 21:15 V35083ENM
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/06/23 21:15 V35083ENM
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/06/23 21:15 V35083ENM
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/06/23 21:15 V35083ENM
<0.430 µg/L 0.430 1.00Chloroethane 1 07/06/23 21:15 V35083ENM
<0.220 µg/L 0.220 0.500Chloroform 1 07/06/23 21:15 V35083ENM
<0.220 µg/L 0.220 0.500Chloromethane 1 07/06/23 21:15 V35083ENM
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/06/23 21:15 V35083ENM
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/06/23 21:15 V35083ENM
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/06/23 21:15 V35083ENM
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/06/23 21:15 V35083ENM
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/06/23 21:15 V35083ENM
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/06/23 21:15 V35083ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:AS-2
99377 Matrix:
6/27/2023 7:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35074 07/06/23 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/06/23 21:15 V35083ENM
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/06/23 21:15 V35083ENM
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/06/23 21:15 V35083ENM
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/06/23 21:15 V35083ENM
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/06/23 21:15 V35083ENM
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/06/23 21:15 V35083ENM
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/06/23 21:15 V35083ENM
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/06/23 21:15 V35083ENM
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/06/23 21:15 V35083ENM
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/06/23 21:15 V35083ENM
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/06/23 21:15 V35083ENM
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/06/23 21:15 V35083ENM
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/06/23 21:15 V35083ENM
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/06/23 21:15 V35083ENM
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/06/23 21:15 V35083ENM
<42.0 µg/L 42.0 200Ethanol 1 07/06/23 21:15 V35083ENM
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/06/23 21:15 V35083ENM
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/06/23 21:15 V35083ENM
52.5 µg/L 0.380 1.002-Hexanone 1 07/06/23 21:15 V35083ENM
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/06/23 21:15 V35083ENM
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/06/23 21:15 V35083ENM
1.75 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/06/23 21:15 V35083ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:AS-2
99377 Matrix:
6/27/2023 7:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35074 07/06/23 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/06/23 21:15 V35083ENM
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/06/23 21:15 V35083ENM
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/06/23 21:15 V35083ENM
<0.470 µg/L 0.470 1.00Naphthalene 1 07/06/23 21:15 V35083ENM
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/06/23 21:15 V35083ENM
<0.220 µg/L 0.220 0.500Styrene 1 07/06/23 21:15 V35083ENM
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/06/23 21:15 V35083ENM
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/06/23 21:15 V35083ENM
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/06/23 21:15 V35083ENM
3.67 µg/L 0.220 0.500Toluene 1 07/06/23 21:15 V35083ENM
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/06/23 21:15 V35083ENM
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/06/23 21:15 V35083ENM
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/06/23 21:15 V35083ENM
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/06/23 21:15 V35083ENM
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/06/23 21:15 V35083ENM
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/06/23 21:15 V35083ENM
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/06/23 21:15 V35083ENM
1.90 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/06/23 21:15 V35083ENM
1.61 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/06/23 21:15 V35083ENM
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/06/23 21:15 V35083ENM
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/06/23 21:15 V35083ENM
1.76 µg/L 0.210 0.500o-Xylene 1 07/06/23 21:15 V35083ENM
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:AS-2
99377 Matrix:
6/27/2023 7:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35074 07/06/23 09:00
1.37 µg/L 0.420 1.00m,p-Xylene 1 07/06/23 21:15 V35083ENM
3.13 µg/L 0.210 0.500Xylene (Total)1 07/06/23 21:15 V35083
Surrogate: 4-Bromofluorobenzene 92.6 Limits: 70-130%07/06/23 21:151 ENM V35083
Surrogate: Dibromofluoromethane 97.6 Limits: 70-130%07/06/23 21:151 ENM V35083
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%07/06/23 21:151 ENM V35083
Surrogate: Toluene-d8 94.0 Limits: 70-130%07/06/23 21:151 ENM V35083
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:WSW-3
99378 Matrix:
6/27/2023 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
11.1 µg/L 1.80 10.0Acetone 1 07/06/23 08:10 V35034MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/06/23 08:10 V35034MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/06/23 08:10 V35034MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/06/23 08:10 V35034MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/06/23 08:10 V35034MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/06/23 08:10 V35034MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 07/06/23 08:10 V35034MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/06/23 08:10 V35034MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/06/23 08:10 V35034MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/06/23 08:10 V35034MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/06/23 08:10 V35034MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/06/23 08:10 V35034MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/06/23 08:10 V35034MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/06/23 08:10 V35034MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/06/23 08:10 V35034MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/06/23 08:10 V35034MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/06/23 08:10 V35034MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/06/23 08:10 V35034MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/06/23 08:10 V35034MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/06/23 08:10 V35034MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/06/23 08:10 V35034MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/06/23 08:10 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:WSW-3
99378 Matrix:
6/27/2023 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/06/23 08:10 V35034MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/06/23 08:10 V35034MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/06/23 08:10 V35034MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/06/23 08:10 V35034MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/06/23 08:10 V35034MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/06/23 08:10 V35034MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/06/23 08:10 V35034MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/06/23 08:10 V35034MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/06/23 08:10 V35034MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/06/23 08:10 V35034MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/06/23 08:10 V35034MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/06/23 08:10 V35034MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/06/23 08:10 V35034MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/06/23 08:10 V35034MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/06/23 08:10 V35034MSA
<42.0 µg/L 42.0 200Ethanol 1 07/06/23 08:10 V35034MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/06/23 08:10 V35034MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/06/23 08:10 V35034MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 07/06/23 08:10 V35034MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/06/23 08:10 V35034MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/06/23 08:10 V35034MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/06/23 08:10 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:WSW-3
99378 Matrix:
6/27/2023 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/06/23 08:10 V35034MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/06/23 08:10 V35034MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/06/23 08:10 V35034MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 07/06/23 08:10 V35034MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/06/23 08:10 V35034MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/06/23 08:10 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/06/23 08:10 V35034MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/06/23 08:10 V35034MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/06/23 08:10 V35034MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/06/23 08:10 V35034MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/06/23 08:10 V35034MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/06/23 08:10 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/06/23 08:10 V35034MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/06/23 08:10 V35034MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/06/23 08:10 V35034MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/06/23 08:10 V35034MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/06/23 08:10 V35034MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/06/23 08:10 V35034MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/06/23 08:10 V35034MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/06/23 08:10 V35034MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/06/23 08:10 V35034MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/06/23 08:10 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:WSW-3
99378 Matrix:
6/27/2023 9:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/06/23 08:10 V35034MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/06/23 08:10 V35034
Surrogate: 4-Bromofluorobenzene 93.6 Limits: 70-130%07/06/23 08:101 MSA V35034
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%07/06/23 08:101 MSA V35034
Surrogate: 1,2-Dichloroethane - d4 93.0 Limits: 70-130%07/06/23 08:101 MSA V35034
Surrogate: Toluene-d8 93.8 Limits: 70-130%07/06/23 08:101 MSA V35034
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:WSW-11
99379 Matrix:
6/27/2023 9:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
1.89 J µg/L 1.80 10.0Acetone 1 07/06/23 08:38 V35034MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/06/23 08:38 V35034MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/06/23 08:38 V35034MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/06/23 08:38 V35034MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/06/23 08:38 V35034MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/06/23 08:38 V35034MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 07/06/23 08:38 V35034MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/06/23 08:38 V35034MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/06/23 08:38 V35034MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/06/23 08:38 V35034MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/06/23 08:38 V35034MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/06/23 08:38 V35034MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/06/23 08:38 V35034MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/06/23 08:38 V35034MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/06/23 08:38 V35034MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/06/23 08:38 V35034MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/06/23 08:38 V35034MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/06/23 08:38 V35034MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/06/23 08:38 V35034MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/06/23 08:38 V35034MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/06/23 08:38 V35034MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/06/23 08:38 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:WSW-11
99379 Matrix:
6/27/2023 9:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/06/23 08:38 V35034MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/06/23 08:38 V35034MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/06/23 08:38 V35034MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/06/23 08:38 V35034MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/06/23 08:38 V35034MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/06/23 08:38 V35034MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/06/23 08:38 V35034MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/06/23 08:38 V35034MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/06/23 08:38 V35034MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/06/23 08:38 V35034MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/06/23 08:38 V35034MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/06/23 08:38 V35034MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/06/23 08:38 V35034MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/06/23 08:38 V35034MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/06/23 08:38 V35034MSA
<42.0 µg/L 42.0 200Ethanol 1 07/06/23 08:38 V35034MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/06/23 08:38 V35034MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/06/23 08:38 V35034MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 07/06/23 08:38 V35034MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/06/23 08:38 V35034MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/06/23 08:38 V35034MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/06/23 08:38 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:WSW-11
99379 Matrix:
6/27/2023 9:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
0.559 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/06/23 08:38 V35034MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/06/23 08:38 V35034MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/06/23 08:38 V35034MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 07/06/23 08:38 V35034MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/06/23 08:38 V35034MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/06/23 08:38 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/06/23 08:38 V35034MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/06/23 08:38 V35034MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/06/23 08:38 V35034MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/06/23 08:38 V35034MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/06/23 08:38 V35034MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/06/23 08:38 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/06/23 08:38 V35034MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/06/23 08:38 V35034MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/06/23 08:38 V35034MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/06/23 08:38 V35034MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/06/23 08:38 V35034MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/06/23 08:38 V35034MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/06/23 08:38 V35034MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/06/23 08:38 V35034MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/06/23 08:38 V35034MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/06/23 08:38 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:WSW-11
99379 Matrix:
6/27/2023 9:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/06/23 08:38 V35034MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/06/23 08:38 V35034
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%07/06/23 08:381 MSA V35034
Surrogate: Dibromofluoromethane 96.6 Limits: 70-130%07/06/23 08:381 MSA V35034
Surrogate: 1,2-Dichloroethane - d4 93.0 Limits: 70-130%07/06/23 08:381 MSA V35034
Surrogate: Toluene-d8 94.0 Limits: 70-130%07/06/23 08:381 MSA V35034
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:Trip Blank
99380 Matrix:
6/27/2023 6:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 07/06/23 05:25 V35034MSA
<0.180 µg/L 0.180 0.500Benzene 1 07/06/23 05:25 V35034MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/06/23 05:25 V35034MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/06/23 05:25 V35034MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/06/23 05:25 V35034MSA
<1.50 µg/L 1.50 5.00Bromoform 1 07/06/23 05:25 V35034MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 07/06/23 05:25 V35034MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/06/23 05:25 V35034MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 07/06/23 05:25 V35034MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/06/23 05:25 V35034MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/06/23 05:25 V35034MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/06/23 05:25 V35034MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/06/23 05:25 V35034MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 07/06/23 05:25 V35034MSA
<0.220 µg/L 0.220 0.500Chloroform 1 07/06/23 05:25 V35034MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 07/06/23 05:25 V35034MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/06/23 05:25 V35034MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/06/23 05:25 V35034MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/06/23 05:25 V35034MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/06/23 05:25 V35034MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/06/23 05:25 V35034MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/06/23 05:25 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:Trip Blank
99380 Matrix:
6/27/2023 6:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/06/23 05:25 V35034MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/06/23 05:25 V35034MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/06/23 05:25 V35034MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/06/23 05:25 V35034MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/06/23 05:25 V35034MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/06/23 05:25 V35034MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/06/23 05:25 V35034MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/06/23 05:25 V35034MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/06/23 05:25 V35034MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/06/23 05:25 V35034MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/06/23 05:25 V35034MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/06/23 05:25 V35034MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/06/23 05:25 V35034MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/06/23 05:25 V35034MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/06/23 05:25 V35034MSA
<42.0 µg/L 42.0 200Ethanol 1 07/06/23 05:25 V35034MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/06/23 05:25 V35034MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/06/23 05:25 V35034MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 07/06/23 05:25 V35034MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/06/23 05:25 V35034MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/06/23 05:25 V35034MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/06/23 05:25 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:Trip Blank
99380 Matrix:
6/27/2023 6:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/06/23 05:25 V35034MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/06/23 05:25 V35034MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/06/23 05:25 V35034MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 07/06/23 05:25 V35034MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/06/23 05:25 V35034MSA
<0.220 µg/L 0.220 0.500Styrene 1 07/06/23 05:25 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/06/23 05:25 V35034MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/06/23 05:25 V35034MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/06/23 05:25 V35034MSA
<0.220 µg/L 0.220 0.500Toluene 1 07/06/23 05:25 V35034MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/06/23 05:25 V35034MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/06/23 05:25 V35034MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/06/23 05:25 V35034MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/06/23 05:25 V35034MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/06/23 05:25 V35034MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/06/23 05:25 V35034MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/06/23 05:25 V35034MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/06/23 05:25 V35034MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/06/23 05:25 V35034MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/06/23 05:25 V35034MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/06/23 05:25 V35034MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 07/06/23 05:25 V35034MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 56
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-178-0016
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #3992 Received : 06/27/2023
The Corner Store
Report Date : 07/10/2023
Sample ID :
Lab No :
Sampled:Trip Blank
99380 Matrix:
6/27/2023 6:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V35033 07/05/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/06/23 05:25 V35034MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/06/23 05:25 V35034
Surrogate: 4-Bromofluorobenzene 95.0 Limits: 70-130%07/06/23 05:251 MSA V35034
Surrogate: Dibromofluoromethane 96.8 Limits: 70-130%07/06/23 05:251 MSA V35034
Surrogate: 1,2-Dichloroethane - d4 92.8 Limits: 70-130%07/06/23 05:251 MSA V35034
Surrogate: Toluene-d8 94.0 Limits: 70-130%07/06/23 05:251 MSA V35034
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35034QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35033
Associated Lab Samples: 99372, 99373, 99374, 99375, 99378, 99379, 99380
LRB-V35033 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/23 04:5710.01.80<1.80µg/LAcetone
07/06/23 04:570.5000.180<0.180µg/LBenzene
07/06/23 04:570.5000.210<0.210µg/LBromobenzene
07/06/23 04:571.000.420<0.420µg/LBromochloromethane
07/06/23 04:570.5000.160<0.160µg/LBromodichloromethane
07/06/23 04:575.001.50<1.50µg/LBromoform
07/06/23 04:571.000.280<0.280µg/LBromomethane
07/06/23 04:570.5000.180<0.180µg/Ln-Butylbenzene
07/06/23 04:570.5000.200<0.200µg/Lsec-Butyl benzene
07/06/23 04:572.000.920<0.920µg/Ltert-Butyl benzene
07/06/23 04:570.5000.180<0.180µg/LCarbon Tetrachloride
07/06/23 04:570.5000.190<0.190µg/LChlorobenzene
07/06/23 04:570.5000.190<0.190µg/LChlorodibromomethane
07/06/23 04:571.000.430<0.430µg/LChloroethane
07/06/23 04:570.5000.220<0.220µg/LChloroform
07/06/23 04:570.5000.220<0.220µg/LChloromethane
07/06/23 04:570.5000.200<0.200µg/L2-Chlorotoluene
07/06/23 04:570.5000.200<0.200µg/L4-Chlorotoluene
07/06/23 04:570.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/06/23 04:572.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/06/23 04:570.5000.200<0.200µg/L1,2-Dibromoethane
07/06/23 04:570.5000.230<0.230µg/LDibromomethane
07/06/23 04:570.5000.220<0.220µg/L1,2-Dichlorobenzene
07/06/23 04:570.5000.190<0.190µg/L1,3-Dichlorobenzene
07/06/23 04:570.5000.210<0.210µg/L1,4-Dichlorobenzene
07/06/23 04:575.001.20<1.20µg/LDichlorodifluoromethane
07/06/23 04:570.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 12Date:07/10/2023 12:37 PM
Page 43 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35034QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35033
Associated Lab Samples: 99372, 99373, 99374, 99375, 99378, 99379, 99380
LRB-V35033 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/23 04:570.5000.150<0.150µg/L1,2-Dichloroethane
07/06/23 04:570.5000.150<0.150µg/L1,1-Dichloroethene
07/06/23 04:570.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/06/23 04:570.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/06/23 04:570.5000.190<0.190µg/L1,2-Dichloropropane
07/06/23 04:570.5000.130<0.130µg/L1,3-Dichloropropane
07/06/23 04:572.000.210<0.210µg/L2,2-Dichloropropane
07/06/23 04:570.5000.200<0.200µg/L1,1-Dichloropropene
07/06/23 04:570.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/06/23 04:570.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/06/23 04:5720042.0<42.0µg/LEthanol
07/06/23 04:570.5000.170<0.170µg/LEthylbenzene
07/06/23 04:573.000.350<0.350µg/LHexachlorobutadiene
07/06/23 04:571.000.380<0.380µg/L2-Hexanone
07/06/23 04:570.5000.180<0.180µg/LIsopropylbenzene
07/06/23 04:570.5000.089<0.089µg/L4-Isopropyl toluene
07/06/23 04:575.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/06/23 04:571.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/06/23 04:571.000.078<0.078µg/L4-Methyl-2-Pentanone
07/06/23 04:572.000.330<0.330µg/LMethylene Chloride
07/06/23 04:571.000.470<0.470µg/LNaphthalene
07/06/23 04:570.5000.190<0.190µg/Ln-Propylbenzene
07/06/23 04:570.5000.220<0.220µg/LStyrene
07/06/23 04:570.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
07/06/23 04:570.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/06/23 04:570.5000.220<0.220µg/LTetrachloroethene
07/06/23 04:570.5000.220<0.220µg/LToluene
Page 2 of 12Date:07/10/2023 12:37 PM
Page 44 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35034QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35033
Associated Lab Samples: 99372, 99373, 99374, 99375, 99378, 99379, 99380
LRB-V35033 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/23 04:570.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/06/23 04:570.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/06/23 04:570.5000.160<0.160µg/L1,1,1-Trichloroethane
07/06/23 04:570.5000.096<0.096µg/L1,1,2-Trichloroethane
07/06/23 04:570.5000.180<0.180µg/LTrichloroethene
07/06/23 04:570.5000.180<0.180µg/LTrichlorofluoromethane
07/06/23 04:570.5000.270<0.270µg/L1,2,3-Trichloropropane
07/06/23 04:570.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/06/23 04:570.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/06/23 04:575.001.00<1.00µg/LVinyl Acetate
07/06/23 04:570.5000.170<0.170µg/LVinyl Chloride
07/06/23 04:570.5000.210<0.210µg/Lo-Xylene
07/06/23 04:571.000.420<0.420µg/Lm,p-Xylene
07/06/23 04:574-Bromofluorobenzene (S)94.4 70-130
07/06/23 04:57Dibromofluoromethane (S)96.2 70-130
07/06/23 04:571,2-Dichloroethane - d4 (S)93.6 70-130
07/06/23 04:57Toluene-d8 (S)93.6 70-130
LCS-V35033 LCSD-V35033Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.4 10110240.640.0µg/LAcetone 40-160 0.4 20.0
19.1 95.596.019.220.0µg/LBenzene 70-130 0.5 20.0
17.7 88.587.517.520.0µg/LBromobenzene 70-130 1.1 20.0
20.2 10199.019.820.0µg/LBromochloromethane 70-130 2.0 20.0
17.9 89.593.018.620.0µg/LBromodichloromethane 70-130 3.8 20.0
Page 3 of 12Date:07/10/2023 12:37 PM
Page 45 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35034QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35033
LCS-V35033 LCSD-V35033Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.8 94.090.018.020.0µg/LBromoform 70-130 4.3 20.0
19.4 97.097.519.520.0µg/LBromomethane 60-140 0.5 20.0
18.2 91.089.017.820.0µg/Ln-Butylbenzene 70-130 2.2 20.0
17.9 89.590.518.120.0µg/Lsec-Butyl benzene 70-130 1.1 20.0
18.1 90.590.518.120.0µg/Ltert-Butyl benzene 70-130 0.0 20.0
18.4 92.091.018.220.0µg/LCarbon Tetrachloride 70-130 1.0 20.0
19.5 97.597.519.520.0µg/LChlorobenzene 70-130 0.0 20.0
18.2 91.090.018.020.0µg/LChlorodibromomethane 70-130 1.1 20.0
19.9 99.599.519.920.0µg/LChloroethane 60-140 0.0 20.0
19.2 96.094.518.920.0µg/LChloroform 70-130 1.5 20.0
16.3 81.586.517.320.0µg/LChloromethane 60-140 5.9 20.0
17.9 89.588.017.620.0µg/L2-Chlorotoluene 70-130 1.6 20.0
17.2 86.087.517.520.0µg/L4-Chlorotoluene 70-130 1.7 20.0
17.0 85.085.517.120.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.5 20.0
19.3 96.592.018.420.0µg/L1,2-Dibromo-3-Chloropropane 70-130 4.7 20.0
18.7 93.593.018.620.0µg/L1,2-Dibromoethane 70-130 0.5 20.0
19.3 96.598.019.620.0µg/LDibromomethane 70-130 1.5 20.0
18.9 94.595.019.020.0µg/L1,2-Dichlorobenzene 70-130 0.5 20.0
18.8 94.094.518.920.0µg/L1,3-Dichlorobenzene 70-130 0.5 20.0
18.5 92.593.018.620.0µg/L1,4-Dichlorobenzene 70-130 0.5 20.0
19.9 99.598.519.720.0µg/LDichlorodifluoromethane 60-140 1.0 20.0
18.5 92.593.518.720.0µg/L1,1-Dichloroethane 70-130 1.0 20.0
18.2 91.091.518.320.0µg/L1,2-Dichloroethane 70-130 0.5 20.0
19.3 96.595.519.120.0µg/L1,1-Dichloroethene 70-130 1.0 20.0
17.9 89.589.017.820.0µg/Lcis-1,2-Dichloroethene 70-130 0.5 20.0
18.3 91.592.518.520.0µg/Ltrans-1,2-Dichloroethene 70-130 1.0 20.0
Page 4 of 12Date:07/10/2023 12:37 PM
Page 46 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35034QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35033
LCS-V35033 LCSD-V35033Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.0 90.091.018.220.0µg/L1,2-Dichloropropane 70-130 1.1 20.0
17.9 89.588.517.720.0µg/L1,3-Dichloropropane 70-130 1.1 20.0
16.5 82.584.016.820.0µg/L2,2-Dichloropropane 70-130 1.8 20.0
20.5 10310120.120.0µg/L1,1-Dichloropropene 70-130 1.9 20.0
17.9 89.589.017.820.0µg/Lcis-1,3-Dichloropropene 70-130 0.5 20.0
17.9 89.587.017.420.0µg/Ltrans-1,3-Dichloropropene 70-130 2.8 20.0
508 10288.4442500µg/LEthanol 60-140 13.8 20.0
17.8 89.090.018.020.0µg/LEthylbenzene 70-130 1.1 20.0
20.1 10110020.020.0µg/LHexachlorobutadiene 70-130 0.4 20.0
15.2 76.076.515.320.0µg/L2-Hexanone 60-140 0.6 20.0
18.1 90.590.018.020.0µg/LIsopropylbenzene 70-130 0.5 20.0
18.7 93.593.518.720.0µg/L4-Isopropyl toluene 70-130 0.0 20.0
16.4 82.080.516.120.0µg/LMethyl Ethyl Ketone (MEK)60-140 1.8 20.0
19.1 95.593.518.720.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.1 20.0
15.6 78.078.515.720.0µg/L4-Methyl-2-Pentanone 60-140 0.6 20.0
18.5 92.592.518.520.0µg/LMethylene Chloride 70-130 0.0 20.0
15.4 77.077.515.520.0µg/LNaphthalene 70-130 0.6 20.0
17.4 87.088.517.720.0µg/Ln-Propylbenzene 70-130 1.7 20.0
19.3 96.596.019.220.0µg/LStyrene 70-130 0.5 20.0
19.2 96.094.518.920.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.5 20.0
17.3 86.585.517.120.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.1 20.0
19.9 99.599.519.920.0µg/LTetrachloroethene 70-130 0.0 20.0
18.7 93.594.518.920.0µg/LToluene 70-130 1.0 20.0
19.8 99.010020.020.0µg/L1,2,3-Trichlorobenzene 70-130 1.0 20.0
19.6 98.010120.120.0µg/L1,2,4-Trichlorobenzene 70-130 2.5 20.0
19.2 96.099.019.820.0µg/L1,1,1-Trichloroethane 70-130 3.0 20.0
Page 5 of 12Date:07/10/2023 12:37 PM
Page 47 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35034QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35033
LCS-V35033 LCSD-V35033Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.5 97.597.519.520.0µg/L1,1,2-Trichloroethane 70-130 0.0 20.0
20.8 10410420.720.0µg/LTrichloroethene 70-130 0.4 20.0
20.2 10110220.420.0µg/LTrichlorofluoromethane 60-140 0.9 20.0
18.0 90.087.517.520.0µg/L1,2,3-Trichloropropane 70-130 2.8 20.0
18.1 90.590.518.120.0µg/L1,2,4-Trimethylbenzene 70-130 0.0 20.0
18.5 92.591.518.320.0µg/L1,3,5-Trimethylbenzene 70-130 1.0 20.0
17.5 87.595.019.020.0µg/LVinyl Acetate 60-140 8.2 20.0
19.4 97.095.019.020.0µg/LVinyl Chloride 60-140 2.0 20.0
18.7 93.591.518.320.0µg/Lo-Xylene 70-130 2.1 20.0
38.8 97.097.238.940.0µg/Lm,p-Xylene 70-130 0.2 20.0
92.893.04-Bromofluorobenzene (S)70-130
97.295.4Dibromofluoromethane (S)70-130
94.895.01,2-Dichloroethane - d4 (S)70-130
94.693.4Toluene-d8 (S)70-130
Page 6 of 12Date:07/10/2023 12:37 PM
Page 48 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35083QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35074
Associated Lab Samples: 99372, 99376, 99377
LRB-V35074 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/23 18:5710.01.80<1.80µg/LAcetone
07/06/23 18:570.5000.180<0.180µg/LBenzene
07/06/23 18:570.5000.210<0.210µg/LBromobenzene
07/06/23 18:571.000.420<0.420µg/LBromochloromethane
07/06/23 18:570.5000.160<0.160µg/LBromodichloromethane
07/06/23 18:575.001.50<1.50µg/LBromoform
07/06/23 18:571.000.280<0.280µg/LBromomethane
07/06/23 18:570.5000.180<0.180µg/Ln-Butylbenzene
07/06/23 18:570.5000.200<0.200µg/Lsec-Butyl benzene
07/06/23 18:572.000.920<0.920µg/Ltert-Butyl benzene
07/06/23 18:570.5000.180<0.180µg/LCarbon Tetrachloride
07/06/23 18:570.5000.190<0.190µg/LChlorobenzene
07/06/23 18:570.5000.190<0.190µg/LChlorodibromomethane
07/06/23 18:571.000.430<0.430µg/LChloroethane
07/06/23 18:570.5000.220<0.220µg/LChloroform
07/06/23 18:570.5000.220<0.220µg/LChloromethane
07/06/23 18:570.5000.200<0.200µg/L2-Chlorotoluene
07/06/23 18:570.5000.200<0.200µg/L4-Chlorotoluene
07/06/23 18:570.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/06/23 18:572.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/06/23 18:570.5000.200<0.200µg/L1,2-Dibromoethane
07/06/23 18:570.5000.230<0.230µg/LDibromomethane
07/06/23 18:570.5000.220<0.220µg/L1,2-Dichlorobenzene
07/06/23 18:570.5000.190<0.190µg/L1,3-Dichlorobenzene
07/06/23 18:570.5000.210<0.210µg/L1,4-Dichlorobenzene
07/06/23 18:575.001.20<1.20µg/LDichlorodifluoromethane
07/06/23 18:570.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 12Date:07/10/2023 12:37 PM
Page 49 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35083QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35074
Associated Lab Samples: 99372, 99376, 99377
LRB-V35074 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/23 18:570.5000.150<0.150µg/L1,2-Dichloroethane
07/06/23 18:570.5000.150<0.150µg/L1,1-Dichloroethene
07/06/23 18:570.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/06/23 18:570.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/06/23 18:570.5000.190<0.190µg/L1,2-Dichloropropane
07/06/23 18:570.5000.130<0.130µg/L1,3-Dichloropropane
07/06/23 18:572.000.210<0.210µg/L2,2-Dichloropropane
07/06/23 18:570.5000.200<0.200µg/L1,1-Dichloropropene
07/06/23 18:570.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/06/23 18:570.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/06/23 18:5720042.0<42.0µg/LEthanol
07/06/23 18:570.5000.170<0.170µg/LEthylbenzene
07/06/23 18:573.000.350<0.350µg/LHexachlorobutadiene
07/06/23 18:571.000.380<0.380µg/L2-Hexanone
07/06/23 18:570.5000.180<0.180µg/LIsopropylbenzene
07/06/23 18:570.5000.089<0.089µg/L4-Isopropyl toluene
07/06/23 18:575.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/06/23 18:571.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/06/23 18:571.000.078<0.078µg/L4-Methyl-2-Pentanone
07/06/23 18:572.000.330<0.330µg/LMethylene Chloride
07/06/23 18:571.000.470<0.470µg/LNaphthalene
07/06/23 18:570.5000.190<0.190µg/Ln-Propylbenzene
07/06/23 18:570.5000.220<0.220µg/LStyrene
07/06/23 18:570.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
07/06/23 18:570.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/06/23 18:570.5000.220<0.220µg/LTetrachloroethene
07/06/23 18:570.5000.220<0.220µg/LToluene
Page 8 of 12Date:07/10/2023 12:37 PM
Page 50 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35083QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35074
Associated Lab Samples: 99372, 99376, 99377
LRB-V35074 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/23 18:570.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/06/23 18:570.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/06/23 18:570.5000.160<0.160µg/L1,1,1-Trichloroethane
07/06/23 18:570.5000.096<0.096µg/L1,1,2-Trichloroethane
07/06/23 18:570.5000.180<0.180µg/LTrichloroethene
07/06/23 18:570.5000.180<0.180µg/LTrichlorofluoromethane
07/06/23 18:570.5000.270<0.270µg/L1,2,3-Trichloropropane
07/06/23 18:570.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/06/23 18:570.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/06/23 18:575.001.00<1.00µg/LVinyl Acetate
07/06/23 18:570.5000.170<0.170µg/LVinyl Chloride
07/06/23 18:570.5000.210<0.210µg/Lo-Xylene
07/06/23 18:571.000.420<0.420µg/Lm,p-Xylene
07/06/23 18:574-Bromofluorobenzene (S)92.6 70-130
07/06/23 18:57Dibromofluoromethane (S)97.8 70-130
07/06/23 18:571,2-Dichloroethane - d4 (S)94.4 70-130
07/06/23 18:57Toluene-d8 (S)95.0 70-130
LCS-V35074 LCSD-V35074Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
49.0 12311746.940.0µg/LAcetone 40-160 4.3 20.0
20.1 10198.019.620.0µg/LBenzene 70-130 2.5 20.0
18.6 93.091.518.320.0µg/LBromobenzene 70-130 1.6 20.0
19.8 99.010220.420.0µg/LBromochloromethane 70-130 2.9 20.0
19.3 96.595.519.120.0µg/LBromodichloromethane 70-130 1.0 20.0
Page 9 of 12Date:07/10/2023 12:37 PM
Page 51 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35083QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35074
LCS-V35074 LCSD-V35074Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.1 95.596.019.220.0µg/LBromoform 70-130 0.5 20.0
21.5 10810320.520.0µg/LBromomethane 60-140 4.7 20.0
19.4 97.092.018.420.0µg/Ln-Butylbenzene 70-130 5.2 20.0
18.8 94.092.518.520.0µg/Lsec-Butyl benzene 70-130 1.6 20.0
19.2 96.092.018.420.0µg/Ltert-Butyl benzene 70-130 4.2 20.0
19.9 99.592.518.520.0µg/LCarbon Tetrachloride 70-130 7.2 20.0
20.9 10510020.020.0µg/LChlorobenzene 70-130 4.4 20.0
19.0 95.093.518.720.0µg/LChlorodibromomethane 70-130 1.5 20.0
21.3 10710420.720.0µg/LChloroethane 60-140 2.8 20.0
19.8 99.097.019.420.0µg/LChloroform 70-130 2.0 20.0
17.4 87.082.516.520.0µg/LChloromethane 60-140 5.3 20.0
18.5 92.590.018.020.0µg/L2-Chlorotoluene 70-130 2.7 20.0
18.2 91.087.517.520.0µg/L4-Chlorotoluene 70-130 3.9 20.0
18.2 91.089.017.820.0µg/LDi-Isopropyl Ether (DIPE)70-130 2.2 20.0
19.8 99.010120.220.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.0 20.0
19.3 96.510220.420.0µg/L1,2-Dibromoethane 70-130 5.5 20.0
20.0 10010120.220.0µg/LDibromomethane 70-130 0.9 20.0
20.2 10198.019.620.0µg/L1,2-Dichlorobenzene 70-130 3.0 20.0
19.7 98.598.519.720.0µg/L1,3-Dichlorobenzene 70-130 0.0 20.0
20.1 10196.519.320.0µg/L1,4-Dichlorobenzene 70-130 4.0 20.0
22.7 11410721.420.0µg/LDichlorodifluoromethane 60-140 5.8 20.0
19.7 98.592.518.520.0µg/L1,1-Dichloroethane 70-130 6.2 20.0
19.0 95.095.519.120.0µg/L1,2-Dichloroethane 70-130 0.5 20.0
20.4 10294.518.920.0µg/L1,1-Dichloroethene 70-130 7.6 20.0
19.0 95.093.518.720.0µg/Lcis-1,2-Dichloroethene 70-130 1.5 20.0
19.6 98.093.518.720.0µg/Ltrans-1,2-Dichloroethene 70-130 4.6 20.0
Page 10 of 12Date:07/10/2023 12:37 PM
Page 52 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35083QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35074
LCS-V35074 LCSD-V35074Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.1 95.593.018.620.0µg/L1,2-Dichloropropane 70-130 2.6 20.0
19.4 97.093.518.720.0µg/L1,3-Dichloropropane 70-130 3.6 20.0
19.2 96.092.518.520.0µg/L2,2-Dichloropropane 70-130 3.7 20.0
21.2 10610320.520.0µg/L1,1-Dichloropropene 70-130 3.3 20.0
19.7 98.594.018.820.0µg/Lcis-1,3-Dichloropropene 70-130 4.6 20.0
18.8 94.095.019.020.0µg/Ltrans-1,3-Dichloropropene 70-130 1.0 20.0
399 79.8118591500µg/LEthanol 60-140 38.7*20.0
18.7 93.590.518.120.0µg/LEthylbenzene 70-130 3.2 20.0
20.8 10410320.520.0µg/LHexachlorobutadiene 70-130 1.4 20.0
17.2 86.089.017.820.0µg/L2-Hexanone 60-140 3.4 20.0
19.1 95.592.018.420.0µg/LIsopropylbenzene 70-130 3.7 20.0
19.9 99.596.519.320.0µg/L4-Isopropyl toluene 70-130 3.0 20.0
14.9 74.579.515.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 6.4 20.0
19.9 99.599.519.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 0.0 20.0
17.3 86.583.516.720.0µg/L4-Methyl-2-Pentanone 60-140 3.5 20.0
19.3 96.593.518.720.0µg/LMethylene Chloride 70-130 3.1 20.0
16.4 82.083.016.620.0µg/LNaphthalene 70-130 1.2 20.0
18.9 94.589.517.920.0µg/Ln-Propylbenzene 70-130 5.4 20.0
20.0 10099.519.920.0µg/LStyrene 70-130 0.5 20.0
20.3 10298.519.720.0µg/L1,1,1,2-Tetrachloroethane 70-130 3.0 20.0
18.3 91.593.018.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 1.6 20.0
21.4 10710120.120.0µg/LTetrachloroethene 70-130 6.2 20.0
20.0 10095.519.120.0µg/LToluene 70-130 4.6 20.0
22.5 11311122.120.0µg/L1,2,3-Trichlorobenzene 70-130 1.7 20.0
21.8 10911122.120.0µg/L1,2,4-Trichlorobenzene 70-130 1.3 20.0
20.7 10496.019.220.0µg/L1,1,1-Trichloroethane 70-130 7.5 20.0
Page 11 of 12* QC Fail Date:07/10/2023 12:37 PM
Page 53 of 56
Quality Control Data
23-178-0016Report No:
Project Description:
Client ID:Geological Resources, Inc.
The Corner Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V35083QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V35074
LCS-V35074 LCSD-V35074Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.2 10110020.020.0µg/L1,1,2-Trichloroethane 70-130 0.9 20.0
21.6 10810320.520.0µg/LTrichloroethene 70-130 5.2 20.0
22.0 11010420.720.0µg/LTrichlorofluoromethane 60-140 6.0 20.0
19.0 95.092.518.520.0µg/L1,2,3-Trichloropropane 70-130 2.6 20.0
19.2 96.093.518.720.0µg/L1,2,4-Trimethylbenzene 70-130 2.6 20.0
19.5 97.593.518.720.0µg/L1,3,5-Trimethylbenzene 70-130 4.1 20.0
20.7 10411122.220.0µg/LVinyl Acetate 60-140 6.9 20.0
20.9 10598.519.720.0µg/LVinyl Chloride 60-140 5.9 20.0
19.4 97.094.518.920.0µg/Lo-Xylene 70-130 2.6 20.0
41.0 10310140.340.0µg/Lm,p-Xylene 70-130 1.7 20.0
92.291.24-Bromofluorobenzene (S)70-130
96.096.6Dibromofluoromethane (S)70-130
94.494.41,2-Dichloroethane - d4 (S)70-130
94.695.8Toluene-d8 (S)70-130
Page 12 of 12Date:07/10/2023 12:37 PM
Page 54 of 56
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-178-0016
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:06/27/2023 16:12:30
Special precautions or instructions included?
Comments:
Page 55 of 56
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