IH1587_2022-07-05_SAR_Soil and Groundwater Sampling Report

615 Bruce Thomas Road
Monroe, North Carolina 28112
July 5, 2022
Mr. John Griffing
Griffing Leaser, PLLC
Harmon Environmental, P A
518 S. NewHope Road
Gastonia, North Carolina 28054
Re: Soil and Groundwater Sampling Activities
Former Dana/ex Facilityy
515 E. Alabama Avenue in Bessemer City, North Carolina
Project No. 897-05
Dear Mr. Griffing:
704-292-4527
[e-mail]
Harmon Environmental, P A respectfully submits for your review and comment this brief report
summarizing the methods and results of the soil and groundwater sampling project at the forerm
Danalex facility located at 515 E. Alabama Avenue in Bessemer City, North Carolina. Figure 1
shows the location of the site on an excerpt of a United States Geologic Survey Map of the Region.
As outlined in Proposal No. 22-1361 dated April13, 2022, Harmon Environmental, PA retained
Integrated Scanning Solutions, LLC to survey the interior of the facility using ground penetrating
radar (GPR). Using a Proceq 8800 GPR and a GSSI Mini TX GPR to delineate sub-slab features
which may provide preferential flow pathways for vapor migration through the facility. Use of
GPR technology in the former Danalex facility was limited by historic activities at the site. GPR
technology is not able to penetrate metal decking material. At the former Danalex facility site,
metal decking was apparently used to cover many of the larger floor trenches prior to patching
these areas with new concrete. Further, smaller trenches filled with concrete appear to GPR as
concrete floor and are not easily differentiated from the original floor. To address these concerns,
initially, concrete patches in the floor were visually delineated and marked with white spray paint.
Following the marking of the concrete patches, Integrated Scanning Solutions, LLC scanned the
former Danalex facility building with both a Proceq 8800 GPR and a GSSI Mini TX GPR.
Subgrade piping and electrical conduits documented by Integrated Scanning Solutions, LLC were
marked with pink spray paint. A copy of the Integrated Scanning Solutions, LLC report is
presented in Attachment A.
Based on the results of the GPR survey, 20 Geoprobe® soil borings were advanced through the
floor of the former Danalex facility at the approximate locations depicted on Figure 2. As
advanced soil samples were collected continuously from the base of the floor slab to each boring
terminus. As collected each soil sample was screened for the presence of volatile organic vapors
using a MultiRea® photoionizing organic vapor detector calibrated to an isobutylene standard.
Further, each soil sample was visually described in general accordance with the Unified Soil
Classification System (USCS). Boring logs summarizing the field screening results and soil
descriptions are presented in Attachment B. These descriptions were used to generate geologic
Mr. John Griffing
July 5, 2022
Page2
cross section of the soils encountered beneath the floor slab at the former Danalex facility. Figure
3 shows the location of the cross-sections depicted in Figures 4 and 5. As indicated in these figures,
the site is underlain by silts and clays. Fill material was encountered beneath the building primarily
in the southeast end. The fill material also consisted of silts and clays.
With the exception of borings GP-2, GP-3 and GP-14, the 20 borings were advanced to 12 feet
below the floor slab. Boring GP-2 and GP-14 were terminated when a second concrete surface
was encountered beneath the surface. Each of these borings encountered black textile material
between these two concrete layers.
Based on the field screening results, 29 soil samples were selected for laboratory analysis. These
selected samples were contained in glassware provided by Pace Analytical Services, LLC and
placed in a cooler on ice pending delivery to the laboratory. Chain-of-Custody protocol was
maintained throughout the sample delivery process. Upon receipt, these samples were analyzed
for volatile organic compounds in accordance with SW-846 Method 8260D.
A complete analytical report is presented in Attachment C. The analytical results associated with
the soil samples are summarized on Table 1. Further, the analytical results are presented on Figure
6, 7 and 8.
Boring GP-3 was advanced to a termination depth of 20 feet below the floor slab. Following
completion of the Geoprobe® advancement, a temporary monitor well was installed at this location
screened for 9.5 to 19.5 feet below the floor. After allowing 24-hours for the well to equilibrate,
the water level was measured in this well at 13.05 feet below the floor slab. Following
measurement of the water level, the well was developed, purged and sampled in general
accordance with North Carolina Department of Environmental Quality (DEQ) accepted protocol.
As collected the water sample was contained in glassware provided by the Pace Analytical
Services, LLC and placed in a cooler on ice pending delivery to the laboratory. Chain-of-Custody
protocol was maintained throughout the sample delivery process. Upon receipt, the sample was
analyzed for VOCs in accordance with SW-846 Method 8260D.
The analytical results associated with the June 1, 2022 sample indicated the presence of cis-1,2-
dichloroethene, tetrachloroethene and trichloroethene at concentrations of 7,690 micrograms per
liter (J..LgiL), 124,000 J..LgiL and 4,490 J..Lg/L, respectively. The North Carolina Groundwater Quality
Standards as established in 15A NCAC 2L for cis-1,2-dichloroethene, tetrachloroethene and
trichloroethene are 70 J..Lg/L, 0.7 J..Lg/L and 3 J..Lg/L, respectively.
As indicated by these analytical data, both North Carolina Preliminary Soil Remediation Goals
and North Carolina Groundwater Standards have been exceeded beneath the floor slab at the
former Danalex facility. While the magnitude and extent of the impacted soil and groundwater
warranted remediation, initial actions at the site should address potential vapor intrusion issues.
Harmon Environmental, P A recommends vapor mitigation be designed and installed at the site
Mr. John Griffing
July 5, 2022
Page 3
initially and further assessment and remediation activities follow.
Please call or email if you have any questions.
Figures
SOURCE: TOPO! 2003 NATIONAL GEOGRAPHIC
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA
704-292:-4527
harmonenvironmental.com
APPROXIMATE SCALE IN FEET
0 2000 4000
FIGURE 1
SITE LOCATION MAP
FORMER DANALEX FACILITY SITE
515 E. ALABAMA AVENUE
BESSEMER CITY, NORTH CAROLINA
GP-14
0
0
GP-15
f--
I LJ L_J
AREA4
AREA2
AREA 1
GP-13 0
I I I~ --,-r---r -~--------------------r----
I !
I I
r-·-
-
GP-8
0
GP-7
r----------.--.-1 rrjJ
GP-11
0
I
GP-12 lD
GP-17
0
till
I~P-6
GP-5
0
GP-18
0
GP-4
0
: J I
I
I
AREA6 OG~
AREAS
GP-3 0
GP-1 0
GP-90
r­
GP-20oo GP-2
LEGEND
0 APPROXIMATE LOCATION OF SOIL BORINGS
BUILDING WALLS
APPROXIMATE SCALE IN FEET
BASED ON BASE MAP PROVIDED BY BENMAR PROPERTIES, LLC AND FIELD MEASUREMENTS 0 50 100
897-' nmr
<(
0..
AREA2
---
------------------AREA 1 /
/ ---------/ GP-14 /'
~
----GP-13(0-4)--...._
PCE 135 ug/KG 0
NOTES
0
GP-15(0.5-4)
PCE 137 ug/KG
-....,__
'----
----
""" """
AREA4
"' "' "' f--
""
GP-2(2)
PCE 1,950,000 ug/KG
'f.-U ::::::='1 ---==r-I ! I /, AI "''!) I I - -" Cb
'\ ov· C ~ --PCE 4,47~KG 0 ~ ~ 10 /G~-8(4-8) GP-7(0-4) I ~ 'P~~-~a45~o g/KG--( ~"-.._ (< c~ ~c PCE 2,010 ug/KG ' u GP-9(8-12) I'() '-. ~ '-~ PCE 5,480 ug/KG \ PCE 2,190,000 ug/KG \ '-. C"' ~j ~ lj ~"' 1
= -:U:J ~ ~\ AREA 5 II l -~~)
\ GP-ll(0-4) PCE 774 ug/KG I 8.-...-, \ IS
0 PeE 63.6 ug/KG ~ §'
J GP 10(8 12) \ GP-5(8-12) \ I-· 1 0 PCE 152' ug/KG 'o PCE 5,100 ug/KG 1 I PCE 19,300 ug/K
-~ -GP-181(4-8) I /j "'~
\ 3--PCE 76.4 ug/KG / / J/ #. u/
;,_ --------/ 7 ,c. I "'~
-u '(e., GP-17(4-8) ------GP-4(4=8) GP-3(4-8) II I '\~ SOIL SAMPLES WERE COLLECTED BY HARMON
ENVIRONMENTAL, PA PERSONNEL ON MAY 31,
2022 AND JUNE 1, 2022 AND ANALYZED BY
PACE ANALYTICAL SERVICES, LLC FOR
VOLATILE ORGANIC COMPOUNDS BY SW-846
METHOD 8260D.
""
--r.c PCE 3,340 ug/KG 0 ,n PCE 94 900 g/KG PCE 1,260,000"ug!KG/ I
t-r----,r-.--.------"'<-----=-"""-<:-r----r-.,.I,--.--L'--.. ~ , u I \0 1 I 7 __
\, '',,_~~] r 'I
GP-19(8-12)
PCE 719 ug/KG
ISOCONCENTRATION CONTOURS PRESENTED I
HEREIN ARE BASED ON INTERPOLATION
BETWEEN THE TETRACHLOROETHENE
CONCENTRATIONS DETECTED IN THE MAY 31,
2022 AND JUNE 1, 2022 SAMPLES.
APPROXIMATE SCALE IN FEET
0 50 100
AREA6 ""' L ..! I LEGEND -----------------------------
"" -I
"" GP-16(8-12) 0 __d
\"CE 42.2 ug/KG
0
PCE
APPROXIMATE LOCATION OF SOIL BORINGS
TETRACHLOROETHENE
ug/KG MICROGRAMS PER KILOGRAM
BUILDING WALLS
(4-8) SAMPLE DEPTH IN FEET BELOW THE FLOOR SLAB
TETRACHLOROETHENE ISOCONCENTRATION
CONTOUR
BASED ON BASE MAP PROVIDED BY BENMAR PROPERTIES, LLC AND FIELD MEASUREMENTS
<(
0..
A
GP-14
0
f--
AREA6
AREA 1
GP-8
GP-11
0
I~
GP-7
GP-17
0
GP-13
GP-5
0
GP-4
0
I
L----------------------------------------------OG~
B
AREA2
GP-1 0 I A'
GP-9
AREAS
GP-19 ---'--'---'----'
LEGEND
0 APPROXIMATE LOCATION OF SOIL BORINGS
BUILDING WALLS
A'
A._! _ _.! CROSS SECTION LOCATION
APPROXIMATE SCALE IN FEET
BASED ON BASE MAP PROVIDED BY BENMAR PROPERTIES, LLC AND FIELD MEASUREMENTS 0 50 100
<(
0..
OFT
I FT
2FT
3FT
4FT
5FT
6FT
7FT
8FT
9FT
10FT
11FT
12FT
13FT
0 50 100
APPROXIMATE HORIZONTAL SCALE IN FEET
NOTES
THE LITHOLOGICAL CONTACTS PRESENTED
HEREIN ARE BASED ON INTERPOLATION
BETWEEN THE SOIL DESCRIPTIONS PRESENTED
ON THE BORING LOGS. FOR DETAILED
DESCRIPTIONS OF THE SOIL ENCOUNTERED
ON-SITE, PLEASE REFER TO THE BORING LOGS.
LEGEND
~ ~
OFT
1FT
2FT
3FT
4FT
5FT
6FT
7FT
8FT
9FT
10FT
11FT
12FT
13FT
FINE TO SAND (FILL MATERIAL)
SILTY CLAY AND CLAY
m CLAYEY SILT AND SILT
CONCRETE
SHALLOW GROUNDWATER
DEPTH AS MEASURED IN
GP-3 ON JUNE I, 2022
<( - z <( -' ?:: ....1 <( UJO Z::::i::>a! OCiZ< -<(UJV tJu..~:c "'~GS<t;: ~~~~0 =>oz<z ~a!<(~~ u..vo
<(
0..
VQ!<C-i3UJ .v ~UJQ! 0 lOUJ
....1 -~ 00 10 UJU.. UJ
IJ ~ UJ
al
1.)
B~ .....
5 ""
OFf
1Fr
2Fr
3Fr
4Fr
5Fr
6Fr
7Fr
BFr
9Fr
10 Fr
11FT
12 Fr
13Fr
14 Fr
15 Fr
16 Fr
17 Fr
18 Fr
19 Fr
20
0 50 100
APPROXIMATE HORIZONTAL SCALE IN FEET
B'
NOTES
THE LITHOLOGICAL CONTACTS PRESENTED
HEREIN ARE BASED ON INTERPOLATION
BETWEEN THE SOIL DESCRIPTIONS PRESENTED
ON THE BORING LOGS. FOR DETAILED
DESCRIPTIONS OF THE SOIL ENCOUNTERED
ON-SITE, PLEASE REFER TO THE BORING LOGS.
OFf
1Fr
2Fr
3Fr
4Fr
5Fr
6Fr
7Fr
8Fr
9Fr
10FT
11Fr
12 Fr
13Fr
14 Fr
15 Fr
16 Fr
17 Fr
18 Fr
19 Fr
20 Fr
LEGEND
~ ~
~ ~
SANDY CLAY AND SILT FILL MATERIAL
FINE TO COARSE SAND
CLAY, SANDY CLAY AND SILTY CLAY
m CLAYEY SILT AND SILT
CONCRETE
SHALLOW GROUNDWATER
DEPTH AS MEASURED IN
GP-3 ON JUNE I, 2022
<(
0..
0 50
"' r:i.. IJ
NOTES
THE LITHOLOGICAL CONTACTS PRESENTED
HEREIN ARE BASED ON INTERPOLATION
BElWEEN THE SOIL DESCRIPTIONS PRESENTED
ON THE BORING LOGS. FOR DETAILED
DESCRIPTIONS OF THE SOIL ENCOUNTERED
ON·SITE, PLEASE REFER TO THE BORING LOGS.
ANAL TICAL RESULTS PRESENTED HEREIN ARE
BASED ON SOIL SAMPLES COLLECTED BY
HARMON ENVIRONMENTAL. PA PERSONNEL
ON MAY 31, 2022 AND JUNE 1, 2022 AND
ANALYZED BY PACE ANALYTICALSERVICES, LLC
FOR VOLATILE ORGANIC COMPOUNS (VOCs)
IN ACCORDANCE WITH SW·846 METHOD
8260D.
100
APPROXIMATE HORIZONTAL SCALE IN FEET
..... r:i.. IJ "' r:i.. IJ
CB = CHLOROBENZENE
LEGEND
1,1·DCE = 1,1-DICHLOROETHENE
C-1,2-DCE = CIS-1,2-DICHLOROOETHENE
PCE = TETRACHLOROETHENE
1,2,3-TCB = 1,2,3-TRICHLOROBENZENE
TCE = TRICHLOROETHENE
ug/KG = MICROGRAMS PER KILOGRAM
~ ~
"' r:i.. IJ
IJ ~A'
-' 5 "'
FINE TO SAND (FILL MATERIAL)
SILTY CLAY AND CLAY
m CLAYEY SILT AND SILT
CONCRETE
SHALLOW GROUNDWATER
DEPTH AS MEASURED IN
GP-3 ON JUNE 1, 2022
<(
0..
OFT
1FT
2FT
3FT
4FT
SFT
6FT
7FT
8FT
9FT
lOFT
11FT
12FT
13FT
14FT
15FT
16FT
17FT
18FT
19FT
20
0 50 100
APPROXIMATE HORIZONTAL SCALE IN FEET
OFT
1FT
2FT
3FT
4FT
SFT
6FT
7FT
8FT
9FT
10FT
11FT
12FT
13FT
14FT
15FT
16FT
17FT
18FT
19FT
20FT
NOTES
THE LITHOLOGICAL CONTACTS PRESENTED
HEREIN ARE BASED ON INTERPOLATION
BElWEEN THE SOIL DESCRIPTIONS PRESENTED
ON THE BORING LOGS. FOR DFTAILED
DESCRIPTIONS OF THE SOIL ENCOUNTERED
ON-SITE, PLEASE REFER TO THE BORING LOGS.
ANAL TICAL RESULTS PRESENTED HEREIN ARE
BASED ON SOIL SAMPLES COLLECTED BY
HARMON ENVIRONMENTAL, PA PERSONNEL
ON MAY 31, 2022 AND JUNE 1, 2022 AND
ANALYZED BY PACE ANALYTICAL SERVICES, LLC
FOR VOLATILE ORGANIC COMPOUNS (VOCs)
IN ACCORDANCE WITH SW-B46 MFTHOD
8260D.
LEGEND
CB = CHLOROBENZENE
1,1-DCE = 1,1-D1CHLOROFTHENE
C-1,2-DCE = C1S-1,2-D1CHLOROOFTHENE
PCE = TFTRACHLOROFTHENE
1,2,3-TCB = 1,2,3-TR1CHLOROBENZENE
TCE = TRICHLOROFTHENE
ug/KG = MICROGRAMS PER KILOGRAM
~ SANDY CLAY AND SILT FILL MATERIAL
~ ~
FINE TO COARSE SAND
CLAY, SANDY CLAY AND SILTY CLAY
~ CLAYEY SILT AND SILT
CONCRFTE
SHALLOW GROUNDWATER
DEPTH AS MEASURED IN
GP-3 ON JUNE 1, 2022
<(
0..
NOTES
SOIL SAMPLES WERE COLLECTED BY HARMON
ENVIRONMENTAL, PA PERSONNEL ON MAY 31,
2022 AND JUNE 1, 2022 AND ANALYZED BY
PACE ANALYTICAL SERVICES, LLC FOR
VOLATILE ORGANIC COMPOUNDS BY SW-846
METHOD 8260D.
ISOCONCENTRATION CONTOURS PRESENTED
HEREIN ARE BASED ON INTERPOLATION
BETWEEN THE TOTAL VOLATILE ORGANIC
COMPOUNDS CONCENTRATIONS DETECTED
IN THE MAY 31, 2022 AND JUNE 1. 2022
SAMPLES.
APPROXIMATE SCALE IN FEET
0 50 100
I ----
r ----------------GP-14 /
) • GP-15(0.5-4)
137 ug/KG
"-
f--
AREA6
\Ou'iJV..G-------
--AREA 1
-----
----1
--.......j
'--.... GP-16(8-12) e _d
42.2 ug/Kf(
•
AREA2
LEGEND
GP-2(2)
1,993,850 ug/KG
GP-19(8-12)
889 ug/KG
APPROXIMATE LOCATION OF SOIL BORINGS
ug/KG MICROGRAMS PER KILOGRAM
BUILDING WALLS
(4-8) SAMPLE DEPTH IN FEET BELOW THE FLOOR SLAB
TOTAL VOLATILE ORGAINC COMPOUNDS
ISOCONCENTRATION CONTOUR
BASED ON BASE MAP PROVIDED BY BENMAR PROPERTIES, LLC AND FIELD MEASUREMENTS
897-05 FIGURE 9.DWG
Table
chlorobenzene 1,1-dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene methylene chloride tetrachloroethene 1,2,3-trichlorobenzene trichloroethene o-xylene
ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg
GP-1(8-12) <46.1 273 119 <46.1 <184 4,470 <46.1 31,800 <46.1
GP-2(2) <2,990 <2,990 7,050 <2,990 <120,000 1,950,000 <2,990 36,800 <2,990
GP-3(4-8) <2,570 <2,570 4,640 <2,570 <10,300 1,260,000 <2,570 10,100 <2,570
GP-3(8-12) <26.1 66.0 2,370 <26.1 <105 17,000 <26.1 1,530 <26.1
GP-4(4-8) <124 <124 46,500 312 <495 94,900 <124 5,580 <124
GP-4(8-12) <13.5 <13.5 4,220 101 <54.0 8,390 <13.5 1,320 <13.5
GP-5(4-8) <6.3 <6.3 693 <6.3 <25.3 713 <6.3 161 8.3
GP-5(8-12) <7.2 <7.2 976 31.7 <28.7 5,100 <7.2 149 <7.2
GP-6(4-8) <18.3 <18.3 108 <18.3 <73.3 10,500 <18.3 3,530 <18.3
GP-6(8-12) <18.2 <9.1 53.3 <9.1 <36.4 4,850 <9.1 1,330 <9.1
GP-7(0-4) <7.8 <7.8 23.6 <7.8 <31.4 5,480 <7.8 128 <7.8
GP-7(4-8) <14.6 <7.3 20.9 <7.3 <29.2 5,140 33.8 195 <14.6
GP-8(4-8) <9.5 <9.5 87.8 <9.5 <38.0 2,010 74.0 26.5 <9.5
GP-9(0.5-4) 67.6 116 80.0 <36.2 <145 22,400 <36.2 5,910 <36.2
GP-9(4-8) <860 <860 <860 <860 <3,440 506,000 <860 17,800 <860
GP-9(8-12) <3,110 <3,110 <3,110 <3,110 <12,400 2,190,000 <3,110 136,000 <3,110
GP-10(8-12) <7.2 <7.2 88.0 <7.2 <26.6 152 <7.2 10.0 <7.2
GP-11(0-4) <5.0 <5.0 <5.0 <5.0 <20.1 63.6 <5.0 <5.0 <5.0
GP-12(4-8) <7.0 <7.0 39.5 <7.0 <27.8 774 <7.0 14.3 7.6
GP-13(0-4) <7.6 <7.6 <7.6 <7.6 <30.6 135 <7.6 <7.6 <7.6
GP-15(0.5-4) <7.2 <7.2 <7.2 <7.2 <28.9 137 <7.2 <7.2 <7.2
GP-16(8-12) <6.1 <6.1 <6.1 <6.1 <24.4 42.2 <6.1 <6.1 <6.1
GP-17(4-8) 39.1 <29.2 20,300 176 121 3,340 <29.2 531 <29.2
GP-17(8-12) <30.5 <30.5 19,400 134 <122 1,040 <30.5 539 <30.5
GP-18(4-8) <5.8 <5.8 <5.8 <5.8 <23.0 76.4 <5.8 <5.8 <5.8
GP-19(8-12) <6.5 <6.5 71.7 <6.5 <26.1 719 <6.5 29.3 6.9
GP-20(4-8) <18.2 <18.2 394 <18.2 328 12,600 <18.2 107 <18.2
GP-20(8-12) <41.2 <41.2 662 <41.2 4,460 19,300 <41.2 174 <41.2
Residential PSRG 5,800 48,000 31,000 15,000 58,000 170,000 13,000 870 140,000
Ind/Com PSRG 280,000 210,000 470,000 64,000 650,000 82,000 190,000 4,000 590,000
Prot GW PSRG 680 2,500 410 620 25 6.3 330 21 9,800
Notes: Soil samples collected by Harmon Environmental, PA personnel on May 31, 2022 and June 1, 2022 and analyzed by Pace Analytical Services, LLC for volatile organic compounds
by SW-846 Method 8260D.
Only detected constituents presented herein for a complete analytical report, please refer to the analytical repor
ug/Kg = microgerams per kilogram
Residental PSRG = Residential Preliminary Soil Remediation Goals as established by the North Carolina Department of Environmental Quality in January 2022
Ind/Com PSRG = Industrial/ Commercial Preliminary Soil Remediation Goals as established by the North Carolina Department of Environmental Quality in January 2022
Prot GWQ PSRG = Protection of the Groundwater Preliminary Soil Remediation Goal as established by the North Carolina Department of Environmental Quality in January 2022
Sample
able 1
Former Danalex Facility
515 E. Alabama Avenue
Bessemer City, North Carolina
Project No. 897-05
Attachment A
Integrated Scanning Solutions, LLC Report
Utility Locate Report

11330 Vanstory Dr Ste 115D
Huntersville NC 28078
[phone], [phone]
[e-mail]
DATE 05/26/2022 -
TECH(S)Joseph Whitehill
JOB #75576187
PO #
CUSTOMER
Mid-South Environmental
Don Warren
1570 Morgan Road
Gold Hill, NC, 28071
[phone]
[e-mail]
SERVICE LOCATION
Mid-South Environmental
Bessemer City
515 East Alabama Avenue
Bessemer City, NC, 28016
[phone]
[e-mail]
JOB DETAILS Site assessment for Harmon Environmental.
Utility and Concrete possible as determined onsite by Don & Rick.
Site data attached.
COMPLETION NOTES Scope of work: Investigate warehouse space prior to soil boring and soil remediation project.
Method: Techs used Proceq 8800 GPR to investigate concrete and sub slab. Techs also used GSSI Mini XT
GPR to investigate slab and sub slab to better detect shallow objects and concrete reinforcing. Techs used
TX10 EM transmitter to transmit EM frequencies through conductive material. Techs used RD8100 to detect
passive and transmitted frequencies.
Results: Techs marked out new concrete and probable original concrete using white dashes. Old concrete
was approximately 5" thick with what appears to be wire mesh throughout. New concrete varies depending
on when it was poured, as some have reinforcing and some does not. Anything detected by GPR and
RD8100 are marked in purple. GPR does not differentiate between different utilities so techs are not able to
definitively state what detected objects are.
Next steps: Typically when clearing for soil borings we allow drillers to lay out spots and we clear specific
areas. It appears most utilities run overhead, however we prefer to clear specific areas once laid out by
driller and on site consultant. This allows for the best and safest possible drilling scenario. Therefore we
recommend being on site once drilling areas are laid out.
ADDITIONAL INFORMATION COLLECTED AT JOB SITE
Any relevant and collected data in the form of images and GPS will be attached in the email corresponding with this document.
Links to the collected data are also included at the end of this report.

11330 Vanstory Dr Ste 115D
Huntersville NC 28078
[phone], [phone]
[e-mail]
DATE 05/26/2022 -
TECH(S)Joseph Whitehill
JOB #75576187
PO #
CUSTOMER Mid-South Environmental
SERVICE LOCATION Bessemer City
ADDITIONAL DOCUMENTS
Documents Attached To This Job:
Danalex Building Details.pdf
 The standard reports we do include a PDF & a Google Earth file. The links are in
the space above. They are also included as attachments to the email corresponding
with this document. The Google Earth file can be opened on a phone with the
Google Earth app installed.  If you open it on a computer it will include photos as
well.
The linked folder contains a folder with photos from the site.  If you need an ESRI
or geodatabase file for import into an existing GIS system please do not hesitate to
ask.
ADDITIONAL PICTURES COLLECTED
CUSTOMER MESSAGE
Ground Penetrating Radar & 3D Laser Scanning are technologies designed to gather data for interpretation. These technologies
are limited in their ability by the conditions of any given project. Any information collected by these technologies should be
verified by other available means.
No liability is accepted by iSS. 
For more information on -
Concrete scanning: https://goo.gl/XAsv4E
Utility Locating: https://goo.gl/QbEuWM
This is not an invoice. Invoice will be sent per your company's invoice guidelines.
Attachment B
Geoprobe® Boring Logs
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.5-
SAMPLING
METHOD
GP-1
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
MAY 31,2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
REMARKS/
COMMENTS
1-----" CONCRETE /------1
MACRO-CORE DARK RED CLAY 22.1 PPM-V
4.0-
MACRO-CORE
8.0-
DARK RED, BROWN AND LIGHT BROWN
MOTILED CLAY
83.6 PPM-V
MACRO-CORE DARK RED AND BROWN MOTILED CLAY
MOIST AT 9 FEET BELOW GRADE
83.2 PPM-V
COLLECTED SAMPLE
~---------------~
BORING TERMINATED AT 12.0 FEET
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.67-
SAMPLING
METHOD
GP-2
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
MAY 31, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
REMARKS/
COMMENTS
1--------.., CONCRETE ,,....-----1
MACRO-CORE BLACK TEXTILE FIBERS
2.1 PPM-V
COLLECTED SAMPLE
2.0-
2.5-1-----~C~C:J!::!,CRUE-;_------1
GEOPROBE REFUSAL AT 2.5 FEET
BORING/WELL NO.: GP-3 BORING LOG
PROJECT NAME: FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
PROJECT NO.:
CONTRACTOR:
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.41-
4.0-
7.0-
9.0-
12.0-
13.05-
16.0-
19.0-
20.0-
MAY 31,2022
NOT MEASURED
SAMPLING
METHOD
MACRO-CORE
MACRO-CORE
MACRO-CORE
MACRO-CORE
SAMPLE
DESCRIPTION
1-----., CONCRETE /------1
LIGHT RED, DARK BROWN AND TAN
MOTTLED SILT
RED, TAN AND BLACK MOTTLED SILT
(FILL MATERIAL)
RED AND LIGHT ORANGE SPECKLED CLAY
(MOIST) (RESIDUAL SOIL)
RED AND BROWN MOTTLED SILTY CLAY
MACRO-CORE · RED, BROWN AND WHITE MOTTLED CLAYEY
SILT
1----------------~
BORING TERMINATED AT 20.0 FEET
REMARKS/
COMMENTS
11.0 PPM-V
1,344 PPM-V
COLLECTED SAMPLE
TOP OF WELL SCREEN
78.8 PPM-V
COLLECTED SAMPLE
WATER TABLE
62.5 PPM-V
1,042 PPM-V
BOTTOM OF WELL SCREEN
BORING/WELL NO.: GP-4 BORING LOG
PROJECT NAME: FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
PROJECT NO.:
CONTRACTOR:
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.41 -
4.0-
6.0-
8.0-
10.5-
11.0-
12.0-
[e-mail] MAY 31,2022
NOT MEASURED
SAMPLING
METHOD
MACRO-CORE
MACRO-CORE
MACRO-CORE
MACRO-CORE
SAMPLE
DESCRIPTION
..,__ ____ '-CONCRETE /
TAN AND RED MOTTLED SILT WITH QUARTZ
FRAGMENTS (FILL MATERIAL)
DARK RED CLAY (FILL MATERIAL)
RED CLAY (FILL MATERIAL)
GRAY SAND (FILL MATERIAL)
._ ___ R_E_D_C_LA_YjFIL!:_ M_A_T_ER_I_A...;.L) ___ -1
BORING TERMINATED AT 12.0 FEET
REMARKS/
COMMENTS
0.0 PPM-V
29.1 PPM-V
COLLECTED SAMPLE
0.0 PPM-V
COLLECTED SAMPLE
0.0 PPM-V
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.41-
SAMPLING
METHOD
GP-5
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
MAY 31, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
CONCRETE /-----1
REMARKS/
COMMENTS
0.0 PPM-V
MACRO-CORE TAN AND LIGHT RED SPECKLED SANDY SILT
4.0-(FILL MATERIAL)
0.0 PPM-V
6.0-.RAY SAND 6.5-
MACRO-CORE RED AND TAN MOTTLED CLAY 0.0 PPM-V
8.0-(RESIDUAL SOIL) COLLECTED SAMPLE
MACRO-CORE TAN AND BROWN MOTTLED GRAVELY FINE 0.0 PPM-V
TO COARSE SANDY SILT COLLECTED SAMPLE
12.0 ---
BORING TERMINATED AT 12.0 FEET
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.41-
SAMPLING
METHOD
GP-6
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
MAY 31,2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
, CONCRETE /
REMARKS/
COMMENTS
MACRO-CORE BROWN AND RED MOTTLED CLAY 0.0 PPM-V
4.0-
MACRO-CORE
8.0-
MACRO-CORE
..J
12.0-
BROWN AND RED MOTTLED SILTY CLAY
TAN, LIGHT BROWN AND RED MOTTLED
CLAYEY SILT (MOIST)
1----------------1
BORING TERMINATED AT 12.0 FEET
0.0 PPM-V
COLLECTED SAMPLE
0.0 PPM-V
COLLECTED SAMPLE
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.5-
SAMPLING
METHOD
GP-7
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
MAY 31,2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
REMARKS/
COMMENTS
1-----~, CONCRETE /------1
MACRO-CORI; RED AND TAN SPECKLED SILT
(FILL MATERIAL) 0.0 PPM-V COLLECTED SAMPLE
4.0-
MACRO-CORE
8.0-
MACRO-CORE
12.0 -
RED, TAN AND BLACK MOTTLED SILT
(RESIDUAL SOIL)
RED, TAN AND BLACK MOTTLED SILT (MOIST)
~---------------~
BORING TERMINATED AT 12.0 FEET
0.0 PPM-V COLLECTED SAMPLE
0.0 PPM-V
COLLECTED SAMPLE
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.41-
SAMPLING
METHOD
GP-8
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
MAY 31, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
'-CONCRETE /
REMARKS/
COMMENTS
MACRO-CORE DARK REDDISH BROWN SILT 0.0 PPM-V
4.0-
MACRO-CORE
8.0-
MACRO-CORE
12.0-
TAN, RED AND BLACK MOTTLED SILT (MOIST)
TAN AND LIGHT BROWN MOTTLED SILT
(MOIST)
~-------------------------~
BORING TERMINATED AT 12.0 FEET
0.0 PPM-V
COLLECTED SAMPLE
0.0 PPM-V
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH SAMPLING
(FEET) METHOD
0.5-
GP-9
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
MAY 31,2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
, CONCRETE ~
REMARKS/
COMMENTS
MACRO-CORE HARD RED, TAN AND BROWN MOTTLED SILT 0.0 PPM-V
COLLECTED SAMPLE
4.0-
MACRO-CORE
8.0-
MACRO-CORE
12.0-
DARK BROWN AND RED MOTTLED SILTY CLAY
WITH QUARTZ FRAGMENTS
BROWN SILTY CLAY WITH GRAVEL
FRAGMENTS (WET)
--
BORING TERMINATED AT 12.0 FEET
67.6 PPM-V COLLECTED SAMPLE
520 PPM-V
COLLECTED SAMPLE
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.38-
SAMPLING
METHOD
GP-10
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
'-CONCRETE /
REMARKS/
COMMENTS
MACRO-CORE RED, TAN AND BROWN MOTTLED SILT
(FILL MATERIAL) 0.0 PPM-V
5.0--
MACRO-CORE
8.0-
MACRO-CORE
12.0-
GRAVEL (FILL MATERIAL)
DARK RED SILT (RESIDUAL SOIL)
TAN AND RED MOTTLED SILT
...._ ______ - --------i
BORING TERMINATED AT 12.0 FEET
0.0 PPM-V
0.0 PPM-V
COLLECTED SAMPLE
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.58-
SAMPLING
METHOD
GP-11
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
REMARKS/
COMMENTS
1------, CONCRETE /~-----1
MACRO-CORE RED AND TAN MOTTLED CLAYEY SILT 0.0 PPM-V
COLLECTED SAMPLE
4.0-
MACRO-CORE RED CLAYEY SILT 0.0 PPM-V
8.0-
MACRO-CORE DARK RED AND TAN MOTTLED SILT 0.0 PPM-V
12.0-~---------------~
BORING TERMINATED AT 12.0 FEET
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.46-
SAMPLING
METHOD
GP-12
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
REMARKS/
COMMENTS
t----~, CONCRETE /------1
MACRO-CORE RED AND TAN MOTTLED FINE SANDY 0.0 PPM-V
4.0-
MACRO-CORE
8.0-
MACRO-CORE
12.0-
MICACEOUS SILT WITH QUARTZ GRAVEL SEAM
RED, TAN AND LIGHT BROWN MOTTLED FINE
SANDY SILT
RED, TAN AND LIGHT BROWN FINE SANDY
SILT
1-----------------~
BORING TERMINATED AT 12.0 FEET
3.2 PPM-V
COLLECTED SAMPLE
2.9 PPM-V
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.58-
SAMPLING
METHOD
GP-13
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
REMARKS/
COMMENTS
1------, CONCRETE /------1
MACRO-CORE RED, TAN AND BLACK MOTTLED SILT 0.0 PPM-V
COLLECTED SAMPLE 4.0-
MACRO-CORE
8.0-
MACRO-CORE
12.0 -
ORANGE, RED, BLACK AND TAN MOTTLED
MICACEOUS SILT (MOIST)
RED, TAN AND BLACK MOTTLED SLIGHTLY
MICACEOUS SILT (MOIST)
1-----------------~
BORING TERMINATED AT 12.0 FEET
0.0 PPM-V
0.0 PPM-V
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
SAMPLING
METHOD
GP-14
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
REMARKS/
COMMENTS
0. 71 _ MACRO-CORE CONCRETE
1.0 -'-BLACK TEXTILE FIBERS / --GEOPROBE REFUSAL ON CONCRETE AT
1 FOOT
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.42-0.92-
SAMPLING
METHOD
GP-15
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
CONCRETE
AN \AND
REMARKS/
COMMENTS
MACRO-CORE RED CLAY 0.0 PPM-V
COLLECTED SAMPLE 4.0-
MACRO-CORE RED AND TAN MOTTLED SILT 0.0 PPM-V
8.0-
MACRO-CORE RED AND TAN MOTTLED SILT (MOIST) 0.0 PPM-V
12.0-~-------------------------~
BORING TERMINATED AT 12.0 FEET
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.37-
SAMPLING
METHOD
GP-16
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
CONCRETE
REMARKS/
COMMENTS
MACRO-CORE TAN, BROWN AND RED FINE TO MEDIUM
MOTTLED SANDY SILT 0.0 PPM-V
4.0-
MACRO-CORE
8.0-
MACRO-CORE
12.0-
DARK RED FINE TO COARSE SANDY
MICACEOUS SILT
~-------------------------~
BORING TERMINATED AT 12.0 FEET
0.0 PPM-V
0.0 PPM-V
COLLECTED SAMPLE
BORING/WELL NO.:
PROJECT NAM.E:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.37-
SAMPLING
METHOD
GP-17
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
CONCRETE
REMARKS/
COMMENTS
MACRO-CORE TAN, LIGHT BROWN AND RED MOTTLED FINE
TO COARSE SANDY MICACEOUS SILT 65.2 PPM-V
4.0-
MACRO-CORE
6.0-
8.0-
MACRO-CORE
12.0 -
TAN, LIGHT BROWN AND RED MOTTLED FINE
TO COARSE SANDY CLAY
GRAY FINE TO COARSE SAND
DARK RED SILTY CLAY
-----------------1
BORING TERMINATED AT 12.0 FEET
171 PPM-V
60.4 PPM-V
COLLECTED SAMPLE
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.5-
SAMPLING
METHOD
GP-18
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
CONCRETE
REMARKS/
COMMENTS
MACRO-CORE
BLACK, BROWN AND RED FINE SANDY CLAY
WITH GRAVEL AND TEXTILE FRAGMENTS
(FILL MATERIAL)
0.0 PPM-V
4.0-
MACRO-CORE
8.0-
MACRO-CORE
12.0-
TAN, LIGHT BROWN AND RED MOTTLED FINE
TO COARSE SANDY CLAY
BLACK, TAN AND LIGHT GRAY MOTTLED SILT
(MOIST)
1-----------------1
BORING TERMINATED AT 12.0 FEET
0.0 PPM-V
COLLECTED SAMPLE
0.0 PPM-V
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH SAMPLING
(FEET) METHOD
0.5-
GP-19
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
CONCRETE
REMARKS/
COMMENTS
MACRO-CORE RED CLAY (FILL MATERIAL) 0.0 PPM-V
3.0-
3.5-
4.0-
MACRO-CORE
8.0-
MACRO-CORE
12.0-
GRA-y~([L MA li:K.lALI
RED CLAY FILL MATERIAL)
TAN, GRAY AND ORANGE MOTTLED SILT
(RESIDUAL SOIL)
~-------------------------~
BORING TERMINATED AT 12.0 FEET
0.0 PPM-V
0.0 PPM-V
COLLECTED SAMPLE
BORING/WELL NO.:
PROJECT NAME:
PROJECT NO.:
CONTRACTOR:
OPERATOR:
METHOD:
DATE:
ELEVATION:
DEPTH
(FEET)
0.44-
SAMPLING
METHOD
GP-20
FORMER DANALEX
897-05
MID-ATLANTIC
DON WARREN
GEO-PROBE
JUNE 1, 2022
NOT MEASURED
BORING LOG
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
704-292-4527
[e-mail]
SAMPLE
DESCRIPTION
CONCRETE
REMARKS/
COMMENTS
MACRO-CORE RED CLAYEY SILT 0.0 PPM-V
4.0-
MACRO-CORE
8.0-
MACRO-CORE
12.0 -
ORANGE, RED AND BLACK MOTTLED SILT
(MOIST)
TAN AND LIGHT BROWN MOTTLED SILT
(WET)
..,_ ______ - --------1
BORING TERMINATED AT 12.0 FEET
12.2 PPM-V
COLLECTED SAMPLE
31.5 PPM-V
COLLECTED SAMPLE
Attachment B
Analytical Report and
Chain-of-Custody
#=CL#
June 13, 2022
LIMS USE: FR - RICK HARMON
LIMS OBJECT ID: 92607493
92607493
Project:
Pace Project No.:
RE:
Mr. Rick Harmon
Harmon Environmental
615 Bruce Thomas Road
Monroe, NC 28112
BENMAR 897-05
Dear Mr. Harmon:
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyler Forney
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 135
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 135
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92607493
BENMAR 897-05
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92607493001 GP-1 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493002 GP-3 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493003 GP-3 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493004 GP-4 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493005 GP-4 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493006 GP-5 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493007 GP-6 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493008 GP-7 (0-4)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493009 GP-7 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493010 GP-8 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493011 GP-9 (0.5-4)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493012 GP-9 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493013 GP-9 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493014 GP-2 (2)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493015 GP-5 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493016 GP-6 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493017 GP-10 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493018 GP-11 (0-4)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493019 GP-12 (4-8)EPA 8260D 70 PASI-CLMB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 135
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92607493
BENMAR 897-05
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SW-846 1 PASI-CKDF
92607493020 GP-13 (0-4)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493021 GP-15 (0.5-4)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493022 GP-16 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493023 GP-17 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493024 GP-17 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493025 GP-18 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493026 GP-19 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493027 GP-20 (4-8)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493028 GP-20 (8-12)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92607493029 GP-3 EPA 8260D 63 PASI-CCL
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 135
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92607493
BENMAR 897-05
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92607493001 GP-1 (8-12)
1,1-Dichloroethene 273 ug/kg 06/04/22 12:1746.1EPA 8260D
cis-1,2-Dichloroethene 119 ug/kg 06/04/22 12:1746.1EPA 8260D
Tetrachloroethene 4470 ug/kg 06/04/22 12:1746.1EPA 8260D
Trichloroethene 31800 ug/kg 06/04/22 12:1746.1EPA 8260D
Percent Moisture 33.6 %06/06/22 15:34 N20.10SW-846
92607493002 GP-3 (4-8)
cis-1,2-Dichloroethene 4640 ug/kg 06/08/22 14:172570EPA 8260D
Tetrachloroethene 1260000 ug/kg 06/08/22 14:172570EPA 8260D
Trichloroethene 10100 ug/kg 06/08/22 14:172570EPA 8260D
Percent Moisture 17.6 %06/06/22 15:34 N20.10SW-846
92607493003 GP-3 (8-12)
1,1-Dichloroethane 66.0 ug/kg 06/04/22 13:3226.1EPA 8260D
cis-1,2-Dichloroethene 2370 ug/kg 06/04/22 13:3226.1EPA 8260D
Tetrachloroethene 17000 ug/kg 06/04/22 13:3226.1EPA 8260D
Trichloroethene 1530 ug/kg 06/04/22 13:3226.1EPA 8260D
Percent Moisture 18.2 %06/06/22 15:34 N20.10SW-846
92607493004 GP-4 (4-8)
cis-1,2-Dichloroethene 46500 ug/kg 06/04/22 13:51124EPA 8260D
trans-1,2-Dichloroethene 312 ug/kg 06/04/22 13:51124EPA 8260D
Tetrachloroethene 94900 ug/kg 06/04/22 13:51124EPA 8260D
Trichloroethene 5580 ug/kg 06/04/22 13:51124EPA 8260D
Percent Moisture 18.6 %06/06/22 15:34 N20.10SW-846
92607493005 GP-4 (8-12)
cis-1,2-Dichloroethene 4220 ug/kg 06/04/22 14:1013.5EPA 8260D
trans-1,2-Dichloroethene 101 ug/kg 06/04/22 14:1013.5EPA 8260D
Tetrachloroethene 8390 ug/kg 06/04/22 14:1013.5EPA 8260D
Trichloroethene 1320 ug/kg 06/04/22 14:1013.5EPA 8260D
Percent Moisture 21.2 %06/06/22 15:34 N20.10SW-846
92607493006 GP-5 (4-8)
cis-1,2-Dichloroethene 693 ug/kg 06/04/22 20:426.3EPA 8260D
Tetrachloroethene 713 ug/kg 06/04/22 20:426.3EPA 8260D
Trichloroethene 161 ug/kg 06/04/22 20:426.3EPA 8260D
o-Xylene 8.3 ug/kg 06/04/22 20:426.3EPA 8260D
Percent Moisture 13.2 %06/06/22 15:53 N20.10SW-846
92607493007 GP-6 (4-8)
cis-1,2-Dichloroethene 108 ug/kg 06/04/22 14:2818.3EPA 8260D
Tetrachloroethene 10500 ug/kg 06/04/22 14:2818.3EPA 8260D
Trichloroethene 3530 ug/kg 06/04/22 14:2818.3EPA 8260D
Percent Moisture 33.1 %06/06/22 15:54 N20.10SW-846
92607493008 GP-7 (0-4)
cis-1,2-Dichloroethene 23.6 ug/kg 06/04/22 21:197.8EPA 8260D
Tetrachloroethene 5480 ug/kg 06/04/22 21:19 M17.8EPA 8260D
Trichloroethene 128 ug/kg 06/04/22 21:197.8EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 135
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92607493
BENMAR 897-05
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92607493008 GP-7 (0-4)
Percent Moisture 24.8 %06/06/22 15:54 N20.10SW-846
92607493009 GP-7 (4-8)
cis-1,2-Dichloroethene 20.9 ug/kg 06/04/22 11:407.3EPA 8260D
Tetrachloroethene 5140 ug/kg 06/04/22 11:407.3EPA 8260D
1,2,3-Trichlorobenzene 33.8 ug/kg 06/04/22 11:407.3EPA 8260D
Trichloroethene 195 ug/kg 06/04/22 11:407.3EPA 8260D
Percent Moisture 24.3 %06/06/22 15:54 N20.10SW-846
92607493010 GP-8 (4-8)
cis-1,2-Dichloroethene 87.8 ug/kg 06/04/22 20:239.5EPA 8260D
Tetrachloroethene 2010 ug/kg 06/04/22 20:239.5EPA 8260D
Trichloroethene 74.0 ug/kg 06/04/22 20:239.5EPA 8260D
Percent Moisture 26.5 %06/06/22 15:54 N20.10SW-846
92607493011 GP-9 (0.5-4)
Chlorobenzene 67.6 ug/kg 06/04/22 14:4736.2EPA 8260D
1,1-Dichloroethene 116 ug/kg 06/04/22 14:4736.2EPA 8260D
cis-1,2-Dichloroethene 80.0 ug/kg 06/04/22 14:4736.2EPA 8260D
Tetrachloroethene 22400 ug/kg 06/04/22 14:4736.2EPA 8260D
Trichloroethene 5910 ug/kg 06/04/22 14:4736.2EPA 8260D
Percent Moisture 24.9 %06/06/22 15:54 N20.10SW-846
92607493012 GP-9 (4-8)
Tetrachloroethene 506000 ug/kg 06/06/22 19:40860EPA 8260D
Trichloroethene 17800 ug/kg 06/06/22 19:40860EPA 8260D
Percent Moisture 27.4 %06/06/22 15:54 N20.10SW-846
92607493013 GP-9 (8-12)
Tetrachloroethene 2190000 ug/kg 06/06/22 19:583110EPA 8260D
Trichloroethene 136000 ug/kg 06/06/22 19:583110EPA 8260D
Percent Moisture 41.5 %06/06/22 15:54 N20.10SW-846
92607493014 GP-2 (2)
cis-1,2-Dichloroethene 7570 ug/kg 06/06/22 20:152990EPA 8260D
Tetrachloroethene 1950000 ug/kg 06/06/22 20:152990EPA 8260D
Trichloroethene 36800 ug/kg 06/06/22 20:152990EPA 8260D
Percent Moisture 33.6 %06/06/22 15:55 N20.10SW-846
92607493015 GP-5 (8-12)
cis-1,2-Dichloroethene 976 ug/kg 06/03/22 21:027.2EPA 8260D
trans-1,2-Dichloroethene 31.7 ug/kg 06/03/22 21:027.2EPA 8260D
Tetrachloroethene 5100 ug/kg 06/03/22 21:027.2EPA 8260D
Trichloroethene 149 ug/kg 06/03/22 21:027.2EPA 8260D
Percent Moisture 21.0 %06/06/22 15:55 N20.10SW-846
92607493016 GP-6 (8-12)
cis-1,2-Dichloroethene 53.3 ug/kg 06/03/22 21:409.1EPA 8260D
Tetrachloroethene 4850 ug/kg 06/03/22 21:40 M19.1EPA 8260D
Trichloroethene 1330 ug/kg 06/03/22 21:40 M19.1EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 135
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92607493
BENMAR 897-05
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92607493016 GP-6 (8-12)
Percent Moisture 30.5 %06/06/22 15:55 N20.10SW-846
92607493017 GP-10 (8-12)
cis-1,2-Dichloroethene 88.0 ug/kg 06/03/22 21:597.2EPA 8260D
Tetrachloroethene 152 ug/kg 06/03/22 21:597.2EPA 8260D
Trichloroethene 10.0 ug/kg 06/03/22 21:597.2EPA 8260D
Percent Moisture 22.5 %06/06/22 15:55 N20.10SW-846
92607493018 GP-11 (0-4)
Tetrachloroethene 63.6 ug/kg 06/03/22 22:175.0EPA 8260D
Percent Moisture 5.0 %06/06/22 15:55 N20.10SW-846
92607493019 GP-12 (4-8)
cis-1,2-Dichloroethene 39.5 ug/kg 06/03/22 22:367.0EPA 8260D
Tetrachloroethene 744 ug/kg 06/03/22 22:367.0EPA 8260D
Trichloroethene 14.3 ug/kg 06/03/22 22:367.0EPA 8260D
o-Xylene 7.6 ug/kg 06/03/22 22:367.0EPA 8260D
Percent Moisture 17.3 %06/06/22 15:55 N20.10SW-846
92607493020 GP-13 (0-4)
Tetrachloroethene 135 ug/kg 06/03/22 22:547.6EPA 8260D
Percent Moisture 25.1 %06/06/22 15:55 N20.10SW-846
92607493021 GP-15 (0.5-4)
Tetrachloroethene 137 ug/kg 06/03/22 23:137.2EPA 8260D
Percent Moisture 20.6 %06/06/22 15:55 N20.10SW-846
92607493022 GP-16 (8-12)
Tetrachloroethene 42.2 ug/kg 06/03/22 23:326.1EPA 8260D
Percent Moisture 19.6 %06/06/22 15:55 N20.10SW-846
92607493023 GP-17 (4-8)
Chlorobenzene 39.1 ug/kg 06/06/22 20:5129.2EPA 8260D
cis-1,2-Dichloroethene 20300 ug/kg 06/06/22 20:5129.2EPA 8260D
trans-1,2-Dichloroethene 176 ug/kg 06/06/22 20:5129.2EPA 8260D
Methylene Chloride 121 ug/kg 06/06/22 20:51 C7117EPA 8260D
Tetrachloroethene 3340 ug/kg 06/06/22 20:5129.2EPA 8260D
Trichloroethene 531 ug/kg 06/06/22 20:5129.2EPA 8260D
Percent Moisture 13.3 %06/06/22 15:55 N20.10SW-846
92607493024 GP-17 (8-12)
cis-1,2-Dichloroethene 19400 ug/kg 06/06/22 21:2630.5EPA 8260D
trans-1,2-Dichloroethene 134 ug/kg 06/06/22 21:2630.5EPA 8260D
Tetrachloroethene 1040 ug/kg 06/06/22 21:2630.5EPA 8260D
Trichloroethene 539 ug/kg 06/06/22 21:2630.5EPA 8260D
Percent Moisture 18.2 %06/06/22 15:56 N20.10SW-846
92607493025 GP-18 (4-8)
Tetrachloroethene 76.4 ug/kg 06/06/22 17:545.8EPA 8260D
Percent Moisture 17.7 %06/06/22 15:56 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 135
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92607493
BENMAR 897-05
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92607493026 GP-19 (8-12)
cis-1,2-Dichloroethene 71.7 ug/kg 06/06/22 18:126.5EPA 8260D
Tetrachloroethene 719 ug/kg 06/06/22 18:126.5EPA 8260D
Trichloroethene 29.3 ug/kg 06/06/22 18:126.5EPA 8260D
o-Xylene 6.9 ug/kg 06/06/22 18:126.5EPA 8260D
Percent Moisture 22.1 %06/06/22 16:17 N20.10SW-846
92607493027 GP-20 (4-8)
cis-1,2-Dichloroethene 394 ug/kg 06/08/22 00:2518.2EPA 8260D
Methylene Chloride 328 ug/kg 06/08/22 00:25 C972.7EPA 8260D
Tetrachloroethene 12600 ug/kg 06/08/22 00:2518.2EPA 8260D
Trichloroethene 107 ug/kg 06/08/22 00:2518.2EPA 8260D
Percent Moisture 31.0 %06/06/22 16:17 N20.10SW-846
92607493028 GP-20 (8-12)
cis-1,2-Dichloroethene 662 ug/kg 06/08/22 01:0041.2EPA 8260D
Methylene Chloride 4460 ug/kg 06/08/22 01:00 C9165EPA 8260D
Tetrachloroethene 19300 ug/kg 06/08/22 01:0041.2EPA 8260D
Trichloroethene 174 ug/kg 06/08/22 01:0041.2EPA 8260D
Percent Moisture 36.3 %06/06/22 16:17 N20.10SW-846
92607493029 GP-3
cis-1,2-Dichloroethene 7690 ug/L 06/06/22 22:591000EPA 8260D
Tetrachloroethene 124000 ug/L 06/06/22 22:591000EPA 8260D
Trichloroethene 4490 ug/L 06/06/22 22:591000EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
General Information:
28 samples were analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A/5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
QC Batch: 702038
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3664140)
• Bromomethane
• DUP (Lab ID: 3664142)
• Bromomethane
• GP-10 (8-12) (Lab ID: 92607493017)
• Bromomethane
• GP-11 (0-4) (Lab ID: 92607493018)
• Bromomethane
• GP-12 (4-8) (Lab ID: 92607493019)
• Bromomethane
• GP-13 (0-4) (Lab ID: 92607493020)
• Bromomethane
• GP-15 (0.5-4) (Lab ID: 92607493021)
• Bromomethane
• GP-16 (8-12) (Lab ID: 92607493022)
• Bromomethane
• GP-5 (8-12) (Lab ID: 92607493015)
• Bromomethane
• GP-6 (8-12) (Lab ID: 92607493016)
• Bromomethane
• LCS (Lab ID: 3664141)
• Bromomethane
• MS (Lab ID: 3664143)
• Bromomethane
QC Batch: 702238
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3664946)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702238
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• Bromomethane
• DUP (Lab ID: 3664948)
• Bromomethane
• GP-5 (4-8) (Lab ID: 92607493006)
• Bromomethane
• GP-7 (0-4) (Lab ID: 92607493008)
• Bromomethane
• GP-8 (4-8) (Lab ID: 92607493010)
• Bromomethane
• LCS (Lab ID: 3664947)
• Bromomethane
• MS (Lab ID: 3664949)
• Bromomethane
QC Batch: 702295
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3665360)
• Bromomethane
• GP-17 (4-8) (Lab ID: 92607493023)
• Bromomethane
• GP-17 (8-12) (Lab ID: 92607493024)
• Bromomethane
• GP-18 (4-8) (Lab ID: 92607493025)
• Bromomethane
• GP-19 (8-12) (Lab ID: 92607493026)
• Bromomethane
• GP-2 (2) (Lab ID: 92607493014)
• Bromomethane
• GP-9 (4-8) (Lab ID: 92607493012)
• Bromomethane
• GP-9 (8-12) (Lab ID: 92607493013)
• Bromomethane
• LCS (Lab ID: 3665361)
• Bromomethane
• MS (Lab ID: 3666182)
• Bromomethane
• MSD (Lab ID: 3666183)
• Bromomethane
QC Batch: 702338
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3665455)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702338
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• Bromomethane
• DUP (Lab ID: 3665457)
• Bromomethane
• GP-1 (8-12) (Lab ID: 92607493001)
• Bromomethane
• GP-3 (8-12) (Lab ID: 92607493003)
• Bromomethane
• GP-4 (4-8) (Lab ID: 92607493004)
• Bromomethane
• GP-4 (8-12) (Lab ID: 92607493005)
• Bromomethane
• GP-6 (4-8) (Lab ID: 92607493007)
• Bromomethane
• GP-7 (4-8) (Lab ID: 92607493009)
• Bromomethane
• GP-9 (0.5-4) (Lab ID: 92607493011)
• Bromomethane
• LCS (Lab ID: 3665456)
• Bromomethane
• MS (Lab ID: 3665458)
• Bromomethane
QC Batch: 702818
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3667863)
• Bromomethane
• DUP (Lab ID: 3667866)
• Bromomethane
• GP-20 (4-8) (Lab ID: 92607493027)
• Bromomethane
• GP-20 (8-12) (Lab ID: 92607493028)
• Bromomethane
• LCS (Lab ID: 3667864)
• Bromomethane
• MS (Lab ID: 3667865)
• Bromomethane
QC Batch: 702875
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3668242)
• Bromomethane
• DUP (Lab ID: 3668245)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702875
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• Bromomethane
• GP-3 (4-8) (Lab ID: 92607493002)
• Bromomethane
• LCS (Lab ID: 3668243)
• Bromomethane
• MS (Lab ID: 3668244)
• Bromomethane
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 702038
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3664140)
• Dichlorodifluoromethane
• Vinyl chloride
• DUP (Lab ID: 3664142)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-10 (8-12) (Lab ID: 92607493017)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-11 (0-4) (Lab ID: 92607493018)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-12 (4-8) (Lab ID: 92607493019)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-13 (0-4) (Lab ID: 92607493020)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-15 (0.5-4) (Lab ID: 92607493021)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-16 (8-12) (Lab ID: 92607493022)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-5 (8-12) (Lab ID: 92607493015)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-6 (8-12) (Lab ID: 92607493016)
• Dichlorodifluoromethane
• Vinyl chloride
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702038
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• LCS (Lab ID: 3664141)
• Dichlorodifluoromethane
• Vinyl chloride
• MS (Lab ID: 3664143)
• Dichlorodifluoromethane
• Vinyl chloride
QC Batch: 702238
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3664946)
• Bromoform
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Styrene
• Vinyl chloride
• DUP (Lab ID: 3664948)
• Bromoform
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Styrene
• Vinyl chloride
• GP-5 (4-8) (Lab ID: 92607493006)
• Bromoform
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Styrene
• Vinyl chloride
• GP-7 (0-4) (Lab ID: 92607493008)
• Bromoform
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Styrene
• Vinyl chloride
• GP-8 (4-8) (Lab ID: 92607493010)
• Bromoform
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Styrene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702238
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• Vinyl chloride
• LCS (Lab ID: 3664947)
• Bromoform
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Styrene
• Vinyl chloride
• MS (Lab ID: 3664949)
• Dichlorodifluoromethane
• Vinyl chloride
QC Batch: 702295
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3665360)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
• GP-17 (4-8) (Lab ID: 92607493023)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
• GP-17 (8-12) (Lab ID: 92607493024)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
• GP-18 (4-8) (Lab ID: 92607493025)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
• GP-19 (8-12) (Lab ID: 92607493026)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
• GP-2 (2) (Lab ID: 92607493014)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702295
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• Vinyl chloride
• GP-9 (4-8) (Lab ID: 92607493012)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
• GP-9 (8-12) (Lab ID: 92607493013)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
• LCS (Lab ID: 3665361)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
• MS (Lab ID: 3666182)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
• MSD (Lab ID: 3666183)
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Vinyl chloride
QC Batch: 702338
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3665455)
• Dichlorodifluoromethane
• Vinyl chloride
• DUP (Lab ID: 3665457)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-1 (8-12) (Lab ID: 92607493001)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-3 (8-12) (Lab ID: 92607493003)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-4 (4-8) (Lab ID: 92607493004)
• Dichlorodifluoromethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702338
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• Vinyl chloride
• GP-4 (8-12) (Lab ID: 92607493005)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-6 (4-8) (Lab ID: 92607493007)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-7 (4-8) (Lab ID: 92607493009)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-9 (0.5-4) (Lab ID: 92607493011)
• Dichlorodifluoromethane
• Vinyl chloride
• LCS (Lab ID: 3665456)
• Dichlorodifluoromethane
• Vinyl chloride
• MS (Lab ID: 3665458)
• Dichlorodifluoromethane
• Vinyl chloride
QC Batch: 702818
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3667863)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-20 (4-8) (Lab ID: 92607493027)
• Dichlorodifluoromethane
• Vinyl chloride
• GP-20 (8-12) (Lab ID: 92607493028)
• Dichlorodifluoromethane
• Vinyl chloride
• LCS (Lab ID: 3667864)
• Dichlorodifluoromethane
• Vinyl chloride
v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated
samples and the sensitivity of the instrument was verified with a reporting limit check standard.
• DUP (Lab ID: 3667866)
• Bromochloromethane
v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated
samples may have low bias.
• MS (Lab ID: 3667865)
• Bromochloromethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702875
v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated
samples and the sensitivity of the instrument was verified with a reporting limit check standard.
• BLANK (Lab ID: 3668242)
• Bromodichloromethane
• DUP (Lab ID: 3668245)
• Bromodichloromethane
• GP-3 (4-8) (Lab ID: 92607493002)
• Bromodichloromethane
v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated
samples may have low bias.
• LCS (Lab ID: 3668243)
• Bromodichloromethane
• MS (Lab ID: 3668244)
• Bromodichloromethane
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 702238
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
• LCS (Lab ID: 3664947)
• Dichlorodifluoromethane
• Vinyl chloride
QC Batch: 702338
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
• LCS (Lab ID: 3665456)
• Dichlorodifluoromethane
QC Batch: 702818
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
• LCS (Lab ID: 3667864)
• Dichlorodifluoromethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702875
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
• LCS (Lab ID: 3668243)
• Vinyl chloride
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 702038
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92607493016
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3664143)
• Chloromethane
• Tetrachloroethene
• Trichloroethene
QC Batch: 702238
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92607493008
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3664949)
• Tetrachloroethene
QC Batch: 702295
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92607407002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3666182)
• 1,1,1,2-Tetrachloroethane
• 1,1,2,2-Tetrachloroethane
• 1,2,3-Trichloropropane
• 1,2-Dibromoethane (EDB)
• 1,3,5-Trimethylbenzene
• 1,3-Dichlorobenzene
• 1,3-Dichloropropane
• Bromodichloromethane
• Bromoform
• Chloroform
• Dibromochloromethane
• Methyl-tert-butyl ether
• Methylene Chloride
• Tetrachloroethene
• Trichloroethene
• n-Propylbenzene
• MSD (Lab ID: 3666183)
• 1,3,5-Trimethylbenzene
• n-Propylbenzene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702295
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92607407002
R1: RPD value was outside control limits.
• MSD (Lab ID: 3666183)
• Hexachloro-1,3-butadiene
• sec-Butylbenzene
• tert-Butylbenzene
QC Batch: 702338
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92607896001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3665458)
• Chloromethane
QC Batch: 702818
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92607883001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3667865)
• Bromomethane
• Chloromethane
QC Batch: 702875
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92608051001
M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MS (Lab ID: 3668244)
• Vinyl chloride
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3668244)
• 1,1,1,2-Tetrachloroethane
• 1,1,1-Trichloroethane
• 1,1,2,2-Tetrachloroethane
• 1,1,2-Trichloroethane
• 1,1-Dichloroethane
• 1,1-Dichloropropene
• 1,2,3-Trichlorobenzene
• 1,2,3-Trichloropropane
• 1,2,4-Trichlorobenzene
• 1,2,4-Trimethylbenzene
• 1,2-Dibromo-3-chloropropane
• 1,2-Dibromoethane (EDB)
• 1,2-Dichlorobenzene
• 1,2-Dichloroethane
• 1,2-Dichloropropane
• 1,3,5-Trimethylbenzene
• 1,3-Dichlorobenzene
• 1,3-Dichloropropane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
QC Batch: 702875
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92608051001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• 1,4-Dichlorobenzene
• 2-Chlorotoluene
• 4-Chlorotoluene
• Benzene
• Bromobenzene
• Bromochloromethane
• Bromodichloromethane
• Bromoform
• Bromomethane
• Carbon tetrachloride
• Chlorobenzene
• Chloroform
• Chloromethane
• Dibromochloromethane
• Dibromomethane
• Diisopropyl ether
• Ethylbenzene
• Hexachloro-1,3-butadiene
• Isopropylbenzene (Cumene)
• Methyl-tert-butyl ether
• Methylene Chloride
• Styrene
• Tetrachloroethene
• Toluene
• Trichloroethene
• Vinyl acetate
• cis-1,2-Dichloroethene
• cis-1,3-Dichloropropene
• m&p-Xylene
• n-Butylbenzene
• n-Propylbenzene
• o-Xylene
• p-Isopropyltoluene
• sec-Butylbenzene
• tert-Butylbenzene
• trans-1,2-Dichloroethene
• trans-1,3-Dichloropropene
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D/5035A/5030B Volatiles
Analyte Comments:
QC Batch: 702295
C7: Analyte is a possible laboratory contaminant (not present in method blank).
• GP-17 (4-8) (Lab ID: 92607493023)
• Methylene Chloride
QC Batch: 702338
C7: Analyte is a possible laboratory contaminant (not present in method blank).
• DUP (Lab ID: 3665457)
• 2-Butanone (MEK)
QC Batch: 702818
C9: Common Laboratory Contaminant.
• GP-20 (4-8) (Lab ID: 92607493027)
• Methylene Chloride
• GP-20 (8-12) (Lab ID: 92607493028)
• Methylene Chloride
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D MSV Low Level
General Information:
1 sample was analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
QC Batch: 702561
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3666517)
• Bromoform
• GP-3 (Lab ID: 92607493029)
• Bromoform
• LCS (Lab ID: 3666518)
• Bromoform
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 702561
v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated
samples and the sensitivity of the instrument was verified with a reporting limit check standard.
• BLANK (Lab ID: 3666517)
• Bromomethane
• Hexachloro-1,3-butadiene
• GP-3 (Lab ID: 92607493029)
• Bromomethane
• Hexachloro-1,3-butadiene
v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated
samples may have low bias.
• LCS (Lab ID: 3666518)
• Bromomethane
• Hexachloro-1,3-butadiene
• MS (Lab ID: 3666519)
• Bromomethane
• MSD (Lab ID: 3666520)
• Bromomethane
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 135
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Method:
Client:Harmon Environmental
EPA 8260D
Date:June 13, 2022
Description:8260D MSV Low Level
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-1 (8-12)Lab ID:92607493001 Collected:05/31/22 09:55 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 12:17 67-64-106/04/22 04:189225
Benzene ND ug/kg 06/04/22 12:17 71-43-206/04/22 04:1846.1 5
Bromobenzene ND ug/kg 06/04/22 12:17 108-86-106/04/22 04:1846.1 5
Bromochloromethane ND ug/kg 06/04/22 12:17 74-97-506/04/22 04:1846.1 5
Bromodichloromethane ND ug/kg 06/04/22 12:17 75-27-406/04/22 04:1846.1 5
Bromoform ND ug/kg 06/04/22 12:17 75-25-206/04/22 04:1846.1 5
Bromomethane ND ug/kg 06/04/22 12:17 74-83-9 IK06/04/22 04:1892.2 5
2-Butanone (MEK)ND ug/kg 06/04/22 12:17 78-93-306/04/22 04:189225
n-Butylbenzene ND ug/kg 06/04/22 12:17 104-51-806/04/22 04:1846.1 5
sec-Butylbenzene ND ug/kg 06/04/22 12:17 135-98-806/04/22 04:1846.1 5
tert-Butylbenzene ND ug/kg 06/04/22 12:17 98-06-606/04/22 04:1846.1 5
Carbon tetrachloride ND ug/kg 06/04/22 12:17 56-23-506/04/22 04:1846.1 5
Chlorobenzene ND ug/kg 06/04/22 12:17 108-90-706/04/22 04:1846.1 5
Chloroethane ND ug/kg 06/04/22 12:17 75-00-306/04/22 04:1892.2 5
Chloroform ND ug/kg 06/04/22 12:17 67-66-306/04/22 04:1846.1 5
Chloromethane ND ug/kg 06/04/22 12:17 74-87-306/04/22 04:1892.2 5
2-Chlorotoluene ND ug/kg 06/04/22 12:17 95-49-806/04/22 04:1846.1 5
4-Chlorotoluene ND ug/kg 06/04/22 12:17 106-43-406/04/22 04:1846.1 5
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 12:17 96-12-806/04/22 04:1846.1 5
Dibromochloromethane ND ug/kg 06/04/22 12:17 124-48-106/04/22 04:1846.1 5
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 12:17 106-93-406/04/22 04:1846.1 5
Dibromomethane ND ug/kg 06/04/22 12:17 74-95-306/04/22 04:1846.1 5
1,2-Dichlorobenzene ND ug/kg 06/04/22 12:17 95-50-106/04/22 04:1846.1 5
1,3-Dichlorobenzene ND ug/kg 06/04/22 12:17 541-73-106/04/22 04:1846.1 5
1,4-Dichlorobenzene ND ug/kg 06/04/22 12:17 106-46-706/04/22 04:1846.1 5
Dichlorodifluoromethane ND ug/kg 06/04/22 12:17 75-71-8 L1,v106/04/22 04:1892.2 5
1,1-Dichloroethane ND ug/kg 06/04/22 12:17 75-34-306/04/22 04:1846.1 5
1,2-Dichloroethane ND ug/kg 06/04/22 12:17 107-06-206/04/22 04:1846.1 5
1,1-Dichloroethene 273 ug/kg 06/04/22 12:17 75-35-406/04/22 04:1846.1 5
cis-1,2-Dichloroethene 119 ug/kg 06/04/22 12:17 156-59-206/04/22 04:1846.1 5
trans-1,2-Dichloroethene ND ug/kg 06/04/22 12:17 156-60-506/04/22 04:1846.1 5
1,2-Dichloropropane ND ug/kg 06/04/22 12:17 78-87-506/04/22 04:1846.1 5
1,3-Dichloropropane ND ug/kg 06/04/22 12:17 142-28-906/04/22 04:1846.1 5
2,2-Dichloropropane ND ug/kg 06/04/22 12:17 594-20-706/04/22 04:1846.1 5
1,1-Dichloropropene ND ug/kg 06/04/22 12:17 563-58-606/04/22 04:1846.1 5
cis-1,3-Dichloropropene ND ug/kg 06/04/22 12:17 10061-01-506/04/22 04:1846.1 5
trans-1,3-Dichloropropene ND ug/kg 06/04/22 12:17 10061-02-606/04/22 04:1846.1 5
Diisopropyl ether ND ug/kg 06/04/22 12:17 108-20-306/04/22 04:1846.1 5
Ethylbenzene ND ug/kg 06/04/22 12:17 100-41-406/04/22 04:1846.1 5
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 12:17 87-68-306/04/22 04:1892.2 5
2-Hexanone ND ug/kg 06/04/22 12:17 591-78-606/04/22 04:184615
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 12:17 98-82-806/04/22 04:1846.1 5
p-Isopropyltoluene ND ug/kg 06/04/22 12:17 99-87-606/04/22 04:1846.1 5
Methylene Chloride ND ug/kg 06/04/22 12:17 75-09-206/04/22 04:181845
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 12:17 108-10-106/04/22 04:184615
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-1 (8-12)Lab ID:92607493001 Collected:05/31/22 09:55 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 12:17 1634-04-406/04/22 04:1846.1 5
Naphthalene ND ug/kg 06/04/22 12:17 91-20-306/04/22 04:1846.1 5
n-Propylbenzene ND ug/kg 06/04/22 12:17 103-65-106/04/22 04:1846.1 5
Styrene ND ug/kg 06/04/22 12:17 100-42-506/04/22 04:1846.1 5
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 12:17 630-20-606/04/22 04:1846.1 5
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 12:17 79-34-506/04/22 04:1846.1 5
Tetrachloroethene 4470 ug/kg 06/04/22 12:17 127-18-406/04/22 04:1846.1 5
Toluene ND ug/kg 06/04/22 12:17 108-88-306/04/22 04:1846.1 5
1,2,3-Trichlorobenzene ND ug/kg 06/04/22 12:17 87-61-606/04/22 04:1846.1 5
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 12:17 120-82-106/04/22 04:1846.1 5
1,1,1-Trichloroethane ND ug/kg 06/04/22 12:17 71-55-606/04/22 04:1846.1 5
1,1,2-Trichloroethane ND ug/kg 06/04/22 12:17 79-00-506/04/22 04:1846.1 5
Trichloroethene 31800 ug/kg 06/04/22 12:17 79-01-606/04/22 04:1846.1 5
Trichlorofluoromethane ND ug/kg 06/04/22 12:17 75-69-406/04/22 04:1846.1 5
1,2,3-Trichloropropane ND ug/kg 06/04/22 12:17 96-18-406/04/22 04:1846.1 5
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 12:17 95-63-606/04/22 04:1846.1 5
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 12:17 108-67-806/04/22 04:1846.1 5
Vinyl acetate ND ug/kg 06/04/22 12:17 108-05-406/04/22 04:184615
Vinyl chloride ND ug/kg 06/04/22 12:17 75-01-4 v106/04/22 04:1892.2 5
Xylene (Total)ND ug/kg 06/04/22 12:17 1330-20-706/04/22 04:1892.2 5
m&p-Xylene ND ug/kg 06/04/22 12:17 179601-23-106/04/22 04:1892.2 5
o-Xylene ND ug/kg 06/04/22 12:17 95-47-606/04/22 04:1846.1 5
Surrogates
Toluene-d8 (S)96 %06/04/22 12:17 2037-26-506/04/22 04:1870-130 5
4-Bromofluorobenzene (S)99 %06/04/22 12:17 460-00-406/04/22 04:1869-134 5
1,2-Dichloroethane-d4 (S)105 %06/04/22 12:17 17060-07-006/04/22 04:1870-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 33.6 %06/06/22 15:34 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-3 (4-8)Lab ID:92607493002 Collected:05/31/22 10:35 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/08/22 14:17 67-64-106/08/22 13:2351300400
Benzene ND ug/kg 06/08/22 14:17 71-43-206/08/22 13:232570400
Bromobenzene ND ug/kg 06/08/22 14:17 108-86-106/08/22 13:232570400
Bromochloromethane ND ug/kg 06/08/22 14:17 74-97-506/08/22 13:232570400
Bromodichloromethane ND ug/kg 06/08/22 14:17 75-27-4 v206/08/22 13:232570400
Bromoform ND ug/kg 06/08/22 14:17 75-25-206/08/22 13:232570400
Bromomethane ND ug/kg 06/08/22 14:17 74-83-9 IK06/08/22 13:235130400
2-Butanone (MEK)ND ug/kg 06/08/22 14:17 78-93-306/08/22 13:2351300400
n-Butylbenzene ND ug/kg 06/08/22 14:17 104-51-806/08/22 13:232570400
sec-Butylbenzene ND ug/kg 06/08/22 14:17 135-98-806/08/22 13:232570400
tert-Butylbenzene ND ug/kg 06/08/22 14:17 98-06-606/08/22 13:232570400
Carbon tetrachloride ND ug/kg 06/08/22 14:17 56-23-506/08/22 13:232570400
Chlorobenzene ND ug/kg 06/08/22 14:17 108-90-706/08/22 13:232570400
Chloroethane ND ug/kg 06/08/22 14:17 75-00-306/08/22 13:235130400
Chloroform ND ug/kg 06/08/22 14:17 67-66-306/08/22 13:232570400
Chloromethane ND ug/kg 06/08/22 14:17 74-87-306/08/22 13:235130400
2-Chlorotoluene ND ug/kg 06/08/22 14:17 95-49-806/08/22 13:232570400
4-Chlorotoluene ND ug/kg 06/08/22 14:17 106-43-406/08/22 13:232570400
1,2-Dibromo-3-chloropropane ND ug/kg 06/08/22 14:17 96-12-806/08/22 13:232570400
Dibromochloromethane ND ug/kg 06/08/22 14:17 124-48-106/08/22 13:232570400
1,2-Dibromoethane (EDB)ND ug/kg 06/08/22 14:17 106-93-406/08/22 13:232570400
Dibromomethane ND ug/kg 06/08/22 14:17 74-95-306/08/22 13:232570400
1,2-Dichlorobenzene ND ug/kg 06/08/22 14:17 95-50-106/08/22 13:232570400
1,3-Dichlorobenzene ND ug/kg 06/08/22 14:17 541-73-106/08/22 13:232570400
1,4-Dichlorobenzene ND ug/kg 06/08/22 14:17 106-46-706/08/22 13:232570400
Dichlorodifluoromethane ND ug/kg 06/08/22 14:17 75-71-806/08/22 13:235130400
1,1-Dichloroethane ND ug/kg 06/08/22 14:17 75-34-306/08/22 13:232570400
1,2-Dichloroethane ND ug/kg 06/08/22 14:17 107-06-206/08/22 13:232570400
1,1-Dichloroethene ND ug/kg 06/08/22 14:17 75-35-406/08/22 13:232570400
cis-1,2-Dichloroethene 4640 ug/kg 06/08/22 14:17 156-59-206/08/22 13:232570400
trans-1,2-Dichloroethene ND ug/kg 06/08/22 14:17 156-60-506/08/22 13:232570400
1,2-Dichloropropane ND ug/kg 06/08/22 14:17 78-87-506/08/22 13:232570400
1,3-Dichloropropane ND ug/kg 06/08/22 14:17 142-28-906/08/22 13:232570400
2,2-Dichloropropane ND ug/kg 06/08/22 14:17 594-20-706/08/22 13:232570400
1,1-Dichloropropene ND ug/kg 06/08/22 14:17 563-58-606/08/22 13:232570400
cis-1,3-Dichloropropene ND ug/kg 06/08/22 14:17 10061-01-506/08/22 13:232570400
trans-1,3-Dichloropropene ND ug/kg 06/08/22 14:17 10061-02-606/08/22 13:232570400
Diisopropyl ether ND ug/kg 06/08/22 14:17 108-20-306/08/22 13:232570400
Ethylbenzene ND ug/kg 06/08/22 14:17 100-41-406/08/22 13:232570400
Hexachloro-1,3-butadiene ND ug/kg 06/08/22 14:17 87-68-306/08/22 13:235130400
2-Hexanone ND ug/kg 06/08/22 14:17 591-78-606/08/22 13:2325700400
Isopropylbenzene (Cumene)ND ug/kg 06/08/22 14:17 98-82-806/08/22 13:232570400
p-Isopropyltoluene ND ug/kg 06/08/22 14:17 99-87-606/08/22 13:232570400
Methylene Chloride ND ug/kg 06/08/22 14:17 75-09-206/08/22 13:2310300400
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/08/22 14:17 108-10-106/08/22 13:2325700400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-3 (4-8)Lab ID:92607493002 Collected:05/31/22 10:35 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/08/22 14:17 1634-04-406/08/22 13:232570400
Naphthalene ND ug/kg 06/08/22 14:17 91-20-306/08/22 13:232570400
n-Propylbenzene ND ug/kg 06/08/22 14:17 103-65-106/08/22 13:232570400
Styrene ND ug/kg 06/08/22 14:17 100-42-506/08/22 13:232570400
1,1,1,2-Tetrachloroethane ND ug/kg 06/08/22 14:17 630-20-606/08/22 13:232570400
1,1,2,2-Tetrachloroethane ND ug/kg 06/08/22 14:17 79-34-506/08/22 13:232570400
Tetrachloroethene 1260000 ug/kg 06/08/22 14:17 127-18-406/08/22 13:232570400
Toluene ND ug/kg 06/08/22 14:17 108-88-306/08/22 13:232570400
1,2,3-Trichlorobenzene ND ug/kg 06/08/22 14:17 87-61-606/08/22 13:232570400
1,2,4-Trichlorobenzene ND ug/kg 06/08/22 14:17 120-82-106/08/22 13:232570400
1,1,1-Trichloroethane ND ug/kg 06/08/22 14:17 71-55-606/08/22 13:232570400
1,1,2-Trichloroethane ND ug/kg 06/08/22 14:17 79-00-506/08/22 13:232570400
Trichloroethene 10100 ug/kg 06/08/22 14:17 79-01-606/08/22 13:232570400
Trichlorofluoromethane ND ug/kg 06/08/22 14:17 75-69-406/08/22 13:232570400
1,2,3-Trichloropropane ND ug/kg 06/08/22 14:17 96-18-406/08/22 13:232570400
1,2,4-Trimethylbenzene ND ug/kg 06/08/22 14:17 95-63-606/08/22 13:232570400
1,3,5-Trimethylbenzene ND ug/kg 06/08/22 14:17 108-67-806/08/22 13:232570400
Vinyl acetate ND ug/kg 06/08/22 14:17 108-05-406/08/22 13:2325700400
Vinyl chloride ND ug/kg 06/08/22 14:17 75-01-4 L106/08/22 13:235130400
Xylene (Total)ND ug/kg 06/08/22 14:17 1330-20-706/08/22 13:235130400
m&p-Xylene ND ug/kg 06/08/22 14:17 179601-23-106/08/22 13:235130400
o-Xylene ND ug/kg 06/08/22 14:17 95-47-606/08/22 13:232570400
Surrogates
Toluene-d8 (S)97 %06/08/22 14:17 2037-26-506/08/22 13:2370-130 400
4-Bromofluorobenzene (S)100 %06/08/22 14:17 460-00-406/08/22 13:2369-134 400
1,2-Dichloroethane-d4 (S)97 %06/08/22 14:17 17060-07-006/08/22 13:2370-130 400
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.6 %06/06/22 15:34 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-3 (8-12)Lab ID:92607493003 Collected:05/31/22 10:40 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 13:32 67-64-106/04/22 04:185234
Benzene ND ug/kg 06/04/22 13:32 71-43-206/04/22 04:1826.1 4
Bromobenzene ND ug/kg 06/04/22 13:32 108-86-106/04/22 04:1826.1 4
Bromochloromethane ND ug/kg 06/04/22 13:32 74-97-506/04/22 04:1826.1 4
Bromodichloromethane ND ug/kg 06/04/22 13:32 75-27-406/04/22 04:1826.1 4
Bromoform ND ug/kg 06/04/22 13:32 75-25-206/04/22 04:1826.1 4
Bromomethane ND ug/kg 06/04/22 13:32 74-83-9 IK06/04/22 04:1852.3 4
2-Butanone (MEK)ND ug/kg 06/04/22 13:32 78-93-306/04/22 04:185234
n-Butylbenzene ND ug/kg 06/04/22 13:32 104-51-806/04/22 04:1826.1 4
sec-Butylbenzene ND ug/kg 06/04/22 13:32 135-98-806/04/22 04:1826.1 4
tert-Butylbenzene ND ug/kg 06/04/22 13:32 98-06-606/04/22 04:1826.1 4
Carbon tetrachloride ND ug/kg 06/04/22 13:32 56-23-506/04/22 04:1826.1 4
Chlorobenzene ND ug/kg 06/04/22 13:32 108-90-706/04/22 04:1826.1 4
Chloroethane ND ug/kg 06/04/22 13:32 75-00-306/04/22 04:1852.3 4
Chloroform ND ug/kg 06/04/22 13:32 67-66-306/04/22 04:1826.1 4
Chloromethane ND ug/kg 06/04/22 13:32 74-87-306/04/22 04:1852.3 4
2-Chlorotoluene ND ug/kg 06/04/22 13:32 95-49-806/04/22 04:1826.1 4
4-Chlorotoluene ND ug/kg 06/04/22 13:32 106-43-406/04/22 04:1826.1 4
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 13:32 96-12-806/04/22 04:1826.1 4
Dibromochloromethane ND ug/kg 06/04/22 13:32 124-48-106/04/22 04:1826.1 4
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 13:32 106-93-406/04/22 04:1826.1 4
Dibromomethane ND ug/kg 06/04/22 13:32 74-95-306/04/22 04:1826.1 4
1,2-Dichlorobenzene ND ug/kg 06/04/22 13:32 95-50-106/04/22 04:1826.1 4
1,3-Dichlorobenzene ND ug/kg 06/04/22 13:32 541-73-106/04/22 04:1826.1 4
1,4-Dichlorobenzene ND ug/kg 06/04/22 13:32 106-46-706/04/22 04:1826.1 4
Dichlorodifluoromethane ND ug/kg 06/04/22 13:32 75-71-8 L1,v106/04/22 04:1852.3 4
1,1-Dichloroethane 66.0 ug/kg 06/04/22 13:32 75-34-306/04/22 04:1826.1 4
1,2-Dichloroethane ND ug/kg 06/04/22 13:32 107-06-206/04/22 04:1826.1 4
1,1-Dichloroethene ND ug/kg 06/04/22 13:32 75-35-406/04/22 04:1826.1 4
cis-1,2-Dichloroethene 2370 ug/kg 06/04/22 13:32 156-59-206/04/22 04:1826.1 4
trans-1,2-Dichloroethene ND ug/kg 06/04/22 13:32 156-60-506/04/22 04:1826.1 4
1,2-Dichloropropane ND ug/kg 06/04/22 13:32 78-87-506/04/22 04:1826.1 4
1,3-Dichloropropane ND ug/kg 06/04/22 13:32 142-28-906/04/22 04:1826.1 4
2,2-Dichloropropane ND ug/kg 06/04/22 13:32 594-20-706/04/22 04:1826.1 4
1,1-Dichloropropene ND ug/kg 06/04/22 13:32 563-58-606/04/22 04:1826.1 4
cis-1,3-Dichloropropene ND ug/kg 06/04/22 13:32 10061-01-506/04/22 04:1826.1 4
trans-1,3-Dichloropropene ND ug/kg 06/04/22 13:32 10061-02-606/04/22 04:1826.1 4
Diisopropyl ether ND ug/kg 06/04/22 13:32 108-20-306/04/22 04:1826.1 4
Ethylbenzene ND ug/kg 06/04/22 13:32 100-41-406/04/22 04:1826.1 4
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 13:32 87-68-306/04/22 04:1852.3 4
2-Hexanone ND ug/kg 06/04/22 13:32 591-78-606/04/22 04:182614
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 13:32 98-82-806/04/22 04:1826.1 4
p-Isopropyltoluene ND ug/kg 06/04/22 13:32 99-87-606/04/22 04:1826.1 4
Methylene Chloride ND ug/kg 06/04/22 13:32 75-09-206/04/22 04:181054
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 13:32 108-10-106/04/22 04:182614
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-3 (8-12)Lab ID:92607493003 Collected:05/31/22 10:40 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 13:32 1634-04-406/04/22 04:1826.1 4
Naphthalene ND ug/kg 06/04/22 13:32 91-20-306/04/22 04:1826.1 4
n-Propylbenzene ND ug/kg 06/04/22 13:32 103-65-106/04/22 04:1826.1 4
Styrene ND ug/kg 06/04/22 13:32 100-42-506/04/22 04:1826.1 4
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 13:32 630-20-606/04/22 04:1826.1 4
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 13:32 79-34-506/04/22 04:1826.1 4
Tetrachloroethene 17000 ug/kg 06/04/22 13:32 127-18-406/04/22 04:1826.1 4
Toluene ND ug/kg 06/04/22 13:32 108-88-306/04/22 04:1826.1 4
1,2,3-Trichlorobenzene ND ug/kg 06/04/22 13:32 87-61-606/04/22 04:1826.1 4
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 13:32 120-82-106/04/22 04:1826.1 4
1,1,1-Trichloroethane ND ug/kg 06/04/22 13:32 71-55-606/04/22 04:1826.1 4
1,1,2-Trichloroethane ND ug/kg 06/04/22 13:32 79-00-506/04/22 04:1826.1 4
Trichloroethene 1530 ug/kg 06/04/22 13:32 79-01-606/04/22 04:1826.1 4
Trichlorofluoromethane ND ug/kg 06/04/22 13:32 75-69-406/04/22 04:1826.1 4
1,2,3-Trichloropropane ND ug/kg 06/04/22 13:32 96-18-406/04/22 04:1826.1 4
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 13:32 95-63-606/04/22 04:1826.1 4
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 13:32 108-67-806/04/22 04:1826.1 4
Vinyl acetate ND ug/kg 06/04/22 13:32 108-05-406/04/22 04:182614
Vinyl chloride ND ug/kg 06/04/22 13:32 75-01-4 v106/04/22 04:1852.3 4
Xylene (Total)ND ug/kg 06/04/22 13:32 1330-20-706/04/22 04:1852.3 4
m&p-Xylene ND ug/kg 06/04/22 13:32 179601-23-106/04/22 04:1852.3 4
o-Xylene ND ug/kg 06/04/22 13:32 95-47-606/04/22 04:1826.1 4
Surrogates
Toluene-d8 (S)99 %06/04/22 13:32 2037-26-506/04/22 04:1870-130 4
4-Bromofluorobenzene (S)96 %06/04/22 13:32 460-00-406/04/22 04:1869-134 4
1,2-Dichloroethane-d4 (S)106 %06/04/22 13:32 17060-07-006/04/22 04:1870-130 4
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.2 %06/06/22 15:34 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-4 (4-8)Lab ID:92607493004 Collected:05/31/22 11:06 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 13:51 67-64-106/04/22 04:18247020
Benzene ND ug/kg 06/04/22 13:51 71-43-206/04/22 04:1812420
Bromobenzene ND ug/kg 06/04/22 13:51 108-86-106/04/22 04:1812420
Bromochloromethane ND ug/kg 06/04/22 13:51 74-97-506/04/22 04:1812420
Bromodichloromethane ND ug/kg 06/04/22 13:51 75-27-406/04/22 04:1812420
Bromoform ND ug/kg 06/04/22 13:51 75-25-206/04/22 04:1812420
Bromomethane ND ug/kg 06/04/22 13:51 74-83-9 IK06/04/22 04:1824720
2-Butanone (MEK)ND ug/kg 06/04/22 13:51 78-93-306/04/22 04:18247020
n-Butylbenzene ND ug/kg 06/04/22 13:51 104-51-806/04/22 04:1812420
sec-Butylbenzene ND ug/kg 06/04/22 13:51 135-98-806/04/22 04:1812420
tert-Butylbenzene ND ug/kg 06/04/22 13:51 98-06-606/04/22 04:1812420
Carbon tetrachloride ND ug/kg 06/04/22 13:51 56-23-506/04/22 04:1812420
Chlorobenzene ND ug/kg 06/04/22 13:51 108-90-706/04/22 04:1812420
Chloroethane ND ug/kg 06/04/22 13:51 75-00-306/04/22 04:1824720
Chloroform ND ug/kg 06/04/22 13:51 67-66-306/04/22 04:1812420
Chloromethane ND ug/kg 06/04/22 13:51 74-87-306/04/22 04:1824720
2-Chlorotoluene ND ug/kg 06/04/22 13:51 95-49-806/04/22 04:1812420
4-Chlorotoluene ND ug/kg 06/04/22 13:51 106-43-406/04/22 04:1812420
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 13:51 96-12-806/04/22 04:1812420
Dibromochloromethane ND ug/kg 06/04/22 13:51 124-48-106/04/22 04:1812420
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 13:51 106-93-406/04/22 04:1812420
Dibromomethane ND ug/kg 06/04/22 13:51 74-95-306/04/22 04:1812420
1,2-Dichlorobenzene ND ug/kg 06/04/22 13:51 95-50-106/04/22 04:1812420
1,3-Dichlorobenzene ND ug/kg 06/04/22 13:51 541-73-106/04/22 04:1812420
1,4-Dichlorobenzene ND ug/kg 06/04/22 13:51 106-46-706/04/22 04:1812420
Dichlorodifluoromethane ND ug/kg 06/04/22 13:51 75-71-8 L1,v106/04/22 04:1824720
1,1-Dichloroethane ND ug/kg 06/04/22 13:51 75-34-306/04/22 04:1812420
1,2-Dichloroethane ND ug/kg 06/04/22 13:51 107-06-206/04/22 04:1812420
1,1-Dichloroethene ND ug/kg 06/04/22 13:51 75-35-406/04/22 04:1812420
cis-1,2-Dichloroethene 46500 ug/kg 06/04/22 13:51 156-59-206/04/22 04:1812420
trans-1,2-Dichloroethene 312 ug/kg 06/04/22 13:51 156-60-506/04/22 04:1812420
1,2-Dichloropropane ND ug/kg 06/04/22 13:51 78-87-506/04/22 04:1812420
1,3-Dichloropropane ND ug/kg 06/04/22 13:51 142-28-906/04/22 04:1812420
2,2-Dichloropropane ND ug/kg 06/04/22 13:51 594-20-706/04/22 04:1812420
1,1-Dichloropropene ND ug/kg 06/04/22 13:51 563-58-606/04/22 04:1812420
cis-1,3-Dichloropropene ND ug/kg 06/04/22 13:51 10061-01-506/04/22 04:1812420
trans-1,3-Dichloropropene ND ug/kg 06/04/22 13:51 10061-02-606/04/22 04:1812420
Diisopropyl ether ND ug/kg 06/04/22 13:51 108-20-306/04/22 04:1812420
Ethylbenzene ND ug/kg 06/04/22 13:51 100-41-406/04/22 04:1812420
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 13:51 87-68-306/04/22 04:1824720
2-Hexanone ND ug/kg 06/04/22 13:51 591-78-606/04/22 04:18124020
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 13:51 98-82-806/04/22 04:1812420
p-Isopropyltoluene ND ug/kg 06/04/22 13:51 99-87-606/04/22 04:1812420
Methylene Chloride ND ug/kg 06/04/22 13:51 75-09-206/04/22 04:1849520
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 13:51 108-10-106/04/22 04:18124020
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-4 (4-8)Lab ID:92607493004 Collected:05/31/22 11:06 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 13:51 1634-04-406/04/22 04:1812420
Naphthalene ND ug/kg 06/04/22 13:51 91-20-306/04/22 04:1812420
n-Propylbenzene ND ug/kg 06/04/22 13:51 103-65-106/04/22 04:1812420
Styrene ND ug/kg 06/04/22 13:51 100-42-506/04/22 04:1812420
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 13:51 630-20-606/04/22 04:1812420
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 13:51 79-34-506/04/22 04:1812420
Tetrachloroethene 94900 ug/kg 06/04/22 13:51 127-18-406/04/22 04:1812420
Toluene ND ug/kg 06/04/22 13:51 108-88-306/04/22 04:1812420
1,2,3-Trichlorobenzene ND ug/kg 06/04/22 13:51 87-61-606/04/22 04:1812420
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 13:51 120-82-106/04/22 04:1812420
1,1,1-Trichloroethane ND ug/kg 06/04/22 13:51 71-55-606/04/22 04:1812420
1,1,2-Trichloroethane ND ug/kg 06/04/22 13:51 79-00-506/04/22 04:1812420
Trichloroethene 5580 ug/kg 06/04/22 13:51 79-01-606/04/22 04:1812420
Trichlorofluoromethane ND ug/kg 06/04/22 13:51 75-69-406/04/22 04:1812420
1,2,3-Trichloropropane ND ug/kg 06/04/22 13:51 96-18-406/04/22 04:1812420
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 13:51 95-63-606/04/22 04:1812420
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 13:51 108-67-806/04/22 04:1812420
Vinyl acetate ND ug/kg 06/04/22 13:51 108-05-406/04/22 04:18124020
Vinyl chloride ND ug/kg 06/04/22 13:51 75-01-4 v106/04/22 04:1824720
Xylene (Total)ND ug/kg 06/04/22 13:51 1330-20-706/04/22 04:1824720
m&p-Xylene ND ug/kg 06/04/22 13:51 179601-23-106/04/22 04:1824720
o-Xylene ND ug/kg 06/04/22 13:51 95-47-606/04/22 04:1812420
Surrogates
Toluene-d8 (S)98 %06/04/22 13:51 2037-26-506/04/22 04:1870-130 20
4-Bromofluorobenzene (S)99 %06/04/22 13:51 460-00-406/04/22 04:1869-134 20
1,2-Dichloroethane-d4 (S)105 %06/04/22 13:51 17060-07-006/04/22 04:1870-130 20
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.6 %06/06/22 15:34 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-4 (8-12)Lab ID:92607493005 Collected:05/31/22 11:10 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 14:10 67-64-106/04/22 04:182702
Benzene ND ug/kg 06/04/22 14:10 71-43-206/04/22 04:1813.5 2
Bromobenzene ND ug/kg 06/04/22 14:10 108-86-106/04/22 04:1813.5 2
Bromochloromethane ND ug/kg 06/04/22 14:10 74-97-506/04/22 04:1813.5 2
Bromodichloromethane ND ug/kg 06/04/22 14:10 75-27-406/04/22 04:1813.5 2
Bromoform ND ug/kg 06/04/22 14:10 75-25-206/04/22 04:1813.5 2
Bromomethane ND ug/kg 06/04/22 14:10 74-83-9 IK06/04/22 04:1827.0 2
2-Butanone (MEK)ND ug/kg 06/04/22 14:10 78-93-306/04/22 04:182702
n-Butylbenzene ND ug/kg 06/04/22 14:10 104-51-806/04/22 04:1813.5 2
sec-Butylbenzene ND ug/kg 06/04/22 14:10 135-98-806/04/22 04:1813.5 2
tert-Butylbenzene ND ug/kg 06/04/22 14:10 98-06-606/04/22 04:1813.5 2
Carbon tetrachloride ND ug/kg 06/04/22 14:10 56-23-506/04/22 04:1813.5 2
Chlorobenzene ND ug/kg 06/04/22 14:10 108-90-706/04/22 04:1813.5 2
Chloroethane ND ug/kg 06/04/22 14:10 75-00-306/04/22 04:1827.0 2
Chloroform ND ug/kg 06/04/22 14:10 67-66-306/04/22 04:1813.5 2
Chloromethane ND ug/kg 06/04/22 14:10 74-87-306/04/22 04:1827.0 2
2-Chlorotoluene ND ug/kg 06/04/22 14:10 95-49-806/04/22 04:1813.5 2
4-Chlorotoluene ND ug/kg 06/04/22 14:10 106-43-406/04/22 04:1813.5 2
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 14:10 96-12-806/04/22 04:1813.5 2
Dibromochloromethane ND ug/kg 06/04/22 14:10 124-48-106/04/22 04:1813.5 2
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 14:10 106-93-406/04/22 04:1813.5 2
Dibromomethane ND ug/kg 06/04/22 14:10 74-95-306/04/22 04:1813.5 2
1,2-Dichlorobenzene ND ug/kg 06/04/22 14:10 95-50-106/04/22 04:1813.5 2
1,3-Dichlorobenzene ND ug/kg 06/04/22 14:10 541-73-106/04/22 04:1813.5 2
1,4-Dichlorobenzene ND ug/kg 06/04/22 14:10 106-46-706/04/22 04:1813.5 2
Dichlorodifluoromethane ND ug/kg 06/04/22 14:10 75-71-8 L1,v106/04/22 04:1827.0 2
1,1-Dichloroethane ND ug/kg 06/04/22 14:10 75-34-306/04/22 04:1813.5 2
1,2-Dichloroethane ND ug/kg 06/04/22 14:10 107-06-206/04/22 04:1813.5 2
1,1-Dichloroethene ND ug/kg 06/04/22 14:10 75-35-406/04/22 04:1813.5 2
cis-1,2-Dichloroethene 4220 ug/kg 06/04/22 14:10 156-59-206/04/22 04:1813.5 2
trans-1,2-Dichloroethene 101 ug/kg 06/04/22 14:10 156-60-506/04/22 04:1813.5 2
1,2-Dichloropropane ND ug/kg 06/04/22 14:10 78-87-506/04/22 04:1813.5 2
1,3-Dichloropropane ND ug/kg 06/04/22 14:10 142-28-906/04/22 04:1813.5 2
2,2-Dichloropropane ND ug/kg 06/04/22 14:10 594-20-706/04/22 04:1813.5 2
1,1-Dichloropropene ND ug/kg 06/04/22 14:10 563-58-606/04/22 04:1813.5 2
cis-1,3-Dichloropropene ND ug/kg 06/04/22 14:10 10061-01-506/04/22 04:1813.5 2
trans-1,3-Dichloropropene ND ug/kg 06/04/22 14:10 10061-02-606/04/22 04:1813.5 2
Diisopropyl ether ND ug/kg 06/04/22 14:10 108-20-306/04/22 04:1813.5 2
Ethylbenzene ND ug/kg 06/04/22 14:10 100-41-406/04/22 04:1813.5 2
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 14:10 87-68-306/04/22 04:1827.0 2
2-Hexanone ND ug/kg 06/04/22 14:10 591-78-606/04/22 04:181352
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 14:10 98-82-806/04/22 04:1813.5 2
p-Isopropyltoluene ND ug/kg 06/04/22 14:10 99-87-606/04/22 04:1813.5 2
Methylene Chloride ND ug/kg 06/04/22 14:10 75-09-206/04/22 04:1854.0 2
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 14:10 108-10-106/04/22 04:181352
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-4 (8-12)Lab ID:92607493005 Collected:05/31/22 11:10 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 14:10 1634-04-406/04/22 04:1813.5 2
Naphthalene ND ug/kg 06/04/22 14:10 91-20-306/04/22 04:1813.5 2
n-Propylbenzene ND ug/kg 06/04/22 14:10 103-65-106/04/22 04:1813.5 2
Styrene ND ug/kg 06/04/22 14:10 100-42-506/04/22 04:1813.5 2
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 14:10 630-20-606/04/22 04:1813.5 2
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 14:10 79-34-506/04/22 04:1813.5 2
Tetrachloroethene 8390 ug/kg 06/04/22 14:10 127-18-406/04/22 04:1813.5 2
Toluene ND ug/kg 06/04/22 14:10 108-88-306/04/22 04:1813.5 2
1,2,3-Trichlorobenzene ND ug/kg 06/04/22 14:10 87-61-606/04/22 04:1813.5 2
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 14:10 120-82-106/04/22 04:1813.5 2
1,1,1-Trichloroethane ND ug/kg 06/04/22 14:10 71-55-606/04/22 04:1813.5 2
1,1,2-Trichloroethane ND ug/kg 06/04/22 14:10 79-00-506/04/22 04:1813.5 2
Trichloroethene 1320 ug/kg 06/04/22 14:10 79-01-606/04/22 04:1813.5 2
Trichlorofluoromethane ND ug/kg 06/04/22 14:10 75-69-406/04/22 04:1813.5 2
1,2,3-Trichloropropane ND ug/kg 06/04/22 14:10 96-18-406/04/22 04:1813.5 2
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 14:10 95-63-606/04/22 04:1813.5 2
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 14:10 108-67-806/04/22 04:1813.5 2
Vinyl acetate ND ug/kg 06/04/22 14:10 108-05-406/04/22 04:181352
Vinyl chloride ND ug/kg 06/04/22 14:10 75-01-4 v106/04/22 04:1827.0 2
Xylene (Total)ND ug/kg 06/04/22 14:10 1330-20-706/04/22 04:1827.0 2
m&p-Xylene ND ug/kg 06/04/22 14:10 179601-23-106/04/22 04:1827.0 2
o-Xylene ND ug/kg 06/04/22 14:10 95-47-606/04/22 04:1813.5 2
Surrogates
Toluene-d8 (S)100 %06/04/22 14:10 2037-26-506/04/22 04:1870-130 2
4-Bromofluorobenzene (S)96 %06/04/22 14:10 460-00-406/04/22 04:1869-134 2
1,2-Dichloroethane-d4 (S)103 %06/04/22 14:10 17060-07-006/04/22 04:1870-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.2 %06/06/22 15:34 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-5 (4-8)Lab ID:92607493006 Collected:05/31/22 11:21 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 20:42 67-64-106/03/22 15:021271
Benzene ND ug/kg 06/04/22 20:42 71-43-206/03/22 15:026.3 1
Bromobenzene ND ug/kg 06/04/22 20:42 108-86-106/03/22 15:026.3 1
Bromochloromethane ND ug/kg 06/04/22 20:42 74-97-506/03/22 15:026.3 1
Bromodichloromethane ND ug/kg 06/04/22 20:42 75-27-406/03/22 15:026.3 1
Bromoform ND ug/kg 06/04/22 20:42 75-25-2 v106/03/22 15:026.3 1
Bromomethane ND ug/kg 06/04/22 20:42 74-83-9 IK06/03/22 15:0212.7 1
2-Butanone (MEK)ND ug/kg 06/04/22 20:42 78-93-306/03/22 15:021271
n-Butylbenzene ND ug/kg 06/04/22 20:42 104-51-806/03/22 15:026.3 1
sec-Butylbenzene ND ug/kg 06/04/22 20:42 135-98-806/03/22 15:026.3 1
tert-Butylbenzene ND ug/kg 06/04/22 20:42 98-06-606/03/22 15:026.3 1
Carbon tetrachloride ND ug/kg 06/04/22 20:42 56-23-506/03/22 15:026.3 1
Chlorobenzene ND ug/kg 06/04/22 20:42 108-90-706/03/22 15:026.3 1
Chloroethane ND ug/kg 06/04/22 20:42 75-00-3 v106/03/22 15:0212.7 1
Chloroform ND ug/kg 06/04/22 20:42 67-66-306/03/22 15:026.3 1
Chloromethane ND ug/kg 06/04/22 20:42 74-87-3 v106/03/22 15:0212.7 1
2-Chlorotoluene ND ug/kg 06/04/22 20:42 95-49-806/03/22 15:026.3 1
4-Chlorotoluene ND ug/kg 06/04/22 20:42 106-43-406/03/22 15:026.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 20:42 96-12-806/03/22 15:026.3 1
Dibromochloromethane ND ug/kg 06/04/22 20:42 124-48-106/03/22 15:026.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 20:42 106-93-406/03/22 15:026.3 1
Dibromomethane ND ug/kg 06/04/22 20:42 74-95-306/03/22 15:026.3 1
1,2-Dichlorobenzene ND ug/kg 06/04/22 20:42 95-50-106/03/22 15:026.3 1
1,3-Dichlorobenzene ND ug/kg 06/04/22 20:42 541-73-106/03/22 15:026.3 1
1,4-Dichlorobenzene ND ug/kg 06/04/22 20:42 106-46-706/03/22 15:026.3 1
Dichlorodifluoromethane ND ug/kg 06/04/22 20:42 75-71-8 L1,v106/03/22 15:0212.7 1
1,1-Dichloroethane ND ug/kg 06/04/22 20:42 75-34-306/03/22 15:026.3 1
1,2-Dichloroethane ND ug/kg 06/04/22 20:42 107-06-206/03/22 15:026.3 1
1,1-Dichloroethene ND ug/kg 06/04/22 20:42 75-35-406/03/22 15:026.3 1
cis-1,2-Dichloroethene 693 ug/kg 06/04/22 20:42 156-59-206/03/22 15:026.3 1
trans-1,2-Dichloroethene ND ug/kg 06/04/22 20:42 156-60-506/03/22 15:026.3 1
1,2-Dichloropropane ND ug/kg 06/04/22 20:42 78-87-506/03/22 15:026.3 1
1,3-Dichloropropane ND ug/kg 06/04/22 20:42 142-28-906/03/22 15:026.3 1
2,2-Dichloropropane ND ug/kg 06/04/22 20:42 594-20-706/03/22 15:026.3 1
1,1-Dichloropropene ND ug/kg 06/04/22 20:42 563-58-606/03/22 15:026.3 1
cis-1,3-Dichloropropene ND ug/kg 06/04/22 20:42 10061-01-506/03/22 15:026.3 1
trans-1,3-Dichloropropene ND ug/kg 06/04/22 20:42 10061-02-606/03/22 15:026.3 1
Diisopropyl ether ND ug/kg 06/04/22 20:42 108-20-306/03/22 15:026.3 1
Ethylbenzene ND ug/kg 06/04/22 20:42 100-41-406/03/22 15:026.3 1
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 20:42 87-68-306/03/22 15:0212.7 1
2-Hexanone ND ug/kg 06/04/22 20:42 591-78-606/03/22 15:0263.4 1
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 20:42 98-82-806/03/22 15:026.3 1
p-Isopropyltoluene ND ug/kg 06/04/22 20:42 99-87-606/03/22 15:026.3 1
Methylene Chloride ND ug/kg 06/04/22 20:42 75-09-206/03/22 15:0225.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 20:42 108-10-106/03/22 15:0263.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 135
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-5 (4-8)Lab ID:92607493006 Collected:05/31/22 11:21 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 20:42 1634-04-406/03/22 15:026.3 1
Naphthalene ND ug/kg 06/04/22 20:42 91-20-306/03/22 15:026.3 1
n-Propylbenzene ND ug/kg 06/04/22 20:42 103-65-106/03/22 15:026.3 1
Styrene ND ug/kg 06/04/22 20:42 100-42-5 v106/03/22 15:026.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 20:42 630-20-606/03/22 15:026.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 20:42 79-34-506/03/22 15:026.3 1
Tetrachloroethene 713 ug/kg 06/04/22 20:42 127-18-406/03/22 15:026.3 1
Toluene ND ug/kg 06/04/22 20:42 108-88-306/03/22 15:026.3 1
1,2,3-Trichlorobenzene ND ug/kg 06/04/22 20:42 87-61-606/03/22 15:026.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 20:42 120-82-106/03/22 15:026.3 1
1,1,1-Trichloroethane ND ug/kg 06/04/22 20:42 71-55-606/03/22 15:026.3 1
1,1,2-Trichloroethane ND ug/kg 06/04/22 20:42 79-00-506/03/22 15:026.3 1
Trichloroethene 161 ug/kg 06/04/22 20:42 79-01-606/03/22 15:026.3 1
Trichlorofluoromethane ND ug/kg 06/04/22 20:42 75-69-406/03/22 15:026.3 1
1,2,3-Trichloropropane ND ug/kg 06/04/22 20:42 96-18-406/03/22 15:026.3 1
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 20:42 95-63-606/03/22 15:026.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 20:42 108-67-806/03/22 15:026.3 1
Vinyl acetate ND ug/kg 06/04/22 20:42 108-05-406/03/22 15:0263.4 1
Vinyl chloride ND ug/kg 06/04/22 20:42 75-01-4 L1,v106/03/22 15:0212.7 1
Xylene (Total)ND ug/kg 06/04/22 20:42 1330-20-706/03/22 15:0212.7 1
m&p-Xylene ND ug/kg 06/04/22 20:42 179601-23-106/03/22 15:0212.7 1
o-Xylene 8.3 ug/kg 06/04/22 20:42 95-47-606/03/22 15:026.3 1
Surrogates
Toluene-d8 (S)101 %06/04/22 20:42 2037-26-506/03/22 15:0270-130 1
4-Bromofluorobenzene (S)98 %06/04/22 20:42 460-00-406/03/22 15:0269-134 1
1,2-Dichloroethane-d4 (S)102 %06/04/22 20:42 17060-07-006/03/22 15:0270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.2 %06/06/22 15:53 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-6 (4-8)Lab ID:92607493007 Collected:05/31/22 11:26 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 14:28 67-64-106/04/22 04:183672
Benzene ND ug/kg 06/04/22 14:28 71-43-206/04/22 04:1818.3 2
Bromobenzene ND ug/kg 06/04/22 14:28 108-86-106/04/22 04:1818.3 2
Bromochloromethane ND ug/kg 06/04/22 14:28 74-97-506/04/22 04:1818.3 2
Bromodichloromethane ND ug/kg 06/04/22 14:28 75-27-406/04/22 04:1818.3 2
Bromoform ND ug/kg 06/04/22 14:28 75-25-206/04/22 04:1818.3 2
Bromomethane ND ug/kg 06/04/22 14:28 74-83-9 IK06/04/22 04:1836.7 2
2-Butanone (MEK)ND ug/kg 06/04/22 14:28 78-93-306/04/22 04:183672
n-Butylbenzene ND ug/kg 06/04/22 14:28 104-51-806/04/22 04:1818.3 2
sec-Butylbenzene ND ug/kg 06/04/22 14:28 135-98-806/04/22 04:1818.3 2
tert-Butylbenzene ND ug/kg 06/04/22 14:28 98-06-606/04/22 04:1818.3 2
Carbon tetrachloride ND ug/kg 06/04/22 14:28 56-23-506/04/22 04:1818.3 2
Chlorobenzene ND ug/kg 06/04/22 14:28 108-90-706/04/22 04:1818.3 2
Chloroethane ND ug/kg 06/04/22 14:28 75-00-306/04/22 04:1836.7 2
Chloroform ND ug/kg 06/04/22 14:28 67-66-306/04/22 04:1818.3 2
Chloromethane ND ug/kg 06/04/22 14:28 74-87-306/04/22 04:1836.7 2
2-Chlorotoluene ND ug/kg 06/04/22 14:28 95-49-806/04/22 04:1818.3 2
4-Chlorotoluene ND ug/kg 06/04/22 14:28 106-43-406/04/22 04:1818.3 2
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 14:28 96-12-806/04/22 04:1818.3 2
Dibromochloromethane ND ug/kg 06/04/22 14:28 124-48-106/04/22 04:1818.3 2
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 14:28 106-93-406/04/22 04:1818.3 2
Dibromomethane ND ug/kg 06/04/22 14:28 74-95-306/04/22 04:1818.3 2
1,2-Dichlorobenzene ND ug/kg 06/04/22 14:28 95-50-106/04/22 04:1818.3 2
1,3-Dichlorobenzene ND ug/kg 06/04/22 14:28 541-73-106/04/22 04:1818.3 2
1,4-Dichlorobenzene ND ug/kg 06/04/22 14:28 106-46-706/04/22 04:1818.3 2
Dichlorodifluoromethane ND ug/kg 06/04/22 14:28 75-71-8 L1,v106/04/22 04:1836.7 2
1,1-Dichloroethane ND ug/kg 06/04/22 14:28 75-34-306/04/22 04:1818.3 2
1,2-Dichloroethane ND ug/kg 06/04/22 14:28 107-06-206/04/22 04:1818.3 2
1,1-Dichloroethene ND ug/kg 06/04/22 14:28 75-35-406/04/22 04:1818.3 2
cis-1,2-Dichloroethene 108 ug/kg 06/04/22 14:28 156-59-206/04/22 04:1818.3 2
trans-1,2-Dichloroethene ND ug/kg 06/04/22 14:28 156-60-506/04/22 04:1818.3 2
1,2-Dichloropropane ND ug/kg 06/04/22 14:28 78-87-506/04/22 04:1818.3 2
1,3-Dichloropropane ND ug/kg 06/04/22 14:28 142-28-906/04/22 04:1818.3 2
2,2-Dichloropropane ND ug/kg 06/04/22 14:28 594-20-706/04/22 04:1818.3 2
1,1-Dichloropropene ND ug/kg 06/04/22 14:28 563-58-606/04/22 04:1818.3 2
cis-1,3-Dichloropropene ND ug/kg 06/04/22 14:28 10061-01-506/04/22 04:1818.3 2
trans-1,3-Dichloropropene ND ug/kg 06/04/22 14:28 10061-02-606/04/22 04:1818.3 2
Diisopropyl ether ND ug/kg 06/04/22 14:28 108-20-306/04/22 04:1818.3 2
Ethylbenzene ND ug/kg 06/04/22 14:28 100-41-406/04/22 04:1818.3 2
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 14:28 87-68-306/04/22 04:1836.7 2
2-Hexanone ND ug/kg 06/04/22 14:28 591-78-606/04/22 04:181832
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 14:28 98-82-806/04/22 04:1818.3 2
p-Isopropyltoluene ND ug/kg 06/04/22 14:28 99-87-606/04/22 04:1818.3 2
Methylene Chloride ND ug/kg 06/04/22 14:28 75-09-206/04/22 04:1873.3 2
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 14:28 108-10-106/04/22 04:181832
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-6 (4-8)Lab ID:92607493007 Collected:05/31/22 11:26 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 14:28 1634-04-406/04/22 04:1818.3 2
Naphthalene ND ug/kg 06/04/22 14:28 91-20-306/04/22 04:1818.3 2
n-Propylbenzene ND ug/kg 06/04/22 14:28 103-65-106/04/22 04:1818.3 2
Styrene ND ug/kg 06/04/22 14:28 100-42-506/04/22 04:1818.3 2
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 14:28 630-20-606/04/22 04:1818.3 2
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 14:28 79-34-506/04/22 04:1818.3 2
Tetrachloroethene 10500 ug/kg 06/04/22 14:28 127-18-406/04/22 04:1818.3 2
Toluene ND ug/kg 06/04/22 14:28 108-88-306/04/22 04:1818.3 2
1,2,3-Trichlorobenzene ND ug/kg 06/04/22 14:28 87-61-606/04/22 04:1818.3 2
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 14:28 120-82-106/04/22 04:1818.3 2
1,1,1-Trichloroethane ND ug/kg 06/04/22 14:28 71-55-606/04/22 04:1818.3 2
1,1,2-Trichloroethane ND ug/kg 06/04/22 14:28 79-00-506/04/22 04:1818.3 2
Trichloroethene 3530 ug/kg 06/04/22 14:28 79-01-606/04/22 04:1818.3 2
Trichlorofluoromethane ND ug/kg 06/04/22 14:28 75-69-406/04/22 04:1818.3 2
1,2,3-Trichloropropane ND ug/kg 06/04/22 14:28 96-18-406/04/22 04:1818.3 2
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 14:28 95-63-606/04/22 04:1818.3 2
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 14:28 108-67-806/04/22 04:1818.3 2
Vinyl acetate ND ug/kg 06/04/22 14:28 108-05-406/04/22 04:181832
Vinyl chloride ND ug/kg 06/04/22 14:28 75-01-4 v106/04/22 04:1836.7 2
Xylene (Total)ND ug/kg 06/04/22 14:28 1330-20-706/04/22 04:1836.7 2
m&p-Xylene ND ug/kg 06/04/22 14:28 179601-23-106/04/22 04:1836.7 2
o-Xylene ND ug/kg 06/04/22 14:28 95-47-606/04/22 04:1818.3 2
Surrogates
Toluene-d8 (S)97 %06/04/22 14:28 2037-26-506/04/22 04:1870-130 2
4-Bromofluorobenzene (S)97 %06/04/22 14:28 460-00-406/04/22 04:1869-134 2
1,2-Dichloroethane-d4 (S)105 %06/04/22 14:28 17060-07-006/04/22 04:1870-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 33.1 %06/06/22 15:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-7 (0-4)Lab ID:92607493008 Collected:05/31/22 12:10 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 21:19 67-64-106/03/22 15:021571
Benzene ND ug/kg 06/04/22 21:19 71-43-206/03/22 15:027.8 1
Bromobenzene ND ug/kg 06/04/22 21:19 108-86-106/03/22 15:027.8 1
Bromochloromethane ND ug/kg 06/04/22 21:19 74-97-506/03/22 15:027.8 1
Bromodichloromethane ND ug/kg 06/04/22 21:19 75-27-406/03/22 15:027.8 1
Bromoform ND ug/kg 06/04/22 21:19 75-25-2 v106/03/22 15:027.8 1
Bromomethane ND ug/kg 06/04/22 21:19 74-83-9 IK06/03/22 15:0215.7 1
2-Butanone (MEK)ND ug/kg 06/04/22 21:19 78-93-306/03/22 15:021571
n-Butylbenzene ND ug/kg 06/04/22 21:19 104-51-806/03/22 15:027.8 1
sec-Butylbenzene ND ug/kg 06/04/22 21:19 135-98-806/03/22 15:027.8 1
tert-Butylbenzene ND ug/kg 06/04/22 21:19 98-06-606/03/22 15:027.8 1
Carbon tetrachloride ND ug/kg 06/04/22 21:19 56-23-506/03/22 15:027.8 1
Chlorobenzene ND ug/kg 06/04/22 21:19 108-90-706/03/22 15:027.8 1
Chloroethane ND ug/kg 06/04/22 21:19 75-00-3 v106/03/22 15:0215.7 1
Chloroform ND ug/kg 06/04/22 21:19 67-66-306/03/22 15:027.8 1
Chloromethane ND ug/kg 06/04/22 21:19 74-87-3 v106/03/22 15:0215.7 1
2-Chlorotoluene ND ug/kg 06/04/22 21:19 95-49-806/03/22 15:027.8 1
4-Chlorotoluene ND ug/kg 06/04/22 21:19 106-43-406/03/22 15:027.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 21:19 96-12-806/03/22 15:027.8 1
Dibromochloromethane ND ug/kg 06/04/22 21:19 124-48-106/03/22 15:027.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 21:19 106-93-406/03/22 15:027.8 1
Dibromomethane ND ug/kg 06/04/22 21:19 74-95-306/03/22 15:027.8 1
1,2-Dichlorobenzene ND ug/kg 06/04/22 21:19 95-50-106/03/22 15:027.8 1
1,3-Dichlorobenzene ND ug/kg 06/04/22 21:19 541-73-106/03/22 15:027.8 1
1,4-Dichlorobenzene ND ug/kg 06/04/22 21:19 106-46-706/03/22 15:027.8 1
Dichlorodifluoromethane ND ug/kg 06/04/22 21:19 75-71-8 L1,v106/03/22 15:0215.7 1
1,1-Dichloroethane ND ug/kg 06/04/22 21:19 75-34-306/03/22 15:027.8 1
1,2-Dichloroethane ND ug/kg 06/04/22 21:19 107-06-206/03/22 15:027.8 1
1,1-Dichloroethene ND ug/kg 06/04/22 21:19 75-35-406/03/22 15:027.8 1
cis-1,2-Dichloroethene 23.6 ug/kg 06/04/22 21:19 156-59-206/03/22 15:027.8 1
trans-1,2-Dichloroethene ND ug/kg 06/04/22 21:19 156-60-506/03/22 15:027.8 1
1,2-Dichloropropane ND ug/kg 06/04/22 21:19 78-87-506/03/22 15:027.8 1
1,3-Dichloropropane ND ug/kg 06/04/22 21:19 142-28-906/03/22 15:027.8 1
2,2-Dichloropropane ND ug/kg 06/04/22 21:19 594-20-706/03/22 15:027.8 1
1,1-Dichloropropene ND ug/kg 06/04/22 21:19 563-58-606/03/22 15:027.8 1
cis-1,3-Dichloropropene ND ug/kg 06/04/22 21:19 10061-01-506/03/22 15:027.8 1
trans-1,3-Dichloropropene ND ug/kg 06/04/22 21:19 10061-02-606/03/22 15:027.8 1
Diisopropyl ether ND ug/kg 06/04/22 21:19 108-20-306/03/22 15:027.8 1
Ethylbenzene ND ug/kg 06/04/22 21:19 100-41-406/03/22 15:027.8 1
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 21:19 87-68-306/03/22 15:0215.7 1
2-Hexanone ND ug/kg 06/04/22 21:19 591-78-606/03/22 15:0278.4 1
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 21:19 98-82-806/03/22 15:027.8 1
p-Isopropyltoluene ND ug/kg 06/04/22 21:19 99-87-606/03/22 15:027.8 1
Methylene Chloride ND ug/kg 06/04/22 21:19 75-09-206/03/22 15:0231.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 21:19 108-10-106/03/22 15:0278.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-7 (0-4)Lab ID:92607493008 Collected:05/31/22 12:10 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 21:19 1634-04-406/03/22 15:027.8 1
Naphthalene ND ug/kg 06/04/22 21:19 91-20-306/03/22 15:027.8 1
n-Propylbenzene ND ug/kg 06/04/22 21:19 103-65-106/03/22 15:027.8 1
Styrene ND ug/kg 06/04/22 21:19 100-42-5 v106/03/22 15:027.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 21:19 630-20-606/03/22 15:027.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 21:19 79-34-506/03/22 15:027.8 1
Tetrachloroethene 5480 ug/kg 06/04/22 21:19 127-18-4 M106/03/22 15:027.8 1
Toluene ND ug/kg 06/04/22 21:19 108-88-306/03/22 15:027.8 1
1,2,3-Trichlorobenzene ND ug/kg 06/04/22 21:19 87-61-606/03/22 15:027.8 1
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 21:19 120-82-106/03/22 15:027.8 1
1,1,1-Trichloroethane ND ug/kg 06/04/22 21:19 71-55-606/03/22 15:027.8 1
1,1,2-Trichloroethane ND ug/kg 06/04/22 21:19 79-00-506/03/22 15:027.8 1
Trichloroethene 128 ug/kg 06/04/22 21:19 79-01-606/03/22 15:027.8 1
Trichlorofluoromethane ND ug/kg 06/04/22 21:19 75-69-406/03/22 15:027.8 1
1,2,3-Trichloropropane ND ug/kg 06/04/22 21:19 96-18-406/03/22 15:027.8 1
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 21:19 95-63-606/03/22 15:027.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 21:19 108-67-806/03/22 15:027.8 1
Vinyl acetate ND ug/kg 06/04/22 21:19 108-05-406/03/22 15:0278.4 1
Vinyl chloride ND ug/kg 06/04/22 21:19 75-01-4 L1,v106/03/22 15:0215.7 1
Xylene (Total)ND ug/kg 06/04/22 21:19 1330-20-706/03/22 15:0215.7 1
m&p-Xylene ND ug/kg 06/04/22 21:19 179601-23-106/03/22 15:0215.7 1
o-Xylene ND ug/kg 06/04/22 21:19 95-47-606/03/22 15:027.8 1
Surrogates
Toluene-d8 (S)100 %06/04/22 21:19 2037-26-506/03/22 15:0270-130 1
4-Bromofluorobenzene (S)99 %06/04/22 21:19 460-00-406/03/22 15:0269-134 1
1,2-Dichloroethane-d4 (S)105 %06/04/22 21:19 17060-07-006/03/22 15:0270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.8 %06/06/22 15:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-7 (4-8)Lab ID:92607493009 Collected:05/31/22 12:15 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 11:40 67-64-106/04/22 04:181461
Benzene ND ug/kg 06/04/22 11:40 71-43-206/04/22 04:187.3 1
Bromobenzene ND ug/kg 06/04/22 11:40 108-86-106/04/22 04:187.3 1
Bromochloromethane ND ug/kg 06/04/22 11:40 74-97-506/04/22 04:187.3 1
Bromodichloromethane ND ug/kg 06/04/22 11:40 75-27-406/04/22 04:187.3 1
Bromoform ND ug/kg 06/04/22 11:40 75-25-206/04/22 04:187.3 1
Bromomethane ND ug/kg 06/04/22 11:40 74-83-9 IK06/04/22 04:1814.6 1
2-Butanone (MEK)ND ug/kg 06/04/22 11:40 78-93-306/04/22 04:181461
n-Butylbenzene ND ug/kg 06/04/22 11:40 104-51-806/04/22 04:187.3 1
sec-Butylbenzene ND ug/kg 06/04/22 11:40 135-98-806/04/22 04:187.3 1
tert-Butylbenzene ND ug/kg 06/04/22 11:40 98-06-606/04/22 04:187.3 1
Carbon tetrachloride ND ug/kg 06/04/22 11:40 56-23-506/04/22 04:187.3 1
Chlorobenzene ND ug/kg 06/04/22 11:40 108-90-706/04/22 04:187.3 1
Chloroethane ND ug/kg 06/04/22 11:40 75-00-306/04/22 04:1814.6 1
Chloroform ND ug/kg 06/04/22 11:40 67-66-306/04/22 04:187.3 1
Chloromethane ND ug/kg 06/04/22 11:40 74-87-306/04/22 04:1814.6 1
2-Chlorotoluene ND ug/kg 06/04/22 11:40 95-49-806/04/22 04:187.3 1
4-Chlorotoluene ND ug/kg 06/04/22 11:40 106-43-406/04/22 04:187.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 11:40 96-12-806/04/22 04:187.3 1
Dibromochloromethane ND ug/kg 06/04/22 11:40 124-48-106/04/22 04:187.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 11:40 106-93-406/04/22 04:187.3 1
Dibromomethane ND ug/kg 06/04/22 11:40 74-95-306/04/22 04:187.3 1
1,2-Dichlorobenzene ND ug/kg 06/04/22 11:40 95-50-106/04/22 04:187.3 1
1,3-Dichlorobenzene ND ug/kg 06/04/22 11:40 541-73-106/04/22 04:187.3 1
1,4-Dichlorobenzene ND ug/kg 06/04/22 11:40 106-46-706/04/22 04:187.3 1
Dichlorodifluoromethane ND ug/kg 06/04/22 11:40 75-71-8 L1,v106/04/22 04:1814.6 1
1,1-Dichloroethane ND ug/kg 06/04/22 11:40 75-34-306/04/22 04:187.3 1
1,2-Dichloroethane ND ug/kg 06/04/22 11:40 107-06-206/04/22 04:187.3 1
1,1-Dichloroethene ND ug/kg 06/04/22 11:40 75-35-406/04/22 04:187.3 1
cis-1,2-Dichloroethene 20.9 ug/kg 06/04/22 11:40 156-59-206/04/22 04:187.3 1
trans-1,2-Dichloroethene ND ug/kg 06/04/22 11:40 156-60-506/04/22 04:187.3 1
1,2-Dichloropropane ND ug/kg 06/04/22 11:40 78-87-506/04/22 04:187.3 1
1,3-Dichloropropane ND ug/kg 06/04/22 11:40 142-28-906/04/22 04:187.3 1
2,2-Dichloropropane ND ug/kg 06/04/22 11:40 594-20-706/04/22 04:187.3 1
1,1-Dichloropropene ND ug/kg 06/04/22 11:40 563-58-606/04/22 04:187.3 1
cis-1,3-Dichloropropene ND ug/kg 06/04/22 11:40 10061-01-506/04/22 04:187.3 1
trans-1,3-Dichloropropene ND ug/kg 06/04/22 11:40 10061-02-606/04/22 04:187.3 1
Diisopropyl ether ND ug/kg 06/04/22 11:40 108-20-306/04/22 04:187.3 1
Ethylbenzene ND ug/kg 06/04/22 11:40 100-41-406/04/22 04:187.3 1
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 11:40 87-68-306/04/22 04:1814.6 1
2-Hexanone ND ug/kg 06/04/22 11:40 591-78-606/04/22 04:1873.0 1
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 11:40 98-82-806/04/22 04:187.3 1
p-Isopropyltoluene ND ug/kg 06/04/22 11:40 99-87-606/04/22 04:187.3 1
Methylene Chloride ND ug/kg 06/04/22 11:40 75-09-206/04/22 04:1829.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 11:40 108-10-106/04/22 04:1873.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-7 (4-8)Lab ID:92607493009 Collected:05/31/22 12:15 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 11:40 1634-04-406/04/22 04:187.3 1
Naphthalene ND ug/kg 06/04/22 11:40 91-20-306/04/22 04:187.3 1
n-Propylbenzene ND ug/kg 06/04/22 11:40 103-65-106/04/22 04:187.3 1
Styrene ND ug/kg 06/04/22 11:40 100-42-506/04/22 04:187.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 11:40 630-20-606/04/22 04:187.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 11:40 79-34-506/04/22 04:187.3 1
Tetrachloroethene 5140 ug/kg 06/04/22 11:40 127-18-406/04/22 04:187.3 1
Toluene ND ug/kg 06/04/22 11:40 108-88-306/04/22 04:187.3 1
1,2,3-Trichlorobenzene 33.8 ug/kg 06/04/22 11:40 87-61-606/04/22 04:187.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 11:40 120-82-106/04/22 04:187.3 1
1,1,1-Trichloroethane ND ug/kg 06/04/22 11:40 71-55-606/04/22 04:187.3 1
1,1,2-Trichloroethane ND ug/kg 06/04/22 11:40 79-00-506/04/22 04:187.3 1
Trichloroethene 195 ug/kg 06/04/22 11:40 79-01-606/04/22 04:187.3 1
Trichlorofluoromethane ND ug/kg 06/04/22 11:40 75-69-406/04/22 04:187.3 1
1,2,3-Trichloropropane ND ug/kg 06/04/22 11:40 96-18-406/04/22 04:187.3 1
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 11:40 95-63-606/04/22 04:187.3 1
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 11:40 108-67-806/04/22 04:187.3 1
Vinyl acetate ND ug/kg 06/04/22 11:40 108-05-406/04/22 04:1873.0 1
Vinyl chloride ND ug/kg 06/04/22 11:40 75-01-4 v106/04/22 04:1814.6 1
Xylene (Total)ND ug/kg 06/04/22 11:40 1330-20-706/04/22 04:1814.6 1
m&p-Xylene ND ug/kg 06/04/22 11:40 179601-23-106/04/22 04:1814.6 1
o-Xylene ND ug/kg 06/04/22 11:40 95-47-606/04/22 04:187.3 1
Surrogates
Toluene-d8 (S)100 %06/04/22 11:40 2037-26-506/04/22 04:1870-130 1
4-Bromofluorobenzene (S)99 %06/04/22 11:40 460-00-406/04/22 04:1869-134 1
1,2-Dichloroethane-d4 (S)99 %06/04/22 11:40 17060-07-006/04/22 04:1870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.3 %06/06/22 15:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-8 (4-8)Lab ID:92607493010 Collected:05/31/22 12:35 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 20:23 67-64-106/03/22 15:021901
Benzene ND ug/kg 06/04/22 20:23 71-43-206/03/22 15:029.5 1
Bromobenzene ND ug/kg 06/04/22 20:23 108-86-106/03/22 15:029.5 1
Bromochloromethane ND ug/kg 06/04/22 20:23 74-97-506/03/22 15:029.5 1
Bromodichloromethane ND ug/kg 06/04/22 20:23 75-27-406/03/22 15:029.5 1
Bromoform ND ug/kg 06/04/22 20:23 75-25-2 v106/03/22 15:029.5 1
Bromomethane ND ug/kg 06/04/22 20:23 74-83-9 IK06/03/22 15:0219.0 1
2-Butanone (MEK)ND ug/kg 06/04/22 20:23 78-93-306/03/22 15:021901
n-Butylbenzene ND ug/kg 06/04/22 20:23 104-51-806/03/22 15:029.5 1
sec-Butylbenzene ND ug/kg 06/04/22 20:23 135-98-806/03/22 15:029.5 1
tert-Butylbenzene ND ug/kg 06/04/22 20:23 98-06-606/03/22 15:029.5 1
Carbon tetrachloride ND ug/kg 06/04/22 20:23 56-23-506/03/22 15:029.5 1
Chlorobenzene ND ug/kg 06/04/22 20:23 108-90-706/03/22 15:029.5 1
Chloroethane ND ug/kg 06/04/22 20:23 75-00-3 v106/03/22 15:0219.0 1
Chloroform ND ug/kg 06/04/22 20:23 67-66-306/03/22 15:029.5 1
Chloromethane ND ug/kg 06/04/22 20:23 74-87-3 v106/03/22 15:0219.0 1
2-Chlorotoluene ND ug/kg 06/04/22 20:23 95-49-806/03/22 15:029.5 1
4-Chlorotoluene ND ug/kg 06/04/22 20:23 106-43-406/03/22 15:029.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 20:23 96-12-806/03/22 15:029.5 1
Dibromochloromethane ND ug/kg 06/04/22 20:23 124-48-106/03/22 15:029.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 20:23 106-93-406/03/22 15:029.5 1
Dibromomethane ND ug/kg 06/04/22 20:23 74-95-306/03/22 15:029.5 1
1,2-Dichlorobenzene ND ug/kg 06/04/22 20:23 95-50-106/03/22 15:029.5 1
1,3-Dichlorobenzene ND ug/kg 06/04/22 20:23 541-73-106/03/22 15:029.5 1
1,4-Dichlorobenzene ND ug/kg 06/04/22 20:23 106-46-706/03/22 15:029.5 1
Dichlorodifluoromethane ND ug/kg 06/04/22 20:23 75-71-8 L1,v106/03/22 15:0219.0 1
1,1-Dichloroethane ND ug/kg 06/04/22 20:23 75-34-306/03/22 15:029.5 1
1,2-Dichloroethane ND ug/kg 06/04/22 20:23 107-06-206/03/22 15:029.5 1
1,1-Dichloroethene ND ug/kg 06/04/22 20:23 75-35-406/03/22 15:029.5 1
cis-1,2-Dichloroethene 87.8 ug/kg 06/04/22 20:23 156-59-206/03/22 15:029.5 1
trans-1,2-Dichloroethene ND ug/kg 06/04/22 20:23 156-60-506/03/22 15:029.5 1
1,2-Dichloropropane ND ug/kg 06/04/22 20:23 78-87-506/03/22 15:029.5 1
1,3-Dichloropropane ND ug/kg 06/04/22 20:23 142-28-906/03/22 15:029.5 1
2,2-Dichloropropane ND ug/kg 06/04/22 20:23 594-20-706/03/22 15:029.5 1
1,1-Dichloropropene ND ug/kg 06/04/22 20:23 563-58-606/03/22 15:029.5 1
cis-1,3-Dichloropropene ND ug/kg 06/04/22 20:23 10061-01-506/03/22 15:029.5 1
trans-1,3-Dichloropropene ND ug/kg 06/04/22 20:23 10061-02-606/03/22 15:029.5 1
Diisopropyl ether ND ug/kg 06/04/22 20:23 108-20-306/03/22 15:029.5 1
Ethylbenzene ND ug/kg 06/04/22 20:23 100-41-406/03/22 15:029.5 1
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 20:23 87-68-306/03/22 15:0219.0 1
2-Hexanone ND ug/kg 06/04/22 20:23 591-78-606/03/22 15:0295.1 1
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 20:23 98-82-806/03/22 15:029.5 1
p-Isopropyltoluene ND ug/kg 06/04/22 20:23 99-87-606/03/22 15:029.5 1
Methylene Chloride ND ug/kg 06/04/22 20:23 75-09-206/03/22 15:0238.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 20:23 108-10-106/03/22 15:0295.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-8 (4-8)Lab ID:92607493010 Collected:05/31/22 12:35 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 20:23 1634-04-406/03/22 15:029.5 1
Naphthalene ND ug/kg 06/04/22 20:23 91-20-306/03/22 15:029.5 1
n-Propylbenzene ND ug/kg 06/04/22 20:23 103-65-106/03/22 15:029.5 1
Styrene ND ug/kg 06/04/22 20:23 100-42-5 v106/03/22 15:029.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 20:23 630-20-606/03/22 15:029.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 20:23 79-34-506/03/22 15:029.5 1
Tetrachloroethene 2010 ug/kg 06/04/22 20:23 127-18-406/03/22 15:029.5 1
Toluene ND ug/kg 06/04/22 20:23 108-88-306/03/22 15:029.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/04/22 20:23 87-61-606/03/22 15:029.5 1
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 20:23 120-82-106/03/22 15:029.5 1
1,1,1-Trichloroethane ND ug/kg 06/04/22 20:23 71-55-606/03/22 15:029.5 1
1,1,2-Trichloroethane ND ug/kg 06/04/22 20:23 79-00-506/03/22 15:029.5 1
Trichloroethene 74.0 ug/kg 06/04/22 20:23 79-01-606/03/22 15:029.5 1
Trichlorofluoromethane ND ug/kg 06/04/22 20:23 75-69-406/03/22 15:029.5 1
1,2,3-Trichloropropane ND ug/kg 06/04/22 20:23 96-18-406/03/22 15:029.5 1
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 20:23 95-63-606/03/22 15:029.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 20:23 108-67-806/03/22 15:029.5 1
Vinyl acetate ND ug/kg 06/04/22 20:23 108-05-406/03/22 15:0295.1 1
Vinyl chloride ND ug/kg 06/04/22 20:23 75-01-4 L1,v106/03/22 15:0219.0 1
Xylene (Total)ND ug/kg 06/04/22 20:23 1330-20-706/03/22 15:0219.0 1
m&p-Xylene ND ug/kg 06/04/22 20:23 179601-23-106/03/22 15:0219.0 1
o-Xylene ND ug/kg 06/04/22 20:23 95-47-606/03/22 15:029.5 1
Surrogates
Toluene-d8 (S)100 %06/04/22 20:23 2037-26-506/03/22 15:0270-130 1
4-Bromofluorobenzene (S)100 %06/04/22 20:23 460-00-406/03/22 15:0269-134 1
1,2-Dichloroethane-d4 (S)104 %06/04/22 20:23 17060-07-006/03/22 15:0270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.5 %06/06/22 15:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-9 (0.5-4)Lab ID:92607493011 Collected:05/31/22 13:00 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/04/22 14:47 67-64-106/04/22 04:187245
Benzene ND ug/kg 06/04/22 14:47 71-43-206/04/22 04:1836.2 5
Bromobenzene ND ug/kg 06/04/22 14:47 108-86-106/04/22 04:1836.2 5
Bromochloromethane ND ug/kg 06/04/22 14:47 74-97-506/04/22 04:1836.2 5
Bromodichloromethane ND ug/kg 06/04/22 14:47 75-27-406/04/22 04:1836.2 5
Bromoform ND ug/kg 06/04/22 14:47 75-25-206/04/22 04:1836.2 5
Bromomethane ND ug/kg 06/04/22 14:47 74-83-9 IK06/04/22 04:1872.4 5
2-Butanone (MEK)ND ug/kg 06/04/22 14:47 78-93-306/04/22 04:187245
n-Butylbenzene ND ug/kg 06/04/22 14:47 104-51-806/04/22 04:1836.2 5
sec-Butylbenzene ND ug/kg 06/04/22 14:47 135-98-806/04/22 04:1836.2 5
tert-Butylbenzene ND ug/kg 06/04/22 14:47 98-06-606/04/22 04:1836.2 5
Carbon tetrachloride ND ug/kg 06/04/22 14:47 56-23-506/04/22 04:1836.2 5
Chlorobenzene 67.6 ug/kg 06/04/22 14:47 108-90-706/04/22 04:1836.2 5
Chloroethane ND ug/kg 06/04/22 14:47 75-00-306/04/22 04:1872.4 5
Chloroform ND ug/kg 06/04/22 14:47 67-66-306/04/22 04:1836.2 5
Chloromethane ND ug/kg 06/04/22 14:47 74-87-306/04/22 04:1872.4 5
2-Chlorotoluene ND ug/kg 06/04/22 14:47 95-49-806/04/22 04:1836.2 5
4-Chlorotoluene ND ug/kg 06/04/22 14:47 106-43-406/04/22 04:1836.2 5
1,2-Dibromo-3-chloropropane ND ug/kg 06/04/22 14:47 96-12-806/04/22 04:1836.2 5
Dibromochloromethane ND ug/kg 06/04/22 14:47 124-48-106/04/22 04:1836.2 5
1,2-Dibromoethane (EDB)ND ug/kg 06/04/22 14:47 106-93-406/04/22 04:1836.2 5
Dibromomethane ND ug/kg 06/04/22 14:47 74-95-306/04/22 04:1836.2 5
1,2-Dichlorobenzene ND ug/kg 06/04/22 14:47 95-50-106/04/22 04:1836.2 5
1,3-Dichlorobenzene ND ug/kg 06/04/22 14:47 541-73-106/04/22 04:1836.2 5
1,4-Dichlorobenzene ND ug/kg 06/04/22 14:47 106-46-706/04/22 04:1836.2 5
Dichlorodifluoromethane ND ug/kg 06/04/22 14:47 75-71-8 L1,v106/04/22 04:1872.4 5
1,1-Dichloroethane ND ug/kg 06/04/22 14:47 75-34-306/04/22 04:1836.2 5
1,2-Dichloroethane ND ug/kg 06/04/22 14:47 107-06-206/04/22 04:1836.2 5
1,1-Dichloroethene 116 ug/kg 06/04/22 14:47 75-35-406/04/22 04:1836.2 5
cis-1,2-Dichloroethene 80.0 ug/kg 06/04/22 14:47 156-59-206/04/22 04:1836.2 5
trans-1,2-Dichloroethene ND ug/kg 06/04/22 14:47 156-60-506/04/22 04:1836.2 5
1,2-Dichloropropane ND ug/kg 06/04/22 14:47 78-87-506/04/22 04:1836.2 5
1,3-Dichloropropane ND ug/kg 06/04/22 14:47 142-28-906/04/22 04:1836.2 5
2,2-Dichloropropane ND ug/kg 06/04/22 14:47 594-20-706/04/22 04:1836.2 5
1,1-Dichloropropene ND ug/kg 06/04/22 14:47 563-58-606/04/22 04:1836.2 5
cis-1,3-Dichloropropene ND ug/kg 06/04/22 14:47 10061-01-506/04/22 04:1836.2 5
trans-1,3-Dichloropropene ND ug/kg 06/04/22 14:47 10061-02-606/04/22 04:1836.2 5
Diisopropyl ether ND ug/kg 06/04/22 14:47 108-20-306/04/22 04:1836.2 5
Ethylbenzene ND ug/kg 06/04/22 14:47 100-41-406/04/22 04:1836.2 5
Hexachloro-1,3-butadiene ND ug/kg 06/04/22 14:47 87-68-306/04/22 04:1872.4 5
2-Hexanone ND ug/kg 06/04/22 14:47 591-78-606/04/22 04:183625
Isopropylbenzene (Cumene)ND ug/kg 06/04/22 14:47 98-82-806/04/22 04:1836.2 5
p-Isopropyltoluene ND ug/kg 06/04/22 14:47 99-87-606/04/22 04:1836.2 5
Methylene Chloride ND ug/kg 06/04/22 14:47 75-09-206/04/22 04:181455
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/04/22 14:47 108-10-106/04/22 04:183625
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-9 (0.5-4)Lab ID:92607493011 Collected:05/31/22 13:00 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/04/22 14:47 1634-04-406/04/22 04:1836.2 5
Naphthalene ND ug/kg 06/04/22 14:47 91-20-306/04/22 04:1836.2 5
n-Propylbenzene ND ug/kg 06/04/22 14:47 103-65-106/04/22 04:1836.2 5
Styrene ND ug/kg 06/04/22 14:47 100-42-506/04/22 04:1836.2 5
1,1,1,2-Tetrachloroethane ND ug/kg 06/04/22 14:47 630-20-606/04/22 04:1836.2 5
1,1,2,2-Tetrachloroethane ND ug/kg 06/04/22 14:47 79-34-506/04/22 04:1836.2 5
Tetrachloroethene 22400 ug/kg 06/04/22 14:47 127-18-406/04/22 04:1836.2 5
Toluene ND ug/kg 06/04/22 14:47 108-88-306/04/22 04:1836.2 5
1,2,3-Trichlorobenzene ND ug/kg 06/04/22 14:47 87-61-606/04/22 04:1836.2 5
1,2,4-Trichlorobenzene ND ug/kg 06/04/22 14:47 120-82-106/04/22 04:1836.2 5
1,1,1-Trichloroethane ND ug/kg 06/04/22 14:47 71-55-606/04/22 04:1836.2 5
1,1,2-Trichloroethane ND ug/kg 06/04/22 14:47 79-00-506/04/22 04:1836.2 5
Trichloroethene 5910 ug/kg 06/04/22 14:47 79-01-606/04/22 04:1836.2 5
Trichlorofluoromethane ND ug/kg 06/04/22 14:47 75-69-406/04/22 04:1836.2 5
1,2,3-Trichloropropane ND ug/kg 06/04/22 14:47 96-18-406/04/22 04:1836.2 5
1,2,4-Trimethylbenzene ND ug/kg 06/04/22 14:47 95-63-606/04/22 04:1836.2 5
1,3,5-Trimethylbenzene ND ug/kg 06/04/22 14:47 108-67-806/04/22 04:1836.2 5
Vinyl acetate ND ug/kg 06/04/22 14:47 108-05-406/04/22 04:183625
Vinyl chloride ND ug/kg 06/04/22 14:47 75-01-4 v106/04/22 04:1872.4 5
Xylene (Total)ND ug/kg 06/04/22 14:47 1330-20-706/04/22 04:1872.4 5
m&p-Xylene ND ug/kg 06/04/22 14:47 179601-23-106/04/22 04:1872.4 5
o-Xylene ND ug/kg 06/04/22 14:47 95-47-606/04/22 04:1836.2 5
Surrogates
Toluene-d8 (S)98 %06/04/22 14:47 2037-26-506/04/22 04:1870-130 5
4-Bromofluorobenzene (S)98 %06/04/22 14:47 460-00-406/04/22 04:1869-134 5
1,2-Dichloroethane-d4 (S)107 %06/04/22 14:47 17060-07-006/04/22 04:1870-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.9 %06/06/22 15:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-9 (4-8)Lab ID:92607493012 Collected:05/31/22 13:06 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/06/22 19:40 67-64-106/06/22 13:1817200100
Benzene ND ug/kg 06/06/22 19:40 71-43-206/06/22 13:18860100
Bromobenzene ND ug/kg 06/06/22 19:40 108-86-106/06/22 13:18860100
Bromochloromethane ND ug/kg 06/06/22 19:40 74-97-506/06/22 13:18860100
Bromodichloromethane ND ug/kg 06/06/22 19:40 75-27-406/06/22 13:18860100
Bromoform ND ug/kg 06/06/22 19:40 75-25-206/06/22 13:18860100
Bromomethane ND ug/kg 06/06/22 19:40 74-83-9 IK06/06/22 13:181720100
2-Butanone (MEK)ND ug/kg 06/06/22 19:40 78-93-306/06/22 13:1817200100
n-Butylbenzene ND ug/kg 06/06/22 19:40 104-51-806/06/22 13:18860100
sec-Butylbenzene ND ug/kg 06/06/22 19:40 135-98-806/06/22 13:18860100
tert-Butylbenzene ND ug/kg 06/06/22 19:40 98-06-606/06/22 13:18860100
Carbon tetrachloride ND ug/kg 06/06/22 19:40 56-23-506/06/22 13:18860100
Chlorobenzene ND ug/kg 06/06/22 19:40 108-90-706/06/22 13:18860100
Chloroethane ND ug/kg 06/06/22 19:40 75-00-3 v106/06/22 13:181720100
Chloroform ND ug/kg 06/06/22 19:40 67-66-306/06/22 13:18860100
Chloromethane ND ug/kg 06/06/22 19:40 74-87-3 v106/06/22 13:181720100
2-Chlorotoluene ND ug/kg 06/06/22 19:40 95-49-806/06/22 13:18860100
4-Chlorotoluene ND ug/kg 06/06/22 19:40 106-43-406/06/22 13:18860100
1,2-Dibromo-3-chloropropane ND ug/kg 06/06/22 19:40 96-12-806/06/22 13:18860100
Dibromochloromethane ND ug/kg 06/06/22 19:40 124-48-106/06/22 13:18860100
1,2-Dibromoethane (EDB)ND ug/kg 06/06/22 19:40 106-93-406/06/22 13:18860100
Dibromomethane ND ug/kg 06/06/22 19:40 74-95-306/06/22 13:18860100
1,2-Dichlorobenzene ND ug/kg 06/06/22 19:40 95-50-106/06/22 13:18860100
1,3-Dichlorobenzene ND ug/kg 06/06/22 19:40 541-73-106/06/22 13:18860100
1,4-Dichlorobenzene ND ug/kg 06/06/22 19:40 106-46-706/06/22 13:18860100
Dichlorodifluoromethane ND ug/kg 06/06/22 19:40 75-71-8 v106/06/22 13:181720100
1,1-Dichloroethane ND ug/kg 06/06/22 19:40 75-34-306/06/22 13:18860100
1,2-Dichloroethane ND ug/kg 06/06/22 19:40 107-06-206/06/22 13:18860100
1,1-Dichloroethene ND ug/kg 06/06/22 19:40 75-35-406/06/22 13:18860100
cis-1,2-Dichloroethene ND ug/kg 06/06/22 19:40 156-59-206/06/22 13:18860100
trans-1,2-Dichloroethene ND ug/kg 06/06/22 19:40 156-60-506/06/22 13:18860100
1,2-Dichloropropane ND ug/kg 06/06/22 19:40 78-87-506/06/22 13:18860100
1,3-Dichloropropane ND ug/kg 06/06/22 19:40 142-28-906/06/22 13:18860100
2,2-Dichloropropane ND ug/kg 06/06/22 19:40 594-20-706/06/22 13:18860100
1,1-Dichloropropene ND ug/kg 06/06/22 19:40 563-58-606/06/22 13:18860100
cis-1,3-Dichloropropene ND ug/kg 06/06/22 19:40 10061-01-506/06/22 13:18860100
trans-1,3-Dichloropropene ND ug/kg 06/06/22 19:40 10061-02-606/06/22 13:18860100
Diisopropyl ether ND ug/kg 06/06/22 19:40 108-20-306/06/22 13:18860100
Ethylbenzene ND ug/kg 06/06/22 19:40 100-41-406/06/22 13:18860100
Hexachloro-1,3-butadiene ND ug/kg 06/06/22 19:40 87-68-306/06/22 13:181720100
2-Hexanone ND ug/kg 06/06/22 19:40 591-78-606/06/22 13:188600100
Isopropylbenzene (Cumene)ND ug/kg 06/06/22 19:40 98-82-806/06/22 13:18860100
p-Isopropyltoluene ND ug/kg 06/06/22 19:40 99-87-606/06/22 13:18860100
Methylene Chloride ND ug/kg 06/06/22 19:40 75-09-206/06/22 13:183440100
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/06/22 19:40 108-10-106/06/22 13:188600100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-9 (4-8)Lab ID:92607493012 Collected:05/31/22 13:06 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/06/22 19:40 1634-04-406/06/22 13:18860100
Naphthalene ND ug/kg 06/06/22 19:40 91-20-306/06/22 13:18860100
n-Propylbenzene ND ug/kg 06/06/22 19:40 103-65-106/06/22 13:18860100
Styrene ND ug/kg 06/06/22 19:40 100-42-506/06/22 13:18860100
1,1,1,2-Tetrachloroethane ND ug/kg 06/06/22 19:40 630-20-606/06/22 13:18860100
1,1,2,2-Tetrachloroethane ND ug/kg 06/06/22 19:40 79-34-506/06/22 13:18860100
Tetrachloroethene 506000 ug/kg 06/06/22 19:40 127-18-406/06/22 13:18860100
Toluene ND ug/kg 06/06/22 19:40 108-88-306/06/22 13:18860100
1,2,3-Trichlorobenzene ND ug/kg 06/06/22 19:40 87-61-606/06/22 13:18860100
1,2,4-Trichlorobenzene ND ug/kg 06/06/22 19:40 120-82-106/06/22 13:18860100
1,1,1-Trichloroethane ND ug/kg 06/06/22 19:40 71-55-606/06/22 13:18860100
1,1,2-Trichloroethane ND ug/kg 06/06/22 19:40 79-00-506/06/22 13:18860100
Trichloroethene 17800 ug/kg 06/06/22 19:40 79-01-606/06/22 13:18860100
Trichlorofluoromethane ND ug/kg 06/06/22 19:40 75-69-406/06/22 13:18860100
1,2,3-Trichloropropane ND ug/kg 06/06/22 19:40 96-18-406/06/22 13:18860100
1,2,4-Trimethylbenzene ND ug/kg 06/06/22 19:40 95-63-606/06/22 13:18860100
1,3,5-Trimethylbenzene ND ug/kg 06/06/22 19:40 108-67-806/06/22 13:18860100
Vinyl acetate ND ug/kg 06/06/22 19:40 108-05-406/06/22 13:188600100
Vinyl chloride ND ug/kg 06/06/22 19:40 75-01-4 v106/06/22 13:181720100
Xylene (Total)ND ug/kg 06/06/22 19:40 1330-20-706/06/22 13:181720100
m&p-Xylene ND ug/kg 06/06/22 19:40 179601-23-106/06/22 13:181720100
o-Xylene ND ug/kg 06/06/22 19:40 95-47-606/06/22 13:18860100
Surrogates
Toluene-d8 (S)99 %06/06/22 19:40 2037-26-506/06/22 13:1870-130 100
4-Bromofluorobenzene (S)102 %06/06/22 19:40 460-00-406/06/22 13:1869-134 100
1,2-Dichloroethane-d4 (S)101 %06/06/22 19:40 17060-07-006/06/22 13:1870-130 100
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.4 %06/06/22 15:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-9 (8-12)Lab ID:92607493013 Collected:05/31/22 13:15 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/06/22 19:58 67-64-106/06/22 13:1862200250
Benzene ND ug/kg 06/06/22 19:58 71-43-206/06/22 13:183110250
Bromobenzene ND ug/kg 06/06/22 19:58 108-86-106/06/22 13:183110250
Bromochloromethane ND ug/kg 06/06/22 19:58 74-97-506/06/22 13:183110250
Bromodichloromethane ND ug/kg 06/06/22 19:58 75-27-406/06/22 13:183110250
Bromoform ND ug/kg 06/06/22 19:58 75-25-206/06/22 13:183110250
Bromomethane ND ug/kg 06/06/22 19:58 74-83-9 IK06/06/22 13:186220250
2-Butanone (MEK)ND ug/kg 06/06/22 19:58 78-93-306/06/22 13:1862200250
n-Butylbenzene ND ug/kg 06/06/22 19:58 104-51-806/06/22 13:183110250
sec-Butylbenzene ND ug/kg 06/06/22 19:58 135-98-806/06/22 13:183110250
tert-Butylbenzene ND ug/kg 06/06/22 19:58 98-06-606/06/22 13:183110250
Carbon tetrachloride ND ug/kg 06/06/22 19:58 56-23-506/06/22 13:183110250
Chlorobenzene ND ug/kg 06/06/22 19:58 108-90-706/06/22 13:183110250
Chloroethane ND ug/kg 06/06/22 19:58 75-00-3 v106/06/22 13:186220250
Chloroform ND ug/kg 06/06/22 19:58 67-66-306/06/22 13:183110250
Chloromethane ND ug/kg 06/06/22 19:58 74-87-3 v106/06/22 13:186220250
2-Chlorotoluene ND ug/kg 06/06/22 19:58 95-49-806/06/22 13:183110250
4-Chlorotoluene ND ug/kg 06/06/22 19:58 106-43-406/06/22 13:183110250
1,2-Dibromo-3-chloropropane ND ug/kg 06/06/22 19:58 96-12-806/06/22 13:183110250
Dibromochloromethane ND ug/kg 06/06/22 19:58 124-48-106/06/22 13:183110250
1,2-Dibromoethane (EDB)ND ug/kg 06/06/22 19:58 106-93-406/06/22 13:183110250
Dibromomethane ND ug/kg 06/06/22 19:58 74-95-306/06/22 13:183110250
1,2-Dichlorobenzene ND ug/kg 06/06/22 19:58 95-50-106/06/22 13:183110250
1,3-Dichlorobenzene ND ug/kg 06/06/22 19:58 541-73-106/06/22 13:183110250
1,4-Dichlorobenzene ND ug/kg 06/06/22 19:58 106-46-706/06/22 13:183110250
Dichlorodifluoromethane ND ug/kg 06/06/22 19:58 75-71-8 v106/06/22 13:186220250
1,1-Dichloroethane ND ug/kg 06/06/22 19:58 75-34-306/06/22 13:183110250
1,2-Dichloroethane ND ug/kg 06/06/22 19:58 107-06-206/06/22 13:183110250
1,1-Dichloroethene ND ug/kg 06/06/22 19:58 75-35-406/06/22 13:183110250
cis-1,2-Dichloroethene ND ug/kg 06/06/22 19:58 156-59-206/06/22 13:183110250
trans-1,2-Dichloroethene ND ug/kg 06/06/22 19:58 156-60-506/06/22 13:183110250
1,2-Dichloropropane ND ug/kg 06/06/22 19:58 78-87-506/06/22 13:183110250
1,3-Dichloropropane ND ug/kg 06/06/22 19:58 142-28-906/06/22 13:183110250
2,2-Dichloropropane ND ug/kg 06/06/22 19:58 594-20-706/06/22 13:183110250
1,1-Dichloropropene ND ug/kg 06/06/22 19:58 563-58-606/06/22 13:183110250
cis-1,3-Dichloropropene ND ug/kg 06/06/22 19:58 10061-01-506/06/22 13:183110250
trans-1,3-Dichloropropene ND ug/kg 06/06/22 19:58 10061-02-606/06/22 13:183110250
Diisopropyl ether ND ug/kg 06/06/22 19:58 108-20-306/06/22 13:183110250
Ethylbenzene ND ug/kg 06/06/22 19:58 100-41-406/06/22 13:183110250
Hexachloro-1,3-butadiene ND ug/kg 06/06/22 19:58 87-68-306/06/22 13:186220250
2-Hexanone ND ug/kg 06/06/22 19:58 591-78-606/06/22 13:1831100250
Isopropylbenzene (Cumene)ND ug/kg 06/06/22 19:58 98-82-806/06/22 13:183110250
p-Isopropyltoluene ND ug/kg 06/06/22 19:58 99-87-606/06/22 13:183110250
Methylene Chloride ND ug/kg 06/06/22 19:58 75-09-206/06/22 13:1812400250
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/06/22 19:58 108-10-106/06/22 13:1831100250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-9 (8-12)Lab ID:92607493013 Collected:05/31/22 13:15 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/06/22 19:58 1634-04-406/06/22 13:183110250
Naphthalene ND ug/kg 06/06/22 19:58 91-20-306/06/22 13:183110250
n-Propylbenzene ND ug/kg 06/06/22 19:58 103-65-106/06/22 13:183110250
Styrene ND ug/kg 06/06/22 19:58 100-42-506/06/22 13:183110250
1,1,1,2-Tetrachloroethane ND ug/kg 06/06/22 19:58 630-20-606/06/22 13:183110250
1,1,2,2-Tetrachloroethane ND ug/kg 06/06/22 19:58 79-34-506/06/22 13:183110250
Tetrachloroethene 2190000 ug/kg 06/06/22 19:58 127-18-406/06/22 13:183110250
Toluene ND ug/kg 06/06/22 19:58 108-88-306/06/22 13:183110250
1,2,3-Trichlorobenzene ND ug/kg 06/06/22 19:58 87-61-606/06/22 13:183110250
1,2,4-Trichlorobenzene ND ug/kg 06/06/22 19:58 120-82-106/06/22 13:183110250
1,1,1-Trichloroethane ND ug/kg 06/06/22 19:58 71-55-606/06/22 13:183110250
1,1,2-Trichloroethane ND ug/kg 06/06/22 19:58 79-00-506/06/22 13:183110250
Trichloroethene 136000 ug/kg 06/06/22 19:58 79-01-606/06/22 13:183110250
Trichlorofluoromethane ND ug/kg 06/06/22 19:58 75-69-406/06/22 13:183110250
1,2,3-Trichloropropane ND ug/kg 06/06/22 19:58 96-18-406/06/22 13:183110250
1,2,4-Trimethylbenzene ND ug/kg 06/06/22 19:58 95-63-606/06/22 13:183110250
1,3,5-Trimethylbenzene ND ug/kg 06/06/22 19:58 108-67-806/06/22 13:183110250
Vinyl acetate ND ug/kg 06/06/22 19:58 108-05-406/06/22 13:1831100250
Vinyl chloride ND ug/kg 06/06/22 19:58 75-01-4 v106/06/22 13:186220250
Xylene (Total)ND ug/kg 06/06/22 19:58 1330-20-706/06/22 13:186220250
m&p-Xylene ND ug/kg 06/06/22 19:58 179601-23-106/06/22 13:186220250
o-Xylene ND ug/kg 06/06/22 19:58 95-47-606/06/22 13:183110250
Surrogates
Toluene-d8 (S)98 %06/06/22 19:58 2037-26-506/06/22 13:1870-130 250
4-Bromofluorobenzene (S)101 %06/06/22 19:58 460-00-406/06/22 13:1869-134 250
1,2-Dichloroethane-d4 (S)102 %06/06/22 19:58 17060-07-006/06/22 13:1870-130 250
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 41.5 %06/06/22 15:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-2 (2)Lab ID:92607493014 Collected:05/31/22 10:20 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/06/22 20:15 67-64-106/06/22 13:1859900125
Benzene ND ug/kg 06/06/22 20:15 71-43-206/06/22 13:182990125
Bromobenzene ND ug/kg 06/06/22 20:15 108-86-106/06/22 13:182990125
Bromochloromethane ND ug/kg 06/06/22 20:15 74-97-506/06/22 13:182990125
Bromodichloromethane ND ug/kg 06/06/22 20:15 75-27-406/06/22 13:182990125
Bromoform ND ug/kg 06/06/22 20:15 75-25-206/06/22 13:182990125
Bromomethane ND ug/kg 06/06/22 20:15 74-83-9 IK06/06/22 13:185990125
2-Butanone (MEK)ND ug/kg 06/06/22 20:15 78-93-306/06/22 13:1859900125
n-Butylbenzene ND ug/kg 06/06/22 20:15 104-51-806/06/22 13:182990125
sec-Butylbenzene ND ug/kg 06/06/22 20:15 135-98-806/06/22 13:182990125
tert-Butylbenzene ND ug/kg 06/06/22 20:15 98-06-606/06/22 13:182990125
Carbon tetrachloride ND ug/kg 06/06/22 20:15 56-23-506/06/22 13:182990125
Chlorobenzene ND ug/kg 06/06/22 20:15 108-90-706/06/22 13:182990125
Chloroethane ND ug/kg 06/06/22 20:15 75-00-3 v106/06/22 13:185990125
Chloroform ND ug/kg 06/06/22 20:15 67-66-306/06/22 13:182990125
Chloromethane ND ug/kg 06/06/22 20:15 74-87-3 v106/06/22 13:185990125
2-Chlorotoluene ND ug/kg 06/06/22 20:15 95-49-806/06/22 13:182990125
4-Chlorotoluene ND ug/kg 06/06/22 20:15 106-43-406/06/22 13:182990125
1,2-Dibromo-3-chloropropane ND ug/kg 06/06/22 20:15 96-12-806/06/22 13:182990125
Dibromochloromethane ND ug/kg 06/06/22 20:15 124-48-106/06/22 13:182990125
1,2-Dibromoethane (EDB)ND ug/kg 06/06/22 20:15 106-93-406/06/22 13:182990125
Dibromomethane ND ug/kg 06/06/22 20:15 74-95-306/06/22 13:182990125
1,2-Dichlorobenzene ND ug/kg 06/06/22 20:15 95-50-106/06/22 13:182990125
1,3-Dichlorobenzene ND ug/kg 06/06/22 20:15 541-73-106/06/22 13:182990125
1,4-Dichlorobenzene ND ug/kg 06/06/22 20:15 106-46-706/06/22 13:182990125
Dichlorodifluoromethane ND ug/kg 06/06/22 20:15 75-71-8 v106/06/22 13:185990125
1,1-Dichloroethane ND ug/kg 06/06/22 20:15 75-34-306/06/22 13:182990125
1,2-Dichloroethane ND ug/kg 06/06/22 20:15 107-06-206/06/22 13:182990125
1,1-Dichloroethene ND ug/kg 06/06/22 20:15 75-35-406/06/22 13:182990125
cis-1,2-Dichloroethene 7570 ug/kg 06/06/22 20:15 156-59-206/06/22 13:182990125
trans-1,2-Dichloroethene ND ug/kg 06/06/22 20:15 156-60-506/06/22 13:182990125
1,2-Dichloropropane ND ug/kg 06/06/22 20:15 78-87-506/06/22 13:182990125
1,3-Dichloropropane ND ug/kg 06/06/22 20:15 142-28-906/06/22 13:182990125
2,2-Dichloropropane ND ug/kg 06/06/22 20:15 594-20-706/06/22 13:182990125
1,1-Dichloropropene ND ug/kg 06/06/22 20:15 563-58-606/06/22 13:182990125
cis-1,3-Dichloropropene ND ug/kg 06/06/22 20:15 10061-01-506/06/22 13:182990125
trans-1,3-Dichloropropene ND ug/kg 06/06/22 20:15 10061-02-606/06/22 13:182990125
Diisopropyl ether ND ug/kg 06/06/22 20:15 108-20-306/06/22 13:182990125
Ethylbenzene ND ug/kg 06/06/22 20:15 100-41-406/06/22 13:182990125
Hexachloro-1,3-butadiene ND ug/kg 06/06/22 20:15 87-68-306/06/22 13:185990125
2-Hexanone ND ug/kg 06/06/22 20:15 591-78-606/06/22 13:1829900125
Isopropylbenzene (Cumene)ND ug/kg 06/06/22 20:15 98-82-806/06/22 13:182990125
p-Isopropyltoluene ND ug/kg 06/06/22 20:15 99-87-606/06/22 13:182990125
Methylene Chloride ND ug/kg 06/06/22 20:15 75-09-206/06/22 13:1812000125
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/06/22 20:15 108-10-106/06/22 13:1829900125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 50 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-2 (2)Lab ID:92607493014 Collected:05/31/22 10:20 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/06/22 20:15 1634-04-406/06/22 13:182990125
Naphthalene ND ug/kg 06/06/22 20:15 91-20-306/06/22 13:182990125
n-Propylbenzene ND ug/kg 06/06/22 20:15 103-65-106/06/22 13:182990125
Styrene ND ug/kg 06/06/22 20:15 100-42-506/06/22 13:182990125
1,1,1,2-Tetrachloroethane ND ug/kg 06/06/22 20:15 630-20-606/06/22 13:182990125
1,1,2,2-Tetrachloroethane ND ug/kg 06/06/22 20:15 79-34-506/06/22 13:182990125
Tetrachloroethene 1950000 ug/kg 06/06/22 20:15 127-18-406/06/22 13:182990125
Toluene ND ug/kg 06/06/22 20:15 108-88-306/06/22 13:182990125
1,2,3-Trichlorobenzene ND ug/kg 06/06/22 20:15 87-61-606/06/22 13:182990125
1,2,4-Trichlorobenzene ND ug/kg 06/06/22 20:15 120-82-106/06/22 13:182990125
1,1,1-Trichloroethane ND ug/kg 06/06/22 20:15 71-55-606/06/22 13:182990125
1,1,2-Trichloroethane ND ug/kg 06/06/22 20:15 79-00-506/06/22 13:182990125
Trichloroethene 36800 ug/kg 06/06/22 20:15 79-01-606/06/22 13:182990125
Trichlorofluoromethane ND ug/kg 06/06/22 20:15 75-69-406/06/22 13:182990125
1,2,3-Trichloropropane ND ug/kg 06/06/22 20:15 96-18-406/06/22 13:182990125
1,2,4-Trimethylbenzene ND ug/kg 06/06/22 20:15 95-63-606/06/22 13:182990125
1,3,5-Trimethylbenzene ND ug/kg 06/06/22 20:15 108-67-806/06/22 13:182990125
Vinyl acetate ND ug/kg 06/06/22 20:15 108-05-406/06/22 13:1829900125
Vinyl chloride ND ug/kg 06/06/22 20:15 75-01-4 v106/06/22 13:185990125
Xylene (Total)ND ug/kg 06/06/22 20:15 1330-20-706/06/22 13:185990125
m&p-Xylene ND ug/kg 06/06/22 20:15 179601-23-106/06/22 13:185990125
o-Xylene ND ug/kg 06/06/22 20:15 95-47-606/06/22 13:182990125
Surrogates
Toluene-d8 (S)99 %06/06/22 20:15 2037-26-506/06/22 13:1870-130 125
4-Bromofluorobenzene (S)101 %06/06/22 20:15 460-00-406/06/22 13:1869-134 125
1,2-Dichloroethane-d4 (S)103 %06/06/22 20:15 17060-07-006/06/22 13:1870-130 125
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 33.6 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-5 (8-12)Lab ID:92607493015 Collected:05/31/22 11:25 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 21:02 67-64-106/02/22 20:101441
Benzene ND ug/kg 06/03/22 21:02 71-43-206/02/22 20:107.2 1
Bromobenzene ND ug/kg 06/03/22 21:02 108-86-106/02/22 20:107.2 1
Bromochloromethane ND ug/kg 06/03/22 21:02 74-97-506/02/22 20:107.2 1
Bromodichloromethane ND ug/kg 06/03/22 21:02 75-27-406/02/22 20:107.2 1
Bromoform ND ug/kg 06/03/22 21:02 75-25-206/02/22 20:107.2 1
Bromomethane ND ug/kg 06/03/22 21:02 74-83-9 IK06/02/22 20:1014.4 1
2-Butanone (MEK)ND ug/kg 06/03/22 21:02 78-93-306/02/22 20:101441
n-Butylbenzene ND ug/kg 06/03/22 21:02 104-51-806/02/22 20:107.2 1
sec-Butylbenzene ND ug/kg 06/03/22 21:02 135-98-806/02/22 20:107.2 1
tert-Butylbenzene ND ug/kg 06/03/22 21:02 98-06-606/02/22 20:107.2 1
Carbon tetrachloride ND ug/kg 06/03/22 21:02 56-23-506/02/22 20:107.2 1
Chlorobenzene ND ug/kg 06/03/22 21:02 108-90-706/02/22 20:107.2 1
Chloroethane ND ug/kg 06/03/22 21:02 75-00-306/02/22 20:1014.4 1
Chloroform ND ug/kg 06/03/22 21:02 67-66-306/02/22 20:107.2 1
Chloromethane ND ug/kg 06/03/22 21:02 74-87-306/02/22 20:1014.4 1
2-Chlorotoluene ND ug/kg 06/03/22 21:02 95-49-806/02/22 20:107.2 1
4-Chlorotoluene ND ug/kg 06/03/22 21:02 106-43-406/02/22 20:107.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 21:02 96-12-806/02/22 20:107.2 1
Dibromochloromethane ND ug/kg 06/03/22 21:02 124-48-106/02/22 20:107.2 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 21:02 106-93-406/02/22 20:107.2 1
Dibromomethane ND ug/kg 06/03/22 21:02 74-95-306/02/22 20:107.2 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 21:02 95-50-106/02/22 20:107.2 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 21:02 541-73-106/02/22 20:107.2 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 21:02 106-46-706/02/22 20:107.2 1
Dichlorodifluoromethane ND ug/kg 06/03/22 21:02 75-71-8 v106/02/22 20:1014.4 1
1,1-Dichloroethane ND ug/kg 06/03/22 21:02 75-34-306/02/22 20:107.2 1
1,2-Dichloroethane ND ug/kg 06/03/22 21:02 107-06-206/02/22 20:107.2 1
1,1-Dichloroethene ND ug/kg 06/03/22 21:02 75-35-406/02/22 20:107.2 1
cis-1,2-Dichloroethene 976 ug/kg 06/03/22 21:02 156-59-206/02/22 20:107.2 1
trans-1,2-Dichloroethene 31.7 ug/kg 06/03/22 21:02 156-60-506/02/22 20:107.2 1
1,2-Dichloropropane ND ug/kg 06/03/22 21:02 78-87-506/02/22 20:107.2 1
1,3-Dichloropropane ND ug/kg 06/03/22 21:02 142-28-906/02/22 20:107.2 1
2,2-Dichloropropane ND ug/kg 06/03/22 21:02 594-20-706/02/22 20:107.2 1
1,1-Dichloropropene ND ug/kg 06/03/22 21:02 563-58-606/02/22 20:107.2 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 21:02 10061-01-506/02/22 20:107.2 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 21:02 10061-02-606/02/22 20:107.2 1
Diisopropyl ether ND ug/kg 06/03/22 21:02 108-20-306/02/22 20:107.2 1
Ethylbenzene ND ug/kg 06/03/22 21:02 100-41-406/02/22 20:107.2 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 21:02 87-68-306/02/22 20:1014.4 1
2-Hexanone ND ug/kg 06/03/22 21:02 591-78-606/02/22 20:1071.9 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 21:02 98-82-806/02/22 20:107.2 1
p-Isopropyltoluene ND ug/kg 06/03/22 21:02 99-87-606/02/22 20:107.2 1
Methylene Chloride ND ug/kg 06/03/22 21:02 75-09-206/02/22 20:1028.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 21:02 108-10-106/02/22 20:1071.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-5 (8-12)Lab ID:92607493015 Collected:05/31/22 11:25 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/03/22 21:02 1634-04-406/02/22 20:107.2 1
Naphthalene ND ug/kg 06/03/22 21:02 91-20-306/02/22 20:107.2 1
n-Propylbenzene ND ug/kg 06/03/22 21:02 103-65-106/02/22 20:107.2 1
Styrene ND ug/kg 06/03/22 21:02 100-42-506/02/22 20:107.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 21:02 630-20-606/02/22 20:107.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 21:02 79-34-506/02/22 20:107.2 1
Tetrachloroethene 5100 ug/kg 06/03/22 21:02 127-18-406/02/22 20:107.2 1
Toluene ND ug/kg 06/03/22 21:02 108-88-306/02/22 20:107.2 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 21:02 87-61-606/02/22 20:107.2 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 21:02 120-82-106/02/22 20:107.2 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 21:02 71-55-606/02/22 20:107.2 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 21:02 79-00-506/02/22 20:107.2 1
Trichloroethene 149 ug/kg 06/03/22 21:02 79-01-606/02/22 20:107.2 1
Trichlorofluoromethane ND ug/kg 06/03/22 21:02 75-69-406/02/22 20:107.2 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 21:02 96-18-406/02/22 20:107.2 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 21:02 95-63-606/02/22 20:107.2 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 21:02 108-67-806/02/22 20:107.2 1
Vinyl acetate ND ug/kg 06/03/22 21:02 108-05-406/02/22 20:1071.9 1
Vinyl chloride ND ug/kg 06/03/22 21:02 75-01-4 v106/02/22 20:1014.4 1
Xylene (Total)ND ug/kg 06/03/22 21:02 1330-20-706/02/22 20:1014.4 1
m&p-Xylene ND ug/kg 06/03/22 21:02 179601-23-106/02/22 20:1014.4 1
o-Xylene ND ug/kg 06/03/22 21:02 95-47-606/02/22 20:107.2 1
Surrogates
Toluene-d8 (S)102 %06/03/22 21:02 2037-26-506/02/22 20:1070-130 1
4-Bromofluorobenzene (S)99 %06/03/22 21:02 460-00-406/02/22 20:1069-134 1
1,2-Dichloroethane-d4 (S)104 %06/03/22 21:02 17060-07-006/02/22 20:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.0 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-6 (8-12)Lab ID:92607493016 Collected:05/31/22 11:40 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 21:40 67-64-106/02/22 20:101821
Benzene ND ug/kg 06/03/22 21:40 71-43-206/02/22 20:109.1 1
Bromobenzene ND ug/kg 06/03/22 21:40 108-86-106/02/22 20:109.1 1
Bromochloromethane ND ug/kg 06/03/22 21:40 74-97-506/02/22 20:109.1 1
Bromodichloromethane ND ug/kg 06/03/22 21:40 75-27-406/02/22 20:109.1 1
Bromoform ND ug/kg 06/03/22 21:40 75-25-206/02/22 20:109.1 1
Bromomethane ND ug/kg 06/03/22 21:40 74-83-9 IK06/02/22 20:1018.2 1
2-Butanone (MEK)ND ug/kg 06/03/22 21:40 78-93-306/02/22 20:101821
n-Butylbenzene ND ug/kg 06/03/22 21:40 104-51-806/02/22 20:109.1 1
sec-Butylbenzene ND ug/kg 06/03/22 21:40 135-98-806/02/22 20:109.1 1
tert-Butylbenzene ND ug/kg 06/03/22 21:40 98-06-606/02/22 20:109.1 1
Carbon tetrachloride ND ug/kg 06/03/22 21:40 56-23-506/02/22 20:109.1 1
Chlorobenzene ND ug/kg 06/03/22 21:40 108-90-706/02/22 20:109.1 1
Chloroethane ND ug/kg 06/03/22 21:40 75-00-306/02/22 20:1018.2 1
Chloroform ND ug/kg 06/03/22 21:40 67-66-306/02/22 20:109.1 1
Chloromethane ND ug/kg 06/03/22 21:40 74-87-3 M106/02/22 20:1018.2 1
2-Chlorotoluene ND ug/kg 06/03/22 21:40 95-49-806/02/22 20:109.1 1
4-Chlorotoluene ND ug/kg 06/03/22 21:40 106-43-406/02/22 20:109.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 21:40 96-12-806/02/22 20:109.1 1
Dibromochloromethane ND ug/kg 06/03/22 21:40 124-48-106/02/22 20:109.1 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 21:40 106-93-406/02/22 20:109.1 1
Dibromomethane ND ug/kg 06/03/22 21:40 74-95-306/02/22 20:109.1 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 21:40 95-50-106/02/22 20:109.1 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 21:40 541-73-106/02/22 20:109.1 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 21:40 106-46-706/02/22 20:109.1 1
Dichlorodifluoromethane ND ug/kg 06/03/22 21:40 75-71-8 v106/02/22 20:1018.2 1
1,1-Dichloroethane ND ug/kg 06/03/22 21:40 75-34-306/02/22 20:109.1 1
1,2-Dichloroethane ND ug/kg 06/03/22 21:40 107-06-206/02/22 20:109.1 1
1,1-Dichloroethene ND ug/kg 06/03/22 21:40 75-35-406/02/22 20:109.1 1
cis-1,2-Dichloroethene 53.3 ug/kg 06/03/22 21:40 156-59-206/02/22 20:109.1 1
trans-1,2-Dichloroethene ND ug/kg 06/03/22 21:40 156-60-506/02/22 20:109.1 1
1,2-Dichloropropane ND ug/kg 06/03/22 21:40 78-87-506/02/22 20:109.1 1
1,3-Dichloropropane ND ug/kg 06/03/22 21:40 142-28-906/02/22 20:109.1 1
2,2-Dichloropropane ND ug/kg 06/03/22 21:40 594-20-706/02/22 20:109.1 1
1,1-Dichloropropene ND ug/kg 06/03/22 21:40 563-58-606/02/22 20:109.1 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 21:40 10061-01-506/02/22 20:109.1 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 21:40 10061-02-606/02/22 20:109.1 1
Diisopropyl ether ND ug/kg 06/03/22 21:40 108-20-306/02/22 20:109.1 1
Ethylbenzene ND ug/kg 06/03/22 21:40 100-41-406/02/22 20:109.1 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 21:40 87-68-306/02/22 20:1018.2 1
2-Hexanone ND ug/kg 06/03/22 21:40 591-78-606/02/22 20:1091.1 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 21:40 98-82-806/02/22 20:109.1 1
p-Isopropyltoluene ND ug/kg 06/03/22 21:40 99-87-606/02/22 20:109.1 1
Methylene Chloride ND ug/kg 06/03/22 21:40 75-09-206/02/22 20:1036.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 21:40 108-10-106/02/22 20:1091.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-6 (8-12)Lab ID:92607493016 Collected:05/31/22 11:40 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/03/22 21:40 1634-04-406/02/22 20:109.1 1
Naphthalene ND ug/kg 06/03/22 21:40 91-20-306/02/22 20:109.1 1
n-Propylbenzene ND ug/kg 06/03/22 21:40 103-65-106/02/22 20:109.1 1
Styrene ND ug/kg 06/03/22 21:40 100-42-506/02/22 20:109.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 21:40 630-20-606/02/22 20:109.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 21:40 79-34-506/02/22 20:109.1 1
Tetrachloroethene 4850 ug/kg 06/03/22 21:40 127-18-4 M106/02/22 20:109.1 1
Toluene ND ug/kg 06/03/22 21:40 108-88-306/02/22 20:109.1 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 21:40 87-61-606/02/22 20:109.1 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 21:40 120-82-106/02/22 20:109.1 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 21:40 71-55-606/02/22 20:109.1 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 21:40 79-00-506/02/22 20:109.1 1
Trichloroethene 1330 ug/kg 06/03/22 21:40 79-01-6 M106/02/22 20:109.1 1
Trichlorofluoromethane ND ug/kg 06/03/22 21:40 75-69-406/02/22 20:109.1 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 21:40 96-18-406/02/22 20:109.1 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 21:40 95-63-606/02/22 20:109.1 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 21:40 108-67-806/02/22 20:109.1 1
Vinyl acetate ND ug/kg 06/03/22 21:40 108-05-406/02/22 20:1091.1 1
Vinyl chloride ND ug/kg 06/03/22 21:40 75-01-4 v106/02/22 20:1018.2 1
Xylene (Total)ND ug/kg 06/03/22 21:40 1330-20-706/02/22 20:1018.2 1
m&p-Xylene ND ug/kg 06/03/22 21:40 179601-23-106/02/22 20:1018.2 1
o-Xylene ND ug/kg 06/03/22 21:40 95-47-606/02/22 20:109.1 1
Surrogates
Toluene-d8 (S)100 %06/03/22 21:40 2037-26-506/02/22 20:1070-130 1
4-Bromofluorobenzene (S)100 %06/03/22 21:40 460-00-406/02/22 20:1069-134 1
1,2-Dichloroethane-d4 (S)105 %06/03/22 21:40 17060-07-006/02/22 20:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.5 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-10 (8-12)Lab ID:92607493017 Collected:06/01/22 09:20 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 21:59 67-64-106/02/22 20:101431
Benzene ND ug/kg 06/03/22 21:59 71-43-206/02/22 20:107.2 1
Bromobenzene ND ug/kg 06/03/22 21:59 108-86-106/02/22 20:107.2 1
Bromochloromethane ND ug/kg 06/03/22 21:59 74-97-506/02/22 20:107.2 1
Bromodichloromethane ND ug/kg 06/03/22 21:59 75-27-406/02/22 20:107.2 1
Bromoform ND ug/kg 06/03/22 21:59 75-25-206/02/22 20:107.2 1
Bromomethane ND ug/kg 06/03/22 21:59 74-83-9 IK06/02/22 20:1014.3 1
2-Butanone (MEK)ND ug/kg 06/03/22 21:59 78-93-306/02/22 20:101431
n-Butylbenzene ND ug/kg 06/03/22 21:59 104-51-806/02/22 20:107.2 1
sec-Butylbenzene ND ug/kg 06/03/22 21:59 135-98-806/02/22 20:107.2 1
tert-Butylbenzene ND ug/kg 06/03/22 21:59 98-06-606/02/22 20:107.2 1
Carbon tetrachloride ND ug/kg 06/03/22 21:59 56-23-506/02/22 20:107.2 1
Chlorobenzene ND ug/kg 06/03/22 21:59 108-90-706/02/22 20:107.2 1
Chloroethane ND ug/kg 06/03/22 21:59 75-00-306/02/22 20:1014.3 1
Chloroform ND ug/kg 06/03/22 21:59 67-66-306/02/22 20:107.2 1
Chloromethane ND ug/kg 06/03/22 21:59 74-87-306/02/22 20:1014.3 1
2-Chlorotoluene ND ug/kg 06/03/22 21:59 95-49-806/02/22 20:107.2 1
4-Chlorotoluene ND ug/kg 06/03/22 21:59 106-43-406/02/22 20:107.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 21:59 96-12-806/02/22 20:107.2 1
Dibromochloromethane ND ug/kg 06/03/22 21:59 124-48-106/02/22 20:107.2 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 21:59 106-93-406/02/22 20:107.2 1
Dibromomethane ND ug/kg 06/03/22 21:59 74-95-306/02/22 20:107.2 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 21:59 95-50-106/02/22 20:107.2 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 21:59 541-73-106/02/22 20:107.2 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 21:59 106-46-706/02/22 20:107.2 1
Dichlorodifluoromethane ND ug/kg 06/03/22 21:59 75-71-8 v106/02/22 20:1014.3 1
1,1-Dichloroethane ND ug/kg 06/03/22 21:59 75-34-306/02/22 20:107.2 1
1,2-Dichloroethane ND ug/kg 06/03/22 21:59 107-06-206/02/22 20:107.2 1
1,1-Dichloroethene ND ug/kg 06/03/22 21:59 75-35-406/02/22 20:107.2 1
cis-1,2-Dichloroethene 88.0 ug/kg 06/03/22 21:59 156-59-206/02/22 20:107.2 1
trans-1,2-Dichloroethene ND ug/kg 06/03/22 21:59 156-60-506/02/22 20:107.2 1
1,2-Dichloropropane ND ug/kg 06/03/22 21:59 78-87-506/02/22 20:107.2 1
1,3-Dichloropropane ND ug/kg 06/03/22 21:59 142-28-906/02/22 20:107.2 1
2,2-Dichloropropane ND ug/kg 06/03/22 21:59 594-20-706/02/22 20:107.2 1
1,1-Dichloropropene ND ug/kg 06/03/22 21:59 563-58-606/02/22 20:107.2 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 21:59 10061-01-506/02/22 20:107.2 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 21:59 10061-02-606/02/22 20:107.2 1
Diisopropyl ether ND ug/kg 06/03/22 21:59 108-20-306/02/22 20:107.2 1
Ethylbenzene ND ug/kg 06/03/22 21:59 100-41-406/02/22 20:107.2 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 21:59 87-68-306/02/22 20:1014.3 1
2-Hexanone ND ug/kg 06/03/22 21:59 591-78-606/02/22 20:1071.5 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 21:59 98-82-806/02/22 20:107.2 1
p-Isopropyltoluene ND ug/kg 06/03/22 21:59 99-87-606/02/22 20:107.2 1
Methylene Chloride ND ug/kg 06/03/22 21:59 75-09-206/02/22 20:1028.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 21:59 108-10-106/02/22 20:1071.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-10 (8-12)Lab ID:92607493017 Collected:06/01/22 09:20 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/03/22 21:59 1634-04-406/02/22 20:107.2 1
Naphthalene ND ug/kg 06/03/22 21:59 91-20-306/02/22 20:107.2 1
n-Propylbenzene ND ug/kg 06/03/22 21:59 103-65-106/02/22 20:107.2 1
Styrene ND ug/kg 06/03/22 21:59 100-42-506/02/22 20:107.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 21:59 630-20-606/02/22 20:107.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 21:59 79-34-506/02/22 20:107.2 1
Tetrachloroethene 152 ug/kg 06/03/22 21:59 127-18-406/02/22 20:107.2 1
Toluene ND ug/kg 06/03/22 21:59 108-88-306/02/22 20:107.2 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 21:59 87-61-606/02/22 20:107.2 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 21:59 120-82-106/02/22 20:107.2 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 21:59 71-55-606/02/22 20:107.2 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 21:59 79-00-506/02/22 20:107.2 1
Trichloroethene 10.0 ug/kg 06/03/22 21:59 79-01-606/02/22 20:107.2 1
Trichlorofluoromethane ND ug/kg 06/03/22 21:59 75-69-406/02/22 20:107.2 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 21:59 96-18-406/02/22 20:107.2 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 21:59 95-63-606/02/22 20:107.2 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 21:59 108-67-806/02/22 20:107.2 1
Vinyl acetate ND ug/kg 06/03/22 21:59 108-05-406/02/22 20:1071.5 1
Vinyl chloride ND ug/kg 06/03/22 21:59 75-01-4 v106/02/22 20:1014.3 1
Xylene (Total)ND ug/kg 06/03/22 21:59 1330-20-706/02/22 20:1014.3 1
m&p-Xylene ND ug/kg 06/03/22 21:59 179601-23-106/02/22 20:1014.3 1
o-Xylene ND ug/kg 06/03/22 21:59 95-47-606/02/22 20:107.2 1
Surrogates
Toluene-d8 (S)100 %06/03/22 21:59 2037-26-506/02/22 20:1070-130 1
4-Bromofluorobenzene (S)97 %06/03/22 21:59 460-00-406/02/22 20:1069-134 1
1,2-Dichloroethane-d4 (S)102 %06/03/22 21:59 17060-07-006/02/22 20:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.5 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-11 (0-4)Lab ID:92607493018 Collected:06/01/22 09:30 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 22:17 67-64-106/02/22 20:101001
Benzene ND ug/kg 06/03/22 22:17 71-43-206/02/22 20:105.0 1
Bromobenzene ND ug/kg 06/03/22 22:17 108-86-106/02/22 20:105.0 1
Bromochloromethane ND ug/kg 06/03/22 22:17 74-97-506/02/22 20:105.0 1
Bromodichloromethane ND ug/kg 06/03/22 22:17 75-27-406/02/22 20:105.0 1
Bromoform ND ug/kg 06/03/22 22:17 75-25-206/02/22 20:105.0 1
Bromomethane ND ug/kg 06/03/22 22:17 74-83-9 IK06/02/22 20:1010.0 1
2-Butanone (MEK)ND ug/kg 06/03/22 22:17 78-93-306/02/22 20:101001
n-Butylbenzene ND ug/kg 06/03/22 22:17 104-51-806/02/22 20:105.0 1
sec-Butylbenzene ND ug/kg 06/03/22 22:17 135-98-806/02/22 20:105.0 1
tert-Butylbenzene ND ug/kg 06/03/22 22:17 98-06-606/02/22 20:105.0 1
Carbon tetrachloride ND ug/kg 06/03/22 22:17 56-23-506/02/22 20:105.0 1
Chlorobenzene ND ug/kg 06/03/22 22:17 108-90-706/02/22 20:105.0 1
Chloroethane ND ug/kg 06/03/22 22:17 75-00-306/02/22 20:1010.0 1
Chloroform ND ug/kg 06/03/22 22:17 67-66-306/02/22 20:105.0 1
Chloromethane ND ug/kg 06/03/22 22:17 74-87-306/02/22 20:1010.0 1
2-Chlorotoluene ND ug/kg 06/03/22 22:17 95-49-806/02/22 20:105.0 1
4-Chlorotoluene ND ug/kg 06/03/22 22:17 106-43-406/02/22 20:105.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 22:17 96-12-806/02/22 20:105.0 1
Dibromochloromethane ND ug/kg 06/03/22 22:17 124-48-106/02/22 20:105.0 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 22:17 106-93-406/02/22 20:105.0 1
Dibromomethane ND ug/kg 06/03/22 22:17 74-95-306/02/22 20:105.0 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 22:17 95-50-106/02/22 20:105.0 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 22:17 541-73-106/02/22 20:105.0 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 22:17 106-46-706/02/22 20:105.0 1
Dichlorodifluoromethane ND ug/kg 06/03/22 22:17 75-71-8 v106/02/22 20:1010.0 1
1,1-Dichloroethane ND ug/kg 06/03/22 22:17 75-34-306/02/22 20:105.0 1
1,2-Dichloroethane ND ug/kg 06/03/22 22:17 107-06-206/02/22 20:105.0 1
1,1-Dichloroethene ND ug/kg 06/03/22 22:17 75-35-406/02/22 20:105.0 1
cis-1,2-Dichloroethene ND ug/kg 06/03/22 22:17 156-59-206/02/22 20:105.0 1
trans-1,2-Dichloroethene ND ug/kg 06/03/22 22:17 156-60-506/02/22 20:105.0 1
1,2-Dichloropropane ND ug/kg 06/03/22 22:17 78-87-506/02/22 20:105.0 1
1,3-Dichloropropane ND ug/kg 06/03/22 22:17 142-28-906/02/22 20:105.0 1
2,2-Dichloropropane ND ug/kg 06/03/22 22:17 594-20-706/02/22 20:105.0 1
1,1-Dichloropropene ND ug/kg 06/03/22 22:17 563-58-606/02/22 20:105.0 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 22:17 10061-01-506/02/22 20:105.0 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 22:17 10061-02-606/02/22 20:105.0 1
Diisopropyl ether ND ug/kg 06/03/22 22:17 108-20-306/02/22 20:105.0 1
Ethylbenzene ND ug/kg 06/03/22 22:17 100-41-406/02/22 20:105.0 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 22:17 87-68-306/02/22 20:1010.0 1
2-Hexanone ND ug/kg 06/03/22 22:17 591-78-606/02/22 20:1050.2 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 22:17 98-82-806/02/22 20:105.0 1
p-Isopropyltoluene ND ug/kg 06/03/22 22:17 99-87-606/02/22 20:105.0 1
Methylene Chloride ND ug/kg 06/03/22 22:17 75-09-206/02/22 20:1020.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 22:17 108-10-106/02/22 20:1050.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-11 (0-4)Lab ID:92607493018 Collected:06/01/22 09:30 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/03/22 22:17 1634-04-406/02/22 20:105.0 1
Naphthalene ND ug/kg 06/03/22 22:17 91-20-306/02/22 20:105.0 1
n-Propylbenzene ND ug/kg 06/03/22 22:17 103-65-106/02/22 20:105.0 1
Styrene ND ug/kg 06/03/22 22:17 100-42-506/02/22 20:105.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 22:17 630-20-606/02/22 20:105.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 22:17 79-34-506/02/22 20:105.0 1
Tetrachloroethene 63.6 ug/kg 06/03/22 22:17 127-18-406/02/22 20:105.0 1
Toluene ND ug/kg 06/03/22 22:17 108-88-306/02/22 20:105.0 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 22:17 87-61-606/02/22 20:105.0 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 22:17 120-82-106/02/22 20:105.0 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 22:17 71-55-606/02/22 20:105.0 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 22:17 79-00-506/02/22 20:105.0 1
Trichloroethene ND ug/kg 06/03/22 22:17 79-01-606/02/22 20:105.0 1
Trichlorofluoromethane ND ug/kg 06/03/22 22:17 75-69-406/02/22 20:105.0 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 22:17 96-18-406/02/22 20:105.0 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 22:17 95-63-606/02/22 20:105.0 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 22:17 108-67-806/02/22 20:105.0 1
Vinyl acetate ND ug/kg 06/03/22 22:17 108-05-406/02/22 20:1050.2 1
Vinyl chloride ND ug/kg 06/03/22 22:17 75-01-4 v106/02/22 20:1010.0 1
Xylene (Total)ND ug/kg 06/03/22 22:17 1330-20-706/02/22 20:1010.0 1
m&p-Xylene ND ug/kg 06/03/22 22:17 179601-23-106/02/22 20:1010.0 1
o-Xylene ND ug/kg 06/03/22 22:17 95-47-606/02/22 20:105.0 1
Surrogates
Toluene-d8 (S)101 %06/03/22 22:17 2037-26-506/02/22 20:1070-130 1
4-Bromofluorobenzene (S)98 %06/03/22 22:17 460-00-406/02/22 20:1069-134 1
1,2-Dichloroethane-d4 (S)106 %06/03/22 22:17 17060-07-006/02/22 20:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 5.0 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-12 (4-8)Lab ID:92607493019 Collected:06/01/22 09:52 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 22:36 67-64-106/02/22 20:101391
Benzene ND ug/kg 06/03/22 22:36 71-43-206/02/22 20:107.0 1
Bromobenzene ND ug/kg 06/03/22 22:36 108-86-106/02/22 20:107.0 1
Bromochloromethane ND ug/kg 06/03/22 22:36 74-97-506/02/22 20:107.0 1
Bromodichloromethane ND ug/kg 06/03/22 22:36 75-27-406/02/22 20:107.0 1
Bromoform ND ug/kg 06/03/22 22:36 75-25-206/02/22 20:107.0 1
Bromomethane ND ug/kg 06/03/22 22:36 74-83-9 IK06/02/22 20:1013.9 1
2-Butanone (MEK)ND ug/kg 06/03/22 22:36 78-93-306/02/22 20:101391
n-Butylbenzene ND ug/kg 06/03/22 22:36 104-51-806/02/22 20:107.0 1
sec-Butylbenzene ND ug/kg 06/03/22 22:36 135-98-806/02/22 20:107.0 1
tert-Butylbenzene ND ug/kg 06/03/22 22:36 98-06-606/02/22 20:107.0 1
Carbon tetrachloride ND ug/kg 06/03/22 22:36 56-23-506/02/22 20:107.0 1
Chlorobenzene ND ug/kg 06/03/22 22:36 108-90-706/02/22 20:107.0 1
Chloroethane ND ug/kg 06/03/22 22:36 75-00-306/02/22 20:1013.9 1
Chloroform ND ug/kg 06/03/22 22:36 67-66-306/02/22 20:107.0 1
Chloromethane ND ug/kg 06/03/22 22:36 74-87-306/02/22 20:1013.9 1
2-Chlorotoluene ND ug/kg 06/03/22 22:36 95-49-806/02/22 20:107.0 1
4-Chlorotoluene ND ug/kg 06/03/22 22:36 106-43-406/02/22 20:107.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 22:36 96-12-806/02/22 20:107.0 1
Dibromochloromethane ND ug/kg 06/03/22 22:36 124-48-106/02/22 20:107.0 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 22:36 106-93-406/02/22 20:107.0 1
Dibromomethane ND ug/kg 06/03/22 22:36 74-95-306/02/22 20:107.0 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 22:36 95-50-106/02/22 20:107.0 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 22:36 541-73-106/02/22 20:107.0 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 22:36 106-46-706/02/22 20:107.0 1
Dichlorodifluoromethane ND ug/kg 06/03/22 22:36 75-71-8 v106/02/22 20:1013.9 1
1,1-Dichloroethane ND ug/kg 06/03/22 22:36 75-34-306/02/22 20:107.0 1
1,2-Dichloroethane ND ug/kg 06/03/22 22:36 107-06-206/02/22 20:107.0 1
1,1-Dichloroethene ND ug/kg 06/03/22 22:36 75-35-406/02/22 20:107.0 1
cis-1,2-Dichloroethene 39.5 ug/kg 06/03/22 22:36 156-59-206/02/22 20:107.0 1
trans-1,2-Dichloroethene ND ug/kg 06/03/22 22:36 156-60-506/02/22 20:107.0 1
1,2-Dichloropropane ND ug/kg 06/03/22 22:36 78-87-506/02/22 20:107.0 1
1,3-Dichloropropane ND ug/kg 06/03/22 22:36 142-28-906/02/22 20:107.0 1
2,2-Dichloropropane ND ug/kg 06/03/22 22:36 594-20-706/02/22 20:107.0 1
1,1-Dichloropropene ND ug/kg 06/03/22 22:36 563-58-606/02/22 20:107.0 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 22:36 10061-01-506/02/22 20:107.0 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 22:36 10061-02-606/02/22 20:107.0 1
Diisopropyl ether ND ug/kg 06/03/22 22:36 108-20-306/02/22 20:107.0 1
Ethylbenzene ND ug/kg 06/03/22 22:36 100-41-406/02/22 20:107.0 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 22:36 87-68-306/02/22 20:1013.9 1
2-Hexanone ND ug/kg 06/03/22 22:36 591-78-606/02/22 20:1069.5 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 22:36 98-82-806/02/22 20:107.0 1
p-Isopropyltoluene ND ug/kg 06/03/22 22:36 99-87-606/02/22 20:107.0 1
Methylene Chloride ND ug/kg 06/03/22 22:36 75-09-206/02/22 20:1027.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 22:36 108-10-106/02/22 20:1069.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 60 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-12 (4-8)Lab ID:92607493019 Collected:06/01/22 09:52 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/03/22 22:36 1634-04-406/02/22 20:107.0 1
Naphthalene ND ug/kg 06/03/22 22:36 91-20-306/02/22 20:107.0 1
n-Propylbenzene ND ug/kg 06/03/22 22:36 103-65-106/02/22 20:107.0 1
Styrene ND ug/kg 06/03/22 22:36 100-42-506/02/22 20:107.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 22:36 630-20-606/02/22 20:107.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 22:36 79-34-506/02/22 20:107.0 1
Tetrachloroethene 744 ug/kg 06/03/22 22:36 127-18-406/02/22 20:107.0 1
Toluene ND ug/kg 06/03/22 22:36 108-88-306/02/22 20:107.0 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 22:36 87-61-606/02/22 20:107.0 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 22:36 120-82-106/02/22 20:107.0 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 22:36 71-55-606/02/22 20:107.0 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 22:36 79-00-506/02/22 20:107.0 1
Trichloroethene 14.3 ug/kg 06/03/22 22:36 79-01-606/02/22 20:107.0 1
Trichlorofluoromethane ND ug/kg 06/03/22 22:36 75-69-406/02/22 20:107.0 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 22:36 96-18-406/02/22 20:107.0 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 22:36 95-63-606/02/22 20:107.0 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 22:36 108-67-806/02/22 20:107.0 1
Vinyl acetate ND ug/kg 06/03/22 22:36 108-05-406/02/22 20:1069.5 1
Vinyl chloride ND ug/kg 06/03/22 22:36 75-01-4 v106/02/22 20:1013.9 1
Xylene (Total)ND ug/kg 06/03/22 22:36 1330-20-706/02/22 20:1013.9 1
m&p-Xylene ND ug/kg 06/03/22 22:36 179601-23-106/02/22 20:1013.9 1
o-Xylene 7.6 ug/kg 06/03/22 22:36 95-47-606/02/22 20:107.0 1
Surrogates
Toluene-d8 (S)101 %06/03/22 22:36 2037-26-506/02/22 20:1070-130 1
4-Bromofluorobenzene (S)97 %06/03/22 22:36 460-00-406/02/22 20:1069-134 1
1,2-Dichloroethane-d4 (S)100 %06/03/22 22:36 17060-07-006/02/22 20:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.3 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-13 (0-4)Lab ID:92607493020 Collected:06/01/22 10:15 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 22:54 67-64-106/02/22 20:101531
Benzene ND ug/kg 06/03/22 22:54 71-43-206/02/22 20:107.6 1
Bromobenzene ND ug/kg 06/03/22 22:54 108-86-106/02/22 20:107.6 1
Bromochloromethane ND ug/kg 06/03/22 22:54 74-97-506/02/22 20:107.6 1
Bromodichloromethane ND ug/kg 06/03/22 22:54 75-27-406/02/22 20:107.6 1
Bromoform ND ug/kg 06/03/22 22:54 75-25-206/02/22 20:107.6 1
Bromomethane ND ug/kg 06/03/22 22:54 74-83-9 IK06/02/22 20:1015.3 1
2-Butanone (MEK)ND ug/kg 06/03/22 22:54 78-93-306/02/22 20:101531
n-Butylbenzene ND ug/kg 06/03/22 22:54 104-51-806/02/22 20:107.6 1
sec-Butylbenzene ND ug/kg 06/03/22 22:54 135-98-806/02/22 20:107.6 1
tert-Butylbenzene ND ug/kg 06/03/22 22:54 98-06-606/02/22 20:107.6 1
Carbon tetrachloride ND ug/kg 06/03/22 22:54 56-23-506/02/22 20:107.6 1
Chlorobenzene ND ug/kg 06/03/22 22:54 108-90-706/02/22 20:107.6 1
Chloroethane ND ug/kg 06/03/22 22:54 75-00-306/02/22 20:1015.3 1
Chloroform ND ug/kg 06/03/22 22:54 67-66-306/02/22 20:107.6 1
Chloromethane ND ug/kg 06/03/22 22:54 74-87-306/02/22 20:1015.3 1
2-Chlorotoluene ND ug/kg 06/03/22 22:54 95-49-806/02/22 20:107.6 1
4-Chlorotoluene ND ug/kg 06/03/22 22:54 106-43-406/02/22 20:107.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 22:54 96-12-806/02/22 20:107.6 1
Dibromochloromethane ND ug/kg 06/03/22 22:54 124-48-106/02/22 20:107.6 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 22:54 106-93-406/02/22 20:107.6 1
Dibromomethane ND ug/kg 06/03/22 22:54 74-95-306/02/22 20:107.6 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 22:54 95-50-106/02/22 20:107.6 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 22:54 541-73-106/02/22 20:107.6 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 22:54 106-46-706/02/22 20:107.6 1
Dichlorodifluoromethane ND ug/kg 06/03/22 22:54 75-71-8 v106/02/22 20:1015.3 1
1,1-Dichloroethane ND ug/kg 06/03/22 22:54 75-34-306/02/22 20:107.6 1
1,2-Dichloroethane ND ug/kg 06/03/22 22:54 107-06-206/02/22 20:107.6 1
1,1-Dichloroethene ND ug/kg 06/03/22 22:54 75-35-406/02/22 20:107.6 1
cis-1,2-Dichloroethene ND ug/kg 06/03/22 22:54 156-59-206/02/22 20:107.6 1
trans-1,2-Dichloroethene ND ug/kg 06/03/22 22:54 156-60-506/02/22 20:107.6 1
1,2-Dichloropropane ND ug/kg 06/03/22 22:54 78-87-506/02/22 20:107.6 1
1,3-Dichloropropane ND ug/kg 06/03/22 22:54 142-28-906/02/22 20:107.6 1
2,2-Dichloropropane ND ug/kg 06/03/22 22:54 594-20-706/02/22 20:107.6 1
1,1-Dichloropropene ND ug/kg 06/03/22 22:54 563-58-606/02/22 20:107.6 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 22:54 10061-01-506/02/22 20:107.6 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 22:54 10061-02-606/02/22 20:107.6 1
Diisopropyl ether ND ug/kg 06/03/22 22:54 108-20-306/02/22 20:107.6 1
Ethylbenzene ND ug/kg 06/03/22 22:54 100-41-406/02/22 20:107.6 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 22:54 87-68-306/02/22 20:1015.3 1
2-Hexanone ND ug/kg 06/03/22 22:54 591-78-606/02/22 20:1076.4 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 22:54 98-82-806/02/22 20:107.6 1
p-Isopropyltoluene ND ug/kg 06/03/22 22:54 99-87-606/02/22 20:107.6 1
Methylene Chloride ND ug/kg 06/03/22 22:54 75-09-206/02/22 20:1030.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 22:54 108-10-106/02/22 20:1076.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-13 (0-4)Lab ID:92607493020 Collected:06/01/22 10:15 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/03/22 22:54 1634-04-406/02/22 20:107.6 1
Naphthalene ND ug/kg 06/03/22 22:54 91-20-306/02/22 20:107.6 1
n-Propylbenzene ND ug/kg 06/03/22 22:54 103-65-106/02/22 20:107.6 1
Styrene ND ug/kg 06/03/22 22:54 100-42-506/02/22 20:107.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 22:54 630-20-606/02/22 20:107.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 22:54 79-34-506/02/22 20:107.6 1
Tetrachloroethene 135 ug/kg 06/03/22 22:54 127-18-406/02/22 20:107.6 1
Toluene ND ug/kg 06/03/22 22:54 108-88-306/02/22 20:107.6 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 22:54 87-61-606/02/22 20:107.6 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 22:54 120-82-106/02/22 20:107.6 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 22:54 71-55-606/02/22 20:107.6 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 22:54 79-00-506/02/22 20:107.6 1
Trichloroethene ND ug/kg 06/03/22 22:54 79-01-606/02/22 20:107.6 1
Trichlorofluoromethane ND ug/kg 06/03/22 22:54 75-69-406/02/22 20:107.6 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 22:54 96-18-406/02/22 20:107.6 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 22:54 95-63-606/02/22 20:107.6 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 22:54 108-67-806/02/22 20:107.6 1
Vinyl acetate ND ug/kg 06/03/22 22:54 108-05-406/02/22 20:1076.4 1
Vinyl chloride ND ug/kg 06/03/22 22:54 75-01-4 v106/02/22 20:1015.3 1
Xylene (Total)ND ug/kg 06/03/22 22:54 1330-20-706/02/22 20:1015.3 1
m&p-Xylene ND ug/kg 06/03/22 22:54 179601-23-106/02/22 20:1015.3 1
o-Xylene ND ug/kg 06/03/22 22:54 95-47-606/02/22 20:107.6 1
Surrogates
Toluene-d8 (S)102 %06/03/22 22:54 2037-26-506/02/22 20:1070-130 1
4-Bromofluorobenzene (S)98 %06/03/22 22:54 460-00-406/02/22 20:1069-134 1
1,2-Dichloroethane-d4 (S)106 %06/03/22 22:54 17060-07-006/02/22 20:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.1 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-15 (0.5-4)Lab ID:92607493021 Collected:06/01/22 10:45 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 23:13 67-64-106/02/22 20:101441
Benzene ND ug/kg 06/03/22 23:13 71-43-206/02/22 20:107.2 1
Bromobenzene ND ug/kg 06/03/22 23:13 108-86-106/02/22 20:107.2 1
Bromochloromethane ND ug/kg 06/03/22 23:13 74-97-506/02/22 20:107.2 1
Bromodichloromethane ND ug/kg 06/03/22 23:13 75-27-406/02/22 20:107.2 1
Bromoform ND ug/kg 06/03/22 23:13 75-25-206/02/22 20:107.2 1
Bromomethane ND ug/kg 06/03/22 23:13 74-83-9 IK06/02/22 20:1014.4 1
2-Butanone (MEK)ND ug/kg 06/03/22 23:13 78-93-306/02/22 20:101441
n-Butylbenzene ND ug/kg 06/03/22 23:13 104-51-806/02/22 20:107.2 1
sec-Butylbenzene ND ug/kg 06/03/22 23:13 135-98-806/02/22 20:107.2 1
tert-Butylbenzene ND ug/kg 06/03/22 23:13 98-06-606/02/22 20:107.2 1
Carbon tetrachloride ND ug/kg 06/03/22 23:13 56-23-506/02/22 20:107.2 1
Chlorobenzene ND ug/kg 06/03/22 23:13 108-90-706/02/22 20:107.2 1
Chloroethane ND ug/kg 06/03/22 23:13 75-00-306/02/22 20:1014.4 1
Chloroform ND ug/kg 06/03/22 23:13 67-66-306/02/22 20:107.2 1
Chloromethane ND ug/kg 06/03/22 23:13 74-87-306/02/22 20:1014.4 1
2-Chlorotoluene ND ug/kg 06/03/22 23:13 95-49-806/02/22 20:107.2 1
4-Chlorotoluene ND ug/kg 06/03/22 23:13 106-43-406/02/22 20:107.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 23:13 96-12-806/02/22 20:107.2 1
Dibromochloromethane ND ug/kg 06/03/22 23:13 124-48-106/02/22 20:107.2 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 23:13 106-93-406/02/22 20:107.2 1
Dibromomethane ND ug/kg 06/03/22 23:13 74-95-306/02/22 20:107.2 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 23:13 95-50-106/02/22 20:107.2 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 23:13 541-73-106/02/22 20:107.2 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 23:13 106-46-706/02/22 20:107.2 1
Dichlorodifluoromethane ND ug/kg 06/03/22 23:13 75-71-8 v106/02/22 20:1014.4 1
1,1-Dichloroethane ND ug/kg 06/03/22 23:13 75-34-306/02/22 20:107.2 1
1,2-Dichloroethane ND ug/kg 06/03/22 23:13 107-06-206/02/22 20:107.2 1
1,1-Dichloroethene ND ug/kg 06/03/22 23:13 75-35-406/02/22 20:107.2 1
cis-1,2-Dichloroethene ND ug/kg 06/03/22 23:13 156-59-206/02/22 20:107.2 1
trans-1,2-Dichloroethene ND ug/kg 06/03/22 23:13 156-60-506/02/22 20:107.2 1
1,2-Dichloropropane ND ug/kg 06/03/22 23:13 78-87-506/02/22 20:107.2 1
1,3-Dichloropropane ND ug/kg 06/03/22 23:13 142-28-906/02/22 20:107.2 1
2,2-Dichloropropane ND ug/kg 06/03/22 23:13 594-20-706/02/22 20:107.2 1
1,1-Dichloropropene ND ug/kg 06/03/22 23:13 563-58-606/02/22 20:107.2 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 23:13 10061-01-506/02/22 20:107.2 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 23:13 10061-02-606/02/22 20:107.2 1
Diisopropyl ether ND ug/kg 06/03/22 23:13 108-20-306/02/22 20:107.2 1
Ethylbenzene ND ug/kg 06/03/22 23:13 100-41-406/02/22 20:107.2 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 23:13 87-68-306/02/22 20:1014.4 1
2-Hexanone ND ug/kg 06/03/22 23:13 591-78-606/02/22 20:1072.2 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 23:13 98-82-806/02/22 20:107.2 1
p-Isopropyltoluene ND ug/kg 06/03/22 23:13 99-87-606/02/22 20:107.2 1
Methylene Chloride ND ug/kg 06/03/22 23:13 75-09-206/02/22 20:1028.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 23:13 108-10-106/02/22 20:1072.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-15 (0.5-4)Lab ID:92607493021 Collected:06/01/22 10:45 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/03/22 23:13 1634-04-406/02/22 20:107.2 1
Naphthalene ND ug/kg 06/03/22 23:13 91-20-306/02/22 20:107.2 1
n-Propylbenzene ND ug/kg 06/03/22 23:13 103-65-106/02/22 20:107.2 1
Styrene ND ug/kg 06/03/22 23:13 100-42-506/02/22 20:107.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 23:13 630-20-606/02/22 20:107.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 23:13 79-34-506/02/22 20:107.2 1
Tetrachloroethene 137 ug/kg 06/03/22 23:13 127-18-406/02/22 20:107.2 1
Toluene ND ug/kg 06/03/22 23:13 108-88-306/02/22 20:107.2 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 23:13 87-61-606/02/22 20:107.2 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 23:13 120-82-106/02/22 20:107.2 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 23:13 71-55-606/02/22 20:107.2 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 23:13 79-00-506/02/22 20:107.2 1
Trichloroethene ND ug/kg 06/03/22 23:13 79-01-606/02/22 20:107.2 1
Trichlorofluoromethane ND ug/kg 06/03/22 23:13 75-69-406/02/22 20:107.2 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 23:13 96-18-406/02/22 20:107.2 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 23:13 95-63-606/02/22 20:107.2 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 23:13 108-67-806/02/22 20:107.2 1
Vinyl acetate ND ug/kg 06/03/22 23:13 108-05-406/02/22 20:1072.2 1
Vinyl chloride ND ug/kg 06/03/22 23:13 75-01-4 v106/02/22 20:1014.4 1
Xylene (Total)ND ug/kg 06/03/22 23:13 1330-20-706/02/22 20:1014.4 1
m&p-Xylene ND ug/kg 06/03/22 23:13 179601-23-106/02/22 20:1014.4 1
o-Xylene ND ug/kg 06/03/22 23:13 95-47-606/02/22 20:107.2 1
Surrogates
Toluene-d8 (S)102 %06/03/22 23:13 2037-26-506/02/22 20:1070-130 1
4-Bromofluorobenzene (S)97 %06/03/22 23:13 460-00-406/02/22 20:1069-134 1
1,2-Dichloroethane-d4 (S)104 %06/03/22 23:13 17060-07-006/02/22 20:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.6 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-16 (8-12)Lab ID:92607493022 Collected:06/01/22 11:25 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/03/22 23:32 67-64-106/02/22 20:101221
Benzene ND ug/kg 06/03/22 23:32 71-43-206/02/22 20:106.1 1
Bromobenzene ND ug/kg 06/03/22 23:32 108-86-106/02/22 20:106.1 1
Bromochloromethane ND ug/kg 06/03/22 23:32 74-97-506/02/22 20:106.1 1
Bromodichloromethane ND ug/kg 06/03/22 23:32 75-27-406/02/22 20:106.1 1
Bromoform ND ug/kg 06/03/22 23:32 75-25-206/02/22 20:106.1 1
Bromomethane ND ug/kg 06/03/22 23:32 74-83-9 IK06/02/22 20:1012.2 1
2-Butanone (MEK)ND ug/kg 06/03/22 23:32 78-93-306/02/22 20:101221
n-Butylbenzene ND ug/kg 06/03/22 23:32 104-51-806/02/22 20:106.1 1
sec-Butylbenzene ND ug/kg 06/03/22 23:32 135-98-806/02/22 20:106.1 1
tert-Butylbenzene ND ug/kg 06/03/22 23:32 98-06-606/02/22 20:106.1 1
Carbon tetrachloride ND ug/kg 06/03/22 23:32 56-23-506/02/22 20:106.1 1
Chlorobenzene ND ug/kg 06/03/22 23:32 108-90-706/02/22 20:106.1 1
Chloroethane ND ug/kg 06/03/22 23:32 75-00-306/02/22 20:1012.2 1
Chloroform ND ug/kg 06/03/22 23:32 67-66-306/02/22 20:106.1 1
Chloromethane ND ug/kg 06/03/22 23:32 74-87-306/02/22 20:1012.2 1
2-Chlorotoluene ND ug/kg 06/03/22 23:32 95-49-806/02/22 20:106.1 1
4-Chlorotoluene ND ug/kg 06/03/22 23:32 106-43-406/02/22 20:106.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/03/22 23:32 96-12-806/02/22 20:106.1 1
Dibromochloromethane ND ug/kg 06/03/22 23:32 124-48-106/02/22 20:106.1 1
1,2-Dibromoethane (EDB)ND ug/kg 06/03/22 23:32 106-93-406/02/22 20:106.1 1
Dibromomethane ND ug/kg 06/03/22 23:32 74-95-306/02/22 20:106.1 1
1,2-Dichlorobenzene ND ug/kg 06/03/22 23:32 95-50-106/02/22 20:106.1 1
1,3-Dichlorobenzene ND ug/kg 06/03/22 23:32 541-73-106/02/22 20:106.1 1
1,4-Dichlorobenzene ND ug/kg 06/03/22 23:32 106-46-706/02/22 20:106.1 1
Dichlorodifluoromethane ND ug/kg 06/03/22 23:32 75-71-8 v106/02/22 20:1012.2 1
1,1-Dichloroethane ND ug/kg 06/03/22 23:32 75-34-306/02/22 20:106.1 1
1,2-Dichloroethane ND ug/kg 06/03/22 23:32 107-06-206/02/22 20:106.1 1
1,1-Dichloroethene ND ug/kg 06/03/22 23:32 75-35-406/02/22 20:106.1 1
cis-1,2-Dichloroethene ND ug/kg 06/03/22 23:32 156-59-206/02/22 20:106.1 1
trans-1,2-Dichloroethene ND ug/kg 06/03/22 23:32 156-60-506/02/22 20:106.1 1
1,2-Dichloropropane ND ug/kg 06/03/22 23:32 78-87-506/02/22 20:106.1 1
1,3-Dichloropropane ND ug/kg 06/03/22 23:32 142-28-906/02/22 20:106.1 1
2,2-Dichloropropane ND ug/kg 06/03/22 23:32 594-20-706/02/22 20:106.1 1
1,1-Dichloropropene ND ug/kg 06/03/22 23:32 563-58-606/02/22 20:106.1 1
cis-1,3-Dichloropropene ND ug/kg 06/03/22 23:32 10061-01-506/02/22 20:106.1 1
trans-1,3-Dichloropropene ND ug/kg 06/03/22 23:32 10061-02-606/02/22 20:106.1 1
Diisopropyl ether ND ug/kg 06/03/22 23:32 108-20-306/02/22 20:106.1 1
Ethylbenzene ND ug/kg 06/03/22 23:32 100-41-406/02/22 20:106.1 1
Hexachloro-1,3-butadiene ND ug/kg 06/03/22 23:32 87-68-306/02/22 20:1012.2 1
2-Hexanone ND ug/kg 06/03/22 23:32 591-78-606/02/22 20:1060.9 1
Isopropylbenzene (Cumene)ND ug/kg 06/03/22 23:32 98-82-806/02/22 20:106.1 1
p-Isopropyltoluene ND ug/kg 06/03/22 23:32 99-87-606/02/22 20:106.1 1
Methylene Chloride ND ug/kg 06/03/22 23:32 75-09-206/02/22 20:1024.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/03/22 23:32 108-10-106/02/22 20:1060.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-16 (8-12)Lab ID:92607493022 Collected:06/01/22 11:25 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/03/22 23:32 1634-04-406/02/22 20:106.1 1
Naphthalene ND ug/kg 06/03/22 23:32 91-20-306/02/22 20:106.1 1
n-Propylbenzene ND ug/kg 06/03/22 23:32 103-65-106/02/22 20:106.1 1
Styrene ND ug/kg 06/03/22 23:32 100-42-506/02/22 20:106.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/03/22 23:32 630-20-606/02/22 20:106.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/03/22 23:32 79-34-506/02/22 20:106.1 1
Tetrachloroethene 42.2 ug/kg 06/03/22 23:32 127-18-406/02/22 20:106.1 1
Toluene ND ug/kg 06/03/22 23:32 108-88-306/02/22 20:106.1 1
1,2,3-Trichlorobenzene ND ug/kg 06/03/22 23:32 87-61-606/02/22 20:106.1 1
1,2,4-Trichlorobenzene ND ug/kg 06/03/22 23:32 120-82-106/02/22 20:106.1 1
1,1,1-Trichloroethane ND ug/kg 06/03/22 23:32 71-55-606/02/22 20:106.1 1
1,1,2-Trichloroethane ND ug/kg 06/03/22 23:32 79-00-506/02/22 20:106.1 1
Trichloroethene ND ug/kg 06/03/22 23:32 79-01-606/02/22 20:106.1 1
Trichlorofluoromethane ND ug/kg 06/03/22 23:32 75-69-406/02/22 20:106.1 1
1,2,3-Trichloropropane ND ug/kg 06/03/22 23:32 96-18-406/02/22 20:106.1 1
1,2,4-Trimethylbenzene ND ug/kg 06/03/22 23:32 95-63-606/02/22 20:106.1 1
1,3,5-Trimethylbenzene ND ug/kg 06/03/22 23:32 108-67-806/02/22 20:106.1 1
Vinyl acetate ND ug/kg 06/03/22 23:32 108-05-406/02/22 20:1060.9 1
Vinyl chloride ND ug/kg 06/03/22 23:32 75-01-4 v106/02/22 20:1012.2 1
Xylene (Total)ND ug/kg 06/03/22 23:32 1330-20-706/02/22 20:1012.2 1
m&p-Xylene ND ug/kg 06/03/22 23:32 179601-23-106/02/22 20:1012.2 1
o-Xylene ND ug/kg 06/03/22 23:32 95-47-606/02/22 20:106.1 1
Surrogates
Toluene-d8 (S)100 %06/03/22 23:32 2037-26-506/02/22 20:1070-130 1
4-Bromofluorobenzene (S)97 %06/03/22 23:32 460-00-406/02/22 20:1069-134 1
1,2-Dichloroethane-d4 (S)104 %06/03/22 23:32 17060-07-006/02/22 20:1070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.6 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-17 (4-8)Lab ID:92607493023 Collected:06/01/22 11:50 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/06/22 20:51 67-64-106/06/22 13:185855
Benzene ND ug/kg 06/06/22 20:51 71-43-206/06/22 13:1829.2 5
Bromobenzene ND ug/kg 06/06/22 20:51 108-86-106/06/22 13:1829.2 5
Bromochloromethane ND ug/kg 06/06/22 20:51 74-97-506/06/22 13:1829.2 5
Bromodichloromethane ND ug/kg 06/06/22 20:51 75-27-406/06/22 13:1829.2 5
Bromoform ND ug/kg 06/06/22 20:51 75-25-206/06/22 13:1829.2 5
Bromomethane ND ug/kg 06/06/22 20:51 74-83-9 IK06/06/22 13:1858.5 5
2-Butanone (MEK)ND ug/kg 06/06/22 20:51 78-93-306/06/22 13:185855
n-Butylbenzene ND ug/kg 06/06/22 20:51 104-51-806/06/22 13:1829.2 5
sec-Butylbenzene ND ug/kg 06/06/22 20:51 135-98-806/06/22 13:1829.2 5
tert-Butylbenzene ND ug/kg 06/06/22 20:51 98-06-606/06/22 13:1829.2 5
Carbon tetrachloride ND ug/kg 06/06/22 20:51 56-23-506/06/22 13:1829.2 5
Chlorobenzene 39.1 ug/kg 06/06/22 20:51 108-90-706/06/22 13:1829.2 5
Chloroethane ND ug/kg 06/06/22 20:51 75-00-3 v106/06/22 13:1858.5 5
Chloroform ND ug/kg 06/06/22 20:51 67-66-306/06/22 13:1829.2 5
Chloromethane ND ug/kg 06/06/22 20:51 74-87-3 v106/06/22 13:1858.5 5
2-Chlorotoluene ND ug/kg 06/06/22 20:51 95-49-806/06/22 13:1829.2 5
4-Chlorotoluene ND ug/kg 06/06/22 20:51 106-43-406/06/22 13:1829.2 5
1,2-Dibromo-3-chloropropane ND ug/kg 06/06/22 20:51 96-12-806/06/22 13:1829.2 5
Dibromochloromethane ND ug/kg 06/06/22 20:51 124-48-106/06/22 13:1829.2 5
1,2-Dibromoethane (EDB)ND ug/kg 06/06/22 20:51 106-93-406/06/22 13:1829.2 5
Dibromomethane ND ug/kg 06/06/22 20:51 74-95-306/06/22 13:1829.2 5
1,2-Dichlorobenzene ND ug/kg 06/06/22 20:51 95-50-106/06/22 13:1829.2 5
1,3-Dichlorobenzene ND ug/kg 06/06/22 20:51 541-73-106/06/22 13:1829.2 5
1,4-Dichlorobenzene ND ug/kg 06/06/22 20:51 106-46-706/06/22 13:1829.2 5
Dichlorodifluoromethane ND ug/kg 06/06/22 20:51 75-71-8 v106/06/22 13:1858.5 5
1,1-Dichloroethane ND ug/kg 06/06/22 20:51 75-34-306/06/22 13:1829.2 5
1,2-Dichloroethane ND ug/kg 06/06/22 20:51 107-06-206/06/22 13:1829.2 5
1,1-Dichloroethene ND ug/kg 06/06/22 20:51 75-35-406/06/22 13:1829.2 5
cis-1,2-Dichloroethene 20300 ug/kg 06/06/22 20:51 156-59-206/06/22 13:1829.2 5
trans-1,2-Dichloroethene 176 ug/kg 06/06/22 20:51 156-60-506/06/22 13:1829.2 5
1,2-Dichloropropane ND ug/kg 06/06/22 20:51 78-87-506/06/22 13:1829.2 5
1,3-Dichloropropane ND ug/kg 06/06/22 20:51 142-28-906/06/22 13:1829.2 5
2,2-Dichloropropane ND ug/kg 06/06/22 20:51 594-20-706/06/22 13:1829.2 5
1,1-Dichloropropene ND ug/kg 06/06/22 20:51 563-58-606/06/22 13:1829.2 5
cis-1,3-Dichloropropene ND ug/kg 06/06/22 20:51 10061-01-506/06/22 13:1829.2 5
trans-1,3-Dichloropropene ND ug/kg 06/06/22 20:51 10061-02-606/06/22 13:1829.2 5
Diisopropyl ether ND ug/kg 06/06/22 20:51 108-20-306/06/22 13:1829.2 5
Ethylbenzene ND ug/kg 06/06/22 20:51 100-41-406/06/22 13:1829.2 5
Hexachloro-1,3-butadiene ND ug/kg 06/06/22 20:51 87-68-306/06/22 13:1858.5 5
2-Hexanone ND ug/kg 06/06/22 20:51 591-78-606/06/22 13:182925
Isopropylbenzene (Cumene)ND ug/kg 06/06/22 20:51 98-82-806/06/22 13:1829.2 5
p-Isopropyltoluene ND ug/kg 06/06/22 20:51 99-87-606/06/22 13:1829.2 5
Methylene Chloride 121 ug/kg 06/06/22 20:51 75-09-2 C706/06/22 13:181175
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/06/22 20:51 108-10-106/06/22 13:182925
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-17 (4-8)Lab ID:92607493023 Collected:06/01/22 11:50 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/06/22 20:51 1634-04-406/06/22 13:1829.2 5
Naphthalene ND ug/kg 06/06/22 20:51 91-20-306/06/22 13:1829.2 5
n-Propylbenzene ND ug/kg 06/06/22 20:51 103-65-106/06/22 13:1829.2 5
Styrene ND ug/kg 06/06/22 20:51 100-42-506/06/22 13:1829.2 5
1,1,1,2-Tetrachloroethane ND ug/kg 06/06/22 20:51 630-20-606/06/22 13:1829.2 5
1,1,2,2-Tetrachloroethane ND ug/kg 06/06/22 20:51 79-34-506/06/22 13:1829.2 5
Tetrachloroethene 3340 ug/kg 06/06/22 20:51 127-18-406/06/22 13:1829.2 5
Toluene ND ug/kg 06/06/22 20:51 108-88-306/06/22 13:1829.2 5
1,2,3-Trichlorobenzene ND ug/kg 06/06/22 20:51 87-61-606/06/22 13:1829.2 5
1,2,4-Trichlorobenzene ND ug/kg 06/06/22 20:51 120-82-106/06/22 13:1829.2 5
1,1,1-Trichloroethane ND ug/kg 06/06/22 20:51 71-55-606/06/22 13:1829.2 5
1,1,2-Trichloroethane ND ug/kg 06/06/22 20:51 79-00-506/06/22 13:1829.2 5
Trichloroethene 531 ug/kg 06/06/22 20:51 79-01-606/06/22 13:1829.2 5
Trichlorofluoromethane ND ug/kg 06/06/22 20:51 75-69-406/06/22 13:1829.2 5
1,2,3-Trichloropropane ND ug/kg 06/06/22 20:51 96-18-406/06/22 13:1829.2 5
1,2,4-Trimethylbenzene ND ug/kg 06/06/22 20:51 95-63-606/06/22 13:1829.2 5
1,3,5-Trimethylbenzene ND ug/kg 06/06/22 20:51 108-67-806/06/22 13:1829.2 5
Vinyl acetate ND ug/kg 06/06/22 20:51 108-05-406/06/22 13:182925
Vinyl chloride ND ug/kg 06/06/22 20:51 75-01-4 v106/06/22 13:1858.5 5
Xylene (Total)ND ug/kg 06/06/22 20:51 1330-20-706/06/22 13:1858.5 5
m&p-Xylene ND ug/kg 06/06/22 20:51 179601-23-106/06/22 13:1858.5 5
o-Xylene ND ug/kg 06/06/22 20:51 95-47-606/06/22 13:1829.2 5
Surrogates
Toluene-d8 (S)98 %06/06/22 20:51 2037-26-506/06/22 13:1870-130 5
4-Bromofluorobenzene (S)100 %06/06/22 20:51 460-00-406/06/22 13:1869-134 5
1,2-Dichloroethane-d4 (S)101 %06/06/22 20:51 17060-07-006/06/22 13:1870-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.3 %06/06/22 15:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-17 (8-12)Lab ID:92607493024 Collected:06/01/22 11:55 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/06/22 21:26 67-64-106/06/22 13:186095
Benzene ND ug/kg 06/06/22 21:26 71-43-206/06/22 13:1830.5 5
Bromobenzene ND ug/kg 06/06/22 21:26 108-86-106/06/22 13:1830.5 5
Bromochloromethane ND ug/kg 06/06/22 21:26 74-97-506/06/22 13:1830.5 5
Bromodichloromethane ND ug/kg 06/06/22 21:26 75-27-406/06/22 13:1830.5 5
Bromoform ND ug/kg 06/06/22 21:26 75-25-206/06/22 13:1830.5 5
Bromomethane ND ug/kg 06/06/22 21:26 74-83-9 IK06/06/22 13:1860.9 5
2-Butanone (MEK)ND ug/kg 06/06/22 21:26 78-93-306/06/22 13:186095
n-Butylbenzene ND ug/kg 06/06/22 21:26 104-51-806/06/22 13:1830.5 5
sec-Butylbenzene ND ug/kg 06/06/22 21:26 135-98-806/06/22 13:1830.5 5
tert-Butylbenzene ND ug/kg 06/06/22 21:26 98-06-606/06/22 13:1830.5 5
Carbon tetrachloride ND ug/kg 06/06/22 21:26 56-23-506/06/22 13:1830.5 5
Chlorobenzene ND ug/kg 06/06/22 21:26 108-90-706/06/22 13:1830.5 5
Chloroethane ND ug/kg 06/06/22 21:26 75-00-3 v106/06/22 13:1860.9 5
Chloroform ND ug/kg 06/06/22 21:26 67-66-306/06/22 13:1830.5 5
Chloromethane ND ug/kg 06/06/22 21:26 74-87-3 v106/06/22 13:1860.9 5
2-Chlorotoluene ND ug/kg 06/06/22 21:26 95-49-806/06/22 13:1830.5 5
4-Chlorotoluene ND ug/kg 06/06/22 21:26 106-43-406/06/22 13:1830.5 5
1,2-Dibromo-3-chloropropane ND ug/kg 06/06/22 21:26 96-12-806/06/22 13:1830.5 5
Dibromochloromethane ND ug/kg 06/06/22 21:26 124-48-106/06/22 13:1830.5 5
1,2-Dibromoethane (EDB)ND ug/kg 06/06/22 21:26 106-93-406/06/22 13:1830.5 5
Dibromomethane ND ug/kg 06/06/22 21:26 74-95-306/06/22 13:1830.5 5
1,2-Dichlorobenzene ND ug/kg 06/06/22 21:26 95-50-106/06/22 13:1830.5 5
1,3-Dichlorobenzene ND ug/kg 06/06/22 21:26 541-73-106/06/22 13:1830.5 5
1,4-Dichlorobenzene ND ug/kg 06/06/22 21:26 106-46-706/06/22 13:1830.5 5
Dichlorodifluoromethane ND ug/kg 06/06/22 21:26 75-71-8 v106/06/22 13:1860.9 5
1,1-Dichloroethane ND ug/kg 06/06/22 21:26 75-34-306/06/22 13:1830.5 5
1,2-Dichloroethane ND ug/kg 06/06/22 21:26 107-06-206/06/22 13:1830.5 5
1,1-Dichloroethene ND ug/kg 06/06/22 21:26 75-35-406/06/22 13:1830.5 5
cis-1,2-Dichloroethene 19400 ug/kg 06/06/22 21:26 156-59-206/06/22 13:1830.5 5
trans-1,2-Dichloroethene 134 ug/kg 06/06/22 21:26 156-60-506/06/22 13:1830.5 5
1,2-Dichloropropane ND ug/kg 06/06/22 21:26 78-87-506/06/22 13:1830.5 5
1,3-Dichloropropane ND ug/kg 06/06/22 21:26 142-28-906/06/22 13:1830.5 5
2,2-Dichloropropane ND ug/kg 06/06/22 21:26 594-20-706/06/22 13:1830.5 5
1,1-Dichloropropene ND ug/kg 06/06/22 21:26 563-58-606/06/22 13:1830.5 5
cis-1,3-Dichloropropene ND ug/kg 06/06/22 21:26 10061-01-506/06/22 13:1830.5 5
trans-1,3-Dichloropropene ND ug/kg 06/06/22 21:26 10061-02-606/06/22 13:1830.5 5
Diisopropyl ether ND ug/kg 06/06/22 21:26 108-20-306/06/22 13:1830.5 5
Ethylbenzene ND ug/kg 06/06/22 21:26 100-41-406/06/22 13:1830.5 5
Hexachloro-1,3-butadiene ND ug/kg 06/06/22 21:26 87-68-306/06/22 13:1860.9 5
2-Hexanone ND ug/kg 06/06/22 21:26 591-78-606/06/22 13:183055
Isopropylbenzene (Cumene)ND ug/kg 06/06/22 21:26 98-82-806/06/22 13:1830.5 5
p-Isopropyltoluene ND ug/kg 06/06/22 21:26 99-87-606/06/22 13:1830.5 5
Methylene Chloride ND ug/kg 06/06/22 21:26 75-09-206/06/22 13:181225
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/06/22 21:26 108-10-106/06/22 13:183055
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-17 (8-12)Lab ID:92607493024 Collected:06/01/22 11:55 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/06/22 21:26 1634-04-406/06/22 13:1830.5 5
Naphthalene ND ug/kg 06/06/22 21:26 91-20-306/06/22 13:1830.5 5
n-Propylbenzene ND ug/kg 06/06/22 21:26 103-65-106/06/22 13:1830.5 5
Styrene ND ug/kg 06/06/22 21:26 100-42-506/06/22 13:1830.5 5
1,1,1,2-Tetrachloroethane ND ug/kg 06/06/22 21:26 630-20-606/06/22 13:1830.5 5
1,1,2,2-Tetrachloroethane ND ug/kg 06/06/22 21:26 79-34-506/06/22 13:1830.5 5
Tetrachloroethene 1040 ug/kg 06/06/22 21:26 127-18-406/06/22 13:1830.5 5
Toluene ND ug/kg 06/06/22 21:26 108-88-306/06/22 13:1830.5 5
1,2,3-Trichlorobenzene ND ug/kg 06/06/22 21:26 87-61-606/06/22 13:1830.5 5
1,2,4-Trichlorobenzene ND ug/kg 06/06/22 21:26 120-82-106/06/22 13:1830.5 5
1,1,1-Trichloroethane ND ug/kg 06/06/22 21:26 71-55-606/06/22 13:1830.5 5
1,1,2-Trichloroethane ND ug/kg 06/06/22 21:26 79-00-506/06/22 13:1830.5 5
Trichloroethene 539 ug/kg 06/06/22 21:26 79-01-606/06/22 13:1830.5 5
Trichlorofluoromethane ND ug/kg 06/06/22 21:26 75-69-406/06/22 13:1830.5 5
1,2,3-Trichloropropane ND ug/kg 06/06/22 21:26 96-18-406/06/22 13:1830.5 5
1,2,4-Trimethylbenzene ND ug/kg 06/06/22 21:26 95-63-606/06/22 13:1830.5 5
1,3,5-Trimethylbenzene ND ug/kg 06/06/22 21:26 108-67-806/06/22 13:1830.5 5
Vinyl acetate ND ug/kg 06/06/22 21:26 108-05-406/06/22 13:183055
Vinyl chloride ND ug/kg 06/06/22 21:26 75-01-4 v106/06/22 13:1860.9 5
Xylene (Total)ND ug/kg 06/06/22 21:26 1330-20-706/06/22 13:1860.9 5
m&p-Xylene ND ug/kg 06/06/22 21:26 179601-23-106/06/22 13:1860.9 5
o-Xylene ND ug/kg 06/06/22 21:26 95-47-606/06/22 13:1830.5 5
Surrogates
Toluene-d8 (S)98 %06/06/22 21:26 2037-26-506/06/22 13:1870-130 5
4-Bromofluorobenzene (S)99 %06/06/22 21:26 460-00-406/06/22 13:1869-134 5
1,2-Dichloroethane-d4 (S)99 %06/06/22 21:26 17060-07-006/06/22 13:1870-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.2 %06/06/22 15:56 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-18 (4-8)Lab ID:92607493025 Collected:06/01/22 12:05 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/06/22 17:54 67-64-106/06/22 13:181151
Benzene ND ug/kg 06/06/22 17:54 71-43-206/06/22 13:185.8 1
Bromobenzene ND ug/kg 06/06/22 17:54 108-86-106/06/22 13:185.8 1
Bromochloromethane ND ug/kg 06/06/22 17:54 74-97-506/06/22 13:185.8 1
Bromodichloromethane ND ug/kg 06/06/22 17:54 75-27-406/06/22 13:185.8 1
Bromoform ND ug/kg 06/06/22 17:54 75-25-206/06/22 13:185.8 1
Bromomethane ND ug/kg 06/06/22 17:54 74-83-9 IK06/06/22 13:1811.5 1
2-Butanone (MEK)ND ug/kg 06/06/22 17:54 78-93-306/06/22 13:181151
n-Butylbenzene ND ug/kg 06/06/22 17:54 104-51-806/06/22 13:185.8 1
sec-Butylbenzene ND ug/kg 06/06/22 17:54 135-98-806/06/22 13:185.8 1
tert-Butylbenzene ND ug/kg 06/06/22 17:54 98-06-606/06/22 13:185.8 1
Carbon tetrachloride ND ug/kg 06/06/22 17:54 56-23-506/06/22 13:185.8 1
Chlorobenzene ND ug/kg 06/06/22 17:54 108-90-706/06/22 13:185.8 1
Chloroethane ND ug/kg 06/06/22 17:54 75-00-3 v106/06/22 13:1811.5 1
Chloroform ND ug/kg 06/06/22 17:54 67-66-306/06/22 13:185.8 1
Chloromethane ND ug/kg 06/06/22 17:54 74-87-3 v106/06/22 13:1811.5 1
2-Chlorotoluene ND ug/kg 06/06/22 17:54 95-49-806/06/22 13:185.8 1
4-Chlorotoluene ND ug/kg 06/06/22 17:54 106-43-406/06/22 13:185.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/06/22 17:54 96-12-806/06/22 13:185.8 1
Dibromochloromethane ND ug/kg 06/06/22 17:54 124-48-106/06/22 13:185.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/06/22 17:54 106-93-406/06/22 13:185.8 1
Dibromomethane ND ug/kg 06/06/22 17:54 74-95-306/06/22 13:185.8 1
1,2-Dichlorobenzene ND ug/kg 06/06/22 17:54 95-50-106/06/22 13:185.8 1
1,3-Dichlorobenzene ND ug/kg 06/06/22 17:54 541-73-106/06/22 13:185.8 1
1,4-Dichlorobenzene ND ug/kg 06/06/22 17:54 106-46-706/06/22 13:185.8 1
Dichlorodifluoromethane ND ug/kg 06/06/22 17:54 75-71-8 v106/06/22 13:1811.5 1
1,1-Dichloroethane ND ug/kg 06/06/22 17:54 75-34-306/06/22 13:185.8 1
1,2-Dichloroethane ND ug/kg 06/06/22 17:54 107-06-206/06/22 13:185.8 1
1,1-Dichloroethene ND ug/kg 06/06/22 17:54 75-35-406/06/22 13:185.8 1
cis-1,2-Dichloroethene ND ug/kg 06/06/22 17:54 156-59-206/06/22 13:185.8 1
trans-1,2-Dichloroethene ND ug/kg 06/06/22 17:54 156-60-506/06/22 13:185.8 1
1,2-Dichloropropane ND ug/kg 06/06/22 17:54 78-87-506/06/22 13:185.8 1
1,3-Dichloropropane ND ug/kg 06/06/22 17:54 142-28-906/06/22 13:185.8 1
2,2-Dichloropropane ND ug/kg 06/06/22 17:54 594-20-706/06/22 13:185.8 1
1,1-Dichloropropene ND ug/kg 06/06/22 17:54 563-58-606/06/22 13:185.8 1
cis-1,3-Dichloropropene ND ug/kg 06/06/22 17:54 10061-01-506/06/22 13:185.8 1
trans-1,3-Dichloropropene ND ug/kg 06/06/22 17:54 10061-02-606/06/22 13:185.8 1
Diisopropyl ether ND ug/kg 06/06/22 17:54 108-20-306/06/22 13:185.8 1
Ethylbenzene ND ug/kg 06/06/22 17:54 100-41-406/06/22 13:185.8 1
Hexachloro-1,3-butadiene ND ug/kg 06/06/22 17:54 87-68-306/06/22 13:1811.5 1
2-Hexanone ND ug/kg 06/06/22 17:54 591-78-606/06/22 13:1857.6 1
Isopropylbenzene (Cumene)ND ug/kg 06/06/22 17:54 98-82-806/06/22 13:185.8 1
p-Isopropyltoluene ND ug/kg 06/06/22 17:54 99-87-606/06/22 13:185.8 1
Methylene Chloride ND ug/kg 06/06/22 17:54 75-09-206/06/22 13:1823.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/06/22 17:54 108-10-106/06/22 13:1857.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-18 (4-8)Lab ID:92607493025 Collected:06/01/22 12:05 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/06/22 17:54 1634-04-406/06/22 13:185.8 1
Naphthalene ND ug/kg 06/06/22 17:54 91-20-306/06/22 13:185.8 1
n-Propylbenzene ND ug/kg 06/06/22 17:54 103-65-106/06/22 13:185.8 1
Styrene ND ug/kg 06/06/22 17:54 100-42-506/06/22 13:185.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/06/22 17:54 630-20-606/06/22 13:185.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/06/22 17:54 79-34-506/06/22 13:185.8 1
Tetrachloroethene 76.4 ug/kg 06/06/22 17:54 127-18-406/06/22 13:185.8 1
Toluene ND ug/kg 06/06/22 17:54 108-88-306/06/22 13:185.8 1
1,2,3-Trichlorobenzene ND ug/kg 06/06/22 17:54 87-61-606/06/22 13:185.8 1
1,2,4-Trichlorobenzene ND ug/kg 06/06/22 17:54 120-82-106/06/22 13:185.8 1
1,1,1-Trichloroethane ND ug/kg 06/06/22 17:54 71-55-606/06/22 13:185.8 1
1,1,2-Trichloroethane ND ug/kg 06/06/22 17:54 79-00-506/06/22 13:185.8 1
Trichloroethene ND ug/kg 06/06/22 17:54 79-01-606/06/22 13:185.8 1
Trichlorofluoromethane ND ug/kg 06/06/22 17:54 75-69-406/06/22 13:185.8 1
1,2,3-Trichloropropane ND ug/kg 06/06/22 17:54 96-18-406/06/22 13:185.8 1
1,2,4-Trimethylbenzene ND ug/kg 06/06/22 17:54 95-63-606/06/22 13:185.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/06/22 17:54 108-67-806/06/22 13:185.8 1
Vinyl acetate ND ug/kg 06/06/22 17:54 108-05-406/06/22 13:1857.6 1
Vinyl chloride ND ug/kg 06/06/22 17:54 75-01-4 v106/06/22 13:1811.5 1
Xylene (Total)ND ug/kg 06/06/22 17:54 1330-20-706/06/22 13:1811.5 1
m&p-Xylene ND ug/kg 06/06/22 17:54 179601-23-106/06/22 13:1811.5 1
o-Xylene ND ug/kg 06/06/22 17:54 95-47-606/06/22 13:185.8 1
Surrogates
Toluene-d8 (S)99 %06/06/22 17:54 2037-26-506/06/22 13:1870-130 1
4-Bromofluorobenzene (S)100 %06/06/22 17:54 460-00-406/06/22 13:1869-134 1
1,2-Dichloroethane-d4 (S)97 %06/06/22 17:54 17060-07-006/06/22 13:1870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.7 %06/06/22 15:56 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-19 (8-12)Lab ID:92607493026 Collected:06/01/22 12:30 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/06/22 18:12 67-64-106/06/22 13:181311
Benzene ND ug/kg 06/06/22 18:12 71-43-206/06/22 13:186.5 1
Bromobenzene ND ug/kg 06/06/22 18:12 108-86-106/06/22 13:186.5 1
Bromochloromethane ND ug/kg 06/06/22 18:12 74-97-506/06/22 13:186.5 1
Bromodichloromethane ND ug/kg 06/06/22 18:12 75-27-406/06/22 13:186.5 1
Bromoform ND ug/kg 06/06/22 18:12 75-25-206/06/22 13:186.5 1
Bromomethane ND ug/kg 06/06/22 18:12 74-83-9 IK06/06/22 13:1813.1 1
2-Butanone (MEK)ND ug/kg 06/06/22 18:12 78-93-306/06/22 13:181311
n-Butylbenzene ND ug/kg 06/06/22 18:12 104-51-806/06/22 13:186.5 1
sec-Butylbenzene ND ug/kg 06/06/22 18:12 135-98-806/06/22 13:186.5 1
tert-Butylbenzene ND ug/kg 06/06/22 18:12 98-06-606/06/22 13:186.5 1
Carbon tetrachloride ND ug/kg 06/06/22 18:12 56-23-506/06/22 13:186.5 1
Chlorobenzene ND ug/kg 06/06/22 18:12 108-90-706/06/22 13:186.5 1
Chloroethane ND ug/kg 06/06/22 18:12 75-00-3 v106/06/22 13:1813.1 1
Chloroform ND ug/kg 06/06/22 18:12 67-66-306/06/22 13:186.5 1
Chloromethane ND ug/kg 06/06/22 18:12 74-87-3 v106/06/22 13:1813.1 1
2-Chlorotoluene ND ug/kg 06/06/22 18:12 95-49-806/06/22 13:186.5 1
4-Chlorotoluene ND ug/kg 06/06/22 18:12 106-43-406/06/22 13:186.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/06/22 18:12 96-12-806/06/22 13:186.5 1
Dibromochloromethane ND ug/kg 06/06/22 18:12 124-48-106/06/22 13:186.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/06/22 18:12 106-93-406/06/22 13:186.5 1
Dibromomethane ND ug/kg 06/06/22 18:12 74-95-306/06/22 13:186.5 1
1,2-Dichlorobenzene ND ug/kg 06/06/22 18:12 95-50-106/06/22 13:186.5 1
1,3-Dichlorobenzene ND ug/kg 06/06/22 18:12 541-73-106/06/22 13:186.5 1
1,4-Dichlorobenzene ND ug/kg 06/06/22 18:12 106-46-706/06/22 13:186.5 1
Dichlorodifluoromethane ND ug/kg 06/06/22 18:12 75-71-8 v106/06/22 13:1813.1 1
1,1-Dichloroethane ND ug/kg 06/06/22 18:12 75-34-306/06/22 13:186.5 1
1,2-Dichloroethane ND ug/kg 06/06/22 18:12 107-06-206/06/22 13:186.5 1
1,1-Dichloroethene ND ug/kg 06/06/22 18:12 75-35-406/06/22 13:186.5 1
cis-1,2-Dichloroethene 71.7 ug/kg 06/06/22 18:12 156-59-206/06/22 13:186.5 1
trans-1,2-Dichloroethene ND ug/kg 06/06/22 18:12 156-60-506/06/22 13:186.5 1
1,2-Dichloropropane ND ug/kg 06/06/22 18:12 78-87-506/06/22 13:186.5 1
1,3-Dichloropropane ND ug/kg 06/06/22 18:12 142-28-906/06/22 13:186.5 1
2,2-Dichloropropane ND ug/kg 06/06/22 18:12 594-20-706/06/22 13:186.5 1
1,1-Dichloropropene ND ug/kg 06/06/22 18:12 563-58-606/06/22 13:186.5 1
cis-1,3-Dichloropropene ND ug/kg 06/06/22 18:12 10061-01-506/06/22 13:186.5 1
trans-1,3-Dichloropropene ND ug/kg 06/06/22 18:12 10061-02-606/06/22 13:186.5 1
Diisopropyl ether ND ug/kg 06/06/22 18:12 108-20-306/06/22 13:186.5 1
Ethylbenzene ND ug/kg 06/06/22 18:12 100-41-406/06/22 13:186.5 1
Hexachloro-1,3-butadiene ND ug/kg 06/06/22 18:12 87-68-306/06/22 13:1813.1 1
2-Hexanone ND ug/kg 06/06/22 18:12 591-78-606/06/22 13:1865.3 1
Isopropylbenzene (Cumene)ND ug/kg 06/06/22 18:12 98-82-806/06/22 13:186.5 1
p-Isopropyltoluene ND ug/kg 06/06/22 18:12 99-87-606/06/22 13:186.5 1
Methylene Chloride ND ug/kg 06/06/22 18:12 75-09-206/06/22 13:1826.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/06/22 18:12 108-10-106/06/22 13:1865.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-19 (8-12)Lab ID:92607493026 Collected:06/01/22 12:30 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/06/22 18:12 1634-04-406/06/22 13:186.5 1
Naphthalene ND ug/kg 06/06/22 18:12 91-20-306/06/22 13:186.5 1
n-Propylbenzene ND ug/kg 06/06/22 18:12 103-65-106/06/22 13:186.5 1
Styrene ND ug/kg 06/06/22 18:12 100-42-506/06/22 13:186.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/06/22 18:12 630-20-606/06/22 13:186.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/06/22 18:12 79-34-506/06/22 13:186.5 1
Tetrachloroethene 719 ug/kg 06/06/22 18:12 127-18-406/06/22 13:186.5 1
Toluene ND ug/kg 06/06/22 18:12 108-88-306/06/22 13:186.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/06/22 18:12 87-61-606/06/22 13:186.5 1
1,2,4-Trichlorobenzene ND ug/kg 06/06/22 18:12 120-82-106/06/22 13:186.5 1
1,1,1-Trichloroethane ND ug/kg 06/06/22 18:12 71-55-606/06/22 13:186.5 1
1,1,2-Trichloroethane ND ug/kg 06/06/22 18:12 79-00-506/06/22 13:186.5 1
Trichloroethene 29.3 ug/kg 06/06/22 18:12 79-01-606/06/22 13:186.5 1
Trichlorofluoromethane ND ug/kg 06/06/22 18:12 75-69-406/06/22 13:186.5 1
1,2,3-Trichloropropane ND ug/kg 06/06/22 18:12 96-18-406/06/22 13:186.5 1
1,2,4-Trimethylbenzene ND ug/kg 06/06/22 18:12 95-63-606/06/22 13:186.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/06/22 18:12 108-67-806/06/22 13:186.5 1
Vinyl acetate ND ug/kg 06/06/22 18:12 108-05-406/06/22 13:1865.3 1
Vinyl chloride ND ug/kg 06/06/22 18:12 75-01-4 v106/06/22 13:1813.1 1
Xylene (Total)ND ug/kg 06/06/22 18:12 1330-20-706/06/22 13:1813.1 1
m&p-Xylene ND ug/kg 06/06/22 18:12 179601-23-106/06/22 13:1813.1 1
o-Xylene 6.9 ug/kg 06/06/22 18:12 95-47-606/06/22 13:186.5 1
Surrogates
Toluene-d8 (S)99 %06/06/22 18:12 2037-26-506/06/22 13:1870-130 1
4-Bromofluorobenzene (S)98 %06/06/22 18:12 460-00-406/06/22 13:1869-134 1
1,2-Dichloroethane-d4 (S)99 %06/06/22 18:12 17060-07-006/06/22 13:1870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.1 %06/06/22 16:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-20 (4-8)Lab ID:92607493027 Collected:06/01/22 12:45 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/08/22 00:25 67-64-106/07/22 16:123642
Benzene ND ug/kg 06/08/22 00:25 71-43-206/07/22 16:1218.2 2
Bromobenzene ND ug/kg 06/08/22 00:25 108-86-106/07/22 16:1218.2 2
Bromochloromethane ND ug/kg 06/08/22 00:25 74-97-506/07/22 16:1218.2 2
Bromodichloromethane ND ug/kg 06/08/22 00:25 75-27-406/07/22 16:1218.2 2
Bromoform ND ug/kg 06/08/22 00:25 75-25-206/07/22 16:1218.2 2
Bromomethane ND ug/kg 06/08/22 00:25 74-83-9 IK06/07/22 16:1236.4 2
2-Butanone (MEK)ND ug/kg 06/08/22 00:25 78-93-306/07/22 16:123642
n-Butylbenzene ND ug/kg 06/08/22 00:25 104-51-806/07/22 16:1218.2 2
sec-Butylbenzene ND ug/kg 06/08/22 00:25 135-98-806/07/22 16:1218.2 2
tert-Butylbenzene ND ug/kg 06/08/22 00:25 98-06-606/07/22 16:1218.2 2
Carbon tetrachloride ND ug/kg 06/08/22 00:25 56-23-506/07/22 16:1218.2 2
Chlorobenzene ND ug/kg 06/08/22 00:25 108-90-706/07/22 16:1218.2 2
Chloroethane ND ug/kg 06/08/22 00:25 75-00-306/07/22 16:1236.4 2
Chloroform ND ug/kg 06/08/22 00:25 67-66-306/07/22 16:1218.2 2
Chloromethane ND ug/kg 06/08/22 00:25 74-87-306/07/22 16:1236.4 2
2-Chlorotoluene ND ug/kg 06/08/22 00:25 95-49-806/07/22 16:1218.2 2
4-Chlorotoluene ND ug/kg 06/08/22 00:25 106-43-406/07/22 16:1218.2 2
1,2-Dibromo-3-chloropropane ND ug/kg 06/08/22 00:25 96-12-806/07/22 16:1218.2 2
Dibromochloromethane ND ug/kg 06/08/22 00:25 124-48-106/07/22 16:1218.2 2
1,2-Dibromoethane (EDB)ND ug/kg 06/08/22 00:25 106-93-406/07/22 16:1218.2 2
Dibromomethane ND ug/kg 06/08/22 00:25 74-95-306/07/22 16:1218.2 2
1,2-Dichlorobenzene ND ug/kg 06/08/22 00:25 95-50-106/07/22 16:1218.2 2
1,3-Dichlorobenzene ND ug/kg 06/08/22 00:25 541-73-106/07/22 16:1218.2 2
1,4-Dichlorobenzene ND ug/kg 06/08/22 00:25 106-46-706/07/22 16:1218.2 2
Dichlorodifluoromethane ND ug/kg 06/08/22 00:25 75-71-8 L1,v106/07/22 16:1236.4 2
1,1-Dichloroethane ND ug/kg 06/08/22 00:25 75-34-306/07/22 16:1218.2 2
1,2-Dichloroethane ND ug/kg 06/08/22 00:25 107-06-206/07/22 16:1218.2 2
1,1-Dichloroethene ND ug/kg 06/08/22 00:25 75-35-406/07/22 16:1218.2 2
cis-1,2-Dichloroethene 394 ug/kg 06/08/22 00:25 156-59-206/07/22 16:1218.2 2
trans-1,2-Dichloroethene ND ug/kg 06/08/22 00:25 156-60-506/07/22 16:1218.2 2
1,2-Dichloropropane ND ug/kg 06/08/22 00:25 78-87-506/07/22 16:1218.2 2
1,3-Dichloropropane ND ug/kg 06/08/22 00:25 142-28-906/07/22 16:1218.2 2
2,2-Dichloropropane ND ug/kg 06/08/22 00:25 594-20-706/07/22 16:1218.2 2
1,1-Dichloropropene ND ug/kg 06/08/22 00:25 563-58-606/07/22 16:1218.2 2
cis-1,3-Dichloropropene ND ug/kg 06/08/22 00:25 10061-01-506/07/22 16:1218.2 2
trans-1,3-Dichloropropene ND ug/kg 06/08/22 00:25 10061-02-606/07/22 16:1218.2 2
Diisopropyl ether ND ug/kg 06/08/22 00:25 108-20-306/07/22 16:1218.2 2
Ethylbenzene ND ug/kg 06/08/22 00:25 100-41-406/07/22 16:1218.2 2
Hexachloro-1,3-butadiene ND ug/kg 06/08/22 00:25 87-68-306/07/22 16:1236.4 2
2-Hexanone ND ug/kg 06/08/22 00:25 591-78-606/07/22 16:121822
Isopropylbenzene (Cumene)ND ug/kg 06/08/22 00:25 98-82-806/07/22 16:1218.2 2
p-Isopropyltoluene ND ug/kg 06/08/22 00:25 99-87-606/07/22 16:1218.2 2
Methylene Chloride 328 ug/kg 06/08/22 00:25 75-09-2 C906/07/22 16:1272.7 2
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/08/22 00:25 108-10-106/07/22 16:121822
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-20 (4-8)Lab ID:92607493027 Collected:06/01/22 12:45 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/08/22 00:25 1634-04-406/07/22 16:1218.2 2
Naphthalene ND ug/kg 06/08/22 00:25 91-20-306/07/22 16:1218.2 2
n-Propylbenzene ND ug/kg 06/08/22 00:25 103-65-106/07/22 16:1218.2 2
Styrene ND ug/kg 06/08/22 00:25 100-42-506/07/22 16:1218.2 2
1,1,1,2-Tetrachloroethane ND ug/kg 06/08/22 00:25 630-20-606/07/22 16:1218.2 2
1,1,2,2-Tetrachloroethane ND ug/kg 06/08/22 00:25 79-34-506/07/22 16:1218.2 2
Tetrachloroethene 12600 ug/kg 06/08/22 00:25 127-18-406/07/22 16:1218.2 2
Toluene ND ug/kg 06/08/22 00:25 108-88-306/07/22 16:1218.2 2
1,2,3-Trichlorobenzene ND ug/kg 06/08/22 00:25 87-61-606/07/22 16:1218.2 2
1,2,4-Trichlorobenzene ND ug/kg 06/08/22 00:25 120-82-106/07/22 16:1218.2 2
1,1,1-Trichloroethane ND ug/kg 06/08/22 00:25 71-55-606/07/22 16:1218.2 2
1,1,2-Trichloroethane ND ug/kg 06/08/22 00:25 79-00-506/07/22 16:1218.2 2
Trichloroethene 107 ug/kg 06/08/22 00:25 79-01-606/07/22 16:1218.2 2
Trichlorofluoromethane ND ug/kg 06/08/22 00:25 75-69-406/07/22 16:1218.2 2
1,2,3-Trichloropropane ND ug/kg 06/08/22 00:25 96-18-406/07/22 16:1218.2 2
1,2,4-Trimethylbenzene ND ug/kg 06/08/22 00:25 95-63-606/07/22 16:1218.2 2
1,3,5-Trimethylbenzene ND ug/kg 06/08/22 00:25 108-67-806/07/22 16:1218.2 2
Vinyl acetate ND ug/kg 06/08/22 00:25 108-05-406/07/22 16:121822
Vinyl chloride ND ug/kg 06/08/22 00:25 75-01-4 v106/07/22 16:1236.4 2
Xylene (Total)ND ug/kg 06/08/22 00:25 1330-20-706/07/22 16:1236.4 2
m&p-Xylene ND ug/kg 06/08/22 00:25 179601-23-106/07/22 16:1236.4 2
o-Xylene ND ug/kg 06/08/22 00:25 95-47-606/07/22 16:1218.2 2
Surrogates
Toluene-d8 (S)98 %06/08/22 00:25 2037-26-506/07/22 16:1270-130 2
4-Bromofluorobenzene (S)98 %06/08/22 00:25 460-00-406/07/22 16:1269-134 2
1,2-Dichloroethane-d4 (S)95 %06/08/22 00:25 17060-07-006/07/22 16:1270-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 31.0 %06/06/22 16:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-20 (8-12)Lab ID:92607493028 Collected:06/01/22 12:46 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/08/22 01:00 67-64-106/07/22 16:128234
Benzene ND ug/kg 06/08/22 01:00 71-43-206/07/22 16:1241.2 4
Bromobenzene ND ug/kg 06/08/22 01:00 108-86-106/07/22 16:1241.2 4
Bromochloromethane ND ug/kg 06/08/22 01:00 74-97-506/07/22 16:1241.2 4
Bromodichloromethane ND ug/kg 06/08/22 01:00 75-27-406/07/22 16:1241.2 4
Bromoform ND ug/kg 06/08/22 01:00 75-25-206/07/22 16:1241.2 4
Bromomethane ND ug/kg 06/08/22 01:00 74-83-9 IK06/07/22 16:1282.3 4
2-Butanone (MEK)ND ug/kg 06/08/22 01:00 78-93-306/07/22 16:128234
n-Butylbenzene ND ug/kg 06/08/22 01:00 104-51-806/07/22 16:1241.2 4
sec-Butylbenzene ND ug/kg 06/08/22 01:00 135-98-806/07/22 16:1241.2 4
tert-Butylbenzene ND ug/kg 06/08/22 01:00 98-06-606/07/22 16:1241.2 4
Carbon tetrachloride ND ug/kg 06/08/22 01:00 56-23-506/07/22 16:1241.2 4
Chlorobenzene ND ug/kg 06/08/22 01:00 108-90-706/07/22 16:1241.2 4
Chloroethane ND ug/kg 06/08/22 01:00 75-00-306/07/22 16:1282.3 4
Chloroform ND ug/kg 06/08/22 01:00 67-66-306/07/22 16:1241.2 4
Chloromethane ND ug/kg 06/08/22 01:00 74-87-306/07/22 16:1282.3 4
2-Chlorotoluene ND ug/kg 06/08/22 01:00 95-49-806/07/22 16:1241.2 4
4-Chlorotoluene ND ug/kg 06/08/22 01:00 106-43-406/07/22 16:1241.2 4
1,2-Dibromo-3-chloropropane ND ug/kg 06/08/22 01:00 96-12-806/07/22 16:1241.2 4
Dibromochloromethane ND ug/kg 06/08/22 01:00 124-48-106/07/22 16:1241.2 4
1,2-Dibromoethane (EDB)ND ug/kg 06/08/22 01:00 106-93-406/07/22 16:1241.2 4
Dibromomethane ND ug/kg 06/08/22 01:00 74-95-306/07/22 16:1241.2 4
1,2-Dichlorobenzene ND ug/kg 06/08/22 01:00 95-50-106/07/22 16:1241.2 4
1,3-Dichlorobenzene ND ug/kg 06/08/22 01:00 541-73-106/07/22 16:1241.2 4
1,4-Dichlorobenzene ND ug/kg 06/08/22 01:00 106-46-706/07/22 16:1241.2 4
Dichlorodifluoromethane ND ug/kg 06/08/22 01:00 75-71-8 L1,v106/07/22 16:1282.3 4
1,1-Dichloroethane ND ug/kg 06/08/22 01:00 75-34-306/07/22 16:1241.2 4
1,2-Dichloroethane ND ug/kg 06/08/22 01:00 107-06-206/07/22 16:1241.2 4
1,1-Dichloroethene ND ug/kg 06/08/22 01:00 75-35-406/07/22 16:1241.2 4
cis-1,2-Dichloroethene 662 ug/kg 06/08/22 01:00 156-59-206/07/22 16:1241.2 4
trans-1,2-Dichloroethene ND ug/kg 06/08/22 01:00 156-60-506/07/22 16:1241.2 4
1,2-Dichloropropane ND ug/kg 06/08/22 01:00 78-87-506/07/22 16:1241.2 4
1,3-Dichloropropane ND ug/kg 06/08/22 01:00 142-28-906/07/22 16:1241.2 4
2,2-Dichloropropane ND ug/kg 06/08/22 01:00 594-20-706/07/22 16:1241.2 4
1,1-Dichloropropene ND ug/kg 06/08/22 01:00 563-58-606/07/22 16:1241.2 4
cis-1,3-Dichloropropene ND ug/kg 06/08/22 01:00 10061-01-506/07/22 16:1241.2 4
trans-1,3-Dichloropropene ND ug/kg 06/08/22 01:00 10061-02-606/07/22 16:1241.2 4
Diisopropyl ether ND ug/kg 06/08/22 01:00 108-20-306/07/22 16:1241.2 4
Ethylbenzene ND ug/kg 06/08/22 01:00 100-41-406/07/22 16:1241.2 4
Hexachloro-1,3-butadiene ND ug/kg 06/08/22 01:00 87-68-306/07/22 16:1282.3 4
2-Hexanone ND ug/kg 06/08/22 01:00 591-78-606/07/22 16:124124
Isopropylbenzene (Cumene)ND ug/kg 06/08/22 01:00 98-82-806/07/22 16:1241.2 4
p-Isopropyltoluene ND ug/kg 06/08/22 01:00 99-87-606/07/22 16:1241.2 4
Methylene Chloride 4460 ug/kg 06/08/22 01:00 75-09-2 C906/07/22 16:121654
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/08/22 01:00 108-10-106/07/22 16:124124
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-20 (8-12)Lab ID:92607493028 Collected:06/01/22 12:46 Received:06/02/22 08:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 06/08/22 01:00 1634-04-406/07/22 16:1241.2 4
Naphthalene ND ug/kg 06/08/22 01:00 91-20-306/07/22 16:1241.2 4
n-Propylbenzene ND ug/kg 06/08/22 01:00 103-65-106/07/22 16:1241.2 4
Styrene ND ug/kg 06/08/22 01:00 100-42-506/07/22 16:1241.2 4
1,1,1,2-Tetrachloroethane ND ug/kg 06/08/22 01:00 630-20-606/07/22 16:1241.2 4
1,1,2,2-Tetrachloroethane ND ug/kg 06/08/22 01:00 79-34-506/07/22 16:1241.2 4
Tetrachloroethene 19300 ug/kg 06/08/22 01:00 127-18-406/07/22 16:1241.2 4
Toluene ND ug/kg 06/08/22 01:00 108-88-306/07/22 16:1241.2 4
1,2,3-Trichlorobenzene ND ug/kg 06/08/22 01:00 87-61-606/07/22 16:1241.2 4
1,2,4-Trichlorobenzene ND ug/kg 06/08/22 01:00 120-82-106/07/22 16:1241.2 4
1,1,1-Trichloroethane ND ug/kg 06/08/22 01:00 71-55-606/07/22 16:1241.2 4
1,1,2-Trichloroethane ND ug/kg 06/08/22 01:00 79-00-506/07/22 16:1241.2 4
Trichloroethene 174 ug/kg 06/08/22 01:00 79-01-606/07/22 16:1241.2 4
Trichlorofluoromethane ND ug/kg 06/08/22 01:00 75-69-406/07/22 16:1241.2 4
1,2,3-Trichloropropane ND ug/kg 06/08/22 01:00 96-18-406/07/22 16:1241.2 4
1,2,4-Trimethylbenzene ND ug/kg 06/08/22 01:00 95-63-606/07/22 16:1241.2 4
1,3,5-Trimethylbenzene ND ug/kg 06/08/22 01:00 108-67-806/07/22 16:1241.2 4
Vinyl acetate ND ug/kg 06/08/22 01:00 108-05-406/07/22 16:124124
Vinyl chloride ND ug/kg 06/08/22 01:00 75-01-4 v106/07/22 16:1282.3 4
Xylene (Total)ND ug/kg 06/08/22 01:00 1330-20-706/07/22 16:1282.3 4
m&p-Xylene ND ug/kg 06/08/22 01:00 179601-23-106/07/22 16:1282.3 4
o-Xylene ND ug/kg 06/08/22 01:00 95-47-606/07/22 16:1241.2 4
Surrogates
Toluene-d8 (S)98 %06/08/22 01:00 2037-26-506/07/22 16:1270-130 4
4-Bromofluorobenzene (S)99 %06/08/22 01:00 460-00-406/07/22 16:1269-134 4
1,2-Dichloroethane-d4 (S)95 %06/08/22 01:00 17060-07-006/07/22 16:1270-130 4
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 36.3 %06/06/22 16:17 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-3 Lab ID:92607493029 Collected:06/01/22 10:35 Received:06/02/22 08:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/06/22 22:59 67-64-1250001000
Benzene ND ug/L 06/06/22 22:59 71-43-210001000
Bromobenzene ND ug/L 06/06/22 22:59 108-86-110001000
Bromochloromethane ND ug/L 06/06/22 22:59 74-97-510001000
Bromodichloromethane ND ug/L 06/06/22 22:59 75-27-410001000
Bromoform ND ug/L 06/06/22 22:59 75-25-2 IK10001000
Bromomethane ND ug/L 06/06/22 22:59 74-83-9 v220001000
2-Butanone (MEK)ND ug/L 06/06/22 22:59 78-93-350001000
Carbon tetrachloride ND ug/L 06/06/22 22:59 56-23-510001000
Chlorobenzene ND ug/L 06/06/22 22:59 108-90-710001000
Chloroethane ND ug/L 06/06/22 22:59 75-00-310001000
Chloroform ND ug/L 06/06/22 22:59 67-66-310001000
Chloromethane ND ug/L 06/06/22 22:59 74-87-310001000
2-Chlorotoluene ND ug/L 06/06/22 22:59 95-49-810001000
4-Chlorotoluene ND ug/L 06/06/22 22:59 106-43-410001000
1,2-Dibromo-3-chloropropane ND ug/L 06/06/22 22:59 96-12-820001000
Dibromochloromethane ND ug/L 06/06/22 22:59 124-48-110001000
1,2-Dibromoethane (EDB)ND ug/L 06/06/22 22:59 106-93-410001000
Dibromomethane ND ug/L 06/06/22 22:59 74-95-310001000
1,2-Dichlorobenzene ND ug/L 06/06/22 22:59 95-50-110001000
1,3-Dichlorobenzene ND ug/L 06/06/22 22:59 541-73-110001000
1,4-Dichlorobenzene ND ug/L 06/06/22 22:59 106-46-710001000
Dichlorodifluoromethane ND ug/L 06/06/22 22:59 75-71-810001000
1,1-Dichloroethane ND ug/L 06/06/22 22:59 75-34-310001000
1,2-Dichloroethane ND ug/L 06/06/22 22:59 107-06-210001000
1,1-Dichloroethene ND ug/L 06/06/22 22:59 75-35-410001000
cis-1,2-Dichloroethene 7690 ug/L 06/06/22 22:59 156-59-210001000
trans-1,2-Dichloroethene ND ug/L 06/06/22 22:59 156-60-510001000
1,2-Dichloropropane ND ug/L 06/06/22 22:59 78-87-510001000
1,3-Dichloropropane ND ug/L 06/06/22 22:59 142-28-910001000
2,2-Dichloropropane ND ug/L 06/06/22 22:59 594-20-710001000
1,1-Dichloropropene ND ug/L 06/06/22 22:59 563-58-610001000
cis-1,3-Dichloropropene ND ug/L 06/06/22 22:59 10061-01-510001000
trans-1,3-Dichloropropene ND ug/L 06/06/22 22:59 10061-02-610001000
Diisopropyl ether ND ug/L 06/06/22 22:59 108-20-310001000
Ethylbenzene ND ug/L 06/06/22 22:59 100-41-410001000
Hexachloro-1,3-butadiene ND ug/L 06/06/22 22:59 87-68-3 v220001000
2-Hexanone ND ug/L 06/06/22 22:59 591-78-650001000
p-Isopropyltoluene ND ug/L 06/06/22 22:59 99-87-610001000
Methylene Chloride ND ug/L 06/06/22 22:59 75-09-250001000
4-Methyl-2-pentanone (MIBK)ND ug/L 06/06/22 22:59 108-10-150001000
Methyl-tert-butyl ether ND ug/L 06/06/22 22:59 1634-04-410001000
Naphthalene ND ug/L 06/06/22 22:59 91-20-310001000
Styrene ND ug/L 06/06/22 22:59 100-42-510001000
1,1,1,2-Tetrachloroethane ND ug/L 06/06/22 22:59 630-20-610001000
1,1,2,2-Tetrachloroethane ND ug/L 06/06/22 22:59 79-34-510001000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 135
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92607493
BENMAR 897-05
Sample:GP-3 Lab ID:92607493029 Collected:06/01/22 10:35 Received:06/02/22 08:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene 124000 ug/L 06/06/22 22:59 127-18-410001000
Toluene ND ug/L 06/06/22 22:59 108-88-310001000
1,2,3-Trichlorobenzene ND ug/L 06/06/22 22:59 87-61-610001000
1,2,4-Trichlorobenzene ND ug/L 06/06/22 22:59 120-82-110001000
1,1,1-Trichloroethane ND ug/L 06/06/22 22:59 71-55-610001000
1,1,2-Trichloroethane ND ug/L 06/06/22 22:59 79-00-510001000
Trichloroethene 4490 ug/L 06/06/22 22:59 79-01-610001000
Trichlorofluoromethane ND ug/L 06/06/22 22:59 75-69-410001000
1,2,3-Trichloropropane ND ug/L 06/06/22 22:59 96-18-410001000
Vinyl acetate ND ug/L 06/06/22 22:59 108-05-420001000
Vinyl chloride ND ug/L 06/06/22 22:59 75-01-410001000
Xylene (Total)ND ug/L 06/06/22 22:59 1330-20-710001000
m&p-Xylene ND ug/L 06/06/22 22:59 179601-23-120001000
o-Xylene ND ug/L 06/06/22 22:59 95-47-610001000
Surrogates
4-Bromofluorobenzene (S)96 %06/06/22 22:59 460-00-470-130 1000
1,2-Dichloroethane-d4 (S)103 %06/06/22 22:59 17060-07-070-130 1000
Toluene-d8 (S)97 %06/06/22 22:59 2037-26-570-130 1000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702038
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493015, 92607493016, 92607493017, 92607493018, 92607493019, 92607493020, 92607493021,
92607493022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664140
Associated Lab Samples:92607493015, 92607493016, 92607493017, 92607493018, 92607493019, 92607493020, 92607493021,
92607493022
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/03/22 18:52
1,1,1-Trichloroethane ug/kg ND 5.0 06/03/22 18:52
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/03/22 18:52
1,1,2-Trichloroethane ug/kg ND 5.0 06/03/22 18:52
1,1-Dichloroethane ug/kg ND 5.0 06/03/22 18:52
1,1-Dichloroethene ug/kg ND 5.0 06/03/22 18:52
1,1-Dichloropropene ug/kg ND 5.0 06/03/22 18:52
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/03/22 18:52
1,2,3-Trichloropropane ug/kg ND 5.0 06/03/22 18:52
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/03/22 18:52
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/03/22 18:52
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/03/22 18:52
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/03/22 18:52
1,2-Dichlorobenzene ug/kg ND 5.0 06/03/22 18:52
1,2-Dichloroethane ug/kg ND 5.0 06/03/22 18:52
1,2-Dichloropropane ug/kg ND 5.0 06/03/22 18:52
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/03/22 18:52
1,3-Dichlorobenzene ug/kg ND 5.0 06/03/22 18:52
1,3-Dichloropropane ug/kg ND 5.0 06/03/22 18:52
1,4-Dichlorobenzene ug/kg ND 5.0 06/03/22 18:52
2,2-Dichloropropane ug/kg ND 5.0 06/03/22 18:52
2-Butanone (MEK)ug/kg ND 100 06/03/22 18:52
2-Chlorotoluene ug/kg ND 5.0 06/03/22 18:52
2-Hexanone ug/kg ND 50.0 06/03/22 18:52
4-Chlorotoluene ug/kg ND 5.0 06/03/22 18:52
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/03/22 18:52
Acetone ug/kg ND 100 06/03/22 18:52
Benzene ug/kg ND 5.0 06/03/22 18:52
Bromobenzene ug/kg ND 5.0 06/03/22 18:52
Bromochloromethane ug/kg ND 5.0 06/03/22 18:52
Bromodichloromethane ug/kg ND 5.0 06/03/22 18:52
Bromoform ug/kg ND 5.0 06/03/22 18:52
Bromomethane ug/kg ND 10.0 IK06/03/22 18:52
Carbon tetrachloride ug/kg ND 5.0 06/03/22 18:52
Chlorobenzene ug/kg ND 5.0 06/03/22 18:52
Chloroethane ug/kg ND 10.0 06/03/22 18:52
Chloroform ug/kg ND 5.0 06/03/22 18:52
Chloromethane ug/kg ND 10.0 06/03/22 18:52
cis-1,2-Dichloroethene ug/kg ND 5.0 06/03/22 18:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664140
Associated Lab Samples:92607493015, 92607493016, 92607493017, 92607493018, 92607493019, 92607493020, 92607493021,
92607493022
Matrix:Solid
Analyzed
cis-1,3-Dichloropropene ug/kg ND 5.0 06/03/22 18:52
Dibromochloromethane ug/kg ND 5.0 06/03/22 18:52
Dibromomethane ug/kg ND 5.0 06/03/22 18:52
Dichlorodifluoromethane ug/kg ND 10.0 v106/03/22 18:52
Diisopropyl ether ug/kg ND 5.0 06/03/22 18:52
Ethylbenzene ug/kg ND 5.0 06/03/22 18:52
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/03/22 18:52
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/03/22 18:52
m&p-Xylene ug/kg ND 10.0 06/03/22 18:52
Methyl-tert-butyl ether ug/kg ND 5.0 06/03/22 18:52
Methylene Chloride ug/kg ND 20.0 06/03/22 18:52
n-Butylbenzene ug/kg ND 5.0 06/03/22 18:52
n-Propylbenzene ug/kg ND 5.0 06/03/22 18:52
Naphthalene ug/kg ND 5.0 06/03/22 18:52
o-Xylene ug/kg ND 5.0 06/03/22 18:52
p-Isopropyltoluene ug/kg ND 5.0 06/03/22 18:52
sec-Butylbenzene ug/kg ND 5.0 06/03/22 18:52
Styrene ug/kg ND 5.0 06/03/22 18:52
tert-Butylbenzene ug/kg ND 5.0 06/03/22 18:52
Tetrachloroethene ug/kg ND 5.0 06/03/22 18:52
Toluene ug/kg ND 5.0 06/03/22 18:52
trans-1,2-Dichloroethene ug/kg ND 5.0 06/03/22 18:52
trans-1,3-Dichloropropene ug/kg ND 5.0 06/03/22 18:52
Trichloroethene ug/kg ND 5.0 06/03/22 18:52
Trichlorofluoromethane ug/kg ND 5.0 06/03/22 18:52
Vinyl acetate ug/kg ND 50.0 06/03/22 18:52
Vinyl chloride ug/kg ND 10.0 v106/03/22 18:52
Xylene (Total)ug/kg ND 10.0 06/03/22 18:52
1,2-Dichloroethane-d4 (S)%106 70-130 06/03/22 18:52
4-Bromofluorobenzene (S)%97 69-134 06/03/22 18:52
Toluene-d8 (S)%100 70-130 06/03/22 18:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664141LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 13501250 108 70-130
1,1,1-Trichloroethane ug/kg 12701250 102 70-130
1,1,2,2-Tetrachloroethane ug/kg 12801250 103 70-130
1,1,2-Trichloroethane ug/kg 13401250 107 70-130
1,1-Dichloroethane ug/kg 12301250 98 70-130
1,1-Dichloroethene ug/kg 13301250 106 70-130
1,1-Dichloropropene ug/kg 13501250 108 70-130
1,2,3-Trichlorobenzene ug/kg 13701250 110 65-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664141LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,3-Trichloropropane ug/kg 12201250 98 70-130
1,2,4-Trichlorobenzene ug/kg 13201250 105 68-130
1,2,4-Trimethylbenzene ug/kg 13901250 111 70-130
1,2-Dibromo-3-chloropropane ug/kg 11801250 95 70-130
1,2-Dibromoethane (EDB)ug/kg 12901250 103 70-130
1,2-Dichlorobenzene ug/kg 12901250 103 70-130
1,2-Dichloroethane ug/kg 11701250 94 63-130
1,2-Dichloropropane ug/kg 13301250 106 70-130
1,3,5-Trimethylbenzene ug/kg 13501250 108 70-130
1,3-Dichlorobenzene ug/kg 12801250 103 70-130
1,3-Dichloropropane ug/kg 12901250 103 70-130
1,4-Dichlorobenzene ug/kg 12201250 98 70-130
2,2-Dichloropropane ug/kg 12201250 98 66-130
2-Butanone (MEK)ug/kg 23802500 95 70-130
2-Chlorotoluene ug/kg 13201250 105 70-130
2-Hexanone ug/kg 26402500 105 70-130
4-Chlorotoluene ug/kg 12901250 103 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 26802500 107 70-130
Acetone ug/kg 22402500 89 69-130
Benzene ug/kg 12501250 100 70-130
Bromobenzene ug/kg 13301250 106 70-130
Bromochloromethane ug/kg 12101250 97 70-130
Bromodichloromethane ug/kg 11701250 93 69-130
Bromoform ug/kg 14501250 116 70-130
Bromomethane ug/kg 1330 IK125010752-130
Carbon tetrachloride ug/kg 14201250 114 70-130
Chlorobenzene ug/kg 13101250 105 70-130
Chloroethane ug/kg 14101250 113 65-130
Chloroform ug/kg 12001250 96 70-130
Chloromethane ug/kg 14801250 119 55-130
cis-1,2-Dichloroethene ug/kg 12801250 102 70-130
cis-1,3-Dichloropropene ug/kg 13601250 109 70-130
Dibromochloromethane ug/kg 13401250 107 70-130
Dibromomethane ug/kg 13401250 107 70-130
Dichlorodifluoromethane ug/kg 1930 v1125015545-156
Diisopropyl ether ug/kg 13001250 104 70-130
Ethylbenzene ug/kg 12401250 99 70-130
Hexachloro-1,3-butadiene ug/kg 13801250 110 66-130
Isopropylbenzene (Cumene)ug/kg 13701250 110 70-130
m&p-Xylene ug/kg 27202500 109 70-130
Methyl-tert-butyl ether ug/kg 11601250 93 70-130
Methylene Chloride ug/kg 12001250 96 65-130
n-Butylbenzene ug/kg 13701250 109 67-130
n-Propylbenzene ug/kg 12701250 102 70-130
Naphthalene ug/kg 12701250 102 70-130
o-Xylene ug/kg 14401250 115 70-130
p-Isopropyltoluene ug/kg 13801250 110 67-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664141LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene ug/kg 13701250 109 69-130
Styrene ug/kg 14901250 120 70-130
tert-Butylbenzene ug/kg 12901250 103 67-130
Tetrachloroethene ug/kg 13601250 109 70-130
Toluene ug/kg 12501250 100 70-130
trans-1,2-Dichloroethene ug/kg 13101250 105 70-130
trans-1,3-Dichloropropene ug/kg 13501250 108 68-130
Trichloroethene ug/kg 13901250 111 70-130
Trichlorofluoromethane ug/kg 14001250 112 70-130
Vinyl acetate ug/kg 26602500 107 70-130
Vinyl chloride ug/kg 1540 v1125012361-130
Xylene (Total)ug/kg 41703750 111 70-130
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%104 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3664143MATRIX SPIKE SAMPLE:
MSSpike
Result
92607493016
1,1,1,2-Tetrachloroethane ug/kg 1070911 118 70-131ND
1,1,1-Trichloroethane ug/kg 1080911 118 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 987911 108 66-130ND
1,1,2-Trichloroethane ug/kg 964911 106 66-133ND
1,1-Dichloroethane ug/kg 973911 107 65-130ND
1,1-Dichloroethene ug/kg 1060911 116 10-158ND
1,1-Dichloropropene ug/kg 1120911 123 68-133ND
1,2,3-Trichlorobenzene ug/kg 1100911 121 27-138ND
1,2,3-Trichloropropane ug/kg 905911 99 67-130ND
1,2,4-Trichlorobenzene ug/kg 1060911 117 51-134ND
1,2,4-Trimethylbenzene ug/kg 1080911 118 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 863911 95 32-130ND
1,2-Dibromoethane (EDB)ug/kg 987911 108 70-130ND
1,2-Dichlorobenzene ug/kg 1060911 116 69-130ND
1,2-Dichloroethane ug/kg 950911 104 59-130ND
1,2-Dichloropropane ug/kg 1060911 117 70-130ND
1,3,5-Trimethylbenzene ug/kg 1080911 119 65-137ND
1,3-Dichlorobenzene ug/kg 1050911 116 70-130ND
1,3-Dichloropropane ug/kg 1010911 111 70-130ND
1,4-Dichlorobenzene ug/kg 976911 107 68-130ND
2,2-Dichloropropane ug/kg 793911 87 32-130ND
2-Butanone (MEK)ug/kg 15301830 84 10-136ND
2-Chlorotoluene ug/kg 1050911 115 69-141ND
2-Hexanone ug/kg 18301830 100 10-144ND
4-Chlorotoluene ug/kg 1010911 110 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 18301830 100 25-143ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3664143MATRIX SPIKE SAMPLE:
MSSpike
Result
92607493016
Acetone ug/kg 12301830 68 10-130ND
Benzene ug/kg 1040911 115 67-130ND
Bromobenzene ug/kg 1020911 112 70-130ND
Bromochloromethane ug/kg 897911 99 69-134ND
Bromodichloromethane ug/kg 887911 97 64-130ND
Bromoform ug/kg 1050911 115 62-130ND
Bromomethane ug/kg 597 IK9116520-176ND
Carbon tetrachloride ug/kg 1170911 128 65-140ND
Chlorobenzene ug/kg 1070911 116 70-130ND
Chloroethane ug/kg 302911 33 10-130ND
Chloroform ug/kg 859911 94 63-130ND
Chloromethane ug/kg 1270 M191113958-130ND
cis-1,2-Dichloroethene ug/kg 1090911 114 66-13053.3
cis-1,3-Dichloropropene ug/kg 974911 107 67-130ND
Dibromochloromethane ug/kg 975911 107 67-130ND
Dibromomethane ug/kg 997911 109 63-131ND
Dichlorodifluoromethane ug/kg 1540 v191116944-180ND
Diisopropyl ether ug/kg 1020911 112 63-130ND
Ethylbenzene ug/kg 1020911 112 66-130ND
Hexachloro-1,3-butadiene ug/kg 1150911 127 64-150ND
Isopropylbenzene (Cumene)ug/kg 1100911 121 69-135ND
m&p-Xylene ug/kg 22001830 120 60-133ND
Methyl-tert-butyl ether ug/kg 866911 95 65-130ND
Methylene Chloride ug/kg 892911 98 61-130ND
n-Butylbenzene ug/kg 1090911 119 65-140ND
n-Propylbenzene ug/kg 1040911 114 67-140ND
Naphthalene ug/kg 976911 107 15-145ND
o-Xylene ug/kg 1140911 125 66-133ND
p-Isopropyltoluene ug/kg 1110911 122 56-147ND
sec-Butylbenzene ug/kg 1130911 124 65-139ND
Styrene ug/kg 1120911 123 70-132ND
tert-Butylbenzene ug/kg 1030911 113 62-135ND
Tetrachloroethene ug/kg 5320 M19115270-1354850
Toluene ug/kg 1000911 109 67-130ND
trans-1,2-Dichloroethene ug/kg 1040911 115 69-130ND
trans-1,3-Dichloropropene ug/kg 949911 104 62-130ND
Trichloroethene ug/kg 2660 M191114670-1351330
Trichlorofluoromethane ug/kg 438911 48 10-130ND
Vinyl acetate ug/kg 17201830 94 53-130ND
Vinyl chloride ug/kg 1170 v191112861-148ND
Xylene (Total)ug/kg 33402730 122 63-132ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92607493015
3664142SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IKND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg 6.4JND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg 932 5976
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg ND v1ND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92607493015
3664142SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg 4940 35100
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg 32.0 131.7
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg 145 3149
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg ND v1ND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%104104
4-Bromofluorobenzene (S)%9899
Toluene-d8 (S)%100102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702238
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493006, 92607493008, 92607493010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664946
Associated Lab Samples:92607493006, 92607493008, 92607493010
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/04/22 19:27
1,1,1-Trichloroethane ug/kg ND 5.0 06/04/22 19:27
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/04/22 19:27
1,1,2-Trichloroethane ug/kg ND 5.0 06/04/22 19:27
1,1-Dichloroethane ug/kg ND 5.0 06/04/22 19:27
1,1-Dichloroethene ug/kg ND 5.0 06/04/22 19:27
1,1-Dichloropropene ug/kg ND 5.0 06/04/22 19:27
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/04/22 19:27
1,2,3-Trichloropropane ug/kg ND 5.0 06/04/22 19:27
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/04/22 19:27
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/04/22 19:27
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/04/22 19:27
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/04/22 19:27
1,2-Dichlorobenzene ug/kg ND 5.0 06/04/22 19:27
1,2-Dichloroethane ug/kg ND 5.0 06/04/22 19:27
1,2-Dichloropropane ug/kg ND 5.0 06/04/22 19:27
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/04/22 19:27
1,3-Dichlorobenzene ug/kg ND 5.0 06/04/22 19:27
1,3-Dichloropropane ug/kg ND 5.0 06/04/22 19:27
1,4-Dichlorobenzene ug/kg ND 5.0 06/04/22 19:27
2,2-Dichloropropane ug/kg ND 5.0 06/04/22 19:27
2-Butanone (MEK)ug/kg ND 100 06/04/22 19:27
2-Chlorotoluene ug/kg ND 5.0 06/04/22 19:27
2-Hexanone ug/kg ND 50.0 06/04/22 19:27
4-Chlorotoluene ug/kg ND 5.0 06/04/22 19:27
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/04/22 19:27
Acetone ug/kg ND 100 06/04/22 19:27
Benzene ug/kg ND 5.0 06/04/22 19:27
Bromobenzene ug/kg ND 5.0 06/04/22 19:27
Bromochloromethane ug/kg ND 5.0 06/04/22 19:27
Bromodichloromethane ug/kg ND 5.0 06/04/22 19:27
Bromoform ug/kg ND 5.0 v106/04/22 19:27
Bromomethane ug/kg ND 10.0 IK06/04/22 19:27
Carbon tetrachloride ug/kg ND 5.0 06/04/22 19:27
Chlorobenzene ug/kg ND 5.0 06/04/22 19:27
Chloroethane ug/kg ND 10.0 v106/04/22 19:27
Chloroform ug/kg ND 5.0 06/04/22 19:27
Chloromethane ug/kg ND 10.0 v106/04/22 19:27
cis-1,2-Dichloroethene ug/kg ND 5.0 06/04/22 19:27
cis-1,3-Dichloropropene ug/kg ND 5.0 06/04/22 19:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3664946
Associated Lab Samples:92607493006, 92607493008, 92607493010
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/04/22 19:27
Dibromomethane ug/kg ND 5.0 06/04/22 19:27
Dichlorodifluoromethane ug/kg ND 10.0 v106/04/22 19:27
Diisopropyl ether ug/kg ND 5.0 06/04/22 19:27
Ethylbenzene ug/kg ND 5.0 06/04/22 19:27
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/04/22 19:27
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/04/22 19:27
m&p-Xylene ug/kg ND 10.0 06/04/22 19:27
Methyl-tert-butyl ether ug/kg ND 5.0 06/04/22 19:27
Methylene Chloride ug/kg ND 20.0 06/04/22 19:27
n-Butylbenzene ug/kg ND 5.0 06/04/22 19:27
n-Propylbenzene ug/kg ND 5.0 06/04/22 19:27
Naphthalene ug/kg ND 5.0 06/04/22 19:27
o-Xylene ug/kg ND 5.0 06/04/22 19:27
p-Isopropyltoluene ug/kg ND 5.0 06/04/22 19:27
sec-Butylbenzene ug/kg ND 5.0 06/04/22 19:27
Styrene ug/kg ND 5.0 v106/04/22 19:27
tert-Butylbenzene ug/kg ND 5.0 06/04/22 19:27
Tetrachloroethene ug/kg ND 5.0 06/04/22 19:27
Toluene ug/kg ND 5.0 06/04/22 19:27
trans-1,2-Dichloroethene ug/kg ND 5.0 06/04/22 19:27
trans-1,3-Dichloropropene ug/kg ND 5.0 06/04/22 19:27
Trichloroethene ug/kg ND 5.0 06/04/22 19:27
Trichlorofluoromethane ug/kg ND 5.0 06/04/22 19:27
Vinyl acetate ug/kg ND 50.0 06/04/22 19:27
Vinyl chloride ug/kg ND 10.0 v106/04/22 19:27
Xylene (Total)ug/kg ND 10.0 06/04/22 19:27
1,2-Dichloroethane-d4 (S)%106 70-130 06/04/22 19:27
4-Bromofluorobenzene (S)%96 69-134 06/04/22 19:27
Toluene-d8 (S)%99 70-130 06/04/22 19:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664947LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 13601250 109 70-130
1,1,1-Trichloroethane ug/kg 13301250 106 70-130
1,1,2,2-Tetrachloroethane ug/kg 13601250 108 70-130
1,1,2-Trichloroethane ug/kg 13901250 111 70-130
1,1-Dichloroethane ug/kg 13101250 105 70-130
1,1-Dichloroethene ug/kg 14501250 116 70-130
1,1-Dichloropropene ug/kg 14401250 115 70-130
1,2,3-Trichlorobenzene ug/kg 14701250 117 65-130
1,2,3-Trichloropropane ug/kg 12801250 102 70-130
1,2,4-Trichlorobenzene ug/kg 13901250 111 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664947LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 14201250 113 70-130
1,2-Dibromo-3-chloropropane ug/kg 13601250 109 70-130
1,2-Dibromoethane (EDB)ug/kg 13401250 108 70-130
1,2-Dichlorobenzene ug/kg 13701250 110 70-130
1,2-Dichloroethane ug/kg 12701250 102 63-130
1,2-Dichloropropane ug/kg 14101250 112 70-130
1,3,5-Trimethylbenzene ug/kg 14301250 115 70-130
1,3-Dichlorobenzene ug/kg 13401250 107 70-130
1,3-Dichloropropane ug/kg 13501250 108 70-130
1,4-Dichlorobenzene ug/kg 13001250 104 70-130
2,2-Dichloropropane ug/kg 12101250 97 66-130
2-Butanone (MEK)ug/kg 27102500 108 70-130
2-Chlorotoluene ug/kg 13801250 110 70-130
2-Hexanone ug/kg 29402500 118 70-130
4-Chlorotoluene ug/kg 13501250 108 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 29802500 119 70-130
Acetone ug/kg 26402500 105 69-130
Benzene ug/kg 13101250 105 70-130
Bromobenzene ug/kg 14001250 112 70-130
Bromochloromethane ug/kg 12801250 102 70-130
Bromodichloromethane ug/kg 12401250 100 69-130
Bromoform ug/kg 1500 v1125012070-130
Bromomethane ug/kg 1390 IK125011252-130
Carbon tetrachloride ug/kg 14401250 116 70-130
Chlorobenzene ug/kg 13501250 108 70-130
Chloroethane ug/kg 1510 v1125012165-130
Chloroform ug/kg 12901250 103 70-130
Chloromethane ug/kg 1580 v1125012655-130
cis-1,2-Dichloroethene ug/kg 13801250 110 70-130
cis-1,3-Dichloropropene ug/kg 14201250 113 70-130
Dibromochloromethane ug/kg 13701250 110 70-130
Dibromomethane ug/kg 14001250 112 70-130
Dichlorodifluoromethane ug/kg 2020 L1,v1125016245-156
Diisopropyl ether ug/kg 14201250 114 70-130
Ethylbenzene ug/kg 12701250 102 70-130
Hexachloro-1,3-butadiene ug/kg 14101250 113 66-130
Isopropylbenzene (Cumene)ug/kg 13901250 111 70-130
m&p-Xylene ug/kg 27402500 110 70-130
Methyl-tert-butyl ether ug/kg 12601250 100 70-130
Methylene Chloride ug/kg 12901250 103 65-130
n-Butylbenzene ug/kg 14501250 116 67-130
n-Propylbenzene ug/kg 13801250 110 70-130
Naphthalene ug/kg 14501250 116 70-130
o-Xylene ug/kg 14601250 117 70-130
p-Isopropyltoluene ug/kg 14701250 118 67-130
sec-Butylbenzene ug/kg 14301250 115 69-130
Styrene ug/kg 1520 v1125012270-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3664947LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 14101250 112 67-130
Tetrachloroethene ug/kg 13801250 110 70-130
Toluene ug/kg 13001250 104 70-130
trans-1,2-Dichloroethene ug/kg 14001250 112 70-130
trans-1,3-Dichloropropene ug/kg 14101250 113 68-130
Trichloroethene ug/kg 14401250 115 70-130
Trichlorofluoromethane ug/kg 14701250 118 70-130
Vinyl acetate ug/kg 28902500 116 70-130
Vinyl chloride ug/kg 1650 L1,v1125013261-130
Xylene (Total)ug/kg 42003750 112 70-130
1,2-Dichloroethane-d4 (S)%84 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3664949MATRIX SPIKE SAMPLE:
MSSpike
Result
92607493008
1,1,1,2-Tetrachloroethane ug/kg 852784 109 70-131ND
1,1,1-Trichloroethane ug/kg 846784 108 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 815784 104 66-130ND
1,1,2-Trichloroethane ug/kg 792784 101 66-133ND
1,1-Dichloroethane ug/kg 775784 99 65-130ND
1,1-Dichloroethene ug/kg 842784 107 10-158ND
1,1-Dichloropropene ug/kg 887784 113 68-133ND
1,2,3-Trichlorobenzene ug/kg 917784 117 27-138ND
1,2,3-Trichloropropane ug/kg 740784 94 67-130ND
1,2,4-Trichlorobenzene ug/kg 867784 111 51-134ND
1,2,4-Trimethylbenzene ug/kg 843784 108 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 735784 94 32-130ND
1,2-Dibromoethane (EDB)ug/kg 814784 104 70-130ND
1,2-Dichlorobenzene ug/kg 814784 104 69-130ND
1,2-Dichloroethane ug/kg 751784 96 59-130ND
1,2-Dichloropropane ug/kg 853784 109 70-130ND
1,3,5-Trimethylbenzene ug/kg 832784 106 65-137ND
1,3-Dichlorobenzene ug/kg 803784 102 70-130ND
1,3-Dichloropropane ug/kg 825784 105 70-130ND
1,4-Dichlorobenzene ug/kg 767784 98 68-130ND
2,2-Dichloropropane ug/kg 630784 80 32-130ND
2-Butanone (MEK)ug/kg 14201570 91 10-136ND
2-Chlorotoluene ug/kg 809784 103 69-141ND
2-Hexanone ug/kg 15901570 101 10-144ND
4-Chlorotoluene ug/kg 795784 101 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 15501570 99 25-143ND
Acetone ug/kg 12301570 78 10-130ND
Benzene ug/kg 811784 103 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3664949MATRIX SPIKE SAMPLE:
MSSpike
Result
92607493008
Bromobenzene ug/kg 796784 102 70-130ND
Bromochloromethane ug/kg 720784 92 69-134ND
Bromodichloromethane ug/kg 718784 92 64-130ND
Bromoform ug/kg 828784 106 62-130ND
Bromomethane ug/kg 514 IK7846620-176ND
Carbon tetrachloride ug/kg 917784 117 65-140ND
Chlorobenzene ug/kg 837784 106 70-130ND
Chloroethane ug/kg 304784 39 10-130ND
Chloroform ug/kg 675784 86 63-130ND
Chloromethane ug/kg 997784 127 58-130ND
cis-1,2-Dichloroethene ug/kg 835784 103 66-13023.6
cis-1,3-Dichloropropene ug/kg 780784 99 67-130ND
Dibromochloromethane ug/kg 802784 102 67-130ND
Dibromomethane ug/kg 792784 101 63-131ND
Dichlorodifluoromethane ug/kg 1280 v178416344-180ND
Diisopropyl ether ug/kg 818784 104 63-130ND
Ethylbenzene ug/kg 812784 104 66-130ND
Hexachloro-1,3-butadiene ug/kg 955784 122 64-150ND
Isopropylbenzene (Cumene)ug/kg 862784 110 69-135ND
m&p-Xylene ug/kg 17301570 110 60-133ND
Methyl-tert-butyl ether ug/kg 688784 88 65-130ND
Methylene Chloride ug/kg 684784 87 61-130ND
n-Butylbenzene ug/kg 868784 111 65-140ND
n-Propylbenzene ug/kg 802784 102 67-140ND
Naphthalene ug/kg 825784 105 15-145ND
o-Xylene ug/kg 896784 114 66-133ND
p-Isopropyltoluene ug/kg 865784 110 56-147ND
sec-Butylbenzene ug/kg 871784 111 65-139ND
Styrene ug/kg 898784 115 70-132ND
tert-Butylbenzene ug/kg 777784 99 62-135ND
Tetrachloroethene ug/kg 6570 M178413970-1355480
Toluene ug/kg 789784 101 67-130ND
trans-1,2-Dichloroethene ug/kg 839784 107 69-130ND
trans-1,3-Dichloropropene ug/kg 768784 98 62-130ND
Trichloroethene ug/kg 1020784 114 70-135128
Trichlorofluoromethane ug/kg 621784 79 10-130ND
Vinyl acetate ug/kg 14401570 92 53-130ND
Vinyl chloride ug/kg 953 v178412261-148ND
Xylene (Total)ug/kg 26202350 112 63-132ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%103 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92607493006
3664948SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg ND v1ND
Bromomethane ug/kg ND IKND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg 3.9JND
Chloroethane ug/kg ND v1ND
Chloroform ug/kg NDND
Chloromethane ug/kg ND v1ND
cis-1,2-Dichloroethene ug/kg 670 3693
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg ND v1ND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92607493006
3664948SAMPLE DUPLICATE:
m&p-Xylene ug/kg 9JND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg 7.6 98.3
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg ND v1ND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg 711 0713
Toluene ug/kg 4.9JND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg 163 1161
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg ND v1ND
Xylene (Total)ug/kg 7.6JND
1,2-Dichloroethane-d4 (S)%102102
4-Bromofluorobenzene (S)%10098
Toluene-d8 (S)%100101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702295
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493012, 92607493013, 92607493014, 92607493023, 92607493024, 92607493025, 92607493026
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3665360
Associated Lab Samples:92607493012, 92607493013, 92607493014, 92607493023, 92607493024, 92607493025, 92607493026
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/06/22 14:40
1,1,1-Trichloroethane ug/kg ND 5.0 06/06/22 14:40
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/06/22 14:40
1,1,2-Trichloroethane ug/kg ND 5.0 06/06/22 14:40
1,1-Dichloroethane ug/kg ND 5.0 06/06/22 14:40
1,1-Dichloroethene ug/kg ND 5.0 06/06/22 14:40
1,1-Dichloropropene ug/kg ND 5.0 06/06/22 14:40
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/06/22 14:40
1,2,3-Trichloropropane ug/kg ND 5.0 06/06/22 14:40
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/06/22 14:40
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/06/22 14:40
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/06/22 14:40
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/06/22 14:40
1,2-Dichlorobenzene ug/kg ND 5.0 06/06/22 14:40
1,2-Dichloroethane ug/kg ND 5.0 06/06/22 14:40
1,2-Dichloropropane ug/kg ND 5.0 06/06/22 14:40
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/06/22 14:40
1,3-Dichlorobenzene ug/kg ND 5.0 06/06/22 14:40
1,3-Dichloropropane ug/kg ND 5.0 06/06/22 14:40
1,4-Dichlorobenzene ug/kg ND 5.0 06/06/22 14:40
2,2-Dichloropropane ug/kg ND 5.0 06/06/22 14:40
2-Butanone (MEK)ug/kg ND 100 06/06/22 14:40
2-Chlorotoluene ug/kg ND 5.0 06/06/22 14:40
2-Hexanone ug/kg ND 50.0 06/06/22 14:40
4-Chlorotoluene ug/kg ND 5.0 06/06/22 14:40
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/06/22 14:40
Acetone ug/kg ND 100 06/06/22 14:40
Benzene ug/kg ND 5.0 06/06/22 14:40
Bromobenzene ug/kg ND 5.0 06/06/22 14:40
Bromochloromethane ug/kg ND 5.0 06/06/22 14:40
Bromodichloromethane ug/kg ND 5.0 06/06/22 14:40
Bromoform ug/kg ND 5.0 06/06/22 14:40
Bromomethane ug/kg ND 10.0 IK06/06/22 14:40
Carbon tetrachloride ug/kg ND 5.0 06/06/22 14:40
Chlorobenzene ug/kg ND 5.0 06/06/22 14:40
Chloroethane ug/kg ND 10.0 v106/06/22 14:40
Chloroform ug/kg ND 5.0 06/06/22 14:40
Chloromethane ug/kg ND 10.0 v106/06/22 14:40
cis-1,2-Dichloroethene ug/kg ND 5.0 06/06/22 14:40
cis-1,3-Dichloropropene ug/kg ND 5.0 06/06/22 14:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3665360
Associated Lab Samples:92607493012, 92607493013, 92607493014, 92607493023, 92607493024, 92607493025, 92607493026
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/06/22 14:40
Dibromomethane ug/kg ND 5.0 06/06/22 14:40
Dichlorodifluoromethane ug/kg ND 10.0 v106/06/22 14:40
Diisopropyl ether ug/kg ND 5.0 06/06/22 14:40
Ethylbenzene ug/kg ND 5.0 06/06/22 14:40
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/06/22 14:40
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/06/22 14:40
m&p-Xylene ug/kg ND 10.0 06/06/22 14:40
Methyl-tert-butyl ether ug/kg ND 5.0 06/06/22 14:40
Methylene Chloride ug/kg ND 20.0 06/06/22 14:40
n-Butylbenzene ug/kg ND 5.0 06/06/22 14:40
n-Propylbenzene ug/kg ND 5.0 06/06/22 14:40
Naphthalene ug/kg ND 5.0 06/06/22 14:40
o-Xylene ug/kg ND 5.0 06/06/22 14:40
p-Isopropyltoluene ug/kg ND 5.0 06/06/22 14:40
sec-Butylbenzene ug/kg ND 5.0 06/06/22 14:40
Styrene ug/kg ND 5.0 06/06/22 14:40
tert-Butylbenzene ug/kg ND 5.0 06/06/22 14:40
Tetrachloroethene ug/kg ND 5.0 06/06/22 14:40
Toluene ug/kg ND 5.0 06/06/22 14:40
trans-1,2-Dichloroethene ug/kg ND 5.0 06/06/22 14:40
trans-1,3-Dichloropropene ug/kg ND 5.0 06/06/22 14:40
Trichloroethene ug/kg ND 5.0 06/06/22 14:40
Trichlorofluoromethane ug/kg ND 5.0 06/06/22 14:40
Vinyl acetate ug/kg ND 50.0 06/06/22 14:40
Vinyl chloride ug/kg ND 10.0 v106/06/22 14:40
Xylene (Total)ug/kg ND 10.0 06/06/22 14:40
1,2-Dichloroethane-d4 (S)%102 70-130 06/06/22 14:40
4-Bromofluorobenzene (S)%98 69-134 06/06/22 14:40
Toluene-d8 (S)%98 70-130 06/06/22 14:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3665361LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 13101250 105 70-130
1,1,1-Trichloroethane ug/kg 12201250 98 70-130
1,1,2,2-Tetrachloroethane ug/kg 12501250 100 70-130
1,1,2-Trichloroethane ug/kg 12601250 101 70-130
1,1-Dichloroethane ug/kg 13001250 104 70-130
1,1-Dichloroethene ug/kg 14301250 114 70-130
1,1-Dichloropropene ug/kg 13801250 110 70-130
1,2,3-Trichlorobenzene ug/kg 12801250 102 65-130
1,2,3-Trichloropropane ug/kg 12001250 96 70-130
1,2,4-Trichlorobenzene ug/kg 13201250 106 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3665361LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 13401250 107 70-130
1,2-Dibromo-3-chloropropane ug/kg 13501250 108 70-130
1,2-Dibromoethane (EDB)ug/kg 12701250 101 70-130
1,2-Dichlorobenzene ug/kg 13601250 108 70-130
1,2-Dichloroethane ug/kg 11801250 94 63-130
1,2-Dichloropropane ug/kg 13601250 109 70-130
1,3,5-Trimethylbenzene ug/kg 13701250 110 70-130
1,3-Dichlorobenzene ug/kg 13101250 105 70-130
1,3-Dichloropropane ug/kg 12601250 101 70-130
1,4-Dichlorobenzene ug/kg 13201250 105 70-130
2,2-Dichloropropane ug/kg 12201250 97 66-130
2-Butanone (MEK)ug/kg 23902500 96 70-130
2-Chlorotoluene ug/kg 13601250 109 70-130
2-Hexanone ug/kg 24802500 99 70-130
4-Chlorotoluene ug/kg 13501250 108 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24802500 99 70-130
Acetone ug/kg 22302500 89 69-130
Benzene ug/kg 12601250 100 70-130
Bromobenzene ug/kg 13301250 106 70-130
Bromochloromethane ug/kg 13201250 105 70-130
Bromodichloromethane ug/kg 11401250 92 69-130
Bromoform ug/kg 13101250 105 70-130
Bromomethane ug/kg 1130 IK12509052-130
Carbon tetrachloride ug/kg 12801250 102 70-130
Chlorobenzene ug/kg 12801250 103 70-130
Chloroethane ug/kg 1550 v1125012465-130
Chloroform ug/kg 11601250 93 70-130
Chloromethane ug/kg 1530 v1125012255-130
cis-1,2-Dichloroethene ug/kg 13101250 105 70-130
cis-1,3-Dichloropropene ug/kg 13301250 107 70-130
Dibromochloromethane ug/kg 12601250 101 70-130
Dibromomethane ug/kg 12301250 98 70-130
Dichlorodifluoromethane ug/kg 1830 v1125014645-156
Diisopropyl ether ug/kg 13101250 105 70-130
Ethylbenzene ug/kg 12101250 97 70-130
Hexachloro-1,3-butadiene ug/kg 12901250 103 66-130
Isopropylbenzene (Cumene)ug/kg 12301250 99 70-130
m&p-Xylene ug/kg 25302500 101 70-130
Methyl-tert-butyl ether ug/kg 11201250 90 70-130
Methylene Chloride ug/kg 11801250 95 65-130
n-Butylbenzene ug/kg 14201250 113 67-130
n-Propylbenzene ug/kg 13301250 107 70-130
Naphthalene ug/kg 13301250 106 70-130
o-Xylene ug/kg 12801250 103 70-130
p-Isopropyltoluene ug/kg 14001250 112 67-130
sec-Butylbenzene ug/kg 13601250 109 69-130
Styrene ug/kg 13201250 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3665361LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 13101250 105 67-130
Tetrachloroethene ug/kg 13001250 104 70-130
Toluene ug/kg 11801250 95 70-130
trans-1,2-Dichloroethene ug/kg 13501250 108 70-130
trans-1,3-Dichloropropene ug/kg 13201250 106 68-130
Trichloroethene ug/kg 12701250 101 70-130
Trichlorofluoromethane ug/kg 13801250 111 70-130
Vinyl acetate ug/kg 25102500 100 70-130
Vinyl chloride ug/kg 1560 v1125012561-130
Xylene (Total)ug/kg 38103750 102 70-130
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%96 69-134
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3666182MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92607407002
3666183
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg M1349006670-13184 2434900ND2310029400
1,1,1-Trichloroethane ug/kg 34900 66 65-13386 2634900ND2290029800
1,1,2,2-Tetrachloroethane ug/kg M1349006566-13081 2234900ND2270028300
1,1,2-Trichloroethane ug/kg 34900 67 66-13384 2334900ND2320029200
1,1-Dichloroethane ug/kg 34900 70 65-13089 2434900ND2440031000
1,1-Dichloroethene ug/kg 34900 80 10-158101 2434900ND2780035300
1,1-Dichloropropene ug/kg 34900 73 68-13396 2734900ND2540033300
1,2,3-Trichlorobenzene ug/kg 34900 66 27-13886 2534900ND2320029800
1,2,3-Trichloropropane ug/kg M1349006467-13077 1934900ND2230026800
1,2,4-Trichlorobenzene ug/kg 34900 68 51-13489 2834900ND2360031200
1,2,4-Trimethylbenzene ug/kg 34900 93 63-13694 034900198000230000231000
1,2-Dibromo-3-chloropropane ug/kg 34900 60 32-13078 2634900ND2080027100
1,2-Dibromoethane (EDB)ug/kg M1349006870-13084 2234900ND2360029400
1,2-Dichlorobenzene ug/kg 34900 71 69-13090 2334900ND2490031200
1,2-Dichloroethane ug/kg 34900 63 59-13078 2134900ND2210027200
1,2-Dichloropropane ug/kg 34900 72 70-13091 2334900ND2510031800
1,3,5-Trimethylbenzene ug/kg M13490021865-137229 534900ND7600079900
1,3-Dichlorobenzene ug/kg M1349006870-13090 2834900ND2360031400
1,3-Dichloropropane ug/kg M1349006970-13085 2134900ND2400029600
1,4-Dichlorobenzene ug/kg 34900 71 68-13085 1934900ND2470029800
2,2-Dichloropropane ug/kg 34900 66 32-13085 2634900ND2280029700
2-Butanone (MEK)ug/kg 69700 59 10-13676 2469700ND4130052700
2-Chlorotoluene ug/kg 34900 85 69-141104 2034900ND2960036300
2-Hexanone ug/kg 69700 62 10-14478 2369700ND4290054100
4-Chlorotoluene ug/kg 34900 77 70-13293 1934900ND2680032300
4-Methyl-2-pentanone (MIBK)ug/kg 69700 62 25-14377 2369700ND4290053800
Acetone ug/kg 69700 51 10-13068 2869700ND3570047400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3666182MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92607407002
3666183
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Benzene ug/kg 34900 71 67-13087 1334900153004000045700
Bromobenzene ug/kg 34900 70 70-13088 2334900ND2430030600
Bromochloromethane ug/kg 34900 69 69-13485 2134900ND2410029700
Bromodichloromethane ug/kg M1349005864-13073 2334900ND2010025300
Bromoform ug/kg M1349006162-13078 2534900ND2120027200
Bromomethane ug/kg IK349003820-17651 2934900ND1330017800
Carbon tetrachloride ug/kg 34900 65 65-14085 2634900ND2260029500
Chlorobenzene ug/kg 34900 70 70-13088 2234900ND2440030600
Chloroethane ug/kg v1349008810-130108 2134900ND3050037500
Chloroform ug/kg M1349005263-13067 2734900ND1800023500
Chloromethane ug/kg v1349008558-130108 2434900ND2960037500
cis-1,2-Dichloroethene ug/kg 34900 70 66-13089 2334900ND2440030900
cis-1,3-Dichloropropene ug/kg 34900 67 67-13085 2334900ND2340029600
Dibromochloromethane ug/kg M1349006367-13081 2434900ND2210028100
Dibromomethane ug/kg 34900 66 63-13181 2134900ND2310028300
Dichlorodifluoromethane ug/kg v13490010244-180135 2834900ND3570047200
Diisopropyl ether ug/kg 34900 68 63-13085 2334900ND2380029900
Ethylbenzene ug/kg 34900 73 66-13080 23490097600123000126000
Hexachloro-1,3-butadiene ug/kg R1349006464-15092 3534900ND2250032100
Isopropylbenzene (Cumene)ug/kg 34900 71 69-13588 163490094903430040200
m&p-Xylene ug/kg 69700 72 60-13367 169700382000432000429000
Methyl-tert-butyl ether ug/kg M1349005865-13074 2434900ND2030025800
Methylene Chloride ug/kg M1349005961-13074 2234900ND2060025800
n-Butylbenzene ug/kg 34900 72 65-14096 1834900183004320051700
n-Propylbenzene ug/kg M13490015867-140173 934900ND5490060400
Naphthalene ug/kg 34900 79 15-14592 734900392006670071400
o-Xylene ug/kg 34900 80 66-13379 034900180000208000208000
p-Isopropyltoluene ug/kg 34900 74 56-14797 223490067003250040700
sec-Butylbenzene ug/kg R1349007565-139107 3534900ND2600037300
Styrene ug/kg 34900 86 70-132102 1734900ND3000035600
tert-Butylbenzene ug/kg R1349007162-13598 3334900ND2460034200
Tetrachloroethene ug/kg M1349006970-13589 2634900ND2410031200
Toluene ug/kg 34900 88 67-13083 134900271000302000300000
trans-1,2-Dichloroethene ug/kg 34900 73 69-13092 2434900ND2540032200
trans-1,3-Dichloropropene ug/kg 34900 64 62-13082 2434900ND2230028400
Trichloroethene ug/kg M1349006970-13587 2334900ND2390030200
Trichlorofluoromethane ug/kg 34900 77 10-13099 2634900ND2670034600
Vinyl acetate ug/kg 69700 61 53-13080 2669700ND4270055600
Vinyl chloride ug/kg v1349008961-148113 2434900ND3110039600
Xylene (Total)ug/kg 105000 74 63-13271 1105000562000640000636000
1,2-Dichloroethane-d4 (S)%97 70-13095
4-Bromofluorobenzene (S)%98 69-13498
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702338
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493001, 92607493003, 92607493004, 92607493005, 92607493007, 92607493009, 92607493011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3665455
Associated Lab Samples:92607493001, 92607493003, 92607493004, 92607493005, 92607493007, 92607493009, 92607493011
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/04/22 07:38
1,1,1-Trichloroethane ug/kg ND 5.0 06/04/22 07:38
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/04/22 07:38
1,1,2-Trichloroethane ug/kg ND 5.0 06/04/22 07:38
1,1-Dichloroethane ug/kg ND 5.0 06/04/22 07:38
1,1-Dichloroethene ug/kg ND 5.0 06/04/22 07:38
1,1-Dichloropropene ug/kg ND 5.0 06/04/22 07:38
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/04/22 07:38
1,2,3-Trichloropropane ug/kg ND 5.0 06/04/22 07:38
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/04/22 07:38
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/04/22 07:38
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/04/22 07:38
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/04/22 07:38
1,2-Dichlorobenzene ug/kg ND 5.0 06/04/22 07:38
1,2-Dichloroethane ug/kg ND 5.0 06/04/22 07:38
1,2-Dichloropropane ug/kg ND 5.0 06/04/22 07:38
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/04/22 07:38
1,3-Dichlorobenzene ug/kg ND 5.0 06/04/22 07:38
1,3-Dichloropropane ug/kg ND 5.0 06/04/22 07:38
1,4-Dichlorobenzene ug/kg ND 5.0 06/04/22 07:38
2,2-Dichloropropane ug/kg ND 5.0 06/04/22 07:38
2-Butanone (MEK)ug/kg ND 100 06/04/22 07:38
2-Chlorotoluene ug/kg ND 5.0 06/04/22 07:38
2-Hexanone ug/kg ND 50.0 06/04/22 07:38
4-Chlorotoluene ug/kg ND 5.0 06/04/22 07:38
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/04/22 07:38
Acetone ug/kg ND 100 06/04/22 07:38
Benzene ug/kg ND 5.0 06/04/22 07:38
Bromobenzene ug/kg ND 5.0 06/04/22 07:38
Bromochloromethane ug/kg ND 5.0 06/04/22 07:38
Bromodichloromethane ug/kg ND 5.0 06/04/22 07:38
Bromoform ug/kg ND 5.0 06/04/22 07:38
Bromomethane ug/kg ND 10.0 IK06/04/22 07:38
Carbon tetrachloride ug/kg ND 5.0 06/04/22 07:38
Chlorobenzene ug/kg ND 5.0 06/04/22 07:38
Chloroethane ug/kg ND 10.0 06/04/22 07:38
Chloroform ug/kg ND 5.0 06/04/22 07:38
Chloromethane ug/kg ND 10.0 06/04/22 07:38
cis-1,2-Dichloroethene ug/kg ND 5.0 06/04/22 07:38
cis-1,3-Dichloropropene ug/kg ND 5.0 06/04/22 07:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3665455
Associated Lab Samples:92607493001, 92607493003, 92607493004, 92607493005, 92607493007, 92607493009, 92607493011
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/04/22 07:38
Dibromomethane ug/kg ND 5.0 06/04/22 07:38
Dichlorodifluoromethane ug/kg ND 10.0 v106/04/22 07:38
Diisopropyl ether ug/kg ND 5.0 06/04/22 07:38
Ethylbenzene ug/kg ND 5.0 06/04/22 07:38
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/04/22 07:38
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/04/22 07:38
m&p-Xylene ug/kg ND 10.0 06/04/22 07:38
Methyl-tert-butyl ether ug/kg ND 5.0 06/04/22 07:38
Methylene Chloride ug/kg ND 20.0 06/04/22 07:38
n-Butylbenzene ug/kg ND 5.0 06/04/22 07:38
n-Propylbenzene ug/kg ND 5.0 06/04/22 07:38
Naphthalene ug/kg ND 5.0 06/04/22 07:38
o-Xylene ug/kg ND 5.0 06/04/22 07:38
p-Isopropyltoluene ug/kg ND 5.0 06/04/22 07:38
sec-Butylbenzene ug/kg ND 5.0 06/04/22 07:38
Styrene ug/kg ND 5.0 06/04/22 07:38
tert-Butylbenzene ug/kg ND 5.0 06/04/22 07:38
Tetrachloroethene ug/kg ND 5.0 06/04/22 07:38
Toluene ug/kg ND 5.0 06/04/22 07:38
trans-1,2-Dichloroethene ug/kg ND 5.0 06/04/22 07:38
trans-1,3-Dichloropropene ug/kg ND 5.0 06/04/22 07:38
Trichloroethene ug/kg ND 5.0 06/04/22 07:38
Trichlorofluoromethane ug/kg ND 5.0 06/04/22 07:38
Vinyl acetate ug/kg ND 50.0 06/04/22 07:38
Vinyl chloride ug/kg ND 10.0 v106/04/22 07:38
Xylene (Total)ug/kg ND 10.0 06/04/22 07:38
1,2-Dichloroethane-d4 (S)%105 70-130 06/04/22 07:38
4-Bromofluorobenzene (S)%99 69-134 06/04/22 07:38
Toluene-d8 (S)%99 70-130 06/04/22 07:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3665456LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 13501250 108 70-130
1,1,1-Trichloroethane ug/kg 13401250 107 70-130
1,1,2,2-Tetrachloroethane ug/kg 13001250 104 70-130
1,1,2-Trichloroethane ug/kg 13701250 109 70-130
1,1-Dichloroethane ug/kg 12801250 102 70-130
1,1-Dichloroethene ug/kg 13901250 111 70-130
1,1-Dichloropropene ug/kg 14001250 112 70-130
1,2,3-Trichlorobenzene ug/kg 14101250 112 65-130
1,2,3-Trichloropropane ug/kg 12301250 98 70-130
1,2,4-Trichlorobenzene ug/kg 13301250 106 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3665456LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 15001250 120 70-130
1,2-Dibromo-3-chloropropane ug/kg 12801250 102 70-130
1,2-Dibromoethane (EDB)ug/kg 13301250 106 70-130
1,2-Dichlorobenzene ug/kg 13401250 107 70-130
1,2-Dichloroethane ug/kg 12401250 99 63-130
1,2-Dichloropropane ug/kg 13501250 108 70-130
1,3,5-Trimethylbenzene ug/kg 14601250 117 70-130
1,3-Dichlorobenzene ug/kg 13301250 107 70-130
1,3-Dichloropropane ug/kg 13101250 105 70-130
1,4-Dichlorobenzene ug/kg 12901250 103 70-130
2,2-Dichloropropane ug/kg 12901250 103 66-130
2-Butanone (MEK)ug/kg 24902500 100 70-130
2-Chlorotoluene ug/kg 14001250 112 70-130
2-Hexanone ug/kg 26502500 106 70-130
4-Chlorotoluene ug/kg 13701250 110 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 26902500 108 70-130
Acetone ug/kg 23602500 95 69-130
Benzene ug/kg 12801250 102 70-130
Bromobenzene ug/kg 14001250 112 70-130
Bromochloromethane ug/kg 12801250 103 70-130
Bromodichloromethane ug/kg 12101250 97 69-130
Bromoform ug/kg 14501250 116 70-130
Bromomethane ug/kg 1270 IK125010252-130
Carbon tetrachloride ug/kg 14301250 114 70-130
Chlorobenzene ug/kg 13201250 106 70-130
Chloroethane ug/kg 14701250 118 65-130
Chloroform ug/kg 12601250 101 70-130
Chloromethane ug/kg 14301250 115 55-130
cis-1,2-Dichloroethene ug/kg 13401250 108 70-130
cis-1,3-Dichloropropene ug/kg 13801250 111 70-130
Dibromochloromethane ug/kg 13501250 108 70-130
Dibromomethane ug/kg 13501250 108 70-130
Dichlorodifluoromethane ug/kg 1970 L1,v1125015845-156
Diisopropyl ether ug/kg 13401250 107 70-130
Ethylbenzene ug/kg 12701250 101 70-130
Hexachloro-1,3-butadiene ug/kg 13301250 106 66-130
Isopropylbenzene (Cumene)ug/kg 13701250 110 70-130
m&p-Xylene ug/kg 27302500 109 70-130
Methyl-tert-butyl ether ug/kg 12401250 99 70-130
Methylene Chloride ug/kg 12101250 97 65-130
n-Butylbenzene ug/kg 14301250 115 67-130
n-Propylbenzene ug/kg 13901250 112 70-130
Naphthalene ug/kg 14101250 113 70-130
o-Xylene ug/kg 14501250 116 70-130
p-Isopropyltoluene ug/kg 14601250 117 67-130
sec-Butylbenzene ug/kg 14401250 115 69-130
Styrene ug/kg 15001250 120 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3665456LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 13901250 111 67-130
Tetrachloroethene ug/kg 13401250 107 70-130
Toluene ug/kg 12701250 102 70-130
trans-1,2-Dichloroethene ug/kg 13701250 109 70-130
trans-1,3-Dichloropropene ug/kg 13801250 110 68-130
Trichloroethene ug/kg 14101250 113 70-130
Trichlorofluoromethane ug/kg 14801250 118 70-130
Vinyl acetate ug/kg 27402500 110 70-130
Vinyl chloride ug/kg 1530 v1125012361-130
Xylene (Total)ug/kg 41803750 111 70-130
1,2-Dichloroethane-d4 (S)%86 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3665458MATRIX SPIKE SAMPLE:
MSSpike
Result
92607896001
1,1,1,2-Tetrachloroethane ug/kg 822717 115 70-131ND
1,1,1-Trichloroethane ug/kg 874717 122 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 794717 111 66-130ND
1,1,2-Trichloroethane ug/kg 777717 108 66-133ND
1,1-Dichloroethane ug/kg 801717 112 65-130ND
1,1-Dichloroethene ug/kg 852717 119 10-158ND
1,1-Dichloropropene ug/kg 926717 129 68-133ND
1,2,3-Trichlorobenzene ug/kg 829717 116 27-138ND
1,2,3-Trichloropropane ug/kg 745717 104 67-130ND
1,2,4-Trichlorobenzene ug/kg 876717 122 51-134ND
1,2,4-Trimethylbenzene ug/kg 873717 122 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 718717 100 32-130ND
1,2-Dibromoethane (EDB)ug/kg 754717 105 70-130ND
1,2-Dichlorobenzene ug/kg 831717 116 69-130ND
1,2-Dichloroethane ug/kg 774717 108 59-130ND
1,2-Dichloropropane ug/kg 860717 120 70-130ND
1,3,5-Trimethylbenzene ug/kg 859717 120 65-137ND
1,3-Dichlorobenzene ug/kg 834717 116 70-130ND
1,3-Dichloropropane ug/kg 792717 110 70-130ND
1,4-Dichlorobenzene ug/kg 772717 108 68-130ND
2,2-Dichloropropane ug/kg 765717 107 32-130ND
2-Butanone (MEK)ug/kg 13401440 88 10-136ND
2-Chlorotoluene ug/kg 819717 114 69-141ND
2-Hexanone ug/kg 14701440 102 10-144ND
4-Chlorotoluene ug/kg 814717 114 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 15301440 107 25-143ND
Acetone ug/kg 9551440 67 10-130ND
Benzene ug/kg 850717 119 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3665458MATRIX SPIKE SAMPLE:
MSSpike
Result
92607896001
Bromobenzene ug/kg 811717 113 70-130ND
Bromochloromethane ug/kg 744717 104 69-134ND
Bromodichloromethane ug/kg 718717 100 64-130ND
Bromoform ug/kg 832717 116 62-130ND
Bromomethane ug/kg 515 IK7177220-176ND
Carbon tetrachloride ug/kg 924717 129 65-140ND
Chlorobenzene ug/kg 816717 114 70-130ND
Chloroethane ug/kg 193717 27 10-130ND
Chloroform ug/kg 696717 97 63-130ND
Chloromethane ug/kg 1060 M171714858-130ND
cis-1,2-Dichloroethene ug/kg 851717 119 66-130ND
cis-1,3-Dichloropropene ug/kg 810717 113 67-130ND
Dibromochloromethane ug/kg 763717 106 67-130ND
Dibromomethane ug/kg 800717 112 63-131ND
Dichlorodifluoromethane ug/kg 1240 v171717444-180ND
Diisopropyl ether ug/kg 858717 120 63-130ND
Ethylbenzene ug/kg 785717 110 66-130ND
Hexachloro-1,3-butadiene ug/kg 1050717 147 64-150ND
Isopropylbenzene (Cumene)ug/kg 858717 120 69-135ND
m&p-Xylene ug/kg 16901440 118 60-133ND
Methyl-tert-butyl ether ug/kg 708717 99 65-130ND
Methylene Chloride ug/kg 753717 105 61-130ND
n-Butylbenzene ug/kg 935717 130 65-140ND
n-Propylbenzene ug/kg 833717 116 67-140ND
Naphthalene ug/kg 738717 103 15-145ND
o-Xylene ug/kg 882717 123 66-133ND
p-Isopropyltoluene ug/kg 920717 128 56-147ND
sec-Butylbenzene ug/kg 929717 130 65-139ND
Styrene ug/kg 865717 121 70-132ND
tert-Butylbenzene ug/kg 850717 119 62-135ND
Tetrachloroethene ug/kg 872717 122 70-135ND
Toluene ug/kg 806717 112 67-130ND
trans-1,2-Dichloroethene ug/kg 853717 119 69-130ND
trans-1,3-Dichloropropene ug/kg 789717 110 62-130ND
Trichloroethene ug/kg 908717 127 70-135ND
Trichlorofluoromethane ug/kg 318717 44 10-130ND
Vinyl acetate ug/kg 15701440 109 53-130ND
Vinyl chloride ug/kg 932 v171713061-148ND
Xylene (Total)ug/kg 25802150 120 63-132ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%97 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92607358001
3665457SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg 84.8J C7ND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IKND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg ND v1ND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92607358001
3665457SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg ND v1ND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%100100
4-Bromofluorobenzene (S)%100101
Toluene-d8 (S)%101100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702818
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493027, 92607493028
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3667863
Associated Lab Samples:92607493027, 92607493028
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/07/22 17:04
1,1,1-Trichloroethane ug/kg ND 5.0 06/07/22 17:04
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/07/22 17:04
1,1,2-Trichloroethane ug/kg ND 5.0 06/07/22 17:04
1,1-Dichloroethane ug/kg ND 5.0 06/07/22 17:04
1,1-Dichloroethene ug/kg ND 5.0 06/07/22 17:04
1,1-Dichloropropene ug/kg ND 5.0 06/07/22 17:04
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/07/22 17:04
1,2,3-Trichloropropane ug/kg ND 5.0 06/07/22 17:04
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/07/22 17:04
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/07/22 17:04
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/07/22 17:04
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/07/22 17:04
1,2-Dichlorobenzene ug/kg ND 5.0 06/07/22 17:04
1,2-Dichloroethane ug/kg ND 5.0 06/07/22 17:04
1,2-Dichloropropane ug/kg ND 5.0 06/07/22 17:04
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/07/22 17:04
1,3-Dichlorobenzene ug/kg ND 5.0 06/07/22 17:04
1,3-Dichloropropane ug/kg ND 5.0 06/07/22 17:04
1,4-Dichlorobenzene ug/kg ND 5.0 06/07/22 17:04
2,2-Dichloropropane ug/kg ND 5.0 06/07/22 17:04
2-Butanone (MEK)ug/kg ND 100 06/07/22 17:04
2-Chlorotoluene ug/kg ND 5.0 06/07/22 17:04
2-Hexanone ug/kg ND 50.0 06/07/22 17:04
4-Chlorotoluene ug/kg ND 5.0 06/07/22 17:04
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/07/22 17:04
Acetone ug/kg ND 100 06/07/22 17:04
Benzene ug/kg ND 5.0 06/07/22 17:04
Bromobenzene ug/kg ND 5.0 06/07/22 17:04
Bromochloromethane ug/kg ND 5.0 06/07/22 17:04
Bromodichloromethane ug/kg ND 5.0 06/07/22 17:04
Bromoform ug/kg ND 5.0 06/07/22 17:04
Bromomethane ug/kg ND 10.0 IK06/07/22 17:04
Carbon tetrachloride ug/kg ND 5.0 06/07/22 17:04
Chlorobenzene ug/kg ND 5.0 06/07/22 17:04
Chloroethane ug/kg ND 10.0 06/07/22 17:04
Chloroform ug/kg ND 5.0 06/07/22 17:04
Chloromethane ug/kg ND 10.0 06/07/22 17:04
cis-1,2-Dichloroethene ug/kg ND 5.0 06/07/22 17:04
cis-1,3-Dichloropropene ug/kg ND 5.0 06/07/22 17:04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 108 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3667863
Associated Lab Samples:92607493027, 92607493028
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/07/22 17:04
Dibromomethane ug/kg ND 5.0 06/07/22 17:04
Dichlorodifluoromethane ug/kg ND 10.0 v106/07/22 17:04
Diisopropyl ether ug/kg ND 5.0 06/07/22 17:04
Ethylbenzene ug/kg ND 5.0 06/07/22 17:04
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/07/22 17:04
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/07/22 17:04
m&p-Xylene ug/kg ND 10.0 06/07/22 17:04
Methyl-tert-butyl ether ug/kg ND 5.0 06/07/22 17:04
Methylene Chloride ug/kg ND 20.0 06/07/22 17:04
n-Butylbenzene ug/kg ND 5.0 06/07/22 17:04
n-Propylbenzene ug/kg ND 5.0 06/07/22 17:04
Naphthalene ug/kg ND 5.0 06/07/22 17:04
o-Xylene ug/kg ND 5.0 06/07/22 17:04
p-Isopropyltoluene ug/kg ND 5.0 06/07/22 17:04
sec-Butylbenzene ug/kg ND 5.0 06/07/22 17:04
Styrene ug/kg ND 5.0 06/07/22 17:04
tert-Butylbenzene ug/kg ND 5.0 06/07/22 17:04
Tetrachloroethene ug/kg ND 5.0 06/07/22 17:04
Toluene ug/kg ND 5.0 06/07/22 17:04
trans-1,2-Dichloroethene ug/kg ND 5.0 06/07/22 17:04
trans-1,3-Dichloropropene ug/kg ND 5.0 06/07/22 17:04
Trichloroethene ug/kg ND 5.0 06/07/22 17:04
Trichlorofluoromethane ug/kg ND 5.0 06/07/22 17:04
Vinyl acetate ug/kg ND 50.0 06/07/22 17:04
Vinyl chloride ug/kg ND 10.0 v106/07/22 17:04
Xylene (Total)ug/kg ND 10.0 06/07/22 17:04
1,2-Dichloroethane-d4 (S)%98 70-130 06/07/22 17:04
4-Bromofluorobenzene (S)%99 69-134 06/07/22 17:04
Toluene-d8 (S)%97 70-130 06/07/22 17:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3667864LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12501250 100 70-130
1,1,1-Trichloroethane ug/kg 11801250 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 11501250 92 70-130
1,1,2-Trichloroethane ug/kg 12201250 98 70-130
1,1-Dichloroethane ug/kg 12601250 101 70-130
1,1-Dichloroethene ug/kg 13801250 111 70-130
1,1-Dichloropropene ug/kg 13101250 105 70-130
1,2,3-Trichlorobenzene ug/kg 10901250 87 65-130
1,2,3-Trichloropropane ug/kg 11301250 90 70-130
1,2,4-Trichlorobenzene ug/kg 12101250 97 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3667864LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12801250 102 70-130
1,2-Dibromo-3-chloropropane ug/kg 11501250 92 70-130
1,2-Dibromoethane (EDB)ug/kg 12501250 100 70-130
1,2-Dichlorobenzene ug/kg 12901250 103 70-130
1,2-Dichloroethane ug/kg 11001250 88 63-130
1,2-Dichloropropane ug/kg 13201250 105 70-130
1,3,5-Trimethylbenzene ug/kg 13201250 106 70-130
1,3-Dichlorobenzene ug/kg 13001250 104 70-130
1,3-Dichloropropane ug/kg 12301250 99 70-130
1,4-Dichlorobenzene ug/kg 12401250 99 70-130
2,2-Dichloropropane ug/kg 12801250 102 66-130
2-Butanone (MEK)ug/kg 22302500 89 70-130
2-Chlorotoluene ug/kg 13001250 104 70-130
2-Hexanone ug/kg 24102500 96 70-130
4-Chlorotoluene ug/kg 13001250 104 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 23102500 92 70-130
Acetone ug/kg 20002500 80 69-130
Benzene ug/kg 12201250 98 70-130
Bromobenzene ug/kg 13001250 104 70-130
Bromochloromethane ug/kg 12801250 102 70-130
Bromodichloromethane ug/kg 10401250 83 69-130
Bromoform ug/kg 11401250 91 70-130
Bromomethane ug/kg 1230 IK12509852-130
Carbon tetrachloride ug/kg 12201250 98 70-130
Chlorobenzene ug/kg 12501250 100 70-130
Chloroethane ug/kg 15601250 125 65-130
Chloroform ug/kg 10801250 87 70-130
Chloromethane ug/kg 15901250 127 55-130
cis-1,2-Dichloroethene ug/kg 12701250 102 70-130
cis-1,3-Dichloropropene ug/kg 12801250 102 70-130
Dibromochloromethane ug/kg 11601250 93 70-130
Dibromomethane ug/kg 11901250 95 70-130
Dichlorodifluoromethane ug/kg 1980 L1,v1125015845-156
Diisopropyl ether ug/kg 12901250 103 70-130
Ethylbenzene ug/kg 11601250 92 70-130
Hexachloro-1,3-butadiene ug/kg 12201250 98 66-130
Isopropylbenzene (Cumene)ug/kg 11701250 94 70-130
m&p-Xylene ug/kg 24202500 97 70-130
Methyl-tert-butyl ether ug/kg 11301250 90 70-130
Methylene Chloride ug/kg 11501250 92 65-130
n-Butylbenzene ug/kg 13301250 106 67-130
n-Propylbenzene ug/kg 12801250 102 70-130
Naphthalene ug/kg 11301250 90 70-130
o-Xylene ug/kg 12401250 99 70-130
p-Isopropyltoluene ug/kg 13301250 106 67-130
sec-Butylbenzene ug/kg 12901250 103 69-130
Styrene ug/kg 12801250 103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3667864LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12801250 102 67-130
Tetrachloroethene ug/kg 12601250 101 70-130
Toluene ug/kg 11401250 91 70-130
trans-1,2-Dichloroethene ug/kg 13201250 105 70-130
trans-1,3-Dichloropropene ug/kg 12601250 101 68-130
Trichloroethene ug/kg 12201250 98 70-130
Trichlorofluoromethane ug/kg 13601250 109 70-130
Vinyl acetate ug/kg 26002500 104 70-130
Vinyl chloride ug/kg 1610 v1125012961-130
Xylene (Total)ug/kg 36603750 98 70-130
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%96 69-134
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3667865MATRIX SPIKE SAMPLE:
MSSpike
Result
92607883001
1,1,1,2-Tetrachloroethane ug/kg 541612 88 70-131ND
1,1,1-Trichloroethane ug/kg 556612 91 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 493612 80 66-130ND
1,1,2-Trichloroethane ug/kg 522612 85 66-133ND
1,1-Dichloroethane ug/kg 594612 97 65-130ND
1,1-Dichloroethene ug/kg 664612 108 10-158ND
1,1-Dichloropropene ug/kg 651612 106 68-133ND
1,2,3-Trichlorobenzene ug/kg 350612 57 27-138ND
1,2,3-Trichloropropane ug/kg 472612 77 67-130ND
1,2,4-Trichlorobenzene ug/kg 531612 87 51-134ND
1,2,4-Trimethylbenzene ug/kg 612612 100 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 376612 61 32-130ND
1,2-Dibromoethane (EDB)ug/kg 540612 88 70-130ND
1,2-Dichlorobenzene ug/kg 600612 98 69-130ND
1,2-Dichloroethane ug/kg 491612 80 59-130ND
1,2-Dichloropropane ug/kg 626612 102 70-130ND
1,3,5-Trimethylbenzene ug/kg 634612 104 65-137ND
1,3-Dichlorobenzene ug/kg 588612 96 70-130ND
1,3-Dichloropropane ug/kg 562612 92 70-130ND
1,4-Dichlorobenzene ug/kg 589612 96 68-130ND
2,2-Dichloropropane ug/kg 574612 94 32-130ND
2-Butanone (MEK)ug/kg 8591220 70 10-136ND
2-Chlorotoluene ug/kg 601612 98 69-141ND
2-Hexanone ug/kg 8721220 71 10-144ND
4-Chlorotoluene ug/kg 600612 98 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 9041220 74 25-143ND
Acetone ug/kg 6891220 56 10-130ND
Benzene ug/kg 604612 99 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3667865MATRIX SPIKE SAMPLE:
MSSpike
Result
92607883001
Bromobenzene ug/kg 574612 94 70-130ND
Bromochloromethane ug/kg 559 v36129169-134ND
Bromodichloromethane ug/kg 432612 71 64-130ND
Bromoform ug/kg 415612 68 62-130ND
Bromomethane ug/kg 97.7 IK,M16121620-176ND
Carbon tetrachloride ug/kg 539612 88 65-140ND
Chlorobenzene ug/kg 582612 95 70-130ND
Chloroethane ug/kg 182612 30 10-130ND
Chloroform ug/kg 457612 75 63-130ND
Chloromethane ug/kg 810 M161213258-130ND
cis-1,2-Dichloroethene ug/kg 605612 99 66-130ND
cis-1,3-Dichloropropene ug/kg 547612 89 67-130ND
Dibromochloromethane ug/kg 449612 73 67-130ND
Dibromomethane ug/kg 505612 82 63-131ND
Dichlorodifluoromethane ug/kg 982612 160 44-180ND
Diisopropyl ether ug/kg 615612 100 63-130ND
Ethylbenzene ug/kg 556612 91 66-130ND
Hexachloro-1,3-butadiene ug/kg 648612 106 64-150ND
Isopropylbenzene (Cumene)ug/kg 579612 95 69-135ND
m&p-Xylene ug/kg 11601220 94 60-133ND
Methyl-tert-butyl ether ug/kg 507612 83 65-130ND
Methylene Chloride ug/kg 594612 75 61-1300.14 mg/kg
n-Butylbenzene ug/kg 676612 110 65-140ND
n-Propylbenzene ug/kg 616612 101 67-140ND
Naphthalene ug/kg 328612 54 15-145ND
o-Xylene ug/kg 577612 94 66-133ND
p-Isopropyltoluene ug/kg 670612 109 56-147ND
sec-Butylbenzene ug/kg 659612 108 65-139ND
Styrene ug/kg 585612 95 70-132ND
tert-Butylbenzene ug/kg 621612 101 62-135ND
Tetrachloroethene ug/kg 603612 98 70-135ND
Toluene ug/kg 541612 88 67-130ND
trans-1,2-Dichloroethene ug/kg 642612 105 69-130ND
trans-1,3-Dichloropropene ug/kg 513612 84 62-130ND
Trichloroethene ug/kg 587612 96 70-135ND
Trichlorofluoromethane ug/kg 168612 27 10-130ND
Vinyl acetate ug/kg 10501220 86 53-130ND
Vinyl chloride ug/kg 796612 130 61-148ND
Xylene (Total)ug/kg 17301830 94 63-132ND
1,2-Dichloroethane-d4 (S)%84 70-130
4-Bromofluorobenzene (S)%95 69-134
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92608051002
3667866SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg ND v2ND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IKND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92608051002
3667866SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg ND252
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%8991
4-Bromofluorobenzene (S)%9998
Toluene-d8 (S)%9797
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702875
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3668242
Associated Lab Samples:92607493002
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/08/22 05:25
1,1,1-Trichloroethane ug/kg ND 5.0 06/08/22 05:25
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/08/22 05:25
1,1,2-Trichloroethane ug/kg ND 5.0 06/08/22 05:25
1,1-Dichloroethane ug/kg ND 5.0 06/08/22 05:25
1,1-Dichloroethene ug/kg ND 5.0 06/08/22 05:25
1,1-Dichloropropene ug/kg ND 5.0 06/08/22 05:25
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/08/22 05:25
1,2,3-Trichloropropane ug/kg ND 5.0 06/08/22 05:25
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/08/22 05:25
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/08/22 05:25
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/08/22 05:25
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/08/22 05:25
1,2-Dichlorobenzene ug/kg ND 5.0 06/08/22 05:25
1,2-Dichloroethane ug/kg ND 5.0 06/08/22 05:25
1,2-Dichloropropane ug/kg ND 5.0 06/08/22 05:25
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/08/22 05:25
1,3-Dichlorobenzene ug/kg ND 5.0 06/08/22 05:25
1,3-Dichloropropane ug/kg ND 5.0 06/08/22 05:25
1,4-Dichlorobenzene ug/kg ND 5.0 06/08/22 05:25
2,2-Dichloropropane ug/kg ND 5.0 06/08/22 05:25
2-Butanone (MEK)ug/kg ND 100 06/08/22 05:25
2-Chlorotoluene ug/kg ND 5.0 06/08/22 05:25
2-Hexanone ug/kg ND 50.0 06/08/22 05:25
4-Chlorotoluene ug/kg ND 5.0 06/08/22 05:25
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/08/22 05:25
Acetone ug/kg ND 100 06/08/22 05:25
Benzene ug/kg ND 5.0 06/08/22 05:25
Bromobenzene ug/kg ND 5.0 06/08/22 05:25
Bromochloromethane ug/kg ND 5.0 06/08/22 05:25
Bromodichloromethane ug/kg ND 5.0 v206/08/22 05:25
Bromoform ug/kg ND 5.0 06/08/22 05:25
Bromomethane ug/kg ND 10.0 IK06/08/22 05:25
Carbon tetrachloride ug/kg ND 5.0 06/08/22 05:25
Chlorobenzene ug/kg ND 5.0 06/08/22 05:25
Chloroethane ug/kg ND 10.0 06/08/22 05:25
Chloroform ug/kg ND 5.0 06/08/22 05:25
Chloromethane ug/kg ND 10.0 06/08/22 05:25
cis-1,2-Dichloroethene ug/kg ND 5.0 06/08/22 05:25
cis-1,3-Dichloropropene ug/kg ND 5.0 06/08/22 05:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3668242
Associated Lab Samples:92607493002
Matrix:Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 06/08/22 05:25
Dibromomethane ug/kg ND 5.0 06/08/22 05:25
Dichlorodifluoromethane ug/kg ND 10.0 06/08/22 05:25
Diisopropyl ether ug/kg ND 5.0 06/08/22 05:25
Ethylbenzene ug/kg ND 5.0 06/08/22 05:25
Hexachloro-1,3-butadiene ug/kg ND 10.0 06/08/22 05:25
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/08/22 05:25
m&p-Xylene ug/kg ND 10.0 06/08/22 05:25
Methyl-tert-butyl ether ug/kg ND 5.0 06/08/22 05:25
Methylene Chloride ug/kg ND 20.0 06/08/22 05:25
n-Butylbenzene ug/kg ND 5.0 06/08/22 05:25
n-Propylbenzene ug/kg ND 5.0 06/08/22 05:25
Naphthalene ug/kg ND 5.0 06/08/22 05:25
o-Xylene ug/kg ND 5.0 06/08/22 05:25
p-Isopropyltoluene ug/kg ND 5.0 06/08/22 05:25
sec-Butylbenzene ug/kg ND 5.0 06/08/22 05:25
Styrene ug/kg ND 5.0 06/08/22 05:25
tert-Butylbenzene ug/kg ND 5.0 06/08/22 05:25
Tetrachloroethene ug/kg ND 5.0 06/08/22 05:25
Toluene ug/kg ND 5.0 06/08/22 05:25
trans-1,2-Dichloroethene ug/kg ND 5.0 06/08/22 05:25
trans-1,3-Dichloropropene ug/kg ND 5.0 06/08/22 05:25
Trichloroethene ug/kg ND 5.0 06/08/22 05:25
Trichlorofluoromethane ug/kg ND 5.0 06/08/22 05:25
Vinyl acetate ug/kg ND 50.0 06/08/22 05:25
Vinyl chloride ug/kg ND 10.0 06/08/22 05:25
Xylene (Total)ug/kg ND 10.0 06/08/22 05:25
1,2-Dichloroethane-d4 (S)%97 70-130 06/08/22 05:25
4-Bromofluorobenzene (S)%99 69-134 06/08/22 05:25
Toluene-d8 (S)%98 70-130 06/08/22 05:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3668243LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12601250 100 70-130
1,1,1-Trichloroethane ug/kg 11901250 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 11201250 90 70-130
1,1,2-Trichloroethane ug/kg 11801250 95 70-130
1,1-Dichloroethane ug/kg 12601250 101 70-130
1,1-Dichloroethene ug/kg 14101250 113 70-130
1,1-Dichloropropene ug/kg 13201250 105 70-130
1,2,3-Trichlorobenzene ug/kg 10801250 86 65-130
1,2,3-Trichloropropane ug/kg 10801250 86 70-130
1,2,4-Trichlorobenzene ug/kg 12101250 97 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3668243LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 13001250 104 70-130
1,2-Dibromo-3-chloropropane ug/kg 10501250 84 70-130
1,2-Dibromoethane (EDB)ug/kg 12101250 97 70-130
1,2-Dichlorobenzene ug/kg 13001250 104 70-130
1,2-Dichloroethane ug/kg 10601250 85 63-130
1,2-Dichloropropane ug/kg 13301250 106 70-130
1,3,5-Trimethylbenzene ug/kg 13601250 109 70-130
1,3-Dichlorobenzene ug/kg 12901250 103 70-130
1,3-Dichloropropane ug/kg 12401250 99 70-130
1,4-Dichlorobenzene ug/kg 12801250 102 70-130
2,2-Dichloropropane ug/kg 12501250 100 66-130
2-Butanone (MEK)ug/kg 20402500 81 70-130
2-Chlorotoluene ug/kg 13301250 107 70-130
2-Hexanone ug/kg 22202500 89 70-130
4-Chlorotoluene ug/kg 13301250 106 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 21702500 87 70-130
Acetone ug/kg 18702500 75 69-130
Benzene ug/kg 12301250 99 70-130
Bromobenzene ug/kg 13201250 106 70-130
Bromochloromethane ug/kg 12401250 99 70-130
Bromodichloromethane ug/kg 1020 v312508269-130
Bromoform ug/kg 10901250 87 70-130
Bromomethane ug/kg 1280 IK125010352-130
Carbon tetrachloride ug/kg 12001250 96 70-130
Chlorobenzene ug/kg 12501250 100 70-130
Chloroethane ug/kg 15901250 127 65-130
Chloroform ug/kg 10701250 85 70-130
Chloromethane ug/kg 16301250 130 55-130
cis-1,2-Dichloroethene ug/kg 12601250 101 70-130
cis-1,3-Dichloropropene ug/kg 12501250 100 70-130
Dibromochloromethane ug/kg 11301250 91 70-130
Dibromomethane ug/kg 11501250 92 70-130
Dichlorodifluoromethane ug/kg 18201250 145 45-156
Diisopropyl ether ug/kg 12901250 104 70-130
Ethylbenzene ug/kg 11701250 94 70-130
Hexachloro-1,3-butadiene ug/kg 12301250 99 66-130
Isopropylbenzene (Cumene)ug/kg 12001250 96 70-130
m&p-Xylene ug/kg 24602500 98 70-130
Methyl-tert-butyl ether ug/kg 11201250 89 70-130
Methylene Chloride ug/kg 11701250 94 65-130
n-Butylbenzene ug/kg 13601250 109 67-130
n-Propylbenzene ug/kg 13201250 106 70-130
Naphthalene ug/kg 10901250 88 70-130
o-Xylene ug/kg 12601250 101 70-130
p-Isopropyltoluene ug/kg 13601250 109 67-130
sec-Butylbenzene ug/kg 13201250 106 69-130
Styrene ug/kg 12901250 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3668243LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 13101250 105 67-130
Tetrachloroethene ug/kg 13001250 104 70-130
Toluene ug/kg 11401250 91 70-130
trans-1,2-Dichloroethene ug/kg 13401250 107 70-130
trans-1,3-Dichloropropene ug/kg 12201250 97 68-130
Trichloroethene ug/kg 12401250 99 70-130
Trichlorofluoromethane ug/kg 13001250 104 70-130
Vinyl acetate ug/kg 24802500 99 70-130
Vinyl chloride ug/kg 1640 L1125013161-130
Xylene (Total)ug/kg 37203750 99 70-130
1,2-Dichloroethane-d4 (S)%82 70-130
4-Bromofluorobenzene (S)%96 69-134
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3668244MATRIX SPIKE SAMPLE:
MSSpike
Result
92608051001
1,1,1,2-Tetrachloroethane ug/kg 263 M17413670-131ND
1,1,1-Trichloroethane ug/kg 274 M17413765-133ND
1,1,2,2-Tetrachloroethane ug/kg 263 M17413666-130ND
1,1,2-Trichloroethane ug/kg 273 M17413766-133ND
1,1-Dichloroethane ug/kg 302 M17414165-130ND
1,1-Dichloroethene ug/kg 336741 45 10-158ND
1,1-Dichloropropene ug/kg 317 M17414368-133ND
1,2,3-Trichlorobenzene ug/kg 159 M17412227-138ND
1,2,3-Trichloropropane ug/kg 252 M17413467-130ND
1,2,4-Trichlorobenzene ug/kg 251 M17413451-134ND
1,2,4-Trimethylbenzene ug/kg 316 M17414363-136ND
1,2-Dibromo-3-chloropropane ug/kg 166 M17412232-130ND
1,2-Dibromoethane (EDB)ug/kg 279 M17413870-130ND
1,2-Dichlorobenzene ug/kg 315 M17414369-130ND
1,2-Dichloroethane ug/kg 261 M17413559-130ND
1,2-Dichloropropane ug/kg 317 M17414370-130ND
1,3,5-Trimethylbenzene ug/kg 329 M17414465-137ND
1,3-Dichlorobenzene ug/kg 316 M17414370-130ND
1,3-Dichloropropane ug/kg 300 M17414070-130ND
1,4-Dichlorobenzene ug/kg 299 M17414068-130ND
2,2-Dichloropropane ug/kg 256741 35 32-130ND
2-Butanone (MEK)ug/kg 5021490 34 10-136ND
2-Chlorotoluene ug/kg 317 M17414369-141ND
2-Hexanone ug/kg 4751490 32 10-144ND
4-Chlorotoluene ug/kg 308 M17414270-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 4931490 33 25-143ND
Acetone ug/kg 3391490 23 10-130ND
Benzene ug/kg 308 M17414267-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3668244MATRIX SPIKE SAMPLE:
MSSpike
Result
92608051001
Bromobenzene ug/kg 298 M17414070-130ND
Bromochloromethane ug/kg 291 M17413969-134ND
Bromodichloromethane ug/kg 209 M1,v37412864-130ND
Bromoform ug/kg 197 M17412762-130ND
Bromomethane ug/kg ND IK,M1741020-176ND
Carbon tetrachloride ug/kg 262 M17413565-140ND
Chlorobenzene ug/kg 306 M17414170-130ND
Chloroethane ug/kg 93.0741 13 10-130ND
Chloroform ug/kg 170 M17412363-130ND
Chloromethane ug/kg 416 M17415658-130ND
cis-1,2-Dichloroethene ug/kg 309 M17414266-130ND
cis-1,3-Dichloropropene ug/kg 262 M17413567-130ND
Dibromochloromethane ug/kg 215 M17412967-130ND
Dibromomethane ug/kg 255 M17413463-131ND
Dichlorodifluoromethane ug/kg 475741 64 44-180ND
Diisopropyl ether ug/kg 312 M17414263-130ND
Ethylbenzene ug/kg 291 M17413966-130ND
Hexachloro-1,3-butadiene ug/kg 297 M17414064-150ND
Isopropylbenzene (Cumene)ug/kg 310 M17414269-135ND
m&p-Xylene ug/kg 607 M114904160-133ND
Methyl-tert-butyl ether ug/kg 284 M17413865-130ND
Methylene Chloride ug/kg 239 M17413261-130ND
n-Butylbenzene ug/kg 331 M17414565-140ND
n-Propylbenzene ug/kg 313 M17414267-140ND
Naphthalene ug/kg 158741 21 15-145ND
o-Xylene ug/kg 302 M17414166-133ND
p-Isopropyltoluene ug/kg 334 M17414556-147ND
sec-Butylbenzene ug/kg 338 M17414665-139ND
Styrene ug/kg 300 M17414070-132ND
tert-Butylbenzene ug/kg 314 M17414262-135ND
Tetrachloroethene ug/kg 301 M17414170-135ND
Toluene ug/kg 277 M17413767-130ND
trans-1,2-Dichloroethene ug/kg 321 M17414369-130ND
trans-1,3-Dichloropropene ug/kg 247 M17413362-130ND
Trichloroethene ug/kg 291 M17413970-135ND
Trichlorofluoromethane ug/kg 83.8741 11 10-130ND
Vinyl acetate ug/kg 492 M114903353-130ND
Vinyl chloride ug/kg 405 M07415561-148ND
Xylene (Total)ug/kg 909 MS22204163-132ND
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92608113001
3668245SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg ND v2ND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IKND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92608113001
3668245SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg 12.6 611.9
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%9090
4-Bromofluorobenzene (S)%101100
Toluene-d8 (S)%9897
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702561
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493029
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3666517
Associated Lab Samples:92607493029
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/06/22 14:24
1,1,1-Trichloroethane ug/L ND 1.0 06/06/22 14:24
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/06/22 14:24
1,1,2-Trichloroethane ug/L ND 1.0 06/06/22 14:24
1,1-Dichloroethane ug/L ND 1.0 06/06/22 14:24
1,1-Dichloroethene ug/L ND 1.0 06/06/22 14:24
1,1-Dichloropropene ug/L ND 1.0 06/06/22 14:24
1,2,3-Trichlorobenzene ug/L ND 1.0 06/06/22 14:24
1,2,3-Trichloropropane ug/L ND 1.0 06/06/22 14:24
1,2,4-Trichlorobenzene ug/L ND 1.0 06/06/22 14:24
1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/06/22 14:24
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/06/22 14:24
1,2-Dichlorobenzene ug/L ND 1.0 06/06/22 14:24
1,2-Dichloroethane ug/L ND 1.0 06/06/22 14:24
1,2-Dichloropropane ug/L ND 1.0 06/06/22 14:24
1,3-Dichlorobenzene ug/L ND 1.0 06/06/22 14:24
1,3-Dichloropropane ug/L ND 1.0 06/06/22 14:24
1,4-Dichlorobenzene ug/L ND 1.0 06/06/22 14:24
2,2-Dichloropropane ug/L ND 1.0 06/06/22 14:24
2-Butanone (MEK)ug/L ND 5.0 06/06/22 14:24
2-Chlorotoluene ug/L ND 1.0 06/06/22 14:24
2-Hexanone ug/L ND 5.0 06/06/22 14:24
4-Chlorotoluene ug/L ND 1.0 06/06/22 14:24
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/06/22 14:24
Acetone ug/L ND 25.0 06/06/22 14:24
Benzene ug/L ND 1.0 06/06/22 14:24
Bromobenzene ug/L ND 1.0 06/06/22 14:24
Bromochloromethane ug/L ND 1.0 06/06/22 14:24
Bromodichloromethane ug/L ND 1.0 06/06/22 14:24
Bromoform ug/L ND 1.0 IK06/06/22 14:24
Bromomethane ug/L ND 2.0 v206/06/22 14:24
Carbon tetrachloride ug/L ND 1.0 06/06/22 14:24
Chlorobenzene ug/L ND 1.0 06/06/22 14:24
Chloroethane ug/L ND 1.0 06/06/22 14:24
Chloroform ug/L ND 1.0 06/06/22 14:24
Chloromethane ug/L ND 1.0 06/06/22 14:24
cis-1,2-Dichloroethene ug/L ND 1.0 06/06/22 14:24
cis-1,3-Dichloropropene ug/L ND 1.0 06/06/22 14:24
Dibromochloromethane ug/L ND 1.0 06/06/22 14:24
Dibromomethane ug/L ND 1.0 06/06/22 14:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3666517
Associated Lab Samples:92607493029
Matrix:Water
Analyzed
Dichlorodifluoromethane ug/L ND 1.0 06/06/22 14:24
Diisopropyl ether ug/L ND 1.0 06/06/22 14:24
Ethylbenzene ug/L ND 1.0 06/06/22 14:24
Hexachloro-1,3-butadiene ug/L ND 2.0 v206/06/22 14:24
m&p-Xylene ug/L ND 2.0 06/06/22 14:24
Methyl-tert-butyl ether ug/L ND 1.0 06/06/22 14:24
Methylene Chloride ug/L ND 5.0 06/06/22 14:24
Naphthalene ug/L ND 1.0 06/06/22 14:24
o-Xylene ug/L ND 1.0 06/06/22 14:24
p-Isopropyltoluene ug/L ND 1.0 06/06/22 14:24
Styrene ug/L ND 1.0 06/06/22 14:24
Tetrachloroethene ug/L ND 1.0 06/06/22 14:24
Toluene ug/L ND 1.0 06/06/22 14:24
trans-1,2-Dichloroethene ug/L ND 1.0 06/06/22 14:24
trans-1,3-Dichloropropene ug/L ND 1.0 06/06/22 14:24
Trichloroethene ug/L ND 1.0 06/06/22 14:24
Trichlorofluoromethane ug/L ND 1.0 06/06/22 14:24
Vinyl acetate ug/L ND 2.0 06/06/22 14:24
Vinyl chloride ug/L ND 1.0 06/06/22 14:24
Xylene (Total)ug/L ND 1.0 06/06/22 14:24
1,2-Dichloroethane-d4 (S)%105 70-130 06/06/22 14:24
4-Bromofluorobenzene (S)%96 70-130 06/06/22 14:24
Toluene-d8 (S)%99 70-130 06/06/22 14:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3666518LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.950 104 70-130
1,1,1-Trichloroethane ug/L 53.050 106 70-130
1,1,2,2-Tetrachloroethane ug/L 54.550 109 70-130
1,1,2-Trichloroethane ug/L 55.650 111 70-130
1,1-Dichloroethane ug/L 56.450 113 70-130
1,1-Dichloroethene ug/L 58.050 116 70-132
1,1-Dichloropropene ug/L 56.350 113 70-131
1,2,3-Trichlorobenzene ug/L 45.450 91 70-134
1,2,3-Trichloropropane ug/L 53.750 107 70-130
1,2,4-Trichlorobenzene ug/L 46.050 92 70-130
1,2-Dibromo-3-chloropropane ug/L 52.150 104 70-132
1,2-Dibromoethane (EDB)ug/L 54.950 110 70-130
1,2-Dichlorobenzene ug/L 52.450 105 70-130
1,2-Dichloroethane ug/L 53.050 106 70-130
1,2-Dichloropropane ug/L 55.650 111 70-130
1,3-Dichlorobenzene ug/L 52.650 105 70-130
1,3-Dichloropropane ug/L 55.550 111 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3666518LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 51.950 104 70-130
2,2-Dichloropropane ug/L 52.550 105 70-130
2-Butanone (MEK)ug/L 110100 110 70-133
2-Chlorotoluene ug/L 53.050 106 70-130
2-Hexanone ug/L 109100 109 70-130
4-Chlorotoluene ug/L 53.250 106 70-130
4-Methyl-2-pentanone (MIBK)ug/L 106100 106 70-130
Acetone ug/L 106100 106 70-144
Benzene ug/L 51.850 104 70-130
Bromobenzene ug/L 53.450 107 70-130
Bromochloromethane ug/L 58.050 116 70-130
Bromodichloromethane ug/L 54.550 109 70-130
Bromoform ug/L 52.0 IK5010470-131
Bromomethane ug/L 40.4 v3508130-177
Carbon tetrachloride ug/L 47.750 95 70-130
Chlorobenzene ug/L 53.850 108 70-130
Chloroethane ug/L 40.250 80 46-131
Chloroform ug/L 57.950 116 70-130
Chloromethane ug/L 57.950 116 49-130
cis-1,2-Dichloroethene ug/L 56.750 113 70-130
cis-1,3-Dichloropropene ug/L 56.350 113 70-130
Dibromochloromethane ug/L 53.150 106 70-130
Dibromomethane ug/L 52.050 104 70-130
Dichlorodifluoromethane ug/L 54.850 110 52-134
Diisopropyl ether ug/L 55.650 111 70-131
Ethylbenzene ug/L 52.450 105 70-130
Hexachloro-1,3-butadiene ug/L 38.1 v3507670-131
m&p-Xylene ug/L 106100 106 70-130
Methyl-tert-butyl ether ug/L 55.250 110 70-130
Methylene Chloride ug/L 54.150 108 68-130
Naphthalene ug/L 53.250 106 70-133
o-Xylene ug/L 52.750 105 70-130
p-Isopropyltoluene ug/L 49.750 99 70-130
Styrene ug/L 56.050 112 70-130
Tetrachloroethene ug/L 48.250 96 70-130
Toluene ug/L 53.450 107 70-130
trans-1,2-Dichloroethene ug/L 57.850 116 70-130
trans-1,3-Dichloropropene ug/L 55.350 111 70-130
Trichloroethene ug/L 52.550 105 70-130
Trichlorofluoromethane ug/L 45.350 91 61-130
Vinyl acetate ug/L 101100 101 70-140
Vinyl chloride ug/L 57.550 115 59-142
Xylene (Total)ug/L 159150 106 70-130
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 124 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3666519MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92607618001
3666520
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 105 70-135102 320ND21.0 20.4
1,1,1-Trichloroethane ug/L 20 105 70-148103 120ND21.0 20.7
1,1,2,2-Tetrachloroethane ug/L 20 104 70-131103 120ND20.9 20.7
1,1,2-Trichloroethane ug/L 20 105 70-136107 220ND21.0 21.4
1,1-Dichloroethane ug/L 20 102 70-147102 020ND20.4 20.4
1,1-Dichloroethene ug/L 20 105 70-158105 020ND20.9 21.0
1,1-Dichloropropene ug/L 20 112 70-149111 020ND22.3 22.3
1,2,3-Trichlorobenzene ug/L 20 104 68-140108 320ND20.9 21.5
1,2,3-Trichloropropane ug/L 20 103 67-13798 520ND20.7 19.6
1,2,4-Trichlorobenzene ug/L 20 108 70-139108 120ND21.5 21.7
1,2-Dibromo-3-chloropropane ug/L 20 105 69-136107 220ND20.9 21.3
1,2-Dibromoethane (EDB)ug/L 20 109 70-137104 520ND21.8 20.7
1,2-Dichlorobenzene ug/L 20 106 70-133104 120ND21.2 20.9
1,2-Dichloroethane ug/L 20 99 67-13896 320ND19.7 19.2
1,2-Dichloropropane ug/L 20 108 70-138109 120ND21.6 21.8
1,3-Dichlorobenzene ug/L 20 107 70-133107 120ND21.3 21.5
1,3-Dichloropropane ug/L 20 104 70-136101 420ND20.9 20.1
1,4-Dichlorobenzene ug/L 20 104 70-133104 120ND20.9 20.7
2,2-Dichloropropane ug/L 20 107 52-155107 120ND21.5 21.4
2-Butanone (MEK)ug/L 40 111 61-147115 440ND44.2 46.0
2-Chlorotoluene ug/L 20 107 70-141104 320ND21.4 20.7
2-Hexanone ug/L 40 110 67-139108 240ND43.9 43.2
4-Chlorotoluene ug/L 20 106 70-135105 120ND21.2 21.0
4-Methyl-2-pentanone (MIBK)ug/L 40 105 67-136107 240ND42.0 42.6
Acetone ug/L 40 92 55-159101 740ND46.0 49.5
Benzene ug/L 20 101 67-15099 220ND20.1 19.8
Bromobenzene ug/L 20 105 70-134106 020ND21.1 21.1
Bromochloromethane ug/L 20 97 70-146102 420ND19.5 20.4
Bromodichloromethane ug/L 20 99 70-138103 420ND19.9 20.6
Bromoform ug/L 20 104 57-138102 220ND20.9 20.5
Bromomethane ug/L v3208110-20082 220ND16.2 16.5
Carbon tetrachloride ug/L 20 107 70-147107 020ND21.5 21.5
Chlorobenzene ug/L 20 108 70-137104 420ND21.7 20.8
Chloroethane ug/L 20 116 51-166116 020ND23.2 23.1
Chloroform ug/L 20 99 70-14496 320ND19.9 19.2
Chloromethane ug/L 20 118 24-161118 020ND23.6 23.6
cis-1,2-Dichloroethene ug/L 20 107 67-148107 020ND21.3 21.4
cis-1,3-Dichloropropene ug/L 20 104 70-142105 120ND20.8 21.0
Dibromochloromethane ug/L 20 104 68-138102 220ND20.8 20.3
Dibromomethane ug/L 20 100 70-134101 120ND20.1 20.3
Dichlorodifluoromethane ug/L 20 123 43-155121 120ND24.6 24.3
Diisopropyl ether ug/L 20 104 65-146106 220ND20.7 21.1
Ethylbenzene ug/L 20 107 68-143105 220ND21.4 20.9
Hexachloro-1,3-butadiene ug/L 20 121 62-151117 320ND24.2 23.4
m&p-Xylene ug/L 40 107 53-157102 540ND42.6 40.6
Methyl-tert-butyl ether ug/L 20 98 59-156100 320ND19.6 20.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 125 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3666519MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92607618001
3666520
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 106 64-148107 120ND21.2 21.4
Naphthalene ug/L 20 109 57-150109 020ND21.7 21.7
o-Xylene ug/L 20 108 68-143103 520ND21.5 20.5
p-Isopropyltoluene ug/L 20 111 70-141109 220ND22.2 21.8
Styrene ug/L 20 109 70-136106 320ND21.7 21.1
Tetrachloroethene ug/L 20 111 70-139106 520ND22.2 21.2
Toluene ug/L 20 102 47-157105 320ND20.4 21.0
trans-1,2-Dichloroethene ug/L 20 108 70-149107 120ND21.6 21.4
trans-1,3-Dichloropropene ug/L 20 103 70-138103 020ND20.6 20.6
Trichloroethene ug/L 20 106 70-149107 120ND21.2 21.4
Trichlorofluoromethane ug/L 20 96 61-15494 320ND19.2 18.7
Vinyl acetate ug/L 40 103 48-156105 240ND41.2 41.8
Vinyl chloride ug/L 20 114 55-172117 220ND22.9 23.4
Xylene (Total)ug/L 60 107 66-145102 560ND64.1 61.1
1,2-Dichloroethane-d4 (S)%92 70-13094
4-Bromofluorobenzene (S)%99 70-13098
Toluene-d8 (S)%96 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702546
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493001, 92607493002, 92607493003, 92607493004, 92607493005
Parameter Units
Dup
Result QualifiersRPDResult
92606816001
3666452SAMPLE DUPLICATE:
Percent Moisture %24.9 N2626.3
Parameter Units
Dup
Result QualifiersRPDResult
92607777017
3666453SAMPLE DUPLICATE:
Percent Moisture %24.9 N2325.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 127 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702553
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493006, 92607493007, 92607493008, 92607493009, 92607493010, 92607493011, 92607493012,
92607493013, 92607493014, 92607493015, 92607493016, 92607493017, 92607493018, 92607493019,
92607493020, 92607493021, 92607493022, 92607493023, 92607493024, 92607493025
Parameter Units
Dup
Result QualifiersRPDResult
92607493006
3666478SAMPLE DUPLICATE:
Percent Moisture %11.9 N21013.2
Parameter Units
Dup
Result QualifiersRPDResult
92607493025
3666479SAMPLE DUPLICATE:
Percent Moisture %17.5 N2117.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 135
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92607493
BENMAR 897-05
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
702556
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92607493026, 92607493027, 92607493028
Parameter Units
Dup
Result QualifiersRPDResult
92607657001
3666499SAMPLE DUPLICATE:
Percent Moisture %14.3 N2713.3
Parameter Units
Dup
Result QualifiersRPDResult
92607883001
3666500SAMPLE DUPLICATE:
Percent Moisture %10.3 N2310
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 135
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92607493
BENMAR 897-05
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte is a possible laboratory contaminant (not present in method blank).C7
Common Laboratory Contaminant.C9
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 130 of 135
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92607493001 702338 702437GP-1 (8-12)EPA 5035A/5030B EPA 8260D
92607493002 702875 703058GP-3 (4-8)EPA 5035A/5030B EPA 8260D
92607493003 702338 702437GP-3 (8-12)EPA 5035A/5030B EPA 8260D
92607493004 702338 702437GP-4 (4-8)EPA 5035A/5030B EPA 8260D
92607493005 702338 702437GP-4 (8-12)EPA 5035A/5030B EPA 8260D
92607493006 702238 702277GP-5 (4-8)EPA 5035A/5030B EPA 8260D
92607493007 702338 702437GP-6 (4-8)EPA 5035A/5030B EPA 8260D
92607493008 702238 702277GP-7 (0-4)EPA 5035A/5030B EPA 8260D
92607493009 702338 702437GP-7 (4-8)EPA 5035A/5030B EPA 8260D
92607493010 702238 702277GP-8 (4-8)EPA 5035A/5030B EPA 8260D
92607493011 702338 702437GP-9 (0.5-4)EPA 5035A/5030B EPA 8260D
92607493012 702295 702296GP-9 (4-8)EPA 5035A/5030B EPA 8260D
92607493013 702295 702296GP-9 (8-12)EPA 5035A/5030B EPA 8260D
92607493014 702295 702296GP-2 (2)EPA 5035A/5030B EPA 8260D
92607493015 702038 702052GP-5 (8-12)EPA 5035A/5030B EPA 8260D
92607493016 702038 702052GP-6 (8-12)EPA 5035A/5030B EPA 8260D
92607493017 702038 702052GP-10 (8-12)EPA 5035A/5030B EPA 8260D
92607493018 702038 702052GP-11 (0-4)EPA 5035A/5030B EPA 8260D
92607493019 702038 702052GP-12 (4-8)EPA 5035A/5030B EPA 8260D
92607493020 702038 702052GP-13 (0-4)EPA 5035A/5030B EPA 8260D
92607493021 702038 702052GP-15 (0.5-4)EPA 5035A/5030B EPA 8260D
92607493022 702038 702052GP-16 (8-12)EPA 5035A/5030B EPA 8260D
92607493023 702295 702296GP-17 (4-8)EPA 5035A/5030B EPA 8260D
92607493024 702295 702296GP-17 (8-12)EPA 5035A/5030B EPA 8260D
92607493025 702295 702296GP-18 (4-8)EPA 5035A/5030B EPA 8260D
92607493026 702295 702296GP-19 (8-12)EPA 5035A/5030B EPA 8260D
92607493027 702818 702856GP-20 (4-8)EPA 5035A/5030B EPA 8260D
92607493028 702818 702856GP-20 (8-12)EPA 5035A/5030B EPA 8260D
92607493029 702561GP-3 EPA 8260D
92607493001 702546GP-1 (8-12)SW-846
92607493002 702546GP-3 (4-8)SW-846
92607493003 702546GP-3 (8-12)SW-846
92607493004 702546GP-4 (4-8)SW-846
92607493005 702546GP-4 (8-12)SW-846
92607493006 702553GP-5 (4-8)SW-846
92607493007 702553GP-6 (4-8)SW-846
92607493008 702553GP-7 (0-4)SW-846
92607493009 702553GP-7 (4-8)SW-846
92607493010 702553GP-8 (4-8)SW-846
92607493011 702553GP-9 (0.5-4)SW-846
92607493012 702553GP-9 (4-8)SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 131 of 135
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92607493
BENMAR 897-05
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92607493013 702553GP-9 (8-12)SW-846
92607493014 702553GP-2 (2)SW-846
92607493015 702553GP-5 (8-12)SW-846
92607493016 702553GP-6 (8-12)SW-846
92607493017 702553GP-10 (8-12)SW-846
92607493018 702553GP-11 (0-4)SW-846
92607493019 702553GP-12 (4-8)SW-846
92607493020 702553GP-13 (0-4)SW-846
92607493021 702553GP-15 (0.5-4)SW-846
92607493022 702553GP-16 (8-12)SW-846
92607493023 702553GP-17 (4-8)SW-846
92607493024 702553GP-17 (8-12)SW-846
92607493025 702553GP-18 (4-8)SW-846
92607493026 702556GP-19 (8-12)SW-846
92607493027 702556GP-20 (4-8)SW-846
92607493028 702556GP-20 (8-12)SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/13/2022 05:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 132 of 135
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P5ce Analyticar
CHAIN-OF-CUSTODY Analytical Request Document
Chain-of-Custody is a LEGAL DOCUMENT -Complete all relevent fields
Address: ~ l5 13rv...t.t.. /h.o""'-A} f{(J I ~::)I,J:;;, Zein.
Report To: ~ \ / 1 I Email To: {-/ 1 I<.. :c..<... -t Cl rho "' 0. rMo11 e.Ao./@ vc;. n v.:>, (.or.,
Copy To:
Customer Project Name/Number:
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Phone: 4-V~ l-~ t.-'1 f'ri!
Email: A 11_...., .P:'-1 ~
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F-1-.J<,. ~
Collected By (s~)l\lture): __, __ ...__ I' V--
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lspose as appropriate I I Return
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1 I Hold:
Site Collection lnfo/Add)ie!jS: L l 5 I S t: · t-t t C0".J ttMe-
State: County/City: Time Zone Collected:
f.J.C I ( IPT( IMT( ICT (lET
Site/Facility 10 II: ~r-..v Compliance ~rytoring?
[ I Yes ["f No
Purchase Order II: DWPWSIDII:
Quote II: OW Location Code:
Turnaround Date Required: Immediately Packed on Ice:
[ }!tes [ I No
Rush: Field Filtered (\{ a_pplicable):
( ) Yes ['(No ( ) Same Day [ I Next Day
[ 1 2 Day ( ] 3 Day [ I 4 Day [ I S Day , A 1 .
na YSIS: -------(Expedite Charges Apply)
LAB USE ONLY-Affix Workorder/1 n oin I ~hal ._.oro nr I ict P:aro W n rlt-nrl'lor N urnhor n r rWOI:92607493
container p~~~N~::~:e~' 1111111111111111111111
I I I I I 92607413 ~I
'• Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (O) Other
Analyses I Lab Profile/Line:
Lab sample Receipt Checkl ist :
Custody Seals Present/Intact Y N N.;
Custody Signatures Present t/N ir~
Collector Signature Present ~, N NA
Bottles Intact }?-N NA
Correct Bottles ~N NA
Sufficient Volume ~/'N NA
Samples Received on Ice ~ N NA
VOA -Beadspace Acceptable Y I_ NA
USD.A Regulated Soils Y j( NA
Samples in Holding Time )fN N~
Residual Chlorine Present Y N ~
Cl Strips: .. .1
Sampl e pH Acceptable Y N ~-
pH Strips: '/
Sulfide Present Y N J(A
--
---
* Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater {WW), ~ Lead Acetate Strips:
Product {P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue {TS), Bioassay (B), Vapor (V), Other (OT) ~
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Customer Remarks I Special Conditions I Possible Hazards: Type of Ice Used: t Blue Dry None SHORT HOLDS PRESENT (<72 hours): Y N N/A Lab Sample Temperature Info:
Packing Material Used: Lab Tracking II: Temp Blank Receiveq:'f Y N J*A"
R~,l.:any: (Si '
1
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V~~/&ce
Relinquished bY7€fT1Pany: (Signature)
y Samples received via:
FEDEX UPS Radchem sample(s) screened (<500 cpm): N NA
Date/Time: Received by/Company: (Signature) Date/Time:
lt;;h/z.7 ~:
fi~;e:
2 616 3 2 9 Therm 1011: ~lJ7)6 ~ (r 4,
Cooler 1 Temp Upon Receipd-6 1 6o't1 '
Client Courier Pa~r
MTJL LAB'USE ONLY
PB:
Cooler 1 Therm Corr. Factor: _{)_,Q_oc
Cooler 1 Corrected Temp: oC
Comments: ~ 0 I {).b 1 {). 4
~--------------------1 Trip Blank Received: Y N NA
HCL MeOH TSP Other
Non Conforma'Y(s): I Page: __ _
YES I )10 of: __ _
Pa
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~ CHAIN-OF-CUSTODY Analytical Request Document
'ace Analyticar
Chain-of-Custody is a LEGAL DOCUMENT-Complete all rei event fields
Company:
t-1 a. r """ol'\ ~ v :r ~n ""'t...-,.h_ I
Billing Information:
s aM.R..
Address:(, / ~ pn,...u.. 1hot~A J
ReportTo:1( ,0 \<. l-+a.l'thD/' Email To: {_1 1 ,..~(1\""'c;v, ~v tP \.fo... ...... o. vo,-.
Copy To: Site Co[le&):ionj[lfo/Ajld(esr C: I :> !::1 A' e~.?~"'-o..
Customer Project Name/Number: State: County/City: Time Zone Collected: Y '(), OS (\I.e_ / [ 1 PT [ 1 MT [ 1 CT [ 1 ET
Phone: 1 .:l<.{ • J q').-'-{ f:'):Z I Site/Facility 10 II: f)
Email: ~I\ M e. r
Compliance Monitoring?
[ 1 Yes [)(No
Collected By (print): 12_, l-1 Ci IYvln ~
C~gn~
~ample Disposal:
(\4 Dispose as appropriate [ I Return
[ I Archive:------
[ ) Hold:
Purchase Order II: DWPWSIDII:
Quote II: OW Location Code:
Turnaround Date Required: Immediately Packed on Ice:
(;CJ Yes [ 1 No
Rush: Field Filtered (if applicable):
[ 1 Same Day [ 1 Next Day [ 1 Yes [ )J:No
[ 1 2 Day [ 1 3 Day [ 1 4 Day [ 1 5 Day , 1 .
Ana ySIS: -------(Expedite Charges Apply)
• Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue [TS), Bioassay [B), Vapor (V), Other (OT)
LAB USE ONLY-Affix Workorder/Login label Here or list Pace Workorder Number or
MTWOI : 92607 493
All SHADED J p": ATF Due Data : 06/09/22
n Container Preservative Typi'"" CLIENT: 92-Hal"'mon En
I I I I I
• • Preservative Types: (1) nitric acid, (2) sulfuric acie;., . , ., _ .............. , .... v ... •uc, \..JJ~:nlt.. dCetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (O) Other
Analyses I Lab Profile/Line:
0
-....9
Lab Sample Receipt Checklist:
Custody Seals Present/Intact Y N NA
Custody Signatures Present Y N NA
Collector Signature Present Y N NA
Bottles I ntact Y N NA
Correct Bottles Y N NA
Sufficient Volume Y N NA
Samples Received on I ce Y N NA
VOA -Headspace Acceptable Y N NA
USDA Regulated Soils Y N NA
Samples in Holding Time Y N NA
Residual Chlorine Present Y N NA
Cl Strips:
Sample pH Acceptable Y N NA
pR Strips:
Sulfide Present Y N NA
Lead Acetate Strips:
LAB USE ONLY:
--
--
Customer Sample ID Matrix •
Comp/
Grab
Collected (or
Composite Start) Composite End Res I" of I "' Cl Ctns ~
Lab Sample# I Comments :
t,z)61t/~) Date Time Date Time
S" /J I I): oo ~ o.o (}~'11/ Ot\ -) /3 ( l>:oc, .:l G.--f., l... PPW f"ll-t-
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Nc I .. ~one I SHORT HOLDS PRESENT (<72 hours): Y N N/A I Lab Sample Temperature Info:
Temp Blank Received: Y N NA
Customer Remarks I Special Conditions I Possible Hazards:
Packing Material Used:
Radchem sample(s) screened (<500 cpm): y N
Date/Time: Received by/Company: (Signature)
~~~~!e:
C-/z/zz ~
082.~
/1 z.o
NA
Lab Tracking II: 2616330
Samples received via:
FEDEX UPS Client Courier Pace Courier
Date/Time: MTJL LAB USE ONLY
Table II:
Therm ID/1: -------­
Cooler 1 Tem p Upon Receipt: __ oC
Cooler 1 Therm Corr. Factor: ___ oC
Cooler 1 Corrected Temp: oC
Comments:
~~r"'-.!::=-......!;<4.!.!:....LJAcctnum: 1
Template: Trip Blank Received: Y N NA
~--=:..L-!:::.....!:::::....J....:,__:::~Prelogin: HCL MeOH TSP Other
Non Conformance(s): l Page: __ _
YES/¢' of: __
PM:
PB:
Pa
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~ CHAIN-OF-CUSTODY Analytical Request Document
Pace Analytical"
Chain-of-Custody is a LEGAL DOCUMENT-Complete all rei event fields
Company:
H G. r ~"""-£"" v ~ r-o f) rYl e,... b.l
Billing Information:
Sv-h~ Address:(, 15 l)r'-'C.R. -(h or-..t>J 'f2 d
Report To: {( ;,c,_k 1--l ovA Of'\, Email To: /-1 1
cdtl-'l::>(l el\ v (;) v o..i'\oo-( ofl'\
Copy To: Site Collection lnfo..{A.ddr~ss: 5"/ <) £, /-1-lc..!::H~fr'l &l..
Customer Project Name/Number: State: County/City: Time Zone Collected:
<?'9 1 -0 5 tJ_c_ I [ I PT [ I MT I I CT I I ET
Phone: I 0 \f -). '\ ~ ~
Email: 4.521
Site/Facility 10 11:;,
l>er. ""oV
Compliance Monitoring?
I I Yes [~]No
Collected By (print):
"Q • 1.-lC\.rn ol\
Purchase Order II:
Quote#:
OW PWSID tl:
OW Location Code:
Immediately Packed on Ice:
~Yes I I No
:% (s~:::_ !Turnaround Date Required:
!sample Disposal: Rush:
[ 1 Dispose as appropriate [ 1 Return I I Same Day [ I Next Day
Field Filtered (if applicable):
[ ) Yes [>;l'No
[ I Archive: I I 2 Day [ ) 3 Day I ) 4 Day [ I 5 Day . [ I Hold: (Expedite Charges Apply) I Analysis:--------
• Matrix Codes (Insert in Matrix box below): Drinking Water (OW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
LAB USE ONLY· Affix Workorder/Looin t :~hoi ~oro nr I ict D::aro Wnrl,nrrlor Nuft'lh.or n r
MT WOI : 92607 493
All SHADED A Pl'l: ATF Due Date : 06/09/22
]_J_
Container Preservative Type.. CLIENT : 92-Harmon En
I I I I I
• • Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (O) Other
Analyses
0
v
Lab Profile/Line:
Lab Sample Receipt Checklist:
Custody Seals Present/Intact Y N NA
Custody Signatures Present Y N NA
Collector Signature Present Y N NA
Bottles Intact Y N NA
Corr ect Bottles Y N NA
Sufficient Volume Y N NA
Samples Received on Ice Y N NA
VOA -Beadspace Acceptable Y N NA
USDA Regulated Soils Y N NA
Samples in Holding Time Y N NA
Residual Chlori ne Present Y N NA
Cl Strips:
Sample pH Acceptable Y N NA
pH Strips :
Sulfide Present Y N NA
Lead Acetate Strips:
LAB USE ONLY:
--
Lab Sample# I Comments:
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Cl Ctns ~ . Comp I I Collected (or
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Com osite End Customer Sample ID I Matnx • I Grab Compos1te Start) P
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Date Time j Date j Time
(;-p_ 11 (0 -4) 5 L c; (. t lo ;J~
G?-15 (o, ~-'l) SL c; Cl I to ;<..(~
G?-t c (~-IJ .. ) 5 L 6 (, I I u :J.s
61->-\l ('-l -q ) S L 6 t:, lt ;so
c~, \} -l--, ( '?-, ;). ) S L 6 (!; I tL . 5'.>
a-. 0 Y.J • .-4v ~""t...\
LJ.t!ll~t>/V./ D~'L
L<il tJ gl'/'l-/ ()l..~
,bP •~fO~...J o-itl (; ?-I <? { l f-X') s l 6 ~ I I ).: o :2 CJ. ()I P.-JrU 0'->
6?-1<1 (¥-11) s (_ 6 c. I IJ ·,)a l (/' t1 /rf tVJ ().J..b...
6 ~ :ttl L 4 ,£-.J Sl q ' I L>'·Li&" ;), 1 '2 tl :f. J?fJ ,-1J 011
0P -?-o C~-t :l.) )L (") ,,, i l !'( (, l. .?/, 5 j}J],.-./ 1:)2.~
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Customer Remarks I Special Conditions 1 Possible Hazards: Type of Ice Used: Wet Blue Dry None SHORT HOLDS PRESENT (<72 hours): Y N N/A Lab Sample Temperature Info:
1~d~anv, 'r f:;>v;~
Relinquished by/Comp ny: (Signature)
Packing Material Used: Lab Tracking tl: Temp Blank Received: Y N NA
2616 3 31 ThermiD#: ___ _
Radchem sample(s) screened (<500 cpm): Y N NA
Date/Time:
~e: c:~~~
oate'/Time:
Received by/Company: (Signature)
t/1z.{
//:2/)
Cooler 1 Temp Upon Receipt: __ oc
Samples received via: Cooler 1 Therm Corr. Factor: ___ oC
FEDEX UPS Client Courier Pace Courier Cooler 1 Corrected Temp: ____ oC
Date/Time: MTJL LAB USE ONLY Comments:
~ /) L ([fz.t; I Table tl: ~Zm% ~Acctn=:--um· --~ t.ao (.__ ( ( J:;:;:~ r--;;ri;;IB;,;F~:::-:;-:---::-----~1
PM:
PB:
Trip Blank Received: Y N NA
HCL MeOH TSP Other
Non Conformance(s): I Page: __ _
YES I pi6 of: __