IH1587_2022-01-25_PROGR_Fromer Danalex Sub-Slab Vapor Sampling Report

Sub-Slab Vapor Sampling Report
Former Danalex Facility
515 E. Alabama Avenue
Bessemer City, North Carolina
Prepared for:
Benmar Properties, LLC-Property Owner
c/o John Griffing
Griffing Leaser, PLLC
518 S. Hope Road
Gastonia, North Carolina 28054
Prepared by:
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, North Carolina 28112
704-292-4527
harmonenvironmental.com
Project 897-02
January 25, 2022
Richard L. Harmon, P. G.
President/Principal Hydrogeologist
Section
Sub-Slab Vapor Sampling Report
Former Dana/ex Facility
515 E. Alabama Avenue
Bessemer City, North Carolina
Table of Contents
Introduction ............................................................................................................................. 1
Sub-Slab Vapor Point Locations and Installation Procedures ............................................ ]
Sub-Slab Vapor Point Leak Testing Procedures ................................................................. 1
Sub-Slab Vapor Point Sample Procedures .......................................................................... 2
Analytical Results and Conclusions ..................................................................................... 6
List of Figures
Figure 1 Site Location Map
Figure 2 Sub-Slab Vapor Sample Locations
List of Tables
Table 1 Sub-Slab Vapor Point Vacuum Testing Results
Table 2 Field Measurements During Sub-Slab Vapor Sampling Activities
Table 3 Sub-Slab Vapor Sample Analytical Results
List of Attachments
Attachment A Analytical Results and Chain-of-Custody Records
i •
Introduction
Sub-Slab Vapor Sampling Report
Former Dana/ex Facility
515 E. Alabama Avenue
Bessemer City, Nortlz Carolina
In November 2021, Harmon Environmental, PA initiated a Phase I Environmental
Assessment of the industrial/commercial facility at 515 E. Alabama Avenue in Bessemer
City, North Carolina. Information collected during this assessment indicated that
tetrachloroethene had historically been detected in soil samples collected from beneath the
floor slab in this facility. Based on the historical findings, Harmon Environmental, P A
recommended sub-slab vapor samples be collected to evaluate the potential for vapor
intrusion.
On January 5, 2022 Harmon Environmental, PA personnel advanced ten sub-slab vapor
sampling points at the former Danalex facility. Figure 1 depicts the location of the site on
an excerpt of a United Stated Geologic Survey (USGS) topographic map of the region.
Figure 2 depicts the approximate locations of the sampling points on a map depicting the
layout of the building and property.
Soil Vapor Sampling Point Locations and Installation Procedures
On January 5, 2022 ten sampling points were advanced through the concrete floor slab and
sampled at the former Danalex facility at the approximate locations depicted on Figure 2.
Each boring was advanced into the concrete floor to a depth of approximately 1 inch using
a l-inch diameter drill bit. The borings were then extended through the remainder ofthe
concrete slab using a 0.25-inch diameter drill bit into the gravel material beneath the slab.
A 0.25-inch diameter polyethylene tube was inserted through the slab and a hydrated
bentonite clay seal was compacted into the l-inch diameter outer hole to seal the point.
Sample point construction details are presented in Table 1.
Sub-Slab Vapor Point Leak Testing Procedures
On January 5, 2022 Harmon Environmental, PA personnel leak tested each of the three
sampling points with helium in general accordance with Vapor Intrusion Pathway: A
Practical Guideline, published by the Interstate Technology and Regulatory Council in
January 2007. These tests consisted of constructing a tent of polyethylene sheeting over
each sample point and inflating the tent with helium gas. A Dielectric MGD 2002 Helium­
Hydrogen Detector (SIN 42201) was utilized to verify the helium concentration within the
tent. After in;flating and measuring the helium concentration within each tent, the helium
gas detector was connected to each sampling point to measure the helium concentration
Attorney-Client Privileged Work Product
Sub-Slab Vapor Sampling Report
Former Dana/ex Facility
January 25, 2022
1 Harmon Environmental, P A
615 Bruce Thomas Road
Monroe, North Carolina
[e-mail]
beneath the slab. The helium testing results are summarized on Table 1. As indicated in
Table 1, the ten sub-slab vapor sampling points passed the leak test protocol.
Sub-Slab Vapor Point Sample Procedures
Following the completion of satisfactory leak testing, Harmon Environmental, PA
personnel sampled each of the ten sub-slab vapor sampling points. Sample point P-1 was
purged of approximately 300 milliliters (ml) of air using a 60 ml syringe. The extraction
rate was maintained at less than 200 milliliters per minute (ml/min). Following completion
of the purging process, a Suma® 1liter vacuum canister (ID Number 3763) was connected
to sample point P-1. Sampling was initiated at 12:55. The initial vacuum measured on the
canister regulator was 29.5 inches of Mercury (in Hg). The vacuum was applied to sample
point P-1 until 13:01 at which time the canister regulator reported 5 in Hg of vacuum
remaining. The temperature and barometric pressure measured in the vicinity of the
canister at the time of the test are presented on Table 2.
Sample point P-2 was initially purged of approximately 300 ml of air using a 60 ml syringe.
The extraction rate was maintained at less than 200 ml/min. Following completion of the
purging process, a Suma® 1liter vacuum canister (ID Number 3722) was connected to the
sample point and sampling was initiated at 13:06. The initial vacuum measured on the
canister regulator was 26 in Hg. The vacuum was applied to sample point P-2 until13:23
at which time the canister regulator reported 5 in Hg of vacuum remaining. The
temperature and barometric pressure measured in the vicinity of the canister at the time of
the test are presented on Table 2.
Sample point P-3 was purged of approximately 300 ml of air using a 60 ml syringe. The
extraction rate was maintained at less than 200 ml/min. Following completion of the
purging process, a Suma® 1 liter vacuum canister (ID Number 1457) was connected to the
sample point and the sampling was initiated at 13: 17. The initial vacuum measured on the
canister regulator was 30 in Hg. The vacuum was applied to sample point P-3 until13:23
at which time the canister regulator reported 5 in Hg of vacuum remaining. The
temperature and barometric pressure measured in the vicinity of the canister at the time of
the test are presented on Table 2.
Sample point P-4 was purged of approximately 300 ml of air using a 60 ml syringe. The
extraction rate was maintained at less than 200 ml/min. Following completion of the
purging process, a Suma® 1 liter vacuum canister (ID Number 3262) was connected to the
sample point and the sampling was initiated at 13:29. The initial vacuum measured on the
canister regulator was 30 in Hg. The vacuum was applied to sample point P-4 until13:36
at which time the canister regulator reported 5 in Hg of vacuum remaining. The
temperature and barometric pressure measured in the vicinity of the canister at the time of
the test are presented on Table 2.
Attorney-Client Privileged Work Product
Sub-Slab Vapor Sampling Report
Former Danalex Facility
January 25, 2022
2 Harmon Environmental, P A
615 Bruce Thomas Road
Monroe, North Carolina
[e-mail]
Sample point P-5 was purged of approximately 300 ml of air using a 60 ml syringe. The
extraction rate was maintained at less than 200 ml/min. Following completion of the
purging process, a Suma® 1liter vacuum canister (ID Number 3793) was connected to the
sample point and the sampling was initiated at 13:41. The initial vacuum measured on the
canister regulator was 29 in Hg. The vacuum was applied to sample point P-5 until13:47
at which time the canister regulator reported 5 in Hg of vacuum remaining. The
temperature and barometric pressure measured in the vicinity of the canister at the time of
the test are presented on Table 2.
Sample point P-6 was purged of approximately 300 ml of air using a 60 ml syringe. The
extraction rate was maintained at less than 200 ml/min. Following completion of the
purging process, a Suma® 1 liter vacuum canister (ID Number 2995) was connected to the
sample point and the sampling was initiated at 13:51. The initial vacuum measured on the
canister regulator was 29 in Hg. The vacuum was applied to sample point P-6 until 13:57
at which time the canister regulator reported 5 in Hg of vacuum remaining. The
temperature and barometric pressure measured in the vicinity of the canister at the time of
the test are presented on Table 2.
Sample point P-7 was purged of approximately 300 ml of air using a 60 ml syringe. The
extraction rate was maintained at less than 200 ml/min. Following completion of the
purging process, a Suma® 1liter vacuum canister (ID Number 3780) was connected to the
sample point and the sampling was initiated at 14:02. The initial vacuum measured on the
canister regulator was 30 in Hg. The vacuum was applied to sample point P-7 until13:09
at which time the canister regulator reported 5 in Hg of vacuum remaining. The
temperature and barometric pressure measured in the vicinity of the canister at the time of
the test are presented on Table 2.
Sample point P-8 was purged of approximately 300 ml of air using a 60 ml syringe. The
extraction rate was maintained at less than 200 ml/min. Following completion of the
purging process, a Suma® 1 liter vacuum canister (ID Number 2846) was connected to the
sample point and the sampling was initiated at 14:13. The initial vacuum measured on the
canister regulator was 30 in Hg. The vacuum was applied to sample point P-8 until 14:31
at which time the canister regulator reported 5 in Hg of vacuum remaining. The
temperature and barometric pressure measured in the vicinity of the canister at the time of
the test are presented on Table 2.
Sample point P-9 was purged of approximately 300 ml of air using a 60 ml syringe. The
extraction rate was maintained at less than 200 ml/min. Following completion of the
purging process, a Suma® 1 liter vacuum canister (ID Number 2422) was connected to the
sample point and the sampling was initiated at 14:25. The initial vacuum measured on the
canister regulator was 29 in Hg. The vacuum was applied to sample point P-9 until 14:31
at which time the canister regulator reported 5 in Hg of vacuum remaining. The
temperature and barometric pressure measured in the vicinity of the canister at the time of
the test are presented on Table 2.
Attorney-C!ilmt Privileged Work Product
Sub-Slab Vapor Sampling Report
Former Dana/ex Facility
January 25, 2022
3 Harnzon Environmental, P A
615 Bruce Thomas Road
Monroe, North Carolina
harmonenv@yahoo. com
Sample point P-1 0 was purged of approximately 300 ml of air using a 60 ml syringe. The
extraction rate was maintained at less than 200 ml/min. Following completion of the
purging process, a Suma® 1liter vacuum canister (ID Number 3251) was connected to the
sample point and the sampling was initiated at 14:36. The initial vacuum measured on the
canister regulator was 29 in Hg. The vacuum was applied to sample point P-1 0 until14:42
at which time the canister regulator reported 5 in Hg of vacuum remaining. The
temperature and barometric pressure measured in the vicinity of the canister at the time of
the test are presented on Table 2.
Analytical Results and Conclusions
Table 3 presents the soil vapor concentrations detected in samples collected from beneath
the slab at the former Danalex facility compared with the Sub-Slab and Exterior Soil Gas
Screening Levels (SGSL) as defined by the North Carolina Department of Environmental
Quality (DEQ) in June 2021. As indicated in this table, tetrachloroethene concentrations
collected from sub-slab vapor sample points P-2, P-3, P-6, P-7 and P-8 exceeded the Non­
Residential SGSLs. Further, the concentration of 1,1,2-trichloroethane detected in the sub­
slab vapor sample collected from point P-2 and concentration oftrichloroethene in the sub­
slab vapor samples collected from points P-2, P-3 and P-8 exceeded the respective Non­
Residential SGSLs.
When the NCDEQ June 2021 Risk Based Calculator was applied to the sub-slab vapor
analytical results associated with sample point P-2, the results indicate the detected
concentrations exceed acceptable risk levels for Non-Residential Workers within the
facility.
Attorney-Client Privileged Work Product
Sub-Slab Vapor Sampling Report
Former Dana/ex Facility
January 25, 2022
4 Harmon Environmental, P A
615 Bruce Thomas Road
Monroe, North Carolina
[e-mail]
Figures
SOURCE: TOPOl 2003 NATIONAL CiE'OCiRA"PHlC
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE. NORTH CAROLINA
704-292-4527
hannonenvironmental.com
APPROXIMATE SCAlE IN FEET
L..__ __ l __ _
0 2000
FIGURE I
SITE t.OCAnON MAP
FORMER OANALEX FACILnY SITE
515 E. ALABAMA AVENUE
BESSEMER CllY. NORTH CAROLINA
SOURCE, GASTON COUNTY GIS
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE. NORTH CAROLINA 28112
704-292-4527
harmonenvironmental.com
APPROXIMATE SCALE IN FEET
0 100
FIGURE 2
SUB-SOIL VAPOR SAMPLE LOCATIONS
FORMER DANALEX FACILITY SITE
515 E. ALABAMA AVENUE
BESSEMER CITY. NORTH CAROLINA
200
Tables
Sample
Point Installation Date Time
Bentonite Seal
Depth
Floor
Thickness Leak Testing Date Time
Helium
Concentation in
Tent
Helium
Concentration
Sample Tube
P-1 January 5, 2022 9:25 1-inch 5-inches January 5, 2022 11:30 12.9% 0.0 ppmv
P-2 January 5, 2022 9:43 1-inch 6-inches January 5, 2022 11:41 81% 0.0 ppmv
P-3 January 5, 2022 9:52 1-inch 6-inches January 5, 2022 11:45 10.2% 0.0 ppmv
P-4 January 5, 2022 10:06 1-inch 6-inches January 5, 2022 12:01 2.3% 0.0 ppmv
P-5 January 5, 2022 10:17 1-inch 6-inches January 5, 2022 12:04 7.2% 0.0 ppmv
P-6 January 5, 2022 10:24 1-inch 5-inches January 5, 2022 12:08 2.6% 0.0 ppmv
P-7 January 5, 2022 10:34 1-inch 6-inches January 5, 2022 12:12 2.7% 0.0 ppmv
P-8 January 5, 2022 10:50 1-inch 9-inches January 5, 2022 12:16 3.1% 0.0 ppmv
P-9 January 5, 2022 11:00 1-inch 6-inches January 5, 2022 12:20 3.4% 0.0 ppmv
P-10 January 5, 2022 11:10 1-inch 6-inches January 5, 2022 12:24 2.7% 0.0 ppmv
Notes: Vacuum Testing Conducted By Harmon Environmental, PA personnel using a Dielectric MGD 2002
Helium-Hydrogen Detecctor (S/N 42201)
ppmv = parts per million by volume
Table 1
Sub-Slab Vapor Point Vacuum Testing Results
Former Danalex Facility
515 E. Alabama Avenue
Project No. 897-02
Bessemer City, North Carolina
Temperature Barometric Pressure
(ºC) (in Hg)
P-1 12:55-13:01 14.6 28.93
P-2 13:06-13:12 15.4 28.92
P-3 13:17-13:23 14.3 28.91
P-4 13:29-13:36 14.1 28.91
P-5 13:41-13:47 13.2 28.90
P-6 13:52-13:57 13.2 28.89
P-7 14:02-14:09 14.3 28.88
P-8 14:13-14:20 14.3 28.88
P-9 14:25-14:31 14.5 28.87
P-10 14:36-14:42 14.9 28.87
Notes: Temperature and barometric pressure readings
collected by Harmon Environmental, PA personnel using
Mannix Digital Pocket Weatherman SAM700BAR
Sample Point Time
Table 2
Field Measurements During Sub-Slab Vapor Sampling Activities
January 5, 2022
Project No. 897-02
Bessemer City, North Carolina
Former Danalex Facility
515 E. Alabama Avenue
Constituent
ug/M3
acetone 220000 2700000 59.2 359 44.7 242 17.5 27.3 25.2 122 84.4 81.0
benzene 12 160 3.02 69.6 12.5 <1.19 <1.15 <1.15 <1.11 8.15 <1.19 1.42
carbon disulfide 4900 61000 8.78 6.57 8.19 <1.16 4.30 <1.12 27.4 9.99 <1.16 <1.16
carbon tetrachloride 16 200 <2.27 17.3 <2.12 <2.36 <2.27 <2.27 <2.19 <2.19 <2.36 <2.36
chloromethane 630 7900 2.23 2.09 2.89 <0.772 <0.744 2.46 0.962 2.03 0.834 2.60
chlorobenzene 350 4400 <1.66 373 19.8 <1.73 <1.66 <1.66 <1.61 <1.61 <1.73 <1.73
chloroform 4.1 53 <1.75 3860 35.4 <1.82 <1.75 <1.75 <1.69 <1.69 <1.82 <1.82
1,2-dichloroethane 3.6 47 <1.46 26.3 <1.36 <1.51 <2.16 <1.46 <1.41 <1.41 <1.51 <1.51
1,1-dichloroethane 58 770 <1.44 266 153 <1.50 <1.44 <1.44 <1.39 1.41 <1.50 <1.50
1,1-dichloroethene 1400 18000 <1.43 3020 152 <1.48 <1.43 <1.43 <1.38 71.3 <1.48 <1.48
cis-1,2-dichloroethene 3.40 1170 62200 84.4 <1.43 2.24 1.60 147 3.04 19.4
trans-1,2-dichloroethene 280 3500 <1.43 426 979 1.53 <1.43 <1.43 <1.38 4.16 <1.48 <1.48
1,4-dioxane 19 250 <1.30 <1.30 4.04 <1.35 <1.30 <1.30 <1.25 3.18 <1.35 <1.35
ethanol 65.0 70.5 72.6 253 50.7 23.2 33.6 153 58.4 42.8
ethylbenzene 37 490 3.98 <78.0 2.25 1.73 <1.56 <1.56 <1.51 1.63 <1.62 2.07
4-ethyltoluene 2.96 <88.3 1.68 3.59 <1.77 <1.77 <1.71 <1.71 <1.84 <1.84
trichlorofluoromethane 13.5 36.5 13.4 6.91 5.84 12.5 19.8 20.7 20.3 8.54
dichlorodifluoromethane 700 8800 3.06 3.50 3.09 3.29 3.07 3.08 3.18 3.16 3.47 3.26
n-heptane 2800 35000 8.02 <1.47 <1.37 <1.53 <1.47 <1.47 <3.88 <1.42 <1.53 4.29
n-hexane 4900 61000 4.12 111 <3.74 <4.16 <3.98 <3.98 <8.92 <3.88 <4.16 <4.16
methylene chloride 3400 53000 3.68 127 <1.17 <1.30 <1.25 <1.25 <1.21 3.27 1.86 4.97
2-butanone 35000 440000 7.02 <6.63 <6.19 29.3 <6.63 <6.63 <6.43 <6.43 9.11 9.44
methyl-tert-butyl ether 360 4700 <1.30 <1.30 <1.21 21.0 <1.30 <1.30 <1.25 3.75 <1.35 <1.35
2-propanol 18.4 33.9 <5.16 101 12.1 7.74 7.23 41.0 16.9 25.1
styrene 7000 88000 2.88 <76.6 4.38 3.94 2.82 4.59 3.86 3.16 3.30 3.86
tetrachloroethene 280 3500 132 3380000 242000 355 41.5 14600 22900 44300 1740 1090
toluene 35000 440000 94.9 82.9 52.4 6.55 <3.39 12.9 18.6 58.8 16.9 106
1,1,1-trichloroethane 35000 440000 <1.96 772 135 <2.03 <1.96 10.3 53.8 9.79 6.09 <2.03
1,1,2-trichloroethane 1.4 18 <1.96 543 <1.83 <2.03 <1.96 <1.96 <1.89 <1.89 <2.03 <2.03
trichloroethene 14 180 25.1 44000 31500 44.3 2.23 10.2 224 3900 171 60.0
1,2,4-trimethylbenzene 420 5300 3.77 <420 3.63 5.50 <1.77 <1.77 <1.71 <1.71 <1.84 <1.84
vinyl chloride 5.6 280 <0.920 30.9 178 <0.956 <0.920 <0.920 <0.890 <0.890 <0.956 <0.956
2,2,4-trimethylpentane <1.68 <1.68 <1.57 <1.75 <1.68 <1.68 <1.71 <1.63 <1.75 9.90
m&p-xylenes 700 8800 16.4 <156 8.24 5.64 <3.12 3.14 3.13 6.85 <3.24 8.97
o-xylenes 700 8800 5.68 <78.0 3.21 1.91 <1.56 <1.56 <1.51 2.14 <1.62 2.99
Samples collected by Harmon Environmental, PA on January 5, 2022 and analyzed by Pace Analytical Services.
Only compounds detected in the samples are presented herein. For a complete list of analytes, please refer to the analytical report.
ug/m3 = micrograms per cubic meter
SGSL = Soil Gas Screening Level as updated by the NCDEQ in June 2021
SGSLs based on Carcenigentic Screening Level of 1.0E-6 and Hazard Quotient of 0.2 (n)
Table 3
Former Danalex Facility
Sub-Slab Vapor Sample Analytical Results
515 E. Alabama Avenue, Bessemer City, North Carolina
Project No. 897-02
P-10P-9P-8P-7P-6P-5P-4P-3P-2P-1Residential SGSL Non-Residential SGSL
Attachment A
Analytical Results and
Chain-of-Custody Records
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
January 21 , 2022
Mr. Rick Harmon
Harmon Environmental
615 Bruce Thomas Road
Monroe, NC 28112
RE: Project: BENMAR 897-03
Pace Project No.: 92582172
Dear Mr. Harmon:
Enclosed are the analytical results for sample(s) received by the laboratory on January 11 , 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National -Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
~Y¥""'-
Tyler Forney
tyler. [e-mail]
(704 )875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
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REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
{704)875-9092
Page 2 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Lab 1D Sample 10
92582172001 P-1 #3763
92582172002 P-2 #3722
92582172003 P-3 #1457
92582172004 P-4 #3262
92582172005 P-5 #3793
92582172006 P-6 #2995
92582172007 P-7 #3780
92582172008 P-8 #2846
92582172009 P-9 #2422
92582172010 P-10 #3251
PAN = Pace National-Mt. Juliet
SAMPLE ANALYTE COUNT
Method
T0-15
T0-15
T0-15
T0-15
T0-15
T0-15
T0-15
T0-15
T0-15
T0-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analysts
CEP
CEP
CEP
CEP
CEP
CEP
CEP
CEP
CEP
CEP
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Analytes
Reported Laboratory
68 PAN
68 PAN
68 PAN
68 PAN
68 PAN
68 PAN
68 PAN
68 PAN
68 PAN
68 PAN
Page 3 of 41
SU~MARY OF DETECTION
Project: BEN MAR 897-03
Pace Project No.: 92582172
Lab Sample ID Client Sample ID
Method Parameters Result Units
92582172001 P-1 #3763
T0-15 Acetone 59.2 ug/m3
T0-15 Benzene 3.02 ug/m3
T0-15 Carbon disulfide 8.78 ug/m3
T0-15 Chloromethane 2.23 ug/m3
T0-15 cis-1,2-Dichloroethene 3.40 ug/m3
T0-15 Ethanol 65.0 ug/m3
T0-15 Ethylbenzene 3.98 ug/m3
T0-15 4-Ethyltoluene 2.96 ug/m3
T0-15 Trichlorofluoromethane 13.5 ug/m3
T0-15 Dichlorodifluoromethane 3.06 ug/m3
T0-15 n-Heptane 8.02 ug/m3
T0-15 n-Hexane 4.12 ug/m3
T0-15 Methylene Chloride 3.68 ug/m3
T0-15 2-Butanone (MEK) 7.02 ug/m3
T0-15 2-Propanol 18.4 ug/m3
T0-15 Styrene 2.88 ug/m3
T0-15 Tetrachloroethene 132 ug/m3
T0-15 Toluene 94.9 ug/m3
T0-15 Trichloroethene 25.1 ug/m3
T0-15 1,2,4-Trimethylbenzene 3.77 ug/m3
T0-15 m&p-Xylene 16.4 ug/m3
T0-15 a-Xylene 5.68 ug/m3
92582172002 P-2 #3722
T0-15 Acetone 359 ug/m3
T0-15 Benzene 69.6 ug/m3
T0-15 Carbon disulfide 6.57 ug/m3
T0-15 Carbon tetrachloride 17.3 ug/m3
T0-15 Chlorobenzene 373 ug/m3
T0-15 Chloroform 3860 ug/m3
T0-15 Chloromethane 2.09 ug/m3
T0-15 1,2-Dichloroethane 26.3 ug/m3
T0-15 1,1-Dichloroethane 266 ug/m3
T0-15 1,1-Dichloroethene 3020 ug/m3
T0-15 cis-1 ,2-Dichloroethene 1170 ug/m3
T0-15 trans-1 ,2-Dichloroethene 424 ug/m3
T0-15 Ethanol 70.5 ug/m3
T0-15 Trichlorofluoromethane 36.5 ug/m3
T0-15 Dichlorodifluoromethane 3.50 ug/m3
T0-15 n-Hexane 111 ug/m3
T0-15 Methylene Chloride 127 ug/m3
T0-15 2-Propanol 33.9 ug/m3
T0-15 Tetrachloroethene 3380000 ug/m3
T0-15 Toluene 82.9 ug/m3
T0-15 1,1 ,1-Trichloroethane 772 ug/m3
T0-15 1 ,1,2-Trichloroethane 543 ug/m3
T0-15 Trichloroethene 44000 ug/m3
T0-15 Vinyl chloride 30.9 ug/m3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Report Limit
5.35
1.15
1.12
0.744
1.43
4.24
1.56
1.77
2.02
1.78
1.47
3.98
1.25
6.63
5.53
1.53
2.44
3.39
1.93
1.77
3.12
1.56
5.35
1.15
1.12
2.27
1.66
87.6
0.744
1.46
1.44
71 .3
71 .3
1.43
4.24
2.02
1.78
3.98
1.25
5.53
13600
3.39
97.9
97.9
1930
0.920
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Analyzed Qualifiers
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/2216:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 16:59
01/18/22 17:35
01/18/22 17:35
01/18/22 17:35
01/18/22 17:35
01/18/22 17:35
01/19/22 16:24
01/18/22 17:35
01/18/22 17:35
01/18/22 17:35
01/19/22 16:24
01/19/22 16:24
01/18/22 17:35
01/18/22 17:35
01/18/22 17:35
01/18/22 17:35
01/18/22 17:35
01/18/22 17:35
01/18/22 17:35
01/21/22 11:57
01/18/22 17:35
01/19/22 16:24
01/19/22 16:24
01/20/22 17:45
01/18/22 17:35
Page 4 of 41
SUMMARY OF DETECTION
Project: BEN MAR 897-03
Pace Project No.: 92582172
Lab Sample ID Client Sample ID
Method Parameters Result Units
92582172003 P-3 #1457
T0-15 Acetone 44.7 ug/m3
T0-15 Benzene 12.5 ug/m3
T0-15 Carbon disulfide 8.19 ug/m3
T0-15 Chlorobenzene 19.8 ug/m3
T0-15 Chloroform 35.4 ug/m3
T0-15 Chloromethane 2.89 ug/m3
T0-15 1, 1-Dichloroethane 153 ug/m3
T0-15 1, 1-Dichloroethene 152 ug/m3
T0-15 cis-1 ,2-Dichloroethene 62200 ug/m3
T0-15 trans-1 ,2-Dichloroethene 979 ug/m3
T0-15 1 ,4-Dioxane (p-Dioxane) 4.04 ug/m3
T0-15 Ethanol 72.6 ug/m3
T0-15 Ethylbenzene 2.25 ug/m3
T0-15 4-Ethyltoluene 1.68 ug/m3
T0-15 Trichlorofluoromethane 13.4 ug/m3
T0-15 Dichlorodifluoromethane 3.09 ug/m3
T0-15 Styrene 4.38 ug/m3
T0-15 Tetrachloroethene 242000 ug/m3
T0-15 Toluene 52.4 ug/m3
T0-15 1,1, 1-Trichloroethane 135 ug/m3
T0-15 Trichloroethene 31500 ug/m3
T0-15 1 ,2,4-Trimethylbenzene 3.63 ug/m3
T0-15 Vinyl chloride 178 ug/m3
T0-15 m&p-Xylene 8.24 ug/m3
T0-15 o-Xylene 3.21 ug/m3
92582172004 P-4 #3262
T0-15 Acetone 242 ug/m3
T0-15 cis-1 ,2-Dichloroethene 84.4 ug/m3
T0-15 trans-1 ,2-Dichloroethene 1.53 ug/m3
T0-15 Ethanol 253 ug/m3
T0-15 Ethyl benzene 1.73 ug/m3
T0-15 4-Ethyltoluene 3.59 ug/m3
T0-15 Trichlorofluoromethane 6.91 ug/m3
T0-15 Dichlorodifluoromethane 3.29 ug/m3
T0-15 2-Butanone (MEK) 29.3 ug/m3
T0-15 Methyl-tert-butyl ether 21 .0 ug/m3
T0-15 2-Propanol 101 ug/m3
T0-15 Styrene 3.94 ug'/m3
T0-15 Tetrachloroethene 355 ug/m3
T0-15 Toluene 6.55 ug/m3
T0-15 Trichloroethene 44.3 ug/m3
T0-15 1 ,2,4-Trimethylbenzene 5.50 ug/m3
T0-15 m&p-Xylene 5.64 ug/m3
T0-15 o-Xylene 1.91 ug/m3
92582172005 P-5 #3793
T0-15 Acetone 17.5 ug/m3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Report Limit
4.99
1.07
1.05
1.55
1.64
0.694
1.35
1.33
666
66.6
1.21
3.96
1.46
1.65
1.89
1.66
1.43
1140
3.16
1.83
90.0
1.65
0.859
2.91
1.46
5.56
1.48
1.48
4.41
1.62
1.84
2.10
1.85
6.90
1.35
5.75
1.59
2.54
3.52
2.00
1.84
3.24
1.62
5.35
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Analyzed Qualifiers
01/18/22 18:11
01/18/2218:11
01/18/2218:11
01/18/22 18:11
01/18/2218:11
01/18/22 18:11
01/18/22 18:11
01/18/22 18:11
01/20/22 18:20
01/19/22 17:02
01/18/2218:11
01/18/2218:11
01/18/22 18:11
01/18/2218:11
01/18/22 18:11
01/18/22 18:11
01/18/2218:11
01/20/22 18:20
01/18/22 18:11
01/18/2218:11
01/19/22 17:02
01/18/22 18:11
01/18/22 18:11
01/18/22 18:11
01/18/2218:11
01/18/22 18:46
01/19/22 17:46
01/19/22 17:46
01/18/22 18:46
01/18/22 18:46
01/18/22 18:46
01/18/22 18:46
01/18/22 18:46
01/18/22 18:46
01/18/22 18:46
01/18/22 18:46
01/18/22 18:46
01/19/22 17:46
01/18/22 18:46
01/19/22 17:46
01/18/22 18:46
01/18/22 18:46
01 /18/22 18:46
01/18/22 19:20
Page 5 of 41
SUMMARY OF DETECTION
Project: BEN MAR 897-03
Pace Project No.: 92582172
Lab Sample ID Client Sample ID
Method Parameters Result Units
92582172005 P-5 #3793
T0-15 Carbon disulfide 4.30 ug/m3
T0-15 Ethanol 50.7 ug/m3
T0-15 Trichlorofluoromethane 5.84 ug/m3
T0-15 Dichlorodifluoromethane 3.07 ug/m3
T0-15 2-Propanol 12.1 ug/m3
T0-15 Styrene 2.82 ug/m3
T0-15 Tetrachloroethene 41 .5 ug/m3
T0-15 Trichloroethene 2.23 ug/m3
92582172006 P-6 #2995
T0-15 Acetone 27.3 ug/m3
T0-15 Chloromethane 2.46 ug/m3
T0-15 cis-1 ,2-Dichloroethene 2.24 ug/m3
T0-15 Ethanol 23.2 ug/m3
T0-15 Trichlorofluoromethane 12.5 ug/m3
T0-15 Dichlorodifluoromethane 3.08 ug/m3
T0-15 2-Propanol 7.74 ug/m3
T0-15 Styrene 4.59 ug/m3
T0-15 Tetrachloroethene 14600 ug/m3
T0-15 Toluene 12.9 ug/m3
T0-15 1,1, 1-Trichloroethane 10.3 ug/m3
T0-15 Trichloroethene 10.2 ug/m3
T0-15 m&p-Xylene 3.14 ug/m3
92582172007 P-7 #3780
T0-15 Acetone 25.2 ug/m3
T0-15 Carbon disulfide 27.4 ug/m3
T0-15 Chloromethane 0.962 ug/m3
T0-15 cis-1 ,2-Dichloroethene 1.60 ug/m3
T0-15 Ethanol 33.6 ug/m3
T0-15 Trichlorofluoromethane 19.8 ug/m3
T0-15 Dichlorodifluoromethane 3.18 ug/m3
T0-15 2-Propanol 7.23 ug/m3
T0-15 Styrene 3.86 ug/m3
T0-15 Tetrachloroethene 22900 ug/m3
T0-15 Toluene 18.6 ug/m3
T0-15 1,1, 1-Trichloroethane 53.8 ug/m3
T0-15 Trichloroethene 224 ug/m3
T0-15 m&p-Xylene 3.13 ug/m3
92582172008 P-8 #2846
T0-15 Acetone 122 ug/m3
T0-15 Benzene 8.15 ug/m3
T0-15 Carbon disulfide 9.99 ug/m3
T0-15 Chloromethane 203 ug/m3
T0-15 1, 1-Dichloroethane 1.41 ug/m3
T0-15 1 , 1-Dichloroethene 71 .3 ug/m3
T0-15 cis-1 ,2-Dichloroethene 147 ug/m3
T0-15 trans-1 ,2-Dichloroethene 4.16 ug/m3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Report Limit
1.12
4.24
2.02
1.78
5.53
1.53
2.44
1.93
5.35
0.744
1.43
4.24
2.02
1.78
5.53
1.53
48.9
3.39
1.96
1.93
3.12
5.18
1.08
0.719
1.38
4.11
1.96
1.72
5.36
1.48
47.3
3.28
1.89
1.86
3.02
5.18
1.11
1.08
0.719
1.39
1.38
1.38
1.38
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Analyzed Qualifiers
01/18/22 19:20
01/18/22 19:20
01/18/22 19:20
01/18/22 19:20
01/18/22 19:20
01/18/22 19:20
01/19/22 18:27
01/19/22 18:27
01/18/22 19:59
01/18/22 19:59
01/18/22 19:59
01/18/22 19:59
01 /18/22 19:59
01/18/22 19:59
01/18/22 19:59
01/18/22 19:59
01/20/22 18:56
01/18/22 19:59
01/18/22 19:59
01/18/22 19:59
01/18/22 19:59
01/18/22 20:35
01/18/22 20:35
01/18/22 20:35
01/18/22 20:35
01/18/22 20:35
01/18/22 20:35
01/18/22 20:35
01/18/22 20:35
01/18/22 20:35
01/19/22 19:44
01/18/22 20:35
01/18/22 20:35
01/18/22 20:35
01/18/22 20:35
01/18/22 21 :12
01/18/22 21:12
01/18/22 21:12
01/18/22 21 :12
01 /18/22 21 :12
01/18/22 21 :12
01/18/22 21 :12
01/18/22 21 :12
Page 6 of 41
SUMMARY OF DETECTION
Project: BEN MAR 897-03
Pace Project No.: 92582172
Lab Sample ID Client Sample ID
Method Parameters Result Units
92582172008 P-8 #2846
T0-15 1 ,4-Dioxane (p-Dioxane) 3.18 ug/m3
T0-1 5 Ethanol 153 ug/m3
T0-15 Ethylbenzene 1.63 ug/m3
T0-15 Trichlorofluoromethane 20.7 ug/m3
T0-15 Dichlorodifluoromethane 3.16 ug/m3
T0-15 Methylene Chloride 3.27 ug/m3
T0-15 Methyl-tert-butyl ether 3.75 ug/m3
T0-15 2-Propanol 41.0 ug/m3
T0-15 Styrene 3.16 ug/m3
T0-15 Tetrachloroethene 44300 ug/m3
T0-15 Toluene 58.8 ug/m3
T0-1 5 1,1, 1-Trichloroethane 9.79 ug/m3
T0-15 Trichloroethene 3900 ug/m3
T0-1 5 m&p-Xylene 6.85 ug/m3
T0-15 o-Xylene 2.14 ug/m3
92582172009 P-9 #2422
T0-15 Acetone 84.4 ug/m3
T0-15 Chloromethane 0.834 ug/m3
T0-15 cis-1 ,2-Dichloroethene 3.04 ug/m3
T0-15 Ethanol 58.4 ug/m3
T0-15 Trichlorofluoromethane 20.3 ug/m3
T0-15 Dichlorodifluoromethane 3.47 ug/m3
T0-15 Methylene Chloride 1.86 ug/m3
T0-15 2-Butanone (MEK) 9.11 ug/m3
T0-15 2-Propanol 16.9 ug/m3
T0-15 Styrene 3.30 ug/m3
T0-15 Tetrachloroethene 1740 ug/m3
T0-15 Toluene 16.9 ug/m3
T0-15 1,1, 1-Trichloroethane 6.09 ug/m3
T0-15 Trichloroethene 171 ug/m3
92582172010 P-10 #3251
T0-15 Acetone 81 .0 ug/m3
T0-15 Benzene 1.42 ug/m3
T0-15 Chloromethane 2.60 ug/m3
T0-15 cis-1 ,2-Dichloroethene 19.4 ug/m3
T0-15 Ethanol 42.8 ug/m3
T0-15 Ethyl benzene 2.07 ug/m3
T0-15 Trichlorofluoromethane 8.54 ug/m3
T0-15 Dichlorodifluoromethane 3.26 ug/m3
T0-15 n-Heptane 4.29 ug/m3
T0-15 Methylene Chloride 4.97 ug/m3
T0-15 2-Butanone (MEK) 9.44 ug/m3
T0-15 2-Propanol 25.1 ug/m3
T0-15 Styrene 3.86 ug/m3
T0-15 Tetrachloroethene 1090 ug/m3
T0-15 Toluene 106 ug/m3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC.
Report Limit
1.25
4.11
1.51
1.96
1.72
1.21
1.25
5.36
1.48
236
3.28
1.89
186
3.02
1.51
5.56
0.772
1.48
4.41
2.10
1.85
1.30
6.90
5.75
1.59
25.4
3.52
2.03
2.00
5.56
1.19
0.772
1.48
4.41
1.62
2.10
1.85
1.53
1.30
6.90
5.75
1.59
2.54
3.52
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 }875-9092
Analyzed Qualifiers
01/18/22 21 :12
01/18/22 21 :12
01 /18/22 21 :12
01/18/22 21 :12
01/18/22 21:12
01/18/22 21:12
01/18/22 21:12
01/18/22 21 :12
01/18/22 21 :12
01/20/22 19:31
01/18/22 21 :12
01/1 8/22 21 :12
01/20/22 19:31
01/18/22 21 :12
01/18/22 21:12
01/18/22 21:49
01/18/22 21:49
01/18/22 21 :49
01/18/22 21:49
01/18/22 21 :49
01 /18/22 21 :49
01/18/22 21:49
01/18/22 21:49
01/18/22 21 :49
01 /18/22 21 :49
01/19/22 21 :01
01/1 8/22 21 :49
01/18/22 21 :49
01/18/22 21 :49
01/1 8/22 22:27
01/18/22 22:27
01/18/22 22:27
01/18/22 22:27
01/18/22 22:27
01/18/22 22:27
01/18/22 22:27
01/18/22 22:27
01 /18/22 22:27
01 /18/22 22:27
01/18/22 22:27
01/18/22 22:27
01/1 8/22 22:27
01/18/22 22:27
01/1 8/22 22:27
Page 7 of 41
Project:
Pace Project No.:
Lab Sample ID
Method
92582172010
T0-15
T0-15
T0-15
T0-15
SUMMARY OF DETECTION
BEN MAR 897-03
92582172
Client Sample ID
Parameters Result Units
P-10 #3251
Trichloroethene 60.0 ug/m3
2,2,4-Trimethylpentane 9.90 ug/m3
m&p-Xylene
a-Xylene
8.97 ug/m3
2.99 ug/m3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC.
Report Limit
2.00
1.75
3.24
1.62
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Analyzed Qualifiers
01/18/22 22:27
01/18/22 22:27
01/18/22 22:27
01/18/22 22:27
Page 8 of41
PROJECT NARRATIVE
Project: BENMAR 897-03
Pace Project No.: 92582172
Date: January 21,2022
P-2 #3722 (Lab 10: 92582172002)
• Volatile Organic Compounds (MS) by Method T0-15-Surrogate failure due to matrix interference
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Page 9 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Method: T0-15
Description: VOA (MS) T0-15
Client: Harmon Environmental
Date: January 21,2022
General Information:
PROJECT NARRATIVE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
10 samples were analyzed for T0-15 by Pace National Mt. Juliet. All samples were received in acceptable condition with any
exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this
report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 1804677
LO: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
• LCS (Lab ID: R3751728-1)
• 1 A-Dichlorobenzene
• LCSD (Lab ID: R3751728-2)
• 1 A-Dichlorobenzene
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Sample: P-1 #3763
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
B romodich lorometha ne
Bromoform
Bromomethane
1,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethane
1 ,1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
1 ,4-Dioxane (p-Dioxane)
Ethanol
Ethyl benzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1 , 1 ,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab 10: 92582172001 Collected: 01/05/22 13:01 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
59.2
ND
3.02
ND
ND
ND
ND
NO
8.78
ND
ND
ND
ND
2.23
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.40
ND
ND
ND
ND
ND
65.0
3.98
2.96
13.5
3.06
ND
ND
8.02
ND
4.12
ND
3.68
ND
7.02
ND
ND
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
5.35 1.8
1.13 1.8
1.15 1.8
1.87 1.8
2.41 1.8
11.2 1.8
1.40 1.8
7.97 1.8
1.12 1.8
2.27 1.8
1.66 1.8
0.950 1.8
1.75 1.8
0.744 1.8
1.86 1.8
1.24 1.8
3.06 1.8
2.77 1.8
2.16 1.8
2.16 1.8
2.16 1.8
1.46 1.8
1.44 1.8
1.43 1.8
1.43 1.8
1.43 1.8
1.66 1.8
1.63 1.8
1.63 1.8
1.30 1.8
4.24 1.8
1.56 1.8
1.77 1.8
2.02 1.8
1.78 1.8
2.76 1.8
2.52 1.8
1.47 1.8
12.1 1.8
3.98 1.8
1.77 1.8
1.25 1.8
9.20 1.8
6.63 1.8
9.21 1.8
1.47 1.8
Prepared Analyzed CAS No.
01/18/22 16:59 01/18/2216:59 67-64-1
01/18/2216:59 01/18/2216:59 107-05-1
01/18/2216:59 01 /1 8/2216:59 71-43-2
01/1 8/2216:59 01 /18/2216:59 100-44-7
01/18/22 16:59 01/18/2216:59 75-27-4
01/18/2216:59 01/18/2216:59 75-25-2
01/1 8/22 16:59 01/18/2216:59 74-83-9
01/1 8/2216:59 01/18/2216:59 106-99-0
01/1 8/221 6:59 01/18/2216:59 75-15-0
01/18/22 16:59 01/18/22 16:59 56-23-5
01/18/22 16:59 01/18/2216:59 108-90-7
01/18/22 16:59 01/18/221 6:59 75-00-3
01/18/22 16:59 01/18/2216:59 67-66-3
01/18/22 16:59 01/18/2216:59 74-87-3
01/18/22 16:59 01/18/22 16:59 95-49-8
01/18/22 16:59 01/18/2216:59 110-82-7
01 /18/22 16:59 01/18/2216:59 124-48-1
01/1 8/22 16:59 01/18/2216:59 106-93-4
01/18/22 16:59 01/18/2216:59 95-50-1
01/18/22 16:59 01/18/2216:59 541-73-1
01/18/22 16:59 01/18/2216:59 106-46-7
01/18/22 16:59 01/18/2216:59 107-06-2
01/18/22 16:59 01/18/22 16:59 75-34-3
01/18/22 16:59 01 /18/2216:59 75-35-4
01/18/22 16:59 01/18/22 16:59 156-59-2
01/18/22 16:59 01/18/22 16:59 156-60-5
01/18/22 16:59 01 /18/2216:59 78-87-5
01/18/22 16:59 01/18/22 16:59 10061-01-5
01/18/22 16:59 01 /18/2216:59 10061-02-6
01/18/22 16:59 01/18/22 16:59 123-91-1
01/18/221 6:59 01/18/2216:59 64-17-5
01/18/22 16:59 01/1 8/2216:59 100-41-4
01/18/22 16:59 01/18/22 16:59 622-96-8
01/18/22 16:59 01/1 8/2216:59 75-69-4
01 /18/22 16:59 01/18/2216:59 75-71-8
01 /18/22 16:59 01/18/2216:59 76-13-1
01 /18/22 16:59 01/18/221 6:59 76-14-2
01/18/22 16:59 01/18/2216:59 142-82-5
01 /1 8/22 16:59 01/18/2216:59 87-68-3
01 /18/22 16:59 01/18/2216:59 110-54-3
01 /18/22 16:59 01 /18/2216:59 98-82-8
01 /18/22 16:59 01 /18/2216:59 75-09-2
01 /18/22 16:59 01/18/2216:59 591-78-6
01/18/22 16:59 01/18/2216:59 78-93-3
01/1 8/22 16:59 01 /18/2216:59 108-10-1
01/18/22 16:59 01 /18/22 16:59 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC. Page 11 of41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Sample: P-1 #3763
Parameters
VOA (MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1 ,2,4-Trichlorobenzene
1, 1,1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
1 ,2,4-Trimethylbenzene
1 ,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1,4-Dichlorobenzene-d4 (IS)
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab ID: 92582172001 Collected: 01/05/22 13:01 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
ND ug/m3 1.30 1.8 01/18/22 16:59
ND ug/m3 5.92 1.8 01/18/22 16:59
18.4 ug/m3 5.53 1.8 01/18/22 16:59
ND ug/m3 3.87 1.8 01/18/22 16:59
2.88 ug/m3 1.53 1.8 01/1 8/22 16:59
ND ug/m3 2.47 1.8 01/18/22 16:59
132 ug/m3 2.44 1.8 01/18/22 16:59
ND ug/m3 1.06 1.8 01/18/22 16:59
94.9 ug/m3 3.39 1.8 01/18/22 16:59
ND ug/m3 8.37 1.8 01/1 8/22 16:59
ND ug/m3 1.96 1.8 01/18/22 16:59
ND ug/m3 1.96 1.8 01/18/22 16:59
25.1 ug/m3 1.93 1.8 01/18/22 16:59
3.77 ug/m3 1.77 1.8 01 /18/22 16:59
ND ug/m3 1.77 1.8 01 /18/221 6:59
ND ug/m3 1.68 1.8 01 /18/22 16:59
ND ug/m3 0.920 1.8 01 /18/22 16:59
ND ug/m3 1.57 1.8 01/18/22 16:59
ND ug/m3 1.27 1.8 01/18/22 16:59
16.4 ug/m3 3.12 1.8 01/18/22 16:59
5.68 ug/m3 1.56 1.8 01/18/22 16:59
98.2 % 60.0-140 1.8 01/1 8/22 16:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01/18/22 16:59 1634-04-4
01 /1 8/22 16:59 91-20-3
01/18/2216:59 67-63-0
01/18/22 16:59 115-07-1
01/18/22 16:59 100-42-5
01/18/22 16:59 79-34-5
01/1 8/22 16:59 127-18-4
01/1 8/22 16:59 109-99-9
01/18/2216:59 108-88-3
01/18/2216:59 120-82-1
01/18/2216:59 71-55-6
01/18/22 16:59 79-00-5
01/18/22 16:59 79-01-6
01/18/22 16:59 95-63-6
01/18/22 16:59 108-67-8
01/18/2216:59 540-84-1
01/18/2216:59 75-01-4
01/18/22 16:59 593-60-2
01/18/22 16:59 108-05-4
01/18/22 16:59 179601-23-1
01/18/2216:59 95-47-6
01/18/22 16:59 3855-82-1
Page12of41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Sample: P-2 #3722
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1 ,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
1 ,2-Dichloroethane
1, 1-Dichloroethane
1 , 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1,3-Dichloropropene
1 ,4-Dioxane (p-Dioxane)
Ethanol
Ethylbenzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1,1 ,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab ID: 92582172002 Collected: 01/05/22 13:12 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
359
ND
69.6
ND
ND
ND
ND
ND
6.57
17.3
373
ND
3860
2.09
ND
ND
ND
ND
ND
ND
ND
26.3
266
3020
1170
424
ND
ND
ND
ND
70.5
ND
ND
36.5
3.50
ND
ND
ND
NO
111
ND
127
ND
NO
ND
ND
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
5.35 1.8
1.13 1.8
1.15 1.8
93.5 90
2.41 1.8
559 90
1.40 1.8
7.97 1.8
1.12 1.8
2.27 1.8
1.66 1.8
0.950 1.8
87.6 90
0.744 1.8
92.8 90
1.24 1.8
3.06 1.8
2.77 1.8
108 90
108 90
108 90
1.46 1.8
1.44 1.8
71.3 90
71.3 90
1.43 1.8
1.66 1.8
1.63 1.8
1.63 1.8
1.30 1.8
4.24 1.8
78.0 90
88.3 90
2.02 1.8
1.78 1.8
2.76 1.8
2.52 1.8
1.47 1.8
605 90
3.98 1.8
88.5 90
1.25 1.8
9.20 1.8
6.63 1.8
9.21 1.8
1.4 7 1.8
Prepared Analyzed CAS No.
01/18/22 17:35 01/18/2217:35 67-64-1
01/18/22 17:35 01/18/2217:35 107-05-1
01/18/22 17:35 01/18/2217:35 71-43-2
01/19/22 16:24 01/19/2216:24 100-44-7
01/18/22 17:35 01/18/22 17:35 75-27-4
01/19/22 16:24 01/19/22 16:24 75-25-2
01/18/22 17:35 01/18/2217:35 74-83-9
01/18/22 17:35 01/18/2217:35 106-99-0
01/18/2217:35 01/18/2217:35 75-15-0
01/18/2217:35 01/18/2217:35 56-23-5
01/18/2217:35 01/18/2217:35 108-90-7
01/18/22 17:35 01/18/22 17:35 75-00-3
01/19/22 16:24 01/19/22 16:24 67-66-3
01/18/22 17:35 01/18/22 17:35 74-87-3
01/19/22 16:24 01/19/22 16:24 95-49-8
01/18/2217:35 01/18/2217:35 110-82-7
01/18/2217:35 01/18/2217:35 124-48-1
01/18/22 17:35 01/18/2217:35 106-93-4
01/19/2216:24 01/19/2216:24 95-50-1
01/19/22 16:24 01/19/2216:24 541-73-1
01/19/2216:24 01/19/2216:24 106-46-7 LO
01/18/22 17:35 01/18/2217:35 107-06-2
01/18/22 17:35 01/18/22 17:35 75-34-3
01 /19/2216:24 01/19/2216:24 75-35-4
01/19/2216:24 01/19/2216:24 156-59-2
01/18/22 17:35 01/18/22 17:35 156-60-5
01/18/22 17:35 01/18/22 17:35 78-87-5
01/18/22 17:35 01/18/2217:35 10061 -01-5
01/18/2217:35 01/18/22 17:35 10061-02-6
01/18/2217:35 01/18/2217:35 123-91-1
01/18/22 17:35 01/18/2217:35 64-17-5
01/19/22 16:24 01/19/2216:24 100-41-4
01/19/22 16:24 01/19/22 16:24 622-96-8
01/18/2217:35 01/18/2217:35 75-69-4
01/18/2217:35 01/18/2217:35 75-71-8
01/18/2217:35 01/18/2217:35 76-13-1
01/18/22 17:35 01/18/2217:35 76-14-2
01/18/22 17:35 01/18/22 17:35 142-82-5
01/19/22 16:24 01/19/22 16:24 87-68-3
01/18/22 17:35 01/18/22 17:35 110-54-3
01/19/22 16:24 01/19/22 16:24 98-82-8
01/18/22 17:35 01/18/2217:35 75-09-2
01/18/22 17:35 01/18/22 17:35 591-78-6
01/18/2217:35 01/18/2217:35 78-93-3
01/18/2217:35 01/18/2217:35 108-10-1
01/18/2217:35 01/18/2217:35 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 13 of 41
fhe~Pf.!£~·
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-2 #3722
Parameters
VOA (MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1 ,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
1 ,2,4-Trimethylbenzene
1 ,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1 ,4-Dichlorobenzene-d4 (IS)
1 ,4-Dichlorobenzene-d4 (IS)
1 ,4-Dichlorobenzene-d4 (IS)
1 ,4-Dichlorobenzene-d4 (IS)
Date: 01/21/2022 02:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
ANALYTICAL RESULTS
Lab 10: 92582172002 Collected: 01/05/22 13:12 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
NO ug/m3 1.30 1.8 01/18/22 17:35
NO ug/m3 297 90 01/19/22 16:24
33.9 ug/m3 5.53 1.8 01/18/22 17:35
NO ug/m3 3.87 1.8 01/18/22 17:35
NO ug/m3 76.6 90 01/19/22 16:24
NO ug/m3 124 90 01/19/22 16:24
3380000 ug/m3 13600 10000 01/21 /22 11 :57
NO ug/m3 1.06 1.8 01 /18/22 17:35
82.9 ug/m3 3.39 1.8 01 /18/22 17:35
NO ug/m3 420 90 01 /19/22 16:24
772 ug/m3 97.9 90 01/19/22 16:24
543 ug/m3 97.9 90 01 /19/22 16:24
44000 ug/m3 1930 1800 01 /20/22 17:45
NO ug/m3 88.3 90 01/19/22 16:24
NO ug/m3 88.3 90 01/19/22 16:24
NO ug/m3 1.68 1.8 01/1 8/22 17:35
30.9 ug/m3 0.920 1.8 01/18/22 17:35
NO ug/m3 1.57 1.8 01/18/22 17:35
NO ug/m3 1.27 1.8 01/18/22 17:35
NO ug/m3 156 90 01/19/22 16:24
NO ug/m3 78.0 90 01/1 9/22 16:24
2.27 % 60.0-140 1.8 01/18/22 17:35
106 % 60.0-140 90 01/19/22 16:24
90.7 % 60.0-140 1800 01/20/22 17:45
89.2 % 60.0-140 10000 01/21/22 11:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01 /1 8/22 17:35 1634-04-4
01 /19/2216:24 91-20-3
01/18/22 17:35 67-63-0
01/18/22 17:35 115-07-1
01/19/2216:24 100-42-5
01/19/2216:24 79-34-5
01/21/22 11:57 127-18-4
01/18/221 7:35 109-99-9
01/18/22 17:35 108-88-3
01/19/22 16:24 120-82-1
01/19/22 16:24 71-55-6
01/19/22 16:24 79-00-5
01/20/22 17:45 79-01-6
01/19/2216:24 95-63-6
01/19/2216:24 108-67-8
01/18/22 17:35 540-84-1
01/18/2217:35 75-01-4
01/18/22 17:35 593-60-2
01 /18/2217:35 108-05-4
01 /19/221 6:24 179601-23-1
01 /19/22 16:24 95-47-6
01/18/22 17:35 3855-82-1 SR
01 /19/22 16:24 3855-82-1
01/20/22 17:45 3855-82-1
01 /21/2211 :57 3855-82-1
Page 14 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Sample: P-3 #1457
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromo methane
1 ,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
1 ,2-Dichloroethane
1, 1-Dichloroethane
1,1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethanol
Ethylbenzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1,1 ,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01/21/2022 02:42 PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab ID: 92582172003 Collected: 01 /05/22 13:23 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -MI. Juliet
44.7
ND
12.5
ND
ND
ND
ND
ND
8.19
ND
19.8
ND
35.4
2.89
ND
ND
ND
ND
ND
ND
ND
ND
153
152
62200
979
ND
ND
ND
4.04
72.6
2.25
1.68
13.4
3.09
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
4.99 1.68
1.05 1.68
1.07 1.68
1.75 1.68
2.25 1.68
10.5 1.68
1.30 1.68
7.43 1.68
1.05 1.68
2.12 1.68
1.55 1.68
0.886 1.68
1.64 1.68
0.694 1.68
1.73 1.68
1.16 1.68
2.86 1.68
2.58 1.68
2.02 1.68
2.02 1.68
2.02 1.68
1.36 1.68
1.35 1.68
1.33 1.68
666 840
66.6 84
1.55 1.68
1.53 1.68
1.53 1.68
1.21 1.68
3.96 1.68
1.46 1.68
1.65 1.68
1.89 1.68
1.66 1.68
2.58 1.68
2.35 1.68
1.37 1.68
11.3 1.68
3.74 1.68
1.65 1.68
1.17 1.68
8.59 1.68
6.19 1.68
8.60 1.68
1.38 1.68
Prepared Analyzed CAS No.
01/18/2218:11 01/18/2218:11 67-64-1
01/18/22 18:11 01/18/22 18:11 107-05-1
01/18/2218:11 01/18/2218:11 71-43-2
01/18/2218:11 01/18/2218:11 100-44-7
01/18/22 18:11 01/18/2218:11 75-27-4
01/18/2218:11 01/18/2218:11 75-25-2
01/18/22 18:11 01/18/2218:11 74-83-9
01/18/22 18:11 01/18/2218:11 106-99-0
01/18/22 18:11 01/18/2218:11 75-15-0
01/18/22 18:11 01/18/2218:11 56-23-5
01/18/22 18:11 01/18/2218:11 108-90-7
01 /18/2218:11 01/18/2218:11 75-00-3
01 /18/2218:11 01/1 8/2218:11 67-66-3
01 /18/2218:11 01/18/2218:11 74-87-3
01/18/22 18:11 01/18/22 18:11 95-49-8
01/18/22 18:11 01/18/2218:11 110-82-7
01/18/22 18:11 01/18/22 18:11 124-48-1
01/18/2218:11 01/18/2218:11 106-93-4
01/18/2218:11 01/18/2218:11 95-50-1
01/18/2218:11 01/18/2218:11 541-73-1
01/18/2218:11 01/18/2218:11 106-46-7
01/18/22 18:11 01/18/2218:11 107-06-2
01/18/22 18:11 01/18/2218:11 75-34-3
01/18/22 18:11 01 /18/2218:11 75-35-4
01/20/22 18:20 01/20/22 18:20 156-59-2
01/19/22 17:02 01/19/22 17:02 156-60-5
01/18/22 18:11 01/18/2218:11 78-87-5
01/18/22 18:11 01/18/2218:11 10061-01-5
01/18/22 18:11 01/18/2218:11 10061-02-6
01/18/22 18:11 01/18/2218:11 123-91 -1
01/18/2218:11 01/18/2218:11 64-17-5
01/18/2218:11 01 /18/2218:11 100-41-4
01/18/2218:11 01/18/2218:11 622-96-8
01/18/2218:11 01/18/2218:11 75-69-4
01/18/2218:11 01/18/2218:11 75-71-8
01/18/2218:11 01/18/2218:11 76-13-1
01/18/22 18:11 01 /18/2218:11 76-14-2
01/18/22 18:11 01/18/2218:11 142-82-5
01/18/2218:11 01/18/2218:11 87-68-3
01/18/2218:11 01/18/2218:11 110-54-3
01/18/22 18:11 01/18/22 18:11 98-82-8
01/18/2218:11 01/18/2218:11 75-09-2
01/18/2218:11 01/18/2218:11 591-78-6
01/18/22 18:11 01/18/2218:11 78-93-3
01/18/2218:11 01/18/2218:11 108-10-1
01/18/22 18:11 01/18/2218:11 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC. Page 15 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Sample: P-3 #1457
Parameters
VOA (MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1 ,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
1 ,2,4-Trimethylbenzene
1 ,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1.4-Dichlorobenzene-d4 (IS)
1 ,4-Dichlorobenzene-d4 (IS)
1.4-Dichlorobenzene-d4 (IS)
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab ID: 92582172003 Collected: 01/05/22 13:23 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
NO ug/m3 1.21 1.68 01/18/22 18:11
NO ug/m3 5.55 1.68 01/18/22 18:11
NO ug/m3 5.16 1.68 01/18/22 18:11
NO ug/m3 3.62 1.68 01/18/22 18:11
4.38 ug/m3 1.43 1.68 01/18/22 18:11
NO ug/m3 2.31 1.68 01/18/22 18:11
242000 ug/m3 1140 840 01/20/22 18:20
NO ug/m3 0.991 1.68 01/18/22 18:11
52.4 ug/m3 3.16 1.68 01/18/22 18:11
NO ug/m3 7.85 1.68 01/18/22 18:11
135 ug/m3 1.83 1.68 01/18/22 18:11
NO ug/m3 1.83 1.68 01/18/22 18:11
31500 ug/m3 90.0 84 01/19/22 17:02
3.63 ug/m3 1.65 1.68 01/18/22 18:11
NO ug/m3 1.65 1.68 01/18/2218:11
NO ug/m3 1.57 1.68 01/18/22 18:11
178 ug/m3 0.859 1.68 01/18/22 18:11
NO ug/m3 1.47 1.68 01/18/2218:11
NO ug/m3 1.18 1.68 01/18/22 18:11
8.24 ug/m3 2.91 1.68 01/18/22 18:11
3.21 ug/m3 1.46 1.68 01/18/22 18:11
97.5 % 60.0-140 1.68 01/18/22 18:11
104 % 60.0-140 84 01/19/22 17:02
92.1 % 60.0-140 840 01/20/22 18:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01/18/2218:11 1634-04-4
01/18/22 18:11 91-20-3
01/18/2218:11 67-63-0
01/18/2218:11 115-07-1
01/18/2218:11 100-42-5
01/18/2218:11 79-34-5
01/20/22 18:20 127-18-4
01/18/22 18:11 109-99-9
01/18/22 18:11 108-88-3
01/18/22 18:11 120-82-1
01/18/2218:11 71-55-6
01/18/22 18:11 79-00-5
01/19/2217:02 79-01-6
01/18/2218:11 95-63-6
01/18/2218:11 108-67-8
01/18/22 18:11 540-84-1
01/18/22 18:11 75-01-4
01/18/2218:11 593-60-2
01/18/2218:11 108-05-4
01/18/22 18:11 179601-23-1
01/18/2218:1 1 95-47-6
01/18/22 18:11 3855-82-1
01/19/22 17:02 3855-82-1
01/20/22 18:20 3855-82-1
Page 16 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-4 #3262
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1 ,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
1 ,2-Dichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
1 ,4-Dioxane (p-Dioxane)
Ethanol
Ethylbenzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1,1 ,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab 10: 92582172004 Collected: 01/05/22 13:36 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF Prepared Analyzed CAS No. ------------------------------
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
242
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
84.4
1.53
ND
ND
ND
ND
253
1.73
3.59
6.91
3.29
ND
ND
ND
ND
ND
ND
ND
ND
29.3
ND
ND
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
5.56 1.87
1.17 1.87
1.19 1.87
1.94 1.87
2.51 1.87
11 .6 1.87
1.45 1.87
8.28 1.87
1.16 1.87
2.36 1.87
1.73 1.87
0.987 1.87
1.82 1.87
0.772 1.87
1.93 1.87
1.29 1.87
3.18 1.87
2.88 1.87
2.25 1.87
2.25 1.87
2.25 1.87
1.51 1.87
1.50 1.87
1.48 1.87
1.48 1.87
1.48 1.87
1.73 1.87
1.70 1.87
1.70 1.87
1.35 1.87
4.41 1.87
1.62 1.87
1.84 1.87
2.10 1.87
1.85 1.87
2.87 1.87
2.62 1.87
1.53 1.87
12.6 1.87
4.16 1.87
1.84 1.87
1.30 1.87
9.57 1.87
6.90 1.87
9.58 1.87
1.53 1.87
01/18/2218:46 01/18/2218:46 67-64-1
01/18/22 18:46 01/18/2218:46 107-05-1
01/18/2218:46 01/18/2218:46 71-43-2
01/18/2218:46 01/18/2218:46 100-44-7
01 /18/2218:46 01/18/2218:46 75-27-4
01/18/22 18:46 01/18/2218:46 75-25-2
01/18/22 18:46 01/18/22 18:46 74-83-9
01 /18/22 18:46 01/18/2218:46 106-99-0
01/18/2218:46 01/18/2218:46 75-15-0
01/18/22 18:46 01/18/22 18:46 56-23-5
01/18/22 18:46 01/18/2218:46 108-90-7
01/18/2218:46 01/18/2218:46 75-00-3
01/18/22 18:46 01/18/2218:46 67-66-3
01/18/22 18:46 01/18/2218:46 74-87-3
01/18/22 18:46 01/18/2218:46 95-49-8
01/18/22 18:46 01/18/2218:46 110-82-7
01/18/2218:46 01/18/2218:46 124-48-1
01/18/22 18:46 01/18/2218:46 106-93-4
01/18/22 18:46 01/18/2218:46 95-50-1
01/18/2218:46 01/18/2218:46 541-73-1
01/18/2218:46 01/18/2218:46 106-46-7
01/18/2218:46 01/18/2218:46 107-06-2
01/18/2218:46 01/18/2218:46 75-34-3
01/18/22 18:46 01/18/2218:46 75-35-4
01/19/2217:46 01/19/2217:46 156-59-2
01/19/2217:46 01/19/2217:46 156-60-5
01/18/22 18:46 01/18/2218:46 78-87-5
01/18/2218:46 01/18/2218:46 10061-01-5
01/18/22 18:46 01/18/2218:46 10061-02-6
01/18/2218:46 01/18/2218:46 123-91-1
01/18/2218:46 01/18/2218:46 64-17-5
01/18/22 18:46 01/18/2218:46 100-41-4
01/18/22 18:46 01/18/22 18:46 622-96-8
01/18/22 18:46 01/18/2218:46 75-69-4
01/18/22 18:46 01/18/22 18:46 75-71-8
01/18/22 18:46 01/18/2218:46 76-13-1
01/18/2218:46 01/18/2218:46 76-14-2
01/18/22 18:46 01/18/2218:46 142-82-5
01/18/2218:46 01/18/2218:46 87-68-3
01/18/22 18:46 01/18/2218:46 110-54-3
01/18/22 18:46 01/18/2218:46 98-82-8
01/18/22 18:46 01/18/2218:46 75-09-2
01/18/22 18:46 01/18/2218:46 591-78-6
01/18/22 18:46 01/18/22 18:46 78-93-3
01/18/22 18:46 01/18/2218:46 108-10-1
01/18/22 18:46 01/18/2218:46 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 17 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-4 #3262
Parameters
VOA {MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1 ,2,4-Trichlorobenzene
1,1, 1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
1 ,2,4-Trimethylbenzene
1 ,3,5-Trimethylbenzene
2,2 ,4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1 ,4-Dichlorobenzene-d4 (IS)
1 ,4-Dichlorobenzene-d4 (IS)
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab 10: 92582172004 Collected: 01 /05/22 13:36 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
21.0 ug/m3 1.35 1.87 01/18/22 18:46
NO ug/m3 6.18 1.87 01/1 8/22 18:46
101 ug/m3 5.75 1.87 01/18/22 18:46
NO ug/m3 4.03 1.87 01/18/22 18:46
3.94 ug/m3 1.59 1.87 01/18/22 18:46
NO ug/m3 2.57 1.87 01/18/22 18:46
355 ug/m3 2.54 1.87 01/19/22 17:46
NO ug/m3 1.10 1.87 01/18/22 18:46
6.55 ug/m3 3.52 1.87 01 /18/22 18:46
NO ug/m3 8.74 1.87 01 /18/22 18:46
NO ug/m3 2.03 1.87 01/18/22 18:46
NO ug/m3 2.03 1.87 01/18/22 18:46
44.3 ug/m3 2.00 1.87 01/1 9/22 17:46
5.50 ug/m3 1.84 1.87 01/18/22 18:46
NO ug/m3 1.84 1.87 01/1 8/22 18:46
NO ug/m3 1.75 1.87 01/18/22 18:46
NO ug/m3 0.956 1.87 01/18/22 18:46
NO ug/m3 1.64 1.87 01/18/22 18:46
NO ug/m3 1.32 1.87 01/18/22 18:46
5.64 ug/m3 3.24 1.87 01/18/22 18:46
1.91 ug/m3 1.62 1.87 01/18/22 18:46
98.8 % 60.0-140 1.87 01/18/22 18:46
123 % 60.0-140 1.87 01/1 9/22 17:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01/18/2218:46 1634-04-4
01 /1 8/22 18:46 91-20-3
01/18/22 18:46 67-63-0
01/18/22 18:46 115-07-1
01/18/22 18:46 100-42-5
01/18/2218:46 79-34-5
01/19/22 17:46 127-18-4
01/18/2218:46 109-99-9
01/1 8/2218:46 108-88-3
01/1 8/22 18:46 120-82-1
01/18/2218:46 71-55-6
01/18/2218:46 79-00-5
01/19/22 17:46 79-01-6
01/18/22 18:46 95-63-6
01/18/22 18:46 108-67-8
01/18/22 18:46 540-84-1
01/18/22 18:46 75-01-4
01/18/22 18:46 593-60-2
01/18/22 18:46 108-05-4
01 /18/2218:46 179601-23-1
01 /18/2218:46 95-47-6
01 /18/2218:46 3855-82-1
01 /19/22 17:46 3855-82-1
Page 18 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-5 #3793
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1 ,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
1 ,2-Dichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
1 ,4-Dioxane (p-Dioxane)
Ethanol
Ethylbenzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1,1 ,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01 /21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab ID: 92582172005 Collected: 01/05/22 13:47 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
17.5
NO
NO
NO
NO
NO
NO
NO
4.30
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
50.7
NO
NO
5.84
3.07
NO
NO
NO
ND
NO
NO
NO
NO
NO
NO
NO
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
u9/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
5.35 1.8
1.13 1.8
1.15 1.8
1.87 1.8
2.41 1.8
11.2 1.8
1.40 1.8
7.97 1.8
1.12 1.8
2.27 1.8
1.66 1.8
0.950 1.8
1.75 1.8
0.744 1.8
1.86 1.8
1.24 1.8
3.06 1.8
2.77 1.8
2.16 1.8
2.16 1.8
2.16 1.8
1.46 1.8
1.44 1.8
1.43 1.8
1.43 1.8
1.43 1.8
1.66 1.8
1.63 1.8
1.63 1.8
1.30 1.8
4.24 1.8
1.56 1.8
1.77 1.8
2.02 1.8
1.78 1.8
2.76 1.8
2.52 1.8
1.47 1.8
12.1 1.8
3.98 1.8
1.77 1.8
1.25 1.8
9.20 1.8
6.63 1.8
9.21 1.8
1.47 1.8
Prepared Analyzed CAS No.
01/18/2219:20 01/18/2219:20 67-64-1
01/18/22 19:20 01 /18/22 19:20 107-05-1
01/18/22 19:20 01 /18/221 9:20 71-43-2
01/18/22 19:20 01/18/2219:20 100-44-7
01/18/22 19:20 01/18/2219:20 75-27-4
01/18/22 19:20 01/1 8/22 19:20 75-25-2
01/1 8/22 19:20 01/18/2219:20 74-83-9
01/18/22 19:20 01 /18/22 19:20 106-99-0
01/18/22 19:20 01/18/2219:20 75-15-0
01 /18/22 19:20 01 /18/22 19:20 56-23-5
01 /18/22 19:20 01 /1 8/2219:20 108-90-7
01 /18/22 19:20 01/18/2219:20 75-00-3
01 /18/22 19:20 01/1 8/22 19:20 67-66-3
01 /18/22 19:20 01/18/2219:20 74-87-3
01 /18/22 19:20 01/18/2219:20 95-49-8
01/18/22 19:20 01/18/22 19:20 11 0-82-7
01 /18/22 19:20 01/18/2219:20 124-48-1
01 /18/22 19:20 01/18/2219:20 106-93-4
01 /18/22 19:20 01/18/2219:20 95-50-1
01/18/22 19:20 01/18/2219:20 541-73-1
01/18/22 19:20 01/18/22 19:20 106-46-7
01/18/22 19:20 01/18/2219:20 107-06-2
01/18/22 19:20 01/18/2219:20 75-34-3
01/18/22 19:20 01/18/2219:20 75-35-4
01/19/22 18:27 01/19/2218:27 156-59-2
01/18/22 19:20 01/18/22 19:20 156-60-5
01/18/22 19:20 01/18/22 19:20 78-87-5
01/18/22 19:20 01/18/2219:20 10061-01-5
01/18/22 19:20 01 /1 8/2219:20 10061-02-6
01/18/2219:20 01 /18/2219:20 123-91-1
01/18/22 19:20 01 /18/2219:20 64-17-5
01/18/22 19:20 01 /18/2219:20 100-41-4
01/18/22 19:20 01/18/22 19:20 622-96-8
01/18/22 19:20 01 /18/22 19:20 75-69-4
01/18/22 19:20 01/1 8/22 19:20 75-71-8
01/18/22 19:20 01/18/2219:20 76-13-1
01/18/22 19:20 01/18/2219:20 76-14-2
01/18/22 19:20 01/18/22 19:20 142-82-5
01/18/22 19:20 01/18/2219:20 87-68-3
01/18/22 19:20 01/18/22 19:20 110-54-3
01/18/22 19:20 01/18/2219:20 98-82-8
01/18/22 19:20 01/18/2219:20 75-09-2
01/18/22 19:20 01/18/2219:20 591-78-6
01/1 8/22 19:20 01/18/2219:20 78-93-3
01/18/22 19:20 01/18/2219:20 108-10-1
01/18/22 19:20 01/18/22 19:20 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 19 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-5 #3793
Parameters
VOA (MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,4-Trichlorobenzene
1, 1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
1 ,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1,4-Dichlorobenzene-d4 (IS)
1,4-Dichlorobenzene-d4 (IS)
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab 10: 92582172005 Collected: 01/05/22 13:47 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
ND ug/m3 1.30 1.8 01/18/22 19:20
ND ug/m3 5.92 1.8 01/18/22 19:20
12.1 ug/m3 5.53 1.8 01/18/22 19:20
ND ug/m3 3.87 1.8 01/18/22 19:20
2.82 ug/m3 1.53 1.8 01/18/22 19:20
ND ug/m3 2.47 1.8 01/18/22 19:20
41.5 ug/m3 2.44 1.8 01/1 9/22 18:27
ND ug/m3 1.06 1.8 01/18/22 19:20
ND ug/m3 3.39 1.8 01/18/22 19:20
ND ug/m3 8.37 1.8 01/18/22 19:20
ND ug/m3 1.96 1.8 01/18/22 19:20
ND ug/m3 1.96 1.8 01/18/22 19:20
2.23 ug/m3 1.93 1.8 01/19/22 18:27
ND ug/m3 1.77 1.8 01/18/22 19:20
ND ug/m3 1.77 1.8 01/18/22 19:20
ND ug/m3 1.68 1.8 01/18/22 19:20
ND ug/m3 0.920 1.8 01/18/22 19:20
ND ug/m3 1.57 1.8 01/18/22 19:20
ND ug/m3 1.27 1.8 01/18/22 19:20
ND ug/m3 3.12 1.8 01/18/22 19:20
ND ug/m3 1.56 1.8 01 /18/22 19:20
97.1 % 60.0-140 1.8 01/18/22 19:20
101 % 60.0-140 1.8 01/19/22 18:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01/18/22 19:20 1634-04-4
01/18/2219:20 91-20-3
01/18/22 19:20 67-63-0
01/18/22 19:20 115-07-1
01/18/22 19:20 100-42-5
01/18/22 19:20 79-34-5
01/19/2218:27 127-18-4
01/18/22 19:20 109-99-9
01/18/2219:20 108-88-3
01/18/22 19:20 120-82-1
01/18/22 19:20 71 -55-6
01/18/22 19:20 79-00-5
01/19/22 18:27 79-01-6
01/18/22 19:20 95-63-6
01/18/22 19:20 108-67-8
01/18/22 19:20 540-84-1
01/18/22 19:20 75-01-4
01/18/22 19:20 593-60-2
01/18/2219:20 108-05-4
01/18/2219:20 179601-23-1
01/18/22 19:20 95-47-6
01/18/2219:20 3855-82-1
01/19/2218:27 3855-82-1
Page 20 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-6 #2995
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1 ,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1,4-Dichlorobenzene
1 ,2-Dichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1 ,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethanol
Ethylbenzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1,1 ,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
(704 )875-9092
Lab 10: 92582172006 Collected: 01/05/22 13:57 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -MI. Juliet
27.3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.46
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.24
ND
ND
ND
ND
ND
23.2
ND
ND
12.5
3.08
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
5.35 1.8
1.13 1.8
1.15 1.8
1.87 1.8
2.41 1.8
11.2 1.8
1.40 1.8
7.97 1.8
1.12 1.8
2.27 1.8
1.66 1.8
0.950 1.8
1.75 1.8
0.744 1.8
1.86 1.8
1.24 1.8
3.06 1.8
2.77 1.8
2.16 1.8
2.16 1.8
2.16 1.8
1.46 1.8
1.44 1.8
1.43 1.8
1.43 1.8
1.43 1.8
1.66 1.8
1.63 1.8
1.63 1.8
1.30 1.8
4.24 1.8
1.56 1.8
1.77 1.8
2.02 1.8
1.78 1.8
2.76 1.8
2.52 1.8
1.47 1.8
12.1 1.8
3.98 1.8
1.77 1.8
1.25 1.8
9.20 1.8
6.63 1.8
9.21 1.8
1.47 1.8
Prepared Analyzed CAS No.
01/18/22 19:59 01 /1 8/2219:59 67-64-1
01/18/2219:59 01/18/2219:59 107-05-1
01/1 8/22 19:59 01 /1 8/2219:59 71-43-2
01/1 8/22 19:59 01/18/2219:59 100-44-7
01/18/22 19:59 01/18/2219:59 75-27-4
01/18/22 19:59 01/18/22 19:59 75-25-2
01/18/2219:59 01/18/2219:59 74-83-9
01/18/22 19:59 01/1 8/2219:59 106-99-0
01/18/22 19:59 01/18/2219:59 75-15-0
01/18/22 19:59 01/18/22 19:59 56-23-5
01/18/2219:59 01/18/2219:59 108-90-7
01 /18/22 19:59 01/18/22 19:59 75-00-3
01/18/22 19:59 01/18/2219:59 67-66-3
01/18/22 19:59 01/18/2219:59 74-87-3
01/18/22 19:59 01/18/2219:59 95-49-8
01/18/2219:59 01/18/2219:59 110-82-7
01/18/221 9:59 01/18/2219:59 124-48-1
01/18/2219:59 01/18/2219:59 106-93-4
01/18/2219:59 01/18/2219:59 95-50-1
01/18/221 9:59 01/18/2219:59 541-73-1
01/18/221 9:59 01/18/221 9:59 106-46-7
01/18/2219:59 01/18/2219:59 107-06-2
01/18/22 19:59 01/18/22 19:59 75-34-3
01/18/22 19:59 01/18/22 19:59 75-35-4
01/1 8/22 19:59 01 /18/2219:59 156-59-2
01/18/22 19:59 01/18/22 19:59 156-60-5
01/18/22 19:59 01 /18/2219:59 78-87-5
01/18/2219:59 01/18/2219:59 10061-01-5
01/18/22 19:59 01 /1 8/221 9:59 10061-02-6
01/18/22 19:59 01/18/2219:59 123-91-1
01/1 8/22 19:59 01/18/2219:59 64-17-5
01/18/22 19:59 01/18/2219:59 100-41-4
01/18/22 19:59 01/18/22 19:59 622-96-8
01/18/22 19:59 01/18/2219:59 75-69-4
01/18/22 19:59 01/18/22 19:59 75-71-8
01/18/22 19:59 01/18/22 19:59 76-13-1
01/18/22 19:59 01/18/2219:59 76-14-2
01/18/2219:59 01/18/2219:59 142-82-5
01/18/22 19:59 01/18/22 19:59 87-68-3
01 /18/22 19:59 01/1 8/2219:59 110-54-3
01/18/22 19:59 01/18/22 19:59 98-82-8
01/18/22 19:59 01/18/22 19:59 75-09-2
01/18/22 19:59 01/18/22 19:59 591-78-6
01/18/22 19:59 01/18/22 19:59 78-93-3
01/18/22 19:59 01/18/2219:59 108-10-1
01/18/22 19:59 01/18/2219:59 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC. Page 21 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-6 #2995
Parameters
VOA (MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1 ,2,4-Trichlorobenzene
1, 1,1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
1,2,4-Trimethylbenzene
1 ,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1,4-Dichlorobenzene-d4 (IS)
1,4-Dichlorobenzene-d4 (IS)
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab ID: 92582172006 Collected: 01/05/22 13:57 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -MI. Juliet
NO ug/m3 1.30 1.8 01/18/22 19:59
NO ug/m3 5.92 1.8 01/18/22 19:59
7.74 ug/m3 5.53 1.8 01/18/22 19:59
NO ug/m3 3.87 1.8 01/18/22 19:59
4.59 ug/m3 1.53 1.8 01/18/22 19:59
NO ug/m3 2.47 1.8 01 /1 8/22 19:59
14600 ug/m3 48.9 36 01/20/22 18:56
NO ug/m3 1.06 1.8 01/18/22 19:59
12.9 ug/m3 3.39 1.8 01 /1 8/22 19:59
NO ug/m3 8.37 1.8 01/18/22 19:59
10.3 ug/m3 1.96 1.8 01/18/22 19:59
NO ug/m3 1.96 1.8 01/1 8/22 19:59
10.2 ug/m3 1.93 1.8 01/1 8/22 19:59
NO ug/m3 1.77 1.8 01/18/22 19:59
NO ug/m3 1.77 1.8 01/18/22 19:59
NO ug/m3 1.68 1.8 01/18/22 19:59
NO ug/m3 0.920 1.8 01/18/22 19:59
NO ug/m3 1.57 1.8 01/18/22 19:59
NO ug/m3 1.27 1.8 01/18/22 19:59
3.14 ug/m3 3.12 1.8 01/18/22 19:59
NO ug/m3 1.56 1.8 01/18/22 19:59
95.9 % 60.0-140 1.8 01/1 8/22 19:59
91.8 % 60.0-140 36 01/20/22 18:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01/18/22 19:59 1634-04-4
01/18/2219:59 91-20-3
01/18/22 19:59 67-63-0
01/18/22 19:59 115-07-1
01/18/22 19:59 100-42-5
01/18/22 19:59 79-34-5
01/20/22 18:56 127-18-4
01/18/22 19:59 109-99-9
01/18/22 19:59 108-88-3
01/18/2219:59 120-82-1
01/18/22 19:59 71-55-6
01/18/22 19:59 79-00-5
01/18/22 19:59 79-01-6
01/18/22 19:59 95-63-6
01 /18/2219:59 108-67-8
01/18/22 19:59 540-84-1
01/18/2219:59 75-01-4
01/18/22 19:59 593-60-2
01/18/2219:59 108-05-4
01 /18/2219:59 179601-23-1
01 /18/22 19:59 95-47-6
01/18/22 19:59 3855-82-1
01/20/22 18:56 3855-82-1
Page 22 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Sample: P-7 #3780
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1 ,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
1 ,2-Dichloroethane
1, 1-Dichloroethane
1 , 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
1 ,4-Dioxane (p-Dioxane)
Ethanol
Ethyl benzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1,1 ,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01/21/2022 02:42 PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab 10: 92582172007 Collected: 01 /05/22 14:09 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
25.2
ND
ND
ND
ND
ND
ND
ND
27.4
ND
ND
ND
ND
0.962
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.60
ND
ND
ND
ND
ND
33.6
ND
ND
19.8
3.18
ND
ND
ND
NO
ND
ND
ND
ND
ND
ND
ND
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
5.18 1.74
1.09 1.74
1.11 1.74
1.81 1.74
2.33 1.74
10.8 1.74
1.35 1.74
7.70 1.74
1.08 1.74
2.19 1.74
1.61 1.74
0.918 1.74
1.69 1.74
0.719 1.74
1.79 1.74
1.20 1.74
2.96 1.74
2.68 1.74
2.09 1.74
2.09 1.74
2.09 1.74
1.41 1.74
1.39 1.74
1.38 1.74
1.38 1.74
1.38 1.74
1.61 1.74
1.58 1.74
1.58 1.74
1.25 1.74
4.11 1.74
1.51 1.74
1.71 1.74
1.96 1.74
1.72 1.74
2.67 1.74
2.43 1.74
1.42 1.74
11 .7 1.74
3.88 1.74
1.71 1.74
1.21 1.74
8.92 1.74
6.43 1.74
8.93 1.74
1.43 1.74
Prepared Analyzed CAS No.
01/18/22 20:35 01 /18/22 20:35 67-64-1
01/18/22 20:35 01/18/22 20:35 107-05-1
01/18/22 20:35 01/18/22 20:35 71-43-2
01/18/22 20:35 01/18/22 20:35 100-44-7
01/18/22 20:35 01/18/22 20:35 75-27-4
01/18/22 20:35 01/18/22 20:35 75-25-2
01/18/22 20:35 01/18/22 20:35 74-83-9
01 /18/22 20:35 01/18/22 20:35 106-99-0
01/18/22 20:35 01/18/22 20:35 75-15-0
01/1 8/22 20:35 01/18/22 20:35 56-23-5
01/18/22 20:35 01/18/22 20:35 108-90-7
01/18/22 20:35 01/18/22 20:35 75-00-3
01/18/22 20:35 01/18/22 20:35 67-66-3
01/18/22 20:35 01/18/22 20:35 74-87-3
01/18/22 20:35 01/18/22 20:35 95-49-8
01/18/22 20:35 01/18/22 20:35 110-82-7
01/1 8/22 20:35 01/18/22 20 :35 124-48-1
01/18/22 20:35 01/18/22 20:35 106-93-4
01/18/22 20:35 01/18/22 20:35 95-50-1
01/18/22 20:35 01/18/22 20:35 541-73-1
01/18/22 20:35 01 /18/22 20:35 106-46-7
01/18/22 20:35 01/18/22 20:35 107-06-2
01/18/22 20:35 01 /1 8/22 20:35 75-34-3
01/1 8/22 20:35 01/18/22 20:35 75-35-4
01/18/22 20:35 01/18/22 20:35 156-59-2
01/18/22 20:35 01/18/22 20:35 156-60-5
01/18/22 20:35 01/18/22 20:35 78-87-5
01/18/22 20:35 01/18/22 20:35 10061-01-5
01 /18/22 20:35 01/18/22 20:35 10061-02-6
01 /18/22 20:35 01/18/22 20:35 123-91-1
01 /18/22 20:35 01/18/22 20:35 64-17-5
01 /18/22 20:35 01/18/22 20:35 100-41-4
01/18/22 20:35 01/18/22 20:35 622-96-8
01/1 8/22 20:35 01/18/22 20:35 75-69-4
01/18/22 20:35 01/18/22 20:35 75-71-8
01/18/22 20:35 01/18/22 20:35 76-13-1
01/18/22 20:35 01/18/22 20:35 76-14-2
01/18/22 20:35 01/18/22 20:35 142-82-5
01/18/22 20:35 01 /18/22 20:35 87-68-3
01/18/22 20:35 01/18/22 20:35 110-54-3
01/18/22 20:35 01 /18/22 20:35 98-82-8
01/18/22 20:35 01 /18/22 20:35 75-09-2
01/18/22 20:35 01/18/22 20:35 591-78-6
01/18/22 20:35 01 /18/22 20:35 78-93-3
01/18/22 20:35 01 /18/22 20:35 108-10-1
01/1 8/22 20:35 01/18/22 20:35 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 23 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-7 #3780
Parameters
VOA (MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1 ,2 ,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1 ,4-Dichlorobenzene-d4 (IS)
1 ,4-Dichlorobenzene-d4 (IS)
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab 10: 92582172007 Collected: 01/05/22 14:09 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
NO ug/m3 1.25 1.74 01/18/22 20:35
NO ug/m3 5.76 1.74 01/18/22 20:35
7.23 ug/m3 5.36 1.74 01/18/22 20:35
NO ug/m3 3.75 1.74 01/18/22 20:35
3.86 ug/m3 1.48 1.74 01/18/22 20:35
NO ug/m3 2.39 1.74 01/18/22 20:35
22900 ug/m3 47.3 34.8 01/19/22 19:44
NO ug/m3 1.03 1.74 01/18/22 20:35
18.6 ug/m3 3.28 1.74 01/18/22 20:35
NO ug/m3 8.1 4 1.74 01/18/22 20:35
53.8 ug/m3 1.89 1.74 01/18/22 20:35
NO ug/m3 1.89 1.74 01/18/22 20:35
224 ug/m3 1.86 1.74 01/1 8/22 20:35
NO ug/m3 1.71 1.74 01/1 8/22 20:35
NO ug/m3 1.71 1.74 01/18/22 20:35
NO ug/m3 1.63 1.74 01/18/22 20:35
NO ug/m3 0.890 1.74 01/18/22 20:35
NO ug/m3 1.52 1.74 01/18/22 20:35
NO ug/m3 1.23 1.74 01/18/22 20:35
3.13 ug/m3 3.02 1.74 01/18/22 20:35
NO ug/m3 1.51 1.74 01/18/22 20:35
97.8 % 60.0-140 1.74 01 /18/22 20:35
99.8 % 60.0-140 34.8 01/19/22 19:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01/18/22 20:35 1634-04-4
01/18/22 20:35 91-20-3
01/18/22 20:35 67-63-0
01/18/22 20:35 115-07-1
01 /18/22 20:35 100-42-5
01/18/22 20:35 79-34-5
01/19/22 19:44 127-18-4
01/18/22 20:35 109-99-9
01/18/22 20:35 108-88-3
01 /18/22 20:35 120-82-1
01/18/22 20:35 71-55-6
01 /18/22 20:35 79-00-5
01 /18/22 20:35 79-01-6
01 /18/22 20:35 95-63-6
01/18/22 20:35 108-67-8
01/18/22 20:35 540-84-1
01/18/22 20:35 75-01-4
01/18/22 20:35 593-60-2
01/18/22 20:35 108-05-4
01/18/22 20:35 179601-23-1
01/18/22 20:35 95-4 7-6
01/18/22 20:35 3855-82-1
01/19/22 19:44 3855-82-1
Page 24 of 41
Project:
Pace Project No.:
Sample: P-8 #2846
BENMAR 897-03
92582172
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
1 ,2-Dichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
1 ,4-Dioxane (p-Dioxane)
Ethanol
Ethyl benzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1,1,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01 /21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab 10: 92582172008 Collected: 01/05/22 14:20 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
122
NO
8.15
NO
NO
NO
NO
NO
9.99
NO
NO
NO
NO
2.03
NO
NO
NO
NO
NO
NO
NO
NO
1.41
71 .3
147
4.16
NO
NO
NO
3.18
153
1.63
NO
20.7
3.16
NO
NO
NO
NO
NO
NO
3.27
NO
NO
NO
NO
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
5.18 1.74
1.09 1.74
1.11 1.74
1.81 1.74
2.33 1.74
10.8 1.74
1.35 1.74
7.70 1.74
1.08 1.74
2.19 1.74
1.61 1.74
0.918 1.74
1.69 1.74
0.719 1.74
1.79 1.74
1.20 1.74
2.96 1.74
2.68 1.74
2.09 1.74
2.09 1.74
2.09 1.74
1.41 1.74
1.39 1.74
1.38 1.74
1.38 1.74
1.38 1.74
1.61 1.74
1.58 1.74
1.58 1.74
1.25 1.74
4.11 1.74
1.51 1.74
1.71 1.74
1.96 1.74
1.72 1.74
2.67 1.74
2.43 1.74
1.42 1.74
11.7 1.74
3.88 1.74
1.71 1.74
1.21 1.74
8.92 1.74
6.43 1.74
8.93 1.74
1.43 1.74
Prepared Analyzed CAS No.
01/1 8/22 21 :12 01/18/22 21 :12 67-64-1
01/1 8/22 21 :12 01/18/22 21:12 107-05-1
01/18/22 21:12 01/18/22 21 :12 71-43-2
01/18/22 21:12 01/18/22 21 :12 100-44-7
01/18/22 21:12 01/18/22 21 :12 75-27-4
01/18/22 21 :12 01/18/22 21 :12 75-25-2
01/18/22 21 :12 01/18/22 21 :12 74-83-9
01/18/22 21:12 01/18/22 21:12 106-99-0
01/18/22 21 :12 01/18/22 21 :12 75-15-0
01/18/22 21 :12 01/18/22 21 :12 56-23-5
01/18/22 21 :12 01/18/22 21 :12 108-90-7
01/18/22 21:12 01 /18/22 21 :12 75-00-3
01/18/22 21 :12 01/18/22 21 :12 67-66-3
01/18/22 21:12 01/18/22 21 :12 74-87-3
01/18/22 21:12 01/18/22 21 :12 95-49-8
01/1 8/22 21:12 01/18/22 21 :12 110-82-7
01/18/22 21:12 01/18/22 21:12 124-48-1
01/18/22 21:12 01/18/22 21:12 106-93-4
01/18/22 21 :12 01/18/22 21 :12 95-50-1
01/18/22 21:12 01/18/22 21:12 541-73-1
01/18/22 21 :12 01/18/22 21 :12 106-46-7
01/18/22 21:12 01/18/22 21:12 107-06-2
01/18/22 21:12 01/18/22 21 :12 75-34-3
01/18/22 21 :12 01/18/22 21 :12 75-35-4
01/18/22 21 :12 01/18/22 21:12 156-59-2
01/18/22 21 :12 01/18/22 21:12 156-60-5
01/18/22 21 :12 01/18/22 21:12 78-87-5
01/18/2221:12 01 /18/2221 :12 10061-01-5
01/18/22 21:12 01/18/22 21 :12 10061-02-6
01/18/22 21:12 01/18/22 21:12 123-91-1
01/18/22 21:12 01/18/22 21 :12 64-17-5
01/18/22 21 :12 01/18/22 21 :12 100-41-4
01/18/22 21 :12 01/18/22 21 :12 622-96-8
01/18/22 21 :12 01 /18/22 21 :12 75-69-4
01/18/22 21 :12 01/18/22 21 :12 75-71-8
01/18/22 21:12 01/1 8/22 21:12 76-13-1
01/18/22 21 :12 01/18/22 21:12 76-14-2
01/18/22 21:12 01/1 8/22 21 :12 142-82-5
01/18/22 21:12 01/18/22 21 :12 87-68-3
01/18/22 21:12 01/18/22 21:12 110-54-3
01 /18/22 21:12 01/18/22 21:12 98-82-8
01/18/22 21:12 01/1 8/22 21 :12 75-09-2
01/18/22 21:12 01/18/22 21 :12 591-78-6
01/18/22 21:12 01/18/22 21 :12 78-93-3
01/18/22 21:12 01/18/22 21:12 108-10-1
01/18/22 21:12 01/1 8/22 21:12 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 25 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Sample: P-8 #2846
Parameters
VOA {MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1 ,2.4-Trichlorobenzene
1 ,1,1-Trichloroethane
1,1 ,2-Trichloroethane
Trichloroethene
1,2.4-Trimethylbenzene
1 ,3,5-Trimethylbenzene
2,2.4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1,4-Dichlorobenzene-d4 (IS)
1 ,4-Dichlorobenzene-d4 (IS)
Date: 01 /21 /2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab 10: 92582172008 Collected: 01/05/22 14:20 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
3.75 ug/m3 1.25 1.74 01/1 8/22 21 :12
NO ug/m3 5.76 1.74 01/18/22 21:12
41.0 ug/m3 5.36 1.74 01/18/22 21:12
NO ug/m3 3.75 1.74 01/18/22 21 :12
3.16 ug/m3 1.48 1.74 01/18/22 21 :12
NO ug/m3 2.39 1.74 01/18/22 21 :12
44300 ug/m3 236 174 01/20/22 19:31
NO ug/m3 1.03 1.74 01/18/22 21:12
58.8 ug/m3 3.28 1.74 01/18/22 21:12
NO ug/m3 8.14 1.74 01/18/22 21:12
9.79 ug/m3 1.89 1.74 01/18/22 21:12
NO ug/m3 1.89 1.74 01/18/22 21:12
3900 ug/m3 186 174 01/20/22 19:31
NO ug/m3 1.71 1.74 01/18/22 21:12
NO ug/m3 1.71 1.74 01/18/22 21:12
NO ug/m3 1.63 1.74 01/18/22 21 :12
NO ug/m3 0.890 1.74 01/18/22 21 :12
NO ug/m3 1.52 1.74 01/18/22 21 :12
NO ug/m3 1.23 1.74 01/18/22 21 :12
6.85 ug/m3 3.02 1.74 01/18/22 21 :12
2.14 ug/m3 1.51 1.74 01/18/22 21:12
98.0 % 60.0-140 1.74 01/18/22 21 :12
92.5 % 60.0-140 174 01/20/22 19:31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01/18/22 21:12 1634-04-4
01/18/22 21:12 91-20-3
01/18/22 21 :12 67-63-0
01 /18/22 21 :12 115-07-1
01/18/22 21 :12 100-42-5
01/18/22 21 :12 79-34-5
01/20/22 19:31 127-18-4
01/18/22 21 :12 109-99-9
01/18/22 21 :12 108-88-3
01/18/22 21 :12 120-82-1
01/18/22 21 :12 71-55-6
01/18/22 21 :12 79-00-5
01/20/22 19:31 79-01-6
01/18/22 21:12 95-63-6
01/18/22 21 :12 108-67-8
01/18/22 21 :12 540-84-1
01/18/22 21 :12 75-01-4
01/18/22 21 :12 593-60-2
01/18/22 21 :12 108-05-4
01/18/22 21 :12 179601-23-1
01/18/22 21:12 95-47-6
01/18/22 21 :12 3855-82-1
01/20/22 19:31 3855-82-1
Page 26 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Sample: P-9 #2422
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1 ,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
1 ,2-Dichloroethane
1, 1-Dichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
1 ,4-Dioxane (p-Dioxane)
Ethanol
Ethylbenzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1,1 ,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01/21/2022 02:42 PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab ID: 92582172009 Collected: 01/05/22 14:31 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
84.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.834
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.04
ND
ND
ND
ND
ND
58.4
ND
ND
20.3
3.47
ND
ND
ND
NO
ND
ND
1.86
ND
9.11
ND
ND
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
5.56 1.87
1.17 1.87
1.19 1.87
1.94 1.87
2.51 1.87
11 .6 1.87
1.45 1.87
8.28 1.87
1.16 1.87
2.36 1.87
1.73 1.87
0.987 1.87
1.82 1.87
0.772 1.87
1.93 1.87
1.29 1.87
3.18 1.87
2.88 1.87
2.25 1.87
2.25 1.87
2.25 1.87
1.51 1.87
1.50 1.87
1.48 1.87
1.48 1.87
1.48 1.87
1.73 1.87
1.70 1.87
1.70 1.87
1.35 1.87
4.41 1.87
1.62 1.87
1.84 1.87
2.10 1.87
1.85 1.87
2.87 1.87
2.62 1.87
1.53 1.87
12.6 1.87
4.16 1.87
1.84 1.87
1.30 1.87
9.57 1.87
6.90 1.87
9.58 1.87
1.53 1.87
Prepared Analyzed CAS No.
01/18/22 21:49 01/18/22 21 :49 67-64-1
01/18/22 21:49 01/18/22 21:49 107-05-1
01/18/22 21:49 01/18/22 21 :49 71-43-2
01/18/22 21:49 01/18/22 21 :49 100-44-7
01/18/22 21:49 01/18/22 21:49 75-27-4
01/18/22 21:49 01/18/22 21:49 75-25-2
01/18/22 21:49 01/1 8/22 21 :49 74-83-9
01/1 8/22 21:49 01/18/22 21 :49 106-99-0
01/18/22 21:49 01/18/22 21 :49 75-15-0
01/18/22 21:49 01/18/22 21:49 56-23-5
01/18/22 21 :49 01/18/22 21 :49 108-90-7
01/18/22 21 :49 01/18/22 21 :49 75-00-3
01/18/22 21 :49 01/18/22 21:49 67-66-3
01/18/22 21 :49 01/18/22 21 :49 74-87-3
01/18/22 21:49 01/18/22 21:49 95-49-8
01/18/22 21:49 01/18/22 21:49 110-82-7
01/18/22 21:49 01/18/22 21:49 124-48-1
01/18/22 21:49 01/18/22 21:49 106-93-4
01/18/22 21:49 01/18/22 21:49 95-50-1
01/18/22 21 :49 01 /1 8/22 21:49 541-73-1
01/1 8/22 21:49 01/18/22 21:49 106-46-7
01/18/22 21:49 01/18/22 21 :49 107-06-2
01/18/22 21 :49 01/18/22 21:49 75-34-3
01/18/22 21:49 01/1 8/22 21:49 75-35-4
01/18/22 21:49 01/18/22 21 :49 156-59-2
01/18/22 21:49 01/18/22 21:49 156-60-5
01/18/22 21:49 01/18/22 21:49 78-87-5
01/18/22 21:49 01/18/22 21 :49 10061-01-5
01 /18/22 21:49 01/18/22 21:49 10061-02-6
01/18/22 21:49 01/18/22 21:49 123-91-1
01 /18/22 21:49 01/1 8/22 21:49 64-17-5
01/18/22 21:49 01/18/22 21:49 100-41-4
01/18/22 21:49 01/18/22 21:49 622-96-8
01 /1 8/22 21:49 01/18/22 21 :49 75-69-4
01 /1 8/22 21:49 01/18/22 21:49 75-71-8
01 /18/22 21:49 01/18/22 21:49 76-13-1
01 /1 8/2221:49 01/18/2221:49 76-14-2
01 /18/22 21:49 01/18/22 21:49 142-82-5
01/18/22 21:49 01/18/22 21:49 87-68-3
01/18/22 21:49 01/18/22 21 :49 110-54-3
01/18/22 21:49 01/18/22 21:49 98-82-8
01/18/22 21:49 01/18/22 21:49 75-09-2
01/18/22 21:49 01/18/22 21:49 591-78-6
01/18/22 21 :49 01/18/22 21:49 78-93-3
01/18/22 21 :49 01/18/22 21 :49 108-10-1
01/18/22 21:49 01/18/22 21:49 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 27 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-9 #2422
Parameters
VOA (MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,4-Trichlorobenzene
1,1 ,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1 ,4-Dichlorobenzene-d4 (IS)
1 ,4-Dichlorobenzene-d4 (IS)
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab 10: 92582172009 Collected: 01 /05/22 14:31 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit DF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
ND ug/m3 1.35 1.87 01/18/22 21:49
ND ug/m3 6.18 1.87 01/18/22 21:49
16.9 ug/m3 5.75 1.87 01/1 8/22 21:49
ND ug/m3 4.03 1.87 01/18/22 21:49
3.30 ug/m3 1.59 1.87 01/18/22 21:49
ND ug/m3 2.57 1.87 01 /18/22 21:49
1740 ug/m3 25.4 18.7 01/19/22 21:01
ND ug/m3 1.10 1.87 01/18/22 21:49
16.9 ug/m3 3.52 1.87 01/18/22 21:49
ND ug/m3 8.74 1.87 01/18/22 21:49
6.09 ug/m3 2.03 1.87 01/18/22 21 :49
ND ug/m3 2.03 1.87 01/18/22 21:49
171 ug/m3 2.00 1.87 01/18/22 21:49
ND ug/m3 1.84 1.87 01/1 8/22 21:49
ND ug/m3 1.84 1.87 01/1 8/22 21 :49
ND ug/m3 1.75 1.87 01/18/22 21:49
ND ug/m3 0.956 1.87 01/18/22 21:49
ND ug/m3 1.64 1.87 01/18/22 21:49
ND ug/m3 1.32 1.87 01/18/22 21:49
ND ug/m3 3.24 1.87 01/18/22 21 :49
ND ug/m3 1.62 1.87 01/18/22 21 :49
97.5 % 60.0-140 1.87 01/18/22 21:49
97.2 % 60.0-140 18.7 01/19/22 21:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01/18/22 21:49 1634-04-4
01/18/22 21 :49 91-20-3
01/18/22 21:49 67-63-0
01/18/22 21:49 115-07-1
01/18/22 21:49 100-42-5
01/18/22 21:49 79-34-5
01/19/22 21 :01 127-18-4
01/18/22 21 :49 109-99-9
01/18/22 21:49 108-88-3
01/18/22 21 :49 120-82-1
01/18/22 21:49 71-55-6
01/18/22 21:49 79-00-5
01/18/22 21:49 79-01-6
01/18/22 21:49 95-63-6
01 /18/22 21 :49 108-67-8
01/18/22 21:49 540-84-1
01/18/22 21:49 75-01-4
01 /1 8/22 21 :49 593-60-2
01/18/22 21:49 108-05-4
01/18/22 21 :49 179601-23-1
01/18/22 21 :49 95-47-6
01/18/22 21:49 3855-82-1
01/19/22 21 :01 3855-82-1
Page 28 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
Sample: P-10 #3251
Parameters
VOA (MS) T0-15
Acetone
Allyl chloride
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1 ,3-Butadiene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
Cyclohexane
Dibromochloromethane
1 ,2-Dibromoethane (EDB)
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
1 ,2-Dichloroethane
1, 1-0ichloroethane
1, 1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
1 ,4-Dioxane (p-Dioxane)
Ethanol
Ethyl benzene
4-Ethyltoluene
Trichlorofluoromethane
Dichlorodifluoromethane
1,1 ,2-Trichlorotrifluoroethane
Dichlorotetrafluoroethane
n-Heptane
Hexachloro-1 ,3-butadiene
n-Hexane
lsopropylbenzene (Cumene)
Methylene Chloride
2-Hexanone
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Methyl methacrylate
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab ID: 92582172010 Collected: 01/05/22 14:42 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF Prepared Analyzed CAS No. ------------------------------------
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
81.0
NO
1.42
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
2.60
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
19.4
NO
NO
NO
NO
NO
42.8
2.07
NO
8.54
3.26
NO
NO
4.29
ND
NO
NO
4.97
NO
9.44
NO
NO
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
ug/m3
5.56 1.87
1.17 1.87
1.19 1.87
1.94 1.87
2.51 1.87
11.6 1.87
1.45 1.87
8.28 1.87
1.16 1.87
2.36 1.87
1.73 1.87
0.987 1.87
1.82 1.87
0.772 1.87
1.93 1.87
1.29 1.87
3.18 1.87
2.88 1.87
2.25 1.87
2.25 1.87
2.25 1.87
1.51 1.87
1.50 1.87
1.48 1.87
1.48 1.87
1.48 1.87
1.73 1.87
1.70 1.87
1.70 1.87
1.35 1.87
4.41 1.87
1.62 1.87
1.84 1.87
2.10 1.87
1.85 1.87
2.87 1.87
2.62 1.87
1.53 1.87
12.6 1.87
4.16 1.87
1.84 1.87
1.30 1.87
9.57 1.87
6.90 1.87
9.58 1.87
1.53 1.87
01/18/22 22:27 01/18/22 22:27 67-64-1
01/18/22 22:27 01/18/22 22:27 107-05-1
01/18/22 22:27 01/18/22 22:27 71-43-2
01/18/22 22:27 01/18/22 22:27 100-44-7
01/18/22 22:27 01/18/22 22:27 75-27-4
01/18/22 22:27 01/18/22 22:27 75-25-2
01/18/22 22:27 01/18/22 22:27 74-83-9
01/18/22 22:27 01/18/22 22:27 106-99-0
01/18/22 22:27 01/18/22 22:27 75-15-0
01/18/22 22:27 01/18/22 22:27 56-23-5
01/18/22 22:27 01/18/22 22:27 108-90-7
01/18/22 22:27 01/18/22 22:27 75-00-3
01/18/22 22:27 01/1 8/22 22:27 67-66-3
01/18/22 22:27 01/18/22 22:27 74-87-3
01/18/22 22:27 01/18/22 22:27 95-49-8
01/18/22 22:27 01/18/22 22:27 110-82-7
01/18/22 22:27 01/18/22 22:27 124-48-1
01/18/22 22:27 01/18/22 22:27 106-93-4
01/18/22 22:27 01/18/22 22:27 95-50-1
01/18/22 22:27 01/18/22 22:27 541-73-1
01/18/22 22:27 01/18/22 22:27 106-46-7
01/18/22 22:27 01/18/22 22:27 107-06-2
01/18/22 22:27 01/18/22 22:27 75-34-3
01 /18/22 22:27 01/18/22 22:27 75-35-4
01/18/22 22:27 01/18/22 22:27 156-59-2
01/18/22 22:27 01/18/22 22:27 156-60-5
01/18/22 22:27 01/18/22 22:27 78-87-5
01/18/22 22:27 01/18/22 22:27 10061-01-5
01 /18/22 22:27 01/18/22 22:27 10061-02-6
01/18/22 22:27 01/18/22 22:27 123-91-1
01/18/22 22:27 01/18/22 22:27 64-17-5
01/18/22 22:27 01/18/22 22:27 100-41-4
01/18/22 22:27 01/18/22 22:27 622-96-8
01/18/22 22:27 01/18/22 22:27 75-69-4
01 /18/22 22:27 01/18/22 22:27 75-71-8
01/18/22 22:27 01/18/22 22:27 76-13-1
01 /18/22 22:27 01/18/22 22:27 76-14-2
01/18/22 22:27 01/18/22 22:27 142-82-5
01/18/22 22:27 01/18/22 22:27 87-68-3
01 /18/22 22:27 01 /18/22 22:27 110-54-3
01 /18/22 22:27 01/18/22 22:27 98-82-8
01 /18/22 22:27 01/18/22 22:27 75-09-2
01 /18/22 22:27 01 /18/22 22:27 591-78-6
01/18/22 22:27 01 /18/22 22:27 78-93-3
01 /18/22 22:27 01 /18/22 22:27 108-10-1
01/18/22 22:27 01/18/22 22:27 80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC. Page 29 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
Sample: P-10 #3251
Parameters
VOA (MS) T0-15
Methyl-tert-butyl ether
Naphthalene
2-Propanol
Propylene
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,2,4-Trichlorobenzene
1, 1,1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
1 ,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2,2,4-Trimethylpentane
Vinyl chloride
Vinyl bromide
Vinyl acetate
m&p-Xylene
o-Xylene
Surrogates
1 ,4-Dichlorobenzene-d4 (IS)
Date: 01/21/2022 02:42PM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Lab ID: 92582172010 Collected: 01/05/22 14:42 Received: 01/11/22 00:00 Matrix: Air
Results Units Report Limit OF Prepared
Analytical Method: T0-15 Preparation Method: T0-15
Pace National -Mt. Juliet
NO ug/m3 1.35 1.87 01/18/22 22:27
NO ug/m3 6.18 1.87 01/18/22 22:27
25.1 ug/m3 5.75 1.87 01 /18/22 22:27
NO ug/m3 4.03 1.87 01/18/22 22:27
3.86 ug/m3 1.59 1.87 01 /18/22 22:27
NO ug/m3 2.57 1.87 01 /18/22 22:27
1090 ug/m3 2.54 1.87 01/18/22 22:27
NO ug/m3 1.10 1.87 01/18/22 22:27
106 ug/m3 3.52 1.87 01 /18/22 22:27
NO ug/m3 8.74 1.87 01 /18/22 22:27
NO ug/m3 2.03 1.87 01 /1 8/22 22:27
NO ug/m3 2.03 1.87 01 /18/22 22:27
60.0 ug/m3 2.00 1.87 01/18/22 22:27
NO ug/m3 1.84 1.87 01/18/22 22:27
NO ug/m3 1.84 1.87 01/18/22 22:27
9.90 ug/m3 1.75 1.87 01/18/22 22:27
NO ug/m3 0.956 1.87 01/18/22 22:27
NO ug/m3 1.64 1.87 01/18/22 22:27
NO ug/m3 1.32 1.87 01 /18/22 22:27
8.97 ug/m3 3.24 1.87 01 /18/22 22:27
2.99 ug/m3 1.62 1.87 01/18/22 22:27
97.7 % 60.0-140 1.87 01 /18/22 22:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No. Qual
01/18/22 22:27 1634-04-4
01/18/22 22:27 91-20-3
01/18/22 22:27 67-63-0
01/18/22 22:27 115-07-1
01/18/22 22:27 100-42-5
01/18/22 22:27 79-34-5
01/18/22 22:27 127-18-4
01/18/22 22:27 109-99-9
01/18/22 22:27 108-88-3
01/18/22 22:27 120-82-1
01/18/22 22:27 71-55-6
01/18/22 22:27 79-00-5
01/18/22 22:27 79-01-6
01/18/22 22:27 95-63-6
01/18/22 22:27 108-67-8
01/18/22 22:27 540-84-1
01/18/22 22:27 75-01-4
01/18/22 22:27 593-60-2
01/18/22 22:27 108-05-4
01/18/22 22:27 179601-23-1
01/18/22 22:27 95-47-6
01 /18/22 22:27 3855-82-1
Page 30 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
QC Batch: 1803836
QC Batch Method: T0-15
QUALITY CONTROL DATA
Analysis Method: T0-15
Analysis Description: VOA (MS) T0-15
Laboratory: Pace National -MI. Juliet
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Associated Lab Samples: 92582172001,92582172002, 92582172003,92582172004, 92582172005, 92582172006,92582172007,
92582172008,92582172009,92582172010
METHOD BLANK: R3750952-3 Matrix: Air
Associated Lab Samples: 92582172001 ,92582172002,92582172003,92582172004,92582172005,92582172006,92582172007,
92582172008,92582172009,92582172010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Acetone ppbv NO 1.25 01/18/22 09:39
Allyl chloride ppbv NO 0.200 01/18/22 09:39
Benzene ppbv NO 0.200 01/18/22 09:39
Benzyl chloride ppbv NO 0.200 01/18/22 09:39
Bromodichloromethane ppbv NO 0.200 01/18/22 09:39
Bromoform ppbv NO 0.600 01/18/22 09:39
Bromomethane ppbv NO 0.200 01/18/22 09:39
1 ,3-Butadiene ppbv NO 2.00 01/18/22 09:39
Carbon disulfide ppbv NO 0.200 01/18/22 09:39
Carbon tetrachloride ppbv NO 0.200 01/18/22 09:39
Chlorobenzene ppbv NO 0.200 01/1 8/22 09:39
Chloroethane ppbv NO 0.200 01/18/22 09:39
Chloroform ppbv NO 0.200 01/18/22 09:39
Chloromethane ppbv NO 0.200 01/18/22 09:39
2-Chlorotoluene ppbv NO 0.200 01/18/22 09:39
Cyclohexane ppbv NO 0.200 01/18/22 09:39
Dibromochloromethane ppbv NO 0.200 01/18/22 09:39
1 ,2-Dibromoethane (EDB) ppbv NO 0.200 01/18/22 09:39
1 ,2-Dichlorobenzene ppbv NO 0.200 01/18/22 09:39
1 ,3-Dichlorobenzene ppbv NO 0.200 01 /1 8/22 09:39
1 A-Dichlorobenzene ppbv NO 0.200 01 /18/22 09:39
1 ,2-Dichloroethane ppbv NO 0.200 01/18/22 09:39
1, 1-Dichloroethane ppbv NO 0.200 01/18/22 09:39
1, 1-Dichloroethene ppbv NO 0.200 01/18/22 09:39
cis-1 ,2-Dichloroethene ppbv NO 0.200 01/18/22 09:39
trans-1 ,2-Dichloroethene ppbv NO 0.200 01/18/22 09:39
1 ,2-Dichloropropane ppbv NO 0.200 01/18/22 09:39
cis-1 ,3-Dichloropropene ppbv NO 0.200 01/18/22 09:39
trans-1 ,3-0ichloropropene ppbv NO 0.200 01/18/22 09:39
1 ,4-Dioxane (p-Dioxane) ppbv NO 0.200 01/18/22 09:39
Ethyl benzene ppbv NO 0.200 01/18/22 09:39
4-Ethyltoluene ppbv NO 0.200 01/18/22 09:39
Trichlorofluoromethane ppbv NO 0.200 01/18/22 09:39
Oichlorodifluoromethane ppbv NO 0.200 01/18/22 09:39
1 , 1 ,2-Trichlorotrifluoroethane ppbv NO 0.200 01/18/22 09:39
Oichlorotetrafluoroethane ppbv NO 0.200 01/18/22 09:39
n-Heptane ppbv NO 0.200 01/18/22 09:39
Hexachloro-1 ,3-butadiene ppbv NO 0.630 01 /18/22 09:39
n-Hexane ppbv NO 0.630 01/18/22 09:39
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 01/21/2022 02:42PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 31 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
METHOD BLANK: R3750952-3
QUALITY CONTROL DATA
Matrix: Air
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Associated Lab Samples: 92582172001 ,92582172002,92582172003,92582172004,92582172005,92582172006,92582172007,
92582172008,92582172009,92582172010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
lsopropylbenzene (Cumene) ppbv NO 0.200 01/18/22 09:39
Methylene Chloride ppbv NO 0.200 01/18/22 09:39
2-Hexanone ppbv NO 1.25 01/18/22 09:39
2-Butanone (MEK) ppbv NO 1.25 01/18/22 09:39
4-Methyl-2-pentanone (MIBK) ppbv ND 1.25 01/18/22 09:39
Methyl methacrylate ppbv NO 0.200 01/18/22 09:39
Methyl-tert-butyl ether ppbv NO 0.200 01/18/22 09:39
Naphthalene ppbv ND 0.630 01/18/22 09:39
2-Propanol ppbv NO 1.25 01/18/22 09:39
Propylene ppbv ND 1.25 01/18/22 09:39
Styrene ppbv NO 0.200 01/18/22 09:39
1,1 ,2,2-Tetrachloroethane ppbv NO 0.200 01/18/22 09:39
Tetrachloroethene ppbv NO 0.200 01/18/22 09:39
Tetrahydrofuran ppbv NO 0.200 01/18/22 09:39
Toluene ppbv NO 0.500 01/18/22 09:39
1 ,2,4-Trichlorobenzene ppbv NO 0.630 01/18/22 09:39
1,1, 1-Trichloroethane ppbv NO 0.200 01/18/22 09:39
1,1 ,2-Trichloroethane ppbv NO 0.200 01/18/22 09:39
Trichloroethene ppbv ND 0.200 01/18/22 09:39
1 ,2,4-Trimethylbenzene ppbv NO 0.200 01/18/22 09:39
1 ,3,5-Trimethylbenzene ppbv NO 0.200 01/18/22 09:39
2,2,4-Trimethylpentane ppbv ND 0.200 01/18/22 09:39
Vinyl chloride ppbv ND 0.200 01/18/22 09:39
Vinyl bromide ppbv NO 0.200 01/18/22 09:39
Vinyl acetate ppbv ND 0.200 01/18/22 09:39
m&p-Xylene ppbv NO 0.400 01/18/22 09:39
o-Xylene ppbv NO 0.200 01/18/22 09:39
Ethanol ppbv NO 1.25 01/18/22 09:39
1 ,4-Dichlorobenzene-d4 (IS) % 97.4 60.0-140 01/18/22 09:39
LABORATORY CONTROL SAMPLE & LCSD: R3750952-1 R3750952-2
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Cone. Result Result % Rec % Rec Limits RPD RPD ----
Ethanol ppbv 3.75 4.01 3.84 107 102 55.0-148 4.33 25
Propylene ppbv 3.75 4.26 4.09 114 109 64.0-144 4.07 25
Dichlorodifluoromethane ppbv 3.75 3.91 3.76 104 100 64.0-139 3.91 25
Dichlorotetrafluoroethane ppbv 3.75 4.46 4.30 119 115 70.0-130 3.65 25
Chloromethane ppbv 3.75 4.17 4.04 111 108 70.0-130 3.17 25
Vinyl chloride ppbv 3.75 4.32 4.14 115 110 70.0-130 4.26 25
1 ,3-Butadiene ppbv 3.75 4.36 4.23 116 113 70.0-130 3.03 25
Bromomethane ppbv 3.75 4.36 4.23 116 113 70.0-130 3.03 25
Chloroethane ppbv 3.75 4.32 4.21 115 112 70.0-130 2.58 25
Trichlorofluoromethane ppbv 3.75 4.43 4.25 118 113 70.0-130 4.15 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 01/21/2022 02:42PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 32 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
QUALITY CONTROL DATA
R3750952-1
Spike
Units Cone.
LCS
Result
R3750952-2
LCSD
Result
LCS LCSD
% Rec % Rec
% Rec
Limits RPD
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD Qualifiers ---------------------------------------------
1,1 ,2-Trichlorotrifluoroethane
1, 1-Dichloroethene
1, 1-Dichloroethane
Acetone
2-Propanol
Carbon disulfide
Methylene Chloride
Methyl-tert-butyl ether
trans-1 ,2-Dichloroethene
n-Hexane
Vinyl acetate
2-Butanone (MEK)
cis-1 ,2-Dichloroethene
Chloroform
Cyclohexane
1 , 1,1-Trichloroethane
Carbon tetrachloride
Benzene
1 ,2-Dichloroethane
n-Heptane
Trichloroethene
1 ,2-Dichloropropane
1,4-Dioxane (p-Dioxane)
Bromodichloromethane
cis-1 ,3-Dichloropropene
4-Methyl-2-pentanone (MIBK)
Toluene
trans-1 ,3-Dichloropropene
1,1 ,2-Trichloroethane
Tetrachloroethene
2-Hexanone
D ibromoch lorometha ne
1 ,2-Dibromoethane (EDB)
Chlorobenzene
Ethylbenzene
m&p-Xylene
o-Xylene
Styrene
Bromoform
1,1 ,2,2-Tetrachloroethane
4-Ethyltoluene
1 ,3,5-Trimethylbenzene
1 ,2,4-Trimethylbenzene
1 ,3-Dichlorobenzene
1 A-Dichlorobenzene
Benzyl chloride
1 ,2-Dichlorobenzene
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
ppbv
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
7.50
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
3.75
4.33
4.33
4.23
4.70
4.46
4.04
4.29
4.25
4.30
4.28
4.21
4.21
4.28
4.25
4.18
4.35
4.26
4.26
4.39
4.19
4.36
4.25
4.07
4.33
4.19
4.18
4.26
4.24
4.28
4.19
4.11
4.27
4.36
4.20
4.13
8.42
4.11
4.23
4.11
4.30
4.17
4.14
4.11
4.08
4.1 2
4.21
4.01
4.13 115
4.21 115
4.08 113
4.52 125
4.34 119
4.35 108
4.11 114
4.09 113
4.15 115
4.03 114
3.98 112
4.10 112
4.18 114
4.25 113
4.01 111
4.17 116
4.08 114
4.09 114
4.23 117
4.00 112
4.17 116
4.07 113
3.83 109
4.17 115
4.05 112
4.04 111
4.06 114
4.08 113
4.05 114
4.00 112
4.01 110
4.10 114
4.17 116
4.03 112
4.03 110
8.13 112
4.03 110
4.06 113
4.00 110
4.02 115
4.07 111
3.98 110
4.09 110
4.00 109
4.04 110
4.13 112
3.92 107
110 70.0-130
112 70.0-130
109 70.0-130
121 70.0-130
116 70.0-139
116 70.0-130
110 70.0-1 30
109 70 .0-130
111 70 .0-130
107 70.0-130
106 70.0-130
109 70.0-130
111 70.0-130
113 70.0-130
107 70.0-130
111 70.0-130
109 70.0-130
109 70.0-130
113 70.0-130
107 70.0-130
111 70.0-130
109 70.0-130
102 70.0-140
111 70.0-130
108 70.0-130
108 70.0-139
108 70.0-130
109 70.0-130
108 70.0-130
107 70.0-130
107 70.0-149
109 70.0-130
111 70.0-130
107 70.0-130
107 70.0-130
108 70.0-130
107 70.0-130
108 70 .0-130
107 70.0-130
107 70 .0-130
109 70.0-130
106 70.0-130
109 70.0-130
107 70.0-130
108 70.0-130
110 70.0-152
105 70.0-130
4.73
2.81
3.61
3.90
2.73
7.39
4.29
3.84
3.55
6.02
5.62
2.65
2.36
0.00
4.15
4.23
4.32
4.07
3.71
4.64
4.45
4.33
6.08
3.76
3.40
3.41
4.81
3.85
5.52
4.64
2.46
4.06
4.45
4.13
2.45
3.50
1.97
4.10
2.71
6.73
2.43
3.94
0.488
1.98
1.96
1.92
2.27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 01/21/2022 02:42PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
Page 33 of 41
QUALITY CONTROL DATA
Project: BENMAR 897-03
Pace Project No.: 92582172
LABORATORY CONTROL SAMPLE & LCSD: R3750952-1 R3750952-2
Spike LCS LCSD LCS LCSD
Parameter Units Cone. Result Result % Rec % Rec ----
1 ,2,4-Trichlorobenzene ppbv 3.75 4.43 4.21 118 112
Hexachloro-1 ,3-butadiene ppbv 3.75 4.09 4.02 109 107
Naphthalene ppbv 3.75 4.40 4.27 117 114
Allyl chloride ppbv 3.75 4.58 4.04 122 108
2-Chlorotoluene ppbv 3.75 4.21 4.05 112 108
Methyl methacrylate ppbv 3.75 4.17 4.09 111 109
Tetrahydrofuran ppbv 3.75 4.23 4.08 113 109
2,2,4-Trimethylpentane ppbv 3.75 4.28 4.10 114 109
Vinyl bromide ppbv 3.75 4.30 4.22 115 113
lsopropylbenzene (Cumene) ppbv 3.75 4.04 3.91 108 104
1 ,4-Dichlorobenzene-d4 (IS) % 99.4 98.4
% Rec
Limits
70.0-160
70.0-151
70.0-159
70.0-130
70.0-130
70.0-130
70.0-137
70.0-130
70.0-130
70.0-130
60.0-140
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Max
RPD RPD Qualifiers
5.09 25
1.73 25
3.00 25
12.5 25
3.87 25
1.94 25
3.61 25
4.30 25
1.88 25
3.27 25
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 01/21/2022 02:42PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 34 of 41
QUALITY CONTROL DATA
Project: BEN MAR 897-03
Pace Project No.: 92582172
QC Batch: 1804677 Analysis Method: T0-15
QC Batch Method: T0-15 Analysis Description: VOA (MS) T0-15
Laboratory: Pace National -Mt. Juliet
Associated Lab Samples: 92582172002,92582172003,92582172004,92582172005,92582172007, 92582172009
METHOD BLANK: R3751728-3 Matrix: Air
Associated Lab Samples: 92582172002,92582172003,92582172004,92582172005,92582172007,92582172009
Blank Reporting
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Parameter Units Result Limit Analyzed Qualifiers
Benzyl chloride ppbv ND 0.200 01/19/22 1 0:22
Bromoform ppbv ND 0.600 01/19/22 1 0:22
Chloroform ppbv ND 0.200 01/19/22 10:22
2-Chlorotoluene ppbv ND 0.200 01/19/22 10:22
1 ,2-Dichlorobenzene ppbv ND 0.200 01/19/22 10:22
1 ,3-Dichlorobenzene ppbv ND 0.200 01/19/22 1 0:22
1 A-Dichlorobenzene ppbv ND 0.200 01/19/22 1 0:22
1, 1-Dichloroethene ppbv ND 0.200 01/19/22 10:22
cis-1 ,2-Dichloroethene ppbv ND 0.200 01/19/22 10:22
trans-1 ,2-Dichloroethene ppbv ND 0.200 01/19/22 10:22
Ethyl benzene ppbv ND 0.200 01/19/22 10:22
4-Ethyltoluene ppbv ND 0.200 01/19/22 10:22
Hexachloro-1 ,3-butadiene ppbv ND 0.630 01/19/22 10:22
lsopropylbenzene (Cumene) ppbv ND 0.200 01 /19/22 1 0:22
Naphthalene ppbv ND 0.630 01/19/22 1 0:22
Styrene ppbv ND 0.200 01/19/22 1 0:22
1,1 ,2,2-Tetrachloroethane ppbv ND 0.200 01/19/22 10:22
Tetrachloroethene ppbv ND 0.200 01/19/22 1 0:22
1 ,2,4-Trichlorobenzene ppbv ND 0.630 01/19/22 1 0:22
1,1, 1-Trichloroethane ppbv ND 0.200 01/19/22 10:22
1 , 1 ,2-Trichloroethane ppbv ND 0.200 01/19/22 10:22
Trichloroethene ppbv ND 0.200 01/19/22 10:22
1 ,2,4-Trimethylbenzene ppbv ND 0.200 01/19/22 10:22
1 ,3,5-Trimethylbenzene ppbv ND 0.200 01/19/22 10:22
m&p-Xylene ppbv ND 0.400 01/19/22 1 0:22
o-Xylene ppbv ND 0.200 01/19/22 1 0:22
1 ,4-Dichlorobenzene-d4 (IS) % 99.6 60.0-140 01/19/22 10:22
LABORATORY CONTROL SAMPLE & LCSD: R3751728-1 R3751728-2
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Cone. Result Result % Rec % Rec Limits RPD RPD ----
1, 1-Dichloroethene ppbv 3.75 4.18 4.19 111 112 70.0-130 0.239 25
trans-1 ,2-Dichloroethene ppbv 3.75 4.08 4.09 109 109 70.0-130 0.245 25
cis-1 ,2-Dichloroethene ppbv 3.75 4.04 4.09 108 109 70.0-130 1.23 25
Chloroform ppbv 3.75 4.26 4.27 114 114 70.0-130 0.234 25
1,1 , 1-Trichloroethane ppbv 3.75 4.25 4.26 113 114 70.0-130 0.235 25
Trichloroethene ppbv 3.75 4.04 4.07 108 109 70.0-130 0.740 25
1,1 ,2-Trichloroethane ppbv 3.75 4.27 4.28 114 114 70.0-130 0.234 25
Tetrachloroethene ppbv 3.75 4.33 4.34 115 116 70.0-130 0.231 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 01/21/2022 02:42PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 35 of 41
QUALITY CONTROL DATA
Project: BENMAR 897-03
Pace Project No.: 92582172
LABORATORY CONTROL SAMPLE & LCSD: R3751728-1 R3751728-2
Spike LCS LCSD LCS LCSD
Parameter Units Cone. Result Result % Rec % Rec ----
Ethylbenzene ppbv 3.75 4.49 4.50 120 120
m&p-Xylene ppbv 7.50 8.96 9.02 119 120
o-Xylene ppbv 3.75 4.30 4.34 115 116
Styrene ppbv 3.75 4.47 4.51 119 120
Bromoform ppbv 3.75 4.42 4.42 118 118
1,1,2,2-Tetrachloroethane ppbv 3.75 4.44 4.46 118 119
4-Ethyltoluene ppbv 3.75 4.63 4.62 123 123
1,3,5-Trimethylbenzene ppbv 3.75 4.33 4.38 115 117
1 ,2,4-Trimethylbenzene ppbv 3.75 4.42 4.45 118 119
1 ,3-Dichlorobenzene ppbv 3.75 4.77 4.79 127 128
1 A-Dichlorobenzene ppbv 3.75 4.95 4.98 132 133
Benzyl chloride ppbv 3.75 4.78 4.78 127 127
1,2-Dichlorobenzene ppbv 3.75 4.57 4.61 122 123
1,2,4-Trichlorobenzene ppbv 3.75 5.71 5.87 152 157
Hexachloro-1 ,3-butadiene ppbv 3.75 4.17 4.22 111 113
Naphthalene ppbv 3.75 4.83 4.94 129 132
2-Chlorotoluene ppbv 3.75 4.52 4.54 121 121
lsopropylbenzene (Cumene) ppbv 3.75 4.40 4.38 117 117
1 ,4-Dichlorobenzene-d4 (IS) % 101 102
% Rec
Limits
70.0-130
70.0-130
70.0-130
70.0-130
70.0-130
70.0-130
70.0-130
70.0-130
70.0-130
70.0-130
70.0-130
70.0-152
70.0-130
70.0-160
70.0-151
70.0-159
70.0-130
70.0-130
60.0-140
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Max
RPD RPD Qualifiers
0.222 25
0.667 25
0.926 25
0.891 25
0.00 25
0.449 25
0.216 25
1.15 25
0.676 25
0.418 25
0.604 25 LO
0.00 25
0.871 25
2.76 25
1.19 25
2.25 25
0.442 25
0.456 25
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 01/21/2022 02:42PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 36 of 41
QUALITY CONTROL DATA
Project: BENMAR 897-03
Pace Project No.: 92582172
QC Batch: 1805235 Analysis Method: T0-15
QC Batch Method: T0-15 Analysis Description: VOA (MS) T0-15
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Laboratory: Pace National -MI. Juliet
Associated Lab Samples: 92582172002, 92582172003, 92582172006, 92582172008
METHOD BLANK: R3752163-3 Matrix: Air
Associated Lab Samples: 92582172002,92582172003, 92582172006,92582172008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
cis-1 ,2-Dichloroethene ppbv NO 0.200 01/20/22 11:57
Tetrachloroethene ppbv NO 0.200 01/20/22 11 :57
Trichloroethene ppbv NO 0.200 01/20/22 11 :57
1 ,4-Dichlorobenzene-d4 (IS) % 93.3 60.0-140 01/20/22 11:57
LABORATORY CONTROL SAMPLE & LCSD: R3752163-1 R3752163-2
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Cone. Result Result % Rec % Rec Limits RPD RPD ----
cis-1 ,2-Dichloroethene ppbv 3.75 3.28 3.31 87.5 88.3 70.0-130 0.910 25
Trichloroethene ppbv 3.75 3.85 3.82 103 102 70.0-130 0.782 25
Tetrachloroethene ppbv 3.75 4.41 4.35 118 116 70.0-130 1.37 25
1 ,4-Dichlorobenzene-d4 (IS) % 94.4 95.1 60.0-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 01/21/2022 02:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 37 of 41
Project: BENMAR 897-03
Pace Project No.: 92582172
QC Batch: 1805946
QC Batch Method: M18-Mod!T0-15
Associated Lab Samples: 92582172002
METHOD BLANK: R3752278-3
Associated Lab Samples: 92582172002
Parameter
Tetrachloroethene
1,4-Dichlorobenzene-d4 (IS)
Units
ppbv
%
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
T0-15
VOA (MS)T0-15
Laboratory: Pace National -Mt. Juliet
Matrix: Air
Blank
Result
NO
91 .1
Reporting
Limit Analyzed
0.200 01/21/22 10:02
60.0-140 01/21/22 10:02
Qualifiers
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704 )875-9092
LABORATORY CONTROL SAMPLE & LCSD: R3752278-1 R3752278-2
Parameter
Tetrachloroethene
1,4-Dichlorobenzene-d4 (IS)
Units
ppbv
%
Spike
Cone.
3.75
LCS LCSD
Result Result
4.43 4.60
LCS LCSD % Rec Max
% Rec % Rec Limits RPD RPD ------
118 123 70.0-130 3.77 25
94.0 93.8 60.0-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 01/21/2022 02:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 38 of 41
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
QUALIFIERS
Project: BENMAR 897-03
Pace Project No.: 92582172
DEFINITIONS
OF -Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO -Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J -Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
POL -Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S -Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D)-Laboratory Control Sample (Duplicate)
MS(D)-Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPD -Relative Percent Difference
NC -Not Calculable.
SG -Silica Gel -Clean-Up
U-Indicates the compound was analyzed for, but not detected .
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92582172002
(1) Volatile Organic Compounds (MS) by Method T0-15-Surrogate failure due to matrix interference
ANALYTE QUALIFIERS
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
SR Surrogate recovery was below laboratory control limits. Results may be biased low.
Date: 01/21/2022 02:42PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 39 of 41
Project: BEN MAR 897-03
Pace Project No.: 92582172
LabiD Sample 10
92582172001 P-1 #3763
92582172002 P-2 #3722
92582172002 P-2 #3722
92582172002 P-2 #3722
92582172002 P-2 #3722
92582172003 P-3 #1457
92582172003 P-3 #1457
92582172003 P-3 #1457
92582172004 P-4 #3262
92582172004 P-4 #3262
92582172005 P-5 #3793
92582172005 P-5 #3793
92582172006 P-6 #2995
92582172006 P-6 #2995
92582172007 P-7 #3780
92582172007 P-7 #3780
92582172008 P-8 #2846
92582172008 P-8 #2846
92582172009 P-9 #2422
92582172009 P-9 #2422
92582172010 P-10 #3251
Date: 01/21/2022 02:42PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QC Batch Method QC Batch
T0-15 1803836
T0-15 1803836
T0-15 1804677
T0-15 1805235
T0-15 1805946
T0-15 1803836
T0-15 1804677
T0-15 1805235
T0-15 1803836
T0-15 1804677
T0-15 1803836
T0-15 1804677
T0-15 1803836
T0-15 1805235
T0-15 1803836
T0-15 1804677
T0-15 1803836
T0-15 1805235
T0-15 1803836
T0-15 1804677
T0-15 1803836
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Analytical Method Batch
T0-15 1803836
T0-15 1803836
T0-15 1804677
T0-15 1805235
T0-15 1805946
T0-15 1803836
T0-15 1804677
T0-15 1805235
T0-15 1803836
T0-15 1804677
T0-15 1803836
T0-15 1804677
T0-15 1803836
T0-15 1805235
T0-15 1803836
T0-15 1804677
T0-15 1803836
T0-15 1805235
T0-15 1803836
T0-15 1804677
T0-15 1803836
Page 40 of 41
Attachment B
NCDEQ Risk Calculator Results
North Carolina Department of Environmental Quality
Risk Calculator
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site Name: Fonner Danalex Facility
Site Address: 515 E. Alabama Ave.
DEQ Section:
Site ID: P-2
Exposure Unit ID:
Submittal Date:
Prepared By: RLH
Reviewed By: RLH
North Carolina DEQ Risk Calculator
Ea rt Potnt Con«nln1tloru
\'~nion lbt~: JUM1011
Basis: 1\11 1021 EPA RSL T1bk
stt~ m: r.z
t:aposurtUnltiD:
SoD Gu E1 n l'otnl Conr~nlnllkln T•bk
DescriPtion ofEx00$1,lf(l Point CllfiCefllnlion Selottion:
Note: Chemicals highlighted in oringe are noo.volarile chemic.ls. Since these ehemic.Js do not pose 1 ~·•,n intrusion risl;. no risk , .. lues u-e c.lculatod for these ehcmials.
lftht thtmkallbt h tfulnacd front • prior a kula lor ruft, rnncmbtr lo .ckd "SHAH C'hflnkllb" on the •••• ouCpul alltd or -ty •dciH rhnnkah wW !Mil be kldud" in rhk alcubtloru
Exposu.rcl'oint Minimum Maximum Loe.tionof R.•.nacof COtKcnlration Saooili• J>otenti•l Potcntill Ratiooale for
Concmlr•rion Notes: CAS Number Chcmial Concentration Concenlntion Uniu Maximum Detoction Detoction Used for Background Toxicity Value 1\RAIVrBC ARAKITIJC COPC Flag Selection or
(uglmJ) (Qualifier) (Qualifier) Conccntntion frequency Lim irs -V1lue (Scr«ning V1lue """" {YfN) Deletion Lcvel)(nlc)
"' 67#1 "Jm'
69.6 71-43-2 Jknl.cne u,Wm1
6.57 75-15-0 CIIJbonDisulfidc u 'm1
17.3 56--23·5 CartloltTctnoehloridc " m'
373 10&.-90-7 Chlorobcn?.enc u,Rim1
2.09 74-&7·3 Chlouncthanc u 'm) .., 75-71·8 Dichlorodifluoromcllwle m'
26.3 75-34-3 Diehloroclhllnc,l l-u,Riml
3860 107-06-2 Diehloroelhllnc l 2-u2/ml ,.., 75-35-4 Diehlomctlwlcnc I J. u lml
1170 IS6·59-2 l)iehloroedwlcnc ci5-1.2· """'' 426 156~-S Dicltloroeth\·lcnctrans--1.2-"'m'
Ill 110-54--3 llexanc N-uA{ml
33.9 67-63-0 '"""""""' uRfml
127 n-09-2 1'-.lctll\'lcncChk:Jridc m'
33800000 127-18-4 Tctnehloroclt11-'lene 3380000 uA{m1 1'·2 3380000
82.9 108-88-3 Toluene "Wm'
m 71-55-6 Trkhloroethme I I 1-" '
'" 79-00-S Trichloroclhllnc I 12· "' uA{ml P-2 S42
44000 .,., .. Triehloroclh\'knc 44000 """'' P-2 44000
36.5 7S-69-4 1'riehloroflooromelhlll'le " 30.9 75-01-4 Vin\'IChloride """''
Risk for Individual Pathways Output Form 1
Version Date: June 2021
Basis: May 2021 EPA RSL Table
SiteiD: P-2
Ex osure Unit ID:
Dm.ECT CONTACT SOIL AND WATER CALCULA'IlORS
Receptor Pathway Carcinogenici Hazard Index Risk exceeded? Risk
Resident Soil NC NC NC
Groundwater Use* NC NC NC
Non-Residential Worker Soil NC NC NC
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Recreator/Trespasser Soil NC NC NC
Surface Water* NC NC NC
VAPOR INTRUSION CALCULATORS
Receptor Pathway Carcinogenic Hazard Index Risk exceeded? Risk
Groundwater to Indoor Air NC NC NC
Resident Soil Gas to Indoor Air 9.8E-02 2.5E+04 YES
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Non-Residential Worker Soil Gas to Indoor Air 7.4E-03 2.0E+03 YES
Indoor Air NC I NC NC
CONTAMINANT MIGRATION CALCULATORS
Pathway Source Target Receptor Concentrations Exceeded?
Exceedence of 2L at Receptor? Source Soil NC Groundwater Exceedence of2L at Receptor? Source Groundwater NC
Exceedence df 2B at Receptor? Source Soil NC Surface Water Exceedence of 2B at Receptor? Source Groundwater NC
Notes:
1. Iflead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulatiye risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
3. NM =Not Modeled
4. NC = Pathway not calculated
North Carolina DEQ Risk Calculator
DEQ Risk Calculator-Vapot: Intrusion-Non-Residential Worker Soil Gas to Indoor Air
Venion Date: .Jnne2021
Basis: May2021 EPA RSL Table
SiteiD: P"2 'l
Exposure UnitiD:
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
All concentrations are in ug/m3
Calculated
f, Calculated
Soil Gas Target Indoor Target Indoor Air Calculated Non-
CAS# Chemical Name: Concentration Indoor Air Air Cone. for 'Cone. for Non-Carcinogenic Carcinogenic
(ug/m3)
Concentration Carcinogens @ ~arcinogens @ Risk Hazard (ug/m3) TCR= lE-06 , THQ=0.2
' Quotient
67-64-1 Acetone 359 3.59 -2.7E+04 2.6E-05
71-43-2 Benzene 69.6 0.696 1.6E+OO 2.6E+01 4.4E-07 5.3E-03
75-15-0 Carbon Disulfide 6.57 0.0657 -6.1E+02 2.1E-05
56-23-5 Carbon Tetrachloride 17.3 0.173 2.0E+OO 8.8E+01 8.5E-08 3.9E-04
108-90-7 Chlorobenzene 373 3.73 -4.4E+01 1.7E-02
74-87-3 Chloromethane 2.09 0.0209 -7.9E+01 5.3E-05
75-71-8 Dichlorodifluoromethane 3.5 0.035 -8.8E+01 S.OE-05
75-34-3 Dichloroethane, 1,1-26.3 0.263 7.7E+OO -3.4E-08
107-06-2 Dichloroethane 1,2-3860 38.6 4.7E-01 'I 6.1E+OO 8.2E-05 1.3E+OO
75-35-4 Dichloroethvlene, 1,1-3020 30.2 -1.8E+02 3.4E-02
156-59-2 Dichloroethylene cis-1 2-1170 11.7 - -
156-60-5 Dichloroethvlene trans-1,2-426 4.26 -3.5E+01 2.4E-02
110-54-3 Hexane N-111 1.11 -~ 6.1E+02 3.6E-04
67-63-0 Isopropanol 33.9 0.339 -'I 1.8E+02 3.9E-04
75-09-2 Methylene Chloride 127 1.27 1.2E+03 ' 5.3E+02 l.OE-09 4.8E-04
127-18-4 Tetrachloroethvlene 33800000 338000 4.7E+01 3.5E+Ol 7.2E-03 1.9E+03
108-88-3 Toluene 82.9 0.829 -4.4E+03 3.8E-05
71-55-6 Trichloroethane, 1,1,1-772 7.72 -4.4E+03 3.5E-04
79-00-5 Trichloroethane, 1,1,2-543 5.43 7.7E-01 1.8E-01 7.1E-06 6.2E+OO
79-01-6 Trichloroethvlene 44000 440 3.0E+OO ,, 1.8E+OO l.SE-04 S.OE+Ol
75-69-4 Trichlorofluoromethane 36.5 0.365 --
75-01-4 Vinvl Chloride 30.9 0.309 2.8E+OO 8.8E+01 l.lE-07 7.1E-04
I Cumulative: I 7.4E-03 I 2.0E+03 I
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