09058_Midtown_BAR_Metropolitan_20250524

May 20, 2024
Ms. Carolyn Minnich, Brownfields Project Manager
North Carolina Department of Environmental Quality
Division of Waste Management, Brownfield Redevelopment Section
Mail Service Center 1646
Raleigh, North Carolina 27699-1646

Subject: Pre-Redevelopment Assessment Report
Midtown Square Mall
1200 Metropolitan Avenue
Charlotte, North Carolina
Brownfields Project #09058-05-060
Mid-Atlantic Project #H1824.00 – Task 50000

Dear Ms. Minnich:

On behalf of NR Met Property Owner LP (the Prospective Developer or PD) Mid-Atlantic
Associates, Inc. (Mid-Atlantic) has prepared this Pre-Redevelopment Assessment Report
for a portion of the Midtown Square Mall Brownfields property (Brownfields Project
#09058-05-060) to document recent assessment activities conducted between November
2023 and April 2024. The Brownfields property is located at 1200 Metropolitan Avenue,
Mecklenburg County, North Carolina (subject site). The subject site consists of one (1)
parcel of land encompassing approximately 1.3 acres (Parcel #12522705).

The assessment activities were conducted in accordance with the North Carolina
Department of Environmental Quality (NCDEQ) approved Soil Gas Assessment Work
Plan dated October 17, 2023 and In-Situ Soil Characterization Work Plan dated April 11,
2024.

1.0 INTRODUCTION

The subject site is comprised of one (1) approximate 1.3-acre parcel of land that is zoned
Mixed Use Development District (MUDD) and located 0.5 miles southeast of Uptown
Charlotte. The subject site does not have any permanent structures but has recently been
utilized as green space adjacent to the Little Sugar Creek Greenway. The Midtown
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NCDEQ Brownfield Project #09058-05-060
Mid-Atlantic Project #H1824.00 – Task 50000

Square Mall Brownfields property includes the subject site parcel, a north adjacent parcel
which is developed with three (3) mixed use structures collectively known as the
Metropolitan, and an east adjacent parcel developed as a parking lot for a commercial
strip mall. A site layout map is provided as Drawing 1.

2.0 BACKGROUND

The PD has recently begun initial clearing activities ahead of the planned redevelopment
of the subject site. Redevelopment activities include the construction of a mixed-use
building including retail, residential and parking. The foundation for the new building has
ground-floor slab-on-grade at two levels. The lowest level will be utilized as a mechanical
floor which has a small footprint for building support facilities. The first floor includes a
larger footprint that includes lobby/amenities, retail, building operations facilities and
parking uses and incorporates podium construction for the parking garage. The parking
structure is on the first through fifth floors. The building’s sixth through twenty-seventh
floors are residential apartments.

Mid-Atlantic submitted an Environmental Management Plan (EMP) for the planned
redevelopment and received North Carolina Department of Environmental Quality
(NCDEQ) approval on November 30, 2023. As part of redevelopment activities, the PD
and their construction team plan on excavating portions of subject site soils at depths
ranging from 0 to 6 feet below ground surface (ft bgs) prior to advancing their continuous
flight auger (CFA) piles. The areas of excavation will be necessary to bring the CFA pile
areas to grade and install the necessary concrete footer caps. Based on the limited area
for stockpiling on the subject site, the PD will need to export excavated material prior to
mobilizing the deep foundation drilling equipment to the site. As such, it will be necessary
to sample this material in-situ prior to excavation activities. Additionally, the PD
anticipates encountering a large volume of groundwater during advancement of the CFA
piles. Per stipulations in the EMP, groundwater encountered during redevelopment
activities will be allowed to naturally dissipate back into the subsurface. However, the
large volume of groundwater may not be feasible and thus will require alternative storage
methods.

Based on discussions with the PD and Ms. Carolyn Minnich of the Brownfields
Redevelopment Section (BRS), Mid-Atlantic proposes to collect in-situ composite soil
samples in the vicinity of soils proposed for export following excavation activities. Mid-
Atlantic also proposes to advance up to three (3) piezometer borings to determine the
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relative depth to water and hydrogeologic characteristics in areas where the CFA piles
will be advanced. Additionally, no soil vapor samples had been collected on the subject
site. As such, Mid-Atlantic conducted exterior soil vapor sampling in November 2023. A
summary of assessment activities conducted is provided below.

3.0 SCOPE OF WORK

The assessment activities were conducted in general accordance with the NCDEQ
Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup dated
July 2021, NCDEQ Division of Waste Management (DWM) Vapor Intrusion Guidance
dated March 2018, most recent versions of the USEPA Region IV Science and
Ecosystem Support Division (SESD) Field Branches Quality System and Technical
Procedures guidelines, and the NCDEQ approved Soil Gas Assessment Work Plan and
In-Situ Soil Characterization Work Plan dated October 17, 2023 and April 11, 2024,
respectively.

A previous Subsurface Investigation Permit (SIP) was issued through the Mecklenburg
County Environmental Health Department (SIP # 1000417). Mid-Atlantic contacted the
North Carolina public utility locating company (North Carolina 811) to mark utilities at the
proposed sample locations. All sampling locations were documented in the field using a
hand-held global position system (GPS) unit. The sampling locations are depicted on
Drawing 1, and described below:

• Four (4) exterior soil vapor samples (SG-1 through SG-4) were advanced across
the subject site structures to determine potential vapor intrusion risks for future
redevelopment.
• Five (5) composite soil samples (ES-1 through ES-5) were collected in areas
proposed for excavation and off-site disposal during redevelopment activities.
• Three (3) piezometer borings were advanced for the installation of 2” temporary
monitoring wells (TMW-1 through TMW-3) and hydrogeologic characterization.

4.0 BROWNFIELDS ASSESSMENT ACTIVITIES

On November 1 and 2, 2023, Mid-Atlantic contracted with AmeriProbe for the exterior soil
vapor sampling. On April 25 and 26, 2024, Mid-Atlantic contracted with South Atlantic
Environmental Drilling and Construction Company (SAEDACCO) for the soil and
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groundwater assessment activities. The assessment methodology are provided in the
sections below.

4.1 Soil Vapor Implant Installation

AmeriProbe installed four (4) soil vapor implants across the subject site within the
proposed footprint of the future structure. The soil vapor borings were advanced utilizing
a track-mounted Geoprobe® drill rig and DPT drilling methods to a depth of approximately
6.5 ft bgs. The soil vapor implants were installed using 6-inch stainless steel soil vapor
probes inserted to the bottom of each boring and attached to 1/8-inch diameter Nylaflow®
tubing that extended above the ground surface for sample collection. A sand filter pack
was installed in the annulus of the boring to cover 6-inches above the top of the soil vapor
probe followed by a hydrated bentonite seal in the remainder of the borehole to the ground
surface. Following installation of the soil vapor implants, Mid-Atlantic allowed the soil
vapor probes to equilibrate for at least 24 hours prior to conducting a shut-in test, leak
check, and collecting the soil vapor samples. Soil vapor boring logs are provided in
Appendix A.

4.2 Soil Vapor Sampling Methodology

Following implant installation, Mid-Atlantic conducted a leak check at each soil vapor
sampling location by utilizing helium as the tracer compound. The helium was introduced
through a shroud over the probe and entire sampling train to a minimum concentration of
50% as measured using a LandTech Gem™ 5000 helium detector. With the canister
valve closed, Mid-Atlantic checked for the presence of helium from air collected into a
Tedlar® bag using a 60-milliliter syringe connected to the tubing. During the leak check,
Mid-Atlantic collected approximately three purge volumes from each sampling implant
into the Tedlar® bag and field screened each for the absence of Helium prior to opening
the sampling train between the Tedlar® bag and the Summa canister.

During leak check confirmation, helium was not detected in the soil vapor implants
installed at the subject site. Thus, Mid-Atlantic considered the integrity of the soil vapor
implants to be adequate for sampling. Helium concentrations in the shroud, along with
concentrations from each purge volume, were recorded in the field data sheets. Mid-
Atlantic also conducted a shut-in test on the sampling process lines to ensure an air-tight
connection. The shut-in tests were conducted by applying vacuum pressure to the lines
and observing for vacuum pressure loss. Soil vapor sampling forms are included in
Appendix B.
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NCDEQ Brownfield Project #09058-05-060
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Following successful shut-in tests and leak check to verify sample integrity, the soil vapor
samples were collected using laboratory-supplied 1-Liter Summa canisters with
calibrated flow regulators set to 100 milliliters per minute (mL/min) to avoid sample short
circuiting and to further ensure sample integrity. Prior to sampling, vacuum readings,
Summa identification and flow controller identification for each sample were recorded on
the field data sheets. Following field documentation, the sample train was opened to the
Summa flow controller and the Summa canister was opened to allow collection of soil
vapor volume. Sampling was deemed complete when the flow controller exhibited no
greater than -5 inches of mercury (approximately 10 minutes). Following sample
collection, the Summa canisters were closed, the final vacuum reading and sampling time
intervals were recorded on the canister tag, field data sheets, and laboratory chain-of-
custody form. Samples were delivered under proper chain-of-custody protocol to Con-
test (a Pace Analytical laboratory), for analysis of volatile organic compounds (VOCs) by
EPA Method TO-15, plus naphthalene.

4.3 Soil Sampling Methodology

According to the most recent site plan, the PD anticipates needing to excavate and export
approximately 5,000 cubic yards of soil prior to deep foundation drilling activities for the
multi-story residential structure. As such, Mid-Atlantic collected five (5) composite soil
samples (ES-1 through ES-5) in areas proposed for excavation and off-site disposal
during redevelopment activities. Each composite soil sampling area represented
approximately 1,000 cubic yards of the proposed export soil. SAEDACCO advanced four
(4) aliquot soil borings per composite soil sample area to depths ranging from 2 to 6 ft
bgs. Mid-Atlantic collected two (2) soil samples per aliquot sampling location: one (1) was
logged for lithological description and field screened for indication of potential impacts by
observation for staining, unusual odors, and the presence of organic vapors using a
calibrated photoionization detector (PID) and one (1) was placed on ice. The additional
aliquot soil samples placed on ice for each screening interval were collected in this
manner to prevent volatilization (i.e., not homogenized and not screened by the PID).
Following field screening results, the additional aliquot soil samples were collected as
discrete grab samples for laboratory analysis of VOCs from the aliquot soil sample
intervals exhibiting the highest likelihood for impact (i.e., not be collected from the
bag/container used to screen for PID readings). Following VOC sample collection, the
remaining soil volume from the non-volatilized bag was combined and homogenized in a
decontaminated stainless-steel bowl to form one composite soil sample for analysis of
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semi-volatile organic compounds (SVOCs), Resource Conservation and Recovery Act
(RCRA) metals plus hexavalent chromium.

Soil boring logs are provided in Appendix A. The soil samples were collected into
laboratory-supplied glassware and placed on ice for delivery under chain-of-custody
protocol within 24 hours of collection to Waypoint Analytical (Waypoint), a North Carolina
accredited laboratory. Soil samples collected were analyzed for VOCs by EPA Method
8260, SVOCs by EPA Method 8270, RCRA metals plus hexavalent chromium by EPA
Methods 6020/7471/7199.

4.4 Temporary Monitoring Well Installation

SAEDACCO advanced three (3) soil borings past the water table for the installation of
temporary monitoring wells using a track-mounted Geoprobe® drill rig via a combination
of DPT and hollow-stem auger (HSA) methods. The temporary monitoring wells were
advanced to depths ranging from approximately 24 to 34 ft bgs and constructed of 2-inch
polyvinyl chloride riser pipe and 15 feet of 0.010-inch slotted well screen. A sand filter
pack was placed from the bottom of the borings to approximately 2 feet above the top of
the well screens. The wells were then completed by placing a minimum of 2 feet of
hydrated bentonite seal above the sand filter pack. Temporary monitoring well boring logs
with lithologic description, field screening results, and well construction details are
provided in Appendix A.

Upon completion of temporary monitoring well installation activities, the wells were
developed by purging up to three volumes of water from each location. Following
development, the temporary monitoring wells were allowed to equilibrate to static
conditions for a period of 24 hours. Following the 24-hour period, Mid-Atlantic personnel
utilized a decontaminated electronic water level indicator to measure the depth to the
water table relative to the ground surface and to the top of the well casing in each well.
Groundwater was measured at depths ranging from approximately 11.95 ft bgs in well
TMW-3 to 19.8 ft bgs in well TMW-2. Based on top of casing elevation information
collected with the GPS unit and depth to water information measured, groundwater flow
is generally estimated to be to the southwest. A summary of well construction and water
level data is provided in Table 2. A groundwater contour map is depicted on Drawing 2.

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4.5 Groundwater Sampling Methodology

Following the collection of water level readings, Mid-Atlantic collected groundwater
samples from the temporary monitoring wells utilizing low flow/low stress purging
techniques using a peristaltic pump and dedicated polyethylene tubing. The intake point
of the pump tubing was placed in the approximate mid-portion of the screened interval of
the well and purged at a rate no greater than 200 milliliters per minute (mL/min). Mid-
Atlantic utilized a Horiba U-52 Multiparameter water quality meter to collect
measurements of pH, temperature, dissolved oxygen, oxidation reduction potential,
turbidity, and specific conductivity at three to five-minute intervals during the purging
process. Pre-sampling purging was considered complete when the field parameters
stabilized (pH ± 0.1 SU, conductivity varied no more than 5%, and turbidity was less than
10 Nephelometric Turbidity Units [NTUs]). Groundwater samples were collected directly
into laboratory supplied sample containers using the “soda straw” method to minimize the
potential for volatile compound loss through the peristaltic pump head. The sample
containers were labeled with a unique sample identification, date, time, and requested
analysis, and placed in a laboratory supplied cooler with ice. The samples were delivered
to Waypoint in Charlotte, North Carolina under standard chain-of-custody protocol for
analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and RCRA metals
by EPA Methods 6020/7470. Groundwater sampling forms are included in Appendix B.

Following the collection of groundwater samples, Mid-Atlantic conducted slug tests at
each temporary monitoring well using the “slug-out” methodology, also known as a rising-
head slug test. The slug tests were conducted in general accordance with NCDEQ
Performance and Analysis of Aquifer Slug Tests and Pumping Test Policy dated May
2007. The slug tests were performed by removing a slug of water via an approximate 4-
foot dedicated polyethylene bailer. Continuous (i.e., every second) water level data were
collected using a Solinst® Levelogger pressure transducer and data logger.

4.6 Quality Assurance and Quality Control

For quality assurance/quality control (QA/QC) purposes, Mid-Atlantic collected one (1)
duplicate soil vapor sample (DUP-1), one (1) duplicate soil sample (DUP-1), and one (1)
duplicate groundwater sample (DUP-2) which were submitted for the same laboratory
analysis as the parent sample. The duplicate soil vapor sample was collected
simultaneously as the parent sample (SG-1) via a laboratory-supplied “T-connector.”
Samples submitted for laboratory analysis included an adequate sample volume for
laboratory matrix spike (MS) and matrix spike duplicate (MSD) analysis.
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NCDEQ Brownfield Project #09058-05-060
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Nondedicated sampling equipment used for collecting the samples was decontaminated
prior to use at each sampling location. Laboratory QA/QC procedures were employed to
ensure appropriate sample handling and analysis and to aid in the review and validation
of the analytical data. Mid-Atlantic requested that the laboratory include estimated
concentrations for compounds that were detected at levels above the laboratory method
detection limit, but below the laboratory reporting limit (J flags). The laboratory analytical
data report and QA package for each group of samples submitted to and analyzed by the
subcontracted laboratory were provided in an appendix to the final report and included as
Appendix C. Laboratory QA data consistent with Level II documentation was provided
for this project.

4.7 Investigative Derived Waste

Investigative derived waste (IDW) generated during the assessment activities were
managed in general accordance with NCDEQ IHSB Guidelines for Assessment and
Cleanup. Soil generated during soil boring advancement and temporary monitoring well
install was thin spread on-site. The groundwater generated was temporarily staged in 55-
gallon drums and properly labeled. Based on analytical results described below, Mid-
Atlantic proposes to disperse the generated groundwater back to the ground surface
during CFA advancement.

5.0 BROWNFIELDS ASSESSMENT RESULTS

5.1 Soil Vapor Analytical Results

A tabular summary of the soil vapor analytical results is provided in Table 1. The analytical
results were compared to the NCDEQ DWM Residential Sub-slab and Exterior Soil Gas
Screening Levels (SGSLs) dated February 2024. Soil vapor sample laboratory results
indicated the following:

• Several VOCs were detected above laboratory method detection limits in soil vapor
samples collected across the site.
• Of the detected VOCs, only chloroform and ethylbenzene were detected at
concentrations exceeding Residential SGSLs. Chloroform was detected at
concentrations ranging from 4.9 micrograms per cubic meter (µg/m3) to 19 µg/m3.
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NCDEQ Brownfield Project #09058-05-060
Mid-Atlantic Project #H1824.00 – Task 50000

Etyhlbenzene was detected at concentrations ranging from 4.9 micrograms per
cubic meter (µg/m3) to 19 µg/m3.
• No soil gas concentrations exceeded their respective Non-Residential SGSLs.

5.2 Vapor Intrusion Risk Evaluation

The cumulative risk is calculated by entering the maximum concentrations of all
contaminants detected at each established exposure unit (EU) into the NCDEQ Risk
Calculator. An EU is a defined area of a site represented by a specific set of land use(s),
receptors, contaminant concentrations, and exposure pathways. For this assessment, a
“worst case” EU was calculated using the highest concentrations in each sub-slab vapor
sample collected. The NCDEQ Risk Calculator determines the cancer risk sum for all
carcinogens and the cumulative hazard index for all non-carcinogens. The NCDEQ DWM
allows a maximum cancer risk sum for all carcinogens of 1.0 x 10-4 and a maximum non-
carcinogenic hazard index of 1.0. The hazard index is the sum of the hazard quotient
(HQs) calculated for each compound detected. Using the highest concentrations detected
in the “worst case” scenario, Mid-Atlantic utilized the NCDEQ Risk Calculator dated
February 2024 to evaluate the potential cumulative risk for the soil vapor to indoor air
vapor intrusion pathway. Risk calculator results are provided in Appendix D and
summarized in the table below:

Risk Input LICR HI Risk Exceedance?
Worst Case 6.5 x 10-6 0.13 No

As shown in the table above, cumulative risk exceedances were not calculated under the
most conservative residential use from the soil vapor concentrations detected in the
“worst case” scenario. Risk calculator results indicate that there is not likely the potential
for carcinogenic and/or non-carcinogenic vapor intrusion risks to be present within the
ground floor of the future structures.

5.3 Soil Analytical Results

A tabular summary of the soil analytical results is provided in Table 3. The analytical
results were compared to the NCDEQ Residential Preliminary Soil Remediation Goals
(PSRGs) dated February 2024 and Maximum Soil Contaminant Concentrations (MSCCs)
dated September 2022. Additionally, metals results were also compared to mean values
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of background concentrations for North Carolina soils taken from Elements in North
American Soils (Dragun and Chekri, 2005). Soil laboratory results indicated the following:

• Several VOCs and SVOCs were detected above laboratory method detection limits
in soil samples collected. No VOCs were detected above Residential PSRGs.
• Benzo(a)pyrene was detected in ES-1 (0.261 mg/kg), ES-3 (0.365 mg/kg), and ES-
4 (0.468 mg/kg) at concentrations exceeding the Residential PSRG of 0.11 mg/kg.
Dibenz(a,h)anthracene was detected in ES-4 (0.289 mg/kg) at concentrations
exceeding the Residential PSRG of 0.11 mg/kg. Remaining SVOCs were below
Residential PSRGs.
• With the exception of hexavalent chromium, concentrations of metals were below
Residential PSRGs, Residential MSCCs, and/or within the range of background
concentrations for North Carolina soils.
• No VOCs, SVOCs, or metals were detected above their respective
Industrial/Commercial PSRGs.

5.4 Groundwater Analytical Results

A tabular summary of the groundwater analytical results is provided in Table 4. The
analytical results were compared to the 2L Standards dated April 2022. Groundwater
laboratory results indicated the following:

• Several VOCs above laboratory method detection limits in the groundwater
samples collected. Only tetrachloroethylene (PCE) exceeded the 2L Standard of
0.7 micrograms per liter (µg/L) in TMW-2 (7.58 µg/L).
• No SVOCs were detected above laboratory method detection limits.
• The metals arsenic, barium, chromium, and selenium were detected in
groundwater samples collected. However, the concentrations were below their
respective 2L Standards.

5.5 Hydrogeologic Analysis

Mid-Atlantic analyzed the slug testing data using AQTESOLV software and the Bouwer
and Rice (1976) solution for an unconfined aquifer. The results of the slug test evaluation
indicate that the average estimated hydraulic conductivity is approximately 0.084 ft/day
in the surficial aquifer. The slug tests results are included in Appendix E.

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NCDEQ Brownfield Project #09058-05-060
Mid-Atlantic Project #H1824.00 – Task 50000

The average linear groundwater flow velocity of groundwater can be calculated utilizing
the following equation:

Vx = Ki / ne

Where:
Vx = average linear groundwater velocity parallel to groundwater flow direction;
K = hydraulic conductivity;
ne = effective porosity; and
i = hydraulic gradient

Utilizing the hydraulic gradient calculated between TMW-3 and TMW-2 (0.038 ft/ft), the
geometric mean hydraulic conductivity for the shallow aquifer zone (0.084 ft/day), and an
assumed effective porosity of 0.3, the average groundwater flow velocity is estimated to
be approximately 0.01 ft/day (3.88 ft/year) in the shallow surficial aquifer. As such, it is
not likely that the CFA pile advancement will displace a large quantity of water to the
surface.

6.0 SUMMARY AND CONCLUSIONS

Mid-Atlantic has completed Brownfields assessment activities a portion of the Midtown
Square Mall Brownfields property (Brownfields Project #09058-05-060) located at 1200
Metropolitan Avenue in Charlotte, Mecklenburg County, North Carolina. The assessment
activities were conducted in accordance with the NCDEQ approved Soil Gas Assessment
Work Plan dated October 17, 2023 and In-Situ Soil Characterization Work Plan dated
April 11, 2024. The Work Plans were prepared and submitted to 1) characterize pre-
development soil vapor conditions prior to developing the VIMS plan, 2) characterize
proposed export soil in the vicinity of the CFA piles, 3) characterize current groundwater
conditions, and 4) quantify the estimated hydraulic yield of the surficial aquifer during CFA
advancement. A brief summary of the Brownfields assessment activity results are
provided below:

• Several VOCs were detected above laboratory method detection limits in soil vapor
samples across the subject site. Concentrations of chloroform and ethylbenzene
exceeded Residential SGSLs.

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• Risk calculator results indicated that unacceptable risk exceedances were not
calculated under a residential use scenario from the highest soil vapor
concentrations detected.

• With the exception of the SVOCs benzo(a)pyrene and dibenz(a,h)anthracene and
the metal hexavalent chromium, no VOCs, SVOCs, or metals, were detected at
concentrations exceeding Residential PSRGs. No concentrations exceeded
Industrial/Commercial PSRGs.

• Due to the inability to locate existing site monitoring well MW-4 and inaccessibility
of located well MW-3, Mid-Atlantic was unable to collect groundwater samples from
these locations. Based on the condition of monitoring wells MW-1, MW-2, and MW-
3, it is likely that MW-4 is still on-site and will need to be addressed during
redevelopment activities. All site monitoring wells will be properly abandoned
during subsequent redevelopment of the site.

• The VOC PCE was detected above the 2L Standard in temporary monitoring well
TMW-2. Remaining VOCs, SVOCs, and metals were below 2L Standards.

• Slug test results indicate that the average hydraulic conductivity for the surficial
aquifer at the site is approximately 0.084 ft/day which resulted in a calculated
groundwater flow velocity of approximately 0.01 ft/day. As such, future CFA
advancement during the redevelopment of the site will not likely displace a high
volume of water to the surface. The water generated should be allowed to dissipate
into the ground surface per stipulations in the NCDEQ-approved EMP.

The “worst-case” soil vapor results indicate that unacceptable risk levels were not
calculated under non-residential use scenarios for the existing site structures. Risk
calculator results indicate that vapor intrusion risks are likely not present. However, the
PD has elected to proceed with a vapor intrusion mitigation system (VIMS) which was
submitted under separate cover and is pending NCDEQ approval.

Based on analytical results, proposed export soil within the vicinity of the in-situ composite
sampling and CFA piles can be disposed off-site, pending applicable approval, at either
1) an accepting Brownfields property or 2) a Land Clearing and Inert Debris (LCID) landfill
such as Old 27 in Mount Holly, North Carolina. The final disposal location will be approved
by NCDEQ (and accepting Brownfields facility if applicable) and/or Old 27 landfill. As a
precautionary measure, Mid-Atlantic will seek to profile the proposed export soil at a
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Subtitle D Municipal Solid Waste Landfill (MSWLF) such as Republic in Concord, North
Carolina in case a Brownfields transfer and LCID disposal are not permitted. Final
disposal activities will be documented with disposal manifests and submitted to NCDEQ.
Please contact the undersigned if there are questions concerning the results and/or
conclusions reached for this Pre-Redevelopment Assessment Report.

With best regards,

MID-ATLANTIC ASSOCIATES, INC.

Shane Sisco, P.G. Greg D. Icenhour, P.G., MBA
Project Hydrogeologist Principal Geologist

Attachments: Tables
Table 1 – Soil Vapor Analytical Summary
Table 2 – Well Construction and Water Level Elevation Data
Table 3 – Soil Analytical Summary
Table 4 – Groundwater Analytical Summary

Drawings
Drawing 1 – Site and Sample Location Map
Drawing 2 – Groundwater Contour Map
Drawing 3 – Soil Vapor Contaminant Concentration Map
Drawing 4 – Soil Contaminant Concentration Map
Drawing 5 – Groundwater Contaminant Concentration Map

Appendices
Appendix A – Boring Logs and Well Construction Records
Appendix B – Brownfields Sampling Forms
Appendix C – Laboratory Analytical Reports
Appendix D – NCDEQ Risk Calculator (February 2024)

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NCDEQ Brownfield Project #09058-05-060
Mid-Atlantic Project #H1824.00 – Task 50000

Appendix E – Slug Test Results

Mid-Atlantic is authorized to practice engineering by the North Carolina Board of Examiners for Engineers
and Surveyors, License F-0967 and Geology under the North Carolina Board for Licensing of Geologists,
License C-186.

TABLES

TABLE 1
Soil Vapor Analytical SummaryMidtown Square Mall
1200 Metropolitan Avenue, Charlotte, North Carolina
NCDEQ Brownfields Project #09058-05-060Mid-Atlantic Project #H1824.00
Sample ID SG-2 SG-3 SG-4
Sample Depth (ft bgs)6-6.5 6-6.5 6-6.5
Sample Date 11/2/2023 11/2/2023 11/2/2023
Sample Location
VOCs (EPA Method TO-15)
Acetone NE NE --72 73 150 73 71
Benzene 12 160 --7.6 7.6 4.2 8.9 5.6
Bromodichloromethane 2.5 33 --<0.36 1.2 <0.36 <0.36 <0.36
2-Butanone 35,000 440,000 --<6.6 <6.6 12 7.3 <6.6
Carbon Disulfide 4,900 61,000 --35 36 10 17 24
Carbon Tetrachloride 16 200 --0.75 0.81 0.38 0.45 0.78
Chloroform 4.1 53 --19 19 13 5.1 4.9
Chloromethane 630 7,900 --<0.17 0.35 <0.17 <0.17 0.59
Cyclohexane 42,000 530,000 --28 28 7.3 16 22
Dichlorodifluoromethane (Freon 12)700 8,800 --1.3 1.2 1.1 1.3 1.3
Ethanol NE NE --35 36 57 46 52
Ethyl Acetate 490 6,100 --2.2 <2.1 3.3 <2.1 <2.1
Ethylbenzene 3.7 490 --4.5 4.5 3.0 2.5 2.3
4-Ethyltoluene NE NE --0.9 1.0 0.94 0.73 0.67
Heptane 2,800 35,000 --6.6 6.4 3.1 5.0 4.9
Hexane 4,900 61,000 --15 15 <9.3 21 15
Methyl tert-butyl ether (MTBE)360 4,700 --1.0 1.1 <0.35 <0.35 0.53
Methylene chloride 3,400 53,000 --2.3 2.4 2.6 2.0 2.3
4-Methyl-2-pentanone (MIBK)21,000 260,000 --3.6 3.7 4.2 2.9 3.3
Propene 21,000 260,000 --39 40 <3.7 77 23
Styrene 7,000 88,000 --0.66 0.65 0.63 0.5 0.61
Tetrachloroethylene 280 3,500 --110 120 0.79 1.1 <0.51
Tetrahydrofuran 14,000 180,000 --6.5 6.9 7.5 1.8 <1.2
Toluene 35,000 440,000 --54 53 34 27 25
Trichloroethylene 14 180 --0.9 1.1 <0.44 <0.44 <0.44
Trichlorofluoromethane (Freon 11)NE NE --2.3 2.4 6.0 4.4 1.4
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)35,000 440,000 --0.8 1.2 0.43 0.74 0.46
1,2,4-Trimethylbenzene 420 5,300 --4.1 4.4 4.4 3.7 3.8
1,3,5-Trimethylbenzene 420 5,300 --0.77 0.81 0.65 0.59 0.67
m&p-Xylene 700 8,800 --13 13 10 8.2 8.2
o-Xylene 700 8,800 --4.4 4.4 3.6 3.0 3.0
Residential Risk Calculator
LICR ----< 1.00E-04
Non-Carcinogenic HI ----< 1
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) Division of Waste Management (DWM) Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) (February 2024).
2) NCDEQ DWM Risk Calculator (February 2024).
3) Risk Calculator results were calculated using the highest concentrations of each constituent detected in soil vapor samples across entire site.
Only compounds detected in at least one sample are shown
Compound concentrations are reported to the laboratory method detection limits
Laboratory analytical methods are shown in parantheses
values indicate the VOC was below the laboratory method reporting limit
Bold values indicates the an exceedance of the Residential SGSL or the cumulative LICR/HI exceeds the risk level
VOCs = volatile organic compounds
LICR = Lifetime Incremental Carcinogenic Risk; HI = Hazard Index
NE = Not Established; -- = Not Applicable
ft bgs = feet below ground surface
J = estimated concentration between laboratory method detection limit and reporting limit
SGSLs (1)
DEQ Acceptable Cumulative Risk
Levels (3)
SG-1 / DUP-1
Residential Non-Residential
6-6.5
11/2/2023
Proposed Mixed-Use High Rise
TABLE 2
Well Construction and Water Level Elevation Data
Midtown Square Mall
1200 Metropolitan Avenue, Charlotte, North Carolina
NCDEQ Brownfield Project #09058-05-060
Mid-Atlantic Project #H1824.00
Well ID Total Depth
(ft bgs)
Screen Depth
(ft bgs)
Depth to Water
(ft TOC)
TOC Elevation
(ft amsl)
Water Elevation
(ft amsl)
TMW-1 29.0 14.0 - 29.0 19.30 101.01 81.71
TMW-2 34.0 19.0 - 34.0 19.80 99.65 79.85
TMW-3 24.0 9.0 - 24.0 11.95 99.08 87.13
Notes:
1) Depth to water measurements were collected on April 26, 2024
ft bgs = feet below ground surface
TOC = top of casing
TABLE 3Soil Analytical SummaryMidtown Square Mall1200 Metropolitan Avenue, Charlotte, North CarolinaNCDEQ Brownfield Project #09058-05-060Mid-Atlantic Project #H1824.00
Sample ID ES-1 ES-1E ES-2 ES-2E ES-3 ES-3A ES-4 ES-4B ES-5 ES-5E
Sample Depth (ft bgs)--1-2 --1-2 --1-2 --1-2 --4-5 --4-5
Sample Date 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024
PID Results (ppm)--2.8 --2.6 --2.9 --2.9 --7.0 --10.3
Sample Location
VOCs (EPA Method 8260)
Acetone 14,000 210,000 NA 0.058 NA 0.016 J NA 0.027 NA 0.021 J NA 0.036 NA 0.017 J
Carbon Disulfide 160 740 NA <0.0008 NA 0.0007 J NA 0.001 J NA <0.0007 NA <0.0009 NA <0.0009
Methylene Chloride 58 650 NA 0.003 J NA 0.003 J NA 0.003 J NA 0.003 J NA 0.004 J NA 0.007 J
Naphthalene 2.1 8.8 NA <0.001 NA <0.001 NA 0.055 NA <0.001 NA <0.001 NA <0.001
Tetrachloroethylene NA <0.001 NA <0.001 NA <0.001 NA <0.001 NA <0.001 NA <0.001
Trichloroethylene NA <0.001 NA <0.001 NA <0.001 NA <0.001 NA <0.001 NA <0.001
SVOCs (EPA Method 8270)
Anthracene 3,600 45,000 <0.194 NA <0.188 NA <0.193 NA <0.192 NA 0.225 J NA <0.216 NA
Benzo(a)anthracene 1.1 21 0.280 J NA <0.177 NA 0.437 J NA <0.181 NA 0.623 J NA <0.203 NA
Benzo(a)pyrene 0.11 2.1 0.261 J NA <0.187 NA 0.365 J NA <0.191 NA 0.468 J NA <0.215 NA
Benzo(b)fluoranthene 1.1 21 0.333 J NA <0.166 NA 0.518 J NA <0.170 NA 0.860 NA <0.191 NA
Benzo(g,h,i)perylene NE NE <0.168 NA <0.163 NA 0.221 J NA <0.167 NA 0.263 J NA <0.187 NA
Chrysene 110 2,100 0.210 J NA <0.165 NA 0.331 J NA <0.169 NA 0.475 J NA <0.190 NA
Dibenz(a,h)anthracene 0.11 2.1 <0.129 NA <0.125 NA <0.129 NA <0.128 NA 0.289 J NA <0.144 NA
Fluoranthene 480 6,000 0.401 J NA 0.203 J NA 0.932 NA 0.210 J NA 1.30 NA <0.205 NA
Indeno(1,2,3-cd)pyrene 1.1 21 0.201 J NA <0.171 NA 0.318 J NA <0.175 NA 0.399 J NA <0.196 NA
Phenanthrene NE NE 0.231 J NA <0.179 NA 0.683 J NA <0.183 NA 0.850 NA <0.205 NA
Pyrene 360 4,500 0.350 J NA <0.181 NA 0.602 J NA <0.185 NA 0.819 NA <0.208 NA
RCRA Metals (EPA Methods 6020/7471/7199)
Arsenic 0.68 3.0 1.46 NA 1.20 NA 1.33 NA 1.22 NA 0.88 NA 3.55 NA
Barium 3,100 47,000 70.6 NA 74.7 NA 77.6 NA 74.8 NA 74.6 NA 78.0 NA
Cadmium 1.4 20 0.0835 J NA 0.0670 J NA 0.0628 J NA 0.0494 J NA 0.0339 J NA 0.0375 J NA
Chromium (total)NE NE 34.2 NA 35.2 NA 44.8 NA 44.4 NA 26.0 NA 54.1 NA
Trivalent Chromium 23,000 350,000 33.935 NA 34.786 NA 44.473 NA 43.93 NA 25.639 NA 53.716 NA
Hexavalent Chromium 0.31 6.5 0.265 NA 0.414 B NA 0.327 B NA 0.470 B NA 0.361 B NA 0.384 B NA
Lead 200*800*13.1 NA 9.88 NA 8.63 NA 6.79 NA 5.89 NA 5.61 NA
Mercury 2.3 9.7 0.0292 J NA 0.0170 J NA 0.0219 J NA 0.0141 J NA <0.0147 NA <0.0156 NA
Selenium 78 1,200 0.347 NA 0.30 NA 0.279 J NA 0.209 J NA 0.249 J NA 0.189 J NA
Silver 78 1,200 0.102 J NA 0.107 J NA 0.0772 J NA 0.0719 J NA 0.0328 J NA 0.0426 J NA
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) Preliminary Soil Remediation Goals (PSRGs) (February 2024).
2) Each composite soil sampling area (ES-1 through ES-5) represented approximately 1,000 cubic yards of the proposed export soil.
* = No PSRGs established for this compound. NCDEQ Maximum Soil Contaminant Concentrations (MSCCs) dated September 2022 used instead.
Only compounds detected in at least one sample are shown
Compound concentrations are reported in milligrams per kilogram (mg/kg)
Compound concentrations are reported to the laboratory method detection limits
Laboratory analytical methods are shown in parantheses
Bold values indicates the an exceedance of the Residential PSRG and/or mean background levels for metals
PID = photoionization detector
ppm = parts per million
VOCs = volatile organic compounds
SVOCs = semi-volatile organic compounds
RCRA = Resource Conservation and Recovery Act
ft bgs = feet below ground surface
NE = Not Established; -- = Not Applicable
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
B = compound detected in laboratory blank
values indicate the concentration was below the laboratory method detection limit
Proposed Export Soil Area
4/26/2024
PSRGs (1)
Residential Industrial/
Commercial
TABLE 4
Groundwater Analytical Summary
Midtown Square Mall
1200 Metropolitan Avenue, Charlotte, North Carolina
NCDEQ Brownfield Project #09058-05-060
Mid-Atlantic Project #H1824.00
Sample ID TMW-2 TMW-3
Sample Date 4/27/2027 4/27/2024
Sample Location West Site East Site
VOCs (EPA Method 8260)
Acetone 6,000 1.83 J <1.80 1.86 J 3.73 J
Chloroform 70 1.50 1.64 <0.220 4.72
cis-1,2-Dichloroethene 70 5.88 5.94 2.11 <0.200
2-Hexanone 40 0.501 J 0.511 J <0.380 1.56 J
Tetrachloroethene 0.7 0.422 J 0.341 J 7.58 0.337 J
Trichloroethene 3.0 <0.180 <0.180 1.62 <0.180
SVOCs (EPA Method 8270)--BRL BRL BRL BRL
RCRA Metals (EPA Methods 6020/7471)
Arsenic 10 0.414 J 1.21 <0.297 0.495 J
Barium 700 35.3 34.0 21.7 67.3
Chromium (total)10 <0.346 0.946 J 1.91 1.65
Selenium 20 <0.703 0.887 J 0.706 J <0.703
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) 15A NCAC 02L .0202 Groundwater Quality Standards (2L Standards) (April 2022).
Only compounds detected in at least one sample are shown
Compound concentrations are reported to the laboratory method detection limits
Laboratory analytical methods are shown in parantheses
Bold values indicates the an exceedance of the 2L Standard
VOCs = volatile organic compounds
SVOCs = semi-volatile organic compounds
RCRA = Resource Conservation and Recovery Act
BRL = Below Reporting Limits
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
values indicate the concentration was below the laboratory method detection limit
2L
Standards (1)
TMW-1 / DUP-2
4/27/2024
Northwest Site

DRAWINGS

!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
@A@A
@A
ES-1
ES-2
ES-3 ES-4
ES-5
TMW-3
TMW-2
TMW-1
SG-1SG-2
SG-3
SG-4
´
DRAWN BY:DATE: MAY 2024
JOB NO.: H1824.00
GIS NO.: 03G-H1824.00-02
DRAWING NO.: 1
Legend
@A TemporaryMonitoring Well
!(In-Situ Aliquot SoilBoring
!(Soil Vapor Sample
In-Situ Sampling Grid
Subject Property05010015020025Feet
1 inch = 50 feet
MSS
GCI
KRC
AGH
@A@A
@A
TMW-3TMW-2
TMW-1
(81.71)
(79.85)(87.13)
81
83
85
87
81
83 85
87
´
DRAWN BY:
Legend
@A TemporaryMonitoring Well
GroundwaterElevation (ft amsl)
Groundwater Contour(ft amsl)
EstimatedGroundwater FlowDirection
Subject Property05010015020025Feet
1 inch = 50 feet
MSS
GCI
AGH
Notes:1.) Groundwater levels wereguaged on April 26, 2024.
81
(79.85)
!(
!(
!(
!(
SG-1SG-2
SG-3
SG-4
DRAWN BY:
3
MSS
GCI
AGH
0 50 100 150 20025Feet
1 inch = 50 feet
´
Notes:
1 ) Only concentrations exceeding applicable regulatory standards are shown.2 ) Concentrations are in micrograms per cubic meter (µg/m3)3 ) Soil vapor results compared to NCDEQ Residential PSRGs dated February 2024.
Legend
!(Soil Vapor Sample
Subject Property
Chloroform 13
SG-211/2/2024
Chloroform 5.1
SG-311/2/2024
Chloroform 13
SG-211/2/2024
Sample ID
Date ofCollection
Constituent Concentration
Chloroform 19 / 19Ethylbenzene4.5 / 4.5
SG-1 / DUP-111/2/2024
Chloroform 4.9
SG-411/2/2024
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
ES-5
ES-1
ES-2 ES-4ES-3
DRAWN BY:
DRAFT CHECK
BY:
ENGINEER CHECK
BY:
APPROVED
BY:
SOIL COMPOUND CONCENTRATION MAP
MIDTOWN SQUARE MALL
1200 METROPOLITAN AVENUE
CHARLOTTE, NORTH CAROLINA
REFERENCE: BOUNDARY DATA FROM MECKLENBURG COUNTY GIS. 2022 AERIAL IMAGERY FROM NCONE MAP. 1/16TH BUILDING SITE PLAN PROVIDED BY SK+I ARCHITECTURE DATED MAY 2023. GRADING OVERLAY PROVIDED BY NORTHWOOD RAVIN.
DATE: MAY 2024
JOB NO.: H1824.00
GIS NO.: 03G-H1824.00-05
DRAWING NO.: 4
MSS
GCI
AGH
0 50 100 150 20025Feet
1 inch = 50 feet
´
Notes:
1 ) Only concentrations exceeding applicable regulatory
standards are shown.
2 ) Concentrations are in milligrams per kilogram (mg/kg)
3 ) Soil results compared to NCDEQ Residential PSRGs
dated February 2024.
4 ) Highlighted soil aliquots indicate VOC grab sample.
Legend
!(In-Situ Aliquot Soil
Boring
In-Situ Sampling
Grid
Subject Property
Benzo(a)pyrene 0.261 J
ES-1
4/26/2024
Chromium (IV)0.414
ES-2
4/26/2024
Sample ID
Date of
Collection
Constituent Concentration
Chromium (IV)0.414
ES-2
4/26/2024
Benzo(a)pyrene 0.365 J / <0.191
Chromium (IV)0.327 / 0.470
ES-3 / DUP-1
4/26/2024
Benzo(a)pyrene 0.468 J
Dibenz(a,h)anthracene 0.289 J
Chromium (IV)0.361
ES-4
4/26/2024
Benzo(a)pyrene 0.384
ES-5
4/26/2024
A
EC
D
B
A
A
A
A
B
B
B
B
C
C
C
CD
D
D
D
E
E
E
E
@A@A
@A
TMW-1
TMW-2 TMW-3
DRAWN BY:
5
MSS
GCI
AGH
0 50 100 150 20025Feet
1 inch = 50 feet
´
Notes:
1 ) Only concentrations exceeding applicable regulatory standards are shown.2 ) Concentrations are in micrograms per liter (µg/L)3 ) Groundwater results compared to NCDEQ 2L Standards dated April 2022.
Legend
@A TemporaryMonitoring Well
Subject Property
PCE 7.58
TMW-24/27/2024
Sample ID
Date ofCollection
Constituent Concentration
PCE 7.58
TMW-24/27/2024
APPENDIX A
Boring Logs and Well Construction Records

APPENDIX B
Brownfields Sampling Forms

ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
18 18
19 19
15 15
16 16
17 17
12 12
13 13
14 14
8
9 9
10 10
11 11
5
6 6
7 7
8
1
Red Silty CLAY
1
2 2
3 3
4 4
5
SOIL DESCRIPTION Construction Details
None ----
Date Completed:Monitoring Equipment:MAA Field Staff:
Date Started: Driller :DTW (ft):
Location: Subcontractor/Drillers: Vapor Screen (ft):
Project Number:Sampling Method: Vapor Probe Depth (ft):
Site Name: Drilling/Boring Method: Boring Depth (ft):
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
LOG OF BORING: SG-1
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
18 18
19 19
15 15
16 16
17 17
12 12
13 13
14 14
8
9 9
10 10
11 11
5
6 6
7 7
8
1
Red Silty CLAY
1
2 2
3 3
4 4
5
SOIL DESCRIPTION Construction Details
None ----
Date Completed:Monitoring Equipment:MAA Field Staff:
Date Started: Driller :DTW (ft):
Location: Subcontractor/Drillers: Vapor Screen (ft):
Project Number:Sampling Method: Vapor Probe Depth (ft):
Site Name: Drilling/Boring Method: Boring Depth (ft):
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
LOG OF BORING: SG-2
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
18 18
19 19
15 15
16 16
17 17
12 12
13 13
14 14
8
9 9
10 10
11 11
5
6 6
7 7
8
1
Red Silty CLAY
1
2 2
3 3
4 4
5
SOIL DESCRIPTION Construction Details
None ----
Date Completed:Monitoring Equipment:MAA Field Staff:
Date Started: Driller :DTW (ft):
Location: Subcontractor/Drillers: Vapor Screen (ft):
Project Number:Sampling Method: Vapor Probe Depth (ft):
Site Name: Drilling/Boring Method: Boring Depth (ft):
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
LOG OF BORING: SG-3
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
None ----
16 16
17 17
18 18
19 19
12 12
13 13
14 14
15 15
8
9 9
10 10
11 11
5
6 6
7 7
8
1 1
2 2
3 3
4 4
5
SOIL DESCRIPTION Construction Details
Red Silty CLAY
Date Completed:Monitoring Equipment:MAA Field Staff:
Date Started: Driller :DTW (ft):
Location: Subcontractor/Drillers: Vapor Screen (ft):
Project Number:Sampling Method: Vapor Probe Depth (ft):
Site Name: Drilling/Boring Method: Boring Depth (ft):
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
LOG OF BORING: SG-4
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
13
----
--
15
9
11
1
3
5
17
18
19
14 14
10 10
12 12
15
16
17
18
19
16
7
9
11
13
6 6
8 8
2 2
4 4
SOIL DESCRIPTION Construction Details
1
3
5
7
Grass and Brown SILT
Date Completed:Monitoring Equipment:MAA Field Staff:
Date Started: Driller :DTW (ft):
Location: Subcontractor/Drillers: Screen Depth (ft):
Project Number:Sampling Method:Well Depth (ft):
Site Name: Drilling/Boring Method: Boring Depth (ft):
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
LOG OF BORING: TMW-1
Page:1 of 2
Tannish Brown Clayey SILT
Orangish Brown Clayey SILT
Brown Clayey SILT
--
----
----None
None
None
None
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
40 40
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
27
29
31
None ----
38
32 32
34 34
33
26 26
28 28
30
37
39
37
39
21
23
30
22 22
24 24
SOIL DESCRIPTION Construction Details
38
36 36
35
25
27
29
31
33
35
21
23
25
Date Started: Driller :DTW (ft):
Location: Subcontractor/Drillers: Screen Depth (ft):
Date Completed:Monitoring Equipment:MAA Field Staff:
Site Name: Drilling/Boring Method: Boring Depth (ft):
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
H1824.00 Task 50,000 Hollow Stem Auger
----None
Tan Sandy Clayey SILT
Tannish Brown Clayey SILT
Stefan Smith
3576A
SAEDACCO
1000417
X
4-25-24 TMW-1
Metropolitan Redevelopment
1200 Metropolitan Ave., Charlotte, NC, 28204
Mecklenburg
35.211639 80.836017
X
X
1
29
19.8
8.25"
HSA
0 14 2 SCH-40 PVC
14 29 2 .010 SCH-40 PVC
12 29 Sand 2
0 17 Silt
17 29 Sandy silt
Bentonite seal from 10 to 12'
4/30/2024
Stefan Smith
3576A
SAEDACCO
1000417, ,
X
4-26-24
Metropolitan Redevelopment
1200 Metropolitan Ave, Charlotte, NC 28204
Mecklenburg
35.211639 80.836017
TMW-1
29
2
19.8
19
15
1
2.4
X
Bentonite.:39lb ,Wtr:gal.
Pour
4/30/2024
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
LOG OF BORING: TMW-2
Page:1 of 2
H1824.00 Task 50,000 Hollow Stem Auger 34.0
Midtown Square Mall Hollow Stem Auger 34.0
4/25/2024 Stefan Smith 19.80
1200 Metropolitan Avenue, Charlotte, NC Saedacco 19 - 34
SOIL DESCRIPTION Construction Details
None ----
Date Completed:Monitoring Equipment:MAA Field Staff:
1 1
2 2
3 3
4 4
5 5
None ----
6 6
7 7
8 8
9 9
10 10
None ----
11 11
12 12
13 13
14 14
15 15
None ----
16 16
17 17
18 18
19 19
Grass and Brown SILT
Brown Clayey SILT
Yellowish Brown Clayey SILT
Orangish Brown Clayey SILT
Grayish Brown SILT
Black and Brown Clayey SILT
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
40 40
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
LOG OF BORING: TMW-2
Page:2 of 2
H1824.00 Task 50,000 Hollow Stem Auger 34.0
Midtown Square Mall Hollow Stem Auger 34.0
4/25/2024 Stefan Smith 19.80
Metropolitan Avenue, Charlott Saedacco 19 - 34
SOIL DESCRIPTION Construction Details
None ----
Yellowish Brown Clayey SILT
Date Completed:Monitoring Equipment:MAA Field Staff:
21 21
22 22
23 23
24 24
25 25
None ----
26 26
27 27
28 28
34 34
Yellow Sandy Clayey SILT----None
29 29
30 30
31 31
38 38
39 39
35 35
36 36
37 37
32 32
33 33
Stefan Smith
3576A
SAEDACCO
1000417
X
4-25-24 TMW-2
Metropolitan Redevelopment
1200 Metropolitan Ave., Charlotte, NC, 28204
Mecklenburg
35.211237 80.836369
X
X
1
34
19.4
8.25"
HSA
0 19 2 SCH-40 PVC
19 34 2 .010 SCH-40 PVC
17 34 Sand 2
0 20 Silt
20 34 Sandy silt
Bentonite seal from 15 to 17'
4/30/2024
Stefan Smith
3576-A
SAEDACCO
1000417, ,
X
4-26-24
Metropolitan Redevelopment
1200 Metropolitan Ave, Charlotte, NC 28204
Mecklenburg
35.211237 80.836369
TMW-2
34
2
19.4
19
15
1
2.4
X
Bentonite.:49lb ,Wtr:gal.
Pour
4/30/2024
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
LOG OF BORING: TMW-3
Page:1 of 2
H1824.00 Task 50,000 Hollow Stem Auger 24.0
Midtown Square Mall Hollow Stem Auger 25.0
4/25/2024 Stefan Smith 11.95
1200 Metropolitan Avenue, Charlotte, NC Saedacco 9 - 24
SOIL DESCRIPTION Construction Details
None ----
Grass and Brown Clayey SILT
Date Completed:Monitoring Equipment:MAA Field Staff:
1 1
2 2
3 3
4 4
5 5
None ----
6 6
7 7
8 8
9 9
Tan Sandy Clayey SILT
10 10
None ----
11
19
11
12 12
13 13
14 14
15 15
19
None ----
16 16
17 17
18 18
Orangish Brown Clayey SILT
Brown Clayey SILT
Tan Sandy Clayey SILT
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
40 40
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
Site Name: Drilling/Boring Method: Boring Depth (ft):
1125 E. Morehead Street, Suite 104.Charlotte, NC 28204Ph: [phone]
LOG OF BORING: TMW-3
Page:2 of 2
Metropolitan Avenue, Charlott Saedacco 9 - 24
H1824.00 Task 50,000 Hollow Stem Auger 24.0
4/25/2024 PID MiniRae 3000 Troy Holzschuh
4/25/2024 Stefan Smith 11.95
21 21
22 22
23 23
Tan Sandy Clayey SILT
SOIL DESCRIPTION Construction Details
None ----
34
27
28 28
29 29
30 30
24 24
25 25
26 26
27
38
39 39
35 35
36 36
37 37
38
31 31
32 32
33 33
34
Stefan Smith
3576A
SAEDACCO
1000417
X
4-25-24 TMW-3
Metropolitan Redevelopment
1200 Metropolitan Ave., Charlotte, NC, 28204
Mecklenburg
35.211309 80.835742
X
X
1
24
12
8.25"
HSA
0 9 2 SCH-40 PVC
9 24 2 .010 SCH-40 PVC
7 24 Sand 2
0 17 Silt
17 24 Sandy silt
Bentonite seal from 5 to 7'
4/30/2024
Stefan Smith
3576A
SAEDACCO
1000417, ,
X
4-26-24
Metropolitan Redevelopment
1200 Metropolitan Ave. Charlotte, NC 28204
Mecklenburg
35.211309 80.835742
TMW-3
24
2
12.35
9
15
1
>2
X
Bentonite.:33lb ,Wtr:gal.
Pour
4/30/2024
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):5.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-1A
Page:1 of 1
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.0 --
None 0.3
3 3
4 4
5 5
1 1
None 0.0 --
2 2
None 0.5 --
--
Dry Brown Gravelly CLAY
6 6
7 7
8 8
14 14
9 9
10 10
11 11
18 18
19 19
None 0.2 --
15 15
16 16
17 17
12 12
13 13
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
Dry Red Brown Gravelly Silty CLAY
Dry Red Brown Gravelly CLAY
19 19
17
18 18
16 16
17
14 14
15 15
12
13 13
11 11
12
9 9
10 10
7 7
8 8
5 5
6 6
3 3
None 1.2 --
4 4
1 1
None 1.5 --
2 2
None 1.7 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 1.4 --
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):4.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-1B
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 1.0 --
4 4
1 1
None 1.2 --
2 2
None 1.4 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 1.1 --
Dry Red Brown Gravelly Silty CLAY
Dry Red Brown CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):4.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-1C
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 2.1 --
4 4
1 1
None 1.0 --
2 2
None 1.5 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.9 --
Dry Red Brown Gravelly Silty CLAY
Dry Red Brown CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):4.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-1D
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 2.1 --
4 4
None 2.2 --
1 1
None 2.8 ES-1E
(1-2)2 2
None 2.4 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.7 --
Dry Red Brown CLAY
Dry Red Brown Silty CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):5.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-1E
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
4 4
1 1
None 2.2 --
2 2
None 1.5 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 1.8 --
Dry Red Brown Gravelly CLAY
Dry Red Brown Silty CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):3.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-2A
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
18 18
19 19
Dry Red Brown CLAY
Dry Red Brown Gravelly Silty CLAY
15 15
16 16
17 17
12 12
13 13
14 14
9 9
10 10
11 11
6 6
7 7
8 8
3 3
4 4
5 5
1 1
None 1.4 --
2 2
None 1.3
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.8 --
--
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):3.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-2B
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
18 18
19 19
Dry Red Brown Gravelly CLAY
15 15
16 16
17 17
12 12
13 13
14 14
9 9
10 10
11 11
6 6
7 7
8 8
3 3
4 4
5 5
1 1
None 0.8 --
2 2
None 1.2 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.4 --
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):3.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-2C
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
18 18
19 19
None 0.7 --
15 15
16 16
17 17
12 12
13 13
14 14
9 9
10 10
11 11
6 6
7 7
8 8
3 3
4 4
5 5
1 1
None 1.0 --
2 2
None 1.1
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.9 -- Dry Red Brown and Tan Gravelly Silty CLAY
-- Dry Red Brown Gravelly CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):4.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-2D
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 1.9 --
4 4
1 1
None 2.6 ES-2E
(1-2)2 2
None 2.1 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 2.5 --
Dry Red Brown Gravelly Silty CLAY
Dry Red Brown CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):4.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-2E
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS: DUP-1 (1-2) sampled from ES-3A (1-2).
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 2.6 --
4 4
1 1
None 2.9 ES-3A
(1-2)
Dry Red Brown CLAY
2 2
None 2.7
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 1.7 -- Dry Red Brown Gravelly CLAY
--
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):4.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-3A
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
18 18
19 19
15 15
16 16
17 17
12 12
13 13
14 14
9 9
10 10
11 11
6 6
7 7
8 8
3 3
4 4
5 5
1 1
None 1.1 --
2 2
None 1.2 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.6 --
Dry Red Brown CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):3.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-3B
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 0.3 --
4 4
1 1
None 0.6 --
2 2
None 0.6 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.4 --
Dry Red Brown and Tan Silty CLAY
Dry Red Brown Gravelly CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):4.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-3C
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 0.3 --
4 4
1 1
None 0.0 --
2 2
None 0.0 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.0 --
Dry Red Brown CLAY
Dry Brown and Red Brown CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):4.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-3D
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 0.3 --
4 4
None 0.0 --
1 1
None 0.2 --
2 2
None 0.5 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.2 --
Dry Red Brown Silty CLAY
Dry Red Brown CLAY
Dry Red Brown Gravelly CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):5.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-3E
Page:1 of 1
ft
-
b
g
s
Odors
PI
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(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
Dry Red Brown Gravelly CLAY
Dry Brown and Tan Silty CLAYNone 6.6 --
Dry Red CLAY
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 3.9 --
4 4
None 4.8
1 1
None 4.5 --
2 2
None 3.9 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 4.2 --
--
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):6.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-4A
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 6.0 --
Dry Red Brown and Black CLAY4 4
None 7.0
1 1
None 4.4 --
2 2
None 6.0 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 3.2 --
ES-4B
(4-5)
Dry Red Brown CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):5.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-4B
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
19 19
Dry Red Brown CLAY
16 16
17 17
18 18
13 13
14 14
15 15
10 10
11 11
12 12
7 7
8 8
9 9
5 5
None 3.9 -- Dry Orange and Red Brown CLAY
6 6
3 3
None 2.7 --
4 4
None 2.9 --
1 1
None 3.4 --
2 2
None 2.9
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 3.4 --
--
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):6.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-4C
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
19 19
Dry Red Brown and Orange CLAY
Dry Red CLAY
16 16
17 17
18 18
13 13
14 14
15 15
10 10
11 11
12 12
7 7
8 8
9 9
5 5
None 4.8 --
6 6
3 3
None 4.8 --
4 4
None 4.3
1 1
None 6.2 --
2 2
None 5.7 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 5.3 --
--
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):6.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-4D
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
19 19
Dry Orange and Red Brown Silty CLAY
Dry Red Brown CLAY
16 16
17 17
18 18
13 13
14 14
15 15
10 10
11 11
12 12
7 7
8 8
9 9
5 5
None 5.4 -- Dry Orange and Red Brown Clayey SILT
6 6
3 3
None 4.7 --
4 4
None 5.2 --
1 1
None 5.3 --
2 2
None 5.9 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 4.2 --
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):6.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-4E
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 1.3 --
Dry Red Brown CLAY4 4
None 2.4
1 1
None 0.6 --
2 2
None 1.7 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.5 --
Dry Red Brown CLAY
Dry Red Brown Gravelly CLAY
--
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):5.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-5A
Page:1 of 1
ft
-
b
g
s
Odors
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 0.3 --
4 4
1 1
None 0.8 --
2 2
None 0.5 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.0 --
Dry Red Brown CLAY
Dry Red Brown and Tan Gravelly CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):4.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-5B
Page:1 of 1
ft
-
b
g
s
Odors
PI
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(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 0.5 --
4 4
None 0.2
1 1
None 0.0 --
2 2
None 0.0 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.0 --
Dry Red Brown CLAY
--
Dry Tan and Orange Silty CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):5.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-5C
Page:1 of 1
ft
-
b
g
s
Odors
PI
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(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
Dry Red Brown CLAY
Dry Red Brown Gravelly CLAY
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 0.8 --
4 4
None 0.7
1 1
None 0.7 --
2 2
None 0.4 --
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.0 --
--
Dry Orange and Tan Silty CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):5.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-5D
Page:1 of 1
ft
-
b
g
s
Odors
PI
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(
p
p
m
)
La
b

S
a
m
p
l
e
ft
-
b
g
s
20 20
COMMENTS:
DTW = Depth to Water ft = indicates depth in feet ppm = indicates parts per million Filtered Sand
PWR = Partially Weatherd Rock ft-bgs = indicates feet below ground surface -- = Not Applicable BentoniteGrout
17 17
18 18
19 19
14 14
15 15
16 16
11 11
12 12
13 13
8 8
9 9
10 10
5 5
6 6
7 7
3 3
None 8.3 --
4 4
None 10.3 ES-5E
(4-5)
1 1
None 0.6 --
2 2
None 6.9
SOIL DESCRIPTION
(Moisture, Color, Soil Description)Construction Details
None 0.0 -- Dry Red Brown Gravelly Silty CLAY
--
Dry Red Brown CLAY
Date Completed:4/26/2024 Monitoring Equipment:PID MiniRae 3000 MAA Field Staff:Austen Rubenstein
Date Started:4/26/2024 Driller :Stefan Smith DTW (ft):NA
Location:
1200 Metropolitan Avenue,
Charlotte, NC Subcontractor/Drillers: Saedacco Screen Depth (ft):NA
Project Number:H1824.00 Task 50,000 Sampling Method:Direct Push Macro-Core Well Depth (ft):NA
Site Name: Midtown Square Mall Drilling/Boring Method:Direct Push Macro-Core Boring Depth (ft):5.0
1125 E. Morehead Street,
Suite 104.
Charlotte, NC 28204
Ph: [phone]
LOG OF BORING: ES-5E
Page:1 of 1
Midtown Square Mall Well ID: TMW-1
H1824.00 Task 50,000 2"
101.01
04/26/2024 30.00
04/26/2024 19.30
81.71
(TOC-DTW)
70°F
30.00
19.30 0.041
10.70 0.163
(TWD-DTW) 0.652
Well Volume = WC x CF 1.468
1.74
5.23
Start
10:00 10:05 10:10 10:15 10:20 10:25
19.30 19.30 19.30 19.30 19.30 19.30
6.60 6.60 6.60 6.59 6.59 6.59
0.435 0.435 0.435 0.435 0.435 0.435
18.27 18.46 18.53 18.61 18.78 18.79
190 189 191 192 192 192
27 19.8 15.4 13.6 10.4 8.2
5.99 5.48 5.56 5.55 5.54 5.55
Troy Holzschuh
10:30
DTW stabalized prior to start of collecting field measurements
DUP-2 taken at 10:30 with TMW-1
Dissolved Oxygen (mg/L):
Sample Information
Sampled By:
Time:
Additional Comments:
DTW (ft):
pH (+-0.1 s.u.):
Conductivity (5% µs/cm):
Temperature (°C):
ORP (mV):
Turbidity (<10 NTU):
1 Well Volume:
3 Well Volumes:
Field Measurements
Time (3 to 5 min):
Purge Rate: 200 ml/min
Depth to Water (DTW): CF 1 inch =
Water Column (WC): CF 2 inch =
CF 4 inch=
CF 6 inch =
GW Elevation:
Weather Conditions
Air Temperature:
Volume Calculations
Total Well Depth (TWD): Converstion Factors (WC to Gallons)
Location:1200 Metropolitan Ave. Charlotte, NC TOC Elev:
Date Started: Total Well Depth (TWD):
Date Completed: Depth to Water (DTW):
Lowflow Sampling - Field Data Sheet
Site Information Well Information
Facility Name:
Project Number: Casing Diameter:
Clear Rain Windy Cloudy Hot Cold
Midtown Square Mall Well ID: TMW-2
H1824.00 Task 50,000 2"
99.65
04/26/2024 34.00
04/26/2024 19.80
79.85
(TOC-DTW)
70°F
34.00
19.80 0.041
14.20 0.163
(TWD-DTW) 0.652
Well Volume = WC x CF 1.468
2.31
6.94
Start
7:40 7:45 7:50 7:55 8:00 8:05
19.80 19.80 19.80 19.80 19.80 19.80
6.08 6.08 6.08 6.07 6.07 6.07
0.387 0.387 0.386 0.386 0.386 0.386
18.39 18.32 18.51 18.34 18.29 18.16
81 81 80 80 81 81
12.9 14.9 12.6 11.9 10.3 9.7
8.22 8.19 8.18 8.18 8.18 8.18
Troy Holzschuh
8:10
DTW stabalized prior to start of collecting field measurements
1200 Metropolitan Ave. Charlotte, NC
Total Well Depth (TWD):
Depth to Water (DTW):
Field Measurements
200 ml/min
3 Well Volumes:
Air Temperature:
Total Well Depth (TWD):
Depth to Water (DTW):
ORP (mV):
Lowflow Sampling - Field Data Sheet
Time (3 to 5 min):
Purge Rate:
DTW (ft):
Project Number:
Location:
Date Completed:
Facility Name:
Date Started:
TOC Elev:
GW Elevation:
Well InformationSite Information
Casing Diameter:
Water Column (WC):
1 Well Volume:
Sampled By:
Time:
Additional Comments:
Dissolved Oxygen (mg/L):
Weather Conditions
Volume Calculations
Converstion Factors (WC to Gallons)
Sample Information
CF 1 inch =
CF 2 inch =
CF 4 inch=
CF 6 inch =
pH (+-0.1 s.u.):
Conductivity (5% µs/cm):
Temperature (°C):
Turbidity (<10 NTU):
Clear Rain Windy Cloudy Hot Cold
Midtown Square Mall Well ID: TMW-3
H1824.00 Task 50,000 2"
99.08
04/26/2024 25.00
04/26/2024 11.95
87.13
(TOC-DTW)
70°F
25.00
11.95 0.041
13.05 0.163
(TWD-DTW) 0.652
Well Volume = WC x CF 1.468
2.13
6.38
Start
12:35 12:40 12:45 12:50 12:55 13:00
11.95 11.95 11.95 11.95 11.95 11.95
6.46 6.45 6.44 6.44 6.44 6.44
0.355 0.354 0.355 0.356 0.356 0.355
21.55 21.60 21.72 21.81 21.87 21.80
208 210 210 210 210 210
26.4 21.9 16.5 14.1 12.6 9.9
6.15 6.15 6.12 6.11 6.11 6.10
Troy Holzschuh
13:05
DTW stabalized prior to start of collecting field measurements
Dissolved Oxygen (mg/L):
Sample Information
Sampled By:
Time:
Additional Comments:
DTW (ft):
pH (+-0.1 s.u.):
Conductivity (5% µs/cm):
Temperature (°C):
ORP (mV):
Turbidity (<10 NTU):
1 Well Volume:
3 Well Volumes:
Field Measurements
Time (3 to 5 min):
Purge Rate: 200 ml/min
Depth to Water (DTW): CF 1 inch =
Water Column (WC): CF 2 inch =
CF 4 inch=
CF 6 inch =
GW Elevation:
Weather Conditions
Air Temperature:
Volume Calculations
Total Well Depth (TWD): Converstion Factors (WC to Gallons)
Location:1200 Metropolitan Ave. Charlotte, NC TOC Elev:
Date Started: Total Well Depth (TWD):
Date Completed: Depth to Water (DTW):
Lowflow Sampling - Field Data Sheet
Site Information Well Information
Facility Name:
Project Number: Casing Diameter:
Clear Rain Windy Cloudy Hot Cold

APPENDIX C
Laboratory Analytical Reports

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
November 15, 2023
Greg Icenhour
Mid-Atlantic Associates, Inc. - Charlotte, NC
1125 E. Morehead Street Suite 104
Charlotte, NC 28204
Project Location: 1200 Metropolitan Ave, Charlotte, NC
Client Job Number:
Project Number: 000H1824.00
Laboratory Work Order Number: 23K1152
Enclosed are results of analyses for samples as received by the laboratory on November 7, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
11/15/2023Mid-Atlantic Associates, Inc. - Charlotte, NC
1125 E. Morehead Street Suite 104
Charlotte, NC 28204
ATTN: Greg Icenhour
000H1824.00
23K1152
The results of analyses performed on the following samples submitted to Con-Test, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
1200 Metropolitan Ave, Charlotte, NC
SG-1 23K1152-01 Soil Gas -
EPA TO-15
SG-2 23K1152-02 Soil Gas -
EPA TO-15
SG-3 23K1152-03 Soil Gas -
EPA TO-15
SG-4 23K1152-04 Soil Gas -
EPA TO-15
DUP-1 23K1152-05 Soil Gas -
EPA TO-15
UNUSED 23K1152-06 -
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased
on the low side.
Analyte & Samples(s) Qualified:
L-03
Isopropanol
23K1152-01[SG-1], 23K1152-02[SG-2], 23K1152-03[SG-3], 23K1152-04[SG-4], 23K1152-05[DUP-1], B358063-BLK1, B358063-BS1, B358063-DUP1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Dichlorodifluoromethane (Freon 12)
23K1152-01[SG-1], 23K1152-02[SG-2], 23K1152-03[SG-3], 23K1152-04[SG-4], 23K1152-05[DUP-1], B358063-BLK1, B358063-BS1, B358063-DUP1, S096287-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
V-06
Naphthalene
B358063-BS1, S096287-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected since
sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
1,2,4-Trichlorobenzene, Benzyl chloride
S096287-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
Carbon Tetrachloride
23K1152-01[SG-1], 23K1152-02[SG-2], 23K1152-03[SG-3], 23K1152-04[SG-4], 23K1152-05[DUP-1], B358063-BLK1, B358063-BS1, B358063-DUP1, S096287-CCV1
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this
document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my
knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: SG-1
Sample ID: 23K1152-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -5.2
Sampled: 11/2/2023 14:40
Canister ID: 2886
Flow Controller ID: 4659
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 30 8.0 11/10/23 15:01 KMC724191.9 4.5
Benzene 2.4 0.20 11/10/23 15:01 KMC7.6 40.640.062 0.20
Benzyl chloride ND 0.20 11/10/23 15:01 KMCND41.00.11 0.56
Bromodichloromethane ND 0.20 11/10/23 15:01 KMCND41.30.054 0.36
Bromoform ND 0.20 11/10/23 15:01 KMCND42.10.071 0.73
Bromomethane ND 0.20 11/10/23 15:01 KMCND40.780.11 0.41
1,3-Butadiene ND 0.20 11/10/23 15:01 KMCND40.440.17 0.37
2-Butanone (MEK)ND 8.0 11/10/23 15:01 KMCND4242.2 6.6
Carbon Disulfide 11 2.0 11/10/23 15:01 KMC3546.20.38 1.2
Carbon Tetrachloride 0.12 0.20 11/10/23 15:01 KMCV-34, J 0.75 41.30.058 0.36
Chlorobenzene ND 0.20 11/10/23 15:01 KMCND40.920.050 0.23
Chloroethane ND 0.20 11/10/23 15:01 KMCND40.530.13 0.33
Chloroform 3.9 0.20 11/10/23 15:01 KMC1940.980.052 0.25
Chloromethane ND 0.40 11/10/23 15:01 KMCND40.830.082 0.17
Cyclohexane 8.2 0.20 11/10/23 15:01 KMC2840.690.088 0.30
Dibromochloromethane ND 0.20 11/10/23 15:01 KMCND41.70.054 0.46
1,2-Dibromoethane (EDB)ND 0.20 11/10/23 15:01 KMCND41.50.067 0.51
1,2-Dichlorobenzene ND 0.20 11/10/23 15:01 KMCND41.20.070 0.42
1,3-Dichlorobenzene ND 0.20 11/10/23 15:01 KMCND41.20.074 0.45
1,4-Dichlorobenzene ND 0.20 11/10/23 15:01 KMCND41.20.074 0.44
Dichlorodifluoromethane (Freon 12)0.27 0.20 11/10/23 15:01 KMCV-05 1.3 40.990.084 0.42
1,1-Dichloroethane ND 0.20 11/10/23 15:01 KMCND40.810.064 0.26
1,2-Dichloroethane ND 0.20 11/10/23 15:01 KMCND40.810.075 0.30
1,1-Dichloroethylene ND 0.20 11/10/23 15:01 KMCND40.790.057 0.23
cis-1,2-Dichloroethylene ND 0.20 11/10/23 15:01 KMCND40.790.062 0.24
trans-1,2-Dichloroethylene ND 0.20 11/10/23 15:01 KMCND40.790.065 0.26
1,2-Dichloropropane ND 0.20 11/10/23 15:01 KMCND40.920.055 0.25
cis-1,3-Dichloropropene ND 0.20 11/10/23 15:01 KMCND40.910.090 0.41
trans-1,3-Dichloropropene ND 0.20 11/10/23 15:01 KMCND40.910.10 0.47
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 11/10/23 15:01 KMCND41.40.080 0.56
1,4-Dioxane ND 2.0 11/10/23 15:01 KMCND47.20.98 3.5
Ethanol 19 8.0 11/10/23 15:01 KMC354155.3 10.0
Ethyl Acetate 0.60 2.0 11/10/23 15:01 KMCJ2.2 47.20.58 2.1
Ethylbenzene 1.0 0.20 11/10/23 15:01 KMC4.5 40.870.058 0.25
4-Ethyltoluene 0.18 0.20 11/10/23 15:01 KMCJ0.90 40.980.087 0.43
Heptane 1.6 0.20 11/10/23 15:01 KMC6.6 40.820.13 0.52
Hexachlorobutadiene ND 0.20 11/10/23 15:01 KMCND42.10.12 1.2
Hexane 4.4 8.0 11/10/23 15:01 KMCJ154282.6 9.3
2-Hexanone (MBK)ND 0.20 11/10/23 15:01 KMCND40.820.087 0.35
Isopropanol ND 8.0 11/10/23 15:01 KMCL-03 ND 4202.5 6.2
Methyl tert-Butyl Ether (MTBE)0.29 0.20 11/10/23 15:01 KMC1.0 40.720.098 0.35
Methylene Chloride 0.68 2.0 11/10/23 15:01 KMCJ2.3 46.90.54 1.9
4-Methyl-2-pentanone (MIBK)0.88 0.20 11/10/23 15:01 KMC3.6 40.820.11 0.43
Naphthalene ND 0.20 11/10/23 15:01 KMCND41.00.13 0.70
Propene 23 8.0 11/10/23 15:01 KMC394142.2 3.7
Styrene 0.16 0.20 11/10/23 15:01 KMCJ0.66 40.850.11 0.46
1,1,2,2-Tetrachloroethane ND 0.20 11/10/23 15:01 KMCND41.40.050 0.34
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: SG-1
Sample ID: 23K1152-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -5.2
Sampled: 11/2/2023 14:40
Canister ID: 2886
Flow Controller ID: 4659
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 17 0.20 11/10/23 15:01 KMC11041.40.075 0.51
Tetrahydrofuran 2.2 2.0 11/10/23 15:01 KMC6.5 45.90.41 1.2
Toluene 14 0.20 11/10/23 15:01 KMC5440.750.073 0.27
1,2,4-Trichlorobenzene ND 0.20 11/10/23 15:01 KMCND41.50.11 0.80
1,1,1-Trichloroethane ND 0.20 11/10/23 15:01 KMCND41.10.063 0.34
1,1,2-Trichloroethane ND 0.20 11/10/23 15:01 KMCND41.10.051 0.28
Trichloroethylene 0.17 0.20 11/10/23 15:01 KMCJ0.90 41.10.082 0.44
Trichlorofluoromethane (Freon 11)0.41 0.80 11/10/23 15:01 KMCJ2.3 44.50.082 0.46
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.10 0.80 11/10/23 15:01 KMCJ0.80 46.10.044 0.34
1,2,4-Trimethylbenzene 0.84 0.20 11/10/23 15:01 KMC4.1 40.980.092 0.45
1,3,5-Trimethylbenzene 0.16 0.20 11/10/23 15:01 KMCJ0.77 40.980.10 0.51
Vinyl Acetate ND 4.0 11/10/23 15:01 KMCND4140.71 2.5
Vinyl Chloride ND 0.20 11/10/23 15:01 KMCND40.510.091 0.23
m&p-Xylene 3.0 0.40 11/10/23 15:01 KMC1341.70.14 0.61
o-Xylene 1.0 0.20 11/10/23 15:01 KMC4.4 40.870.073 0.32
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)101 11/10/23 15:0170-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: SG-2
Sample ID: 23K1152-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.0
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -5.8
Sampled: 11/2/2023 15:10
Canister ID: 2764
Flow Controller ID: 4463
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 61 8.0 11/10/23 15:41 KMC1504191.9 4.5
Benzene 1.3 0.20 11/10/23 15:41 KMC4.2 40.640.062 0.20
Benzyl chloride ND 0.20 11/10/23 15:41 KMCND41.00.11 0.56
Bromodichloromethane ND 0.20 11/10/23 15:41 KMCND41.30.054 0.36
Bromoform ND 0.20 11/10/23 15:41 KMCND42.10.071 0.73
Bromomethane ND 0.20 11/10/23 15:41 KMCND40.780.11 0.41
1,3-Butadiene ND 0.20 11/10/23 15:41 KMCND40.440.17 0.37
2-Butanone (MEK)4.0 8.0 11/10/23 15:41 KMCJ124242.2 6.6
Carbon Disulfide 3.2 2.0 11/10/23 15:41 KMC1046.20.38 1.2
Carbon Tetrachloride 0.060 0.20 11/10/23 15:41 KMCV-34, J 0.38 41.30.058 0.36
Chlorobenzene ND 0.20 11/10/23 15:41 KMCND40.920.050 0.23
Chloroethane ND 0.20 11/10/23 15:41 KMCND40.530.13 0.33
Chloroform 2.6 0.20 11/10/23 15:41 KMC1340.980.052 0.25
Chloromethane ND 0.40 11/10/23 15:41 KMCND40.830.082 0.17
Cyclohexane 2.1 0.20 11/10/23 15:41 KMC7.3 40.690.088 0.30
Dibromochloromethane ND 0.20 11/10/23 15:41 KMCND41.70.054 0.46
1,2-Dibromoethane (EDB)ND 0.20 11/10/23 15:41 KMCND41.50.067 0.51
1,2-Dichlorobenzene ND 0.20 11/10/23 15:41 KMCND41.20.070 0.42
1,3-Dichlorobenzene ND 0.20 11/10/23 15:41 KMCND41.20.074 0.45
1,4-Dichlorobenzene ND 0.20 11/10/23 15:41 KMCND41.20.074 0.44
Dichlorodifluoromethane (Freon 12)0.23 0.20 11/10/23 15:41 KMCV-05 1.1 40.990.084 0.42
1,1-Dichloroethane ND 0.20 11/10/23 15:41 KMCND40.810.064 0.26
1,2-Dichloroethane ND 0.20 11/10/23 15:41 KMCND40.810.075 0.30
1,1-Dichloroethylene ND 0.20 11/10/23 15:41 KMCND40.790.057 0.23
cis-1,2-Dichloroethylene ND 0.20 11/10/23 15:41 KMCND40.790.062 0.24
trans-1,2-Dichloroethylene ND 0.20 11/10/23 15:41 KMCND40.790.065 0.26
1,2-Dichloropropane ND 0.20 11/10/23 15:41 KMCND40.920.055 0.25
cis-1,3-Dichloropropene ND 0.20 11/10/23 15:41 KMCND40.910.090 0.41
trans-1,3-Dichloropropene ND 0.20 11/10/23 15:41 KMCND40.910.10 0.47
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 11/10/23 15:41 KMCND41.40.080 0.56
1,4-Dioxane ND 2.0 11/10/23 15:41 KMCND47.20.98 3.5
Ethanol 31 8.0 11/10/23 15:41 KMC574155.3 10.0
Ethyl Acetate 0.91 2.0 11/10/23 15:41 KMCJ3.3 47.20.58 2.1
Ethylbenzene 0.69 0.20 11/10/23 15:41 KMC3.0 40.870.058 0.25
4-Ethyltoluene 0.19 0.20 11/10/23 15:41 KMCJ0.94 40.980.087 0.43
Heptane 0.77 0.20 11/10/23 15:41 KMC3.1 40.820.13 0.52
Hexachlorobutadiene ND 0.20 11/10/23 15:41 KMCND42.10.12 1.2
Hexane ND 8.0 11/10/23 15:41 KMCND4282.6 9.3
2-Hexanone (MBK)ND 0.20 11/10/23 15:41 KMCND40.820.087 0.35
Isopropanol ND 8.0 11/10/23 15:41 KMCL-03 ND 4202.5 6.2
Methyl tert-Butyl Ether (MTBE)ND 0.20 11/10/23 15:41 KMCND40.720.098 0.35
Methylene Chloride 0.76 2.0 11/10/23 15:41 KMCJ2.6 46.90.54 1.9
4-Methyl-2-pentanone (MIBK)1.0 0.20 11/10/23 15:41 KMC4.2 40.820.11 0.43
Naphthalene ND 0.20 11/10/23 15:41 KMCND41.00.13 0.70
Propene ND 8.0 11/10/23 15:41 KMCND4142.2 3.7
Styrene 0.15 0.20 11/10/23 15:41 KMCJ0.63 40.850.11 0.46
1,1,2,2-Tetrachloroethane ND 0.20 11/10/23 15:41 KMCND41.40.050 0.34
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: SG-2
Sample ID: 23K1152-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.0
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -5.8
Sampled: 11/2/2023 15:10
Canister ID: 2764
Flow Controller ID: 4463
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.12 0.20 11/10/23 15:41 KMCJ0.79 41.40.075 0.51
Tetrahydrofuran 2.6 2.0 11/10/23 15:41 KMC7.5 45.90.41 1.2
Toluene 9.1 0.20 11/10/23 15:41 KMC3440.750.073 0.27
1,2,4-Trichlorobenzene ND 0.20 11/10/23 15:41 KMCND41.50.11 0.80
1,1,1-Trichloroethane ND 0.20 11/10/23 15:41 KMCND41.10.063 0.34
1,1,2-Trichloroethane ND 0.20 11/10/23 15:41 KMCND41.10.051 0.28
Trichloroethylene ND 0.20 11/10/23 15:41 KMCND41.10.082 0.44
Trichlorofluoromethane (Freon 11)1.1 0.80 11/10/23 15:41 KMC6.0 44.50.082 0.46
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.056 0.80 11/10/23 15:41 KMCJ0.43 46.10.044 0.34
1,2,4-Trimethylbenzene 0.89 0.20 11/10/23 15:41 KMC4.4 40.980.092 0.45
1,3,5-Trimethylbenzene 0.13 0.20 11/10/23 15:41 KMCJ0.65 40.980.10 0.51
Vinyl Acetate ND 4.0 11/10/23 15:41 KMCND4140.71 2.5
Vinyl Chloride ND 0.20 11/10/23 15:41 KMCND40.510.091 0.23
m&p-Xylene 2.3 0.40 11/10/23 15:41 KMC1041.70.14 0.61
o-Xylene 0.83 0.20 11/10/23 15:41 KMC3.6 40.870.073 0.32
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)103 11/10/23 15:4170-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: SG-3
Sample ID: 23K1152-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29.5
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -4.5
Sampled: 11/2/2023 15:41
Canister ID: 2888
Flow Controller ID: 4464
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 31 8.0 11/10/23 16:22 KMC734191.9 4.5
Benzene 2.8 0.20 11/10/23 16:22 KMC8.9 40.640.062 0.20
Benzyl chloride ND 0.20 11/10/23 16:22 KMCND41.00.11 0.56
Bromodichloromethane ND 0.20 11/10/23 16:22 KMCND41.30.054 0.36
Bromoform ND 0.20 11/10/23 16:22 KMCND42.10.071 0.73
Bromomethane ND 0.20 11/10/23 16:22 KMCND40.780.11 0.41
1,3-Butadiene ND 0.20 11/10/23 16:22 KMCND40.440.17 0.37
2-Butanone (MEK)2.5 8.0 11/10/23 16:22 KMCJ7.3 4242.2 6.6
Carbon Disulfide 5.3 2.0 11/10/23 16:22 KMC1746.20.38 1.2
Carbon Tetrachloride 0.072 0.20 11/10/23 16:22 KMCV-34, J 0.45 41.30.058 0.36
Chlorobenzene ND 0.20 11/10/23 16:22 KMCND40.920.050 0.23
Chloroethane ND 0.20 11/10/23 16:22 KMCND40.530.13 0.33
Chloroform 1.0 0.20 11/10/23 16:22 KMC5.1 40.980.052 0.25
Chloromethane ND 0.40 11/10/23 16:22 KMCND40.830.082 0.17
Cyclohexane 4.7 0.20 11/10/23 16:22 KMC1640.690.088 0.30
Dibromochloromethane ND 0.20 11/10/23 16:22 KMCND41.70.054 0.46
1,2-Dibromoethane (EDB)ND 0.20 11/10/23 16:22 KMCND41.50.067 0.51
1,2-Dichlorobenzene ND 0.20 11/10/23 16:22 KMCND41.20.070 0.42
1,3-Dichlorobenzene ND 0.20 11/10/23 16:22 KMCND41.20.074 0.45
1,4-Dichlorobenzene ND 0.20 11/10/23 16:22 KMCND41.20.074 0.44
Dichlorodifluoromethane (Freon 12)0.27 0.20 11/10/23 16:22 KMCV-05 1.3 40.990.084 0.42
1,1-Dichloroethane ND 0.20 11/10/23 16:22 KMCND40.810.064 0.26
1,2-Dichloroethane ND 0.20 11/10/23 16:22 KMCND40.810.075 0.30
1,1-Dichloroethylene ND 0.20 11/10/23 16:22 KMCND40.790.057 0.23
cis-1,2-Dichloroethylene ND 0.20 11/10/23 16:22 KMCND40.790.062 0.24
trans-1,2-Dichloroethylene ND 0.20 11/10/23 16:22 KMCND40.790.065 0.26
1,2-Dichloropropane ND 0.20 11/10/23 16:22 KMCND40.920.055 0.25
cis-1,3-Dichloropropene ND 0.20 11/10/23 16:22 KMCND40.910.090 0.41
trans-1,3-Dichloropropene ND 0.20 11/10/23 16:22 KMCND40.910.10 0.47
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 11/10/23 16:22 KMCND41.40.080 0.56
1,4-Dioxane ND 2.0 11/10/23 16:22 KMCND47.20.98 3.5
Ethanol 24 8.0 11/10/23 16:22 KMC464155.3 10.0
Ethyl Acetate ND 2.0 11/10/23 16:22 KMCND47.20.58 2.1
Ethylbenzene 0.57 0.20 11/10/23 16:22 KMC2.5 40.870.058 0.25
4-Ethyltoluene 0.15 0.20 11/10/23 16:22 KMCJ0.73 40.980.087 0.43
Heptane 1.2 0.20 11/10/23 16:22 KMC5.0 40.820.13 0.52
Hexachlorobutadiene ND 0.20 11/10/23 16:22 KMCND42.10.12 1.2
Hexane 6.0 8.0 11/10/23 16:22 KMCJ214282.6 9.3
2-Hexanone (MBK)ND 0.20 11/10/23 16:22 KMCND40.820.087 0.35
Isopropanol ND 8.0 11/10/23 16:22 KMCL-03 ND 4202.5 6.2
Methyl tert-Butyl Ether (MTBE)ND 0.20 11/10/23 16:22 KMCND40.720.098 0.35
Methylene Chloride 0.56 2.0 11/10/23 16:22 KMCJ2.0 46.90.54 1.9
4-Methyl-2-pentanone (MIBK)0.71 0.20 11/10/23 16:22 KMC2.9 40.820.11 0.43
Naphthalene ND 0.20 11/10/23 16:22 KMCND41.00.13 0.70
Propene 45 8.0 11/10/23 16:22 KMC774142.2 3.7
Styrene 0.12 0.20 11/10/23 16:22 KMCJ0.51 40.850.11 0.46
1,1,2,2-Tetrachloroethane ND 0.20 11/10/23 16:22 KMCND41.40.050 0.34
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: SG-3
Sample ID: 23K1152-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29.5
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -4.5
Sampled: 11/2/2023 15:41
Canister ID: 2888
Flow Controller ID: 4464
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.17 0.20 11/10/23 16:22 KMCJ1.1 41.40.075 0.51
Tetrahydrofuran 0.62 2.0 11/10/23 16:22 KMCJ1.8 45.90.41 1.2
Toluene 7.3 0.20 11/10/23 16:22 KMC2740.750.073 0.27
1,2,4-Trichlorobenzene ND 0.20 11/10/23 16:22 KMCND41.50.11 0.80
1,1,1-Trichloroethane ND 0.20 11/10/23 16:22 KMCND41.10.063 0.34
1,1,2-Trichloroethane ND 0.20 11/10/23 16:22 KMCND41.10.051 0.28
Trichloroethylene ND 0.20 11/10/23 16:22 KMCND41.10.082 0.44
Trichlorofluoromethane (Freon 11)0.79 0.80 11/10/23 16:22 KMCJ4.4 44.50.082 0.46
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.096 0.80 11/10/23 16:22 KMCJ0.74 46.10.044 0.34
1,2,4-Trimethylbenzene 0.75 0.20 11/10/23 16:22 KMC3.7 40.980.092 0.45
1,3,5-Trimethylbenzene 0.12 0.20 11/10/23 16:22 KMCJ0.59 40.980.10 0.51
Vinyl Acetate ND 4.0 11/10/23 16:22 KMCND4140.71 2.5
Vinyl Chloride ND 0.20 11/10/23 16:22 KMCND40.510.091 0.23
m&p-Xylene 1.9 0.40 11/10/23 16:22 KMC8.2 41.70.14 0.61
o-Xylene 0.68 0.20 11/10/23 16:22 KMC3.0 40.870.073 0.32
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 11/10/23 16:2270-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: SG-4
Sample ID: 23K1152-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -3.9
Sampled: 11/2/2023 16:11
Canister ID: 2112
Flow Controller ID: 4537
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 30 8.0 11/10/23 17:02 KMC714191.9 4.5
Benzene 1.8 0.20 11/10/23 17:02 KMC5.6 40.640.062 0.20
Benzyl chloride ND 0.20 11/10/23 17:02 KMCND41.00.11 0.56
Bromodichloromethane ND 0.20 11/10/23 17:02 KMCND41.30.054 0.36
Bromoform ND 0.20 11/10/23 17:02 KMCND42.10.071 0.73
Bromomethane ND 0.20 11/10/23 17:02 KMCND40.780.11 0.41
1,3-Butadiene ND 0.20 11/10/23 17:02 KMCND40.440.17 0.37
2-Butanone (MEK)ND 8.0 11/10/23 17:02 KMCND4242.2 6.6
Carbon Disulfide 7.7 2.0 11/10/23 17:02 KMC2446.20.38 1.2
Carbon Tetrachloride 0.12 0.20 11/10/23 17:02 KMCV-34, J 0.78 41.30.058 0.36
Chlorobenzene ND 0.20 11/10/23 17:02 KMCND40.920.050 0.23
Chloroethane ND 0.20 11/10/23 17:02 KMCND40.530.13 0.33
Chloroform 1.0 0.20 11/10/23 17:02 KMC4.9 40.980.052 0.25
Chloromethane 0.29 0.40 11/10/23 17:02 KMCJ0.59 40.830.082 0.17
Cyclohexane 6.5 0.20 11/10/23 17:02 KMC2240.690.088 0.30
Dibromochloromethane ND 0.20 11/10/23 17:02 KMCND41.70.054 0.46
1,2-Dibromoethane (EDB)ND 0.20 11/10/23 17:02 KMCND41.50.067 0.51
1,2-Dichlorobenzene ND 0.20 11/10/23 17:02 KMCND41.20.070 0.42
1,3-Dichlorobenzene ND 0.20 11/10/23 17:02 KMCND41.20.074 0.45
1,4-Dichlorobenzene ND 0.20 11/10/23 17:02 KMCND41.20.074 0.44
Dichlorodifluoromethane (Freon 12)0.27 0.20 11/10/23 17:02 KMCV-05 1.3 40.990.084 0.42
1,1-Dichloroethane ND 0.20 11/10/23 17:02 KMCND40.810.064 0.26
1,2-Dichloroethane ND 0.20 11/10/23 17:02 KMCND40.810.075 0.30
1,1-Dichloroethylene ND 0.20 11/10/23 17:02 KMCND40.790.057 0.23
cis-1,2-Dichloroethylene ND 0.20 11/10/23 17:02 KMCND40.790.062 0.24
trans-1,2-Dichloroethylene ND 0.20 11/10/23 17:02 KMCND40.790.065 0.26
1,2-Dichloropropane ND 0.20 11/10/23 17:02 KMCND40.920.055 0.25
cis-1,3-Dichloropropene ND 0.20 11/10/23 17:02 KMCND40.910.090 0.41
trans-1,3-Dichloropropene ND 0.20 11/10/23 17:02 KMCND40.910.10 0.47
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 11/10/23 17:02 KMCND41.40.080 0.56
1,4-Dioxane ND 2.0 11/10/23 17:02 KMCND47.20.98 3.5
Ethanol 28 8.0 11/10/23 17:02 KMC524155.3 10.0
Ethyl Acetate ND 2.0 11/10/23 17:02 KMCND47.20.58 2.1
Ethylbenzene 0.54 0.20 11/10/23 17:02 KMC2.3 40.870.058 0.25
4-Ethyltoluene 0.14 0.20 11/10/23 17:02 KMCJ0.67 40.980.087 0.43
Heptane 1.2 0.20 11/10/23 17:02 KMC4.9 40.820.13 0.52
Hexachlorobutadiene ND 0.20 11/10/23 17:02 KMCND42.10.12 1.2
Hexane 4.3 8.0 11/10/23 17:02 KMCJ154282.6 9.3
2-Hexanone (MBK)ND 0.20 11/10/23 17:02 KMCND40.820.087 0.35
Isopropanol ND 8.0 11/10/23 17:02 KMCL-03 ND 4202.5 6.2
Methyl tert-Butyl Ether (MTBE)0.15 0.20 11/10/23 17:02 KMCJ0.53 40.720.098 0.35
Methylene Chloride 0.66 2.0 11/10/23 17:02 KMCJ2.3 46.90.54 1.9
4-Methyl-2-pentanone (MIBK)0.81 0.20 11/10/23 17:02 KMC3.3 40.820.11 0.43
Naphthalene ND 0.20 11/10/23 17:02 KMCND41.00.13 0.70
Propene 13 8.0 11/10/23 17:02 KMC234142.2 3.7
Styrene 0.14 0.20 11/10/23 17:02 KMCJ0.61 40.850.11 0.46
1,1,2,2-Tetrachloroethane ND 0.20 11/10/23 17:02 KMCND41.40.050 0.34
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: SG-4
Sample ID: 23K1152-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -3.9
Sampled: 11/2/2023 16:11
Canister ID: 2112
Flow Controller ID: 4537
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 11/10/23 17:02 KMCND41.40.075 0.51
Tetrahydrofuran ND 2.0 11/10/23 17:02 KMCND45.90.41 1.2
Toluene 6.6 0.20 11/10/23 17:02 KMC2540.750.073 0.27
1,2,4-Trichlorobenzene ND 0.20 11/10/23 17:02 KMCND41.50.11 0.80
1,1,1-Trichloroethane ND 0.20 11/10/23 17:02 KMCND41.10.063 0.34
1,1,2-Trichloroethane ND 0.20 11/10/23 17:02 KMCND41.10.051 0.28
Trichloroethylene ND 0.20 11/10/23 17:02 KMCND41.10.082 0.44
Trichlorofluoromethane (Freon 11)0.25 0.80 11/10/23 17:02 KMCJ1.4 44.50.082 0.46
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.060 0.80 11/10/23 17:02 KMCJ0.46 46.10.044 0.34
1,2,4-Trimethylbenzene 0.78 0.20 11/10/23 17:02 KMC3.8 40.980.092 0.45
1,3,5-Trimethylbenzene 0.14 0.20 11/10/23 17:02 KMCJ0.67 40.980.10 0.51
Vinyl Acetate ND 4.0 11/10/23 17:02 KMCND4140.71 2.5
Vinyl Chloride ND 0.20 11/10/23 17:02 KMCND40.510.091 0.23
m&p-Xylene 1.9 0.40 11/10/23 17:02 KMC8.2 41.70.14 0.61
o-Xylene 0.68 0.20 11/10/23 17:02 KMC3.0 40.870.073 0.32
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)103 11/10/23 17:0270-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: DUP-1
Sample ID: 23K1152-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -4.4
Sampled: 11/2/2023 14:40
Canister ID: 2311
Flow Controller ID: 4659
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 31 8.0 11/10/23 17:43 KMC734191.9 4.5
Benzene 2.4 0.20 11/10/23 17:43 KMC7.6 40.640.062 0.20
Benzyl chloride ND 0.20 11/10/23 17:43 KMCND41.00.11 0.56
Bromodichloromethane 0.18 0.20 11/10/23 17:43 KMCJ1.2 41.30.054 0.36
Bromoform ND 0.20 11/10/23 17:43 KMCND42.10.071 0.73
Bromomethane ND 0.20 11/10/23 17:43 KMCND40.780.11 0.41
1,3-Butadiene ND 0.20 11/10/23 17:43 KMCND40.440.17 0.37
2-Butanone (MEK)ND 8.0 11/10/23 17:43 KMCND4242.2 6.6
Carbon Disulfide 11 2.0 11/10/23 17:43 KMC3646.20.38 1.2
Carbon Tetrachloride 0.13 0.20 11/10/23 17:43 KMCV-34, J 0.81 41.30.058 0.36
Chlorobenzene ND 0.20 11/10/23 17:43 KMCND40.920.050 0.23
Chloroethane ND 0.20 11/10/23 17:43 KMCND40.530.13 0.33
Chloroform 3.9 0.20 11/10/23 17:43 KMC1940.980.052 0.25
Chloromethane 0.17 0.40 11/10/23 17:43 KMCJ0.35 40.830.082 0.17
Cyclohexane 8.2 0.20 11/10/23 17:43 KMC2840.690.088 0.30
Dibromochloromethane ND 0.20 11/10/23 17:43 KMCND41.70.054 0.46
1,2-Dibromoethane (EDB)ND 0.20 11/10/23 17:43 KMCND41.50.067 0.51
1,2-Dichlorobenzene ND 0.20 11/10/23 17:43 KMCND41.20.070 0.42
1,3-Dichlorobenzene ND 0.20 11/10/23 17:43 KMCND41.20.074 0.45
1,4-Dichlorobenzene ND 0.20 11/10/23 17:43 KMCND41.20.074 0.44
Dichlorodifluoromethane (Freon 12)0.24 0.20 11/10/23 17:43 KMCV-05 1.2 40.990.084 0.42
1,1-Dichloroethane ND 0.20 11/10/23 17:43 KMCND40.810.064 0.26
1,2-Dichloroethane ND 0.20 11/10/23 17:43 KMCND40.810.075 0.30
1,1-Dichloroethylene ND 0.20 11/10/23 17:43 KMCND40.790.057 0.23
cis-1,2-Dichloroethylene ND 0.20 11/10/23 17:43 KMCND40.790.062 0.24
trans-1,2-Dichloroethylene ND 0.20 11/10/23 17:43 KMCND40.790.065 0.26
1,2-Dichloropropane ND 0.20 11/10/23 17:43 KMCND40.920.055 0.25
cis-1,3-Dichloropropene ND 0.20 11/10/23 17:43 KMCND40.910.090 0.41
trans-1,3-Dichloropropene ND 0.20 11/10/23 17:43 KMCND40.910.10 0.47
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 11/10/23 17:43 KMCND41.40.080 0.56
1,4-Dioxane ND 2.0 11/10/23 17:43 KMCND47.20.98 3.5
Ethanol 19 8.0 11/10/23 17:43 KMC364155.3 10.0
Ethyl Acetate ND 2.0 11/10/23 17:43 KMCND47.20.58 2.1
Ethylbenzene 1.0 0.20 11/10/23 17:43 KMC4.5 40.870.058 0.25
4-Ethyltoluene 0.21 0.20 11/10/23 17:43 KMC1.0 40.980.087 0.43
Heptane 1.6 0.20 11/10/23 17:43 KMC6.4 40.820.13 0.52
Hexachlorobutadiene ND 0.20 11/10/23 17:43 KMCND42.10.12 1.2
Hexane 4.3 8.0 11/10/23 17:43 KMCJ154282.6 9.3
2-Hexanone (MBK)ND 0.20 11/10/23 17:43 KMCND40.820.087 0.35
Isopropanol ND 8.0 11/10/23 17:43 KMCL-03 ND 4202.5 6.2
Methyl tert-Butyl Ether (MTBE)0.31 0.20 11/10/23 17:43 KMC1.1 40.720.098 0.35
Methylene Chloride 0.68 2.0 11/10/23 17:43 KMCJ2.4 46.90.54 1.9
4-Methyl-2-pentanone (MIBK)0.90 0.20 11/10/23 17:43 KMC3.7 40.820.11 0.43
Naphthalene ND 0.20 11/10/23 17:43 KMCND41.00.13 0.70
Propene 23 8.0 11/10/23 17:43 KMC404142.2 3.7
Styrene 0.15 0.20 11/10/23 17:43 KMCJ0.65 40.850.11 0.46
1,1,2,2-Tetrachloroethane ND 0.20 11/10/23 17:43 KMCND41.40.050 0.34
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1200 Metropolitan Ave, Charlotte,
Date Received: 11/7/2023
Work Order: 23K1152Sample Description/Location:
Field Sample #: DUP-1
Sample ID: 23K1152-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -5.0
Receipt Vacuum(in Hg): -4.4
Sampled: 11/2/2023 14:40
Canister ID: 2311
Flow Controller ID: 4659
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 18 0.20 11/10/23 17:43 KMC12041.40.075 0.51
Tetrahydrofuran 2.3 2.0 11/10/23 17:43 KMC6.9 45.90.41 1.2
Toluene 14 0.20 11/10/23 17:43 KMC5340.750.073 0.27
1,2,4-Trichlorobenzene ND 0.20 11/10/23 17:43 KMCND41.50.11 0.80
1,1,1-Trichloroethane ND 0.20 11/10/23 17:43 KMCND41.10.063 0.34
1,1,2-Trichloroethane ND 0.20 11/10/23 17:43 KMCND41.10.051 0.28
Trichloroethylene 0.20 0.20 11/10/23 17:43 KMCJ1.1 41.10.082 0.44
Trichlorofluoromethane (Freon 11)0.43 0.80 11/10/23 17:43 KMCJ2.4 44.50.082 0.46
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.15 0.80 11/10/23 17:43 KMCJ1.2 46.10.044 0.34
1,2,4-Trimethylbenzene 0.89 0.20 11/10/23 17:43 KMC4.4 40.980.092 0.45
1,3,5-Trimethylbenzene 0.16 0.20 11/10/23 17:43 KMCJ0.81 40.980.10 0.51
Vinyl Acetate ND 4.0 11/10/23 17:43 KMCND4140.71 2.5
Vinyl Chloride ND 0.20 11/10/23 17:43 KMCND40.510.091 0.23
m&p-Xylene 3.1 0.40 11/10/23 17:43 KMC1341.70.14 0.61
o-Xylene 1.0 0.20 11/10/23 17:43 KMC4.4 40.870.073 0.32
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)103 11/10/23 17:4370-130
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
23K1152-01 [SG-1]B358063 1.5 1 N/A 1000 400 150 11/10/23
23K1152-02 [SG-2]B358063 1.5 1 N/A 1000 400 150 11/10/23
23K1152-03 [SG-3]B358063 1.5 1 N/A 1000 400 150 11/10/23
23K1152-04 [SG-4]B358063 1.5 1 N/A 1000 400 150 11/10/23
23K1152-05 [DUP-1]B358063 1.5 1 N/A 1000 400 150 11/10/23
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B358063 - TO-15 Prep
Blank (B358063-BLK1)Prepared & Analyzed: 11/10/23
1.4NDAcetone
0.035NDBenzene
0.035NDBenzyl chloride
0.035NDBromodichloromethane
0.035NDBromoform
0.035NDBromomethane
0.035ND1,3-Butadiene
1.4ND2-Butanone (MEK)
0.35NDCarbon Disulfide
0.035 V-34NDCarbon Tetrachloride
0.035NDChlorobenzene
0.035NDChloroethane
0.035NDChloroform
0.070NDChloromethane
0.035NDCyclohexane
0.035NDDibromochloromethane
0.035ND1,2-Dibromoethane (EDB)
0.035ND1,2-Dichlorobenzene
0.035ND1,3-Dichlorobenzene
0.035ND1,4-Dichlorobenzene
0.035 V-05NDDichlorodifluoromethane (Freon 12)
0.035ND1,1-Dichloroethane
0.035ND1,2-Dichloroethane
0.035ND1,1-Dichloroethylene
0.035NDcis-1,2-Dichloroethylene
0.035NDtrans-1,2-Dichloroethylene
0.035ND1,2-Dichloropropane
0.035NDcis-1,3-Dichloropropene
0.035NDtrans-1,3-Dichloropropene
0.035ND1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon
114)
0.35ND1,4-Dioxane
1.4NDEthanol
0.35NDEthyl Acetate
0.035NDEthylbenzene
0.035ND4-Ethyltoluene
0.035NDHeptane
0.035NDHexachlorobutadiene
1.4NDHexane
0.035ND2-Hexanone (MBK)
1.4 L-03NDIsopropanol
0.035NDMethyl tert-Butyl Ether (MTBE)
0.35NDMethylene Chloride
0.035ND4-Methyl-2-pentanone (MIBK)
0.035NDNaphthalene
1.4NDPropene
0.035NDStyrene
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B358063 - TO-15 Prep
Blank (B358063-BLK1)Prepared & Analyzed: 11/10/23
0.035ND1,1,2,2-Tetrachloroethane
0.035NDTetrachloroethylene
0.35NDTetrahydrofuran
0.035NDToluene
0.035ND1,2,4-Trichlorobenzene
0.035ND1,1,1-Trichloroethane
0.035ND1,1,2-Trichloroethane
0.035NDTrichloroethylene
0.14NDTrichlorofluoromethane (Freon 11)
0.14ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.035ND1,2,4-Trimethylbenzene
0.035ND1,3,5-Trimethylbenzene
0.70NDVinyl Acetate
0.035NDVinyl Chloride
0.070NDm&p-Xylene
0.035NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1018.09
LCS (B358063-BS1)Prepared & Analyzed: 11/10/23
5.00 70-13073.23.66Acetone
5.00 70-1301055.26Benzene
5.00 70-1301025.09Benzyl chloride
5.00 70-13096.04.80Bromodichloromethane
5.00 70-1301135.65Bromoform
5.00 70-13083.74.18Bromomethane
5.00 70-13077.53.871,3-Butadiene
5.00 70-1301065.312-Butanone (MEK)
5.00 70-1301035.13Carbon Disulfide
5.00 V-3470-13098.44.92Carbon Tetrachloride
5.00 70-13097.04.85Chlorobenzene
5.00 70-13078.43.92Chloroethane
5.00 70-1301045.19Chloroform
5.00 70-13078.63.93Chloromethane
5.00 70-1301155.74Cyclohexane
5.00 70-1301065.31Dibromochloromethane
5.00 70-13099.95.001,2-Dibromoethane (EDB)
5.00 70-13091.74.591,2-Dichlorobenzene
5.00 70-13095.04.751,3-Dichlorobenzene
5.00 70-13092.74.631,4-Dichlorobenzene
5.00 V-0570-1301035.16Dichlorodifluoromethane (Freon 12)
5.00 70-13098.74.941,1-Dichloroethane
5.00 70-1301055.241,2-Dichloroethane
5.00 70-13091.64.581,1-Dichloroethylene
5.00 70-1301035.15cis-1,2-Dichloroethylene
5.00 70-1301045.21trans-1,2-Dichloroethylene
5.00 70-13093.54.671,2-Dichloropropane
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B358063 - TO-15 Prep
LCS (B358063-BS1)Prepared & Analyzed: 11/10/23
5.00 70-1301035.14cis-1,3-Dichloropropene
5.00 70-1301085.42trans-1,3-Dichloropropene
5.00 70-13086.44.321,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon
114)
5.00 70-1301155.731,4-Dioxane
5.00 70-1301015.06Ethanol
5.00 70-13093.74.69Ethyl Acetate
5.00 70-1301115.55Ethylbenzene
5.00 70-1301145.704-Ethyltoluene
5.00 70-1301105.52Heptane
4.25 70-13099.84.24Hexachlorobutadiene
5.00 70-1301095.45Hexane
5.00 70-1301145.682-Hexanone (MBK)
5.00 L-0370-13068.73.44Isopropanol *
5.00 70-1301115.57Methyl tert-Butyl Ether (MTBE)
5.00 70-13082.94.14Methylene Chloride
5.00 70-1301095.434-Methyl-2-pentanone (MIBK)
3.68 V-0670-1301094.03Naphthalene
5.00 70-13093.54.67Propene
5.00 70-1301075.36Styrene
5.00 70-13089.74.481,1,2,2-Tetrachloroethane
5.00 70-1301015.07Tetrachloroethylene
5.00 70-1301246.20Tetrahydrofuran
5.00 70-1301135.67Toluene
3.90 70-13095.13.711,2,4-Trichlorobenzene
5.00 70-13095.64.781,1,1-Trichloroethane
5.00 70-1301025.091,1,2-Trichloroethane
5.00 70-1301005.01Trichloroethylene
5.00 70-13083.44.17Trichlorofluoromethane (Freon 11)
5.00 70-13094.44.721,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-1301075.331,2,4-Trimethylbenzene
5.00 70-1301065.301,3,5-Trimethylbenzene
5.00 70-1301125.60Vinyl Acetate
5.00 70-13079.13.96Vinyl Chloride
10.0 70-13010810.8m&p-Xylene
5.00 70-1301115.54o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1139.02
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B358063 - TO-15 Prep
Duplicate (B358063-DUP1)Prepared & Analyzed: 11/10/23 Source: 23K1152-05
8.0 31 255.7433Acetone1978
0.20 2.4 259.112.6Benzene 0.648.4
0.20 ND 25NDBenzyl chloride 1.0ND
0.20 0.18 2514.10.21Bromodichloromethane 1.31.4
0.20 ND 25NDBromoform2.1ND
0.20 ND 25NDBromomethane0.78ND
0.20 ND 25ND1,3-Butadiene 0.44ND
8.0 ND 25 J2.32-Butanone (MEK)246.7
2.0 11 255.7412Carbon Disulfide 6.238
0.20 0.13 25 V-34, J0.000.13Carbon Tetrachloride 1.30.81
0.20 ND 25NDChlorobenzene0.92ND
0.20 ND 25NDChloroethane0.53ND
0.20 3.9 256.054.2Chloroform 0.9820
0.40 0.17 25 J4.650.18Chloromethane 0.830.36
0.20 8.2 257.828.8Cyclohexane 0.6930
0.20 ND 25NDDibromochloromethane1.7ND
0.20 ND 25ND1,2-Dibromoethane (EDB)1.5ND
0.20 ND 25ND1,2-Dichlorobenzene 1.2ND
0.20 ND 25 J0.0761,3-Dichlorobenzene 1.20.46
0.20 ND 25ND1,4-Dichlorobenzene 1.2ND
0.20 0.24 25 V-0513.70.28Dichlorodifluoromethane (Freon 12)0.991.4
0.20 ND 25ND1,1-Dichloroethane 0.81ND
0.20 ND 25ND1,2-Dichloroethane 0.81ND
0.20 ND 25ND1,1-Dichloroethylene 0.79ND
0.20 ND 25NDcis-1,2-Dichloroethylene 0.79ND
0.20 ND 25NDtrans-1,2-Dichloroethylene 0.79ND
0.20 ND 25ND1,2-Dichloropropane 0.92ND
0.20 ND 25NDcis-1,3-Dichloropropene 0.91ND
0.20 ND 25NDtrans-1,3-Dichloropropene 0.91ND
0.20 ND 25ND1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon
114)
1.4ND
2.0 ND 25ND1,4-Dioxane 7.2ND
8.0 19 257.5021Ethanol1539
2.0 ND 25NDEthyl Acetate 7.2ND
0.20 1.0 2512.61.2Ethylbenzene 0.875.1
0.20 0.21 259.170.234-Ethyltoluene 0.981.1
0.20 1.6 257.881.7Heptane 0.826.9
0.20 ND 25NDHexachlorobutadiene2.1ND
8.0 4.3 25 J8.464.7Hexane 2817
0.20 ND 25ND2-Hexanone (MBK)0.82ND
8.0 ND 25 L-03NDIsopropanol20ND
0.20 0.31 253.820.32Methyl tert-Butyl Ether (MTBE)0.721.2
2.0 0.68 25 J8.400.74Methylene Chloride 6.92.6
0.20 0.90 255.170.954-Methyl-2-pentanone (MIBK)0.823.9
0.20 ND 25NDNaphthalene1.0ND
8.0 23 257.5725Propene1443
0.20 0.15 25 J16.90.18Styrene 0.850.77
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B358063 - TO-15 Prep
Duplicate (B358063-DUP1)Prepared & Analyzed: 11/10/23 Source: 23K1152-05
0.20 ND 25ND1,1,2,2-Tetrachloroethane 1.4ND
0.20 18 259.3419Tetrachloroethylene1.4130
2.0 2.3 257.882.5Tetrahydrofuran 5.97.5
0.20 14 259.3515Toluene0.7558
0.20 ND 25ND1,2,4-Trichlorobenzene 1.5ND
0.20 ND 25ND1,1,1-Trichloroethane 1.1ND
0.20 ND 25ND1,1,2-Trichloroethane 1.1ND
0.20 0.20 25 J0.000.20Trichloroethylene 1.11.1
0.80 0.43 25 J7.210.46Trichlorofluoromethane (Freon 11)4.52.6
0.80 0.15 25 J5.130.161,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
6.11.2
0.20 0.89 259.400.981,2,4-Trimethylbenzene 0.984.8
0.20 0.16 25 J0.000.161,3,5-Trimethylbenzene 0.980.81
4.0 ND 25NDVinyl Acetate 14ND
0.20 ND 25NDVinyl Chloride 0.51ND
0.40 3.1 258.373.3m&p-Xylene 1.714
0.20 1.0 2516.31.2o-Xylene 0.875.2
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1038.24
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation
which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramµg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration
(CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this
compound is likely to be biased on the low side.
L-03
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this
compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this
compound.
V-06
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data
validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYST
Thomas P. HniteckiTPH
Rebecca FaustRLF
Kristen M CoutureKMC
Karriem G. Mariuskgm
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S095502-ICV1 )Lab File ID: G23A292017.D Analyzed: 10/20/23 16:14
Bromochloromethane (1)1107131 8.036 1080445 8.03 60 - 140102 0.0060 +/-0.50
1,4-Difluorobenzene (1)2388965 9.804 2308848 9.804 60 - 140103 0.0000 +/-0.50
Chlorobenzene-d5 (1)2148001 14.157 2077591 14.157 60 - 140103 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S096287-CCV1 )Lab File ID: G23A313002.D Analyzed: 11/10/23 09:33
Bromochloromethane (1)972237 8.036 1080445 8.03 60 - 14090 0.0060 +/-0.50
1,4-Difluorobenzene (1)2181212 9.804 2308848 9.804 60 - 14094 0.0000 +/-0.50
Chlorobenzene-d5 (1)2006199 14.157 2077591 14.157 60 - 14097 0.0000 +/-0.50
LCS (B358063-BS1 )Lab File ID: G23A313004.D Analyzed: 11/10/23 10:53
Bromochloromethane (1)963062 8.03 972237 8.036 60 - 14099 -0.0060 +/-0.50
1,4-Difluorobenzene (1)2230765 9.804 2181212 9.804 60 - 140102 0.0000 +/-0.50
Chlorobenzene-d5 (1)1970377 14.156 2006199 14.157 60 - 14098 -0.0010 +/-0.50
Blank (B358063-BLK1 )Lab File ID: G23A313009.D Analyzed: 11/10/23 14:21
Bromochloromethane (1)894831 8.036 972237 8.036 60 - 14092 0.0000 +/-0.50
1,4-Difluorobenzene (1)2054925 9.804 2181212 9.804 60 - 14094 0.0000 +/-0.50
Chlorobenzene-d5 (1)1834468 14.157 2006199 14.157 60 - 14091 0.0000 +/-0.50
SG-1 (23K1152-01 )Lab File ID: G23A313010.D Analyzed: 11/10/23 15:01
Bromochloromethane (1)897556 8.036 972237 8.036 60 - 14092 0.0000 +/-0.50
1,4-Difluorobenzene (1)1999652 9.804 2181212 9.804 60 - 14092 0.0000 +/-0.50
Chlorobenzene-d5 (1)1778879 14.157 2006199 14.157 60 - 14089 0.0000 +/-0.50
SG-2 (23K1152-02 )Lab File ID: G23A313011.D Analyzed: 11/10/23 15:41
Bromochloromethane (1)917729 8.036 972237 8.036 60 - 14094 0.0000 +/-0.50
1,4-Difluorobenzene (1)2104482 9.804 2181212 9.804 60 - 14096 0.0000 +/-0.50
Chlorobenzene-d5 (1)1851111 14.157 2006199 14.157 60 - 14092 0.0000 +/-0.50
SG-3 (23K1152-03 )Lab File ID: G23A313012.D Analyzed: 11/10/23 16:22
Bromochloromethane (1)894288 8.03 972237 8.036 60 - 14092 -0.0060 +/-0.50
1,4-Difluorobenzene (1)2004791 9.804 2181212 9.804 60 - 14092 0.0000 +/-0.50
Chlorobenzene-d5 (1)1736320 14.157 2006199 14.157 60 - 14087 0.0000 +/-0.50
SG-4 (23K1152-04 )Lab File ID: G23A313013.D Analyzed: 11/10/23 17:02
Bromochloromethane (1)921830 8.036 972237 8.036 60 - 14095 0.0000 +/-0.50
1,4-Difluorobenzene (1)2100067 9.804 2181212 9.804 60 - 14096 0.0000 +/-0.50
Chlorobenzene-d5 (1)1828618 14.157 2006199 14.157 60 - 14091 0.0000 +/-0.50
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
DUP-1 (23K1152-05 )Lab File ID: G23A313014.D Analyzed: 11/10/23 17:43
Bromochloromethane (1)925683 8.03 972237 8.036 60 - 14095 -0.0060 +/-0.50
1,4-Difluorobenzene (1)2146541 9.804 2181212 9.804 60 - 14098 0.0000 +/-0.50
Chlorobenzene-d5 (1)1919554 14.157 2006199 14.157 60 - 14096 0.0000 +/-0.50
Duplicate (B358063-DUP1 )Lab File ID: G23A313015.D Analyzed: 11/10/23 18:24
Bromochloromethane (1)923954 8.03 972237 8.036 60 - 14095 -0.0060 +/-0.50
1,4-Difluorobenzene (1)2094308 9.798 2181212 9.804 60 - 14096 -0.0060 +/-0.50
Chlorobenzene-d5 (1)1836594 14.157 2006199 14.157 60 - 14092 0.0000 +/-0.50
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S096287-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.9009161A -28.1 303.59 1.2538375.00Acetone
0.8957875A 3.1 305.16 0.86846265.00Benzene
1.08726A 31.1 *306.56 0.82911255.00Benzyl chloride
0.6483522A 0.3 305.01 0.64660795.00Bromodichloromethane
0.5430704A 10.4 305.52 0.491815.00Bromoform
0.5313931A -18.5 304.08 0.65206475.00Bromomethane
0.4802171A -22.3 303.88 0.61834585.001,3-Butadiene
1.379464A 0.8 305.04 1.3684915.002-Butanone (MEK)
1.770251A -4.9 304.76 1.8607085.00Carbon Disulfide
0.4645894A -7.6 304.62 0.50286635.00Carbon Tetrachloride
0.8060616A 1.5 305.08 0.79380955.00Chlorobenzene
0.295523A -23.6 303.82 0.38672425.00Chloroethane
1.330553A -0.2 304.99 1.3331545.00Chloroform
0.6219899A -22.8 303.86 0.80600895.00Chloromethane
0.3527081A 8.1 305.40 0.32636625.00Cyclohexane
0.5818821A 2.3 305.11 0.56906025.00Dibromochloromethane
0.5604166A 1.7 305.09 0.55084195.001,2-Dibromoethane (EDB)
0.7123888A 16.4 305.82 0.6117715.001,2-Dichlorobenzene
0.7679318A 15.4 305.77 0.66556015.001,3-Dichlorobenzene
0.7606344A 16.2 305.81 0.65487255.001,4-Dichlorobenzene
1.009168A -31.5 *303.42 1.4736495.00Dichlorodifluoromethane (Freon 12)
1.224422A -4.7 304.76 1.2854575.001,1-Dichloroethane
0.8663962A 0.9 305.05 0.85834685.001,2-Dichloroethane
1.03346A -10.8 304.46 1.1581915.001,1-Dichloroethylene
0.9001246A 0.6 305.03 0.89512285.00cis-1,2-Dichloroethylene
0.9374636A -1.2 304.94 0.94910985.00trans-1,2-Dichloroethylene
0.3583974A -6.7 304.66 0.38423945.001,2-Dichloropropane
0.5282898A 8.3 305.42 0.48772785.00cis-1,3-Dichloropropene
0.4717781A 12.7 305.64 0.4184645.00trans-1,3-Dichloropropene
1.559179A -11.9 304.40 1.770165.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.1519889A 8.9 305.45 0.13955065.001,4-Dioxane
0.1576669A -29.9 303.51 0.22484595.00Ethanol
0.2582218A 5.6 305.28 0.24444235.00Ethyl Acetate
1.456675A 14.5 305.72 1.2724725.00Ethylbenzene
1.493142A 23.9 306.20 1.2051755.004-Ethyltoluene
0.3021425A 8.9 305.45 0.27732775.00Heptane
0.5177991A 20.3 306.01 0.43059315.00Hexachlorobutadiene
0.807306A 2.4 305.12 0.7882155.00Hexane
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S096287-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.7810424A 11.9 305.59 0.69810375.002-Hexanone (MBK)
1.030718A -27.4 303.63 1.420455.00Isopropanol
1.735922A 4.7 305.24 1.6572415.00Methyl tert-Butyl Ether (MTBE)
0.7687475A -18.2 304.09 0.94008375.00Methylene Chloride
0.7872343A 8.4 305.42 0.72652345.004-Methyl-2-pentanone (MIBK)
1.069861A 42.3 *307.12 0.75168145.00Naphthalene
0.6609845A -12.6 304.37 0.75654245.00Propene
0.8146765A 18.0 305.90 0.69066715.00Styrene
0.9270921A 5.7 305.28 0.87720825.001,1,2,2-Tetrachloroethane
0.4642363A 2.7 305.13 0.45215555.00Tetrachloroethylene
0.2770847A 9.7 305.48 0.25261715.00Tetrahydrofuran
1.112372A 10.1 305.50 1.0105265.00Toluene
0.5278798A 31.0 *306.55 0.40296425.001,2,4-Trichlorobenzene
0.5478686A 0.6 305.03 0.54480665.001,1,1-Trichloroethane
0.3768838A 2.0 305.10 0.36956075.001,1,2-Trichloroethane
0.3647066A 0.5 305.03 0.36278165.00Trichloroethylene
1.345509A -18.7 304.07 1.6541395.00Trichlorofluoromethane (Freon 11)
1.173176A -8.1 304.60 1.2766295.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
1.221293A 26.7 306.34 0.96385465.001,2,4-Trimethylbenzene
1.219361A 20.7 306.04 1.0101165.001,3,5-Trimethylbenzene
1.399422A -2.9 304.80 1.4417885.00Vinyl Acetate
0.659719A -21.6 303.92 0.84195475.00Vinyl Chloride
1.110213A 13.3 3011.3 0.979630910.0m&p-Xylene
1.160143A 17.6 305.88 0.98631065.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
NY,ME,NHAcetone
FL,NJ,NY,ME,NH,VABenzene
FL,NJ,NY,ME,NH,VABenzyl chloride
NJ,NY,ME,NH,VABromodichloromethane
NJ,NY,ME,NH,VABromoform
FL,NJ,NY,ME,NHBromomethane
NJ,NY,ME,NH,VA1,3-Butadiene
FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
NJ,NY,ME,NH,VACarbon Disulfide
FL,NJ,NY,ME,NH,VACarbon Tetrachloride
FL,NJ,NY,ME,NH,VAChlorobenzene
FL,NJ,NY,ME,NH,VAChloroethane
FL,NJ,NY,ME,NH,VAChloroform
FL,NJ,NY,ME,NH,VAChloromethane
NJ,NY,ME,NH,VACyclohexane
NY,ME,NHDibromochloromethane
NJ,NY,ME,NH1,2-Dibromoethane (EDB)
FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
NJ,NY,ME,NH1,3-Dichlorobenzene
FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
NY,ME,NHDichlorodifluoromethane (Freon 12)
FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
NY,ME,NHtrans-1,3-Dichloropropene
NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
NJ,NY,ME,NH,VA1,4-Dioxane
FL,NJ,NY,ME,NH,VAEthylbenzene
NJ,NY,ME,NH,VAHeptane
NJ,NY,ME,NH,VAHexachlorobutadiene
FL,NJ,NY,ME,NH,VAHexane
NY,ME,NHIsopropanol
FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
FL,NJ,NY,ME,NH,VAMethylene Chloride
FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
FL,NJ,NY,ME,NH,VAStyrene
FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
FL,NJ,NY,ME,NH,VATetrachloroethylene
FL,NJ,NY,ME,NH,VAToluene
NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
FL,NJ,NY,ME,NH,VATrichloroethylene
NY,ME,NHTrichlorofluoromethane (Freon 11)
NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NJ,NY,ME,NH1,2,4-Trimethylbenzene
NJ,NY,ME,NH1,3,5-Trimethylbenzene
FL,NJ,NY,ME,NH,VAVinyl Acetate
FL,NJ,NY,ME,NH,VAVinyl Chloride
FL,NJ,NY,ME,NH,VAm&p-Xylene
FL,NJ,NY,ME,NH,VAo-Xylene
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
10899 NELAPNew York State Department of HealthNY 04/1/2024
2516 NELAPNew Hampshire Environmental LabNH 02/5/2024
MA007 NELAPNew Jersey DEPNJ 06/30/2024
E871027 NELAPFlorida Department of HealthFL 06/30/2024
MA00100State of MaineME 06/9/2025
460217Commonwealth of VirginiaVA 12/14/2023

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/9/2024
Mid-Atlantic Associates, Inc. - Charlotte Shane Sisco
1125 E. Morehead Street, Suite 104 Charlotte, NC, 28204
Ref: Analytical Testing
Lab Report Number: 24-120-0005 Client Project Description: Metropolitan
Dear Shane Sisco:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/26/2024 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 163
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2024402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202499012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202540750State ProgramAlabama
02/07/202588-0650State ProgramArkansas
06/30/20242904State ProgramCalifornia
06/30/2024E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202404015State ProgramGeorgia
10/31/2024200078State Program - NELAPIllinois
06/30/202480215State ProgramKentucky
12/31/2024KY90047State ProgramKentucky
12/31/2024LA037State Program - NELAPLouisiana
06/30/202404015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202447701State ProgramNorth Carolina
12/31/2024415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202484002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2024T104704180State Program - NELAPTexas
06/30/202400106State ProgramVirginia
09/14/2024460181State Program - NELAPVirginia
Page 1 of 1 00016/24-120-0005
Page 2 of 163
Report Number:
Sample Summary Table
Client Project Description:
24-120-0005
Metropolitan
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
04/26/2024 12:25Solids 92180 ES-1E (1-2)04/26/2024 15:25
04/26/2024 12:30Solids 92181 ES-1 04/26/2024 15:25
04/26/2024 12:30Solids 92181 ES-1 04/26/2024 15:25 6020B WP MTN -
04/26/2024 12:30Solids 92181 ES-1 04/26/2024 15:25 SW-7199 WP MTN -
04/26/2024 12:35Solids 92182 ES-2E (1-2)04/26/2024 15:25
04/26/2024 12:40Solids 92183 ES-2 04/26/2024 15:25
04/26/2024 12:40Solids 92183 ES-2 04/26/2024 15:25 6020B WP MTN -
04/26/2024 12:40Solids 92183 ES-2 04/26/2024 15:25 SW-7199 WP MTN -
04/26/2024 12:45Solids 92184 ES-3A (1-2)04/26/2024 15:25
04/26/2024 12:50Solids 92185 ES-3 04/26/2024 15:25
04/26/2024 12:50Solids 92185 ES-3 04/26/2024 15:25 SW-7199 WP MTN -
04/26/2024 12:50Solids 92185 ES-3 04/26/2024 15:25 6020B WP MTN -
04/26/2024Solids 92186 DUP-1 (1-2)04/26/2024 15:25
04/26/2024Solids 92187 DUP-1 04/26/2024 15:25
04/26/2024Solids 92187 DUP-1 04/26/2024 15:25 6020B WP MTN -
04/26/2024Solids 92187 DUP-1 04/26/2024 15:25 SW-7199 WP MTN -
04/26/2024 13:45Solids 92188 ES-4B (4-5)04/26/2024 15:25
04/26/2024 07:00Aqueous 92189 Trip Blank 04/26/2024 15:25
04/26/2024 10:30Aqueous 92190 TMW-1 04/26/2024 15:25
04/26/2024 10:30Aqueous 92190 TMW-1 04/26/2024 15:25 6020B WP MTN -
04/26/2024 08:10Aqueous 92191 TMW-2 04/26/2024 15:25
04/26/2024 08:10Aqueous 92191 TMW-2 04/26/2024 15:25 6020B WP MTN -
04/26/2024 13:05Aqueous 92192 TMW-3 04/26/2024 15:25
04/26/2024 13:05Aqueous 92192 TMW-3 04/26/2024 15:25 6020B WP MTN -
04/26/2024Aqueous 92193 DUP-2 04/26/2024 15:25
04/26/2024Aqueous 92193 DUP-2 04/26/2024 15:25 6020B WP MTN -
04/26/2024 13:50Solids 92194 ES-4 04/26/2024 15:25
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 163
Report Number:
Sample Summary Table
Client Project Description:
24-120-0005
Metropolitan
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
04/26/2024 13:50Solids 92194 ES-4 04/26/2024 15:25 SW-7199 WP MTN -
04/26/2024 13:50Solids 92194 ES-4 04/26/2024 15:25 6020B WP MTN -
04/26/2024 12:55Solids 92195 ES-5E (4-5)04/26/2024 15:25
04/26/2024 13:00Solids 92196 ES-5 04/26/2024 15:25
04/26/2024 13:00Solids 92196 ES-5 04/26/2024 15:25 SW-7199 WP MTN -
04/26/2024 13:00Solids 92196 ES-5 04/26/2024 15:25 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 4 of 163
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-120-0005
Report Limit
Project:Metropolitan
V 92180ES-1E (1-2)
0.058 04/29/2024 16:328260DAcetonemg/Kg - dry 0.002
J0.003 04/29/2024 16:328260DMethylene Chloride mg/Kg - dry 0.001
17.4 05/01/2024 10:05SW-DRYWT Moisture %
V 92181ES-1
1460 05/04/2024 14:046020BArsenicµg/Kg - dry 100
70600 05/04/2024 14:046020BBariumµg/Kg - dry 50.1
J83.5 05/04/2024 14:046020BCadmiumµg/Kg - dry 30.4
34200 05/04/2024 14:046020BChromiumµg/Kg - dry 136
13100 05/04/2024 14:046020BLeadµg/Kg - dry 36.3
347 05/04/2024 14:046020BSeleniumµg/Kg - dry 120
J10205/04/2024 14:046020BSilverµg/Kg - dry 7.88
J0.0292 05/03/2024 12:407471BMercury (Total)mg/Kg - dry 0.0140
J0.280 05/01/2024 15:128270EBenzo(a)anthracene mg/Kg - dry 0.182
J0.261 05/01/2024 15:128270EBenzo(a)pyrene mg/Kg - dry 0.192
J0.333 05/01/2024 15:128270EBenzo(b)fluoranthene mg/Kg - dry 0.171
J0.210 05/01/2024 15:128270EChrysenemg/Kg - dry 0.170
J0.401 05/01/2024 15:128270EFluoranthenemg/Kg - dry 0.184
J0.201 05/01/2024 15:128270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.176
J0.231 05/01/2024 15:128270EPhenanthrenemg/Kg - dry 0.184
J0.350 05/01/2024 15:128270EPyrenemg/Kg - dry 0.187
0.265 05/02/2024 17:48SW-7199 Chromium, Hexavalent mg/Kg - dry 0.164
14.5 05/01/2024 10:05SW-DRYWT Moisture %
V 92182ES-2E (1-2)
J0.016 04/29/2024 16:598260DAcetonemg/Kg - dry 0.002
J0.0007 04/29/2024 16:598260DCarbon Disulfide mg/Kg - dry 0.0007
J0.003 04/29/2024 16:598260DMethylene Chloride mg/Kg - dry 0.001
12.5 05/01/2024 10:05SW-DRYWT Moisture %
V 92183ES-2
1200 05/04/2024 14:106020BArsenicµg/Kg - dry 97.0
74700 05/04/2024 14:106020BBariumµg/Kg - dry 48.6
J67.0 05/04/2024 14:106020BCadmiumµg/Kg - dry 29.5
35200 05/04/2024 14:106020BChromiumµg/Kg - dry 132
9880 05/04/2024 14:106020BLeadµg/Kg - dry 35.2
300 05/04/2024 14:106020BSeleniumµg/Kg - dry 117
J10705/04/2024 14:106020BSilverµg/Kg - dry 7.65
Page 5 of 163
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-120-0005
Report Limit
Project:Metropolitan
V 92183ES-2
J0.0170 05/03/2024 12:437471BMercury (Total)mg/Kg - dry 0.0136
J0.203 05/01/2024 14:488270EFluoranthenemg/Kg - dry 0.179
B0.414 05/02/2024 18:53SW-7199 Chromium, Hexavalent mg/Kg - dry 0.160
11.9 05/01/2024 10:05SW-DRYWT Moisture %
V 92184ES-3A (1-2)
0.027 04/30/2024 14:028260DAcetonemg/Kg - dry 0.002
J0.001 04/30/2024 14:028260DCarbon Disulfide mg/Kg - dry 0.0007
J0.003 04/30/2024 14:028260DMethylene Chloride mg/Kg - dry 0.001
0.055 04/30/2024 14:028260DNaphthalenemg/Kg - dry 0.001
14.0 05/01/2024 10:05SW-DRYWT Moisture %
V 92185ES-3
1330 05/04/2024 14:156020BArsenicµg/Kg - dry 99.8
77600 05/04/2024 14:156020BBariumµg/Kg - dry 49.9
J62.8 05/04/2024 14:156020BCadmiumµg/Kg - dry 30.3
44800 05/04/2024 14:156020BChromiumµg/Kg - dry 135
8630 05/04/2024 14:156020BLeadµg/Kg - dry 36.2
J27905/04/2024 14:156020BSeleniumµg/Kg - dry 120
J77.2 05/04/2024 14:156020BSilverµg/Kg - dry 7.86
J0.0219 05/03/2024 12:457471BMercury (Total)mg/Kg - dry 0.0140
J0.437 05/01/2024 16:028270EBenzo(a)anthracene mg/Kg - dry 0.182
J0.365 05/01/2024 16:028270EBenzo(a)pyrene mg/Kg - dry 0.192
J0.518 05/01/2024 16:028270EBenzo(b)fluoranthene mg/Kg - dry 0.171
J0.221 05/01/2024 16:028270EBenzo(g,h,i)perylene mg/Kg - dry 0.168
J0.331 05/01/2024 16:028270EChrysenemg/Kg - dry 0.170
0.932 05/01/2024 16:028270EFluoranthenemg/Kg - dry 0.184
J0.318 05/01/2024 16:028270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.176
J0.683 05/01/2024 16:028270EPhenanthrenemg/Kg - dry 0.184
J0.602 05/01/2024 16:028270EPyrenemg/Kg - dry 0.186
B0.327 05/02/2024 19:04SW-7199 Chromium, Hexavalent mg/Kg - dry 0.164
14.3 05/01/2024 10:05SW-DRYWT Moisture %
V 92186DUP-1 (1-2)
J0.021 04/29/2024 17:548260DAcetonemg/Kg - dry 0.002
J0.003 04/29/2024 17:548260DMethylene Chloride mg/Kg - dry 0.001
13.9 05/01/2024 10:05SW-DRYWT Moisture %
Page 6 of 163
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-120-0005
Report Limit
Project:Metropolitan
V 92187DUP-1
1220 05/04/2024 14:216020BArsenicµg/Kg - dry 99.3
74800 05/04/2024 14:216020BBariumµg/Kg - dry 49.7
J49.4 05/04/2024 14:216020BCadmiumµg/Kg - dry 30.2
44400 05/04/2024 14:216020BChromiumµg/Kg - dry 135
6790 05/04/2024 14:216020BLeadµg/Kg - dry 36.0
J20905/04/2024 14:216020BSeleniumµg/Kg - dry 120
J71.9 05/04/2024 14:216020BSilverµg/Kg - dry 7.83
J0.0141 05/03/2024 12:487471BMercury (Total)mg/Kg - dry 0.0139
J0.265 05/01/2024 15:378270EBis(2-ethylhexyl)phthalate mg/Kg - dry 0.205
J0.210 05/01/2024 15:378270EFluoranthenemg/Kg - dry 0.183
B0.470 05/02/2024 19:15SW-7199 Chromium, Hexavalent mg/Kg - dry 0.163
13.9 05/01/2024 10:05SW-DRYWT Moisture %
V 92188ES-4B (4-5)
0.036 04/29/2024 18:218260DAcetonemg/Kg - dry 0.003
J0.004 04/29/2024 18:218260DMethylene Chloride mg/Kg - dry 0.002
27.3 05/01/2024 10:05SW-DRYWT Moisture %
V 92189Trip Blank
J0.457 05/03/2024 14:548260DChloromethaneµg/L 0.220
V 92190TMW-1
J0.414 05/07/2024 02:266020BArsenicµg/L 0.297
35.3 05/07/2024 02:266020BBariumµg/L 0.453
J1.83 05/03/2024 15:198260DAcetoneµg/L 1.80
1.50 05/03/2024 15:198260DChloroformµg/L 0.220
5.88 05/03/2024 15:198260Dcis-1,2-Dichloroethene µg/L 0.200
J0.501 05/03/2024 15:198260D2-Hexanone µg/L 0.380
J0.422 05/03/2024 15:198260DTetrachloroetheneµg/L 0.220
V 92191TMW-2
21.7 05/07/2024 02:306020BBariumµg/L 0.453
1.91 05/07/2024 02:306020BChromiumµg/L 0.346
J0.706 05/07/2024 02:306020BSeleniumµg/L 0.703
J1.86 05/03/2024 15:448260DAcetoneµg/L 1.80
2.11 05/03/2024 15:448260Dcis-1,2-Dichloroethene µg/L 0.200
7.58 05/03/2024 15:448260DTetrachloroetheneµg/L 0.220
1.62 05/03/2024 15:448260DTrichloroetheneµg/L 0.180
Page 7 of 163
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-120-0005
Report Limit
Project:Metropolitan
V 92192TMW-3
J0.495 05/07/2024 02:346020BArsenicµg/L 0.297
67.3 05/07/2024 02:346020BBariumµg/L 0.453
1.65 05/07/2024 02:346020BChromiumµg/L 0.346
J3.73 05/03/2024 16:098260DAcetoneµg/L 1.80
4.72 05/03/2024 16:098260DChloroformµg/L 0.220
J1.56 05/03/2024 16:098260D2-Hexanone µg/L 0.380
J0.337 05/03/2024 16:098260DTetrachloroetheneµg/L 0.220
V 92193DUP-2
B1.21 05/03/2024 21:156020BArsenicµg/L 0.297
34.0 05/03/2024 21:156020BBariumµg/L 0.453
J0.946 05/03/2024 21:156020BChromiumµg/L 0.346
J0.887 05/03/2024 21:156020BSeleniumµg/L 0.703
1.64 05/03/2024 16:348260DChloroformµg/L 0.220
5.94 05/03/2024 16:348260Dcis-1,2-Dichloroethene µg/L 0.200
J0.511 05/03/2024 16:348260D2-Hexanone µg/L 0.380
J0.341 05/03/2024 16:348260DTetrachloroetheneµg/L 0.220
V 92194ES-4
876 05/04/2024 14:266020BArsenicµg/Kg - dry 105
74600 05/04/2024 14:266020BBariumµg/Kg - dry 52.5
J33.9 05/04/2024 14:266020BCadmiumµg/Kg - dry 31.9
26000 05/04/2024 14:266020BChromiumµg/Kg - dry 142
5890 05/04/2024 14:266020BLeadµg/Kg - dry 38.0
J24905/04/2024 14:266020BSeleniumµg/Kg - dry 126
J32.8 05/04/2024 14:266020BSilverµg/Kg - dry 8.26
J0.225 05/07/2024 22:278270EAnthracenemg/Kg - dry 0.203
J0.623 05/07/2024 22:278270EBenzo(a)anthracene mg/Kg - dry 0.191
J0.468 05/07/2024 22:278270EBenzo(a)pyrene mg/Kg - dry 0.202
0.860 05/07/2024 22:278270EBenzo(b)fluoranthene mg/Kg - dry 0.180
J0.263 05/07/2024 22:278270EBenzo(g,h,i)perylene mg/Kg - dry 0.176
J0.475 05/07/2024 22:278270EChrysenemg/Kg - dry 0.178
JM0.289 05/07/2024 22:278270EDibenz(a,h)anthracene mg/Kg - dry 0.136
1.30 05/07/2024 22:278270EFluoranthenemg/Kg - dry 0.193
J0.399 05/07/2024 22:278270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.185
0.850 05/07/2024 22:278270EPhenanthrenemg/Kg - dry 0.193
0.819 05/07/2024 22:278270EPyrenemg/Kg - dry 0.196
B0.361 05/02/2024 19:26SW-7199 Chromium, Hexavalent mg/Kg - dry 0.172
Page 8 of 163
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
24-120-0005
Report Limit
Project:Metropolitan
V 92194ES-4
18.4 05/01/2024 10:05SW-DRYWT Moisture %
V 92195ES-5E (4-5)
J0.017 04/29/2024 18:488260DAcetonemg/Kg - dry 0.003
J0.007 04/29/2024 18:488260DMethylene Chloride mg/Kg - dry 0.002
27.7 05/01/2024 10:05SW-DRYWT Moisture %
V 92196ES-5
3550 05/04/2024 14:316020BArsenicµg/Kg - dry 111
78000 05/04/2024 14:316020BBariumµg/Kg - dry 55.8
J37.5 05/04/2024 14:316020BCadmiumµg/Kg - dry 33.9
54100 05/04/2024 14:316020BChromiumµg/Kg - dry 151
5610 05/04/2024 14:316020BLeadµg/Kg - dry 40.4
J18905/04/2024 14:316020BSeleniumµg/Kg - dry 134
J42.6 05/04/2024 14:316020BSilverµg/Kg - dry 8.79
B0.384 05/02/2024 19:37SW-7199 Chromium, Hexavalent mg/Kg - dry 0.183
23.3 05/01/2024 10:05SW-DRYWT Moisture %
Page 9 of 163

Client: Mid-Atlantic Associates, Inc. - Charlotte CASE NARRATIVE
Project: Metropolitan Lab Report Number: 24-120-0005
Date: 5/8/2024
Metals Analyses Method 6020B Sample 92193 (DUP-2) Analyte: Arsenic
QC Batch No: L748679/L748340 Target analyte(s) was identified in the method blank associated with this project, below the Method Quantitation
Limit. Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected in the method blank.
Sample 92252 (S-6)
Analyte: Chromium QC Batch No: L748699/L748510
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 92252 (S-6) Analyte: Selenium
QC Batch No: L748699/L748510 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Hexavalent Chromium by Ion Chromatography Method SW-7199 Analyte: Hexavalent Chromium QC Batch No: L748932
Target analyte(s) was identified in the method blank associated with this project. Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected in the method blank.
Solids Total Mercury Analysis - CVAA Method 7471B Sample 92111
Analyte: Mercury QC Batch No: V46808/V46746
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Volatile Organic Compounds - GC/MS Method 8260D Analyte: Chloromethane
QC Batch No: V46655/V46653 Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there was adequate sensitivity to report this compound at the laboratory reporting limit as non-detect. Analyte: Styrene QC Batch No: V46655/V46653
Page 10 of 163

Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 2,4-Dimethylphenol QC Batch No: V46903/V46647
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: Benzo(b)fluoranthene QC Batch No: V46903/V46647
This target analyte was flagged for recoveries outside QC limits in the associated CCV. Results should be considered estimated due to the potential for a high bias.
Analyte: Benzoic Acid
QC Batch No: V46677/V46647 Refer to LCS/LCSD.
Analyte: Benzoic Acid
QC Batch No: V46677/V46647 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Benzoic Acid
QC Batch No: V46903/V46647 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Analyte: Dibenz(a,h)anthracene QC Batch No: V46675/V46647 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Dibenz(a,h)anthracene
QC Batch No: V46903/V46647 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias. Analyte: Indeno(1,2,3-cd)pyrene
QC Batch No: V46903/V46647 This target analyte was flagged for recoveries outside QC limits in the associated CCV. Results should be considered estimated due to the potential for a high bias. Analyte: Pyridine QC Batch No: V46675/V46647 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 91797 (SS-2) QC Batch No: V46903/V46854 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Page 11 of 163

Sample 91797 (SS-2) QC Batch No: V46903/V46854
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.

Page 12 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1E (1-2)
92180 Matrix:
4/26/2024 12:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.4 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 13 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1E (1-2)
92180 Matrix:
4/26/2024 12:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
0.058 mg/Kg - dry 0.002 0.024Acetone 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 04/29/24 16:32 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 04/29/24 16:32 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 04/29/24 16:32 V46655TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/29/24 16:32 V46655TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 04/29/24 16:32 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/29/24 16:32 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 04/29/24 16:32 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/29/24 16:32 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/29/24 16:32 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 04/29/24 16:32 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 04/29/24 16:32 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/29/24 16:32 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 04/29/24 16:32 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 14 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1E (1-2)
92180 Matrix:
4/26/2024 12:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 04/29/24 16:32 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/29/24 16:32 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 04/29/24 16:32 V46655TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 04/29/24 16:32 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 04/29/24 16:32 V46655TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/29/24 16:32 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/29/24 16:32 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/29/24 16:32 V46655TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 04/29/24 16:32 V46655TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 04/29/24 16:32 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 04/29/24 16:32 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 15 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1E (1-2)
92180 Matrix:
4/26/2024 12:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 04/29/24 16:32 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/29/24 16:32 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 04/29/24 16:32 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 04/29/24 16:32 V46655TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 04/29/24 16:32 V46655TBL
0.003 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/29/24 16:32 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/29/24 16:32 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 04/29/24 16:32 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/29/24 16:32 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/29/24 16:32 V46655TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 04/29/24 16:32 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 04/29/24 16:32 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/29/24 16:32 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1E (1-2)
92180 Matrix:
4/26/2024 12:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 04/29/24 16:32 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 04/29/24 16:32 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 04/29/24 16:32 V46655TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 04/29/24 16:32 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 04/29/24 16:32 V46655
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/29/24 16:321 TBL V46655
Surrogate: Dibromofluoromethane 102 Limits: 84-123%04/29/24 16:321 TBL V46655
Surrogate: Toluene-d8 97.2 Limits: 76-129%04/29/24 16:321 TBL V46655
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1
92181 Matrix:
4/26/2024 12:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.5 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
0.265 mg/Kg - dry 0.164 0.233Chromium, Hexavalent 1 05/02/24 17:48 SW-7199MKD
1460 µg/Kg - dry 100 292Arsenic 5 05/04/24 14:04 6020BCPW
70600 µg/Kg - dry 50.1 292Barium 5 05/04/24 14:04 6020BCPW
83.5 J µg/Kg - dry 30.4 292Cadmium 5 05/04/24 14:04 6020BCPW
34200 µg/Kg - dry 136 292Chromium 5 05/04/24 14:04 6020BCPW
13100 µg/Kg - dry 36.3 292Lead 5 05/04/24 14:04 6020BCPW
0.0292 J mg/Kg - dry 0.0140 0.0351Mercury (Total)1 05/03/24 12:40 7471BJKC
347 µg/Kg - dry 120 292Selenium 5 05/04/24 14:04 6020BCPW
102 J µg/Kg - dry 7.88 292Silver 5 05/04/24 14:04 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 18 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1
92181 Matrix:
4/26/2024 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.171 mg/Kg - dry 0.171 0.771Acenaphthene 1 05/01/24 15:12 V46677AMP
<0.175 mg/Kg - dry 0.175 0.771Acenaphthylene 1 05/01/24 15:12 V46677AMP
<0.245 mg/Kg - dry 0.245 0.771Aniline 1 05/01/24 15:12 V46677AMP
<0.194 mg/Kg - dry 0.194 0.771Anthracene 1 05/01/24 15:12 V46677AMP
0.280 J mg/Kg - dry 0.182 0.771Benzo(a)anthracene 1 05/01/24 15:12 V46677AMP
0.261 J mg/Kg - dry 0.192 0.771Benzo(a)pyrene 1 05/01/24 15:12 V46677AMP
0.333 J mg/Kg - dry 0.171 0.771Benzo(b)fluoranthene 1 05/01/24 15:12 V46677AMP
<0.168 mg/Kg - dry 0.168 0.771Benzo(g,h,i)perylene 1 05/01/24 15:12 V46677AMP
<0.182 mg/Kg - dry 0.182 0.771Benzo(k)fluoranthene 1 05/01/24 15:12 V46677AMP
<0.678 mg/Kg - dry 0.678 2.34Benzoic Acid 1 05/01/24 15:12 V46677AMP
<0.182 mg/Kg - dry 0.182 0.771Benzyl alcohol 1 05/01/24 15:12 V46677AMP
<0.161 mg/Kg - dry 0.161 0.771Bis(2-Chloroethoxy)methane 1 05/01/24 15:12 V46677AMP
<0.142 mg/Kg - dry 0.142 0.771Bis(2-Chloroethyl)ether 1 05/01/24 15:12 V46677AMP
<0.153 mg/Kg - dry 0.153 0.385Bis(2-Chloroisopropyl)ether 1 05/01/24 15:12 V46677AMP
<0.207 mg/Kg - dry 0.207 0.771Bis(2-ethylhexyl)phthalate 1 05/01/24 15:12 V46677AMP
<0.184 mg/Kg - dry 0.184 0.7714-Bromophenyl phenyl ether 1 05/01/24 15:12 V46677AMP
<0.187 mg/Kg - dry 0.187 0.385Butyl benzyl phthalate 1 05/01/24 15:12 V46677AMP
<0.174 mg/Kg - dry 0.174 0.7714-Chloro-3-methylphenol 1 05/01/24 15:12 V46677AMP
<0.175 mg/Kg - dry 0.175 0.3854-Chloroaniline 1 05/01/24 15:12 V46677AMP
<0.180 mg/Kg - dry 0.180 0.7712-Chloronaphthalene 1 05/01/24 15:12 V46677AMP
<0.166 mg/Kg - dry 0.166 0.7712-Chlorophenol 1 05/01/24 15:12 V46677AMP
<0.171 mg/Kg - dry 0.171 1.174-Chlorophenyl phenyl ether 1 05/01/24 15:12 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 19 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1
92181 Matrix:
4/26/2024 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
0.210 J mg/Kg - dry 0.170 0.771Chrysene 1 05/01/24 15:12 V46677AMP
<0.129 mg/Kg - dry 0.129 0.771Dibenz(a,h)anthracene 1 05/01/24 15:12 V46677AMP
<0.184 mg/Kg - dry 0.184 0.771Dibenzofuran 1 05/01/24 15:12 V46677AMP
<0.149 mg/Kg - dry 0.149 0.7711,2-Dichlorobenzene 1 05/01/24 15:12 V46677AMP
<0.146 mg/Kg - dry 0.146 0.7711,3-Dichlorobenzene 1 05/01/24 15:12 V46677AMP
<0.138 mg/Kg - dry 0.138 0.3851,4-Dichlorobenzene 1 05/01/24 15:12 V46677AMP
<0.175 mg/Kg - dry 0.175 0.7713,3'-Dichlorobenzidine 1 05/01/24 15:12 V46677AMP
<0.163 mg/Kg - dry 0.163 0.7712,4-Dichlorophenol 1 05/01/24 15:12 V46677AMP
<0.171 mg/Kg - dry 0.171 0.771Diethyl phthalate 1 05/01/24 15:12 V46677AMP
<0.183 mg/Kg - dry 0.183 0.771Dimethyl phthalate 1 05/01/24 15:12 V46677AMP
<0.247 mg/Kg - dry 0.247 0.7712,4-Dimethylphenol 1 05/01/24 15:12 V46677AMP
<0.200 mg/Kg - dry 0.200 0.771Di-n-butyl phthalate 1 05/01/24 15:12 V46677AMP
<0.280 mg/Kg - dry 0.280 1.754,6-Dinitro-2-methylphenol 1 05/01/24 15:12 V46677AMP
<0.608 mg/Kg - dry 0.608 1.752,4-Dinitrophenol 1 05/01/24 15:12 V46677AMP
<0.188 mg/Kg - dry 0.188 0.7712,4-Dinitrotoluene 1 05/01/24 15:12 V46677AMP
<0.194 mg/Kg - dry 0.194 0.7712,6-Dinitrotoluene 1 05/01/24 15:12 V46677AMP
<0.190 mg/Kg - dry 0.190 0.385Di-n-Octyl Phthalate 1 05/01/24 15:12 V46677AMP
0.401 J mg/Kg - dry 0.184 0.771Fluoranthene 1 05/01/24 15:12 V46677AMP
<0.178 mg/Kg - dry 0.178 0.771Fluorene 1 05/01/24 15:12 V46677AMP
<0.175 mg/Kg - dry 0.175 0.771Hexachlorobenzene 1 05/01/24 15:12 V46677AMP
<0.114 mg/Kg - dry 0.114 0.771Hexachlorobutadiene 1 05/01/24 15:12 V46677AMP
<0.116 mg/Kg - dry 0.116 0.771Hexachlorocyclopentadiene 1 05/01/24 15:12 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 20 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1
92181 Matrix:
4/26/2024 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.142 mg/Kg - dry 0.142 0.771Hexachloroethane 1 05/01/24 15:12 V46677AMP
0.201 J mg/Kg - dry 0.176 0.771Indeno(1,2,3-cd)pyrene 1 05/01/24 15:12 V46677AMP
<0.141 mg/Kg - dry 0.141 0.771Isophorone 1 05/01/24 15:12 V46677AMP
<0.162 mg/Kg - dry 0.162 0.7711-Methylnaphthalene 1 05/01/24 15:12 V46677AMP
<0.168 mg/Kg - dry 0.168 0.7712-Methylnaphthalene 1 05/01/24 15:12 V46677AMP
<0.148 mg/Kg - dry 0.148 0.7712-Methylphenol 1 05/01/24 15:12 V46677AMP
<0.149 mg/Kg - dry 0.149 0.7713&4 Methylphenol 1 05/01/24 15:12 V46677AMP
<0.155 mg/Kg - dry 0.155 0.771Naphthalene 1 05/01/24 15:12 V46677AMP
<0.154 mg/Kg - dry 0.154 0.7712-Nitroaniline 1 05/01/24 15:12 V46677AMP
<0.181 mg/Kg - dry 0.181 0.7713-Nitroaniline 1 05/01/24 15:12 V46677AMP
<0.159 mg/Kg - dry 0.159 0.3854-Nitroaniline 1 05/01/24 15:12 V46677AMP
<0.150 mg/Kg - dry 0.150 0.385Nitrobenzene 1 05/01/24 15:12 V46677AMP
<0.155 mg/Kg - dry 0.155 0.7712-Nitrophenol 1 05/01/24 15:12 V46677AMP
<0.195 mg/Kg - dry 0.195 0.7714-Nitrophenol 1 05/01/24 15:12 V46677AMP
<0.307 mg/Kg - dry 0.307 0.771N-Nitrosodimethylamine 1 05/01/24 15:12 V46677AMP
<0.212 mg/Kg - dry 0.212 0.771N-Nitrosodiphenylamine 1 05/01/24 15:12 V46677AMP
<0.173 mg/Kg - dry 0.173 0.771N-Nitroso-di-n-propylamine 1 05/01/24 15:12 V46677AMP
<0.405 mg/Kg - dry 0.405 1.17Pentachlorophenol 1 05/01/24 15:12 V46677AMP
0.231 J mg/Kg - dry 0.184 0.771Phenanthrene 1 05/01/24 15:12 V46677AMP
<0.166 mg/Kg - dry 0.166 0.771Phenol 1 05/01/24 15:12 V46677AMP
0.350 J mg/Kg - dry 0.187 0.771Pyrene 1 05/01/24 15:12 V46677AMP
<0.089 mg/Kg - dry 0.089 0.385Pyridine 1 05/01/24 15:12 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 21 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-1
92181 Matrix:
4/26/2024 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.154 mg/Kg - dry 0.154 0.7711,2,4-Trichlorobenzene 1 05/01/24 15:12 V46677AMP
<0.167 mg/Kg - dry 0.167 0.7712,4,5-Trichlorophenol 1 05/01/24 15:12 V46677AMP
<0.163 mg/Kg - dry 0.163 0.7712,4,6-Trichlorophenol 1 05/01/24 15:12 V46677AMP
8270ESurrogate: Phenol-d5 80.5 Limits: 34-121%05/01/24 15:121 AMP
Surrogate: 2-Fluorobiphenyl 71.9 Limits: 44-115%05/01/24 15:121 AMP V46677
Surrogate: 2-Fluorophenol 78.4 Limits: 35-115%05/01/24 15:121 AMP V46677
Surrogate: Nitrobenzene-d5 73.1 Limits: 37-122%05/01/24 15:121 AMP V46677
Surrogate: 4-Terphenyl-d14 74.3 Limits: 54-127%05/01/24 15:121 AMP V46677
Surrogate: 2,4,6-Tribromophenol 66.5 Limits: 39-132%05/01/24 15:121 AMP V46677
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 22 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2E (1-2)
92182 Matrix:
4/26/2024 12:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.5 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 23 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2E (1-2)
92182 Matrix:
4/26/2024 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
0.016 J mg/Kg - dry 0.002 0.022Acetone 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 04/29/24 16:59 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 04/29/24 16:59 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 04/29/24 16:59 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 04/29/24 16:59 V46655TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 04/29/24 16:59 V46655TBL
0.0007 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 04/29/24 16:59 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 04/29/24 16:59 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 04/29/24 16:59 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 04/29/24 16:59 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 04/29/24 16:59 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 24 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2E (1-2)
92182 Matrix:
4/26/2024 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 04/29/24 16:59 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 04/29/24 16:59 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 04/29/24 16:59 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 04/29/24 16:59 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 04/29/24 16:59 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 04/29/24 16:59 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 04/29/24 16:59 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 04/29/24 16:59 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 04/29/24 16:59 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 04/29/24 16:59 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 04/29/24 16:59 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 04/29/24 16:59 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.057Ethyl Tertiary Butyl Ether (ETBE)1 04/29/24 16:59 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 04/29/24 16:59 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 04/29/24 16:59 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2E (1-2)
92182 Matrix:
4/26/2024 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 04/29/24 16:59 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 04/29/24 16:59 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 04/29/24 16:59 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 04/29/24 16:59 V46655TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 04/29/24 16:59 V46655TBL
0.003 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 04/29/24 16:59 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 04/29/24 16:59 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 04/29/24 16:59 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 04/29/24 16:59 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 04/29/24 16:59 V46655TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 04/29/24 16:59 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 04/29/24 16:59 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 26 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2E (1-2)
92182 Matrix:
4/26/2024 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 04/29/24 16:59 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 04/29/24 16:59 V46655TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 04/29/24 16:59 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 04/29/24 16:59 V46655
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/29/24 16:591 TBL V46655
Surrogate: Dibromofluoromethane 106 Limits: 84-123%04/29/24 16:591 TBL V46655
Surrogate: Toluene-d8 100 Limits: 76-129%04/29/24 16:591 TBL V46655
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 27 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2
92183 Matrix:
4/26/2024 12:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.9 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
0.414 B mg/Kg - dry 0.160 0.227Chromium, Hexavalent 1 05/02/24 18:53 SW-7199MKD
1200 µg/Kg - dry 97.0 284Arsenic 5 05/04/24 14:10 6020BCPW
74700 µg/Kg - dry 48.6 284Barium 5 05/04/24 14:10 6020BCPW
67.0 J µg/Kg - dry 29.5 284Cadmium 5 05/04/24 14:10 6020BCPW
35200 µg/Kg - dry 132 284Chromium 5 05/04/24 14:10 6020BCPW
9880 µg/Kg - dry 35.2 284Lead 5 05/04/24 14:10 6020BCPW
0.0170 J mg/Kg - dry 0.0136 0.0341Mercury (Total)1 05/03/24 12:43 7471BJKC
300 µg/Kg - dry 117 284Selenium 5 05/04/24 14:10 6020BCPW
107 J µg/Kg - dry 7.65 284Silver 5 05/04/24 14:10 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 28 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2
92183 Matrix:
4/26/2024 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.166 mg/Kg - dry 0.166 0.750Acenaphthene 1 05/01/24 14:48 V46677AMP
<0.170 mg/Kg - dry 0.170 0.750Acenaphthylene 1 05/01/24 14:48 V46677AMP
<0.238 mg/Kg - dry 0.238 0.750Aniline 1 05/01/24 14:48 V46677AMP
<0.188 mg/Kg - dry 0.188 0.750Anthracene 1 05/01/24 14:48 V46677AMP
<0.177 mg/Kg - dry 0.177 0.750Benzo(a)anthracene 1 05/01/24 14:48 V46677AMP
<0.187 mg/Kg - dry 0.187 0.750Benzo(a)pyrene 1 05/01/24 14:48 V46677AMP
<0.166 mg/Kg - dry 0.166 0.750Benzo(b)fluoranthene 1 05/01/24 14:48 V46677AMP
<0.163 mg/Kg - dry 0.163 0.750Benzo(g,h,i)perylene 1 05/01/24 14:48 V46677AMP
<0.177 mg/Kg - dry 0.177 0.750Benzo(k)fluoranthene 1 05/01/24 14:48 V46677AMP
<0.658 mg/Kg - dry 0.658 2.27Benzoic Acid 1 05/01/24 14:48 V46677AMP
<0.177 mg/Kg - dry 0.177 0.750Benzyl alcohol 1 05/01/24 14:48 V46677AMP
<0.156 mg/Kg - dry 0.156 0.750Bis(2-Chloroethoxy)methane 1 05/01/24 14:48 V46677AMP
<0.138 mg/Kg - dry 0.138 0.750Bis(2-Chloroethyl)ether 1 05/01/24 14:48 V46677AMP
<0.148 mg/Kg - dry 0.148 0.374Bis(2-Chloroisopropyl)ether 1 05/01/24 14:48 V46677AMP
<0.200 mg/Kg - dry 0.200 0.750Bis(2-ethylhexyl)phthalate 1 05/01/24 14:48 V46677AMP
<0.179 mg/Kg - dry 0.179 0.7504-Bromophenyl phenyl ether 1 05/01/24 14:48 V46677AMP
<0.181 mg/Kg - dry 0.181 0.374Butyl benzyl phthalate 1 05/01/24 14:48 V46677AMP
<0.169 mg/Kg - dry 0.169 0.7504-Chloro-3-methylphenol 1 05/01/24 14:48 V46677AMP
<0.170 mg/Kg - dry 0.170 0.3744-Chloroaniline 1 05/01/24 14:48 V46677AMP
<0.174 mg/Kg - dry 0.174 0.7502-Chloronaphthalene 1 05/01/24 14:48 V46677AMP
<0.161 mg/Kg - dry 0.161 0.7502-Chlorophenol 1 05/01/24 14:48 V46677AMP
<0.166 mg/Kg - dry 0.166 1.144-Chlorophenyl phenyl ether 1 05/01/24 14:48 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 29 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2
92183 Matrix:
4/26/2024 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.165 mg/Kg - dry 0.165 0.750Chrysene 1 05/01/24 14:48 V46677AMP
<0.125 mg/Kg - dry 0.125 0.750Dibenz(a,h)anthracene 1 05/01/24 14:48 V46677AMP
<0.179 mg/Kg - dry 0.179 0.750Dibenzofuran 1 05/01/24 14:48 V46677AMP
<0.145 mg/Kg - dry 0.145 0.7501,2-Dichlorobenzene 1 05/01/24 14:48 V46677AMP
<0.141 mg/Kg - dry 0.141 0.7501,3-Dichlorobenzene 1 05/01/24 14:48 V46677AMP
<0.133 mg/Kg - dry 0.133 0.3741,4-Dichlorobenzene 1 05/01/24 14:48 V46677AMP
<0.170 mg/Kg - dry 0.170 0.7503,3'-Dichlorobenzidine 1 05/01/24 14:48 V46677AMP
<0.158 mg/Kg - dry 0.158 0.7502,4-Dichlorophenol 1 05/01/24 14:48 V46677AMP
<0.166 mg/Kg - dry 0.166 0.750Diethyl phthalate 1 05/01/24 14:48 V46677AMP
<0.178 mg/Kg - dry 0.178 0.750Dimethyl phthalate 1 05/01/24 14:48 V46677AMP
<0.240 mg/Kg - dry 0.240 0.7502,4-Dimethylphenol 1 05/01/24 14:48 V46677AMP
<0.194 mg/Kg - dry 0.194 0.750Di-n-butyl phthalate 1 05/01/24 14:48 V46677AMP
<0.272 mg/Kg - dry 0.272 1.704,6-Dinitro-2-methylphenol 1 05/01/24 14:48 V46677AMP
<0.590 mg/Kg - dry 0.590 1.702,4-Dinitrophenol 1 05/01/24 14:48 V46677AMP
<0.182 mg/Kg - dry 0.182 0.7502,4-Dinitrotoluene 1 05/01/24 14:48 V46677AMP
<0.188 mg/Kg - dry 0.188 0.7502,6-Dinitrotoluene 1 05/01/24 14:48 V46677AMP
<0.185 mg/Kg - dry 0.185 0.374Di-n-Octyl Phthalate 1 05/01/24 14:48 V46677AMP
0.203 J mg/Kg - dry 0.179 0.750Fluoranthene 1 05/01/24 14:48 V46677AMP
<0.173 mg/Kg - dry 0.173 0.750Fluorene 1 05/01/24 14:48 V46677AMP
<0.170 mg/Kg - dry 0.170 0.750Hexachlorobenzene 1 05/01/24 14:48 V46677AMP
<0.110 mg/Kg - dry 0.110 0.750Hexachlorobutadiene 1 05/01/24 14:48 V46677AMP
<0.113 mg/Kg - dry 0.113 0.750Hexachlorocyclopentadiene 1 05/01/24 14:48 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 30 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2
92183 Matrix:
4/26/2024 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.138 mg/Kg - dry 0.138 0.750Hexachloroethane 1 05/01/24 14:48 V46677AMP
<0.171 mg/Kg - dry 0.171 0.750Indeno(1,2,3-cd)pyrene 1 05/01/24 14:48 V46677AMP
<0.137 mg/Kg - dry 0.137 0.750Isophorone 1 05/01/24 14:48 V46677AMP
<0.157 mg/Kg - dry 0.157 0.7501-Methylnaphthalene 1 05/01/24 14:48 V46677AMP
<0.163 mg/Kg - dry 0.163 0.7502-Methylnaphthalene 1 05/01/24 14:48 V46677AMP
<0.144 mg/Kg - dry 0.144 0.7502-Methylphenol 1 05/01/24 14:48 V46677AMP
<0.145 mg/Kg - dry 0.145 0.7503&4 Methylphenol 1 05/01/24 14:48 V46677AMP
<0.150 mg/Kg - dry 0.150 0.750Naphthalene 1 05/01/24 14:48 V46677AMP
<0.149 mg/Kg - dry 0.149 0.7502-Nitroaniline 1 05/01/24 14:48 V46677AMP
<0.175 mg/Kg - dry 0.175 0.7503-Nitroaniline 1 05/01/24 14:48 V46677AMP
<0.154 mg/Kg - dry 0.154 0.3744-Nitroaniline 1 05/01/24 14:48 V46677AMP
<0.146 mg/Kg - dry 0.146 0.374Nitrobenzene 1 05/01/24 14:48 V46677AMP
<0.150 mg/Kg - dry 0.150 0.7502-Nitrophenol 1 05/01/24 14:48 V46677AMP
<0.189 mg/Kg - dry 0.189 0.7504-Nitrophenol 1 05/01/24 14:48 V46677AMP
<0.298 mg/Kg - dry 0.298 0.750N-Nitrosodimethylamine 1 05/01/24 14:48 V46677AMP
<0.206 mg/Kg - dry 0.206 0.750N-Nitrosodiphenylamine 1 05/01/24 14:48 V46677AMP
<0.167 mg/Kg - dry 0.167 0.750N-Nitroso-di-n-propylamine 1 05/01/24 14:48 V46677AMP
<0.393 mg/Kg - dry 0.393 1.14Pentachlorophenol 1 05/01/24 14:48 V46677AMP
<0.179 mg/Kg - dry 0.179 0.750Phenanthrene 1 05/01/24 14:48 V46677AMP
<0.161 mg/Kg - dry 0.161 0.750Phenol 1 05/01/24 14:48 V46677AMP
<0.181 mg/Kg - dry 0.181 0.750Pyrene 1 05/01/24 14:48 V46677AMP
<0.087 mg/Kg - dry 0.087 0.374Pyridine 1 05/01/24 14:48 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 31 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-2
92183 Matrix:
4/26/2024 12:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.149 mg/Kg - dry 0.149 0.7501,2,4-Trichlorobenzene 1 05/01/24 14:48 V46677AMP
<0.162 mg/Kg - dry 0.162 0.7502,4,5-Trichlorophenol 1 05/01/24 14:48 V46677AMP
<0.158 mg/Kg - dry 0.158 0.7502,4,6-Trichlorophenol 1 05/01/24 14:48 V46677AMP
8270ESurrogate: Phenol-d5 88.0 Limits: 34-121%05/01/24 14:481 AMP
Surrogate: 2-Fluorobiphenyl 77.2 Limits: 44-115%05/01/24 14:481 AMP V46677
Surrogate: 2-Fluorophenol 84.4 Limits: 35-115%05/01/24 14:481 AMP V46677
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%05/01/24 14:481 AMP V46677
Surrogate: 4-Terphenyl-d14 76.0 Limits: 54-127%05/01/24 14:481 AMP V46677
Surrogate: 2,4,6-Tribromophenol 68.0 Limits: 39-132%05/01/24 14:481 AMP V46677
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 32 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3A (1-2)
92184 Matrix:
4/26/2024 12:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.0 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 33 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3A (1-2)
92184 Matrix:
4/26/2024 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46717 04/30/24 08:00
0.027 mg/Kg - dry 0.002 0.023Acetone 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 04/30/24 14:02 V46718TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 04/30/24 14:02 V46718TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 04/30/24 14:02 V46718TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 04/30/24 14:02 V46718TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 04/30/24 14:02 V46718TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 04/30/24 14:02 V46718TBL
0.001 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 04/30/24 14:02 V46718TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 04/30/24 14:02 V46718TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 04/30/24 14:02 V46718TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 04/30/24 14:02 V46718TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 04/30/24 14:02 V46718TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 34 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3A (1-2)
92184 Matrix:
4/26/2024 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46717 04/30/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 04/30/24 14:02 V46718TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 04/30/24 14:02 V46718TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 04/30/24 14:02 V46718TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 04/30/24 14:02 V46718TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 04/30/24 14:02 V46718TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 04/30/24 14:02 V46718TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 04/30/24 14:02 V46718TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 04/30/24 14:02 V46718TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 04/30/24 14:02 V46718TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 04/30/24 14:02 V46718TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 04/30/24 14:02 V46718TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 04/30/24 14:02 V46718TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 04/30/24 14:02 V46718TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 04/30/24 14:02 V46718TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 04/30/24 14:02 V46718TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 04/30/24 14:02 V46718TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 35 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3A (1-2)
92184 Matrix:
4/26/2024 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46717 04/30/24 08:00
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 04/30/24 14:02 V46718TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 04/30/24 14:02 V46718TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 04/30/24 14:02 V46718TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 04/30/24 14:02 V46718TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 04/30/24 14:02 V46718TBL
0.003 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 04/30/24 14:02 V46718TBL
0.055 mg/Kg - dry 0.001 0.011Naphthalene 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 04/30/24 14:02 V46718TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 04/30/24 14:02 V46718TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 04/30/24 14:02 V46718TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 04/30/24 14:02 V46718TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 04/30/24 14:02 V46718TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 04/30/24 14:02 V46718TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 04/30/24 14:02 V46718TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 36 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3A (1-2)
92184 Matrix:
4/26/2024 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46717 04/30/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 04/30/24 14:02 V46718TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 04/30/24 14:02 V46718TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 04/30/24 14:02 V46718
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%04/30/24 14:021 TBL V46718
Surrogate: Dibromofluoromethane 106 Limits: 84-123%04/30/24 14:021 TBL V46718
Surrogate: Toluene-d8 99.4 Limits: 76-129%04/30/24 14:021 TBL V46718
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 37 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3
92185 Matrix:
4/26/2024 12:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.3 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
0.327 B mg/Kg - dry 0.164 0.233Chromium, Hexavalent 1 05/02/24 19:04 SW-7199MKD
1330 µg/Kg - dry 99.8 292Arsenic 5 05/04/24 14:15 6020BCPW
77600 µg/Kg - dry 49.9 292Barium 5 05/04/24 14:15 6020BCPW
62.8 J µg/Kg - dry 30.3 292Cadmium 5 05/04/24 14:15 6020BCPW
44800 µg/Kg - dry 135 292Chromium 5 05/04/24 14:15 6020BCPW
8630 µg/Kg - dry 36.2 292Lead 5 05/04/24 14:15 6020BCPW
0.0219 J mg/Kg - dry 0.0140 0.0350Mercury (Total)1 05/03/24 12:45 7471BJKC
279 J µg/Kg - dry 120 292Selenium 5 05/04/24 14:15 6020BCPW
77.2 J µg/Kg - dry 7.86 292Silver 5 05/04/24 14:15 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 38 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3
92185 Matrix:
4/26/2024 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.171 mg/Kg - dry 0.171 0.770Acenaphthene 1 05/01/24 16:02 V46677AMP
<0.175 mg/Kg - dry 0.175 0.770Acenaphthylene 1 05/01/24 16:02 V46677AMP
<0.245 mg/Kg - dry 0.245 0.770Aniline 1 05/01/24 16:02 V46677AMP
<0.193 mg/Kg - dry 0.193 0.770Anthracene 1 05/01/24 16:02 V46677AMP
0.437 J mg/Kg - dry 0.182 0.770Benzo(a)anthracene 1 05/01/24 16:02 V46677AMP
0.365 J mg/Kg - dry 0.192 0.770Benzo(a)pyrene 1 05/01/24 16:02 V46677AMP
0.518 J mg/Kg - dry 0.171 0.770Benzo(b)fluoranthene 1 05/01/24 16:02 V46677AMP
0.221 J mg/Kg - dry 0.168 0.770Benzo(g,h,i)perylene 1 05/01/24 16:02 V46677AMP
<0.182 mg/Kg - dry 0.182 0.770Benzo(k)fluoranthene 1 05/01/24 16:02 V46677AMP
<0.676 mg/Kg - dry 0.676 2.33Benzoic Acid 1 05/01/24 16:02 V46677AMP
<0.182 mg/Kg - dry 0.182 0.770Benzyl alcohol 1 05/01/24 16:02 V46677AMP
<0.161 mg/Kg - dry 0.161 0.770Bis(2-Chloroethoxy)methane 1 05/01/24 16:02 V46677AMP
<0.142 mg/Kg - dry 0.142 0.770Bis(2-Chloroethyl)ether 1 05/01/24 16:02 V46677AMP
<0.152 mg/Kg - dry 0.152 0.385Bis(2-Chloroisopropyl)ether 1 05/01/24 16:02 V46677AMP
<0.206 mg/Kg - dry 0.206 0.770Bis(2-ethylhexyl)phthalate 1 05/01/24 16:02 V46677AMP
<0.184 mg/Kg - dry 0.184 0.7704-Bromophenyl phenyl ether 1 05/01/24 16:02 V46677AMP
<0.186 mg/Kg - dry 0.186 0.385Butyl benzyl phthalate 1 05/01/24 16:02 V46677AMP
<0.173 mg/Kg - dry 0.173 0.7704-Chloro-3-methylphenol 1 05/01/24 16:02 V46677AMP
<0.175 mg/Kg - dry 0.175 0.3854-Chloroaniline 1 05/01/24 16:02 V46677AMP
<0.179 mg/Kg - dry 0.179 0.7702-Chloronaphthalene 1 05/01/24 16:02 V46677AMP
<0.165 mg/Kg - dry 0.165 0.7702-Chlorophenol 1 05/01/24 16:02 V46677AMP
<0.171 mg/Kg - dry 0.171 1.174-Chlorophenyl phenyl ether 1 05/01/24 16:02 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 39 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3
92185 Matrix:
4/26/2024 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
0.331 J mg/Kg - dry 0.170 0.770Chrysene 1 05/01/24 16:02 V46677AMP
<0.129 mg/Kg - dry 0.129 0.770Dibenz(a,h)anthracene 1 05/01/24 16:02 V46677AMP
<0.184 mg/Kg - dry 0.184 0.770Dibenzofuran 1 05/01/24 16:02 V46677AMP
<0.149 mg/Kg - dry 0.149 0.7701,2-Dichlorobenzene 1 05/01/24 16:02 V46677AMP
<0.145 mg/Kg - dry 0.145 0.7701,3-Dichlorobenzene 1 05/01/24 16:02 V46677AMP
<0.137 mg/Kg - dry 0.137 0.3851,4-Dichlorobenzene 1 05/01/24 16:02 V46677AMP
<0.175 mg/Kg - dry 0.175 0.7703,3'-Dichlorobenzidine 1 05/01/24 16:02 V46677AMP
<0.163 mg/Kg - dry 0.163 0.7702,4-Dichlorophenol 1 05/01/24 16:02 V46677AMP
<0.171 mg/Kg - dry 0.171 0.770Diethyl phthalate 1 05/01/24 16:02 V46677AMP
<0.183 mg/Kg - dry 0.183 0.770Dimethyl phthalate 1 05/01/24 16:02 V46677AMP
<0.247 mg/Kg - dry 0.247 0.7702,4-Dimethylphenol 1 05/01/24 16:02 V46677AMP
<0.199 mg/Kg - dry 0.199 0.770Di-n-butyl phthalate 1 05/01/24 16:02 V46677AMP
<0.280 mg/Kg - dry 0.280 1.754,6-Dinitro-2-methylphenol 1 05/01/24 16:02 V46677AMP
<0.606 mg/Kg - dry 0.606 1.752,4-Dinitrophenol 1 05/01/24 16:02 V46677AMP
<0.187 mg/Kg - dry 0.187 0.7702,4-Dinitrotoluene 1 05/01/24 16:02 V46677AMP
<0.193 mg/Kg - dry 0.193 0.7702,6-Dinitrotoluene 1 05/01/24 16:02 V46677AMP
<0.190 mg/Kg - dry 0.190 0.385Di-n-Octyl Phthalate 1 05/01/24 16:02 V46677AMP
0.932 mg/Kg - dry 0.184 0.770Fluoranthene 1 05/01/24 16:02 V46677AMP
<0.178 mg/Kg - dry 0.178 0.770Fluorene 1 05/01/24 16:02 V46677AMP
<0.175 mg/Kg - dry 0.175 0.770Hexachlorobenzene 1 05/01/24 16:02 V46677AMP
<0.113 mg/Kg - dry 0.113 0.770Hexachlorobutadiene 1 05/01/24 16:02 V46677AMP
<0.116 mg/Kg - dry 0.116 0.770Hexachlorocyclopentadiene 1 05/01/24 16:02 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 40 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3
92185 Matrix:
4/26/2024 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.142 mg/Kg - dry 0.142 0.770Hexachloroethane 1 05/01/24 16:02 V46677AMP
0.318 J mg/Kg - dry 0.176 0.770Indeno(1,2,3-cd)pyrene 1 05/01/24 16:02 V46677AMP
<0.141 mg/Kg - dry 0.141 0.770Isophorone 1 05/01/24 16:02 V46677AMP
<0.162 mg/Kg - dry 0.162 0.7701-Methylnaphthalene 1 05/01/24 16:02 V46677AMP
<0.168 mg/Kg - dry 0.168 0.7702-Methylnaphthalene 1 05/01/24 16:02 V46677AMP
<0.148 mg/Kg - dry 0.148 0.7702-Methylphenol 1 05/01/24 16:02 V46677AMP
<0.149 mg/Kg - dry 0.149 0.7703&4 Methylphenol 1 05/01/24 16:02 V46677AMP
<0.155 mg/Kg - dry 0.155 0.770Naphthalene 1 05/01/24 16:02 V46677AMP
<0.154 mg/Kg - dry 0.154 0.7702-Nitroaniline 1 05/01/24 16:02 V46677AMP
<0.180 mg/Kg - dry 0.180 0.7703-Nitroaniline 1 05/01/24 16:02 V46677AMP
<0.158 mg/Kg - dry 0.158 0.3854-Nitroaniline 1 05/01/24 16:02 V46677AMP
<0.150 mg/Kg - dry 0.150 0.385Nitrobenzene 1 05/01/24 16:02 V46677AMP
<0.155 mg/Kg - dry 0.155 0.7702-Nitrophenol 1 05/01/24 16:02 V46677AMP
<0.194 mg/Kg - dry 0.194 0.7704-Nitrophenol 1 05/01/24 16:02 V46677AMP
<0.306 mg/Kg - dry 0.306 0.770N-Nitrosodimethylamine 1 05/01/24 16:02 V46677AMP
<0.212 mg/Kg - dry 0.212 0.770N-Nitrosodiphenylamine 1 05/01/24 16:02 V46677AMP
<0.172 mg/Kg - dry 0.172 0.770N-Nitroso-di-n-propylamine 1 05/01/24 16:02 V46677AMP
<0.404 mg/Kg - dry 0.404 1.17Pentachlorophenol 1 05/01/24 16:02 V46677AMP
0.683 J mg/Kg - dry 0.184 0.770Phenanthrene 1 05/01/24 16:02 V46677AMP
<0.165 mg/Kg - dry 0.165 0.770Phenol 1 05/01/24 16:02 V46677AMP
0.602 J mg/Kg - dry 0.186 0.770Pyrene 1 05/01/24 16:02 V46677AMP
<0.089 mg/Kg - dry 0.089 0.385Pyridine 1 05/01/24 16:02 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 41 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-3
92185 Matrix:
4/26/2024 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.154 mg/Kg - dry 0.154 0.7701,2,4-Trichlorobenzene 1 05/01/24 16:02 V46677AMP
<0.166 mg/Kg - dry 0.166 0.7702,4,5-Trichlorophenol 1 05/01/24 16:02 V46677AMP
<0.163 mg/Kg - dry 0.163 0.7702,4,6-Trichlorophenol 1 05/01/24 16:02 V46677AMP
8270ESurrogate: Phenol-d5 80.8 Limits: 34-121%05/01/24 16:021 AMP
Surrogate: 2-Fluorobiphenyl 73.7 Limits: 44-115%05/01/24 16:021 AMP V46677
Surrogate: 2-Fluorophenol 77.8 Limits: 35-115%05/01/24 16:021 AMP V46677
Surrogate: Nitrobenzene-d5 76.0 Limits: 37-122%05/01/24 16:021 AMP V46677
Surrogate: 4-Terphenyl-d14 77.2 Limits: 54-127%05/01/24 16:021 AMP V46677
Surrogate: 2,4,6-Tribromophenol 68.2 Limits: 39-132%05/01/24 16:021 AMP V46677
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 42 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1 (1-2)
92186 Matrix:
4/26/2024 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.9 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 43 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1 (1-2)
92186 Matrix:
4/26/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
0.021 J mg/Kg - dry 0.002 0.023Acetone 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 04/29/24 17:54 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 04/29/24 17:54 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 04/29/24 17:54 V46655TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 04/29/24 17:54 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 04/29/24 17:54 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 04/29/24 17:54 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 04/29/24 17:54 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 44 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1 (1-2)
92186 Matrix:
4/26/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 04/29/24 17:54 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 04/29/24 17:54 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 04/29/24 17:54 V46655TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 04/29/24 17:54 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 04/29/24 17:54 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 04/29/24 17:54 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 04/29/24 17:54 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 04/29/24 17:54 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 04/29/24 17:54 V46655TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 04/29/24 17:54 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 04/29/24 17:54 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 04/29/24 17:54 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 45 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1 (1-2)
92186 Matrix:
4/26/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 04/29/24 17:54 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 04/29/24 17:54 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 04/29/24 17:54 V46655TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 04/29/24 17:54 V46655TBL
0.003 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 04/29/24 17:54 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 04/29/24 17:54 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 04/29/24 17:54 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 04/29/24 17:54 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 04/29/24 17:54 V46655TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 04/29/24 17:54 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 04/29/24 17:54 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 46 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1 (1-2)
92186 Matrix:
4/26/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 04/29/24 17:54 V46655TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 04/29/24 17:54 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 04/29/24 17:54 V46655
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%04/29/24 17:541 TBL V46655
Surrogate: Dibromofluoromethane 105 Limits: 84-123%04/29/24 17:541 TBL V46655
Surrogate: Toluene-d8 96.8 Limits: 76-129%04/29/24 17:541 TBL V46655
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 47 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1
92187 Matrix:
4/26/2024 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.9 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
0.470 B mg/Kg - dry 0.163 0.232Chromium, Hexavalent 1 05/02/24 19:15 SW-7199MKD
1220 µg/Kg - dry 99.3 290Arsenic 5 05/04/24 14:21 6020BCPW
74800 µg/Kg - dry 49.7 290Barium 5 05/04/24 14:21 6020BCPW
49.4 J µg/Kg - dry 30.2 290Cadmium 5 05/04/24 14:21 6020BCPW
44400 µg/Kg - dry 135 290Chromium 5 05/04/24 14:21 6020BCPW
6790 µg/Kg - dry 36.0 290Lead 5 05/04/24 14:21 6020BCPW
0.0141 J mg/Kg - dry 0.0139 0.0348Mercury (Total)1 05/03/24 12:48 7471BJKC
209 J µg/Kg - dry 120 290Selenium 5 05/04/24 14:21 6020BCPW
71.9 J µg/Kg - dry 7.83 290Silver 5 05/04/24 14:21 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 48 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1
92187 Matrix:
4/26/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.170 mg/Kg - dry 0.170 0.766Acenaphthene 1 05/01/24 15:37 V46677AMP
<0.174 mg/Kg - dry 0.174 0.766Acenaphthylene 1 05/01/24 15:37 V46677AMP
<0.243 mg/Kg - dry 0.243 0.766Aniline 1 05/01/24 15:37 V46677AMP
<0.192 mg/Kg - dry 0.192 0.766Anthracene 1 05/01/24 15:37 V46677AMP
<0.181 mg/Kg - dry 0.181 0.766Benzo(a)anthracene 1 05/01/24 15:37 V46677AMP
<0.191 mg/Kg - dry 0.191 0.766Benzo(a)pyrene 1 05/01/24 15:37 V46677AMP
<0.170 mg/Kg - dry 0.170 0.766Benzo(b)fluoranthene 1 05/01/24 15:37 V46677AMP
<0.167 mg/Kg - dry 0.167 0.766Benzo(g,h,i)perylene 1 05/01/24 15:37 V46677AMP
<0.181 mg/Kg - dry 0.181 0.766Benzo(k)fluoranthene 1 05/01/24 15:37 V46677AMP
<0.673 mg/Kg - dry 0.673 2.32Benzoic Acid 1 05/01/24 15:37 V46677AMP
<0.181 mg/Kg - dry 0.181 0.766Benzyl alcohol 1 05/01/24 15:37 V46677AMP
<0.160 mg/Kg - dry 0.160 0.766Bis(2-Chloroethoxy)methane 1 05/01/24 15:37 V46677AMP
<0.141 mg/Kg - dry 0.141 0.766Bis(2-Chloroethyl)ether 1 05/01/24 15:37 V46677AMP
<0.152 mg/Kg - dry 0.152 0.383Bis(2-Chloroisopropyl)ether 1 05/01/24 15:37 V46677AMP
0.265 J mg/Kg - dry 0.205 0.766Bis(2-ethylhexyl)phthalate 1 05/01/24 15:37 V46677AMP
<0.183 mg/Kg - dry 0.183 0.7664-Bromophenyl phenyl ether 1 05/01/24 15:37 V46677AMP
<0.185 mg/Kg - dry 0.185 0.383Butyl benzyl phthalate 1 05/01/24 15:37 V46677AMP
<0.173 mg/Kg - dry 0.173 0.7664-Chloro-3-methylphenol 1 05/01/24 15:37 V46677AMP
<0.174 mg/Kg - dry 0.174 0.3834-Chloroaniline 1 05/01/24 15:37 V46677AMP
<0.178 mg/Kg - dry 0.178 0.7662-Chloronaphthalene 1 05/01/24 15:37 V46677AMP
<0.164 mg/Kg - dry 0.164 0.7662-Chlorophenol 1 05/01/24 15:37 V46677AMP
<0.170 mg/Kg - dry 0.170 1.164-Chlorophenyl phenyl ether 1 05/01/24 15:37 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 49 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1
92187 Matrix:
4/26/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.169 mg/Kg - dry 0.169 0.766Chrysene 1 05/01/24 15:37 V46677AMP
<0.128 mg/Kg - dry 0.128 0.766Dibenz(a,h)anthracene 1 05/01/24 15:37 V46677AMP
<0.183 mg/Kg - dry 0.183 0.766Dibenzofuran 1 05/01/24 15:37 V46677AMP
<0.148 mg/Kg - dry 0.148 0.7661,2-Dichlorobenzene 1 05/01/24 15:37 V46677AMP
<0.145 mg/Kg - dry 0.145 0.7661,3-Dichlorobenzene 1 05/01/24 15:37 V46677AMP
<0.137 mg/Kg - dry 0.137 0.3831,4-Dichlorobenzene 1 05/01/24 15:37 V46677AMP
<0.174 mg/Kg - dry 0.174 0.7663,3'-Dichlorobenzidine 1 05/01/24 15:37 V46677AMP
<0.162 mg/Kg - dry 0.162 0.7662,4-Dichlorophenol 1 05/01/24 15:37 V46677AMP
<0.170 mg/Kg - dry 0.170 0.766Diethyl phthalate 1 05/01/24 15:37 V46677AMP
<0.182 mg/Kg - dry 0.182 0.766Dimethyl phthalate 1 05/01/24 15:37 V46677AMP
<0.246 mg/Kg - dry 0.246 0.7662,4-Dimethylphenol 1 05/01/24 15:37 V46677AMP
<0.198 mg/Kg - dry 0.198 0.766Di-n-butyl phthalate 1 05/01/24 15:37 V46677AMP
<0.278 mg/Kg - dry 0.278 1.744,6-Dinitro-2-methylphenol 1 05/01/24 15:37 V46677AMP
<0.603 mg/Kg - dry 0.603 1.742,4-Dinitrophenol 1 05/01/24 15:37 V46677AMP
<0.186 mg/Kg - dry 0.186 0.7662,4-Dinitrotoluene 1 05/01/24 15:37 V46677AMP
<0.192 mg/Kg - dry 0.192 0.7662,6-Dinitrotoluene 1 05/01/24 15:37 V46677AMP
<0.189 mg/Kg - dry 0.189 0.383Di-n-Octyl Phthalate 1 05/01/24 15:37 V46677AMP
0.210 J mg/Kg - dry 0.183 0.766Fluoranthene 1 05/01/24 15:37 V46677AMP
<0.177 mg/Kg - dry 0.177 0.766Fluorene 1 05/01/24 15:37 V46677AMP
<0.174 mg/Kg - dry 0.174 0.766Hexachlorobenzene 1 05/01/24 15:37 V46677AMP
<0.113 mg/Kg - dry 0.113 0.766Hexachlorobutadiene 1 05/01/24 15:37 V46677AMP
<0.116 mg/Kg - dry 0.116 0.766Hexachlorocyclopentadiene 1 05/01/24 15:37 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 50 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1
92187 Matrix:
4/26/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.141 mg/Kg - dry 0.141 0.766Hexachloroethane 1 05/01/24 15:37 V46677AMP
<0.175 mg/Kg - dry 0.175 0.766Indeno(1,2,3-cd)pyrene 1 05/01/24 15:37 V46677AMP
<0.140 mg/Kg - dry 0.140 0.766Isophorone 1 05/01/24 15:37 V46677AMP
<0.161 mg/Kg - dry 0.161 0.7661-Methylnaphthalene 1 05/01/24 15:37 V46677AMP
<0.167 mg/Kg - dry 0.167 0.7662-Methylnaphthalene 1 05/01/24 15:37 V46677AMP
<0.147 mg/Kg - dry 0.147 0.7662-Methylphenol 1 05/01/24 15:37 V46677AMP
<0.148 mg/Kg - dry 0.148 0.7663&4 Methylphenol 1 05/01/24 15:37 V46677AMP
<0.154 mg/Kg - dry 0.154 0.766Naphthalene 1 05/01/24 15:37 V46677AMP
<0.153 mg/Kg - dry 0.153 0.7662-Nitroaniline 1 05/01/24 15:37 V46677AMP
<0.180 mg/Kg - dry 0.180 0.7663-Nitroaniline 1 05/01/24 15:37 V46677AMP
<0.157 mg/Kg - dry 0.157 0.3834-Nitroaniline 1 05/01/24 15:37 V46677AMP
<0.149 mg/Kg - dry 0.149 0.383Nitrobenzene 1 05/01/24 15:37 V46677AMP
<0.154 mg/Kg - dry 0.154 0.7662-Nitrophenol 1 05/01/24 15:37 V46677AMP
<0.193 mg/Kg - dry 0.193 0.7664-Nitrophenol 1 05/01/24 15:37 V46677AMP
<0.305 mg/Kg - dry 0.305 0.766N-Nitrosodimethylamine 1 05/01/24 15:37 V46677AMP
<0.211 mg/Kg - dry 0.211 0.766N-Nitrosodiphenylamine 1 05/01/24 15:37 V46677AMP
<0.171 mg/Kg - dry 0.171 0.766N-Nitroso-di-n-propylamine 1 05/01/24 15:37 V46677AMP
<0.403 mg/Kg - dry 0.403 1.16Pentachlorophenol 1 05/01/24 15:37 V46677AMP
<0.183 mg/Kg - dry 0.183 0.766Phenanthrene 1 05/01/24 15:37 V46677AMP
<0.164 mg/Kg - dry 0.164 0.766Phenol 1 05/01/24 15:37 V46677AMP
<0.185 mg/Kg - dry 0.185 0.766Pyrene 1 05/01/24 15:37 V46677AMP
<0.089 mg/Kg - dry 0.089 0.383Pyridine 1 05/01/24 15:37 V46677AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 51 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-1
92187 Matrix:
4/26/2024 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46647 04/30/24 11:10
<0.153 mg/Kg - dry 0.153 0.7661,2,4-Trichlorobenzene 1 05/01/24 15:37 V46677AMP
<0.166 mg/Kg - dry 0.166 0.7662,4,5-Trichlorophenol 1 05/01/24 15:37 V46677AMP
<0.162 mg/Kg - dry 0.162 0.7662,4,6-Trichlorophenol 1 05/01/24 15:37 V46677AMP
8270ESurrogate: Phenol-d5 84.7 Limits: 34-121%05/01/24 15:371 AMP
Surrogate: 2-Fluorobiphenyl 79.6 Limits: 44-115%05/01/24 15:371 AMP V46677
Surrogate: 2-Fluorophenol 82.3 Limits: 35-115%05/01/24 15:371 AMP V46677
Surrogate: Nitrobenzene-d5 79.0 Limits: 37-122%05/01/24 15:371 AMP V46677
Surrogate: 4-Terphenyl-d14 77.8 Limits: 54-127%05/01/24 15:371 AMP V46677
Surrogate: 2,4,6-Tribromophenol 70.6 Limits: 39-132%05/01/24 15:371 AMP V46677
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 52 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4B (4-5)
92188 Matrix:
4/26/2024 13:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
27.3 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 53 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4B (4-5)
92188 Matrix:
4/26/2024 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
0.036 mg/Kg - dry 0.003 0.027Acetone 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 04/29/24 18:21 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/29/24 18:21 V46655TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 04/29/24 18:21 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 04/29/24 18:21 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 04/29/24 18:21 V46655TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 04/29/24 18:21 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/29/24 18:21 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 04/29/24 18:21 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 04/29/24 18:21 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 54 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4B (4-5)
92188 Matrix:
4/26/2024 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 04/29/24 18:21 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 04/29/24 18:21 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 04/29/24 18:21 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/29/24 18:21 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/29/24 18:21 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/29/24 18:21 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 04/29/24 18:21 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 04/29/24 18:21 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.068Ethyl Tertiary Butyl Ether (ETBE)1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/29/24 18:21 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 04/29/24 18:21 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 55 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4B (4-5)
92188 Matrix:
4/26/2024 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 04/29/24 18:21 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/29/24 18:21 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 04/29/24 18:21 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 04/29/24 18:21 V46655TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 04/29/24 18:21 V46655TBL
0.004 J mg/Kg - dry 0.002 0.013Methylene Chloride 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/29/24 18:21 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/29/24 18:21 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 04/29/24 18:21 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/29/24 18:21 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/29/24 18:21 V46655TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 04/29/24 18:21 V46655TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/29/24 18:21 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 56 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4B (4-5)
92188 Matrix:
4/26/2024 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 04/29/24 18:21 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/29/24 18:21 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/29/24 18:21 V46655
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%04/29/24 18:211 TBL V46655
Surrogate: Dibromofluoromethane 103 Limits: 84-123%04/29/24 18:211 TBL V46655
Surrogate: Toluene-d8 95.2 Limits: 76-129%04/29/24 18:211 TBL V46655
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 57 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:Trip Blank
92189 Matrix:
4/26/2024 7:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.80 µg/L 1.80 5.00Acetone 1 05/03/24 14:54 V46953MSA
<2.00 µg/L 2.00 5.00Acrolein 1 05/03/24 14:54 V46953MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 05/03/24 14:54 V46953MSA
<0.180 µg/L 0.180 0.500Benzene 1 05/03/24 14:54 V46953MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/03/24 14:54 V46953MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/03/24 14:54 V46953MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/03/24 14:54 V46953MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/03/24 14:54 V46953MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/03/24 14:54 V46953MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 05/03/24 14:54 V46953MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 05/03/24 14:54 V46953MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/03/24 14:54 V46953MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 05/03/24 14:54 V46953MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/03/24 14:54 V46953MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/03/24 14:54 V46953MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/03/24 14:54 V46953MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/03/24 14:54 V46953MSA
<0.220 µg/L 0.220 0.500Chloroform 1 05/03/24 14:54 V46953MSA
0.457 J µg/L 0.220 0.500Chloromethane 1 05/03/24 14:54 V46953MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/03/24 14:54 V46953MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/03/24 14:54 V46953MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 05/03/24 14:54 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 58 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:Trip Blank
92189 Matrix:
4/26/2024 7:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/03/24 14:54 V46953MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/03/24 14:54 V46953MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 05/03/24 14:54 V46953MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/03/24 14:54 V46953MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/03/24 14:54 V46953MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/03/24 14:54 V46953MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/03/24 14:54 V46953MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/03/24 14:54 V46953MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/03/24 14:54 V46953MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/03/24 14:54 V46953MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/03/24 14:54 V46953MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/03/24 14:54 V46953MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/03/24 14:54 V46953MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/03/24 14:54 V46953MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/03/24 14:54 V46953MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/03/24 14:54 V46953MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/03/24 14:54 V46953MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/03/24 14:54 V46953MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 05/03/24 14:54 V46953MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 05/03/24 14:54 V46953MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 05/03/24 14:54 V46953MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 05/03/24 14:54 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 59 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:Trip Blank
92189 Matrix:
4/26/2024 7:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<0.380 µg/L 0.380 5.002-Hexanone 1 05/03/24 14:54 V46953MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 05/03/24 14:54 V46953MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/03/24 14:54 V46953MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/03/24 14:54 V46953MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 05/03/24 14:54 V46953MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 05/03/24 14:54 V46953MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 05/03/24 14:54 V46953MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/03/24 14:54 V46953MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/03/24 14:54 V46953MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/03/24 14:54 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/03/24 14:54 V46953MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/03/24 14:54 V46953MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 05/03/24 14:54 V46953MSA
<0.220 µg/L 0.220 0.500Toluene 1 05/03/24 14:54 V46953MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 05/03/24 14:54 V46953MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 05/03/24 14:54 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/03/24 14:54 V46953MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/03/24 14:54 V46953MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 05/03/24 14:54 V46953MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/03/24 14:54 V46953MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 05/03/24 14:54 V46953MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/03/24 14:54 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 60 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:Trip Blank
92189 Matrix:
4/26/2024 7:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 05/03/24 14:54 V46953MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/03/24 14:54 V46953MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 05/03/24 14:54 V46953MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 05/03/24 14:54 V46953MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 05/03/24 14:54 V46953
Surrogate: 4-Bromofluorobenzene 102 Limits: 80-124%05/03/24 14:541 MSA V46953
Surrogate: Dibromofluoromethane 102 Limits: 75-129%05/03/24 14:541 MSA V46953
Surrogate: 1,2-Dichloroethane - d4 98.6 Limits: 63-136%05/03/24 14:541 MSA V46953
Surrogate: Toluene-d8 101 Limits: 77-123%05/03/24 14:541 MSA V46953
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 61 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-1
92190 Matrix:
4/26/2024 10:30
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
0.414 J µg/L 0.297 1.00Arsenic 1 05/07/24 02:26 6020BCPW
35.3 µg/L 0.453 1.00Barium 1 05/07/24 02:26 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 05/07/24 02:26 6020BTJS
<0.346 µg/L 0.346 1.00Chromium 1 05/07/24 02:26 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 05/07/24 02:26 6020BCPW
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 05/01/24 16:40 7470ANPC
<0.703 µg/L 0.703 1.00Selenium 1 05/07/24 02:26 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 05/07/24 02:26 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 62 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-1
92190 Matrix:
4/26/2024 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
1.83 J µg/L 1.80 5.00Acetone 1 05/03/24 15:19 V46953MSA
<2.00 µg/L 2.00 5.00Acrolein 1 05/03/24 15:19 V46953MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 05/03/24 15:19 V46953MSA
<0.180 µg/L 0.180 0.500Benzene 1 05/03/24 15:19 V46953MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/03/24 15:19 V46953MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/03/24 15:19 V46953MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/03/24 15:19 V46953MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/03/24 15:19 V46953MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/03/24 15:19 V46953MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 05/03/24 15:19 V46953MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 05/03/24 15:19 V46953MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/03/24 15:19 V46953MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 05/03/24 15:19 V46953MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/03/24 15:19 V46953MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/03/24 15:19 V46953MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/03/24 15:19 V46953MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/03/24 15:19 V46953MSA
1.50 µg/L 0.220 0.500Chloroform 1 05/03/24 15:19 V46953MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 05/03/24 15:19 V46953MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/03/24 15:19 V46953MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/03/24 15:19 V46953MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 05/03/24 15:19 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 63 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-1
92190 Matrix:
4/26/2024 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/03/24 15:19 V46953MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/03/24 15:19 V46953MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 05/03/24 15:19 V46953MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/03/24 15:19 V46953MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/03/24 15:19 V46953MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/03/24 15:19 V46953MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/03/24 15:19 V46953MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/03/24 15:19 V46953MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/03/24 15:19 V46953MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/03/24 15:19 V46953MSA
5.88 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/03/24 15:19 V46953MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/03/24 15:19 V46953MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/03/24 15:19 V46953MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/03/24 15:19 V46953MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/03/24 15:19 V46953MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/03/24 15:19 V46953MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/03/24 15:19 V46953MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/03/24 15:19 V46953MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 05/03/24 15:19 V46953MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 05/03/24 15:19 V46953MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 05/03/24 15:19 V46953MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 05/03/24 15:19 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 64 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-1
92190 Matrix:
4/26/2024 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
0.501 J µg/L 0.380 5.002-Hexanone 1 05/03/24 15:19 V46953MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 05/03/24 15:19 V46953MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/03/24 15:19 V46953MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/03/24 15:19 V46953MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 05/03/24 15:19 V46953MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 05/03/24 15:19 V46953MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 05/03/24 15:19 V46953MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/03/24 15:19 V46953MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/03/24 15:19 V46953MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/03/24 15:19 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/03/24 15:19 V46953MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/03/24 15:19 V46953MSA
0.422 J µg/L 0.220 0.500Tetrachloroethene 1 05/03/24 15:19 V46953MSA
<0.220 µg/L 0.220 0.500Toluene 1 05/03/24 15:19 V46953MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 05/03/24 15:19 V46953MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 05/03/24 15:19 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/03/24 15:19 V46953MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/03/24 15:19 V46953MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 05/03/24 15:19 V46953MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/03/24 15:19 V46953MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 05/03/24 15:19 V46953MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/03/24 15:19 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 65 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-1
92190 Matrix:
4/26/2024 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 05/03/24 15:19 V46953MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/03/24 15:19 V46953MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 05/03/24 15:19 V46953MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 05/03/24 15:19 V46953MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 05/03/24 15:19 V46953
Surrogate: 4-Bromofluorobenzene 101 Limits: 80-124%05/03/24 15:191 MSA V46953
Surrogate: Dibromofluoromethane 101 Limits: 75-129%05/03/24 15:191 MSA V46953
Surrogate: 1,2-Dichloroethane - d4 98.8 Limits: 63-136%05/03/24 15:191 MSA V46953
Surrogate: Toluene-d8 99.4 Limits: 77-123%05/03/24 15:191 MSA V46953
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<0.302 µg/L 0.302 2.00Acenaphthene 1 04/30/24 18:49 V46675AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 04/30/24 18:49 V46675AMP
<2.05 µg/L 2.05 5.00Aniline 1 04/30/24 18:49 V46675AMP
<0.836 µg/L 0.836 2.00Anthracene 1 04/30/24 18:49 V46675AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 04/30/24 18:49 V46675AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 04/30/24 18:49 V46675AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 04/30/24 18:49 V46675AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 04/30/24 18:49 V46675AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 04/30/24 18:49 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 66 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-1
92190 Matrix:
4/26/2024 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<1.10 µg/L 1.10 10.0Benzoic Acid 1 04/30/24 18:49 V46675AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 04/30/24 18:49 V46675AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 04/30/24 18:49 V46675AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 04/30/24 18:49 V46675AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 04/30/24 18:49 V46675AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 04/30/24 18:49 V46675AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 04/30/24 18:49 V46675AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 04/30/24 18:49 V46675AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 04/30/24 18:49 V46675AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 04/30/24 18:49 V46675AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 04/30/24 18:49 V46675AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 04/30/24 18:49 V46675AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 04/30/24 18:49 V46675AMP
<0.405 µg/L 0.405 2.00Chrysene 1 04/30/24 18:49 V46675AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 04/30/24 18:49 V46675AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 04/30/24 18:49 V46675AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 04/30/24 18:49 V46675AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 04/30/24 18:49 V46675AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 04/30/24 18:49 V46675AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 04/30/24 18:49 V46675AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 04/30/24 18:49 V46675AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 04/30/24 18:49 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 67 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-1
92190 Matrix:
4/26/2024 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 04/30/24 18:49 V46675AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 04/30/24 18:49 V46675AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 04/30/24 18:49 V46675AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 04/30/24 18:49 V46675AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 04/30/24 18:49 V46675AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 04/30/24 18:49 V46675AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 04/30/24 18:49 V46675AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 04/30/24 18:49 V46675AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 04/30/24 18:49 V46675AMP
<0.807 µg/L 0.807 2.00Fluorene 1 04/30/24 18:49 V46675AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 04/30/24 18:49 V46675AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 04/30/24 18:49 V46675AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 04/30/24 18:49 V46675AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 04/30/24 18:49 V46675AMP
<0.444 µg/L 0.444 5.00Isophorone 1 04/30/24 18:49 V46675AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 04/30/24 18:49 V46675AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 04/30/24 18:49 V46675AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 04/30/24 18:49 V46675AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 04/30/24 18:49 V46675AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 04/30/24 18:49 V46675AMP
<1.39 µg/L 1.39 5.002-Nitroaniline 1 04/30/24 18:49 V46675AMP
<1.39 µg/L 1.39 5.003-Nitroaniline 1 04/30/24 18:49 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 68 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-1
92190 Matrix:
4/26/2024 10:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<1.53 µg/L 1.53 5.004-Nitroaniline 1 04/30/24 18:49 V46675AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 04/30/24 18:49 V46675AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 04/30/24 18:49 V46675AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 04/30/24 18:49 V46675AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 04/30/24 18:49 V46675AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 04/30/24 18:49 V46675AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 04/30/24 18:49 V46675AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 04/30/24 18:49 V46675AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 04/30/24 18:49 V46675AMP
<0.651 µg/L 0.651 5.00Phenol 1 04/30/24 18:49 V46675AMP
<0.434 µg/L 0.434 2.00Pyrene 1 04/30/24 18:49 V46675AMP
<1.20 µg/L 1.20 5.00Pyridine 1 04/30/24 18:49 V46675AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 04/30/24 18:49 V46675AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 04/30/24 18:49 V46675AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 04/30/24 18:49 V46675AMP
8270ESurrogate: Phenol-d5 28.0 Limits: 11-100%04/30/24 18:491 AMP
Surrogate: 2-Fluorobiphenyl 58.4 Limits: 44-119%04/30/24 18:491 AMP V46675
Surrogate: 2-Fluorophenol 38.2 Limits: 19-119%04/30/24 18:491 AMP V46675
Surrogate: Nitrobenzene-d5 63.6 Limits: 44-120%04/30/24 18:491 AMP V46675
Surrogate: 4-Terphenyl-d14 77.6 Limits: 50-134%04/30/24 18:491 AMP V46675
Surrogate: 2,4,6-Tribromophenol 61.4 Limits: 43-140%04/30/24 18:491 AMP V46675
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 69 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-2
92191 Matrix:
4/26/2024 8:10
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.297 µg/L 0.297 1.00Arsenic 1 05/07/24 02:30 6020BCPW
21.7 µg/L 0.453 1.00Barium 1 05/07/24 02:30 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 05/07/24 02:30 6020BTJS
1.91 µg/L 0.346 1.00Chromium 1 05/07/24 02:30 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 05/07/24 02:30 6020BCPW
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 05/01/24 16:56 7470ANPC
0.706 J µg/L 0.703 1.00Selenium 1 05/07/24 02:30 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 05/07/24 02:30 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 70 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-2
92191 Matrix:
4/26/2024 8:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
1.86 J µg/L 1.80 5.00Acetone 1 05/03/24 15:44 V46953MSA
<2.00 µg/L 2.00 5.00Acrolein 1 05/03/24 15:44 V46953MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 05/03/24 15:44 V46953MSA
<0.180 µg/L 0.180 0.500Benzene 1 05/03/24 15:44 V46953MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/03/24 15:44 V46953MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/03/24 15:44 V46953MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/03/24 15:44 V46953MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/03/24 15:44 V46953MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/03/24 15:44 V46953MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 05/03/24 15:44 V46953MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 05/03/24 15:44 V46953MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/03/24 15:44 V46953MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 05/03/24 15:44 V46953MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/03/24 15:44 V46953MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/03/24 15:44 V46953MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/03/24 15:44 V46953MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/03/24 15:44 V46953MSA
<0.220 µg/L 0.220 0.500Chloroform 1 05/03/24 15:44 V46953MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 05/03/24 15:44 V46953MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/03/24 15:44 V46953MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/03/24 15:44 V46953MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 05/03/24 15:44 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 71 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-2
92191 Matrix:
4/26/2024 8:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/03/24 15:44 V46953MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/03/24 15:44 V46953MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 05/03/24 15:44 V46953MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/03/24 15:44 V46953MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/03/24 15:44 V46953MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/03/24 15:44 V46953MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/03/24 15:44 V46953MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/03/24 15:44 V46953MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/03/24 15:44 V46953MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/03/24 15:44 V46953MSA
2.11 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/03/24 15:44 V46953MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/03/24 15:44 V46953MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/03/24 15:44 V46953MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/03/24 15:44 V46953MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/03/24 15:44 V46953MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/03/24 15:44 V46953MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/03/24 15:44 V46953MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/03/24 15:44 V46953MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 05/03/24 15:44 V46953MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 05/03/24 15:44 V46953MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 05/03/24 15:44 V46953MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 05/03/24 15:44 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 72 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-2
92191 Matrix:
4/26/2024 8:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<0.380 µg/L 0.380 5.002-Hexanone 1 05/03/24 15:44 V46953MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 05/03/24 15:44 V46953MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/03/24 15:44 V46953MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/03/24 15:44 V46953MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 05/03/24 15:44 V46953MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 05/03/24 15:44 V46953MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 05/03/24 15:44 V46953MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/03/24 15:44 V46953MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/03/24 15:44 V46953MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/03/24 15:44 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/03/24 15:44 V46953MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/03/24 15:44 V46953MSA
7.58 µg/L 0.220 0.500Tetrachloroethene 1 05/03/24 15:44 V46953MSA
<0.220 µg/L 0.220 0.500Toluene 1 05/03/24 15:44 V46953MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 05/03/24 15:44 V46953MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 05/03/24 15:44 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/03/24 15:44 V46953MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/03/24 15:44 V46953MSA
1.62 µg/L 0.180 0.500Trichloroethene 1 05/03/24 15:44 V46953MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/03/24 15:44 V46953MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 05/03/24 15:44 V46953MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/03/24 15:44 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 73 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-2
92191 Matrix:
4/26/2024 8:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 05/03/24 15:44 V46953MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/03/24 15:44 V46953MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 05/03/24 15:44 V46953MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 05/03/24 15:44 V46953MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 05/03/24 15:44 V46953
Surrogate: 4-Bromofluorobenzene 101 Limits: 80-124%05/03/24 15:441 MSA V46953
Surrogate: Dibromofluoromethane 102 Limits: 75-129%05/03/24 15:441 MSA V46953
Surrogate: 1,2-Dichloroethane - d4 99.2 Limits: 63-136%05/03/24 15:441 MSA V46953
Surrogate: Toluene-d8 99.4 Limits: 77-123%05/03/24 15:441 MSA V46953
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<0.302 µg/L 0.302 2.00Acenaphthene 1 04/30/24 19:14 V46675AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 04/30/24 19:14 V46675AMP
<2.05 µg/L 2.05 5.00Aniline 1 04/30/24 19:14 V46675AMP
<0.836 µg/L 0.836 2.00Anthracene 1 04/30/24 19:14 V46675AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 04/30/24 19:14 V46675AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 04/30/24 19:14 V46675AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 04/30/24 19:14 V46675AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 04/30/24 19:14 V46675AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 04/30/24 19:14 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 74 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-2
92191 Matrix:
4/26/2024 8:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<1.10 µg/L 1.10 10.0Benzoic Acid 1 04/30/24 19:14 V46675AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 04/30/24 19:14 V46675AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 04/30/24 19:14 V46675AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 04/30/24 19:14 V46675AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 04/30/24 19:14 V46675AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 04/30/24 19:14 V46675AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 04/30/24 19:14 V46675AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 04/30/24 19:14 V46675AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 04/30/24 19:14 V46675AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 04/30/24 19:14 V46675AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 04/30/24 19:14 V46675AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 04/30/24 19:14 V46675AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 04/30/24 19:14 V46675AMP
<0.405 µg/L 0.405 2.00Chrysene 1 04/30/24 19:14 V46675AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 04/30/24 19:14 V46675AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 04/30/24 19:14 V46675AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 04/30/24 19:14 V46675AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 04/30/24 19:14 V46675AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 04/30/24 19:14 V46675AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 04/30/24 19:14 V46675AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 04/30/24 19:14 V46675AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 04/30/24 19:14 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 75 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-2
92191 Matrix:
4/26/2024 8:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 04/30/24 19:14 V46675AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 04/30/24 19:14 V46675AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 04/30/24 19:14 V46675AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 04/30/24 19:14 V46675AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 04/30/24 19:14 V46675AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 04/30/24 19:14 V46675AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 04/30/24 19:14 V46675AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 04/30/24 19:14 V46675AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 04/30/24 19:14 V46675AMP
<0.807 µg/L 0.807 2.00Fluorene 1 04/30/24 19:14 V46675AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 04/30/24 19:14 V46675AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 04/30/24 19:14 V46675AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 04/30/24 19:14 V46675AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 04/30/24 19:14 V46675AMP
<0.444 µg/L 0.444 5.00Isophorone 1 04/30/24 19:14 V46675AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 04/30/24 19:14 V46675AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 04/30/24 19:14 V46675AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 04/30/24 19:14 V46675AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 04/30/24 19:14 V46675AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 04/30/24 19:14 V46675AMP
<1.39 µg/L 1.39 5.002-Nitroaniline 1 04/30/24 19:14 V46675AMP
<1.39 µg/L 1.39 5.003-Nitroaniline 1 04/30/24 19:14 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 76 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-2
92191 Matrix:
4/26/2024 8:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<1.53 µg/L 1.53 5.004-Nitroaniline 1 04/30/24 19:14 V46675AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 04/30/24 19:14 V46675AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 04/30/24 19:14 V46675AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 04/30/24 19:14 V46675AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 04/30/24 19:14 V46675AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 04/30/24 19:14 V46675AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 04/30/24 19:14 V46675AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 04/30/24 19:14 V46675AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 04/30/24 19:14 V46675AMP
<0.651 µg/L 0.651 5.00Phenol 1 04/30/24 19:14 V46675AMP
<0.434 µg/L 0.434 2.00Pyrene 1 04/30/24 19:14 V46675AMP
<1.20 µg/L 1.20 5.00Pyridine 1 04/30/24 19:14 V46675AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 04/30/24 19:14 V46675AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 04/30/24 19:14 V46675AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 04/30/24 19:14 V46675AMP
8270ESurrogate: Phenol-d5 27.8 Limits: 11-100%04/30/24 19:141 AMP
Surrogate: 2-Fluorobiphenyl 64.0 Limits: 44-119%04/30/24 19:141 AMP V46675
Surrogate: 2-Fluorophenol 39.4 Limits: 19-119%04/30/24 19:141 AMP V46675
Surrogate: Nitrobenzene-d5 65.0 Limits: 44-120%04/30/24 19:141 AMP V46675
Surrogate: 4-Terphenyl-d14 80.8 Limits: 50-134%04/30/24 19:141 AMP V46675
Surrogate: 2,4,6-Tribromophenol 64.8 Limits: 43-140%04/30/24 19:141 AMP V46675
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 77 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-3
92192 Matrix:
4/26/2024 13:05
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
0.495 J µg/L 0.297 1.00Arsenic 1 05/07/24 02:34 6020BCPW
67.3 µg/L 0.453 1.00Barium 1 05/07/24 02:34 6020BCPW
<0.350 µg/L 0.350 1.00Cadmium 1 05/07/24 02:34 6020BTJS
1.65 µg/L 0.346 1.00Chromium 1 05/07/24 02:34 6020BCPW
<0.264 µg/L 0.264 1.00Lead 1 05/07/24 02:34 6020BCPW
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 05/01/24 16:58 7470ANPC
<0.703 µg/L 0.703 1.00Selenium 1 05/07/24 02:34 6020BCPW
<0.0570 µg/L 0.0570 1.00Silver 1 05/07/24 02:34 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 78 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-3
92192 Matrix:
4/26/2024 13:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
3.73 J µg/L 1.80 5.00Acetone 1 05/03/24 16:09 V46953MSA
<2.00 µg/L 2.00 5.00Acrolein 1 05/03/24 16:09 V46953MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 05/03/24 16:09 V46953MSA
<0.180 µg/L 0.180 0.500Benzene 1 05/03/24 16:09 V46953MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/03/24 16:09 V46953MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/03/24 16:09 V46953MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/03/24 16:09 V46953MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/03/24 16:09 V46953MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/03/24 16:09 V46953MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 05/03/24 16:09 V46953MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 05/03/24 16:09 V46953MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/03/24 16:09 V46953MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 05/03/24 16:09 V46953MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/03/24 16:09 V46953MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/03/24 16:09 V46953MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/03/24 16:09 V46953MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/03/24 16:09 V46953MSA
4.72 µg/L 0.220 0.500Chloroform 1 05/03/24 16:09 V46953MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 05/03/24 16:09 V46953MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/03/24 16:09 V46953MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/03/24 16:09 V46953MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 05/03/24 16:09 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 79 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-3
92192 Matrix:
4/26/2024 13:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/03/24 16:09 V46953MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/03/24 16:09 V46953MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 05/03/24 16:09 V46953MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/03/24 16:09 V46953MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/03/24 16:09 V46953MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/03/24 16:09 V46953MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/03/24 16:09 V46953MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/03/24 16:09 V46953MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/03/24 16:09 V46953MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/03/24 16:09 V46953MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/03/24 16:09 V46953MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/03/24 16:09 V46953MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/03/24 16:09 V46953MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/03/24 16:09 V46953MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/03/24 16:09 V46953MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/03/24 16:09 V46953MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/03/24 16:09 V46953MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/03/24 16:09 V46953MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 05/03/24 16:09 V46953MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 05/03/24 16:09 V46953MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 05/03/24 16:09 V46953MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 05/03/24 16:09 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 80 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-3
92192 Matrix:
4/26/2024 13:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
1.56 J µg/L 0.380 5.002-Hexanone 1 05/03/24 16:09 V46953MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 05/03/24 16:09 V46953MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/03/24 16:09 V46953MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/03/24 16:09 V46953MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 05/03/24 16:09 V46953MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 05/03/24 16:09 V46953MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 05/03/24 16:09 V46953MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/03/24 16:09 V46953MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/03/24 16:09 V46953MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/03/24 16:09 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/03/24 16:09 V46953MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/03/24 16:09 V46953MSA
0.337 J µg/L 0.220 0.500Tetrachloroethene 1 05/03/24 16:09 V46953MSA
<0.220 µg/L 0.220 0.500Toluene 1 05/03/24 16:09 V46953MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 05/03/24 16:09 V46953MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 05/03/24 16:09 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/03/24 16:09 V46953MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/03/24 16:09 V46953MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 05/03/24 16:09 V46953MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/03/24 16:09 V46953MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 05/03/24 16:09 V46953MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/03/24 16:09 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 81 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-3
92192 Matrix:
4/26/2024 13:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 05/03/24 16:09 V46953MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/03/24 16:09 V46953MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 05/03/24 16:09 V46953MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 05/03/24 16:09 V46953MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 05/03/24 16:09 V46953
Surrogate: 4-Bromofluorobenzene 102 Limits: 80-124%05/03/24 16:091 MSA V46953
Surrogate: Dibromofluoromethane 102 Limits: 75-129%05/03/24 16:091 MSA V46953
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 63-136%05/03/24 16:091 MSA V46953
Surrogate: Toluene-d8 99.0 Limits: 77-123%05/03/24 16:091 MSA V46953
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<0.302 µg/L 0.302 2.00Acenaphthene 1 04/30/24 19:39 V46675AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 04/30/24 19:39 V46675AMP
<2.05 µg/L 2.05 5.00Aniline 1 04/30/24 19:39 V46675AMP
<0.836 µg/L 0.836 2.00Anthracene 1 04/30/24 19:39 V46675AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 04/30/24 19:39 V46675AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 04/30/24 19:39 V46675AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 04/30/24 19:39 V46675AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 04/30/24 19:39 V46675AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 04/30/24 19:39 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 82 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-3
92192 Matrix:
4/26/2024 13:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<1.10 µg/L 1.10 10.0Benzoic Acid 1 04/30/24 19:39 V46675AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 04/30/24 19:39 V46675AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 04/30/24 19:39 V46675AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 04/30/24 19:39 V46675AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 04/30/24 19:39 V46675AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 04/30/24 19:39 V46675AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 04/30/24 19:39 V46675AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 04/30/24 19:39 V46675AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 04/30/24 19:39 V46675AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 04/30/24 19:39 V46675AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 04/30/24 19:39 V46675AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 04/30/24 19:39 V46675AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 04/30/24 19:39 V46675AMP
<0.405 µg/L 0.405 2.00Chrysene 1 04/30/24 19:39 V46675AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 04/30/24 19:39 V46675AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 04/30/24 19:39 V46675AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 04/30/24 19:39 V46675AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 04/30/24 19:39 V46675AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 04/30/24 19:39 V46675AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 04/30/24 19:39 V46675AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 04/30/24 19:39 V46675AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 04/30/24 19:39 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 83 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-3
92192 Matrix:
4/26/2024 13:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 04/30/24 19:39 V46675AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 04/30/24 19:39 V46675AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 04/30/24 19:39 V46675AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 04/30/24 19:39 V46675AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 04/30/24 19:39 V46675AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 04/30/24 19:39 V46675AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 04/30/24 19:39 V46675AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 04/30/24 19:39 V46675AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 04/30/24 19:39 V46675AMP
<0.807 µg/L 0.807 2.00Fluorene 1 04/30/24 19:39 V46675AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 04/30/24 19:39 V46675AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 04/30/24 19:39 V46675AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 04/30/24 19:39 V46675AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 04/30/24 19:39 V46675AMP
<0.444 µg/L 0.444 5.00Isophorone 1 04/30/24 19:39 V46675AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 04/30/24 19:39 V46675AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 04/30/24 19:39 V46675AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 04/30/24 19:39 V46675AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 04/30/24 19:39 V46675AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 04/30/24 19:39 V46675AMP
<1.39 µg/L 1.39 5.002-Nitroaniline 1 04/30/24 19:39 V46675AMP
<1.39 µg/L 1.39 5.003-Nitroaniline 1 04/30/24 19:39 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 84 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:TMW-3
92192 Matrix:
4/26/2024 13:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<1.53 µg/L 1.53 5.004-Nitroaniline 1 04/30/24 19:39 V46675AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 04/30/24 19:39 V46675AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 04/30/24 19:39 V46675AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 04/30/24 19:39 V46675AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 04/30/24 19:39 V46675AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 04/30/24 19:39 V46675AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 04/30/24 19:39 V46675AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 04/30/24 19:39 V46675AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 04/30/24 19:39 V46675AMP
<0.651 µg/L 0.651 5.00Phenol 1 04/30/24 19:39 V46675AMP
<0.434 µg/L 0.434 2.00Pyrene 1 04/30/24 19:39 V46675AMP
<1.20 µg/L 1.20 5.00Pyridine 1 04/30/24 19:39 V46675AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 04/30/24 19:39 V46675AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 04/30/24 19:39 V46675AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 04/30/24 19:39 V46675AMP
8270ESurrogate: Phenol-d5 29.6 Limits: 11-100%04/30/24 19:391 AMP
Surrogate: 2-Fluorobiphenyl 60.6 Limits: 44-119%04/30/24 19:391 AMP V46675
Surrogate: 2-Fluorophenol 39.8 Limits: 19-119%04/30/24 19:391 AMP V46675
Surrogate: Nitrobenzene-d5 61.8 Limits: 44-120%04/30/24 19:391 AMP V46675
Surrogate: 4-Terphenyl-d14 75.8 Limits: 50-134%04/30/24 19:391 AMP V46675
Surrogate: 2,4,6-Tribromophenol 60.3 Limits: 43-140%04/30/24 19:391 AMP V46675
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 85 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-2
92193 Matrix:
4/26/2024 0:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
1.21 B µg/L 0.297 1.00Arsenic 1 05/03/24 21:15 6020BTJS
34.0 µg/L 0.453 1.00Barium 1 05/03/24 21:15 6020BTJS
<0.350 µg/L 0.350 1.00Cadmium 1 05/03/24 21:15 6020BTJS
0.946 J µg/L 0.346 1.00Chromium 1 05/03/24 21:15 6020BTJS
<0.264 µg/L 0.264 1.00Lead 1 05/03/24 21:15 6020BTJS
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 05/01/24 17:01 7470ANPC
0.887 J µg/L 0.703 1.00Selenium 1 05/03/24 21:15 6020BTJS
<0.0570 µg/L 0.0570 1.00Silver 1 05/03/24 21:15 6020BTJS
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 86 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-2
92193 Matrix:
4/26/2024 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.80 µg/L 1.80 5.00Acetone 1 05/03/24 16:34 V46953MSA
<2.00 µg/L 2.00 5.00Acrolein 1 05/03/24 16:34 V46953MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 05/03/24 16:34 V46953MSA
<0.180 µg/L 0.180 0.500Benzene 1 05/03/24 16:34 V46953MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/03/24 16:34 V46953MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/03/24 16:34 V46953MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/03/24 16:34 V46953MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/03/24 16:34 V46953MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/03/24 16:34 V46953MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 05/03/24 16:34 V46953MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 05/03/24 16:34 V46953MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/03/24 16:34 V46953MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 05/03/24 16:34 V46953MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/03/24 16:34 V46953MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/03/24 16:34 V46953MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/03/24 16:34 V46953MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/03/24 16:34 V46953MSA
1.64 µg/L 0.220 0.500Chloroform 1 05/03/24 16:34 V46953MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 05/03/24 16:34 V46953MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/03/24 16:34 V46953MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/03/24 16:34 V46953MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 05/03/24 16:34 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 87 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-2
92193 Matrix:
4/26/2024 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/03/24 16:34 V46953MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/03/24 16:34 V46953MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 05/03/24 16:34 V46953MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/03/24 16:34 V46953MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/03/24 16:34 V46953MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/03/24 16:34 V46953MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/03/24 16:34 V46953MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/03/24 16:34 V46953MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/03/24 16:34 V46953MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/03/24 16:34 V46953MSA
5.94 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/03/24 16:34 V46953MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/03/24 16:34 V46953MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/03/24 16:34 V46953MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/03/24 16:34 V46953MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/03/24 16:34 V46953MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/03/24 16:34 V46953MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/03/24 16:34 V46953MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/03/24 16:34 V46953MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 05/03/24 16:34 V46953MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 05/03/24 16:34 V46953MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 05/03/24 16:34 V46953MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 05/03/24 16:34 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 88 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-2
92193 Matrix:
4/26/2024 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
0.511 J µg/L 0.380 5.002-Hexanone 1 05/03/24 16:34 V46953MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 05/03/24 16:34 V46953MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/03/24 16:34 V46953MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/03/24 16:34 V46953MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 05/03/24 16:34 V46953MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 05/03/24 16:34 V46953MSA
<0.330 µg/L 0.330 1.00Methylene Chloride 1 05/03/24 16:34 V46953MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/03/24 16:34 V46953MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/03/24 16:34 V46953MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/03/24 16:34 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/03/24 16:34 V46953MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/03/24 16:34 V46953MSA
0.341 J µg/L 0.220 0.500Tetrachloroethene 1 05/03/24 16:34 V46953MSA
<0.220 µg/L 0.220 0.500Toluene 1 05/03/24 16:34 V46953MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 05/03/24 16:34 V46953MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 05/03/24 16:34 V46953MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/03/24 16:34 V46953MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/03/24 16:34 V46953MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 05/03/24 16:34 V46953MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/03/24 16:34 V46953MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 05/03/24 16:34 V46953MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/03/24 16:34 V46953MSA
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 89 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-2
92193 Matrix:
4/26/2024 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V46952 05/03/24 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 05/03/24 16:34 V46953MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/03/24 16:34 V46953MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 05/03/24 16:34 V46953MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 05/03/24 16:34 V46953MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 05/03/24 16:34 V46953
Surrogate: 4-Bromofluorobenzene 100 Limits: 80-124%05/03/24 16:341 MSA V46953
Surrogate: Dibromofluoromethane 102 Limits: 75-129%05/03/24 16:341 MSA V46953
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 63-136%05/03/24 16:341 MSA V46953
Surrogate: Toluene-d8 99.0 Limits: 77-123%05/03/24 16:341 MSA V46953
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<0.302 µg/L 0.302 2.00Acenaphthene 1 04/30/24 20:04 V46675AMP
<0.297 µg/L 0.297 2.00Acenaphthylene 1 04/30/24 20:04 V46675AMP
<2.05 µg/L 2.05 5.00Aniline 1 04/30/24 20:04 V46675AMP
<0.836 µg/L 0.836 2.00Anthracene 1 04/30/24 20:04 V46675AMP
<0.637 µg/L 0.637 2.00Benzo(a)anthracene 1 04/30/24 20:04 V46675AMP
<1.02 µg/L 1.02 2.00Benzo(a)pyrene 1 04/30/24 20:04 V46675AMP
<2.49 µg/L 2.49 5.00Benzo(b)fluoranthene 1 04/30/24 20:04 V46675AMP
<1.01 µg/L 1.01 5.00Benzo(g,h,i)perylene 1 04/30/24 20:04 V46675AMP
<1.99 µg/L 1.99 5.00Benzo(k)fluoranthene 1 04/30/24 20:04 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 90 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-2
92193 Matrix:
4/26/2024 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<1.10 µg/L 1.10 10.0Benzoic Acid 1 04/30/24 20:04 V46675AMP
<0.684 µg/L 0.684 5.00Benzyl alcohol 1 04/30/24 20:04 V46675AMP
<0.468 µg/L 0.468 5.00Bis(2-Chloroethoxy)methane 1 04/30/24 20:04 V46675AMP
<1.04 µg/L 1.04 5.00Bis(2-Chloroethyl)ether 1 04/30/24 20:04 V46675AMP
<1.08 µg/L 1.08 5.00Bis(2-Chloroisopropyl)ether 1 04/30/24 20:04 V46675AMP
<3.46 µg/L 3.46 10.0Bis(2-ethylhexyl)phthalate 1 04/30/24 20:04 V46675AMP
<1.11 µg/L 1.11 5.004-Bromophenyl phenyl ether 1 04/30/24 20:04 V46675AMP
<1.83 µg/L 1.83 5.00Butyl benzyl phthalate 1 04/30/24 20:04 V46675AMP
<1.18 µg/L 1.18 5.004-Chloro-3-methylphenol 1 04/30/24 20:04 V46675AMP
<1.33 µg/L 1.33 5.004-Chloroaniline 1 04/30/24 20:04 V46675AMP
<1.83 µg/L 1.83 20.02-Chloronaphthalene 1 04/30/24 20:04 V46675AMP
<0.938 µg/L 0.938 10.02-Chlorophenol 1 04/30/24 20:04 V46675AMP
<1.71 µg/L 1.71 5.004-Chlorophenyl phenyl ether 1 04/30/24 20:04 V46675AMP
<0.405 µg/L 0.405 2.00Chrysene 1 04/30/24 20:04 V46675AMP
<0.434 µg/L 0.434 2.00Dibenz(a,h)anthracene 1 04/30/24 20:04 V46675AMP
<0.856 µg/L 0.856 5.00Dibenzofuran 1 04/30/24 20:04 V46675AMP
<2.00 µg/L 2.00 5.001,2-Dichlorobenzene 1 04/30/24 20:04 V46675AMP
<2.00 µg/L 2.00 5.001,3-Dichlorobenzene 1 04/30/24 20:04 V46675AMP
<2.05 µg/L 2.05 5.001,4-Dichlorobenzene 1 04/30/24 20:04 V46675AMP
<1.89 µg/L 1.89 5.003,3'-Dichlorobenzidine 1 04/30/24 20:04 V46675AMP
<1.46 µg/L 1.46 10.02,4-Dichlorophenol 1 04/30/24 20:04 V46675AMP
<0.745 µg/L 0.745 5.00Diethyl phthalate 1 04/30/24 20:04 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 91 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-2
92193 Matrix:
4/26/2024 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<0.939 µg/L 0.939 5.00Dimethyl phthalate 1 04/30/24 20:04 V46675AMP
<1.57 µg/L 1.57 20.02,4-Dimethylphenol 1 04/30/24 20:04 V46675AMP
<2.06 µg/L 2.06 5.00Di-n-butyl phthalate 1 04/30/24 20:04 V46675AMP
<2.07 µg/L 2.07 10.04,6-Dinitro-2-methylphenol 1 04/30/24 20:04 V46675AMP
<1.92 µg/L 1.92 10.02,4-Dinitrophenol 1 04/30/24 20:04 V46675AMP
<1.11 µg/L 1.11 5.002,4-Dinitrotoluene 1 04/30/24 20:04 V46675AMP
<0.809 µg/L 0.809 5.002,6-Dinitrotoluene 1 04/30/24 20:04 V46675AMP
<1.65 µg/L 1.65 5.00Di-n-Octyl Phthalate 1 04/30/24 20:04 V46675AMP
<0.250 µg/L 0.250 2.00Fluoranthene 1 04/30/24 20:04 V46675AMP
<0.807 µg/L 0.807 2.00Fluorene 1 04/30/24 20:04 V46675AMP
<0.979 µg/L 0.979 5.00Hexachlorobenzene 1 04/30/24 20:04 V46675AMP
<2.73 µg/L 2.73 5.00Hexachlorobutadiene 1 04/30/24 20:04 V46675AMP
<1.76 µg/L 1.76 5.00Hexachloroethane 1 04/30/24 20:04 V46675AMP
<0.477 µg/L 0.477 2.00Indeno(1,2,3-cd)pyrene 1 04/30/24 20:04 V46675AMP
<0.444 µg/L 0.444 5.00Isophorone 1 04/30/24 20:04 V46675AMP
<1.14 µg/L 1.14 2.001-Methylnaphthalene 1 04/30/24 20:04 V46675AMP
<0.666 µg/L 0.666 2.002-Methylnaphthalene 1 04/30/24 20:04 V46675AMP
<1.15 µg/L 1.15 5.002-Methylphenol 1 04/30/24 20:04 V46675AMP
<0.880 µg/L 0.880 10.03&4 Methylphenol 1 04/30/24 20:04 V46675AMP
<0.728 µg/L 0.728 2.00Naphthalene 1 04/30/24 20:04 V46675AMP
<1.39 µg/L 1.39 5.002-Nitroaniline 1 04/30/24 20:04 V46675AMP
<1.39 µg/L 1.39 5.003-Nitroaniline 1 04/30/24 20:04 V46675AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 92 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:DUP-2
92193 Matrix:
4/26/2024 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V46634 04/30/24 10:25
<1.53 µg/L 1.53 5.004-Nitroaniline 1 04/30/24 20:04 V46675AMP
<0.905 µg/L 0.905 5.00Nitrobenzene 1 04/30/24 20:04 V46675AMP
<0.493 µg/L 0.493 5.002-Nitrophenol 1 04/30/24 20:04 V46675AMP
<1.23 µg/L 1.23 10.04-Nitrophenol 1 04/30/24 20:04 V46675AMP
<0.450 µg/L 0.450 5.00N-Nitrosodimethylamine 1 04/30/24 20:04 V46675AMP
<1.10 µg/L 1.10 5.00N-Nitrosodiphenylamine 1 04/30/24 20:04 V46675AMP
<0.641 µg/L 0.641 5.00N-Nitroso-di-n-propylamine 1 04/30/24 20:04 V46675AMP
<1.43 µg/L 1.43 5.00Pentachlorophenol 1 04/30/24 20:04 V46675AMP
<0.428 µg/L 0.428 2.00Phenanthrene 1 04/30/24 20:04 V46675AMP
<0.651 µg/L 0.651 5.00Phenol 1 04/30/24 20:04 V46675AMP
<0.434 µg/L 0.434 2.00Pyrene 1 04/30/24 20:04 V46675AMP
<1.20 µg/L 1.20 5.00Pyridine 1 04/30/24 20:04 V46675AMP
<2.21 µg/L 2.21 5.001,2,4-Trichlorobenzene 1 04/30/24 20:04 V46675AMP
<1.31 µg/L 1.31 5.002,4,5-Trichlorophenol 1 04/30/24 20:04 V46675AMP
<1.32 µg/L 1.32 5.002,4,6-Trichlorophenol 1 04/30/24 20:04 V46675AMP
8270ESurrogate: Phenol-d5 30.9 Limits: 11-100%04/30/24 20:041 AMP
Surrogate: 2-Fluorobiphenyl 64.2 Limits: 44-119%04/30/24 20:041 AMP V46675
Surrogate: 2-Fluorophenol 42.2 Limits: 19-119%04/30/24 20:041 AMP V46675
Surrogate: Nitrobenzene-d5 64.8 Limits: 44-120%04/30/24 20:041 AMP V46675
Surrogate: 4-Terphenyl-d14 80.8 Limits: 50-134%04/30/24 20:041 AMP V46675
Surrogate: 2,4,6-Tribromophenol 64.8 Limits: 43-140%04/30/24 20:041 AMP V46675
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 93 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4
92194 Matrix:
4/26/2024 13:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.4 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
0.361 B mg/Kg - dry 0.172 0.245Chromium, Hexavalent 1 05/02/24 19:26 SW-7199MKD
876 µg/Kg - dry 105 306Arsenic 5 05/04/24 14:26 6020BCPW
74600 µg/Kg - dry 52.5 306Barium 5 05/04/24 14:26 6020BCPW
33.9 J µg/Kg - dry 31.9 306Cadmium 5 05/04/24 14:26 6020BCPW
26000 µg/Kg - dry 142 306Chromium 5 05/04/24 14:26 6020BCPW
5890 µg/Kg - dry 38.0 306Lead 5 05/04/24 14:26 6020BCPW
<0.0147 mg/Kg - dry 0.0147 0.0368Mercury (Total)1 05/03/24 12:50 7471BJKC
249 J µg/Kg - dry 126 306Selenium 5 05/04/24 14:26 6020BCPW
32.8 J µg/Kg - dry 8.26 306Silver 5 05/04/24 14:26 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 94 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4
92194 Matrix:
4/26/2024 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46854 05/06/24 09:20
<0.180 mg/Kg - dry 0.180 0.808Acenaphthene 1 05/07/24 22:27 V46903AMP
<0.183 mg/Kg - dry 0.183 0.808Acenaphthylene 1 05/07/24 22:27 V46903AMP
<0.257 mg/Kg - dry 0.257 0.808Aniline 1 05/07/24 22:27 V46903AMP
0.225 J mg/Kg - dry 0.203 0.808Anthracene 1 05/07/24 22:27 V46903AMP
0.623 J mg/Kg - dry 0.191 0.808Benzo(a)anthracene 1 05/07/24 22:27 V46903AMP
0.468 J mg/Kg - dry 0.202 0.808Benzo(a)pyrene 1 05/07/24 22:27 V46903AMP
0.860 mg/Kg - dry 0.180 0.808Benzo(b)fluoranthene 1 05/07/24 22:27 V46903AMP
0.263 J mg/Kg - dry 0.176 0.808Benzo(g,h,i)perylene 1 05/07/24 22:27 V46903AMP
<0.191 mg/Kg - dry 0.191 0.808Benzo(k)fluoranthene 1 05/07/24 22:27 V46903AMP
<0.710 mg/Kg - dry 0.710 2.45Benzoic Acid 1 05/07/24 22:27 V46903AMP
<0.191 mg/Kg - dry 0.191 0.808Benzyl alcohol 1 05/07/24 22:27 V46903AMP
<0.169 mg/Kg - dry 0.169 0.808Bis(2-Chloroethoxy)methane 1 05/07/24 22:27 V46903AMP
<0.149 mg/Kg - dry 0.149 0.808Bis(2-Chloroethyl)ether 1 05/07/24 22:27 V46903AMP
<0.160 mg/Kg - dry 0.160 0.404Bis(2-Chloroisopropyl)ether 1 05/07/24 22:27 V46903AMP
<0.216 mg/Kg - dry 0.216 0.808Bis(2-ethylhexyl)phthalate 1 05/07/24 22:27 V46903AMP
<0.193 mg/Kg - dry 0.193 0.8084-Bromophenyl phenyl ether 1 05/07/24 22:27 V46903AMP
<0.196 mg/Kg - dry 0.196 0.404Butyl benzyl phthalate 1 05/07/24 22:27 V46903AMP
<0.182 mg/Kg - dry 0.182 0.8084-Chloro-3-methylphenol 1 05/07/24 22:27 V46903AMP
<0.183 mg/Kg - dry 0.183 0.4044-Chloroaniline 1 05/07/24 22:27 V46903AMP
<0.188 mg/Kg - dry 0.188 0.8082-Chloronaphthalene 1 05/07/24 22:27 V46903AMP
<0.174 mg/Kg - dry 0.174 0.8082-Chlorophenol 1 05/07/24 22:27 V46903AMP
<0.180 mg/Kg - dry 0.180 1.234-Chlorophenyl phenyl ether 1 05/07/24 22:27 V46903AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 95 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4
92194 Matrix:
4/26/2024 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46854 05/06/24 09:20
0.475 J mg/Kg - dry 0.178 0.808Chrysene 1 05/07/24 22:27 V46903AMP
0.289 JM mg/Kg - dry 0.136 0.808Dibenz(a,h)anthracene 1 05/07/24 22:27 V46903AMP
<0.193 mg/Kg - dry 0.193 0.808Dibenzofuran 1 05/07/24 22:27 V46903AMP
<0.156 mg/Kg - dry 0.156 0.8081,2-Dichlorobenzene 1 05/07/24 22:27 V46903AMP
<0.153 mg/Kg - dry 0.153 0.8081,3-Dichlorobenzene 1 05/07/24 22:27 V46903AMP
<0.144 mg/Kg - dry 0.144 0.4041,4-Dichlorobenzene 1 05/07/24 22:27 V46903AMP
<0.183 mg/Kg - dry 0.183 0.8083,3'-Dichlorobenzidine 1 05/07/24 22:27 V46903AMP
<0.171 mg/Kg - dry 0.171 0.8082,4-Dichlorophenol 1 05/07/24 22:27 V46903AMP
<0.180 mg/Kg - dry 0.180 0.808Diethyl phthalate 1 05/07/24 22:27 V46903AMP
<0.192 mg/Kg - dry 0.192 0.808Dimethyl phthalate 1 05/07/24 22:27 V46903AMP
<0.259 mg/Kg - dry 0.259 0.8082,4-Dimethylphenol 1 05/07/24 22:27 V46903AMP
<0.209 mg/Kg - dry 0.209 0.808Di-n-butyl phthalate 1 05/07/24 22:27 V46903AMP
<0.294 mg/Kg - dry 0.294 1.844,6-Dinitro-2-methylphenol 1 05/07/24 22:27 V46903AMP
<0.637 mg/Kg - dry 0.637 1.842,4-Dinitrophenol 1 05/07/24 22:27 V46903AMP
<0.197 mg/Kg - dry 0.197 0.8082,4-Dinitrotoluene 1 05/07/24 22:27 V46903AMP
<0.203 mg/Kg - dry 0.203 0.8082,6-Dinitrotoluene 1 05/07/24 22:27 V46903AMP
<0.199 mg/Kg - dry 0.199 0.404Di-n-Octyl Phthalate 1 05/07/24 22:27 V46903AMP
1.30 mg/Kg - dry 0.193 0.808Fluoranthene 1 05/07/24 22:27 V46903AMP
<0.187 mg/Kg - dry 0.187 0.808Fluorene 1 05/07/24 22:27 V46903AMP
<0.183 mg/Kg - dry 0.183 0.808Hexachlorobenzene 1 05/07/24 22:27 V46903AMP
<0.119 mg/Kg - dry 0.119 0.808Hexachlorobutadiene 1 05/07/24 22:27 V46903AMP
<0.122 mg/Kg - dry 0.122 0.808Hexachlorocyclopentadiene 1 05/07/24 22:27 V46903AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 96 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4
92194 Matrix:
4/26/2024 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46854 05/06/24 09:20
<0.149 mg/Kg - dry 0.149 0.808Hexachloroethane 1 05/07/24 22:27 V46903AMP
0.399 J mg/Kg - dry 0.185 0.808Indeno(1,2,3-cd)pyrene 1 05/07/24 22:27 V46903AMP
<0.148 mg/Kg - dry 0.148 0.808Isophorone 1 05/07/24 22:27 V46903AMP
<0.170 mg/Kg - dry 0.170 0.8081-Methylnaphthalene 1 05/07/24 22:27 V46903AMP
<0.176 mg/Kg - dry 0.176 0.8082-Methylnaphthalene 1 05/07/24 22:27 V46903AMP
<0.155 mg/Kg - dry 0.155 0.8082-Methylphenol 1 05/07/24 22:27 V46903AMP
<0.156 mg/Kg - dry 0.156 0.8083&4 Methylphenol 1 05/07/24 22:27 V46903AMP
<0.162 mg/Kg - dry 0.162 0.808Naphthalene 1 05/07/24 22:27 V46903AMP
<0.161 mg/Kg - dry 0.161 0.8082-Nitroaniline 1 05/07/24 22:27 V46903AMP
<0.189 mg/Kg - dry 0.189 0.8083-Nitroaniline 1 05/07/24 22:27 V46903AMP
<0.166 mg/Kg - dry 0.166 0.4044-Nitroaniline 1 05/07/24 22:27 V46903AMP
<0.158 mg/Kg - dry 0.158 0.404Nitrobenzene 1 05/07/24 22:27 V46903AMP
<0.162 mg/Kg - dry 0.162 0.8082-Nitrophenol 1 05/07/24 22:27 V46903AMP
<0.204 mg/Kg - dry 0.204 0.8084-Nitrophenol 1 05/07/24 22:27 V46903AMP
<0.322 mg/Kg - dry 0.322 0.808N-Nitrosodimethylamine 1 05/07/24 22:27 V46903AMP
<0.223 mg/Kg - dry 0.223 0.808N-Nitrosodiphenylamine 1 05/07/24 22:27 V46903AMP
<0.181 mg/Kg - dry 0.181 0.808N-Nitroso-di-n-propylamine 1 05/07/24 22:27 V46903AMP
<0.425 mg/Kg - dry 0.425 1.23Pentachlorophenol 1 05/07/24 22:27 V46903AMP
0.850 mg/Kg - dry 0.193 0.808Phenanthrene 1 05/07/24 22:27 V46903AMP
<0.174 mg/Kg - dry 0.174 0.808Phenol 1 05/07/24 22:27 V46903AMP
0.819 mg/Kg - dry 0.196 0.808Pyrene 1 05/07/24 22:27 V46903AMP
<0.094 mg/Kg - dry 0.094 0.404Pyridine 1 05/07/24 22:27 V46903AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 97 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-4
92194 Matrix:
4/26/2024 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46854 05/06/24 09:20
<0.161 mg/Kg - dry 0.161 0.8081,2,4-Trichlorobenzene 1 05/07/24 22:27 V46903AMP
<0.175 mg/Kg - dry 0.175 0.8082,4,5-Trichlorophenol 1 05/07/24 22:27 V46903AMP
<0.171 mg/Kg - dry 0.171 0.8082,4,6-Trichlorophenol 1 05/07/24 22:27 V46903AMP
8270ESurrogate: Phenol-d5 90.1 Limits: 34-121%05/07/24 22:271 AMP
Surrogate: 2-Fluorobiphenyl 77.1 Limits: 44-115%05/07/24 22:271 AMP V46903
Surrogate: 2-Fluorophenol 85.0 Limits: 35-115%05/07/24 22:271 AMP V46903
Surrogate: Nitrobenzene-d5 80.1 Limits: 37-122%05/07/24 22:271 AMP V46903
Surrogate: 4-Terphenyl-d14 81.9 Limits: 54-127%05/07/24 22:271 AMP V46903
Surrogate: 2,4,6-Tribromophenol 82.9 Limits: 39-132%05/07/24 22:271 AMP V46903
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 98 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5E (4-5)
92195 Matrix:
4/26/2024 12:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
27.7 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 99 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5E (4-5)
92195 Matrix:
4/26/2024 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
0.017 J mg/Kg - dry 0.003 0.027Acetone 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 04/29/24 18:48 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/29/24 18:48 V46655TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 04/29/24 18:48 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 04/29/24 18:48 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 04/29/24 18:48 V46655TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 04/29/24 18:48 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/29/24 18:48 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 04/29/24 18:48 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 04/29/24 18:48 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 100 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5E (4-5)
92195 Matrix:
4/26/2024 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 04/29/24 18:48 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 04/29/24 18:48 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 04/29/24 18:48 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/29/24 18:48 V46655TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/29/24 18:48 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/29/24 18:48 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 04/29/24 18:48 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 04/29/24 18:48 V46655TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/29/24 18:48 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 04/29/24 18:48 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 101 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5E (4-5)
92195 Matrix:
4/26/2024 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 04/29/24 18:48 V46655TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/29/24 18:48 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 04/29/24 18:48 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 04/29/24 18:48 V46655TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 04/29/24 18:48 V46655TBL
0.007 J mg/Kg - dry 0.002 0.013Methylene Chloride 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/29/24 18:48 V46655TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/29/24 18:48 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 04/29/24 18:48 V46655TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/29/24 18:48 V46655TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 04/29/24 18:48 V46655TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/29/24 18:48 V46655TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 102 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5E (4-5)
92195 Matrix:
4/26/2024 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V46653 04/29/24 08:00
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 04/29/24 18:48 V46655TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/29/24 18:48 V46655TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/29/24 18:48 V46655
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%04/29/24 18:481 TBL V46655
Surrogate: Dibromofluoromethane 100 Limits: 84-123%04/29/24 18:481 TBL V46655
Surrogate: Toluene-d8 96.4 Limits: 76-129%04/29/24 18:481 TBL V46655
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 103 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5
92196 Matrix:
4/26/2024 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.3 %Moisture 1 05/01/24 10:05 SW-DRYWTAKF
0.384 B mg/Kg - dry 0.183 0.260Chromium, Hexavalent 1 05/02/24 19:37 SW-7199MKD
3550 µg/Kg - dry 111 326Arsenic 5 05/04/24 14:31 6020BCPW
78000 µg/Kg - dry 55.8 326Barium 5 05/04/24 14:31 6020BCPW
37.5 J µg/Kg - dry 33.9 326Cadmium 5 05/04/24 14:31 6020BCPW
54100 µg/Kg - dry 151 326Chromium 5 05/04/24 14:31 6020BCPW
5610 µg/Kg - dry 40.4 326Lead 5 05/04/24 14:31 6020BCPW
<0.0156 mg/Kg - dry 0.0156 0.0391Mercury (Total)1 05/03/24 12:53 7471BJKC
189 J µg/Kg - dry 134 326Selenium 5 05/04/24 14:31 6020BCPW
42.6 J µg/Kg - dry 8.79 326Silver 5 05/04/24 14:31 6020BCPW
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 104 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5
92196 Matrix:
4/26/2024 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46854 05/06/24 09:20
<0.191 mg/Kg - dry 0.191 0.860Acenaphthene 1 05/07/24 22:52 V46903AMP
<0.195 mg/Kg - dry 0.195 0.860Acenaphthylene 1 05/07/24 22:52 V46903AMP
<0.273 mg/Kg - dry 0.273 0.860Aniline 1 05/07/24 22:52 V46903AMP
<0.216 mg/Kg - dry 0.216 0.860Anthracene 1 05/07/24 22:52 V46903AMP
<0.203 mg/Kg - dry 0.203 0.860Benzo(a)anthracene 1 05/07/24 22:52 V46903AMP
<0.215 mg/Kg - dry 0.215 0.860Benzo(a)pyrene 1 05/07/24 22:52 V46903AMP
<0.191 mg/Kg - dry 0.191 0.860Benzo(b)fluoranthene 1 05/07/24 22:52 V46903AMP
<0.187 mg/Kg - dry 0.187 0.860Benzo(g,h,i)perylene 1 05/07/24 22:52 V46903AMP
<0.203 mg/Kg - dry 0.203 0.860Benzo(k)fluoranthene 1 05/07/24 22:52 V46903AMP
<0.756 mg/Kg - dry 0.756 2.61Benzoic Acid 1 05/07/24 22:52 V46903AMP
<0.203 mg/Kg - dry 0.203 0.860Benzyl alcohol 1 05/07/24 22:52 V46903AMP
<0.179 mg/Kg - dry 0.179 0.860Bis(2-Chloroethoxy)methane 1 05/07/24 22:52 V46903AMP
<0.159 mg/Kg - dry 0.159 0.860Bis(2-Chloroethyl)ether 1 05/07/24 22:52 V46903AMP
<0.170 mg/Kg - dry 0.170 0.430Bis(2-Chloroisopropyl)ether 1 05/07/24 22:52 V46903AMP
<0.230 mg/Kg - dry 0.230 0.860Bis(2-ethylhexyl)phthalate 1 05/07/24 22:52 V46903AMP
<0.205 mg/Kg - dry 0.205 0.8604-Bromophenyl phenyl ether 1 05/07/24 22:52 V46903AMP
<0.208 mg/Kg - dry 0.208 0.430Butyl benzyl phthalate 1 05/07/24 22:52 V46903AMP
<0.194 mg/Kg - dry 0.194 0.8604-Chloro-3-methylphenol 1 05/07/24 22:52 V46903AMP
<0.195 mg/Kg - dry 0.195 0.4304-Chloroaniline 1 05/07/24 22:52 V46903AMP
<0.200 mg/Kg - dry 0.200 0.8602-Chloronaphthalene 1 05/07/24 22:52 V46903AMP
<0.185 mg/Kg - dry 0.185 0.8602-Chlorophenol 1 05/07/24 22:52 V46903AMP
<0.191 mg/Kg - dry 0.191 1.304-Chlorophenyl phenyl ether 1 05/07/24 22:52 V46903AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 105 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5
92196 Matrix:
4/26/2024 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46854 05/06/24 09:20
<0.190 mg/Kg - dry 0.190 0.860Chrysene 1 05/07/24 22:52 V46903AMP
<0.144 M mg/Kg - dry 0.144 0.860Dibenz(a,h)anthracene 1 05/07/24 22:52 V46903AMP
<0.205 mg/Kg - dry 0.205 0.860Dibenzofuran 1 05/07/24 22:52 V46903AMP
<0.166 mg/Kg - dry 0.166 0.8601,2-Dichlorobenzene 1 05/07/24 22:52 V46903AMP
<0.162 mg/Kg - dry 0.162 0.8601,3-Dichlorobenzene 1 05/07/24 22:52 V46903AMP
<0.153 mg/Kg - dry 0.153 0.4301,4-Dichlorobenzene 1 05/07/24 22:52 V46903AMP
<0.195 mg/Kg - dry 0.195 0.8603,3'-Dichlorobenzidine 1 05/07/24 22:52 V46903AMP
<0.182 mg/Kg - dry 0.182 0.8602,4-Dichlorophenol 1 05/07/24 22:52 V46903AMP
<0.191 mg/Kg - dry 0.191 0.860Diethyl phthalate 1 05/07/24 22:52 V46903AMP
<0.204 mg/Kg - dry 0.204 0.860Dimethyl phthalate 1 05/07/24 22:52 V46903AMP
<0.276 mg/Kg - dry 0.276 0.8602,4-Dimethylphenol 1 05/07/24 22:52 V46903AMP
<0.222 mg/Kg - dry 0.222 0.860Di-n-butyl phthalate 1 05/07/24 22:52 V46903AMP
<0.312 mg/Kg - dry 0.312 1.964,6-Dinitro-2-methylphenol 1 05/07/24 22:52 V46903AMP
<0.677 mg/Kg - dry 0.677 1.962,4-Dinitrophenol 1 05/07/24 22:52 V46903AMP
<0.209 mg/Kg - dry 0.209 0.8602,4-Dinitrotoluene 1 05/07/24 22:52 V46903AMP
<0.216 mg/Kg - dry 0.216 0.8602,6-Dinitrotoluene 1 05/07/24 22:52 V46903AMP
<0.212 mg/Kg - dry 0.212 0.430Di-n-Octyl Phthalate 1 05/07/24 22:52 V46903AMP
<0.205 mg/Kg - dry 0.205 0.860Fluoranthene 1 05/07/24 22:52 V46903AMP
<0.199 mg/Kg - dry 0.199 0.860Fluorene 1 05/07/24 22:52 V46903AMP
<0.195 mg/Kg - dry 0.195 0.860Hexachlorobenzene 1 05/07/24 22:52 V46903AMP
<0.127 mg/Kg - dry 0.127 0.860Hexachlorobutadiene 1 05/07/24 22:52 V46903AMP
<0.130 mg/Kg - dry 0.130 0.860Hexachlorocyclopentadiene 1 05/07/24 22:52 V46903AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 106 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5
92196 Matrix:
4/26/2024 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46854 05/06/24 09:20
<0.159 mg/Kg - dry 0.159 0.860Hexachloroethane 1 05/07/24 22:52 V46903AMP
<0.196 mg/Kg - dry 0.196 0.860Indeno(1,2,3-cd)pyrene 1 05/07/24 22:52 V46903AMP
<0.157 mg/Kg - dry 0.157 0.860Isophorone 1 05/07/24 22:52 V46903AMP
<0.181 mg/Kg - dry 0.181 0.8601-Methylnaphthalene 1 05/07/24 22:52 V46903AMP
<0.187 mg/Kg - dry 0.187 0.8602-Methylnaphthalene 1 05/07/24 22:52 V46903AMP
<0.165 mg/Kg - dry 0.165 0.8602-Methylphenol 1 05/07/24 22:52 V46903AMP
<0.166 mg/Kg - dry 0.166 0.8603&4 Methylphenol 1 05/07/24 22:52 V46903AMP
<0.173 mg/Kg - dry 0.173 0.860Naphthalene 1 05/07/24 22:52 V46903AMP
<0.172 mg/Kg - dry 0.172 0.8602-Nitroaniline 1 05/07/24 22:52 V46903AMP
<0.202 mg/Kg - dry 0.202 0.8603-Nitroaniline 1 05/07/24 22:52 V46903AMP
<0.177 mg/Kg - dry 0.177 0.4304-Nitroaniline 1 05/07/24 22:52 V46903AMP
<0.168 mg/Kg - dry 0.168 0.430Nitrobenzene 1 05/07/24 22:52 V46903AMP
<0.173 mg/Kg - dry 0.173 0.8602-Nitrophenol 1 05/07/24 22:52 V46903AMP
<0.217 mg/Kg - dry 0.217 0.8604-Nitrophenol 1 05/07/24 22:52 V46903AMP
<0.342 mg/Kg - dry 0.342 0.860N-Nitrosodimethylamine 1 05/07/24 22:52 V46903AMP
<0.237 mg/Kg - dry 0.237 0.860N-Nitrosodiphenylamine 1 05/07/24 22:52 V46903AMP
<0.192 mg/Kg - dry 0.192 0.860N-Nitroso-di-n-propylamine 1 05/07/24 22:52 V46903AMP
<0.452 mg/Kg - dry 0.452 1.30Pentachlorophenol 1 05/07/24 22:52 V46903AMP
<0.205 mg/Kg - dry 0.205 0.860Phenanthrene 1 05/07/24 22:52 V46903AMP
<0.185 mg/Kg - dry 0.185 0.860Phenol 1 05/07/24 22:52 V46903AMP
<0.208 mg/Kg - dry 0.208 0.860Pyrene 1 05/07/24 22:52 V46903AMP
<0.100 mg/Kg - dry 0.100 0.430Pyridine 1 05/07/24 22:52 V46903AMP
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 107 of 163
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28204
24-120-0005
01138
Mid-Atlantic Associates, Inc. - Charlotte
1125 E. Morehead Street, Suite 104
Shane Sisco
Charlotte
Received : 04/26/2024
Metropolitan
Report Date : 05/09/2024
Sample ID :
Lab No :
Sampled:ES-5
92196 Matrix:
4/26/2024 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V46854 05/06/24 09:20
<0.172 mg/Kg - dry 0.172 0.8601,2,4-Trichlorobenzene 1 05/07/24 22:52 V46903AMP
<0.186 mg/Kg - dry 0.186 0.8602,4,5-Trichlorophenol 1 05/07/24 22:52 V46903AMP
<0.182 mg/Kg - dry 0.182 0.8602,4,6-Trichlorophenol 1 05/07/24 22:52 V46903AMP
8270ESurrogate: Phenol-d5 81.7 Limits: 34-121%05/07/24 22:521 AMP
Surrogate: 2-Fluorobiphenyl 72.5 Limits: 44-115%05/07/24 22:521 AMP V46903
Surrogate: 2-Fluorophenol 80.8 Limits: 35-115%05/07/24 22:521 AMP V46903
Surrogate: Nitrobenzene-d5 73.7 Limits: 37-122%05/07/24 22:521 AMP V46903
Surrogate: 4-Terphenyl-d14 73.1 Limits: 54-127%05/07/24 22:521 AMP V46903
Surrogate: 2,4,6-Tribromophenol 76.0 Limits: 39-132%05/07/24 22:521 AMP V46903
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 108 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Metals Analyses
6020B
L748679,L748948,L749173QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:L748339
Associated Lab Samples: 92190, 92191, 92192
LRB-L748339 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/07/24 01:011.000.297<0.297µg/LArsenic
05/03/24 18:571.000.453<0.453µg/LBarium
05/03/24 18:571.000.350<0.350µg/LCadmium
05/03/24 18:571.000.346<0.346µg/LChromium
05/03/24 18:571.000.264<0.264µg/LLead
05/03/24 18:571.000.703<0.703µg/LSelenium
05/03/24 18:571.000.0570<0.0570µg/LSilver
LCS-L748339Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10150.650.0µg/LArsenic 80-120
91.090.8100µg/LBarium 80-120
10210.210.0µg/LCadmium 80-120
10099.8100µg/LChromium 80-120
10251.250.0µg/LLead 80-120
108108100µg/LSelenium 80-120
10110.110.0µg/LSilver 80-120
V 92192-MS-L748339 V 92192-MSD-L748339Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
51.3 10247.550.050.00.495µg/LArsenic 94.0 75-125 7.6 20.0
179 11216910010067.3µg/LBarium 102 75-125 5.7 20.0
9.71 97.09.5810.010.0< 0.350µg/LCadmium 96.0 75-125 1.3 20.0
108 10699.21001001.65µg/LChromium 98.0 75-125 8.4 20.0
Page 1 of 52Date:05/09/2024 02:05 PM
Page 109 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Metals Analyses
6020B
L748679,L748948,L749173QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:L748339
V 92192-MS-L748339 V 92192-MSD-L748339Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
50.9 10247.950.050.0< 0.264µg/LLead 96.0 75-125 6.0 20.0
109 109101100100< 0.703µg/LSelenium 101 75-125 7.6 20.0
9.76 98.09.0510.010.0< 0.0570µg/LSilver 91.0 75-125 7.5 20.0
Page 2 of 52Date:05/09/2024 02:05 PM
Page 110 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Metals Analyses
6020B
L748679QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:L748340
Associated Lab Samples: 92193
LRB-L748340 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/03/24 21:081.000.2970.633µg/LArsenic
05/03/24 21:081.000.453<0.453µg/LBarium
05/03/24 21:081.000.350<0.350µg/LCadmium
05/03/24 21:081.000.346<0.346µg/LChromium
05/03/24 21:081.000.264<0.264µg/LLead
05/03/24 21:081.000.703<0.703µg/LSelenium
05/03/24 21:081.000.0570<0.0570µg/LSilver
LCS-L748340Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.049.050.0µg/LArsenic 80-120
90.090.4100µg/LBarium 80-120
97.09.6910.0µg/LCadmium 80-120
95.095.0100µg/LChromium 80-120
99.049.450.0µg/LLead 80-120
101101100µg/LSelenium 80-120
97.09.6510.0µg/LSilver 80-120
V 91794-MS-L748340 V 91794-MSD-L748340Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
60.7 99.059.550.050.011.1µg/LArsenic 97.0 75-125 1.9 20.0
233 128*228100100105µg/LBarium 123 75-125 2.1 20.0
9.28 93.09.0610.010.0< 0.350µg/LCadmium 91.0 75-125 2.3 20.0
146 99.013910010047.2µg/LChromium 92.0 75-125 4.9 20.0
Page 3 of 52Date:05/09/2024 02:05 PM
Page 111 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Metals Analyses
6020B
L748679QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:L748340
V 91794-MS-L748340 V 91794-MSD-L748340Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
56.3 10654.450.050.03.26µg/LLead 102 75-125 3.4 20.0
128 11412110010013.9µg/LSelenium 107 75-125 5.6 20.0
8.90 89.08.7710.010.0< 0.0570µg/LSilver 88.0 75-125 1.4 20.0
V 91794-PDS-L748340Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/03/24 22:5296.029.3µg/LArsenic
05/03/24 22:5297.098.7µg/LBarium
05/03/24 22:5292.04.62µg/LCadmium
05/03/24 22:5293.068.2µg/LChromium
05/03/24 22:5210026.6µg/LLead
05/03/24 22:5210358.7µg/LSelenium
05/03/24 22:5288.04.40µg/LSilver
Page 4 of 52Date:05/09/2024 02:05 PM
Page 112 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Metals Analyses
6020B
L748699QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L748510
Associated Lab Samples: 92181, 92183, 92185, 92187, 92194, 92196
LRB-L748510 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/04/24 13:3925085.5<85.5µg/KgArsenic
05/04/24 13:3925042.8<42.8µg/KgBarium
05/04/24 13:3925026.0<26.0µg/KgCadmium
05/04/24 13:39250116<116µg/KgChromium
05/04/24 13:3925031.0<31.0µg/KgLead
05/04/24 13:39250103<103µg/KgSelenium
05/04/24 13:392506.74<6.74µg/KgSilver
LCS-L748510Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.024002500µg/KgArsenic 80-120
96.047805000µg/KgBarium 80-120
92.0459500µg/KgCadmium 80-120
98.049205000µg/KgChromium 80-120
90.022502500µg/KgLead 80-120
91.045305000µg/KgSelenium 80-120
93.0463500µg/KgSilver 80-120
V 92252-MS-L748510 V 92252-MSD-L748510Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2210 77.0261023202350397µg/KgArsenic 95.0 75-125 16.5 80.0
7310 92.06950465047102970µg/KgBarium 86.0 75-125 5.0 80.0
396 84.0392465471< 26.0µg/KgCadmium 84.0 75-125 1.0 80.0
10800 10911900465047105650µg/KgChromium 135*75-125 9.6 80.0
Page 5 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 113 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Metals Analyses
6020B
L748699QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L748510
V 92252-MS-L748510 V 92252-MSD-L748510Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
4840 82.04770232023502900µg/KgLead 80.0 75-125 1.4 80.0
3390 72.0*345046504710< 103µg/KgSelenium 74.0*75-125 1.7 80.0
V 92252-PDS-L748510Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/04/24 16:0287.01090µg/KgArsenic
05/04/24 16:0290.02430µg/KgBarium
05/04/24 16:0284.0203µg/KgCadmium
05/04/24 16:0289.02660µg/KgChromium
05/04/24 16:0288.01310µg/KgLead
05/04/24 16:0287.02090µg/KgSelenium
Page 6 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 114 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
V46711QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:V46690
Associated Lab Samples: 92190, 92191, 92192, 92193
LRB-V46690 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/01/24 16:110.000200.00007<0.00007mg/LMercury (Total)
LCS-V46690Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1060.004950.00468mg/LMercury (Total)80-120
V 92190-MS-V46690 V 92190-MSD-V46690Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00441 94.00.004520.004680.00468< 0.00007mg/LMercury (Total)96.0 80-120 2.4 20.0
V 92190-PDS-V46690Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/01/24 16:4394.00.00220mg/LMercury (Total)
Page 7 of 52Date:05/09/2024 02:05 PM
Page 115 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V46808QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V46746
Associated Lab Samples: 92181, 92183, 92185, 92187, 92194, 92196
LRB-V46746 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/03/24 12:030.03000.0120<0.0120mg/KgMercury (Total)
LCS-V46746Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1050.4360.417mg/KgMercury (Total)80-120
V 92111-MS-V46746 V 92111-MSD-V46746Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.459 1010.5370.4100.4170.0380mg/KgMercury (Total)122*80-120 15.6 20.0
V 92111-PDS-V46746Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/03/24 12:1699.00.216mg/KgMercury (Total)
Page 8 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 116 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46655QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46653
Associated Lab Samples: 92180, 92182, 92186, 92188, 92195
LRB-V46653 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/29/24 11:100.0200.002<0.002mg/KgAcetone
04/29/24 11:100.0200.001<0.001mg/KgAcrolein
04/29/24 11:100.0200.0008<0.0008mg/KgAcrylonitrile
04/29/24 11:100.0050.0006<0.0006mg/KgBenzene
04/29/24 11:100.0050.0005<0.0005mg/KgBromobenzene
04/29/24 11:100.0050.0008<0.0008mg/KgBromochloromethane
04/29/24 11:100.0050.001<0.001mg/KgBromodichloromethane
04/29/24 11:100.0050.001<0.001mg/KgBromoform
04/29/24 11:100.0100.001<0.001mg/KgBromomethane
04/29/24 11:100.0050.0005<0.0005mg/Kgn-Butylbenzene
04/29/24 11:100.0050.0006<0.0006mg/Kgsec-Butyl benzene
04/29/24 11:100.0050.0005<0.0005mg/Kgtert-Butyl benzene
04/29/24 11:100.0050.0006<0.0006mg/KgCarbon Disulfide
04/29/24 11:100.0050.001<0.001mg/KgCarbon Tetrachloride
04/29/24 11:100.0050.0007<0.0007mg/KgChlorobenzene
04/29/24 11:100.0050.0009<0.0009mg/KgChlorodibromomethane
04/29/24 11:100.0100.0009<0.0009mg/KgChloroethane
04/29/24 11:100.0050.001<0.001mg/KgChloroform
04/29/24 11:100.0100.0006<0.0006mg/KgChloromethane
04/29/24 11:100.0050.0005<0.0005mg/Kg2-Chlorotoluene
04/29/24 11:100.0050.0004<0.0004mg/Kg4-Chlorotoluene
04/29/24 11:100.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
04/29/24 11:100.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
04/29/24 11:100.0050.0006<0.0006mg/Kg1,2-Dibromoethane
04/29/24 11:100.0050.0006<0.0006mg/KgDibromomethane
04/29/24 11:100.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
04/29/24 11:100.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 9 of 52Date:05/09/2024 02:05 PM
Page 117 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46655QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46653
Associated Lab Samples: 92180, 92182, 92186, 92188, 92195
LRB-V46653 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/29/24 11:100.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
04/29/24 11:100.0100.001<0.001mg/KgDichlorodifluoromethane
04/29/24 11:100.0050.0008<0.0008mg/Kg1,1-Dichloroethane
04/29/24 11:100.0050.001<0.001mg/Kg1,2-Dichloroethane
04/29/24 11:100.0050.0007<0.0007mg/Kg1,1-Dichloroethene
04/29/24 11:100.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
04/29/24 11:100.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
04/29/24 11:100.0050.0004<0.0004mg/Kg1,2-Dichloropropane
04/29/24 11:100.0050.0006<0.0006mg/Kg1,3-Dichloropropane
04/29/24 11:100.0050.001<0.001mg/Kg2,2-Dichloropropane
04/29/24 11:100.0050.0008<0.0008mg/Kg1,1-Dichloropropene
04/29/24 11:100.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
04/29/24 11:100.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
04/29/24 11:100.0050.0006<0.0006mg/KgEthylbenzene
04/29/24 11:100.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
04/29/24 11:100.0100.0008<0.0008mg/KgHexachlorobutadiene
04/29/24 11:100.0100.0007<0.0007mg/Kgn-Hexane
04/29/24 11:100.0200.0006<0.0006mg/Kg2-Hexanone
04/29/24 11:100.0050.0005<0.0005mg/KgIsopropylbenzene
04/29/24 11:100.0050.001<0.001mg/Kg4-Isopropyl toluene
04/29/24 11:100.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
04/29/24 11:100.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
04/29/24 11:100.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
04/29/24 11:100.0100.001<0.001mg/KgMethylene Chloride
04/29/24 11:100.0100.0010<0.0010mg/KgNaphthalene
04/29/24 11:100.0050.0005<0.0005mg/Kgn-Propylbenzene
04/29/24 11:100.0050.001<0.001mg/KgStyrene
Page 10 of 52Date:05/09/2024 02:05 PM
Page 118 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46655QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46653
Associated Lab Samples: 92180, 92182, 92186, 92188, 92195
LRB-V46653 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/29/24 11:100.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
04/29/24 11:100.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
04/29/24 11:100.0050.0009<0.0009mg/KgTetrachloroethene
04/29/24 11:100.0050.0007<0.0007mg/KgToluene
04/29/24 11:100.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
04/29/24 11:100.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
04/29/24 11:100.0050.001<0.001mg/Kg1,1,1-Trichloroethane
04/29/24 11:100.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
04/29/24 11:100.0050.0009<0.0009mg/KgTrichloroethene
04/29/24 11:100.0100.002<0.002mg/KgTrichlorofluoromethane
04/29/24 11:100.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
04/29/24 11:100.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
04/29/24 11:100.0100.0005<0.0005mg/KgVinyl Acetate
04/29/24 11:100.0100.0005<0.0005mg/KgVinyl Chloride
04/29/24 11:100.0050.0005<0.0005mg/Kgo-Xylene
04/29/24 11:100.0100.001<0.001mg/Kgm,p-Xylene
04/29/24 11:104-Bromofluorobenzene (S)94.8 70-130
04/29/24 11:10Dibromofluoromethane (S)105 84-123
04/29/24 11:10Toluene-d8 (S)109 76-129
LCS-V46653 LCSD-V46653Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.087 87.583.10.0830.100mg/KgAcetone 29-198 5.1 20
0.105 10599.10.0990.100mg/KgAcrolein 70-130 5.7 20
0.092 92.31020.1020.100mg/KgAcrylonitrile 65-134 9.9 20
Page 11 of 52Date:05/09/2024 02:05 PM
Page 119 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46655QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46653
LCS-V46653 LCSD-V46653Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 97.885.00.0420.050mg/KgBenzene 74-127 14.0 20
0.052 10589.60.0440.050mg/KgBromobenzene 73-125 16.2 20
0.050 10198.40.0490.050mg/KgBromochloromethane 72-134 3.0 20
0.050 10196.80.0480.050mg/KgBromodichloromethane 75-122 4.6 20
0.048 96.681.20.0400.050mg/KgBromoform 66-135 17.3 20
0.044 88.094.40.0470.050mg/KgBromomethane 20-180 7.0 20
0.055 1121160.0580.050mg/Kgn-Butylbenzene 65-135 3.6 20
0.050 10297.00.0480.050mg/Kgsec-Butyl benzene 66-131 4.6 20
0.048 97.093.40.0460.050mg/Kgtert-Butyl benzene 67-132 3.7 20
0.046 93.894.00.0470.050mg/KgCarbon Disulfide 61-129 0.2 20
0.047 94.897.00.0480.050mg/KgCarbon Tetrachloride 64-143 2.2 20
0.047 94.697.60.0480.050mg/KgChlorobenzene 74-118 3.1 20
0.050 10293.80.0460.050mg/KgChlorodibromomethane 73-122 8.1 20
0.050 1011040.0510.050mg/KgChloroethane 33-149 3.1 20
0.050 1011000.0500.050mg/KgChloroform 73-127 1.3 20
0.031 63.666.60.0330.050mg/KgChloromethane 45-143 4.6 20
0.051 10290.80.0450.050mg/Kg2-Chlorotoluene 67-124 11.8 20
0.051 10290.80.0450.050mg/Kg4-Chlorotoluene 71-126 11.8 20
0.049 99.287.60.0430.050mg/KgDi-Isopropyl Ether (DIPE)59-159 12.4 20
0.047 95.81050.0520.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 8.7 20
0.051 1031020.0510.050mg/Kg1,2-Dibromoethane 70-132 0.5 20
0.051 10299.80.0490.050mg/KgDibromomethane 74-133 2.3 20
0.050 1011100.0540.050mg/Kg1,2-Dichlorobenzene 72-123 8.3 20
0.049 99.899.60.0490.050mg/Kg1,3-Dichlorobenzene 71-120 0.2 20
0.047 95.493.20.0460.050mg/Kg1,4-Dichlorobenzene 71-123 2.3 20
0.035 71.272.00.0360.050mg/KgDichlorodifluoromethane 26-146 1.1 20
Page 12 of 52Date:05/09/2024 02:05 PM
Page 120 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46655QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46653
LCS-V46653 LCSD-V46653Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 88.21000.0500.050mg/Kg1,1-Dichloroethane 74-127 12.5 20
0.047 94.692.60.0460.050mg/Kg1,2-Dichloroethane 68-128 2.1 20
0.046 92.293.80.0460.050mg/Kg1,1-Dichloroethene 67-149 1.7 20
0.051 10498.60.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 5.1 20
0.047 94.693.00.0460.050mg/Kgtrans-1,2-Dichloroethene 73-132 1.7 20
0.049 99.697.40.0480.050mg/Kg1,2-Dichloropropane 73-130 2.2 20
0.054 1091010.0500.050mg/Kg1,3-Dichloropropane 75-124 7.4 20
0.050 10099.60.0490.050mg/Kg2,2-Dichloropropane 50-142 0.4 20
0.049 98.61020.0510.050mg/Kg1,1-Dichloropropene 71-130 3.7 20
0.054 10899.40.0490.050mg/Kgcis-1,3-Dichloropropene 71-125 8.6 20
0.053 1071030.0510.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.2 20
0.047 95.899.40.0490.050mg/KgEthylbenzene 74-128 3.6 20
0.089 89.497.40.0970.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 8.5 20
0.045 91.494.20.0470.050mg/KgHexachlorobutadiene 64-125 3.0 20
0.051 10298.20.0490.050mg/Kgn-Hexane 70-130 4.1 20
0.045 91.484.80.0420.050mg/Kg2-Hexanone 61-157 7.4 20
0.048 96.692.20.0460.050mg/KgIsopropylbenzene 68-126 4.6 20
0.050 1001020.0500.050mg/Kg4-Isopropyl toluene 68-129 1.1 20
0.039 79.679.00.0390.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.7 20
0.047 95.491.60.0450.050mg/KgMethyl tert-butyl ether (MTBE)70-130 4.0 20
0.043 86.488.60.0440.050mg/Kg4-Methyl-2-Pentanone 57-162 2.5 20
0.042 84.882.80.0410.050mg/KgMethylene Chloride 74-129 2.3 20
0.057 1161070.0530.050mg/KgNaphthalene 57-157 7.5 20
0.052 10591.20.0450.050mg/Kgn-Propylbenzene 67-130 14.4 20
0.052 10585.40.0420.050mg/KgStyrene 77-121 20.3*20
0.047 95.094.60.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.4 20
Page 13 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 121 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46655QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46653
LCS-V46653 LCSD-V46653Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.053 10687.60.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 19.1 20
0.047 95.697.60.0480.050mg/KgTetrachloroethene 68-130 2.0 20
0.052 10699.40.0490.050mg/KgToluene 71-129 6.2 20
0.052 10597.60.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 6.9 20
0.052 1051030.0510.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.3 20
0.046 93.895.60.0470.050mg/Kg1,1,1-Trichloroethane 67-131 1.9 20
0.054 10996.80.0480.050mg/Kg1,1,2-Trichloroethane 70-133 11.6 20
0.046 93.694.40.0470.050mg/KgTrichloroethene 75-133 0.8 20
0.045 91.086.20.0430.050mg/KgTrichlorofluoromethane 44-146 5.4 20
0.049 99.687.80.0430.050mg/Kg1,2,3-Trichloropropane 60-137 12.5 20
0.051 10393.80.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 8.9 20
0.058 1161270.0630.050mg/KgVinyl Acetate 60-140 8.5 20
0.046 92.490.00.0450.050mg/KgVinyl Chloride 48-147 2.6 20
0.051 10291.00.0450.050mg/Kgo-Xylene 74-126 11.5 20
0.098 98.01010.1010.100mg/Kgm,p-Xylene 75-124 3.0 20
99.091.64-Bromofluorobenzene (S)70-130
99.098.8Dibromofluoromethane (S)84-123
116105Toluene-d8 (S)76-129
Page 14 of 52Date:05/09/2024 02:05 PM
Page 122 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46718QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46717
Associated Lab Samples: 92184
LRB-V46717 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/24 13:350.0200.002<0.002mg/KgAcetone
04/30/24 13:350.0200.001<0.001mg/KgAcrolein
04/30/24 13:350.0200.0008<0.0008mg/KgAcrylonitrile
04/30/24 13:350.0050.0006<0.0006mg/KgBenzene
04/30/24 13:350.0050.0005<0.0005mg/KgBromobenzene
04/30/24 13:350.0050.0008<0.0008mg/KgBromochloromethane
04/30/24 13:350.0050.001<0.001mg/KgBromodichloromethane
04/30/24 13:350.0050.001<0.001mg/KgBromoform
04/30/24 13:350.0100.001<0.001mg/KgBromomethane
04/30/24 13:350.0050.0005<0.0005mg/Kgn-Butylbenzene
04/30/24 13:350.0050.0006<0.0006mg/Kgsec-Butyl benzene
04/30/24 13:350.0050.0005<0.0005mg/Kgtert-Butyl benzene
04/30/24 13:350.0050.0006<0.0006mg/KgCarbon Disulfide
04/30/24 13:350.0050.001<0.001mg/KgCarbon Tetrachloride
04/30/24 13:350.0050.0007<0.0007mg/KgChlorobenzene
04/30/24 13:350.0050.0009<0.0009mg/KgChlorodibromomethane
04/30/24 13:350.0100.0009<0.0009mg/KgChloroethane
04/30/24 13:350.0050.001<0.001mg/KgChloroform
04/30/24 13:350.0100.0006<0.0006mg/KgChloromethane
04/30/24 13:350.0050.0005<0.0005mg/Kg2-Chlorotoluene
04/30/24 13:350.0050.0004<0.0004mg/Kg4-Chlorotoluene
04/30/24 13:350.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
04/30/24 13:350.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
04/30/24 13:350.0050.0006<0.0006mg/Kg1,2-Dibromoethane
04/30/24 13:350.0050.0006<0.0006mg/KgDibromomethane
04/30/24 13:350.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
04/30/24 13:350.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 15 of 52Date:05/09/2024 02:05 PM
Page 123 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46718QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46717
Associated Lab Samples: 92184
LRB-V46717 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/24 13:350.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
04/30/24 13:350.0100.001<0.001mg/KgDichlorodifluoromethane
04/30/24 13:350.0050.0008<0.0008mg/Kg1,1-Dichloroethane
04/30/24 13:350.0050.001<0.001mg/Kg1,2-Dichloroethane
04/30/24 13:350.0050.0007<0.0007mg/Kg1,1-Dichloroethene
04/30/24 13:350.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
04/30/24 13:350.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
04/30/24 13:350.0050.0004<0.0004mg/Kg1,2-Dichloropropane
04/30/24 13:350.0050.0006<0.0006mg/Kg1,3-Dichloropropane
04/30/24 13:350.0050.001<0.001mg/Kg2,2-Dichloropropane
04/30/24 13:350.0050.0008<0.0008mg/Kg1,1-Dichloropropene
04/30/24 13:350.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
04/30/24 13:350.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
04/30/24 13:350.0050.0006<0.0006mg/KgEthylbenzene
04/30/24 13:350.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
04/30/24 13:350.0100.0008<0.0008mg/KgHexachlorobutadiene
04/30/24 13:350.0100.0007<0.0007mg/Kgn-Hexane
04/30/24 13:350.0200.0006<0.0006mg/Kg2-Hexanone
04/30/24 13:350.0050.0005<0.0005mg/KgIsopropylbenzene
04/30/24 13:350.0050.001<0.001mg/Kg4-Isopropyl toluene
04/30/24 13:350.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
04/30/24 13:350.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
04/30/24 13:350.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
04/30/24 13:350.0100.001<0.001mg/KgMethylene Chloride
04/30/24 13:350.0100.0010<0.0010mg/KgNaphthalene
04/30/24 13:350.0050.0005<0.0005mg/Kgn-Propylbenzene
04/30/24 13:350.0050.001<0.001mg/KgStyrene
Page 16 of 52Date:05/09/2024 02:05 PM
Page 124 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46718QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46717
Associated Lab Samples: 92184
LRB-V46717 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/24 13:350.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
04/30/24 13:350.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
04/30/24 13:350.0050.0009<0.0009mg/KgTetrachloroethene
04/30/24 13:350.0050.0007<0.0007mg/KgToluene
04/30/24 13:350.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
04/30/24 13:350.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
04/30/24 13:350.0050.001<0.001mg/Kg1,1,1-Trichloroethane
04/30/24 13:350.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
04/30/24 13:350.0050.0009<0.0009mg/KgTrichloroethene
04/30/24 13:350.0100.002<0.002mg/KgTrichlorofluoromethane
04/30/24 13:350.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
04/30/24 13:350.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
04/30/24 13:350.0100.0005<0.0005mg/KgVinyl Acetate
04/30/24 13:350.0100.0005<0.0005mg/KgVinyl Chloride
04/30/24 13:350.0050.0005<0.0005mg/Kgo-Xylene
04/30/24 13:350.0100.001<0.001mg/Kgm,p-Xylene
04/30/24 13:354-Bromofluorobenzene (S)104 70-130
04/30/24 13:35Dibromofluoromethane (S)98.2 84-123
04/30/24 13:35Toluene-d8 (S)96.2 76-129
LCS-V46717 LCSD-V46717Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.085 85.086.80.0860.100mg/KgAcetone 29-198 2.0 20
0.106 1061110.1110.100mg/KgAcrolein 70-130 4.6 20
0.097 97.21040.1040.100mg/KgAcrylonitrile 65-134 6.7 20
Page 17 of 52Date:05/09/2024 02:05 PM
Page 125 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46718QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46717
LCS-V46717 LCSD-V46717Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.038 77.080.60.0400.050mg/KgBenzene 74-127 4.5 20
0.038 76.477.60.0380.050mg/KgBromobenzene 73-125 1.5 20
0.045 90.892.40.0460.050mg/KgBromochloromethane 72-134 1.7 20
0.043 87.488.80.0440.050mg/KgBromodichloromethane 75-122 1.5 20
0.050 1001020.0510.050mg/KgBromoform 66-135 1.9 20
0.041 83.089.00.0440.050mg/KgBromomethane 20-180 6.9 20
0.042 84.687.00.0430.050mg/Kgn-Butylbenzene 65-135 2.7 20
0.038 77.881.60.0400.050mg/Kgsec-Butyl benzene 66-131 4.7 20
0.040 80.084.60.0420.050mg/Kgtert-Butyl benzene 67-132 5.5 20
0.036 72.278.80.0390.050mg/KgCarbon Disulfide 61-129 8.7 20
0.042 84.894.20.0470.050mg/KgCarbon Tetrachloride 64-143 10.5 20
0.043 86.288.80.0440.050mg/KgChlorobenzene 74-118 2.9 20
0.046 92.096.00.0480.050mg/KgChlorodibromomethane 73-122 4.2 20
0.040 81.887.80.0430.050mg/KgChloroethane 33-149 7.0 20
0.041 82.287.00.0430.050mg/KgChloroform 73-127 5.6 20
0.036 73.680.40.0400.050mg/KgChloromethane 45-143 8.8 20
0.039 78.280.00.0400.050mg/Kg2-Chlorotoluene 67-124 2.2 20
0.039 78.279.80.0390.050mg/Kg4-Chlorotoluene 71-126 2.0 20
0.040 80.683.40.0410.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.4 20
0.046 93.897.00.0480.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.3 20
0.046 93.897.80.0480.050mg/Kg1,2-Dibromoethane 70-132 4.1 20
0.043 86.490.20.0450.050mg/KgDibromomethane 74-133 4.3 20
0.045 90.891.20.0450.050mg/Kg1,2-Dichlorobenzene 72-123 0.4 20
0.044 89.089.80.0440.050mg/Kg1,3-Dichlorobenzene 71-120 0.8 20
0.041 83.285.40.0420.050mg/Kg1,4-Dichlorobenzene 71-123 2.6 20
0.040 80.891.00.0450.050mg/KgDichlorodifluoromethane 26-146 11.8 20
Page 18 of 52Date:05/09/2024 02:05 PM
Page 126 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46718QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46717
LCS-V46717 LCSD-V46717Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.038 77.880.80.0400.050mg/Kg1,1-Dichloroethane 74-127 3.7 20
0.043 87.889.20.0440.050mg/Kg1,2-Dichloroethane 68-128 1.5 20
0.037 75.283.00.0410.050mg/Kg1,1-Dichloroethene 67-149 9.8 20
0.039 79.483.60.0410.050mg/Kgcis-1,2-Dichloroethene 76-134 5.1 20
0.038 77.885.00.0420.050mg/Kgtrans-1,2-Dichloroethene 73-132 8.8 20
0.040 80.083.60.0410.050mg/Kg1,2-Dichloropropane 73-130 4.4 20
0.043 86.287.80.0430.050mg/Kg1,3-Dichloropropane 75-124 1.8 20
0.040 80.286.40.0430.050mg/Kg2,2-Dichloropropane 50-142 7.4 20
0.037 75.281.40.0400.050mg/Kg1,1-Dichloropropene 71-130 7.9 20
0.042 85.688.40.0440.050mg/Kgcis-1,3-Dichloropropene 71-125 3.2 20
0.045 91.295.20.0470.050mg/Kgtrans-1,3-Dichloropropene 68-123 4.2 20
0.040 80.284.00.0420.050mg/KgEthylbenzene 74-128 4.6 20
0.084 84.585.50.0850.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.1 20
0.045 91.294.80.0470.050mg/KgHexachlorobutadiene 64-125 3.8 20
0.038 77.882.60.0410.050mg/Kgn-Hexane 70-130 5.9 20
0.039 79.084.80.0420.050mg/Kg2-Hexanone 61-157 7.0 20
0.039 78.082.00.0410.050mg/KgIsopropylbenzene 68-126 5.0 20
0.041 83.087.20.0430.050mg/Kg4-Isopropyl toluene 68-129 4.9 20
0.038 77.883.60.0410.050mg/KgMethyl Ethyl Ketone (MEK)63-149 7.1 20
0.042 85.687.00.0430.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.6 20
0.040 81.485.20.0420.050mg/Kg4-Methyl-2-Pentanone 57-162 4.5 20
0.038 76.680.40.0400.050mg/KgMethylene Chloride 74-129 4.8 20
0.047 94.897.80.0480.050mg/KgNaphthalene 57-157 3.1 20
0.037 75.879.00.0390.050mg/Kgn-Propylbenzene 67-130 4.1 20
0.044 89.291.20.0450.050mg/KgStyrene 77-121 2.2 20
0.046 92.293.00.0460.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.8 20
Page 19 of 52Date:05/09/2024 02:05 PM
Page 127 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46718QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V46717
LCS-V46717 LCSD-V46717Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.038 77.679.40.0390.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.2 20
0.045 91.098.80.0490.050mg/KgTetrachloroethene 68-130 8.2 20
0.040 80.484.40.0420.050mg/KgToluene 71-129 4.8 20
0.048 96.295.60.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.6 20
0.047 95.499.40.0490.050mg/Kg1,2,4-Trichlorobenzene 66-125 4.1 20
0.041 82.489.00.0440.050mg/Kg1,1,1-Trichloroethane 67-131 7.7 20
0.044 88.889.80.0440.050mg/Kg1,1,2-Trichloroethane 70-133 1.1 20
0.042 85.689.40.0440.050mg/KgTrichloroethene 75-133 4.3 20
0.042 84.693.00.0460.050mg/KgTrichlorofluoromethane 44-146 9.4 20
0.042 84.687.60.0430.050mg/Kg1,2,3-Trichloropropane 60-137 3.4 20
0.040 81.483.60.0410.050mg/Kg1,3,5-Trimethylbenzene 69-128 2.6 20
0.054 1081150.0570.050mg/KgVinyl Acetate 60-140 6.2 20
0.035 71.677.20.0380.050mg/KgVinyl Chloride 48-147 7.5 20
0.042 84.288.80.0440.050mg/Kgo-Xylene 74-126 5.3 20
0.083 83.688.30.0880.100mg/Kgm,p-Xylene 75-124 5.4 20
1011024-Bromofluorobenzene (S)70-130
98.498.0Dibromofluoromethane (S)84-123
98.698.8Toluene-d8 (S)76-129
Page 20 of 52Date:05/09/2024 02:05 PM
Page 128 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46953QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V46952
Associated Lab Samples: 92189, 92190, 92191, 92192, 92193
LRB-V46952 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/24 14:295.001.80<1.80µg/LAcetone
05/03/24 14:295.002.00<2.00µg/LAcrolein
05/03/24 14:295.000.230<0.230µg/LAcrylonitrile
05/03/24 14:290.5000.180<0.180µg/LBenzene
05/03/24 14:290.5000.210<0.210µg/LBromobenzene
05/03/24 14:291.000.420<0.420µg/LBromochloromethane
05/03/24 14:290.5000.160<0.160µg/LBromodichloromethane
05/03/24 14:295.001.50<1.50µg/LBromoform
05/03/24 14:291.000.280<0.280µg/LBromomethane
05/03/24 14:291.000.185<0.185µg/Ln-Butylbenzene
05/03/24 14:290.5000.200<0.200µg/Lsec-Butyl benzene
05/03/24 14:292.000.920<0.920µg/Ltert-Butyl benzene
05/03/24 14:295.000.150<0.150µg/LCarbon Disulfide
05/03/24 14:290.5000.180<0.180µg/LCarbon Tetrachloride
05/03/24 14:290.5000.190<0.190µg/LChlorobenzene
05/03/24 14:290.5000.190<0.190µg/LChlorodibromomethane
05/03/24 14:291.000.430<0.430µg/LChloroethane
05/03/24 14:290.5000.220<0.220µg/LChloroform
05/03/24 14:290.5000.220<0.220µg/LChloromethane
05/03/24 14:290.5000.200<0.200µg/L2-Chlorotoluene
05/03/24 14:290.5000.200<0.200µg/L4-Chlorotoluene
05/03/24 14:295.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
05/03/24 14:292.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
05/03/24 14:290.5000.200<0.200µg/L1,2-Dibromoethane
05/03/24 14:290.5000.230<0.230µg/LDibromomethane
05/03/24 14:290.5000.220<0.220µg/L1,2-Dichlorobenzene
05/03/24 14:290.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 21 of 52Date:05/09/2024 02:05 PM
Page 129 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46953QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V46952
Associated Lab Samples: 92189, 92190, 92191, 92192, 92193
LRB-V46952 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/24 14:290.5000.210<0.210µg/L1,4-Dichlorobenzene
05/03/24 14:295.001.20<1.20µg/LDichlorodifluoromethane
05/03/24 14:290.5000.240<0.240µg/L1,1-Dichloroethane
05/03/24 14:290.5000.150<0.150µg/L1,2-Dichloroethane
05/03/24 14:290.5000.150<0.150µg/L1,1-Dichloroethene
05/03/24 14:290.5000.200<0.200µg/Lcis-1,2-Dichloroethene
05/03/24 14:290.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
05/03/24 14:290.5000.190<0.190µg/L1,2-Dichloropropane
05/03/24 14:290.5000.130<0.130µg/L1,3-Dichloropropane
05/03/24 14:292.000.210<0.210µg/L2,2-Dichloropropane
05/03/24 14:290.5000.200<0.200µg/L1,1-Dichloropropene
05/03/24 14:290.5000.210<0.210µg/Lcis-1,3-Dichloropropene
05/03/24 14:290.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
05/03/24 14:290.5000.170<0.170µg/LEthylbenzene
05/03/24 14:2910.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
05/03/24 14:292.000.350<0.350µg/LHexachlorobutadiene
05/03/24 14:2910.01.30<1.30µg/Ln-Hexane
05/03/24 14:295.000.380<0.380µg/L2-Hexanone
05/03/24 14:295.000.180<0.180µg/LIsopropylbenzene
05/03/24 14:290.5000.089<0.089µg/L4-Isopropyl toluene
05/03/24 14:295.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
05/03/24 14:290.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
05/03/24 14:295.001.00<1.00µg/L4-Methyl-2-Pentanone
05/03/24 14:291.000.330<0.330µg/LMethylene Chloride
05/03/24 14:291.000.470<0.470µg/LNaphthalene
05/03/24 14:290.5000.190<0.190µg/Ln-Propylbenzene
05/03/24 14:290.5000.220<0.220µg/LStyrene
Page 22 of 52Date:05/09/2024 02:05 PM
Page 130 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46953QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V46952
Associated Lab Samples: 92189, 92190, 92191, 92192, 92193
LRB-V46952 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/24 14:290.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
05/03/24 14:290.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
05/03/24 14:290.5000.220<0.220µg/LTetrachloroethene
05/03/24 14:290.5000.220<0.220µg/LToluene
05/03/24 14:292.000.380<0.380µg/L1,2,3-Trichlorobenzene
05/03/24 14:291.000.310<0.310µg/L1,2,4-Trichlorobenzene
05/03/24 14:290.5000.160<0.160µg/L1,1,1-Trichloroethane
05/03/24 14:290.5000.096<0.096µg/L1,1,2-Trichloroethane
05/03/24 14:290.5000.180<0.180µg/LTrichloroethene
05/03/24 14:290.5000.180<0.180µg/LTrichlorofluoromethane
05/03/24 14:291.000.270<0.270µg/L1,2,3-Trichloropropane
05/03/24 14:290.5000.180<0.180µg/L1,3,5-Trimethylbenzene
05/03/24 14:292.001.00<1.00µg/LVinyl Acetate
05/03/24 14:290.5000.170<0.170µg/LVinyl Chloride
05/03/24 14:290.5000.210<0.210µg/Lo-Xylene
05/03/24 14:291.000.420<0.420µg/Lm,p-Xylene
05/03/24 14:294-Bromofluorobenzene (S)100 80-124
05/03/24 14:29Dibromofluoromethane (S)101 75-129
05/03/24 14:291,2-Dichloroethane - d4 (S)98.6 63-136
05/03/24 14:29Toluene-d8 (S)100 77-123
LCS-V46952 LCSD-V46952Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
38.0 95.099.239.740.0µg/LAcetone 40-166 4.3 20.0
39.9 99.710341.140.0µg/LAcrolein 70-130 2.9 20.0
Page 23 of 52Date:05/09/2024 02:05 PM
Page 131 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46953QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V46952
LCS-V46952 LCSD-V46952Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.9 10210240.640.0µg/LAcrylonitrile 81-127 0.7 20.0
20.2 10110120.220.0µg/LBenzene 77-128 0.0 20.0
20.1 10110320.620.0µg/LBromobenzene 78-129 2.4 20.0
20.2 10110220.320.0µg/LBromochloromethane 78-135 0.4 20.0
19.6 98.099.519.920.0µg/LBromodichloromethane 76-138 1.5 20.0
18.2 91.094.018.820.0µg/LBromoform 71-135 3.2 20.0
21.9 11010220.420.0µg/LBromomethane 41-168 7.0 20.0
20.0 10010120.120.0µg/Ln-Butylbenzene 68-134 0.4 20.0
20.4 10210220.420.0µg/Lsec-Butyl benzene 71-131 0.0 20.0
20.3 10210220.420.0µg/Ltert-Butyl benzene 70-132 0.4 20.0
20.3 10210220.320.0µg/LCarbon Disulfide 59-135 0.0 20.0
20.7 10410320.620.0µg/LCarbon Tetrachloride 72-142 0.4 20.0
20.3 10210020.020.0µg/LChlorobenzene 78-119 1.4 20.0
19.7 98.597.519.520.0µg/LChlorodibromomethane 75-134 1.0 20.0
25.9 13012324.620.0µg/LChloroethane 57-142 5.1 20.0
20.3 10210320.520.0µg/LChloroform 77-130 0.9 20.0
21.0 10510621.220.0µg/LChloromethane 47-145 0.9 20.0
20.1 10110220.420.0µg/L2-Chlorotoluene 74-126 1.4 20.0
20.7 10410520.920.0µg/L4-Chlorotoluene 78-129 0.9 20.0
20.6 10310521.020.0µg/LDi-Isopropyl Ether (DIPE)60-154 1.9 20.0
21.5 10810821.620.0µg/L1,2-Dibromo-3-Chloropropane 63-134 0.4 20.0
20.5 10310120.120.0µg/L1,2-Dibromoethane 77-135 1.9 20.0
19.8 99.010020.020.0µg/LDibromomethane 76-138 1.0 20.0
20.3 10210220.320.0µg/L1,2-Dichlorobenzene 78-128 0.0 20.0
20.6 10310420.820.0µg/L1,3-Dichlorobenzene 77-125 0.9 20.0
20.5 10310120.220.0µg/L1,4-Dichlorobenzene 75-126 1.4 20.0
Page 24 of 52Date:05/09/2024 02:05 PM
Page 132 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46953QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V46952
LCS-V46952 LCSD-V46952Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
28.0 14013927.720.0µg/LDichlorodifluoromethane 28-163 1.0 20.0
20.4 10210020.020.0µg/L1,1-Dichloroethane 70-130 1.9 20.0
19.0 95.094.518.920.0µg/L1,2-Dichloroethane 68-131 0.5 20.0
20.0 10010020.020.0µg/L1,1-Dichloroethene 70-154 0.0 20.0
19.6 98.099.019.820.0µg/Lcis-1,2-Dichloroethene 76-141 1.0 20.0
19.7 98.510220.420.0µg/Ltrans-1,2-Dichloroethene 76-135 3.4 20.0
20.4 10210120.220.0µg/L1,2-Dichloropropane 77-130 0.9 20.0
19.1 95.597.519.520.0µg/L1,3-Dichloropropane 76-132 2.0 20.0
19.8 99.010120.220.0µg/L2,2-Dichloropropane 29-149 2.0 20.0
20.4 10210320.620.0µg/L1,1-Dichloropropene 71-136 0.9 20.0
19.5 97.598.019.620.0µg/Lcis-1,3-Dichloropropene 65-140 0.5 20.0
19.3 96.599.519.920.0µg/Ltrans-1,3-Dichloropropene 67-140 3.0 20.0
19.3 96.595.519.120.0µg/LEthylbenzene 80-127 1.0 20.0
41.8 10510541.940.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 0.2 20.0
21.3 10710621.220.0µg/LHexachlorobutadiene 61-134 0.4 20.0
18.8 94.099.519.920.0µg/Ln-Hexane 70-130 5.6 20.0
19.6 98.010220.420.0µg/L2-Hexanone 64-137 4.0 20.0
20.4 10210320.620.0µg/LIsopropylbenzene 70-130 0.9 20.0
20.0 10010120.220.0µg/L4-Isopropyl toluene 69-132 0.9 20.0
19.7 98.597.519.520.0µg/LMethyl Ethyl Ketone (MEK)71-134 1.0 20.0
19.9 99.510220.420.0µg/LMethyl tert-butyl ether (MTBE)68-135 2.4 20.0
19.2 96.097.019.420.0µg/L4-Methyl-2-Pentanone 69-134 1.0 20.0
19.2 96.096.019.220.0µg/LMethylene Chloride 73-131 0.0 20.0
19.6 98.099.019.820.0µg/LNaphthalene 64-136 1.0 20.0
20.2 10110320.520.0µg/Ln-Propylbenzene 72-132 1.4 20.0
19.7 98.597.519.520.0µg/LStyrene 78-129 1.0 20.0
Page 25 of 52Date:05/09/2024 02:05 PM
Page 133 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V46953QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V46952
LCS-V46952 LCSD-V46952Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.4 97.098.019.620.0µg/L1,1,1,2-Tetrachloroethane 79-134 1.0 20.0
19.7 98.510120.120.0µg/L1,1,2,2-Tetrachloroethane 62-127 2.0 20.0
19.8 99.010120.120.0µg/LTetrachloroethene 80-129 1.5 20.0
19.6 98.099.519.920.0µg/LToluene 76-131 1.5 20.0
21.3 10710420.820.0µg/L1,2,3-Trichlorobenzene 58-144 2.3 20.0
20.8 10410521.020.0µg/L1,2,4-Trichlorobenzene 66-139 0.9 20.0
19.2 96.097.519.520.0µg/L1,1,1-Trichloroethane 75-135 1.5 20.0
19.5 97.598.019.620.0µg/L1,1,2-Trichloroethane 70-140 0.5 20.0
20.3 10210120.120.0µg/LTrichloroethene 77-133 0.9 20.0
21.7 10911422.720.0µg/LTrichlorofluoromethane 62-148 4.5 20.0
19.1 95.599.519.920.0µg/L1,2,3-Trichloropropane 71-127 4.1 20.0
19.9 99.599.519.920.0µg/L1,3,5-Trimethylbenzene 75-131 0.0 20.0
22.2 11110520.920.0µg/LVinyl Acetate 34-167 6.0 20.0
23.1 11611222.320.0µg/LVinyl Chloride 57-141 3.5 20.0
19.9 99.510120.120.0µg/Lo-Xylene 78-128 1.0 20.0
40.9 10210240.740.0µg/Lm,p-Xylene 77-133 0.4 20.0
99.898.64-Bromofluorobenzene (S)80-124
100100Dibromofluoromethane (S)75-129
98.299.01,2-Dichloroethane - d4 (S)63-136
99.698.8Toluene-d8 (S)77-123
Page 26 of 52Date:05/09/2024 02:05 PM
Page 134 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46675QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V46634
Associated Lab Samples: 92190, 92191, 92192, 92193
LRB-V46634 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/24 16:462.000.302<0.302µg/LAcenaphthene
04/30/24 16:462.000.297<0.297µg/LAcenaphthylene
04/30/24 16:465.002.05<2.05µg/LAniline
04/30/24 16:462.000.836<0.836µg/LAnthracene
04/30/24 16:462.000.637<0.637µg/LBenzo(a)anthracene
04/30/24 16:462.001.02<1.02µg/LBenzo(a)pyrene
04/30/24 16:465.002.49<2.49µg/LBenzo(b)fluoranthene
04/30/24 16:465.001.01<1.01µg/LBenzo(g,h,i)perylene
04/30/24 16:465.001.99<1.99µg/LBenzo(k)fluoranthene
04/30/24 16:4610.01.10<1.10µg/LBenzoic Acid
04/30/24 16:465.000.684<0.684µg/LBenzyl alcohol
04/30/24 16:465.000.468<0.468µg/LBis(2-Chloroethoxy)methane
04/30/24 16:465.001.04<1.04µg/LBis(2-Chloroethyl)ether
04/30/24 16:465.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
04/30/24 16:4610.03.46<3.46µg/LBis(2-ethylhexyl)phthalate
04/30/24 16:465.001.11<1.11µg/L4-Bromophenyl phenyl ether
04/30/24 16:465.001.83<1.83µg/LButyl benzyl phthalate
04/30/24 16:465.001.18<1.18µg/L4-Chloro-3-methylphenol
04/30/24 16:465.001.33<1.33µg/L4-Chloroaniline
04/30/24 16:4620.01.83<1.83µg/L2-Chloronaphthalene
04/30/24 16:4610.00.938<0.938µg/L2-Chlorophenol
04/30/24 16:465.001.71<1.71µg/L4-Chlorophenyl phenyl ether
04/30/24 16:462.000.405<0.405µg/LChrysene
04/30/24 16:462.000.434<0.434µg/LDibenz(a,h)anthracene
04/30/24 16:465.000.856<0.856µg/LDibenzofuran
04/30/24 16:465.002.00<2.00µg/L1,2-Dichlorobenzene
04/30/24 16:465.002.00<2.00µg/L1,3-Dichlorobenzene
Page 27 of 52Date:05/09/2024 02:05 PM
Page 135 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46675QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V46634
Associated Lab Samples: 92190, 92191, 92192, 92193
LRB-V46634 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/24 16:465.002.05<2.05µg/L1,4-Dichlorobenzene
04/30/24 16:465.001.89<1.89µg/L3,3'-Dichlorobenzidine
04/30/24 16:4610.01.46<1.46µg/L2,4-Dichlorophenol
04/30/24 16:465.000.745<0.745µg/LDiethyl phthalate
04/30/24 16:465.000.939<0.939µg/LDimethyl phthalate
04/30/24 16:4620.01.57<1.57µg/L2,4-Dimethylphenol
04/30/24 16:465.002.06<2.06µg/LDi-n-butyl phthalate
04/30/24 16:4610.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
04/30/24 16:4610.01.92<1.92µg/L2,4-Dinitrophenol
04/30/24 16:465.001.11<1.11µg/L2,4-Dinitrotoluene
04/30/24 16:465.000.809<0.809µg/L2,6-Dinitrotoluene
04/30/24 16:465.001.65<1.65µg/LDi-n-Octyl Phthalate
04/30/24 16:462.000.250<0.250µg/LFluoranthene
04/30/24 16:462.000.807<0.807µg/LFluorene
04/30/24 16:465.000.979<0.979µg/LHexachlorobenzene
04/30/24 16:465.002.73<2.73µg/LHexachlorobutadiene
04/30/24 16:465.001.76<1.76µg/LHexachloroethane
04/30/24 16:462.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
04/30/24 16:465.000.444<0.444µg/LIsophorone
04/30/24 16:462.001.14<1.14µg/L1-Methylnaphthalene
04/30/24 16:462.000.666<0.666µg/L2-Methylnaphthalene
04/30/24 16:465.001.15<1.15µg/L2-Methylphenol
04/30/24 16:4610.00.880<0.880µg/L3&4 Methylphenol
04/30/24 16:462.000.728<0.728µg/LNaphthalene
04/30/24 16:465.001.39<1.39µg/L2-Nitroaniline
04/30/24 16:465.001.39<1.39µg/L3-Nitroaniline
04/30/24 16:465.001.53<1.53µg/L4-Nitroaniline
Page 28 of 52Date:05/09/2024 02:05 PM
Page 136 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46675QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V46634
Associated Lab Samples: 92190, 92191, 92192, 92193
LRB-V46634 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/24 16:465.000.905<0.905µg/LNitrobenzene
04/30/24 16:465.000.493<0.493µg/L2-Nitrophenol
04/30/24 16:4610.01.23<1.23µg/L4-Nitrophenol
04/30/24 16:465.000.450<0.450µg/LN-Nitrosodimethylamine
04/30/24 16:465.001.10<1.10µg/LN-Nitrosodiphenylamine
04/30/24 16:465.000.641<0.641µg/LN-Nitroso-di-n-propylamine
04/30/24 16:465.001.43<1.43µg/LPentachlorophenol
04/30/24 16:462.000.428<0.428µg/LPhenanthrene
04/30/24 16:465.000.651<0.651µg/LPhenol
04/30/24 16:462.000.434<0.434µg/LPyrene
04/30/24 16:465.001.20<1.20µg/LPyridine
04/30/24 16:465.002.21<2.21µg/L1,2,4-Trichlorobenzene
04/30/24 16:465.001.31<1.31µg/L2,4,5-Trichlorophenol
04/30/24 16:465.001.32<1.32µg/L2,4,6-Trichlorophenol
04/30/24 16:462-Fluorobiphenyl (S)72.2 44-119
04/30/24 16:462-Fluorophenol (S)43.0 19-119
04/30/24 16:46Nitrobenzene-d5 (S)73.0 44-120
04/30/24 16:464-Terphenyl-d14 (S)84.0 50-134
04/30/24 16:462,4,6-Tribromophenol (S)66.8 43-140
04/30/24 16:46Phenol-d5 (S)30.6 11-100
LCS-V46634 LCSD-V46634Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.3 64.671.435.750.0µg/LAcenaphthene 38-117 10.0 20.0
34.8 69.675.837.950.0µg/LAcenaphthylene 41-130 8.5 20.0
Page 29 of 52Date:05/09/2024 02:05 PM
Page 137 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46675QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V46634
LCS-V46634 LCSD-V46634Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
59.6 11913366.750.0µg/LAniline 12-197 11.2 20.0
42.2 84.488.044.050.0µg/LAnthracene 57-123 4.1 20.0
42.9 85.881.440.750.0µg/LBenzo(a)anthracene 58-125 5.2 20.0
49.6 99.210150.350.0µg/LBenzo(a)pyrene 54-128 1.4 20.0
46.9 93.898.249.150.0µg/LBenzo(b)fluoranthene 53-131 4.5 20.0
42.2 84.492.646.350.0µg/LBenzo(g,h,i)perylene 50-134 9.2 20.0
37.1 74.279.639.850.0µg/LBenzo(k)fluoranthene 53-131 7.0 20.0
31.6 63.260.230.150.0µg/LBenzoic Acid 10-125 4.8 20.0
38.9 77.877.238.650.0µg/LBenzyl alcohol 31-112 0.7 20.0
36.1 72.275.837.950.0µg/LBis(2-Chloroethoxy)methane 48-120 4.8 20.0
29.9 59.863.431.750.0µg/LBis(2-Chloroethyl)ether 43-118 5.8 20.0
30.0 60.063.831.950.0µg/LBis(2-Chloroisopropyl)ether 37-130 6.1 20.0
47.2 94.495.047.550.0µg/LBis(2-ethylhexyl)phthalate 55-135 0.6 20.0
34.7 69.476.038.050.0µg/L4-Bromophenyl phenyl ether 55-124 9.0 20.0
47.8 95.693.046.550.0µg/LButyl benzyl phthalate 53-134 2.7 20.0
42.4 84.885.242.650.0µg/L4-Chloro-3-methylphenol 52-119 0.4 20.0
46.3 92.692.646.350.0µg/L4-Chloroaniline 33-117 0.0 20.0
29.7 59.463.231.650.0µg/L2-Chloronaphthalene 40-116 6.1 20.0
34.1 68.270.435.250.0µg/L2-Chlorophenol 38-117 3.1 20.0
31.4 62.867.033.550.0µg/L4-Chlorophenyl phenyl ether 53-121 6.4 20.0
40.5 81.090.645.350.0µg/LChrysene 59-123 11.1 20.0
34.4 68.810251.150.0µg/LDibenz(a,h)anthracene 51-134 39.0*20.0
34.6 69.276.238.150.0µg/LDibenzofuran 53-118 9.6 20.0
25.3 50.647.823.950.0µg/L1,2-Dichlorobenzene 32-111 5.6 20.0
23.7 47.445.822.950.0µg/L1,3-Dichlorobenzene 28-110 3.4 20.0
22.3 44.643.221.650.0µg/L1,4-Dichlorobenzene 29-112 3.1 20.0
Page 30 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 138 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46675QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V46634
LCS-V46634 LCSD-V46634Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.4 74.877.638.850.0µg/L3,3'-Dichlorobenzidine 27-129 3.6 20.0
39.1 78.281.640.850.0µg/L2,4-Dichlorophenol 47-121 4.2 20.0
41.6 83.287.843.950.0µg/LDiethyl phthalate 56-125 5.3 20.0
41.6 83.288.244.150.0µg/LDimethyl phthalate 45-127 5.8 20.0
55.1 11011456.850.0µg/L2,4-Dimethylphenol 31-124 3.0 20.0
43.5 87.086.643.350.0µg/LDi-n-butyl phthalate 59-127 0.4 20.0
43.2 86.482.441.250.0µg/L4,6-Dinitro-2-methylphenol 44-137 4.7 20.0
46.7 93.491.645.850.0µg/L2,4-Dinitrophenol 23-143 1.9 20.0
40.2 80.484.442.250.0µg/L2,4-Dinitrotoluene 57-128 4.8 20.0
47.3 94.610150.450.0µg/L2,6-Dinitrotoluene 57-124 6.3 20.0
49.6 99.298.849.450.0µg/LDi-n-Octyl Phthalate 51-140 0.4 20.0
41.5 83.084.442.250.0µg/LFluoranthene 57-128 1.6 20.0
37.0 74.078.439.250.0µg/LFluorene 52-124 5.7 20.0
36.7 73.479.639.850.0µg/LHexachlorobenzene 53-125 8.1 20.0
28.6 57.253.826.950.0µg/LHexachlorobutadiene 22-124 6.1 20.0
22.2 44.443.421.750.0µg/LHexachloroethane 21-115 2.2 20.0
44.4 88.883.841.950.0µg/LIndeno(1,2,3-cd)pyrene 52-134 5.7 20.0
31.6 63.267.233.650.0µg/LIsophorone 42-124 6.1 20.0
29.6 59.260.830.450.0µg/L1-Methylnaphthalene 41-119 2.6 20.0
29.9 59.860.830.450.0µg/L2-Methylnaphthalene 40-121 1.6 20.0
33.9 67.867.033.550.0µg/L2-Methylphenol 30-117 1.1 20.0
27.9 55.855.427.750.0µg/L3&4 Methylphenol 29-110 0.7 20.0
28.1 56.256.428.250.0µg/LNaphthalene 40-121 0.3 20.0
39.6 79.281.240.650.0µg/L2-Nitroaniline 55-127 2.4 20.0
46.4 92.891.445.750.0µg/L3-Nitroaniline 41-128 1.5 20.0
45.5 91.093.846.950.0µg/L4-Nitroaniline 45-135 3.0 20.0
Page 31 of 52Date:05/09/2024 02:05 PM
Page 139 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46675QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V46634
LCS-V46634 LCSD-V46634Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
33.1 66.268.234.150.0µg/LNitrobenzene 45-121 2.9 20.0
34.3 68.672.036.050.0µg/L2-Nitrophenol 47-123 4.8 20.0
19.8 39.640.220.150.0µg/L4-Nitrophenol 10-105 1.5 20.0
22.0 44.045.422.750.0µg/LN-Nitrosodimethylamine 10-119 3.1 20.0
50.3 10110552.650.0µg/LN-Nitrosodiphenylamine 51-123 4.4 20.0
38.6 77.281.840.950.0µg/LN-Nitroso-di-n-propylamine 49-119 5.7 20.0
44.6 89.289.244.650.0µg/LPentachlorophenol 35-138 0.0 20.0
40.5 81.084.842.450.0µg/LPhenanthrene 59-120 4.5 20.0
17.7 35.432.816.450.0µg/LPhenol 12-58 7.6 20.0
41.5 83.087.243.650.0µg/LPyrene 57-126 4.9 20.0
5.28 10.526.013.050.0µg/LPyridine 10-80 84.4*20.0
25.7 51.452.826.450.0µg/L1,2,4-Trichlorobenzene 29-126 2.6 20.0
39.3 78.683.441.750.0µg/L2,4,5-Trichlorophenol 53-123 5.9 20.0
38.1 76.280.240.150.0µg/L2,4,6-Trichlorophenol 50-125 5.1 20.0
63.870.62-Fluorobiphenyl (S)44-119
40.340.32-Fluorophenol (S)19-119
66.473.6Nitrobenzene-d5 (S)44-120
74.878.84-Terphenyl-d14 (S)50-134
72.075.02,4,6-Tribromophenol (S)43-140
29.728.9Phenol-d5 (S)11-100
Page 32 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 140 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46647
Associated Lab Samples: 92181, 92183, 92185, 92187
LRB-V46647 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/24 18:000.6600.147<0.147mg/KgAcenaphthene
04/30/24 18:000.6600.150<0.150mg/KgAcenaphthylene
04/30/24 18:000.6600.210<0.210mg/KgAniline
04/30/24 18:000.6600.166<0.166mg/KgAnthracene
04/30/24 18:000.6600.156<0.156mg/KgBenzo(a)anthracene
04/30/24 18:000.6600.165<0.165mg/KgBenzo(a)pyrene
04/30/24 18:000.6600.147<0.147mg/KgBenzo(b)fluoranthene
04/30/24 18:000.6600.144<0.144mg/KgBenzo(g,h,i)perylene
04/30/24 18:000.6600.156<0.156mg/KgBenzo(k)fluoranthene
04/30/24 18:002.000.580<0.580mg/KgBenzoic Acid
04/30/24 18:000.6600.156<0.156mg/KgBenzyl alcohol
04/30/24 18:000.6600.138<0.138mg/KgBis(2-Chloroethoxy)methane
04/30/24 18:000.6600.122<0.122mg/KgBis(2-Chloroethyl)ether
04/30/24 18:000.3300.131<0.131mg/KgBis(2-Chloroisopropyl)ether
04/30/24 18:000.6600.177<0.177mg/KgBis(2-ethylhexyl)phthalate
04/30/24 18:000.6600.158<0.158mg/Kg4-Bromophenyl phenyl ether
04/30/24 18:000.3300.160<0.160mg/KgButyl benzyl phthalate
04/30/24 18:000.6600.149<0.149mg/Kg4-Chloro-3-methylphenol
04/30/24 18:000.3300.150<0.150mg/Kg4-Chloroaniline
04/30/24 18:000.6600.154<0.154mg/Kg2-Chloronaphthalene
04/30/24 18:000.6600.142<0.142mg/Kg2-Chlorophenol
04/30/24 18:001.000.147<0.147mg/Kg4-Chlorophenyl phenyl ether
04/30/24 18:000.6600.146<0.146mg/KgChrysene
04/30/24 18:000.6600.111<0.111mg/KgDibenz(a,h)anthracene
04/30/24 18:000.6600.158<0.158mg/KgDibenzofuran
04/30/24 18:000.6600.128<0.128mg/Kg1,2-Dichlorobenzene
04/30/24 18:000.6600.125<0.125mg/Kg1,3-Dichlorobenzene
Page 33 of 52Date:05/09/2024 02:05 PM
Page 141 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46647
Associated Lab Samples: 92181, 92183, 92185, 92187
LRB-V46647 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/24 18:000.3300.118<0.118mg/Kg1,4-Dichlorobenzene
04/30/24 18:000.6600.150<0.150mg/Kg3,3'-Dichlorobenzidine
04/30/24 18:000.6600.140<0.140mg/Kg2,4-Dichlorophenol
04/30/24 18:000.6600.147<0.147mg/KgDiethyl phthalate
04/30/24 18:000.6600.157<0.157mg/KgDimethyl phthalate
04/30/24 18:000.6600.212<0.212mg/Kg2,4-Dimethylphenol
04/30/24 18:000.6600.171<0.171mg/KgDi-n-butyl phthalate
04/30/24 18:001.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
04/30/24 18:001.500.520<0.520mg/Kg2,4-Dinitrophenol
04/30/24 18:000.6600.161<0.161mg/Kg2,4-Dinitrotoluene
04/30/24 18:000.6600.166<0.166mg/Kg2,6-Dinitrotoluene
04/30/24 18:000.3300.163<0.163mg/KgDi-n-Octyl Phthalate
04/30/24 18:000.6600.158<0.158mg/KgFluoranthene
04/30/24 18:000.6600.153<0.153mg/KgFluorene
04/30/24 18:000.6600.150<0.150mg/KgHexachlorobenzene
04/30/24 18:000.6600.097<0.097mg/KgHexachlorobutadiene
04/30/24 18:000.6600.100<0.100mg/KgHexachlorocyclopentadiene
04/30/24 18:000.6600.122<0.122mg/KgHexachloroethane
04/30/24 18:000.6600.151<0.151mg/KgIndeno(1,2,3-cd)pyrene
04/30/24 18:000.6600.121<0.121mg/KgIsophorone
04/30/24 18:000.6600.139<0.139mg/Kg1-Methylnaphthalene
04/30/24 18:000.6600.144<0.144mg/Kg2-Methylnaphthalene
04/30/24 18:000.6600.127<0.127mg/Kg2-Methylphenol
04/30/24 18:000.6600.128<0.128mg/Kg3&4 Methylphenol
04/30/24 18:000.6600.133<0.133mg/KgNaphthalene
04/30/24 18:000.6600.132<0.132mg/Kg2-Nitroaniline
04/30/24 18:000.6600.155<0.155mg/Kg3-Nitroaniline
Page 34 of 52Date:05/09/2024 02:05 PM
Page 142 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46647
Associated Lab Samples: 92181, 92183, 92185, 92187
LRB-V46647 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/30/24 18:000.3300.136<0.136mg/Kg4-Nitroaniline
04/30/24 18:000.3300.129<0.129mg/KgNitrobenzene
04/30/24 18:000.6600.133<0.133mg/Kg2-Nitrophenol
04/30/24 18:000.6600.167<0.167mg/Kg4-Nitrophenol
04/30/24 18:000.6600.263<0.263mg/KgN-Nitrosodimethylamine
04/30/24 18:000.6600.182<0.182mg/KgN-Nitrosodiphenylamine
04/30/24 18:000.6600.148<0.148mg/KgN-Nitroso-di-n-propylamine
04/30/24 18:001.000.347<0.347mg/KgPentachlorophenol
04/30/24 18:000.6600.158<0.158mg/KgPhenanthrene
04/30/24 18:000.6600.142<0.142mg/KgPhenol
04/30/24 18:000.6600.160<0.160mg/KgPyrene
04/30/24 18:000.3300.076<0.076mg/KgPyridine
04/30/24 18:000.6600.132<0.132mg/Kg1,2,4-Trichlorobenzene
04/30/24 18:000.6600.143<0.143mg/Kg2,4,5-Trichlorophenol
04/30/24 18:000.6600.140<0.140mg/Kg2,4,6-Trichlorophenol
04/30/24 18:002-Fluorobiphenyl (S)88.0 44-115
04/30/24 18:002-Fluorophenol (S)90.6 35-115
04/30/24 18:00Nitrobenzene-d5 (S)89.2 37-122
04/30/24 18:004-Terphenyl-d14 (S)88.6 54-127
04/30/24 18:002,4,6-Tribromophenol (S)70.2 39-132
04/30/24 18:00Phenol-d5 (S)95.1 34-121
LCS-V46647Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.61.481.67mg/KgAcenaphthene 40-123
93.41.561.67mg/KgAcenaphthylene 32-132
Page 35 of 52Date:05/09/2024 02:05 PM
Page 143 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46647
LCS-V46647Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1742.911.67mg/KgAniline 12-197
93.41.561.67mg/KgAnthracene 47-123
95.21.591.67mg/KgBenzo(a)anthracene 49-126
1101.841.67mg/KgBenzo(a)pyrene 45-129
1061.771.67mg/KgBenzo(b)fluoranthene 45-132
97.01.621.67mg/KgBenzo(g,h,i)perylene 43-134
84.41.411.67mg/KgBenzo(k)fluoranthene 47-132
84.4*1.411.67mg/KgBenzoic Acid 10-83
1021.711.67mg/KgBenzyl alcohol 29-122
86.21.441.67mg/KgBis(2-Chloroethoxy)methane 36-121
78.41.311.67mg/KgBis(2-Chloroethyl)ether 31-120
83.81.401.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1031.721.67mg/KgBis(2-ethylhexyl)phthalate 51-133
85.61.431.67mg/Kg4-Bromophenyl phenyl ether 46-124
1051.751.67mg/KgButyl benzyl phthalate 48-132
1041.731.67mg/Kg4-Chloro-3-methylphenol 45-122
91.01.521.67mg/Kg4-Chloroaniline 17-106
86.21.441.67mg/Kg2-Chloronaphthalene 41-114
94.61.581.67mg/Kg2-Chlorophenol 34-121
77.21.291.67mg/Kg4-Chlorophenyl phenyl ether 45-121
84.41.411.67mg/KgChrysene 50-124
59.20.9891.67mg/KgDibenz(a,h)anthracene 45-134
88.61.481.67mg/KgDibenzofuran 44-120
86.21.441.67mg/Kg1,2-Dichlorobenzene 33-117
82.61.381.67mg/Kg1,3-Dichlorobenzene 30-115
77.21.291.67mg/Kg1,4-Dichlorobenzene 31-115
69.41.161.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 36 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 144 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46647
LCS-V46647Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
97.61.631.67mg/Kg2,4-Dichlorophenol 40-122
92.81.551.67mg/KgDiethyl phthalate 50-124
93.41.561.67mg/KgDimethyl phthalate 48-124
1272.121.67mg/Kg2,4-Dimethylphenol 30-127
94.61.581.67mg/KgDi-n-butyl phthalate 51-128
94.01.571.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
98.21.641.67mg/Kg2,4-Dinitrophenol 27-129
94.01.571.67mg/Kg2,4-Dinitrotoluene 48-126
1131.881.67mg/Kg2,6-Dinitrotoluene 46-124
1131.891.67mg/KgDi-n-Octyl Phthalate 45-140
92.21.541.67mg/KgFluoranthene 50-127
91.01.521.67mg/KgFluorene 43-125
89.81.501.67mg/KgHexachlorobenzene 45-122
92.81.551.67mg/KgHexachlorobutadiene 32-123
78.41.311.67mg/KgHexachlorocyclopentadiene 32-117
79.61.331.67mg/KgHexachloroethane 28-117
95.81.601.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
76.01.271.67mg/KgIsophorone 30-122
89.81.501.67mg/Kg1-Methylnaphthalene 40-119
92.81.551.67mg/Kg2-Methylnaphthalene 38-122
94.01.571.67mg/Kg2-Methylphenol 32-122
84.41.411.67mg/Kg3&4 Methylphenol 34-119
86.81.451.67mg/KgNaphthalene 35-123
88.01.471.67mg/Kg2-Nitroaniline 44-127
84.41.411.67mg/Kg3-Nitroaniline 33-119
99.41.661.67mg/Kg4-Nitroaniline 63-147
86.21.441.67mg/KgNitrobenzene 34-122
Page 37 of 52Date:05/09/2024 02:05 PM
Page 145 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46647
LCS-V46647Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
82.01.371.67mg/Kg2-Nitrophenol 36-123
88.61.481.67mg/Kg4-Nitrophenol 30-132
73.61.231.67mg/KgN-Nitrosodimethylamine 10-146
1161.931.67mg/KgN-Nitrosodiphenylamine 38-127
89.81.501.67mg/KgN-Nitroso-di-n-propylamine 36-120
96.41.611.67mg/KgPentachlorophenol 25-133
91.61.531.67mg/KgPhenanthrene 50-121
94.01.571.67mg/KgPhenol 34-121
93.41.561.67mg/KgPyrene 47-127
59.60.9961.67mg/KgPyridine 10-80
86.81.451.67mg/Kg1,2,4-Trichlorobenzene 34-118
89.21.491.67mg/Kg2,4,5-Trichlorophenol 41-124
92.81.551.67mg/Kg2,4,6-Trichlorophenol 39-126
79.62-Fluorobiphenyl (S)44-115
87.02-Fluorophenol (S)35-115
85.6Nitrobenzene-d5 (S)37-122
82.04-Terphenyl-d14 (S)54-127
80.12,4,6-Tribromophenol (S)39-132
92.1Phenol-d5 (S)34-121
V 91973-MS-V46647 V 91973-MSD-V46647Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.45 86.81.291.671.67<0.147mg/KgAcenaphthene 77.2 40-123 11.6 20
1.54 92.21.401.671.67<0.150mg/KgAcenaphthylene 83.8 32-132 9.5 20
1.87 1121.831.671.67<0.210mg/KgAniline 110 12-197 2.1 20
Page 38 of 52Date:05/09/2024 02:05 PM
Page 146 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46647
V 91973-MS-V46647 V 91973-MSD-V46647Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.54 92.21.421.671.67<0.166mg/KgAnthracene 85.0 47-123 8.1 20
1.47 88.01.311.671.67<0.156mg/KgBenzo(a)anthracene 78.4 49-126 11.5 20
1.76 1051.511.671.67<0.165mg/KgBenzo(a)pyrene 90.4 45-129 15.2 20
1.58 94.61.451.671.67<0.147mg/KgBenzo(b)fluoranthene 86.8 45-132 8.5 20
1.55 92.81.421.671.67<0.144mg/KgBenzo(g,h,i)perylene 85.0 43-134 8.7 20
1.47 88.01.271.671.67<0.156mg/KgBenzo(k)fluoranthene 76.0 47-132 14.5 20
1.68 101*1.591.671.67<0.580mg/KgBenzoic Acid 95.2*10-83 5.5 20
1.49 89.21.501.671.67<0.156mg/KgBenzyl alcohol 89.8 29-122 0.6 20
1.37 82.01.251.671.67<0.138mg/KgBis(2-Chloroethoxy)methane 74.8 36-121 9.1 20
1.17 70.01.121.671.67<0.122mg/KgBis(2-Chloroethyl)ether 67.0 31-120 4.3 20
1.22 73.01.191.671.67<0.131mg/KgBis(2-Chloroisopropyl)ether 71.2 33-131 2.4 20
1.71 1021.591.671.67<0.177mg/KgBis(2-ethylhexyl)phthalate 95.2 51-133 7.2 20
1.39 83.21.271.671.67<0.158mg/Kg4-Bromophenyl phenyl ether 76.0 46-124 9.0 20
1.76 1051.571.671.67<0.160mg/KgButyl benzyl phthalate 94.0 48-132 11.4 20
1.59 95.21.481.671.67<0.149mg/Kg4-Chloro-3-methylphenol 88.6 45-122 7.1 20
1.46 87.41.351.671.67<0.150mg/Kg4-Chloroaniline 80.8 17-106 7.8 20
1.40 83.81.281.671.67<0.154mg/Kg2-Chloronaphthalene 76.6 41-114 8.9 20
1.40 83.81.431.671.67<0.142mg/Kg2-Chlorophenol 85.6 34-121 2.1 20
1.31 78.41.191.671.67<0.147mg/Kg4-Chlorophenyl phenyl ether 71.2 45-121 9.6 20
1.48 88.61.311.671.67<0.146mg/KgChrysene 78.4 50-124 12.1 20
1.11 66.41.011.671.67<0.111mg/KgDibenz(a,h)anthracene 60.4 45-134 9.4 20
1.46 87.41.311.671.67<0.158mg/KgDibenzofuran 78.4 44-120 10.8 20
1.26 75.41.251.671.67<0.128mg/Kg1,2-Dichlorobenzene 74.8 33-117 0.7 20
1.22 73.01.191.671.67<0.125mg/Kg1,3-Dichlorobenzene 71.2 30-115 2.4 20
1.14 68.21.111.671.67<0.118mg/Kg1,4-Dichlorobenzene 66.4 31-115 2.6 20
0.861 51.50.7281.671.67<0.150mg/Kg3,3'-Dichlorobenzidine 43.5 22-121 16.7 20
Page 39 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 147 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46647
V 91973-MS-V46647 V 91973-MSD-V46647Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.50 89.81.421.671.67<0.140mg/Kg2,4-Dichlorophenol 85.0 40-122 5.4 20
1.49 89.21.351.671.67<0.147mg/KgDiethyl phthalate 80.8 50-124 9.8 20
1.50 89.81.361.671.67<0.157mg/KgDimethyl phthalate 81.4 48-124 9.7 30
1.90 1141.701.671.67<0.212mg/Kg2,4-Dimethylphenol 102 30-127 11.1 20
1.55 92.81.431.671.67<0.171mg/KgDi-n-butyl phthalate 85.6 51-128 8.0 20
1.45 86.81.421.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 85.0 29-132 2.0 20
1.60 95.81.531.671.67<0.520mg/Kg2,4-Dinitrophenol 91.6 27-129 4.4 20
1.48 88.61.331.671.67<0.161mg/Kg2,4-Dinitrotoluene 79.6 48-126 10.6 20
1.77 1061.601.671.67<0.166mg/Kg2,6-Dinitrotoluene 95.8 46-124 10.0 20
1.81 1081.661.671.67<0.163mg/KgDi-n-Octyl Phthalate 99.4 45-140 8.6 20
1.50 89.81.411.671.67<0.158mg/KgFluoranthene 84.4 50-127 6.1 20
1.48 88.61.321.671.67<0.153mg/KgFluorene 79.0 43-125 11.4 20
1.38 82.61.331.671.67<0.150mg/KgHexachlorobenzene 79.6 45-122 3.6 20
1.45 86.81.401.671.67<0.097mg/KgHexachlorobutadiene 83.8 32-123 3.5 20
1.29 77.21.181.671.67<0.100mg/KgHexachlorocyclopentadiene 70.6 32-117 8.9 20
1.16 69.41.121.671.67<0.122mg/KgHexachloroethane 67.0 28-117 3.5 20
1.64 98.21.401.671.67<0.151mg/KgIndeno(1,2,3-cd)pyrene 83.8 45-133 15.7 20
1.16 69.41.101.671.67<0.121mg/KgIsophorone 65.8 30-122 5.3 20
1.41 84.41.311.671.67<0.139mg/Kg1-Methylnaphthalene 78.4 40-119 7.3 20
1.43 85.61.341.671.67<0.144mg/Kg2-Methylnaphthalene 80.2 38-122 6.4 20
1.36 81.41.341.671.67<0.127mg/Kg2-Methylphenol 80.2 32-122 1.4 20
1.23 73.61.231.671.67<0.128mg/Kg3&4 Methylphenol 73.6 34-119 0.0 20
1.35 80.81.301.671.67<0.133mg/KgNaphthalene 77.8 35-123 3.7 20
1.40 83.81.311.671.67<0.132mg/Kg2-Nitroaniline 78.4 44-127 6.6 20
1.44 86.21.361.671.67<0.155mg/Kg3-Nitroaniline 81.4 33-119 5.7 20
1.56 93.41.411.671.67<0.136mg/Kg4-Nitroaniline 84.4 63-147 10.1 20
Page 40 of 52Date:05/09/2024 02:05 PM
Page 148 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46677QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46647
V 91973-MS-V46647 V 91973-MSD-V46647Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.31 78.41.281.671.67<0.129mg/KgNitrobenzene 76.6 34-122 2.3 20
1.30 77.81.291.671.67<0.133mg/Kg2-Nitrophenol 77.2 32-123 0.7 20
1.48 88.61.311.671.67<0.167mg/Kg4-Nitrophenol 78.4 30-132 12.1 20
1.11 66.41.071.671.67<0.263mg/KgN-Nitrosodimethylamine 64.0 10-146 3.6 30
1.72 1031.591.671.67<0.182mg/KgN-Nitrosodiphenylamine 95.2 38-127 7.8 20
1.40 83.81.391.671.67<0.148mg/KgN-Nitroso-di-n-propylamine 83.2 36-120 0.7 20
1.58 94.61.471.671.67<0.347mg/KgPentachlorophenol 88.0 25-133 7.2 20
1.48 88.61.351.671.67<0.158mg/KgPhenanthrene 80.8 50-121 9.1 20
1.35 80.81.321.671.67<0.142mg/KgPhenol 79.0 34-121 2.2 20
1.47 88.01.331.671.67<0.160mg/KgPyrene 79.6 47-127 10.0 20
0.569 34.00.5961.671.67<0.076mg/KgPyridine 35.6 10-80 4.6 20
1.35 80.81.291.671.67<0.132mg/Kg1,2,4-Trichlorobenzene 77.2 34-118 4.5 20
1.52 91.01.371.671.67<0.143mg/Kg2,4,5-Trichlorophenol 82.0 41-124 10.3 20
1.46 87.41.321.671.67<0.140mg/Kg2,4,6-Trichlorophenol 79.0 39-126 10.0 20
79.62-Fluorobiphenyl (S)71.8 44-115
78.02-Fluorophenol (S)78.0 35-115
79.0Nitrobenzene-d5 (S)74.8 37-122
80.84-Terphenyl-d14 (S)71.2 54-127
74.72,4,6-Tribromophenol (S)68.7 39-132
81.0Phenol-d5 (S)79.8 34-121
Page 41 of 52Date:05/09/2024 02:05 PM
Page 149 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46903QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46854
Associated Lab Samples: 92194, 92196
LRB-V46854 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/07/24 16:130.6600.147<0.147mg/KgAcenaphthene
05/07/24 16:130.6600.150<0.150mg/KgAcenaphthylene
05/07/24 16:130.6600.210<0.210mg/KgAniline
05/07/24 16:130.6600.166<0.166mg/KgAnthracene
05/07/24 16:130.6600.156<0.156mg/KgBenzo(a)anthracene
05/07/24 16:130.6600.165<0.165mg/KgBenzo(a)pyrene
05/07/24 16:130.6600.147<0.147mg/KgBenzo(b)fluoranthene
05/07/24 16:130.6600.144<0.144mg/KgBenzo(g,h,i)perylene
05/07/24 16:130.6600.156<0.156mg/KgBenzo(k)fluoranthene
05/07/24 16:132.000.580<0.580mg/KgBenzoic Acid
05/07/24 16:130.6600.156<0.156mg/KgBenzyl alcohol
05/07/24 16:130.6600.138<0.138mg/KgBis(2-Chloroethoxy)methane
05/07/24 16:130.6600.122<0.122mg/KgBis(2-Chloroethyl)ether
05/07/24 16:130.3300.131<0.131mg/KgBis(2-Chloroisopropyl)ether
05/07/24 16:130.6600.177<0.177mg/KgBis(2-ethylhexyl)phthalate
05/07/24 16:130.6600.158<0.158mg/Kg4-Bromophenyl phenyl ether
05/07/24 16:130.3300.160<0.160mg/KgButyl benzyl phthalate
05/07/24 16:130.6600.149<0.149mg/Kg4-Chloro-3-methylphenol
05/07/24 16:130.3300.150<0.150mg/Kg4-Chloroaniline
05/07/24 16:130.6600.154<0.154mg/Kg2-Chloronaphthalene
05/07/24 16:130.6600.142<0.142mg/Kg2-Chlorophenol
05/07/24 16:131.000.147<0.147mg/Kg4-Chlorophenyl phenyl ether
05/07/24 16:130.6600.146<0.146mg/KgChrysene
05/07/24 16:130.6600.111<0.111mg/KgDibenz(a,h)anthracene
05/07/24 16:130.6600.158<0.158mg/KgDibenzofuran
05/07/24 16:130.6600.128<0.128mg/Kg1,2-Dichlorobenzene
05/07/24 16:130.6600.125<0.125mg/Kg1,3-Dichlorobenzene
Page 42 of 52Date:05/09/2024 02:05 PM
Page 150 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46903QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46854
Associated Lab Samples: 92194, 92196
LRB-V46854 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/07/24 16:130.3300.118<0.118mg/Kg1,4-Dichlorobenzene
05/07/24 16:130.6600.150<0.150mg/Kg3,3'-Dichlorobenzidine
05/07/24 16:130.6600.140<0.140mg/Kg2,4-Dichlorophenol
05/07/24 16:130.6600.147<0.147mg/KgDiethyl phthalate
05/07/24 16:130.6600.157<0.157mg/KgDimethyl phthalate
05/07/24 16:130.6600.212<0.212mg/Kg2,4-Dimethylphenol
05/07/24 16:130.6600.171<0.171mg/KgDi-n-butyl phthalate
05/07/24 16:131.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
05/07/24 16:131.500.520<0.520mg/Kg2,4-Dinitrophenol
05/07/24 16:130.6600.161<0.161mg/Kg2,4-Dinitrotoluene
05/07/24 16:130.6600.166<0.166mg/Kg2,6-Dinitrotoluene
05/07/24 16:130.3300.163<0.163mg/KgDi-n-Octyl Phthalate
05/07/24 16:130.6600.158<0.158mg/KgFluoranthene
05/07/24 16:130.6600.153<0.153mg/KgFluorene
05/07/24 16:130.6600.150<0.150mg/KgHexachlorobenzene
05/07/24 16:130.6600.097<0.097mg/KgHexachlorobutadiene
05/07/24 16:130.6600.100<0.100mg/KgHexachlorocyclopentadiene
05/07/24 16:130.6600.122<0.122mg/KgHexachloroethane
05/07/24 16:130.6600.151<0.151mg/KgIndeno(1,2,3-cd)pyrene
05/07/24 16:130.6600.121<0.121mg/KgIsophorone
05/07/24 16:130.6600.139<0.139mg/Kg1-Methylnaphthalene
05/07/24 16:130.6600.144<0.144mg/Kg2-Methylnaphthalene
05/07/24 16:130.6600.127<0.127mg/Kg2-Methylphenol
05/07/24 16:130.6600.128<0.128mg/Kg3&4 Methylphenol
05/07/24 16:130.6600.133<0.133mg/KgNaphthalene
05/07/24 16:130.6600.132<0.132mg/Kg2-Nitroaniline
05/07/24 16:130.6600.155<0.155mg/Kg3-Nitroaniline
Page 43 of 52Date:05/09/2024 02:05 PM
Page 151 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46903QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46854
Associated Lab Samples: 92194, 92196
LRB-V46854 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/07/24 16:130.3300.136<0.136mg/Kg4-Nitroaniline
05/07/24 16:130.3300.129<0.129mg/KgNitrobenzene
05/07/24 16:130.6600.133<0.133mg/Kg2-Nitrophenol
05/07/24 16:130.6600.167<0.167mg/Kg4-Nitrophenol
05/07/24 16:130.6600.263<0.263mg/KgN-Nitrosodimethylamine
05/07/24 16:130.6600.182<0.182mg/KgN-Nitrosodiphenylamine
05/07/24 16:130.6600.148<0.148mg/KgN-Nitroso-di-n-propylamine
05/07/24 16:131.000.347<0.347mg/KgPentachlorophenol
05/07/24 16:130.6600.158<0.158mg/KgPhenanthrene
05/07/24 16:130.6600.142<0.142mg/KgPhenol
05/07/24 16:130.6600.160<0.160mg/KgPyrene
05/07/24 16:130.3300.076<0.076mg/KgPyridine
05/07/24 16:130.6600.132<0.132mg/Kg1,2,4-Trichlorobenzene
05/07/24 16:130.6600.143<0.143mg/Kg2,4,5-Trichlorophenol
05/07/24 16:130.6600.140<0.140mg/Kg2,4,6-Trichlorophenol
05/07/24 16:132-Fluorobiphenyl (S)88.0 44-115
05/07/24 16:132-Fluorophenol (S)90.3 35-115
05/07/24 16:13Nitrobenzene-d5 (S)85.0 37-122
05/07/24 16:134-Terphenyl-d14 (S)89.2 54-127
05/07/24 16:132,4,6-Tribromophenol (S)82.8 39-132
05/07/24 16:13Phenol-d5 (S)94.8 34-121
LCS-V46854Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
91.01.521.67mg/KgAcenaphthene 40-123
98.81.651.67mg/KgAcenaphthylene 32-132
Page 44 of 52Date:05/09/2024 02:05 PM
Page 152 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46903QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46854
LCS-V46854Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1572.631.67mg/KgAniline 12-197
94.01.571.67mg/KgAnthracene 47-123
93.41.561.67mg/KgBenzo(a)anthracene 49-126
1262.111.67mg/KgBenzo(a)pyrene 45-129
1282.141.67mg/KgBenzo(b)fluoranthene 45-132
1131.881.67mg/KgBenzo(g,h,i)perylene 43-134
95.81.601.67mg/KgBenzo(k)fluoranthene 47-132
126*2.101.67mg/KgBenzoic Acid 10-83
1051.761.67mg/KgBenzyl alcohol 29-122
86.81.451.67mg/KgBis(2-Chloroethoxy)methane 36-121
74.81.251.67mg/KgBis(2-Chloroethyl)ether 31-120
80.21.341.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1041.741.67mg/KgBis(2-ethylhexyl)phthalate 51-133
90.41.511.67mg/Kg4-Bromophenyl phenyl ether 46-124
1031.721.67mg/KgButyl benzyl phthalate 48-132
1071.791.67mg/Kg4-Chloro-3-methylphenol 45-122
94.61.581.67mg/Kg4-Chloroaniline 17-106
88.61.481.67mg/Kg2-Chloronaphthalene 41-114
95.81.601.67mg/Kg2-Chlorophenol 34-121
86.81.451.67mg/Kg4-Chlorophenyl phenyl ether 45-121
77.21.291.67mg/KgChrysene 50-124
40.4*0.6751.67mg/KgDibenz(a,h)anthracene 45-134
95.21.591.67mg/KgDibenzofuran 44-120
86.21.441.67mg/Kg1,2-Dichlorobenzene 33-117
80.21.341.67mg/Kg1,3-Dichlorobenzene 30-115
74.21.241.67mg/Kg1,4-Dichlorobenzene 31-115
85.01.421.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 45 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 153 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46903QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46854
LCS-V46854Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1021.711.67mg/Kg2,4-Dichlorophenol 40-122
99.41.661.67mg/KgDiethyl phthalate 50-124
99.41.661.67mg/KgDimethyl phthalate 48-124
129*2.161.67mg/Kg2,4-Dimethylphenol 30-127
95.81.601.67mg/KgDi-n-butyl phthalate 51-128
1081.811.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
1292.151.67mg/Kg2,4-Dinitrophenol 27-129
1021.701.67mg/Kg2,4-Dinitrotoluene 48-126
1202.011.67mg/Kg2,6-Dinitrotoluene 46-124
1312.181.67mg/KgDi-n-Octyl Phthalate 45-140
97.01.621.67mg/KgFluoranthene 50-127
97.01.621.67mg/KgFluorene 43-125
91.01.521.67mg/KgHexachlorobenzene 45-122
96.41.611.67mg/KgHexachlorobutadiene 32-123
82.01.371.67mg/KgHexachlorocyclopentadiene 32-117
76.01.271.67mg/KgHexachloroethane 28-117
1292.161.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
76.01.271.67mg/KgIsophorone 30-122
90.41.511.67mg/Kg1-Methylnaphthalene 40-119
91.61.531.67mg/Kg2-Methylnaphthalene 38-122
97.01.621.67mg/Kg2-Methylphenol 32-122
88.61.481.67mg/Kg3&4 Methylphenol 34-119
85.61.431.67mg/KgNaphthalene 35-123
99.41.661.67mg/Kg2-Nitroaniline 44-127
1011.681.67mg/Kg3-Nitroaniline 33-119
1111.851.67mg/Kg4-Nitroaniline 63-147
87.41.461.67mg/KgNitrobenzene 34-122
Page 46 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 154 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46903QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46854
LCS-V46854Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.01.571.67mg/Kg2-Nitrophenol 36-123
98.21.641.67mg/Kg4-Nitrophenol 30-132
70.01.171.67mg/KgN-Nitrosodimethylamine 10-146
1131.881.67mg/KgN-Nitrosodiphenylamine 38-127
95.81.601.67mg/KgN-Nitroso-di-n-propylamine 36-120
1091.821.67mg/KgPentachlorophenol 25-133
93.41.561.67mg/KgPhenanthrene 50-121
93.41.561.67mg/KgPhenol 34-121
90.41.511.67mg/KgPyrene 47-127
52.40.8761.67mg/KgPyridine 10-80
86.81.451.67mg/Kg1,2,4-Trichlorobenzene 34-118
1061.771.67mg/Kg2,4,5-Trichlorophenol 41-124
1031.721.67mg/Kg2,4,6-Trichlorophenol 39-126
89.22-Fluorobiphenyl (S)44-115
91.82-Fluorophenol (S)35-115
87.4Nitrobenzene-d5 (S)37-122
86.24-Terphenyl-d14 (S)54-127
97.52,4,6-Tribromophenol (S)39-132
96.9Phenol-d5 (S)34-121
V 91797-MS-V46854 V 91797-MSD-V46854Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.35 80.81.321.671.67<0.588mg/KgAcenaphthene 79.0 40-123 2.2 20
1.43 85.61.511.671.67<0.600mg/KgAcenaphthylene 90.4 32-132 5.4 20
1.49 89.21.401.671.67<0.839mg/KgAniline 83.8 12-197 6.2 20
Page 47 of 52Date:05/09/2024 02:05 PM
Page 155 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46903QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46854
V 91797-MS-V46854 V 91797-MSD-V46854Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.39 83.21.431.671.67<0.664mg/KgAnthracene 85.6 47-123 2.8 20
1.46 87.41.531.671.67<0.624mg/KgBenzo(a)anthracene 91.6 49-126 4.6 20
1.76 1051.751.671.67<0.660mg/KgBenzo(a)pyrene 105 45-129 0.5 20
1.67 1001.871.671.67<0.588mg/KgBenzo(b)fluoranthene 112 45-132 11.2 20
1.54 92.21.471.671.67<0.576mg/KgBenzo(g,h,i)perylene 88.0 43-134 4.6 20
1.34 80.21.111.671.67<0.624mg/KgBenzo(k)fluoranthene 66.4 47-132 18.7 20
3.63 217*3.631.671.67<2.32mg/KgBenzoic Acid 217*10-83 0.0 20
1.31 78.41.391.671.67<0.624mg/KgBenzyl alcohol 83.2 29-122 5.9 20
1.19 71.21.191.671.67<0.552mg/KgBis(2-Chloroethoxy)methane 71.2 36-121 0.0 20
0.986 59.01.001.671.67<0.488mg/KgBis(2-Chloroethyl)ether 59.8 31-120 1.4 20
1.08 64.61.111.671.67<0.524mg/KgBis(2-Chloroisopropyl)ether 66.4 33-131 2.7 20
2.14 1282.151.671.67<0.708mg/KgBis(2-ethylhexyl)phthalate 129 51-133 0.4 20
1.31 78.41.661.671.67<0.632mg/Kg4-Bromophenyl phenyl ether 99.4 46-124 23.5*20
2.09 1252.311.671.67<0.640mg/KgButyl benzyl phthalate 138*48-132 10.0 20
1.51 90.41.581.671.67<0.596mg/Kg4-Chloro-3-methylphenol 94.6 45-122 4.5 20
1.05 62.81.101.671.67<0.600mg/Kg4-Chloroaniline 65.8 17-106 4.6 20
1.29 77.21.311.671.67<0.616mg/Kg2-Chloronaphthalene 78.4 41-114 1.5 20
1.23 73.61.291.671.67<0.568mg/Kg2-Chlorophenol 77.2 34-121 4.7 20
1.28 76.61.311.671.67<0.588mg/Kg4-Chlorophenyl phenyl ether 78.4 45-121 2.3 20
1.61 96.40.9581.671.67<0.584mg/KgChrysene 57.3 50-124 50.7*20
2.13 1281.291.671.67<0.444mg/KgDibenz(a,h)anthracene 77.2 45-134 49.1*20
1.34 80.21.381.671.67<0.632mg/KgDibenzofuran 82.6 44-120 2.9 20
1.14 68.21.161.671.67<0.512mg/Kg1,2-Dichlorobenzene 69.4 33-117 1.7 20
1.13 67.61.141.671.67<0.500mg/Kg1,3-Dichlorobenzene 68.2 30-115 0.8 20
1.10 65.81.111.671.67<0.472mg/Kg1,4-Dichlorobenzene 66.4 31-115 0.9 20
1.24 74.21.181.671.67<0.600mg/Kg3,3'-Dichlorobenzidine 70.6 22-121 4.9 20
Page 48 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 156 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46903QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46854
V 91797-MS-V46854 V 91797-MSD-V46854Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.37 82.01.501.671.67<0.560mg/Kg2,4-Dichlorophenol 89.8 40-122 9.0 20
1.38 82.61.461.671.67<0.588mg/KgDiethyl phthalate 87.4 50-124 5.6 20
1.41 84.41.411.671.67<0.628mg/KgDimethyl phthalate 84.4 48-124 0.0 30
1.81 1081.911.671.67<0.848mg/Kg2,4-Dimethylphenol 114 30-127 5.3 20
1.77 1061.841.671.67<0.684mg/KgDi-n-butyl phthalate 110 51-128 3.8 20
2.98 178*3.041.671.67<0.960mg/Kg4,6-Dinitro-2-methylphenol 182*29-132 1.9 20
3.78 226*3.911.671.67<2.08mg/Kg2,4-Dinitrophenol 234*27-129 3.3 20
1.82 1091.741.671.67<0.644mg/Kg2,4-Dinitrotoluene 104 48-126 4.4 20
1.81 1081.981.671.67<0.664mg/Kg2,6-Dinitrotoluene 119 46-124 8.9 20
2.56 153*2.601.671.67<0.652mg/KgDi-n-Octyl Phthalate 156*45-140 1.5 20
1.47 88.01.511.671.67<0.632mg/KgFluoranthene 90.4 50-127 2.6 20
1.34 80.21.381.671.67<0.612mg/KgFluorene 82.6 43-125 2.9 20
1.36 81.41.371.671.67<0.600mg/KgHexachlorobenzene 82.0 45-122 0.7 20
1.45 86.81.411.671.67<0.390mg/KgHexachlorobutadiene 84.4 32-123 2.7 20
1.24 74.21.271.671.67<0.400mg/KgHexachlorocyclopentadiene 76.0 32-117 2.3 20
1.06 63.41.151.671.67<0.488mg/KgHexachloroethane 68.8 28-117 8.1 20
1.93 1161.891.671.67<0.604mg/KgIndeno(1,2,3-cd)pyrene 113 45-133 2.0 20
0.960 57.41.031.671.67<0.484mg/KgIsophorone 61.6 30-122 7.0 20
1.29 77.21.381.671.67<0.556mg/Kg1-Methylnaphthalene 82.6 40-119 6.7 20
1.38 82.61.351.671.67<0.576mg/Kg2-Methylnaphthalene 80.8 38-122 2.1 20
1.29 77.21.271.671.67<0.508mg/Kg2-Methylphenol 76.0 32-122 1.5 20
1.18 70.61.181.671.67<0.510mg/Kg3&4 Methylphenol 70.6 34-119 0.0 20
1.24 74.21.241.671.67<0.532mg/KgNaphthalene 74.2 35-123 0.0 20
1.71 1021.781.671.67<0.528mg/Kg2-Nitroaniline 107 44-127 4.0 20
1.41 84.41.441.671.67<0.620mg/Kg3-Nitroaniline 86.2 33-119 2.1 20
1.46 87.41.371.671.67<0.544mg/Kg4-Nitroaniline 82.0 63-147 6.3 20
Page 49 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 157 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V46903QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V46854
V 91797-MS-V46854 V 91797-MSD-V46854Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.13 67.61.181.671.67<0.516mg/KgNitrobenzene 70.6 34-122 4.3 20
1.87 1121.921.671.67<0.532mg/Kg2-Nitrophenol 115 32-123 2.6 20
1.98 1191.991.671.67<0.668mg/Kg4-Nitrophenol 119 30-132 0.5 20
<1.05 0.0*<1.051.671.67<1.05mg/KgN-Nitrosodimethylamine 0.0*10-146 0.0 30
1.62 97.01.671.671.67<0.728mg/KgN-Nitrosodiphenylamine 100 38-127 3.0 20
1.24 74.21.251.671.67<0.592mg/KgN-Nitroso-di-n-propylamine 74.8 36-120 0.8 20
2.29 137*2.261.671.67<1.39mg/KgPentachlorophenol 135*25-133 1.3 20
1.35 80.81.361.671.67<0.632mg/KgPhenanthrene 81.4 50-121 0.7 20
1.16 69.41.181.671.67<0.568mg/KgPhenol 70.6 34-121 1.7 20
1.30 77.81.341.671.67<0.640mg/KgPyrene 80.2 47-127 3.0 20
<0.307 0.0*<0.3071.671.67<0.307mg/KgPyridine 0.0*10-80 0.0 20
1.23 73.61.271.671.67<0.528mg/Kg1,2,4-Trichlorobenzene 76.0 34-118 3.2 20
1.34 80.21.541.671.67<0.572mg/Kg2,4,5-Trichlorophenol 92.2 41-124 13.8 20
1.44 86.21.391.671.67<0.560mg/Kg2,4,6-Trichlorophenol 83.2 39-126 3.5 20
73.62-Fluorobiphenyl (S)75.4 44-115
73.22-Fluorophenol (S)70.5 35-115
70.0Nitrobenzene-d5 (S)72.4 37-122
72.44-Terphenyl-d14 (S)73.6 54-127
93.02,4,6-Tribromophenol (S)94.8 39-132
76.5Phenol-d5 (S)74.1 34-121
Page 50 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 158 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L748932QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L748029
Associated Lab Samples: 92181, 92183, 92185, 92187, 92194, 92196
LRB-L748029 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/02/24 17:260.2000.1410.158mg/KgChromium, Hexavalent
LCS-L748029Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.03.724.00mg/KgChromium, Hexavalent 80-120
V 92181-DUP-L748029Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20 05/02/24 18:2025.3*0.2930.227mg/KgChromium, Hexavalent
V 92181-MS-L748029Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
33.8 85.039.7<1.40mg/KgChromium, Hexavalent 75-125
Page 51 of 52* QC Fail Date:05/09/2024 02:05 PM
Page 159 of 163
Quality Control Data
24-120-0005Report No:
Project Description:
Client ID:Mid-Atlantic Associates, Inc. - Charlotte
Metropolitan
Dry Weight Determination
SW-DRYWT
V46679QC Analytical Batch:
Analysis Method:
Analysis Description:
V 92109-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/01/24 10:050.021.821.8%Moisture
V 92110-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/01/24 10:050.921.521.3%Moisture
Page 52 of 52Date:05/09/2024 02:05 PM
Page 160 of 163
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:24-120-0005
Mid-Atlantic Associates, Inc. - Charlotte
01138
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:04/29/2024 10:31:36
Special precautions or instructions included?
Comments:
Page 161 of 163
Page 162 of 163
Page 163 of 163

APPENDIX D
NCDEQ Risk Calculator (February 2024)

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
5/5/2024
Prepared By:Shane Sisco, P.G.
Mid-Atlantic Associates, Inc.
Greg Icenhour, P.G.
Soil Vapor (Highest Concentrations)
North Carolina Department of Environmental Quality
Risk Calculator
Midtown Square Mall
1200 Metropolitan Avenue, Charlotte, North Carolina
Brownfields
09058-05-060
February 2024
November 2023 EPA RSL Table
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: February 2024
Basis: November 2023 EPA RSL Table
Site ID: 09058-05-060
Exposure Unit ID: Soil Vapor (Highest Concentrations)
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: February 2024
Basis: November 2023 EPA RSL Table
Site ID: 09058-05-060
Exposure Unit ID: Soil Vapor (Highest Concentrations)
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: February 2024Basis: November 2023 EPA RSL Table
Site ID: 09058-05-060
Exposure Unit ID: Soil Vapor (Highest Concentrations)
Description of Exposure Point Concentration Selection:
Exposure Point Concentration
(ug/m3)Notes:CAS Number Chemical Minimum Concentration (Qualifier)
Maximum Concentration (Qualifier)
Units Location of Maximum Concentration
Detection Frequency
Range of Detection Limits
Concentration Used for Screening
Background Value
Screening Toxicity Value (Screening Level) (n/c)
Potential ARAR/TBC Value
Potential ARAR/TBC Source
COPC Flag (Y/N)
Rationale for Selection or Deletion
150 67-64-1 Acetone ug/m3
8.9 71-43-2 Benzene ug/m3
1.2 75-27-4 Bromodichloromethane ug/m3
35 75-15-0 Carbon Disulfide ug/m3
0.81 56-23-5 Carbon Tetrachloride ug/m3
19 67-66-3 Chloroform ug/m3
0.59 74-87-3 Chloromethane ug/m3
28 110-83-8 Cyclohexene ug/m3
1.3 75-71-8 Dichlorodifluoromethane ug/m3
3.3 141-78-6 Ethyl Acetate ug/m3
4.5 100-41-4 Ethylbenzene ug/m3
6.6 142-82-5 Heptane, N-ug/m3
21 110-54-3 Hexane, N-ug/m3
12 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3
4.2 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m3
1.1 1634-04-4 Methyl tert-Butyl Ether (MTBE)ug/m3
2.6 75-09-2 Methylene Chloride ug/m3
77 115-07-1 Propylene ug/m3
0.66 100-42-5 Styrene ug/m3
120 127-18-4 Tetrachloroethylene ug/m3
54 108-88-3 Toluene ug/m3
1.2 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m3
1.1 79-01-6 Trichloroethylene ug/m3
6 75-69-4 Trichlorofluoromethane ug/m3
4.4 95-63-6 Trimethylbenzene, 1,2,4-ug/m3
0.81 108-67-8 Trimethylbenzene, 1,3,5-ug/m3
17.4 1330-20-7 Xylenes ug/m3
Input Form 2D
Soil Gas Exposure Point Concentration Table
Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: February 2024
Basis: November 2023 EPA RSL Table
Site ID: 09058-05-060
Exposure Unit ID: Soil Vapor (Highest Concentrations)
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 6.5E-06 1.3E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 4.9E-07 1.0E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator

APPENDIX E
Slug Test Results